FA-3764_29702_CA_RMR_20231120_FTBR308 CAP RMR

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________________________________________________
FINAL
CORRECTIVE ACTION PLAN
MONITORING REPORT

FTBR-308 (SITE 308)
MAY 2023 SAMPLING EVENT
FORT LIBERTY/FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA

October 2023

Prepared By:

U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
100 West Oglethorpe Avenue
Savannah, Georgia 31401
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ACRONYMS AND ABBREVIATIONS AFB Airforce Base AFVR Advanced Fluid and Vapor Recovery bgs below ground surface CAP Corrective Action Plan DPU Department of Public Utilities DPW Directorate of Public Works EPH Extractable Hydrocarbons GCL Gross Contamination Levels GWQS Groundwater Quality Standard JP-4 Jet Fuel-4 LNAPL Light non-aqueous Phase Liquid MADEP Massachusetts Department of Environmental Protection µg/L micrograms per liter NC2L North Carolina Subchapter 2L groundwater standards NCDEQ North Carolina Department of Environmental Quality NPDES National Pollutant Discharge Elimination System NTU Nephelometric Turbidity Unit OWS Oil Water Separator PAAF Pope Army Airfield PWC Public Works Commission RPD Relative Percent Difference SER System Enhancement Report SVE Soil Vapor Extration SVOC Semi-volatile Petroleum Hydrocarbons SU Standard Unit UST Underground Storage Tank VOCs Volatile Organic Compounds VPH Volatile Petroleum Hydrocarbon USACE United States Army Corps of Engineers WS-III Water Supply III
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A. SITE INFORMATION
1. Site Identification Site Name: Site SS007 (FTBR-308, Blue Ramp Hydrant) Facility I.D.: 29702 UST Incident Number: Unknown Risk Classification: Intermediate Land Use Category: Industrial Date of Report: October 2023
Site Location: Blue Ramp, Pope Army Airfield Fort Liberty, Cumberland County, North Carolina (NC) 28310 Nearest City: Fayetteville NC
Description of Geographical Data Point: N 35°10’25”, W 79°01’10”
Location Method: Location information obtained from Black & Veatch (2005)
2. UST System Contacts UST Owner/Operator: Fort Liberty Directorate of Public Works Address: AMIM-LIP-EM, Bldg 3-1137, Fort Liberty, NC 28310 Phone: [phone]
Property Owner/Occupant: Fort Liberty Directorate of Public Works Address: AMIM-LIP-EM, Bldg 3-1137, Fort Liberty, NC 28310 Phone: [phone]
3. Information about Release Date Discovered: 1980s Estimated Quantity of Release: Unknown; Estimated 50,000-60,000 gallons. Cause of Release: Unknown
Source of Release: Blue Ramp hydrant piping system Sizes, contents, and location of UST system(s) from which the release occurred: Tank: Eighteen (18) non-regulated USTs and hydrant system Capacity: UST: 50,000 gallons each
Hydrant System: 110,500 gallons Contents: Jet Fuel-4 (JP-4) Location: N 35º 10’25” W 79º 01’10”
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B. Executive Summary
Fort Liberty Site FTBR-308 (Site) is at the location of the Blue Ramp on Pope Army Airfield (Figure 1). In 1956, the Blue Ramp hydrant system consisted of two pump houses and six underground fuel hydrant lines for aircraft refueling. In 1966, this
was expanded to a hydrant system consisting of three pump houses, each including six underground storage tanks (USTs), and nine hydrant lines. Each pump house conveyed jet fuel to the Blue Ramp hydrant system from the six 50,000-gallon USTs, located immediately adjacent to the pump houses. In total, there were 18 non-regulated USTs which had a storage capacity of 900,000
gallons. This accounted for a total of 900,000 gallons of jet fuel stored within 18 non- regulated USTs. The volume of the hydrant pipeline system was approximately 110,500 gallons. According to historical documents, the Blue Ramp fueling system was discontinued in the 1990s.
During the spring 2023 gauging and groundwater sampling event, the maximum
thickness of free product was 2.12-feet at monitoring well PT-2. Free product was found under the airfield and in areas extending towards the unnamed tributary to Little River. The current extent is comparable to the historical extent.
The sampling results from the spring 2023 event show that the highest concentrations were detected in MW7-20 with the following above applicable
NC2L: benzene at 1,300 micrograms per liter (µg/L), toluene (1,400 µg/L), Xylenes (1,500 µg/L), 2-Methylnaphthalene (43 µg/L), naphthalene (110 µg/L), C5-C8 aliphatics (5,500 µg/L), C9-C18 aliphatics (4,840 µg/L), and C9-C22 aromatics (1,470 µg/L). No gross contaminant levels (GCLs) were exceeded.
Previously, multiple remedial technologies have been utilized and will be discussed
in greater detail later in this report. The most recent technology employed was Advanced Fluid Vapor Recovery (AFVR). This was utilized until 2019 when, due to a lack of recovery, a change was made to hydrophobic socks. The socks have been employed at the site skimming product that enters the monitoring or recovery well where they are deployed.
The receptors in the area include those in the office buildings over the dissolved plume and the unnamed tributary which historically has had product entering the stream. Due to the extensive vegetative growth in this area, it is no longer possible to safely observe this tributary. Past responses to free product in this area involved a cut-off trench and later multiple biosparge wells in an attempt to keep fuel out of
the tributary. Free-product has not been observed in the wells adjacent to the stream until this most recent sampling event. This was discussed at the Tier I in August 2023 to determine a path forward at the Site and is discussed in detail in the conclusions and recommendations section.

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C. TABLE OF CONTENTS
A. SITE INFORMATION ................................................................................. II
B. EXECUTIVE SUMMARY........................................................................... III
C. TABLE OF CONTENTS ............................................................................IV
D. SITE HISTORY AND CHARACTERIZATION................................................... 1
1.0 INTRODUCTION ........................................................................................ 1
2.0 Site History and Characterization ............................................................... 1 2.1 Land Use ......................................................................................... 2 2.2 Property Owners and Occupants .................................................... 2 2.3 Receptor Information ....................................................................... 2 2.4 Deep Aquifers in the Coastal Plain Physiographic Region ............................................................................................. 3 2.5 Site Geology and Hydrogeology ...................................................... 4 2.6 Previous Remedial Efforts ............................................................... 4
3.0 FIELD ACTIVITIES AND SAMPLING METHODOLOGY ........................... 6
3.1 Water Level and Free Product Gauging .......................................... 7 3.2 Low-flow Sample Collection ............................................................ 7 4.0 GROUNDWATER ANALYTICAL RESULTS SUMMARY ........................... 8 4.1 Historical Analytical Data ................................................................. 8 4.2 2023 Groundwater Results......................................................................... 8 4.3 Free Product Recovery .............................................................................. 9 5.0 CONCLUSIONS AND RECOMMENDATIONS .......................................... 9 6.0 REFERENCES ......................................................................................... 10 E. Statements and Certification .......................................................................... 10 LIST OF FIGURES
Figure 1 Site Vicinity Map Figure 2 Site Map with Former Hydrant System, Pumps Houses, and USTs
Figure 3 Well Network Map Figure 4 Potential Receptor Map Figure 5 Potentiometric Map Figure 6 Estimated Free Product Map Figure 7 Groundwater Concentration Map
Figure 8 Cross-Section A-A’
LIST OF TABLES
Table 1 UST System Information Table 2 UST Owner/Operator Information Table 3 Property Owners and Occupants
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Table 4 Monitoring and Remediation Well Construction Information Table 5 AFVR Free Product Recovery Information Table 6 Cumulative Volume of Free Product Recovered from the Site
Table 7 Current and Historical Groundwater Elevations and Free Product
Thickness Table 8 Analytical Summary Table 9 Historical Data Table 10 Relative Percent Difference

LIST OF APPENDICES
Appendix A Field Forms and Notes Appendix B Laboratory Data Sheets
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Certification
This report was prepared by the Savannah District of the U.S. Army Corps of Engineers. The initials or signatures and registration designation of individuals appear on these documents within the scope of their employment as required by the Engineer Regulation 1110-1-8152.

Prepared by:
Kevin Moon, P.G. Kansas Registration No. 912

Reviewed by: Jason Lennane, P.G.
Georgia Registration No. 1891
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D. SITE HISTORY AND CHARACTERIZATION
1.0 Introduction
This Corrective Action Plan (CAP) monitoring report presents the results of the April-May 2023 groundwater monitoring event conducted by United States Army Corps of Engineers (USACE), Savannah District at compliance cleanup site SS07 (FTBR-308, Blue Ramp
Hydrant System) on Pope Army Airfield (PAAF). FTBR-308 is hereafter referred to as Site
308 in this report. AFVR was selected as the preferred remedial technology in the System Enhancement Report (URS, 2009) which amended the cleanup strategy in the Corrective Action Plan (CAP) for this site (Black & Veatch, 2005). In 2019, AFVR events were changed to absorbent socks as either a sheen or no product was observed in the vacuum
truck after previous AFVR events. Currently, the absorbent socks are replaced on a semi-
annual schedule when conducting groundwater sampling and gauging at the site.
2.0 Site History and Characterization
The U.S. Army Reservation at Fort Liberty was established in 1918 as a major logistic, training, and mobilization deployment center for the XVIII Airborne Corps, which is part of the U.S. Army’s mobile infantry, assault, and armored forces. Fort Liberty occupies
approximately 161,024 acres in southeast North Carolina. Approximately 143,140 acres are designated for field maneuvers and military exercises. The cantonment area, which is in the eastern part of Fort Liberty, occupies 11,354 acres and includes approximately 6,195 buildings. Most military maintenance and production facilities, supply facilities, operation and training facilities, community installations, and family and troop housing are
located within the cantonment area.
The Blue Ramp hydrant system was originally constructed in 1956 and consisted of two pump houses and six USTs for aircraft refueling. This system was expanded in 1966 to three pump houses, 12 new USTs (6 for each pump house), and nine hydrant lines. Each pump house was connected to six 50,000-gallon USTs and conveyed fuel to the Blue Ramp via the hydrant system. The total storage of the 18 unregulated USTs was 900,000 gallons (Figure 1 and 2). A further 110,500 gallons was in the hydrant pipeline system. The Blue Ramp hydrant system was decommissioned in the 1990’s. Table 1 and 2 provide information for the UST and the hydrant system. Little information is known or available about the USTs that were in place at the Site.
A major spill occurred in the 1960s, in an area currently known as the Claw Ramp. Several thousand gallons of JP-4 was released during a fuel transfer. The JP-4 reportedly traversed through the storm sewer system and was contained at drainage gates. An unknown amount of JP-4 was recovered, while a further unknown amount infiltrated the ground.
In the mid-1980s, Pope Air Force Base personnel found JP-4 discharging into an unnamed tributary to the Little River. The unnamed tributary is adjacent to Building 740.
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Figure 4 depicts a potential receptor map which shows the proximity of the site, unnamed tributary, and Little River.
The historic JP-4 product plume observed at the site indicates the source of the release could include one or more of the USTs, associated piping, the hydrant system, or hydrant vaults located in the area of the Claw and Blue Ramps. All infrastructure is located upgradient of the JP-4 plume as shown in the cross-section provided in the CAP (Black & Veatch, 2005) and is provided as Figure 2 and 7.
2.1 Land Use
After removal of the USTs, land use at the Site remained as an airfield. Typical of an airfield, there are hangars and an office in the area of the Site. The site has little topographic relief in the area where the USTs were located as they were under the
airfield. The main topographic feature is immediately downgradient of the site where
an unnamed tributary is located and has formed a steep ravine. No land use changes are expected for this area.
2.2 Property Owners and Occupants
The owner of Site 308 and all surrounding property is the U.S. Army which is provided in Table 3. The Site Map is provided in Figure 2 and 3 which includes the former UST locations, buildings in the area and utilities.
2.3 Receptor Information
There are 25 water supply wells on Fort Liberty. Eight of these wells are located near the cantonment area and are used for golf course irrigation. The remaining wells are
outside the cantonment area and are used for purposes other than potable water supply. There are no known water supply wells within 1,500 feet of Site (Figure 4).
In 2010, the Fayetteville Public Works Commission (PWC) and Harnett County Department of Public Utilities (DPU) began providing all of Fort Liberty’s water. Harnett County DPU obtains their water from the Cape Fear River. The Fayetteville PWC also
obtains their water from the Cape Fear River, as well as Glenville Lake, and Big Cross Creek (all sources are part of the Cape Fear River basin). Prior to 2010, water was obtained from the Little River via an intake downstream of Site 308. This water intake and Little River are beyond the 1,500-foot perimeter around the site.
No surface water features are within 500-feet of the center of the site. The unnamed
tributary is approximately 750 feet from the Site. The unnamed stream flows to the northwest to an area of wetland before entering the Little River. Little River is classified by NCDEQ as Water Supply III (WS-III) stream due to the presence of water intakes along the stream. No wellhead protection areas are within 1,500-feet of Site 308 and no water wells are known to exist within 1,500-feet of the site.
Vapor intrusion for local buildings is not a concern as the depth to free product and groundwater is outside the screening zone for petroleum compounds (>15 feet) (ITRC,
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2014). Depth to water in the area of the building is approximately 21-feet below ground surface (bgs), therefore the building is outside the screening zone for petroleum compounds.
2.4 Deep Aquifers in the Coastal Plain Physiographic Region
The Fort Liberty area is underlain by three freshwater aquifers: the Middendorf Aquifer (also known locally as the Black Creek Aquifer), the Cape Fear Aquifer, and the saprolite-basement aquifer.
The major water-bearing strata at Fort Liberty are within the Middendorf Formation and are referred to as the Middendorf Aquifer. The Middendorf Aquifer consists of
coarse to fine-grained silty or clayey sands with interbedded light gray or tan clays. When combined with the surficial aquifer, the Middendorf Aquifer is locally known as the Black Creek Aquifer.
Unconfined conditions are typical near the top of the saturated zone of the Middendorf Aquifer, but semi-confined and confined conditions can occur at greater depths. In
upland areas of Fort Liberty, the potentiometric surface of the Middendorf Aquifer is as deep as 80 feet bgs. Near perennial streams in the eastern part of the reservation, the potentiometric surface is near the ground surface. The interbedded and discontinuous clay layers in this aquifer support localized, unconfined, perched water zones within 20 feet of the ground surface and are referred to as the surficial aquifer.
Many of the perched water zones dry out seasonally and are not a reliable water supply source. Sandy surface soils at Fort Liberty are highly permeable and allow precipitation to rapidly infiltrate and enter the groundwater system. The surficial groundwater system is recharged almost entirely by percolation of area precipitation through these sands.
The Cape Fear Aquifer is within the Cape Fear Formation, which is composed primarily of clay interbedded with silt and silty sand under confined conditions. In the vicinity of Fort Liberty, the uppermost 5 to 10 feet of the Cape Fear Formation form a confining unit that restricts vertical movement of water between the overlying Black Creek Aquifer sediments and the silt sand units of the Cape Fear Formation. The Cape
Fear Aquifer, therefore, receives little or no recharge from the overlying Black Creek Aquifer. None of the wells in the cantonment area are screened in the Cape Fear Aquifer; however, some of the more distal wells at Fort Liberty may be screened in this aquifer. The Cape Fear Aquifer is used for potable and industrial water supplies by the community of Spring Lake.
The saprolite-basement aquifer underlies the Cape Fear Formation at depths ranging from 140 to 300 feet bgs. This aquifer is generally assumed to yield little water, and no supply wells in the area are known to tap solely into this aquifer.
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2.5 Site Geology and Hydrogeology
The soils at Site 308 generally consist of alternating sequences of silt, silty to clayey sand, and discontinuous clay lenses. Sand grain sizes range from very fine to very coarse with isolate gravel. Geologic cross-section maps are presented on Figure 8.
Figure 8 represents an approximate north-south geologic section. Soils consists of silt to silty sand from the ground surface to a depth ranging from 12 to 20 feet bgs with interspersed thin clay lenses. The silty unit overlies a laterally continuous and homogenous sandy unit ranging in thickness from 10 feet in the eastern portion of the site to 30 feet in the western portion of the site. A discontinuous clay unit underlies the
sandy unit on the east transitioning to sand and silty sand in the west.
During past investigative activities, five exploratory soil borings were advanced to bedrock at PAAF. The Middendorf Formation and Cape Fear Formations were identified. The Middendorf Formation was encountered at depths ranging from 25-30 feet bgs and the Cape Fear Formation was encountered at depths ranging from 58-
80 feet bgs. A saprolitic zone of gray green to red silts and silty clay was observed beneath the Cape Fear Formation. Quartz veins were observed in the saprolite at some boring locations. At four boring locations, micaceous chlorite schist (bedrock) was observed.
Isolated areas of fill are present in the western portions of the site consisting of clay,
clayey sand, and asphalt. It was estimated that the fill thickness is approximately 20 feet in the vicinity of Building 740. While installing MW7-20, asphalt was encountered at a depth of 10-feet bgs.
During the current monitoring event, depth to groundwater at the site ranged from approximately 11 to 21 feet bgs. A potentiometric surface map based on May 2023
data is included as Figure 5. Groundwater was flowing to the south-southeast during the most recent sampling event.
Based on rising-head permeability tests performed at 15 monitoring wells at the site, the hydraulic conductivity of the surficial aquifer ranged from 0.5 to 82.3 feet/day with an average of 29 feet/day. A step-drawdown test was also completed at MW7-15
which yielded a transmissivity of 0.32 feet2/minute. To determine the hydraulic conductivity from the step drawdown test, an assumed aquifer thickness of 22-feet was used and yielded a hydraulic conductivity of 26 feet/day. The groundwater velocity calculated at the site is 1.16 feet/day or 423 feet/year.
2.6 Previous Remedial Efforts
In the mid-1980’s, fuel was found discharging into an unnamed tributary. To attempt
to prevent further discharges of fuel to the stream, a cut-off trench and sump was installed adjacent to the stream. The system was reconfigured in 1992 to rebuild and extend the north-south leg beyond storm drain utilizing a seal around the 30-inch diameter pipe. The existing 24-inch sump was removed and replaced with a 48-inch
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sump. This trench operated until 2000 when it was concluded it was no longer operationally effective as a barrier to the stream due to the geotextile installed during trench construction becoming fouled.
In 1996, a bioslurping pilot test was conducted near the cut-off trench. This system
was moved to be adjacent to Building 736 in 1997 to better assess the feasibility of the system. Full operation was not achieved until 1999 due to electrical and pump issues. Once operational, the system was plagued with operational issues but was able to remove 67,500 gallons of water and 3,500 gallons of free product; removal
through the vapor phase was not quantified.
Biovent wells were installed in 1999 adjacent to Building 736 where the bioslurping wells were also installed. The biovents appeared to reduce the vadose zone hydrocarbon concentrations but the effectiveness was limited due to free product floating on the water table.
An AFVR pilot test was completed in December 1999. During the test, 1,880 gallons
of total fluids were recovered including 628 gallons of measurable light non-aqueous phase liquid (LNAPL).
The CAP was approved in 2005 by the North Carolina Department of Environmental Quality (NCDEQ). In the fall of 2006, a multi-phase total fluids recovery and treatment system to remove contaminated soil vapors, contaminated groundwater, and LNAPL was installed at the site. The multi-phase recovery system consisted of 14 six-inch diameter recovery wells located throughout the LNAPL plume and a soil vapor extraction (SVE) blower system.
In September of 2009, URS submitted a System Enhancement Report (SER) recommending that the system be amended to improve LNAPL recovery efficiency (URS, 2009). The methodology for LNAPL and vapor recovery was modified from the multi-phase total fluids recovery system to performing periodic and frequent AFVR events at the site and then treating the recovered fluids through the existing groundwater treatment system. Following the recommendations of the SER, the recovery system was partially dismantled to allow for the conversion of the multi-phase recovery wells to AFVR recovery wells, and an additional 15 two-inch diameter recovery wells were installed. Conversion of the multi-phase wells was performed by removing the total fluids recovery pumps from the wells and removing the SVE blower system. Additionally, a 1,500-gallon phase separation tank was installed adjacent to the location of the former SVE system, and a curtain of four biosparging wells was installed to limit potential LNAPL and contaminated groundwater discharge to the unnamed creek located immediately downgradient of the site.
Total fluids recovered by AFVR were historically treated and disposed through an onsite groundwater treatment system consisting of an oil/water separator (OWS), a recovered LNAPL storage tank, effluent transfer pump, filter housing(s) equipped with oleophilic filter socks, and a two-tray low profile air stripper. The final treated effluent was discharged by gravity line to the unnamed tributary of the Little River
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under a General National Pollutant Discharge Elimination System (NPDES) permit. The groundwater treatment system has not been operational since November 2012, and fluids generated from AFVR events have been transported offsite for disposal since that time. The groundwater treatment system has been dismantled and removed from the site.
Monitoring well MW7-22, which is located downgradient of the site, was sampled on February 25, 2014, to determine if there were any GCL exceedances and to confirm that the groundwater contaminant plume was stable. Three analytes exceeded the North Carolina 2L (NC2L) Groundwater Quality Standard (GWQS) at MW7-22: benzene (80.9 µg/L), naphthalene (25.4 µg/L), and final C9-C22 aromatics (370 µg/L). GCLs were not exceeded. Groundwater results were discussed at the October 15, 2014 Tier 1 meeting. The team determined that groundwater monitoring frequency would be every five years in advance of the 5-year review. A total of 29 wells were also abandoned in November 2014 in advance of upcoming construction. During the well abandonment in November 2014, three wells were discovered on the airfield that were not shown on historical maps; these wells were surveyed prior to a comprehensive gauging event. These wells were arbitrarily assigned the following well IDs: RW-A, RW-B, and RW-C.
Following the January 26, 2016, Tier 1 meeting, the compressor that powers the biosparge wells was inspected and found not to be running. Parsons contracted with Lewis Systems and Service Company to troubleshoot the compressor. On February 11, 2016, Lewis Systems inspected the compressor and determined that it needed to be replaced. Lewis Systems replaced the Becker compressor on March 2, 2016, with an identical model. In 2018, the compressor failed again and during a Tier I meeting in November it was determined not to replace the compressor until after data from the February 2019 sampling was reviewed. Based upon that review, the system was not placed back into operation. AFVR at the time was being completed by utilizing a vacuum truck to remove fluids and vapors from extraction wells. AFVR was discontinued in 2019 due to the lack of recovered product.
In 2019, absorbent hydrophobic socks were instead deployed to skim off free product that accumulates in the monitoring and recovery wells. These socks are replaced on a semi-annual basis when gauging and sampling of the groundwater occurs. Current sampling results are similar to those observed in 2014 with exceedances of the NC2L but below the GCL.
3.0 Field Activities and Sampling Methodology
A long-term monitoring event for groundwater was conducted by USACE, Savannah District in April-May 2023. Groundwater samples were collected from ten monitoring wells
at Site 308 and analyzed for volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), extractable petroleum hydrocarbons (EPH), and volatile petroleum hydrocarbons (VPH) using low-flow sampling methods.
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3.1 Water Level and Free Product Gauging
Depth to groundwater was measured on April 28 – May 1, 2023, at site monitoring wells prior to the sampling activities. Static groundwater level measurements were collected using an electronic oil-water interface probe. The indicator probe was
lowered into each monitoring well until the alarm sounded and/or the indicator light illuminated. The probe was then withdrawn several feet and slowly lowered again until the oil and/or groundwater surface was contacted, as noted by the alarm and/or indicator light. Water level measurements were measured to the nearest 0.01-feet from the top of the well casing. Depth to product, depth to water measurements, and
groundwater elevations from accessible monitoring wells are summarized in Table 4 and 7. A potentiometric surface map depicting groundwater flow is provided in Figure 5. Groundwater flow at the site is generally toward the northwest. Free product was encountered at the following wells:
MW7-16 (0.17-feet) PT-2 (2.12-feet) RW-03 (0.01-feet) RW-04 (0.04-feet) RW-05 (0.01-feet)
RW-12 (0.01-feet) MW-308A (1.62-feet) MW-308E (0.01-feet) MW-308F (2.10-feet)
Depth to water ranged from approximately 12-feet bgs to 23-feet bgs and free product ranged in thickness from a sheen to approximately 2-feet. MW-308A is not on the map but is assumed to be in the area north of Hurst Drive where other similarly named wells are located.
3.2 Low-flow Sample Collection
Groundwater samples were collected using a low-flow purge method with a bladder pump. Immediately before purging a well, the static water level below the top of the well casing and the total depth of the well were measured to the nearest 0.01-feet and recorded in the field logbook or on sampling forms. The volume of water in the well
was calculated based on the static water level and the well construction information.
Well volume calculations were recorded in the field logbook or on sampling forms. The inlet of the sampling pump was placed at the mid-point of the screened interval. This level was adjusted for wells where the static water level was within the well screen.
The wells were purged until the water quality had stabilized or five purge volumes were
removed. The wells were considered stable when the following requirements were met
for three consecutive readings: turbidity values were lower than 10 Nephelometric Turbidity Units (NTUs) or within 10%, temperature values within a range of 0.5
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degrees Celsius, pH readings within 0.1 Standard Units (SU), conductivity values within 3%, and DO values within 5%.
The rate of pumping was noted in the field logbook or on sampling forms with the purge
rate adjusted, as necessary, to avoid purging any monitoring well to dryness. Attempts
were made to equilibrate the recharge rate of the aquifer and purge rate. All sampling equipment was protected to prevent contamination of the samples (e.g., equipment may be placed on disposable polyethylene plastic sheeting). Groundwater samples were collected after purging was complete. The tubing was disconnected from the flow
through cell, and the samples were collected from the pump outlet. The samples were
labeled and placed immediately in an ice-filled cooler for preservation. The sampling information was logged on the laboratory provided chains-of-custody.
4.0 GROUNDWATER ANALYTICAL RESULTS SUMMARY
This section presents the results of groundwater analysis from the April/May 2023 event at the Site. A summary of the groundwater analytical data is presented in Table 8 and on
Figure 7. Laboratory data sheets are included in Appendix B with field notes and forms included in Appendix A.
4.1 Historical Analytical Data
Historical data for the Site is summarized in Table 9. All concentrations at the site have been and remain below the GCL but above applicable NC2L values. The detections at MW7-20 were higher than those detected in the past at the site. This is a well where
free product was historically found and is likely why the concentration is higher in that well.
4.2 2023 Groundwater Results
During the 2023 sampling event, no detections were above the GCL for any analyte. The following analytes were detected above the NC2L: 2-methylnaphthalene, Acrolein, Benzene, Naphthalene, Toluene, Xylenes, bis(2-ethylhexyl) phthalate, C5-
C8 aliphatics, C9-C18 aliphatics, and C9-C22 aromatics.
The relative percent difference (RPD) was calculated and presented in Table 10. Calculated RPDs for most analytes were below 20% indicating the data is usable for decision making. VOCs that had RPD >20% include naphthalene. Naphthalene is flagged in the data and is not expected to be related to sampling procedural issues.
RPD for all SVOC data was <20%. Massachusetts Department of Environmental
Protection (MADEP) EPH RPD was >20% for C11-C22 Aromatics (135%) and C9-C18 Aliphatics (140%). For the duplicate sample, the first lab run of MADEP EPH data was flagged due to calibration issues and was run again outside of hold time. This high RPD does not indicate an issue with the sampling or field procedures.
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4.3 Free Product Recovery
During gauging of the free product at the Site, hydrophobic socks and any free product recovered from the wells was placed in a sealable bucket for transport to the Directorate of Public Works (DPW). Materials were properly disposed of at the DPW. Approximately 1.5 gallons of product were removed from the monitoring and recovery wells at the Site.
5.0 CONCLUSIONS AND RECOMMENDATIONS
During the spring 2023 gauging and sampling event, a more comprehensive gauging was able to be completed due to construction activities being completed at the airfield. This gauging found free product in several wells on the airfield as well as product being
observed in wells that were clear for a number of events near the unnamed tributary. Free product was observed to vary in thickness from a sheen to approximately 2 feet.
MW-308A is not on the map but was found to have 1.62-feet of product in the well. This is currently a 1-inch well and it is recommended to be replaced with a 4-inch well to better facilitate product recovery. The construction of the well is unknown but a new well will be
installed as to be screened across the water table to allow LNAPL to enter the well.
Based on the free product periodically observed in the monitoring wells, especially those nearest the unnamed tributary to Little River, it is recommended that an updated investigation be completed to determine the current extent of the plume and determine which zones are saturated with product. Consultation with NCDEQ will determine if an
updated CAP is needed or if the current CAP can be utilized and a New Technology Cleanup Plan be submitted prior to any additional remedial actions at the site. Many of the remedial options in the 2005 CAP have been utilized at the Site either at pilot scale or full scale. Thermal treatment was determined to be applicable but was ruled out due to cost in the CAP. A pilot study may provide information to determine if this is a technology
that may be useful to target areas of residual product at the Site which have not been able to be addressed through the other remedial technologies.
Restarting AFVR was considered but these events rapidly show diminishing rates of return. It is recommended to continue with the absorbent socks currently and to discuss the gauging schedule at the next Tier I.
Groundwater sampling did not find any concentrations above the GCLs but several contaminants were above the NC2L. During the sampling, several of the large vaults had locking mechanisms that were inoperable and two of the lids were found to be heavier than what the field crew could safely lift to gain access. Sampling will be completed again in October 2023 at select monitoring wells where product is not present, and the vault is
accessible. Additional supplies will be available to attempt access into vaults that were inaccessible either due to the mass or broken latches/locking mechanisms.
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No change is recommended to the sampling and gauging schedule until after data is received from the October 2023 sampling and gauging event.
6.0 REFERENCES
Black and Veatch, 2005. Final Corrective Action Plan for Pope Air Force Base, Site SS007,
March 11, 2005.
Parsons 2013. Final Quality Assurance Project Plan/Sampling and Analysis Plan for Performance Based Remediation of 66 Sites at Fort Bragg-Pope AAF, January
2013.

E. Statements and Certification

The following statements must be included at the closing of the document text and must display the seal and signature of the certifying P.E. or L.G. in addition to the name and certification number of the company or corporation [See 15A NCAC 2L .0103(e).]

1 Enter the date the monitoring report was due. 9/19/2023 Will this report be submitted after the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO

3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
Free product is being found in various wells around the site including those next to the unnamed stream. The free product in the monitoring wells is ephemeral in nature indicating that product is bound in the fine-grained soils and being slowly released over time.

Figures
U.S. ARMY ENGINEER DISTRICT
CORPS OF ENGINEERS
SAVANNAH, GEORGIA
Site Vicinity Map
FTBR-308
Figure 1
Copyright:© 2013 National Geographic Society, i-cubed
±0 2,000 4,0001,000 Feet
1 inch equals 2,000 feet
FTBR-308 Former Hydrant System
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
NC CGIA, Earthstar
Geographics
FTBR-308
Site Map with Former Hydrant System,
Pump Houses, and USTs
Fort Liberty, North Carolina
Figure 2
Tit
a
n
St SurveyorStFortress StA
ero

S
t
Hurst Dr
@A@A@A
@A
@A@A@A
@A
@A@A@A@A
@A@A
@A@A
@A@A@A@A@A@A
@A
@A
@A@A@A@A@A @A
PT-2MW7-22 MW7-20
MW7-18
RW-03
RW-05
TW7-07RW-20
RW-B
RW-A
MW7-16
RW-18
RW-11
RW-10
RW-08
RW-16
RW-21
MW-308-HMW-308-E MW-1 TW7-03
Esri Community Maps Contributors, County of Cumberland, State of North Carolina DOT, © OpenStreetMap, Microsoft, Esri,
HERE, Garmin, SafeGraph, GeoTechnologies, Inc, METI/NASA, USGS, EPA, NPS, US Census Bureau, USDA, NC CGIA, Maxar,
Microsoft
@A Monitoring or Recovery
Well
Cross Section A-A'
Former Hydrant System
Natural Gas
Water
Wastewater
Stormwater
Electric
Pump House
UST
A'
A
September 2023
0 200 400100Feet
1 inch equals 200 feet
±
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
Figure 3
@A @A@A
@A
@A@A
@A
@A
@A@A
@A
@A
@A
@A
@A
@A
@A
@A
@A @A
@A @A
@A
@A
@A@A@A@A@A
@A
725
732
734
736
737
738740
741
744
750
90920
90921
NA
PT-2
MW-3
MW7-22
MW7-20
MW7-18
RW-04
RW-03
RW-05
TW7-07RW-20
RW-B
RW-A
MW7-16
RW-17
RW-18
RW-11
RW-10
UNK RW-09 RW-12
RW-08
RW-13
RW-16
RW-21
MW-308-H
MW-308-G
MW-308-F
MW-308-E
MW-1
TW7-03
FTBR-308
Well Network
Fort Liberty, North Carolina
September 2023
0 80 16040Feet
1 inch equals 80 feet
±
@A Monitoring or Recovery
Well
Former Hydrant System
Building
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
NC CGIA, Earthstar
Geographics
Figure 4LittleRiverHurstDr
W

Man chesterR d
SurveyorStFortress StSurveyor St
Booster

S
t
Su
r
v
e
yo
r

S
t
TankCreekTank CreekLittle

R
i
v
er
Esri Community Maps Contributors, County of Cumberland, State of North Carolina DOT, © OpenStreetMap, Microsoft, Esri,
HERE, Garmin, SafeGraph, GeoTechnologies, Inc, METI/NASA, USGS, EPA, NPS, US Census Bureau, USDA, NC CGIA, Maxar,
Microsoft
FTBR-308
Potential Receptor Map
Fort Liberty, North Carolina
No surface water features
within 500-feet of FTBR-308
No groundwater production wells
within 1,000-feet of FTBR-308
No groundwater production wells
within 1,500-feet of FTBR-308
FTBR-308
500-foot Radius
1,000-foot Radius
1,500-foot Radius
Stream
Wetland
September 2023
0 400 800200Feet
1 inch equals 400 feet
±
Note: Surface water features measured
from the site location marker. Surface
water has historically been affected by
this site.
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
Figure 5
Ti
t
a
n

S
t
Surveyor StSurveyor StFortress StTi
tan
S
tSurveyor StFortress StTit
an
S
t Fortress St@A @A@A
@A
@A@A
@A
@A
@A@A
@A
@A
@A
@A
@A
@A
@A
@A
@A @A
@A @A
@A
@A
@A@A@A@A@A
@A
169168167
170171PT-2
MW-3
168.84
MW7-22
166.78
MW7-20
169.44
MW7-18
169.18 RW-04
170.54
RW-03
170.28
RW-05
170.02
TW7-07RW-20
RW-B
RW-A
MW7-16
171.34
RW-17
171.25
RW-18
171.58
RW-11
RW-10 UNK
RW-09
RW-12
171.25
RW-08
170.79
RW-13
RW-16
171.14
RW-21
MW-308-H
MW-308-G
MW-308-F
MW-308-E
MW-1
166.38
TW7-03
FTBR-308
Potentiometric Map
Fort Liberty, North Carolina
September 2023
0 80 16040Feet
1 inch equals 80 feet
±
@A Monitoring or Recovery
Well
Potentiometric Contour
$Gro
u
n
d
w
a
t
e
r

F
l
o
w
Dir
e
c
t
i
o
n
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
Figure 6
Ti
ta
n
St
Surveyor StSurveyor StFortress StTi
tan
S
tSurveyor StFortress StTi
ta
nSt Fortress St
Aer
o
St
@A @A@A
@A
@A@A
@A
@A
@A@A
@A
@A
@A
@A
@A
@A
@A
@A
@A @A
@A @A
@A
@A
@A@A@A@A@A
@A
TW7-07RW-20
RW-B
RW-A
RW-11
RW-10
UNK
RW-09 RW-13
RW-21
FTBR-308
Estimated Free Product
Extent
Fort Liberty, North Carolina
September 2023
2/20/2018 0.56
8/25/2018 0.40
2/5/2019 0.28
4/23/2019 0.26
10/31/2019 0.55
1/14/2020 0.45
2/4/2020 0.01
5/1/2023 0.00
MW7-18
Date Product
Thickness (ft)
2/20/2018 0.08
8/25/2018 0.00
4/24/2019 0.00
10/31/2019 0.00
1/14/2020 0.00
4/28/2023 0.00
Date Product
Thickness (ft)
MW7-20
2/20/2018 0.15
8/25/2018 0.18
2/5/2019 0.00
4/24/2019 0.00
4/30/2023 0.17
MW7-16
Date Product
Thickness (ft)
2/20/2018 0.42
8/25/2018 0.11
2/5/2019 0.00
4/24/2019 0.00
10/31/2019 0.00
1/14/2019 0.00
4/27/2023 0.00
MW-3
Date Product
Thickness (ft)
2/20/2018 0.02
8/25/2018 0.00
2/5/2019 0.00
4/24/2019 0.00
5/1/2023 0.01
RW-05
Date Product
Thickness (ft)
10/26/2017 0.00
2/5/2019 0.00
4/24/2019 0.00
4/27/2023 0.00
MW7-22
Date Product
Thickness (ft)
2/25/2014 0.00
11/13/2014 0.02
4/23/2019 0.00
4/28/2023 2.12
PT-2
Date Product
Thickness (ft)
10/25/2016 0.00
4/24/2019 0.00
4/28/2023 0.00
Date Product
Thickness (ft)
MW-1
10/25/2016 0.00
10/26/2017 0.00
2/5/2019 0.00
4/30/2023 0.00
RW-16
Date Product
Thickness (ft)
10/25/2016 0.00
10/26/2017 0.00
2/5/2019 0.00
4/30/2023 0.00
RW-08
Date Product
Thickness (ft)
10/25/2016 0.00
10/26/2017 0.00
2/5/2019 0.00
4/30/2023 0.01
RW-12
Date Product
Thickness (ft)
10/25/2016 0.00
10/26/2017 0.00
2/5/2019 0.00
4/24/2019 0.00
5/1/2023 0.00
RW-18
Date Product
Thickness (ft)
10/25/2016 0.00
10/26/2017 0.00
2/5/2019 0.00
4/30/2023 0.00
RW-17
Date Product
Thickness (ft)
4/28/2023 0.00
TW7-03
Date Product
Thickness (ft)
2/20/2018 0.37
8/25/2018 0.38
2/5/2019 0.37
4/24/2019 0.23
10/31/2019 0.45
1/14/2020 0.03
2/4/2020 0.00
5/1/2023 0.04
RW-03
Date Product
Thickness (ft)
4/30/2023 1.62
MW-308A
Date Product
Thickness (ft)
4/30/2023 0.01
MW-308E
Date Product
Thickness (ft)
4/30/2023 2.10
MW-308F
Date Product
Thickness (ft)
4/30/2023 0.00
MW-308G
Date Product
Thickness (ft)
4/30/2023 0.00
MW-308H
Date Product
Thickness (ft)
2/20/2018 0.37
8/25/2018 0.38
2/5/2019 0.37
4/24/2019 0.23
10/31/2019 0.45
1/14/2020 0.03
2/4/2020 0.00
5/1/2023 0.04
RW-04
Date Product
Thickness (ft)
@A Monitoring or Recovery Well
Estimated Free Product Extent
Stream
0 80 16040Feet
1 inch equals 80 feet
±
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
September 2023 Figure 7
Tita
n

S
t
Surveyor StSurveyor StFortress StTit
an S
tSurveyor StFortress StTi
tan
S
t Fortress St
A
e
r
o

S
t
@A @A@A
@A
@A@A
@A
@A
@A@A
@A
@A
@A
@A
@A
@A
@A
@A
@A @A
@A @A
@A
@A
@A@A@A@A@A
@A
PT-2 MW-3
RW-04
RW-03
RW-05
TW7-07RW-20
RW-B
RW-A
RW-11
RW-10
UNK
RW-09
RW-12
RW-13
RW-21
MW-308-HMW-308-G
MW-308-FMW-308-E
FTBR-308
Spring 2023
Groundwater Concentrations
Fort Liberty, North Carolina
0 80 16040Feet
1 inch equals 80 feet
±
@A Monitoring or Recovery
Well
Stream
MW-1 Detection NC 2L
VOC
Carbon Disulfide 0.71 J 700
Cyclohexane 0.69 J NE
Isopropylbenzene 0.51 J 70
sec-Butylbenzene 0.67 J 70
MA VPH and EPH
C9-C18 Aliphatics (a+b)32 JM 700
C9-C22 Aromatics (c+d)16 JM 200
µg/L
µg/L MW7-16 Detection NC 2L
VOC
2-Methylnaphthalene 35 Q 30
Acetone 9.9 JQ 6,000
Acetonitile 210 QM NE
Acrolein 34 J 4
Benzene 6.5 1
Cyclohexane 160 NE
Ethylbenzene 6.0 600
Isopropylbenzene 31 70
Methylcyclohexane 85 NE
Naphthalene 110 6
n-Propylbenzene 26 70
o-Xylene 0.29 J NE
sec-Butylbenzene 4.7 70
tert-Butylbenzene 1.3 J 70
SVOCs
2-Methylnaphthalene 20 30
Naphthalene 6.9 JHQ 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)1,100 400
C9-C18 Aliphatics (a+b)1,400 700
C9-C22 Aromatics (c+d)650 200
µg/L
µg/L
µg/L
MW7-18 Detection NC 2L
VOC
Benzene 1,300 D 1
Cyclohexane 83 JDQ NE
Ethylbenzene 300 D 600
Methylcyclohexane 35 JDM NE
Toluene 1,400 D 600
Total Xylenes 1,500 D 500
SVOCs
2-Methylnaphthalene 43 30
bis(2-ethylhexyl) phthalate 6.3 JB 3
Naphthalene 110 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)5,500 DM 400
C9-C18 Aliphatics (a+b)4,840 DMBQ 700
C9-C22 Aromatics (c+d)1,470 JDM 200
µg/L
µg/L
µg/L
MW7-20 Detection NC 2L
VOC
1,2,3-Trimethylbenzene 11 Q NE
1,2,4-Trimethylbenzene 44 400
2-Methylnaphthalene 6.7 JQ 30
4-Isopropyltoluene 1.9 J 25
Acrolein 23 J 4
Benzene 4.5 1
Carbon Disulfide 0.79 J 700
Cyclohexane 6.3 NE
Ethylbenzene 4.4 600
Isopropylbenzene 11 70
Methylcyclohexane 2.5 NE
Naphthalene 1.9 J 6
n-Propylbenzene 11 70
sec-Butylbenzene 4.0 70
tert-Butylbenzene 0.95 J 70
SVOCs
2-Methylnaphthalene 3.6 J 30
Naphthalene 17 Q 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)100 400
C9-C18 Aliphatics (a+b)357 700
C9-C22 Aromatics (c+d)192 200
µg/L
µg/L
µg/L
MW7-22 Detection NC 2L
VOC
1,2,3-Trimethylbenzene 26 Q NE
1,2,4-Trimethylbenzene 53 400
1,3,5-Trimethylbenzene 14 400
2-Methylnaphthalene 13 Q 30
4-Isopropyltoluene 1.3 J 25
Acetonitile 310 QM NE
Benzene 46 1
Carbon Disulfide 0.68 J 700
Cyclohexane 32 NE
Ethylbenzene 3.2 600
Hexane 17 400
Isopropylbenzene 5.9 70
Methylcyclohexane 12 NE
m-Xylene & p-Xylene 130 NE
Naphthalene 36 6
n-Propylbenzene 1.1 J 70
o-Xylene 9.2 NE
sec-Butylbenzene 2.2 J 70
tert-Butylbenzene 0.54 J 70
Total Xylenes 140 500
SVOCs
Naphthalene 1.3 JHQ 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)550 M 400
C9-C18 Aliphatics (a+b)592 MH 700
C9-C22 Aromatics (c+d)198 MHB 200
µg/L
µg/L
µg/L
TW7-03 Detection NC 2L
VOC
1,2,3-Trimethylbenzene 69 QD NE
1,2,4-Trimethylbenzene 130 J1D 400
1,3,5-Trimethylbenzene 37 J1D 400
2-Methylnaphthalene 24 QD 30
2-Nitropropane 2.7 JQD NE
4-Isopropyltoluene 2.7 JD 25
Acetone 10 JQD 6,000
Acetonitile 140 QDM NE
Allyl Chloride 9.6 JD NE
Benzene 13 D 1
Cyclohexane 23 J1D NE
Ethylbenzene 40 J1D 600
Hexane 13 D 400
Heptane 2.4 JD 400
Isopropylbenzene 12 J1D 70
Methylcyclohexane 12 D NE
m-Xylene & p-Xylene 210 J1D NE
n-Butylbenzene 4.5 JD 70
o-Xylene 6.7 D NE
sec-Butylbenzene 2.5 JD 70
Toluene 1.6 JD 600
Total Xylenes 220 J1D 500
SVOCs
Naphthalene 3.5 JHQ 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)340 DMJ1 400
C9-C18 Aliphatics (a+b)1,250 DMHJ1 700
C9-C22 Aromatics (c+d)495 DMJ1 200
µg/L
µg/L
µg/L
RW-08 Detection NC 2L
VOC
Benzene 20 1
Cyclohexane 8.5 Q NE
Ethylbenzene 1.1 600
Methylcyclohexane 2.6 NE
Toluene 0.32 J 600
Total Xylenes 27 500
MADEP EPH & VPH
C5-C8 Aliphatics (x)340 M 400
C9-C18 Aliphatics (a+b)410 HMB 700
C9-C22 Aromatics (c+d)126 HMB 200
µg/L
µg/L
RW-16 Detection NC 2L
VOC
Benzene 8.7 1
Cyclohexane 76 Q NE
Ethylbenzene 61.0 600
Isopropylbenzene 16 70
Methylcyclohexane 46 NE
Toluene 4.7 600
Total Xylenes 360 D 500
SVOCs
2-Methylnaphthalene 14 J 30
bis(2-ethylhexyl) phthalate 6.3 JB 3
Naphthalene 28 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)980 M 400
C9-C18 Aliphatics (a+b)1,460 DHBM 700
C9-C22 Aromatics (c+d)552 HM 200
µg/L
µg/L
µg/L
RW-17 Detection NC 2L
VOC
Benzene 24 D 1
Cyclohexane 76 DQ NE
Ethylbenzene 220 D 600
Isopropylbenzene 24 D 70
Methylcyclohexane 51 D NE
Toluene 120 D 600
Total Xylenes 980 D 500
SVOCs
2-Methylnaphthalene 33 30
bis(2-ethylhexyl) phthalate 6.3 JB 3
Naphthalene 54 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)1,600 M 400
C9-C18 Aliphatics (a+b)2,440 DMBQ 700
C9-C22 Aromatics (c+d)810 JDMBQ 200
µg/L
µg/L
µg/L
RW-18 Detection NC 2L
VOC
Benzene 0.66 J 1
Cyclohexane 25 Q NE
Ethylbenzene 6.3 600
Isopropylbenzene 11 70
Methylcyclohexane 45 NE
Toluene 2.5 600
Total Xylenes 33 500
SVOCs
2-Methylnaphthalene 27 30
bis(2-ethylhexyl) phthalate 6.4 JB 3
Naphthalene 4.0 J 6
MADEP EPH & VPH
C5-C8 Aliphatics (x)580 M 400
C9-C18 Aliphatics (a+b)1,410 DMBQ 700
C9-C22 Aromatics (c+d)910 DMBQ 200
µg/L
µg/L
µg/L
All concentrations in micrograms per
liter (µg/L)
J: Estimated concentration
H: Hold time exceeded
D: Dilution required
Q: Quality control criteria not met
B: Contaminant found in blank sample
J1: Estimated due to discrepancies in
meeting quality control criteria
M: Manually integrated
FIGURE 8FTBR-308 GEOLOGICCROSS-SECTION A-A’Fort Bragg, North CarolinaDESIGNED BY:DRAWN BY:CHECKED BY:SUBMITTED BY:PROJECT NUMBER:FIGURENUMBER:747356.08000March 2014As Shown8ParsonsFTBR-308draw\747356 Geologic Cross-Section.cdr pup ma 04/17/2014SCALE:DATE:FILE:Source: Black and Veatch, 2005.March 11, 2005Corrective Action Plan;Pope AFB Site S 007 Blue Ramp,S

Tables

FTBR-308Table 1UST System InformationUST ID NumberProduct (gasoline, diesel, jet fuel, etc.)Capacity (gallons)Tank DimensionsDate Tank Installed(m/dd/yy)Date Permanently Closed (m/dd/yy)Was Release Associated With UST System? (Yes / No)Unknown A Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown B Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown C Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown D Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown E Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown F Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown G Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown H Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown I Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown J Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown K Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown L Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown M Jet Fuel 50,000 Unknown Unknown Unknown UnknownUnknown N Jet Fuel 50,000 Unknown Unknown UnknownUnknownUnknown O Jet Fuel 50,000 Unknown Unknown UnknownUnknownUnknown P Jet Fuel 50,000 Unknown Unknown UnknownUnknownUnknown Q Jet Fuel 50,000 Unknown Unknown UnknownUnknownUnknown R Jet Fuel 50,000 Unknown Unknown UnknownUnknownHydrant System Jet Fuel 110,500Unknown Unknown UnknownUnknown
Table 2
FTBR-308
UST Owner/Operator Information
T2-1 of T2-4
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown A XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown B XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown C XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown D XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown E XVIII Airborne Corps and Fort Liberty Unknown to Owner
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Table 2
FTBR-308
UST Owner/Operator Information
T2-2 of T2-4
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown F XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown G XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown H XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown I XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown J XVIII Airborne Corps and Fort Liberty Unknown to Owner
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Table 2
FTBR-308
UST Owner/Operator Information
T2-3 of T2-4
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown K XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown L XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown M XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown N XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown O XVIII Airborne Corps and Fort Liberty Unknown to Owner
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Table 2
FTBR-308
UST Owner/Operator Information
T2-4 of T2-4
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown P XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown Q XVIII Airborne Corps and Fort Liberty Unknown to Owner
UST ID Number Name of Owner or Operator Dates of Ownership / Operation Owner or Operator?
Unknown R XVIII Airborne Corps and Fort Liberty Unknown to Owner
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
(910) 396‐7432
Address Telephone Number
Table 3
FTBR-308
Property Owner Information
Date: 7/24/2023 Incident No. and Name: FTBR‐308 Facility ID #: 29702
Tax Parcel Number/
Map ID
Owner/Occupant Name
(Last, First, MI)Address
NA XVIII Airborne Corps and Fort Liberty
Directorate of Public Works (Environmental Compliance Branch)
ATTN: AMIM‐LIP‐EM
Bldg 3‐1137
Fort Liberty, NC 28310
Table 4FTBR-308Monitoring and Remediation Well Construction InformationWell IDDate Installed (m/dd/yy)Date Water Level Measured (m/dd/yy)Well Casing Depth (ft. BGS)Screened Interval (ft BGS)Bottom of Well (ft. TOC)Top of Casing Elevation* (ft.)Depth to Water from Top of Casing (ft.)Free Product Thickness** (ft.)Ground-water Elevation* (ft.)Northing EastingCommentsMW-1NA4/28/2023 NANA20.22 177.78 11.40 0.00 166.38 518663.76 1993447.90 Unable to locateMW-2 NA-- NANA20.35 180.73 ------ 518700.52 1993492.26 Abandoned on 11/17/2014MW-3NA4/27/2023 NANA32.74 191.63 22.79 0.00 168.84 518613.49 1993483.65MW-4 NA-- NANA27.25 189.48 ------ 518722.64 1993519.92 Abandoned on 11/17/2014MW7-01 2/10/1997 -- 22.5 22.5-37.5 25.83198.17 ------ 517375.08 1994921.44 Abandoned on 11/14/2014MW7-02 2/11/1997 -- 22.5 22.5-37.5 25.56 198.49 ------ 517221.96 1994689.92 Unable to locate 11/14/2014MW7-03 2/12/1997 -- 15.0 15.0-30.0 29.79192.16 ------ 518845.93 1993879.10 Abandoned on 11/17/2014MW7-09 2/20/1997 -- 20.0 20.0-34.5 30.4196.73 ------ 517936.57 1994892.02 Abandoned on 11/14/2014MW7-10 2/20/1997 -- 20.0 20.0-34.5 NA196.95 ------ 517946.68 1994950.81 Abandoned on 11/14/2014MW7-11 2/20/1997 -- 19.5 19.5-34.5 NA194.61 ------ 517849.52 1994286.58 Cannot OpenMW7-12 2/25/1997 -- 41.5 41.5-44.5 NA194.47 ------ 517547.61 1994288.85 Cannot OpenMW7-13 2/26/1997 -- 18.5 18.5-33.5 27.75192.22 ------ 518321.22 1994210.44 Abandoned on 11/13/2014MW7-14 2/27/1997 -- 17.0 17.0-32.0 NA193.97 ------ 518339.76 1994723.53 Cannot OpenMW7-15 2/27/1997 -- 17.5 17.5-32.5 30.7190.27 ------ 518255.53 1993745.61 Abandoned on 11/13/2014MW7-163/10/1997 4/30/2023 18.018.0-28.0NA190.8419.65 0.17 171.34 518461.45 1993928.34MW7-17 3/11/1997 -- 16.5 16.5-31.5 27.5191.15 -- -- -- 518605.20 1994078.31 Abandoned on 11/13/2014MW7-183/12/1997 5/1/2023 17.517.5-32.531.91189.6120.43 0.00 169.05 518506.88 1993692.94MW7-19 NA-- NANA28.69 189.28 ------ 518314.97 1993527.92 Unable to locateMW7-20NA4/28/2023 NANA28.48 190.69 21.25 0.00 169.44 518575.12 1993545.73MW7-21 NA -- NA NA 29.81 187.19 -- -- -- 518628.80 1993359.41Has been sealed shut with asphalt 10/22/2015MW7-22 NA4/27/2023 NANANA189.58 22.80 0.00 166.78 518602.00 1993354.09MW7-23 1/29/2003 -- 17.0 17.0-32.0 NA190.93 ------ 518453.31 1993844.49 Unable to locate 11/15/2014MW7-24 2/4/2003 -- 16.0 16.0-31.0 NA191.03 ------ 518434.89 1993853.45 Unable to locatePT-2NA4/28/2023 NANA24.95 NA15.07 2.12 -- NANARW-01NA-- 18.5 18.5-23.5 33.26 190.98 ---- -- 518416.12 1993614.95 Abandoned 11/15/2014RW-02 NA-- 17.7 17.65-22.65 34.4 190.64 ---- -- 518438.17 1993636.48 Abandoned 11/15/2014RW-03 NA5/1/2023 20.6 20.6-25.6 34.01 190.61 20.34 0.01 170.28 518463.31 1993658.53RW-04NA5/1/2023 NANA34.38190.6520.14 0.04 170.54 518495.58 1993698.57RW-05 NA5/1/2023 NANA33.68 189.15 19.17 0.01 169.99 518534.61 1993743.08RW-06 NA-- 18.3 18.34-23.34 33 190.20 ------ 518564.55 1993760.32 Abandoned 11/15/2014RW-07NA-- 17.9 17.85-22.85 30.57 190.16 ---- -- 518553.49 1993827.40 Abandoned 11/15/2014RW-08 NA4/30/2023 18.4 18.43-23.43 NA190.14 19.35 0.00 170.79 518483.38 1993819.22RW-09NA-- 18.018.0-23.0NA189.60-- -- -- 518460.86 1993808.20RW-10NA-- NA16.97-26.97NA190.24-- -- -- 518436.33 1993775.59RW-11NA-- NANANA190.25 ------ 518401.40 1993806.00RW-12NA4/30/203 NANANA190.70 19.46 0.01 171.25 518437.80 1993830.00RW-13 NA-- NANANA190.43 ------ 518461.20 1993838.00RW-14NA-- NANANA190.20 ------ 518467.42 1993901.33RW-15 2/25/2010 -- 17.0 17.0-27.0 NA191.37 ------ 518505.25 1993841.61 Abandoned 11/14/2014T4-1 of T4-2
Table 4FTBR-308Monitoring and Remediation Well Construction InformationWell IDDate Installed (m/dd/yy)Date Water Level Measured (m/dd/yy)Well Casing Depth (ft. BGS)Screened Interval (ft BGS)Bottom of Well (ft. TOC)Top of Casing Elevation* (ft.)Depth to Water from Top of Casing (ft.)Free Product Thickness** (ft.)Ground-water Elevation* (ft.)Northing EastingCommentsRW-16 2/26/2010 4/30/2023 17.0 17.0-27.027.25 190.99 19.85 0.00 171.14 518332.72 1993780.52RW-17 2/25/2010 4/30/2023 18.0 18.0-28.0 NA191.24 19.99 0.00 171.25 518418.60 1993915.18RW-18 2/26/2010 5/1/2023 18.0 18.0-28.027.7 191.63 20.05 0.00 171.58 518370.74 1993901.95RW-19 2/26/2010 -- 18.0 18.0-28.0 28.3191.88 -- -- -- 518318.25 1993874.79 Abandoned 11/13/2014RW-20 2/25/2010 -- 18.0 18.0-28.0 27.7 192.10 -- -- -- 518439.74 1994027.83RW-21 NA-- NANANA188.35 ------ 518633.11 1993544.80DestroyedRW-22NA-- NANANA188.44 ------ 518616.08 1993535.96 Cannot AccessRW-23 2/25/2010 -- 18.0 18.0-28.0 28192.46 ------ 518391.16 19994015.07 Abandoned 11/13/2014RW-24 2/25/2010 -- 18.0 18.0-28.0 28192.84 ------ 518330.95 1993998.95 Abandoned 11/13/2014RW-25 2/25/2010 -- 18.0 18.0-28.0 28.45193.40 ------ 518401.28 1994131.34 Abandoned 11/13/2014RW-26 2/25/2010 -- 18.0 18.0-28.0 28.1193.56 ------ 518353.78 1994115.01 Abandoned 11/13/2014RW-27 2/25/2010 -- 18.0 18.0-28.0 28.3193.74 ------ 518313.12 1994101.33 Abandoned 11/13/2014RW-28 2/25/2010 -- 18.0 18.0-28.0 28.2193.48 ------ 518367.44 1994228.93 Abandoned 11/13/2014RW-29 2/25/2010 -- 18.0 18.0-28.0 27.9192.86 ------ 518291.66 1994213.16 Abandoned 11/13/2014TW7-01 3/5/2003 -- 11.5 11.5-31.5 NA191.19 ------ 518613.43 1993970.04 Abandoned 11/13/2014TW7-02 3/6/2003 -- 15.0 15.0-35.0 29191.41 ------ 518273.42 1993789.16 Abandoned 11/13/2014TW7-03 3/6/2003 4/28/2023 15.0 15.0-35.034.3 188.88 19.95 0.00 168.93 518688.70 1993571.48Abandoned 11/13/2014Fully Abandoned 2023TW7-04 3/11/2003 -- 15.0 15.0-35.0 28.16 188.64 ------ 518279.28 1993495.35TW7-05 3/11/2003 -- 15.0 15.0-35.0 34.47190.03 ------ 518636.77 1993795.46 Abandoned 11/13/2014TW7-06 3/11/2003 -- 15.0 15.0-35.0 NA193.46 ------ 518332.37 1994220.93 Abandoned 11/13/2014TW7-07 3/12/2003 -- 15.0 15.0-35.0 28.3 193.12 ------ 518450.45 1994151.20TW7-08 3/13/2003 -- 15.0 15.0-35.0 NA193.56 ------ 518269.01 1994255.14 Cannot OpenTW7-09 5/6/2003 -- 12.0 12.0-24.0 NA193.59 ------ 518548.67 1994384.74 Abandoned 11/13/2014RW-ANA-- NANANA192.81 ------ 518369.62 1993995.36RW-BNA-- NANANA192.59 ------ 518420.28 1994004.66RW-CNA-- NANANANA------ 518517.64 1994050.01UNKNA-- NANANANA------ 518429.56 1993775.45* Reference Point for Elevation Measurements USGS Survey Monument HARP 1987. All elevations in ft mean sea level.ft BGS = feet below ground surfaceNA = Not Available** If free product is present in a well, groundwater elevation should be calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]Unknown wells not on historical mapsT4-2 of T4-2
Table 5FTBR-308AFVR Free Product Recovery InformationDate (m/dd/yy)Well ID #Product Type (gas, diesel, etc.)Free Product Recovery Method*Product Thickness before Recovery (feet)Product Thickness after Recovery (feet)Amount of Vaporized ProductAmount of Liquid (Water and Product) (gallons)Amount of Liquid Product (gallons)Total Amount of Product Recovered (gallons) 18-Nov-2013RW-11RW-09RW-04 MW7-18Jet FuelAggressive Fluid Vapor RecoveryRW-11 = 0.02RW-09 = 0.01RW-04 = 1.5 MW7-18 = 2.87RW-11 = 0RW-09 = 0RW-04 = 0 MW7-18 = 0--1007 15.515.54-Mar-2014MW7-16RW-11RW-09RW-04 MW7-18 RW-24 RW-20 RW-05 MW-3Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.14RW-11 = 0.06RW-09 = 0.00RW-04 = 1.83 MW7-18 = 1.73 RW-24 = 0.07 RW-20 = 0.11 RW-05 = 0.19 MW-3 = 0.45MW7-16 = 0.00RW-11 = 0.00RW-09 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-24 = 0.00 RW-20 = 0.00 RW-05 = 0.00 MW-3 = 0.00--113812612621-May-2014MW7-16RW-11RW-09RW-04 MW7-18 RW-24 RW-20 RW-05 MW-3Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.0RW-11 = 0.01RW-09 = 0.00RW-04 = 0.84 MW7-18 = 1.74 RW-24 = 0.42 RW-20 = 0.05 RW-05 = 0.08 MW-3 = 0.03MW7-16 = 0.00RW-11 = 0.00RW-09 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-24 = 0.00 RW-20 = 0.00 RW-05 = 0.00 MW-3 = 0.00--870808020-Aug-2014MW7-16RW-11RW-09RW-04 MW7-18 RW-24 RW-20 RW-05 Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.37RW-11 = 0.28RW-09 = 0.00RW-04 = 0.65 MW7-18 = 1.30 RW-24 = 0.49 RW-20 = 0.13 RW-05 = 0.02 MW7-16 = 0.00RW-11 = 0.00RW-09 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-24 = 0.00 RW-20 = 0.00 RW-05 = 0.00 --784383819-Nov-2014MW7-16RW-11RW-09RW-04 MW7-18 RW-14 RW-20 RW-05 Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.23RW-11 = 1.16RW-09 = 0.00RW-04 = 0.60 MW7-18 = 1.25 RW-14 = 0.23 RW-20 = 0.22 RW-05 = 0.01 MW7-16 = 0.00RW-11 = 0.00RW-09 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-44 = 0.00 RW-20 = 0.00 RW-05 = 0.00 --3968818-Feb-2015MW7-16RW-11RW-09RW-04 MW7-18 RW-14 RW-20 RW-05 MW-03 Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.02RW-11 = 0.20RW-09 = 0.00RW-04 = 0.63 MW7-18 = 1.03 RW-14 = 0.00 RW-20 = 0.01 RW-05 = 0.00 MW-03 = 0.00 MW7-16 = 0.00RW-11 = 0.00RW-09 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-44 = 0.00 RW-20 = 0.00 RW-05 = 0.00 MW-03 = 0.00 --7923232T5-1 of T5-4
Table 5FTBR-308AFVR Free Product Recovery InformationDate (m/dd/yy)Well ID #Product Type (gas, diesel, etc.)Free Product Recovery Method*Product Thickness before Recovery (feet)Product Thickness after Recovery (feet)Amount of Vaporized ProductAmount of Liquid (Water and Product) (gallons)Amount of Liquid Product (gallons)Total Amount of Product Recovered (gallons) 13-May-2015MW7-16RW-11RW-04 MW7-18 RW-14 RW-20 RW-05 MW-03 Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.00RW-11 = 0.00RW-04 = 0.61 MW7-18 = 0.68 RW-14 = 0.00 RW-20 = 0.00 RW-05 = 0.00 MW-03 = 0.00 MW7-16 = 0.00RW-11 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-44 = 0.00 RW-20 = 0.00 RW-05 = 0.00 MW-03 = 0.00 -- 768 15 1518-Aug-2015MW7-16RW-11RW-09RW-04 MW7-18 RW-14 RW-20 Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.36RW-11 = 0.38RW-09 = 0.00RW-04 = 0.68 MW7-18 = 0.51 RW-14 = 0.00 RW-20 = 0.00 MW7-16 = 0.00RW-11 = 0.00RW-09 = 0.00RW-04 = 0.00 MW7-18 = 0.00 RW-44 = 0.00 RW-20 = 0.00 -- 1362 12 1227-Oct-2015MW7-16RW-11RW-ARW-20 MW7-18 RW-04 Jet FuelAggressive Fluid Vapor RecoveryMW7-16 = 0.37RW-11 = 0.79RW-A = 1.08RW-20 = 0.16 MW7-18 = 0.32 RW-04 = 0.40 MW7-16 = 0.00RW-11 = 0.00RW-A = 0.00RW-20 = 0.00 MW7-18 = 0.00 RW-04 = 0.00 -- 509 15 1510-Feb-2016RW-A RW-20 MW7-16 RW-14 RW-9 RW-11 RW-4 MW7-18 Jet FuelAggressive Fluid Vapor RecoveryRW-24 = 0.72 RW-20 = 0.00 MW7-16 = 0.00 RW-14 = 0.00 RW-9 = 0.00 RW-11 = 0.02 RW-4 = 0.55 MW7-18 = 0.49RW-24 = 0.00 RW-20 = 0.00 MW7-16 = 0.00 RW-14 = 0.00 RW-9 = 0.00 RW-11 = 0.00 RW-4 = 0.00 MW7-18 = 0.00 847 15 153-May-2016RW-04 MW7-18 RW-20 RW-A RW-9 MW7-16 RW-11 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.45 MW7-18 = 0.67 RW-20 = 0.08 RW-A = 0.38 RW-9 = 0.00 MW7-16 = 0.02 RW-11 = 0.00 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 RW-9 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 548 6.5 6.510-Aug-2016RW-04 MW7-18 RW-20 RW-A RW-05 MW7-16 RW-11 RW-14 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.37 MW7-18 = 0.48 RW-20 = 0.18 RW-A = 0.52 RW-05 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 RW-14 = 0.00 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 RW-05 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 RW-14 = 0.00 371 2 2T5-2 of T5-4
Table 5FTBR-308AFVR Free Product Recovery InformationDate (m/dd/yy)Well ID #Product Type (gas, diesel, etc.)Free Product Recovery Method*Product Thickness before Recovery (feet)Product Thickness after Recovery (feet)Amount of Vaporized ProductAmount of Liquid (Water and Product) (gallons)Amount of Liquid Product (gallons)Total Amount of Product Recovered (gallons) 25-Oct-2016RW-04 MW7-18 RW-20 RW-A RW-05 MW7-16 RW-11 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.26 MW7-18 = 0.35 RW-20 = 0.00 RW-A = 0.26 RW-09 = 0.21 MW7-16 = 0.00 RW-11 = 0.14 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 RW-09 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 822 2.5 2.515-Feb-2017RW-A RW-20 MW7-16 RW-14 RW-9 RW-11 RW-4 MW7-18 RW-24 Jet FuelAggressive Fluid Vapor RecoveryRW-24 = -0 RW-20 = 0.00 MW7-16 = 0.00 RW-14 = 0.00 RW-9 = 0.04 RW-11 = 0.00 RW-4 = 0.24 MW7-18 = 0.43 RW-A = 0.49RW-24 = 0.00 RW-20 = 0.00 MW7-16 = 0.00 RW-14 = 0.00 RW-9 = 0.00 RW-11 = 0.00 RW-4 = 0.00 MW7-18 = 0.00 RW-A = 0.00 308 2.5 2.517-May-2017RW-04 MW7-18 RW-20 RW-A RW-9 MW7-16 RW-11 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.40 MW7-18 = 0.40 RW-20 = 0.40 RW-A = 0.21 RW-9 = 0.05 MW7-16 = 0.00 RW-11 = 0.00 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 RW-9 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 219 1.5 1.515-Aug-2017RW-04 MW7-18 RW-20 RW-A RW-05 MW7-16 RW-11 RW-14 RW-9 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.23 MW7-18 = .14 RW-20 = .20 RW-A = 0.49 RW-05 = 0 MW7-16 = 0 RW-11 = 0 RW-14 = 0 RW-9 = 0 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 RW-05 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 RW-14 = 0.00 RW-9 = 0.00 371 2 220-Feb-2018RW-04 MW7-18 RW-20 RW-A RW-05 MW7-16 RW-11 MW7-20 MW-03 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.37 MW7-18 = 0.56 RW-20 = 0.74 RW-A = 0.91 RW-05 = 0.02 MW7-16 = 0.15 RW-11 = 0.04 MW7-20 = 0.08 MW-03 =0.42 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 RW-05 = 0.00 MW7-16 = 0.00 RW-11 = 0.00 MW7-20 = 0.00 MW-03 = 0.00 371 2 2T5-3 of T5-4
Table 5FTBR-308AFVR Free Product Recovery InformationDate (m/dd/yy)Well ID #Product Type (gas, diesel, etc.)Free Product Recovery Method*Product Thickness before Recovery (feet)Product Thickness after Recovery (feet)Amount of Vaporized ProductAmount of Liquid (Water and Product) (gallons)Amount of Liquid Product (gallons)Total Amount of Product Recovered (gallons) 25-Aug-2018RW-04 MW7-18 RW-20 RW-A RW-05 MW7-16 RW-11 MW-03 RW-9 Jet FuelAggressive Fluid Vapor RecoveryRW-04 = 0.38 MW7-18 = 0.40 RW-20 = 0.02 RW-A = 0.67 MW7-16 = 0.18 MW-03=0.11 RW-04 = 0.00 MW7-18 = 0.00 RW-20 = 0.00 RW-A = 0.00 MW7-16 = 0.00 MW-03 = 0.00 371 2 2* Bailing, Skimming, Aggressive Fluid Vapor Recovery, Mobile Multiphase Extraction, etc,NA = Not AvailableItalics indicated the work was performed by a previous consultant.*AFVR Discontinued 2019T5-4 of T5-4
Table 6FTBR-308Cumulative Volume of Free Product Recovered from the SiteDate of Recovery Event (m/dd/yy)Total Volume Recovered from Site During Current Recovery Event (gallons)Cumulative Total of Volume Recovered to Date from All Recovery Events (gallons) April 2010 - June 2013 1--634.011/18/201315.5649.53/4/2014126775.55/20/201480855.58/21/201438893.511/21/20148901.52/18/201532933.55/3/201515948.58/18/201512960.510/27/201515975.52/10/201615990.55/3/20166.5997.08/10/20162999.010/25/20162.51,001.52/15/20172.51,004.05/17/20171.51,005.58/15/201721,007.52/22/20181.51,009.08-25 201811,010.01/14/20201.41,011.42/4/20201.31,012.711/1/20200.81,013.53/1/20210.81,014.39/28/20211.41,015.74/7/20221.31,017.19/23/20220.01,017.15/1/20231.51,018.5Cumulative Free Product Recovered to Date Site 308:1,018.52019-Spring 2023: MW7-18: 2 socks, RW-04: 8 socks1 Free product recovery volumes from April 2010 - June 2013 reported by URS, 2013. Semi-Annual Operations and Maintenance Report January – July 2013, SS007, Pope Army Air Field, Fayetteville, Cumberland County, North Carolina. July 12, 2013.*2019 switched to hydrophobic absorbent socks. Each sock can hold up to 17 ounces (0.1328 gal) of product. Initially deployed 10/31/2019.1/1
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
2/25/2014 10.75 0.00 167.03
11/13/2014 15.35 0.00 162.43
10/22/2015 15.28 0.00 162.50
10/25/2016 10.11 0.00 167.67
10/26/2017 NM NM NM
4/24/2019 10.12 0.00 167.66
4/28/2023 11.40 0.00 166.38
2/25/2014 23.02 0.45 169.00
5/20/2014 22.85 0.03 168.81
11/13/2014 23.39 0.00 168.24
2/18/2015 22.96 0.00 168.67
5/13/2015 23.13 0.00 168.508/18/2015 23.39 0.00 168.24
10/22/2015 23.18 0.00 168.45
2/10/2016 22.68 0.00 168.95
8/10/2016 23.00 0.00 168.63
10/25/2016 22.22 0.00 169.41
10/26/2017 14.11 0.00 177.522/20/2018 24.02 0.42 167.97
8/25/2018 23.26 0.11 168.46
2/5/2019 22.10 0.00 169.53
4/24/2019 22.22 0.02 169.43
10/31/2019 23.14 0.00 168.49
1/14/2020 22.92 0.00 168.71
4/27/2023 22.79 0.00 168.84
2/25/2014 22.5-37.5 19.53 0.00 198.49 178.96
11/14/2014
3/4/2014
11/14/2014
3/4/2014
11/14/2014
3/4/2014
11/14/2014
11/18/2013 19.34 0.00 171.50
3/4/2014 19.55 0.14 171.41
5/20/2014 19.10 0.00 171.74
8/20/2014 19.60 0.37 171.5611/13/2014 19.81 0.23 171.23
2/18/2015 19.20 0.02 171.66
5/13/2015 19.21 0.00 171.63
8/18/2015 20.22 0.36 170.93
10/22/2015 19.87 0.37 171.29
2/10/2016 18.78 0.00 172.065/3/2016 18.71 0.02 172.15
8/10/2016 19.35 0.00 171.49
10/25/2016 18.50 0.00 172.34
10/26/2017 19.53 0.00 171.31
2-20-10228 20.22 0.15 170.75
8/25/2018 19.77 0.18 171.22
2/5/2019 18.07 0.00 172.77
4/24/2019 18.28 0.00 172.56
4/30/2023 19.65 0.17 171.34
11/18/2013 22.68 2.87 169.39
2/25/2014 21.94 1.73 169.15
5/20/2014 21.65 1.74 169.45
8/20/2014 21.55 1.30 169.18
11/13/2014 21.56 1.25 169.12
2/18/2015 21.46 1.03 169.03
5/13/2015 20.90 0.68 169.29
8/18/2015 21.03 0.51 169.02
10/22/2015 20.83 0.32 169.05
2/10/2016 20.40 0.49 169.635/3/2016 20.82 0.67 169.36
8/10/2016 20.81 0.48 169.21
10/25/2016 19.89 0.35 170.02
2/15/2017 20.50 0.43 169.48
5/17/2017 20.98 0.40 168.97
8/15/2017 20.37 0.14 169.3610/26/2017 20.82 0.21 168.97
2/20/2018 21.58 0.56 168.51
8/25/2018 21.00 0.40 168.95
2/5/2019 19.45 0.28 170.40
4/23/2019 19.61 0.26 170.22
10/31/2019 20.89 0.55 169.19
1/14/2020 20.86 0.45 169.14
2/4/2020 20.37 0.01 169.25
5/1/2023 20.43 0.00 169.18
MW-1 NA
MW7-18 17.5-32.5
MW-3 NA 191.63
177.78
MW7-02 UNABLE TO LOCATE
MW7-12 41.5-44.5 CANNOT ACCESS 194.47 NACANNOT OPEN
MW7-11 19.5-34.5 CANNOT ACCESS 194.61 NACANNOT OPEN
MW7-14 17.0-32.0 CANNOT ACCESS 193.97CANNOT OPEN NA
189.61
MW7-16 18.0-28.0 190.84
T7-1 of T7-7
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
MW7-19 2/25/2014 NA 21.41 0.00 189.28 167.87
2/25/2014 21.52 0.00 169.17
11/13/2014 21.60 0.00 169.09
10/22/2015 21.52 0.00 169.17
10/25/2016 20.71 0.00 169.98
10/26/2017 21.62 0.01 169.08
2/20/2018 22.10 0.08 168.66
8/25/2018 21.65 0.00 169.04
4/23/2019 20.55 0.00 170.14
10/31/2019 21.39 0.00 169.30
1/14/2020 21.28 0.00 169.41
4/28/2023 21.25 0.00 169.442/25/2014 18.20 0.00 168.99
11/13/2014 18.30 0.00 168.89
10/22/2015
11/13/2014 23.30 0.00 166.28
10/22/2015 23.32 0.00 166.26
10/25/2016 22.70 0.00 166.8810/26/2017 23.44 0.00 166.14
2/5/2019 22.40 0.00 167.18
4/24/2019 22.50 0.00 167.08
4/27/2023 22.80 0.00 166.78
3/4/2014 17.0-32.0 19.40 0.00 190.93 171.53
11/15/2014
MW7-24 3/4/2014 16.0-31.0 20.39 0.00 191.03 170.64
2/25/2014 21.06 0.00
11/13/2014 22.39 0.00
4/23/2019 21.25 0.00
4/28/2023 15.07 2.12
10/22/2015 21.91 1.08 171.82
2/10/2016 21.00 0.72 172.42
5/3/2016 21.01 0.38 172.12
8/10/2016 21.3 0.52 171.95
10/25/2016 20.26 0.26 172.76
2/15/2017 20.95 0.49 172.27
10/26/2017 20.98 0.59 172.33
2/20/2018 22.36 0.91 171.228/25/2018 21.69 0.67 171.68
10/22/2015 20.85 0.00 171.73
10/25/2016 19.8 0.00 172.78
10/26/2017 20.77 0.00 171.81
10/22/2015 20.21 0.00
10/25/2016 19.03 0.0010/26/2017 20.25 0.00
2/25/2014 20.95 0.00 169.66
11/13/2014 20.99 0.00 169.62
10/22/2015 21.00 0.00 169.61
10/25/2016 20.08 0.00 170.53
10/26/2017 20.96 0.00 169.65
2/5/2019 19.30 0.00 171.31
5/1/2023 20.34 0.01 170.28
PT-2 NA NA NA
MW7-22 NA 189.58
NA 187.19
Has been sealed around manhole with asphalt
MW7-21
192.80NARW-A
192.58NARW-B
NA
RW-03
NANARW-C
MW7-23 UNABLE TO LOCATE
20.6-25.6 190.61
MW7-20 NA 190.69
T7-2 of T7-7
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
11/18/2013 21.20 1.50 170.74
2/25/2014 21.91 1.83 170.31
5/20/2014 20.52 0.84 170.85
8/20/2014 20.65 0.65 170.56
11/13/2014 20.72 0.60 170.44
2/18/2015 20.69 0.63 170.50
5/13/2015 20.33 0.61 170.84
8/18/2015 20.69 0.68 170.54
10/22/2015 20.50 0.40 170.49
2/10/2016 20.91 0.55 170.21
5/3/2016 20.17 0.45 170.87
8/10/2016 20.30 0.37 170.6710/25/2016 19.40 0.26 171.47
2/15/2017 19.91 0.24 170.95
5/17/2017 20.40 0.20 170.42
8/15/2017 20.03 0.23 170.82
10/26/2017 20.42 0.24 170.44
2/20/2018 21.00 0.37 169.978/25/2018 20.98 0.38 170.00
2/5/2019 19.12 0.37 171.85
4/23/2019 19.18 0.23 171.67
10/31/2019 20.38 0.45 170.66
1/14/2020 20.08 0.03 170.60
2/4/2020 19.98 0.00 170.67
5/1/2023 20.14 0.04 170.54
2/25/2014 19.46 0.19 169.85
5/20/2014 19.05 0.08 170.17
8/20/2014 19.23 0.02 169.94
11/13/2014 19.34 0.01 169.82
2/18/2015 19.43 0.00 169.72
5/13/2015 19.07 0.00 170.08
8/18/2015 19.41 0.00 169.74
10/22/2015 19.75 0.00 169.40
2/10/2016 18.67 0.00 170.48
5/3/2016 -
8/10/2016 19.19 0.00 169.96
10/25/2016 18.32 0.00 170.8310/26/2017 19.31 0.00 169.84
2/20/2018 19.81 0.02 169.36
8/25/2018 19.33 0.02 169.84
2/5/2019 17.91 0.00 171.24
4/23/2019 18.06 0.00 171.09
5/1/2023 19.14 0.01 170.023/4/2014 19.77 0.00 170.37
11/13/2014 19.73 0.00 170.41
10/22/2015 19.44 0.00 170.70
10/25/2016 18.48 0.00 171.66
10/26/2017 19.46 0.00 170.68
2/5/2019 18.05 0.00 172.09
4/30/2023 19.35 0.00 170.79
11/18/2013 19.63 0.01 169.98
3/4/2014 19.99 0.00 169.61
5/20/2014 19.42 0.00 170.18
8/20/2014 19.89 0.00 169.71
11/13/2014 20.00 0.00 169.60
2/18/2015 19.10 0.00 170.50
5/13/2015 19.51 0.00 170.09
8/18/2015 19.82 0.00 169.78
10/22/2015 19.77 0.00 169.83
2/9/2016 18.70 0.00 170.90
5/3/2016 18.64 0.00 170.96
10/25/2016 18.96 0.21 170.822/15/2017 19.31 0.04 170.32
5/17/2017 19.84 0.05 169.80
8/15/2017 19.32 0.00 170.28
10/26/2017 19.86 0.21 169.92
2/5/2019 18.35 0.00 171.25
4/24/2019 18.23 0.00 171.374/30/2023 NA
11/13/2014 19.83 0.00 170.41
10/22/2015 19.50 0.00 170.74
10/25/2016 18.69 0.00 171.55
10/26/2017 20.11 0.00 170.13
2/20/2018 20.13 0.00 170.11
8/25/2018 19.64 0.00 170.60
2/5/2019 18.23 0.00 172.01
4/24/2019 18.45 0.00 171.79
4/30/2023 NA
11/18/2013 19.02 0.02 171.25
3/4/2014 19.31 0.06 170.99
RW-05 COULD NOT ACCESS WELLNA 189.15
RW-04 NA 190.65
RW-08 18.43-23.43 190.14
RW-09 18.0-23.0 189.60
RW-10 16.97-26.97 190.24
Inaccessible
Inaccessible
T7-3 of T7-7
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
5/20/2014 19.85 0.01 170.41
8/20/2014 19.38 0.28 171.11
11/13/2014 20.37 1.16 170.88
2/18/2015 19.29 0.20 171.13
5/13/2015 18.90 0.00 171.35
8/18/2015 19.74 0.38 170.84
10/22/2015 19.81 0.79 171.12
2/10/2016 18.41 0.02 171.86
5/3/2016 18.81 0.00 171.44
8/10/2016 19.00 0.00 171.25
10/25/2016 18.32 0.14 172.05
2/15/2017 18.58 0.00 171.675/17/2017 19.36 0.00 170.89
8/15/2017 18.68 0.00 171.57
10/26/2017 19.12 0.01 171.14
2/20/2018 19.73 0.04 170.55
8/25/2018 19.18 0.00 171.07
2/5/2019 17.58 0.00 172.674/24/2019 17.79 0.00 172.46
4/30/2023 NA
RW-11 NA 190.25
Inaccessible
T7-4 of T7-7
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
3/4/2014 19.49 0.00 171.21
11/13/2014 19.48 0.00 171.22
10/22/2015 19.63 0.00 171.07
10/25/2016 18.38 0.00 172.32
10/26/2017 19.32 0.00 171.38
2/5/2019 18.00 0.00 172.70
4/24/2019 18.04 0.00 172.66
4/30/2023 19.46 0.01 171.25
3/4/2014 19.69 0.00 170.74
11/19/2014 19.74 0.00 170.69
10/22/2015 19.47 0.00 170.96
10/25/2016 18.50 0.00 171.9310/26/2017 19.51 0.00 170.92
2/5/2019 17.50 0.00 172.93
4/24/2019 18.70 0.00 171.73
4/30/2023 NA
11/13/2014 19.5 0.23 170.90
2/18/2015 19.00 0.00 171.205/13/2015 18.75 0.00 171.45
8/18/2015 19.16 0.00 171.04
10/22/2015 19.11 0.00 171.09
2/10/2016 18.40 0.00 171.80
5/3/2016 18.35 0.00 171.85
8/10/2016 18.93 0.00 171.27
10/25/2016 18.09 0.00 172.11
10/26/2017 19.11 0.00 171.09
2/5/2019 17.55 0.00 172.65
4/24/2019 17.81 0.00 172.39
4/30/2023 NA
3/4/2014 20.29 0.00 170.70
11/19/2014 20.27 0.00 170.72
10/22/2015 20.03 0.00 170.96
10/25/2016 19.16 0.00 171.83
10/26/2017 19.97 0.00 171.02
2/5/2019 18.60 0.00 172.39
4/24/2019 18.74 0.00 172.25
4/30/2023 19.85 0.00 171.143/4/2014 20.05 0.00 171.19
11/19/2014 20.08 0.00 171.16
10/22/2015 20.00 0.00 171.24
10/25/2016 19.05 0.00 172.19
10/26/2017 20.03 0.00 171.21
4/24/2019 18.83 0.00 172.414/30/2023 19.99 0.00 171.25
3/4/2014 20.05 0.00 171.58
11/19/2014 19.71 0.00 171.92
10/22/2015 19.94 0.00 171.69
10/25/2016 19.03 0.00 172.60
10/26/2017 19.62 0.00 172.01
2/5/2019 18.49 0.00 173.14
4/24/2019 18.70 0.00 172.93
5/1/2023 20.05 0.00 171.58
3/4/2014 21.10 0.11 171.09
5/20/2014 20.50 0.05 171.64
8/20/2014 20.91 0.13 171.30
11/19/2014 21.16 0.22 171.13
2/18/2015 20.89 0.01 171.22
5/13/2015 20.41 0.00 171.69
8/18/2015 20.86 0.00 171.24
10/22/2015 20.92 0.16 171.32
2/10/2016 20.66 0.00 171.44
5/3/2016 20.41 0.08 171.768/10/2016 20.75 0.18 171.50
10/25/2016 19.81 0.00 172.29
2/15/2017 20.95 0.49 171.57
5/17/2017 21.15 0.60 171.46
8/15/2017 20.46 0.00 171.64
10/26/2017 20.98 0.22 171.312/20/2018 21.96 0.74 170.77
8/25/2018 20.92 0.02 171.20
2/5/2019 20.42 0.00 171.68
RW-21 4/24/2019
RW-22 2/25/2014 NA 188.44 NA
4/28/2023 NA 19.95 0.00 188.88 168.93
TW7-04 2/25/2014 15.0-35.0 21.56 0.00 188.64 167.08
3/4/2014 21.85 0.00 171.27
11/19/2014 20.29 0.00 172.83
10/22/2015 21.76 0.00 171.36
10/25/2016 20.68 0.00 172.44
TW7-03 Abandoned After 2023 Sampling Event
RW-16 17.0-27.0 190.99
RW-18 18.0-28.0 191.63
RW-20 18.0-28.0 192.10
CANNOT ACCESS
TW7-07 15.0-35.0 193.12
ABANDONED
RW-12 NA 190.70
RW-17 18.0-28.0 191.24
Inaccessible
RW-14 NA 190.20
RW-13 NA 190.43
Inaccessible
T7-5 of T7-7
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
10/26/2017 21.71 0.00 171.41
4/30/2023 NA
3/4/2014
11/13/2014
MW-308A** 4/30/2023 NA 21.51 1.62 NA NA
MW-308E 4/28/2023 NA 15.08 0.01 NA NA
MW-308F 4/28/2023 NA 15.08 2.10 NA NA
MW-308G 4/28/2023 NA 12.51 0.00 NA NA
MW-308H 4/28/2023 NA 12.15 0.00 NA NA
NACANNOT OPENTW7-08 15.0-35.0 CANNOT ACCESS 193.56
Inaccessible
T7-6 of T7-7
Table 7FTBR-308Current and Historical Groundwater Elevations and Free Product Thickness
Well ID # Date
Screened Interval (top of screen,
bottom of screen)
Depth to Water* Uncorrected
(feet)
Free Product Thickness
(feet)
Top of Casing Elevation
(MSL)
Groundwater Surface
Elevation (MSL)
MW-2 11/17/2014
MW-4 11/17/2014
MW7-01 11/14/2014
11/17/2014
4/23/2019 NA 19.12 0.00 NA NA
MW7-09 11/14/2014
MW7-10 11/14/2014
MW7-13 11/13/2014
MW7-15 11/13/2014
11/13/2014
2/5/2019 NA 18.64 0.00 NA NA
RW-01 11/15/2014RW-02 11/15/2014
RW-06 11/15/2014
RW-07 11/15/2014
RW-15 11/14/2014
RW-19 11/13/2014
RW-21 2/25/2014RW-23 11/13/2014
RW-24 11/13/2014
RW-25 11/13/2014
RW-26 11/13/2014
RW-27 11/13/2014
RW-28 11/13/2014
RW-29 11/13/2014
TW7-01 11/14/2014
TW7-02 11/13/2014
TW7-03 11/17/2014
TW7-05 11/15/2014
TW7-06 11/13/2014
TW7-09 11/13/2014
**1-inch well
NA = not available.
MW7-17
MW7-03
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONEDABANDONED
ABANDONED
ABANDONEDABANDONED
Notes:
Depths are measured from the Top of Well Casing (TOC). MSL - mean sea level
*Depth to Water is measured from Top of Casing and corrected for Free Product Thickness: Groundwater Elevation (ft AMSL) = Top of Casing (ft AMSL) - Depth to Water (ft) + Free Product Thickness*0.8581 (ft)
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONEDABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
ABANDONED
T7-7 of T7-7
Table 8Analytical Data SummaryFTBR-308T8-1 of T8-3Lab ID:680-234331-4 680-243331-1 680-234374-5 680-243331-3 680-234331-6 680-234331-5 680-234374-4 680-234374-2 680-234374-3 680-234374-1Client ID:MW1-04-23 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22-04-23 TW7-03-04-23 RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-04-23Sampled Date:4/28/2023 4/28/2023 5/1/2023 4/28/2023 4/28/2023 4/28/2023 5/1/2023 5/1/2023 5/1/2023 5/1/20231,1,1,2-Tetrachloroethane1 1,000 ND ND NA NDNDND NA NA NA NA1,1,1-Trichloroethane200 200,000 ND ND ND NDNDND ND ND ND ND1,1,2,2-Tetrachloroethane0.2 200 ND ND ND NDNDND ND ND ND ND1,1,2-Trichloroethane0.6 600 ND ND ND NDNDND ND ND ND ND1,1-Dichloroethane6 6,000 ND ND ND NDNDND ND ND ND ND1,1-Dichloroethene350 350,000 ND ND ND NDNDND ND ND ND ND1,2,3-TrichlorobenzeneNE NE ND ND NA NDNDND NA NA NA NA1,2,3-Trichloropropane0.005 NE ND ND NA NDNDND NA NA NA NA1,2,3-TrimethylbenzeneNE NE ND ND NA11 Q26 Q69 QDNA NA NA NA1,2,4-Trichlorobenzene70 24,500 ND ND ND NDNDND ND ND ND ND1,2,4-Trimethylbenzene400 28,500 ND NDNA4453 130 J1DNA NA NA NA1,2-Dibromo-3-Chloropropane0.0002 NE ND ND ND NDNDND ND ND ND ND1,2-Dichlorobenzene20 20,000 ND ND ND NDNDND ND ND ND ND1,2-Dichloroethane0.4 400 ND ND ND NDNDND ND ND ND ND1,2-Dichloropropane0.6 600 ND ND ND NDNDND ND ND ND ND1,3,5-Trimethylbenzene400 24,100 ND ND NA ND1437 J1DNA NA NA NA1,3-Dichlorobenzene200 61,500 ND ND ND NDNDND ND ND ND ND1,3-Dichloropropane0.4 NE NDNDNDNDNDND ND ND ND ND1,4-Dichlorobenzene6 405 ND ND ND NDNDND ND ND ND ND2,2-DichloropropaneNE NE ND ND NA NDNDND NA NA NA NA2-Butanone (MEK)4,0004,000,000NDNDNDNDNDNDNDNDNDND2-Chloroethyl vinyl etherNENENDNDNANDNDNDNANANANA2-ChlorotolueneNENENDNDNANDNDNDNANANANA2-Hexanone4040,000NDNDNANDNDNDNANANANA2-Methylnaphthalene3012,000ND35 QNA6.7 JQ13 Q24 QDNANANANA2-NitropropaneNENENDNDNANDND2.7 JQDNANANANA4-Chlorotoluene2424,000NDNDNANDNDNDNANANANA4-Isopropyltoluene (p-Isopropultoluene)2511,700NDNDNA1.9 J1.3 J2.7 JDNANANANA4-Methyl-2-pentanone (MIBK)100100,000NDNDNDNDNDNDNDNDNDNDAcetone6,0006,000,000ND9.9 JQNDNDND10 JQDNDNDNDNDAcetonitrileNENEND210 QMNAND310 QM140 QDMNANANANAAcrolein4NEND34 JNA23 JNDNDNANANANAAllyl ChlorideNENENDNDNANDND9.6 JDNANANANABenzene15,000ND6.51300 D4.54613 D208.724 D0.66 JBromobenzeneNENENDNDNANDNDNANANANANABromoform44,000NDNDNDNDNDNDNDNDNDNDBromomethane10100,000NDNDNDNDNDNDNDNDNDNDCarbon disulfide700550,0000.71 JNDND0.79 J0.68 JNDNDNDNDNDCarbon tetrachloride0.3 NE NDNDNDNDNDNDNDNDNDNDChlorobenzene5050,000NDNDNDNDNDNDNDNDNDNDChlorobromomethaneNENENDNDNDNDNDNANDNDNDNDChlorodibromomethane0.4 NE NDNDNDNDNDNDNDNDNDNDChloroethane3,000NENDNDNDNDNDNDNDNDNDNDChloroform7070,000NDNDNDNDNDNDNDNDNDNDChloromethane33,000NDNDNDNDNDNDNDNDNDNDcis-1,2-Dichloroethene7070,000NDNDNDNDNDNDNDNDNDNDcis-1,3-Dichloropropene0.4400NDNDNDNDNDNDNDNDNDNDCyclohexaneNENE0.69 J16083 JDQ6.33223 J1D 8.5 Q76 Q76 DQ25 QDibromomethaneNENENDNDNANDNDNDNANDNANDDichlorobromomethaneNENENDNDNDNDNDNDNDNDNDNDDichlorodifluoromethane1,000140,000NDNDNDNDNDNDNDNDNDNDEthylbenzene60080,000ND6.0300 D4.43.240 J1D1.161220 D6.3Ethylene Dibromide0.0250NDNDNANDNDNDNANANANAHexachlorobutadiene0.4400NDNDNANDNDNDNANANANAHexane400NENDNDNAND1713 DNANANANAHeptane400NENDNDNANDND2.4 JDNANANANAIsopropylbenzene7030,5000.51 J31ND115.912 J1DND1624 D11Methyl tert-butyl ether2020,000NDNDNDNDNDNDNDNDNDNDMethylcyclohexaneNENEND8535 JDM2.51212 D2.64651 D45Methylene Chloride55,000NDNDNDNDNDNDNDNDNDND15A NCAC 02L GWQS (µg/L)Volatile Organic Compounds by EPA Method 8260 ( µg/L )Gross Contaminant Level (µg/L)
Table 8Analytical Data SummaryFTBR-308T8-2 of T8-3Lab ID:680-234331-4 680-243331-1 680-234374-5 680-243331-3 680-234331-6 680-234331-5 680-234374-4 680-234374-2 680-234374-3 680-234374-1Client ID:MW1-04-23 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22-04-23 TW7-03-04-23 RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-04-23Sampled Date:4/28/2023 4/28/2023 5/1/2023 4/28/2023 4/28/2023 4/28/2023 5/1/2023 5/1/2023 5/1/2023 5/1/202315A NCAC 02L GWQS (µg/L)Gross Contaminant Level (µg/L)m-Xylene & p-XyleneNE NE ND NDNAND130 210 J1DNA NA NA NANaphthalene6 6,000 ND110NA1.9 J36ND NA NA NA NAn-Butylbenzene70 5,900 ND ND NA NDND4.5 JDNA NA NA NAn-Propylbenzene70 26,100 ND26NA111.1 JND NA NA NA NAo-XyleneNE NE ND0.29 JNA ND9.26.7 DNA NA NA NAsec-Butylbenzene70 8,8000.67 J 4.7NA4.02.2 J 2.5 JDNA NA NA NAStyrene70 70,000 ND ND NA NDNDND NA NA NA NAtert-Butylbenzene70 14,750 ND1.3 JNA0.95 J0.54 JND NA NA NA NATetrachloroethene0.7 700 ND ND ND NDNDND ND ND ND NDToluene600 260,000 ND ND1400 DND1.0 J1.6 JD 0.32 J 4.7 120 D 2.5trans-1,2-Dichloroethene100 100,000 ND ND ND NDNDND ND ND ND NDtrans-1,3-Dichloropropene0.4 400 ND ND ND NDNDND ND ND ND NDTrichloroethene3 3,000 ND ND ND NDNDND ND ND ND NDTrichlorofluoromethane2,000 550,000 ND ND ND NDNDND ND ND ND NDVinyl acetate88 88,000 ND ND ND NDNDND NA NA NA NAVinyl chloride0.03 30 ND ND ND NDNDND ND ND ND NDXylenes, Total500 50,000 ND ND1500 DND140 220 J1D 27 360 D980 D331,1'-Biphenyl400 NE ND ND ND ND ND ND ND ND ND ND2,4,5-Trichlorophenol63 NE ND ND ND ND ND ND ND ND ND ND2,4,6-Trichlorophenol4 NE NDNDNDNDNDNDNDNDNDND2,4-Dichlorophenol0.98 980 ND ND ND ND ND ND ND ND ND ND2,4-Dimethylphenol100 100,000 ND ND ND ND ND ND ND ND ND ND2,4-DinitrophenolNENENDNDNDNDNDNDNDNDNDND2,4-Dinitrotoluene0.1NE NDNDNDNDNDNDNDNDNDND2,6-DinitrotolueneNENENDNDNDNDNDNDNDNDNDND2-ChloronaphthaleneNENENDNDNDNDNDNDNDNDNDND2-Chlorophenol0.4 NE NDNDNDNDNDNDNDNDNDND2-Methylnaphthalene3012,000ND20433.6 JNDNDND14 J33272-MethylphenolNE400,000NDNDNDNDNDNDNDNDNDND2-NitroanilineNENENDNDNDNDNDNDNDNDNDND2-NitrophenolNENENDNDNDNDNDNDNDNDNDND3 & 4 MethylphenolNENENDNDNDNDNDNDNDNDNDND3,3'-DichlorobenzidineNENENDNDNDNDNDNDNDNDNDND3-NitroanilineNENENDNDNDNDNDNDNDNDNDND4,6-Dinitro-2-methylphenolNENENDNDNDNDNDNDNDNDNDND4-Bromophenyl phenyl etherNENENDNDNDNDNDNDNDNDNDND4-Chloro-3-methylphenolNENENDNDNDNDNDNDNDNDNDND4-Chloroaniline0.37NENDNDNDNDNDNDNDNDNDND4-Chlorophenyl phenyl etherNENENDNDNDNDNDNDNDNDNDND4-NitroanilineNENENDNDNDNDNDNDNDNDNDND4-NitrophenolNENENDNDNDNDNDNDNDNDNDNDAcenaphthene801,950NDNDNDNDNDNDNDNDNDNDAcenaphthylene2008,000NDNDNDNDNDNDNDNDNDNDAcetophenone700NENDNDNDNDNDNDNDNDNDNDAnthracene2,0002,000NDNDNDNDNDNDNDNDNDNDAtrazine3 NE NDNANANANDNDNDNDNDNDBenzaldehyde700NENDNANANANDNDNDNDNDNDBenzo[a]anthracene0.05 4.7 NDNDNDNDNDNDNDNDNDNDBenzo[a]pyrene0.005 0.8 NDNDNDNDNDNDNDNDNDNDBenzo[b]fluoranthene0.050.75NDNDNDNDNDNDNDNDNDNDBenzo[g,h,i]perylene200200NDNDNDNDNDNDNDNDNDNDBenzo[k]fluoranthene0.50.5NDNDNDNDNDNDNDNDNDNDbis (2-chloroisopropyl) etherNENENDNDNDNDNDNDNDNDNDNDBis(2-chloroethoxy)methaneNENENDNDNDNDNDNDNDNDNDNDBis(2-chloroethyl)ether0.0330NDNDNDNDNDNDNDNDNDNDBis(2-ethylhexyl) phthalate3135NDND6.3 JBNDNDNDND6.3 JB 6.3 JB6.4 JBButyl benzyl phthalate1,000NENDNDNDNDNDNDNDNDNDNDCaprolactam4,000NENDNDNDNDNDNDNDNDNDNDCarbazole2 NE NDNDNDNDNDNDNDNDNDNDChrysene55NDNDNDNDNDNDNDNDNDNDSemi-volatile Organic Compound by EPA Method 8270 (µg/L )
Table 8Analytical Data SummaryFTBR-308T8-3 of T8-3Lab ID:680-234331-4 680-243331-1 680-234374-5 680-243331-3 680-234331-6 680-234331-5 680-234374-4 680-234374-2 680-234374-3 680-234374-1Client ID:MW1-04-23 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22-04-23 TW7-03-04-23 RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-04-23Sampled Date:4/28/2023 4/28/2023 5/1/2023 4/28/2023 4/28/2023 4/28/2023 5/1/2023 5/1/2023 5/1/2023 5/1/202315A NCAC 02L GWQS (µg/L)Gross Contaminant Level (µg/L)Dibenz(a,h)anthracene0.005 1.2 NDNDNDNDNDNDNDNDNDNDDibenzofuran28 1,550 ND ND ND ND ND ND ND ND ND NDDiethyl phthalate6,000 NE ND ND ND ND ND ND ND ND ND NDDimethyl phthalateNE NE ND ND ND ND ND ND ND ND ND NDDi-n-butyl phthalate700 NE ND ND ND ND ND ND ND ND ND NDDi-n-octyl phthalate100 NE ND ND ND ND ND ND ND ND ND NDFluoranthene300 300 ND ND ND ND ND ND ND ND ND NDFluorene300 845 ND ND ND ND ND ND ND ND ND NDHexachlorobenzene0.02 NE ND ND ND ND ND ND ND ND ND NDHexachlorocyclopentadieneNE NE ND ND ND ND ND ND ND ND ND NDHexachloroethaneNE NE ND ND ND ND ND ND ND ND ND NDIndeno[1,2,3-cd]pyrene0.05 0.095 ND ND ND ND ND ND ND ND ND NDIsophorone40 NE ND ND ND ND ND ND ND ND ND NDNaphthalene6 6,000 ND6.9 JHQ 110 17 Q1.3 JHQ3.5 JHQND28 544.0 JNitrobenzeneNE NE ND ND ND ND ND ND ND ND ND NDN-Nitrosodi-n-propylamineNE NE ND ND ND ND ND ND ND ND ND NDN-Nitrosodiphenylamine0.0007 NE ND ND ND ND ND ND ND ND ND NDPentachlorophenol0.3 300 ND ND ND ND ND ND ND ND ND NDPhenanthrene200 550 ND ND ND ND ND ND ND ND ND NDPhenol30 30,000 ND ND ND ND ND ND ND ND ND NDPyrene200 200 ND ND ND ND ND ND ND ND ND NDC5-C8 Aliphatics (x) 400 NEND1,100 5,500 DM 100550 M340 DMJ1 340 M980 M 1,600 M 580 MC9-C10 Aromatics (c) NE NE16 JM 380 1,200 JDM 180150 M450 DMJ1 110 M 460 M 590 JDM 770 MC9-C12 Aliphatics (a) NE NE32 JM 820 4,500 DM 340540 M 1,100 DMJ1 360 M 1,300 DM 2,100 DM 1,300 DMC11-C22 Aromatics (d) NE NEND270 270 M 12 J48 MH 110 MH 16 JHM 92 HM 220 M 160 MHC19-C36 Aliphatics (y) 10,000 NEND ND ND NDND11 JMHND ND12 JMNDC9-C18 Aliphatics (b) NE NEND580 B 340 BQ 17 JB52 HB150 MHBJ1 50 HB 160 HB 340 MBQ 110 HBC9-C18 Aliphatics (a+b)700 NE32 JM1,400 4,840 DMBQ 357592 MH1,250 DMHJ1 410 HMB 1,460 DHBM 2,440 DMBQ 1,410 DMBQC9-C22 Aromatics (c+d)200 NE16 JM650 1,470 JDM192198 MHB495 DMJ1126 HMB552 HM 810 JDMBQ 910 DMBQNotes:B: Contamination in a blank sample was detectedD: Dilution of sample requiredH: Sample was prepped or analyzed beyond the specified holding timeJ: Estimated: The analyte was positively identified; the quantitation is an estimationJ1 = The quantitation is an estimation due to discrepencies in meeting certain analyte-specific quality control criteriaM :Manual integrated compound.Q: One or more quality control criteria failedµg/L: micrograms per literNA: Not analyzedND: Not DetectedNE: Not Established: if GCL is NE, the NC2L is the applicable standard.NCDEQ MADEP Table 11 Worksheet (Rev0421) (µg/L)MADEP VPH ( µg/L )MADEP EPH ( µg/L )
Table 9FTBR-308Historical DataT6-1 of T6-8FTBR308-MW-1-4-19MW1-04-23 MW-3-4-19 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22 MW7-22-4-19 MW7-22-04-234/24/2019 4/28/20234/24/20194/28/2023 5/1/2023 4/28/2023 2/25/20144/24/20194/28/2023680-168158-2 680-234331-4680-168158-3680-243331-1 680-234374-5 680-243331-3 N21402262401680-168158-4680-243331-61,1,1,2-Tetrachloroethane1 1,000 ND ND ND ND NA ND NA NDND1,1,1-Trichloroethane200 200,000 ND ND ND ND ND ND ND NDND1,1,2,2-Tetrachloroethane0.2 200 ND ND ND ND ND ND ND NDND1,1,2-Trichloroethane0.6 600 ND ND ND ND ND ND ND NDND1,1-Dichloroethane6 6,000 ND ND ND ND ND ND ND NDND1,1-Dichloroethene350 350,000 ND ND ND ND ND ND ND NDND1,2,3-TrichlorobenzeneNE NE ND ND ND ND NA ND2.1NDND1,2,3-Trichloropropane0.005 NE ND ND ND ND NA ND ND NDND1,2,3-TrimethylbenzeneNE NE ND ND ND ND NA11 QNA ND26 Q1,2,4-Trichlorobenzene70 24,500 ND ND ND ND ND ND ND NDND1,2,4-Trimethylbenzene400 28,500 ND ND ND NDNA44 29.2 2.4531,2-Dibromo-3-Chloropropane0.0002 NE ND ND ND ND ND ND NA NDND1,2-Dichlorobenzene20 20,000 ND ND ND ND ND ND ND NDND1,2-Dichloroethane0.4 400 ND ND ND ND ND ND ND NDND1,2-Dichloropropane0.6 600 ND ND ND ND ND ND ND NDND1,3,5-Trimethylbenzene400 24,100 ND ND ND ND NA ND5.05ND141,3-Dichlorobenzene200 61,500 ND ND ND ND ND ND ND NDND1,3-Dichloropropane0.4 NE ND NDNDNDNDNDNDNDND1,4-Dichlorobenzene6 405 ND ND ND ND ND ND ND NDND2,2-DichloropropaneNE NE ND ND ND ND NA ND ND NDND2-Butanone (MEK)4,000 4,000,000 ND ND ND ND ND ND ND NDND2-Chloroethyl vinyl etherNE NE ND ND ND ND NA ND NA NDND2-ChlorotolueneNE NE ND ND ND ND NA ND NA NDND2-Hexanone40 40,000 ND ND ND ND NA ND ND NDND2-Methylnaphthalene30 12,000 NA ND NA35 QNA6.7 JQNA NA13 Q2-NitropropaneNENENANDNANDNANDNANAND4-Chlorotoluene2424,000NDNDNDNDNANDNDNDND4-Isopropyltoluene (p-Isopropultoluene)2511,700NDNDNDNDNA1.9 J 0.644 JND1.3 J4-Methyl-2-pentanone (MIBK)100100,000NDNDNDNDNDNDNDNDNDAcetone6,0006,000,00023NDND9.9 JQNDNDNDNDNDAcetonitrileNENENDNDND210 QMNANDNDND310 QMAcrolein4NENANDNA34 JNA23 JNDNANDAllyl ChlorideNENENANDNANDNANDNDNANDBenzene15,000NDND356.51300 D4.580.99.646BromobenzeneNENENDNDNDNDNANDNDNDNDBromoform44,000NDNDNDNDNDNDNDNDNDBromomethane10100,000NDNDNDNDNDNDNDNDNDCarbon disulfide700550,000ND0.71 JNDNDND0.79 JNAND0.68 JCarbon tetrachloride0.3 NE ND NDNDNDNDNDNDNDNDChlorobenzene5050,000NDNDNDNDNDNDNDNDNDChlorobromomethaneNENENDNDNDNDNDNDNANDNDChlorodibromomethane0.4 NE ND NDNDNDNDNDNDNDNDChloroethane3,000NENDNDNDNDNDNDNDNDNDChloroform7070,000NDNDNDNDNDNDNDNDNDChloromethane33,000NDNDNDNDNDNDNDNDNDcis-1,2-Dichloroethene7070,000NDNDNDNDNDNDNDNDNDcis-1,3-Dichloropropene0.4400NDNDNDNDNDNDNDNDNDCyclohexaneNENENA0.69 JNA16083 JDQ6.3NANA32Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant LevelVolatile Organic Compounds by EPA Method 8260 ( µg/L )
Table 9FTBR-308Historical DataT6-2 of T6-8FTBR308-MW-1-4-19MW1-04-23 MW-3-4-19 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22 MW7-22-4-19 MW7-22-04-234/24/2019 4/28/20234/24/20194/28/2023 5/1/2023 4/28/2023 2/25/20144/24/20194/28/2023680-168158-2 680-234331-4680-168158-3680-243331-1 680-234374-5 680-243331-3 N21402262401680-168158-4680-243331-6Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant LevelDibromomethaneNE NE ND ND ND ND NA ND NA NDNDDichlorobromomethaneNE NE ND ND ND ND ND ND NA NDNDDichlorodifluoromethane1,000 140,000 ND ND ND ND ND ND ND NDNDEthylbenzene600 80,000 ND ND17 6.0 300 D 4.4 3.53 0.76 J3.2Ethylene Dibromide0.02 50 ND ND ND ND NA ND NA NDNDHexachlorobutadiene0.4 400 ND ND ND ND NA ND NA NDNDHexane400 NE NA ND NA ND NA ND NA NA17Heptane400 NE NA ND NA ND NA ND NA NANDIsopropylbenzene70 30,500 ND0.51 J 57 31ND11 6.47 1.4 J5.9Methyl tert-butyl ether20 20,000 ND ND ND ND ND ND NA NDNDMethylcyclohexaneNE NE NA ND NA85 35 JDM 2.5NA NA12Methylene Chloride5 5,000 ND ND ND ND ND ND ND NDNDm-Xylene & p-XyleneNE NE ND ND ND NDNAND51.3 4.7130Naphthalene6 6,000 ND ND250 110NA1.9 JNA9.9 J36n-Butylbenzene70 5,900 ND ND6.0ND NA ND0.965 JNDNDn-Propylbenzene70 26,100 ND ND7426NA11 2.12ND1.1 Jo-XyleneNE NE ND ND ND0.29 JNA ND13 2.99.2sec-Butylbenzene70 8,800 ND0.67 J 13 4.7NA4.0 2.13ND2.2 JStyrene70 70,000 ND ND ND ND NA ND ND NDNDtert-Butylbenzene70 14,750 ND ND ND1.3 JNA0.95 J 0.455 JND0.54 JTetrachloroethene0.7 7002.0ND ND ND ND ND ND NDNDToluene600 260,000 ND ND ND ND1400 DND0.985 JND1.0 Jtrans-1,2-Dichloroethene100100,000NDNDNDNDNDNDNDNDNDtrans-1,3-Dichloropropene0.4400NDNDNDNDNDNDNDNDNDTrichloroethene33,000NDNDNDNDNDNDNDNDNDTrichlorofluoromethane2,000550,000NDNDNDNDNDNDNDNDNDVinyl acetate8888,000NDNDNDNDNDNDNDNDNDVinyl chloride0.0330NDNDNDNDNDNDNDNDNDXylenes, Total50050,000NDNDNDND1500 DND64.37.61401,1'-Biphenyl400NENDNDNDNDNDNDNANDND2,4,5-Trichlorophenol63NENDNDNDNDNDNDNANDND2,4,6-Trichlorophenol4 NE ND NDNDNDNDNDNDNDND2,4-Dichlorophenol0.98980NDNDNDNDNDNDNDNDND2,4-Dimethylphenol100100,000NDNDNDNDNDNDNDNDND2,4-DinitrophenolNENENDNDNDNDNDNDNDNDND2,4-Dinitrotoluene0.1 NE ND NDNDNDNDNDNDNDND2,6-DinitrotolueneNENENANDNANDNDNDNDNAND2-ChloronaphthaleneNENENDNDNDNDNDNDNDNDND2-Chlorophenol0.4 NE ND NDNDNDNDNDNDNDND2-Methylnaphthalene3012,000NDND2420433.6 J4.47 JNDND2-MethylphenolNE400,000NDNDNDNDNDNDNDNDND2-NitroanilineNENENDNDNDNDNDNDNANDND2-NitrophenolNENENDNDNDNDNDNDNDNDND3 & 4 MethylphenolNENENDNDNDNDNDNDNANDND3,3'-DichlorobenzidineNENENDNDNDNDNDNDNDNDND3-NitroanilineNENENDNDNDNDNDNDNANDND4,6-Dinitro-2-methylphenolNENENDNDNDNDNDNDNDNDND4-Bromophenyl phenyl etherNENENDNDNDNDNDNDNDNDNDSemi-volatile Organic Compound by EPA Method 8270 (µg/L )
Table 9FTBR-308Historical DataT6-3 of T6-8FTBR308-MW-1-4-19MW1-04-23 MW-3-4-19 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22 MW7-22-4-19 MW7-22-04-234/24/2019 4/28/20234/24/20194/28/2023 5/1/2023 4/28/2023 2/25/20144/24/20194/28/2023680-168158-2 680-234331-4680-168158-3680-243331-1 680-234374-5 680-243331-3 N21402262401680-168158-4680-243331-6Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant Level4-Chloro-3-methylphenolNE NE ND ND ND ND ND ND ND ND ND4-Chloroaniline0.37NENDNDNDNDNDNDNDNDND4-Chlorophenyl phenyl etherNENENDNDNDNDNDNDNDNDND4-NitroanilineNENENDNDNDNDNDNDNDNDND4-NitrophenolNENENDNDNDNDNDNDNDNDNDAcenaphthene801,950NDNDNDNDNDNDNDNDNDAcenaphthylene2008,000NDNDNDNDNDNDNDNDNDAcetophenone700NENDNDNDNDNDNDNANDNDAnthracene2,0002,000NDNDNDNDNDNDNDNDNDAtrazine3 NE ND NDNDNANANANANDNDBenzaldehyde700NENDNDNDNANANANANDNDBenzo[a]anthracene0.05 4.7 ND NDNDNDNDNDNDNDNDBenzo[a]pyrene0.005 0.8 ND NDNDNDNDNDNDNDNDBenzo[b]fluoranthene0.050.75NDNDNDNDNDNDNDNDNDBenzo[g,h,i]perylene200200NDNDNDNDNDNDNDNDNDBenzo[k]fluoranthene0.50.5NDNDNDNDNDNDNDNDNDbis (2-chloroisopropyl) etherNENENDNDNDNDNDNDNDNDNDBis(2-chloroethoxy)methaneNENENDNDNDNDNDNDNANDNDBis(2-chloroethyl)ether0.0330NDNDNDNDNDNDNDNDNDBis(2-ethylhexyl) phthalate3135NDNDNDND6.3 JBNDNDNDNDButyl benzyl phthalate1,000NENDNDNDNDNDNDNANDNDCaprolactam4,000NENDNDNDNDNDNDNANDNDCarbazole2 NE ND NDNDNDNDNDNANDNDChrysene55NDNDNDNDNDNDNDNDNDDibenz(a,h)anthracene0.005 1.2 ND NDNDNDNDNDNDNDNDDibenzofuran281,550NDNDNDNDNDNDNDNDNDDiethyl phthalate6,000NENDNDNDNDNDNDNDNDNDDimethyl phthalateNENENDNDNDNDNDNDNDNDNDDi-n-butyl phthalate700NENDNDNDNDNDNDNDNDNDDi-n-octyl phthalate100NENDNDNDNDNDNDNDNDNDFluoranthene300300NDNDNDNDNDNDNDNDNDFluorene300845NDNDNDNDNDNDNDNDNDHexachlorobenzene0.02NENDNDNDNDNDNDNDNDNDHexachlorocyclopentadieneNENENDNDNDNDNDNDNDNDNDHexachloroethaneNENENDNDNDNDNDNDNDNDNDIndeno[1,2,3-cd]pyrene0.050.095NDNDNDNDNDNDNDNDNDIsophorone40NENDNDNDNDNDNDNDNDNDNaphthalene66,000NANDNA6.9 JHQ 11017 Q25.4NA1.3 JHQNitrobenzeneNENENDNDNDNDNDNDNDNDNDN-Nitrosodi-n-propylamineNENENDNDNDNDNDNDNDNDNDN-Nitrosodiphenylamine0.0007NENDNDNDNDNDNDNDNDNDPentachlorophenol0.3300NDNDNDNDNDNDNDNDNDPhenanthrene200550NDNDNDNDNDNDNDNDNDPhenol3030,000NDNDNDNDNDNDNDNDNDPyrene200200NDNDNDNDNDNDNDNDNDC5-C8 Aliphatics (x)400NENDND1,4001,100 5,500 DM 100574150550 MC9-C10 Aromatics (c)NENEND16 JM440380 1,200 JDM 180264100150 MC9-C12 Aliphatics (a)NENEND32 JM640820 4,500 DM 340574160540 MMADEP VPH ( µg/L )
Table 9FTBR-308Historical DataT6-4 of T6-8FTBR308-MW-1-4-19MW1-04-23 MW-3-4-19 MW7-16-04-23 MW7-18-05-23 MW7-20-04-23 MW7-22 MW7-22-4-19 MW7-22-04-234/24/2019 4/28/20234/24/20194/28/2023 5/1/2023 4/28/2023 2/25/20144/24/20194/28/2023680-168158-2 680-234331-4680-168158-3680-243331-1 680-234374-5 680-243331-3 N21402262401680-168158-4680-243331-6Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant LevelC11-C22 Aromatics (d)NENENDND270 M270270 M12 J106ND48 MHC19-C36 Aliphatics (y)10,000NENDNDNDNDNDNDNDNDNDC9-C18 Aliphatics (b)NENE53 JMND780 M580 B 340 BQ 17 JBND110 M 52 HBC9-C18 Aliphatics (a+b)700NE53 JM32 JM1,420 M1,400 4,840 DMBQ 357574270 M 592 MHC9-C22 Aromatics (c+d)200NEND16 JM710 M650 1,470 JDM192370100 198 MHBNotes:Bolded value = detectable concentration.Red value = an NC 2L Groundwater Standard exceedance.NA = Not Analyzed; NE = Not Established; ND = Not DetectedJ = Analyte positively identified, concentration estimatedB = Analyte was detected in a blankQ = LCS/LCSD recovery and/or RPD was outside control limits/CCV did not meet acceptance criteria.H = Hold time exceeded; M = Manually Integrated; D = Dilution required to get concentration within calibration curveJ1 = The quantitation is an estimation due to discrepencies in meeting certain analyte-specific quality control criteria.NC 2L = North Carolina subchapter 2L groundwater standards.µg/L = micrograms per literMADEP EPH ( µg/L )NCDEQ MADEP Table 11 Worksheet (Rev0421) (µg/L)
Table 9FTBR-308Historical DataT6-5 of T6-81,1,1,2-Tetrachloroethane1 1,0001,1,1-Trichloroethane200200,0001,1,2,2-Tetrachloroethane0.22001,1,2-Trichloroethane0.66001,1-Dichloroethane66,0001,1-Dichloroethene350350,0001,2,3-TrichlorobenzeneNENE1,2,3-Trichloropropane0.005NE1,2,3-TrimethylbenzeneNENE1,2,4-Trichlorobenzene7024,5001,2,4-Trimethylbenzene40028,5001,2-Dibromo-3-Chloropropane0.0002NE1,2-Dichlorobenzene2020,0001,2-Dichloroethane0.44001,2-Dichloropropane0.66001,3,5-Trimethylbenzene40024,1001,3-Dichlorobenzene20061,5001,3-Dichloropropane0.4NE1,4-Dichlorobenzene64052,2-DichloropropaneNENE2-Butanone (MEK)4,0004,000,0002-Chloroethyl vinyl etherNENE2-ChlorotolueneNENE2-Hexanone4040,0002-Methylnaphthalene3012,0002-NitropropaneNENE4-Chlorotoluene2424,0004-Isopropyltoluene (p-Isopropultoluene)2511,7004-Methyl-2-pentanone (MIBK)100100,000Acetone6,0006,000,000AcetonitrileNENEAcrolein4NEAllyl ChlorideNENEBenzene15,000BromobenzeneNENEBromoform44,000Bromomethane10100,000Carbon disulfide700550,000Carbon tetrachloride0.3NEChlorobenzene5050,000ChlorobromomethaneNENEChlorodibromomethane0.4NEChloroethane3,000NEChloroform7070,000Chloromethane33,000cis-1,2-Dichloroethene7070,000cis-1,3-Dichloropropene0.4400CyclohexaneNENEWell IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant LevelVolatile Organic Compounds by EPA Method 8260 ( µg/L )RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-05-23 TW7-03-04-235/1/2023 5/1/2023 5/1/2023 5/1/2023 4/28/2023680-234374-4 680-234374-2 680-234374-3 680-234374-1 680-243331-5NANANANANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANANANANDNANANANANDNANANANA69 QDNDNDNDNDNDNANANANA130 J1DNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANANANA37 J1DNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANANANANDNDNDNDNDNDNANANANANDNANANANANDNANANANANDNANANANA24 QDNANANANA2.7 JQDNANANANANDNANANANA2.7 JDNDNDNDNDNDNDNDNDND10 JQDNANANANA140 QDMNANANANANDNANANANA9.6 JD208.724 D0.66 J13 DNANANANANANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND8.5 Q76 Q76 DQ25 Q 23 J1D
Table 9FTBR-308Historical DataT6-6 of T6-8Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant LevelDibromomethaneNE NEDichlorobromomethaneNENEDichlorodifluoromethane1,000140,000Ethylbenzene60080,000Ethylene Dibromide0.0250Hexachlorobutadiene0.4400Hexane400NEHeptane400NEIsopropylbenzene7030,500Methyl tert-butyl ether2020,000MethylcyclohexaneNENEMethylene Chloride55,000m-Xylene & p-XyleneNENENaphthalene66,000n-Butylbenzene705,900n-Propylbenzene7026,100o-XyleneNENEsec-Butylbenzene708,800Styrene7070,000tert-Butylbenzene7014,750Tetrachloroethene0.7700Toluene600260,000trans-1,2-Dichloroethene100100,000trans-1,3-Dichloropropene0.4400Trichloroethene33,000Trichlorofluoromethane2,000550,000Vinyl acetate8888,000Vinyl chloride0.0330Xylenes, Total50050,0001,1'-Biphenyl400NE2,4,5-Trichlorophenol63NE2,4,6-Trichlorophenol4NE2,4-Dichlorophenol0.989802,4-Dimethylphenol100100,0002,4-DinitrophenolNENE2,4-Dinitrotoluene0.1NE2,6-DinitrotolueneNENE2-ChloronaphthaleneNENE2-Chlorophenol0.4NE2-Methylnaphthalene3012,0002-MethylphenolNE400,0002-NitroanilineNENE2-NitrophenolNENE3 & 4 MethylphenolNENE3,3'-DichlorobenzidineNENE3-NitroanilineNENE4,6-Dinitro-2-methylphenolNENE4-Bromophenyl phenyl etherNENESemi-volatile Organic Compound by EPA Method 8270 (µg/L )RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-05-23 TW7-03-04-235/1/2023 5/1/2023 5/1/2023 5/1/2023 4/28/2023680-234374-4 680-234374-2 680-234374-3 680-234374-1 680-243331-5NANDNANDNDNDNDNDNDNDNDNDNDNDND1.161220 D6.340 J1DNANANANANDNANANANANDNANANANA13 DNANANANA2.4 JDND1624 D1112 J1DNDNDNDNDND2.64651 D4512 DNDNDNDNDNDNANANANA210 J1DNANANANANDNANANANA4.5 JDNANANANANDNANANANA6.7 DNANANANA2.5 JDNANANANANDNANANANANDNDNDNDNDND0.32 J4.7120 D2.51.6 JDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANANANANDNDNDNDNDND27360 D980 D33220 J1DNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND14 J3327NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
Table 9FTBR-308Historical DataT6-7 of T6-8Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant Level4-Chloro-3-methylphenolNE NE4-Chloroaniline0.37NE4-Chlorophenyl phenyl etherNENE4-NitroanilineNENE4-NitrophenolNENEAcenaphthene801,950Acenaphthylene2008,000Acetophenone700NEAnthracene2,0002,000Atrazine3NEBenzaldehyde700NEBenzo[a]anthracene0.054.7Benzo[a]pyrene0.0050.8Benzo[b]fluoranthene0.050.75Benzo[g,h,i]perylene200200Benzo[k]fluoranthene0.50.5bis (2-chloroisopropyl) etherNENEBis(2-chloroethoxy)methaneNENEBis(2-chloroethyl)ether0.0330Bis(2-ethylhexyl) phthalate3135Butyl benzyl phthalate1,000NECaprolactam4,000NECarbazole2NEChrysene55Dibenz(a,h)anthracene0.0051.2Dibenzofuran281,550Diethyl phthalate6,000NEDimethyl phthalateNENEDi-n-butyl phthalate700NEDi-n-octyl phthalate100NEFluoranthene300300Fluorene300845Hexachlorobenzene0.02NEHexachlorocyclopentadieneNENEHexachloroethaneNENEIndeno[1,2,3-cd]pyrene0.050.095Isophorone40NENaphthalene66,000NitrobenzeneNENEN-Nitrosodi-n-propylamineNENEN-Nitrosodiphenylamine0.0007NEPentachlorophenol0.3300Phenanthrene200550Phenol3030,000Pyrene200200C5-C8 Aliphatics (x)400NEC9-C10 Aromatics (c)NENEC9-C12 Aliphatics (a)NENEMADEP VPH ( µg/L )RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-05-23 TW7-03-04-235/1/2023 5/1/2023 5/1/2023 5/1/2023 4/28/2023680-234374-4 680-234374-2 680-234374-3 680-234374-1 680-243331-5NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND6.3 JB 6.3 JB6.4 JBNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND28544.0 J 3.5 JHQNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND340 M980 M 1,600 M 580 M340 DMJ1110 M 460 M 590 JDM 770 M 450 DMJ1360 M 1,300 DM 2,100 DM 1,300 DM 1,100 DMJ1
Table 9FTBR-308Historical DataT6-8 of T6-8Well IDDate SampledLaboratory Control IDNC 2L Groundwater Standard (ug/L)NC Gross Contaminant LevelC11-C22 Aromatics (d)NENEC19-C36 Aliphatics (y)10,000NEC9-C18 Aliphatics (b)NENEC9-C18 Aliphatics (a+b)700NEC9-C22 Aromatics (c+d)200NENotes:Bolded value = detectable concentration.Red value = an NC 2L Groundwater Standard exceedance.NA = Not Analyzed; NE = Not Established; ND = Not DetectedJ = Analyte positively identified, concentration estimatedB = Analyte was detected in a blankQ = LCS/LCSD recovery and/or RPD was outside control limits/CCV did not meet acceptance criteria.H = Hold time exceeded; M = Manually Integrated; D = Dilution required to get concentration within caJ1 = The quantitation is an estimation due to discrepencies in meeting certain analyte-specific quality cNC 2L = North Carolina subchapter 2L groundwater standards.µg/L = micrograms per literMADEP EPH ( µg/L )NCDEQ MADEP Table 11 Worksheet (Rev0421) (µg/L)RW-08-05-23 RW-16-05-23 RW-17-05-23 RW-18-05-23 TW7-03-04-235/1/2023 5/1/2023 5/1/2023 5/1/2023 4/28/2023680-234374-4 680-234374-2 680-234374-3 680-234374-1 680-243331-516 JHM 92 HM 220 M 160 MH 110 MHND ND12 JMND11 JMH50 HB 160 HB 340 MBQ 110 HB 150 MHBJ1410 HMB 1,460 DHBM 2,440 DMBQ 1,410 DMBQ 1,250 DMHJ1126 HMB552 HM 810 JDMBQ 910 DMBQ 495 DMJ1
Table 10
Relative Percent Difference
FTBR-308
Sample ID
Analyte
1,2,3-Trimethylbenzene 11 11 0.00
1,2,4-Trimethylbenzene 44 46 4.44
1,3,5-Trimethylbenzene ND 2.8 NA
2-Methylnaphthalene 6.7 5.5 NA
4-Isopropyltoluene 1.9 2.0 5.13
Acrolein 23 ND NA
Benzene 4.5 4.3 4.55
Carbon Disulfide 0.79 0.95 18.39
Cyclohexane 6.3 6.3 0.00
Ethylbenzene 4.4 3.8 14.63
Isopropylbenzene 11 11 0.00
Methylcyclohexane 2.5 2.5 0.00
Naphthalene 1.9 28 174.58
n-Propylbenzne 11 11 0.00
sec-Butylbenzene 4.0 4.1 2.47
tert-Butylbenzene 0.95 0.94 1.06
m- & p- Xylene ND 3.3 NA
2-Methylnaphthalene 3.6 3.6 0.00
Nitrobenzene 17 16 6.06
C5-C8 Aliphatics 100 110 9.52
C9-C10 Aromatics 180 170 5.71
C9-C12 Aliphatics 340 330 2.99
C11-C22 Aromatics 12 62 135.14
C9-C18 Aliphatics 17 97 140.35
RPD = Relative Percent Difference
MADEP EPH
MW7-20 308-Dup-1 RPD%
SVOCs (EPA Method 8270E)
VOCs (EPA Method 8260D)
MADEP VPH

Appendices

Appendix A
Field Forms

Appendix B
Laboratory Report
ANALYTICAL REPORT
PREPARED FOR
Attn: Ms. Kellie Arstino
Sure-BioChem Laboratories LLC
1000 Atlantic Ave
Camden, New Jersey 08104
Generated 6/5/2023 2:45:21 PM
JOB DESCRIPTION
Ft.Bragg NC (FTBR-308)
JOB NUMBER
680-234331-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
6/5/2023 2:45:21 PM
Authorized for release by
Jerry Lanier, Project Manager I
[e-mail]
[phone]
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Definitions/Glossary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Qualifiers
GC/MS VOA
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
D The reported value is from a dilution.
J Estimated: The analyte was positively identified; the quantitation is an estimation
J1 Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC/MS Semi VOA
Qualifier Description
H Sample was prepped or analyzed beyond the specified holding time. This does not meet regulatory requirements.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J1 Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC VOA
Qualifier Description
D The reported value is from a dilution.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J1 Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC Semi VOA
Qualifier Description
B Blank contamination: The analyte was detected above one-half the reporting limit in an associated blank.
Qualifier
D The reported value is from a dilution.
H Sample was prepped or analyzed beyond the specified holding time. This does not meet regulatory requirements.
J Estimated: The analyte was positively identified; the quantitation is an estimation
J1 Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
Eurofins Savannah
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Definitions/Glossary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Glossary (Continued)
These commonly used abbreviations may or may not be present in this report.
MDA Minimum Detectable Activity (Radiochemistry)
Abbreviation
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Sample Summary
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID Client Sample ID Matrix Collected Received
680-234331-1 MW7-16-04-23 Water 04/28/23 16:05 05/01/23 11:30
680-234331-2 308-DUP-1-04-23 Water 04/28/23 00:00 05/01/23 11:30
680-234331-3 MW7-20-04-23 Water 04/28/23 09:40 05/01/23 11:30
680-234331-4 MW1-04-23 Water 04/28/23 12:05 05/01/23 11:30
680-234331-5 TW7-03-04-23 Water 04/28/23 11:05 05/01/23 11:30
680-234331-6 MW7-22-04-23 Water 04/28/23 14:50 05/01/23 11:30
680-234331-7 Trip Blank Water 04/28/23 00:00 05/01/23 11:30
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Case Narrative
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Job ID: 680-234331-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-234331-1
Receipt
The samples were received on 5/1/2023 11:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 1.8°C, 1.9°C, 2.9°C and 5.2°C
GC/MS VOA
Method 8260D_DOD5: Surrogate recovery was outside acceptance limits for the following matrix spike duplicate (MSD) sample:
TW7-03-04-23 (680-234331-5[MSD]). The parent sample's surrogate recovery was within limits. The MSD sample has been qualified
and reported. <EXPLANATION_REQUIRED>
Method 8260D_DOD5: The surrogate recovery for the blank associated with analytical batch 680-776880 was outside the lower control
limits. The samples were reanalyzed and both sets of data have been reported.
Method 8260D_DOD5: The method blank for analytical batch 680-777079 contained Carbon disulfide above the method detection limit
(MDL). Associated samples were not re-analyzed because results were less than the reporting limit (RL) OR practical quantitation limit
(PQL).
Method 8260D_DOD5: The laboratory control sample duplicate (LCSD) for analytical batch 680-777079 recovered outside control limits
for the following analytes: 1,4-Dioxane. These analytes were biased high in the LCSD and were not detected in the associated samples;
therefore, the data have been reported.
Method 8260D_DOD5: The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for analytical batch
680-777079 recovered outside control limits for the following analyte(s): Iodomethane. Iodomethane has been identified as a poor
performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed.
Method 8260D_DOD5: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical
batch 680-776880 recovered outside control limits for the following analytes: Chloroethane, Hexachlorobutadiene, Naphthalene,
1,2,3-Trichlorobenzene and 1,2,4-Trichlorobenzene.
Method 8260D_DOD5: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 680-777079 were outside control
limits for one or more analytes. See QC Sample Results for detail. Sample matrix interference and/or non-homogeneity are suspected
because the associated laboratory control sample (LCS) recovery is within acceptance limits.
Method 8260D_DOD5: The following sample was diluted to bring the concentration of target analytes within the calibration range:
TW7-03-04-23 (680-234331-5). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E_DOD5: Surrogate recovery for the following samples were outside control limits: MW7-16-04-23 (680-234331-1),
308-DUP-1-04-23 (680-234331-2), MW1-04-23 (680-234331-4), TW7-03-04-23 (680-234331-5) and MW7-22-04-23 (680-234331-6).
Re-extraction and/or re-analysis was performed and surrogate recovery was outside control limits.
Method 8270E_DOD5: The surrogates recoveries for the blank associated with preparation batch 680-779620 and analytical batch
680-780179 were outside control limits. The associated sample(s) was re-prepared and/or re-analyzed outside holding time. Both sets
of data have been reported.
Duplicate sample bottle for 3520/8270E_DOD5 was broken in the lab area. Sample was scheduled for RX, however insufficient volume
remains to RX.
MW7-20-04-23 (680-234331-3)
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Case Narrative
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Job ID: 680-234331-1 (Continued)
Laboratory: Eurofins Savannah (Continued)
Method 8270E_DOD5: The method blank for preparation batch 680-779620 and analytical batch 680-780179 contained Bis(2-ethylhexyl)
phthalate above the method detection limit (MDL). Associated samples were not re-analyzed because results were less than the
reporting limit (RL) OR practical quantitation limit (PQL).
Method 8270E_DOD5: The laboratory control sample (LCS) for preparation batch 680-779620 and analytical batch 680-780179 recovered
outside control limits for multiple analytes. Batch precision also exceeded control limits. The associated sample(s) was re-prepared
and/or re-analyzed outside holding time. Both sets of data have been reported.
Method 8270E_DOD5: The matrix spike / matrix spike duplicate(MS/MSD) recoveries and precision for preparation batch 680-777298 and
analytical batch 680-778040 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: Surrogate recovery for the following samples were outside control limits: MW7-16-04-23 (680-234331-1), TW7-03-04-23
(680-234331-5) and MW7-22-04-23 (680-234331-6). Evidence of matrix interference is confirmed by reanalysis.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH_DOD: The breakthrough for naphthalene is 3% and the breakthrough for 2-methylnaphthalene is 2% in the LCS. The
breakthrough for naphthalene is 2% and the breakthrough for 2-methylnaphthalene is 1% in the LCSD. The method requirement for
breakthrough is <5%. MW7-16-04-23 (680-234331-1), 308-DUP-1-04-23 (680-234331-2), MW7-20-04-23 (680-234331-3), MW1-04-23
(680-234331-4), TW7-03-04-23 (680-234331-5), TW7-03-04-23 (680-234331-5[MS]), TW7-03-04-23 (680-234331-5[MSD]) and
MW7-22-04-23 (680-234331-6)
Method MAEPH_DOD: The method blank for preparation batch 410-372935 and 410-375055 and analytical batch 410-375346 contained
C9-C18 Aliphatics above the limit of detection (LOD). The following sample was not re-extracted and/or re-analyzed because results were
greater than 10X the value found in the method blank: MW7-16-04-23 (680-234331-1).
Method MAEPH_DOD: For analytical batch 410-381594, the breakthrough for naphthalene and 2-methylnaphthalene is <1% in the LCS.
The breakthrough for naphthalene is 2% and the breakthrough for 2-methylnaphthalene is 1% in the LCSD. The method requirement for
breakthrough is <5%. 308-DUP-1-04-23 (680-234331-2), MW7-20-04-23 (680-234331-3), MW1-04-23 (680-234331-4), TW7-03-04-23
(680-234331-5), TW7-03-04-23 (680-234331-5[MS]), TW7-03-04-23 (680-234331-5[MSD]) and MW7-22-04-23 (680-234331-6)
Method MAEPH_DOD: C9-C18 Aliphatics was detected above the reporting limit (RL) in the method blank associated with preparation
batch 410-372935 and 410-375055 and analytical batch 410-375346 as well as in the following samples: 308-DUP-1-04-23
(680-234331-2), MW7-20-04-23 (680-234331-3), MW1-04-23 (680-234331-4), TW7-03-04-23 (680-234331-5), TW7-03-04-23
(680-234331-5[MS]), TW7-03-04-23 (680-234331-5[MSD]) and MW7-22-04-23 (680-234331-6). All affected samples were re-extracted
and re-analyzed outside of holding time and the method blank again had detections. Both sets of data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
9.9 J Q 25 3.7 ug/L 05/05/23 12:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
50 20 ug/L 05/05/23 12:10 1210 Q MAcetonitrile
50 15 ug/L 05/05/23 12:10 134 JAcrolein
50 5.5 ug/L 05/05/23 12:10 120 U MAcrylonitrile
2.0 0.27 ug/L 05/05/23 12:10 16.5Benzene
1.0 0.24 ug/L 05/05/23 12:10 10.50 UBromobenzene
2.0 0.34 ug/L 05/05/23 12:10 11.0 UBromochloromethane
2.0 0.25 ug/L 05/05/23 12:10 11.0 UBromodichloromethane
2.5 0.59 ug/L 05/05/23 12:10 12.0 U QBromoform
20 3.7 ug/L 05/05/23 12:10 110 U QBromomethane
25 6.4 ug/L 05/05/23 12:10 120 U M2-Butanone (MEK)
2.5 0.52 ug/L 05/05/23 12:10 12.0 U Mn-Butylbenzene
2.5 0.53 ug/L 05/05/23 12:10 14.7sec-Butylbenzene
2.0 0.43 ug/L 05/05/23 12:10 11.3 Jtert-Butylbenzene
2.0 0.43 ug/L 05/05/23 12:10 11.0 UCarbon disulfide
2.0 0.30 ug/L 05/05/23 12:10 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/05/23 12:10 10.50 UChlorobenzene
2.5 0.71 ug/L 05/05/23 12:10 12.0 U2-Chloro-1,3-butadiene
20 4.6 ug/L 05/05/23 12:10 110 UChloroethane
25 0.59 ug/L 05/05/23 12:10 120 U2-Chloroethyl vinyl ether
2.0 0.27 ug/L 05/05/23 12:10 11.0 UChloroform
2.5 0.54 ug/L 05/05/23 12:10 12.0 UChloromethane
5.0 1.1 ug/L 05/05/23 12:10 14.0 UAllyl chloride
1.0 0.25 ug/L 05/05/23 12:10 10.50 U2-Chlorotoluene
2.0 0.41 ug/L 05/05/23 12:10 11.0 U4-Chlorotoluene
2.0 0.39 ug/L 05/05/23 12:10 11.0 UChlorodibromomethane
10 1.8 ug/L 05/05/23 12:10 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/05/23 12:10 11.0 U1,2-Dibromoethane
2.0 0.34 ug/L 05/05/23 12:10 11.0 UDibromomethane
2.0 0.31 ug/L 05/05/23 12:10 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 12:10 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 12:10 11.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/05/23 12:10 15.0 U Q Mtrans-1,4-Dichloro-2-butene
2.0 0.36 ug/L 05/05/23 12:10 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/05/23 12:10 11.0 U M1,1-Dichloroethane
2.0 0.25 ug/L 05/05/23 12:10 11.0 U M1,2-Dichloroethane
2.0 0.25 ug/L 05/05/23 12:10 11.0 Ucis-1,2-Dichloroethene
2.0 0.34 ug/L 05/05/23 12:10 11.0 Utrans-1,2-Dichloroethene
2.0 0.37 ug/L 05/05/23 12:10 11.0 U1,2-Dichloroethene, Total
2.0 0.33 ug/L 05/05/23 12:10 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/05/23 12:10 10.50 U M1,2-Dichloropropane
2.0 0.36 ug/L 05/05/23 12:10 11.0 U1,3-Dichloropropane
2.0 0.35 ug/L 05/05/23 12:10 11.0 U2,2-Dichloropropane
2.0 0.28 ug/L 05/05/23 12:10 11.0 U1,1-Dichloropropene
2.0 0.26 ug/L 05/05/23 12:10 11.0 Ucis-1,3-Dichloropropene
2.0 0.23 ug/L 05/05/23 12:10 11.0 Utrans-1,3-Dichloropropene
1.0 0.20 ug/L 05/05/23 12:10 16.0Ethylbenzene
2.0 0.33 ug/L 05/05/23 12:10 11.0 UEthyl methacrylate
5.0 0.22 ug/L 05/05/23 12:10 11.0 UHexachlorobutadiene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U M 20 3.2 ug/L 05/05/23 12:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Hexanone
20 3.9 ug/L 05/05/23 12:10 110 U QIodomethane
500 68 ug/L 05/05/23 12:10 1250 U MIsobutyl alcohol
2.0 0.26 ug/L 05/05/23 12:10 131Isopropylbenzene
2.0 0.44 ug/L 05/05/23 12:10 11.0 Up-Isopropyltoluene
20 5.0 ug/L 05/05/23 12:10 110 U QMethacrylonitrile
20 3.2 ug/L 05/05/23 12:10 110 UMethylene Chloride
2.5 0.78 ug/L 05/05/23 12:10 12.0 U MMethyl methacrylate
20 2.7 ug/L 05/05/23 12:10 110 U M4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/05/23 12:10 12.0 UMethyl tert-butyl ether
10 2.4 ug/L 05/05/23 12:10 1110Naphthalene
5.0 0.50 ug/L 05/05/23 12:10 11.0 U QPentachloroethane
20 5.0 ug/L 05/05/23 12:10 110 U Q MPropionitrile
2.0 0.41 ug/L 05/05/23 12:10 126N-Propylbenzene
2.0 0.27 ug/L 05/05/23 12:10 11.0 U MStyrene
2.0 0.36 ug/L 05/05/23 12:10 11.0 U1,1,1,2-Tetrachloroethane
2.0 0.40 ug/L 05/05/23 12:10 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/05/23 12:10 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/05/23 12:10 11.0 UToluene
5.0 0.81 ug/L 05/05/23 12:10 12.0 U1,2,3-Trichlorobenzene
5.0 0.53 ug/L 05/05/23 12:10 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/05/23 12:10 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/05/23 12:10 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/05/23 12:10 10.50 UTrichloroethene
2.0 0.33 ug/L 05/05/23 12:10 11.0 UTrichlorofluoromethane
2.0 0.48 ug/L 05/05/23 12:10 11.0 U1,2,3-Trichloropropane
1.0 0.23 ug/L 05/05/23 12:10 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.43 ug/L 05/05/23 12:10 11.0 U1,2,4-Trimethylbenzene
2.0 0.28 ug/L 05/05/23 12:10 11.0 U1,3,5-Trimethylbenzene
2.5 0.69 ug/L 05/05/23 12:10 12.0 U MVinyl acetate
2.0 0.40 ug/L 05/05/23 12:10 11.0 UVinyl chloride
2.0 0.26 ug/L 05/05/23 12:10 10.29 Jo-Xylene
2.0 0.49 ug/L 05/05/23 12:10 11.0 Um-Xylene & p-Xylene
2.0 0.49 ug/L 05/05/23 12:10 11.0 UXylenes, Total
2.0 0.28 ug/L 05/05/23 12:10 1160Cyclohexane
5.0 1.1 ug/L 05/05/23 12:10 14.0 U M1-Chlorohexane
20 3.2 ug/L 05/05/23 12:10 110 UMethyl acetate
2.0 0.33 ug/L 05/05/23 12:10 185Methylcyclohexane
10 2.1 ug/L 05/05/23 12:10 15.0 U MTetrahydrofuran
10 0.70 ug/L 05/05/23 12:10 12.0 UDiisopropyl ether
5.0 0.65 ug/L 05/05/23 12:10 12.0 U MHexane
5.0 0.37 ug/L 05/05/23 12:10 11.0 UDiethyl ether
2.0 0.43 ug/L 05/05/23 12:10 11.0 U MHeptane
2.0 0.48 ug/L 05/05/23 12:10 11.0 U1,3-Dichloropropene, Total
10 2.5 ug/L 05/05/23 12:10 135 Q2-Methylnaphthalene
2.0 0.38 ug/L 05/05/23 12:10 11.0 U1,3-Butadiene
5.0 0.50 ug/L 05/05/23 12:10 11.0 U Qn-Butyl acetate
2.0 0.50 ug/L 05/05/23 12:10 11.0 UDichlorofluoromethane
10 2.5 ug/L 05/05/23 12:10 15.0 U Q MBenzyl chloride
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
20 U M 50 6.9 ug/L 05/05/23 12:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
tert-Butyl alcohol
200 50 ug/L 05/05/23 12:10 1100 U QEthanol
250 92 ug/L 05/05/23 12:10 1200 U Q1,4-Dioxane
4.0 0.86 ug/L 05/05/23 12:10 12.0 U Q M2-Nitropropane
10 2.5 ug/L 05/05/23 12:10 15.0 U1,3,5-Trichlorobenzene
10 2.5 ug/L 05/05/23 12:10 15.0 U Q1,2,3-Trimethylbenzene
100 25 ug/L 05/05/23 12:10 150 U Q Mn-Butyl alcohol
2.5 0.78 ug/L 05/05/23 12:10 12.0 UTert-amyl methyl ether
100 25 ug/L 05/05/23 12:10 150 U Q2-Propanol
2.5 0.72 ug/L 05/05/23 12:10 12.0 UEthyl tert-butyl ether
20 5.0 ug/L 05/05/23 12:10 110 U QEthyl acetate
25 8.6 ug/L 05/05/23 12:10 120 U Q2-Butanol, 2-methyl-
5.0 0.99 ug/L 05/05/23 12:10 12.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)101 89-112 05/05/23 12:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)86 05/05/23 12:10 181-118
Dibromofluoromethane (Surr)92 05/05/23 12:10 180-119
4-Bromofluorobenzene (Surr)108 05/05/23 12:10 185-114
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
2.1 U 11 0.80 ug/L 05/05/23 21:00 05/10/23 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
11 0.59 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U1,2,4-Trichlorobenzene
11 0.56 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U1,2-Dichlorobenzene
11 0.62 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U1,3-Dichlorobenzene
11 0.63 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U M1,3-Dinitrobenzene
11 0.57 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U1,4-Dichlorobenzene
11 0.66 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Q1,4-Naphthoquinone
11 1.2 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U1-Naphthylamine
11 0.76 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Q2,3,4,6-Tetrachlorophenol
11 1.3 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Q2,4,5-Trichlorophenol
11 0.90 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U2,4,6-Trichlorophenol
11 1.2 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U2,4-Dichlorophenol
11 4.2 ug/L 05/05/23 21:00 05/10/23 21:07 111 U M2,4-Dimethylphenol
53 11 ug/L 05/05/23 21:00 05/10/23 21:07 121 U Q2,4-Dinitrophenol
11 1.3 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U M2,4-Dinitrotoluene
11 0.77 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U M2,6-Dichlorophenol
11 1.2 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U M2,6-Dinitrotoluene
11 1.7 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U Q2-Acetylaminofluorene
11 0.85 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U2-Chloronaphthalene
11 0.92 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U2-Chlorophenol
11 0.82 ug/L 05/05/23 21:00 05/10/23 21:07 1202-Methylnaphthalene
11 0.94 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U2-Methylphenol
11 1.6 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U2-Naphthylamine
53 1.4 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U M2-Nitroaniline
11 0.80 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U2-Nitrophenol
11 1.4 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U3 & 4 Methylphenol
63 32 ug/L 05/05/23 21:00 05/10/23 21:07 163 U3,3'-Dichlorobenzidine
21 11 ug/L 05/05/23 21:00 05/10/23 21:07 114 U Q3,3'-Dimethylbenzidine
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.3 U Q 11 1.5 ug/L 05/05/23 21:00 05/10/23 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
3-Methylcholanthrene
53 5.3 ug/L 05/05/23 21:00 05/10/23 21:07 111 U M3-Nitroaniline
53 11 ug/L 05/05/23 21:00 05/10/23 21:07 121 U Q4,6-Dinitro-2-methylphenol
11 1.3 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U4-Aminobiphenyl
11 0.81 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U M4-Bromophenyl phenyl ether
11 1.1 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U4-Chloro-3-methylphenol
21 2.3 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U4-Chloroaniline
11 0.89 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U4-Chlorophenyl phenyl ether
53 5.3 ug/L 05/05/23 21:00 05/10/23 21:07 111 U4-Nitroaniline
53 2.0 ug/L 05/05/23 21:00 05/10/23 21:07 14.2 U Q M4-Nitrophenol
26 11 ug/L 05/05/23 21:00 05/10/23 21:07 121 U M4-Nitroquinoline-1-oxide
11 1.6 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U M5-Nitro-o-toluidine
11 1.3 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Q7,12-Dimethylbenz(a)anthracene
11 0.80 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QAcenaphthene
11 0.90 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QAcenaphthylene
11 0.60 ug/L 05/05/23 21:00 05/10/23 21:07 11.1 JAcetophenone
2100 37 ug/L 05/05/23 21:00 05/10/23 21:07 185 Ualpha,alpha-Dimethyl phenethylamine
11 0.73 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QAnthracene
11 0.58 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QBenzo[a]anthracene
11 0.75 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QBenzo[a]pyrene
11 2.7 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U QBenzo[b]fluoranthene
11 0.92 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QBenzo[g,h,i]perylene
11 1.3 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QBenzo[k]fluoranthene
11 1.2 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U MBenzyl alcohol
11 0.82 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 Ubis (2-chloroisopropyl) ether
11 0.99 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U MBis(2-chloroethoxy)methane
11 1.2 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UBis(2-chloroethyl)ether
11 1.7 ug/L 05/05/23 21:00 05/10/23 21:07 12.6 UBis(2-ethylhexyl) phthalate
11 1.3 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UButyl benzyl phthalate
11 0.54 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QChrysene
11 0.82 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QDiallate
11 1.1 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UDibenz(a,h)anthracene
11 0.83 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UDibenzofuran
11 0.93 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U MDiethyl phthalate
11 0.79 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QDimethoate
11 1.0 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UDimethyl phthalate
11 0.88 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UDi-n-butyl phthalate
11 1.5 ug/L 05/05/23 21:00 05/10/23 21:07 12.6 UDi-n-octyl phthalate
11 5.3 ug/L 05/05/23 21:00 05/10/23 21:07 111 U Q MDinoseb
11 0.97 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UDiphenylamine
11 0.83 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QDisulfoton
11 1.0 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QEthyl methanesulfonate
11 1.4 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QEthyl Parathion
11 1.2 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QFamphur
11 0.78 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QFluoranthene
11 1.0 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QFluorene
11 0.83 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UHexachlorobenzene
11 0.66 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QHexachlorobutadiene
11 2.6 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 UHexachlorocyclopentadiene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.1 U 11 0.80 ug/L 05/05/23 21:00 05/10/23 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Hexachloroethane
11 1.5 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U QHexachloropropene
11 1.1 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QIndeno[1,2,3-cd]pyrene
11 0.95 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U MIsophorone
11 0.53 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QIsosafrole
2100 2.9 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U QMethapyrilene
11 0.63 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Q MMethyl methanesulfonate
11 0.93 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UMethyl parathion
11 0.74 ug/L 05/05/23 21:00 05/10/23 21:07 159 QNaphthalene
11 0.77 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UNitrobenzene
11 0.98 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UN-Nitrosodiethylamine
11 3.0 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U QN-Nitrosodimethylamine
11 1.0 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U MN-Nitrosodi-n-butylamine
11 0.76 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U MN-Nitrosodi-n-propylamine
11 0.97 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UN-Nitrosodiphenylamine
11 3.5 ug/L 05/05/23 21:00 05/10/23 21:07 111 UN-Nitrosomethylethylamine
11 0.93 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UN-Nitrosopiperidine
11 1.1 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UN-Nitrosopyrrolidine
11 1.1 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Mo,o',o''-Triethylphosphorothioate
11 1.5 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 Uo-Toluidine
11 0.83 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Mp-Dimethylamino azobenzene
11 0.55 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QPentachlorobenzene
11 0.82 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UPentachloronitrobenzene
53 2.1 ug/L 05/05/23 21:00 05/10/23 21:07 14.2 UPentachlorophenol
11 1.5 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U MPhenacetin
11 0.81 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QPhenanthrene
11 0.88 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UPhenol
11 0.92 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UPhorate
2100 11 ug/L 05/05/23 21:00 05/10/23 21:07 126 U Q Mp-Phenylene diamine
11 0.94 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 UPronamide
11 0.67 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QPyrene
11 0.85 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U QSafrole, Total
11 2.1 ug/L 05/05/23 21:00 05/10/23 21:07 15.3 U Qsym-Trinitrobenzene
11 0.96 ug/L 05/05/23 21:00 05/10/23 21:07 12.1 U Q MThionazin
2,4,6-Tribromophenol (Surr)75 43-140 05/05/23 21:00 05/10/23 21:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)66 05/05/23 21:00 05/10/23 21:07 144-119
2-Fluorophenol (Surr)50 05/05/23 21:00 05/10/23 21:07 119-119
Nitrobenzene-d5 (Surr)66 05/05/23 21:00 05/10/23 21:07 144-120
Phenol-d5 (Surr)35 05/05/23 21:00 05/10/23 21:07 127-110
Terphenyl-d14 (Surr)41 Q 05/05/23 21:00 05/10/23 21:07 150-134
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE
LOQ DL
2.0 U H Q 10 0.78 ug/L 05/20/23 21:30 05/24/23 22:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
10 0.57 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q1,2,4-Trichlorobenzene
10 0.54 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q1,2-Dichlorobenzene
10 0.60 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q1,3-Dichlorobenzene
10 0.61 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q1,3-Dinitrobenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
2.0 U H Q 10 0.55 ug/L 05/20/23 21:30 05/24/23 22:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,4-Dichlorobenzene
10 0.63 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q1,4-Naphthoquinone
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q1-Naphthylamine
10 0.73 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,3,4,6-Tetrachlorophenol
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,4,5-Trichlorophenol
10 0.87 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,4,6-Trichlorophenol
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,4-Dichlorophenol
10 4.1 ug/L 05/20/23 21:30 05/24/23 22:05 110 U H Q2,4-Dimethylphenol
51 10 ug/L 05/20/23 21:30 05/24/23 22:05 120 U H Q2,4-Dinitrophenol
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,4-Dinitrotoluene
10 0.74 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,6-Dichlorophenol
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2,6-Dinitrotoluene
10 1.6 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Q2-Acetylaminofluorene
10 0.82 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2-Chloronaphthalene
10 0.89 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2-Chlorophenol
10 0.80 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2-Methylnaphthalene
10 0.91 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q2-Methylphenol
10 1.5 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Q2-Naphthylamine
51 1.3 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M Q2-Nitroaniline
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M Q2-Nitrophenol
10 1.3 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q3 & 4 Methylphenol
61 31 ug/L 05/20/23 21:30 05/24/23 22:05 161 U H Q3,3'-Dichlorobenzidine
20 10 ug/L 05/20/23 21:30 05/24/23 22:05 113 U H Q3,3'-Dimethylbenzidine
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Q3-Methylcholanthrene
51 5.1 ug/L 05/20/23 21:30 05/24/23 22:05 110 U H M Q3-Nitroaniline
51 10 ug/L 05/20/23 21:30 05/24/23 22:05 120 U H Q4,6-Dinitro-2-methylphenol
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q4-Aminobiphenyl
10 0.79 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M Q4-Bromophenyl phenyl ether
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q4-Chloro-3-methylphenol
20 2.2 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Q4-Chloroaniline
10 0.86 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q4-Chlorophenyl phenyl ether
51 5.1 ug/L 05/20/23 21:30 05/24/23 22:05 110 U H Q4-Nitroaniline
51 1.9 ug/L 05/20/23 21:30 05/24/23 22:05 14.1 U H M Q4-Nitrophenol
26 10 ug/L 05/20/23 21:30 05/24/23 22:05 120 U H Q4-Nitroquinoline-1-oxide
10 1.5 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Q5-Nitro-o-toluidine
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Q7,12-Dimethylbenz(a)anthracene
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QAcenaphthene
10 0.87 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QAcenaphthylene
10 0.58 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QAcetophenone
2000 36 ug/L 05/20/23 21:30 05/24/23 22:05 182 U H Qalpha,alpha-Dimethyl phenethylamine
10 0.70 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QAnthracene
10 0.56 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QBenzo[a]anthracene
10 0.72 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QBenzo[a]pyrene
10 2.7 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H QBenzo[b]fluoranthene
10 0.89 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QBenzo[g,h,i]perylene
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QBenzo[k]fluoranthene
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QBenzyl alcohol
10 0.80 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Qbis (2-chloroisopropyl) ether
10 0.96 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QBis(2-chloroethoxy)methane
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
2.0 U H Q 10 1.1 ug/L 05/20/23 21:30 05/24/23 22:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Bis(2-chloroethyl)ether
10 1.6 ug/L 05/20/23 21:30 05/24/23 22:05 12.6 U H QBis(2-ethylhexyl) phthalate
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QButyl benzyl phthalate
10 0.52 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QChrysene
10 0.80 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDiallate
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDibenz(a,h)anthracene
10 0.81 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDibenzofuran
10 0.90 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QDiethyl phthalate
10 0.77 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDimethoate
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDimethyl phthalate
10 0.85 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDi-n-butyl phthalate
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:05 12.6 U H QDi-n-octyl phthalate
10 5.1 ug/L 05/20/23 21:30 05/24/23 22:05 110 U HDinoseb
10 0.94 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QDiphenylamine
10 0.81 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QDisulfoton
10 0.98 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QEthyl methanesulfonate
10 1.3 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QEthyl Parathion
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QFamphur
10 0.76 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QFluoranthene
10 0.98 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QFluorene
10 0.81 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QHexachlorobenzene
10 0.63 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QHexachlorobutadiene
10 2.6 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H QHexachlorocyclopentadiene
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QHexachloroethane
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H QHexachloropropene
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QIndeno[1,2,3-cd]pyrene
10 0.92 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QIsophorone
10 0.51 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QIsosafrole
2000 2.8 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H QMethapyrilene
10 0.61 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QMethyl methanesulfonate
10 0.90 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QMethyl parathion
10 0.71 ug/L 05/20/23 21:30 05/24/23 22:05 16.9 J H QNaphthalene
10 0.74 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QNitrobenzene
10 0.95 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QN-Nitrosodiethylamine
10 2.9 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H QN-Nitrosodimethylamine
10 0.98 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QN-Nitrosodi-n-butylamine
10 0.73 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QN-Nitrosodi-n-propylamine
10 0.94 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QN-Nitrosodiphenylamine
10 3.4 ug/L 05/20/23 21:30 05/24/23 22:05 110 U H QN-Nitrosomethylethylamine
10 0.90 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QN-Nitrosopiperidine
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QN-Nitrosopyrrolidine
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M Qo,o',o''-Triethylphosphorothioate
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Qo-Toluidine
10 0.81 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H Qp-Dimethylamino azobenzene
10 0.53 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QPentachlorobenzene
10 0.80 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U HPentachloronitrobenzene
51 2.0 ug/L 05/20/23 21:30 05/24/23 22:05 14.1 U H QPentachlorophenol
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U HPhenacetin
10 0.79 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QPhenanthrene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
2.0 U H Q 10 0.85 ug/L 05/20/23 21:30 05/24/23 22:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Phenol
10 0.89 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QPhorate
2000 10 ug/L 05/20/23 21:30 05/24/23 22:05 126 U H M Qp-Phenylene diamine
10 0.91 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QPronamide
10 0.64 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QPyrene
10 0.82 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H QSafrole, Total
10 2.0 ug/L 05/20/23 21:30 05/24/23 22:05 15.1 U H Qsym-Trinitrobenzene
10 0.93 ug/L 05/20/23 21:30 05/24/23 22:05 12.0 U H M QThionazin
2,4,6-Tribromophenol (Surr)71 43-140 05/20/23 21:30 05/24/23 22:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)56 05/20/23 21:30 05/24/23 22:05 144-119
2-Fluorophenol (Surr)7 Q 05/20/23 21:30 05/24/23 22:05 119-119
Nitrobenzene-d5 (Surr)59 05/20/23 21:30 05/24/23 22:05 144-120
Phenol-d5 (Surr)0.9 Q 05/20/23 21:30 05/24/23 22:05 127-110
Terphenyl-d14 (Surr)13 Q 05/20/23 21:30 05/24/23 22:05 150-134
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
1900 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
9.7 5.0 1.0 ug/L 05/10/23 12:36 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 12:36 11100 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 12:36 1380 MC9-C10 Aromatics
100 25 ug/L 05/10/23 12:36 1820 MC9-C12 Aliphatics
5.0 1.0 ug/L 05/10/23 12:36 111Ethylbenzene
5.0 1.0 ug/L 05/10/23 12:36 14.7 JMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 12:36 1140 MNaphthalene
5.0 1.0 ug/L 05/10/23 12:36 12.0 UToluene
100 25 ug/L 05/10/23 12:36 1420C9-C12 Aliphatics (adjusted)
10 2.5 ug/L 05/10/23 12:36 15.0 Um-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 12:36 12.0 Uo-Xylene
100 25 ug/L 05/10/23 12:36 11100C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)733 Q 70-130 05/10/23 12:36 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)375 Q 05/10/23 12:36 170-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U M 2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:55 1850Total EPH
12 5.1 ug/L 05/08/23 09:17 05/13/23 11:50 110 U MPyrene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 11.2 UBenzo[g,h,i]perylene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 11.2 UBenzo[b]fluoranthene
2.0 0.51 ug/L 05/08/23 09:17 05/13/23 11:50 11.0 U MFluoranthene
4.1 1.5 ug/L 05/08/23 09:17 05/13/23 11:50 13.0 UBenzo[k]fluoranthene
2.0 0.71 ug/L 05/08/23 09:17 05/13/23 11:50 15.2 MAcenaphthylene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-1Client Sample ID: MW7-16-04-23
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
1.0 U M 2.0 0.51 ug/L 05/08/23 09:17 05/13/23 11:50 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Chrysene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 11.2 UBenzo[a]pyrene
2.0 0.51 ug/L 05/08/23 09:17 05/13/23 11:50 11.0 UDibenz(a,h)anthracene
2.0 0.71 ug/L 05/08/23 09:17 05/13/23 11:50 11.4 UBenzo[a]anthracene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 10.70 J MAcenaphthene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 11.2 U MPhenanthrene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 11.2 U MFluorene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 11:50 130 M2-Methylnaphthalene
41 10 ug/L 05/08/23 09:17 05/13/23 11:50 1270 MC11-C22 Aromatics (unadjusted)
51 10 ug/L 05/08/23 09:17 05/13/23 13:20 120 UC19-C36 Aliphatics
30 10 ug/L 05/08/23 09:17 05/13/23 13:20 1580 BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)56 40-140 05/08/23 09:17 05/13/23 13:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)70 05/08/23 09:17 05/13/23 11:50 140-140
o- terphenyl (Surr)60 05/08/23 09:17 05/13/23 11:50 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
LOQ DL
73 D M 4.1 1.2 ug/L 05/08/23 09:17 05/15/23 19:15 2
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Naphthalene
81 20 ug/L 05/08/23 09:17 05/15/23 19:15 2160 DC11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)67 40-140 05/08/23 09:17 05/15/23 19:15 2
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
o- terphenyl (Surr)56 05/08/23 09:17 05/15/23 19:15 240-140
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 05/05/23 09:06 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
50 20 ug/L 05/05/23 09:06 140 U Q MAcetonitrile
50 15 ug/L 05/05/23 09:06 140 U MAcrolein
50 5.5 ug/L 05/05/23 09:06 120 U MAcrylonitrile
2.0 0.27 ug/L 05/05/23 09:06 14.3Benzene
1.0 0.24 ug/L 05/05/23 09:06 10.50 UBromobenzene
2.0 0.34 ug/L 05/05/23 09:06 11.0 UBromochloromethane
2.0 0.25 ug/L 05/05/23 09:06 11.0 UBromodichloromethane
2.5 0.59 ug/L 05/05/23 09:06 12.0 U QBromoform
20 3.7 ug/L 05/05/23 09:06 110 U QBromomethane
25 6.4 ug/L 05/05/23 09:06 120 U M2-Butanone (MEK)
2.5 0.52 ug/L 05/05/23 09:06 12.0 Un-Butylbenzene
2.5 0.53 ug/L 05/05/23 09:06 14.1sec-Butylbenzene
2.0 0.43 ug/L 05/05/23 09:06 10.94 Jtert-Butylbenzene
2.0 0.43 ug/L 05/05/23 09:06 10.95 JCarbon disulfide
2.0 0.30 ug/L 05/05/23 09:06 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/05/23 09:06 10.50 UChlorobenzene
2.5 0.71 ug/L 05/05/23 09:06 12.0 U2-Chloro-1,3-butadiene
20 4.6 ug/L 05/05/23 09:06 110 UChloroethane
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
20 U 25 0.59 ug/L 05/05/23 09:06 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Chloroethyl vinyl ether
2.0 0.27 ug/L 05/05/23 09:06 11.0 U MChloroform
2.5 0.54 ug/L 05/05/23 09:06 12.0 UChloromethane
5.0 1.1 ug/L 05/05/23 09:06 14.0 UAllyl chloride
1.0 0.25 ug/L 05/05/23 09:06 10.50 U2-Chlorotoluene
2.0 0.41 ug/L 05/05/23 09:06 11.0 U4-Chlorotoluene
2.0 0.39 ug/L 05/05/23 09:06 11.0 UChlorodibromomethane
10 1.8 ug/L 05/05/23 09:06 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/05/23 09:06 11.0 U1,2-Dibromoethane
2.0 0.34 ug/L 05/05/23 09:06 11.0 UDibromomethane
2.0 0.31 ug/L 05/05/23 09:06 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 09:06 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 09:06 11.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/05/23 09:06 15.0 U Q Mtrans-1,4-Dichloro-2-butene
2.0 0.36 ug/L 05/05/23 09:06 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/05/23 09:06 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 05/05/23 09:06 11.0 U1,2-Dichloroethane
2.0 0.25 ug/L 05/05/23 09:06 11.0 Ucis-1,2-Dichloroethene
2.0 0.34 ug/L 05/05/23 09:06 11.0 Utrans-1,2-Dichloroethene
2.0 0.37 ug/L 05/05/23 09:06 11.0 U1,2-Dichloroethene, Total
2.0 0.33 ug/L 05/05/23 09:06 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/05/23 09:06 10.50 U1,2-Dichloropropane
2.0 0.36 ug/L 05/05/23 09:06 11.0 U1,3-Dichloropropane
2.0 0.35 ug/L 05/05/23 09:06 11.0 U2,2-Dichloropropane
2.0 0.28 ug/L 05/05/23 09:06 11.0 U1,1-Dichloropropene
2.0 0.26 ug/L 05/05/23 09:06 11.0 Ucis-1,3-Dichloropropene
2.0 0.23 ug/L 05/05/23 09:06 11.0 Utrans-1,3-Dichloropropene
1.0 0.20 ug/L 05/05/23 09:06 13.8Ethylbenzene
2.0 0.33 ug/L 05/05/23 09:06 11.0 UEthyl methacrylate
5.0 0.22 ug/L 05/05/23 09:06 11.0 UHexachlorobutadiene
20 3.2 ug/L 05/05/23 09:06 110 U2-Hexanone
20 3.9 ug/L 05/05/23 09:06 110 U QIodomethane
500 68 ug/L 05/05/23 09:06 1250 U MIsobutyl alcohol
2.0 0.26 ug/L 05/05/23 09:06 111Isopropylbenzene
2.0 0.44 ug/L 05/05/23 09:06 12.0p-Isopropyltoluene
20 5.0 ug/L 05/05/23 09:06 110 U Q MMethacrylonitrile
20 3.2 ug/L 05/05/23 09:06 110 UMethylene Chloride
2.5 0.78 ug/L 05/05/23 09:06 12.0 UMethyl methacrylate
20 2.7 ug/L 05/05/23 09:06 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/05/23 09:06 12.0 UMethyl tert-butyl ether
10 2.4 ug/L 05/05/23 09:06 128Naphthalene
5.0 0.50 ug/L 05/05/23 09:06 11.0 U QPentachloroethane
20 5.0 ug/L 05/05/23 09:06 110 U Q MPropionitrile
2.0 0.41 ug/L 05/05/23 09:06 111N-Propylbenzene
2.0 0.27 ug/L 05/05/23 09:06 11.0 U MStyrene
2.0 0.36 ug/L 05/05/23 09:06 11.0 U1,1,1,2-Tetrachloroethane
2.0 0.40 ug/L 05/05/23 09:06 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/05/23 09:06 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/05/23 09:06 11.0 UToluene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U 5.0 0.81 ug/L 05/05/23 09:06 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,3-Trichlorobenzene
5.0 0.53 ug/L 05/05/23 09:06 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/05/23 09:06 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/05/23 09:06 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/05/23 09:06 10.50 UTrichloroethene
2.0 0.33 ug/L 05/05/23 09:06 11.0 UTrichlorofluoromethane
2.0 0.48 ug/L 05/05/23 09:06 11.0 U1,2,3-Trichloropropane
1.0 0.23 ug/L 05/05/23 09:06 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.43 ug/L 05/05/23 09:06 1461,2,4-Trimethylbenzene
2.0 0.28 ug/L 05/05/23 09:06 12.8 M1,3,5-Trimethylbenzene
2.5 0.69 ug/L 05/05/23 09:06 12.0 UVinyl acetate
2.0 0.40 ug/L 05/05/23 09:06 11.0 UVinyl chloride
2.0 0.26 ug/L 05/05/23 09:06 11.0 Uo-Xylene
2.0 0.49 ug/L 05/05/23 09:06 13.3m-Xylene & p-Xylene
2.0 0.49 ug/L 05/05/23 09:06 13.3Xylenes, Total
2.0 0.28 ug/L 05/05/23 09:06 16.3Cyclohexane
5.0 1.1 ug/L 05/05/23 09:06 14.0 U M1-Chlorohexane
20 3.2 ug/L 05/05/23 09:06 110 UMethyl acetate
2.0 0.33 ug/L 05/05/23 09:06 12.5Methylcyclohexane
10 2.1 ug/L 05/05/23 09:06 15.0 U MTetrahydrofuran
10 0.70 ug/L 05/05/23 09:06 12.0 UDiisopropyl ether
5.0 0.65 ug/L 05/05/23 09:06 12.0 U MHexane
5.0 0.37 ug/L 05/05/23 09:06 11.0 UDiethyl ether
2.0 0.43 ug/L 05/05/23 09:06 11.0 U MHeptane
2.0 0.48 ug/L 05/05/23 09:06 11.0 U1,3-Dichloropropene, Total
10 2.5 ug/L 05/05/23 09:06 15.5 J Q2-Methylnaphthalene
2.0 0.38 ug/L 05/05/23 09:06 11.0 U1,3-Butadiene
5.0 0.50 ug/L 05/05/23 09:06 11.0 U Qn-Butyl acetate
2.0 0.50 ug/L 05/05/23 09:06 11.0 UDichlorofluoromethane
10 2.5 ug/L 05/05/23 09:06 15.0 U QBenzyl chloride
50 6.9 ug/L 05/05/23 09:06 120 U Mtert-Butyl alcohol
200 50 ug/L 05/05/23 09:06 1100 U QEthanol
250 92 ug/L 05/05/23 09:06 1200 U Q1,4-Dioxane
4.0 0.86 ug/L 05/05/23 09:06 12.0 U Q M2-Nitropropane
10 2.5 ug/L 05/05/23 09:06 15.0 U1,3,5-Trichlorobenzene
10 2.5 ug/L 05/05/23 09:06 111 Q1,2,3-Trimethylbenzene
100 25 ug/L 05/05/23 09:06 150 U Q Mn-Butyl alcohol
2.5 0.78 ug/L 05/05/23 09:06 12.0 UTert-amyl methyl ether
100 25 ug/L 05/05/23 09:06 150 U Q2-Propanol
2.5 0.72 ug/L 05/05/23 09:06 12.0 UEthyl tert-butyl ether
20 5.0 ug/L 05/05/23 09:06 110 U QEthyl acetate
25 8.6 ug/L 05/05/23 09:06 120 U Q M2-Butanol, 2-methyl-
5.0 0.99 ug/L 05/05/23 09:06 12.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)99 89-112 05/05/23 09:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)85 05/05/23 09:06 181-118
Dibromofluoromethane (Surr)94 05/05/23 09:06 180-119
4-Bromofluorobenzene (Surr)106 05/05/23 09:06 185-114
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
1.9 U Q 9.7 0.73 ug/L 05/05/23 21:00 05/10/23 21:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.7 0.54 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q1,2,4-Trichlorobenzene
9.7 0.51 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q1,2-Dichlorobenzene
9.7 0.57 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q1,3-Dichlorobenzene
9.7 0.58 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q M1,3-Dinitrobenzene
9.7 0.52 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q1,4-Dichlorobenzene
9.7 0.60 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q1,4-Naphthoquinone
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q1-Naphthylamine
9.7 0.70 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q2,3,4,6-Tetrachlorophenol
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q2,4,5-Trichlorophenol
9.7 0.82 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U2,4,6-Trichlorophenol
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U2,4-Dichlorophenol
9.7 3.9 ug/L 05/05/23 21:00 05/10/23 21:29 19.7 U2,4-Dimethylphenol
48 9.7 ug/L 05/05/23 21:00 05/10/23 21:29 119 U Q2,4-Dinitrophenol
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q M2,4-Dinitrotoluene
9.7 0.70 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q2,6-Dichlorophenol
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q2,6-Dinitrotoluene
9.7 1.5 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U Q2-Acetylaminofluorene
9.7 0.77 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q2-Chloronaphthalene
9.7 0.84 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U2-Chlorophenol
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 21:29 13.6 J Q2-Methylnaphthalene
9.7 0.86 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U2-Methylphenol
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U Q2-Naphthylamine
48 1.3 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q2-Nitroaniline
9.7 0.73 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U2-Nitrophenol
9.7 1.3 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U3 & 4 Methylphenol
58 29 ug/L 05/05/23 21:00 05/10/23 21:29 158 U Q3,3'-Dichlorobenzidine
19 9.7 ug/L 05/05/23 21:00 05/10/23 21:29 113 U Q3,3'-Dimethylbenzidine
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U Q3-Methylcholanthrene
48 4.8 ug/L 05/05/23 21:00 05/10/23 21:29 19.7 U Q3-Nitroaniline
48 9.7 ug/L 05/05/23 21:00 05/10/23 21:29 119 U Q4,6-Dinitro-2-methylphenol
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U4-Aminobiphenyl
9.7 0.74 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q M4-Bromophenyl phenyl ether
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U4-Chloro-3-methylphenol
19 2.1 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U Q4-Chloroaniline
9.7 0.81 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q4-Chlorophenyl phenyl ether
48 4.8 ug/L 05/05/23 21:00 05/10/23 21:29 19.7 U Q4-Nitroaniline
48 1.8 ug/L 05/05/23 21:00 05/10/23 21:29 13.9 U Q4-Nitrophenol
24 9.7 ug/L 05/05/23 21:00 05/10/23 21:29 119 U M4-Nitroquinoline-1-oxide
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U Q5-Nitro-o-toluidine
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q7,12-Dimethylbenz(a)anthracene
9.7 0.73 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QAcenaphthene
9.7 0.82 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QAcenaphthylene
9.7 0.55 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U MAcetophenone
1900 34 ug/L 05/05/23 21:00 05/10/23 21:29 177 U Qalpha,alpha-Dimethyl phenethylamine
9.7 0.67 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QAnthracene
9.7 0.53 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QBenzo[a]anthracene
9.7 0.69 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QBenzo[a]pyrene
9.7 2.5 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U QBenzo[b]fluoranthene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.9 U Q 9.7 0.84 ug/L 05/05/23 21:00 05/10/23 21:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzo[g,h,i]perylene
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QBenzo[k]fluoranthene
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q MBenzyl alcohol
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q Mbis (2-chloroisopropyl) ether
9.7 0.91 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QBis(2-chloroethoxy)methane
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q MBis(2-chloroethyl)ether
9.7 1.5 ug/L 05/05/23 21:00 05/10/23 21:29 12.4 U QBis(2-ethylhexyl) phthalate
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QButyl benzyl phthalate
9.7 0.49 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QChrysene
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDiallate
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDibenz(a,h)anthracene
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDibenzofuran
9.7 0.85 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDiethyl phthalate
9.7 0.72 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDimethoate
9.7 0.96 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDimethyl phthalate
9.7 0.80 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDi-n-butyl phthalate
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 12.4 U QDi-n-octyl phthalate
9.7 4.8 ug/L 05/05/23 21:00 05/10/23 21:29 19.7 U QDinoseb
9.7 0.89 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 UDiphenylamine
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QDisulfoton
9.7 0.93 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QEthyl methanesulfonate
9.7 1.3 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q MEthyl Parathion
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QFamphur
9.7 0.71 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QFluoranthene
9.7 0.93 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QFluorene
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QHexachlorobenzene
9.7 0.60 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QHexachlorobutadiene
9.7 2.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U QHexachlorocyclopentadiene
9.7 0.73 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QHexachloroethane
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U QHexachloropropene
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QIndeno[1,2,3-cd]pyrene
9.7 0.87 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QIsophorone
9.7 0.48 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QIsosafrole
1900 2.6 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U QMethapyrilene
9.7 0.58 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QMethyl methanesulfonate
9.7 0.85 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U MMethyl parathion
9.7 0.68 ug/L 05/05/23 21:00 05/10/23 21:29 116 QNaphthalene
9.7 0.70 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QNitrobenzene
9.7 0.90 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 UN-Nitrosodiethylamine
9.7 2.7 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U QN-Nitrosodimethylamine
9.7 0.93 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QN-Nitrosodi-n-butylamine
9.7 0.70 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QN-Nitrosodi-n-propylamine
9.7 0.89 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QN-Nitrosodiphenylamine
9.7 3.2 ug/L 05/05/23 21:00 05/10/23 21:29 19.7 UN-Nitrosomethylethylamine
9.7 0.85 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QN-Nitrosopiperidine
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 UN-Nitrosopyrrolidine
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q Mo,o',o''-Triethylphosphorothioate
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 Uo-Toluidine
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Mp-Dimethylamino azobenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.9 U Q 9.7 0.50 ug/L 05/05/23 21:00 05/10/23 21:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Pentachlorobenzene
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 UPentachloronitrobenzene
48 1.9 ug/L 05/05/23 21:00 05/10/23 21:29 13.9 UPentachlorophenol
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 UPhenacetin
9.7 0.74 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QPhenanthrene
9.7 0.80 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QPhenol
9.7 0.84 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 UPhorate
1900 9.7 ug/L 05/05/23 21:00 05/10/23 21:29 124 U Qp-Phenylene diamine
9.7 0.86 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 UPronamide
9.7 0.61 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QPyrene
9.7 0.77 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U QSafrole, Total
9.7 1.9 ug/L 05/05/23 21:00 05/10/23 21:29 14.8 U Qsym-Trinitrobenzene
9.7 0.88 ug/L 05/05/23 21:00 05/10/23 21:29 11.9 U Q MThionazin
2,4,6-Tribromophenol (Surr)60 43-140 05/05/23 21:00 05/10/23 21:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)43 Q 05/05/23 21:00 05/10/23 21:29 144-119
2-Fluorophenol (Surr)32 05/05/23 21:00 05/10/23 21:29 119-119
Nitrobenzene-d5 (Surr)39 Q 05/05/23 21:00 05/10/23 21:29 144-120
Phenol-d5 (Surr)25 Q 05/05/23 21:00 05/10/23 21:29 127-110
Terphenyl-d14 (Surr)35 Q 05/05/23 21:00 05/10/23 21:29 150-134
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE
LOQ DL
2.0 U H Q 10 0.76 ug/L 05/20/23 21:30 05/24/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
10 0.56 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q1,2,4-Trichlorobenzene
10 0.53 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q1,2-Dichlorobenzene
10 0.59 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q1,3-Dichlorobenzene
10 0.60 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M Q1,3-Dinitrobenzene
10 0.54 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q1,4-Dichlorobenzene
10 0.62 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q1,4-Naphthoquinone
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q1-Naphthylamine
10 0.72 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2,3,4,6-Tetrachlorophenol
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2,4,5-Trichlorophenol
10 0.85 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2,4,6-Trichlorophenol
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2,4-Dichlorophenol
10 4.0 ug/L 05/20/23 21:30 05/24/23 22:27 110 U H Q2,4-Dimethylphenol
50 10 ug/L 05/20/23 21:30 05/24/23 22:27 120 U H Q2,4-Dinitrophenol
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M Q2,4-Dinitrotoluene
10 0.73 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2,6-Dichlorophenol
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2,6-Dinitrotoluene
10 1.6 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Q2-Acetylaminofluorene
10 0.80 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2-Chloronaphthalene
10 0.87 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2-Chlorophenol
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:27 14.8 J H Q2-Methylnaphthalene
10 0.89 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2-Methylphenol
10 1.5 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Q2-Naphthylamine
50 1.3 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2-Nitroaniline
10 0.76 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q2-Nitrophenol
10 1.3 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q3 & 4 Methylphenol
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
60 U H Q 60 30 ug/L 05/20/23 21:30 05/24/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
3,3'-Dichlorobenzidine
20 10 ug/L 05/20/23 21:30 05/24/23 22:27 113 U H Q3,3'-Dimethylbenzidine
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Q3-Methylcholanthrene
50 5.0 ug/L 05/20/23 21:30 05/24/23 22:27 110 U H Q3-Nitroaniline
50 10 ug/L 05/20/23 21:30 05/24/23 22:27 120 U H Q4,6-Dinitro-2-methylphenol
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q4-Aminobiphenyl
10 0.77 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M Q4-Bromophenyl phenyl ether
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q4-Chloro-3-methylphenol
20 2.2 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Q4-Chloroaniline
10 0.84 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q4-Chlorophenyl phenyl ether
50 5.0 ug/L 05/20/23 21:30 05/24/23 22:27 110 U H Q4-Nitroaniline
50 1.9 ug/L 05/20/23 21:30 05/24/23 22:27 14.0 U H Q4-Nitrophenol
25 10 ug/L 05/20/23 21:30 05/24/23 22:27 120 U H Q4-Nitroquinoline-1-oxide
10 1.5 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Q5-Nitro-o-toluidine
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Q7,12-Dimethylbenz(a)anthracene
10 0.76 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QAcenaphthene
10 0.85 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QAcenaphthylene
10 0.57 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QAcetophenone
2000 35 ug/L 05/20/23 21:30 05/24/23 22:27 180 U H Qalpha,alpha-Dimethyl phenethylamine
10 0.69 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QAnthracene
10 0.55 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QBenzo[a]anthracene
10 0.71 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QBenzo[a]pyrene
10 2.6 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H QBenzo[b]fluoranthene
10 0.87 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QBenzo[g,h,i]perylene
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QBenzo[k]fluoranthene
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M QBenzyl alcohol
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H Qbis (2-chloroisopropyl) ether
10 0.94 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QBis(2-chloroethoxy)methane
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QBis(2-chloroethyl)ether
10 1.6 ug/L 05/20/23 21:30 05/24/23 22:27 12.5 U H QBis(2-ethylhexyl) phthalate
10 1.2 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QButyl benzyl phthalate
10 0.51 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QChrysene
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDiallate
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDibenz(a,h)anthracene
10 0.79 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDibenzofuran
10 0.88 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M QDiethyl phthalate
10 0.75 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDimethoate
10 0.99 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDimethyl phthalate
10 0.83 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDi-n-butyl phthalate
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:27 12.5 U H QDi-n-octyl phthalate
10 5.0 ug/L 05/20/23 21:30 05/24/23 22:27 110 U HDinoseb
10 0.92 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDiphenylamine
10 0.79 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QDisulfoton
10 0.96 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QEthyl methanesulfonate
10 1.3 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M QEthyl Parathion
10 1.1 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QFamphur
10 0.74 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QFluoranthene
10 0.96 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QFluorene
10 0.79 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QHexachlorobenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
2.0 U H Q 10 0.62 ug/L 05/20/23 21:30 05/24/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Hexachlorobutadiene
10 2.5 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H QHexachlorocyclopentadiene
10 0.76 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QHexachloroethane
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H QHexachloropropene
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QIndeno[1,2,3-cd]pyrene
10 0.90 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QIsophorone
10 0.50 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QIsosafrole
2000 2.7 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H QMethapyrilene
10 0.60 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QMethyl methanesulfonate
10 0.88 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M QMethyl parathion
10 0.70 ug/L 05/20/23 21:30 05/24/23 22:27 121 H QNaphthalene
10 0.73 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M QNitrobenzene
10 0.93 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QN-Nitrosodiethylamine
10 2.8 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H QN-Nitrosodimethylamine
10 0.96 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QN-Nitrosodi-n-butylamine
10 0.72 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QN-Nitrosodi-n-propylamine
10 0.92 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QN-Nitrosodiphenylamine
10 3.3 ug/L 05/20/23 21:30 05/24/23 22:27 110 U H QN-Nitrosomethylethylamine
10 0.88 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QN-Nitrosopiperidine
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QN-Nitrosopyrrolidine
10 1.0 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M Qo,o',o''-Triethylphosphorothioate
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Qo-Toluidine
10 0.79 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M Qp-Dimethylamino azobenzene
10 0.52 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QPentachlorobenzene
10 0.78 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U HPentachloronitrobenzene
50 2.0 ug/L 05/20/23 21:30 05/24/23 22:27 14.0 U H QPentachlorophenol
10 1.4 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U HPhenacetin
10 0.77 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QPhenanthrene
10 0.83 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QPhenol
10 0.87 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QPhorate
2000 10 ug/L 05/20/23 21:30 05/24/23 22:27 125 U H Qp-Phenylene diamine
10 0.89 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QPronamide
10 0.63 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QPyrene
10 0.80 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H QSafrole, Total
10 2.0 ug/L 05/20/23 21:30 05/24/23 22:27 15.0 U H Qsym-Trinitrobenzene
10 0.91 ug/L 05/20/23 21:30 05/24/23 22:27 12.0 U H M QThionazin
2,4,6-Tribromophenol (Surr)76 43-140 05/20/23 21:30 05/24/23 22:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)55 05/20/23 21:30 05/24/23 22:27 144-119
2-Fluorophenol (Surr)31 Q 05/20/23 21:30 05/24/23 22:27 119-119
Nitrobenzene-d5 (Surr)55 05/20/23 21:30 05/24/23 22:27 144-120
Phenol-d5 (Surr)6 Q 05/20/23 21:30 05/24/23 22:27 127-110
Terphenyl-d14 (Surr)33 Q 05/20/23 21:30 05/24/23 22:27 150-134
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
440 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
3.8 J 5.0 1.0 ug/L 05/10/23 13:17 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 13:17 1110 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 13:17 1170 MC9-C10 Aromatics
100 25 ug/L 05/10/23 13:17 1330 MC9-C12 Aliphatics
5.0 1.0 ug/L 05/10/23 13:17 13.0 JEthylbenzene
5.0 1.0 ug/L 05/10/23 13:17 12.0 UMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 13:17 128 MNaphthalene
5.0 1.0 ug/L 05/10/23 13:17 12.0 UToluene
100 25 ug/L 05/10/23 13:17 1150C9-C12 Aliphatics (adjusted)
10 2.5 ug/L 05/10/23 13:17 15.0 Um-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 13:17 12.0 Uo-Xylene
100 25 ug/L 05/10/23 13:17 1100C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)123 M 70-130 05/10/23 13:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)99 05/10/23 13:17 170-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U 2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:55 1150Total EPH
12 5.1 ug/L 05/08/23 09:17 05/13/23 12:12 110 UPyrene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UBenzo[g,h,i]perylene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UBenzo[b]fluoranthene
2.0 0.51 ug/L 05/08/23 09:17 05/13/23 12:12 11.0 UFluoranthene
4.1 1.5 ug/L 05/08/23 09:17 05/13/23 12:12 13.1 UBenzo[k]fluoranthene
2.0 0.71 ug/L 05/08/23 09:17 05/13/23 12:12 11.4 JAcenaphthylene
2.0 0.51 ug/L 05/08/23 09:17 05/13/23 12:12 11.0 UChrysene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UBenzo[a]pyrene
2.0 0.51 ug/L 05/08/23 09:17 05/13/23 12:12 11.0 UDibenz(a,h)anthracene
2.0 0.71 ug/L 05/08/23 09:17 05/13/23 12:12 11.4 UBenzo[a]anthracene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UAcenaphthene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UPhenanthrene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 UFluorene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 117 MNaphthalene
2.0 0.61 ug/L 05/08/23 09:17 05/13/23 12:12 11.2 U2-Methylnaphthalene
41 10 ug/L 05/08/23 09:17 05/13/23 12:12 153 MC11-C22 Aromatics (unadjusted)
41 10 ug/L 05/08/23 09:17 05/13/23 12:12 133 JC11-C22 Aromatics (Adjusted)
51 10 ug/L 05/08/23 09:17 05/13/23 13:42 120 UC19-C36 Aliphatics
31 10 ug/L 05/08/23 09:17 05/13/23 13:42 192 M BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)47 40-140 05/08/23 09:17 05/13/23 13:42 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)68 05/08/23 09:17 05/13/23 12:12 140-140
o- terphenyl (Surr)45 05/08/23 09:17 05/13/23 12:12 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U M H 2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-2Client Sample ID: 308-DUP-1-04-23
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
10 U M H 12 5.1 ug/L 05/23/23 09:00 06/01/23 06:37 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Pyrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HBenzo[g,h,i]perylene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HIndeno[1,2,3-cd]pyrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HBenzo[b]fluoranthene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 06:37 11.0 U M HFluoranthene
4.1 1.5 ug/L 05/23/23 09:00 06/01/23 06:37 13.1 U M HBenzo[k]fluoranthene
2.0 0.71 ug/L 05/23/23 09:00 06/01/23 06:37 11.4 J M HAcenaphthylene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 06:37 11.0 U HChrysene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HBenzo[a]pyrene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 06:37 11.0 U M HDibenz(a,h)anthracene
2.0 0.71 ug/L 05/23/23 09:00 06/01/23 06:37 11.4 U M HBenzo[a]anthracene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HAcenaphthene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HPhenanthrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 11.2 U M HFluorene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 117 M HNaphthalene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 06:37 15.5 M H2-Methylnaphthalene
41 10 ug/L 05/23/23 09:00 06/01/23 06:37 162 M HC11-C22 Aromatics (unadjusted)
41 10 ug/L 05/23/23 09:00 06/01/23 06:37 137 J HC11-C22 Aromatics (Adjusted)
51 10 ug/L 05/23/23 09:00 06/01/23 07:00 120 U M HC19-C36 Aliphatics
31 10 ug/L 05/23/23 09:00 06/01/23 07:00 197 H BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)50 M 40-140 05/23/23 09:00 06/01/23 07:00 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)84 05/23/23 09:00 06/01/23 06:37 140-140
o- terphenyl (Surr)60 05/23/23 09:00 06/01/23 06:37 140-140
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 05/05/23 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
50 20 ug/L 05/05/23 09:29 140 U Q MAcetonitrile
50 15 ug/L 05/05/23 09:29 123 JAcrolein
50 5.5 ug/L 05/05/23 09:29 120 U MAcrylonitrile
2.0 0.27 ug/L 05/05/23 09:29 14.5Benzene
1.0 0.24 ug/L 05/05/23 09:29 10.50 UBromobenzene
2.0 0.34 ug/L 05/05/23 09:29 11.0 UBromochloromethane
2.0 0.25 ug/L 05/05/23 09:29 11.0 UBromodichloromethane
2.5 0.59 ug/L 05/05/23 09:29 12.0 U QBromoform
20 3.7 ug/L 05/05/23 09:29 110 U QBromomethane
25 6.4 ug/L 05/05/23 09:29 120 U M2-Butanone (MEK)
2.5 0.52 ug/L 05/05/23 09:29 12.0 Un-Butylbenzene
2.5 0.53 ug/L 05/05/23 09:29 14.0sec-Butylbenzene
2.0 0.43 ug/L 05/05/23 09:29 10.95 Jtert-Butylbenzene
2.0 0.43 ug/L 05/05/23 09:29 10.79 JCarbon disulfide
2.0 0.30 ug/L 05/05/23 09:29 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/05/23 09:29 10.50 UChlorobenzene
2.5 0.71 ug/L 05/05/23 09:29 12.0 U2-Chloro-1,3-butadiene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 4.6 ug/L 05/05/23 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Chloroethane
25 0.59 ug/L 05/05/23 09:29 120 U2-Chloroethyl vinyl ether
2.0 0.27 ug/L 05/05/23 09:29 11.0 U MChloroform
2.5 0.54 ug/L 05/05/23 09:29 12.0 UChloromethane
5.0 1.1 ug/L 05/05/23 09:29 14.0 UAllyl chloride
1.0 0.25 ug/L 05/05/23 09:29 10.50 U2-Chlorotoluene
2.0 0.41 ug/L 05/05/23 09:29 11.0 U4-Chlorotoluene
2.0 0.39 ug/L 05/05/23 09:29 11.0 UChlorodibromomethane
10 1.8 ug/L 05/05/23 09:29 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/05/23 09:29 11.0 U1,2-Dibromoethane
2.0 0.34 ug/L 05/05/23 09:29 11.0 UDibromomethane
2.0 0.31 ug/L 05/05/23 09:29 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 09:29 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 09:29 11.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/05/23 09:29 15.0 U Q Mtrans-1,4-Dichloro-2-butene
2.0 0.36 ug/L 05/05/23 09:29 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/05/23 09:29 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 05/05/23 09:29 11.0 U M1,2-Dichloroethane
2.0 0.25 ug/L 05/05/23 09:29 11.0 Ucis-1,2-Dichloroethene
2.0 0.34 ug/L 05/05/23 09:29 11.0 Utrans-1,2-Dichloroethene
2.0 0.37 ug/L 05/05/23 09:29 11.0 U1,2-Dichloroethene, Total
2.0 0.33 ug/L 05/05/23 09:29 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/05/23 09:29 10.50 U1,2-Dichloropropane
2.0 0.36 ug/L 05/05/23 09:29 11.0 U1,3-Dichloropropane
2.0 0.35 ug/L 05/05/23 09:29 11.0 U2,2-Dichloropropane
2.0 0.28 ug/L 05/05/23 09:29 11.0 U1,1-Dichloropropene
2.0 0.26 ug/L 05/05/23 09:29 11.0 Ucis-1,3-Dichloropropene
2.0 0.23 ug/L 05/05/23 09:29 11.0 Utrans-1,3-Dichloropropene
1.0 0.20 ug/L 05/05/23 09:29 14.4Ethylbenzene
2.0 0.33 ug/L 05/05/23 09:29 11.0 UEthyl methacrylate
5.0 0.22 ug/L 05/05/23 09:29 11.0 UHexachlorobutadiene
20 3.2 ug/L 05/05/23 09:29 110 U2-Hexanone
20 3.9 ug/L 05/05/23 09:29 110 U QIodomethane
500 68 ug/L 05/05/23 09:29 1250 U MIsobutyl alcohol
2.0 0.26 ug/L 05/05/23 09:29 111Isopropylbenzene
2.0 0.44 ug/L 05/05/23 09:29 11.9 Jp-Isopropyltoluene
20 5.0 ug/L 05/05/23 09:29 110 U Q MMethacrylonitrile
20 3.2 ug/L 05/05/23 09:29 110 UMethylene Chloride
2.5 0.78 ug/L 05/05/23 09:29 12.0 UMethyl methacrylate
20 2.7 ug/L 05/05/23 09:29 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/05/23 09:29 12.0 UMethyl tert-butyl ether
10 2.4 ug/L 05/05/23 09:29 130Naphthalene
5.0 0.50 ug/L 05/05/23 09:29 11.0 U QPentachloroethane
20 5.0 ug/L 05/05/23 09:29 110 U Q MPropionitrile
2.0 0.41 ug/L 05/05/23 09:29 111N-Propylbenzene
2.0 0.27 ug/L 05/05/23 09:29 11.0 U MStyrene
2.0 0.36 ug/L 05/05/23 09:29 11.0 U1,1,1,2-Tetrachloroethane
2.0 0.40 ug/L 05/05/23 09:29 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/05/23 09:29 11.0 UTetrachloroethene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U 2.0 0.25 ug/L 05/05/23 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Toluene
5.0 0.81 ug/L 05/05/23 09:29 12.0 U1,2,3-Trichlorobenzene
5.0 0.53 ug/L 05/05/23 09:29 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/05/23 09:29 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/05/23 09:29 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/05/23 09:29 10.50 UTrichloroethene
2.0 0.33 ug/L 05/05/23 09:29 11.0 UTrichlorofluoromethane
2.0 0.48 ug/L 05/05/23 09:29 11.0 U1,2,3-Trichloropropane
1.0 0.23 ug/L 05/05/23 09:29 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.43 ug/L 05/05/23 09:29 1441,2,4-Trimethylbenzene
2.0 0.28 ug/L 05/05/23 09:29 11.0 U1,3,5-Trimethylbenzene
2.5 0.69 ug/L 05/05/23 09:29 12.0 UVinyl acetate
2.0 0.40 ug/L 05/05/23 09:29 11.0 UVinyl chloride
2.0 0.26 ug/L 05/05/23 09:29 11.0 Uo-Xylene
2.0 0.49 ug/L 05/05/23 09:29 14.3m-Xylene & p-Xylene
2.0 0.49 ug/L 05/05/23 09:29 14.3Xylenes, Total
2.0 0.28 ug/L 05/05/23 09:29 16.3Cyclohexane
5.0 1.1 ug/L 05/05/23 09:29 14.0 U M1-Chlorohexane
20 3.2 ug/L 05/05/23 09:29 110 UMethyl acetate
2.0 0.33 ug/L 05/05/23 09:29 12.5Methylcyclohexane
10 2.1 ug/L 05/05/23 09:29 15.0 UTetrahydrofuran
10 0.70 ug/L 05/05/23 09:29 12.0 UDiisopropyl ether
5.0 0.65 ug/L 05/05/23 09:29 12.0 U MHexane
5.0 0.37 ug/L 05/05/23 09:29 11.0 UDiethyl ether
2.0 0.43 ug/L 05/05/23 09:29 11.0 U MHeptane
2.0 0.48 ug/L 05/05/23 09:29 11.0 U1,3-Dichloropropene, Total
10 2.5 ug/L 05/05/23 09:29 16.7 J Q2-Methylnaphthalene
2.0 0.38 ug/L 05/05/23 09:29 11.0 U1,3-Butadiene
5.0 0.50 ug/L 05/05/23 09:29 11.0 U Qn-Butyl acetate
2.0 0.50 ug/L 05/05/23 09:29 11.0 UDichlorofluoromethane
10 2.5 ug/L 05/05/23 09:29 15.0 U QBenzyl chloride
50 6.9 ug/L 05/05/23 09:29 120 Utert-Butyl alcohol
200 50 ug/L 05/05/23 09:29 1100 U QEthanol
250 92 ug/L 05/05/23 09:29 1200 U Q1,4-Dioxane
4.0 0.86 ug/L 05/05/23 09:29 12.0 U Q M2-Nitropropane
10 2.5 ug/L 05/05/23 09:29 15.0 U1,3,5-Trichlorobenzene
10 2.5 ug/L 05/05/23 09:29 111 Q1,2,3-Trimethylbenzene
100 25 ug/L 05/05/23 09:29 150 U Q Mn-Butyl alcohol
2.5 0.78 ug/L 05/05/23 09:29 12.0 UTert-amyl methyl ether
100 25 ug/L 05/05/23 09:29 150 U Q2-Propanol
2.5 0.72 ug/L 05/05/23 09:29 12.0 UEthyl tert-butyl ether
20 5.0 ug/L 05/05/23 09:29 110 U QEthyl acetate
25 8.6 ug/L 05/05/23 09:29 120 U Q M2-Butanol, 2-methyl-
5.0 0.99 ug/L 05/05/23 09:29 12.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)99 89-112 05/05/23 09:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)85 05/05/23 09:29 181-118
Dibromofluoromethane (Surr)93 05/05/23 09:29 180-119
4-Bromofluorobenzene (Surr)109 05/05/23 09:29 185-114
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Page 27 of 124 6/5/2023
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
2.0 U 10 0.76 ug/L 05/05/23 21:00 05/10/23 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
10 0.56 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U1,2,4-Trichlorobenzene
10 0.53 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U1,2-Dichlorobenzene
10 0.59 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U1,3-Dichlorobenzene
10 0.60 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U M1,3-Dinitrobenzene
10 0.54 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U1,4-Dichlorobenzene
10 0.62 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Q1,4-Naphthoquinone
10 1.1 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U1-Naphthylamine
10 0.72 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Q2,3,4,6-Tetrachlorophenol
10 1.2 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Q2,4,5-Trichlorophenol
10 0.85 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2,4,6-Trichlorophenol
10 1.1 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2,4-Dichlorophenol
10 4.0 ug/L 05/05/23 21:00 05/10/23 21:51 110 U2,4-Dimethylphenol
50 10 ug/L 05/05/23 21:00 05/10/23 21:51 120 U Q2,4-Dinitrophenol
10 1.2 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2,4-Dinitrotoluene
10 0.73 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2,6-Dichlorophenol
10 1.1 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2,6-Dinitrotoluene
10 1.6 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U Q2-Acetylaminofluorene
10 0.80 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2-Chloronaphthalene
10 0.87 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2-Chlorophenol
10 0.78 ug/L 05/05/23 21:00 05/10/23 21:51 13.6 J2-Methylnaphthalene
10 0.89 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2-Methylphenol
10 1.5 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U2-Naphthylamine
50 1.3 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2-Nitroaniline
10 0.76 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U2-Nitrophenol
10 1.3 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U3 & 4 Methylphenol
60 30 ug/L 05/05/23 21:00 05/10/23 21:51 160 U3,3'-Dichlorobenzidine
20 10 ug/L 05/05/23 21:00 05/10/23 21:51 113 U Q3,3'-Dimethylbenzidine
10 1.4 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U Q3-Methylcholanthrene
50 5.0 ug/L 05/05/23 21:00 05/10/23 21:51 110 U3-Nitroaniline
50 10 ug/L 05/05/23 21:00 05/10/23 21:51 120 U Q4,6-Dinitro-2-methylphenol
10 1.2 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U4-Aminobiphenyl
10 0.77 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U M4-Bromophenyl phenyl ether
10 1.0 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U4-Chloro-3-methylphenol
20 2.2 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U M4-Chloroaniline
10 0.84 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U4-Chlorophenyl phenyl ether
50 5.0 ug/L 05/05/23 21:00 05/10/23 21:51 110 U4-Nitroaniline
50 1.9 ug/L 05/05/23 21:00 05/10/23 21:51 14.0 U Q4-Nitrophenol
25 10 ug/L 05/05/23 21:00 05/10/23 21:51 120 U4-Nitroquinoline-1-oxide
10 1.5 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U5-Nitro-o-toluidine
10 1.2 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Q7,12-Dimethylbenz(a)anthracene
10 0.76 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QAcenaphthene
10 0.85 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QAcenaphthylene
10 0.57 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U MAcetophenone
2000 35 ug/L 05/05/23 21:00 05/10/23 21:51 180 Ualpha,alpha-Dimethyl phenethylamine
10 0.69 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QAnthracene
10 0.55 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QBenzo[a]anthracene
10 0.71 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QBenzo[a]pyrene
10 2.6 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U QBenzo[b]fluoranthene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U Q 10 0.87 ug/L 05/05/23 21:00 05/10/23 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzo[g,h,i]perylene
10 1.2 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QBenzo[k]fluoranthene
10 1.1 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U MBenzyl alcohol
10 0.78 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Mbis (2-chloroisopropyl) ether
10 0.94 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UBis(2-chloroethoxy)methane
10 1.1 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UBis(2-chloroethyl)ether
10 1.6 ug/L 05/05/23 21:00 05/10/23 21:51 12.5 UBis(2-ethylhexyl) phthalate
10 1.2 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UButyl benzyl phthalate
10 0.51 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QChrysene
10 0.78 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QDiallate
10 1.0 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UDibenz(a,h)anthracene
10 0.79 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UDibenzofuran
10 0.88 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UDiethyl phthalate
10 0.75 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QDimethoate
10 0.99 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UDimethyl phthalate
10 0.83 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UDi-n-butyl phthalate
10 1.4 ug/L 05/05/23 21:00 05/10/23 21:51 12.5 UDi-n-octyl phthalate
10 5.0 ug/L 05/05/23 21:00 05/10/23 21:51 110 U QDinoseb
10 0.92 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UDiphenylamine
10 0.79 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Q MDisulfoton
10 0.96 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QEthyl methanesulfonate
10 1.3 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Q MEthyl Parathion
10 1.1 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QFamphur
10 0.74 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QFluoranthene
10 0.96 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QFluorene
10 0.79 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UHexachlorobenzene
10 0.62 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QHexachlorobutadiene
10 2.5 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 UHexachlorocyclopentadiene
10 0.76 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UHexachloroethane
10 1.4 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U QHexachloropropene
10 1.0 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QIndeno[1,2,3-cd]pyrene
10 0.90 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UIsophorone
10 0.50 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QIsosafrole
2000 2.7 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U QMethapyrilene
10 0.60 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QMethyl methanesulfonate
10 0.88 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U MMethyl parathion
10 0.70 ug/L 05/05/23 21:00 05/10/23 21:51 117 QNaphthalene
10 0.73 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UNitrobenzene
10 0.93 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UN-Nitrosodiethylamine
10 2.8 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U QN-Nitrosodimethylamine
10 0.96 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UN-Nitrosodi-n-butylamine
10 0.72 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U MN-Nitrosodi-n-propylamine
10 0.92 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UN-Nitrosodiphenylamine
10 3.3 ug/L 05/05/23 21:00 05/10/23 21:51 110 UN-Nitrosomethylethylamine
10 0.88 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UN-Nitrosopiperidine
10 1.0 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UN-Nitrosopyrrolidine
10 1.0 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Mo,o',o''-Triethylphosphorothioate
10 1.4 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 Uo-Toluidine
10 0.79 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U Mp-Dimethylamino azobenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U Q 10 0.52 ug/L 05/05/23 21:00 05/10/23 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Pentachlorobenzene
10 0.78 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UPentachloronitrobenzene
50 2.0 ug/L 05/05/23 21:00 05/10/23 21:51 14.0 UPentachlorophenol
10 1.4 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 UPhenacetin
10 0.77 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QPhenanthrene
10 0.83 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QPhenol
10 0.87 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UPhorate
2000 10 ug/L 05/05/23 21:00 05/10/23 21:51 125 U Q Mp-Phenylene diamine
10 0.89 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 UPronamide
10 0.63 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QPyrene
10 0.80 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QSafrole, Total
10 2.0 ug/L 05/05/23 21:00 05/10/23 21:51 15.0 U Qsym-Trinitrobenzene
10 0.91 ug/L 05/05/23 21:00 05/10/23 21:51 12.0 U QThionazin
2,4,6-Tribromophenol (Surr)63 43-140 05/05/23 21:00 05/10/23 21:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)47 05/05/23 21:00 05/10/23 21:51 144-119
2-Fluorophenol (Surr)36 05/05/23 21:00 05/10/23 21:51 119-119
Nitrobenzene-d5 (Surr)45 05/05/23 21:00 05/10/23 21:51 144-120
Phenol-d5 (Surr)25 Q 05/05/23 21:00 05/10/23 21:51 127-110
Terphenyl-d14 (Surr)41 Q 05/05/23 21:00 05/10/23 21:51 150-134
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
440 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
4.2 J 5.0 1.0 ug/L 05/10/23 13:58 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 13:58 1100 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 13:58 1180 MC9-C10 Aromatics
100 25 ug/L 05/10/23 13:58 1340 MC9-C12 Aliphatics
5.0 1.0 ug/L 05/10/23 13:58 13.3 JEthylbenzene
5.0 1.0 ug/L 05/10/23 13:58 12.0 UMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 13:58 129 MNaphthalene
5.0 1.0 ug/L 05/10/23 13:58 12.0 UToluene
100 25 ug/L 05/10/23 13:58 1160C9-C12 Aliphatics (adjusted)
10 2.5 ug/L 05/10/23 13:58 12.7 Jm-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 13:58 12.0 Uo-Xylene
100 25 ug/L 05/10/23 13:58 198 JC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)123 70-130 05/10/23 13:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)100 05/10/23 13:58 170-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.1 U 1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:55 160 UTotal EPH
11 4.8 ug/L 05/08/23 09:17 05/13/23 12:35 19.5 UPyrene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UBenzo[g,h,i]perylene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
1.1 U 1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Indeno[1,2,3-cd]pyrene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UBenzo[b]fluoranthene
1.9 0.48 ug/L 05/08/23 09:17 05/13/23 12:35 10.95 UFluoranthene
3.8 1.4 ug/L 05/08/23 09:17 05/13/23 12:35 12.9 UBenzo[k]fluoranthene
1.9 0.67 ug/L 05/08/23 09:17 05/13/23 12:35 11.3 UAcenaphthylene
1.9 0.48 ug/L 05/08/23 09:17 05/13/23 12:35 10.95 UChrysene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UBenzo[a]pyrene
1.9 0.48 ug/L 05/08/23 09:17 05/13/23 12:35 10.95 UDibenz(a,h)anthracene
1.9 0.67 ug/L 05/08/23 09:17 05/13/23 12:35 11.3 UBenzo[a]anthracene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UAcenaphthene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UPhenanthrene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UFluorene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 11.1 UNaphthalene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 12:35 10.59 J2-Methylnaphthalene
38 9.5 ug/L 05/08/23 09:17 05/13/23 12:35 112 JC11-C22 Aromatics (unadjusted)
38 9.5 ug/L 05/08/23 09:17 05/13/23 12:35 110 JC11-C22 Aromatics (Adjusted)
48 9.5 ug/L 05/08/23 09:17 05/13/23 14:05 119 UC19-C36 Aliphatics
29 9.5 ug/L 05/08/23 09:17 05/13/23 14:05 117 J BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)51 40-140 05/08/23 09:17 05/13/23 14:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)67 05/08/23 09:17 05/13/23 12:35 140-140
o- terphenyl (Surr)59 05/08/23 09:17 05/13/23 12:35 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U M H 2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
12 4.9 ug/L 05/23/23 09:00 06/01/23 07:00 19.9 U M HPyrene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U HBenzo[g,h,i]perylene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U HIndeno[1,2,3-cd]pyrene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U HBenzo[b]fluoranthene
2.0 0.49 ug/L 05/23/23 09:00 06/01/23 07:00 10.99 U M HFluoranthene
4.0 1.5 ug/L 05/23/23 09:00 06/01/23 07:00 13.0 U HBenzo[k]fluoranthene
2.0 0.69 ug/L 05/23/23 09:00 06/01/23 07:00 11.7 J M HAcenaphthylene
2.0 0.49 ug/L 05/23/23 09:00 06/01/23 07:00 10.99 U M HChrysene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U HBenzo[a]pyrene
2.0 0.49 ug/L 05/23/23 09:00 06/01/23 07:00 10.99 U HDibenz(a,h)anthracene
2.0 0.69 ug/L 05/23/23 09:00 06/01/23 07:00 11.4 U M HBenzo[a]anthracene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U M HAcenaphthene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U M HPhenanthrene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 11.2 U M HFluorene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 120 M HNaphthalene
2.0 0.59 ug/L 05/23/23 09:00 06/01/23 07:00 16.8 M H2-Methylnaphthalene
40 9.9 ug/L 05/23/23 09:00 06/01/23 07:00 177 M HC11-C22 Aromatics (unadjusted)
40 9.9 ug/L 05/23/23 09:00 06/01/23 07:00 148 HC11-C22 Aromatics (Adjusted)
49 9.9 ug/L 05/23/23 09:00 06/01/23 07:22 120 U M HC19-C36 Aliphatics
30 9.9 ug/L 05/23/23 09:00 06/01/23 07:22 186 H BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)41 M 40-140 05/23/23 09:00 06/01/23 07:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-3Client Sample ID: MW7-20-04-23
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
2-Fluorobiphenyl (Surr)92 40-140 05/23/23 09:00 06/01/23 07:00 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
o- terphenyl (Surr)65 05/23/23 09:00 06/01/23 07:00 140-140
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 05/05/23 09:52 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
50 20 ug/L 05/05/23 09:52 140 U Q MAcetonitrile
50 15 ug/L 05/05/23 09:52 140 UAcrolein
50 5.5 ug/L 05/05/23 09:52 120 UAcrylonitrile
2.0 0.27 ug/L 05/05/23 09:52 11.0 UBenzene
1.0 0.24 ug/L 05/05/23 09:52 10.50 UBromobenzene
2.0 0.34 ug/L 05/05/23 09:52 11.0 UBromochloromethane
2.0 0.25 ug/L 05/05/23 09:52 11.0 UBromodichloromethane
2.5 0.59 ug/L 05/05/23 09:52 12.0 U QBromoform
20 3.7 ug/L 05/05/23 09:52 110 U QBromomethane
25 6.4 ug/L 05/05/23 09:52 120 U2-Butanone (MEK)
2.5 0.52 ug/L 05/05/23 09:52 12.0 Un-Butylbenzene
2.5 0.53 ug/L 05/05/23 09:52 10.67 Jsec-Butylbenzene
2.0 0.43 ug/L 05/05/23 09:52 11.0 Utert-Butylbenzene
2.0 0.43 ug/L 05/05/23 09:52 10.71 JCarbon disulfide
2.0 0.30 ug/L 05/05/23 09:52 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/05/23 09:52 10.50 UChlorobenzene
2.5 0.71 ug/L 05/05/23 09:52 12.0 U2-Chloro-1,3-butadiene
20 4.6 ug/L 05/05/23 09:52 110 UChloroethane
25 0.59 ug/L 05/05/23 09:52 120 U2-Chloroethyl vinyl ether
2.0 0.27 ug/L 05/05/23 09:52 11.0 UChloroform
2.5 0.54 ug/L 05/05/23 09:52 12.0 UChloromethane
5.0 1.1 ug/L 05/05/23 09:52 14.0 U MAllyl chloride
1.0 0.25 ug/L 05/05/23 09:52 10.50 U2-Chlorotoluene
2.0 0.41 ug/L 05/05/23 09:52 11.0 U4-Chlorotoluene
2.0 0.39 ug/L 05/05/23 09:52 11.0 UChlorodibromomethane
10 1.8 ug/L 05/05/23 09:52 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/05/23 09:52 11.0 U1,2-Dibromoethane
2.0 0.34 ug/L 05/05/23 09:52 11.0 UDibromomethane
2.0 0.31 ug/L 05/05/23 09:52 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 09:52 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 09:52 11.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/05/23 09:52 15.0 U Qtrans-1,4-Dichloro-2-butene
2.0 0.36 ug/L 05/05/23 09:52 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/05/23 09:52 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 05/05/23 09:52 11.0 U M1,2-Dichloroethane
2.0 0.25 ug/L 05/05/23 09:52 11.0 Ucis-1,2-Dichloroethene
2.0 0.34 ug/L 05/05/23 09:52 11.0 Utrans-1,2-Dichloroethene
2.0 0.37 ug/L 05/05/23 09:52 11.0 U1,2-Dichloroethene, Total
2.0 0.33 ug/L 05/05/23 09:52 11.0 U1,1-Dichloroethene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
0.50 U 1.0 0.22 ug/L 05/05/23 09:52 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2-Dichloropropane
2.0 0.36 ug/L 05/05/23 09:52 11.0 U1,3-Dichloropropane
2.0 0.35 ug/L 05/05/23 09:52 11.0 U2,2-Dichloropropane
2.0 0.28 ug/L 05/05/23 09:52 11.0 U1,1-Dichloropropene
2.0 0.26 ug/L 05/05/23 09:52 11.0 Ucis-1,3-Dichloropropene
2.0 0.23 ug/L 05/05/23 09:52 11.0 Utrans-1,3-Dichloropropene
1.0 0.20 ug/L 05/05/23 09:52 10.50 U MEthylbenzene
2.0 0.33 ug/L 05/05/23 09:52 11.0 UEthyl methacrylate
5.0 0.22 ug/L 05/05/23 09:52 11.0 UHexachlorobutadiene
20 3.2 ug/L 05/05/23 09:52 110 U2-Hexanone
20 3.9 ug/L 05/05/23 09:52 110 U QIodomethane
500 68 ug/L 05/05/23 09:52 1250 UIsobutyl alcohol
2.0 0.26 ug/L 05/05/23 09:52 10.51 JIsopropylbenzene
2.0 0.44 ug/L 05/05/23 09:52 11.0 Up-Isopropyltoluene
20 5.0 ug/L 05/05/23 09:52 110 U QMethacrylonitrile
20 3.2 ug/L 05/05/23 09:52 110 UMethylene Chloride
2.5 0.78 ug/L 05/05/23 09:52 12.0 UMethyl methacrylate
20 2.7 ug/L 05/05/23 09:52 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/05/23 09:52 12.0 UMethyl tert-butyl ether
10 2.4 ug/L 05/05/23 09:52 15.0 UNaphthalene
5.0 0.50 ug/L 05/05/23 09:52 11.0 U QPentachloroethane
20 5.0 ug/L 05/05/23 09:52 110 U QPropionitrile
2.0 0.41 ug/L 05/05/23 09:52 11.0 UN-Propylbenzene
2.0 0.27 ug/L 05/05/23 09:52 11.0 UStyrene
2.0 0.36 ug/L 05/05/23 09:52 11.0 U1,1,1,2-Tetrachloroethane
2.0 0.40 ug/L 05/05/23 09:52 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/05/23 09:52 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/05/23 09:52 11.0 UToluene
5.0 0.81 ug/L 05/05/23 09:52 12.0 U1,2,3-Trichlorobenzene
5.0 0.53 ug/L 05/05/23 09:52 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/05/23 09:52 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/05/23 09:52 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/05/23 09:52 10.50 UTrichloroethene
2.0 0.33 ug/L 05/05/23 09:52 11.0 UTrichlorofluoromethane
2.0 0.48 ug/L 05/05/23 09:52 11.0 U1,2,3-Trichloropropane
1.0 0.23 ug/L 05/05/23 09:52 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.43 ug/L 05/05/23 09:52 11.0 U1,2,4-Trimethylbenzene
2.0 0.28 ug/L 05/05/23 09:52 11.0 U1,3,5-Trimethylbenzene
2.5 0.69 ug/L 05/05/23 09:52 12.0 UVinyl acetate
2.0 0.40 ug/L 05/05/23 09:52 11.0 UVinyl chloride
2.0 0.26 ug/L 05/05/23 09:52 11.0 Uo-Xylene
2.0 0.49 ug/L 05/05/23 09:52 11.0 Um-Xylene & p-Xylene
2.0 0.49 ug/L 05/05/23 09:52 11.0 UXylenes, Total
2.0 0.28 ug/L 05/05/23 09:52 10.69 JCyclohexane
5.0 1.1 ug/L 05/05/23 09:52 14.0 U1-Chlorohexane
20 3.2 ug/L 05/05/23 09:52 110 UMethyl acetate
2.0 0.33 ug/L 05/05/23 09:52 11.0 UMethylcyclohexane
10 2.1 ug/L 05/05/23 09:52 15.0 U MTetrahydrofuran
10 0.70 ug/L 05/05/23 09:52 12.0 UDiisopropyl ether
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U M 5.0 0.65 ug/L 05/05/23 09:52 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Hexane
5.0 0.37 ug/L 05/05/23 09:52 11.0 UDiethyl ether
2.0 0.43 ug/L 05/05/23 09:52 11.0 UHeptane
2.0 0.48 ug/L 05/05/23 09:52 11.0 U1,3-Dichloropropene, Total
10 2.5 ug/L 05/05/23 09:52 15.0 U Q2-Methylnaphthalene
2.0 0.38 ug/L 05/05/23 09:52 11.0 U1,3-Butadiene
5.0 0.50 ug/L 05/05/23 09:52 11.0 U Qn-Butyl acetate
2.0 0.50 ug/L 05/05/23 09:52 11.0 UDichlorofluoromethane
10 2.5 ug/L 05/05/23 09:52 15.0 U QBenzyl chloride
50 6.9 ug/L 05/05/23 09:52 120 Utert-Butyl alcohol
200 50 ug/L 05/05/23 09:52 1100 U QEthanol
250 92 ug/L 05/05/23 09:52 1200 U Q1,4-Dioxane
4.0 0.86 ug/L 05/05/23 09:52 12.0 U Q M2-Nitropropane
10 2.5 ug/L 05/05/23 09:52 15.0 U1,3,5-Trichlorobenzene
10 2.5 ug/L 05/05/23 09:52 15.0 U Q1,2,3-Trimethylbenzene
100 25 ug/L 05/05/23 09:52 150 U Qn-Butyl alcohol
2.5 0.78 ug/L 05/05/23 09:52 12.0 UTert-amyl methyl ether
100 25 ug/L 05/05/23 09:52 150 U Q2-Propanol
2.5 0.72 ug/L 05/05/23 09:52 12.0 UEthyl tert-butyl ether
20 5.0 ug/L 05/05/23 09:52 110 U QEthyl acetate
25 8.6 ug/L 05/05/23 09:52 120 U Q2-Butanol, 2-methyl-
5.0 0.99 ug/L 05/05/23 09:52 12.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)100 89-112 05/05/23 09:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)85 05/05/23 09:52 181-118
Dibromofluoromethane (Surr)93 05/05/23 09:52 180-119
4-Bromofluorobenzene (Surr)107 05/05/23 09:52 185-114
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
2.0 U 9.8 0.75 ug/L 05/05/23 21:00 05/10/23 22:13 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.8 0.55 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U1,2,4-Trichlorobenzene
9.8 0.52 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U1,2-Dichlorobenzene
9.8 0.58 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U1,3-Dichlorobenzene
9.8 0.59 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U1,3-Dinitrobenzene
9.8 0.53 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U1,4-Dichlorobenzene
9.8 0.61 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U Q1,4-Naphthoquinone
9.8 1.1 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U1-Naphthylamine
9.8 0.71 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U Q2,3,4,6-Tetrachlorophenol
9.8 1.2 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U Q2,4,5-Trichlorophenol
9.8 0.83 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2,4,6-Trichlorophenol
9.8 1.1 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2,4-Dichlorophenol
9.8 3.9 ug/L 05/05/23 21:00 05/10/23 22:13 19.8 U2,4-Dimethylphenol
49 9.8 ug/L 05/05/23 21:00 05/10/23 22:13 120 U Q2,4-Dinitrophenol
9.8 1.2 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U M2,4-Dinitrotoluene
9.8 0.72 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2,6-Dichlorophenol
9.8 1.1 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2,6-Dinitrotoluene
9.8 1.6 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U2-Acetylaminofluorene
9.8 0.78 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2-Chloronaphthalene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U 9.8 0.85 ug/L 05/05/23 21:00 05/10/23 22:13 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Chlorophenol
9.8 0.76 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2-Methylnaphthalene
9.8 0.87 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2-Methylphenol
9.8 1.5 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U2-Naphthylamine
49 1.3 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2-Nitroaniline
9.8 0.75 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U2-Nitrophenol
9.8 1.3 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U3 & 4 Methylphenol
59 29 ug/L 05/05/23 21:00 05/10/23 22:13 159 U3,3'-Dichlorobenzidine
20 9.8 ug/L 05/05/23 21:00 05/10/23 22:13 113 U3,3'-Dimethylbenzidine
9.8 1.4 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U3-Methylcholanthrene
49 4.9 ug/L 05/05/23 21:00 05/10/23 22:13 19.8 U3-Nitroaniline
49 9.8 ug/L 05/05/23 21:00 05/10/23 22:13 120 U Q4,6-Dinitro-2-methylphenol
9.8 1.2 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U4-Aminobiphenyl
9.8 0.76 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U4-Bromophenyl phenyl ether
9.8 0.98 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U4-Chloro-3-methylphenol
20 2.2 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U4-Chloroaniline
9.8 0.82 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U4-Chlorophenyl phenyl ether
49 4.9 ug/L 05/05/23 21:00 05/10/23 22:13 19.8 U4-Nitroaniline
49 1.9 ug/L 05/05/23 21:00 05/10/23 22:13 13.9 U Q4-Nitrophenol
25 9.8 ug/L 05/05/23 21:00 05/10/23 22:13 120 U4-Nitroquinoline-1-oxide
9.8 1.5 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U5-Nitro-o-toluidine
9.8 1.2 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U Q7,12-Dimethylbenz(a)anthracene
9.8 0.75 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UAcenaphthene
9.8 0.83 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UAcenaphthylene
9.8 0.56 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UAcetophenone
2000 34 ug/L 05/05/23 21:00 05/10/23 22:13 178 Ualpha,alpha-Dimethyl phenethylamine
9.8 0.68 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UAnthracene
9.8 0.54 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UBenzo[a]anthracene
9.8 0.70 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UBenzo[a]pyrene
9.8 2.5 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 UBenzo[b]fluoranthene
9.8 0.85 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UBenzo[g,h,i]perylene
9.8 1.2 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UBenzo[k]fluoranthene
9.8 1.1 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U MBenzyl alcohol
9.8 0.76 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 Ubis (2-chloroisopropyl) ether
9.8 0.92 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UBis(2-chloroethoxy)methane
9.8 1.1 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UBis(2-chloroethyl)ether
9.8 1.6 ug/L 05/05/23 21:00 05/10/23 22:13 12.5 UBis(2-ethylhexyl) phthalate
9.8 1.2 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UButyl benzyl phthalate
9.8 0.50 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UChrysene
9.8 0.76 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QDiallate
9.8 0.98 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UDibenz(a,h)anthracene
9.8 0.77 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UDibenzofuran
9.8 0.86 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UDiethyl phthalate
9.8 0.74 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QDimethoate
9.8 0.97 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UDimethyl phthalate
9.8 0.81 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UDi-n-butyl phthalate
9.8 1.4 ug/L 05/05/23 21:00 05/10/23 22:13 12.5 UDi-n-octyl phthalate
9.8 4.9 ug/L 05/05/23 21:00 05/10/23 22:13 19.8 U QDinoseb
9.8 0.90 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UDiphenylamine
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U Q 9.8 0.77 ug/L 05/05/23 21:00 05/10/23 22:13 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Disulfoton
9.8 0.94 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QEthyl methanesulfonate
9.8 1.3 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QEthyl Parathion
9.8 1.1 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UFamphur
9.8 0.73 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UFluoranthene
9.8 0.94 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UFluorene
9.8 0.77 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UHexachlorobenzene
9.8 0.61 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QHexachlorobutadiene
9.8 2.5 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 UHexachlorocyclopentadiene
9.8 0.75 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UHexachloroethane
9.8 1.4 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U QHexachloropropene
9.8 0.98 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UIndeno[1,2,3-cd]pyrene
9.8 0.88 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UIsophorone
9.8 0.49 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QIsosafrole
2000 2.6 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U QMethapyrilene
9.8 0.59 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U Q MMethyl methanesulfonate
9.8 0.86 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UMethyl parathion
9.8 0.69 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UNaphthalene
9.8 0.72 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UNitrobenzene
9.8 0.91 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UN-Nitrosodiethylamine
9.8 2.7 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U QN-Nitrosodimethylamine
9.8 0.94 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UN-Nitrosodi-n-butylamine
9.8 0.71 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UN-Nitrosodi-n-propylamine
9.8 0.90 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UN-Nitrosodiphenylamine
9.8 3.2 ug/L 05/05/23 21:00 05/10/23 22:13 19.8 UN-Nitrosomethylethylamine
9.8 0.86 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UN-Nitrosopiperidine
9.8 0.98 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UN-Nitrosopyrrolidine
9.8 0.98 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 Uo,o',o''-Triethylphosphorothioate
9.8 1.4 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 Uo-Toluidine
9.8 0.77 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U Mp-Dimethylamino azobenzene
9.8 0.51 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QPentachlorobenzene
9.8 0.76 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UPentachloronitrobenzene
49 2.0 ug/L 05/05/23 21:00 05/10/23 22:13 13.9 UPentachlorophenol
9.8 1.4 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 UPhenacetin
9.8 0.76 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UPhenanthrene
9.8 0.81 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QPhenol
9.8 0.85 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UPhorate
2000 9.8 ug/L 05/05/23 21:00 05/10/23 22:13 125 U Qp-Phenylene diamine
9.8 0.87 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UPronamide
9.8 0.62 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 UPyrene
9.8 0.78 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QSafrole, Total
9.8 2.0 ug/L 05/05/23 21:00 05/10/23 22:13 14.9 U Qsym-Trinitrobenzene
9.8 0.89 ug/L 05/05/23 21:00 05/10/23 22:13 12.0 U QThionazin
2,4,6-Tribromophenol (Surr)71 43-140 05/05/23 21:00 05/10/23 22:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)71 05/05/23 21:00 05/10/23 22:13 144-119
2-Fluorophenol (Surr)50 05/05/23 21:00 05/10/23 22:13 119-119
Nitrobenzene-d5 (Surr)69 05/05/23 21:00 05/10/23 22:13 144-120
Phenol-d5 (Surr)7 Q 05/05/23 21:00 05/10/23 22:13 127-110
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Terphenyl-d14 (Surr)63 50-134 05/05/23 21:00 05/10/23 22:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE
LOQ DL
1.9 U H Q 9.5 0.72 ug/L 05/20/23 21:30 05/24/23 22:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.5 0.53 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1,2,4-Trichlorobenzene
9.5 0.50 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1,2-Dichlorobenzene
9.5 0.56 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1,3-Dichlorobenzene
9.5 0.57 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1,3-Dinitrobenzene
9.5 0.51 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1,4-Dichlorobenzene
9.5 0.59 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1,4-Naphthoquinone
9.5 1.0 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q1-Naphthylamine
9.5 0.68 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,3,4,6-Tetrachlorophenol
9.5 1.1 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,4,5-Trichlorophenol
9.5 0.80 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,4,6-Trichlorophenol
9.5 1.0 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,4-Dichlorophenol
9.5 3.8 ug/L 05/20/23 21:30 05/24/23 22:49 19.5 U H Q2,4-Dimethylphenol
47 9.5 ug/L 05/20/23 21:30 05/24/23 22:49 119 U H Q2,4-Dinitrophenol
9.5 1.1 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,4-Dinitrotoluene
9.5 0.69 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,6-Dichlorophenol
9.5 1.0 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2,6-Dinitrotoluene
9.5 1.5 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H2-Acetylaminofluorene
9.5 0.76 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2-Chloronaphthalene
9.5 0.82 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2-Chlorophenol
9.5 0.74 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2-Methylnaphthalene
9.5 0.84 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2-Methylphenol
9.5 1.4 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H Q2-Naphthylamine
47 1.2 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2-Nitroaniline
9.5 0.72 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q2-Nitrophenol
9.5 1.2 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q3 & 4 Methylphenol
57 28 ug/L 05/20/23 21:30 05/24/23 22:49 157 U H Q3,3'-Dichlorobenzidine
19 9.5 ug/L 05/20/23 21:30 05/24/23 22:49 112 U H Q3,3'-Dimethylbenzidine
9.5 1.3 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H3-Methylcholanthrene
47 4.7 ug/L 05/20/23 21:30 05/24/23 22:49 19.5 U H Q3-Nitroaniline
47 9.5 ug/L 05/20/23 21:30 05/24/23 22:49 119 U H Q4,6-Dinitro-2-methylphenol
9.5 1.1 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q4-Aminobiphenyl
9.5 0.73 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q4-Bromophenyl phenyl ether
9.5 0.95 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q4-Chloro-3-methylphenol
19 2.1 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H Q4-Chloroaniline
9.5 0.80 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q4-Chlorophenyl phenyl ether
47 4.7 ug/L 05/20/23 21:30 05/24/23 22:49 19.5 U H Q4-Nitroaniline
47 1.8 ug/L 05/20/23 21:30 05/24/23 22:49 13.8 U H Q4-Nitrophenol
24 9.5 ug/L 05/20/23 21:30 05/24/23 22:49 119 U H Q4-Nitroquinoline-1-oxide
9.5 1.4 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H Q5-Nitro-o-toluidine
9.5 1.1 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Q7,12-Dimethylbenz(a)anthracene
9.5 0.72 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QAcenaphthene
9.5 0.80 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QAcenaphthylene
9.5 0.54 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QAcetophenone
1900 33 ug/L 05/20/23 21:30 05/24/23 22:49 176 U H Qalpha,alpha-Dimethyl phenethylamine
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
1.9 U H Q 9.5 0.65 ug/L 05/20/23 21:30 05/24/23 22:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
9.5 0.52 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QBenzo[a]anthracene
9.5 0.67 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QBenzo[a]pyrene
9.5 2.5 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H QBenzo[b]fluoranthene
9.5 0.82 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QBenzo[g,h,i]perylene
9.5 1.1 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QBenzo[k]fluoranthene
9.5 1.0 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H M QBenzyl alcohol
9.5 0.74 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Qbis (2-chloroisopropyl) ether
9.5 0.89 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QBis(2-chloroethoxy)methane
9.5 1.0 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QBis(2-chloroethyl)ether
9.5 1.5 ug/L 05/20/23 21:30 05/24/23 22:49 12.4 U H QBis(2-ethylhexyl) phthalate
9.5 1.1 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QButyl benzyl phthalate
9.5 0.48 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QChrysene
9.5 0.74 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDiallate
9.5 0.95 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDibenz(a,h)anthracene
9.5 0.75 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDibenzofuran
9.5 0.83 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDiethyl phthalate
9.5 0.71 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDimethoate
9.5 0.94 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDimethyl phthalate
9.5 0.79 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDi-n-butyl phthalate
9.5 1.3 ug/L 05/20/23 21:30 05/24/23 22:49 12.4 U H QDi-n-octyl phthalate
9.5 4.7 ug/L 05/20/23 21:30 05/24/23 22:49 19.5 U HDinoseb
9.5 0.87 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDiphenylamine
9.5 0.75 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QDisulfoton
9.5 0.91 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QEthyl methanesulfonate
9.5 1.2 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QEthyl Parathion
9.5 1.0 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QFamphur
9.5 0.70 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QFluoranthene
9.5 0.91 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QFluorene
9.5 0.75 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QHexachlorobenzene
9.5 0.59 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QHexachlorobutadiene
9.5 2.4 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H QHexachlorocyclopentadiene
9.5 0.72 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QHexachloroethane
9.5 1.3 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H QHexachloropropene
9.5 0.95 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QIndeno[1,2,3-cd]pyrene
9.5 0.85 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QIsophorone
9.5 0.47 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QIsosafrole
1900 2.6 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H QMethapyrilene
9.5 0.57 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QMethyl methanesulfonate
9.5 0.83 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QMethyl parathion
9.5 0.66 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QNaphthalene
9.5 0.69 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QNitrobenzene
9.5 0.88 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QN-Nitrosodiethylamine
9.5 2.7 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H QN-Nitrosodimethylamine
9.5 0.91 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QN-Nitrosodi-n-butylamine
9.5 0.68 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QN-Nitrosodi-n-propylamine
9.5 0.87 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QN-Nitrosodiphenylamine
9.5 3.1 ug/L 05/20/23 21:30 05/24/23 22:49 19.5 U H QN-Nitrosomethylethylamine
9.5 0.83 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QN-Nitrosopiperidine
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
1.9 U H Q 9.5 0.95 ug/L 05/20/23 21:30 05/24/23 22:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
N-Nitrosopyrrolidine
9.5 0.95 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H Qo,o',o''-Triethylphosphorothioate
9.5 1.3 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H Qo-Toluidine
9.5 0.75 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H M Qp-Dimethylamino azobenzene
9.5 0.49 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QPentachlorobenzene
9.5 0.74 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U HPentachloronitrobenzene
47 1.9 ug/L 05/20/23 21:30 05/24/23 22:49 13.8 U H QPentachlorophenol
9.5 1.3 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U HPhenacetin
9.5 0.73 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QPhenanthrene
9.5 0.79 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QPhenol
9.5 0.82 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QPhorate
1900 9.5 ug/L 05/20/23 21:30 05/24/23 22:49 124 U H Qp-Phenylene diamine
9.5 0.84 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QPronamide
9.5 0.60 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QPyrene
9.5 0.76 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QSafrole, Total
9.5 1.9 ug/L 05/20/23 21:30 05/24/23 22:49 14.7 U H Qsym-Trinitrobenzene
9.5 0.86 ug/L 05/20/23 21:30 05/24/23 22:49 11.9 U H QThionazin
2,4,6-Tribromophenol (Surr)38 Q 43-140 05/20/23 21:30 05/24/23 22:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)18 Q 05/20/23 21:30 05/24/23 22:49 144-119
2-Fluorophenol (Surr)9 Q 05/20/23 21:30 05/24/23 22:49 119-119
Nitrobenzene-d5 (Surr)8 Q 05/20/23 21:30 05/24/23 22:49 144-120
Phenol-d5 (Surr)8 Q 05/20/23 21:30 05/24/23 22:49 127-110
Terphenyl-d14 (Surr)63 05/20/23 21:30 05/24/23 22:49 150-134
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
32 J 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.0 U 5.0 1.0 ug/L 05/10/23 14:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 14:39 150 U MC5-C8 Aliphatics
100 10 ug/L 05/10/23 14:39 116 J MC9-C10 Aromatics
100 25 ug/L 05/10/23 14:39 132 J MC9-C12 Aliphatics
5.0 1.0 ug/L 05/10/23 14:39 12.0 UEthylbenzene
5.0 1.0 ug/L 05/10/23 14:39 12.0 UMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 14:39 14.0 U MNaphthalene
5.0 1.0 ug/L 05/10/23 14:39 12.0 UToluene
100 25 ug/L 05/10/23 14:39 150 UC9-C12 Aliphatics (adjusted)
10 2.5 ug/L 05/10/23 14:39 15.0 Um-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 14:39 12.0 Uo-Xylene
100 25 ug/L 05/10/23 14:39 150 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)106 70-130 05/10/23 14:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)91 05/10/23 14:39 170-130
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U 2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:55 1200Total EPH
12 5.0 ug/L 05/08/23 09:17 05/13/23 12:57 110 UPyrene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 UBenzo[g,h,i]perylene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 UBenzo[b]fluoranthene
2.0 0.50 ug/L 05/08/23 09:17 05/13/23 12:57 11.0 UFluoranthene
4.0 1.5 ug/L 05/08/23 09:17 05/13/23 12:57 13.0 UBenzo[k]fluoranthene
2.0 0.70 ug/L 05/08/23 09:17 05/13/23 12:57 12.7 MAcenaphthylene
2.0 0.50 ug/L 05/08/23 09:17 05/13/23 12:57 11.0 UChrysene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 UBenzo[a]pyrene
2.0 0.50 ug/L 05/08/23 09:17 05/13/23 12:57 11.0 UDibenz(a,h)anthracene
2.0 0.70 ug/L 05/08/23 09:17 05/13/23 12:57 11.4 UBenzo[a]anthracene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 U MAcenaphthene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 UPhenanthrene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 11.2 U MFluorene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 130 MNaphthalene
2.0 0.60 ug/L 05/08/23 09:17 05/13/23 12:57 116 M2-Methylnaphthalene
40 10 ug/L 05/08/23 09:17 05/13/23 12:57 1110 MC11-C22 Aromatics (unadjusted)
40 10 ug/L 05/08/23 09:17 05/13/23 12:57 163C11-C22 Aromatics (Adjusted)
50 10 ug/L 05/08/23 09:17 05/13/23 14:27 111 J MC19-C36 Aliphatics
30 10 ug/L 05/08/23 09:17 05/13/23 14:27 175 M BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)41 40-140 05/08/23 09:17 05/13/23 14:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)64 05/08/23 09:17 05/13/23 12:57 140-140
o- terphenyl (Surr)53 05/08/23 09:17 05/13/23 12:57 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.1 U H 1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
11 4.8 ug/L 05/23/23 09:00 06/01/23 07:22 19.5 U HPyrene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HBenzo[g,h,i]perylene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HIndeno[1,2,3-cd]pyrene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HBenzo[b]fluoranthene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 07:22 10.95 U HFluoranthene
3.8 1.4 ug/L 05/23/23 09:00 06/01/23 07:22 12.9 U HBenzo[k]fluoranthene
1.9 0.67 ug/L 05/23/23 09:00 06/01/23 07:22 11.3 U HAcenaphthylene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 07:22 10.95 U HChrysene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HBenzo[a]pyrene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 07:22 10.95 U HDibenz(a,h)anthracene
1.9 0.67 ug/L 05/23/23 09:00 06/01/23 07:22 11.3 U HBenzo[a]anthracene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HAcenaphthene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HPhenanthrene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HFluorene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U HNaphthalene
1.9 0.57 ug/L 05/23/23 09:00 06/01/23 07:22 11.1 U H2-Methylnaphthalene
38 9.5 ug/L 05/23/23 09:00 06/01/23 07:22 129 U HC11-C22 Aromatics (unadjusted)
38 9.5 ug/L 05/23/23 09:00 06/01/23 07:22 129 U HC11-C22 Aromatics (Adjusted)
48 9.5 ug/L 05/23/23 09:00 06/01/23 07:45 119 U M HC19-C36 Aliphatics
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-4Client Sample ID: MW1-04-23
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
24 J H B 29 9.5 ug/L 05/23/23 09:00 06/01/23 07:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C9-C18 Aliphatics
1-Chlorooctadecane (Surr)45 M 40-140 05/23/23 09:00 06/01/23 07:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)88 05/23/23 09:00 06/01/23 07:22 140-140
o- terphenyl (Surr)61 05/23/23 09:00 06/01/23 07:22 140-140
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 J Q D 50 7.4 ug/L 05/05/23 13:50 2
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
100 40 ug/L 05/05/23 13:50 2140 Q D MAcetonitrile
100 30 ug/L 05/05/23 13:50 280 UAcrolein
100 11 ug/L 05/05/23 13:50 240 U MAcrylonitrile
4.0 0.54 ug/L 05/05/23 13:50 213 DBenzene
2.0 0.48 ug/L 05/05/23 13:50 21.0 U J1Bromobenzene
4.0 0.68 ug/L 05/05/23 13:50 22.0 UBromochloromethane
4.0 0.50 ug/L 05/05/23 13:50 22.0 UBromodichloromethane
5.0 1.2 ug/L 05/05/23 13:50 24.0 U QBromoform
40 7.4 ug/L 05/05/23 13:50 220 U J1 QBromomethane
50 13 ug/L 05/05/23 13:50 240 U2-Butanone (MEK)
5.0 1.0 ug/L 05/05/23 13:50 24.5 J Dn-Butylbenzene
5.0 1.1 ug/L 05/05/23 13:50 22.5 J Dsec-Butylbenzene
4.0 0.86 ug/L 05/05/23 13:50 22.0 Utert-Butylbenzene
4.0 0.86 ug/L 05/05/23 13:50 22.0 UCarbon disulfide
4.0 0.60 ug/L 05/05/23 13:50 22.0 UCarbon tetrachloride
2.0 0.30 ug/L 05/05/23 13:50 21.0 UChlorobenzene
5.0 1.4 ug/L 05/05/23 13:50 24.0 U2-Chloro-1,3-butadiene
40 9.2 ug/L 05/05/23 13:50 220 UChloroethane
50 1.2 ug/L 05/05/23 13:50 240 U2-Chloroethyl vinyl ether
4.0 0.54 ug/L 05/05/23 13:50 22.0 U MChloroform
5.0 1.1 ug/L 05/05/23 13:50 24.0 UChloromethane
10 2.2 ug/L 05/05/23 13:50 29.6 J DAllyl chloride
2.0 0.50 ug/L 05/05/23 13:50 21.0 U J12-Chlorotoluene
4.0 0.82 ug/L 05/05/23 13:50 22.0 U4-Chlorotoluene
4.0 0.78 ug/L 05/05/23 13:50 22.0 UChlorodibromomethane
20 3.6 ug/L 05/05/23 13:50 210 U Q1,2-Dibromo-3-Chloropropane
4.0 0.66 ug/L 05/05/23 13:50 22.0 U1,2-Dibromoethane
4.0 0.68 ug/L 05/05/23 13:50 22.0 UDibromomethane
4.0 0.62 ug/L 05/05/23 13:50 22.0 U1,2-Dichlorobenzene
4.0 0.62 ug/L 05/05/23 13:50 22.0 U1,3-Dichlorobenzene
4.0 0.62 ug/L 05/05/23 13:50 22.0 U1,4-Dichlorobenzene
20 2.5 ug/L 05/05/23 13:50 210 U Q J1 Mtrans-1,4-Dichloro-2-butene
4.0 0.72 ug/L 05/05/23 13:50 22.0 UDichlorodifluoromethane
4.0 0.66 ug/L 05/05/23 13:50 22.0 U1,1-Dichloroethane
4.0 0.50 ug/L 05/05/23 13:50 22.0 U M1,2-Dichloroethane
4.0 0.50 ug/L 05/05/23 13:50 22.0 Ucis-1,2-Dichloroethene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U 4.0 0.68 ug/L 05/05/23 13:50 2
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
trans-1,2-Dichloroethene
4.0 0.74 ug/L 05/05/23 13:50 22.0 U1,2-Dichloroethene, Total
4.0 0.66 ug/L 05/05/23 13:50 22.0 U1,1-Dichloroethene
2.0 0.44 ug/L 05/05/23 13:50 21.0 U1,2-Dichloropropane
4.0 0.72 ug/L 05/05/23 13:50 22.0 U1,3-Dichloropropane
4.0 0.70 ug/L 05/05/23 13:50 22.0 U2,2-Dichloropropane
4.0 0.56 ug/L 05/05/23 13:50 22.0 U1,1-Dichloropropene
4.0 0.52 ug/L 05/05/23 13:50 22.0 Ucis-1,3-Dichloropropene
4.0 0.46 ug/L 05/05/23 13:50 22.0 Utrans-1,3-Dichloropropene
2.0 0.40 ug/L 05/05/23 13:50 240 J1 DEthylbenzene
4.0 0.66 ug/L 05/05/23 13:50 22.0 UEthyl methacrylate
10 0.44 ug/L 05/05/23 13:50 22.0 UHexachlorobutadiene
40 6.4 ug/L 05/05/23 13:50 220 U2-Hexanone
40 7.8 ug/L 05/05/23 13:50 220 U Q J1Iodomethane
1000 140 ug/L 05/05/23 13:50 2500 U MIsobutyl alcohol
4.0 0.52 ug/L 05/05/23 13:50 212 J1 DIsopropylbenzene
4.0 0.88 ug/L 05/05/23 13:50 22.7 J Dp-Isopropyltoluene
40 10 ug/L 05/05/23 13:50 220 U Q MMethacrylonitrile
40 6.4 ug/L 05/05/23 13:50 220 UMethylene Chloride
5.0 1.6 ug/L 05/05/23 13:50 24.0 UMethyl methacrylate
40 5.4 ug/L 05/05/23 13:50 220 U4-Methyl-2-pentanone (MIBK)
10 1.6 ug/L 05/05/23 13:50 24.0 UMethyl tert-butyl ether
20 4.8 ug/L 05/05/23 13:50 253 J1 DNaphthalene
10 1.0 ug/L 05/05/23 13:50 22.0 U QPentachloroethane
40 10 ug/L 05/05/23 13:50 220 U Q MPropionitrile
4.0 0.82 ug/L 05/05/23 13:50 216 J1 DN-Propylbenzene
4.0 0.54 ug/L 05/05/23 13:50 22.0 U MStyrene
4.0 0.72 ug/L 05/05/23 13:50 22.0 U1,1,1,2-Tetrachloroethane
4.0 0.80 ug/L 05/05/23 13:50 22.0 U J11,1,2,2-Tetrachloroethane
4.0 0.70 ug/L 05/05/23 13:50 22.0 UTetrachloroethene
4.0 0.50 ug/L 05/05/23 13:50 21.6 J DToluene
10 1.6 ug/L 05/05/23 13:50 24.0 U1,2,3-Trichlorobenzene
10 1.1 ug/L 05/05/23 13:50 24.0 U1,2,4-Trichlorobenzene
2.0 0.42 ug/L 05/05/23 13:50 21.0 U1,1,1-Trichloroethane
4.0 0.64 ug/L 05/05/23 13:50 22.0 U1,1,2-Trichloroethane
2.0 0.40 ug/L 05/05/23 13:50 21.0 UTrichloroethene
4.0 0.66 ug/L 05/05/23 13:50 22.0 UTrichlorofluoromethane
4.0 0.96 ug/L 05/05/23 13:50 22.0 U J11,2,3-Trichloropropane
2.0 0.46 ug/L 05/05/23 13:50 21.0 U1,1,2-Trichloro-1,2,2-trifluoroethane
4.0 0.86 ug/L 05/05/23 13:50 2130 J1 D1,2,4-Trimethylbenzene
4.0 0.56 ug/L 05/05/23 13:50 237 J1 D1,3,5-Trimethylbenzene
5.0 1.4 ug/L 05/05/23 13:50 24.0 U MVinyl acetate
4.0 0.80 ug/L 05/05/23 13:50 22.0 UVinyl chloride
4.0 0.52 ug/L 05/05/23 13:50 26.7 Do-Xylene
4.0 0.98 ug/L 05/05/23 13:50 2210 J1 Dm-Xylene & p-Xylene
4.0 0.98 ug/L 05/05/23 13:50 2220 J1 DXylenes, Total
4.0 0.56 ug/L 05/05/23 13:50 223 J1 DCyclohexane
10 2.2 ug/L 05/05/23 13:50 28.0 U1-Chlorohexane
40 6.4 ug/L 05/05/23 13:50 220 U J1Methyl acetate
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
12 D 4.0 0.66 ug/L 05/05/23 13:50 2
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Methylcyclohexane
20 4.2 ug/L 05/05/23 13:50 210 U MTetrahydrofuran
20 1.4 ug/L 05/05/23 13:50 24.0 UDiisopropyl ether
10 1.3 ug/L 05/05/23 13:50 213 DHexane
10 0.74 ug/L 05/05/23 13:50 22.0 UDiethyl ether
4.0 0.86 ug/L 05/05/23 13:50 22.4 J DHeptane
4.0 0.96 ug/L 05/05/23 13:50 22.0 U1,3-Dichloropropene, Total
20 5.0 ug/L 05/05/23 13:50 224 Q D2-Methylnaphthalene
4.0 0.76 ug/L 05/05/23 13:50 22.0 U1,3-Butadiene
10 1.0 ug/L 05/05/23 13:50 22.0 U Qn-Butyl acetate
4.0 1.0 ug/L 05/05/23 13:50 22.0 UDichlorofluoromethane
20 5.0 ug/L 05/05/23 13:50 210 U QBenzyl chloride
100 14 ug/L 05/05/23 13:50 240 Utert-Butyl alcohol
400 100 ug/L 05/05/23 13:50 2200 U QEthanol
500 180 ug/L 05/05/23 13:50 2400 U Q J11,4-Dioxane
8.0 1.7 ug/L 05/05/23 13:50 22.7 J Q D2-Nitropropane
20 5.0 ug/L 05/05/23 13:50 210 U1,3,5-Trichlorobenzene
20 5.0 ug/L 05/05/23 13:50 269 Q D1,2,3-Trimethylbenzene
200 50 ug/L 05/05/23 13:50 2100 U Qn-Butyl alcohol
5.0 1.6 ug/L 05/05/23 13:50 24.0 UTert-amyl methyl ether
200 50 ug/L 05/05/23 13:50 2100 U Q M2-Propanol
5.0 1.4 ug/L 05/05/23 13:50 24.0 UEthyl tert-butyl ether
40 10 ug/L 05/05/23 13:50 220 U QEthyl acetate
50 17 ug/L 05/05/23 13:50 240 U Q M2-Butanol, 2-methyl-
10 2.0 ug/L 05/05/23 13:50 24.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)98 89-112 05/05/23 13:50 2
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)86 05/05/23 13:50 281-118
Dibromofluoromethane (Surr)96 05/05/23 13:50 280-119
4-Bromofluorobenzene (Surr)110 05/05/23 13:50 285-114
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
1.9 U 9.7 0.73 ug/L 05/05/23 21:00 05/10/23 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.7 0.54 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U1,2,4-Trichlorobenzene
9.7 0.51 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U1,2-Dichlorobenzene
9.7 0.57 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U1,3-Dichlorobenzene
9.7 0.58 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U1,3-Dinitrobenzene
9.7 0.52 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U1,4-Dichlorobenzene
9.7 0.60 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q1,4-Naphthoquinone
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J11-Naphthylamine
9.7 0.70 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q2,3,4,6-Tetrachlorophenol
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q2,4,5-Trichlorophenol
9.7 0.82 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2,4,6-Trichlorophenol
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2,4-Dichlorophenol
9.7 3.9 ug/L 05/05/23 21:00 05/10/23 20:46 19.7 U J12,4-Dimethylphenol
48 9.7 ug/L 05/05/23 21:00 05/10/23 20:46 119 U Q2,4-Dinitrophenol
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M2,4-Dinitrotoluene
9.7 0.71 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2,6-Dichlorophenol
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.9 U 9.7 1.1 ug/L 05/05/23 21:00 05/10/23 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2,6-Dinitrotoluene
9.7 1.5 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U Q2-Acetylaminofluorene
9.7 0.77 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2-Chloronaphthalene
9.7 0.84 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2-Chlorophenol
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 20:46 1112-Methylnaphthalene
9.7 0.86 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J12-Methylphenol
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U J12-Naphthylamine
48 1.3 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2-Nitroaniline
9.7 0.73 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U2-Nitrophenol
9.7 1.3 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J13 & 4 Methylphenol
58 29 ug/L 05/05/23 21:00 05/10/23 20:46 158 U J13,3'-Dichlorobenzidine
19 9.7 ug/L 05/05/23 21:00 05/10/23 20:46 113 U Q J13,3'-Dimethylbenzidine
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U Q3-Methylcholanthrene
48 4.8 ug/L 05/05/23 21:00 05/10/23 20:46 19.7 U J13-Nitroaniline
48 9.7 ug/L 05/05/23 21:00 05/10/23 20:46 119 U Q4,6-Dinitro-2-methylphenol
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J14-Aminobiphenyl
9.7 0.74 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M4-Bromophenyl phenyl ether
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J14-Chloro-3-methylphenol
19 2.1 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U M J14-Chloroaniline
9.7 0.81 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U4-Chlorophenyl phenyl ether
48 4.8 ug/L 05/05/23 21:00 05/10/23 20:46 19.7 U J14-Nitroaniline
48 1.8 ug/L 05/05/23 21:00 05/10/23 20:46 13.9 U Q4-Nitrophenol
24 9.7 ug/L 05/05/23 21:00 05/10/23 20:46 119 U J14-Nitroquinoline-1-oxide
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U5-Nitro-o-toluidine
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J17,12-Dimethylbenz(a)anthracene
9.7 0.73 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Acenaphthene
9.7 0.82 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Acenaphthylene
9.7 0.55 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U MAcetophenone
1900 34 ug/L 05/05/23 21:00 05/10/23 20:46 177 U J1alpha,alpha-Dimethyl phenethylamine
9.7 0.67 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Anthracene
9.7 0.53 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Benzo[a]anthracene
9.7 0.69 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Benzo[a]pyrene
9.7 2.5 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U QBenzo[b]fluoranthene
9.7 0.84 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Benzo[g,h,i]perylene
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Benzo[k]fluoranthene
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1Benzyl alcohol
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 Ubis (2-chloroisopropyl) ether
9.7 0.91 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1Bis(2-chloroethoxy)methane
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1Bis(2-chloroethyl)ether
9.7 1.5 ug/L 05/05/23 21:00 05/10/23 20:46 12.4 U J1Bis(2-ethylhexyl) phthalate
9.7 1.2 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1Butyl benzyl phthalate
9.7 0.49 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U QChrysene
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Diallate
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UDibenz(a,h)anthracene
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UDibenzofuran
9.7 0.85 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1Diethyl phthalate
9.7 0.72 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U QDimethoate
9.7 0.96 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1Dimethyl phthalate
9.7 0.80 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1Di-n-butyl phthalate
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.4 U J1 9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Di-n-octyl phthalate
9.7 4.8 ug/L 05/05/23 21:00 05/10/23 20:46 19.7 U QDinoseb
9.7 0.89 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UDiphenylamine
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1 QDisulfoton
9.7 0.93 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Ethyl methanesulfonate
9.7 1.3 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1 QEthyl Parathion
9.7 1.1 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Famphur
9.7 0.71 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Fluoranthene
9.7 0.93 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Fluorene
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UHexachlorobenzene
9.7 0.60 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U QHexachlorobutadiene
9.7 2.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 UHexachlorocyclopentadiene
9.7 0.73 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UHexachloroethane
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U QHexachloropropene
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Indeno[1,2,3-cd]pyrene
9.7 0.87 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UIsophorone
9.7 0.48 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1 QIsosafrole
1900 2.6 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U QMethapyrilene
9.7 0.58 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1 QMethyl methanesulfonate
9.7 0.85 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UMethyl parathion
9.7 0.68 ug/L 05/05/23 21:00 05/10/23 20:46 124 QNaphthalene
9.7 0.71 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UNitrobenzene
9.7 0.90 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1N-Nitrosodiethylamine
9.7 2.7 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U QN-Nitrosodimethylamine
9.7 0.93 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1N-Nitrosodi-n-butylamine
9.7 0.70 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U MN-Nitrosodi-n-propylamine
9.7 0.89 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UN-Nitrosodiphenylamine
9.7 3.2 ug/L 05/05/23 21:00 05/10/23 20:46 19.7 U J1N-Nitrosomethylethylamine
9.7 0.85 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1N-Nitrosopiperidine
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1N-Nitrosopyrrolidine
9.7 0.97 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1o,o',o''-Triethylphosphorothioate
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U J1o-Toluidine
9.7 0.76 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U M J1p-Dimethylamino azobenzene
9.7 0.50 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1 QPentachlorobenzene
9.7 0.75 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1Pentachloronitrobenzene
48 1.9 ug/L 05/05/23 21:00 05/10/23 20:46 13.9 UPentachlorophenol
9.7 1.4 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 UPhenacetin
9.7 0.74 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U QPhenanthrene
9.7 0.80 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Phenol
9.7 0.84 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UPhorate
1900 9.7 ug/L 05/05/23 21:00 05/10/23 20:46 124 U Q J1p-Phenylene diamine
9.7 0.86 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 UPronamide
9.7 0.61 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Pyrene
9.7 0.77 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U J1 QSafrole, Total
9.7 1.9 ug/L 05/05/23 21:00 05/10/23 20:46 14.8 U Qsym-Trinitrobenzene
9.7 0.88 ug/L 05/05/23 21:00 05/10/23 20:46 11.9 U Q J1Thionazin
2,4,6-Tribromophenol (Surr)49 43-140 05/05/23 21:00 05/10/23 20:46 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)46 05/05/23 21:00 05/10/23 20:46 144-119
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
2-Fluorophenol (Surr)35 19-119 05/05/23 21:00 05/10/23 20:46 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 (Surr)45 05/05/23 21:00 05/10/23 20:46 144-120
Phenol-d5 (Surr)9 Q 05/05/23 21:00 05/10/23 20:46 127-110
Terphenyl-d14 (Surr)37 Q 05/05/23 21:00 05/10/23 20:46 150-134
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE
LOQ DL
1.9 U H Q 9.6 0.73 ug/L 05/20/23 21:30 05/24/23 23:11 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.6 0.54 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1,2,4-Trichlorobenzene
9.6 0.51 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1,2-Dichlorobenzene
9.6 0.57 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1,3-Dichlorobenzene
9.6 0.58 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1,3-Dinitrobenzene
9.6 0.52 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1,4-Dichlorobenzene
9.6 0.59 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1,4-Naphthoquinone
9.6 1.1 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q1-Naphthylamine
9.6 0.69 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,3,4,6-Tetrachlorophenol
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,4,5-Trichlorophenol
9.6 0.81 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,4,6-Trichlorophenol
9.6 1.1 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,4-Dichlorophenol
9.6 3.8 ug/L 05/20/23 21:30 05/24/23 23:11 19.6 U H Q2,4-Dimethylphenol
48 9.6 ug/L 05/20/23 21:30 05/24/23 23:11 119 U H Q2,4-Dinitrophenol
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,4-Dinitrotoluene
9.6 0.70 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,6-Dichlorophenol
9.6 1.1 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2,6-Dinitrotoluene
9.6 1.5 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H Q2-Acetylaminofluorene
9.6 0.77 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2-Chloronaphthalene
9.6 0.83 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2-Chlorophenol
9.6 0.75 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2-Methylnaphthalene
9.6 0.85 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2-Methylphenol
9.6 1.4 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H Q2-Naphthylamine
48 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2-Nitroaniline
9.6 0.73 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q2-Nitrophenol
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q3 & 4 Methylphenol
58 29 ug/L 05/20/23 21:30 05/24/23 23:11 158 U H Q3,3'-Dichlorobenzidine
19 9.6 ug/L 05/20/23 21:30 05/24/23 23:11 112 U H Q3,3'-Dimethylbenzidine
9.6 1.3 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H Q3-Methylcholanthrene
48 4.8 ug/L 05/20/23 21:30 05/24/23 23:11 19.6 U H Q3-Nitroaniline
48 9.6 ug/L 05/20/23 21:30 05/24/23 23:11 119 U H Q4,6-Dinitro-2-methylphenol
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q4-Aminobiphenyl
9.6 0.74 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q4-Bromophenyl phenyl ether
9.6 0.96 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q4-Chloro-3-methylphenol
19 2.1 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H Q4-Chloroaniline
9.6 0.81 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q4-Chlorophenyl phenyl ether
48 4.8 ug/L 05/20/23 21:30 05/24/23 23:11 19.6 U H Q4-Nitroaniline
48 1.8 ug/L 05/20/23 21:30 05/24/23 23:11 13.8 U H Q4-Nitrophenol
24 9.6 ug/L 05/20/23 21:30 05/24/23 23:11 119 U H Q4-Nitroquinoline-1-oxide
9.6 1.4 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H Q5-Nitro-o-toluidine
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Q7,12-Dimethylbenz(a)anthracene
9.6 0.73 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QAcenaphthene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
1.9 U H Q 9.6 0.81 ug/L 05/20/23 21:30 05/24/23 23:11 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthylene
9.6 0.55 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H M QAcetophenone
1900 34 ug/L 05/20/23 21:30 05/24/23 23:11 177 U H Qalpha,alpha-Dimethyl phenethylamine
9.6 0.66 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QAnthracene
9.6 0.53 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QBenzo[a]anthracene
9.6 0.68 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QBenzo[a]pyrene
9.6 2.5 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H QBenzo[b]fluoranthene
9.6 0.83 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QBenzo[g,h,i]perylene
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QBenzo[k]fluoranthene
9.6 1.1 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H M QBenzyl alcohol
9.6 0.75 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Qbis (2-chloroisopropyl) ether
9.6 0.90 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QBis(2-chloroethoxy)methane
9.6 1.1 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QBis(2-chloroethyl)ether
9.6 1.5 ug/L 05/20/23 21:30 05/24/23 23:11 12.4 U H QBis(2-ethylhexyl) phthalate
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QButyl benzyl phthalate
9.6 0.49 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QChrysene
9.6 0.75 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDiallate
9.6 0.96 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDibenz(a,h)anthracene
9.6 0.76 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDibenzofuran
9.6 0.84 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDiethyl phthalate
9.6 0.72 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDimethoate
9.6 0.95 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDimethyl phthalate
9.6 0.80 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDi-n-butyl phthalate
9.6 1.3 ug/L 05/20/23 21:30 05/24/23 23:11 12.4 U H QDi-n-octyl phthalate
9.6 4.8 ug/L 05/20/23 21:30 05/24/23 23:11 19.6 U HDinoseb
9.6 0.88 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDiphenylamine
9.6 0.76 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QDisulfoton
9.6 0.92 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QEthyl methanesulfonate
9.6 1.2 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QEthyl Parathion
9.6 1.1 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QFamphur
9.6 0.71 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QFluoranthene
9.6 0.92 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QFluorene
9.6 0.76 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QHexachlorobenzene
9.6 0.59 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QHexachlorobutadiene
9.6 2.4 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H QHexachlorocyclopentadiene
9.6 0.73 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QHexachloroethane
9.6 1.3 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H QHexachloropropene
9.6 0.96 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QIndeno[1,2,3-cd]pyrene
9.6 0.86 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H M QIsophorone
9.6 0.48 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QIsosafrole
1900 2.6 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H QMethapyrilene
9.6 0.58 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QMethyl methanesulfonate
9.6 0.84 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QMethyl parathion
9.6 0.67 ug/L 05/20/23 21:30 05/24/23 23:11 13.5 J H QNaphthalene
9.6 0.70 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QNitrobenzene
9.6 0.89 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QN-Nitrosodiethylamine
9.6 2.7 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H QN-Nitrosodimethylamine
9.6 0.92 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QN-Nitrosodi-n-butylamine
9.6 0.69 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QN-Nitrosodi-n-propylamine
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
1.9 U H Q 9.6 0.88 ug/L 05/20/23 21:30 05/24/23 23:11 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
N-Nitrosodiphenylamine
9.6 3.2 ug/L 05/20/23 21:30 05/24/23 23:11 19.6 U H QN-Nitrosomethylethylamine
9.6 0.84 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QN-Nitrosopiperidine
9.6 0.96 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QN-Nitrosopyrrolidine
9.6 0.96 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H Qo,o',o''-Triethylphosphorothioate
9.6 1.3 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H M Qo-Toluidine
9.6 0.76 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H M Qp-Dimethylamino azobenzene
9.6 0.50 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QPentachlorobenzene
9.6 0.75 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U HPentachloronitrobenzene
48 1.9 ug/L 05/20/23 21:30 05/24/23 23:11 13.8 U H QPentachlorophenol
9.6 1.3 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U HPhenacetin
9.6 0.74 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QPhenanthrene
9.6 0.80 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QPhenol
9.6 0.83 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QPhorate
1900 9.6 ug/L 05/20/23 21:30 05/24/23 23:11 124 U H Qp-Phenylene diamine
9.6 0.85 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QPronamide
9.6 0.60 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QPyrene
9.6 0.77 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QSafrole, Total
9.6 1.9 ug/L 05/20/23 21:30 05/24/23 23:11 14.8 U H Qsym-Trinitrobenzene
9.6 0.87 ug/L 05/20/23 21:30 05/24/23 23:11 11.9 U H QThionazin
2,4,6-Tribromophenol (Surr)24 Q 43-140 05/20/23 21:30 05/24/23 23:11 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)7 Q 05/20/23 21:30 05/24/23 23:11 144-119
2-Fluorophenol (Surr)9 Q 05/20/23 21:30 05/24/23 23:11 119-119
Nitrobenzene-d5 (Surr)12 Q 05/20/23 21:30 05/24/23 23:11 144-120
Phenol-d5 (Surr)7 Q 05/20/23 21:30 05/24/23 23:11 127-110
Terphenyl-d14 (Surr)32 Q 05/20/23 21:30 05/24/23 23:11 150-134
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
1400 J1 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
13 D 10 2.0 ug/L 05/10/23 15:21 2
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
200 50 ug/L 05/10/23 15:21 2340 D M J1C5-C8 Aliphatics
200 20 ug/L 05/10/23 15:21 2450 D M J1C9-C10 Aromatics
200 50 ug/L 05/10/23 15:21 21100 D M J1C9-C12 Aliphatics
10 2.0 ug/L 05/10/23 15:21 233 DEthylbenzene
10 2.0 ug/L 05/10/23 15:21 24.0 UMethyl tert-butyl ether
12 4.0 ug/L 05/10/23 15:21 247 D MNaphthalene
10 2.0 ug/L 05/10/23 15:21 24.0 UToluene
200 50 ug/L 05/10/23 15:21 2450 DC9-C12 Aliphatics (adjusted)
20 5.0 ug/L 05/10/23 15:21 2180 D J1m-Xylene & p-Xylene
10 2.0 ug/L 05/10/23 15:21 25.5 J Do-Xylene
200 50 ug/L 05/10/23 15:21 2330 DC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)157 M Q 70-130 05/10/23 15:21 2
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
a,a,a-Trifluorotoluene (pid)116 70-130 05/10/23 15:21 2
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.1 U 1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:55 165 JTotal EPH
11 4.8 ug/L 05/08/23 09:17 05/13/23 13:20 19.6 UPyrene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UBenzo[g,h,i]perylene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UIndeno[1,2,3-cd]pyrene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UBenzo[b]fluoranthene
1.9 0.48 ug/L 05/08/23 09:17 05/13/23 13:20 10.96 UFluoranthene
3.8 1.4 ug/L 05/08/23 09:17 05/13/23 13:20 12.9 UBenzo[k]fluoranthene
1.9 0.67 ug/L 05/08/23 09:17 05/13/23 13:20 10.98 JAcenaphthylene
1.9 0.48 ug/L 05/08/23 09:17 05/13/23 13:20 10.96 UChrysene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UBenzo[a]pyrene
1.9 0.48 ug/L 05/08/23 09:17 05/13/23 13:20 10.96 UDibenz(a,h)anthracene
1.9 0.67 ug/L 05/08/23 09:17 05/13/23 13:20 11.3 UBenzo[a]anthracene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UAcenaphthene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UPhenanthrene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 11.1 UFluorene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 115 MNaphthalene
1.9 0.57 ug/L 05/08/23 09:17 05/13/23 13:20 15.3 M2-Methylnaphthalene
38 9.6 ug/L 05/08/23 09:17 05/13/23 13:20 145C11-C22 Aromatics (unadjusted)
38 9.6 ug/L 05/08/23 09:17 05/13/23 13:20 124 JC11-C22 Aromatics (Adjusted)
48 9.6 ug/L 05/08/23 09:17 05/13/23 14:49 119 UC19-C36 Aliphatics
29 9.6 ug/L 05/08/23 09:17 05/13/23 14:49 120 J BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)36 Q 40-140 05/08/23 09:17 05/13/23 14:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)67 05/08/23 09:17 05/13/23 13:20 140-140
o- terphenyl (Surr)49 05/08/23 09:17 05/13/23 13:20 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U M H 1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
12 4.8 ug/L 05/23/23 09:00 06/01/23 03:59 19.6 U M HPyrene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U HBenzo[g,h,i]perylene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U HIndeno[1,2,3-cd]pyrene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U HBenzo[b]fluoranthene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 03:59 10.96 U M HFluoranthene
3.8 1.4 ug/L 05/23/23 09:00 06/01/23 03:59 12.9 U HBenzo[k]fluoranthene
1.9 0.67 ug/L 05/23/23 09:00 06/01/23 03:59 12.4 M HAcenaphthylene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 03:59 10.96 U M HChrysene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U HBenzo[a]pyrene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 03:59 10.96 U HDibenz(a,h)anthracene
1.9 0.67 ug/L 05/23/23 09:00 06/01/23 03:59 11.3 U HBenzo[a]anthracene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U M HAcenaphthene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U M HPhenanthrene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 11.2 U M HFluorene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 136 M H J1Naphthalene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-5Client Sample ID: TW7-03-04-23
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
19 M H 1.9 0.58 ug/L 05/23/23 09:00 06/01/23 03:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Methylnaphthalene
38 9.6 ug/L 05/23/23 09:00 06/01/23 03:59 1110 M HC11-C22 Aromatics (unadjusted)
38 9.6 ug/L 05/23/23 09:00 06/01/23 03:59 155 HC11-C22 Aromatics (Adjusted)
48 9.6 ug/L 05/23/23 09:00 06/01/23 04:22 111 J M HC19-C36 Aliphatics
29 9.6 ug/L 05/23/23 09:00 06/01/23 04:22 1150 M H B J1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)46 40-140 05/23/23 09:00 06/01/23 04:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)92 M 05/23/23 09:00 06/01/23 03:59 140-140
o- terphenyl (Surr)66 M 05/23/23 09:00 06/01/23 03:59 140-140
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 05/05/23 10:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
50 20 ug/L 05/05/23 10:39 1310 Q MAcetonitrile
50 15 ug/L 05/05/23 10:39 158Acrolein
50 5.5 ug/L 05/05/23 10:39 120 U MAcrylonitrile
2.0 0.27 ug/L 05/05/23 10:39 146Benzene
1.0 0.24 ug/L 05/05/23 10:39 10.50 UBromobenzene
2.0 0.34 ug/L 05/05/23 10:39 11.0 UBromochloromethane
2.0 0.25 ug/L 05/05/23 10:39 11.0 UBromodichloromethane
2.5 0.59 ug/L 05/05/23 10:39 12.0 U QBromoform
20 3.7 ug/L 05/05/23 10:39 110 U QBromomethane
25 6.4 ug/L 05/05/23 10:39 120 U M2-Butanone (MEK)
2.5 0.52 ug/L 05/05/23 10:39 12.0 Un-Butylbenzene
2.5 0.53 ug/L 05/05/23 10:39 12.2 Jsec-Butylbenzene
2.0 0.43 ug/L 05/05/23 10:39 10.54 Jtert-Butylbenzene
2.0 0.43 ug/L 05/05/23 10:39 10.68 JCarbon disulfide
2.0 0.30 ug/L 05/05/23 10:39 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/05/23 10:39 10.50 UChlorobenzene
2.5 0.71 ug/L 05/05/23 10:39 12.0 U2-Chloro-1,3-butadiene
20 4.6 ug/L 05/05/23 10:39 110 UChloroethane
25 0.59 ug/L 05/05/23 10:39 120 U2-Chloroethyl vinyl ether
2.0 0.27 ug/L 05/05/23 10:39 11.0 UChloroform
2.5 0.54 ug/L 05/05/23 10:39 12.0 UChloromethane
5.0 1.1 ug/L 05/05/23 10:39 14.0 U MAllyl chloride
1.0 0.25 ug/L 05/05/23 10:39 10.50 U2-Chlorotoluene
2.0 0.41 ug/L 05/05/23 10:39 11.0 U4-Chlorotoluene
2.0 0.39 ug/L 05/05/23 10:39 11.0 UChlorodibromomethane
10 1.8 ug/L 05/05/23 10:39 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/05/23 10:39 11.0 U1,2-Dibromoethane
2.0 0.34 ug/L 05/05/23 10:39 11.0 UDibromomethane
2.0 0.31 ug/L 05/05/23 10:39 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 10:39 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/05/23 10:39 11.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/05/23 10:39 15.0 U Q Mtrans-1,4-Dichloro-2-butene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U 2.0 0.36 ug/L 05/05/23 10:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Dichlorodifluoromethane
2.0 0.33 ug/L 05/05/23 10:39 11.0 U M1,1-Dichloroethane
2.0 0.25 ug/L 05/05/23 10:39 11.0 U M1,2-Dichloroethane
2.0 0.25 ug/L 05/05/23 10:39 11.0 Ucis-1,2-Dichloroethene
2.0 0.34 ug/L 05/05/23 10:39 11.0 Utrans-1,2-Dichloroethene
2.0 0.37 ug/L 05/05/23 10:39 11.0 U1,2-Dichloroethene, Total
2.0 0.33 ug/L 05/05/23 10:39 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/05/23 10:39 10.50 U1,2-Dichloropropane
2.0 0.36 ug/L 05/05/23 10:39 11.0 U1,3-Dichloropropane
2.0 0.35 ug/L 05/05/23 10:39 11.0 U2,2-Dichloropropane
2.0 0.28 ug/L 05/05/23 10:39 11.0 U1,1-Dichloropropene
2.0 0.26 ug/L 05/05/23 10:39 11.0 Ucis-1,3-Dichloropropene
2.0 0.23 ug/L 05/05/23 10:39 11.0 Utrans-1,3-Dichloropropene
1.0 0.20 ug/L 05/05/23 10:39 13.2Ethylbenzene
2.0 0.33 ug/L 05/05/23 10:39 11.0 UEthyl methacrylate
5.0 0.22 ug/L 05/05/23 10:39 11.0 UHexachlorobutadiene
20 3.2 ug/L 05/05/23 10:39 110 U2-Hexanone
20 3.9 ug/L 05/05/23 10:39 110 U QIodomethane
500 68 ug/L 05/05/23 10:39 1250 U MIsobutyl alcohol
2.0 0.26 ug/L 05/05/23 10:39 15.9Isopropylbenzene
2.0 0.44 ug/L 05/05/23 10:39 11.3 Jp-Isopropyltoluene
20 5.0 ug/L 05/05/23 10:39 110 U QMethacrylonitrile
20 3.2 ug/L 05/05/23 10:39 110 UMethylene Chloride
2.5 0.78 ug/L 05/05/23 10:39 12.0 UMethyl methacrylate
20 2.7 ug/L 05/05/23 10:39 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/05/23 10:39 12.0 UMethyl tert-butyl ether
10 2.4 ug/L 05/05/23 10:39 136Naphthalene
5.0 0.50 ug/L 05/05/23 10:39 11.0 U QPentachloroethane
20 5.0 ug/L 05/05/23 10:39 110 U Q MPropionitrile
2.0 0.41 ug/L 05/05/23 10:39 11.1 JN-Propylbenzene
2.0 0.27 ug/L 05/05/23 10:39 11.0 UStyrene
2.0 0.36 ug/L 05/05/23 10:39 11.0 U1,1,1,2-Tetrachloroethane
2.0 0.40 ug/L 05/05/23 10:39 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/05/23 10:39 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/05/23 10:39 11.0 JToluene
5.0 0.81 ug/L 05/05/23 10:39 12.0 U1,2,3-Trichlorobenzene
5.0 0.53 ug/L 05/05/23 10:39 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/05/23 10:39 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/05/23 10:39 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/05/23 10:39 10.50 UTrichloroethene
2.0 0.33 ug/L 05/05/23 10:39 11.0 UTrichlorofluoromethane
2.0 0.48 ug/L 05/05/23 10:39 11.0 U1,2,3-Trichloropropane
1.0 0.23 ug/L 05/05/23 10:39 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.43 ug/L 05/05/23 10:39 1531,2,4-Trimethylbenzene
2.0 0.28 ug/L 05/05/23 10:39 1141,3,5-Trimethylbenzene
2.5 0.69 ug/L 05/05/23 10:39 12.0 U MVinyl acetate
2.0 0.40 ug/L 05/05/23 10:39 11.0 UVinyl chloride
2.0 0.26 ug/L 05/05/23 10:39 19.2o-Xylene
2.0 0.49 ug/L 05/05/23 10:39 1130m-Xylene & p-Xylene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
140 2.0 0.49 ug/L 05/05/23 10:39 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Xylenes, Total
2.0 0.28 ug/L 05/05/23 10:39 132Cyclohexane
5.0 1.1 ug/L 05/05/23 10:39 14.0 U M1-Chlorohexane
20 3.2 ug/L 05/05/23 10:39 110 UMethyl acetate
2.0 0.33 ug/L 05/05/23 10:39 112Methylcyclohexane
10 2.1 ug/L 05/05/23 10:39 15.0 UTetrahydrofuran
10 0.70 ug/L 05/05/23 10:39 12.0 UDiisopropyl ether
5.0 0.65 ug/L 05/05/23 10:39 117Hexane
5.0 0.37 ug/L 05/05/23 10:39 11.0 UDiethyl ether
2.0 0.43 ug/L 05/05/23 10:39 11.0 U MHeptane
2.0 0.48 ug/L 05/05/23 10:39 11.0 U1,3-Dichloropropene, Total
10 2.5 ug/L 05/05/23 10:39 113 Q2-Methylnaphthalene
2.0 0.38 ug/L 05/05/23 10:39 11.0 U M1,3-Butadiene
5.0 0.50 ug/L 05/05/23 10:39 11.0 U Qn-Butyl acetate
2.0 0.50 ug/L 05/05/23 10:39 11.0 UDichlorofluoromethane
10 2.5 ug/L 05/05/23 10:39 15.0 U QBenzyl chloride
50 6.9 ug/L 05/05/23 10:39 120 Utert-Butyl alcohol
200 50 ug/L 05/05/23 10:39 1100 U QEthanol
250 92 ug/L 05/05/23 10:39 1200 U Q1,4-Dioxane
4.0 0.86 ug/L 05/05/23 10:39 12.0 U Q M2-Nitropropane
10 2.5 ug/L 05/05/23 10:39 15.0 U1,3,5-Trichlorobenzene
10 2.5 ug/L 05/05/23 10:39 126 Q1,2,3-Trimethylbenzene
100 25 ug/L 05/05/23 10:39 150 U Q Mn-Butyl alcohol
2.5 0.78 ug/L 05/05/23 10:39 12.0 UTert-amyl methyl ether
100 25 ug/L 05/05/23 10:39 150 U Q M2-Propanol
2.5 0.72 ug/L 05/05/23 10:39 12.0 UEthyl tert-butyl ether
20 5.0 ug/L 05/05/23 10:39 110 U QEthyl acetate
25 8.6 ug/L 05/05/23 10:39 120 U Q M2-Butanol, 2-methyl-
5.0 0.99 ug/L 05/05/23 10:39 12.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)101 89-112 05/05/23 10:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)84 05/05/23 10:39 181-118
Dibromofluoromethane (Surr)94 05/05/23 10:39 180-119
4-Bromofluorobenzene (Surr)107 05/05/23 10:39 185-114
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
1.9 U 9.6 0.73 ug/L 05/05/23 21:00 05/10/23 22:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.6 0.54 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U1,2,4-Trichlorobenzene
9.6 0.51 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U1,2-Dichlorobenzene
9.6 0.56 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U1,3-Dichlorobenzene
9.6 0.57 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U M1,3-Dinitrobenzene
9.6 0.52 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U1,4-Dichlorobenzene
9.6 0.59 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Q1,4-Naphthoquinone
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U1-Naphthylamine
9.6 0.69 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Q2,3,4,6-Tetrachlorophenol
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Q2,4,5-Trichlorophenol
9.6 0.81 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2,4,6-Trichlorophenol
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2,4-Dichlorophenol
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
9.6 U 9.6 3.8 ug/L 05/05/23 21:00 05/10/23 22:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2,4-Dimethylphenol
48 9.6 ug/L 05/05/23 21:00 05/10/23 22:34 119 U Q2,4-Dinitrophenol
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U M2,4-Dinitrotoluene
9.6 0.70 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2,6-Dichlorophenol
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2,6-Dinitrotoluene
9.6 1.5 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U Q2-Acetylaminofluorene
9.6 0.76 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2-Chloronaphthalene
9.6 0.83 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2-Chlorophenol
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 18.9 J2-Methylnaphthalene
9.6 0.85 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2-Methylphenol
9.6 1.4 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U2-Naphthylamine
48 1.2 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2-Nitroaniline
9.6 0.73 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U2-Nitrophenol
9.6 1.2 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U3 & 4 Methylphenol
57 29 ug/L 05/05/23 21:00 05/10/23 22:34 157 U3,3'-Dichlorobenzidine
19 9.6 ug/L 05/05/23 21:00 05/10/23 22:34 112 U Q3,3'-Dimethylbenzidine
9.6 1.3 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U Q3-Methylcholanthrene
48 4.8 ug/L 05/05/23 21:00 05/10/23 22:34 19.6 U3-Nitroaniline
48 9.6 ug/L 05/05/23 21:00 05/10/23 22:34 119 U Q4,6-Dinitro-2-methylphenol
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U4-Aminobiphenyl
9.6 0.74 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U M4-Bromophenyl phenyl ether
9.6 0.96 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U4-Chloro-3-methylphenol
19 2.1 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U4-Chloroaniline
9.6 0.80 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U4-Chlorophenyl phenyl ether
48 4.8 ug/L 05/05/23 21:00 05/10/23 22:34 19.6 U4-Nitroaniline
48 1.8 ug/L 05/05/23 21:00 05/10/23 22:34 13.8 U Q4-Nitrophenol
24 9.6 ug/L 05/05/23 21:00 05/10/23 22:34 119 U4-Nitroquinoline-1-oxide
9.6 1.4 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U5-Nitro-o-toluidine
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Q7,12-Dimethylbenz(a)anthracene
9.6 0.73 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QAcenaphthene
9.6 0.81 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QAcenaphthylene
9.6 0.54 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U MAcetophenone
1900 33 ug/L 05/05/23 21:00 05/10/23 22:34 176 Ualpha,alpha-Dimethyl phenethylamine
9.6 0.66 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QAnthracene
9.6 0.53 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QBenzo[a]anthracene
9.6 0.68 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QBenzo[a]pyrene
9.6 2.5 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U QBenzo[b]fluoranthene
9.6 0.83 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QBenzo[g,h,i]perylene
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QBenzo[k]fluoranthene
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U MBenzyl alcohol
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Mbis (2-chloroisopropyl) ether
9.6 0.90 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UBis(2-chloroethoxy)methane
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U MBis(2-chloroethyl)ether
9.6 1.5 ug/L 05/05/23 21:00 05/10/23 22:34 12.4 UBis(2-ethylhexyl) phthalate
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UButyl benzyl phthalate
9.6 0.49 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QChrysene
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QDiallate
9.6 0.96 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UDibenz(a,h)anthracene
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UDibenzofuran
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.9 U 9.6 0.84 ug/L 05/05/23 21:00 05/10/23 22:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Diethyl phthalate
9.6 0.72 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QDimethoate
9.6 0.95 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UDimethyl phthalate
9.6 0.79 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UDi-n-butyl phthalate
9.6 1.3 ug/L 05/05/23 21:00 05/10/23 22:34 12.4 UDi-n-octyl phthalate
9.6 4.8 ug/L 05/05/23 21:00 05/10/23 22:34 19.6 U QDinoseb
9.6 0.88 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UDiphenylamine
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QDisulfoton
9.6 0.92 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QEthyl methanesulfonate
9.6 1.2 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QEthyl Parathion
9.6 1.1 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QFamphur
9.6 0.71 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QFluoranthene
9.6 0.92 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QFluorene
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UHexachlorobenzene
9.6 0.59 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QHexachlorobutadiene
9.6 2.4 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 UHexachlorocyclopentadiene
9.6 0.73 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UHexachloroethane
9.6 1.3 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U QHexachloropropene
9.6 0.96 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QIndeno[1,2,3-cd]pyrene
9.6 0.86 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U MIsophorone
9.6 0.48 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QIsosafrole
1900 2.6 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U QMethapyrilene
9.6 0.57 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Q MMethyl methanesulfonate
9.6 0.84 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UMethyl parathion
9.6 0.67 ug/L 05/05/23 21:00 05/10/23 22:34 125 QNaphthalene
9.6 0.70 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UNitrobenzene
9.6 0.89 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UN-Nitrosodiethylamine
9.6 2.7 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U QN-Nitrosodimethylamine
9.6 0.92 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UN-Nitrosodi-n-butylamine
9.6 0.69 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UN-Nitrosodi-n-propylamine
9.6 0.88 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UN-Nitrosodiphenylamine
9.6 3.2 ug/L 05/05/23 21:00 05/10/23 22:34 19.6 UN-Nitrosomethylethylamine
9.6 0.84 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UN-Nitrosopiperidine
9.6 0.96 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UN-Nitrosopyrrolidine
9.6 0.96 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Mo,o',o''-Triethylphosphorothioate
9.6 1.3 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 Uo-Toluidine
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Mp-Dimethylamino azobenzene
9.6 0.50 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QPentachlorobenzene
9.6 0.75 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UPentachloronitrobenzene
48 1.9 ug/L 05/05/23 21:00 05/10/23 22:34 13.8 UPentachlorophenol
9.6 1.3 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 UPhenacetin
9.6 0.74 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QPhenanthrene
9.6 0.79 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U Q MPhenol
9.6 0.83 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UPhorate
1900 9.6 ug/L 05/05/23 21:00 05/10/23 22:34 124 U Qp-Phenylene diamine
9.6 0.85 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 UPronamide
9.6 0.60 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QPyrene
9.6 0.76 ug/L 05/05/23 21:00 05/10/23 22:34 11.9 U QSafrole, Total
9.6 1.9 ug/L 05/05/23 21:00 05/10/23 22:34 14.8 U Qsym-Trinitrobenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.9 U Q 9.6 0.87 ug/L 05/05/23 21:00 05/10/23 22:34 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Thionazin
2,4,6-Tribromophenol (Surr)71 43-140 05/05/23 21:00 05/10/23 22:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)69 05/05/23 21:00 05/10/23 22:34 144-119
2-Fluorophenol (Surr)48 05/05/23 21:00 05/10/23 22:34 119-119
Nitrobenzene-d5 (Surr)66 05/05/23 21:00 05/10/23 22:34 144-120
Phenol-d5 (Surr)6 Q 05/05/23 21:00 05/10/23 22:34 127-110
Terphenyl-d14 (Surr)24 Q 05/05/23 21:00 05/10/23 22:34 150-134
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE
LOQ DL
1.9 U H Q 9.7 0.74 ug/L 05/20/23 21:30 05/24/23 23:33 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2,4,5-Tetrachlorobenzene
9.7 0.54 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1,2,4-Trichlorobenzene
9.7 0.52 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1,2-Dichlorobenzene
9.7 0.57 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1,3-Dichlorobenzene
9.7 0.58 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1,3-Dinitrobenzene
9.7 0.52 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1,4-Dichlorobenzene
9.7 0.60 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1,4-Naphthoquinone
9.7 1.1 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q1-Naphthylamine
9.7 0.70 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,3,4,6-Tetrachlorophenol
9.7 1.2 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,4,5-Trichlorophenol
9.7 0.83 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,4,6-Trichlorophenol
9.7 1.1 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,4-Dichlorophenol
9.7 3.9 ug/L 05/20/23 21:30 05/24/23 23:33 19.7 U H Q2,4-Dimethylphenol
49 9.7 ug/L 05/20/23 21:30 05/24/23 23:33 119 U H Q2,4-Dinitrophenol
9.7 1.2 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,4-Dinitrotoluene
9.7 0.71 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,6-Dichlorophenol
9.7 1.1 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2,6-Dinitrotoluene
9.7 1.6 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Q2-Acetylaminofluorene
9.7 0.78 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2-Chloronaphthalene
9.7 0.85 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2-Chlorophenol
9.7 0.76 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2-Methylnaphthalene
9.7 0.86 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2-Methylphenol
9.7 1.5 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Q2-Naphthylamine
49 1.3 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2-Nitroaniline
9.7 0.74 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q2-Nitrophenol
9.7 1.3 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q3 & 4 Methylphenol
58 29 ug/L 05/20/23 21:30 05/24/23 23:33 158 U H Q3,3'-Dichlorobenzidine
19 9.7 ug/L 05/20/23 21:30 05/24/23 23:33 113 U H Q3,3'-Dimethylbenzidine
9.7 1.4 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Q3-Methylcholanthrene
49 4.9 ug/L 05/20/23 21:30 05/24/23 23:33 19.7 U H Q3-Nitroaniline
49 9.7 ug/L 05/20/23 21:30 05/24/23 23:33 119 U H Q4,6-Dinitro-2-methylphenol
9.7 1.2 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q4-Aminobiphenyl
9.7 0.75 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q4-Bromophenyl phenyl ether
9.7 0.97 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q4-Chloro-3-methylphenol
19 2.1 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Q4-Chloroaniline
9.7 0.82 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q4-Chlorophenyl phenyl ether
49 4.9 ug/L 05/20/23 21:30 05/24/23 23:33 19.7 U H Q4-Nitroaniline
49 1.8 ug/L 05/20/23 21:30 05/24/23 23:33 13.9 U H Q4-Nitrophenol
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
19 U H Q 24 9.7 ug/L 05/20/23 21:30 05/24/23 23:33 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
4-Nitroquinoline-1-oxide
9.7 1.5 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Q5-Nitro-o-toluidine
9.7 1.2 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Q7,12-Dimethylbenz(a)anthracene
9.7 0.74 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QAcenaphthene
9.7 0.83 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QAcenaphthylene
9.7 0.55 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H M QAcetophenone
1900 34 ug/L 05/20/23 21:30 05/24/23 23:33 178 U H Qalpha,alpha-Dimethyl phenethylamine
9.7 0.67 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QAnthracene
9.7 0.53 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QBenzo[a]anthracene
9.7 0.69 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QBenzo[a]pyrene
9.7 2.5 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H QBenzo[b]fluoranthene
9.7 0.85 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QBenzo[g,h,i]perylene
9.7 1.2 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QBenzo[k]fluoranthene
9.7 1.1 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H M QBenzyl alcohol
9.7 0.76 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Qbis (2-chloroisopropyl) ether
9.7 0.91 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QBis(2-chloroethoxy)methane
9.7 1.1 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QBis(2-chloroethyl)ether
9.7 1.6 ug/L 05/20/23 21:30 05/24/23 23:33 12.4 U H QBis(2-ethylhexyl) phthalate
9.7 1.2 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QButyl benzyl phthalate
9.7 0.50 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QChrysene
9.7 0.76 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDiallate
9.7 0.97 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDibenz(a,h)anthracene
9.7 0.77 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDibenzofuran
9.7 0.86 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDiethyl phthalate
9.7 0.73 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDimethoate
9.7 0.96 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDimethyl phthalate
9.7 0.81 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDi-n-butyl phthalate
9.7 1.4 ug/L 05/20/23 21:30 05/24/23 23:33 12.4 U H QDi-n-octyl phthalate
9.7 4.9 ug/L 05/20/23 21:30 05/24/23 23:33 19.7 U HDinoseb
9.7 0.89 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDiphenylamine
9.7 0.77 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QDisulfoton
9.7 0.93 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QEthyl methanesulfonate
9.7 1.3 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QEthyl Parathion
9.7 1.1 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QFamphur
9.7 0.72 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QFluoranthene
9.7 0.93 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QFluorene
9.7 0.77 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QHexachlorobenzene
9.7 0.60 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QHexachlorobutadiene
9.7 2.4 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H QHexachlorocyclopentadiene
9.7 0.74 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QHexachloroethane
9.7 1.4 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H QHexachloropropene
9.7 0.97 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QIndeno[1,2,3-cd]pyrene
9.7 0.87 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QIsophorone
9.7 0.49 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QIsosafrole
1900 2.6 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H QMethapyrilene
9.7 0.58 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QMethyl methanesulfonate
9.7 0.86 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QMethyl parathion
9.7 0.68 ug/L 05/20/23 21:30 05/24/23 23:33 11.3 J H QNaphthalene
9.7 0.71 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QNitrobenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
1.9 U H Q 9.7 0.90 ug/L 05/20/23 21:30 05/24/23 23:33 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
N-Nitrosodiethylamine
9.7 2.7 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H QN-Nitrosodimethylamine
9.7 0.93 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QN-Nitrosodi-n-butylamine
9.7 0.70 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QN-Nitrosodi-n-propylamine
9.7 0.89 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QN-Nitrosodiphenylamine
9.7 3.2 ug/L 05/20/23 21:30 05/24/23 23:33 19.7 U H QN-Nitrosomethylethylamine
9.7 0.86 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QN-Nitrosopiperidine
9.7 0.97 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QN-Nitrosopyrrolidine
9.7 0.97 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Qo,o',o''-Triethylphosphorothioate
9.7 1.4 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Qo-Toluidine
9.7 0.77 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H Qp-Dimethylamino azobenzene
9.7 0.51 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QPentachlorobenzene
9.7 0.76 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U HPentachloronitrobenzene
49 1.9 ug/L 05/20/23 21:30 05/24/23 23:33 13.9 U H QPentachlorophenol
9.7 1.4 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U HPhenacetin
9.7 0.75 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QPhenanthrene
9.7 0.81 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QPhenol
9.7 0.85 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QPhorate
1900 9.7 ug/L 05/20/23 21:30 05/24/23 23:33 124 U H M Qp-Phenylene diamine
9.7 0.86 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QPronamide
9.7 0.61 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QPyrene
9.7 0.78 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QSafrole, Total
9.7 1.9 ug/L 05/20/23 21:30 05/24/23 23:33 14.9 U H Qsym-Trinitrobenzene
9.7 0.88 ug/L 05/20/23 21:30 05/24/23 23:33 11.9 U H QThionazin
2,4,6-Tribromophenol (Surr)56 43-140 05/20/23 21:30 05/24/23 23:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)7 Q 05/20/23 21:30 05/24/23 23:33 144-119
2-Fluorophenol (Surr)1 M Q 05/20/23 21:30 05/24/23 23:33 119-119
Nitrobenzene-d5 (Surr)45 05/20/23 21:30 05/24/23 23:33 144-120
Phenol-d5 (Surr)0.6 Q 05/20/23 21:30 05/24/23 23:33 127-110
Terphenyl-d14 (Surr)9 Q 05/20/23 21:30 05/24/23 23:33 150-134
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
1100 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
44 5.0 1.0 ug/L 05/10/23 18:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 18:05 1550 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 18:05 1190 MC9-C10 Aromatics
100 25 ug/L 05/10/23 18:05 1540 MC9-C12 Aliphatics
5.0 1.0 ug/L 05/10/23 18:05 12.4 JEthylbenzene
5.0 1.0 ug/L 05/10/23 18:05 12.0 UMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 18:05 133 MNaphthalene
5.0 1.0 ug/L 05/10/23 18:05 11.1 JToluene
100 25 ug/L 05/10/23 18:05 1230C9-C12 Aliphatics (adjusted)
10 2.5 ug/L 05/10/23 18:05 1110m-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 18:05 18.4o-Xylene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
500 100 25 ug/L 05/10/23 18:05 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)182 Q 70-130 05/10/23 18:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)131 Q 05/10/23 18:05 170-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.3 U 2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:55 1250Total EPH
13 5.2 ug/L 05/08/23 09:17 05/13/23 14:27 110 UPyrene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UBenzo[g,h,i]perylene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UIndeno[1,2,3-cd]pyrene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UBenzo[b]fluoranthene
2.1 0.52 ug/L 05/08/23 09:17 05/13/23 14:27 11.0 UFluoranthene
4.2 1.6 ug/L 05/08/23 09:17 05/13/23 14:27 13.1 UBenzo[k]fluoranthene
2.1 0.73 ug/L 05/08/23 09:17 05/13/23 14:27 11.9 JAcenaphthylene
2.1 0.52 ug/L 05/08/23 09:17 05/13/23 14:27 11.0 UChrysene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UBenzo[a]pyrene
2.1 0.52 ug/L 05/08/23 09:17 05/13/23 14:27 11.0 UDibenz(a,h)anthracene
2.1 0.73 ug/L 05/08/23 09:17 05/13/23 14:27 11.5 UBenzo[a]anthracene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UAcenaphthene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UPhenanthrene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 11.3 UFluorene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 120 MNaphthalene
2.1 0.63 ug/L 05/08/23 09:17 05/13/23 14:27 15.5 M2-Methylnaphthalene
42 10 ug/L 05/08/23 09:17 05/13/23 14:27 171 MC11-C22 Aromatics (unadjusted)
42 10 ug/L 05/08/23 09:17 05/13/23 14:27 142C11-C22 Aromatics (Adjusted)
52 10 ug/L 05/08/23 09:17 05/13/23 15:57 168 MC19-C36 Aliphatics
31 10 ug/L 05/08/23 09:17 05/13/23 15:57 1110 M BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)43 40-140 05/08/23 09:17 05/13/23 15:57 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)68 05/08/23 09:17 05/13/23 14:27 140-140
o- terphenyl (Surr)53 05/08/23 09:17 05/13/23 14:27 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U H 2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
12 5.1 ug/L 05/23/23 09:00 06/01/23 07:45 110 U HPyrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U HBenzo[g,h,i]perylene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U HIndeno[1,2,3-cd]pyrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U HBenzo[b]fluoranthene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 07:45 11.0 U HFluoranthene
4.0 1.5 ug/L 05/23/23 09:00 06/01/23 07:45 13.0 U HBenzo[k]fluoranthene
2.0 0.71 ug/L 05/23/23 09:00 06/01/23 07:45 11.0 J HAcenaphthylene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 07:45 11.0 U HChrysene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U HBenzo[a]pyrene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 07:45 11.0 U HDibenz(a,h)anthracene
2.0 0.71 ug/L 05/23/23 09:00 06/01/23 07:45 11.4 U HBenzo[a]anthracene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-6Client Sample ID: MW7-22-04-23
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
1.2 U H 2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U HPhenanthrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U HFluorene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 119 M HNaphthalene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 07:45 11.2 U H2-Methylnaphthalene
40 10 ug/L 05/23/23 09:00 06/01/23 07:45 148 M HC11-C22 Aromatics (unadjusted)
40 10 ug/L 05/23/23 09:00 06/01/23 07:45 127 J HC11-C22 Aromatics (Adjusted)
51 10 ug/L 05/23/23 09:00 06/01/23 08:07 120 U M HC19-C36 Aliphatics
30 10 ug/L 05/23/23 09:00 06/01/23 08:07 152 H BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)38 M Q 40-140 05/23/23 09:00 06/01/23 08:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)89 05/23/23 09:00 06/01/23 07:45 140-140
o- terphenyl (Surr)61 05/23/23 09:00 06/01/23 07:45 140-140
Lab Sample ID: 680-234331-7Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
5.5 J 25 3.7 ug/L 05/04/23 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
50 20 ug/L 05/04/23 15:51 140 UAcetonitrile
50 15 ug/L 05/04/23 15:51 140 U QAcrolein
50 5.5 ug/L 05/04/23 15:51 120 UAcrylonitrile
2.0 0.27 ug/L 05/04/23 15:51 11.0 UBenzene
1.0 0.24 ug/L 05/04/23 15:51 10.50 UBromobenzene
2.0 0.34 ug/L 05/04/23 15:51 11.0 UBromochloromethane
2.0 0.25 ug/L 05/04/23 15:51 11.0 UBromodichloromethane
2.5 0.59 ug/L 05/04/23 15:51 12.0 U QBromoform
20 3.7 ug/L 05/04/23 15:51 110 UBromomethane
25 6.4 ug/L 05/04/23 15:51 120 U2-Butanone (MEK)
2.5 0.52 ug/L 05/04/23 15:51 12.0 Un-Butylbenzene
2.5 0.53 ug/L 05/04/23 15:51 12.0 Usec-Butylbenzene
2.0 0.43 ug/L 05/04/23 15:51 11.0 U Mtert-Butylbenzene
2.0 0.43 ug/L 05/04/23 15:51 11.0 UCarbon disulfide
2.0 0.30 ug/L 05/04/23 15:51 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/04/23 15:51 10.50 UChlorobenzene
2.5 0.71 ug/L 05/04/23 15:51 12.0 U2-Chloro-1,3-butadiene
20 4.6 ug/L 05/04/23 15:51 110 U QChloroethane
25 0.59 ug/L 05/04/23 15:51 120 U2-Chloroethyl vinyl ether
2.0 0.27 ug/L 05/04/23 15:51 11.0 UChloroform
2.5 0.54 ug/L 05/04/23 15:51 12.0 UChloromethane
5.0 1.1 ug/L 05/04/23 15:51 14.0 UAllyl chloride
1.0 0.25 ug/L 05/04/23 15:51 10.50 U2-Chlorotoluene
2.0 0.41 ug/L 05/04/23 15:51 11.0 U4-Chlorotoluene
2.0 0.39 ug/L 05/04/23 15:51 11.0 UChlorodibromomethane
10 1.8 ug/L 05/04/23 15:51 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/04/23 15:51 11.0 U1,2-Dibromoethane
2.0 0.34 ug/L 05/04/23 15:51 11.0 UDibromomethane
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-7Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U 2.0 0.31 ug/L 05/04/23 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,2-Dichlorobenzene
2.0 0.31 ug/L 05/04/23 15:51 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/04/23 15:51 11.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/04/23 15:51 15.0 U Qtrans-1,4-Dichloro-2-butene
2.0 0.36 ug/L 05/04/23 15:51 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/04/23 15:51 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 05/04/23 15:51 11.0 U M1,2-Dichloroethane
2.0 0.25 ug/L 05/04/23 15:51 11.0 Ucis-1,2-Dichloroethene
2.0 0.34 ug/L 05/04/23 15:51 11.0 Utrans-1,2-Dichloroethene
2.0 0.37 ug/L 05/04/23 15:51 11.0 U1,2-Dichloroethene, Total
2.0 0.33 ug/L 05/04/23 15:51 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/04/23 15:51 10.50 U1,2-Dichloropropane
2.0 0.36 ug/L 05/04/23 15:51 11.0 U1,3-Dichloropropane
2.0 0.35 ug/L 05/04/23 15:51 11.0 U2,2-Dichloropropane
2.0 0.28 ug/L 05/04/23 15:51 11.0 U1,1-Dichloropropene
2.0 0.26 ug/L 05/04/23 15:51 11.0 Ucis-1,3-Dichloropropene
2.0 0.23 ug/L 05/04/23 15:51 11.0 Utrans-1,3-Dichloropropene
1.0 0.20 ug/L 05/04/23 15:51 10.50 UEthylbenzene
2.0 0.33 ug/L 05/04/23 15:51 11.0 UEthyl methacrylate
5.0 0.22 ug/L 05/04/23 15:51 11.0 U QHexachlorobutadiene
20 3.2 ug/L 05/04/23 15:51 110 U2-Hexanone
20 3.9 ug/L 05/04/23 15:51 110 U QIodomethane
500 68 ug/L 05/04/23 15:51 1250 UIsobutyl alcohol
2.0 0.26 ug/L 05/04/23 15:51 11.0 UIsopropylbenzene
2.0 0.44 ug/L 05/04/23 15:51 11.0 Up-Isopropyltoluene
20 5.0 ug/L 05/04/23 15:51 110 UMethacrylonitrile
20 3.2 ug/L 05/04/23 15:51 110 UMethylene Chloride
2.5 0.78 ug/L 05/04/23 15:51 12.0 UMethyl methacrylate
20 2.7 ug/L 05/04/23 15:51 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/04/23 15:51 12.0 UMethyl tert-butyl ether
10 2.4 ug/L 05/04/23 15:51 15.0 U QNaphthalene
5.0 0.50 ug/L 05/04/23 15:51 11.0 U QPentachloroethane
20 5.0 ug/L 05/04/23 15:51 110 UPropionitrile
2.0 0.41 ug/L 05/04/23 15:51 11.0 UN-Propylbenzene
2.0 0.27 ug/L 05/04/23 15:51 11.0 UStyrene
2.0 0.36 ug/L 05/04/23 15:51 11.0 U1,1,1,2-Tetrachloroethane
2.0 0.40 ug/L 05/04/23 15:51 11.0 U Q1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/04/23 15:51 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/04/23 15:51 11.0 UToluene
5.0 0.81 ug/L 05/04/23 15:51 12.0 U Q1,2,3-Trichlorobenzene
5.0 0.53 ug/L 05/04/23 15:51 12.0 U Q1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/04/23 15:51 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/04/23 15:51 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/04/23 15:51 10.50 UTrichloroethene
2.0 0.33 ug/L 05/04/23 15:51 11.0 UTrichlorofluoromethane
2.0 0.48 ug/L 05/04/23 15:51 11.0 U Q1,2,3-Trichloropropane
1.0 0.23 ug/L 05/04/23 15:51 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.43 ug/L 05/04/23 15:51 11.0 U1,2,4-Trimethylbenzene
2.0 0.28 ug/L 05/04/23 15:51 11.0 U1,3,5-Trimethylbenzene
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Client Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Lab Sample ID: 680-234331-7Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U 2.5 0.69 ug/L 05/04/23 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Vinyl acetate
2.0 0.40 ug/L 05/04/23 15:51 11.0 UVinyl chloride
2.0 0.26 ug/L 05/04/23 15:51 11.0 Uo-Xylene
2.0 0.49 ug/L 05/04/23 15:51 11.0 Um-Xylene & p-Xylene
2.0 0.49 ug/L 05/04/23 15:51 11.0 UXylenes, Total
2.0 0.28 ug/L 05/04/23 15:51 11.0 UCyclohexane
5.0 1.1 ug/L 05/04/23 15:51 14.0 U M1-Chlorohexane
20 3.2 ug/L 05/04/23 15:51 110 UMethyl acetate
2.0 0.33 ug/L 05/04/23 15:51 11.0 UMethylcyclohexane
10 2.1 ug/L 05/04/23 15:51 12.7 JTetrahydrofuran
10 0.70 ug/L 05/04/23 15:51 12.0 UDiisopropyl ether
5.0 0.65 ug/L 05/04/23 15:51 12.0 UHexane
5.0 0.37 ug/L 05/04/23 15:51 11.0 UDiethyl ether
2.0 0.43 ug/L 05/04/23 15:51 11.0 UHeptane
2.0 0.48 ug/L 05/04/23 15:51 11.0 U1,3-Dichloropropene, Total
10 2.5 ug/L 05/04/23 15:51 15.0 U Q2-Methylnaphthalene
2.0 0.38 ug/L 05/04/23 15:51 11.0 U1,3-Butadiene
5.0 0.50 ug/L 05/04/23 15:51 11.0 Un-Butyl acetate
2.0 0.50 ug/L 05/04/23 15:51 11.0 UDichlorofluoromethane
10 2.5 ug/L 05/04/23 15:51 15.0 UBenzyl chloride
50 6.9 ug/L 05/04/23 15:51 120 U Mtert-Butyl alcohol
200 50 ug/L 05/04/23 15:51 1100 UEthanol
250 92 ug/L 05/04/23 15:51 1200 U1,4-Dioxane
4.0 0.86 ug/L 05/04/23 15:51 12.0 U Q2-Nitropropane
10 2.5 ug/L 05/04/23 15:51 15.0 U1,3,5-Trichlorobenzene
10 2.5 ug/L 05/04/23 15:51 15.0 U1,2,3-Trimethylbenzene
100 25 ug/L 05/04/23 15:51 150 Un-Butyl alcohol
2.5 0.78 ug/L 05/04/23 15:51 12.0 UTert-amyl methyl ether
100 25 ug/L 05/04/23 15:51 150 U2-Propanol
2.5 0.72 ug/L 05/04/23 15:51 12.0 UEthyl tert-butyl ether
20 5.0 ug/L 05/04/23 15:51 110 UEthyl acetate
25 8.6 ug/L 05/04/23 15:51 120 U2-Butanol, 2-methyl-
5.0 0.99 ug/L 05/04/23 15:51 12.0 U M2,2,4-Trimethylpentane
Toluene-d8 (Surr)98 89-112 05/04/23 15:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)81 05/04/23 15:51 181-118
Dibromofluoromethane (Surr)92 05/04/23 15:51 180-119
4-Bromofluorobenzene (Surr)104 05/04/23 15:51 185-114
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-776880/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
LOQ DL
Acetone 10 U 25 3.7 ug/L 05/04/23 14:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
40 U 2050 ug/L 05/04/23 14:11 1Acetonitrile
40 U 1550 ug/L 05/04/23 14:11 1Acrolein
20 U 5.550 ug/L 05/04/23 14:11 1Acrylonitrile
1.0 U 0.272.0 ug/L 05/04/23 14:11 1Benzene
0.50 U 0.241.0 ug/L 05/04/23 14:11 1Bromobenzene
1.0 U 0.342.0 ug/L 05/04/23 14:11 1Bromochloromethane
1.0 U 0.252.0 ug/L 05/04/23 14:11 1Bromodichloromethane
2.0 U 0.592.5 ug/L 05/04/23 14:11 1Bromoform
10 U 3.720 ug/L 05/04/23 14:11 1Bromomethane
20 U 6.425 ug/L 05/04/23 14:11 12-Butanone (MEK)
2.0 U 0.522.5 ug/L 05/04/23 14:11 1n-Butylbenzene
2.0 U 0.532.5 ug/L 05/04/23 14:11 1sec-Butylbenzene
1.0 U M 0.432.0 ug/L 05/04/23 14:11 1tert-Butylbenzene
1.0 U 0.432.0 ug/L 05/04/23 14:11 1Carbon disulfide
1.0 U 0.302.0 ug/L 05/04/23 14:11 1Carbon tetrachloride
0.50 U 0.151.0 ug/L 05/04/23 14:11 1Chlorobenzene
2.0 U 0.712.5 ug/L 05/04/23 14:11 12-Chloro-1,3-butadiene
10 U 4.620 ug/L 05/04/23 14:11 1Chloroethane
20 U 0.5925 ug/L 05/04/23 14:11 12-Chloroethyl vinyl ether
1.0 U 0.272.0 ug/L 05/04/23 14:11 1Chloroform
2.0 U 0.542.5 ug/L 05/04/23 14:11 1Chloromethane
4.0 U 1.15.0 ug/L 05/04/23 14:11 1Allyl chloride
0.50 U 0.251.0 ug/L 05/04/23 14:11 12-Chlorotoluene
1.0 U 0.412.0 ug/L 05/04/23 14:11 14-Chlorotoluene
1.0 U 0.392.0 ug/L 05/04/23 14:11 1Chlorodibromomethane
5.0 U 1.810 ug/L 05/04/23 14:11 11,2-Dibromo-3-Chloropropane
1.0 U 0.332.0 ug/L 05/04/23 14:11 11,2-Dibromoethane
1.0 U 0.342.0 ug/L 05/04/23 14:11 1Dibromomethane
1.0 U 0.312.0 ug/L 05/04/23 14:11 11,2-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/04/23 14:11 11,3-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/04/23 14:11 11,4-Dichlorobenzene
5.0 U 1.310 ug/L 05/04/23 14:11 1trans-1,4-Dichloro-2-butene
1.0 U 0.362.0 ug/L 05/04/23 14:11 1Dichlorodifluoromethane
1.0 U 0.332.0 ug/L 05/04/23 14:11 11,1-Dichloroethane
1.0 U M 0.252.0 ug/L 05/04/23 14:11 11,2-Dichloroethane
1.0 U 0.252.0 ug/L 05/04/23 14:11 1cis-1,2-Dichloroethene
1.0 U 0.342.0 ug/L 05/04/23 14:11 1trans-1,2-Dichloroethene
1.0 U 0.372.0 ug/L 05/04/23 14:11 11,2-Dichloroethene, Total
1.0 U 0.332.0 ug/L 05/04/23 14:11 11,1-Dichloroethene
0.50 U 0.221.0 ug/L 05/04/23 14:11 11,2-Dichloropropane
1.0 U 0.362.0 ug/L 05/04/23 14:11 11,3-Dichloropropane
1.0 U 0.352.0 ug/L 05/04/23 14:11 12,2-Dichloropropane
1.0 U 0.282.0 ug/L 05/04/23 14:11 11,1-Dichloropropene
1.0 U 0.262.0 ug/L 05/04/23 14:11 1cis-1,3-Dichloropropene
1.0 U 0.232.0 ug/L 05/04/23 14:11 1trans-1,3-Dichloropropene
0.50 U 0.201.0 ug/L 05/04/23 14:11 1Ethylbenzene
1.0 U 0.332.0 ug/L 05/04/23 14:11 1Ethyl methacrylate
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-776880/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
LOQ DL
Hexachlorobutadiene 1.0 U 5.0 0.22 ug/L 05/04/23 14:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 3.220 ug/L 05/04/23 14:11 12-Hexanone
10 U 3.920 ug/L 05/04/23 14:11 1Iodomethane
250 U 68500 ug/L 05/04/23 14:11 1Isobutyl alcohol
1.0 U 0.262.0 ug/L 05/04/23 14:11 1Isopropylbenzene
1.0 U 0.442.0 ug/L 05/04/23 14:11 1p-Isopropyltoluene
10 U 5.020 ug/L 05/04/23 14:11 1Methacrylonitrile
10 U 3.220 ug/L 05/04/23 14:11 1Methylene Chloride
2.0 U 0.782.5 ug/L 05/04/23 14:11 1Methyl methacrylate
10 U 2.720 ug/L 05/04/23 14:11 14-Methyl-2-pentanone (MIBK)
2.0 U 0.815.0 ug/L 05/04/23 14:11 1Methyl tert-butyl ether
5.0 U 2.410 ug/L 05/04/23 14:11 1Naphthalene
1.0 U 0.505.0 ug/L 05/04/23 14:11 1Pentachloroethane
10 U 5.020 ug/L 05/04/23 14:11 1Propionitrile
1.0 U 0.412.0 ug/L 05/04/23 14:11 1N-Propylbenzene
1.0 U 0.272.0 ug/L 05/04/23 14:11 1Styrene
1.0 U 0.362.0 ug/L 05/04/23 14:11 11,1,1,2-Tetrachloroethane
1.0 U 0.402.0 ug/L 05/04/23 14:11 11,1,2,2-Tetrachloroethane
1.0 U 0.352.0 ug/L 05/04/23 14:11 1Tetrachloroethene
1.0 U 0.252.0 ug/L 05/04/23 14:11 1Toluene
2.0 U 0.815.0 ug/L 05/04/23 14:11 11,2,3-Trichlorobenzene
2.0 U 0.535.0 ug/L 05/04/23 14:11 11,2,4-Trichlorobenzene
0.50 U 0.211.0 ug/L 05/04/23 14:11 11,1,1-Trichloroethane
1.0 U 0.322.0 ug/L 05/04/23 14:11 11,1,2-Trichloroethane
0.50 U 0.201.0 ug/L 05/04/23 14:11 1Trichloroethene
1.0 U 0.332.0 ug/L 05/04/23 14:11 1Trichlorofluoromethane
1.0 U 0.482.0 ug/L 05/04/23 14:11 11,2,3-Trichloropropane
0.50 U 0.231.0 ug/L 05/04/23 14:11 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 0.432.0 ug/L 05/04/23 14:11 11,2,4-Trimethylbenzene
1.0 U 0.282.0 ug/L 05/04/23 14:11 11,3,5-Trimethylbenzene
2.0 U 0.692.5 ug/L 05/04/23 14:11 1Vinyl acetate
1.0 U 0.402.0 ug/L 05/04/23 14:11 1Vinyl chloride
1.0 U 0.262.0 ug/L 05/04/23 14:11 1o-Xylene
1.0 U 0.492.0 ug/L 05/04/23 14:11 1m-Xylene & p-Xylene
1.0 U 0.492.0 ug/L 05/04/23 14:11 1Xylenes, Total
1.0 U 0.282.0 ug/L 05/04/23 14:11 1Cyclohexane
4.0 U 1.15.0 ug/L 05/04/23 14:11 11-Chlorohexane
10 U 3.220 ug/L 05/04/23 14:11 1Methyl acetate
1.0 U 0.332.0 ug/L 05/04/23 14:11 1Methylcyclohexane
5.0 U 2.110 ug/L 05/04/23 14:11 1Tetrahydrofuran
2.0 U 0.7010 ug/L 05/04/23 14:11 1Diisopropyl ether
2.0 U 0.655.0 ug/L 05/04/23 14:11 1Hexane
1.0 U 0.375.0 ug/L 05/04/23 14:11 1Diethyl ether
1.0 U 0.432.0 ug/L 05/04/23 14:11 1Heptane
1.0 U 0.482.0 ug/L 05/04/23 14:11 11,3-Dichloropropene, Total
5.0 U 2.510 ug/L 05/04/23 14:11 12-Methylnaphthalene
1.0 U 0.382.0 ug/L 05/04/23 14:11 11,3-Butadiene
1.0 U 0.505.0 ug/L 05/04/23 14:11 1n-Butyl acetate
1.0 U 0.502.0 ug/L 05/04/23 14:11 1Dichlorofluoromethane
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-776880/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
LOQ DL
Benzyl chloride 5.0 U 10 2.5 ug/L 05/04/23 14:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
20 U 6.950 ug/L 05/04/23 14:11 1tert-Butyl alcohol
100 U 50200 ug/L 05/04/23 14:11 1Ethanol
200 U 92250 ug/L 05/04/23 14:11 11,4-Dioxane
2.0 U 0.864.0 ug/L 05/04/23 14:11 12-Nitropropane
5.0 U 2.510 ug/L 05/04/23 14:11 11,3,5-Trichlorobenzene
5.0 U 2.510 ug/L 05/04/23 14:11 11,2,3-Trimethylbenzene
50 U 25100 ug/L 05/04/23 14:11 1n-Butyl alcohol
2.0 U 0.782.5 ug/L 05/04/23 14:11 1Tert-amyl methyl ether
50 U 25100 ug/L 05/04/23 14:11 12-Propanol
2.0 U 0.722.5 ug/L 05/04/23 14:11 1Ethyl tert-butyl ether
10 U 5.020 ug/L 05/04/23 14:11 1Ethyl acetate
20 U 8.625 ug/L 05/04/23 14:11 12-Butanol, 2-methyl-
2.0 U 0.995.0 ug/L 05/04/23 14:11 12,2,4-Trimethylpentane
Toluene-d8 (Surr)98 89-112 05/04/23 14:11 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
80 Q 05/04/23 14:11 11,2-Dichloroethane-d4 (Surr)81-118
89 05/04/23 14:11 1Dibromofluoromethane (Surr)80-119
105 05/04/23 14:11 14-Bromofluorobenzene (Surr)85-114
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-776880/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
Acetone 250 264 ug/L 106 39 -160
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Acrolein 1000 1230 ug/L 123 39 -155
Acrylonitrile 500 535 ug/L 107 63 -135
Benzene 50.0 52.9 ug/L 106 79 -120
Bromobenzene 50.0 48.5 ug/L 97 80 -120
Bromochloromethane 50.0 53.2 ug/L 106 78 -123
Bromodichloromethane 50.0 48.0 ug/L 96 79 -125
Bromoform 50.0 38.7 ug/L 77 66 -130
Bromomethane 50.0 42.4 ug/L 85 53 -141
2-Butanone (MEK)250 276 ug/L 110 56 -143
n-Butylbenzene 50.0 48.7 ug/L 97 75 -128
sec-Butylbenzene 50.0 48.3 ug/L 97 77 -126
tert-Butylbenzene 50.0 48.8 ug/L 98 78 -124
Carbon disulfide 50.0 51.5 ug/L 103 64 -133
Carbon tetrachloride 50.0 44.4 ug/L 89 72 -136
Chlorobenzene 50.0 49.7 ug/L 99 82 -118
Chloroethane 50.0 50.7 ug/L 101 60 -138
2-Chloroethyl vinyl ether 50.0 51.9 ug/L 104 51 -139
Chloroform 50.0 50.5 ug/L 101 79 -124
Chloromethane 50.0 49.6 ug/L 99 50 -139
Allyl chloride 50.0 52.5 ug/L 105 68 -130
2-Chlorotoluene 50.0 48.3 ug/L 97 79 -122
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-776880/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
4-Chlorotoluene 50.0 47.8 ug/L 96 78 -122
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Chlorodibromomethane 50.0 46.1 ug/L 92 74 -126
1,2-Dibromo-3-Chloropropane 50.0 38.3 ug/L 77 62 -128
1,2-Dibromoethane 50.0 50.9 ug/L 102 75 -127
Dibromomethane 50.0 50.6 ug/L 101 79 -123
1,2-Dichlorobenzene 50.0 48.1 ug/L 96 80 -119
1,3-Dichlorobenzene 50.0 48.4 ug/L 97 80 -119
1,4-Dichlorobenzene 50.0 48.4 ug/L 97 79 -118
trans-1,4-Dichloro-2-butene 50.0 45.3 ug/L 91 43 -140
Dichlorodifluoromethane 50.0 54.3 M ug/L 109 32 -152
1,1-Dichloroethane 50.0 51.8 ug/L 104 77 -125
1,2-Dichloroethane 50.0 48.7 ug/L 97 73 -128
cis-1,2-Dichloroethene 50.0 51.5 ug/L 103 78 -123
trans-1,2-Dichloroethene 50.0 52.6 ug/L 105 75 -124
1,2-Dichloroethene, Total 100 104 ug/L 104 79 -121
1,1-Dichloroethene 50.0 51.9 ug/L 104 71 -131
1,2-Dichloropropane 50.0 53.8 ug/L 108 78 -122
1,3-Dichloropropane 50.0 53.4 ug/L 107 80 -119
2,2-Dichloropropane 50.0 47.7 ug/L 95 60 -139
1,1-Dichloropropene 50.0 50.0 ug/L 100 79 -125
cis-1,3-Dichloropropene 50.0 49.7 ug/L 99 75 -124
trans-1,3-Dichloropropene 50.0 53.4 ug/L 107 73 -127
Ethylbenzene 50.0 49.5 ug/L 99 79 -121
Ethyl methacrylate 50.0 51.4 ug/L 103 72 -126
Hexachlorobutadiene 50.0 39.1 ug/L 78 66 -134
2-Hexanone 250 256 ug/L 102 57 -139
Iodomethane 50.0 36.6 ug/L 73 69 -131
Isobutyl alcohol 1250 1390 ug/L 111 63 -133
Isopropylbenzene 50.0 49.4 ug/L 99 72 -131
p-Isopropyltoluene 50.0 47.8 ug/L 96 77 -127
Methylene Chloride 50.0 53.2 ug/L 106 74 -124
4-Methyl-2-pentanone (MIBK)250 252 ug/L 101 67 -130
Methyl tert-butyl ether 50.0 50.6 ug/L 101 71 -124
Naphthalene 50.0 34.7 ug/L 69 61 -128
N-Propylbenzene 50.0 47.7 ug/L 95 76 -126
Styrene 50.0 49.7 ug/L 99 78 -123
1,1,1,2-Tetrachloroethane 50.0 46.4 ug/L 93 78 -124
1,1,2,2-Tetrachloroethane 50.0 47.6 ug/L 95 71 -121
Tetrachloroethene 50.0 50.9 ug/L 102 74 -129
Toluene 50.0 50.9 ug/L 102 80 -121
1,2,3-Trichlorobenzene 50.0 35.9 ug/L 72 69 -129
1,2,4-Trichlorobenzene 50.0 36.8 ug/L 74 69 -130
1,1,1-Trichloroethane 50.0 48.1 ug/L 96 74 -131
1,1,2-Trichloroethane 50.0 51.3 ug/L 103 80 -119
Trichloroethene 50.0 53.1 ug/L 106 79 -123
Trichlorofluoromethane 50.0 42.8 ug/L 86 65 -141
1,2,3-Trichloropropane 50.0 44.3 ug/L 89 73 -122
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 47.2 ug/L 94 70 -136
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-776880/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
1,2,4-Trimethylbenzene 50.0 46.4 ug/L 93 76 -124
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,3,5-Trimethylbenzene 50.0 46.2 ug/L 92 75 -124
Vinyl acetate 100 108 ug/L 108 54 -146
Vinyl chloride 50.0 48.5 ug/L 97 58 -137
o-Xylene 50.0 48.0 ug/L 96 78 -122
m-Xylene & p-Xylene 50.0 49.2 ug/L 98 80 -121
Xylenes, Total 100 97.2 ug/L 97 79 -121
Cyclohexane 50.0 50.3 ug/L 101 71 -130
Methyl acetate 100 103 ug/L 103 56 -136
Methylcyclohexane 50.0 49.3 ug/L 99 72 -132
Tetrahydrofuran 100 98.1 ug/L 98 57 -133
Hexane 50.0 51.6 ug/L 103 48 -143
Diethyl ether 50.0 51.4 ug/L 103 68 -129
Heptane 50.0 52.8 ug/L 106 49 -140
1,3-Dichloropropene, Total 100 103 ug/L 103 77 -123
1,3-Butadiene 50.0 47.8 ug/L 96 43 -158
Dichlorofluoromethane 50.0 49.0 ug/L 98
tert-Butyl alcohol 500 482 ug/L 96 68 -129
1,4-Dioxane 1000 1190 ug/L 119 59 -139
Toluene-d8 (Surr)89 -112
Surrogate
110
LCS LCS
Qualifier Limits%Recovery
981,2-Dichloroethane-d4 (Surr)81 -118
105Dibromofluoromethane (Surr)80 -119
984-Bromofluorobenzene (Surr)85 -114
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-776880/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
Acetone 250 267 ug/L 107 39 -160 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Acrolein 1000 1240 ug/L 124 39 -155 0 20
Acrylonitrile 500 553 ug/L 111 63 -135 3 20
Benzene 50.0 53.4 ug/L 107 79 -120 1 20
Bromobenzene 50.0 50.3 ug/L 101 80 -120 4 20
Bromochloromethane 50.0 53.2 ug/L 106 78 -123 0 20
Bromodichloromethane 50.0 48.5 ug/L 97 79 -125 1 20
Bromoform 50.0 40.2 ug/L 80 66 -130 4 20
Bromomethane 50.0 41.2 ug/L 82 53 -141 3 20
2-Butanone (MEK)250 283 ug/L 113 56 -143 3 20
n-Butylbenzene 50.0 53.4 ug/L 107 75 -128 9 20
sec-Butylbenzene 50.0 45.0 ug/L 90 77 -126 7 20
tert-Butylbenzene 50.0 49.0 ug/L 98 78 -124 0 20
Carbon disulfide 50.0 52.2 ug/L 104 64 -133 1 20
Carbon tetrachloride 50.0 45.9 ug/L 92 72 -136 3 20
Chlorobenzene 50.0 51.7 ug/L 103 82 -118 4 20
Chloroethane 50.0 40.2 Q ug/L 80 60 -138 23 20
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-776880/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
2-Chloroethyl vinyl ether 50.0 52.6 ug/L 105 51 -139 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloroform 50.0 51.3 ug/L 103 79 -124 2 20
Chloromethane 50.0 49.7 ug/L 99 50 -139 0 20
Allyl chloride 50.0 52.8 ug/L 106 68 -130 1 20
2-Chlorotoluene 50.0 50.5 ug/L 101 79 -122 4 20
4-Chlorotoluene 50.0 50.7 ug/L 101 78 -122 6 20
Chlorodibromomethane 50.0 46.5 ug/L 93 74 -126 1 20
1,2-Dibromo-3-Chloropropane 50.0 46.3 ug/L 93 62 -128 19 20
1,2-Dibromoethane 50.0 51.5 ug/L 103 75 -127 1 20
Dibromomethane 50.0 50.6 ug/L 101 79 -123 0 20
1,2-Dichlorobenzene 50.0 56.0 ug/L 112 80 -119 15 20
1,3-Dichlorobenzene 50.0 51.5 ug/L 103 80 -119 6 20
1,4-Dichlorobenzene 50.0 48.9 ug/L 98 79 -118 1 20
trans-1,4-Dichloro-2-butene 50.0 46.9 ug/L 94 43 -140 4 20
Dichlorodifluoromethane 50.0 54.0 M ug/L 108 32 -152 1 20
1,1-Dichloroethane 50.0 52.3 ug/L 105 77 -125 1 20
1,2-Dichloroethane 50.0 49.8 ug/L 100 73 -128 2 20
cis-1,2-Dichloroethene 50.0 52.2 ug/L 104 78 -123 1 20
trans-1,2-Dichloroethene 50.0 54.2 ug/L 108 75 -124 3 20
1,2-Dichloroethene, Total 100 106 ug/L 106 79 -121 2 20
1,1-Dichloroethene 50.0 52.0 ug/L 104 71 -131 0 20
1,2-Dichloropropane 50.0 54.8 ug/L 110 78 -122 2 20
1,3-Dichloropropane 50.0 54.3 ug/L 109 80 -119 2 20
2,2-Dichloropropane 50.0 48.7 ug/L 97 60 -139 2 20
1,1-Dichloropropene 50.0 50.9 ug/L 102 79 -125 2 20
cis-1,3-Dichloropropene 50.0 50.5 ug/L 101 75 -124 2 20
trans-1,3-Dichloropropene 50.0 53.7 ug/L 107 73 -127 1 20
Ethylbenzene 50.0 51.3 ug/L 103 79 -121 4 20
Ethyl methacrylate 50.0 52.5 ug/L 105 72 -126 2 20
Hexachlorobutadiene 50.0 56.4 Q ug/L 113 66 -134 36 20
2-Hexanone 250 260 ug/L 104 57 -139 1 20
Iodomethane 50.0 37.5 ug/L 75 69 -131 3 20
Isobutyl alcohol 1250 1400 ug/L 112 63 -133 1 20
Isopropylbenzene 50.0 51.5 ug/L 103 72 -131 4 20
p-Isopropyltoluene 50.0 49.6 ug/L 99 77 -127 4 20
Methylene Chloride 50.0 53.8 ug/L 108 74 -124 1 20
4-Methyl-2-pentanone (MIBK)250 256 ug/L 102 67 -130 2 20
Methyl tert-butyl ether 50.0 51.5 ug/L 103 71 -124 2 20
Naphthalene 50.0 56.1 Q ug/L 112 61 -128 47 20
N-Propylbenzene 50.0 49.7 ug/L 99 76 -126 4 20
Styrene 50.0 52.0 ug/L 104 78 -123 4 20
1,1,1,2-Tetrachloroethane 50.0 48.1 ug/L 96 78 -124 4 20
1,1,2,2-Tetrachloroethane 50.0 48.5 ug/L 97 71 -121 2 20
Tetrachloroethene 50.0 52.2 ug/L 104 74 -129 2 20
Toluene 50.0 51.3 ug/L 103 80 -121 1 20
1,2,3-Trichlorobenzene 50.0 54.3 Q ug/L 109 69 -129 41 20
1,2,4-Trichlorobenzene 50.0 55.4 Q ug/L 111 69 -130 40 20
1,1,1-Trichloroethane 50.0 48.6 ug/L 97 74 -131 1 20
1,1,2-Trichloroethane 50.0 51.4 ug/L 103 80 -119 0 20
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-776880/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 776880
Trichloroethene 50.0 54.4 ug/L 109 79 -123 2 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Trichlorofluoromethane 50.0 42.3 ug/L 85 65 -141 1 20
1,2,3-Trichloropropane 50.0 46.0 ug/L 92 73 -122 4 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 47.2 ug/L 94 70 -136 0 20
1,2,4-Trimethylbenzene 50.0 44.6 ug/L 89 76 -124 4 20
1,3,5-Trimethylbenzene 50.0 48.8 ug/L 98 75 -124 5 20
Vinyl acetate 100 102 ug/L 102 54 -146 5 20
Vinyl chloride 50.0 48.9 ug/L 98 58 -137 1 20
o-Xylene 50.0 49.5 ug/L 99 78 -122 3 20
m-Xylene & p-Xylene 50.0 50.9 ug/L 102 80 -121 3 20
Xylenes, Total 100 100 ug/L 100 79 -121 3 20
Cyclohexane 50.0 50.7 ug/L 101 71 -130 1 20
Methyl acetate 100 108 ug/L 108 56 -136 5 20
Methylcyclohexane 50.0 49.3 ug/L 99 72 -132 0 20
Tetrahydrofuran 100 106 ug/L 106 57 -133 7 20
Hexane 50.0 51.1 ug/L 102 48 -143 1 20
Diethyl ether 50.0 52.2 ug/L 104 68 -129 2 20
Heptane 50.0 51.2 ug/L 102 49 -140 3 20
1,3-Dichloropropene, Total 100 104 ug/L 104 77 -123 1 20
1,3-Butadiene 50.0 47.5 ug/L 95 43 -158 1 20
Dichlorofluoromethane 50.0 49.4 ug/L 99 1
tert-Butyl alcohol 500 494 ug/L 99 68 -129 2 20
1,4-Dioxane 1000 1230 ug/L 123 59 -139 3 20
Toluene-d8 (Surr)89 -112
Surrogate
112
LCSD LCSD
Qualifier Limits%Recovery
991,2-Dichloroethane-d4 (Surr)81 -118
106Dibromofluoromethane (Surr)80 -119
1134-Bromofluorobenzene (Surr)85 -114
Client Sample ID: Method BlankLab Sample ID: MB 680-777079/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
LOQ DL
Acetone 10 U 25 3.7 ug/L 05/05/23 08:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
40 U 2050 ug/L 05/05/23 08:34 1Acetonitrile
40 U 1550 ug/L 05/05/23 08:34 1Acrolein
20 U M 5.550 ug/L 05/05/23 08:34 1Acrylonitrile
1.0 U 0.272.0 ug/L 05/05/23 08:34 1Benzene
0.50 U 0.241.0 ug/L 05/05/23 08:34 1Bromobenzene
1.0 U 0.342.0 ug/L 05/05/23 08:34 1Bromochloromethane
1.0 U 0.252.0 ug/L 05/05/23 08:34 1Bromodichloromethane
2.0 U 0.592.5 ug/L 05/05/23 08:34 1Bromoform
10 U 3.720 ug/L 05/05/23 08:34 1Bromomethane
20 U 6.425 ug/L 05/05/23 08:34 12-Butanone (MEK)
2.0 U 0.522.5 ug/L 05/05/23 08:34 1n-Butylbenzene
2.0 U 0.532.5 ug/L 05/05/23 08:34 1sec-Butylbenzene
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-777079/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
LOQ DL
tert-Butylbenzene 1.0 U M 2.0 0.43 ug/L 05/05/23 08:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.658 J 0.432.0 ug/L 05/05/23 08:34 1Carbon disulfide
1.0 U 0.302.0 ug/L 05/05/23 08:34 1Carbon tetrachloride
0.50 U 0.151.0 ug/L 05/05/23 08:34 1Chlorobenzene
2.0 U 0.712.5 ug/L 05/05/23 08:34 12-Chloro-1,3-butadiene
10 U M 4.620 ug/L 05/05/23 08:34 1Chloroethane
20 U 0.5925 ug/L 05/05/23 08:34 12-Chloroethyl vinyl ether
1.0 U 0.272.0 ug/L 05/05/23 08:34 1Chloroform
2.0 U 0.542.5 ug/L 05/05/23 08:34 1Chloromethane
4.0 U 1.15.0 ug/L 05/05/23 08:34 1Allyl chloride
0.50 U 0.251.0 ug/L 05/05/23 08:34 12-Chlorotoluene
1.0 U 0.412.0 ug/L 05/05/23 08:34 14-Chlorotoluene
1.0 U 0.392.0 ug/L 05/05/23 08:34 1Chlorodibromomethane
5.0 U 1.810 ug/L 05/05/23 08:34 11,2-Dibromo-3-Chloropropane
1.0 U 0.332.0 ug/L 05/05/23 08:34 11,2-Dibromoethane
1.0 U 0.342.0 ug/L 05/05/23 08:34 1Dibromomethane
1.0 U 0.312.0 ug/L 05/05/23 08:34 11,2-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/05/23 08:34 11,3-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/05/23 08:34 11,4-Dichlorobenzene
5.0 U 1.310 ug/L 05/05/23 08:34 1trans-1,4-Dichloro-2-butene
1.0 U 0.362.0 ug/L 05/05/23 08:34 1Dichlorodifluoromethane
1.0 U 0.332.0 ug/L 05/05/23 08:34 11,1-Dichloroethane
1.0 U 0.252.0 ug/L 05/05/23 08:34 11,2-Dichloroethane
1.0 U 0.252.0 ug/L 05/05/23 08:34 1cis-1,2-Dichloroethene
1.0 U 0.342.0 ug/L 05/05/23 08:34 1trans-1,2-Dichloroethene
1.0 U 0.372.0 ug/L 05/05/23 08:34 11,2-Dichloroethene, Total
1.0 U 0.332.0 ug/L 05/05/23 08:34 11,1-Dichloroethene
0.50 U 0.221.0 ug/L 05/05/23 08:34 11,2-Dichloropropane
1.0 U 0.362.0 ug/L 05/05/23 08:34 11,3-Dichloropropane
1.0 U 0.352.0 ug/L 05/05/23 08:34 12,2-Dichloropropane
1.0 U 0.282.0 ug/L 05/05/23 08:34 11,1-Dichloropropene
1.0 U 0.262.0 ug/L 05/05/23 08:34 1cis-1,3-Dichloropropene
1.0 U 0.232.0 ug/L 05/05/23 08:34 1trans-1,3-Dichloropropene
0.50 U 0.201.0 ug/L 05/05/23 08:34 1Ethylbenzene
1.0 U 0.332.0 ug/L 05/05/23 08:34 1Ethyl methacrylate
1.0 U 0.225.0 ug/L 05/05/23 08:34 1Hexachlorobutadiene
10 U 3.220 ug/L 05/05/23 08:34 12-Hexanone
10 U 3.920 ug/L 05/05/23 08:34 1Iodomethane
250 U 68500 ug/L 05/05/23 08:34 1Isobutyl alcohol
1.0 U 0.262.0 ug/L 05/05/23 08:34 1Isopropylbenzene
1.0 U 0.442.0 ug/L 05/05/23 08:34 1p-Isopropyltoluene
10 U 5.020 ug/L 05/05/23 08:34 1Methacrylonitrile
10 U 3.220 ug/L 05/05/23 08:34 1Methylene Chloride
2.0 U 0.782.5 ug/L 05/05/23 08:34 1Methyl methacrylate
10 U 2.720 ug/L 05/05/23 08:34 14-Methyl-2-pentanone (MIBK)
2.0 U 0.815.0 ug/L 05/05/23 08:34 1Methyl tert-butyl ether
5.0 U 2.410 ug/L 05/05/23 08:34 1Naphthalene
1.0 U 0.505.0 ug/L 05/05/23 08:34 1Pentachloroethane
10 U 5.020 ug/L 05/05/23 08:34 1Propionitrile
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-777079/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
LOQ DL
N-Propylbenzene 1.0 U 2.0 0.41 ug/L 05/05/23 08:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
1.0 U 0.272.0 ug/L 05/05/23 08:34 1Styrene
1.0 U 0.362.0 ug/L 05/05/23 08:34 11,1,1,2-Tetrachloroethane
1.0 U 0.402.0 ug/L 05/05/23 08:34 11,1,2,2-Tetrachloroethane
1.0 U 0.352.0 ug/L 05/05/23 08:34 1Tetrachloroethene
1.0 U 0.252.0 ug/L 05/05/23 08:34 1Toluene
2.0 U 0.815.0 ug/L 05/05/23 08:34 11,2,3-Trichlorobenzene
2.0 U 0.535.0 ug/L 05/05/23 08:34 11,2,4-Trichlorobenzene
0.50 U 0.211.0 ug/L 05/05/23 08:34 11,1,1-Trichloroethane
1.0 U 0.322.0 ug/L 05/05/23 08:34 11,1,2-Trichloroethane
0.50 U 0.201.0 ug/L 05/05/23 08:34 1Trichloroethene
1.0 U 0.332.0 ug/L 05/05/23 08:34 1Trichlorofluoromethane
1.0 U 0.482.0 ug/L 05/05/23 08:34 11,2,3-Trichloropropane
0.50 U 0.231.0 ug/L 05/05/23 08:34 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 0.432.0 ug/L 05/05/23 08:34 11,2,4-Trimethylbenzene
1.0 U 0.282.0 ug/L 05/05/23 08:34 11,3,5-Trimethylbenzene
2.0 U 0.692.5 ug/L 05/05/23 08:34 1Vinyl acetate
1.0 U 0.402.0 ug/L 05/05/23 08:34 1Vinyl chloride
1.0 U 0.262.0 ug/L 05/05/23 08:34 1o-Xylene
1.0 U 0.492.0 ug/L 05/05/23 08:34 1m-Xylene & p-Xylene
1.0 U 0.492.0 ug/L 05/05/23 08:34 1Xylenes, Total
1.0 U 0.282.0 ug/L 05/05/23 08:34 1Cyclohexane
4.0 U 1.15.0 ug/L 05/05/23 08:34 11-Chlorohexane
10 U 3.220 ug/L 05/05/23 08:34 1Methyl acetate
1.0 U 0.332.0 ug/L 05/05/23 08:34 1Methylcyclohexane
5.0 U 2.110 ug/L 05/05/23 08:34 1Tetrahydrofuran
2.0 U 0.7010 ug/L 05/05/23 08:34 1Diisopropyl ether
2.0 U 0.655.0 ug/L 05/05/23 08:34 1Hexane
1.0 U 0.375.0 ug/L 05/05/23 08:34 1Diethyl ether
1.0 U 0.432.0 ug/L 05/05/23 08:34 1Heptane
1.0 U 0.482.0 ug/L 05/05/23 08:34 11,3-Dichloropropene, Total
5.0 U 2.510 ug/L 05/05/23 08:34 12-Methylnaphthalene
1.0 U 0.382.0 ug/L 05/05/23 08:34 11,3-Butadiene
1.0 U 0.505.0 ug/L 05/05/23 08:34 1n-Butyl acetate
1.0 U 0.502.0 ug/L 05/05/23 08:34 1Dichlorofluoromethane
5.0 U 2.510 ug/L 05/05/23 08:34 1Benzyl chloride
20 U 6.950 ug/L 05/05/23 08:34 1tert-Butyl alcohol
100 U 50200 ug/L 05/05/23 08:34 1Ethanol
200 U 92250 ug/L 05/05/23 08:34 11,4-Dioxane
2.0 U 0.864.0 ug/L 05/05/23 08:34 12-Nitropropane
5.0 U 2.510 ug/L 05/05/23 08:34 11,3,5-Trichlorobenzene
5.0 U 2.510 ug/L 05/05/23 08:34 11,2,3-Trimethylbenzene
50 U 25100 ug/L 05/05/23 08:34 1n-Butyl alcohol
2.0 U 0.782.5 ug/L 05/05/23 08:34 1Tert-amyl methyl ether
50 U 25100 ug/L 05/05/23 08:34 12-Propanol
2.0 U 0.722.5 ug/L 05/05/23 08:34 1Ethyl tert-butyl ether
10 U 5.020 ug/L 05/05/23 08:34 1Ethyl acetate
20 U 8.625 ug/L 05/05/23 08:34 12-Butanol, 2-methyl-
2.0 U 0.995.0 ug/L 05/05/23 08:34 12,2,4-Trimethylpentane
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Toluene-d8 (Surr)108 89-112 05/05/23 08:34 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
86 05/05/23 08:34 11,2-Dichloroethane-d4 (Surr)81-118
97 05/05/23 08:34 1Dibromofluoromethane (Surr)80-119
109 05/05/23 08:34 14-Bromofluorobenzene (Surr)85-114
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777079/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
Acetone 250 306 ug/L 122 39 -160
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Acrolein 1000 1110 ug/L 111 39 -155
Acrylonitrile 500 493 ug/L 99 63 -135
Benzene 50.0 51.1 ug/L 102 79 -120
Bromobenzene 50.0 48.3 ug/L 97 80 -120
Bromochloromethane 50.0 49.2 ug/L 98 78 -123
Bromodichloromethane 50.0 47.0 ug/L 94 79 -125
Bromoform 50.0 36.1 ug/L 72 66 -130
Bromomethane 50.0 26.6 ug/L 53 53 -141
2-Butanone (MEK)250 272 ug/L 109 56 -143
n-Butylbenzene 50.0 50.4 ug/L 101 75 -128
sec-Butylbenzene 50.0 49.3 ug/L 99 77 -126
tert-Butylbenzene 50.0 50.1 ug/L 100 78 -124
Carbon disulfide 50.0 50.7 ug/L 101 64 -133
Carbon tetrachloride 50.0 44.3 ug/L 89 72 -136
Chlorobenzene 50.0 49.7 ug/L 99 82 -118
Chloroethane 50.0 61.6 ug/L 123 60 -138
2-Chloroethyl vinyl ether 50.0 48.8 ug/L 98 51 -139
Chloroform 50.0 48.7 ug/L 97 79 -124
Chloromethane 50.0 52.7 ug/L 105 50 -139
Allyl chloride 50.0 45.6 ug/L 91 68 -130
2-Chlorotoluene 50.0 49.2 ug/L 98 79 -122
4-Chlorotoluene 50.0 49.8 ug/L 100 78 -122
Chlorodibromomethane 50.0 44.0 ug/L 88 74 -126
1,2-Dibromo-3-Chloropropane 50.0 37.9 ug/L 76 62 -128
1,2-Dibromoethane 50.0 49.3 ug/L 99 75 -127
Dibromomethane 50.0 48.0 ug/L 96 79 -123
1,2-Dichlorobenzene 50.0 48.7 ug/L 97 80 -119
1,3-Dichlorobenzene 50.0 48.7 ug/L 97 80 -119
1,4-Dichlorobenzene 50.0 48.3 ug/L 97 79 -118
trans-1,4-Dichloro-2-butene 50.0 31.5 ug/L 63 43 -140
Dichlorodifluoromethane 50.0 58.2 M ug/L 116 32 -152
1,1-Dichloroethane 50.0 48.5 ug/L 97 77 -125
1,2-Dichloroethane 50.0 48.1 ug/L 96 73 -128
cis-1,2-Dichloroethene 50.0 49.1 ug/L 98 78 -123
trans-1,2-Dichloroethene 50.0 51.2 ug/L 102 75 -124
1,2-Dichloroethene, Total 100 100 ug/L 100 79 -121
1,1-Dichloroethene 50.0 50.7 ug/L 101 71 -131
1,2-Dichloropropane 50.0 53.0 ug/L 106 78 -122
1,3-Dichloropropane 50.0 52.3 ug/L 105 80 -119
2,2-Dichloropropane 50.0 47.6 ug/L 95 60 -139
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777079/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
1,1-Dichloropropene 50.0 49.1 ug/L 98 79 -125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
cis-1,3-Dichloropropene 50.0 48.5 ug/L 97 75 -124
trans-1,3-Dichloropropene 50.0 51.4 ug/L 103 73 -127
Ethylbenzene 50.0 49.8 ug/L 100 79 -121
Ethyl methacrylate 50.0 49.9 ug/L 100 72 -126
Hexachlorobutadiene 50.0 50.2 ug/L 100 66 -134
2-Hexanone 250 261 ug/L 105 57 -139
Iodomethane 50.0 33.9 Q ug/L 68 69 -131
Isobutyl alcohol 1250 1340 ug/L 107 63 -133
Isopropylbenzene 50.0 50.5 ug/L 101 72 -131
p-Isopropyltoluene 50.0 48.3 ug/L 97 77 -127
Methylene Chloride 50.0 50.4 ug/L 101 74 -124
4-Methyl-2-pentanone (MIBK)250 247 ug/L 99 67 -130
Methyl tert-butyl ether 50.0 47.2 ug/L 94 71 -124
Naphthalene 50.0 48.5 ug/L 97 61 -128
N-Propylbenzene 50.0 49.2 ug/L 98 76 -126
Styrene 50.0 49.8 ug/L 100 78 -123
1,1,1,2-Tetrachloroethane 50.0 45.7 ug/L 91 78 -124
1,1,2,2-Tetrachloroethane 50.0 47.3 ug/L 95 71 -121
Tetrachloroethene 50.0 51.5 ug/L 103 74 -129
Toluene 50.0 50.2 ug/L 100 80 -121
1,2,3-Trichlorobenzene 50.0 47.6 ug/L 95 69 -129
1,2,4-Trichlorobenzene 50.0 48.1 ug/L 96 69 -130
1,1,1-Trichloroethane 50.0 47.1 ug/L 94 74 -131
1,1,2-Trichloroethane 50.0 50.1 ug/L 100 80 -119
Trichloroethene 50.0 52.5 ug/L 105 79 -123
Trichlorofluoromethane 50.0 44.0 ug/L 88 65 -141
1,2,3-Trichloropropane 50.0 44.0 ug/L 88 73 -122
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 48.1 ug/L 96 70 -136
1,2,4-Trimethylbenzene 50.0 47.3 ug/L 95 76 -124
1,3,5-Trimethylbenzene 50.0 47.2 ug/L 94 75 -124
Vinyl acetate 100 102 ug/L 102 54 -146
Vinyl chloride 50.0 52.8 ug/L 106 58 -137
o-Xylene 50.0 48.1 ug/L 96 78 -122
m-Xylene & p-Xylene 50.0 49.8 ug/L 100 80 -121
Xylenes, Total 100 97.9 ug/L 98 79 -121
Cyclohexane 50.0 50.8 ug/L 102 71 -130
Methyl acetate 100 94.5 ug/L 94 56 -136
Methylcyclohexane 50.0 51.8 ug/L 104 72 -132
Tetrahydrofuran 100 94.1 ug/L 94 57 -133
Hexane 50.0 53.7 ug/L 107 48 -143
Diethyl ether 50.0 46.3 ug/L 93 68 -129
Heptane 50.0 56.6 ug/L 113 49 -140
1,3-Dichloropropene, Total 100 99.9 ug/L 100 77 -123
1,3-Butadiene 50.0 55.4 ug/L 111 43 -158
Dichlorofluoromethane 50.0 41.9 ug/L 84
tert-Butyl alcohol 500 457 ug/L 91 68 -129
1,4-Dioxane 1000 1150 ug/L 115 59 -139
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Toluene-d8 (Surr)89 -112
Surrogate
110
LCS LCS
Qualifier Limits%Recovery
961,2-Dichloroethane-d4 (Surr)81 -118
100Dibromofluoromethane (Surr)80 -119
984-Bromofluorobenzene (Surr)85 -114
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-777079/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
Acetone 250 353 ug/L 141 39 -160 14 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Acrolein 1000 1280 ug/L 128 39 -155 14 20
Acrylonitrile 500 576 ug/L 115 63 -135 15 20
Benzene 50.0 52.2 ug/L 104 79 -120 2 20
Bromobenzene 50.0 49.3 ug/L 99 80 -120 2 20
Bromochloromethane 50.0 54.6 ug/L 109 78 -123 10 20
Bromodichloromethane 50.0 48.8 ug/L 98 79 -125 4 20
Bromoform 50.0 38.3 ug/L 77 66 -130 6 20
Bromomethane 50.0 27.9 ug/L 56 53 -141 5 20
2-Butanone (MEK)250 320 ug/L 128 56 -143 16 20
n-Butylbenzene 50.0 47.7 ug/L 95 75 -128 6 20
sec-Butylbenzene 50.0 46.9 ug/L 94 77 -126 5 20
tert-Butylbenzene 50.0 47.5 ug/L 95 78 -124 5 20
Carbon disulfide 50.0 50.0 ug/L 100 64 -133 1 20
Carbon tetrachloride 50.0 43.5 ug/L 87 72 -136 2 20
Chlorobenzene 50.0 49.8 ug/L 100 82 -118 0 20
Chloroethane 50.0 59.8 ug/L 120 60 -138 3 20
2-Chloroethyl vinyl ether 50.0 52.5 ug/L 105 51 -139 7 20
Chloroform 50.0 50.8 ug/L 102 79 -124 4 20
Chloromethane 50.0 50.5 ug/L 101 50 -139 4 20
Allyl chloride 50.0 45.7 ug/L 91 68 -130 0 20
2-Chlorotoluene 50.0 47.8 ug/L 96 79 -122 3 20
4-Chlorotoluene 50.0 48.1 ug/L 96 78 -122 3 20
Chlorodibromomethane 50.0 47.3 ug/L 95 74 -126 7 20
1,2-Dibromo-3-Chloropropane 50.0 41.3 ug/L 83 62 -128 9 20
1,2-Dibromoethane 50.0 53.2 ug/L 106 75 -127 8 20
Dibromomethane 50.0 52.4 ug/L 105 79 -123 9 20
1,2-Dichlorobenzene 50.0 48.9 ug/L 98 80 -119 0 20
1,3-Dichlorobenzene 50.0 48.7 ug/L 97 80 -119 0 20
1,4-Dichlorobenzene 50.0 48.1 ug/L 96 79 -118 0 20
trans-1,4-Dichloro-2-butene 50.0 33.6 ug/L 67 43 -140 6 20
Dichlorodifluoromethane 50.0 54.3 ug/L 109 32 -152 7 20
1,1-Dichloroethane 50.0 50.4 ug/L 101 77 -125 4 20
1,2-Dichloroethane 50.0 50.3 ug/L 101 73 -128 5 20
cis-1,2-Dichloroethene 50.0 51.5 ug/L 103 78 -123 5 20
trans-1,2-Dichloroethene 50.0 52.0 ug/L 104 75 -124 2 20
1,2-Dichloroethene, Total 100 103 ug/L 103 79 -121 3 20
1,1-Dichloroethene 50.0 50.0 ug/L 100 71 -131 1 20
1,2-Dichloropropane 50.0 54.8 ug/L 110 78 -122 3 20
1,3-Dichloropropane 50.0 56.6 ug/L 113 80 -119 8 20
2,2-Dichloropropane 50.0 47.4 ug/L 95 60 -139 0 20
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-777079/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
1,1-Dichloropropene 50.0 48.9 ug/L 98 79 -125 0 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
cis-1,3-Dichloropropene 50.0 50.4 ug/L 101 75 -124 4 20
trans-1,3-Dichloropropene 50.0 54.9 ug/L 110 73 -127 7 20
Ethylbenzene 50.0 47.9 ug/L 96 79 -121 4 20
Ethyl methacrylate 50.0 54.6 ug/L 109 72 -126 9 20
Hexachlorobutadiene 50.0 50.5 ug/L 101 66 -134 1 20
2-Hexanone 250 292 ug/L 117 57 -139 11 20
Iodomethane 50.0 38.4 ug/L 77 69 -131 12 20
Isobutyl alcohol 1250 1580 ug/L 126 63 -133 16 20
Isopropylbenzene 50.0 48.4 ug/L 97 72 -131 4 20
p-Isopropyltoluene 50.0 46.8 ug/L 94 77 -127 3 20
Methylene Chloride 50.0 53.9 ug/L 108 74 -124 7 20
4-Methyl-2-pentanone (MIBK)250 273 ug/L 109 67 -130 10 20
Methyl tert-butyl ether 50.0 52.6 ug/L 105 71 -124 11 20
Naphthalene 50.0 52.0 ug/L 104 61 -128 7 20
N-Propylbenzene 50.0 46.4 ug/L 93 76 -126 6 20
Styrene 50.0 49.3 ug/L 99 78 -123 1 20
1,1,1,2-Tetrachloroethane 50.0 46.5 ug/L 93 78 -124 2 20
1,1,2,2-Tetrachloroethane 50.0 50.0 ug/L 100 71 -121 6 20
Tetrachloroethene 50.0 50.6 ug/L 101 74 -129 2 20
Toluene 50.0 50.3 ug/L 101 80 -121 0 20
1,2,3-Trichlorobenzene 50.0 43.5 ug/L 87 69 -129 9 20
1,2,4-Trichlorobenzene 50.0 49.5 ug/L 99 69 -130 3 20
1,1,1-Trichloroethane 50.0 46.3 ug/L 93 74 -131 2 20
1,1,2-Trichloroethane 50.0 53.9 ug/L 108 80 -119 7 20
Trichloroethene 50.0 51.6 ug/L 103 79 -123 2 20
Trichlorofluoromethane 50.0 43.1 ug/L 86 65 -141 2 20
1,2,3-Trichloropropane 50.0 48.0 ug/L 96 73 -122 9 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 48.3 ug/L 97 70 -136 0 20
1,2,4-Trimethylbenzene 50.0 46.0 ug/L 92 76 -124 3 20
1,3,5-Trimethylbenzene 50.0 45.7 ug/L 91 75 -124 3 20
Vinyl acetate 100 116 ug/L 116 54 -146 13 20
Vinyl chloride 50.0 49.3 ug/L 99 58 -137 7 20
o-Xylene 50.0 47.1 ug/L 94 78 -122 2 20
m-Xylene & p-Xylene 50.0 47.7 ug/L 95 80 -121 4 20
Xylenes, Total 100 94.8 ug/L 95 79 -121 3 20
Cyclohexane 50.0 50.8 ug/L 102 71 -130 0 20
Methyl acetate 100 109 ug/L 109 56 -136 14 20
Methylcyclohexane 50.0 50.0 ug/L 100 72 -132 3 20
Tetrahydrofuran 100 108 ug/L 108 57 -133 14 20
Hexane 50.0 53.5 ug/L 107 48 -143 0 20
Diethyl ether 50.0 53.1 ug/L 106 68 -129 14 20
Heptane 50.0 54.7 ug/L 109 49 -140 3 20
1,3-Dichloropropene, Total 100 105 ug/L 105 77 -123 5 20
1,3-Butadiene 50.0 51.8 ug/L 104 43 -158 7 20
Dichlorofluoromethane 50.0 50.5 ug/L 101 19
tert-Butyl alcohol 500 551 ug/L 110 68 -129 19 20
1,4-Dioxane 1000 1400 Q ug/L 140 59 -139 19 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Toluene-d8 (Surr)89 -112
Surrogate
109
LCSD LCSD
Qualifier Limits%Recovery
1021,2-Dichloroethane-d4 (Surr)81 -118
107Dibromofluoromethane (Surr)80 -119
994-Bromofluorobenzene (Surr)85 -114
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
Acetone 10 J Q D 250 224 ug/L 85 39 -160
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acrolein 80 U 1000 973 ug/L 97 39 -155
Acrylonitrile 40 U M 500 494 ug/L 99 63 -135
Benzene 13 D 50.0 61.0 ug/L 95 79 -120
Bromobenzene 1.0 U J1 50.0 45.2 ug/L 90 80 -120
Bromochloromethane 2.0 U 50.0 49.0 ug/L 98 78 -123
Bromodichloromethane 2.0 U 50.0 47.7 ug/L 95 79 -125
Bromoform 4.0 U Q 50.0 38.1 ug/L 76 66 -130
Bromomethane 20 U J1 Q 50.0 16.6 J J1 ug/L 33 53 -141
2-Butanone (MEK)40 U 250 263 ug/L 105 56 -143
n-Butylbenzene 4.5 J D 50.0 51.6 ug/L 94 75 -128
sec-Butylbenzene 2.5 J D 50.0 47.0 ug/L 89 77 -126
tert-Butylbenzene 2.0 U 50.0 46.8 ug/L 94 78 -124
Carbon disulfide 2.0 U 50.0 50.8 ug/L 102 64 -133
Carbon tetrachloride 2.0 U 50.0 46.9 ug/L 94 72 -136
Chlorobenzene 1.0 U 50.0 47.5 ug/L 95 82 -118
Chloroethane 20 U 50.0 61.2 ug/L 122 60 -138
2-Chloroethyl vinyl ether 40 U 50.0 44.0 ug/L 88 51 -139
Chloroform 2.0 U M 50.0 49.4 ug/L 99 79 -124
Chloromethane 4.0 U 50.0 43.8 ug/L 88 50 -139
Allyl chloride 9.6 J D 50.0 59.6 ug/L 100 68 -130
2-Chlorotoluene 1.0 U J1 50.0 45.2 ug/L 90 79 -122
4-Chlorotoluene 2.0 U 50.0 44.9 ug/L 90 78 -122
Chlorodibromomethane 2.0 U 50.0 46.2 ug/L 92 74 -126
1,2-Dibromo-3-Chloropropane 10 U Q 50.0 40.6 ug/L 81 62 -128
1,2-Dibromoethane 2.0 U 50.0 48.8 ug/L 98 75 -127
Dibromomethane 2.0 U 50.0 48.1 ug/L 96 79 -123
1,2-Dichlorobenzene 2.0 U 50.0 47.4 ug/L 95 80 -119
1,3-Dichlorobenzene 2.0 U 50.0 47.8 ug/L 96 80 -119
1,4-Dichlorobenzene 2.0 U 50.0 47.1 ug/L 94 79 -118
trans-1,4-Dichloro-2-butene 10 U Q J1 M 50.0 34.1 ug/L 68 43 -140
Dichlorodifluoromethane 2.0 U 50.0 49.3 M ug/L 99 32 -152
1,1-Dichloroethane 2.0 U 50.0 50.7 ug/L 101 77 -125
1,2-Dichloroethane 2.0 U M 50.0 46.4 ug/L 93 73 -128
cis-1,2-Dichloroethene 2.0 U 50.0 49.9 ug/L 100 78 -123
trans-1,2-Dichloroethene 2.0 U 50.0 53.2 ug/L 106 75 -124
1,2-Dichloroethene, Total 2.0 U 100 103 ug/L 103 79 -121
1,1-Dichloroethene 2.0 U 50.0 50.3 ug/L 101 71 -131
1,2-Dichloropropane 1.0 U 50.0 53.0 ug/L 106 78 -122
1,3-Dichloropropane 2.0 U 50.0 51.4 ug/L 103 80 -119
2,2-Dichloropropane 2.0 U 50.0 41.2 ug/L 82 60 -139
Eurofins Savannah
Page 75 of 124 6/5/2023
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
1,1-Dichloropropene 2.0 U 50.0 50.8 ug/L 102 79 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
cis-1,3-Dichloropropene 2.0 U 50.0 46.5 ug/L 93 75 -124
trans-1,3-Dichloropropene 2.0 U 50.0 49.6 ug/L 99 73 -127
Ethylbenzene 40 J1 D 50.0 76.4 J1 ug/L 73 79 -121
Ethyl methacrylate 2.0 U 50.0 50.5 ug/L 101 72 -126
Hexachlorobutadiene 2.0 U 50.0 45.1 ug/L 90 66 -134
2-Hexanone 20 U 250 249 ug/L 100 57 -139
Iodomethane 20 U Q J1 50.0 5.17 J J1 ug/L 10 69 -131
Isobutyl alcohol 500 U M 1250 1310 ug/L 105 63 -133
Isopropylbenzene 12 J1 D 50.0 57.6 ug/L 91 72 -131
p-Isopropyltoluene 2.7 J D 50.0 50.2 ug/L 95 77 -127
Methylene Chloride 20 U 50.0 49.5 ug/L 99 74 -124
4-Methyl-2-pentanone (MIBK)20 U 250 247 ug/L 99 67 -130
Methyl tert-butyl ether 4.0 U 50.0 48.3 ug/L 97 71 -124
Naphthalene 53 J1 D 50.0 82.2 J1 ug/L 58 61 -128
N-Propylbenzene 16 J1 D 50.0 59.3 ug/L 87 76 -126
Styrene 2.0 U M 50.0 47.2 ug/L 94 78 -123
1,1,1,2-Tetrachloroethane 2.0 U 50.0 45.4 ug/L 91 78 -124
1,1,2,2-Tetrachloroethane 2.0 U J1 50.0 45.6 ug/L 91 71 -121
Tetrachloroethene 2.0 U 50.0 50.8 ug/L 102 74 -129
Toluene 1.6 J D 50.0 49.3 ug/L 95 80 -121
1,2,3-Trichlorobenzene 4.0 U 50.0 43.4 ug/L 87 69 -129
1,2,4-Trichlorobenzene 4.0 U 50.0 45.0 ug/L 90 69 -130
1,1,1-Trichloroethane 1.0 U 50.0 48.8 ug/L 98 74 -131
1,1,2-Trichloroethane 2.0 U 50.0 50.3 ug/L 101 80 -119
Trichloroethene 1.0 U 50.0 52.8 ug/L 106 79 -123
Trichlorofluoromethane 2.0 U 50.0 41.8 ug/L 84 65 -141
1,2,3-Trichloropropane 2.0 U J1 50.0 43.0 ug/L 86 73 -122
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
1.0 U 50.0 47.6 ug/L 95 70 -136
1,2,4-Trimethylbenzene 130 J1 D 50.0 134 J1 ug/L 11 76 -124
1,3,5-Trimethylbenzene 37 J1 D 50.0 71.7 J1 ug/L 69 75 -124
Vinyl acetate 4.0 U M 100 105 ug/L 105 54 -146
Vinyl chloride 2.0 U 50.0 35.7 ug/L 71 58 -137
o-Xylene 6.7 D 50.0 50.0 ug/L 87 78 -122
m-Xylene & p-Xylene 210 J1 D 50.0 196 4 ug/L -35 80 -121
Xylenes, Total 220 J1 D 100 246 J1 ug/L 29 79 -121
Cyclohexane 23 J1 D 50.0 83.7 ug/L 122 71 -130
Methyl acetate 20 U J1 100 167 J1 ug/L 167 56 -136
Methylcyclohexane 12 D 50.0 68.6 ug/L 113 72 -132
Tetrahydrofuran 10 U M 100 95.5 ug/L 96 57 -133
Hexane 13 D 50.0 71.9 ug/L 119 48 -143
Diethyl ether 2.0 U 50.0 44.2 ug/L 88 68 -129
Heptane 2.4 J D 50.0 56.6 ug/L 108 49 -140
1,3-Dichloropropene, Total 2.0 U 100 96.1 ug/L 96 77 -123
1,3-Butadiene 2.0 U 50.0 44.3 ug/L 89 43 -158
Dichlorofluoromethane 2.0 U 50.0 42.7 ug/L 85
tert-Butyl alcohol 40 U 500 442 ug/L 88 68 -129
1,4-Dioxane 400 U Q J1 1000 787 ug/L 79 59 -139
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Toluene-d8 (Surr)89 -112
Surrogate
107
MS MS
Qualifier Limits%Recovery
931,2-Dichloroethane-d4 (Surr)81 -118
102Dibromofluoromethane (Surr)80 -119
1024-Bromofluorobenzene (Surr)85 -114
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
Acetone 10 J Q D 250 248 ug/L 95 39 -160 10 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Acrolein 80 U 1000 1120 ug/L 112 39 -155 14 20
Acrylonitrile 40 U M 500 515 ug/L 103 63 -135 4 20
Benzene 13 D 50.0 67.6 ug/L 109 79 -120 10 20
Bromobenzene 1.0 U J1 50.0 34.8 J1 ug/L 70 80 -120 26 20
Bromochloromethane 2.0 U 50.0 50.3 ug/L 101 78 -123 3 20
Bromodichloromethane 2.0 U 50.0 48.6 ug/L 97 79 -125 2 20
Bromoform 4.0 U Q 50.0 35.0 ug/L 70 66 -130 9 20
Bromomethane 20 U J1 Q 50.0 24.0 J1 ug/L 48 53 -141 36 20
2-Butanone (MEK)40 U 250 275 ug/L 110 56 -143 5 20
n-Butylbenzene 4.5 J D 50.0 54.3 ug/L 100 75 -128 5 20
sec-Butylbenzene 2.5 J D 50.0 49.8 ug/L 95 77 -126 6 20
tert-Butylbenzene 2.0 U 50.0 48.8 ug/L 98 78 -124 4 20
Carbon disulfide 2.0 U 50.0 53.0 ug/L 106 64 -133 4 20
Carbon tetrachloride 2.0 U 50.0 48.2 ug/L 96 72 -136 3 20
Chlorobenzene 1.0 U 50.0 49.3 ug/L 99 82 -118 4 20
Chloroethane 20 U 50.0 66.2 ug/L 132 60 -138 8 20
2-Chloroethyl vinyl ether 40 U 50.0 48.7 ug/L 97 51 -139 10 20
Chloroform 2.0 U M 50.0 51.2 ug/L 102 79 -124 3 20
Chloromethane 4.0 U 50.0 47.0 ug/L 94 50 -139 7 20
Allyl chloride 9.6 J D 50.0 66.0 ug/L 113 68 -130 10 20
2-Chlorotoluene 1.0 U J1 50.0 36.7 J1 ug/L 73 79 -122 21 20
4-Chlorotoluene 2.0 U 50.0 40.5 ug/L 81 78 -122 10 20
Chlorodibromomethane 2.0 U 50.0 47.0 ug/L 94 74 -126 2 20
1,2-Dibromo-3-Chloropropane 10 U Q 50.0 43.6 ug/L 87 62 -128 7 20
1,2-Dibromoethane 2.0 U 50.0 49.9 ug/L 100 75 -127 2 20
Dibromomethane 2.0 U 50.0 49.2 ug/L 98 79 -123 2 20
1,2-Dichlorobenzene 2.0 U 50.0 49.1 ug/L 98 80 -119 4 20
1,3-Dichlorobenzene 2.0 U 50.0 49.7 ug/L 99 80 -119 4 20
1,4-Dichlorobenzene 2.0 U 50.0 48.9 ug/L 98 79 -118 4 20
trans-1,4-Dichloro-2-butene 10 U Q J1 M 50.0 26.8 J1 ug/L 54 43 -140 24 20
Dichlorodifluoromethane 2.0 U 50.0 52.1 M ug/L 104 32 -152 6 20
1,1-Dichloroethane 2.0 U 50.0 51.9 ug/L 104 77 -125 2 20
1,2-Dichloroethane 2.0 U M 50.0 47.9 ug/L 96 73 -128 3 20
cis-1,2-Dichloroethene 2.0 U 50.0 50.6 ug/L 101 78 -123 1 20
trans-1,2-Dichloroethene 2.0 U 50.0 53.9 ug/L 108 75 -124 1 20
1,2-Dichloroethene, Total 2.0 U 100 104 ug/L 104 79 -121 1 20
1,1-Dichloroethene 2.0 U 50.0 54.9 ug/L 110 71 -131 9 20
1,2-Dichloropropane 1.0 U 50.0 54.0 ug/L 108 78 -122 2 20
1,3-Dichloropropane 2.0 U 50.0 53.3 ug/L 107 80 -119 4 20
2,2-Dichloropropane 2.0 U 50.0 42.1 ug/L 84 60 -139 2 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777079
1,1-Dichloropropene 2.0 U 50.0 52.5 ug/L 105 79 -125 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
cis-1,3-Dichloropropene 2.0 U 50.0 48.6 ug/L 97 75 -124 4 20
trans-1,3-Dichloropropene 2.0 U 50.0 50.6 ug/L 101 73 -127 2 20
Ethylbenzene 40 J1 D 50.0 88.4 ug/L 97 79 -121 15 20
Ethyl methacrylate 2.0 U 50.0 52.3 ug/L 105 72 -126 4 20
Hexachlorobutadiene 2.0 U 50.0 47.8 ug/L 96 66 -134 6 20
2-Hexanone 20 U 250 263 ug/L 105 57 -139 5 20
Iodomethane 20 U Q J1 50.0 10.8 J J1 ug/L 22 69 -131 70 20
Isobutyl alcohol 500 U M 1250 1490 ug/L 120 63 -133 13 20
Isopropylbenzene 12 J1 D 50.0 44.0 J1 ug/L 64 72 -131 27 20
p-Isopropyltoluene 2.7 J D 50.0 52.5 ug/L 100 77 -127 4 20
Methylene Chloride 20 U 50.0 50.8 ug/L 102 74 -124 3 20
4-Methyl-2-pentanone (MIBK)20 U 250 263 ug/L 105 67 -130 7 20
Methyl tert-butyl ether 4.0 U 50.0 50.2 ug/L 100 71 -124 4 20
Naphthalene 53 J1 D 50.0 99.6 ug/L 93 61 -128 19 20
N-Propylbenzene 16 J1 D 50.0 46.2 J1 ug/L 61 76 -126 25 20
Styrene 2.0 U M 50.0 48.5 ug/L 97 78 -123 3 20
1,1,1,2-Tetrachloroethane 2.0 U 50.0 46.8 ug/L 94 78 -124 3 20
1,1,2,2-Tetrachloroethane 2.0 U J1 50.0 33.3 J1 ug/L 67 71 -121 31 20
Tetrachloroethene 2.0 U 50.0 52.0 ug/L 104 74 -129 2 20
Toluene 1.6 J D 50.0 50.7 ug/L 98 80 -121 3 20
1,2,3-Trichlorobenzene 4.0 U 50.0 47.2 ug/L 94 69 -129 8 20
1,2,4-Trichlorobenzene 4.0 U 50.0 47.9 ug/L 96 69 -130 6 20
1,1,1-Trichloroethane 1.0 U 50.0 50.2 ug/L 100 74 -131 3 20
1,1,2-Trichloroethane 2.0 U 50.0 51.4 ug/L 103 80 -119 2 20
Trichloroethene 1.0 U 50.0 53.6 ug/L 107 79 -123 2 20
Trichlorofluoromethane 2.0 U 50.0 46.8 ug/L 94 65 -141 11 20
1,2,3-Trichloropropane 2.0 U J1 50.0 32.6 J1 ug/L 65 73 -122 28 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
1.0 U 50.0 52.6 ug/L 105 70 -136 10 20
1,2,4-Trimethylbenzene 130 J1 D 50.0 170 J1 ug/L 81 76 -124 23 20
1,3,5-Trimethylbenzene 37 J1 D 50.0 68.7 J1 ug/L 63 75 -124 4 20
Vinyl acetate 4.0 U M 100 105 ug/L 105 54 -146 0 20
Vinyl chloride 2.0 U 50.0 38.2 ug/L 76 58 -137 7 20
o-Xylene 6.7 D 50.0 52.8 ug/L 92 78 -122 5 20
m-Xylene & p-Xylene 210 J1 D 50.0 248 J1 4 ug/L 69 80 -121 23 20
Xylenes, Total 220 J1 D 100 301 J1 ug/L 84 79 -121 20 20
Cyclohexane 23 J1 D 50.0 94.9 J1 ug/L 144 71 -130 12 20
Methyl acetate 20 U J1 100 198 J1 ug/L 198 56 -136 17 20
Methylcyclohexane 12 D 50.0 74.8 ug/L 126 72 -132 9 20
Tetrahydrofuran 10 U M 100 101 ug/L 101 57 -133 5 20
Hexane 13 D 50.0 78.6 ug/L 132 48 -143 9 20
Diethyl ether 2.0 U 50.0 51.0 ug/L 102 68 -129 14 20
Heptane 2.4 J D 50.0 57.1 ug/L 109 49 -140 1 20
1,3-Dichloropropene, Total 2.0 U 100 99.2 ug/L 99 77 -123 3 20
1,3-Butadiene 2.0 U 50.0 46.7 ug/L 93 43 -158 5 20
Dichlorofluoromethane 2.0 U 50.0 48.3 ug/L 97 12
tert-Butyl alcohol 40 U 500 491 ug/L 98 68 -129 10 20
1,4-Dioxane 400 U Q J1 1000 1060 J1 ug/L 106 59 -139 29 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Toluene-d8 (Surr)89 -112
Surrogate
111
MSD MSD
Qualifier Limits%Recovery
961,2-Dichloroethane-d4 (Surr)81 -118
104Dibromofluoromethane (Surr)80 -119
68 Q4-Bromofluorobenzene (Surr)85 -114
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-777298/9-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
LOQ DL
1,2,4,5-Tetrachlorobenzene 2.0 U 10 0.76 ug/L 05/05/23 21:00 05/10/23 18:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2.0 U 0.5610 ug/L 05/05/23 21:00 05/10/23 18:11 11,2,4-Trichlorobenzene
2.0 U 0.5310 ug/L 05/05/23 21:00 05/10/23 18:11 11,2-Dichlorobenzene
2.0 U 0.5910 ug/L 05/05/23 21:00 05/10/23 18:11 11,3-Dichlorobenzene
2.0 U 0.6010 ug/L 05/05/23 21:00 05/10/23 18:11 11,3-Dinitrobenzene
2.0 U 0.5410 ug/L 05/05/23 21:00 05/10/23 18:11 11,4-Dichlorobenzene
2.0 U 0.6210 ug/L 05/05/23 21:00 05/10/23 18:11 11,4-Naphthoquinone
2.0 U 1.110 ug/L 05/05/23 21:00 05/10/23 18:11 11-Naphthylamine
2.0 U 0.7210 ug/L 05/05/23 21:00 05/10/23 18:11 12,3,4,6-Tetrachlorophenol
2.0 U 1.210 ug/L 05/05/23 21:00 05/10/23 18:11 12,4,5-Trichlorophenol
2.0 U 0.8510 ug/L 05/05/23 21:00 05/10/23 18:11 12,4,6-Trichlorophenol
2.0 U 1.110 ug/L 05/05/23 21:00 05/10/23 18:11 12,4-Dichlorophenol
10 U 4.010 ug/L 05/05/23 21:00 05/10/23 18:11 12,4-Dimethylphenol
20 U 1050 ug/L 05/05/23 21:00 05/10/23 18:11 12,4-Dinitrophenol
2.0 U M 1.210 ug/L 05/05/23 21:00 05/10/23 18:11 12,4-Dinitrotoluene
2.0 U 0.7310 ug/L 05/05/23 21:00 05/10/23 18:11 12,6-Dichlorophenol
2.0 U 1.110 ug/L 05/05/23 21:00 05/10/23 18:11 12,6-Dinitrotoluene
5.0 U 1.610 ug/L 05/05/23 21:00 05/10/23 18:11 12-Acetylaminofluorene
2.0 U 0.8010 ug/L 05/05/23 21:00 05/10/23 18:11 12-Chloronaphthalene
2.0 U 0.8710 ug/L 05/05/23 21:00 05/10/23 18:11 12-Chlorophenol
2.0 U 0.7810 ug/L 05/05/23 21:00 05/10/23 18:11 12-Methylnaphthalene
2.0 U 0.8910 ug/L 05/05/23 21:00 05/10/23 18:11 12-Methylphenol
5.0 U 1.510 ug/L 05/05/23 21:00 05/10/23 18:11 12-Naphthylamine
2.0 U 1.350 ug/L 05/05/23 21:00 05/10/23 18:11 12-Nitroaniline
2.0 U 0.7610 ug/L 05/05/23 21:00 05/10/23 18:11 12-Nitrophenol
2.0 U 1.310 ug/L 05/05/23 21:00 05/10/23 18:11 13 & 4 Methylphenol
60 U 3060 ug/L 05/05/23 21:00 05/10/23 18:11 13,3'-Dichlorobenzidine
13 U 1020 ug/L 05/05/23 21:00 05/10/23 18:11 13,3'-Dimethylbenzidine
5.0 U 1.410 ug/L 05/05/23 21:00 05/10/23 18:11 13-Methylcholanthrene
10 U 5.050 ug/L 05/05/23 21:00 05/10/23 18:11 13-Nitroaniline
20 U 1050 ug/L 05/05/23 21:00 05/10/23 18:11 14,6-Dinitro-2-methylphenol
2.0 U 1.210 ug/L 05/05/23 21:00 05/10/23 18:11 14-Aminobiphenyl
2.0 U 0.7710 ug/L 05/05/23 21:00 05/10/23 18:11 14-Bromophenyl phenyl ether
2.0 U 1.010 ug/L 05/05/23 21:00 05/10/23 18:11 14-Chloro-3-methylphenol
5.0 U 2.220 ug/L 05/05/23 21:00 05/10/23 18:11 14-Chloroaniline
2.0 U 0.8410 ug/L 05/05/23 21:00 05/10/23 18:11 14-Chlorophenyl phenyl ether
10 U 5.050 ug/L 05/05/23 21:00 05/10/23 18:11 14-Nitroaniline
4.0 U 1.950 ug/L 05/05/23 21:00 05/10/23 18:11 14-Nitrophenol
20 U 1025 ug/L 05/05/23 21:00 05/10/23 18:11 14-Nitroquinoline-1-oxide
5.0 U 1.510 ug/L 05/05/23 21:00 05/10/23 18:11 15-Nitro-o-toluidine
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-777298/9-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
LOQ DL
7,12-Dimethylbenz(a)anthracene 2.0 U 10 1.2 ug/L 05/05/23 21:00 05/10/23 18:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2.0 U 0.7610 ug/L 05/05/23 21:00 05/10/23 18:11 1Acenaphthene
2.0 U 0.8510 ug/L 05/05/23 21:00 05/10/23 18:11 1Acenaphthylene
2.0 U 0.5710 ug/L 05/05/23 21:00 05/10/23 18:11 1Acetophenone
80 U 352000 ug/L 05/05/23 21:00 05/10/23 18:11 1alpha,alpha-Dimethyl phenethylamine
2.0 U 0.6910 ug/L 05/05/23 21:00 05/10/23 18:11 1Anthracene
2.0 U 0.5510 ug/L 05/05/23 21:00 05/10/23 18:11 1Benzo[a]anthracene
2.0 U 0.7110 ug/L 05/05/23 21:00 05/10/23 18:11 1Benzo[a]pyrene
5.0 U 2.610 ug/L 05/05/23 21:00 05/10/23 18:11 1Benzo[b]fluoranthene
2.0 U 0.8710 ug/L 05/05/23 21:00 05/10/23 18:11 1Benzo[g,h,i]perylene
2.0 U 1.210 ug/L 05/05/23 21:00 05/10/23 18:11 1Benzo[k]fluoranthene
2.0 U M 1.110 ug/L 05/05/23 21:00 05/10/23 18:11 1Benzyl alcohol
2.0 U 0.7810 ug/L 05/05/23 21:00 05/10/23 18:11 1bis (2-chloroisopropyl) ether
2.0 U 0.9410 ug/L 05/05/23 21:00 05/10/23 18:11 1Bis(2-chloroethoxy)methane
2.0 U 1.110 ug/L 05/05/23 21:00 05/10/23 18:11 1Bis(2-chloroethyl)ether
2.5 U 1.610 ug/L 05/05/23 21:00 05/10/23 18:11 1Bis(2-ethylhexyl) phthalate
2.0 U 1.210 ug/L 05/05/23 21:00 05/10/23 18:11 1Butyl benzyl phthalate
2.0 U 0.5110 ug/L 05/05/23 21:00 05/10/23 18:11 1Chrysene
2.0 U 0.7810 ug/L 05/05/23 21:00 05/10/23 18:11 1Diallate
2.0 U 1.010 ug/L 05/05/23 21:00 05/10/23 18:11 1Dibenz(a,h)anthracene
2.0 U 0.7910 ug/L 05/05/23 21:00 05/10/23 18:11 1Dibenzofuran
2.0 U 0.8810 ug/L 05/05/23 21:00 05/10/23 18:11 1Diethyl phthalate
2.0 U 0.7510 ug/L 05/05/23 21:00 05/10/23 18:11 1Dimethoate
2.0 U 0.9910 ug/L 05/05/23 21:00 05/10/23 18:11 1Dimethyl phthalate
2.0 U 0.8310 ug/L 05/05/23 21:00 05/10/23 18:11 1Di-n-butyl phthalate
2.5 U 1.410 ug/L 05/05/23 21:00 05/10/23 18:11 1Di-n-octyl phthalate
10 U 5.010 ug/L 05/05/23 21:00 05/10/23 18:11 1Dinoseb
2.0 U 0.9210 ug/L 05/05/23 21:00 05/10/23 18:11 1Diphenylamine
2.0 U 0.7910 ug/L 05/05/23 21:00 05/10/23 18:11 1Disulfoton
2.0 U 0.9610 ug/L 05/05/23 21:00 05/10/23 18:11 1Ethyl methanesulfonate
2.0 U 1.310 ug/L 05/05/23 21:00 05/10/23 18:11 1Ethyl Parathion
2.0 U 1.110 ug/L 05/05/23 21:00 05/10/23 18:11 1Famphur
2.0 U 0.7410 ug/L 05/05/23 21:00 05/10/23 18:11 1Fluoranthene
2.0 U 0.9610 ug/L 05/05/23 21:00 05/10/23 18:11 1Fluorene
2.0 U 0.7910 ug/L 05/05/23 21:00 05/10/23 18:11 1Hexachlorobenzene
2.0 U 0.6210 ug/L 05/05/23 21:00 05/10/23 18:11 1Hexachlorobutadiene
5.0 U 2.510 ug/L 05/05/23 21:00 05/10/23 18:11 1Hexachlorocyclopentadiene
2.0 U 0.7610 ug/L 05/05/23 21:00 05/10/23 18:11 1Hexachloroethane
5.0 U 1.410 ug/L 05/05/23 21:00 05/10/23 18:11 1Hexachloropropene
2.0 U 1.010 ug/L 05/05/23 21:00 05/10/23 18:11 1Indeno[1,2,3-cd]pyrene
2.0 U M 0.9010 ug/L 05/05/23 21:00 05/10/23 18:11 1Isophorone
2.0 U 0.5010 ug/L 05/05/23 21:00 05/10/23 18:11 1Isosafrole
5.0 U 2.72000 ug/L 05/05/23 21:00 05/10/23 18:11 1Methapyrilene
2.0 U M 0.6010 ug/L 05/05/23 21:00 05/10/23 18:11 1Methyl methanesulfonate
2.0 U 0.8810 ug/L 05/05/23 21:00 05/10/23 18:11 1Methyl parathion
2.0 U 0.7010 ug/L 05/05/23 21:00 05/10/23 18:11 1Naphthalene
2.0 U 0.7310 ug/L 05/05/23 21:00 05/10/23 18:11 1Nitrobenzene
2.0 U 0.9310 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosodiethylamine
5.0 U 2.810 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosodimethylamine
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-777298/9-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
LOQ DL
N-Nitrosodi-n-butylamine 2.0 U 10 0.96 ug/L 05/05/23 21:00 05/10/23 18:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2.0 U 0.7210 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosodi-n-propylamine
2.0 U 0.9210 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosodiphenylamine
10 U 3.310 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosomethylethylamine
2.0 U 0.8810 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosopiperidine
2.0 U 1.010 ug/L 05/05/23 21:00 05/10/23 18:11 1N-Nitrosopyrrolidine
2.0 U 1.010 ug/L 05/05/23 21:00 05/10/23 18:11 1o,o',o''-Triethylphosphorothioate
5.0 U 1.410 ug/L 05/05/23 21:00 05/10/23 18:11 1o-Toluidine
2.0 U M 0.7910 ug/L 05/05/23 21:00 05/10/23 18:11 1p-Dimethylamino azobenzene
2.0 U 0.5210 ug/L 05/05/23 21:00 05/10/23 18:11 1Pentachlorobenzene
2.0 U 0.7810 ug/L 05/05/23 21:00 05/10/23 18:11 1Pentachloronitrobenzene
4.0 U 2.050 ug/L 05/05/23 21:00 05/10/23 18:11 1Pentachlorophenol
5.0 U 1.410 ug/L 05/05/23 21:00 05/10/23 18:11 1Phenacetin
2.0 U 0.7710 ug/L 05/05/23 21:00 05/10/23 18:11 1Phenanthrene
2.0 U 0.8310 ug/L 05/05/23 21:00 05/10/23 18:11 1Phenol
2.0 U 0.8710 ug/L 05/05/23 21:00 05/10/23 18:11 1Phorate
25 U 102000 ug/L 05/05/23 21:00 05/10/23 18:11 1p-Phenylene diamine
2.0 U 0.8910 ug/L 05/05/23 21:00 05/10/23 18:11 1Pronamide
2.0 U 0.6310 ug/L 05/05/23 21:00 05/10/23 18:11 1Pyrene
2.0 U 0.8010 ug/L 05/05/23 21:00 05/10/23 18:11 1Safrole, Total
5.0 U 2.010 ug/L 05/05/23 21:00 05/10/23 18:11 1sym-Trinitrobenzene
2.0 U 0.9110 ug/L 05/05/23 21:00 05/10/23 18:11 1Thionazin
2,4,6-Tribromophenol (Surr)65 43-140 05/10/23 18:11 1
MB MB
Surrogate
05/05/23 21:00
Dil FacPrepared AnalyzedQualifier Limits%Recovery
68 05/05/23 21:00 05/10/23 18:11 12-Fluorobiphenyl (Surr)44-119
51 05/05/23 21:00 05/10/23 18:11 12-Fluorophenol (Surr)19-119
66 05/05/23 21:00 05/10/23 18:11 1Nitrobenzene-d5 (Surr)44-120
52 05/05/23 21:00 05/10/23 18:11 1Phenol-d5 (Surr)27-110
81 05/05/23 21:00 05/10/23 18:11 1Terphenyl-d14 (Surr)50-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777298/10-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
1,2,4,5-Tetrachlorobenzene 100 89.2 ug/L 89 35 -121
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trichlorobenzene 100 73.3 ug/L 73 29 -116
1,2-Dichlorobenzene 100 60.7 ug/L 61 32 -111
1,3-Dichlorobenzene 100 58.2 ug/L 58 28 -110
1,3-Dinitrobenzene 100 95.8 ug/L 96 49 -128
1,4-Dichlorobenzene 100 60.9 ug/L 61 29 -112
2,3,4,6-Tetrachlorophenol 100 104 ug/L 104 50 -128
2,4,5-Trichlorophenol 100 97.5 ug/L 98 53 -123
2,4,6-Trichlorophenol 100 94.5 ug/L 94 50 -125
2,4-Dichlorophenol 100 82.9 ug/L 83 47 -121
2,4-Dimethylphenol 100 66.9 ug/L 67 31 -124
2,4-Dinitrophenol 200 211 ug/L 105 23 -143
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777298/10-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
2,4-Dinitrotoluene 100 97.2 ug/L 97 57 -128
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
2,6-Dichlorophenol 100 83.0 ug/L 83 50 -118
2,6-Dinitrotoluene 100 91.7 ug/L 92 57 -124
2-Chloronaphthalene 100 81.3 ug/L 81 40 -116
2-Chlorophenol 100 69.0 ug/L 69 38 -117
2-Methylnaphthalene 100 87.5 ug/L 88 40 -121
2-Methylphenol 100 68.9 ug/L 69 30 -117
2-Nitroaniline 100 94.2 ug/L 94 55 -127
2-Nitrophenol 100 77.5 ug/L 78 47 -123
3 & 4 Methylphenol 100 71.8 ug/L 72 29 -110
3,3'-Dichlorobenzidine 100 70.7 ug/L 71 27 -129
3-Nitroaniline 100 87.5 ug/L 87 41 -128
4,6-Dinitro-2-methylphenol 200 212 ug/L 106 44 -137
4-Bromophenyl phenyl ether 100 95.5 ug/L 95 55 -124
4-Chloro-3-methylphenol 100 88.6 ug/L 89 52 -119
4-Chloroaniline 100 78.4 ug/L 78 33 -117
4-Chlorophenyl phenyl ether 100 94.0 ug/L 94 53 -121
4-Nitroaniline 100 93.9 ug/L 94 44 -119
4-Nitrophenol 200 202 ug/L 101 41 -118
Acenaphthene 100 87.3 ug/L 87 47 -122
Acenaphthylene 100 92.4 ug/L 92 41 -130
Acetophenone 100 80.6 ug/L 81 46 -118
Anthracene 100 91.0 ug/L 91 57 -123
Benzo[a]anthracene 100 105 ug/L 105 58 -125
Benzo[a]pyrene 100 106 ug/L 106 54 -128
Benzo[b]fluoranthene 100 98.1 ug/L 98 53 -131
Benzo[g,h,i]perylene 100 95.7 ug/L 96 50 -134
Benzo[k]fluoranthene 100 98.5 ug/L 98 57 -129
Benzyl alcohol 100 76.8 ug/L 77 31 -112
bis (2-chloroisopropyl) ether 100 75.9 ug/L 76 37 -130
Bis(2-chloroethoxy)methane 100 79.8 ug/L 80 48 -120
Bis(2-chloroethyl)ether 100 57.8 ug/L 58 43 -118
Bis(2-ethylhexyl) phthalate 100 97.3 ug/L 97 55 -135
Butyl benzyl phthalate 100 98.7 ug/L 99 53 -134
Chrysene 100 100 ug/L 100 59 -123
Dibenz(a,h)anthracene 100 96.9 ug/L 97 51 -134
Dibenzofuran 100 86.9 ug/L 87 53 -118
Diethyl phthalate 100 97.5 ug/L 97 56 -125
Dimethyl phthalate 100 92.8 ug/L 93 45 -127
Di-n-butyl phthalate 100 95.6 ug/L 96 59 -127
Di-n-octyl phthalate 100 100 ug/L 100 51 -140
Diphenylamine 85.5 77.6 ug/L 91 51 -123
Fluoranthene 100 102 ug/L 102 57 -128
Fluorene 100 88.8 ug/L 89 52 -124
Hexachlorobenzene 100 89.6 ug/L 90 53 -125
Hexachlorobutadiene 100 69.6 ug/L 70 22 -124
Hexachlorocyclopentadiene 100 49.1 ug/L 49 10 -130
Hexachloroethane 100 56.1 ug/L 56 21 -115
Indeno[1,2,3-cd]pyrene 100 101 ug/L 101 52 -134
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777298/10-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
Isophorone 100 85.8 ug/L 86 42 -124
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Naphthalene 100 73.2 ug/L 73 40 -121
Nitrobenzene 100 81.8 ug/L 82 45 -121
N-Nitrosodimethylamine 100 78.6 ug/L 79 41 -82
N-Nitrosodi-n-propylamine 100 77.8 ug/L 78 49 -119
N-Nitrosodiphenylamine 100 90.7 ug/L 91 51 -123
Pentachlorophenol 200 204 ug/L 102 35 -138
Phenanthrene 100 91.9 ug/L 92 59 -120
Phenol 100 65.3 ug/L 65 35 -101
Pyrene 100 99.2 ug/L 99 57 -126
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
73
LCS LCS
Qualifier Limits%Recovery
722-Fluorobiphenyl (Surr)44 -119
482-Fluorophenol (Surr)19 -119
67Nitrobenzene-d5 (Surr)44 -120
49Phenol-d5 (Surr)27 -110
77Terphenyl-d14 (Surr)50 -134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777298/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
1,4-Naphthoquinone 100 76.6 ug/L 77 10 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1-Naphthylamine 100 82.8 ug/L 83 24 -124
2-Acetylaminofluorene 100 88.3 ug/L 88 60 -138
2-Naphthylamine 100 66.2 ug/L 66 10 -130
3,3'-Dimethylbenzidine 100 48.2 ug/L 48 10 -130
4-Aminobiphenyl 100 64.0 ug/L 64 10 -130
4-Nitroquinoline-1-oxide 100 99.0 ug/L 99 10 -130
5-Nitro-o-toluidine 100 88.3 ug/L 88 38 -126
7,12-Dimethylbenz(a)anthracene 100 75.0 ug/L 75 61 -133
alpha,alpha-Dimethyl
phenethylamine
100 80 U ug/L 24 10 -188
Diallate 100 64.9 Q ug/L 65 67 -124
Dimethoate 100 70.2 ug/L 70 27 -86
Dinoseb 100 84.2 ug/L 84 61 -126
Disulfoton 100 66.5 ug/L 66 55 -130
Ethyl methanesulfonate 100 47.5 Q ug/L 47 62 -118
Ethyl Parathion 100 68.3 ug/L 68 66 -140
Famphur 100 63.1 ug/L 63 10 -130
Hexachloropropene 100 54.0 Q ug/L 54 12 -51
Isosafrole 100 74.4 ug/L 74 56 -126
Methyl methanesulfonate 100 46.7 ug/L 47 33 -107
Methyl parathion 100 73.9 ug/L 74 45 -159
N-Nitrosodiethylamine 100 61.0 ug/L 61 43 -121
N-Nitrosodi-n-butylamine 100 73.8 ug/L 74 60 -121
N-Nitrosomethylethylamine 100 62.0 ug/L 62 41 -117
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777298/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
N-Nitrosopiperidine 100 76.9 ug/L 77 56 -121
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
N-Nitrosopyrrolidine 100 76.2 ug/L 76 48 -113
o,o',o''-Triethylphosphorothioate 100 82.7 ug/L 83 66 -119
o-Toluidine 100 65.1 ug/L 65 30 -110
p-Dimethylamino azobenzene 100 66.6 ug/L 67 62 -132
Pentachlorobenzene 100 71.9 ug/L 72 59 -123
Pentachloronitrobenzene 100 83.7 ug/L 84 54 -135
Phenacetin 100 79.4 ug/L 79 71 -124
Phorate 100 123 ug/L 123 38 -139
p-Phenylene diamine 100 22.6 J ug/L 23 10 -130
Pronamide 100 84.7 ug/L 85 65 -129
Safrole, Total 100 98.3 ug/L 98 61 -119
sym-Trinitrobenzene 100 123 ug/L 123 41 -137
Thionazin 100 66.5 Q ug/L 67 72 -132
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
78
LCS LCS
Qualifier Limits%Recovery
732-Fluorobiphenyl (Surr)44 -119
562-Fluorophenol (Surr)19 -119
73Nitrobenzene-d5 (Surr)44 -120
64Phenol-d5 (Surr)27 -110
79Terphenyl-d14 (Surr)50 -134
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
1,2,4,5-Tetrachlorobenzene 1.9 U 96.5 52.9 ug/L 55 35 -121
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,2,4-Trichlorobenzene 1.9 U 96.5 48.1 ug/L 50 29 -116
1,2-Dichlorobenzene 1.9 U 96.5 43.8 ug/L 45 32 -111
1,3-Dichlorobenzene 1.9 U 96.5 41.2 ug/L 43 28 -110
1,3-Dinitrobenzene 1.9 U 96.5 80.8 ug/L 84 49 -128
1,4-Dichlorobenzene 1.9 U 96.5 41.6 ug/L 43 29 -112
2,3,4,6-Tetrachlorophenol 1.9 U Q 96.5 85.8 ug/L 89 50 -128
2,4,5-Trichlorophenol 1.9 U Q 96.5 74.5 ug/L 77 53 -123
2,4,6-Trichlorophenol 1.9 U 96.5 67.3 ug/L 70 50 -125
2,4-Dichlorophenol 1.9 U 96.5 60.0 ug/L 62 47 -121
2,4-Dimethylphenol 9.7 U J1 96.5 36.7 ug/L 38 31 -124
2,4-Dinitrophenol 19 U Q 193 189 ug/L 98 23 -143
2,4-Dinitrotoluene 1.9 U M 96.5 81.1 ug/L 84 57 -128
2,6-Dichlorophenol 1.9 U 96.5 59.1 ug/L 61 50 -118
2,6-Dinitrotoluene 1.9 U 96.5 73.3 ug/L 76 57 -124
2-Chloronaphthalene 1.9 U 96.5 53.5 ug/L 55 40 -116
2-Chlorophenol 1.9 U 96.5 49.8 ug/L 52 38 -117
2-Methylnaphthalene 11 96.5 64.6 ug/L 56 40 -121
2-Methylphenol 1.9 U J1 96.5 34.3 ug/L 36 30 -117
2-Nitroaniline 1.9 U 96.5 77.5 ug/L 80 55 -127
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
2-Nitrophenol 1.9 U 96.5 54.2 ug/L 56 47 -123
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
3 & 4 Methylphenol 1.9 U J1 96.5 32.9 ug/L 34 29 -110
3,3'-Dichlorobenzidine 58 U J1 96.5 58 U M J1 ug/L 0 27 -129
3-Nitroaniline 9.7 U J1 96.5 9.6 U J1 ug/L 0 41 -128
4,6-Dinitro-2-methylphenol 19 U Q 193 205 ug/L 106 44 -137
4-Bromophenyl phenyl ether 1.9 U M 96.5 63.9 ug/L 66 55 -124
4-Chloro-3-methylphenol 1.9 U J1 96.5 56.7 ug/L 59 52 -119
4-Chloroaniline 4.8 U M J1 96.5 4.72 J J1 ug/L 5 33 -117
4-Chlorophenyl phenyl ether 1.9 U 96.5 60.1 ug/L 62 53 -121
4-Nitroaniline 9.7 U J1 96.5 9.23 J J1 ug/L 10 44 -119
4-Nitrophenol 3.9 U Q 193 192 ug/L 99 41 -118
Acenaphthene 1.9 U Q J1 96.5 19.7 Q J1 ug/L 20 47 -122
Acenaphthylene 1.9 U Q J1 96.5 3.01 J Q J1 ug/L 3 41 -130
Acetophenone 1.9 U M 96.5 63.1 ug/L 65 46 -118
Anthracene 1.9 U Q J1 96.5 39.0 Q J1 ug/L 40 57 -123
Benzo[a]anthracene 1.9 U Q J1 96.5 54.4 Q J1 ug/L 56 58 -125
Benzo[a]pyrene 1.9 U Q J1 96.5 25.6 Q J1 ug/L 27 54 -128
Benzo[b]fluoranthene 4.8 U Q 96.5 73.5 Q ug/L 76 53 -131
Benzo[g,h,i]perylene 1.9 U Q J1 96.5 26.5 Q J1 ug/L 28 50 -134
Benzo[k]fluoranthene 1.9 U Q J1 96.5 42.4 M Q J1 ug/L 44 57 -129
Benzyl alcohol 1.9 U M J1 96.5 5.95 J J1 ug/L 6 31 -112
bis (2-chloroisopropyl) ether 1.9 U 96.5 53.5 ug/L 55 37 -130
Bis(2-chloroethoxy)methane 1.9 U J1 96.5 2.79 J J1 ug/L 3 48 -120
Bis(2-chloroethyl)ether 1.9 U M J1 96.5 40.1 J1 ug/L 42 43 -118
Bis(2-ethylhexyl) phthalate 2.4 U J1 96.5 44.2 J1 ug/L 46 55 -135
Butyl benzyl phthalate 1.9 U J1 96.5 6.49 J J1 ug/L 7 53 -134
Chrysene 1.9 U Q 96.5 60.9 Q ug/L 63 59 -123
Dibenz(a,h)anthracene 1.9 U 96.5 72.8 ug/L 75 51 -134
Dibenzofuran 1.9 U 96.5 56.9 ug/L 59 53 -118
Diethyl phthalate 1.9 U J1 96.5 31.8 J1 ug/L 33 56 -125
Dimethyl phthalate 1.9 U J1 96.5 36.6 J1 ug/L 38 45 -127
Di-n-butyl phthalate 1.9 U J1 96.5 33.4 J1 ug/L 35 59 -127
Di-n-octyl phthalate 2.4 U J1 96.5 38.1 J1 ug/L 39 51 -140
Diphenylamine 1.9 U 82.5 56.8 ug/L 69 21 -153
Fluoranthene 1.9 U Q J1 96.5 56.7 Q ug/L 59 57 -128
Fluorene 1.9 U Q J1 96.5 53.6 Q ug/L 56 52 -124
Hexachlorobenzene 1.9 U 96.5 61.2 ug/L 63 53 -125
Hexachlorobutadiene 1.9 U Q 96.5 44.7 ug/L 46 22 -124
Hexachlorocyclopentadiene 4.8 U 96.5 32.8 ug/L 34 10 -130
Hexachloroethane 1.9 U 96.5 47.7 ug/L 49 21 -115
Indeno[1,2,3-cd]pyrene 1.9 U Q J1 96.5 26.4 Q J1 ug/L 27 52 -134
Isophorone 1.9 U 96.5 63.5 ug/L 66 42 -124
Naphthalene 24 Q 96.5 70.6 Q ug/L 48 40 -121
Nitrobenzene 1.9 U 96.5 57.5 ug/L 60 45 -121
N-Nitrosodimethylamine 4.8 U Q 96.5 62.7 ug/L 65 41 -82
N-Nitrosodi-n-propylamine 1.9 U M 96.5 66.6 ug/L 69 49 -119
N-Nitrosodiphenylamine 1.9 U 96.5 66.4 ug/L 69 51 -123
Pentachlorophenol 3.9 U 193 204 ug/L 106 35 -138
Phenanthrene 1.9 U Q 96.5 67.6 Q ug/L 70 59 -120
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
Phenol 1.9 U Q J1 96.5 37.6 Q ug/L 39 35 -101
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Pyrene 1.9 U Q J1 96.5 17.7 Q J1 ug/L 18 57 -126
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
64
MS MS
Qualifier Limits%Recovery
502-Fluorobiphenyl (Surr)44 -119
322-Fluorophenol (Surr)19 -119
48Nitrobenzene-d5 (Surr)44 -120
3 QPhenol-d5 (Surr)27 -110
42 QTerphenyl-d14 (Surr)50 -134
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
1,4-Naphthoquinone 1.9 U Q 96.1 71.4 Q ug/L 74 10 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1-Naphthylamine 1.9 U J1 96.1 19.5 Q J1 ug/L 20 24 -124
2-Acetylaminofluorene 4.8 U Q 96.1 84.3 M Q ug/L 88 60 -138
2-Naphthylamine 4.8 U J1 96.1 55.4 Q ug/L 58 10 -130
3,3'-Dimethylbenzidine 13 U Q J1 96.1 36.3 Q ug/L 38 10 -130
4-Aminobiphenyl 1.9 U J1 96.1 66.7 ug/L 69 10 -130
4-Nitroquinoline-1-oxide 19 U J1 96.1 89.4 ug/L 93 10 -130
5-Nitro-o-toluidine 4.8 U 96.1 77.5 Q ug/L 81 38 -126
7,12-Dimethylbenz(a)anthracene 1.9 U Q J1 96.1 48.9 Q J1 ug/L 51 61 -133
alpha,alpha-Dimethyl
phenethylamine
77 U J1 96.1 70.5 J Q ug/L 73 10 -188
Diallate 1.9 U Q J1 96.1 33.8 J1 ug/L 35 67 -124
Dimethoate 1.9 U Q 96.1 67.3 ug/L 70 27 -86
Dinoseb 9.7 U Q 96.1 71.5 ug/L 74 61 -126
Disulfoton 1.9 U J1 Q 96.1 41.4 J1 ug/L 43 55 -130
Ethyl methanesulfonate 1.9 U Q J1 96.1 27.5 J1 ug/L 29 62 -118
Ethyl Parathion 1.9 U M J1 Q 96.1 51.2 J1 ug/L 53 66 -140
Famphur 1.9 U Q J1 96.1 56.6 Q ug/L 59 10 -130
Hexachloropropene 4.8 U Q 96.1 17.5 Q ug/L 18 12 -51
Isosafrole 1.9 U J1 Q 96.1 35.2 Q J1 ug/L 37 56 -126
Methyl methanesulfonate 1.9 U M J1 Q 96.1 26.8 J1 ug/L 28 33 -107
Methyl parathion 1.9 U 96.1 59.7 ug/L 62 45 -159
N-Nitrosodiethylamine 1.9 U J1 96.1 36.7 J1 ug/L 38 43 -121
N-Nitrosodi-n-butylamine 1.9 U M J1 96.1 39.7 Q J1 ug/L 41 60 -121
N-Nitrosomethylethylamine 9.7 U J1 96.1 37.9 J1 ug/L 39 41 -117
N-Nitrosopiperidine 1.9 U J1 96.1 44.2 Q J1 ug/L 46 56 -121
N-Nitrosopyrrolidine 1.9 U J1 96.1 42.7 J1 ug/L 44 48 -113
o,o',o''-Triethylphosphorothioate 1.9 U M J1 96.1 47.9 Q J1 ug/L 50 66 -119
o-Toluidine 4.8 U J1 96.1 41.5 ug/L 43 30 -110
p-Dimethylamino azobenzene 1.9 U M J1 96.1 47.7 J1 ug/L 50 62 -132
Pentachlorobenzene 1.9 U J1 Q 96.1 27.9 Q J1 ug/L 29 59 -123
Pentachloronitrobenzene 1.9 U J1 96.1 44.4 J1 ug/L 46 54 -135
Phenacetin 4.8 U 96.1 80.6 ug/L 84 71 -124
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
Phorate 1.9 U 96.1 86.9 ug/L 90 38 -139
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
p-Phenylene diamine 24 U Q J1 96.1 24 U M Q J1 ug/L 0 10 -130
Pronamide 1.9 U 96.1 78.7 ug/L 82 65 -129
Safrole, Total 1.9 U J1 Q 96.1 49.5 Q J1 ug/L 52 61 -119
sym-Trinitrobenzene 4.8 U Q 96.1 113 ug/L 117 41 -137
Thionazin 1.9 U Q J1 96.1 46.9 Q J1 ug/L 49 72 -132
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
57
MS MS
Qualifier Limits%Recovery
43 Q2-Fluorobiphenyl (Surr)44 -119
332-Fluorophenol (Surr)19 -119
42 QNitrobenzene-d5 (Surr)44 -120
37Phenol-d5 (Surr)27 -110
42 QTerphenyl-d14 (Surr)50 -134
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
1,2,4,5-Tetrachlorobenzene 1.9 U 94.8 58.3 ug/L 62 35 -121 10 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,2,4-Trichlorobenzene 1.9 U 94.8 53.2 ug/L 56 29 -116 10 20
1,2-Dichlorobenzene 1.9 U 94.8 45.4 ug/L 48 32 -111 3 20
1,3-Dichlorobenzene 1.9 U 94.8 42.1 ug/L 44 28 -110 2 20
1,3-Dinitrobenzene 1.9 U 94.8 85.7 ug/L 90 49 -128 6 20
1,4-Dichlorobenzene 1.9 U 94.8 44.4 ug/L 47 29 -112 7 20
2,3,4,6-Tetrachlorophenol 1.9 U Q 94.8 92.0 ug/L 97 50 -128 7 20
2,4,5-Trichlorophenol 1.9 U Q 94.8 78.6 ug/L 83 53 -123 5 20
2,4,6-Trichlorophenol 1.9 U 94.8 72.4 ug/L 76 50 -125 7 20
2,4-Dichlorophenol 1.9 U 94.8 65.1 ug/L 69 47 -121 8 20
2,4-Dimethylphenol 9.7 U J1 94.8 50.6 J1 ug/L 53 31 -124 32 20
2,4-Dinitrophenol 19 U Q 190 202 ug/L 107 23 -143 7 20
2,4-Dinitrotoluene 1.9 U M 94.8 85.1 ug/L 90 57 -128 5 20
2,6-Dichlorophenol 1.9 U 94.8 64.3 ug/L 68 50 -118 8 20
2,6-Dinitrotoluene 1.9 U 94.8 78.6 ug/L 83 57 -124 7 20
2-Chloronaphthalene 1.9 U 94.8 57.3 ug/L 60 40 -116 7 20
2-Chlorophenol 1.9 U 94.8 53.0 ug/L 56 38 -117 6 20
2-Methylnaphthalene 11 94.8 67.8 ug/L 60 40 -121 5 20
2-Methylphenol 1.9 U J1 94.8 48.3 J1 ug/L 51 30 -117 34 20
2-Nitroaniline 1.9 U 94.8 63.4 ug/L 67 55 -127 20 20
2-Nitrophenol 1.9 U 94.8 59.6 ug/L 63 47 -123 10 20
3 & 4 Methylphenol 1.9 U J1 94.8 50.0 J1 ug/L 53 29 -110 41 20
3,3'-Dichlorobenzidine 58 U J1 94.8 57 U M J1 ug/L 0 27 -129 NC 20
3-Nitroaniline 9.7 U J1 94.8 9.5 U J1 ug/L 0 41 -128 NC 20
4,6-Dinitro-2-methylphenol 19 U Q 190 207 ug/L 109 44 -137 1 20
4-Bromophenyl phenyl ether 1.9 U M 94.8 70.6 ug/L 74 55 -124 10 20
4-Chloro-3-methylphenol 1.9 U J1 94.8 71.6 J1 ug/L 75 52 -119 23 20
4-Chloroaniline 4.8 U M J1 94.8 3.83 J J1 ug/L 4 33 -117 21 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
4-Chlorophenyl phenyl ether 1.9 U 94.8 69.0 ug/L 73 53 -121 14 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
4-Nitroaniline 9.7 U J1 94.8 4.83 J J1 ug/L 5 44 -119 63 20
4-Nitrophenol 3.9 U Q 190 200 ug/L 105 41 -118 4 20
Acenaphthene 1.9 U Q J1 94.8 52.7 J1 ug/L 56 47 -122 91 20
Acenaphthylene 1.9 U Q J1 94.8 15.6 J1 ug/L 16 41 -130 135 20
Acetophenone 1.9 U M 94.8 70.2 ug/L 74 46 -118 11 20
Anthracene 1.9 U Q J1 94.8 68.4 J1 ug/L 72 57 -123 55 20
Benzo[a]anthracene 1.9 U Q J1 94.8 78.5 J1 ug/L 83 58 -125 36 20
Benzo[a]pyrene 1.9 U Q J1 94.8 60.3 J1 ug/L 64 54 -128 81 20
Benzo[b]fluoranthene 4.8 U Q 94.8 83.9 ug/L 88 53 -131 13 20
Benzo[g,h,i]perylene 1.9 U Q J1 94.8 67.5 J1 ug/L 71 50 -134 87 20
Benzo[k]fluoranthene 1.9 U Q J1 94.8 84.3 M J1 ug/L 89 57 -129 66 20
Benzyl alcohol 1.9 U M J1 94.8 15.5 J1 ug/L 16 31 -112 89 20
bis (2-chloroisopropyl) ether 1.9 U 94.8 55.6 ug/L 59 37 -130 4 20
Bis(2-chloroethoxy)methane 1.9 U J1 94.8 4.71 J J1 ug/L 5 48 -120 51 20
Bis(2-chloroethyl)ether 1.9 U M J1 94.8 44.2 ug/L 47 43 -118 10 20
Bis(2-ethylhexyl) phthalate 2.4 U J1 94.8 70.5 J1 ug/L 74 55 -135 46 20
Butyl benzyl phthalate 1.9 U J1 94.8 29.2 J1 ug/L 31 53 -134 127 20
Chrysene 1.9 U Q 94.8 74.5 ug/L 79 59 -123 20 20
Dibenz(a,h)anthracene 1.9 U 94.8 82.8 ug/L 87 51 -134 13 20
Dibenzofuran 1.9 U 94.8 63.0 ug/L 66 53 -118 10 20
Diethyl phthalate 1.9 U J1 94.8 72.0 J1 ug/L 76 56 -125 77 20
Dimethyl phthalate 1.9 U J1 94.8 66.9 J1 ug/L 71 45 -127 59 20
Di-n-butyl phthalate 1.9 U J1 94.8 73.7 J1 ug/L 78 59 -127 75 20
Di-n-octyl phthalate 2.4 U J1 94.8 69.8 J1 ug/L 74 51 -140 59 20
Diphenylamine 1.9 U 81.1 52.1 ug/L 64 21 -153 9 20
Fluoranthene 1.9 U Q J1 94.8 80.5 J1 ug/L 85 57 -128 35 20
Fluorene 1.9 U Q J1 94.8 67.1 J1 ug/L 71 52 -124 22 20
Hexachlorobenzene 1.9 U 94.8 69.2 ug/L 73 53 -125 12 20
Hexachlorobutadiene 1.9 U Q 94.8 49.2 ug/L 52 22 -124 10 20
Hexachlorocyclopentadiene 4.8 U 94.8 37.5 ug/L 40 10 -130 13 20
Hexachloroethane 1.9 U 94.8 45.7 ug/L 48 21 -115 4 20
Indeno[1,2,3-cd]pyrene 1.9 U Q J1 94.8 62.2 J1 ug/L 66 52 -134 81 20
Isophorone 1.9 U 94.8 70.4 ug/L 74 42 -124 10 20
Naphthalene 24 Q 94.8 74.4 ug/L 53 40 -121 5 20
Nitrobenzene 1.9 U 94.8 62.8 ug/L 66 45 -121 9 20
N-Nitrosodimethylamine 4.8 U Q 94.8 61.9 ug/L 65 41 -82 1 20
N-Nitrosodi-n-propylamine 1.9 U M 94.8 67.8 ug/L 72 49 -119 2 20
N-Nitrosodiphenylamine 1.9 U 94.8 60.9 ug/L 64 51 -123 9 20
Pentachlorophenol 3.9 U 190 199 ug/L 105 35 -138 2 20
Phenanthrene 1.9 U Q 94.8 75.6 ug/L 80 59 -120 11 20
Phenol 1.9 U Q J1 94.8 51.0 Q J1 ug/L 54 35 -101 30 20
Pyrene 1.9 U Q J1 94.8 60.8 J1 ug/L 64 57 -126 110 20
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
70
MSD MSD
Qualifier Limits%Recovery
532-Fluorobiphenyl (Surr)44 -119
392-Fluorophenol (Surr)19 -119
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
Nitrobenzene-d5 (Surr)44 -120
Surrogate
52
MSD MSD
Qualifier Limits%Recovery
15 QPhenol-d5 (Surr)27 -110
54Terphenyl-d14 (Surr)50 -134
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
1,4-Naphthoquinone 1.9 U Q 96.8 58.5 Q ug/L 60 10 -130 20 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1-Naphthylamine 1.9 U J1 96.8 7.07 J Q J1 ug/L 7 24 -124 93 20
2-Acetylaminofluorene 4.8 U Q 96.8 78.4 M Q ug/L 81 60 -138 7 20
2-Naphthylamine 4.8 U J1 96.8 25.6 Q J1 ug/L 26 10 -130 74 20
3,3'-Dimethylbenzidine 13 U Q J1 96.8 13 U M Q J1 ug/L 0 10 -130 200 20
4-Aminobiphenyl 1.9 U J1 96.8 27.7 J1 ug/L 29 10 -130 83 20
4-Nitroquinoline-1-oxide 19 U J1 96.8 70.7 J1 ug/L 73 10 -130 23 20
5-Nitro-o-toluidine 4.8 U 96.8 66.5 Q ug/L 69 38 -126 15 20
7,12-Dimethylbenz(a)anthracene 1.9 U Q J1 96.8 52.1 Q J1 ug/L 54 61 -133 6 20
alpha,alpha-Dimethyl
phenethylamine
77 U J1 96.8 77 U M Q J1 ug/L 0 10 -188 200 20
Diallate 1.9 U Q J1 96.8 29.1 J1 ug/L 30 67 -124 15 20
Dimethoate 1.9 U Q 96.8 60.8 ug/L 63 27 -86 10 20
Dinoseb 9.7 U Q 96.8 65.4 ug/L 68 61 -126 9 20
Disulfoton 1.9 U J1 Q 96.8 37.9 J1 ug/L 39 55 -130 9 20
Ethyl methanesulfonate 1.9 U Q J1 96.8 24.4 J1 ug/L 25 62 -118 12 20
Ethyl Parathion 1.9 U M J1 Q 96.8 49.1 J1 ug/L 51 66 -140 4 20
Famphur 1.9 U Q J1 96.8 77.2 Q J1 ug/L 80 10 -130 31 20
Hexachloropropene 4.8 U Q 96.8 16.8 Q ug/L 17 12 -51 4 20
Isosafrole 1.9 U J1 Q 96.8 29.7 Q J1 ug/L 31 56 -126 17 20
Methyl methanesulfonate 1.9 U M J1 Q 96.8 22.7 J1 ug/L 23 33 -107 16 20
Methyl parathion 1.9 U 96.8 56.3 ug/L 58 45 -159 6 20
N-Nitrosodiethylamine 1.9 U J1 96.8 31.9 J1 ug/L 33 43 -121 14 20
N-Nitrosodi-n-butylamine 1.9 U M J1 96.8 33.2 Q J1 ug/L 34 60 -121 18 20
N-Nitrosomethylethylamine 9.7 U J1 96.8 33.3 J1 ug/L 34 41 -117 13 20
N-Nitrosopiperidine 1.9 U J1 96.8 38.2 Q J1 ug/L 39 56 -121 15 20
N-Nitrosopyrrolidine 1.9 U J1 96.8 36.8 J1 ug/L 38 48 -113 15 20
o,o',o''-Triethylphosphorothioate 1.9 U M J1 96.8 39.5 Q J1 ug/L 41 66 -119 19 20
o-Toluidine 4.8 U J1 96.8 25.4 J1 ug/L 26 30 -110 48 20
p-Dimethylamino azobenzene 1.9 U M J1 96.8 41.2 J1 ug/L 43 62 -132 15 20
Pentachlorobenzene 1.9 U J1 Q 96.8 24.7 Q J1 ug/L 26 59 -123 12 20
Pentachloronitrobenzene 1.9 U J1 96.8 42.5 J1 ug/L 44 54 -135 5 20
Phenacetin 4.8 U 96.8 78.4 ug/L 81 71 -124 3 20
Phorate 1.9 U 96.8 82.0 ug/L 85 38 -139 6 20
p-Phenylene diamine 24 U Q J1 96.8 24 U Q J1 ug/L 0 10 -130 NC 20
Pronamide 1.9 U 96.8 75.2 ug/L 78 65 -129 5 20
Safrole, Total 1.9 U J1 Q 96.8 40.3 Q J1 ug/L 42 61 -119 20 20
sym-Trinitrobenzene 4.8 U Q 96.8 116 ug/L 120 41 -137 3 20
Thionazin 1.9 U Q J1 96.8 41.8 Q J1 ug/L 43 72 -132 12 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778040 Prep Batch: 777298
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
51
MSD MSD
Qualifier Limits%Recovery
35 Q2-Fluorobiphenyl (Surr)44 -119
282-Fluorophenol (Surr)19 -119
37 QNitrobenzene-d5 (Surr)44 -120
30Phenol-d5 (Surr)27 -110
36 QTerphenyl-d14 (Surr)50 -134
Client Sample ID: Method BlankLab Sample ID: MB 680-779620/19-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
LOQ DL
1,2,4,5-Tetrachlorobenzene 2.0 U Q 10 0.76 ug/L 05/20/23 21:30 05/24/23 15:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2.0 U Q 0.5610 ug/L 05/20/23 21:30 05/24/23 15:51 11,2,4-Trichlorobenzene
2.0 U Q 0.5310 ug/L 05/20/23 21:30 05/24/23 15:51 11,2-Dichlorobenzene
2.0 U Q 0.5910 ug/L 05/20/23 21:30 05/24/23 15:51 11,3-Dichlorobenzene
2.0 U Q 0.6010 ug/L 05/20/23 21:30 05/24/23 15:51 11,3-Dinitrobenzene
2.0 U Q 0.5410 ug/L 05/20/23 21:30 05/24/23 15:51 11,4-Dichlorobenzene
2.0 U Q 0.6210 ug/L 05/20/23 21:30 05/24/23 15:51 11,4-Naphthoquinone
2.0 U Q 1.110 ug/L 05/20/23 21:30 05/24/23 15:51 11-Naphthylamine
2.0 U Q 0.7210 ug/L 05/20/23 21:30 05/24/23 15:51 12,3,4,6-Tetrachlorophenol
2.0 U Q 1.210 ug/L 05/20/23 21:30 05/24/23 15:51 12,4,5-Trichlorophenol
2.0 U Q 0.8510 ug/L 05/20/23 21:30 05/24/23 15:51 12,4,6-Trichlorophenol
2.0 U Q 1.110 ug/L 05/20/23 21:30 05/24/23 15:51 12,4-Dichlorophenol
10 U Q 4.010 ug/L 05/20/23 21:30 05/24/23 15:51 12,4-Dimethylphenol
20 U Q 1050 ug/L 05/20/23 21:30 05/24/23 15:51 12,4-Dinitrophenol
2.0 U Q 1.210 ug/L 05/20/23 21:30 05/24/23 15:51 12,4-Dinitrotoluene
2.0 U Q 0.7310 ug/L 05/20/23 21:30 05/24/23 15:51 12,6-Dichlorophenol
2.0 U Q 1.110 ug/L 05/20/23 21:30 05/24/23 15:51 12,6-Dinitrotoluene
5.0 U 1.610 ug/L 05/20/23 21:30 05/24/23 15:51 12-Acetylaminofluorene
2.0 U Q 0.8010 ug/L 05/20/23 21:30 05/24/23 15:51 12-Chloronaphthalene
2.0 U Q 0.8710 ug/L 05/20/23 21:30 05/24/23 15:51 12-Chlorophenol
2.0 U Q 0.7810 ug/L 05/20/23 21:30 05/24/23 15:51 12-Methylnaphthalene
2.0 U Q 0.8910 ug/L 05/20/23 21:30 05/24/23 15:51 12-Methylphenol
5.0 U Q 1.510 ug/L 05/20/23 21:30 05/24/23 15:51 12-Naphthylamine
2.0 U Q 1.350 ug/L 05/20/23 21:30 05/24/23 15:51 12-Nitroaniline
2.0 U Q 0.7610 ug/L 05/20/23 21:30 05/24/23 15:51 12-Nitrophenol
2.0 U Q 1.310 ug/L 05/20/23 21:30 05/24/23 15:51 13 & 4 Methylphenol
60 U Q 3060 ug/L 05/20/23 21:30 05/24/23 15:51 13,3'-Dichlorobenzidine
13 U 1020 ug/L 05/20/23 21:30 05/24/23 15:51 13,3'-Dimethylbenzidine
5.0 U 1.410 ug/L 05/20/23 21:30 05/24/23 15:51 13-Methylcholanthrene
10 U Q 5.050 ug/L 05/20/23 21:30 05/24/23 15:51 13-Nitroaniline
20 U Q 1050 ug/L 05/20/23 21:30 05/24/23 15:51 14,6-Dinitro-2-methylphenol
2.0 U 1.210 ug/L 05/20/23 21:30 05/24/23 15:51 14-Aminobiphenyl
2.0 U Q M 0.7710 ug/L 05/20/23 21:30 05/24/23 15:51 14-Bromophenyl phenyl ether
2.0 U Q 1.010 ug/L 05/20/23 21:30 05/24/23 15:51 14-Chloro-3-methylphenol
5.0 U Q 2.220 ug/L 05/20/23 21:30 05/24/23 15:51 14-Chloroaniline
2.0 U Q 0.8410 ug/L 05/20/23 21:30 05/24/23 15:51 14-Chlorophenyl phenyl ether
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-779620/19-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
LOQ DL
4-Nitroaniline 10 U Q 50 5.0 ug/L 05/20/23 21:30 05/24/23 15:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4.0 U Q 1.950 ug/L 05/20/23 21:30 05/24/23 15:51 14-Nitrophenol
20 U 1025 ug/L 05/20/23 21:30 05/24/23 15:51 14-Nitroquinoline-1-oxide
5.0 U Q 1.510 ug/L 05/20/23 21:30 05/24/23 15:51 15-Nitro-o-toluidine
2.0 U Q 1.210 ug/L 05/20/23 21:30 05/24/23 15:51 17,12-Dimethylbenz(a)anthracene
2.0 U 0.7610 ug/L 05/20/23 21:30 05/24/23 15:51 1Acenaphthene
2.0 U 0.8510 ug/L 05/20/23 21:30 05/24/23 15:51 1Acenaphthylene
2.0 U Q 0.5710 ug/L 05/20/23 21:30 05/24/23 15:51 1Acetophenone
80 U Q 352000 ug/L 05/20/23 21:30 05/24/23 15:51 1alpha,alpha-Dimethyl phenethylamine
2.0 U 0.6910 ug/L 05/20/23 21:30 05/24/23 15:51 1Anthracene
2.0 U 0.5510 ug/L 05/20/23 21:30 05/24/23 15:51 1Benzo[a]anthracene
2.0 U 0.7110 ug/L 05/20/23 21:30 05/24/23 15:51 1Benzo[a]pyrene
5.0 U 2.610 ug/L 05/20/23 21:30 05/24/23 15:51 1Benzo[b]fluoranthene
2.0 U 0.8710 ug/L 05/20/23 21:30 05/24/23 15:51 1Benzo[g,h,i]perylene
2.0 U 1.210 ug/L 05/20/23 21:30 05/24/23 15:51 1Benzo[k]fluoranthene
2.0 U Q M 1.110 ug/L 05/20/23 21:30 05/24/23 15:51 1Benzyl alcohol
2.0 U Q 0.7810 ug/L 05/20/23 21:30 05/24/23 15:51 1bis (2-chloroisopropyl) ether
2.0 U Q 0.9410 ug/L 05/20/23 21:30 05/24/23 15:51 1Bis(2-chloroethoxy)methane
2.0 U Q 1.110 ug/L 05/20/23 21:30 05/24/23 15:51 1Bis(2-chloroethyl)ether
3.24 J Q 1.610 ug/L 05/20/23 21:30 05/24/23 15:51 1Bis(2-ethylhexyl) phthalate
2.0 U Q 1.210 ug/L 05/20/23 21:30 05/24/23 15:51 1Butyl benzyl phthalate
2.0 U 0.5110 ug/L 05/20/23 21:30 05/24/23 15:51 1Chrysene
2.0 U 0.7810 ug/L 05/20/23 21:30 05/24/23 15:51 1Diallate
2.0 U Q 1.010 ug/L 05/20/23 21:30 05/24/23 15:51 1Dibenz(a,h)anthracene
2.0 U Q 0.7910 ug/L 05/20/23 21:30 05/24/23 15:51 1Dibenzofuran
2.0 U Q 0.8810 ug/L 05/20/23 21:30 05/24/23 15:51 1Diethyl phthalate
2.0 U 0.7510 ug/L 05/20/23 21:30 05/24/23 15:51 1Dimethoate
2.0 U Q 0.9910 ug/L 05/20/23 21:30 05/24/23 15:51 1Dimethyl phthalate
2.0 U Q 0.8310 ug/L 05/20/23 21:30 05/24/23 15:51 1Di-n-butyl phthalate
2.5 U Q 1.410 ug/L 05/20/23 21:30 05/24/23 15:51 1Di-n-octyl phthalate
10 U 5.010 ug/L 05/20/23 21:30 05/24/23 15:51 1Dinoseb
2.0 U 0.9210 ug/L 05/20/23 21:30 05/24/23 15:51 1Diphenylamine
2.0 U 0.7910 ug/L 05/20/23 21:30 05/24/23 15:51 1Disulfoton
2.0 U Q 0.9610 ug/L 05/20/23 21:30 05/24/23 15:51 1Ethyl methanesulfonate
2.0 U 1.310 ug/L 05/20/23 21:30 05/24/23 15:51 1Ethyl Parathion
2.0 U 1.110 ug/L 05/20/23 21:30 05/24/23 15:51 1Famphur
2.0 U 0.7410 ug/L 05/20/23 21:30 05/24/23 15:51 1Fluoranthene
2.0 U 0.9610 ug/L 05/20/23 21:30 05/24/23 15:51 1Fluorene
2.0 U Q 0.7910 ug/L 05/20/23 21:30 05/24/23 15:51 1Hexachlorobenzene
2.0 U Q 0.6210 ug/L 05/20/23 21:30 05/24/23 15:51 1Hexachlorobutadiene
5.0 U Q 2.510 ug/L 05/20/23 21:30 05/24/23 15:51 1Hexachlorocyclopentadiene
2.0 U Q 0.7610 ug/L 05/20/23 21:30 05/24/23 15:51 1Hexachloroethane
5.0 U Q 1.410 ug/L 05/20/23 21:30 05/24/23 15:51 1Hexachloropropene
2.0 U 1.010 ug/L 05/20/23 21:30 05/24/23 15:51 1Indeno[1,2,3-cd]pyrene
2.0 U Q M 0.9010 ug/L 05/20/23 21:30 05/24/23 15:51 1Isophorone
2.0 U Q 0.5010 ug/L 05/20/23 21:30 05/24/23 15:51 1Isosafrole
5.0 U 2.72000 ug/L 05/20/23 21:30 05/24/23 15:51 1Methapyrilene
2.0 U Q 0.6010 ug/L 05/20/23 21:30 05/24/23 15:51 1Methyl methanesulfonate
2.0 U 0.8810 ug/L 05/20/23 21:30 05/24/23 15:51 1Methyl parathion
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-779620/19-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
LOQ DL
Naphthalene 2.0 U 10 0.70 ug/L 05/20/23 21:30 05/24/23 15:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2.0 U Q 0.7310 ug/L 05/20/23 21:30 05/24/23 15:51 1Nitrobenzene
2.0 U Q 0.9310 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosodiethylamine
5.0 U Q 2.810 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosodimethylamine
2.0 U Q 0.9610 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosodi-n-butylamine
2.0 U Q 0.7210 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosodi-n-propylamine
2.0 U Q 0.9210 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosodiphenylamine
10 U Q 3.310 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosomethylethylamine
2.0 U Q 0.8810 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosopiperidine
2.0 U Q 1.010 ug/L 05/20/23 21:30 05/24/23 15:51 1N-Nitrosopyrrolidine
2.0 U Q 1.010 ug/L 05/20/23 21:30 05/24/23 15:51 1o,o',o''-Triethylphosphorothioate
5.0 U Q 1.410 ug/L 05/20/23 21:30 05/24/23 15:51 1o-Toluidine
2.0 U M 0.7910 ug/L 05/20/23 21:30 05/24/23 15:51 1p-Dimethylamino azobenzene
2.0 U Q 0.5210 ug/L 05/20/23 21:30 05/24/23 15:51 1Pentachlorobenzene
2.0 U 0.7810 ug/L 05/20/23 21:30 05/24/23 15:51 1Pentachloronitrobenzene
4.0 U Q 2.050 ug/L 05/20/23 21:30 05/24/23 15:51 1Pentachlorophenol
5.0 U 1.410 ug/L 05/20/23 21:30 05/24/23 15:51 1Phenacetin
2.0 U 0.7710 ug/L 05/20/23 21:30 05/24/23 15:51 1Phenanthrene
2.0 U Q 0.8310 ug/L 05/20/23 21:30 05/24/23 15:51 1Phenol
2.0 U 0.8710 ug/L 05/20/23 21:30 05/24/23 15:51 1Phorate
25 U 102000 ug/L 05/20/23 21:30 05/24/23 15:51 1p-Phenylene diamine
2.0 U 0.8910 ug/L 05/20/23 21:30 05/24/23 15:51 1Pronamide
2.0 U 0.6310 ug/L 05/20/23 21:30 05/24/23 15:51 1Pyrene
2.0 U Q 0.8010 ug/L 05/20/23 21:30 05/24/23 15:51 1Safrole, Total
5.0 U 2.010 ug/L 05/20/23 21:30 05/24/23 15:51 1sym-Trinitrobenzene
2.0 U Q 0.9110 ug/L 05/20/23 21:30 05/24/23 15:51 1Thionazin
2,4,6-Tribromophenol (Surr)36 Q 43-140 05/24/23 15:51 1
MB MB
Surrogate
05/20/23 21:30
Dil FacPrepared AnalyzedQualifier Limits%Recovery
22 Q 05/20/23 21:30 05/24/23 15:51 12-Fluorobiphenyl (Surr)44-119
15 Q 05/20/23 21:30 05/24/23 15:51 12-Fluorophenol (Surr)19-119
35 Q 05/20/23 21:30 05/24/23 15:51 1Nitrobenzene-d5 (Surr)44-120
11 Q 05/20/23 21:30 05/24/23 15:51 1Phenol-d5 (Surr)27-110
79 05/20/23 21:30 05/24/23 15:51 1Terphenyl-d14 (Surr)50-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-779620/20-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
1,2,4,5-Tetrachlorobenzene 100 23.8 Q ug/L 24 35 -121
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trichlorobenzene 100 9.98 J Q ug/L 10 29 -116
1,2-Dichlorobenzene 100 14.6 Q ug/L 15 32 -111
1,3-Dichlorobenzene 100 18.8 Q ug/L 19 28 -110
1,3-Dinitrobenzene 100 62.9 Q ug/L 63 49 -128
1,4-Dichlorobenzene 100 18.4 Q ug/L 18 29 -112
2,3,4,6-Tetrachlorophenol 100 69.7 Q ug/L 70 50 -128
2,4,5-Trichlorophenol 100 47.4 Q ug/L 47 53 -123
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-779620/20-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
2,4,6-Trichlorophenol 100 41.4 Q ug/L 41 50 -125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
2,4-Dichlorophenol 100 16.3 Q ug/L 16 47 -121
2,4-Dimethylphenol 100 15.5 Q ug/L 15 31 -124
2,4-Dinitrophenol 200 103 ug/L 52 23 -143
2,4-Dinitrotoluene 100 69.5 Q ug/L 69 57 -128
2,6-Dichlorophenol 100 17.3 Q ug/L 17 50 -118
2,6-Dinitrotoluene 100 62.7 Q ug/L 63 57 -124
2-Chloronaphthalene 100 32.7 Q ug/L 33 40 -116
2-Chlorophenol 100 14.7 Q ug/L 15 38 -117
2-Methylnaphthalene 100 24.6 Q ug/L 25 40 -121
2-Methylphenol 100 14.3 Q ug/L 14 30 -117
2-Nitroaniline 100 35.6 J Q ug/L 36 55 -127
2-Nitrophenol 100 10.3 Q ug/L 10 47 -123
3 & 4 Methylphenol 100 15.7 Q ug/L 16 29 -110
3,3'-Dichlorobenzidine 100 60 U Q ug/L 3 27 -129
3-Nitroaniline 100 11.5 J Q ug/L 11 41 -128
4,6-Dinitro-2-methylphenol 200 134 ug/L 67 44 -137
4-Bromophenyl phenyl ether 100 67.3 Q ug/L 67 55 -124
4-Chloro-3-methylphenol 100 38.5 Q ug/L 39 52 -119
4-Chloroaniline 100 17.9 J Q ug/L 18 33 -117
4-Chlorophenyl phenyl ether 100 64.7 Q ug/L 65 53 -121
4-Nitroaniline 100 6.77 J Q ug/L 7 44 -119
4-Nitrophenol 200 103 ug/L 52 41 -118
Acenaphthene 100 44.8 Q ug/L 45 47 -122
Acenaphthylene 100 2.33 J Q ug/L 2 41 -130
Acetophenone 100 13.4 Q ug/L 13 46 -118
Anthracene 100 58.2 ug/L 58 57 -123
Benzo[a]anthracene 100 76.2 ug/L 76 58 -125
Benzo[a]pyrene 100 25.0 Q ug/L 25 54 -128
Benzo[b]fluoranthene 100 82.3 ug/L 82 53 -131
Benzo[g,h,i]perylene 100 45.6 Q ug/L 46 50 -134
Benzo[k]fluoranthene 100 75.7 M ug/L 76 57 -129
Benzyl alcohol 100 8.12 J Q ug/L 8 31 -112
bis (2-chloroisopropyl) ether 100 9.37 J Q ug/L 9 37 -130
Bis(2-chloroethoxy)methane 100 4.10 J Q ug/L 4 48 -120
Bis(2-chloroethyl)ether 100 13.4 Q ug/L 13 43 -118
Bis(2-ethylhexyl) phthalate 100 76.6 Q ug/L 77 55 -135
Butyl benzyl phthalate 100 59.9 Q ug/L 60 53 -134
Chrysene 100 76.0 ug/L 76 59 -123
Dibenz(a,h)anthracene 100 72.2 Q ug/L 72 51 -134
Dibenzofuran 100 53.3 Q ug/L 53 53 -118
Diethyl phthalate 100 63.4 Q ug/L 63 56 -125
Dimethyl phthalate 100 59.6 Q ug/L 60 45 -127
Di-n-butyl phthalate 100 68.8 Q ug/L 69 59 -127
Di-n-octyl phthalate 100 75.0 Q ug/L 75 51 -140
Diphenylamine 85.5 2.0 U Q M ug/L 0.9 51 -123
Fluoranthene 100 77.5 ug/L 77 57 -128
Fluorene 100 58.1 ug/L 58 52 -124
Hexachlorobenzene 100 68.1 Q ug/L 68 53 -125
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-779620/20-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
Hexachlorobutadiene 100 11.4 Q ug/L 11 22 -124
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Hexachlorocyclopentadiene 100 2.52 J Q ug/L 3 10 -130
Hexachloroethane 100 15.4 Q ug/L 15 21 -115
Indeno[1,2,3-cd]pyrene 100 47.8 Q ug/L 48 52 -134
Isophorone 100 33.4 Q ug/L 33 42 -124
Naphthalene 100 10.7 Q ug/L 11 40 -121
Nitrobenzene 100 10.6 Q ug/L 11 45 -121
N-Nitrosodimethylamine 100 32.7 Q ug/L 33 41 -82
N-Nitrosodi-n-propylamine 100 4.14 J Q ug/L 4 49 -119
N-Nitrosodiphenylamine 100 2.0 U Q ug/L 0.9 51 -123
Pentachlorophenol 200 154 ug/L 77 35 -138
Phenanthrene 100 67.9 ug/L 68 59 -120
Phenol 100 11.6 Q ug/L 12 35 -101
Pyrene 100 63.6 ug/L 64 57 -126
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
51
LCS LCS
Qualifier Limits%Recovery
30 Q2-Fluorobiphenyl (Surr)44 -119
11 Q2-Fluorophenol (Surr)19 -119
9 QNitrobenzene-d5 (Surr)44 -120
8 QPhenol-d5 (Surr)27 -110
63Terphenyl-d14 (Surr)50 -134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-779620/22-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
1,4-Naphthoquinone 100 8.15 J Q ug/L 8 10 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1-Naphthylamine 100 16.7 Q ug/L 17 24 -124
2-Acetylaminofluorene 100 68.2 ug/L 68 60 -138
2-Naphthylamine 100 22.5 Q ug/L 22 10 -130
3,3'-Dimethylbenzidine 100 34.5 ug/L 34 10 -130
4-Aminobiphenyl 100 14.1 ug/L 14 10 -130
4-Nitroquinoline-1-oxide 100 20 U Q ug/L 0.5 10 -130
5-Nitro-o-toluidine 100 29.6 Q ug/L 30 38 -126
7,12-Dimethylbenz(a)anthracene 100 55.6 Q ug/L 56 61 -133
alpha,alpha-Dimethyl
phenethylamine
100 61.5 J Q M ug/L 62 10 -188
Diallate 100 50.5 Q ug/L 51 67 -124
Dimethoate 100 4.94 J Q ug/L 5 27 -86
Dinoseb 100 66.5 ug/L 66 61 -126
Disulfoton 100 45.6 Q ug/L 46 55 -130
Ethyl methanesulfonate 100 5.56 J Q ug/L 6 62 -118
Ethyl Parathion 100 53.1 Q ug/L 53 66 -140
Famphur 100 2.0 U Q M ug/L 0.2 10 -130
Hexachloropropene 100 1.97 J Q ug/L 2 12 -51
Isosafrole 100 9.70 J Q ug/L 10 56 -126
Methyl methanesulfonate 100 3.39 J Q ug/L 3 33 -107
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-779620/22-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
Methyl parathion 100 7.25 J Q ug/L 7 45 -159
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
N-Nitrosodiethylamine 100 6.88 J Q ug/L 7 43 -121
N-Nitrosodi-n-butylamine 100 23.3 Q ug/L 23 60 -121
N-Nitrosomethylethylamine 100 7.08 J Q ug/L 7 41 -117
N-Nitrosopiperidine 100 18.6 Q ug/L 19 56 -121
N-Nitrosopyrrolidine 100 17.7 Q ug/L 18 48 -113
o,o',o''-Triethylphosphorothioate 100 27.7 Q ug/L 28 66 -119
o-Toluidine 100 33.8 Q ug/L 34 30 -110
p-Dimethylamino azobenzene 100 20.6 Q ug/L 21 62 -132
Pentachlorobenzene 100 31.1 Q ug/L 31 59 -123
Pentachloronitrobenzene 100 72.7 ug/L 73 54 -135
Phenacetin 100 72.2 ug/L 72 71 -124
Phorate 100 91.0 ug/L 91 38 -139
p-Phenylene diamine 100 13.1 J M ug/L 13 10 -130
Pronamide 100 56.9 Q ug/L 57 65 -129
Safrole, Total 100 25.6 Q ug/L 26 61 -119
sym-Trinitrobenzene 100 117 ug/L 117 41 -137
Thionazin 100 50.5 Q ug/L 51 72 -132
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
27 Q2-Fluorobiphenyl (Surr)44 -119
6 Q2-Fluorophenol (Surr)19 -119
14 QNitrobenzene-d5 (Surr)44 -120
8 QPhenol-d5 (Surr)27 -110
70Terphenyl-d14 (Surr)50 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-779620/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
1,2,4,5-Tetrachlorobenzene 100 61.5 Q ug/L 62 35 -121 89 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2,4-Trichlorobenzene 100 38.2 Q ug/L 38 29 -116 117 20
1,2-Dichlorobenzene 100 27.1 Q ug/L 27 32 -111 60 20
1,3-Dichlorobenzene 100 25.2 Q ug/L 25 28 -110 29 20
1,3-Dinitrobenzene 100 94.5 Q ug/L 95 49 -128 40 20
1,4-Dichlorobenzene 100 25.9 Q ug/L 26 29 -112 34 20
2,3,4,6-Tetrachlorophenol 100 98.0 Q ug/L 98 50 -128 34 20
2,4,5-Trichlorophenol 100 83.4 Q ug/L 83 53 -123 55 20
2,4,6-Trichlorophenol 100 77.4 Q ug/L 77 50 -125 61 20
2,4-Dichlorophenol 100 53.0 Q ug/L 53 47 -121 106 20
2,4-Dimethylphenol 100 46.1 Q ug/L 46 31 -124 99 20
2,4-Dinitrophenol 200 189 Q ug/L 95 23 -143 59 20
2,4-Dinitrotoluene 100 97.4 Q ug/L 97 57 -128 34 20
2,6-Dichlorophenol 100 56.2 Q ug/L 56 50 -118 106 20
2,6-Dinitrotoluene 100 91.6 Q ug/L 92 57 -124 38 20
2-Chloronaphthalene 100 61.9 Q ug/L 62 40 -116 62 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-779620/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
2-Chlorophenol 100 29.7 Q ug/L 30 38 -117 68 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Methylnaphthalene 100 59.7 Q ug/L 60 40 -121 83 20
2-Methylphenol 100 35.3 Q ug/L 35 30 -117 85 20
2-Nitroaniline 100 90.8 Q ug/L 91 55 -127 87 20
2-Nitrophenol 100 45.8 Q ug/L 46 47 -123 126 20
3 & 4 Methylphenol 100 36.2 Q ug/L 36 29 -110 79 20
3,3'-Dichlorobenzidine 100 59.0 J Q ug/L 59 27 -129 179 20
3-Nitroaniline 100 83.1 Q ug/L 83 41 -128 152 20
4,6-Dinitro-2-methylphenol 200 212 Q ug/L 106 44 -137 45 20
4-Bromophenyl phenyl ether 100 97.0 Q ug/L 97 55 -124 36 20
4-Chloro-3-methylphenol 100 70.9 Q ug/L 71 52 -119 59 20
4-Chloroaniline 100 68.5 Q ug/L 68 33 -117 117 20
4-Chlorophenyl phenyl ether 100 91.2 Q ug/L 91 53 -121 34 20
4-Nitroaniline 100 91.1 Q ug/L 91 44 -119 172 20
4-Nitrophenol 200 177 Q ug/L 89 41 -118 53 20
Acenaphthene 100 73.2 Q ug/L 73 47 -122 48 20
Acenaphthylene 100 68.7 Q ug/L 69 41 -130 187 20
Acetophenone 100 49.0 Q ug/L 49 46 -118 114 20
Anthracene 100 93.8 Q ug/L 94 57 -123 47 20
Benzo[a]anthracene 100 103 Q ug/L 103 58 -125 30 20
Benzo[a]pyrene 100 103 Q ug/L 103 54 -128 122 20
Benzo[b]fluoranthene 100 105 Q ug/L 105 53 -131 24 20
Benzo[g,h,i]perylene 100 94.5 Q ug/L 94 50 -134 70 20
Benzo[k]fluoranthene 100 100 Q ug/L 100 57 -129 28 20
Benzyl alcohol 100 52.1 Q ug/L 52 31 -112 146 20
bis (2-chloroisopropyl) ether 100 35.3 Q ug/L 35 37 -130 116 20
Bis(2-chloroethoxy)methane 100 51.8 Q ug/L 52 48 -120 171 20
Bis(2-chloroethyl)ether 100 30.4 Q ug/L 30 43 -118 78 20
Bis(2-ethylhexyl) phthalate 100 99.8 Q ug/L 100 55 -135 26 20
Butyl benzyl phthalate 100 102 Q ug/L 102 53 -134 52 20
Chrysene 100 98.2 Q ug/L 98 59 -123 25 20
Dibenz(a,h)anthracene 100 95.7 Q ug/L 96 51 -134 28 20
Dibenzofuran 100 78.9 Q ug/L 79 53 -118 39 20
Diethyl phthalate 100 101 Q ug/L 101 56 -125 46 20
Dimethyl phthalate 100 92.2 Q ug/L 92 45 -127 43 20
Di-n-butyl phthalate 100 98.7 Q ug/L 99 59 -127 36 20
Di-n-octyl phthalate 100 97.9 Q ug/L 98 51 -140 27 20
Diphenylamine 85.5 71.5 Q ug/L 84 51 -123 196 20
Fluoranthene 100 104 Q ug/L 104 57 -128 29 20
Fluorene 100 86.7 Q ug/L 87 52 -124 40 20
Hexachlorobenzene 100 90.7 Q ug/L 91 53 -125 28 20
Hexachlorobutadiene 100 36.0 Q ug/L 36 22 -124 104 20
Hexachlorocyclopentadiene 100 15.8 Q ug/L 16 10 -130 145 20
Hexachloroethane 100 24.9 Q ug/L 25 21 -115 47 20
Indeno[1,2,3-cd]pyrene 100 86.8 Q ug/L 87 52 -134 58 20
Isophorone 100 63.7 Q ug/L 64 42 -124 63 20
Naphthalene 100 42.9 Q ug/L 43 40 -121 120 20
Nitrobenzene 100 45.7 Q ug/L 46 45 -121 125 20
N-Nitrosodimethylamine 100 36.2 Q M ug/L 36 41 -82 10 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-779620/21-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
N-Nitrosodi-n-propylamine 100 59.5 Q ug/L 60 49 -119 174 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
N-Nitrosodiphenylamine 100 83.6 Q ug/L 84 51 -123 196 20
Pentachlorophenol 200 190 Q ug/L 95 35 -138 21 20
Phenanthrene 100 94.2 Q ug/L 94 59 -120 32 20
Phenol 100 14.5 Q ug/L 15 35 -101 22 20
Pyrene 100 106 Q ug/L 106 57 -126 50 20
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
73
LCSD LCSD
Qualifier Limits%Recovery
522-Fluorobiphenyl (Surr)44 -119
8 Q2-Fluorophenol (Surr)19 -119
37 QNitrobenzene-d5 (Surr)44 -120
10 QPhenol-d5 (Surr)27 -110
77Terphenyl-d14 (Surr)50 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-779620/23-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
1,4-Naphthoquinone 100 7.88 J Q ug/L 8 10 -130 3 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1-Naphthylamine 100 14.4 Q ug/L 14 24 -124 15 20
2-Acetylaminofluorene 100 80.9 ug/L 81 60 -138 17 20
2-Naphthylamine 100 6.06 J Q ug/L 6 10 -130 115 20
3,3'-Dimethylbenzidine 100 13 U Q M ug/L 0.2 10 -130 198 20
4-Aminobiphenyl 100 8.90 J Q ug/L 9 10 -130 45 20
4-Nitroquinoline-1-oxide 100 37.4 Q ug/L 37 10 -130 194 20
5-Nitro-o-toluidine 100 65.4 Q ug/L 65 38 -126 76 20
7,12-Dimethylbenz(a)anthracene 100 66.5 Q ug/L 66 61 -133 18 20
alpha,alpha-Dimethyl
phenethylamine
100 80 U Q M ug/L 1 10 -188 191 20
Diallate 100 53.1 Q ug/L 53 67 -124 5 20
Dimethoate 100 18.3 Q ug/L 18 27 -86 115 20
Dinoseb 100 72.6 ug/L 73 61 -126 9 20
Disulfoton 100 54.9 ug/L 55 55 -130 19 20
Ethyl methanesulfonate 100 11.1 Q ug/L 11 62 -118 66 20
Ethyl Parathion 100 63.9 Q ug/L 64 66 -140 18 20
Famphur 100 3.99 J Q ug/L 4 10 -130 178 20
Hexachloropropene 100 11.9 Q ug/L 12 12 -51 143 20
Isosafrole 100 19.0 Q ug/L 19 56 -126 65 20
Methyl methanesulfonate 100 8.38 J Q ug/L 8 33 -107 85 20
Methyl parathion 100 19.2 Q ug/L 19 45 -159 90 20
N-Nitrosodiethylamine 100 16.4 Q ug/L 16 43 -121 82 20
N-Nitrosodi-n-butylamine 100 29.9 Q ug/L 30 60 -121 25 20
N-Nitrosomethylethylamine 100 21.8 Q ug/L 22 41 -117 102 20
N-Nitrosopiperidine 100 21.1 Q ug/L 21 56 -121 13 20
N-Nitrosopyrrolidine 100 25.7 Q ug/L 26 48 -113 37 20
o,o',o''-Triethylphosphorothioate 100 30.1 Q ug/L 30 66 -119 8 20
o-Toluidine 100 22.2 Q ug/L 22 30 -110 41 20
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-779620/23-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 780179 Prep Batch: 779620
p-Dimethylamino azobenzene 100 33.9 Q ug/L 34 62 -132 49 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pentachlorobenzene 100 28.6 Q ug/L 29 59 -123 8 20
Pentachloronitrobenzene 100 74.8 ug/L 75 54 -135 3 20
Phenacetin 100 78.3 ug/L 78 71 -124 8 20
Phorate 100 106 ug/L 106 38 -139 15 20
p-Phenylene diamine 100 25 U Q ug/L 0 10 -130 200 20
Pronamide 100 75.4 Q ug/L 75 65 -129 28 20
Safrole, Total 100 26.9 Q ug/L 27 61 -119 5 20
sym-Trinitrobenzene 100 116 ug/L 116 41 -137 2 20
Thionazin 100 55.0 Q ug/L 55 72 -132 8 20
2,4,6-Tribromophenol (Surr)43 -140
Surrogate
58
LCSD LCSD
Qualifier Limits%Recovery
23 Q2-Fluorobiphenyl (Surr)44 -119
10 Q2-Fluorophenol (Surr)19 -119
15 QNitrobenzene-d5 (Surr)44 -120
9 QPhenol-d5 (Surr)27 -110
73Terphenyl-d14 (Surr)50 -134
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-374082/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
LOQ DL
Benzene 2.0 U 5.0 1.0 ug/L 05/10/23 09:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
50 U 25100 ug/L 05/10/23 09:52 1C5-C8 Aliphatics
20 U 10100 ug/L 05/10/23 09:52 1C9-C10 Aromatics
50 U 25100 ug/L 05/10/23 09:52 1C9-C12 Aliphatics
2.0 U 1.05.0 ug/L 05/10/23 09:52 1Ethylbenzene
2.0 U 1.05.0 ug/L 05/10/23 09:52 1Methyl tert-butyl ether
4.0 U 2.06.0 ug/L 05/10/23 09:52 1Naphthalene
2.0 U 1.05.0 ug/L 05/10/23 09:52 1Toluene
50 U 25100 ug/L 05/10/23 09:52 1C9-C12 Aliphatics (adjusted)
5.0 U 2.510 ug/L 05/10/23 09:52 1m-Xylene & p-Xylene
2.0 U 1.05.0 ug/L 05/10/23 09:52 1o-Xylene
50 U 25100 ug/L 05/10/23 09:52 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)105 70-130 05/10/23 09:52 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
92 05/10/23 09:52 1a,a,a-Trifluorotoluene (pid)70-130
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-374082/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
Benzene 50.1 43.2 ug/L 86 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Ethylbenzene 50.1 44.6 ug/L 89 70 -130
Methyl tert-butyl ether 50.2 42.2 ug/L 84 70 -130
Naphthalene 50.2 43.9 ug/L 88 70 -130
Toluene 50.1 42.9 ug/L 86 70 -130
m-Xylene & p-Xylene 101 90.4 ug/L 90 70 -130
o-Xylene 50.4 44.2 ug/L 88 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-374082/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
Benzene 50.1 43.6 ug/L 87 70 -130 1 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Ethylbenzene 50.1 45.0 ug/L 90 70 -130 1 25
Methyl tert-butyl ether 50.2 43.3 ug/L 86 70 -130 3 25
Naphthalene 50.2 44.8 ug/L 89 70 -130 2 25
Toluene 50.1 43.4 ug/L 87 70 -130 1 25
m-Xylene & p-Xylene 101 91.2 ug/L 91 70 -130 1 25
o-Xylene 50.4 44.6 ug/L 89 70 -130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
Benzene 13 D 100 100 D ug/L 87 70 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Ethylbenzene 33 D 100 132 D ug/L 99 70 -130
Methyl tert-butyl ether 4.0 U 100 73.9 D ug/L 74 70 -130
Naphthalene 47 D M 100 142 D M ug/L 95 70 -130
Toluene 4.0 U 100 80.3 D ug/L 80 70 -130
m-Xylene & p-Xylene 180 D J1 201 420 D ug/L 120 70 -130
o-Xylene 5.5 J D 101 89.8 D M ug/L 84 70 -130
a,a,a-Trifluorotoluene (fid)M Q 70 -130
Surrogate
176
MS MS
Qualifier Limits%Recovery
128a,a,a-Trifluorotoluene (pid)70 -130
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
Benzene 13 D 100 112 D ug/L 99 70 -130 11 25
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Ethylbenzene 33 D 100 149 D ug/L 115 70 -130 12 25
Methyl tert-butyl ether 4.0 U 100 83.7 D ug/L 83 70 -130 12 25
Naphthalene 47 D M 100 161 D M ug/L 113 70 -130 12 25
Toluene 4.0 U 100 90.3 D ug/L 90 70 -130 12 25
m-Xylene & p-Xylene 180 D J1 201 471 D J1 ug/L 146 70 -130 12 25
o-Xylene 5.5 J D 101 101 D M ug/L 95 70 -130 12 25
a,a,a-Trifluorotoluene (fid)M Q 70 -130
Surrogate
182
MSD MSD
Qualifier Limits%Recovery
131 Qa,a,a-Trifluorotoluene (pid)70 -130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-372935/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375346 Prep Batch: 372935
LOQ DL
C19-C36 Aliphatics 20 U 50 10 ug/L 05/08/23 09:17 05/13/23 12:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
15.2 J 1030 ug/L 05/08/23 09:17 05/13/23 12:12 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)59 40-140 05/13/23 12:12 1
MB MB
Surrogate
05/08/23 09:17
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-372935/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
LOQ DL
Anthracene 1.2 U 2.0 0.60 ug/L 05/08/23 09:17 05/13/23 10:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 5.012 ug/L 05/08/23 09:17 05/13/23 10:43 1Pyrene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Benzo[g,h,i]perylene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Indeno[1,2,3-cd]pyrene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Benzo[b]fluoranthene
1.0 U 0.502.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Fluoranthene
3.0 U 1.54.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Benzo[k]fluoranthene
1.4 U 0.702.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Acenaphthylene
1.0 U 0.502.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Chrysene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Benzo[a]pyrene
1.0 U 0.502.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Dibenz(a,h)anthracene
1.4 U 0.702.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Benzo[a]anthracene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Acenaphthene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Phenanthrene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Fluorene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 1Naphthalene
1.2 U 0.602.0 ug/L 05/08/23 09:17 05/13/23 10:43 12-Methylnaphthalene
30 U 1040 ug/L 05/08/23 09:17 05/13/23 10:43 1C11-C22 Aromatics (unadjusted)
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-372935/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
LOQ DL
C11-C22 Aromatics (Adjusted)30 U 40 10 ug/L 05/08/23 09:17 05/13/23 10:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2-Fluorobiphenyl (Surr)55 40-140 05/13/23 10:43 1
MB MB
Surrogate
05/08/23 09:17
Dil FacPrepared AnalyzedQualifier Limits%Recovery
47 05/08/23 09:17 05/13/23 10:43 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-372935/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375346 Prep Batch: 372935
C19-C36 Aliphatics 321 238 ug/L 74 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 144 M ug/L 60 40 -140
1-Chlorooctadecane (Surr)40 -140
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-372935/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
Anthracene 40.1 21.5 ug/L 54 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Pyrene 40.1 22.2 ug/L 55 40 -140
Benzo[g,h,i]perylene 40.0 21.2 ug/L 53 40 -140
Indeno[1,2,3-cd]pyrene 40.1 20.0 M ug/L 50 40 -140
Benzo[b]fluoranthene 40.2 19.9 M ug/L 50 40 -140
Fluoranthene 40.1 21.2 ug/L 53 40 -140
Benzo[k]fluoranthene 40.1 25.1 M ug/L 63 40 -140
Acenaphthylene 40.1 18.8 ug/L 47 40 -140
Chrysene 40.2 23.2 ug/L 58 40 -140
Benzo[a]pyrene 40.2 21.0 ug/L 52 40 -140
Dibenz(a,h)anthracene 40.0 21.9 ug/L 55 40 -140
Benzo[a]anthracene 40.1 20.8 ug/L 52 40 -140
Acenaphthene 40.2 19.4 ug/L 48 40 -140
Phenanthrene 40.1 20.2 ug/L 50 40 -140
Fluorene 40.1 20.0 ug/L 50 40 -140
Naphthalene 40.1 17.4 M ug/L 43 40 -140
2-Methylnaphthalene 40.1 17.1 M ug/L 43 40 -140
C11-C22 Aromatics (unadjusted)681 357 M ug/L 52 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
63
LCS LCS
Qualifier Limits%Recovery
55o- terphenyl (Surr)40 -140
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-372935/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375346 Prep Batch: 372935
C19-C36 Aliphatics 321 253 ug/L 79 40 -140 6 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 147 M ug/L 61 40 -140 2 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
65
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-372935/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
Anthracene 40.1 24.9 ug/L 62 40 -140 14 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pyrene 40.1 26.3 ug/L 65 40 -140 17 25
Benzo[g,h,i]perylene 40.0 25.7 ug/L 64 40 -140 19 25
Indeno[1,2,3-cd]pyrene 40.1 23.8 M ug/L 59 40 -140 17 25
Benzo[b]fluoranthene 40.2 24.7 M ug/L 61 40 -140 21 25
Fluoranthene 40.1 25.0 ug/L 62 40 -140 16 25
Benzo[k]fluoranthene 40.1 28.4 M ug/L 71 40 -140 12 25
Acenaphthylene 40.1 21.2 ug/L 53 40 -140 12 25
Chrysene 40.2 29.3 ug/L 73 40 -140 24 25
Benzo[a]pyrene 40.2 25.0 ug/L 62 40 -140 17 25
Dibenz(a,h)anthracene 40.0 27.8 ug/L 69 40 -140 24 25
Benzo[a]anthracene 40.1 23.5 ug/L 59 40 -140 12 25
Acenaphthene 40.2 22.1 ug/L 55 40 -140 13 25
Phenanthrene 40.1 23.6 ug/L 59 40 -140 16 25
Fluorene 40.1 23.1 ug/L 58 40 -140 14 25
Naphthalene 40.1 17.8 M ug/L 44 40 -140 2 25
2-Methylnaphthalene 40.1 18.5 M ug/L 46 40 -140 8 25
C11-C22 Aromatics (unadjusted)681 434 M ug/L 64 40 -140 19 25
2-Fluorobiphenyl (Surr)40 -140
Surrogate
68
LCSD LCSD
Qualifier Limits%Recovery
63o- terphenyl (Surr)40 -140
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
Anthracene 1.1 U 38.7 21.6 ug/L 56 40 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Pyrene 9.6 U 38.8 22.4 ug/L 58 40 -140
Benzo[g,h,i]perylene 1.1 U 38.6 22.1 ug/L 57 40 -140
Indeno[1,2,3-cd]pyrene 1.1 U 38.7 20.5 M ug/L 53 40 -140
Benzo[b]fluoranthene 1.1 U 38.8 20.6 M ug/L 53 40 -140
Fluoranthene 0.96 U 38.7 21.6 ug/L 56 40 -140
Benzo[k]fluoranthene 2.9 U 38.8 25.6 M ug/L 66 40 -140
Acenaphthylene 0.98 J 38.7 21.4 ug/L 53 40 -140
Chrysene 0.96 U 38.8 24.0 ug/L 62 40 -140
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
Benzo[a]pyrene 1.1 U 38.8 21.6 ug/L 56 40 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Dibenz(a,h)anthracene 0.96 U 38.7 22.5 ug/L 58 40 -140
Benzo[a]anthracene 1.3 U 38.7 20.9 ug/L 54 40 -140
Acenaphthene 1.1 U 38.8 20.7 ug/L 53 40 -140
Phenanthrene 1.1 U 38.7 20.7 ug/L 53 40 -140
Fluorene 1.1 U 38.7 20.8 ug/L 54 40 -140
Naphthalene 15 M 38.7 40.9 M ug/L 68 40 -140
2-Methylnaphthalene 5.3 M 38.7 30.5 M ug/L 65 40 -140
C11-C22 Aromatics (unadjusted)45 658 441 M ug/L 60 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
63
MS MS
Qualifier Limits%Recovery
57o- terphenyl (Surr)40 -140
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375346 Prep Batch: 372935
C19-C36 Aliphatics 19 U 310 237 ug/L 76 40 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C9-C18 Aliphatics 20 J B 233 214 ug/L 83 40 -140
1-Chlorooctadecane (Surr)40 -140
Surrogate
59
MS MS
Qualifier Limits%Recovery
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
Anthracene 1.1 U 39.1 23.7 ug/L 61 40 -140 9 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Pyrene 9.6 U 39.2 25.1 ug/L 64 40 -140 11 50
Benzo[g,h,i]perylene 1.1 U 39.1 23.8 ug/L 61 40 -140 8 50
Indeno[1,2,3-cd]pyrene 1.1 U 39.1 22.6 M ug/L 58 40 -140 10 50
Benzo[b]fluoranthene 1.1 U 39.2 21.1 M ug/L 54 40 -140 2 50
Fluoranthene 0.96 U 39.1 24.1 ug/L 62 40 -140 11 50
Benzo[k]fluoranthene 2.9 U 39.2 29.2 M ug/L 75 40 -140 13 50
Acenaphthylene 0.98 J 39.1 23.3 ug/L 57 40 -140 9 50
Chrysene 0.96 U 39.2 25.4 ug/L 65 40 -140 6 50
Benzo[a]pyrene 1.1 U 39.2 23.4 ug/L 60 40 -140 8 50
Dibenz(a,h)anthracene 0.96 U 39.1 24.3 ug/L 62 40 -140 7 50
Benzo[a]anthracene 1.3 U 39.1 23.4 ug/L 60 40 -140 11 50
Acenaphthene 1.1 U 39.2 21.9 ug/L 56 40 -140 6 50
Phenanthrene 1.1 U 39.1 22.8 ug/L 58 40 -140 10 50
Fluorene 1.1 U 39.1 22.8 ug/L 58 40 -140 9 50
Naphthalene 15 M 39.1 46.2 M ug/L 81 40 -140 12 50
2-Methylnaphthalene 5.3 M 39.1 34.6 ug/L 75 40 -140 13 50
C11-C22 Aromatics (unadjusted)45 665 486 M ug/L 66 40 -140 10 50
Eurofins Savannah
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375340 Prep Batch: 372935
2-Fluorobiphenyl (Surr)40 -140
Surrogate
65
MSD MSD
Qualifier Limits%Recovery
61o- terphenyl (Surr)40 -140
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 375346 Prep Batch: 372935
C19-C36 Aliphatics 19 U 314 244 ug/L 78 40 -140 3 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 20 J B 235 214 ug/L 82 40 -140 0 50
1-Chlorooctadecane (Surr)40 -140
Surrogate
57
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-378825/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
LOQ DL
C19-C36 Aliphatics 20 U M 50 10 ug/L 05/23/23 09:00 06/01/23 03:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
25.7 J 1030 ug/L 05/23/23 09:00 06/01/23 03:14 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)51 M 40-140 06/01/23 03:14 1
MB MB
Surrogate
05/23/23 09:00
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-378825/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
LOQ DL
Anthracene 1.2 U 2.0 0.60 ug/L 05/23/23 09:00 06/01/23 02:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 5.012 ug/L 05/23/23 09:00 06/01/23 02:52 1Pyrene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[g,h,i]perylene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Indeno[1,2,3-cd]pyrene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[b]fluoranthene
1.0 U 0.502.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Fluoranthene
3.0 U 1.54.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[k]fluoranthene
1.4 U 0.702.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Acenaphthylene
1.0 U 0.502.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Chrysene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[a]pyrene
1.0 U 0.502.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Dibenz(a,h)anthracene
1.4 U 0.702.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[a]anthracene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Acenaphthene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Phenanthrene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Fluorene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Naphthalene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 12-Methylnaphthalene
30 U 1040 ug/L 05/23/23 09:00 06/01/23 02:52 1C11-C22 Aromatics (unadjusted)
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-378825/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
LOQ DL
C11-C22 Aromatics (Adjusted)30 U 40 10 ug/L 05/23/23 09:00 06/01/23 02:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2-Fluorobiphenyl (Surr)82 40-140 06/01/23 02:52 1
MB MB
Surrogate
05/23/23 09:00
Dil FacPrepared AnalyzedQualifier Limits%Recovery
59 05/23/23 09:00 06/01/23 02:52 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-378825/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
C19-C36 Aliphatics 321 196 M ug/L 61 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 134 M ug/L 56 40 -140
1-Chlorooctadecane (Surr)M 40 -140
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-378825/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Anthracene 40.1 29.4 ug/L 73 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Pyrene 40.1 29.7 ug/L 74 40 -140
Benzo[g,h,i]perylene 40.0 29.2 ug/L 73 40 -140
Indeno[1,2,3-cd]pyrene 40.1 27.6 ug/L 69 40 -140
Benzo[b]fluoranthene 40.2 30.2 M ug/L 75 40 -140
Fluoranthene 40.1 29.7 ug/L 74 40 -140
Benzo[k]fluoranthene 40.1 29.3 M ug/L 73 40 -140
Acenaphthylene 40.1 28.1 ug/L 70 40 -140
Chrysene 40.2 28.8 ug/L 72 40 -140
Benzo[a]pyrene 40.2 28.0 ug/L 70 40 -140
Dibenz(a,h)anthracene 40.0 29.2 ug/L 73 40 -140
Benzo[a]anthracene 40.1 29.8 ug/L 74 40 -140
Acenaphthene 40.2 27.2 ug/L 68 40 -140
Phenanthrene 40.1 29.3 ug/L 73 40 -140
Fluorene 40.1 28.2 ug/L 70 40 -140
Naphthalene 40.1 26.2 ug/L 65 40 -140
2-Methylnaphthalene 40.1 26.0 ug/L 65 40 -140
C11-C22 Aromatics (unadjusted)681 475 M ug/L 70 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
77o- terphenyl (Surr)40 -140
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-378825/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
C19-C36 Aliphatics 321 190 M ug/L 59 40 -140 3 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 134 M ug/L 56 40 -140 0 25
1-Chlorooctadecane (Surr)M 40 -140
Surrogate
50
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-378825/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Anthracene 40.1 27.2 ug/L 68 40 -140 8 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pyrene 40.1 27.1 ug/L 68 40 -140 9 25
Benzo[g,h,i]perylene 40.0 26.9 ug/L 67 40 -140 8 25
Indeno[1,2,3-cd]pyrene 40.1 25.5 ug/L 64 40 -140 8 25
Benzo[b]fluoranthene 40.2 27.6 M ug/L 69 40 -140 9 25
Fluoranthene 40.1 27.2 ug/L 68 40 -140 9 25
Benzo[k]fluoranthene 40.1 27.2 M ug/L 68 40 -140 8 25
Acenaphthylene 40.1 27.1 ug/L 68 40 -140 4 25
Chrysene 40.2 26.2 ug/L 65 40 -140 9 25
Benzo[a]pyrene 40.2 25.9 ug/L 65 40 -140 8 25
Dibenz(a,h)anthracene 40.0 27.1 ug/L 68 40 -140 7 25
Benzo[a]anthracene 40.1 27.5 ug/L 69 40 -140 8 25
Acenaphthene 40.2 25.3 ug/L 63 40 -140 7 25
Phenanthrene 40.1 27.1 ug/L 68 40 -140 8 25
Fluorene 40.1 26.4 ug/L 66 40 -140 7 25
Naphthalene 40.1 23.9 M ug/L 60 40 -140 9 25
2-Methylnaphthalene 40.1 24.0 ug/L 60 40 -140 8 25
C11-C22 Aromatics (unadjusted)681 447 M ug/L 66 40 -140 6 25
2-Fluorobiphenyl (Surr)40 -140
Surrogate
89
LCSD LCSD
Qualifier Limits%Recovery
69o- terphenyl (Surr)40 -140
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Anthracene - RE 1.2 U M H 39.3 23.7 H ug/L 60 40 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Pyrene - RE 9.6 U M H 39.3 24.2 H ug/L 62 40 -140
Benzo[g,h,i]perylene - RE 1.2 U H 39.2 23.7 H ug/L 60 40 -140
Indeno[1,2,3-cd]pyrene - RE 1.2 U H 39.3 22.4 H ug/L 57 40 -140
Benzo[b]fluoranthene - RE 1.2 U H 39.3 24.1 H ug/L 61 40 -140
Fluoranthene - RE 0.96 U M H 39.3 24.2 H ug/L 62 40 -140
Benzo[k]fluoranthene - RE 2.9 U H 39.3 24.2 H ug/L 61 40 -140
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Acenaphthylene - RE 2.4 M H 39.3 24.3 H ug/L 56 40 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Chrysene - RE 0.96 U M H 39.4 23.4 H ug/L 60 40 -140
Benzo[a]pyrene - RE 1.2 U H 39.3 22.7 H ug/L 58 40 -140
Dibenz(a,h)anthracene - RE 0.96 U H 39.2 23.8 H ug/L 61 40 -140
Benzo[a]anthracene - RE 1.3 U H 39.3 24.1 H ug/L 61 40 -140
Acenaphthene - RE 1.2 U M H 39.3 22.2 H ug/L 56 40 -140
Phenanthrene - RE 1.2 U M H 39.3 23.7 H ug/L 60 40 -140
Fluorene - RE 1.2 U M H 39.3 22.8 H ug/L 58 40 -140
Naphthalene - RE 36 M H J1 39.3 47.3 H J1 ug/L 29 40 -140
2-Methylnaphthalene - RE 19 M H 39.3 35.2 H ug/L 41 40 -140
C11-C22 Aromatics (unadjusted)
- RE
110 M H 667 462 H ug/L 52 40 -140
2-Fluorobiphenyl (Surr) - RE 40 -140
Surrogate
86
MS MS
Qualifier Limits%Recovery
61o- terphenyl (Surr) - RE 40 -140
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
C19-C36 Aliphatics - RE 11 J M H 315 174 M H ug/L 52 40 -140
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C9-C18 Aliphatics - RE 150 M H B J1 236 223 M H J1 ug/L 30 40 -140
1-Chlorooctadecane (Surr) - RE M 40 -140
Surrogate
46
MS MS
Qualifier Limits%Recovery
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Anthracene - RE 1.2 U M H 38.9 24.9 H ug/L 64 40 -140 5 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Pyrene - RE 9.6 U M H 38.9 25.7 H ug/L 66 40 -140 6 50
Benzo[g,h,i]perylene - RE 1.2 U H 38.8 25.3 H ug/L 65 40 -140 6 50
Indeno[1,2,3-cd]pyrene - RE 1.2 U H 38.9 23.9 H ug/L 61 40 -140 7 50
Benzo[b]fluoranthene - RE 1.2 U H 38.9 25.8 M H ug/L 66 40 -140 7 50
Fluoranthene - RE 0.96 U M H 38.9 26.0 H ug/L 67 40 -140 7 50
Benzo[k]fluoranthene - RE 2.9 U H 38.9 25.8 M H ug/L 66 40 -140 7 50
Acenaphthylene - RE 2.4 M H 38.9 25.0 H ug/L 58 40 -140 3 50
Chrysene - RE 0.96 U M H 39.0 24.6 H ug/L 63 40 -140 5 50
Benzo[a]pyrene - RE 1.2 U H 38.9 24.4 H ug/L 63 40 -140 7 50
Dibenz(a,h)anthracene - RE 0.96 U H 38.8 25.5 H ug/L 66 40 -140 7 50
Benzo[a]anthracene - RE 1.3 U H 38.9 26.0 H ug/L 67 40 -140 8 50
Acenaphthene - RE 1.2 U M H 38.9 22.6 H ug/L 58 40 -140 2 50
Phenanthrene - RE 1.2 U M H 38.9 25.0 H ug/L 64 40 -140 6 50
Fluorene - RE 1.2 U M H 38.9 23.7 H ug/L 61 40 -140 4 50
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QC Sample Results
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Naphthalene - RE 36 M H J1 38.9 47.7 H J1 ug/L 30 40 -140 1 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
2-Methylnaphthalene - RE 19 M H 38.9 35.1 H ug/L 41 40 -140 0 50
C11-C22 Aromatics (unadjusted)
- RE
110 M H 660 480 M H ug/L 55 40 -140 4 50
2-Fluorobiphenyl (Surr) - RE 40 -140
Surrogate
88
MSD MSD
Qualifier Limits%Recovery
67o- terphenyl (Surr) - RE 40 -140
Client Sample ID: TW7-03-04-23Lab Sample ID: 680-234331-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
C19-C36 Aliphatics - RE 11 J M H 312 175 M H ug/L 53 40 -140 1 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics - RE 150 M H B J1 234 229 M H J1 ug/L 32 40 -140 2 50
1-Chlorooctadecane (Surr) - RE M 40 -140
Surrogate
49
MSD MSD
Qualifier Limits%Recovery
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QC Association Summary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
GC/MS VOA
Analysis Batch: 776880
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-234331-7 Trip Blank Total/NA
Water 8260DMB 680-776880/9 Method Blank Total/NA
Water 8260DLCS 680-776880/5 Lab Control Sample Total/NA
Water 8260DLCSD 680-776880/6 Lab Control Sample Dup Total/NA
Analysis Batch: 777079
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-234331-1 MW7-16-04-23 Total/NA
Water 8260D680-234331-2 308-DUP-1-04-23 Total/NA
Water 8260D680-234331-3 MW7-20-04-23 Total/NA
Water 8260D680-234331-4 MW1-04-23 Total/NA
Water 8260D680-234331-5 TW7-03-04-23 Total/NA
Water 8260D680-234331-6 MW7-22-04-23 Total/NA
Water 8260DMB 680-777079/8 Method Blank Total/NA
Water 8260DLCS 680-777079/4 Lab Control Sample Total/NA
Water 8260DLCSD 680-777079/5 Lab Control Sample Dup Total/NA
Water 8260D680-234331-5 MS TW7-03-04-23 Total/NA
Water 8260D680-234331-5 MSD TW7-03-04-23 Total/NA
GC/MS Semi VOA
Prep Batch: 777298
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C680-234331-1 MW7-16-04-23 Total/NA
Water 3520C680-234331-2 308-DUP-1-04-23 Total/NA
Water 3520C680-234331-3 MW7-20-04-23 Total/NA
Water 3520C680-234331-4 MW1-04-23 Total/NA
Water 3520C680-234331-5 TW7-03-04-23 Total/NA
Water 3520C680-234331-6 MW7-22-04-23 Total/NA
Water 3520CMB 680-777298/9-A Method Blank Total/NA
Water 3520CLCS 680-777298/10-A Lab Control Sample Total/NA
Water 3520CLCS 680-777298/13-A Lab Control Sample Total/NA
Water 3520C680-234331-5 MS TW7-03-04-23 Total/NA
Water 3520C680-234331-5 MS TW7-03-04-23 Total/NA
Water 3520C680-234331-5 MSD TW7-03-04-23 Total/NA
Water 3520C680-234331-5 MSD TW7-03-04-23 Total/NA
Analysis Batch: 778040
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 777298680-234331-1 MW7-16-04-23 Total/NA
Water 8270E 777298680-234331-2 308-DUP-1-04-23 Total/NA
Water 8270E 777298680-234331-3 MW7-20-04-23 Total/NA
Water 8270E 777298680-234331-4 MW1-04-23 Total/NA
Water 8270E 777298680-234331-5 TW7-03-04-23 Total/NA
Water 8270E 777298680-234331-6 MW7-22-04-23 Total/NA
Water 8270E 777298MB 680-777298/9-A Method Blank Total/NA
Water 8270E 777298LCS 680-777298/10-A Lab Control Sample Total/NA
Water 8270E 777298LCS 680-777298/13-A Lab Control Sample Total/NA
Water 8270E 777298680-234331-5 MS TW7-03-04-23 Total/NA
Water 8270E 777298680-234331-5 MS TW7-03-04-23 Total/NA
Water 8270E 777298680-234331-5 MSD TW7-03-04-23 Total/NA
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QC Association Summary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
GC/MS Semi VOA (Continued)
Analysis Batch: 778040 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 777298680-234331-5 MSD TW7-03-04-23 Total/NA
Prep Batch: 779620
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C680-234331-1 - RE MW7-16-04-23 Total/NA
Water 3520C680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water 3520C680-234331-4 - RE MW1-04-23 Total/NA
Water 3520C680-234331-5 - RE TW7-03-04-23 Total/NA
Water 3520C680-234331-6 - RE MW7-22-04-23 Total/NA
Water 3520CMB 680-779620/19-A Method Blank Total/NA
Water 3520CLCS 680-779620/20-A Lab Control Sample Total/NA
Water 3520CLCS 680-779620/22-A Lab Control Sample Total/NA
Water 3520CLCSD 680-779620/21-A Lab Control Sample Dup Total/NA
Water 3520CLCSD 680-779620/23-A Lab Control Sample Dup Total/NA
Analysis Batch: 780179
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 779620680-234331-1 - RE MW7-16-04-23 Total/NA
Water 8270E 779620680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water 8270E 779620680-234331-4 - RE MW1-04-23 Total/NA
Water 8270E 779620680-234331-5 - RE TW7-03-04-23 Total/NA
Water 8270E 779620680-234331-6 - RE MW7-22-04-23 Total/NA
Water 8270E 779620MB 680-779620/19-A Method Blank Total/NA
Water 8270E 779620LCS 680-779620/20-A Lab Control Sample Total/NA
Water 8270E 779620LCS 680-779620/22-A Lab Control Sample Total/NA
Water 8270E 779620LCSD 680-779620/21-A Lab Control Sample Dup Total/NA
Water 8270E 779620LCSD 680-779620/23-A Lab Control Sample Dup Total/NA
GC VOA
Analysis Batch: 374082
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH680-234331-1 MW7-16-04-23 Total/NA
Water MAVPH680-234331-2 308-DUP-1-04-23 Total/NA
Water MAVPH680-234331-3 MW7-20-04-23 Total/NA
Water MAVPH680-234331-4 MW1-04-23 Total/NA
Water MAVPH680-234331-5 TW7-03-04-23 Total/NA
Water MAVPH680-234331-6 MW7-22-04-23 Total/NA
Water MAVPHMB 410-374082/2 Method Blank Total/NA
Water MAVPHLCS 410-374082/3 Lab Control Sample Total/NA
Water MAVPHLCSD 410-374082/4 Lab Control Sample Dup Total/NA
Water MAVPH680-234331-5 MS TW7-03-04-23 Total/NA
Water MAVPH680-234331-5 MSD TW7-03-04-23 Total/NA
Analysis Batch: 375183
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA VPH680-234331-1 MW7-16-04-23 Total/NA
Water MA VPH680-234331-2 308-DUP-1-04-23 Total/NA
Water MA VPH680-234331-3 MW7-20-04-23 Total/NA
Water MA VPH680-234331-4 MW1-04-23 Total/NA
Water MA VPH680-234331-5 TW7-03-04-23 Total/NA
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QC Association Summary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
GC VOA (Continued)
Analysis Batch: 375183 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA VPH680-234331-6 MW7-22-04-23 Total/NA
GC Semi VOA
Prep Batch: 372935
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-234331-1 - DL MW7-16-04-23 Total/NA
Water 3510C680-234331-1 MW7-16-04-23 Total/NA
Water 3510C680-234331-2 308-DUP-1-04-23 Total/NA
Water 3510C680-234331-3 MW7-20-04-23 Total/NA
Water 3510C680-234331-4 MW1-04-23 Total/NA
Water 3510C680-234331-5 TW7-03-04-23 Total/NA
Water 3510C680-234331-6 MW7-22-04-23 Total/NA
Water 3510CMB 410-372935/1-B Method Blank Total/NA
Water 3510CMB 410-372935/1-C Method Blank Total/NA
Water 3510CLCS 410-372935/2-B Lab Control Sample Total/NA
Water 3510CLCS 410-372935/2-C Lab Control Sample Total/NA
Water 3510CLCSD 410-372935/3-B Lab Control Sample Dup Total/NA
Water 3510CLCSD 410-372935/3-C Lab Control Sample Dup Total/NA
Water 3510C680-234331-5 MS TW7-03-04-23 Total/NA
Water 3510C680-234331-5 MSD TW7-03-04-23 Total/NA
Cleanup Batch: 375055
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 372935680-234331-1 - DL MW7-16-04-23 Total/NA
Water 3630C 372935680-234331-1 MW7-16-04-23 Total/NA
Water 3630C 372935680-234331-1 MW7-16-04-23 Total/NA
Water 3630C 372935680-234331-2 308-DUP-1-04-23 Total/NA
Water 3630C 372935680-234331-2 308-DUP-1-04-23 Total/NA
Water 3630C 372935680-234331-3 MW7-20-04-23 Total/NA
Water 3630C 372935680-234331-3 MW7-20-04-23 Total/NA
Water 3630C 372935680-234331-4 MW1-04-23 Total/NA
Water 3630C 372935680-234331-4 MW1-04-23 Total/NA
Water 3630C 372935680-234331-5 TW7-03-04-23 Total/NA
Water 3630C 372935680-234331-5 TW7-03-04-23 Total/NA
Water 3630C 372935680-234331-6 MW7-22-04-23 Total/NA
Water 3630C 372935680-234331-6 MW7-22-04-23 Total/NA
Water 3630C 372935MB 410-372935/1-B Method Blank Total/NA
Water 3630C 372935MB 410-372935/1-C Method Blank Total/NA
Water 3630C 372935LCS 410-372935/2-B Lab Control Sample Total/NA
Water 3630C 372935LCS 410-372935/2-C Lab Control Sample Total/NA
Water 3630C 372935LCSD 410-372935/3-B Lab Control Sample Dup Total/NA
Water 3630C 372935LCSD 410-372935/3-C Lab Control Sample Dup Total/NA
Water 3630C 372935680-234331-5 MS TW7-03-04-23 Total/NA
Water 3630C 372935680-234331-5 MS TW7-03-04-23 Total/NA
Water 3630C 372935680-234331-5 MSD TW7-03-04-23 Total/NA
Water 3630C 372935680-234331-5 MSD TW7-03-04-23 Total/NA
Analysis Batch: 375340
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 375055680-234331-1 MW7-16-04-23 Total/NA
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QC Association Summary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
GC Semi VOA (Continued)
Analysis Batch: 375340 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 375055680-234331-2 308-DUP-1-04-23 Total/NA
Water MA-EPH 375055680-234331-3 MW7-20-04-23 Total/NA
Water MA-EPH 375055680-234331-4 MW1-04-23 Total/NA
Water MA-EPH 375055680-234331-5 TW7-03-04-23 Total/NA
Water MA-EPH 375055680-234331-6 MW7-22-04-23 Total/NA
Water MA-EPH 375055MB 410-372935/1-C Method Blank Total/NA
Water MA-EPH 375055LCS 410-372935/2-C Lab Control Sample Total/NA
Water MA-EPH 375055LCSD 410-372935/3-C Lab Control Sample Dup Total/NA
Water MA-EPH 375055680-234331-5 MS TW7-03-04-23 Total/NA
Water MA-EPH 375055680-234331-5 MSD TW7-03-04-23 Total/NA
Analysis Batch: 375346
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 375055680-234331-1 MW7-16-04-23 Total/NA
Water MA-EPH 375055680-234331-2 308-DUP-1-04-23 Total/NA
Water MA-EPH 375055680-234331-3 MW7-20-04-23 Total/NA
Water MA-EPH 375055680-234331-4 MW1-04-23 Total/NA
Water MA-EPH 375055680-234331-5 TW7-03-04-23 Total/NA
Water MA-EPH 375055680-234331-6 MW7-22-04-23 Total/NA
Water MA-EPH 375055MB 410-372935/1-B Method Blank Total/NA
Water MA-EPH 375055LCS 410-372935/2-B Lab Control Sample Total/NA
Water MA-EPH 375055LCSD 410-372935/3-B Lab Control Sample Dup Total/NA
Water MA-EPH 375055680-234331-5 MS TW7-03-04-23 Total/NA
Water MA-EPH 375055680-234331-5 MSD TW7-03-04-23 Total/NA
Analysis Batch: 375993
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 375055680-234331-1 - DL MW7-16-04-23 Total/NA
Prep Batch: 378825
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water 3510C680-234331-3 - RE MW7-20-04-23 Total/NA
Water 3510C680-234331-4 - RE MW1-04-23 Total/NA
Water 3510C680-234331-5 - RE TW7-03-04-23 Total/NA
Water 3510C680-234331-6 - RE MW7-22-04-23 Total/NA
Water 3510CMB 410-378825/1-B Method Blank Total/NA
Water 3510CMB 410-378825/1-C Method Blank Total/NA
Water 3510CLCS 410-378825/2-B Lab Control Sample Total/NA
Water 3510CLCS 410-378825/2-C Lab Control Sample Total/NA
Water 3510CLCSD 410-378825/3-B Lab Control Sample Dup Total/NA
Water 3510CLCSD 410-378825/3-C Lab Control Sample Dup Total/NA
Water 3510C680-234331-5 MS - RE TW7-03-04-23 Total/NA
Water 3510C680-234331-5 MSD - RE TW7-03-04-23 Total/NA
Cleanup Batch: 381341
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 378825680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water 3630C 378825680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water 3630C 378825680-234331-3 - RE MW7-20-04-23 Total/NA
Water 3630C 378825680-234331-3 - RE MW7-20-04-23 Total/NA
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QC Association Summary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
GC Semi VOA (Continued)
Cleanup Batch: 381341 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 378825680-234331-4 - RE MW1-04-23 Total/NA
Water 3630C 378825680-234331-4 - RE MW1-04-23 Total/NA
Water 3630C 378825680-234331-5 - RE TW7-03-04-23 Total/NA
Water 3630C 378825680-234331-5 - RE TW7-03-04-23 Total/NA
Water 3630C 378825680-234331-6 - RE MW7-22-04-23 Total/NA
Water 3630C 378825680-234331-6 - RE MW7-22-04-23 Total/NA
Water 3630C 378825MB 410-378825/1-B Method Blank Total/NA
Water 3630C 378825MB 410-378825/1-C Method Blank Total/NA
Water 3630C 378825LCS 410-378825/2-B Lab Control Sample Total/NA
Water 3630C 378825LCS 410-378825/2-C Lab Control Sample Total/NA
Water 3630C 378825LCSD 410-378825/3-B Lab Control Sample Dup Total/NA
Water 3630C 378825LCSD 410-378825/3-C Lab Control Sample Dup Total/NA
Water 3630C 378825680-234331-5 MS - RE TW7-03-04-23 Total/NA
Water 3630C 378825680-234331-5 MS - RE TW7-03-04-23 Total/NA
Water 3630C 378825680-234331-5 MSD - RE TW7-03-04-23 Total/NA
Water 3630C 378825680-234331-5 MSD - RE TW7-03-04-23 Total/NA
Analysis Batch: 381590
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 381341680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water MA-EPH 381341680-234331-3 - RE MW7-20-04-23 Total/NA
Water MA-EPH 381341680-234331-4 - RE MW1-04-23 Total/NA
Water MA-EPH 381341680-234331-5 - RE TW7-03-04-23 Total/NA
Water MA-EPH 381341680-234331-6 - RE MW7-22-04-23 Total/NA
Water MA-EPH 381341MB 410-378825/1-C Method Blank Total/NA
Water MA-EPH 381341LCS 410-378825/2-C Lab Control Sample Total/NA
Water MA-EPH 381341LCSD 410-378825/3-C Lab Control Sample Dup Total/NA
Water MA-EPH 381341680-234331-5 MS - RE TW7-03-04-23 Total/NA
Water MA-EPH 381341680-234331-5 MSD - RE TW7-03-04-23 Total/NA
Analysis Batch: 381594
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 381341680-234331-2 - RE 308-DUP-1-04-23 Total/NA
Water MA-EPH 381341680-234331-3 - RE MW7-20-04-23 Total/NA
Water MA-EPH 381341680-234331-4 - RE MW1-04-23 Total/NA
Water MA-EPH 381341680-234331-5 - RE TW7-03-04-23 Total/NA
Water MA-EPH 381341680-234331-6 - RE MW7-22-04-23 Total/NA
Water MA-EPH 381341MB 410-378825/1-B Method Blank Total/NA
Water MA-EPH 381341LCS 410-378825/2-B Lab Control Sample Total/NA
Water MA-EPH 381341LCSD 410-378825/3-B Lab Control Sample Dup Total/NA
Water MA-EPH 381341680-234331-5 MS - RE TW7-03-04-23 Total/NA
Water MA-EPH 381341680-234331-5 MSD - RE TW7-03-04-23 Total/NA
Analysis Batch: 382017
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH680-234331-1 MW7-16-04-23 Total/NA
Water MA-EPH680-234331-2 308-DUP-1-04-23 Total/NA
Water MA-EPH680-234331-3 MW7-20-04-23 Total/NA
Water MA-EPH680-234331-4 MW1-04-23 Total/NA
Water MA-EPH680-234331-5 TW7-03-04-23 Total/NA
Water MA-EPH680-234331-6 MW7-22-04-23 Total/NA
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Client Sample ID: MW7-16-04-23 Lab Sample ID: 680-234331-1
Matrix: WaterDate Collected: 04/28/23 16:05
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/05/23 12:101 EET SAV777079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
Prep 3520C 777298 05/05/23 21:00 IR EET SAVTotal/NA 946.3 mL 1 mL
Analysis 8270E 1 778040 05/10/23 21:07 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 3520C RE 779620 05/20/23 21:30 IR EET SAVTotal/NA 980 mL 1 mL
Analysis 8270E RE 1 780179 05/24/23 22:05 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 12:36 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 987.6 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375340 05/13/23 11:50 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C DL 372935 05/08/23 09:17 A2VL ELLETotal/NA 987.6 mL 1 mL
Cleanup 3630C DL 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH DL 2 375993 05/15/23 19:15 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 987.6 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375346 05/13/23 13:20 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:55 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: 308-DUP-1-04-23 Lab Sample ID: 680-234331-2
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/05/23 09:061 EET SAV777079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
Prep 3520C 777298 05/05/23 21:00 IR EET SAVTotal/NA 1035.8 mL 1 mL
Analysis 8270E 1 778040 05/10/23 21:29 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 3520C RE 779620 05/20/23 21:30 IR EET SAVTotal/NA 995.4 mL 1 mL
Analysis 8270E RE 1 780179 05/24/23 22:27 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 13:17 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Client Sample ID: 308-DUP-1-04-23 Lab Sample ID: 680-234331-2
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Prep 3510C A2VL05/23/23 09:00RE ELLE378825
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 983.6 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 06:37 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 983.6 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 07:00 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 979.2 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375340 05/13/23 12:12 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 979.2 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375346 05/13/23 13:42 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:55 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: MW7-20-04-23 Lab Sample ID: 680-234331-3
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/05/23 09:291 EET SAV777079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
Prep 3520C 777298 05/05/23 21:00 IR EET SAVTotal/NA 1005 mL 1 mL
Analysis 8270E 1 778040 05/10/23 21:51 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 13:58 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1011.1 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 07:00 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1011.1 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 07:22 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 1049 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375340 05/13/23 12:35 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Client Sample ID: MW7-20-04-23 Lab Sample ID: 680-234331-3
Matrix: WaterDate Collected: 04/28/23 09:40
Date Received: 05/01/23 11:30
Prep 3510C A2VL05/08/23 09:17 ELLE372935
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1049 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375346 05/13/23 14:05 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:55 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: MW1-04-23 Lab Sample ID: 680-234331-4
Matrix: WaterDate Collected: 04/28/23 12:05
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/05/23 09:521 EET SAV777079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
Prep 3520C 777298 05/05/23 21:00 IR EET SAVTotal/NA 1019.8 mL 1 mL
Analysis 8270E 1 778040 05/10/23 22:13 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 3520C RE 779620 05/20/23 21:30 IR EET SAVTotal/NA 1056.3 mL 1 mL
Analysis 8270E RE 1 780179 05/24/23 22:49 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 14:39 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1052.6 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 07:22 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1052.6 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 07:45 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 996.5 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375340 05/13/23 12:57 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 996.5 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375346 05/13/23 14:27 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:55 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Client Sample ID: TW7-03-04-23 Lab Sample ID: 680-234331-5
Matrix: WaterDate Collected: 04/28/23 11:05
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/05/23 13:502 EET SAV777079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
Prep 3520C 777298 05/05/23 21:00 IR EET SAVTotal/NA 1035 mL 1 mL
Analysis 8270E 1 778040 05/10/23 20:46 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 3520C RE 779620 05/20/23 21:30 IR EET SAVTotal/NA 1043.1 mL 1 mL
Analysis 8270E RE 1 780179 05/24/23 23:11 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 2 374082 05/10/23 15:21 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1040.3 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 03:59 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1040.3 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 04:22 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 1044.8 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375340 05/13/23 13:20 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 1044.8 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375346 05/13/23 14:49 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:55 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: MW7-22-04-23 Lab Sample ID: 680-234331-6
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/05/23 10:391 EET SAV777079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
Prep 3520C 777298 05/05/23 21:00 IR EET SAVTotal/NA 1046.7 mL 1 mL
Analysis 8270E 1 778040 05/10/23 22:34 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 3520C RE 779620 05/20/23 21:30 IR EET SAVTotal/NA 1029 mL 1 mL
Analysis 8270E RE 1 780179 05/24/23 23:33 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Client Sample ID: MW7-22-04-23 Lab Sample ID: 680-234331-6
Matrix: WaterDate Collected: 04/28/23 14:50
Date Received: 05/01/23 11:30
Analysis MAVPH X87505/10/23 18:051 ELLE374082
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 988.2 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 07:45 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 988.2 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 08:07 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 956.9 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375340 05/13/23 14:27 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 372935 05/08/23 09:17 A2VL ELLETotal/NA 956.9 mL 1 mL
Cleanup 3630C 375055 05/12/23 07:02 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 375346 05/13/23 15:57 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:55 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: Trip Blank Lab Sample ID: 680-234331-7
Matrix: WaterDate Collected: 04/28/23 00:00
Date Received: 05/01/23 11:30
Analysis 8260D P1C05/04/23 15:511 EET SAV776880
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSAA
¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: Sure-BioChem Laboratories LLC Job ID: 680-234331-1
Project/Site: Ft.Bragg NC (FTBR-308)
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
ANAB Dept. of Defense ELAP L2463 09-22-24
North Carolina (WW/SW)State 269 12-31-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
A2LA Dept. of Defense ELAP 0001.01 11-30-24
North Carolina (WW/SW)State 521 12-31-23
Eurofins Savannah
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Method Summary
Job ID: 680-234331-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft.Bragg NC (FTBR-308)
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds (GC/MS)EET SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)EET SAV
MA DEPMA VPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)ELLE
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)ELLE
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)ELLE
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)ELLE
SW8463520CLiquid-Liquid Extraction (Continuous)EET SAV
SW8463630CSilica Gel Cleanup ELLE
SW8465030CPurge and Trap EET SAV
SW8465030CPurge and Trap ELLE
Protocol References:
MA DEP = Massachusetts Department Of Environmental Protection
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Sure-BioChem Laboratories LLC Job Number: 680-234331-1
Login Number: 234331
Question Answer Comment
Creator: Johnson, Corey M
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.IDs on containers do not match the COC.
Logged in per COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Sure-BioChem Laboratories LLC Job Number: 680-234331-1
Login Number: 234331
Question Answer Comment
Creator: Ballard, Megan
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 05/03/23 12:19 PMList Number: 2
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
FalseThere are no discrepancies between the containers received and the COC.Refer to Job Narrative for details.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Savannah
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ANALYTICAL REPORT
PREPARED FOR
Attn: Ms. Kellie Arstino
Sure-BioChem Laboratories LLC
1000 Atlantic Ave
Camden, New Jersey 08104
Generated 6/6/2023 5:17:30 PM
JOB DESCRIPTION
Ft. Bragg NC (FTBR-308)
JOB NUMBER
680-234374-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
6/6/2023 5:17:30 PM
Authorized for release by
Jerry Lanier, Project Manager I
[e-mail]
[phone]
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Definitions/Glossary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Qualifiers
GC/MS VOA
Qualifier Description
D The reported value is from a dilution.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC/MS Semi VOA
Qualifier Description
B Blank contamination: The analyte was detected above one-half the reporting limit in an associated blank.
Qualifier
H Sample was prepped or analyzed beyond the specified holding time. This does not meet regulatory requirements.
J Estimated: The analyte was positively identified; the quantitation is an estimation
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC VOA
Qualifier Description
D The reported value is from a dilution.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC Semi VOA
Qualifier Description
B Blank contamination: The analyte was detected above one-half the reporting limit in an associated blank.
Qualifier
D The reported value is from a dilution.
H Sample was prepped or analyzed beyond the specified holding time. This does not meet regulatory requirements.
J Estimated: The analyte was positively identified; the quantitation is an estimation
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
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Definitions/Glossary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Glossary (Continued)
These commonly used abbreviations may or may not be present in this report.
MQL Method Quantitation Limit
Abbreviation
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Sample Summary
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID Client Sample ID Matrix Collected Received
680-234374-1 RW-18-05-23 Water 05/01/23 09:55 05/02/23 10:30
680-234374-2 RW-16-05-23 Water 05/01/23 11:30 05/02/23 10:30
680-234374-3 RW-17-05-23 Water 05/01/23 09:50 05/02/23 10:30
680-234374-4 RW-08-05-23 Water 05/01/23 11:10 05/02/23 10:30
680-234374-5 MW7-18-05-23 Water 05/01/23 13:35 05/02/23 10:30
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Case Narrative
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Job ID: 680-234374-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-234374-1
Receipt
The samples were received on 5/2/2023 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperatures of the 3 coolers at receipt time were 0.7°C, 1.9°C and 3.2°C
Receipt Exceptions
The following samples were received at the laboratory outside the required temperature criteria: RW-18-05-23 (680-234374-1), RW-16-05-23
(680-234374-2), RW-17-05-23 (680-234374-3), RW-08-05-23 (680-234374-4) and MW7-18-05-23 (680-234374-5). This does not meet
regulatory requirements. The client was contacted regarding this issue, and the laboratory was instructed to proceed with analysis.
GC/MS VOA
Method 8260D_DOD5: Surrogate recovery for the following samples were outside control limits: RW-18-05-23 (680-234374-1), RW-16-05-23
(680-234374-2), RW-17-05-23 (680-234374-3) and MW7-18-05-23 (680-234374-5). Evidence of matrix interference is present; therefore,
re-extraction and/or re-analysis was not performed.
Method 8260D_DOD5: Surrogate recovery for the following sample was outside control limits: RW-08-05-23 (680-234374-4). Evidence of
matrix interferences is not obvious. A reanalysis was attempted for 680-234580-41 but resulted in a mechanical failure on the instrument so
only the original run was reported.
Method 8260D_DOD5: Surrogate recovery for the following samples were outside control limits: RW-17-05-23 (680-234374-3) and
MW7-18-05-23 (680-234374-5). Evidence of matrix interference due to high target analytes is present; therefore, re-extraction and/or
re-analysis was not performed.
Method 8260D_DOD5: Surrogate recovery for the following sample was outside control limits: RW-08-05-23 (680-234374-4). Evidence of
matrix interferences is not obvious.
Method 8260D_DOD5: The surrogate recovery for the blank associated with analytical batch 680-778627 was outside the upper control limits.
Method 8260D_DOD5: The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for analytical batch
680-778568 recovered outside control limits for the following analyte(s): Chloroethane. Chloroethane has been identified as a poor
performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed. These results have been
reported and qualified.
Method 8260D_DOD5: The following samples were diluted to bring the concentration of target analytes within the calibration range:
RW-17-05-23 (680-234374-3) and MW7-18-05-23 (680-234374-5). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E_DOD5: Surrogate recovery for the following sample was outside control limits: RW-08-05-23 (680-234374-4). Re-extraction
and/or re-analysis was performed and surrogate recovery was outside control limits.
Method 8270E_DOD5: The method blank for preparation batch 680-777555 and analytical batch 680-777551 contained Bis(2-ethylhexyl)
phthalate above the method detection limit (MDL). Associated samples were not re-analyzed because results were less than the reporting
limit (RL) OR practical quantitation limit (PQL).
Method 8270E_DOD5: The laboratory control sample (LCS) for preparation batch 680-777555 and analytical batch 680-777551 recovered
outside control limits for the following analytes: 4,6-Dinitro-2-methylphenol and 2,4-Dinitrophenol. These analytes were biased high in the
LCS and were not detected in the associated samples; therefore, the data has been reported.
Method 8270E_DOD5: A portion of the following samples listed was used for analysis, rather than testing the entire sample amount in the
original container, due to the sample container was not the appropriate size: RW-08-05-23 (680-234374-4). As such, the required solvent
rinse of the original container could not be performed.
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Case Narrative
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Job ID: 680-234374-1 (Continued)
Laboratory: Eurofins Savannah (Continued)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: Surrogate recovery for the following samples were outside control limits: RW-18-05-23 (680-234374-1), RW-16-05-23
(680-234374-2), RW-17-05-23 (680-234374-3), RW-08-05-23 (680-234374-4) and MW7-18-05-23 (680-234374-5). Evidence of matrix
interference is confirmed by reanalysis.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH_DOD: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS and LCSD is <1%. The method requirement
for breakthrough is <5%. RW-18-05-23 (680-234374-1), RW-16-05-23 (680-234374-2), RW-17-05-23 (680-234374-3), RW-08-05-23
(680-234374-4) and MW7-18-05-23 (680-234374-5)
Method MAEPH_DOD: The method blank for preparation batch 410-375040 and 410-376670 and analytical batch 410-377003 contained
C9-C18 Aliphatics above the limit of detection (LOD). The following samples were not re-extracted and/or re-analyzed because results were
greater than 10X the value found in the method blank: RW-17-05-23 (680-234374-3) and MW7-18-05-23 (680-234374-5).
Method MAEPH_DOD: For analytical batch 410-381594, the breakthrough for naphthalene and 2-methylnaphthalene is <1% in the LCS. The
breakthrough for naphthalene is 2% and the breakthrough for 2-methylnaphthalene is 1% in the LCSD. The method requirement for
breakthrough is <5%. RW-18-05-23 (680-234374-1)
Method MAEPH_DOD: C9-C18 Aliphatics was detected above the reporting limit (RL) in the method blank associated with preparation batch
410-375040 and 410-376670 and analytical batch 410-377003 as well as in the following samples: RW-18-05-23 (680-234374-1),
RW-16-05-23 (680-234374-2) and RW-08-05-23 (680-234374-4). All affected samples were re-extracted and re-analyzed outside of holding
time and the method blank again had detections. Both sets of data have been reported.
Method MAEPH_DOD: For analytical batch 410-381594, the breakthrough for naphthalene and 2-methylnaphthalene is <1% in the LCS. The
breakthrough for naphthalene is 2% and the breakthrough for 2-methylnaphthalene is 1% in the LCSD. The method requirement for
breakthrough is <5%. RW-16-05-23 (680-234374-2) and RW-08-05-23 (680-234374-4)
Method MAEPH_DOD: Surrogate recovery for the following sample was outside control limits: RW-08-05-23 (680-234374-4). Re-extraction
and/or re-analysis was performed and surrogate recovery was outside control limits. Both trials are reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-1Client Sample ID: RW-18-05-23
Matrix: WaterDate Collected: 05/01/23 09:55
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U M 25 3.7 ug/L 05/14/23 16:19 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
2.0 0.27 ug/L 05/14/23 16:19 10.66 JBenzene
2.5 0.59 ug/L 05/14/23 16:19 12.0 UBromoform
20 3.7 ug/L 05/14/23 16:19 110 UBromomethane
25 6.4 ug/L 05/14/23 16:19 120 U M2-Butanone (MEK)
2.0 0.43 ug/L 05/14/23 16:19 11.0 U QCarbon disulfide
2.0 0.30 ug/L 05/14/23 16:19 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/14/23 16:19 10.50 UChlorobenzene
2.0 0.39 ug/L 05/14/23 16:19 11.0 UChlorodibromomethane
20 4.6 ug/L 05/14/23 16:19 110 U QChloroethane
2.0 0.27 ug/L 05/14/23 16:19 11.0 U MChloroform
2.5 0.54 ug/L 05/14/23 16:19 12.0 U QChloromethane
2.0 0.25 ug/L 05/14/23 16:19 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 05/14/23 16:19 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 05/14/23 16:19 125 QCyclohexane
10 1.8 ug/L 05/14/23 16:19 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/14/23 16:19 11.0 U1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 05/14/23 16:19 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/14/23 16:19 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/14/23 16:19 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 05/14/23 16:19 11.0 UDichlorobromomethane
2.0 0.36 ug/L 05/14/23 16:19 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/14/23 16:19 11.0 U M1,1-Dichloroethane
2.0 0.25 ug/L 05/14/23 16:19 11.0 U M Q1,2-Dichloroethane
2.0 0.33 ug/L 05/15/23 15:08 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/14/23 16:19 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 05/14/23 16:19 16.3Ethylbenzene
20 3.2 ug/L 05/14/23 16:19 110 U2-Hexanone
2.0 0.26 ug/L 05/14/23 16:19 111Isopropylbenzene
20 3.2 ug/L 05/14/23 16:19 110 UMethyl acetate
2.0 0.33 ug/L 05/14/23 16:19 145Methylcyclohexane
20 3.2 ug/L 05/14/23 16:19 110 U QMethylene Chloride
20 2.7 ug/L 05/14/23 16:19 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/14/23 16:19 12.0 UMethyl tert-butyl ether
2.0 0.27 ug/L 05/14/23 16:19 11.0 U MStyrene
2.0 0.40 ug/L 05/14/23 16:19 11.0 U M1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/14/23 16:19 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/14/23 16:19 12.5Toluene
2.0 0.34 ug/L 05/14/23 16:19 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 05/14/23 16:19 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 05/14/23 16:19 12.0 U M1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/14/23 16:19 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/14/23 16:19 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/14/23 16:19 10.50 UTrichloroethene
2.0 0.33 ug/L 05/14/23 16:19 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 05/14/23 16:19 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 05/14/23 16:19 11.0 U QVinyl chloride
2.0 0.49 ug/L 05/14/23 16:19 133Xylenes, Total
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-1Client Sample ID: RW-18-05-23
Matrix: WaterDate Collected: 05/01/23 09:55
Date Received: 05/02/23 10:30
4-Bromofluorobenzene (Surr)104 85-114 05/14/23 16:19 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr)105 05/15/23 15:08 185-114
Dibromofluoromethane (Surr)81 05/14/23 16:19 180-119
Dibromofluoromethane (Surr)104 05/15/23 15:08 180-119
1,2-Dichloroethane-d4 (Surr)78 Q 05/14/23 16:19 181-118
1,2-Dichloroethane-d4 (Surr)88 05/15/23 15:08 181-118
Toluene-d8 (Surr)88 Q 05/14/23 16:19 189-112
Toluene-d8 (Surr)106 05/15/23 15:08 189-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
10 U 20 4.4 ug/L 05/03/23 18:10 05/08/23 17:30 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:30 110 UAcenaphthylene
10 2.2 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 U MAcetophenone
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:30 110 UAnthracene
10 2.2 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 UAtrazine
20 4.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 U MBenzaldehyde
20 4.2 ug/L 05/03/23 18:10 05/08/23 17:30 110 UBenzo[a]anthracene
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 UBenzo[a]pyrene
20 3.1 ug/L 05/03/23 18:10 05/08/23 17:30 110 UBenzo[b]fluoranthene
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:30 110 UBenzo[g,h,i]perylene
20 2.9 ug/L 05/03/23 18:10 05/08/23 17:30 110 U QBenzo[k]fluoranthene
20 4.6 ug/L 05/03/23 18:10 05/08/23 17:30 110 U1,1'-Biphenyl
10 1.8 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UBis(2-chloroethoxy)methane
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:30 110 U MBis(2-chloroethyl)ether
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:30 16.4 J BBis(2-ethylhexyl) phthalate
20 4.7 ug/L 05/03/23 18:10 05/08/23 17:30 110 U4-Bromophenyl phenyl ether
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 UButyl benzyl phthalate
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 UCaprolactam
10 1.8 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UCarbazole
10 1.0 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 U Q4-Chloroaniline
20 2.5 ug/L 05/03/23 18:10 05/08/23 17:30 110 U4-Chloro-3-methylphenol
20 4.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2-Chloronaphthalene
20 3.2 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2-Chlorophenol
20 5.3 ug/L 05/03/23 18:10 05/08/23 17:30 112 U4-Chlorophenyl phenyl ether
20 3.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 UChrysene
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:30 110 UDibenz(a,h)anthracene
10 1.9 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UDibenzofuran
50 10 ug/L 05/03/23 18:10 05/08/23 17:30 120 U3,3'-Dichlorobenzidine
20 3.7 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2,4-Dichlorophenol
10 2.2 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 UDiethyl phthalate
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2,4-Dimethylphenol
10 2.1 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 UDimethyl phthalate
10 2.3 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 UDi-n-butyl phthalate
50 5.3 ug/L 05/03/23 18:10 05/08/23 17:30 120 U Q4,6-Dinitro-2-methylphenol
50 16 ug/L 05/03/23 18:10 05/08/23 17:30 140 U Q2,4-Dinitrophenol
10 2.3 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 U M2,4-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2,6-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:30 110 U MDi-n-octyl phthalate
10 1.6 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UFluoranthene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-1Client Sample ID: RW-18-05-23
Matrix: WaterDate Collected: 05/01/23 09:55
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 3.4 ug/L 05/03/23 18:10 05/08/23 17:30 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Fluorene
10 1.6 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UHexachlorobenzene
20 4.0 ug/L 05/03/23 18:10 05/08/23 17:30 110 UHexachlorobutadiene
20 3.5 ug/L 05/03/23 18:10 05/08/23 17:30 110 UHexachlorocyclopentadiene
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:30 110 UHexachloroethane
20 4.3 ug/L 05/03/23 18:10 05/08/23 17:30 110 UIndeno[1,2,3-cd]pyrene
10 2.0 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UIsophorone
20 4.6 ug/L 05/03/23 18:10 05/08/23 17:30 1272-Methylnaphthalene
10 1.8 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 U2-Methylphenol
10 1.4 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 U3 & 4 Methylphenol
20 3.5 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 JNaphthalene
20 2.9 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 17:30 110 U3-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 17:30 110 U4-Nitroaniline
20 3.5 ug/L 05/03/23 18:10 05/08/23 17:30 110 UNitrobenzene
20 3.9 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2-Nitrophenol
50 8.1 ug/L 05/03/23 18:10 05/08/23 17:30 120 U4-Nitrophenol
10 2.4 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 UN-Nitrosodi-n-propylamine
20 2.9 ug/L 05/03/23 18:10 05/08/23 17:30 110 UN-Nitrosodiphenylamine
20 3.1 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2,2'-oxybis[1-chloropropane]
50 9.9 ug/L 05/03/23 18:10 05/08/23 17:30 120 UPentachlorophenol
20 4.3 ug/L 05/03/23 18:10 05/08/23 17:30 110 UPhenanthrene
10 1.5 ug/L 05/03/23 18:10 05/08/23 17:30 14.0 UPhenol
20 3.7 ug/L 05/03/23 18:10 05/08/23 17:30 110 UPyrene
20 3.3 ug/L 05/03/23 18:10 05/08/23 17:30 110 U2,4,5-Trichlorophenol
20 2.2 ug/L 05/03/23 18:10 05/08/23 17:30 15.0 U2,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)66 44-119 05/03/23 18:10 05/08/23 17:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)27 05/03/23 18:10 05/08/23 17:30 119-119
Nitrobenzene-d5 (Surr)57 05/03/23 18:10 05/08/23 17:30 144-120
Phenol-d5 (Surr)18 05/03/23 18:10 05/08/23 17:30 110-130
Terphenyl-d14 (Surr)103 Q 05/03/23 18:10 05/08/23 17:30 150-134
2,4,6-Tribromophenol (Surr)96 Q 05/03/23 18:10 05/08/23 17:30 143-140
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
1900 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
1.0 J M 5.0 1.0 ug/L 05/10/23 20:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 20:29 1580 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 20:29 1770 MC9-C10 Aromatics
5.0 1.0 ug/L 05/10/23 20:29 16.2 MEthylbenzene
5.0 1.0 ug/L 05/10/23 20:29 12.6 J MMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 20:29 18.0 MNaphthalene
5.0 1.0 ug/L 05/10/23 20:29 12.9 J MToluene
10 2.5 ug/L 05/10/23 20:29 122 Mm-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 20:29 17.8 Mo-Xylene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-1Client Sample ID: RW-18-05-23
Matrix: WaterDate Collected: 05/01/23 09:55
Date Received: 05/02/23 10:30
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
580 100 25 ug/L 05/10/23 20:29 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)413 Q 70-130 05/10/23 20:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)231 M Q 05/10/23 20:29 170-130
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) - DL
LOQ DL
1300 D M 500 130 ug/L 05/11/23 21:59 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C9-C12 Aliphatics
500 130 ug/L 05/11/23 21:59 5580 DC9-C12 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)151 M Q 70-130 05/11/23 21:59 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)110 05/11/23 21:59 570-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U M 2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:56 1390Total EPH
12 5.0 ug/L 05/12/23 08:50 05/17/23 23:11 110 UPyrene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 UBenzo[g,h,i]perylene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 UBenzo[b]fluoranthene
2.0 0.50 ug/L 05/12/23 08:50 05/17/23 23:11 11.0 UFluoranthene
4.0 1.5 ug/L 05/12/23 08:50 05/17/23 23:11 13.0 UBenzo[k]fluoranthene
2.0 0.70 ug/L 05/12/23 08:50 05/17/23 23:11 14.9 MAcenaphthylene
2.0 0.50 ug/L 05/12/23 08:50 05/17/23 23:11 11.0 UChrysene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 UBenzo[a]pyrene
2.0 0.50 ug/L 05/12/23 08:50 05/17/23 23:11 11.0 UDibenz(a,h)anthracene
2.0 0.70 ug/L 05/12/23 08:50 05/17/23 23:11 11.4 UBenzo[a]anthracene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 U MAcenaphthene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 U MPhenanthrene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 11.2 U MFluorene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 13.6 MNaphthalene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:11 121 M2-Methylnaphthalene
40 10 ug/L 05/12/23 08:50 05/17/23 23:11 1140 MC11-C22 Aromatics (unadjusted)
40 10 ug/L 05/12/23 08:50 05/17/23 23:11 1100C11-C22 Aromatics (Adjusted)
50 10 ug/L 05/12/23 08:50 05/17/23 23:11 174 MC19-C36 Aliphatics
30 10 ug/L 05/12/23 08:50 05/17/23 23:11 1180 M B QC9-C18 Aliphatics
1-Chlorooctadecane (Surr)68 40-140 05/12/23 08:50 05/17/23 23:11 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)54 05/12/23 08:50 05/17/23 23:11 140-140
o- terphenyl (Surr)49 05/12/23 08:50 05/17/23 23:11 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U M H 2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
12 5.0 ug/L 05/23/23 09:00 06/01/23 08:07 19.9 U M HPyrene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 11.2 U HBenzo[g,h,i]perylene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 11.2 U HIndeno[1,2,3-cd]pyrene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-1Client Sample ID: RW-18-05-23
Matrix: WaterDate Collected: 05/01/23 09:55
Date Received: 05/02/23 10:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
1.2 U H 2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzo[b]fluoranthene
2.0 0.50 ug/L 05/23/23 09:00 06/01/23 08:07 10.99 U M HFluoranthene
4.0 1.5 ug/L 05/23/23 09:00 06/01/23 08:07 13.0 U HBenzo[k]fluoranthene
2.0 0.69 ug/L 05/23/23 09:00 06/01/23 08:07 14.2 M HAcenaphthylene
2.0 0.50 ug/L 05/23/23 09:00 06/01/23 08:07 10.99 U HChrysene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 11.2 U HBenzo[a]pyrene
2.0 0.50 ug/L 05/23/23 09:00 06/01/23 08:07 10.99 U HDibenz(a,h)anthracene
2.0 0.69 ug/L 05/23/23 09:00 06/01/23 08:07 11.4 U HBenzo[a]anthracene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 11.2 U M HAcenaphthene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 11.2 U M HPhenanthrene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 11.2 U M HFluorene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 17.5 M HNaphthalene
2.0 0.60 ug/L 05/23/23 09:00 06/01/23 08:07 128 M H2-Methylnaphthalene
40 9.9 ug/L 05/23/23 09:00 06/01/23 08:07 1160 M HC11-C22 Aromatics (unadjusted)
40 9.9 ug/L 05/23/23 09:00 06/01/23 08:07 1110 HC11-C22 Aromatics (Adjusted)
50 9.9 ug/L 05/23/23 09:00 06/01/23 08:30 120 U M HC19-C36 Aliphatics
30 9.9 ug/L 05/23/23 09:00 06/01/23 08:30 1110 H BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)46 M 40-140 05/23/23 09:00 06/01/23 08:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)91 M 05/23/23 09:00 06/01/23 08:07 140-140
o- terphenyl (Surr)62 M 05/23/23 09:00 06/01/23 08:07 140-140
Lab Sample ID: 680-234374-2Client Sample ID: RW-16-05-23
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U M 25 3.7 ug/L 05/14/23 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
2.0 0.27 ug/L 05/14/23 16:38 18.7Benzene
2.5 0.59 ug/L 05/14/23 16:38 12.0 UBromoform
20 3.7 ug/L 05/14/23 16:38 110 UBromomethane
25 6.4 ug/L 05/14/23 16:38 120 U2-Butanone (MEK)
2.0 0.43 ug/L 05/14/23 16:38 11.0 U QCarbon disulfide
2.0 0.30 ug/L 05/14/23 16:38 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/14/23 16:38 10.50 UChlorobenzene
2.0 0.39 ug/L 05/14/23 16:38 11.0 UChlorodibromomethane
20 4.6 ug/L 05/14/23 16:38 110 U QChloroethane
2.0 0.27 ug/L 05/14/23 16:38 11.0 U MChloroform
2.5 0.54 ug/L 05/14/23 16:38 12.0 U M QChloromethane
2.0 0.25 ug/L 05/14/23 16:38 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 05/14/23 16:38 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 05/14/23 16:38 176 QCyclohexane
10 1.8 ug/L 05/14/23 16:38 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/14/23 16:38 11.0 U1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 05/14/23 16:38 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/14/23 16:38 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/14/23 16:38 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 05/14/23 16:38 11.0 UDichlorobromomethane
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-2Client Sample ID: RW-16-05-23
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U 2.0 0.36 ug/L 05/14/23 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Dichlorodifluoromethane
2.0 0.33 ug/L 05/14/23 16:38 11.0 U M1,1-Dichloroethane
2.0 0.25 ug/L 05/14/23 16:38 11.0 U M Q1,2-Dichloroethane
1.0 0.22 ug/L 05/14/23 16:38 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 05/14/23 16:38 161Ethylbenzene
20 3.2 ug/L 05/14/23 16:38 110 U M2-Hexanone
2.0 0.26 ug/L 05/14/23 16:38 116Isopropylbenzene
20 3.2 ug/L 05/14/23 16:38 110 UMethyl acetate
2.0 0.33 ug/L 05/14/23 16:38 146Methylcyclohexane
20 3.2 ug/L 05/14/23 16:38 110 U QMethylene Chloride
20 2.7 ug/L 05/14/23 16:38 110 U4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/14/23 16:38 12.0 UMethyl tert-butyl ether
2.0 0.27 ug/L 05/14/23 16:38 11.0 U MStyrene
2.0 0.40 ug/L 05/14/23 16:38 11.0 U M1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/14/23 16:38 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/14/23 16:38 14.7Toluene
2.0 0.34 ug/L 05/14/23 16:38 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 05/14/23 16:38 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 05/14/23 16:38 12.0 U M1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/14/23 16:38 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/14/23 16:38 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/14/23 16:38 10.50 UTrichloroethene
2.0 0.33 ug/L 05/14/23 16:38 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 05/14/23 16:38 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 05/14/23 16:38 11.0 U QVinyl chloride
4-Bromofluorobenzene (Surr)106 85-114 05/14/23 16:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)80 05/14/23 16:38 180-119
1,2-Dichloroethane-d4 (Surr)78 Q 05/14/23 16:38 181-118
Toluene-d8 (Surr)88 Q 05/14/23 16:38 189-112
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) - DL
LOQ DL
5.0 U 10 1.7 ug/L 05/15/23 20:23 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
1,1-Dichloroethene
10 2.5 ug/L 05/15/23 20:23 5360 DXylenes, Total
4-Bromofluorobenzene (Surr)104 85-114 05/15/23 20:23 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)103 05/15/23 20:23 580-119
1,2-Dichloroethane-d4 (Surr)90 05/15/23 20:23 581-118
Toluene-d8 (Surr)112 05/15/23 20:23 589-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
10 U 20 4.4 ug/L 05/03/23 18:10 05/08/23 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:55 110 UAcenaphthylene
10 2.2 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 U MAcetophenone
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:55 110 UAnthracene
10 2.2 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 UAtrazine
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-2Client Sample ID: RW-16-05-23
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U M 20 4.8 ug/L 05/03/23 18:10 05/08/23 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzaldehyde
20 4.2 ug/L 05/03/23 18:10 05/08/23 17:55 110 UBenzo[a]anthracene
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 UBenzo[a]pyrene
20 3.1 ug/L 05/03/23 18:10 05/08/23 17:55 110 UBenzo[b]fluoranthene
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:55 110 UBenzo[g,h,i]perylene
20 2.9 ug/L 05/03/23 18:10 05/08/23 17:55 110 U QBenzo[k]fluoranthene
20 4.6 ug/L 05/03/23 18:10 05/08/23 17:55 110 U1,1'-Biphenyl
10 1.8 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UBis(2-chloroethoxy)methane
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:55 110 UBis(2-chloroethyl)ether
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:55 16.3 J BBis(2-ethylhexyl) phthalate
20 4.7 ug/L 05/03/23 18:10 05/08/23 17:55 110 U M4-Bromophenyl phenyl ether
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 UButyl benzyl phthalate
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 UCaprolactam
10 1.8 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UCarbazole
10 1.0 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 U Q4-Chloroaniline
20 2.5 ug/L 05/03/23 18:10 05/08/23 17:55 110 U4-Chloro-3-methylphenol
20 4.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2-Chloronaphthalene
20 3.2 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2-Chlorophenol
20 5.3 ug/L 05/03/23 18:10 05/08/23 17:55 112 U4-Chlorophenyl phenyl ether
20 3.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 UChrysene
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:55 110 UDibenz(a,h)anthracene
10 1.9 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UDibenzofuran
50 10 ug/L 05/03/23 18:10 05/08/23 17:55 120 U3,3'-Dichlorobenzidine
20 3.7 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2,4-Dichlorophenol
10 2.2 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 UDiethyl phthalate
20 3.0 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2,4-Dimethylphenol
10 2.1 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 UDimethyl phthalate
10 2.3 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 UDi-n-butyl phthalate
50 5.3 ug/L 05/03/23 18:10 05/08/23 17:55 120 U Q4,6-Dinitro-2-methylphenol
50 16 ug/L 05/03/23 18:10 05/08/23 17:55 140 U Q2,4-Dinitrophenol
10 2.3 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 U M2,4-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2,6-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 17:55 110 U MDi-n-octyl phthalate
10 1.6 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UFluoranthene
20 3.4 ug/L 05/03/23 18:10 05/08/23 17:55 110 UFluorene
10 1.6 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UHexachlorobenzene
20 4.0 ug/L 05/03/23 18:10 05/08/23 17:55 110 UHexachlorobutadiene
20 3.5 ug/L 05/03/23 18:10 05/08/23 17:55 110 UHexachlorocyclopentadiene
20 3.6 ug/L 05/03/23 18:10 05/08/23 17:55 110 UHexachloroethane
20 4.3 ug/L 05/03/23 18:10 05/08/23 17:55 110 UIndeno[1,2,3-cd]pyrene
10 2.0 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UIsophorone
20 4.6 ug/L 05/03/23 18:10 05/08/23 17:55 114 J2-Methylnaphthalene
10 1.8 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 U2-Methylphenol
10 1.4 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 U3 & 4 Methylphenol
20 3.5 ug/L 05/03/23 18:10 05/08/23 17:55 128Naphthalene
20 2.9 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 17:55 110 U3-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 17:55 110 U4-Nitroaniline
20 3.5 ug/L 05/03/23 18:10 05/08/23 17:55 110 UNitrobenzene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-2Client Sample ID: RW-16-05-23
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 3.9 ug/L 05/03/23 18:10 05/08/23 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Nitrophenol
50 8.1 ug/L 05/03/23 18:10 05/08/23 17:55 120 U4-Nitrophenol
10 2.4 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 UN-Nitrosodi-n-propylamine
20 2.9 ug/L 05/03/23 18:10 05/08/23 17:55 110 UN-Nitrosodiphenylamine
20 3.1 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2,2'-oxybis[1-chloropropane]
50 9.9 ug/L 05/03/23 18:10 05/08/23 17:55 120 UPentachlorophenol
20 4.3 ug/L 05/03/23 18:10 05/08/23 17:55 110 UPhenanthrene
10 1.5 ug/L 05/03/23 18:10 05/08/23 17:55 14.0 UPhenol
20 3.7 ug/L 05/03/23 18:10 05/08/23 17:55 110 UPyrene
20 3.3 ug/L 05/03/23 18:10 05/08/23 17:55 110 U2,4,5-Trichlorophenol
20 2.2 ug/L 05/03/23 18:10 05/08/23 17:55 15.0 U2,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)57 44-119 05/03/23 18:10 05/08/23 17:55 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)26 05/03/23 18:10 05/08/23 17:55 119-119
Nitrobenzene-d5 (Surr)48 05/03/23 18:10 05/08/23 17:55 144-120
Phenol-d5 (Surr)19 05/03/23 18:10 05/08/23 17:55 110-130
Terphenyl-d14 (Surr)102 Q 05/03/23 18:10 05/08/23 17:55 150-134
2,4,6-Tribromophenol (Surr)87 Q 05/03/23 18:10 05/08/23 17:55 143-140
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2300 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
9.1 5.0 1.0 ug/L 05/10/23 21:10 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 21:10 1980 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 21:10 1460 MC9-C10 Aromatics
5.0 1.0 ug/L 05/10/23 21:10 149Ethylbenzene
5.0 1.0 ug/L 05/10/23 21:10 15.8Methyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 21:10 152 MNaphthalene
5.0 1.0 ug/L 05/10/23 21:10 14.5 JToluene
10 2.5 ug/L 05/10/23 21:10 1240m-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 21:10 198 Mo-Xylene
100 25 ug/L 05/10/23 21:10 1960C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)375 Q 70-130 05/10/23 21:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)216 Q 05/10/23 21:10 170-130
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) - DL
LOQ DL
1300 D M 500 130 ug/L 05/11/23 22:40 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C9-C12 Aliphatics
500 130 ug/L 05/11/23 22:40 5540 DC9-C12 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)145 Q 70-130 05/11/23 22:40 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)108 05/11/23 22:40 570-130
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-2Client Sample ID: RW-16-05-23
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U M 2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:56 1220Total EPH
12 5.0 ug/L 05/12/23 08:50 05/17/23 23:33 110 UPyrene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 UBenzo[g,h,i]perylene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 UBenzo[b]fluoranthene
2.0 0.50 ug/L 05/12/23 08:50 05/17/23 23:33 11.0 UFluoranthene
4.0 1.5 ug/L 05/12/23 08:50 05/17/23 23:33 13.0 UBenzo[k]fluoranthene
2.0 0.70 ug/L 05/12/23 08:50 05/17/23 23:33 11.6 J MAcenaphthylene
2.0 0.50 ug/L 05/12/23 08:50 05/17/23 23:33 11.0 UChrysene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 UBenzo[a]pyrene
2.0 0.50 ug/L 05/12/23 08:50 05/17/23 23:33 11.0 UDibenz(a,h)anthracene
2.0 0.70 ug/L 05/12/23 08:50 05/17/23 23:33 11.4 UBenzo[a]anthracene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 U MAcenaphthene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 U MPhenanthrene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 11.2 U MFluorene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 123 MNaphthalene
2.0 0.60 ug/L 05/12/23 08:50 05/17/23 23:33 111 M2-Methylnaphthalene
40 10 ug/L 05/12/23 08:50 05/17/23 23:33 173 MC11-C22 Aromatics (unadjusted)
40 10 ug/L 05/12/23 08:50 05/17/23 23:33 137 JC11-C22 Aromatics (Adjusted)
50 10 ug/L 05/12/23 08:50 05/17/23 23:33 120 U MC19-C36 Aliphatics
30 10 ug/L 05/12/23 08:50 05/17/23 23:33 1150 M B QC9-C18 Aliphatics
1-Chlorooctadecane (Surr)59 40-140 05/12/23 08:50 05/17/23 23:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)58 05/12/23 08:50 05/17/23 23:33 140-140
o- terphenyl (Surr)50 05/12/23 08:50 05/17/23 23:33 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U H M 2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
12 5.1 ug/L 05/23/23 09:00 06/01/23 10:00 110 U H MPyrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U HBenzo[g,h,i]perylene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U HIndeno[1,2,3-cd]pyrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U HBenzo[b]fluoranthene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 10:00 11.0 U H MFluoranthene
4.0 1.5 ug/L 05/23/23 09:00 06/01/23 10:00 13.0 U HBenzo[k]fluoranthene
2.0 0.71 ug/L 05/23/23 09:00 06/01/23 10:00 11.5 J H MAcenaphthylene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 10:00 11.0 U HChrysene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U HBenzo[a]pyrene
2.0 0.51 ug/L 05/23/23 09:00 06/01/23 10:00 11.0 U HDibenz(a,h)anthracene
2.0 0.71 ug/L 05/23/23 09:00 06/01/23 10:00 11.4 U H MBenzo[a]anthracene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U H MAcenaphthene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U H MPhenanthrene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 11.2 U H MFluorene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 134 H MNaphthalene
2.0 0.61 ug/L 05/23/23 09:00 06/01/23 10:00 116 H M2-Methylnaphthalene
40 10 ug/L 05/23/23 09:00 06/01/23 10:00 192 H MC11-C22 Aromatics (unadjusted)
40 10 ug/L 05/23/23 09:00 06/01/23 10:00 141 HC11-C22 Aromatics (Adjusted)
51 10 ug/L 05/23/23 09:00 06/01/23 10:22 120 U M HC19-C36 Aliphatics
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-2Client Sample ID: RW-16-05-23
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
160 H B 30 10 ug/L 05/23/23 09:00 06/01/23 10:22 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C9-C18 Aliphatics
1-Chlorooctadecane (Surr)48 M 40-140 05/23/23 09:00 06/01/23 10:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)86 05/23/23 09:00 06/01/23 10:00 140-140
o- terphenyl (Surr)63 05/23/23 09:00 06/01/23 10:00 140-140
Lab Sample ID: 680-234374-3Client Sample ID: RW-17-05-23
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
50 U M 130 19 ug/L 05/14/23 21:46 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
10 1.4 ug/L 05/14/23 21:46 524 DBenzene
13 3.0 ug/L 05/14/23 21:46 510 UBromoform
100 19 ug/L 05/14/23 21:46 550 UBromomethane
130 32 ug/L 05/14/23 21:46 5100 U M2-Butanone (MEK)
10 2.2 ug/L 05/14/23 21:46 55.0 U QCarbon disulfide
10 1.5 ug/L 05/14/23 21:46 55.0 UCarbon tetrachloride
5.0 0.75 ug/L 05/14/23 21:46 52.5 UChlorobenzene
10 2.0 ug/L 05/14/23 21:46 55.0 UChlorodibromomethane
100 23 ug/L 05/14/23 21:46 550 U QChloroethane
10 1.4 ug/L 05/14/23 21:46 55.0 UChloroform
13 2.7 ug/L 05/14/23 21:46 510 U QChloromethane
10 1.3 ug/L 05/14/23 21:46 55.0 Ucis-1,2-Dichloroethene
10 1.3 ug/L 05/14/23 21:46 55.0 Ucis-1,3-Dichloropropene
10 1.4 ug/L 05/14/23 21:46 576 D QCyclohexane
50 9.0 ug/L 05/14/23 21:46 525 U Q1,2-Dibromo-3-Chloropropane
10 1.7 ug/L 05/14/23 21:46 55.0 U1,2-Dibromoethane (EDB)
10 1.6 ug/L 05/14/23 21:46 55.0 U1,2-Dichlorobenzene
10 1.6 ug/L 05/14/23 21:46 55.0 U1,3-Dichlorobenzene
10 1.6 ug/L 05/14/23 21:46 55.0 U1,4-Dichlorobenzene
10 1.3 ug/L 05/14/23 21:46 55.0 UDichlorobromomethane
10 1.8 ug/L 05/14/23 21:46 55.0 UDichlorodifluoromethane
10 1.7 ug/L 05/14/23 21:46 55.0 U M1,1-Dichloroethane
10 1.3 ug/L 05/14/23 21:46 55.0 U M Q1,2-Dichloroethane
10 1.7 ug/L 05/15/23 20:43 55.0 U1,1-Dichloroethene
5.0 1.1 ug/L 05/14/23 21:46 52.5 U1,2-Dichloropropane
5.0 1.0 ug/L 05/14/23 21:46 5220 DEthylbenzene
100 16 ug/L 05/14/23 21:46 550 U2-Hexanone
10 1.3 ug/L 05/14/23 21:46 524 DIsopropylbenzene
100 16 ug/L 05/14/23 21:46 550 UMethyl acetate
10 1.7 ug/L 05/14/23 21:46 551 DMethylcyclohexane
100 16 ug/L 05/14/23 21:46 550 U QMethylene Chloride
100 14 ug/L 05/14/23 21:46 550 U4-Methyl-2-pentanone (MIBK)
25 4.1 ug/L 05/14/23 21:46 510 UMethyl tert-butyl ether
10 1.4 ug/L 05/14/23 21:46 55.0 U MStyrene
10 2.0 ug/L 05/14/23 21:46 55.0 U1,1,2,2-Tetrachloroethane
10 1.8 ug/L 05/14/23 21:46 55.0 UTetrachloroethene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-3Client Sample ID: RW-17-05-23
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
120 D 10 1.3 ug/L 05/14/23 21:46 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Toluene
10 1.7 ug/L 05/14/23 21:46 55.0 Utrans-1,2-Dichloroethene
10 1.2 ug/L 05/14/23 21:46 55.0 Utrans-1,3-Dichloropropene
25 2.7 ug/L 05/14/23 21:46 510 U1,2,4-Trichlorobenzene
5.0 1.1 ug/L 05/14/23 21:46 52.5 U1,1,1-Trichloroethane
10 1.6 ug/L 05/14/23 21:46 55.0 U1,1,2-Trichloroethane
5.0 1.0 ug/L 05/14/23 21:46 52.5 UTrichloroethene
10 1.7 ug/L 05/14/23 21:46 55.0 UTrichlorofluoromethane
5.0 1.2 ug/L 05/14/23 21:46 52.5 U1,1,2-Trichloro-1,2,2-trifluoroethane
10 2.0 ug/L 05/14/23 21:46 55.0 U QVinyl chloride
10 2.5 ug/L 05/14/23 21:46 5980 DXylenes, Total
4-Bromofluorobenzene (Surr)105 85-114 05/14/23 21:46 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr)103 05/15/23 20:43 585-114
Dibromofluoromethane (Surr)82 05/14/23 21:46 580-119
Dibromofluoromethane (Surr)104 05/15/23 20:43 580-119
1,2-Dichloroethane-d4 (Surr)78 Q 05/14/23 21:46 581-118
1,2-Dichloroethane-d4 (Surr)92 05/15/23 20:43 581-118
Toluene-d8 (Surr)89 05/14/23 21:46 589-112
Toluene-d8 (Surr)113 Q 05/15/23 20:43 589-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
10 U 20 4.4 ug/L 05/03/23 18:10 05/08/23 18:20 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:20 110 UAcenaphthylene
10 2.2 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 U MAcetophenone
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:20 110 UAnthracene
10 2.2 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 UAtrazine
20 4.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 U MBenzaldehyde
20 4.2 ug/L 05/03/23 18:10 05/08/23 18:20 110 UBenzo[a]anthracene
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 UBenzo[a]pyrene
20 3.1 ug/L 05/03/23 18:10 05/08/23 18:20 110 UBenzo[b]fluoranthene
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:20 110 UBenzo[g,h,i]perylene
20 2.9 ug/L 05/03/23 18:10 05/08/23 18:20 110 U QBenzo[k]fluoranthene
20 4.6 ug/L 05/03/23 18:10 05/08/23 18:20 110 U1,1'-Biphenyl
10 1.8 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 UBis(2-chloroethoxy)methane
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:20 110 UBis(2-chloroethyl)ether
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:20 16.3 J BBis(2-ethylhexyl) phthalate
20 4.7 ug/L 05/03/23 18:10 05/08/23 18:20 110 U4-Bromophenyl phenyl ether
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 UButyl benzyl phthalate
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 UCaprolactam
10 1.8 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 UCarbazole
10 1.0 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 U Q4-Chloroaniline
20 2.5 ug/L 05/03/23 18:10 05/08/23 18:20 110 U4-Chloro-3-methylphenol
20 4.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2-Chloronaphthalene
20 3.2 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2-Chlorophenol
20 5.3 ug/L 05/03/23 18:10 05/08/23 18:20 112 U4-Chlorophenyl phenyl ether
20 3.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 UChrysene
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:20 110 UDibenz(a,h)anthracene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-3Client Sample ID: RW-17-05-23
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
4.0 U 10 1.9 ug/L 05/03/23 18:10 05/08/23 18:20 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Dibenzofuran
50 10 ug/L 05/03/23 18:10 05/08/23 18:20 120 U3,3'-Dichlorobenzidine
20 3.7 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2,4-Dichlorophenol
10 2.2 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 UDiethyl phthalate
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2,4-Dimethylphenol
10 2.1 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 UDimethyl phthalate
10 2.3 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 UDi-n-butyl phthalate
50 5.3 ug/L 05/03/23 18:10 05/08/23 18:20 120 U Q4,6-Dinitro-2-methylphenol
50 16 ug/L 05/03/23 18:10 05/08/23 18:20 140 U Q2,4-Dinitrophenol
10 2.3 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 U2,4-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2,6-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:20 110 U MDi-n-octyl phthalate
10 1.6 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 UFluoranthene
20 3.4 ug/L 05/03/23 18:10 05/08/23 18:20 110 UFluorene
10 1.6 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 UHexachlorobenzene
20 4.0 ug/L 05/03/23 18:10 05/08/23 18:20 110 UHexachlorobutadiene
20 3.5 ug/L 05/03/23 18:10 05/08/23 18:20 110 UHexachlorocyclopentadiene
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:20 110 UHexachloroethane
20 4.3 ug/L 05/03/23 18:10 05/08/23 18:20 110 UIndeno[1,2,3-cd]pyrene
10 2.0 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 UIsophorone
20 4.6 ug/L 05/03/23 18:10 05/08/23 18:20 1332-Methylnaphthalene
10 1.8 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 U2-Methylphenol
10 1.4 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 U3 & 4 Methylphenol
20 3.5 ug/L 05/03/23 18:10 05/08/23 18:20 154Naphthalene
20 2.9 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 18:20 110 U3-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 18:20 110 U4-Nitroaniline
20 3.5 ug/L 05/03/23 18:10 05/08/23 18:20 110 UNitrobenzene
20 3.9 ug/L 05/03/23 18:10 05/08/23 18:20 110 U M2-Nitrophenol
50 8.1 ug/L 05/03/23 18:10 05/08/23 18:20 120 U4-Nitrophenol
10 2.4 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 UN-Nitrosodi-n-propylamine
20 2.9 ug/L 05/03/23 18:10 05/08/23 18:20 110 UN-Nitrosodiphenylamine
20 3.1 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2,2'-oxybis[1-chloropropane]
50 9.9 ug/L 05/03/23 18:10 05/08/23 18:20 120 UPentachlorophenol
20 4.3 ug/L 05/03/23 18:10 05/08/23 18:20 110 UPhenanthrene
10 1.5 ug/L 05/03/23 18:10 05/08/23 18:20 14.0 UPhenol
20 3.7 ug/L 05/03/23 18:10 05/08/23 18:20 110 UPyrene
20 3.3 ug/L 05/03/23 18:10 05/08/23 18:20 110 U2,4,5-Trichlorophenol
20 2.2 ug/L 05/03/23 18:10 05/08/23 18:20 15.0 U2,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)61 44-119 05/03/23 18:10 05/08/23 18:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)28 05/03/23 18:10 05/08/23 18:20 119-119
Nitrobenzene-d5 (Surr)55 05/03/23 18:10 05/08/23 18:20 144-120
Phenol-d5 (Surr)19 05/03/23 18:10 05/08/23 18:20 110-130
Terphenyl-d14 (Surr)98 Q 05/03/23 18:10 05/08/23 18:20 150-134
2,4,6-Tribromophenol (Surr)85 Q 05/03/23 18:10 05/08/23 18:20 143-140
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-3Client Sample ID: RW-17-05-23
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
3700 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
31 5.0 1.0 ug/L 05/10/23 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 21:51 11600 MC5-C8 Aliphatics
5.0 1.0 ug/L 05/10/23 21:51 12.0 UMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 21:51 195Naphthalene
5.0 1.0 ug/L 05/10/23 21:51 1150Toluene
100 25 ug/L 05/10/23 21:51 11400C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)546 Q 70-130 05/10/23 21:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)293 Q 05/10/23 21:51 170-130
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) - DL
LOQ DL
590 J D M 1000 100 ug/L 05/11/23 23:21 10
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
C9-C10 Aromatics
1000 250 ug/L 05/11/23 23:21 102100 D MC9-C12 Aliphatics
50 10 ug/L 05/11/23 23:21 10120 DEthylbenzene
1000 250 ug/L 05/11/23 23:21 10890 J DC9-C12 Aliphatics (adjusted)
100 25 ug/L 05/11/23 23:21 10350 Dm-Xylene & p-Xylene
50 10 ug/L 05/11/23 23:21 10200 Do-Xylene
a,a,a-Trifluorotoluene (fid)126 70-130 05/11/23 23:21 10
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)101 05/11/23 23:21 1070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U M 1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:56 1570Total EPH
12 4.8 ug/L 05/12/23 08:50 05/17/23 23:55 19.7 UPyrene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 UBenzo[g,h,i]perylene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 UIndeno[1,2,3-cd]pyrene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 UBenzo[b]fluoranthene
1.9 0.48 ug/L 05/12/23 08:50 05/17/23 23:55 10.97 UFluoranthene
3.9 1.4 ug/L 05/12/23 08:50 05/17/23 23:55 12.9 UBenzo[k]fluoranthene
1.9 0.68 ug/L 05/12/23 08:50 05/17/23 23:55 16.1 MAcenaphthylene
1.9 0.48 ug/L 05/12/23 08:50 05/17/23 23:55 10.97 UChrysene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 UBenzo[a]pyrene
1.9 0.48 ug/L 05/12/23 08:50 05/17/23 23:55 10.97 UDibenz(a,h)anthracene
1.9 0.68 ug/L 05/12/23 08:50 05/17/23 23:55 11.4 UBenzo[a]anthracene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 U MAcenaphthene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 U MPhenanthrene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 11.2 U MFluorene
1.9 0.58 ug/L 05/12/23 08:50 05/17/23 23:55 133 M2-Methylnaphthalene
39 9.7 ug/L 05/12/23 08:50 05/17/23 23:55 1220 MC11-C22 Aromatics (unadjusted)
48 9.7 ug/L 05/12/23 08:50 05/17/23 23:55 112 J MC19-C36 Aliphatics
29 9.7 ug/L 05/12/23 08:50 05/17/23 23:55 1340 M B QC9-C18 Aliphatics
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-3Client Sample ID: RW-17-05-23
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
1-Chlorooctadecane (Surr)62 40-140 05/12/23 08:50 05/17/23 23:55 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)65 05/12/23 08:50 05/17/23 23:55 140-140
o- terphenyl (Surr)55 05/12/23 08:50 05/17/23 23:55 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
LOQ DL
51 D M 3.9 1.2 ug/L 05/12/23 08:50 05/18/23 15:58 2
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Naphthalene
77 19 ug/L 05/12/23 08:50 05/18/23 15:58 2140 DC11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)64 40-140 05/12/23 08:50 05/18/23 15:58 2
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
o- terphenyl (Surr)55 05/12/23 08:50 05/18/23 15:58 240-140
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U M 25 3.7 ug/L 05/14/23 16:57 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
2.0 0.27 ug/L 05/14/23 16:57 120Benzene
2.5 0.59 ug/L 05/14/23 16:57 12.0 UBromoform
20 3.7 ug/L 05/14/23 16:57 110 UBromomethane
25 6.4 ug/L 05/14/23 16:57 120 U2-Butanone (MEK)
2.0 0.43 ug/L 05/14/23 16:57 11.0 U QCarbon disulfide
2.0 0.30 ug/L 05/14/23 16:57 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 05/14/23 16:57 10.50 UChlorobenzene
2.0 0.39 ug/L 05/14/23 16:57 11.0 UChlorodibromomethane
20 4.6 ug/L 05/14/23 16:57 110 U QChloroethane
2.0 0.27 ug/L 05/14/23 16:57 11.0 U MChloroform
2.5 0.54 ug/L 05/14/23 16:57 12.0 U QChloromethane
2.0 0.25 ug/L 05/14/23 16:57 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 05/14/23 16:57 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 05/14/23 16:57 18.5 QCyclohexane
10 1.8 ug/L 05/14/23 16:57 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 05/14/23 16:57 11.0 U1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 05/14/23 16:57 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 05/14/23 16:57 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 05/14/23 16:57 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 05/14/23 16:57 11.0 UDichlorobromomethane
2.0 0.36 ug/L 05/14/23 16:57 11.0 UDichlorodifluoromethane
2.0 0.33 ug/L 05/14/23 16:57 11.0 U M1,1-Dichloroethane
2.0 0.25 ug/L 05/14/23 16:57 11.0 U M Q1,2-Dichloroethane
2.0 0.33 ug/L 05/15/23 15:28 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 05/14/23 16:57 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 05/14/23 16:57 11.1Ethylbenzene
20 3.2 ug/L 05/14/23 16:57 110 U2-Hexanone
2.0 0.26 ug/L 05/14/23 16:57 11.0 U MIsopropylbenzene
20 3.2 ug/L 05/14/23 16:57 110 UMethyl acetate
2.0 0.33 ug/L 05/14/23 16:57 12.6Methylcyclohexane
20 3.2 ug/L 05/14/23 16:57 110 U QMethylene Chloride
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 2.7 ug/L 05/14/23 16:57 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 05/14/23 16:57 12.0 UMethyl tert-butyl ether
2.0 0.27 ug/L 05/14/23 16:57 11.0 U MStyrene
2.0 0.40 ug/L 05/14/23 16:57 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 05/14/23 16:57 11.0 UTetrachloroethene
2.0 0.25 ug/L 05/14/23 16:57 10.32 JToluene
2.0 0.34 ug/L 05/14/23 16:57 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 05/14/23 16:57 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 05/14/23 16:57 12.0 U M1,2,4-Trichlorobenzene
1.0 0.21 ug/L 05/14/23 16:57 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 05/14/23 16:57 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 05/14/23 16:57 10.50 UTrichloroethene
2.0 0.33 ug/L 05/14/23 16:57 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 05/14/23 16:57 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 05/14/23 16:57 11.0 U QVinyl chloride
2.0 0.49 ug/L 05/14/23 16:57 127Xylenes, Total
4-Bromofluorobenzene (Surr)106 85-114 05/14/23 16:57 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr)103 05/15/23 15:28 185-114
Dibromofluoromethane (Surr)83 05/14/23 16:57 180-119
Dibromofluoromethane (Surr)104 05/15/23 15:28 180-119
1,2-Dichloroethane-d4 (Surr)78 Q 05/14/23 16:57 181-118
1,2-Dichloroethane-d4 (Surr)89 05/15/23 15:28 181-118
Toluene-d8 (Surr)88 Q 05/14/23 16:57 189-112
Toluene-d8 (Surr)113 Q 05/15/23 15:28 189-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
10 U 20 4.4 ug/L 05/03/23 18:10 05/08/23 18:44 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:44 110 UAcenaphthylene
10 2.2 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 U MAcetophenone
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:44 110 UAnthracene
10 2.2 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 UAtrazine
20 4.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 UBenzaldehyde
20 4.2 ug/L 05/03/23 18:10 05/08/23 18:44 110 UBenzo[a]anthracene
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 UBenzo[a]pyrene
20 3.1 ug/L 05/03/23 18:10 05/08/23 18:44 110 U MBenzo[b]fluoranthene
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:44 110 UBenzo[g,h,i]perylene
20 2.9 ug/L 05/03/23 18:10 05/08/23 18:44 110 U QBenzo[k]fluoranthene
20 4.6 ug/L 05/03/23 18:10 05/08/23 18:44 110 U1,1'-Biphenyl
10 1.8 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 U QBis(2-chloroethoxy)methane
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:44 110 U QBis(2-chloroethyl)ether
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:44 16.3 J BBis(2-ethylhexyl) phthalate
20 4.7 ug/L 05/03/23 18:10 05/08/23 18:44 110 U M4-Bromophenyl phenyl ether
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 UButyl benzyl phthalate
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 UCaprolactam
10 1.8 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 UCarbazole
10 1.0 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 U Q4-Chloroaniline
20 2.5 ug/L 05/03/23 18:10 05/08/23 18:44 110 U4-Chloro-3-methylphenol
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 4.8 ug/L 05/03/23 18:10 05/08/23 18:44 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Chloronaphthalene
20 3.2 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2-Chlorophenol
20 5.3 ug/L 05/03/23 18:10 05/08/23 18:44 112 U4-Chlorophenyl phenyl ether
20 3.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 UChrysene
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:44 110 UDibenz(a,h)anthracene
10 1.9 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 UDibenzofuran
50 10 ug/L 05/03/23 18:10 05/08/23 18:44 120 U3,3'-Dichlorobenzidine
20 3.7 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2,4-Dichlorophenol
10 2.2 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 UDiethyl phthalate
20 3.0 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2,4-Dimethylphenol
10 2.1 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 UDimethyl phthalate
10 2.3 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 UDi-n-butyl phthalate
50 5.3 ug/L 05/03/23 18:10 05/08/23 18:44 120 U Q4,6-Dinitro-2-methylphenol
50 16 ug/L 05/03/23 18:10 05/08/23 18:44 140 U Q2,4-Dinitrophenol
10 2.3 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 U M2,4-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2,6-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 18:44 110 U MDi-n-octyl phthalate
10 1.6 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 UFluoranthene
20 3.4 ug/L 05/03/23 18:10 05/08/23 18:44 110 UFluorene
10 1.6 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 UHexachlorobenzene
20 4.0 ug/L 05/03/23 18:10 05/08/23 18:44 110 U QHexachlorobutadiene
20 3.5 ug/L 05/03/23 18:10 05/08/23 18:44 110 UHexachlorocyclopentadiene
20 3.6 ug/L 05/03/23 18:10 05/08/23 18:44 110 U QHexachloroethane
20 4.3 ug/L 05/03/23 18:10 05/08/23 18:44 110 UIndeno[1,2,3-cd]pyrene
10 2.0 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 U QIsophorone
20 4.6 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2-Methylnaphthalene
10 1.8 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 U2-Methylphenol
10 1.4 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 U3 & 4 Methylphenol
20 3.5 ug/L 05/03/23 18:10 05/08/23 18:44 110 UNaphthalene
20 2.9 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 18:44 110 U3-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 18:44 110 U4-Nitroaniline
20 3.5 ug/L 05/03/23 18:10 05/08/23 18:44 110 U QNitrobenzene
20 3.9 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2-Nitrophenol
50 8.1 ug/L 05/03/23 18:10 05/08/23 18:44 120 U4-Nitrophenol
10 2.4 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 U QN-Nitrosodi-n-propylamine
20 2.9 ug/L 05/03/23 18:10 05/08/23 18:44 110 UN-Nitrosodiphenylamine
20 3.1 ug/L 05/03/23 18:10 05/08/23 18:44 110 U Q2,2'-oxybis[1-chloropropane]
50 9.9 ug/L 05/03/23 18:10 05/08/23 18:44 120 UPentachlorophenol
20 4.3 ug/L 05/03/23 18:10 05/08/23 18:44 110 UPhenanthrene
10 1.5 ug/L 05/03/23 18:10 05/08/23 18:44 14.0 UPhenol
20 3.7 ug/L 05/03/23 18:10 05/08/23 18:44 110 UPyrene
20 3.3 ug/L 05/03/23 18:10 05/08/23 18:44 110 U2,4,5-Trichlorophenol
20 2.2 ug/L 05/03/23 18:10 05/08/23 18:44 15.0 U2,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)48 44-119 05/03/23 18:10 05/08/23 18:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)21 05/03/23 18:10 05/08/23 18:44 119-119
Nitrobenzene-d5 (Surr)41 Q 05/03/23 18:10 05/08/23 18:44 144-120
Phenol-d5 (Surr)14 05/03/23 18:10 05/08/23 18:44 110-130
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Terphenyl-d14 (Surr)78 Q 50-134 05/03/23 18:10 05/08/23 18:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2,4,6-Tribromophenol (Surr)63 Q 05/03/23 18:10 05/08/23 18:44 143-140
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE
LOQ DL
10 U H 20 4.4 ug/L 05/10/23 20:46 05/12/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
20 3.6 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HAcenaphthylene
10 2.2 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U H M QAcetophenone
20 3.6 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HAnthracene
10 2.2 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U HAtrazine
20 4.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H QBenzaldehyde
20 4.2 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBenzo[a]anthracene
20 2.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBenzo[a]pyrene
20 3.1 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBenzo[b]fluoranthene
20 3.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBenzo[g,h,i]perylene
20 2.9 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBenzo[k]fluoranthene
20 4.6 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H1,1'-Biphenyl
10 1.8 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U HBis(2-chloroethoxy)methane
20 3.6 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBis(2-chloroethyl)ether
20 3.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HBis(2-ethylhexyl) phthalate
20 4.7 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H M4-Bromophenyl phenyl ether
20 2.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H MButyl benzyl phthalate
20 2.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H QCaprolactam
10 1.8 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U H QCarbazole
10 1.0 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U H4-Chloroaniline
20 2.5 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H Q4-Chloro-3-methylphenol
20 4.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H2-Chloronaphthalene
20 3.2 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H Q2-Chlorophenol
20 5.3 ug/L 05/10/23 20:46 05/12/23 22:27 112 U H4-Chlorophenyl phenyl ether
20 3.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HChrysene
20 3.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HDibenz(a,h)anthracene
10 1.9 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U HDibenzofuran
50 10 ug/L 05/10/23 20:46 05/12/23 22:27 120 U H3,3'-Dichlorobenzidine
20 3.7 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H Q2,4-Dichlorophenol
10 2.2 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U HDiethyl phthalate
20 3.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H Q2,4-Dimethylphenol
10 2.1 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U HDimethyl phthalate
10 2.3 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U HDi-n-butyl phthalate
50 5.3 ug/L 05/10/23 20:46 05/12/23 22:27 120 U H Q4,6-Dinitro-2-methylphenol
50 16 ug/L 05/10/23 20:46 05/12/23 22:27 140 U H Q2,4-Dinitrophenol
10 2.3 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U H2,4-Dinitrotoluene
20 2.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H2,6-Dinitrotoluene
20 2.8 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H MDi-n-octyl phthalate
10 1.6 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U HFluoranthene
20 3.4 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HFluorene
10 1.6 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U HHexachlorobenzene
20 4.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H QHexachlorobutadiene
20 3.5 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HHexachlorocyclopentadiene
20 3.6 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HHexachloroethane
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - RE (Continued)
LOQ DL
10 U H 20 4.3 ug/L 05/10/23 20:46 05/12/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Indeno[1,2,3-cd]pyrene
10 2.0 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U HIsophorone
20 4.6 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H2-Methylnaphthalene
10 1.8 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U H Q2-Methylphenol
10 1.4 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U H Q3 & 4 Methylphenol
20 3.5 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HNaphthalene
20 2.9 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H2-Nitroaniline
50 3.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H3-Nitroaniline
50 3.0 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H4-Nitroaniline
20 3.5 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HNitrobenzene
20 3.9 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H Q2-Nitrophenol
50 8.1 ug/L 05/10/23 20:46 05/12/23 22:27 120 U H Q4-Nitrophenol
10 2.4 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U HN-Nitrosodi-n-propylamine
20 2.9 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HN-Nitrosodiphenylamine
20 3.1 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H2,2'-oxybis[1-chloropropane]
50 9.9 ug/L 05/10/23 20:46 05/12/23 22:27 120 U H QPentachlorophenol
20 4.3 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HPhenanthrene
10 1.5 ug/L 05/10/23 20:46 05/12/23 22:27 14.0 U HPhenol
20 3.7 ug/L 05/10/23 20:46 05/12/23 22:27 110 U HPyrene
20 3.3 ug/L 05/10/23 20:46 05/12/23 22:27 110 U H Q2,4,5-Trichlorophenol
20 2.2 ug/L 05/10/23 20:46 05/12/23 22:27 15.0 U H Q2,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)49 44-119 05/10/23 20:46 05/12/23 22:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)15 Q 05/10/23 20:46 05/12/23 22:27 119-119
Nitrobenzene-d5 (Surr)46 05/10/23 20:46 05/12/23 22:27 144-120
Phenol-d5 (Surr)14 05/10/23 20:46 05/12/23 22:27 110-130
Terphenyl-d14 (Surr)60 05/10/23 20:46 05/12/23 22:27 150-134
2,4,6-Tribromophenol (Surr)30 Q 05/10/23 20:46 05/12/23 22:27 143-140
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
700 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
43 5.0 1.0 ug/L 05/10/23 22:32 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
100 25 ug/L 05/10/23 22:32 1340 MC5-C8 Aliphatics
100 10 ug/L 05/10/23 22:32 1110 MC9-C10 Aromatics
100 25 ug/L 05/10/23 22:32 1360 MC9-C12 Aliphatics
5.0 1.0 ug/L 05/10/23 22:32 16.9Ethylbenzene
5.0 1.0 ug/L 05/10/23 22:32 12.0 UMethyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 22:32 110 MNaphthalene
5.0 1.0 ug/L 05/10/23 22:32 12.2 JToluene
100 25 ug/L 05/10/23 22:32 1150C9-C12 Aliphatics (adjusted)
10 2.5 ug/L 05/10/23 22:32 161m-Xylene & p-Xylene
5.0 1.0 ug/L 05/10/23 22:32 127o-Xylene
100 25 ug/L 05/10/23 22:32 1300C5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
a,a,a-Trifluorotoluene (fid)158 M Q 70-130 05/10/23 22:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)113 05/10/23 22:32 170-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.1 U 1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:56 134 JTotal EPH
11 4.8 ug/L 05/12/23 08:50 05/18/23 01:25 19.6 UPyrene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UBenzo[g,h,i]perylene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UIndeno[1,2,3-cd]pyrene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UBenzo[b]fluoranthene
1.9 0.48 ug/L 05/12/23 08:50 05/18/23 01:25 10.96 UFluoranthene
3.8 1.4 ug/L 05/12/23 08:50 05/18/23 01:25 12.9 UBenzo[k]fluoranthene
1.9 0.67 ug/L 05/12/23 08:50 05/18/23 01:25 11.3 UAcenaphthylene
1.9 0.48 ug/L 05/12/23 08:50 05/18/23 01:25 10.96 UChrysene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UBenzo[a]pyrene
1.9 0.48 ug/L 05/12/23 08:50 05/18/23 01:25 10.96 UDibenz(a,h)anthracene
1.9 0.67 ug/L 05/12/23 08:50 05/18/23 01:25 11.3 UBenzo[a]anthracene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UAcenaphthene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UPhenanthrene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.1 UFluorene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 14.7 MNaphthalene
1.9 0.57 ug/L 05/12/23 08:50 05/18/23 01:25 11.9 M2-Methylnaphthalene
38 9.6 ug/L 05/12/23 08:50 05/18/23 01:25 116 J MC11-C22 Aromatics (unadjusted)
38 9.6 ug/L 05/12/23 08:50 05/18/23 01:25 129 UC11-C22 Aromatics (Adjusted)
48 9.6 ug/L 05/12/23 08:50 05/18/23 01:25 119 UC19-C36 Aliphatics
29 9.6 ug/L 05/12/23 08:50 05/18/23 01:25 118 J M B QC9-C18 Aliphatics
1-Chlorooctadecane (Surr)32 Q 40-140 05/12/23 08:50 05/18/23 01:25 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)65 05/12/23 08:50 05/18/23 01:25 140-140
o- terphenyl (Surr)52 05/12/23 08:50 05/18/23 01:25 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U H 1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
12 4.8 ug/L 05/23/23 09:00 06/01/23 10:22 19.6 U HPyrene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HBenzo[g,h,i]perylene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HIndeno[1,2,3-cd]pyrene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HBenzo[b]fluoranthene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 10:22 10.96 U HFluoranthene
3.8 1.4 ug/L 05/23/23 09:00 06/01/23 10:22 12.9 U HBenzo[k]fluoranthene
1.9 0.67 ug/L 05/23/23 09:00 06/01/23 10:22 11.3 U HAcenaphthylene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 10:22 10.96 U HChrysene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HBenzo[a]pyrene
1.9 0.48 ug/L 05/23/23 09:00 06/01/23 10:22 10.96 U HDibenz(a,h)anthracene
1.9 0.67 ug/L 05/23/23 09:00 06/01/23 10:22 11.3 U HBenzo[a]anthracene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HAcenaphthene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HPhenanthrene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 11.2 U HFluorene
1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 14.8 H MNaphthalene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-4Client Sample ID: RW-08-05-23
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE (Continued)
LOQ DL
1.2 U H 1.9 0.58 ug/L 05/23/23 09:00 06/01/23 10:22 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Methylnaphthalene
38 9.6 ug/L 05/23/23 09:00 06/01/23 10:22 116 J H MC11-C22 Aromatics (unadjusted)
38 9.6 ug/L 05/23/23 09:00 06/01/23 10:22 110 J HC11-C22 Aromatics (Adjusted)
48 9.6 ug/L 05/23/23 09:00 06/01/23 10:45 119 U M HC19-C36 Aliphatics
29 9.6 ug/L 05/23/23 09:00 06/01/23 10:45 150 H BC9-C18 Aliphatics
1-Chlorooctadecane (Surr)25 M Q 40-140 05/23/23 09:00 06/01/23 10:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)86 05/23/23 09:00 06/01/23 10:22 140-140
o- terphenyl (Surr)59 05/23/23 09:00 06/01/23 10:22 140-140
Lab Sample ID: 680-234374-5Client Sample ID: MW7-18-05-23
Matrix: WaterDate Collected: 05/01/23 13:35
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
1000 U 2500 370 ug/L 05/14/23 21:27 100
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acetone
200 27 ug/L 05/14/23 21:27 1001300 DBenzene
250 59 ug/L 05/14/23 21:27 100200 UBromoform
2000 370 ug/L 05/14/23 21:27 1001000 UBromomethane
2500 640 ug/L 05/14/23 21:27 1002000 U2-Butanone (MEK)
200 43 ug/L 05/14/23 21:27 100100 U QCarbon disulfide
200 30 ug/L 05/14/23 21:27 100100 UCarbon tetrachloride
100 15 ug/L 05/14/23 21:27 10050 UChlorobenzene
200 39 ug/L 05/14/23 21:27 100100 UChlorodibromomethane
2000 460 ug/L 05/14/23 21:27 1001000 U QChloroethane
200 27 ug/L 05/14/23 21:27 100100 UChloroform
250 54 ug/L 05/14/23 21:27 100200 U QChloromethane
200 25 ug/L 05/14/23 21:27 100100 Ucis-1,2-Dichloroethene
200 26 ug/L 05/14/23 21:27 100100 Ucis-1,3-Dichloropropene
200 28 ug/L 05/14/23 21:27 10083 J D QCyclohexane
1000 180 ug/L 05/14/23 21:27 100500 U Q1,2-Dibromo-3-Chloropropane
200 33 ug/L 05/14/23 21:27 100100 U1,2-Dibromoethane (EDB)
200 31 ug/L 05/14/23 21:27 100100 U1,2-Dichlorobenzene
200 31 ug/L 05/14/23 21:27 100100 U1,3-Dichlorobenzene
200 31 ug/L 05/14/23 21:27 100100 U1,4-Dichlorobenzene
200 25 ug/L 05/14/23 21:27 100100 UDichlorobromomethane
200 36 ug/L 05/14/23 21:27 100100 UDichlorodifluoromethane
200 33 ug/L 05/14/23 21:27 100100 U1,1-Dichloroethane
200 25 ug/L 05/14/23 21:27 100100 U M Q1,2-Dichloroethane
200 33 ug/L 05/15/23 19:24 100100 U1,1-Dichloroethene
100 22 ug/L 05/14/23 21:27 10050 U1,2-Dichloropropane
100 20 ug/L 05/14/23 21:27 100300 DEthylbenzene
2000 320 ug/L 05/14/23 21:27 1001000 U2-Hexanone
200 26 ug/L 05/14/23 21:27 100100 UIsopropylbenzene
2000 320 ug/L 05/14/23 21:27 1001000 UMethyl acetate
200 33 ug/L 05/14/23 21:27 10035 J D MMethylcyclohexane
2000 320 ug/L 05/14/23 21:27 1001000 U QMethylene Chloride
2000 270 ug/L 05/14/23 21:27 1001000 U4-Methyl-2-pentanone (MIBK)
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-5Client Sample ID: MW7-18-05-23
Matrix: WaterDate Collected: 05/01/23 13:35
Date Received: 05/02/23 10:30
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
200 U 500 81 ug/L 05/14/23 21:27 100
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Methyl tert-butyl ether
200 27 ug/L 05/14/23 21:27 100100 U MStyrene
200 40 ug/L 05/14/23 21:27 100100 U1,1,2,2-Tetrachloroethane
200 35 ug/L 05/14/23 21:27 100100 UTetrachloroethene
200 25 ug/L 05/14/23 21:27 1001400 DToluene
200 34 ug/L 05/14/23 21:27 100100 Utrans-1,2-Dichloroethene
200 23 ug/L 05/14/23 21:27 100100 Utrans-1,3-Dichloropropene
500 53 ug/L 05/14/23 21:27 100200 U1,2,4-Trichlorobenzene
100 21 ug/L 05/14/23 21:27 10050 U1,1,1-Trichloroethane
200 32 ug/L 05/14/23 21:27 100100 U1,1,2-Trichloroethane
100 20 ug/L 05/14/23 21:27 10050 UTrichloroethene
200 33 ug/L 05/14/23 21:27 100100 UTrichlorofluoromethane
100 23 ug/L 05/14/23 21:27 10050 U1,1,2-Trichloro-1,2,2-trifluoroethane
200 40 ug/L 05/14/23 21:27 100100 U QVinyl chloride
200 49 ug/L 05/14/23 21:27 1001500 DXylenes, Total
4-Bromofluorobenzene (Surr)106 85-114 05/14/23 21:27 100
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr)105 05/15/23 19:24 10085-114
Dibromofluoromethane (Surr)82 05/14/23 21:27 10080-119
Dibromofluoromethane (Surr)106 05/15/23 19:24 10080-119
1,2-Dichloroethane-d4 (Surr)78 Q 05/14/23 21:27 10081-118
1,2-Dichloroethane-d4 (Surr)92 05/15/23 19:24 10081-118
Toluene-d8 (Surr)89 05/14/23 21:27 10089-112
Toluene-d8 (Surr)113 Q 05/15/23 19:24 10089-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
10 U 20 4.4 ug/L 05/03/23 18:10 05/08/23 19:09 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Acenaphthene
20 3.6 ug/L 05/03/23 18:10 05/08/23 19:09 110 UAcenaphthylene
10 2.2 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 U MAcetophenone
20 3.6 ug/L 05/03/23 18:10 05/08/23 19:09 110 UAnthracene
10 2.2 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 UAtrazine
20 4.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 U MBenzaldehyde
20 4.2 ug/L 05/03/23 18:10 05/08/23 19:09 110 UBenzo[a]anthracene
20 2.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 UBenzo[a]pyrene
20 3.1 ug/L 05/03/23 18:10 05/08/23 19:09 110 UBenzo[b]fluoranthene
20 3.0 ug/L 05/03/23 18:10 05/08/23 19:09 110 UBenzo[g,h,i]perylene
20 2.9 ug/L 05/03/23 18:10 05/08/23 19:09 110 U QBenzo[k]fluoranthene
20 4.6 ug/L 05/03/23 18:10 05/08/23 19:09 110 U1,1'-Biphenyl
10 1.8 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 UBis(2-chloroethoxy)methane
20 3.6 ug/L 05/03/23 18:10 05/08/23 19:09 110 U MBis(2-chloroethyl)ether
20 3.0 ug/L 05/03/23 18:10 05/08/23 19:09 16.3 J BBis(2-ethylhexyl) phthalate
20 4.7 ug/L 05/03/23 18:10 05/08/23 19:09 110 U M4-Bromophenyl phenyl ether
20 2.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 UButyl benzyl phthalate
20 2.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 UCaprolactam
10 1.8 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 UCarbazole
10 1.0 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 U M Q4-Chloroaniline
20 2.5 ug/L 05/03/23 18:10 05/08/23 19:09 110 U4-Chloro-3-methylphenol
20 4.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2-Chloronaphthalene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-5Client Sample ID: MW7-18-05-23
Matrix: WaterDate Collected: 05/01/23 13:35
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 3.2 ug/L 05/03/23 18:10 05/08/23 19:09 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Chlorophenol
20 5.3 ug/L 05/03/23 18:10 05/08/23 19:09 112 U4-Chlorophenyl phenyl ether
20 3.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 UChrysene
20 3.0 ug/L 05/03/23 18:10 05/08/23 19:09 110 UDibenz(a,h)anthracene
10 1.9 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 UDibenzofuran
50 10 ug/L 05/03/23 18:10 05/08/23 19:09 120 U3,3'-Dichlorobenzidine
20 3.7 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2,4-Dichlorophenol
10 2.2 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 UDiethyl phthalate
20 3.0 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2,4-Dimethylphenol
10 2.1 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 UDimethyl phthalate
10 2.3 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 UDi-n-butyl phthalate
50 5.3 ug/L 05/03/23 18:10 05/08/23 19:09 120 U Q4,6-Dinitro-2-methylphenol
50 16 ug/L 05/03/23 18:10 05/08/23 19:09 140 U Q2,4-Dinitrophenol
10 2.3 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 U2,4-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2,6-Dinitrotoluene
20 2.8 ug/L 05/03/23 18:10 05/08/23 19:09 110 U MDi-n-octyl phthalate
10 1.6 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 UFluoranthene
20 3.4 ug/L 05/03/23 18:10 05/08/23 19:09 110 UFluorene
10 1.6 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 UHexachlorobenzene
20 4.0 ug/L 05/03/23 18:10 05/08/23 19:09 110 UHexachlorobutadiene
20 3.5 ug/L 05/03/23 18:10 05/08/23 19:09 110 UHexachlorocyclopentadiene
20 3.6 ug/L 05/03/23 18:10 05/08/23 19:09 110 UHexachloroethane
20 4.3 ug/L 05/03/23 18:10 05/08/23 19:09 110 UIndeno[1,2,3-cd]pyrene
10 2.0 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 UIsophorone
20 4.6 ug/L 05/03/23 18:10 05/08/23 19:09 1432-Methylnaphthalene
10 1.8 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 U M2-Methylphenol
10 1.4 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 U3 & 4 Methylphenol
20 3.5 ug/L 05/03/23 18:10 05/08/23 19:09 1110Naphthalene
20 2.9 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 19:09 110 U3-Nitroaniline
50 3.0 ug/L 05/03/23 18:10 05/08/23 19:09 110 U4-Nitroaniline
20 3.5 ug/L 05/03/23 18:10 05/08/23 19:09 110 UNitrobenzene
20 3.9 ug/L 05/03/23 18:10 05/08/23 19:09 110 U M2-Nitrophenol
50 8.1 ug/L 05/03/23 18:10 05/08/23 19:09 120 U4-Nitrophenol
10 2.4 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 UN-Nitrosodi-n-propylamine
20 2.9 ug/L 05/03/23 18:10 05/08/23 19:09 110 UN-Nitrosodiphenylamine
20 3.1 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2,2'-oxybis[1-chloropropane]
50 9.9 ug/L 05/03/23 18:10 05/08/23 19:09 120 UPentachlorophenol
20 4.3 ug/L 05/03/23 18:10 05/08/23 19:09 110 UPhenanthrene
10 1.5 ug/L 05/03/23 18:10 05/08/23 19:09 14.0 U MPhenol
20 3.7 ug/L 05/03/23 18:10 05/08/23 19:09 110 UPyrene
20 3.3 ug/L 05/03/23 18:10 05/08/23 19:09 110 U2,4,5-Trichlorophenol
20 2.2 ug/L 05/03/23 18:10 05/08/23 19:09 15.0 U2,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)60 44-119 05/03/23 18:10 05/08/23 19:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)27 05/03/23 18:10 05/08/23 19:09 119-119
Nitrobenzene-d5 (Surr)49 05/03/23 18:10 05/08/23 19:09 144-120
Phenol-d5 (Surr)18 05/03/23 18:10 05/08/23 19:09 110-130
Terphenyl-d14 (Surr)98 Q 05/03/23 18:10 05/08/23 19:09 150-134
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-5Client Sample ID: MW7-18-05-23
Matrix: WaterDate Collected: 05/01/23 13:35
Date Received: 05/02/23 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)86 Q 43-140 05/03/23 18:10 05/08/23 19:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
10000 100 20 ug/L 05/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.0 U 5.0 1.0 ug/L 05/10/23 23:13 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Methyl tert-butyl ether
6.0 2.0 ug/L 05/10/23 23:13 1170Naphthalene
a,a,a-Trifluorotoluene (fid)425 Q 70-130 05/10/23 23:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)227 Q 05/10/23 23:13 170-130
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) - DL
LOQ DL
1200 D 100 20 ug/L 05/12/23 00:43 20
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Benzene
2000 500 ug/L 05/12/23 00:43 205500 D MC5-C8 Aliphatics
2000 200 ug/L 05/12/23 00:43 201200 J D MC9-C10 Aromatics
2000 500 ug/L 05/12/23 00:43 204500 D MC9-C12 Aliphatics
100 20 ug/L 05/12/23 00:43 20240 DEthylbenzene
100 20 ug/L 05/12/23 00:43 201200 DToluene
2000 500 ug/L 05/12/23 00:43 201800 J DC9-C12 Aliphatics (adjusted)
200 50 ug/L 05/12/23 00:43 20810 Dm-Xylene & p-Xylene
100 20 ug/L 05/12/23 00:43 20420 Do-Xylene
2000 500 ug/L 05/12/23 00:43 203000 DC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)114 70-130 05/12/23 00:43 20
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid)99 05/12/23 00:43 2070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U M 1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Anthracene
100 30 ug/L 06/01/23 14:56 1610Total EPH
12 4.8 ug/L 05/12/23 08:50 05/18/23 01:48 19.7 U MPyrene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 UBenzo[g,h,i]perylene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 UIndeno[1,2,3-cd]pyrene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 UBenzo[b]fluoranthene
1.9 0.48 ug/L 05/12/23 08:50 05/18/23 01:48 10.97 U MFluoranthene
3.9 1.4 ug/L 05/12/23 08:50 05/18/23 01:48 12.9 UBenzo[k]fluoranthene
1.9 0.68 ug/L 05/12/23 08:50 05/18/23 01:48 14.9 MAcenaphthylene
1.9 0.48 ug/L 05/12/23 08:50 05/18/23 01:48 10.97 UChrysene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 UBenzo[a]pyrene
1.9 0.48 ug/L 05/12/23 08:50 05/18/23 01:48 10.97 UDibenz(a,h)anthracene
1.9 0.68 ug/L 05/12/23 08:50 05/18/23 01:48 11.4 UBenzo[a]anthracene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 U MAcenaphthene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 U MPhenanthrene
1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 11.2 U MFluorene
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Client Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Lab Sample ID: 680-234374-5Client Sample ID: MW7-18-05-23
Matrix: WaterDate Collected: 05/01/23 13:35
Date Received: 05/02/23 10:30
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
42 M 1.9 0.58 ug/L 05/12/23 08:50 05/18/23 01:48 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
2-Methylnaphthalene
39 9.7 ug/L 05/12/23 08:50 05/18/23 01:48 1270 MC11-C22 Aromatics (unadjusted)
48 9.7 ug/L 05/12/23 08:50 05/18/23 01:48 119 UC19-C36 Aliphatics
29 9.7 ug/L 05/12/23 08:50 05/18/23 01:48 1340 B QC9-C18 Aliphatics
1-Chlorooctadecane (Surr)53 40-140 05/12/23 08:50 05/18/23 01:48 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr)66 M 05/12/23 08:50 05/18/23 01:48 140-140
o- terphenyl (Surr)55 05/12/23 08:50 05/18/23 01:48 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
LOQ DL
110 D M 9.7 2.9 ug/L 05/12/23 08:50 05/18/23 16:20 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Naphthalene
190 48 ug/L 05/12/23 08:50 05/18/23 16:20 5150 J DC11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)66 M 40-140 05/12/23 08:50 05/18/23 16:20 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
o- terphenyl (Surr)56 05/12/23 08:50 05/18/23 16:20 540-140
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-778568/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778568
LOQ DL
Acetone 10 U 25 3.7 ug/L 05/14/23 14:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
1.0 U M 0.272.0 ug/L 05/14/23 14:45 1Benzene
2.0 U 0.592.5 ug/L 05/14/23 14:45 1Bromoform
10 U 3.720 ug/L 05/14/23 14:45 1Bromomethane
20 U 6.425 ug/L 05/14/23 14:45 12-Butanone (MEK)
1.0 U 0.432.0 ug/L 05/14/23 14:45 1Carbon disulfide
1.0 U 0.302.0 ug/L 05/14/23 14:45 1Carbon tetrachloride
0.50 U 0.151.0 ug/L 05/14/23 14:45 1Chlorobenzene
1.0 U 0.392.0 ug/L 05/14/23 14:45 1Chlorodibromomethane
10 U 4.620 ug/L 05/14/23 14:45 1Chloroethane
1.0 U 0.272.0 ug/L 05/14/23 14:45 1Chloroform
2.0 U 0.542.5 ug/L 05/14/23 14:45 1Chloromethane
1.0 U 0.252.0 ug/L 05/14/23 14:45 1cis-1,2-Dichloroethene
1.0 U 0.262.0 ug/L 05/14/23 14:45 1cis-1,3-Dichloropropene
1.0 U 0.282.0 ug/L 05/14/23 14:45 1Cyclohexane
5.0 U 1.810 ug/L 05/14/23 14:45 11,2-Dibromo-3-Chloropropane
1.0 U 0.332.0 ug/L 05/14/23 14:45 11,2-Dibromoethane (EDB)
1.0 U 0.312.0 ug/L 05/14/23 14:45 11,2-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/14/23 14:45 11,3-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/14/23 14:45 11,4-Dichlorobenzene
1.0 U 0.252.0 ug/L 05/14/23 14:45 1Dichlorobromomethane
1.0 U 0.362.0 ug/L 05/14/23 14:45 1Dichlorodifluoromethane
1.0 U 0.332.0 ug/L 05/14/23 14:45 11,1-Dichloroethane
1.0 U M 0.252.0 ug/L 05/14/23 14:45 11,2-Dichloroethane
1.0 U 0.332.0 ug/L 05/14/23 14:45 11,1-Dichloroethene
0.50 U 0.221.0 ug/L 05/14/23 14:45 11,2-Dichloropropane
0.50 U 0.201.0 ug/L 05/14/23 14:45 1Ethylbenzene
10 U 3.220 ug/L 05/14/23 14:45 12-Hexanone
1.0 U 0.262.0 ug/L 05/14/23 14:45 1Isopropylbenzene
10 U 3.220 ug/L 05/14/23 14:45 1Methyl acetate
1.0 U 0.332.0 ug/L 05/14/23 14:45 1Methylcyclohexane
10 U 3.220 ug/L 05/14/23 14:45 1Methylene Chloride
10 U 2.720 ug/L 05/14/23 14:45 14-Methyl-2-pentanone (MIBK)
2.0 U 0.815.0 ug/L 05/14/23 14:45 1Methyl tert-butyl ether
1.0 U 0.272.0 ug/L 05/14/23 14:45 1Styrene
1.0 U 0.402.0 ug/L 05/14/23 14:45 11,1,2,2-Tetrachloroethane
1.0 U 0.352.0 ug/L 05/14/23 14:45 1Tetrachloroethene
1.0 U 0.252.0 ug/L 05/14/23 14:45 1Toluene
1.0 U 0.342.0 ug/L 05/14/23 14:45 1trans-1,2-Dichloroethene
1.0 U 0.232.0 ug/L 05/14/23 14:45 1trans-1,3-Dichloropropene
2.0 U M 0.535.0 ug/L 05/14/23 14:45 11,2,4-Trichlorobenzene
0.50 U 0.211.0 ug/L 05/14/23 14:45 11,1,1-Trichloroethane
1.0 U 0.322.0 ug/L 05/14/23 14:45 11,1,2-Trichloroethane
0.50 U 0.201.0 ug/L 05/14/23 14:45 1Trichloroethene
1.0 U 0.332.0 ug/L 05/14/23 14:45 1Trichlorofluoromethane
0.50 U 0.231.0 ug/L 05/14/23 14:45 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 0.402.0 ug/L 05/14/23 14:45 1Vinyl chloride
1.0 U 0.492.0 ug/L 05/14/23 14:45 1Xylenes, Total
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-778568/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778568
4-Bromofluorobenzene (Surr)109 85-114 05/14/23 14:45 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
88 05/14/23 14:45 1Dibromofluoromethane (Surr)80-119
82 05/14/23 14:45 11,2-Dichloroethane-d4 (Surr)81-118
94 05/14/23 14:45 1Toluene-d8 (Surr)89-112
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778568/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778568
Acetone 250 236 ug/L 94 39 -160
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Benzene 50.0 41.3 ug/L 83 79 -120
Bromoform 50.0 56.2 ug/L 112 66 -130
Bromomethane 50.0 40.2 ug/L 80 53 -141
2-Butanone (MEK)250 247 ug/L 99 56 -143
Carbon disulfide 50.0 33.1 ug/L 66 64 -133
Carbon tetrachloride 50.0 44.4 ug/L 89 72 -136
Chlorobenzene 50.0 51.8 ug/L 104 82 -118
Chlorodibromomethane 50.0 45.7 ug/L 91 74 -126
Chloroethane 50.0 26.2 Q ug/L 52 60 -138
Chloroform 50.0 42.2 ug/L 84 79 -124
Chloromethane 50.0 34.9 M ug/L 70 50 -139
cis-1,2-Dichloroethene 50.0 41.1 ug/L 82 78 -123
cis-1,3-Dichloropropene 50.0 46.5 ug/L 93 75 -124
Cyclohexane 50.0 40.9 ug/L 82 71 -130
1,2-Dibromo-3-Chloropropane 50.0 62.3 ug/L 125 62 -128
1,2-Dibromoethane (EDB)50.0 44.6 ug/L 89 75 -127
1,2-Dichlorobenzene 50.0 52.6 ug/L 105 80 -119
1,3-Dichlorobenzene 50.0 51.7 ug/L 103 80 -119
1,4-Dichlorobenzene 50.0 51.5 ug/L 103 79 -118
Dichlorobromomethane 50.0 40.9 ug/L 82 79 -125
Dichlorodifluoromethane 50.0 41.4 ug/L 83 32 -152
1,1-Dichloroethane 50.0 39.8 ug/L 80 77 -125
1,2-Dichloroethane 50.0 39.0 ug/L 78 73 -128
1,1-Dichloroethene 50.0 33.2 Q ug/L 66 71 -131
1,2-Dichloropropane 50.0 42.1 ug/L 84 78 -122
Ethylbenzene 50.0 50.7 ug/L 101 79 -121
2-Hexanone 250 257 ug/L 103 57 -139
Isopropylbenzene 50.0 50.2 ug/L 100 72 -131
Methyl acetate 100 81.2 ug/L 81 56 -136
Methylcyclohexane 50.0 42.8 ug/L 86 72 -132
Methylene Chloride 50.0 39.3 ug/L 79 74 -124
4-Methyl-2-pentanone (MIBK)250 230 ug/L 92 67 -130
Methyl tert-butyl ether 50.0 46.7 ug/L 93 71 -124
Styrene 50.0 46.8 ug/L 94 78 -123
1,1,2,2-Tetrachloroethane 50.0 54.8 ug/L 110 71 -121
Tetrachloroethene 50.0 43.1 ug/L 86 74 -129
Toluene 50.0 45.7 ug/L 91 80 -121
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778568/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778568
trans-1,2-Dichloroethene 50.0 40.4 ug/L 81 75 -124
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
trans-1,3-Dichloropropene 50.0 42.4 ug/L 85 73 -127
1,2,4-Trichlorobenzene 50.0 56.3 ug/L 113 69 -130
1,1,1-Trichloroethane 50.0 41.0 ug/L 82 74 -131
1,1,2-Trichloroethane 50.0 45.4 ug/L 91 80 -119
Trichloroethene 50.0 45.1 ug/L 90 79 -123
Trichlorofluoromethane 50.0 45.1 ug/L 90 65 -141
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 41.4 ug/L 83 70 -136
Vinyl chloride 50.0 34.2 ug/L 68 58 -137
Xylenes, Total 100 102 ug/L 102 79 -121
4-Bromofluorobenzene (Surr)85 -114
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
86Dibromofluoromethane (Surr)80 -119
851,2-Dichloroethane-d4 (Surr)81 -118
91Toluene-d8 (Surr)89 -112
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-778568/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778568
Acetone 250 242 ug/L 97 39 -160 3 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 50.0 40.9 ug/L 82 79 -120 1 20
Bromoform 50.0 56.7 ug/L 113 66 -130 1 20
Bromomethane 50.0 39.2 ug/L 78 53 -141 3 20
2-Butanone (MEK)250 255 ug/L 102 56 -143 3 20
Carbon disulfide 50.0 32.6 ug/L 65 64 -133 1 20
Carbon tetrachloride 50.0 44.0 ug/L 88 72 -136 1 20
Chlorobenzene 50.0 51.7 ug/L 103 82 -118 0 20
Chlorodibromomethane 50.0 44.9 ug/L 90 74 -126 2 20
Chloroethane 50.0 26.1 Q ug/L 52 60 -138 0 20
Chloroform 50.0 41.9 ug/L 84 79 -124 1 20
Chloromethane 50.0 34.6 M ug/L 69 50 -139 1 20
cis-1,2-Dichloroethene 50.0 40.5 ug/L 81 78 -123 2 20
cis-1,3-Dichloropropene 50.0 46.5 ug/L 93 75 -124 0 20
Cyclohexane 50.0 40.8 ug/L 82 71 -130 0 20
1,2-Dibromo-3-Chloropropane 50.0 62.3 ug/L 125 62 -128 0 20
1,2-Dibromoethane (EDB)50.0 44.9 ug/L 90 75 -127 1 20
1,2-Dichlorobenzene 50.0 52.0 ug/L 104 80 -119 1 20
1,3-Dichlorobenzene 50.0 51.0 ug/L 102 80 -119 1 20
1,4-Dichlorobenzene 50.0 51.0 ug/L 102 79 -118 1 20
Dichlorobromomethane 50.0 40.8 ug/L 82 79 -125 0 20
Dichlorodifluoromethane 50.0 40.8 ug/L 82 32 -152 2 20
1,1-Dichloroethane 50.0 39.4 ug/L 79 77 -125 1 20
1,2-Dichloroethane 50.0 39.4 ug/L 79 73 -128 1 20
1,1-Dichloroethene 50.0 32.6 Q ug/L 65 71 -131 2 20
1,2-Dichloropropane 50.0 42.2 ug/L 84 78 -122 0 20
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-778568/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778568
Ethylbenzene 50.0 50.3 ug/L 101 79 -121 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Hexanone 250 263 ug/L 105 57 -139 2 20
Isopropylbenzene 50.0 49.1 ug/L 98 72 -131 2 20
Methyl acetate 100 82.9 ug/L 83 56 -136 2 20
Methylcyclohexane 50.0 42.6 ug/L 85 72 -132 0 20
Methylene Chloride 50.0 39.3 ug/L 79 74 -124 0 20
4-Methyl-2-pentanone (MIBK)250 233 ug/L 93 67 -130 1 20
Methyl tert-butyl ether 50.0 46.6 ug/L 93 71 -124 0 20
Styrene 50.0 46.7 ug/L 93 78 -123 0 20
1,1,2,2-Tetrachloroethane 50.0 55.7 ug/L 111 71 -121 2 20
Tetrachloroethene 50.0 43.2 ug/L 86 74 -129 0 20
Toluene 50.0 45.0 ug/L 90 80 -121 1 20
trans-1,2-Dichloroethene 50.0 40.1 ug/L 80 75 -124 1 20
trans-1,3-Dichloropropene 50.0 42.7 ug/L 85 73 -127 1 20
1,2,4-Trichlorobenzene 50.0 56.8 ug/L 114 69 -130 1 20
1,1,1-Trichloroethane 50.0 40.7 ug/L 81 74 -131 1 20
1,1,2-Trichloroethane 50.0 46.2 ug/L 92 80 -119 2 20
Trichloroethene 50.0 44.8 ug/L 90 79 -123 1 20
Trichlorofluoromethane 50.0 44.5 ug/L 89 65 -141 1 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 40.8 ug/L 82 70 -136 1 20
Vinyl chloride 50.0 33.7 ug/L 67 58 -137 1 20
Xylenes, Total 100 100 ug/L 100 79 -121 1 20
4-Bromofluorobenzene (Surr)85 -114
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
86Dibromofluoromethane (Surr)80 -119
861,2-Dichloroethane-d4 (Surr)81 -118
90Toluene-d8 (Surr)89 -112
Client Sample ID: Method BlankLab Sample ID: MB 680-778627/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
LOQ DL
Acetone 10 U 25 3.7 ug/L 05/15/23 14:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
1.0 U 0.272.0 ug/L 05/15/23 14:16 1Benzene
2.0 U 0.592.5 ug/L 05/15/23 14:16 1Bromoform
10 U 3.720 ug/L 05/15/23 14:16 1Bromomethane
20 U 6.425 ug/L 05/15/23 14:16 12-Butanone (MEK)
1.0 U 0.432.0 ug/L 05/15/23 14:16 1Carbon disulfide
1.0 U 0.302.0 ug/L 05/15/23 14:16 1Carbon tetrachloride
0.50 U 0.151.0 ug/L 05/15/23 14:16 1Chlorobenzene
1.0 U 0.392.0 ug/L 05/15/23 14:16 1Chlorodibromomethane
10 U 4.620 ug/L 05/15/23 14:16 1Chloroethane
1.0 U 0.272.0 ug/L 05/15/23 14:16 1Chloroform
2.0 U 0.542.5 ug/L 05/15/23 14:16 1Chloromethane
1.0 U 0.252.0 ug/L 05/15/23 14:16 1cis-1,2-Dichloroethene
1.0 U 0.262.0 ug/L 05/15/23 14:16 1cis-1,3-Dichloropropene
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-778627/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
LOQ DL
Cyclohexane 1.0 U 2.0 0.28 ug/L 05/15/23 14:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
5.0 U 1.810 ug/L 05/15/23 14:16 11,2-Dibromo-3-Chloropropane
1.0 U 0.332.0 ug/L 05/15/23 14:16 11,2-Dibromoethane (EDB)
1.0 U 0.312.0 ug/L 05/15/23 14:16 11,2-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/15/23 14:16 11,3-Dichlorobenzene
1.0 U 0.312.0 ug/L 05/15/23 14:16 11,4-Dichlorobenzene
1.0 U 0.252.0 ug/L 05/15/23 14:16 1Dichlorobromomethane
1.0 U 0.362.0 ug/L 05/15/23 14:16 1Dichlorodifluoromethane
1.0 U 0.332.0 ug/L 05/15/23 14:16 11,1-Dichloroethane
1.0 U M 0.252.0 ug/L 05/15/23 14:16 11,2-Dichloroethane
1.0 U 0.332.0 ug/L 05/15/23 14:16 11,1-Dichloroethene
0.50 U 0.221.0 ug/L 05/15/23 14:16 11,2-Dichloropropane
0.50 U 0.201.0 ug/L 05/15/23 14:16 1Ethylbenzene
10 U 3.220 ug/L 05/15/23 14:16 12-Hexanone
1.0 U 0.262.0 ug/L 05/15/23 14:16 1Isopropylbenzene
10 U 3.220 ug/L 05/15/23 14:16 1Methyl acetate
1.0 U 0.332.0 ug/L 05/15/23 14:16 1Methylcyclohexane
10 U 3.220 ug/L 05/15/23 14:16 1Methylene Chloride
10 U 2.720 ug/L 05/15/23 14:16 14-Methyl-2-pentanone (MIBK)
2.0 U 0.815.0 ug/L 05/15/23 14:16 1Methyl tert-butyl ether
1.0 U 0.272.0 ug/L 05/15/23 14:16 1Styrene
1.0 U 0.402.0 ug/L 05/15/23 14:16 11,1,2,2-Tetrachloroethane
1.0 U 0.352.0 ug/L 05/15/23 14:16 1Tetrachloroethene
1.0 U 0.252.0 ug/L 05/15/23 14:16 1Toluene
1.0 U 0.342.0 ug/L 05/15/23 14:16 1trans-1,2-Dichloroethene
1.0 U 0.232.0 ug/L 05/15/23 14:16 1trans-1,3-Dichloropropene
2.0 U 0.535.0 ug/L 05/15/23 14:16 11,2,4-Trichlorobenzene
0.50 U 0.211.0 ug/L 05/15/23 14:16 11,1,1-Trichloroethane
1.0 U 0.322.0 ug/L 05/15/23 14:16 11,1,2-Trichloroethane
0.50 U 0.201.0 ug/L 05/15/23 14:16 1Trichloroethene
1.0 U 0.332.0 ug/L 05/15/23 14:16 1Trichlorofluoromethane
0.50 U 0.231.0 ug/L 05/15/23 14:16 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 0.402.0 ug/L 05/15/23 14:16 1Vinyl chloride
1.0 U 0.492.0 ug/L 05/15/23 14:16 1Xylenes, Total
4-Bromofluorobenzene (Surr)108 85-114 05/15/23 14:16 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
104 05/15/23 14:16 1Dibromofluoromethane (Surr)80-119
91 05/15/23 14:16 11,2-Dichloroethane-d4 (Surr)81-118
119 Q 05/15/23 14:16 1Toluene-d8 (Surr)89-112
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778627/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
Acetone 250 248 ug/L 99 39 -160
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Benzene 50.0 46.2 ug/L 92 79 -120
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778627/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
Bromoform 50.0 59.5 ug/L 119 66 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Bromomethane 50.0 69.4 ug/L 139 53 -141
2-Butanone (MEK)250 202 ug/L 81 56 -143
Carbon disulfide 50.0 40.6 ug/L 81 64 -133
Carbon tetrachloride 50.0 54.2 ug/L 108 72 -136
Chlorobenzene 50.0 54.5 ug/L 109 82 -118
Chlorodibromomethane 50.0 54.9 ug/L 110 74 -126
Chloroethane 50.0 53.6 ug/L 107 60 -138
Chloroform 50.0 52.8 ug/L 106 79 -124
Chloromethane 50.0 44.6 ug/L 89 50 -139
cis-1,2-Dichloroethene 50.0 48.5 ug/L 97 78 -123
cis-1,3-Dichloropropene 50.0 49.9 ug/L 100 75 -124
Cyclohexane 50.0 45.3 ug/L 91 71 -130
1,2-Dibromo-3-Chloropropane 50.0 52.9 ug/L 106 62 -128
1,2-Dibromoethane (EDB)50.0 54.4 ug/L 109 75 -127
1,2-Dichlorobenzene 50.0 51.7 ug/L 103 80 -119
1,3-Dichlorobenzene 50.0 51.7 ug/L 103 80 -119
1,4-Dichlorobenzene 50.0 50.1 ug/L 100 79 -118
Dichlorobromomethane 50.0 53.4 ug/L 107 79 -125
Dichlorodifluoromethane 50.0 49.3 ug/L 99 32 -152
1,1-Dichloroethane 50.0 47.9 ug/L 96 77 -125
1,2-Dichloroethane 50.0 53.1 ug/L 106 73 -128
1,1-Dichloroethene 50.0 44.0 ug/L 88 71 -131
1,2-Dichloropropane 50.0 45.9 ug/L 92 78 -122
Ethylbenzene 50.0 53.4 ug/L 107 79 -121
2-Hexanone 250 215 ug/L 86 57 -139
Isopropylbenzene 50.0 54.6 ug/L 109 72 -131
Methyl acetate 100 75.3 ug/L 75 56 -136
Methylcyclohexane 50.0 44.5 ug/L 89 72 -132
Methylene Chloride 50.0 47.4 ug/L 95 74 -124
4-Methyl-2-pentanone (MIBK)250 198 ug/L 79 67 -130
Methyl tert-butyl ether 50.0 44.6 ug/L 89 71 -124
Styrene 50.0 59.2 ug/L 118 78 -123
1,1,2,2-Tetrachloroethane 50.0 44.6 ug/L 89 71 -121
Tetrachloroethene 50.0 52.6 ug/L 105 74 -129
Toluene 50.0 50.6 ug/L 101 80 -121
trans-1,2-Dichloroethene 50.0 53.2 ug/L 106 75 -124
trans-1,3-Dichloropropene 50.0 50.5 ug/L 101 73 -127
1,2,4-Trichlorobenzene 50.0 51.9 ug/L 104 69 -130
1,1,1-Trichloroethane 50.0 53.0 ug/L 106 74 -131
1,1,2-Trichloroethane 50.0 48.2 ug/L 96 80 -119
Trichloroethene 50.0 53.8 ug/L 108 79 -123
Trichlorofluoromethane 50.0 53.8 ug/L 108 65 -141
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 50.1 ug/L 100 70 -136
Vinyl chloride 50.0 45.3 ug/L 91 58 -137
Xylenes, Total 100 108 ug/L 108 79 -121
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778627/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
4-Bromofluorobenzene (Surr)85 -114
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
114Dibromofluoromethane (Surr)80 -119
1061,2-Dichloroethane-d4 (Surr)81 -118
105Toluene-d8 (Surr)89 -112
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-778627/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
Acetone 250 255 ug/L 102 39 -160 3 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 50.0 45.6 ug/L 91 79 -120 1 20
Bromoform 50.0 60.4 ug/L 121 66 -130 2 20
Bromomethane 50.0 67.7 ug/L 135 53 -141 2 20
2-Butanone (MEK)250 209 ug/L 83 56 -143 3 20
Carbon disulfide 50.0 40.0 ug/L 80 64 -133 2 20
Carbon tetrachloride 50.0 54.3 ug/L 109 72 -136 0 20
Chlorobenzene 50.0 55.2 ug/L 110 82 -118 1 20
Chlorodibromomethane 50.0 55.5 ug/L 111 74 -126 1 20
Chloroethane 50.0 51.1 ug/L 102 60 -138 5 20
Chloroform 50.0 52.8 ug/L 106 79 -124 0 20
Chloromethane 50.0 44.2 ug/L 88 50 -139 1 20
cis-1,2-Dichloroethene 50.0 48.7 ug/L 97 78 -123 0 20
cis-1,3-Dichloropropene 50.0 50.3 ug/L 101 75 -124 1 20
Cyclohexane 50.0 45.0 ug/L 90 71 -130 1 20
1,2-Dibromo-3-Chloropropane 50.0 54.0 ug/L 108 62 -128 2 20
1,2-Dibromoethane (EDB)50.0 55.2 ug/L 110 75 -127 1 20
1,2-Dichlorobenzene 50.0 51.9 ug/L 104 80 -119 1 20
1,3-Dichlorobenzene 50.0 52.2 ug/L 104 80 -119 1 20
1,4-Dichlorobenzene 50.0 50.1 ug/L 100 79 -118 0 20
Dichlorobromomethane 50.0 53.0 ug/L 106 79 -125 1 20
Dichlorodifluoromethane 50.0 50.1 ug/L 100 32 -152 2 20
1,1-Dichloroethane 50.0 47.9 ug/L 96 77 -125 0 20
1,2-Dichloroethane 50.0 52.8 ug/L 106 73 -128 1 20
1,1-Dichloroethene 50.0 41.4 ug/L 83 71 -131 6 20
1,2-Dichloropropane 50.0 45.5 ug/L 91 78 -122 1 20
Ethylbenzene 50.0 53.5 ug/L 107 79 -121 0 20
2-Hexanone 250 219 ug/L 88 57 -139 2 20
Isopropylbenzene 50.0 54.9 ug/L 110 72 -131 1 20
Methyl acetate 100 77.3 ug/L 77 56 -136 3 20
Methylcyclohexane 50.0 44.5 ug/L 89 72 -132 0 20
Methylene Chloride 50.0 47.8 ug/L 96 74 -124 1 20
4-Methyl-2-pentanone (MIBK)250 201 ug/L 81 67 -130 2 20
Methyl tert-butyl ether 50.0 45.2 ug/L 90 71 -124 1 20
Styrene 50.0 59.7 ug/L 119 78 -123 1 20
1,1,2,2-Tetrachloroethane 50.0 45.4 ug/L 91 71 -121 2 20
Tetrachloroethene 50.0 53.1 ug/L 106 74 -129 1 20
Toluene 50.0 50.2 ug/L 100 80 -121 1 20
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-778627/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778627
trans-1,2-Dichloroethene 50.0 52.5 ug/L 105 75 -124 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
trans-1,3-Dichloropropene 50.0 50.7 ug/L 101 73 -127 0 20
1,2,4-Trichlorobenzene 50.0 52.0 ug/L 104 69 -130 0 20
1,1,1-Trichloroethane 50.0 52.2 ug/L 104 74 -131 2 20
1,1,2-Trichloroethane 50.0 48.3 ug/L 97 80 -119 0 20
Trichloroethene 50.0 53.2 ug/L 106 79 -123 1 20
Trichlorofluoromethane 50.0 53.2 ug/L 106 65 -141 1 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 50.6 ug/L 101 70 -136 1 20
Vinyl chloride 50.0 44.8 ug/L 90 58 -137 1 20
Xylenes, Total 100 111 ug/L 111 79 -121 3 20
4-Bromofluorobenzene (Surr)85 -114
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
113Dibromofluoromethane (Surr)80 -119
1061,2-Dichloroethane-d4 (Surr)81 -118
106Toluene-d8 (Surr)89 -112
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-777555/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777551 Prep Batch: 777555
LOQ DL
Acenaphthene 10 U 20 4.4 ug/L 05/03/23 18:10 05/08/23 15:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 3.620 ug/L 05/03/23 18:10 05/08/23 15:28 1Acenaphthylene
5.0 U M 2.210 ug/L 05/03/23 18:10 05/08/23 15:28 1Acetophenone
10 U 3.620 ug/L 05/03/23 18:10 05/08/23 15:28 1Anthracene
5.0 U 2.210 ug/L 05/03/23 18:10 05/08/23 15:28 1Atrazine
10 U 4.820 ug/L 05/03/23 18:10 05/08/23 15:28 1Benzaldehyde
10 U 4.220 ug/L 05/03/23 18:10 05/08/23 15:28 1Benzo[a]anthracene
10 U 2.820 ug/L 05/03/23 18:10 05/08/23 15:28 1Benzo[a]pyrene
10 U 3.120 ug/L 05/03/23 18:10 05/08/23 15:28 1Benzo[b]fluoranthene
10 U 3.020 ug/L 05/03/23 18:10 05/08/23 15:28 1Benzo[g,h,i]perylene
10 U 2.920 ug/L 05/03/23 18:10 05/08/23 15:28 1Benzo[k]fluoranthene
10 U 4.620 ug/L 05/03/23 18:10 05/08/23 15:28 11,1'-Biphenyl
4.0 U 1.810 ug/L 05/03/23 18:10 05/08/23 15:28 1Bis(2-chloroethoxy)methane
10 U 3.620 ug/L 05/03/23 18:10 05/08/23 15:28 1Bis(2-chloroethyl)ether
10.5 J 3.020 ug/L 05/03/23 18:10 05/08/23 15:28 1Bis(2-ethylhexyl) phthalate
10 U 4.720 ug/L 05/03/23 18:10 05/08/23 15:28 14-Bromophenyl phenyl ether
10 U 2.820 ug/L 05/03/23 18:10 05/08/23 15:28 1Butyl benzyl phthalate
10 U 2.820 ug/L 05/03/23 18:10 05/08/23 15:28 1Caprolactam
4.0 U 1.810 ug/L 05/03/23 18:10 05/08/23 15:28 1Carbazole
4.0 U 1.010 ug/L 05/03/23 18:10 05/08/23 15:28 14-Chloroaniline
10 U 2.520 ug/L 05/03/23 18:10 05/08/23 15:28 14-Chloro-3-methylphenol
10 U 4.820 ug/L 05/03/23 18:10 05/08/23 15:28 12-Chloronaphthalene
10 U 3.220 ug/L 05/03/23 18:10 05/08/23 15:28 12-Chlorophenol
12 U 5.320 ug/L 05/03/23 18:10 05/08/23 15:28 14-Chlorophenyl phenyl ether
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-777555/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777551 Prep Batch: 777555
LOQ DL
Chrysene 10 U 20 3.8 ug/L 05/03/23 18:10 05/08/23 15:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 3.020 ug/L 05/03/23 18:10 05/08/23 15:28 1Dibenz(a,h)anthracene
4.0 U 1.910 ug/L 05/03/23 18:10 05/08/23 15:28 1Dibenzofuran
20 U 1050 ug/L 05/03/23 18:10 05/08/23 15:28 13,3'-Dichlorobenzidine
10 U 3.720 ug/L 05/03/23 18:10 05/08/23 15:28 12,4-Dichlorophenol
5.0 U 2.210 ug/L 05/03/23 18:10 05/08/23 15:28 1Diethyl phthalate
10 U 3.020 ug/L 05/03/23 18:10 05/08/23 15:28 12,4-Dimethylphenol
5.0 U 2.110 ug/L 05/03/23 18:10 05/08/23 15:28 1Dimethyl phthalate
5.0 U 2.310 ug/L 05/03/23 18:10 05/08/23 15:28 1Di-n-butyl phthalate
20 U 5.350 ug/L 05/03/23 18:10 05/08/23 15:28 14,6-Dinitro-2-methylphenol
40 U 1650 ug/L 05/03/23 18:10 05/08/23 15:28 12,4-Dinitrophenol
5.0 U 2.310 ug/L 05/03/23 18:10 05/08/23 15:28 12,4-Dinitrotoluene
10 U 2.820 ug/L 05/03/23 18:10 05/08/23 15:28 12,6-Dinitrotoluene
10 U M 2.820 ug/L 05/03/23 18:10 05/08/23 15:28 1Di-n-octyl phthalate
4.0 U 1.610 ug/L 05/03/23 18:10 05/08/23 15:28 1Fluoranthene
10 U 3.420 ug/L 05/03/23 18:10 05/08/23 15:28 1Fluorene
4.0 U 1.610 ug/L 05/03/23 18:10 05/08/23 15:28 1Hexachlorobenzene
10 U 4.020 ug/L 05/03/23 18:10 05/08/23 15:28 1Hexachlorobutadiene
10 U 3.520 ug/L 05/03/23 18:10 05/08/23 15:28 1Hexachlorocyclopentadiene
10 U 3.620 ug/L 05/03/23 18:10 05/08/23 15:28 1Hexachloroethane
10 U 4.320 ug/L 05/03/23 18:10 05/08/23 15:28 1Indeno[1,2,3-cd]pyrene
4.0 U 2.010 ug/L 05/03/23 18:10 05/08/23 15:28 1Isophorone
10 U 4.620 ug/L 05/03/23 18:10 05/08/23 15:28 12-Methylnaphthalene
4.0 U 1.810 ug/L 05/03/23 18:10 05/08/23 15:28 12-Methylphenol
4.0 U 1.410 ug/L 05/03/23 18:10 05/08/23 15:28 13 & 4 Methylphenol
10 U 3.520 ug/L 05/03/23 18:10 05/08/23 15:28 1Naphthalene
10 U 2.920 ug/L 05/03/23 18:10 05/08/23 15:28 12-Nitroaniline
10 U 3.050 ug/L 05/03/23 18:10 05/08/23 15:28 13-Nitroaniline
10 U 3.050 ug/L 05/03/23 18:10 05/08/23 15:28 14-Nitroaniline
10 U 3.520 ug/L 05/03/23 18:10 05/08/23 15:28 1Nitrobenzene
10 U 3.920 ug/L 05/03/23 18:10 05/08/23 15:28 12-Nitrophenol
20 U 8.150 ug/L 05/03/23 18:10 05/08/23 15:28 14-Nitrophenol
5.0 U 2.410 ug/L 05/03/23 18:10 05/08/23 15:28 1N-Nitrosodi-n-propylamine
10 U 2.920 ug/L 05/03/23 18:10 05/08/23 15:28 1N-Nitrosodiphenylamine
10 U 3.120 ug/L 05/03/23 18:10 05/08/23 15:28 12,2'-oxybis[1-chloropropane]
20 U 9.950 ug/L 05/03/23 18:10 05/08/23 15:28 1Pentachlorophenol
10 U 4.320 ug/L 05/03/23 18:10 05/08/23 15:28 1Phenanthrene
4.0 U 1.510 ug/L 05/03/23 18:10 05/08/23 15:28 1Phenol
10 U 3.720 ug/L 05/03/23 18:10 05/08/23 15:28 1Pyrene
10 U 3.320 ug/L 05/03/23 18:10 05/08/23 15:28 12,4,5-Trichlorophenol
5.0 U 2.220 ug/L 05/03/23 18:10 05/08/23 15:28 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)84 44-119 05/08/23 15:28 1
MB MB
Surrogate
05/03/23 18:10
Dil FacPrepared AnalyzedQualifier Limits%Recovery
38 05/03/23 18:10 05/08/23 15:28 12-Fluorophenol (Surr)19-119
69 05/03/23 18:10 05/08/23 15:28 1Nitrobenzene-d5 (Surr)44-120
24 05/03/23 18:10 05/08/23 15:28 1Phenol-d5 (Surr)10-130
107 05/03/23 18:10 05/08/23 15:28 1Terphenyl-d14 (Surr)50-134
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-777555/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777551 Prep Batch: 777555
2,4,6-Tribromophenol (Surr)99 43-140 05/08/23 15:28 1
MB MB
Surrogate
05/03/23 18:10
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777555/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777551 Prep Batch: 777555
Acenaphthene 200 130 ug/L 65 47 -122
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Acenaphthylene 200 138 ug/L 69 41 -130
Acetophenone 200 116 ug/L 58 46 -118
Anthracene 200 173 ug/L 86 57 -123
Atrazine 200 189 ug/L 94 44 -142
Benzaldehyde 200 106 ug/L 53 25 -130
Benzo[a]anthracene 200 209 ug/L 105 58 -125
Benzo[a]pyrene 200 205 ug/L 103 54 -128
Benzo[b]fluoranthene 200 193 ug/L 96 53 -131
Benzo[g,h,i]perylene 200 192 ug/L 96 50 -134
Benzo[k]fluoranthene 200 173 ug/L 86 57 -129
1,1'-Biphenyl 200 124 ug/L 62 49 -115
Bis(2-chloroethoxy)methane 200 122 ug/L 61 48 -120
Bis(2-chloroethyl)ether 200 106 ug/L 53 43 -118
Bis(2-ethylhexyl) phthalate 200 212 ug/L 106 55 -135
4-Bromophenyl phenyl ether 200 169 ug/L 85 55 -124
Butyl benzyl phthalate 200 222 ug/L 111 53 -134
Caprolactam 200 56.0 ug/L 28 13 -130
Carbazole 200 181 ug/L 91 60 -122
4-Chloroaniline 200 95.6 ug/L 48 33 -117
4-Chloro-3-methylphenol 200 137 ug/L 69 52 -119
2-Chloronaphthalene 200 125 ug/L 62 40 -116
2-Chlorophenol 200 94.8 ug/L 47 38 -117
4-Chlorophenyl phenyl ether 200 161 ug/L 81 53 -121
Chrysene 200 180 ug/L 90 59 -123
Dibenz(a,h)anthracene 200 199 ug/L 99 51 -134
Dibenzofuran 200 144 ug/L 72 53 -118
3,3'-Dichlorobenzidine 200 171 ug/L 85 27 -129
2,4-Dichlorophenol 200 123 ug/L 62 47 -121
Diethyl phthalate 200 175 ug/L 88 56 -125
2,4-Dimethylphenol 200 101 ug/L 51 31 -124
Dimethyl phthalate 200 162 ug/L 81 45 -127
Di-n-butyl phthalate 200 197 ug/L 98 56 -122
4,6-Dinitro-2-methylphenol 400 587 Q ug/L 147 44 -137
2,4-Dinitrophenol 400 583 Q ug/L 146 23 -143
2,4-Dinitrotoluene 200 188 ug/L 94 57 -128
2,6-Dinitrotoluene 200 184 ug/L 92 57 -124
Di-n-octyl phthalate 200 211 ug/L 105 59 -128
Fluoranthene 200 192 ug/L 96 57 -128
Fluorene 200 155 ug/L 78 52 -124
Hexachlorobenzene 200 172 ug/L 86 53 -125
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777555/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 777551 Prep Batch: 777555
Hexachlorobutadiene 200 111 ug/L 55 22 -124
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Hexachlorocyclopentadiene 200 71.1 ug/L 36 28 -130
Hexachloroethane 200 95.0 ug/L 48 21 -115
Indeno[1,2,3-cd]pyrene 200 205 ug/L 103 52 -134
Isophorone 200 121 ug/L 61 42 -124
2-Methylnaphthalene 200 133 ug/L 66 40 -121
2-Methylphenol 200 86.6 ug/L 43 30 -117
3 & 4 Methylphenol 200 82.2 ug/L 41 29 -110
Naphthalene 200 111 ug/L 55 40 -121
2-Nitroaniline 200 170 ug/L 85 55 -127
3-Nitroaniline 200 163 ug/L 81 41 -128
4-Nitroaniline 200 176 ug/L 88 55 -115
Nitrobenzene 200 114 ug/L 57 45 -121
2-Nitrophenol 200 135 ug/L 68 47 -123
4-Nitrophenol 400 131 ug/L 33 13 -130
N-Nitrosodi-n-propylamine 200 122 ug/L 61 49 -119
N-Nitrosodiphenylamine 200 163 ug/L 81 51 -123
2,2'-oxybis[1-chloropropane]200 116 ug/L 58 37 -130
Pentachlorophenol 400 411 ug/L 103 35 -138
Phenanthrene 200 170 ug/L 85 59 -120
Phenol 200 43.3 ug/L 22 14 -130
Pyrene 200 208 ug/L 104 57 -126
2,4,5-Trichlorophenol 200 154 ug/L 77 53 -123
2,4,6-Trichlorophenol 200 158 ug/L 79 50 -125
2-Fluorobiphenyl (Surr)44 -119
Surrogate
58
LCS LCS
Qualifier Limits%Recovery
252-Fluorophenol (Surr)19 -119
50Nitrobenzene-d5 (Surr)44 -120
21Phenol-d5 (Surr)10 -130
97Terphenyl-d14 (Surr)50 -134
972,4,6-Tribromophenol (Surr)43 -140
Client Sample ID: Method BlankLab Sample ID: MB 680-778086/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778471 Prep Batch: 778086
LOQ DL
Acenaphthene 10 U 20 4.4 ug/L 05/10/23 20:46 05/12/23 17:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 3.620 ug/L 05/10/23 20:46 05/12/23 17:41 1Acenaphthylene
5.0 U 2.210 ug/L 05/10/23 20:46 05/12/23 17:41 1Acetophenone
10 U 3.620 ug/L 05/10/23 20:46 05/12/23 17:41 1Anthracene
5.0 U 2.210 ug/L 05/10/23 20:46 05/12/23 17:41 1Atrazine
10 U 4.820 ug/L 05/10/23 20:46 05/12/23 17:41 1Benzaldehyde
10 U 4.220 ug/L 05/10/23 20:46 05/12/23 17:41 1Benzo[a]anthracene
10 U 2.820 ug/L 05/10/23 20:46 05/12/23 17:41 1Benzo[a]pyrene
10 U 3.120 ug/L 05/10/23 20:46 05/12/23 17:41 1Benzo[b]fluoranthene
10 U 3.020 ug/L 05/10/23 20:46 05/12/23 17:41 1Benzo[g,h,i]perylene
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-778086/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778471 Prep Batch: 778086
LOQ DL
Benzo[k]fluoranthene 10 U 20 2.9 ug/L 05/10/23 20:46 05/12/23 17:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 4.620 ug/L 05/10/23 20:46 05/12/23 17:41 11,1'-Biphenyl
4.0 U 1.810 ug/L 05/10/23 20:46 05/12/23 17:41 1Bis(2-chloroethoxy)methane
10 U 3.620 ug/L 05/10/23 20:46 05/12/23 17:41 1Bis(2-chloroethyl)ether
10 U 3.020 ug/L 05/10/23 20:46 05/12/23 17:41 1Bis(2-ethylhexyl) phthalate
10 U M 4.720 ug/L 05/10/23 20:46 05/12/23 17:41 14-Bromophenyl phenyl ether
10 U 2.820 ug/L 05/10/23 20:46 05/12/23 17:41 1Butyl benzyl phthalate
10 U 2.820 ug/L 05/10/23 20:46 05/12/23 17:41 1Caprolactam
4.0 U 1.810 ug/L 05/10/23 20:46 05/12/23 17:41 1Carbazole
4.0 U 1.010 ug/L 05/10/23 20:46 05/12/23 17:41 14-Chloroaniline
10 U 2.520 ug/L 05/10/23 20:46 05/12/23 17:41 14-Chloro-3-methylphenol
10 U 4.820 ug/L 05/10/23 20:46 05/12/23 17:41 12-Chloronaphthalene
10 U 3.220 ug/L 05/10/23 20:46 05/12/23 17:41 12-Chlorophenol
12 U 5.320 ug/L 05/10/23 20:46 05/12/23 17:41 14-Chlorophenyl phenyl ether
10 U 3.820 ug/L 05/10/23 20:46 05/12/23 17:41 1Chrysene
10 U 3.020 ug/L 05/10/23 20:46 05/12/23 17:41 1Dibenz(a,h)anthracene
4.0 U 1.910 ug/L 05/10/23 20:46 05/12/23 17:41 1Dibenzofuran
20 U 1050 ug/L 05/10/23 20:46 05/12/23 17:41 13,3'-Dichlorobenzidine
10 U 3.720 ug/L 05/10/23 20:46 05/12/23 17:41 12,4-Dichlorophenol
5.0 U 2.210 ug/L 05/10/23 20:46 05/12/23 17:41 1Diethyl phthalate
10 U 3.020 ug/L 05/10/23 20:46 05/12/23 17:41 12,4-Dimethylphenol
5.0 U 2.110 ug/L 05/10/23 20:46 05/12/23 17:41 1Dimethyl phthalate
5.0 U 2.310 ug/L 05/10/23 20:46 05/12/23 17:41 1Di-n-butyl phthalate
20 U 5.350 ug/L 05/10/23 20:46 05/12/23 17:41 14,6-Dinitro-2-methylphenol
40 U 1650 ug/L 05/10/23 20:46 05/12/23 17:41 12,4-Dinitrophenol
5.0 U 2.310 ug/L 05/10/23 20:46 05/12/23 17:41 12,4-Dinitrotoluene
10 U M 2.820 ug/L 05/10/23 20:46 05/12/23 17:41 12,6-Dinitrotoluene
10 U 2.820 ug/L 05/10/23 20:46 05/12/23 17:41 1Di-n-octyl phthalate
4.0 U 1.610 ug/L 05/10/23 20:46 05/12/23 17:41 1Fluoranthene
10 U 3.420 ug/L 05/10/23 20:46 05/12/23 17:41 1Fluorene
4.0 U 1.610 ug/L 05/10/23 20:46 05/12/23 17:41 1Hexachlorobenzene
10 U 4.020 ug/L 05/10/23 20:46 05/12/23 17:41 1Hexachlorobutadiene
10 U 3.520 ug/L 05/10/23 20:46 05/12/23 17:41 1Hexachlorocyclopentadiene
10 U 3.620 ug/L 05/10/23 20:46 05/12/23 17:41 1Hexachloroethane
10 U 4.320 ug/L 05/10/23 20:46 05/12/23 17:41 1Indeno[1,2,3-cd]pyrene
4.0 U 2.010 ug/L 05/10/23 20:46 05/12/23 17:41 1Isophorone
10 U 4.620 ug/L 05/10/23 20:46 05/12/23 17:41 12-Methylnaphthalene
4.0 U 1.810 ug/L 05/10/23 20:46 05/12/23 17:41 12-Methylphenol
4.0 U 1.410 ug/L 05/10/23 20:46 05/12/23 17:41 13 & 4 Methylphenol
10 U 3.520 ug/L 05/10/23 20:46 05/12/23 17:41 1Naphthalene
10 U 2.920 ug/L 05/10/23 20:46 05/12/23 17:41 12-Nitroaniline
10 U 3.050 ug/L 05/10/23 20:46 05/12/23 17:41 13-Nitroaniline
10 U 3.050 ug/L 05/10/23 20:46 05/12/23 17:41 14-Nitroaniline
10 U 3.520 ug/L 05/10/23 20:46 05/12/23 17:41 1Nitrobenzene
10 U 3.920 ug/L 05/10/23 20:46 05/12/23 17:41 12-Nitrophenol
20 U 8.150 ug/L 05/10/23 20:46 05/12/23 17:41 14-Nitrophenol
5.0 U 2.410 ug/L 05/10/23 20:46 05/12/23 17:41 1N-Nitrosodi-n-propylamine
10 U 2.920 ug/L 05/10/23 20:46 05/12/23 17:41 1N-Nitrosodiphenylamine
10 U 3.120 ug/L 05/10/23 20:46 05/12/23 17:41 12,2'-oxybis[1-chloropropane]
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-778086/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778471 Prep Batch: 778086
LOQ DL
Pentachlorophenol 20 U 50 9.9 ug/L 05/10/23 20:46 05/12/23 17:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 4.320 ug/L 05/10/23 20:46 05/12/23 17:41 1Phenanthrene
4.0 U 1.510 ug/L 05/10/23 20:46 05/12/23 17:41 1Phenol
10 U 3.720 ug/L 05/10/23 20:46 05/12/23 17:41 1Pyrene
10 U 3.320 ug/L 05/10/23 20:46 05/12/23 17:41 12,4,5-Trichlorophenol
5.0 U 2.220 ug/L 05/10/23 20:46 05/12/23 17:41 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)66 44-119 05/12/23 17:41 1
MB MB
Surrogate
05/10/23 20:46
Dil FacPrepared AnalyzedQualifier Limits%Recovery
27 05/10/23 20:46 05/12/23 17:41 12-Fluorophenol (Surr)19-119
60 05/10/23 20:46 05/12/23 17:41 1Nitrobenzene-d5 (Surr)44-120
19 05/10/23 20:46 05/12/23 17:41 1Phenol-d5 (Surr)10-130
72 05/10/23 20:46 05/12/23 17:41 1Terphenyl-d14 (Surr)50-134
66 05/10/23 20:46 05/12/23 17:41 12,4,6-Tribromophenol (Surr)43-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778086/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778471 Prep Batch: 778086
Acenaphthene 200 166 ug/L 83 47 -122
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Acenaphthylene 200 177 ug/L 89 41 -130
Acetophenone 200 154 ug/L 77 46 -118
Anthracene 200 172 ug/L 86 57 -123
Atrazine 200 157 ug/L 78 44 -142
Benzaldehyde 200 93.2 ug/L 47 25 -130
Benzo[a]anthracene 200 191 ug/L 95 58 -125
Benzo[a]pyrene 200 197 ug/L 99 54 -128
Benzo[b]fluoranthene 200 192 ug/L 96 53 -131
Benzo[g,h,i]perylene 200 175 ug/L 88 50 -134
Benzo[k]fluoranthene 200 176 M ug/L 88 57 -129
1,1'-Biphenyl 200 163 ug/L 81 49 -115
Bis(2-chloroethoxy)methane 200 149 ug/L 75 48 -120
Bis(2-chloroethyl)ether 200 107 ug/L 54 43 -118
Bis(2-ethylhexyl) phthalate 200 183 ug/L 92 55 -135
4-Bromophenyl phenyl ether 200 180 ug/L 90 55 -124
Butyl benzyl phthalate 200 182 ug/L 91 53 -134
Caprolactam 200 40.3 ug/L 20 13 -130
Carbazole 200 168 ug/L 84 60 -122
4-Chloroaniline 200 148 ug/L 74 33 -117
4-Chloro-3-methylphenol 200 160 ug/L 80 52 -119
2-Chloronaphthalene 200 160 ug/L 80 40 -116
2-Chlorophenol 200 118 ug/L 59 38 -117
4-Chlorophenyl phenyl ether 200 180 ug/L 90 53 -121
Chrysene 200 185 ug/L 92 59 -123
Dibenz(a,h)anthracene 200 178 ug/L 89 51 -134
Dibenzofuran 200 166 ug/L 83 53 -118
3,3'-Dichlorobenzidine 200 166 ug/L 83 27 -129
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-778086/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 778471 Prep Batch: 778086
2,4-Dichlorophenol 200 158 ug/L 79 47 -121
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Diethyl phthalate 200 181 ug/L 90 56 -125
2,4-Dimethylphenol 200 119 ug/L 60 31 -124
Dimethyl phthalate 200 174 ug/L 87 45 -127
Di-n-butyl phthalate 200 178 ug/L 89 56 -122
4,6-Dinitro-2-methylphenol 400 388 ug/L 97 44 -137
2,4-Dinitrophenol 400 380 ug/L 95 23 -143
2,4-Dinitrotoluene 200 177 ug/L 89 57 -128
2,6-Dinitrotoluene 200 169 ug/L 85 57 -124
Di-n-octyl phthalate 200 186 ug/L 93 59 -128
Fluoranthene 200 185 ug/L 92 57 -128
Fluorene 200 164 ug/L 82 52 -124
Hexachlorobenzene 200 167 ug/L 83 53 -125
Hexachlorobutadiene 200 170 ug/L 85 22 -124
Hexachlorocyclopentadiene 200 128 ug/L 64 28 -130
Hexachloroethane 200 140 ug/L 70 21 -115
Indeno[1,2,3-cd]pyrene 200 181 ug/L 91 52 -134
Isophorone 200 161 ug/L 81 42 -124
2-Methylnaphthalene 200 176 ug/L 88 40 -121
2-Methylphenol 200 106 ug/L 53 30 -117
3 & 4 Methylphenol 200 99.3 ug/L 50 29 -110
Naphthalene 200 149 ug/L 74 40 -121
2-Nitroaniline 200 171 ug/L 85 55 -127
3-Nitroaniline 200 156 ug/L 78 41 -128
4-Nitroaniline 200 160 ug/L 80 55 -115
Nitrobenzene 200 152 ug/L 76 45 -121
2-Nitrophenol 200 151 ug/L 76 47 -123
4-Nitrophenol 400 155 ug/L 39 13 -130
N-Nitrosodi-n-propylamine 200 156 ug/L 78 49 -119
N-Nitrosodiphenylamine 200 168 ug/L 84 51 -123
2,2'-oxybis[1-chloropropane]200 135 ug/L 68 37 -130
Pentachlorophenol 400 383 ug/L 96 35 -138
Phenanthrene 200 172 ug/L 86 59 -120
Phenol 200 61.0 ug/L 30 14 -130
Pyrene 200 187 ug/L 94 57 -126
2,4,5-Trichlorophenol 200 187 ug/L 94 53 -123
2,4,6-Trichlorophenol 200 180 ug/L 90 50 -125
2-Fluorobiphenyl (Surr)44 -119
Surrogate
65
LCS LCS
Qualifier Limits%Recovery
262-Fluorophenol (Surr)19 -119
60Nitrobenzene-d5 (Surr)44 -120
19Phenol-d5 (Surr)10 -130
73Terphenyl-d14 (Surr)50 -134
652,4,6-Tribromophenol (Surr)43 -140
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-374082/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
LOQ DL
Benzene 2.0 U 5.0 1.0 ug/L 05/10/23 09:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
50 U 25100 ug/L 05/10/23 09:52 1C5-C8 Aliphatics
20 U 10100 ug/L 05/10/23 09:52 1C9-C10 Aromatics
50 U 25100 ug/L 05/10/23 09:52 1C9-C12 Aliphatics
2.0 U 1.05.0 ug/L 05/10/23 09:52 1Ethylbenzene
2.0 U 1.05.0 ug/L 05/10/23 09:52 1Methyl tert-butyl ether
4.0 U 2.06.0 ug/L 05/10/23 09:52 1Naphthalene
2.0 U 1.05.0 ug/L 05/10/23 09:52 1Toluene
50 U 25100 ug/L 05/10/23 09:52 1C9-C12 Aliphatics (adjusted)
5.0 U 2.510 ug/L 05/10/23 09:52 1m-Xylene & p-Xylene
2.0 U 1.05.0 ug/L 05/10/23 09:52 1o-Xylene
50 U 25100 ug/L 05/10/23 09:52 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)105 70-130 05/10/23 09:52 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
92 05/10/23 09:52 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-374082/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
Benzene 50.1 43.2 ug/L 86 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Ethylbenzene 50.1 44.6 ug/L 89 70 -130
Methyl tert-butyl ether 50.2 42.2 ug/L 84 70 -130
Naphthalene 50.2 43.9 ug/L 88 70 -130
Toluene 50.1 42.9 ug/L 86 70 -130
m-Xylene & p-Xylene 101 90.4 ug/L 90 70 -130
o-Xylene 50.4 44.2 ug/L 88 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-374082/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
Benzene 50.1 43.6 ug/L 87 70 -130 1 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Ethylbenzene 50.1 45.0 ug/L 90 70 -130 1 25
Methyl tert-butyl ether 50.2 43.3 ug/L 86 70 -130 3 25
Naphthalene 50.2 44.8 ug/L 89 70 -130 2 25
Toluene 50.1 43.4 ug/L 87 70 -130 1 25
m-Xylene & p-Xylene 101 91.2 ug/L 91 70 -130 1 25
o-Xylene 50.4 44.6 ug/L 89 70 -130 1 25
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-374082/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374082
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 410-374511/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374511
LOQ DL
Benzene 2.0 U 5.0 1.0 ug/L 05/11/23 08:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
50 U 25100 ug/L 05/11/23 08:28 1C5-C8 Aliphatics
20 U 10100 ug/L 05/11/23 08:28 1C9-C10 Aromatics
50 U 25100 ug/L 05/11/23 08:28 1C9-C12 Aliphatics
2.0 U 1.05.0 ug/L 05/11/23 08:28 1Ethylbenzene
2.0 U 1.05.0 ug/L 05/11/23 08:28 1Methyl tert-butyl ether
4.0 U 2.06.0 ug/L 05/11/23 08:28 1Naphthalene
2.0 U 1.05.0 ug/L 05/11/23 08:28 1Toluene
50 U 25100 ug/L 05/11/23 08:28 1C9-C12 Aliphatics (adjusted)
5.0 U 2.510 ug/L 05/11/23 08:28 1m-Xylene & p-Xylene
2.0 U 1.05.0 ug/L 05/11/23 08:28 1o-Xylene
50 U 25100 ug/L 05/11/23 08:28 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)104 70-130 05/11/23 08:28 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
91 05/11/23 08:28 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-374511/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374511
Benzene 50.1 42.7 ug/L 85 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Ethylbenzene 50.1 44.3 ug/L 88 70 -130
Methyl tert-butyl ether 50.2 44.7 ug/L 89 70 -130
Naphthalene 50.2 43.9 ug/L 87 70 -130
Toluene 50.1 42.7 ug/L 85 70 -130
m-Xylene & p-Xylene 101 90.0 ug/L 89 70 -130
o-Xylene 50.4 44.1 ug/L 88 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-374511/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374511
Benzene 50.1 42.9 ug/L 86 70 -130 0 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-374511/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 374511
Ethylbenzene 50.1 44.2 ug/L 88 70 -130 0 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methyl tert-butyl ether 50.2 44.9 ug/L 89 70 -130 1 25
Naphthalene 50.2 43.5 ug/L 87 70 -130 1 25
Toluene 50.1 42.8 ug/L 85 70 -130 0 25
m-Xylene & p-Xylene 101 89.8 ug/L 89 70 -130 0 25
o-Xylene 50.4 44.1 ug/L 88 70 -130 0 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
93a,a,a-Trifluorotoluene (pid)70 -130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-375040/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377003 Prep Batch: 375040
LOQ DL
C19-C36 Aliphatics 20 U 50 10 ug/L 05/12/23 08:50 05/17/23 19:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
20.4 J M 1030 ug/L 05/12/23 08:50 05/17/23 19:27 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)64 40-140 05/17/23 19:27 1
MB MB
Surrogate
05/12/23 08:50
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-375040/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377002 Prep Batch: 375040
LOQ DL
Anthracene 1.2 U 2.0 0.60 ug/L 05/12/23 08:50 05/17/23 19:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 5.012 ug/L 05/12/23 08:50 05/17/23 19:27 1Pyrene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Benzo[g,h,i]perylene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Indeno[1,2,3-cd]pyrene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Benzo[b]fluoranthene
1.0 U 0.502.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Fluoranthene
3.0 U 1.54.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Benzo[k]fluoranthene
1.4 U 0.702.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Acenaphthylene
1.0 U 0.502.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Chrysene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Benzo[a]pyrene
1.0 U 0.502.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Dibenz(a,h)anthracene
1.4 U 0.702.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Benzo[a]anthracene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Acenaphthene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Phenanthrene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Fluorene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 1Naphthalene
1.2 U 0.602.0 ug/L 05/12/23 08:50 05/17/23 19:27 12-Methylnaphthalene
30 U 1040 ug/L 05/12/23 08:50 05/17/23 19:27 1C11-C22 Aromatics (unadjusted)
30 U 1040 ug/L 05/12/23 08:50 05/17/23 19:27 1C11-C22 Aromatics (Adjusted)
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-375040/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377002 Prep Batch: 375040
2-Fluorobiphenyl (Surr)60 40-140 05/17/23 19:27 1
MB MB
Surrogate
05/12/23 08:50
Dil FacPrepared AnalyzedQualifier Limits%Recovery
46 05/12/23 08:50 05/17/23 19:27 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-375040/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377003 Prep Batch: 375040
C19-C36 Aliphatics 321 244 M ug/L 76 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 119 ug/L 49 40 -140
1-Chlorooctadecane (Surr)40 -140
Surrogate
48
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-375040/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377002 Prep Batch: 375040
Anthracene 40.1 23.8 ug/L 59 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Pyrene 40.1 25.7 ug/L 64 40 -140
Benzo[g,h,i]perylene 40.0 24.6 ug/L 62 40 -140
Indeno[1,2,3-cd]pyrene 40.1 23.3 ug/L 58 40 -140
Benzo[b]fluoranthene 40.2 22.0 M ug/L 55 40 -140
Fluoranthene 40.1 24.3 ug/L 61 40 -140
Benzo[k]fluoranthene 40.1 28.0 M ug/L 70 40 -140
Acenaphthylene 40.1 21.7 ug/L 54 40 -140
Chrysene 40.2 24.4 ug/L 61 40 -140
Benzo[a]pyrene 40.2 23.6 ug/L 59 40 -140
Dibenz(a,h)anthracene 40.0 24.7 ug/L 62 40 -140
Benzo[a]anthracene 40.1 24.7 ug/L 62 40 -140
Acenaphthene 40.2 21.5 ug/L 54 40 -140
Phenanthrene 40.1 23.0 ug/L 57 40 -140
Fluorene 40.1 22.4 ug/L 56 40 -140
Naphthalene 40.1 20.0 M ug/L 50 40 -140
2-Methylnaphthalene 40.1 18.7 M ug/L 47 40 -140
C11-C22 Aromatics (unadjusted)681 409 M ug/L 60 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
65
LCS LCS
Qualifier Limits%Recovery
63o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-375040/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377003 Prep Batch: 375040
C19-C36 Aliphatics 321 265 M ug/L 82 40 -140 8 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Eurofins Savannah
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-375040/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377003 Prep Batch: 375040
C9-C18 Aliphatics 241 167 Q ug/L 69 40 -140 34 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1-Chlorooctadecane (Surr)40 -140
Surrogate
49
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-375040/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 377002 Prep Batch: 375040
Anthracene 40.1 22.7 ug/L 57 40 -140 5 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pyrene 40.1 23.4 ug/L 58 40 -140 10 25
Benzo[g,h,i]perylene 40.0 23.6 ug/L 59 40 -140 4 25
Indeno[1,2,3-cd]pyrene 40.1 21.6 ug/L 54 40 -140 8 25
Benzo[b]fluoranthene 40.2 22.5 M ug/L 56 40 -140 2 25
Fluoranthene 40.1 22.8 ug/L 57 40 -140 7 25
Benzo[k]fluoranthene 40.1 25.6 M ug/L 64 40 -140 9 25
Acenaphthylene 40.1 20.5 ug/L 51 40 -140 6 25
Chrysene 40.2 25.1 ug/L 62 40 -140 3 25
Benzo[a]pyrene 40.2 23.0 ug/L 57 40 -140 3 25
Dibenz(a,h)anthracene 40.0 24.1 ug/L 60 40 -140 2 25
Benzo[a]anthracene 40.1 22.4 ug/L 56 40 -140 10 25
Acenaphthene 40.2 21.1 ug/L 53 40 -140 2 25
Phenanthrene 40.1 21.7 ug/L 54 40 -140 6 25
Fluorene 40.1 21.6 ug/L 54 40 -140 4 25
Naphthalene 40.1 19.1 M ug/L 48 40 -140 5 25
2-Methylnaphthalene 40.1 19.0 M ug/L 47 40 -140 1 25
C11-C22 Aromatics (unadjusted)681 384 M ug/L 56 40 -140 6 25
2-Fluorobiphenyl (Surr)40 -140
Surrogate
59
LCSD LCSD
Qualifier Limits%Recovery
57o- terphenyl (Surr)40 -140
Client Sample ID: Method BlankLab Sample ID: MB 410-378825/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
LOQ DL
C19-C36 Aliphatics 20 U M 50 10 ug/L 05/23/23 09:00 06/01/23 03:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
25.7 J 1030 ug/L 05/23/23 09:00 06/01/23 03:14 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)51 M 40-140 06/01/23 03:14 1
MB MB
Surrogate
05/23/23 09:00
Dil FacPrepared AnalyzedQualifier Limits%Recovery
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-378825/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
LOQ DL
Anthracene 1.2 U 2.0 0.60 ug/L 05/23/23 09:00 06/01/23 02:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
10 U 5.012 ug/L 05/23/23 09:00 06/01/23 02:52 1Pyrene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[g,h,i]perylene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Indeno[1,2,3-cd]pyrene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[b]fluoranthene
1.0 U 0.502.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Fluoranthene
3.0 U 1.54.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[k]fluoranthene
1.4 U 0.702.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Acenaphthylene
1.0 U 0.502.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Chrysene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[a]pyrene
1.0 U 0.502.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Dibenz(a,h)anthracene
1.4 U 0.702.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Benzo[a]anthracene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Acenaphthene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Phenanthrene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Fluorene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 1Naphthalene
1.2 U 0.602.0 ug/L 05/23/23 09:00 06/01/23 02:52 12-Methylnaphthalene
30 U 1040 ug/L 05/23/23 09:00 06/01/23 02:52 1C11-C22 Aromatics (unadjusted)
30 U 1040 ug/L 05/23/23 09:00 06/01/23 02:52 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)82 40-140 06/01/23 02:52 1
MB MB
Surrogate
05/23/23 09:00
Dil FacPrepared AnalyzedQualifier Limits%Recovery
59 05/23/23 09:00 06/01/23 02:52 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-378825/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
C19-C36 Aliphatics 321 196 M ug/L 61 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 134 M ug/L 56 40 -140
1-Chlorooctadecane (Surr)M 40 -140
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-378825/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Anthracene 40.1 29.4 ug/L 73 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Pyrene 40.1 29.7 ug/L 74 40 -140
Benzo[g,h,i]perylene 40.0 29.2 ug/L 73 40 -140
Indeno[1,2,3-cd]pyrene 40.1 27.6 ug/L 69 40 -140
Benzo[b]fluoranthene 40.2 30.2 M ug/L 75 40 -140
Fluoranthene 40.1 29.7 ug/L 74 40 -140
Benzo[k]fluoranthene 40.1 29.3 M ug/L 73 40 -140
Acenaphthylene 40.1 28.1 ug/L 70 40 -140
Eurofins Savannah
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-378825/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Chrysene 40.2 28.8 ug/L 72 40 -140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Benzo[a]pyrene 40.2 28.0 ug/L 70 40 -140
Dibenz(a,h)anthracene 40.0 29.2 ug/L 73 40 -140
Benzo[a]anthracene 40.1 29.8 ug/L 74 40 -140
Acenaphthene 40.2 27.2 ug/L 68 40 -140
Phenanthrene 40.1 29.3 ug/L 73 40 -140
Fluorene 40.1 28.2 ug/L 70 40 -140
Naphthalene 40.1 26.2 ug/L 65 40 -140
2-Methylnaphthalene 40.1 26.0 ug/L 65 40 -140
C11-C22 Aromatics (unadjusted)681 475 M ug/L 70 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
77o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-378825/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381594 Prep Batch: 378825
C19-C36 Aliphatics 321 190 M ug/L 59 40 -140 3 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 134 M ug/L 56 40 -140 0 25
1-Chlorooctadecane (Surr)M 40 -140
Surrogate
50
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-378825/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
Anthracene 40.1 27.2 ug/L 68 40 -140 8 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pyrene 40.1 27.1 ug/L 68 40 -140 9 25
Benzo[g,h,i]perylene 40.0 26.9 ug/L 67 40 -140 8 25
Indeno[1,2,3-cd]pyrene 40.1 25.5 ug/L 64 40 -140 8 25
Benzo[b]fluoranthene 40.2 27.6 M ug/L 69 40 -140 9 25
Fluoranthene 40.1 27.2 ug/L 68 40 -140 9 25
Benzo[k]fluoranthene 40.1 27.2 M ug/L 68 40 -140 8 25
Acenaphthylene 40.1 27.1 ug/L 68 40 -140 4 25
Chrysene 40.2 26.2 ug/L 65 40 -140 9 25
Benzo[a]pyrene 40.2 25.9 ug/L 65 40 -140 8 25
Dibenz(a,h)anthracene 40.0 27.1 ug/L 68 40 -140 7 25
Benzo[a]anthracene 40.1 27.5 ug/L 69 40 -140 8 25
Acenaphthene 40.2 25.3 ug/L 63 40 -140 7 25
Phenanthrene 40.1 27.1 ug/L 68 40 -140 8 25
Fluorene 40.1 26.4 ug/L 66 40 -140 7 25
Naphthalene 40.1 23.9 M ug/L 60 40 -140 9 25
2-Methylnaphthalene 40.1 24.0 ug/L 60 40 -140 8 25
Eurofins Savannah
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QC Sample Results
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-378825/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381590 Prep Batch: 378825
C11-C22 Aromatics (unadjusted)681 447 M ug/L 66 40 -140 6 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
89
LCSD LCSD
Qualifier Limits%Recovery
69o- terphenyl (Surr)40 -140
Eurofins Savannah
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QC Association Summary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
GC/MS VOA
Analysis Batch: 778568
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-234374-1 RW-18-05-23 Total/NA
Water 8260D680-234374-2 RW-16-05-23 Total/NA
Water 8260D680-234374-3 RW-17-05-23 Total/NA
Water 8260D680-234374-4 RW-08-05-23 Total/NA
Water 8260D680-234374-5 MW7-18-05-23 Total/NA
Water 8260DMB 680-778568/8 Method Blank Total/NA
Water 8260DLCS 680-778568/4 Lab Control Sample Total/NA
Water 8260DLCSD 680-778568/5 Lab Control Sample Dup Total/NA
Analysis Batch: 778627
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-234374-1 RW-18-05-23 Total/NA
Water 8260D680-234374-2 - DL RW-16-05-23 Total/NA
Water 8260D680-234374-3 RW-17-05-23 Total/NA
Water 8260D680-234374-4 RW-08-05-23 Total/NA
Water 8260D680-234374-5 MW7-18-05-23 Total/NA
Water 8260DMB 680-778627/8 Method Blank Total/NA
Water 8260DLCS 680-778627/4 Lab Control Sample Total/NA
Water 8260DLCSD 680-778627/5 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Analysis Batch: 777551
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 777555680-234374-1 RW-18-05-23 Total/NA
Water 8270E 777555680-234374-2 RW-16-05-23 Total/NA
Water 8270E 777555680-234374-3 RW-17-05-23 Total/NA
Water 8270E 777555680-234374-4 RW-08-05-23 Total/NA
Water 8270E 777555680-234374-5 MW7-18-05-23 Total/NA
Water 8270E 777555MB 680-777555/1-B Method Blank Total/NA
Water 8270E 777555LCS 680-777555/2-B Lab Control Sample Total/NA
Prep Batch: 777555
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-234374-1 RW-18-05-23 Total/NA
Water 3510C680-234374-2 RW-16-05-23 Total/NA
Water 3510C680-234374-3 RW-17-05-23 Total/NA
Water 3510C680-234374-4 RW-08-05-23 Total/NA
Water 3510C680-234374-5 MW7-18-05-23 Total/NA
Water 3510CMB 680-777555/1-B Method Blank Total/NA
Water 3510CLCS 680-777555/2-B Lab Control Sample Total/NA
Prep Batch: 778086
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-234374-4 - RE RW-08-05-23 Total/NA
Water 3510CMB 680-778086/1-A Method Blank Total/NA
Water 3510CLCS 680-778086/2-A Lab Control Sample Total/NA
Analysis Batch: 778471
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 778086680-234374-4 - RE RW-08-05-23 Total/NA
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QC Association Summary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
GC/MS Semi VOA (Continued)
Analysis Batch: 778471 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 778086MB 680-778086/1-A Method Blank Total/NA
Water 8270E 778086LCS 680-778086/2-A Lab Control Sample Total/NA
GC VOA
Analysis Batch: 374082
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH680-234374-1 RW-18-05-23 Total/NA
Water MAVPH680-234374-2 RW-16-05-23 Total/NA
Water MAVPH680-234374-3 RW-17-05-23 Total/NA
Water MAVPH680-234374-4 RW-08-05-23 Total/NA
Water MAVPH680-234374-5 MW7-18-05-23 Total/NA
Water MAVPHMB 410-374082/2 Method Blank Total/NA
Water MAVPHLCS 410-374082/3 Lab Control Sample Total/NA
Water MAVPHLCSD 410-374082/4 Lab Control Sample Dup Total/NA
Analysis Batch: 374511
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH680-234374-1 - DL RW-18-05-23 Total/NA
Water MAVPH680-234374-2 - DL RW-16-05-23 Total/NA
Water MAVPH680-234374-3 - DL RW-17-05-23 Total/NA
Water MAVPH680-234374-5 - DL MW7-18-05-23 Total/NA
Water MAVPHMB 410-374511/2 Method Blank Total/NA
Water MAVPHLCS 410-374511/3 Lab Control Sample Total/NA
Water MAVPHLCSD 410-374511/4 Lab Control Sample Dup Total/NA
Analysis Batch: 375183
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA VPH680-234374-1 RW-18-05-23 Total/NA
Water MA VPH680-234374-2 RW-16-05-23 Total/NA
Water MA VPH680-234374-3 RW-17-05-23 Total/NA
Water MA VPH680-234374-4 RW-08-05-23 Total/NA
Water MA VPH680-234374-5 MW7-18-05-23 Total/NA
GC Semi VOA
Prep Batch: 375040
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-234374-1 RW-18-05-23 Total/NA
Water 3510C680-234374-2 RW-16-05-23 Total/NA
Water 3510C680-234374-3 - DL RW-17-05-23 Total/NA
Water 3510C680-234374-3 RW-17-05-23 Total/NA
Water 3510C680-234374-4 RW-08-05-23 Total/NA
Water 3510C680-234374-5 - DL MW7-18-05-23 Total/NA
Water 3510C680-234374-5 MW7-18-05-23 Total/NA
Water 3510CMB 410-375040/1-B Method Blank Total/NA
Water 3510CMB 410-375040/1-C Method Blank Total/NA
Water 3510CLCS 410-375040/2-B Lab Control Sample Total/NA
Water 3510CLCS 410-375040/2-C Lab Control Sample Total/NA
Water 3510CLCSD 410-375040/3-B Lab Control Sample Dup Total/NA
Water 3510CLCSD 410-375040/3-C Lab Control Sample Dup Total/NA
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QC Association Summary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
GC Semi VOA
Cleanup Batch: 376670
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 375040680-234374-1 RW-18-05-23 Total/NA
Water 3630C 375040680-234374-1 RW-18-05-23 Total/NA
Water 3630C 375040680-234374-2 RW-16-05-23 Total/NA
Water 3630C 375040680-234374-2 RW-16-05-23 Total/NA
Water 3630C 375040680-234374-3 - DL RW-17-05-23 Total/NA
Water 3630C 375040680-234374-3 RW-17-05-23 Total/NA
Water 3630C 375040680-234374-3 RW-17-05-23 Total/NA
Water 3630C 375040680-234374-4 RW-08-05-23 Total/NA
Water 3630C 375040680-234374-4 RW-08-05-23 Total/NA
Water 3630C 375040680-234374-5 MW7-18-05-23 Total/NA
Water 3630C 375040680-234374-5 - DL MW7-18-05-23 Total/NA
Water 3630C 375040680-234374-5 MW7-18-05-23 Total/NA
Water 3630C 375040MB 410-375040/1-B Method Blank Total/NA
Water 3630C 375040MB 410-375040/1-C Method Blank Total/NA
Water 3630C 375040LCS 410-375040/2-B Lab Control Sample Total/NA
Water 3630C 375040LCS 410-375040/2-C Lab Control Sample Total/NA
Water 3630C 375040LCSD 410-375040/3-B Lab Control Sample Dup Total/NA
Water 3630C 375040LCSD 410-375040/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 377002
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 376670680-234374-1 RW-18-05-23 Total/NA
Water MA-EPH 376670680-234374-2 RW-16-05-23 Total/NA
Water MA-EPH 376670680-234374-3 RW-17-05-23 Total/NA
Water MA-EPH 376670680-234374-4 RW-08-05-23 Total/NA
Water MA-EPH 376670680-234374-5 MW7-18-05-23 Total/NA
Water MA-EPH 376670MB 410-375040/1-C Method Blank Total/NA
Water MA-EPH 376670LCS 410-375040/2-C Lab Control Sample Total/NA
Water MA-EPH 376670LCSD 410-375040/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 377003
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 376670680-234374-1 RW-18-05-23 Total/NA
Water MA-EPH 376670680-234374-2 RW-16-05-23 Total/NA
Water MA-EPH 376670680-234374-3 RW-17-05-23 Total/NA
Water MA-EPH 376670680-234374-4 RW-08-05-23 Total/NA
Water MA-EPH 376670680-234374-5 MW7-18-05-23 Total/NA
Water MA-EPH 376670MB 410-375040/1-B Method Blank Total/NA
Water MA-EPH 376670LCS 410-375040/2-B Lab Control Sample Total/NA
Water MA-EPH 376670LCSD 410-375040/3-B Lab Control Sample Dup Total/NA
Analysis Batch: 377429
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 376670680-234374-3 - DL RW-17-05-23 Total/NA
Water MA-EPH 376670680-234374-5 - DL MW7-18-05-23 Total/NA
Prep Batch: 378825
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-234374-1 - RE RW-18-05-23 Total/NA
Water 3510C680-234374-2 - RE RW-16-05-23 Total/NA
Water 3510C680-234374-4 - RE RW-08-05-23 Total/NA
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QC Association Summary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
GC Semi VOA (Continued)
Prep Batch: 378825 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510CMB 410-378825/1-B Method Blank Total/NA
Water 3510CMB 410-378825/1-C Method Blank Total/NA
Water 3510CLCS 410-378825/2-B Lab Control Sample Total/NA
Water 3510CLCS 410-378825/2-C Lab Control Sample Total/NA
Water 3510CLCSD 410-378825/3-B Lab Control Sample Dup Total/NA
Water 3510CLCSD 410-378825/3-C Lab Control Sample Dup Total/NA
Cleanup Batch: 381341
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 378825680-234374-1 - RE RW-18-05-23 Total/NA
Water 3630C 378825680-234374-1 - RE RW-18-05-23 Total/NA
Water 3630C 378825680-234374-2 - RE RW-16-05-23 Total/NA
Water 3630C 378825680-234374-2 - RE RW-16-05-23 Total/NA
Water 3630C 378825680-234374-4 - RE RW-08-05-23 Total/NA
Water 3630C 378825680-234374-4 - RE RW-08-05-23 Total/NA
Water 3630C 378825MB 410-378825/1-B Method Blank Total/NA
Water 3630C 378825MB 410-378825/1-C Method Blank Total/NA
Water 3630C 378825LCS 410-378825/2-B Lab Control Sample Total/NA
Water 3630C 378825LCS 410-378825/2-C Lab Control Sample Total/NA
Water 3630C 378825LCSD 410-378825/3-B Lab Control Sample Dup Total/NA
Water 3630C 378825LCSD 410-378825/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 381590
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 381341680-234374-1 - RE RW-18-05-23 Total/NA
Water MA-EPH 381341680-234374-2 - RE RW-16-05-23 Total/NA
Water MA-EPH 381341680-234374-4 - RE RW-08-05-23 Total/NA
Water MA-EPH 381341MB 410-378825/1-C Method Blank Total/NA
Water MA-EPH 381341LCS 410-378825/2-C Lab Control Sample Total/NA
Water MA-EPH 381341LCSD 410-378825/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 381594
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 381341680-234374-1 - RE RW-18-05-23 Total/NA
Water MA-EPH 381341680-234374-2 - RE RW-16-05-23 Total/NA
Water MA-EPH 381341680-234374-4 - RE RW-08-05-23 Total/NA
Water MA-EPH 381341MB 410-378825/1-B Method Blank Total/NA
Water MA-EPH 381341LCS 410-378825/2-B Lab Control Sample Total/NA
Water MA-EPH 381341LCSD 410-378825/3-B Lab Control Sample Dup Total/NA
Analysis Batch: 382017
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH680-234374-1 RW-18-05-23 Total/NA
Water MA-EPH680-234374-2 RW-16-05-23 Total/NA
Water MA-EPH680-234374-3 RW-17-05-23 Total/NA
Water MA-EPH680-234374-4 RW-08-05-23 Total/NA
Water MA-EPH680-234374-5 MW7-18-05-23 Total/NA
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Client Sample ID: RW-18-05-23 Lab Sample ID: 680-234374-1
Matrix: WaterDate Collected: 05/01/23 09:55
Date Received: 05/02/23 10:30
Analysis 8260D P1C05/15/23 15:081 EET SAV778627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSB
Analysis 8260D 1 778568 05/14/23 16:19 Y1S EET SAVTotal/NA 5 mL 5 mL
CMSCInstrument ID:
Prep 3510C 777555 05/03/23 18:10 LA EET SAVTotal/NA 500 mL 1 mL
Analysis 8270E 1 777551 05/08/23 17:30 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 20:29 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Analysis MAVPH DL 5 374511 05/11/23 21:59 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1008.1 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 08:07 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1008.1 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 08:30 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 1000 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377002 05/17/23 23:11 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 1000 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377003 05/17/23 23:11 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:56 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: RW-16-05-23 Lab Sample ID: 680-234374-2
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Analysis 8260D P1C05/15/23 20:235DL EET SAV778627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSB
Analysis 8260D 1 778568 05/14/23 16:38 Y1S EET SAVTotal/NA 5 mL 5 mL
CMSCInstrument ID:
Prep 3510C 777555 05/03/23 18:10 LA EET SAVTotal/NA 500 mL 1 mL
Analysis 8270E 1 777551 05/08/23 17:55 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Client Sample ID: RW-16-05-23 Lab Sample ID: 680-234374-2
Matrix: WaterDate Collected: 05/01/23 11:30
Date Received: 05/02/23 10:30
Analysis MA VPH X87505/12/23 10:591 ELLE375183
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Analysis MAVPH 1 374082 05/10/23 21:10 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Analysis MAVPH DL 5 374511 05/11/23 22:40 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 989.9 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 10:00 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 989.9 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 10:22 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 999.4 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377002 05/17/23 23:33 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 999.4 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377003 05/17/23 23:33 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:56 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: RW-17-05-23 Lab Sample ID: 680-234374-3
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
Analysis 8260D P1C05/15/23 20:435 EET SAV778627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSB
Analysis 8260D 5 778568 05/14/23 21:46 Y1S EET SAVTotal/NA 5 mL 5 mL
CMSCInstrument ID:
Prep 3510C 777555 05/03/23 18:10 LA EET SAVTotal/NA 500 mL 1 mL
Analysis 8270E 1 777551 05/08/23 18:20 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 21:51 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Analysis MAVPH DL 10 374511 05/11/23 23:21 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Client Sample ID: RW-17-05-23 Lab Sample ID: 680-234374-3
Matrix: WaterDate Collected: 05/01/23 09:50
Date Received: 05/02/23 10:30
Prep 3510C A2VL05/12/23 08:50 ELLE375040
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1035.9 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377002 05/17/23 23:55 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C DL 375040 05/12/23 08:50 A2VL ELLETotal/NA 1035.9 mL 1 mL
Cleanup 3630C DL 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH DL 2 377429 05/18/23 15:58 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 1035.9 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377003 05/17/23 23:55 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:56 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: RW-08-05-23 Lab Sample ID: 680-234374-4
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Analysis 8260D P1C05/15/23 15:281 EET SAV778627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSB
Analysis 8260D 1 778568 05/14/23 16:57 Y1S EET SAVTotal/NA 5 mL 5 mL
CMSCInstrument ID:
Prep 3510C 777555 05/03/23 18:10 LA EET SAVTotal/NA 500 mL 1 mL
Analysis 8270E 1 777551 05/08/23 18:44 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 3510C RE 778086 05/10/23 20:46 MR EET SAVTotal/NA 500 mL 1 mL
Analysis 8270E RE 1 778471 05/12/23 22:27 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 22:32 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1040.2 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381590 06/01/23 10:22 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 378825 05/23/23 09:00 A2VL ELLETotal/NA 1040.2 mL 1 mL
Cleanup 3630C RE 381341 05/31/23 07:34 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 381594 06/01/23 10:45 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 1046.5 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377002 05/18/23 01:25 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Client Sample ID: RW-08-05-23 Lab Sample ID: 680-234374-4
Matrix: WaterDate Collected: 05/01/23 11:10
Date Received: 05/02/23 10:30
Prep 3510C A2VL05/12/23 08:50 ELLE375040
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1046.5 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377003 05/18/23 01:25 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:56 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
Client Sample ID: MW7-18-05-23 Lab Sample ID: 680-234374-5
Matrix: WaterDate Collected: 05/01/23 13:35
Date Received: 05/02/23 10:30
Analysis 8260D P1C05/15/23 19:24100 EET SAV778627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID: CMSB
Analysis 8260D 100 778568 05/14/23 21:27 Y1S EET SAVTotal/NA 5 mL 5 mL
CMSCInstrument ID:
Prep 3510C 777555 05/03/23 18:10 LA EET SAVTotal/NA 500 mL 1 mL
Analysis 8270E 1 777551 05/08/23 19:09 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 375183 05/12/23 10:59 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 374082 05/10/23 23:13 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Analysis MAVPH DL 20 374511 05/12/23 00:43 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 1036.2 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377002 05/18/23 01:48 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C DL 375040 05/12/23 08:50 A2VL ELLETotal/NA 1036.2 mL 1 mL
Cleanup 3630C DL 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH DL 5 377429 05/18/23 16:20 UHEW ELLETotal/NA 1 mL 1 mL
19875-SInstrument ID:
Prep 3510C 375040 05/12/23 08:50 A2VL ELLETotal/NA 1036.2 mL 1 mL
Cleanup 3630C 376670 05/17/23 07:04 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 377003 05/18/23 01:48 UHEW ELLETotal/NA 1 mL 1 mL
19875-TInstrument ID:
Analysis MA-EPH 1 382017 06/01/23 14:56 UHEW ELLETotal/NA
NOEQUIPInstrument ID:
¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: Sure-BioChem Laboratories LLC Job ID: 680-234374-1
Project/Site: Ft. Bragg NC (FTBR-308)
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
ANAB Dept. of Defense ELAP L2463 09-22-24
North Carolina (WW/SW)State 269 12-31-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
A2LA Dept. of Defense ELAP 0001.01 11-30-24
North Carolina (WW/SW)State 521 12-31-23
Eurofins Savannah
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Method Summary
Job ID: 680-234374-1Client: Sure-BioChem Laboratories LLC
Project/Site: Ft. Bragg NC (FTBR-308)
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds (GC/MS)EET SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)EET SAV
MA DEPMA VPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)ELLE
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)ELLE
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)ELLE
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET SAV
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)ELLE
SW8463630CSilica Gel Cleanup ELLE
SW8465030CPurge and Trap EET SAV
SW8465030CPurge and Trap ELLE
Protocol References:
MA DEP = Massachusetts Department Of Environmental Protection
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Sure-BioChem Laboratories LLC Job Number: 680-234374-1
Login Number: 234374
Question Answer Comment
Creator: Johnson, Corey M
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Sure-BioChem Laboratories LLC Job Number: 680-234374-1
Login Number: 234374
Question Answer Comment
Creator: Ballard, Megan
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 05/03/23 12:19 PMList Number: 2
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
FalseThere are no discrepancies between the containers received and the COC.Refer to Job Narrative for details.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Savannah
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