FA-2972_29195_CA_MRP_20231002

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
October 2, 2023

Mr. Nathan Beauchamp
NCDEQ-UST Section
Fayetteville Regional Office
Systel Building
225 Green Street, Suite 714
Fayetteville, NC 28301-5043

Re: Ground Water Monitoring & Receptor Survey Report
September 2023
Ya Ya #2
6283 Highway 301 South
Hope Mills, Cumberland County
North Carolina
Facility ID Number: 00-0-0000034183
Incident Number: 29195
GRI Project Number: 2215

Dear Mr. Beauchamp,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Rae Brown at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Gamil Aldalali, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring and Receptor Survey Report
September 2023
Ya Ya #2
6283 Highway 301 South
Hope Mills, Cumberland County
North Carolina
Facility ID Number: 00-0-0000034183
Incident Number: 29195
GRI Project Number: 2215

Prepared for:

Gamil Aldalali
6283 Highway 301 South
Hope Mills, North Carolina 28348

October 2, 2023

Rae Troiano Brown, P.G.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
i
SITE INFORMATION
1. Site Identification
 Ya Ya #2 (Facility ID 00-0-0000034183)
 Incident Number 29195 – High (H280D)
 Location of Source Area: 6283 Highway 301 South
Hope Mills, NC 28314
Cumberland County
34.9233475°N, 78.9491213°W (Topographical Map)

2. Information about Contacts Associated with the Leaking UST System

UST Owner
Mr. Gamil Nagi Al Dalali
6283 U.S. Highway 301 South
Hope Mills, NC 28348
[e-mail]
910-527-7486

UST Operator
Mr. Gamil Nagi Al Dalali
6283 U.S. Highway 301 South
Hope Mills, NC 28348
[e-mail]
910-527-7486

Property Owner
Gamil Nagi Al Dalali
6283 U.S. Highway 301 South
Hope Mills, NC 28348
[e-mail]
910-527-7486

Property Occupant
Pit Stop Express
6283 U. S. Highway 301 South
Hope Mills, NC 28348
[e-mail]
910-527-7486

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Certification No. 402
704-529-6364
3. Information about Release
 A release was discovered in 1994.
 An unknown amount of product was released from the leaking UST System.
 One 1,000-gallon gasoline UST and one 2,000-gallon gasoline UST were removed in May 2005.
One 11,000-gallon gasoline and one 4,000-gallon gasoline USTs are active at the site. One inactive
highway diesel AST is present at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
ii
EXECUTIVE SUMMARY
The former Ya Ya #2 site is located at 6283 Highway 301 South in Hope Mills, Cumberland County, North
Carolina. The site is currently owned and operated by Gamil Nagi Al Dalali as a petroleum retail facility.
One 1,000-gallon gasoline UST and one 2,000-gallon gasoline UST were removed in May 2005. Currently,
one 11,000-gallon gasoline UST and one 4,000-gallon gasoline UST are active at the site. According to
NCDEQ personnel, a previous release from the UST system had been reported.

On September 15, 2020, an updated receptor survey was conducted. According to the information
obtained during receptor survey activities, twenty-one potable water supply wells were identified within
1,000 feet of the source area. Of those twenty-one water supply wells, one is located within 250 feet of
the site. Public water is not available to the site or surrounding properties within a 1,500-foot radius of
the site. The adjoining properties are single family residential or commercial properties. A CAP has not
been completed for this incident.

On September 6 and 7, 2023, eight shallow Type II monitoring wells and six deep Type II monitoring wells,
were gauged, purged, and sampled. Free product was not observed. Concentrations of benzene, toluene,
ethylbenzene, MTBE, naphthalene, n-propylbenzene, and/or 1,2,4-trimethylbenzene that exceeded MACs
were reported in the ground water samples collected from MW-11R, MW-12, DMW-21, and DMW-27. All
the reported contaminant concentrations were below the GCLs. Three water supply wells were purged
and sampled; no detectable contaminant concentrations were reported in any of the supply wells.

Mann-Kendall analysis of petroleum constituents in MW-12 from February 2012 to present indicated that
benzene and toluene concentrations were generally decreasing while ethylbenzene and xylene
concentrations were generally increasing. As a whole, BTEX concentrations at the site have decreased
from February 2012.

Based on this information, a feasibility study should be conducted to determine whether ground water
modeling, ISCO, or MMPE events would be effective remedial strategies for this site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
ISCO: In Situ Chemical Oxidation
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................5
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................6
5.0 CONCLUSIONS .........................................................................................................................6
6.0 LIMITATIONS ...........................................................................................................................6
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................6

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Cross Section A-A’
Figure 7: Cross Section B-B’
Figure 8: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3 Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results
Table 7: Summary of Ground Water Sample Field Parameters

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Report – Ground Water Samples
Appendix C: Contaminant Mass Calculations
Appendix D: Mann-Kendall Analyses

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
1
1.0 SITE HISTORY AND CHARACTERIZATION
Geological Resources, Inc. (GRI) presents the results of the September 2023 ground water sampling event
at the former Ya Ya #2 site located at 6283 Highway 301 South in Hope Mills, Cumberland County, North
Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 23-438, which
was submitted to the North Carolina Department of Environmental Quality (NCDEQ) on July 13, 2023, and
approved as Task Authorization No. 29195-22 on August 3, 2023. State correspondence is included in
Appendix A.

According to NCDEQ personnel, a previous release from the UST system had been reported at the site.
Several owners/operators have managed the site since the release was reported. The current
owner/operator reportedly purchased the site in 2001. According to NCDEQ personnel, site assessment
activities, including a comprehensive site assessment, were initially conducted under the Federal Trust
Fund Program. Three water supply wells were affected by the release. However, these water supply wells
were either taken out of service or abandoned and replaced with new wells.

On May 25, 2005, GRI supervised the removal of one 2,000-gallon gasoline UST and one 1,000-gallon
gasoline UST from the site. Approximately 268 tons of affected soil were excavated during the closure
activities. Phase II Limited Site Assessment activities were conducted between August 24 and September
9, 2005.

Please note that information regarding the site prior to 2005 contained in this report was obtained under
the supervision of previous consultants. Although GRI cannot verify the accuracy of this information, for
the purposes of this report it is assumed to be correct.

The site is currently owned and operated by Gamil Nagi Al Dalali as a petroleum retail facility. Currently,
one 11,000-gallon gasoline UST and one 4,000-gallon gasoline UST are active at the site. UST
owner/operator information and UST system information are included as Tables 1 and 2, respectively.
The Registered Tank Report is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
2

A total of twenty-five shallow Type II monitoring wells and eight deep Type II monitoring wells were
installed at the site during past ground water assessment activities. Monitoring wells MW-1, MW-2R,
MW-3 through MW-5, MW-6R, MW-8, MW-10, MW-13, MW-14, MW-16, MW-17, MW-22, DMW-23,
DMW-28, MW-29, MW-30, and MW-32 could not be located or were reported to be damaged and/or
destroyed and therefore were not sampled.

The site and surrounding area is a mixture of single family residential and commercial properties. The site
contains one building and is primarily capped with concrete and asphalt. The overall topography at the
site is relatively flat.

On September 15, 2020, GRI personnel conducted an updated receptor survey at the site. Twenty-one
active potable water supply wells (SW-1, SW-2B, SW-3 through SW-10, SW-12, SW-13, SW-15 through
SW-18, SW-20, SW-21, SW-22A, and SW-26) were identified within a 1,000-foot radius of the site.
Municipal water is unavailable to the site or surrounding properties. The site does not lie within a
designated wellhead protection area. Water supply well owner information is presented in Table 3.
Adjacent property owner information is presented in Table 4. A Site Vicinity Map showing the locations
of water supply wells and property boundaries has been included as Figure 2. A Site Map showing the
locations of the monitoring wells and the structures on-site has been included as Figure 3.

To date, a CAP has not been completed for this incident.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On September 6 and 7, 2023, eight shallow Type II monitoring wells (MW-7, MW-11R, MW-12, MW-15,
MW-20, MW-24, MW-31, and MW-33), six deep Type II monitoring wells (DMW-9, DMW-18, DMW-19,
DMW-21, DMW-26, and DMW-27) were gauged, purged, and sampled in accordance with the NCDEQ

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
3
guidelines. Free product was not observed during the September 2023 gauging event. Depths to ground
water in the shallow Type II monitoring wells ranged from 7.11 feet to 10.31 feet. Depths to ground water
in the deep Type II monitoring wells ranged from 7.51 feet to 15.91 feet. Ground water elevations in the
deep Type II monitoring wells ranged from 92.22 feet to 90.79 feet. Ground water flow in the deep Type
II wells was generally toward the east-southeast with a horizontal gradient of approximately 0.003 feet
per foot. Well construction and gauging information is presented in Table 5. A Water Table Surface Map
based on the deep Type II monitoring wells is included as Figure 4. A summary of the current ground
water gauging data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-2R 2 - 12 12 103.06 DRY NM NM
MW-7 2 - 12 12 99.55 7.17 --- 92.38
DMW-9 30 - 35 35 99.73 7.51 --- 92.22
MW-11R NM NM 99.61 7.19 --- 92.42
MW-12 2 - 12 12 99.65 7.23 --- 92.42
MW-15 2 - 12 12 99.42 7.11 --- 92.31
DMW-18 15 - 30 30 103.65 12.86 --- 90.79
DMW-19 13 - 28 28 107.63 15.91 --- 91.72
MW-20 2 - 12 12 102.18 10.24 --- 91.94
DMW-21 15 - 30 30 102.41 10.19 --- 92.22
MW-24 2 - 12 12 102.57 10.31 --- 92.26
MW-25 2 - 12 12 104.77 DRY NM NM
DMW-26 15.5 – 30.5 30.5 104.61 12.72 --- 91.89
DMW-27 15 - 30 30 104.90 12.89 --- 92.01
MW-31 2 - 12 12 99.73 7.25 --- 92.48
MW-33 2 - 12 12 101.07 9.56 --- 91.51

On September 7, 2023, and three water supply wells (SW-1, SW-3, and SW-4) were purged and sampled.
Water supply well SW-2B was inactive at the time of sampling. Water supply well SW-22A was inaccessible
at the time of sampling.

Ground water samples collected from the monitoring wells and supply wells were submitted for
laboratory analyses using EPA Method 6200B. The concentrations of benzene, toluene, ethylbenzene,
xylenes, MTBE, naphthalene, n-propylbenzene, and/or 1,2,4-trimethylbenzene reported in the ground
water samples collected from MW-11R, MW-12, DMW-21, and DMW-27 exceeded the MACs. All the
reported contaminant concentrations were below the GCLs. No detectable contaminant concentrations
were reported in any of the supply wells.

A summary of the analytical results for ground water samples collected on September 7, 2023, is
presented in Table 6. A Ground Water Quality Map based on the September 2023 data is included as
Figure 5. Cross sections are included as Figures 6 and 7. A complete report of laboratory analyses of the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
4
ground water samples collected from the monitoring wells during the September 2023 sampling event
has been included as Appendix B. A summary of the current ground water analytical data is shown below:

Contaminant
of Concern

Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well ID
MAC (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-7 <0.180 <0.220 <0.170 <0.210 0.253 J <0.470
DMW-9 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-11R 6.15 27.2 104 37.2 <1.40 24.2
MW-12 30.8 J 7,290 1,380 5,390 <14.0 434
MW-15 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
DMW-18 <0.180 <0.220 <0.170 <0.210 0.216J <0.470
DMW-19 <0.180 <0.220 <0.170 <0.210 1.03 <0.470
MW-20 <0.180 <0.220 <0.170 <0.210 <0.140 2.84
DMW-21 4.18 0.314 J 32.8 1.11 0.611 J 10.2
MW-24 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
DMW-26 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
DMW-27 <0.180 <0.220 <0.170 <0.210 43.9 <0.470
MW-31 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-33 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
SW-1 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
SW-3 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470M
SW-4 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470M
Trip Blank <0.180 <0.220 <0.170 <0.210 <0.140 <0.470

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the February 2008 ground water sampling event, as well as the
maximum historical water column height observed in each area. A theoretical contaminant mass area
was calculated around MW-11R and MW-12 and used in the contaminant mass calculations. The
contaminant mass decreased by 24% between February 2008 and September 2023. Contaminant mass
calculations are included as Appendix C. A map of the contaminant mass area has been included as Figure
8. A chart depicting the overall trend in contaminant mass is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
5

Mann-Kendall plume stability analysis was conducted for the concentrations of benzene, toluene,
ethylbenzene, xylenes, and total BTEX in MW-12 for thirteen sampling events conducted between
February 22, 2013 (after FP was no longer observed at the site) and September 7, 2023. Although the
overall BTEX, benzene, and toluene concentrations have trended towards levels below the MACs in MW-
12, the concentrations of ethylbenzene and xylenes trend upward. Graphs displaying the trend lines for
each contaminant and total BTEX are included as Appendix D. Please note that two benzene results were
omitted because they were considered outliers.

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately 2 to 20 feet BGS.
3.0 FREE PRODUCT REMOVAL
Free product has historically been observed in MW-11R and MW-12. Five MMPE events have been
conducted at the site between June 2012 and February 2015. Approximately 60.96 gallons of vapor phase
free product have been removed from the site. Free product has not been observed at the site since
August 2012.
0.00
2.00
4.00
6.00
8.00
10.00
12.00
0.00
500.00
1000.00
1500.00
2000.00
2500.00
3000.00
3500.00
4000.00
4500.00
5000.00
Av
e
r
a
g
e

W
a
t
e
r

C
o
l
u
m
n

H
e
i
g
h
t

(
f
t
)
Co
n
t
a
m
i
n
a
n
t

M
a
s
s

(
g
r
a
m
s
)
Time
Total Contaminant Mass vs. Time
Water Column Height vs. Time
YA YA #2 (Incident No. 29195)
Contaminant Mass (grams)Water Column Height (ft)Linear (Contaminant Mass (grams))

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
6
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
MMPE events were conducted at the site as the primary method of corrective action at the site. No
natural attenuation monitoring plan is currently in place at the site. Field parameters were collected
during the September 2023 sampling event and are presented in Table 7.
5.0 CONCLUSIONS
 On September 6 and 7, 2023, ground water samples were collected from eight shallow Type II
monitoring wells, six deep Type II monitoring wells, and three water supply wells.
 Concentrations of benzene, toluene, ethylbenzene, MTBE, naphthalene, n-propylbenzene, and/or
1,2,4-trimethylbenzene that exceeded MACs were reported in the ground water samples
collected from MW-11R, MW-12, DMW-21, and DMW-27. All the reported contaminant
concentrations were below the GCLs. No free product was present in any of the monitoring wells.
 No detectable contaminant concentrations were reported in any of the supply wells.
 The contaminant mass has decreased by 24% between February 2008 and September 2023.
 Mann-Kendall analysis of petroleum constituents in MW-12 from February 2012 to present
indicated that benzene and toluene concentrations were generally decreasing while ethylbenzene
and xylene concentrations were generally increasing.
 Based on this information, a feasibility study should be conducted to determine whether ground
water modeling, ISCO, or MMPE events would be effective remedial strategies for this site.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Gamil Nagi Dalali for specific application to the
referenced site in Cumberland County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring and Receptor Survey Report
Prepared on: October 2, 2023 Ya Ya #2
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2215
7
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

6 Certification:
I, Rae Troiano Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The
certification number of the company or corporation is C-2727/C-127.

FIGURES
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"J SITE0412-57-5175
0412-47-7529
0412-46-6945
0412-46-9284
0412-67-0629
0412-57-7249
0412-67-0058
0412-57-5960
0412-56-7866
0412-57-0433
0412-67-6758
0412-57-1210
0412-67-2280
0412-56-0906
0412-57-4702
0412-47-3077
0412-56-0435
0412-67-3385
0412-58-7074
0412-57-4409
0412-46-7653
0412-57-5031
0412-67-0904
0412-56-3824
0412-56-1870
0412-57-0234
0412-57-3088
SW-9
SW-8
SW-7
SW-6
SW-5
SW-4 SW-3
SW-1
SW-26
SW-25
SW-24SW-23
SW-21
SW-20
SW-18
SW-17
SW-16
SW-15
SW-13
SW-12
SW-11
SW-10
SW-2B
SW-22A
I 95 S
I 95 N
US HWY 301 S
BRAXTON RD
MABRY RD
ROSLIN FARM RD
MCDONALD RD
I 95 N OFF RAMP EXIT 40
I 95 BUS SCONGREVE RD STATE RD
FIGURE 2: SITE VICINITY MAPYA YA #26283 HIGHWAY 301 SOUTHHOPE MILLS, CUMBERLAND COUNTYNORTH CAROLINAINCIDENT NO. 29195GRI NO. 2215
PREPARED BY:GEOLOGICAL RESOURCES, INC.JUNE 23, 2016REVISED: SEPTEMBER 29, 2020
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
³
0 300150Feet
1 inch = 319 feet
500-FOOT RADIUS
LEGEND
"J Potable Water Supply Well
Centerlines
Hydrolines
Pond or Lake
Subject Site
Well Owners and Adjacent Properties
Tax_Parcels

TABLES
UST ID Number 1A, 1B Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1A, 1B Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1, 2 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1, 2 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1, 2 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
Unknown Unknown
00-0-0000034183
Name of Owner or Operator Dates of Ownership / Operation
Various - John Paul Arnold, Ya Ya Food Stop,
Parker Brothers Pit Stop 01/01/1964 - 11/10/1994
Jean S. Bramble 11/10/1994 - 02/21/2002
Address Telephone Number
Unknown Unknown
6238 US Highway 301 S, Hope Mills, NC 28348 1-910-527-7486
00-0-0000034183
Name of Owner or Operator Dates of Ownership / Operation
Name of Owner or Operator Dates of Ownership / Operation
Gamil N. Aldalali 02/21/2002 - 05/25/2005
Address Telephone Number
Address Telephone Number
Unknown Unknown
00-0-0000034183
00-0-0000034183
Name of Owner or Operator Dates of Ownership / Operation
Waheeb A Abdulla 06/01/2006 - 11/01/2012
6238 US Highway 301 S, Hope Mills, NC 28348 1-910-527-7486
Address Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
YA YA # 2 (INCIDENT NO. 29195)
00-0-0000034183
Name of Owner or Operator Dates of Ownership / Operation
Gamil N. Aldalali 11/01/2012 - Current
Page 1 of 1
Date: 03/13/2020 Facility ID # : 00-0-0000034183
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 1,000 01/01/1964 Single Wall Steel 64" x 72" Other Removed
(05/25/2005)Yes
1A Gasoline 11,000 06/01/2006 Double Wall Steel 8' x 29' 3" Other Current No
1B Gasoline 4,000 06/01/2006 Double Wall Steel 64" x 24' Other Current No
2 Gasoline 2,000 01/01/1964 Single Wall Steel 64" x 12' Other Removed
(05/25/2005)Yes
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
TABLE 2
UST SYSTEM INFORMATION
YA YA # 2 (INCIDENT NO. 29195)
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Page 1 of 1
Date : 10/02/2023
Well #
(Can use Tax Number)
Well Owner/ User (indicate
which)Address Phone
Number
Well Use
(Potable/
Agricultural,
etc.)
Well Depth
(ft BGS)
Type of Well
(Drilled/
Bored)
Well Casing Depth
(ft. BGS)
Well Screen
Interval (x to y ft.
BGS)
Distance from
source area of
release
(ft.)
SW-1
(0412-57-5175)
Gamil Nagi Aldalali, Ibrahim A.
Alsaidi, & Enas A. Alsaidi
6283 U.S. Highway 301 South
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~310
SW-2B
(0412-57-5031)Brian K. Corbie 491 Norment Road
Lumberton, North Carolina 28358 Unknown Active/Potable Unknown Unknown Unknown Unknown ~215
SW-3
(0412-56-2897)David L. & Rita M. Pait 6815 Cooper Creek Drive
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~325
SW-4
(0412-56-1870)Betty L. Adcox 6321 U.S. Highway 301 South
Parkton, North Carolina 28371-9514 Unknown Active/Potable Unknown Unknown Unknown Unknown ~490
SW-5
(0412-57-0234)David Gregson 6175 McDonald Road
Parkton, North Carolina 28371 Unknown Active/Potable Unknown Unknown Unknown Unknown ~510
SW-6
(0412-57-0234)William Randall Caulder 6165 McDonald Road
Parkton, North Carolina 28371 Unknown Active/Potable Unknown Unknown Unknown Unknown ~530
SW-7
(0412-57-4409)Julia B. Upchurch 6266 U.S. Highway 301 South
Hope Mills, North Carolina 28348 [phone] Active/Potable Unknown Unknown Unknown Unknown ~285
SW-8
(0412-57-4702)Graham W. Bramble, Jr.6254 U.S. Highway 301 South
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~580
SW-9
(0412-57-5960)Kelvin S. Bramble 5080 Madison Avenue
Hope Mills, North Carolina 28348 [phone] Active/Potable Unknown Unknown Unknown Unknown ~750
SW-10
(0412-58-7074)Jose Eugenio Gonzalez Patlan 6202 U.S. Highway 301 South
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~880
SW-11
(0412-67-0629)Jorge V. Elias 5909 Watercrest Court
Fatetteville, North Carolina 28304 Unknown Inactive Unknown Unknown Unknown Unknown ~785
SW-12
(0412-67-0904)Rachel D. Martinez Heirs 6195 U.S. Highway 301 South
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~975
Facility ID # : 00-0-0000034183
TABLE 3
WATER SUPPLY WELL INFORMATION
YA YA # 2 (INCIDENT NO. 29195)
Page 1 of 2
Date : 10/02/2023
Well #
(Can use Tax Number)
Well Owner/ User (indicate
which)Address Phone
Number
Well Use
(Potable/
Agricultural,
etc.)
Well Depth
(ft BGS)
Type of Well
(Drilled/
Bored)
Well Casing Depth
(ft. BGS)
Well Screen
Interval (x to y ft.
BGS)
Distance from
source area of
release
(ft.)
Facility ID # : 00-0-0000034183
TABLE 3
WATER SUPPLY WELL INFORMATION
YA YA # 2 (INCIDENT NO. 29195)
SW-13
(0412-46-6945)Steve & Jeanette Elliott 6156 McDonald Road
Parkton, North Carolina 28371 [phone] Active/Potable Unknown Unknown Unknown Unknown ~820
SW-15
(0412-56-0906)
Ibrahim Alsaidi, Fuad Alsaidi,
Hana Alsaidi, & Gamil Aldalali
5320 South Forty Drive
Hope Mills North Carolina, 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~635
SW-16
(0412-46-7653)
Charles Mitchell Bartlemus, Jr.
Trustee
6360 U.S. Highway 301 South
Parkton, North Carolina 28371 Unknown Active/Potable Unknown Unknown Unknown Unknown ~880
SW-17
(0412-56-0435)Oscar W. & Doris B. Sealey 6365 U.S. Highway 301 South
Parkton, North Carolina 28371-9418 Unknown Active/Potable Unknown Unknown Unknown Unknown ~850
SW-18
(0412-46-9284)Allen W. & Mildred E. Jarman 6385 U.S. Highway 301 South
Parkton, North Carolina 28371-9514 [phone] Active/Potable Unknown Unknown Unknown Unknown ~985
SW-20
(0412-67-2280)Michael G. McLean 6246 Mabry Road
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~835
SW-21
(0412-67-3385)David F. Ferruzzi 6809 Towbridge Road
Fayetteville, North Carolina 28306 [phone] Active/Potable Unknown Unknown Unknown Unknown ~950
SW-22A
(0412-56-7866)Brenda Hood 6233 Roslin Farm Road
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~495
SW-23
(0412-67-0629)Jorge V. Elias 5909 Watercrest Court
Fatetteville, North Carolina 28304 Unknown Active/Potable Unknown Unknown Unknown Unknown ~727 NE
SW-24
(0412-67-6758)Esther Lee Morrison 6142 U.S. 301 Highway South
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~1,400 NE
SW-25
(0412-47-7529)
New Vison Christian Chuch
Inc.
P.O. Box 193
Hope Mills, North Carolina 28348 Unknown Active/Potable Unknown Unknown Unknown Unknown ~1,290 W
SW-26
(0412-47-2120)Steve & Jeanette Elliott 6156 McDonald Road
Parkton, North Carolina 28371 Unknown Active/Potable Unknown Unknown Unknown Unknown ~956 W
Notes:
• Water supply wells are keyed to Figure 2
• Ft. BGS : Feet below ground surface
Page 2 of 2
Facility ID # : 00-0-0000034183
0412-57-5175 (Site)Gamil Nagi Aldalali, Ibrahim A.
Alsaidi, & Enas A. Alsaidi
6283 U.S. Highway 301 South
Hope Mills, North Carolina 28348
0412-57-3088 Pit Stop 301 Express, LLC 6283 U.S. Highway 301 South
Hope Mills, North Carolina 28348
0412-57-5031 Brian K. Corbie 491 Norment Road
Lumberton, North Carolina 28358
0412-56-7866 Brenda Hood 6233 Roslin Farm Road
Hope Mills, North Carolina 28348
0412-67-0058 Zachary M. Taylor 6250 Mabry Road
Hope Mills, North Carolina 28348
0412-57-7249 Pit Stop 301 Express, LLC 6279 U.S. Highway 301 South
Hope Mills, North Carolina 28348
0412-57-4409 Julia B. Upchurch 6266 U.S. Highway 301 South
Hope Mills, North Carolina 29348
0412-57-1470 Graham Wesley Bramble, Jr.6254 U.S. Highway 301 South
Hope Mills, North Carolina 28348
0412-57-1210 Ibrahim Alsaidi 5320 South Forty Drive
Hope Mills, North Carolina 28348
Note:
• Properties are keyed to Figure 2.
Tax Parcel Number/ Map ID
TABLE 4
ADJACENT PROPERTY OWNERS
YA YA # 2 (INCIDENT NO. 29195)
Owner/ Occupant Name
(Last , First MI)Address
Date: 09/24/2020
Date: 09/12/2023 Facility ID # : 00-0-0000034183
02/13/08 8.26 0.00 91.16
01/06/10 7.14 0.00 92.2801/27/11 7.30 0.00 92.12
10/18/11 9.90 0.00 89.5208/02/12 10.12 0.00 89.3002/19/13 9.08 0.00 90.34
01/20/14 3.61 0.00 95.8109/11/14 9.34 0.00 90.08
03/09/15 2.22 0.00 97.2012/15/15 NM NM NM
02/27/20 3.09 0.00 96.3309/14/20 6.45 0.00 92.97
09/06/23 NM NM NM Destroyed02/13/08 8.43 0.00 94.63
01/06/10 10.71 0.00 92.3501/27/11 8.11 0.00 94.95
10/18/11 13.57 0.00 89.4908/02/12 13.80 0.00 89.26
02/19/13 12.71 0.00 90.3501/20/14 7.21 0.00 95.85
09/11/14 12.89 0.00 90.1703/09/15 5.89 0.00 97.17
12/15/15 7.75 0.00 95.3102/27/20 4.73 0.00 98.33
09/14/20 7.22 0.00 95.84 Damaged09/06/23 NM NM NM Dry
MW-3 01/31/95 02/13/08 NM NM NM NM NM NM NM DestroyedMW-4 06/04/99 02/13/08 NM NM NM NM NM NM NM Destroyed
MW-5 06/04/99 02/13/08 NM NM NM NM NM NM NM DestroyedMW-6R 10/28/04 02/13/08 NM NM NM NM NM NM NM Destroyed02/13/08 8.44 0.00 91.11
01/06/10 7.36 0.00 92.1901/27/11 7.49 0.00 92.06
10/18/11 10.15 0.00 89.4008/02/12 10.41 0.00 89.14
02/19/13 9.31 0.00 90.2401/20/14 3.84 0.00 95.71
09/11/14 9.54 0.00 90.0103/09/15 2.41 0.00 97.14
12/15/15 4.18 0.00 95.3702/27/20 2.64 0.00 96.91
09/14/20 6.17 0.00 93.3809/06/23 7.17 0.00 92.38
MW-8 06/04/99 02/13/08 NM NM NM NM NM NM NM Destroyed02/13/08 9.71 0.00 90.02
01/06/10 10.26 0.00 89.4701/27/11 7.39 0.00 92.34
10/18/11 10.62 0.00 89.1108/02/12 11.35 0.00 88.38
02/19/13 9.62 0.00 90.1101/20/14 4.64 0.00 95.09
09/11/14 10.24 0.00 89.4903/09/15 3.10 0.00 96.63
12/15/15 4.81 0.00 94.9202/27/20 3.34 0.00 96.3909/14/20 NM NM NM
09/06/23 7.51 0.00 92.22MW-10 09/22/99 02/13/08 NM NM NM NM NM NM NM Destroyed
06/04/99DMW-9 30-35 99.733530
12.5 99.42
TABLE 5
WELL CONSTRUCTION AND GAUGING DATA
YA YA # 2 (INCIDENT NO. 29195)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
Well Casing
Depth
(ft. BGS)
10/27/04MW-2R
01/30/95MW-1
99.55122-12206/04/99MW-7
103.06122-122
2.5 2.5-12.5
Page 1 of 5
Date: 09/12/2023 Facility ID # : 00-0-0000034183
TABLE 5
WELL CONSTRUCTION AND GAUGING DATA
YA YA # 2 (INCIDENT NO. 29195)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
Well Casing
Depth
(ft. BGS)
02/13/08 8.48 NA NM
01/06/10 7.35 NA NM01/27/11 7.54 0.00 NM
10/18/11 10.15 0.16 NM06/25/12 9.43 0.02 NM Before MMPE
06/29/12 9.50 0.00 NM After MMPE08/02/12 10.40 0.00 NM01/14/13 10.02 0.00 NM Before MMPE
01/17/13 10.12 0.00 NM After MMPE02/19/13 9.35 0.00 NM
12/16/13 8.18 0.00 NM Before MMPE12/20/13 8.20 0.00 NM After MMPE
01/20/14 3.82 0.00 NM08/04/14 8.81 0.00 NM Before MMPE
08/08/14 9.08 0.00 NM After MMPE09/11/14 9.73 0.00 NM
02/02/15 3.56 0.00 NM Before MMPE02/06/15 4.03 0.00 NM After MMPE
03/09/15 2.43 0.00 NM12/15/15 4.33 0.00 NM
06/08/16 4.06 0.00 NM12/06/16 4.00 0.00 NM
02/27/20 2.62 0.00 NM09/14/20 6.72 0.00 NM
03/09/21 1.92 0.00 NM03/22/23 7.02 0.00 NM
09/06/23 99.61 7.19 0.00 92.4202/13/08 8.47 0.00 91.18
01/06/10 7.37 0.00 92.2801/27/11 7.55 0.00 92.10
10/18/11 11.85 1.65 89.2206/25/12 9.48 0.03 90.20 Before MMPE06/29/12 9.44 0.00 90.21 After MMPE
08/02/12 10.46 0.03 89.2201/14/13 10.53 0.56 89.60 Before MMPE
01/17/13 10.08 0.00 89.57 After MMPE02/22/13 9.30 0.00 90.35
12/16/13 8.19 0.00 91.46 Before MMPE12/20/13 8.13 0.00 91.52 After MMPE
01/20/14 3.84 0.00 95.8108/04/14 8.88 0.00 90.77 Before MMPE
08/08/14 9.02 0.00 90.63 After MMPE09/11/14 9.66 0.00 89.99
02/02/15 3.59 0.00 96.06 Before MMPE02/06/15 4.05 0.00 95.60 After MMPE
03/09/15 2.43 0.00 97.2212/15/15 4.38 0.00 95.27
06/08/16 4.15 0.00 95.5012/06/16 4.00 0.00 95.65
02/27/20 2.66 0.00 96.99
09/14/20 6.70 0.00 92.95
03/09/21 1.92 0.00 97.73
03/22/23 7.17 0.00 92.48
09/06/23 7.23 0.00 92.42
MW-13 09/22/99 02/13/08 NM NM NM NM NM NM NM Destroyed
MW-14 09/23/99 02/13/08 NM NM NM NM NM NM NM Destroyed02/13/08 8.29 0.00 91.13
01/06/10 7.19 0.00 92.2301/27/11 7.32 0.00 92.10
10/18/11 9.92 0.00 89.5008/02/12 10.17 0.00 89.25
02/22/13 9.15 0.00 90.2701/20/14 3.64 0.00 95.78
09/11/14 9.34 0.00 90.0803/09/15 2.27 0.00 97.15
12/15/15 NM NM NM
02/27/20 2.98 0.00 96.44
09/14/20 6.51 0.00 92.91
09/06/23 7.11 0.00 92.31
02/13/08 8.84 0.00 91.11 01/06/10 7.14 0.00 92.81
01/27/11 7.95 0.00 92.0010/18/11 NM NM NM
08/02/12 NM NM NM NF09/11/14 10.12 0.00 89.83
03/09/15 2.88 0.00 97.07
12/15/15 NM NM NM
02/27/20 4.23 0.00 95.72
09/14/20 7.15 0.00 92.8009/06/23 NM NM NM NF
2-12209/22/99MW-15
99.95122-12209/23/99MW-16
NMNMNM08/24/05MW-11R NM
99.65122-12209/22/99MW-12
99.4212
Page 2 of 5
Date: 09/12/2023 Facility ID # : 00-0-0000034183
TABLE 5
WELL CONSTRUCTION AND GAUGING DATA
YA YA # 2 (INCIDENT NO. 29195)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
Well Casing
Depth
(ft. BGS)
02/13/08 7.62 0.00 91.04
01/06/10 6.57 0.00 92.0901/27/11 6.65 0.00 92.01
10/18/11 9.29 0.00 89.3708/02/12 7.82 0.00 90.84
02/22/13 NM NM NM NF09/11/14 NM NM NM NF03/09/15 NM NM NM NF
12/15/15 NM NM NM NF09/14/20 NM NM NM NF
09/06/23 NM NM NM NF02/13/08 9.95 0.00 93.70
01/06/10 12.12 0.00 91.5301/27/11 12.10 0.00 91.55
10/18/11 14.85 0.00 88.8008/02/12 15.77 0.00 87.88
02/19/13 13.94 0.00 89.7101/20/14 8.68 0.00 94.97
09/11/14 14.51 0.00 89.1403/09/15 7.27 0.00 96.38
12/15/15 NM NM NM09/14/20 8.14 0.00 95.51
09/06/23 12.86 0.00 90.7902/13/08 13.90 0.00 93.73
01/06/10 16.17 0.00 91.4601/27/11 16.20 0.00 91.43
10/18/11 18.95 0.00 88.6808/02/12 20.14 0.00 87.49
02/19/13 17.91 0.00 89.7201/20/14 12.72 0.00 94.91
09/11/14 18.84 0.00 88.7903/09/15 11.35 0.00 96.2812/15/15 NM NM NM
02/27/20 5.73 0.00 101.9009/14/20 12.12 0.00 95.51
09/06/23 15.91 0.00 91.7202/13/08 8.30 0.00 93.88
01/06/10 10.40 0.00 91.7801/27/11 10.51 0.00 91.67 Damaged
10/18/11 13.16 0.00 89.0208/02/12 13.45 0.00 88.73
02/22/13 12.26 0.00 89.9201/20/14 6.89 0.00 95.29
09/11/14 12.58 0.00 89.6003/09/15 5.45 0.00 96.73
12/15/15 NM NM NM09/14/20 7.62 0.00 94.56 Damaged
09/06/23 10.24 0.00 91.9402/13/08 8.28 0.00 94.13
01/06/10 10.34 0.00 92.0701/27/11 10.44 0.00 91.97
10/18/11 13.09 0.00 89.3208/02/12 13.41 0.00 89.00
02/19/13 12.22 0.00 90.1901/20/14 6.81 0.00 95.60
09/11/14 12.56 0.00 89.8503/09/15 5.41 0.00 97.0012/15/15 7.10 0.00 95.31
09/14/20 6.54 0.00 95.8703/09/21 4.71 0.00 97.70
03/22/23 9.92 0.00 92.4909/06/23 10.19 0.00 92.22
02/13/08 8.94 0.00 93.9601/06/10 10.70 0.00 92.20
01/27/11 10.89 0.00 92.0110/18/11 13.52 0.00 89.38
08/02/12 13.82 0.00 89.0802/19/13 12.64 0.00 90.26
01/20/14 7.23 0.00 95.6709/11/14 12.98 0.00 89.92
03/09/15 5.80 0.00 97.1012/15/15 NM NM NM
09/06/23 NM NM NM NF
107.632813-281310/27/04DMW-19
MW-20
10/27/04DMW-18
09/23/99MW-17
102.18122-12210/27/04
102.413015-301510/27/04DMW-21
102.90122-12210/27/04MW-22
103.653015-3015
98.66122-122
Page 3 of 5
Date: 09/12/2023 Facility ID # : 00-0-0000034183
TABLE 5
WELL CONSTRUCTION AND GAUGING DATA
YA YA # 2 (INCIDENT NO. 29195)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
Well Casing
Depth
(ft. BGS)
02/13/08 8.81 0.00 93.77
01/06/10 10.41 0.00 92.1701/27/11 10.59 0.00 91.99
10/18/11 13.25 0.00 89.3308/02/12 13.54 0.00 89.04
02/19/13 12.34 0.00 90.2401/20/14 6.95 0.00 95.6309/11/14 12.76 0.00 89.82
03/09/15 5.52 0.00 97.0612/15/15 7.44 0.00 95.14
06/08/16 7.31 0.00 95.2712/06/16 7.05 0.00 95.53
09/06/23 NM NM NM NF02/14/08 11.74 0.00 90.83
01/06/10 10.39 0.00 92.1801/27/11 10.59 0.00 91.98
10/18/11 NM NM NM DRY08/02/12 11.59 0.00 90.98
02/19/13 NM NM NM09/11/14 11.62 0.00 90.95
03/09/15 5.54 0.00 97.0312/15/15 7.43 0.00 95.14
02/27/20 4.02 0.00 98.5509/14/20 NM NM NM NF
09/06/23 10.31 0.00 92.2602/14/08 10.81 0.00 93.96
01/06/10 13.08 0.00 91.6901/27/11 13.09 0.00 91.68
10/18/11 NM NM NM DRY08/02/12 NM NM NM DRY
02/19/13 NM NM NM09/11/14 NM NM NM DRY03/09/15 8.16 0.00 96.61
12/15/15 10.07 0.00 94.7002/27/20 8.73 0.00 96.04
09/14/20 NM NM NM Not Accessible 09/06/23 NM NM NM DRY
02/14/08 10.87 0.00 93.7401/06/10 12.94 0.00 91.67
01/27/11 12.93 0.00 91.6810/18/11 15.65 0.00 88.96
08/02/12 16.30 0.00 88.3102/19/13 14.75 0.00 89.86
01/20/14 9.41 0.00 95.2009/11/14 15.30 0.00 89.31
03/09/15 8.01 0.00 96.6012/15/15 9.86 0.00 94.75
02/27/20 7.32 0.00 97.2909/14/20 8.64 0.00 95.97
09/06/23 12.72 0.00 91.8902/14/08 10.81 0.00 94.09
01/06/10 13.02 0.00 91.8801/27/11 13.13 0.00 91.77
10/18/11 15.83 0.00 89.0708/02/12 16.35 0.00 88.55
02/19/13 14.88 0.00 90.0201/20/14 9.62 0.00 95.2809/11/14 15.38 0.00 89.52
03/09/15 8.21 0.00 96.6912/15/15 10.03 0.00 94.87
06/08/16 10.01 0.00 94.8912/06/16 9.56 0.00 95.34
02/27/20 8.11 0.00 96.7909/14/20 9.02 0.00 95.88
03/09/21 7.27 0.00 97.6303/22/23 12.55 0.00 92.35
09/06/23 12.89 0.00 92.0102/14/08 11.56 0.00 90.88
01/06/10 10.55 0.00 91.8901/27/11 10.62 0.00 91.82
10/18/11 13.35 0.00 89.0908/02/12 11.55 0.00 90.89
02/19/13 NM NM NM DRY09/11/14 12.89 0.00 89.55
03/09/15 5.63 0.00 96.8112/15/15 7.52 0.00 94.92
06/08/16 NF NF NF Destroyed09/06/23 NM NM NM NF
102.582914-291410/28/04DMW-23
104.77122-122
102.572-122
10/26/04MW-25
10/28/04MW-24 12
104.903015-301510/26/04DMW-27
104.6130.515.5-30.515.510/26/04DMW-26
102.4429.514.510/28/04DMW-28 14.5-29.5
Page 4 of 5
Date: 09/12/2023 Facility ID # : 00-0-0000034183
TABLE 5
WELL CONSTRUCTION AND GAUGING DATA
YA YA # 2 (INCIDENT NO. 29195)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
Well Casing
Depth
(ft. BGS)
02/14/08 11.33 0.00 91.23
01/06/10 10.64 0.00 91.9201/27/11 10.76 0.00 91.80
10/18/11 NM NM NM DRY08/02/12 13.83 0.00 88.73
02/19/13 NM NM NM DRY01/20/14 7.23 0.00 95.3309/11/14 NM NM NM DRY
03/09/15 NM NM NM DRY12/15/15 NM NM NM
02/27/20 NM NM NM DRY09/14/20 NM NM NM NF
09/06/23 NM NM NM NF02/14/08 NF NF NF
01/06/10 NF NF NF10/18/11 NM NM NM DRY
08/02/12 NM NM NM Destroyed01/27/11 7.59 0.00 92.14
10/18/11 10.25 0.00 89.4808/02/12 10.50 0.00 89.23
02/19/13 9.32 0.00 90.4101/20/14 3.87 0.00 95.86
09/11/14 9.71 0.00 90.0203/09/15 2.49 0.00 97.24
12/15/15 NM NM NM09/14/20 6.77 0.00 92.96
09/06/23 7.25 0.00 92.4801/27/11 8.75 0.00 92.17
10/18/11 11.43 0.00 89.4908/02/12 11.72 0.00 89.20
02/19/13 10.53 0.00 90.3901/20/14 5.11 0.00 95.8109/11/14 10.91 0.00 90.01
03/09/15 3.70 0.00 97.2212/15/15 NM NM NM
09/14/20 NM NM NM NF09/06/23 NM NM NM NF
01/27/11 8.90 0.00 92.1710/18/11 11.62 0.00 89.45
08/02/12 11.93 0.00 89.1402/19/13 10.65 0.00 90.42
01/20/14 5.32 0.00 95.7509/11/14 11.02 0.00 90.05
03/09/15 3.87 0.00 97.2012/15/15 NM NM NM
09/06/23 9.56 0.00 91.51Notes:
MW-29
NANA
101.0712
102.56122-12210/28/04
99.73122-12201/27/11
2-122
10/28/04MW-30 NA NA
• NA: Data not available.
• * : Reference point for elevation measurements, assumed elevation 100.00 ft.• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• ft BGS : feet below ground surface.• NM: Not measured.
• NF: Not found.
01/27/11MW-33
MW-31
100.92122-12201/27/11MW-32
Page 5 of 5
Date : 09/26/2023 Facility ID #: 00-0-0000034183
RSK-175 SM-3500-FE-B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 25 70 400 400 NE 300 10,000 250,0005,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 30,500 11,700 26,100 28,500 24,100 NE NE NE NE02/13/08 <1.0 <1.0 <1.0 <3.0 6.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 0.700 J <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.21 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 11.1 <0.13 <0.25 <0.13 0.13 J NR NR NR NR NR NR NR NR NR NR NR09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/13/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR
01/06/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.700 <0.950 3.50 J 6.23 <1.25 26.9 10.4 13.4 8.40 14.6 10.3 108 39.4 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-3 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-4 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-5 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-6R 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/13/08 71.3 39.6 5.02 4.92 146 3.93 <1.0 <1.0 <1.0 <1.0 <1.0 2.59 <1.0 NR NR NR NR01/06/10 18.3 0.850 J <0.150 <0.220 23.1 3.69 <0.180 <0.140 <0.150 <0.200 <0.220 0.480 J <0.180 NR NR NR NR01/28/11 <0.700 <0.950 <0.750 <1.10 <1.25 <2.50 <0.900 <0.700 <0.750 <1.00 <1.10 <0.750 <0.900 NR NR NR NR
10/18/11 26.8 0.62 0.99 0.44 J 18.5 3.4 0.13 J 0.50 0.25 J <0.10 0.26 J 0.87 <0.10 NR NR NR NR08/02/12 15.9 <0.13 <0.15 <0.30 12.3 0.83 <0.10 0.18 J <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 522 879 236 765 249 133 4.3 7.8 17.6 4.8 34.4 197 33.3 NR NR NR NR
01/20/14 22.1 6.6 6.0 6.4 24.3 7.0 0.35 J 0.68 0.94 0.17 J 1.5 0.80 0.14 J NR NR NR NR09/11/14 1.0 0.49 J <0.10 <0.20 0.68 0.98 <0.10 0.17 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 8.7 <0.17 <0.15 6.6 2.8 2.5 <0.14 0.20 J <0.12 <0.12 <0.16 0.81 <0.14 NR NR NR NR12/15/15 0.48 J <0.17 <0.15 <0.43 0.33 J 0.33 J <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 3.7 <0.13 <0.13 10.1 2.4 3.9 0.24 J 0.83 0.65 <0.13 <0.13 9.2 <0.13 NR NR NR NR09/15/20 0.31 J <0.13 <0.13 <0.25 0.27 J <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 0.253 J <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 5.92 J <50.0 H 4,820 15,100
MW-8 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/13/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 0.696 J <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 0.20 J <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 230 H 92.0 J 11,300MW-10 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Contaminant of Concern 
Be
n
z
e
n
e
Nit
r
a
t
e
Fe
r
r
o
u
s

I
r
o
n
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YA YA # 2 (INCIDENT NO. 29195)
Analytical Method EPA Method 6200B/6210D/602 SW-9056A
Me
t
h
a
n
e
MW-7
To
l
u
e
n
e
MAC (µg/l)
Et
h
y
l
b
e
n
z
e
n
e
GCL (µg/l)
Su
l
f
a
t
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
MT
B
E
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MW-1
MW-2R
DMW-9
Page 1 of 6
Date : 09/26/2023 Facility ID #: 00-0-0000034183
RSK-175 SM-3500-FE-B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 25 70 400 400 NE 300 10,000 250,0005,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 30,500 11,700 26,100 28,500 24,100 NE NE NE NE
Contaminant of Concern 
Be
n
z
e
n
e
Nit
r
a
t
e
Fe
r
r
o
u
s

I
r
o
n
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YA YA # 2 (INCIDENT NO. 29195)
Analytical Method EPA Method 6200B/6210D/602 SW-9056A
Me
t
h
a
n
e
To
l
u
e
n
e
MAC (µg/l)
Et
h
y
l
b
e
n
z
e
n
e
GCL (µg/l)
Su
l
f
a
t
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
MT
B
E
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
02/13/08 581 2,200 300 1,180 182 221 <50 <50 <50 95.5 65.0 703 200 NR NR NR NR01/06/10 31.7 343 78.1 306 <0.250 22.2 5.20 1.54 4.28 2.38 9.13 83.3 27.8 NR NR NR NR
01/28/11 90.9 477 167 553 <12.5 124 <9.00 138 40.8 J <10.0 14.7 J 162 23.3 J NR NR NR NR10/18/11 FP FP FP FP FP FP FP FP FP FP FP FP FP NR NR NR NR08/02/12 37.8 75.9 50.7 173 8.8 18.5 0.63 0.71 3.4 0.90 7.3 48.2 14.8 NR NR NR NR
02/19/13 769 9,190 1,180 5,200 32.0 J 256 <10 13.6 J 41.6 J 11.2 J 94.9 724 167 NR NR NR NR01/20/14 3.0 19.1 13.0 88.1 0.36 J 6.2 0.73 0.70 1.9 0.54 5.1 29.5 5.9 NR NR NR NR09/11/14 16.6 299 147 654 <1.0 85.1 16.4 13.2 23.4 10.2 76.7 585 126 NR NR NR NR
02/02/15 2.5 36.3 23.7 109 <0.16 10.9 0.79 0.72 2.8 0.36 J 7.5 42 10.6 NR NR NR NR03/10/15 14.2 16.3 19.4 114 0.83 14.7 1 0.97 3.7 0.35 J 8.2 40.2 5.2 NR NR NR NR12/15/15 2.2 49.9 24.3 99.1 0.47 J 10.4 0.30 J 0.30 J 1.5 0.16 J 3.6 25.5 5.2 NR NR NR NR06/08/16 21.2 223 41.1 235 0.39 J 40.4 1.8 1.5 6 0.75 11.4 83.5 19.3 NR NR NR NR12/06/16 67.9 1,720 440 1,720 <6.3 112 <6.3 <6.3 25.3 <6.3 69.8 488 112 NR NR NR NR02/27/20 3.3 21.2 98.9 132 <0.13 38.8 1.5 1.9 8.1 1.2 20.7 62.3 10.6 NR NR NR NR09/15/20 26.2 272 144 369 <1.3 42.6 NR NR NR NR NR NR NR NR NR NR NR03/09/21 23.7 J 1,690 339 1,420 <6.3 47.1 NR NR NR NR NR NR NR NR NR NR NR03/22/23 12.7 547 232 506 0.828 J 55.3 NR NR NR NR NR NR NR NR NR NR NR09/07/23 6.15 27.2 104 37.2 <1.40 24.2 <1.80 <2.00 5.90 <0.890 15.1 68.4 2.77 J 1,400 2,350 H <76.0 24,900
02/13/08 3,140 11,900 840 3,620 1,370 880 V <500 <500 <500 <500 <500 620 <500 NR NR NR NR01/06/10 1,870 8,960 1,020 4,700 <5.00 349 125 70.0 78.5 66.3 162 1,280 303 NR NR NR NR01/28/11 1,410 6,450 1,040 4,240 102 317 88.5 53.2 90.4 46.0 J 157 1,100 309 NR NR NR NR
10/18/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP08/02/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP02/22/13 809 11,600 1,260 6,180 30.3 J 324 <20 25.6 J 41.6 J <20 109 876 198 NR NR NR NR
01/20/14 195 1,610 432 1,890 11.5 J 113 9.3 J 13.6 J 21.9 J 12.7 J 49.0 431 101 NR NR NR NR09/11/14 617 5,210 780 3,770 23.7 J 171 <10 12.0 J 30.1 J 10.3 J 72.8 612 146 NR NR NR NR02/02/15 220 3,660 678 3270 <16 192 <14 <14 36.3 J 14.7 J 93.4 721 186 NR NR NR NR
03/10/15 157 3750 682 3430 6.7 206 10.2 14.4 39.3 17.1 96 708 186 NR NR NR NR12/15/15 210 4,750 723 3,330 <16 197 <14 <14 30.2 J <12 64.6 588 142 NR NR NR NR06/08/16 99.3 6,080 849 4,620 <6.3 314 19.5 J 21.1 J 39.8 25.7 93.2 912 206 NR NR NR NR12/06/16 76.5 3,250 587 2,730 7.1 J 172 7.2 J 10.3 J 26.1 17.8 J 62.1 551 153 NR NR NR NR02/27/20 61.6 4,300 746 3,450 <13 163 <13 <13 19.0 J <13 40.4 J 390 117 NR NR NR NR09/15/20 63.1 J 5,330 1,020 3,850 <25 268 NR NR NR NR NR NR NR NR NR NR NR03/09/21 21.3 J 2,330 730 2,660 <6.3 185 NR NR NR NR NR NR NR NR NR NR NR03/22/23 25.6 2,317 E 758 3,404.7 E 2.03 J 270 NR NR NR NR NR NR NR NR NR NR NR09/07/23 30.8 J 7,290 1,380 5,390 <14.0 434 <18.0 <20.0 42.6 J <8.90 92.8 814 212 2250 5,530 H <76.0 766 J
MW-13 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-14 02/13/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/13/08 <1.0 <1.0 <1.0 <3.0 4.58 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 0.346 J <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 0.687 J <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 0.16 J <0.10 <0.20 <0.10 0.18 J <0.10 <0.10 <0.10 0.13 J <0.10 0.22 J <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 1.4 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 <50.0 H 3,770 48,40002/13/08 1.70 <1.0 7.56 7.14 6.02 20.6V 1.08 1.96 2.97 3.93 3.83 38.8 9.94 NR NR NR NR01/06/10 1.60 <0.190 4.87 3.89 1.69 13.7 2.71 2.19 2.65 1.89 3.98 29.8 8.65 NR NR NR NR
01/28/11 0.178 J <0.190 2.86 4.85 <0.250 8.03 1.38 1.34 2.14 1.15 2.17 19.9 5.31 NR NR NR NR10/18/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/02/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-12
MW-11R
MW-15
MW-16
Page 2 of 6
Date : 09/26/2023 Facility ID #: 00-0-0000034183
RSK-175 SM-3500-FE-B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 25 70 400 400 NE 300 10,000 250,0005,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 30,500 11,700 26,100 28,500 24,100 NE NE NE NE
Contaminant of Concern 
Be
n
z
e
n
e
Nit
r
a
t
e
Fe
r
r
o
u
s

I
r
o
n
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YA YA # 2 (INCIDENT NO. 29195)
Analytical Method EPA Method 6200B/6210D/602 SW-9056A
Me
t
h
a
n
e
To
l
u
e
n
e
MAC (µg/l)
Et
h
y
l
b
e
n
z
e
n
e
GCL (µg/l)
Su
l
f
a
t
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
MT
B
E
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
02/13/08 <1.0 <1.0 <1.0 <3.0 1.15 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 1.43 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 0.50 <0.11 <0.10 <0.10 NR NR NR NR
02/22/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/11/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/10/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/13/08 <1.0 <1.0 <1.0 <3.0 3.71 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 0.216 J <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 190 JH 1,110 20,50002/13/08 <1.0 <1.0 <1.0 <3.0 9.21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR
01/06/10 <0.140 <0.190 <0.150 <0.220 2.46 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.140 <0.190 <0.150 <0.220 3.19 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
08/02/12 <0.13 <0.13 <0.15 <0.30 0.71 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 3.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 1.6 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 0.71 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/27/20 <0.13 <0.13 <0.13 <0.25 0.52 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 0.25 J <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 1.03 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 <50.0 H 3,140 27,500
02/13/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 1.65 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 2.84 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 <50.0 H 10,500 13,50002/13/08 <1.0 <1.0 <1.0 <3.0 4.03 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR
01/06/10 <0.140 <0.190 <0.150 <0.220 0.816 J <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 0.195 J <0.190 <0.150 <0.220 16.5 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 0.20 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
08/02/12 <0.13 <0.13 <0.15 <0.30 1.8 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 <0.10 <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 1.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 9.9 <0.17 <0.15 12.8 1.1 11.4 0.41 J 0.84 1.2 <0.12 <0.16 3.4 0.31 J NR NR NR NR12/15/15 0.24 J <0.17 <0.15 <0.43 <0.16 0.19 J <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR09/15/20 2.2 <0.13 1.4 <0.25 0.21 J 2.1 NR NR NR NR NR NR NR NR NR NR NR03/09/21 2.1 <0.13 <0.13 <0.25 <0.13 8.2 NR NR NR NR NR NR NR NR NR NR NR03/22/23 3.77 <0.220 9.37 0.540 J 1.04 3.73 NR NR NR NR NR NR NR NR NR NR NR09/07/23 4.18 0.314 J 32.8 1.11 0.611 J 10.2 1.04 1.76 3.12 <0.089 4.96 1.43 <0.180 568 1,140 H <76.0 16,300
MW-17
DMW-21
MW-20
DMW-19
DMW-18
Page 3 of 6
Date : 09/26/2023 Facility ID #: 00-0-0000034183
RSK-175 SM-3500-FE-B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 25 70 400 400 NE 300 10,000 250,0005,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 30,500 11,700 26,100 28,500 24,100 NE NE NE NE
Contaminant of Concern 
Be
n
z
e
n
e
Nit
r
a
t
e
Fe
r
r
o
u
s

I
r
o
n
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YA YA # 2 (INCIDENT NO. 29195)
Analytical Method EPA Method 6200B/6210D/602 SW-9056A
Me
t
h
a
n
e
To
l
u
e
n
e
MAC (µg/l)
Et
h
y
l
b
e
n
z
e
n
e
GCL (µg/l)
Su
l
f
a
t
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
MT
B
E
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
02/13/08 85.9 3.77 28.8 26.8 152 87.5V 3.72 6.39 10.1 10.4 11.4 99.8 20.9 NR NR NR NR01/06/10 29.1 1.93 11.1 6.35 19.0 28.1 4.47 3.63 4.22 2.78 6.40 33.9 13.9 NR NR NR NR
01/28/11 6.02 <0.950 8.92 5.73 6.18 34.7 <0.900 3.50 J 7.88 3.26 J 6.26 34.1 14.0 NR NR NR NR10/18/11 5.6 0.14 J 25 28.4 2.2 69.9 8.8 14.8 17.3 13.4 28 125 48.2 NR NR NR NR08/02/12 2.6 <0.13 11.6 4.4 0.93 39.7 3.4 6.1 6.3 5.3 10.2 38.7 11.1 NR NR NR NR
02/19/13 1.5 <0.10 0.40 J <0.22 0.46 J 9.2 0.46 J 1 0.64 0.25 J 1.1 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 4.4 <0.10 10.3 2.9 2.3 53.8 4.6 8.6 7.5 7.7 12.9 34.1 6.8 NR NR NR NR
03/10/15 <0.17 <0.17 0.54 <0.43 <0.16 6 0.34 J 0.72 0.44 J 0.12 J 0.66 0.38 J <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/13/08 460 12.6 48.4 29.6 624 85.7V 3.13 5.10 9.18 9.45 14.4 57.3 26.2 NR NR NR NR01/06/10 206 123 66.3 78.9 83.0 64.2 7.97 7.27 11.9 5.60 19.8 77.6 20.3 NR NR NR NR01/28/11 44.1 <0.950 7.07 <1.10 27.0 60.3 4.52 J 5.50 10.8 2.92 J 11.1 2.58 J 3.58 J NR NR NR NR10/18/11 31.9 2.8 11.5 1.6 14.3 51 8.8 13.8 12.2 12.6 21.9 5.3 4.1 NR NR NR NR
08/02/12 46.1 1.2 11.4 2.6 12.8 34.9 2.5 4.1 5.7 2.3 9.6 4.7 0.55 NR NR NR NR02/19/13 21.8 0.75 5.6 0.69 J 6.4 34.4 2.4 4.2 4.4 1.8 7.8 0.46 J 0.42 J NR NR NR NR01/20/14 2.2 <0.10 0.25 J 0.24 J 1.3 5.6 0.33 J 0.73 0.41 J <0.10 0.46 J 0.74 <0.10 NR NR NR NR
09/11/14 26.6 2.2 20.1 10.9 10.7 40.3 2.3 4.5 4.5 2.5 7.6 10.5 0.48 J NR NR NR NR03/10/15 3.6 <0.17 5.3 0.60 J 1.5 30.5 1.9 3.5 3 2.2 5.2 5.3 0.91 NR NR NR NR12/15/15 10.5 3.9 26.5 19.4 1.7 56.9 3.7 5.8 6.3 3.8 11.2 35.3 4.1 NR NR NR NR06/08/16 0.79 <0.13 3.1 0.63 J 0.35 J 29.4 2 3.3 2.2 1.7 4 5.4 1.2 NR NR NR NR12/06/16 2.0 <0.13 0.81 <0.31 0.88 22.5 1.8 4 1.7 0.32 J 2.1 0.75 <0.13 NR NR NR NR09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/14/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 0.672 J <0.200 <0.220 <0.150 <0.180 NR NR NR NR
10/18/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/02/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 80.0 JH <76.0 23,40002/14/08 <1.0 <1.0 <1.0 <3.0 2.04 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR
01/06/10 <0.140 <0.190 <0.150 <0.220 <0.250 1.80 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.140 <0.190 <0.150 <0.220 0.306 J <0.500 <0.180 <0.140 <0.150 0.767 J <0.220 <0.150 <0.180 NR NR NR NR10/18/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/02/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 0.15 J <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 0.51 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/14/08 <1.0 <1.0 <1.0 <3.0 2.57 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/06/10 <0.140 <0.190 <0.150 <0.220 2.36 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.140 <0.190 <0.150 <0.220 3.20 <0.500 <0.180 <0.140 0.691 J <0.200 <0.220 <0.150 <0.180 NR NR NR NR
10/18/11 <0.13 <0.13 <0.15 <0.30 5.7 0.25 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 0.76 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 <0.10 <0.10 <0.10 <0.22 4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/20/14 <0.10 <0.10 <0.10 <0.20 4.3 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 2.3 0.20 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 0.8 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 3.6 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 0.54 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 16.3 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 16.2 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 60.0 JH 92.0 J 28,400
DMW-26
DMW-23
MW-25
MW-24
MW-22
Page 4 of 6
Date : 09/26/2023 Facility ID #: 00-0-0000034183
RSK-175 SM-3500-FE-B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 25 70 400 400 NE 300 10,000 250,0005,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 30,500 11,700 26,100 28,500 24,100 NE NE NE NE
Contaminant of Concern 
Be
n
z
e
n
e
Nit
r
a
t
e
Fe
r
r
o
u
s

I
r
o
n
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YA YA # 2 (INCIDENT NO. 29195)
Analytical Method EPA Method 6200B/6210D/602 SW-9056A
Me
t
h
a
n
e
To
l
u
e
n
e
MAC (µg/l)
Et
h
y
l
b
e
n
z
e
n
e
GCL (µg/l)
Su
l
f
a
t
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
MT
B
E
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
02/14/08 <1.0 <1.0 <1.0 <3.0 87.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/07/10 0.521 J <0.190 <0.150 <0.220 64.1 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 0.184 J <0.190 <0.150 <0.220 102 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 0.17 J <0.13 <0.15 <0.30 55 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.26 <0.26 <0.29 <0.60 58.9 <0.20 <0.20 <0.20 <0.20 <0.20 <0.21 <0.20 <0.20 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 64 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 0.47 J <0.10 <0.10 <0.20 77.3 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 53.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 1.4 <0.17 <0.15 <0.43 49.4 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 0.62 <0.17 <0.15 <0.43 65.7 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR06/08/16 <0.13 <0.13 <0.13 <0.31 65.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR12/06/16 0.86 <0.13 <0.13 <0.31 35 0.16 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 0.51 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 56.4 <0.13 NR NR NR NR NR NR NR NR NR NR NR03/09/21 4.1 <0.13 <0.13 <0.25 14.8 <0.13 NR NR NR NR NR NR NR NR NR NR NR03/22/23 <0.180 <0.220 <0.170 <0.210 43 <0.470 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 43.9 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 410 H <76.0 26,30002/14/08 4.68 <1.0 <1.0 <3.0 110 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/07/10 15.7 <0.190 <0.150 <0.220 96.1 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 26.5 <0.190 <0.150 <0.220 43.1 3.82 0.327 J 0.976 J 0.955 J <0.200 <0.220 <0.150 <0.180 NR NR NR NR
10/18/11 12.4 <0.13 <0.15 <0.30 29.6 0.31 J <0.10 0.15 J 0.13 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/11/14 8.7 <0.10 <0.10 <0.20 6.6 7.6 0.27 J 0.88 0.49 J <0.10 0.25 J <0.10 <0.10 NR NR NR NR03/10/15 5.4 <0.17 <0.15 <0.43 3.2 1.7 <0.14 0.26 J 0.25 J <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 16.3 0.19 J 3.4 1.9 4.1 6 0.53 1.3 1.6 <0.12 1.9 0.66 <0.14 NR NR NR NR09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/14/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/10 <0.140 <0.190 <0.150 <0.220 0.618 J <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/02/12 35.3 0.22 J 2.1 0.63 J 32.5 3.3 0.28 J 0.61 0.69 <0.10 1.0 0.24 J <0.10 NR NR NR NR02/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/27/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-30 02/14/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/28/11 0.292 J 0.902 J 0.229 J 1.40 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 0.544 J <0.180 NR NR NR NR
10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 <50.0 H 773 16,100
01/28/11 <0.280 <0.380 <0.300 0.634 J <0.500 <1.00 <0.360 <0.280 <0.300 <0.400 <0.440 <0.300 <0.360 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/28/11 0.245 J 0.708 J 0.171 J 1.12 <0.250 2.66 <0.180 <0.140 <0.150 <0.200 <0.220 0.668 J 0.181 J NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 <2.51 <50.0 H 2,450 9,940SW-1 09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 NS NS NS NS
DMW-28
MW-29
MW-32
MW-31
MW-33
DMW-27
Page 5 of 6
Date : 09/26/2023 Facility ID #: 00-0-0000034183
RSK-175 SM-3500-FE-B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 25 70 400 400 NE 300 10,000 250,0005,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 30,500 11,700 26,100 28,500 24,100 NE NE NE NE
Contaminant of Concern 
Be
n
z
e
n
e
Nit
r
a
t
e
Fe
r
r
o
u
s

I
r
o
n
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YA YA # 2 (INCIDENT NO. 29195)
Analytical Method EPA Method 6200B/6210D/602 SW-9056A
Me
t
h
a
n
e
To
l
u
e
n
e
MAC (µg/l)
Et
h
y
l
b
e
n
z
e
n
e
GCL (µg/l)
Su
l
f
a
t
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
MT
B
E
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
02/14/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/07/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 0.15 J <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS02/14/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR01/07/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 M <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 NS NS NS NS02/14/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR
01/07/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
02/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR01/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.12 <0.16 <0.14 <0.14 NR NR NR NR02/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR09/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 M <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 NS NS NS NS02/14/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR
01/07/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.200 <0.220 <0.150 <0.180 NR NR NR NR01/28/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS10/18/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
08/02/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR02/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
03/10/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS12/15/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS09/07/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSTrip Blank 09/07/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.200 <0.180 <0.089 <0.190 <0.190 <0.180 NS NS NS NSNotes:
• MAC: Maximum allowable concentration as specified in 15A NCAC 2L.0202.
• J: Estimated value.• Refer to laboratory report for other compounds detected at concentrations below the MAC.
• NS: Not sampled.
• GCL : Gross contamination level.
• H: Beyond holding time.
SW-2B
SW-22A
• FP: Free Product.• V: Present in blank.
• μg/l : micrograms per liter.
• NR: Not Requested.
• E: Exceeds calibration range.
SW-4
SW-3
• H : Outside of hold time.
• Concentrations in bold face type exceed the MAC.• Results reported in μg/l.• < : Less than the method detection limit specified in the laboratory report.
Page 6 of 6
Date: 09/12/23 Facility ID #: 00-0-0000034183
Well No. Sample Date DO (mg/L) pH Temp(oC)Conductivity
(µS/m)
Oxidation-
Reduction
Potential (mV)
MW-7 9/7/2023 0.84 5.47 26.30 129.00 202.50
DMW-9 9/7/2023 0.77 4.98 24.78 111.00 202.30
03/22/23 1.25 6.25 18.12 231 -43.9
9/7/2023 0.89 6.44 27.93 287 -80.6
03/22/23 1.36 5.99 18.08 158 -5.5
9/7/2023 0.85 6.16 27.12 272 -40.1
MW-15 9/7/2023 0.78 4.91 25.70 286 216.7
MW-18 9/7/2023 0.91 4.80 20.53 93 214.2
MW-19 9/7/2023 0.76 5.04 20.12 109 233.6
MW-20 9/7/2023 0.80 5.97 23.68 216 164.6
03/22/23 1.68 5.46 15.52 82 239.1
9/7/2023 0.90 5.41 23.21 97 118.4
MW-24 9/7/2023 0.88 5.02 22.53 81 238.2
DMW-26 9/7/2023 0.87 6.22 21.24 97 217.1
03/22/23 2.02 5.10 14.68 62 190.6
9/7/2023 0.65 4.56 20.11 72 279.1
MW-31 9/7/2023 0.78 4.87 22.63 46 245.1
MW-33 9/7/2023 0.90 5.19 23.27 48 232.5
Notes:
TABLE 7
SUMMARY OF GROUND WATER SAMPLE FIELD PARAMETERS
YA YA # 2 (INCIDENT NO. 29195)
• Field measurements of dissolved oxygen, pH, temperature, conductivity, and ORP were collected during
sampling using a field meter.
MW-12
MW-11R
DMW-21
DMW-27
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville,
NC 28301 | [phone]

June 8, 2023

Gamil Nagi Dalali
6283 Highway 301 South
Hope Mills, NC 28348

Re: Acknowledgement of Report Receipt
YaYa #2
6283 Highway 301 South
Hope Mills, Cumberland County
Incident Number: 29195
Risk Classification: High
Ranking: H245D
Dear Mr. Dalali:
The UST Section, Division of Waste Management, is in receipt of the report dated April 27, 2023. The
report has been reviewed and will be maintained in the Fayetteville Regional Office. The UST Section
agrees with the conclusion and recommendations presented in the report.
If you have questions regarding the information contained in this letter, please contact me at the address or
telephone number listed below.

Sincerely,

Nathan Beauchamp
Hydrogeologist
Fayetteville Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Rae Brown – GRI (email only)
Site Name City / County /Cumberland Incident #29195
Resp Pty Name / Contact Incident Mgr Region FAY
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #21
Consultant / Project Mgr /Rae Troiano Brown
Telephone / Fax Number /Task Authorization Number:22 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:H245D RRA Date:8/13/2016
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w
3r
d

P
t
y

D
e
d
?
Task #Lab /
SubCode
RO

I
M

A
u
t
h
Proposed
Rate/Price
(Consultant)RO

S
u
p
v
.

Au
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
3.351 1 /well y $80.00 Y $80.00 $80.00 /
4.031 24 / wells y $110.00 Y $2,640.00 $2,640.00 /
4.090 #240 29 / samples y $94.00 Y $2,726.00 $2,726.00 /
4.090 #272 1 / sample y $66.00 Y $66.00 $66.00 /
4.090 #441 24 / samples y $14.00 Y $336.00 $336.00 /
4.090 #490 24 / samples y $20.00 Y $480.00 $480.00 /
4.090 #510 24 / samples y $15.00 Y $360.00 $360.00 /
4.090 #521 24 / samples y $70.00 Y $1,680.00 $1,680.00 /
4.091 4 /shipments y $60.00 Y $240.00 $240.00 /
5.070 1 / event N $2,800.00 N $2,800.00 $0.00 /
6.090 1 / report y $1,125.00 Y $1,125.00 $1,125.00 /
12.030 1 / night y $151.00 Y $151.00 $151.00 /
12.050 1 / trip y $250.00 Y $250.00 $250.00 /
12.055 1 / trip y $50.00 Y $50.00 $50.00 /
4.041 5 / well Y $75.00 Y $375.00 $375.00 /
6.064 1 / report y $500.00 Y $500.00 $500.00 /
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$13,859.00 $11,059.00 TOTAL:
Total Standard Costs (Not Third Party)$13,859.00 $11,059.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:7/13/23 by:(PM)(Reserved for RO)
RO Review: 8/2/23 by:(IM)Joint UST Preapproval Confirmed By:Date1
RO Supv. Review: 8/3/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work
proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the
UST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED - CAB ONLY
Hope Mills
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Ya Ya 2
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If, following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this form to
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12months of the completion dateof the FIRST completed task to remain within the Statute ofLimitations. All ePATAs submitted within a claim are closed with that
claim, and may not be re-used in a separate submittal, even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
NJB
MHH
(Initials)
RTB
Proposed
Units / Type
(Consultant)
Nathan Beauchamp
ACTIVEYES
23-438 September 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Gamil Nagi Dalali
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality - Division of Waste Management
6.090 - Future MRP must include pertinent information as outlined in our guidance documents - including but not limited to;
all historical groundwater elevations in one table, analytical data in one table, depth to water vs. COC concentration figure,
updated cross-sections, updated water supply well construction data (see incident 14119), and plume stability analysis.
5.070 - Not required at this time.
4.041 - added SW-1, SW-2B, SW-3, SW-4, SW-22A
4.090 - increased #240 to 29 samples to include WSWs
6.064 - added plume stability analysis
- Purpose of this comprehensive sampling event is to establish next steps moving forward.
NJB
8/3/2023
8/3/23
2215 Received AUG 04 2023

APPENDIX B
Laboratory Report – Ground Water Samples

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/13/2023
Geological Resources, Inc. Rae Brown
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-251-0004 Client Project Description: YaYa #2
GRI #2215
Dear Rae Brown:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/8/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 114
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-251-0004
Page 2 of 114
Report Number:
Sample Summary Table
Client Project Description:
23-251-0004
YaYa #2
GRI #2215
Lab No Client Sample ID Matrix Date Collected Date Received
09/07/2023 07:41Aqueous 94473 Trip Blank 09/08/2023 10:10
09/07/2023 07:56Aqueous 94474 DMW-26 09/08/2023 10:10
09/07/2023 08:17Aqueous 94475 DMW-27 09/08/2023 10:10
09/07/2023 08:32Aqueous 94476 SW-1 09/08/2023 10:10
09/07/2023 08:48Aqueous 94477 DMW-21 09/08/2023 10:10
09/07/2023 09:09Aqueous 94478 MW-20 09/08/2023 10:10
09/07/2023 09:24Aqueous 94479 DMW-19 09/08/2023 10:10
09/07/2023 09:45Aqueous 94480 DMW-18 09/08/2023 10:10
09/07/2023 10:02Aqueous 94481 MW-24 09/08/2023 10:10
09/07/2023 10:19Aqueous 94482 MW-33 09/08/2023 10:10
09/07/2023 10:36Aqueous 94483 MW-31 09/08/2023 10:10
09/07/2023 10:53Aqueous 94484 DMW-9 09/08/2023 10:10
09/07/2023 11:14Aqueous 94485 MW-7 09/08/2023 10:10
09/07/2023 11:29Aqueous 94486 MW-15 09/08/2023 10:10
09/07/2023 11:47Aqueous 94487 MW-12 09/08/2023 10:10
09/07/2023 12:02Aqueous 94488 MW-11R 09/08/2023 10:10
09/07/2023 12:10Aqueous 94489 SW-3 09/08/2023 10:10
09/07/2023 12:17Aqueous 94490 SW-4 09/08/2023 10:10
Page 3 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-251-0004
Report Limit
Project:YaYa #2
V 94474DMW-26
J1.17 09/09/2023 03:026200BMethyl Ethyl Ketone (MEK)µg/L 0.710
16.2 09/09/2023 03:026200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J2.18 09/09/2023 03:026200Btert-Butyl Alcohol (TBA)µg/L 1.60
J92.0 09/08/2023 13:309056ANitrate (NO3-N)µg/L 76.0
28400 09/08/2023 13:309056ASulfateµg/L 650
J60.0 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
V 94475DMW-27
43.9 09/09/2023 03:266200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J2.57 09/09/2023 03:266200Btert-Butyl Alcohol (TBA)µg/L 1.60
J1.85 09/09/2023 03:266200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
26300 09/08/2023 13:429056ASulfateµg/L 650
410 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
V 94476SW-1
J1.43 09/09/2023 03:516200BMethyl Ethyl Ketone (MEK)µg/L 0.710
V 94477DMW-21
4.18 09/09/2023 04:166200BBenzeneµg/L 0.180
1.04 09/09/2023 04:166200Bn-Butylbenzene µg/L 0.180
1.76 09/09/2023 04:166200Bsec-Butyl benzene µg/L 0.200
32.8 09/09/2023 04:166200BEthylbenzeneµg/L 0.170
3.12 09/09/2023 04:166200BIsopropylbenzeneµg/L 0.180
J0.611 09/09/2023 04:166200BMethyl tert-butyl ether (MTBE)µg/L 0.140
10.2 09/09/2023 04:166200BNaphthaleneµg/L 0.470
4.96 09/09/2023 04:166200Bn-Propylbenzene µg/L 0.190
J0.314 09/09/2023 04:166200BTolueneµg/L 0.220
1.43 09/09/2023 04:166200B1,2,4-Trimethylbenzene µg/L 0.190
1.11 09/09/2023 04:166200Bo-Xylene µg/L 0.210
1.11 09/09/2023 04:166200BXylene (Total)µg/L 0.210
16300 09/08/2023 13:549056ASulfateµg/L 650
568 09/12/2023 12:53RSK-175 Methane µg/L 2.51
1140 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
V 94478MW-20
J1.27 09/09/2023 04:406200BMethyl Ethyl Ketone (MEK)µg/L 0.710
2.84 09/09/2023 04:406200BNaphthaleneµg/L 0.470
10500 09/08/2023 14:079056ANitrate (NO3-N)µg/L 76.0
Page 4 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-251-0004
Report Limit
Project:YaYa #2
V 94478MW-20
13500 09/08/2023 14:079056ASulfateµg/L 650
V 94479DMW-19
J1.36 09/09/2023 05:056200BMethyl Ethyl Ketone (MEK)µg/L 0.710
1.03 09/09/2023 05:056200BMethyl tert-butyl ether (MTBE)µg/L 0.140
3140 09/08/2023 14:199056ANitrate (NO3-N)µg/L 76.0
27500 09/08/2023 14:199056ASulfateµg/L 650
V 94480DMW-18
J0.216 09/09/2023 05:306200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J1.81 09/09/2023 05:306200Btert-Butyl Alcohol (TBA)µg/L 1.60
1110 09/08/2023 14:319056ANitrate (NO3-N)µg/L 76.0
20500 09/08/2023 14:319056ASulfateµg/L 650
J19009/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
V 94481MW-24
J1.91 09/09/2023 05:556200BAcetoneµg/L 1.80
23400 09/08/2023 14:449056ASulfateµg/L 650
J80.0 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
V 94482MW-33
2450 09/08/2023 14:569056ANitrate (NO3-N)µg/L 76.0
9940 09/08/2023 14:569056ASulfateµg/L 650
V 94483MW-31
773 09/08/2023 15:099056ANitrate (NO3-N)µg/L 76.0
16100 09/08/2023 15:099056ASulfateµg/L 650
V 94484DMW-9
J92.0 09/08/2023 15:219056ANitrate (NO3-N)µg/L 76.0
11300 09/08/2023 15:219056ASulfateµg/L 650
230 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
V 94485MW-7
J0.253 09/09/2023 07:346200BMethyl tert-butyl ether (MTBE)µg/L 0.140
4820 09/08/2023 15:589056ANitrate (NO3-N)µg/L 76.0
15100 09/08/2023 15:589056ASulfateµg/L 650
J5.92 09/12/2023 12:02RSK-175 Methane µg/L 2.51
Page 5 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-251-0004
Report Limit
Project:YaYa #2
V 94486MW-15
J1.97 09/09/2023 07:596200BAcetoneµg/L 1.80
3770 09/08/2023 16:109056ANitrate (NO3-N)µg/L 76.0
48400 09/08/2023 16:109056ASulfateµg/L 650
V 94487MW-12
J30.8 09/09/2023 10:286200BBenzeneµg/L 18.0
1380 09/09/2023 10:286200BEthylbenzeneµg/L 17.0
J42.6 09/09/2023 10:286200BIsopropylbenzeneµg/L 18.0
434 09/09/2023 10:286200BNaphthaleneµg/L 47.0
92.8 09/09/2023 10:286200Bn-Propylbenzene µg/L 19.0
7290 09/09/2023 10:286200BTolueneµg/L 22.0
814 09/09/2023 10:286200B1,2,4-Trimethylbenzene µg/L 19.0
212 09/09/2023 10:286200B1,3,5-Trimethylbenzene µg/L 18.0
1560 09/09/2023 10:286200Bo-Xylene µg/L 21.0
3830 09/09/2023 10:286200Bm,p-Xylene µg/L 42.0
5390 09/09/2023 10:286200BXylene (Total)µg/L 21.0
J76609/08/2023 16:239056ASulfateµg/L 650
2250 09/12/2023 14:49RSK-175 Methane µg/L 25.1
5530 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 250
V 94488MW-11R
6.15 09/09/2023 08:496200BBenzeneµg/L 1.80
104 09/09/2023 08:496200BEthylbenzeneµg/L 1.70
5.90 09/09/2023 08:496200BIsopropylbenzeneµg/L 1.80
24.2 09/09/2023 08:496200BNaphthaleneµg/L 4.70
15.1 09/09/2023 08:496200Bn-Propylbenzene µg/L 1.90
27.2 09/09/2023 08:496200BTolueneµg/L 2.20
68.4 09/09/2023 08:496200B1,2,4-Trimethylbenzene µg/L 1.90
J2.77 09/09/2023 08:496200B1,3,5-Trimethylbenzene µg/L 1.80
15.4 09/09/2023 08:496200Bo-Xylene µg/L 2.10
21.8 09/09/2023 08:496200Bm,p-Xylene µg/L 4.20
37.2 09/09/2023 08:496200BXylene (Total)µg/L 2.10
24900 09/08/2023 16:359056ASulfateµg/L 650
1400 09/12/2023 13:06RSK-175 Methane µg/L 2.51
2350 09/08/2023 12:00SM-3500-FE-B Ferrous Iron µg/L 50.0
Page 6 of 114

Client: Geological Resources, Inc. CASE NARRATIVE
Project: YaYa #2 Lab Report Number: 23-251-0004
Date: 9/13/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2,3-Trichlorobenzene QC Batch No: V37674/V37678
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V37674/V37678
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Naphthalene QC Batch No: V37674/V37678
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: tert-Amyl alcohol QC Batch No: V37674/V37678 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Vinyl acetate QC Batch No: V37674/V37678
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Page 7 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94473 Matrix:
9/7/2023 7:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 02:12 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 02:12 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 02:12 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 02:12 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 02:12 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 02:12 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 02:12 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 02:12 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 02:12 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 02:12 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 02:12 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 02:12 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 02:12 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 02:12 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 02:12 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 02:12 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 02:12 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 02:12 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 02:12 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 02:12 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 8 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94473 Matrix:
9/7/2023 7:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 02:12 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 02:12 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 02:12 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 02:12 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 02:12 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 02:12 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 02:12 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 02:12 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 02:12 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 02:12 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 02:12 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 02:12 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 02:12 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 02:12 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 02:12 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 02:12 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 02:12 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 02:12 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 02:12 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 02:12 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 02:12 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 9 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94473 Matrix:
9/7/2023 7:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 02:12 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 02:12 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 02:12 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 02:12 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 02:12 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 02:12 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 02:12 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 02:12 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 02:12 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 02:12 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 02:12 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 02:12 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 02:12 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 02:12 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 02:12 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 02:12 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 02:12 V37679MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 02:12 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 02:12 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 10 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94473 Matrix:
9/7/2023 7:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 02:12 V37679
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%09/09/23 02:121 MSA V37679
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%09/09/23 02:121 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%09/09/23 02:121 MSA V37679
Surrogate: Toluene-d8 97.0 Limits: 70-130%09/09/23 02:121 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 11 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-26
94474 Matrix:
9/7/2023 7:56
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 03:02 6200BMSA
60.0 JH µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 10:18 RSK-175TBL
92.0 J µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 13:30 9056AKNC
28400 µg/L 650 2000Sulfate 1 09/08/23 13:30 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-26
94474 Matrix:
9/7/2023 7:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 03:02 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 03:02 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 03:02 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 03:02 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 03:02 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 03:02 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 03:02 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 03:02 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 03:02 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 03:02 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 03:02 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 03:02 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 03:02 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 03:02 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 03:02 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 03:02 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 03:02 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 03:02 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 03:02 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 03:02 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-26
94474 Matrix:
9/7/2023 7:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 03:02 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 03:02 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 03:02 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 03:02 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 03:02 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 03:02 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 03:02 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 03:02 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 03:02 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 03:02 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 03:02 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 03:02 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 03:02 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 03:02 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 03:02 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 03:02 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 03:02 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 03:02 V37679MSA
1.17 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 03:02 V37679MSA
16.2 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 03:02 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 03:02 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-26
94474 Matrix:
9/7/2023 7:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 03:02 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 03:02 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 03:02 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 03:02 V37679MSA
2.18 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 03:02 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 03:02 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 03:02 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 03:02 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 03:02 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 03:02 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 03:02 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 03:02 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 03:02 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 03:02 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 03:02 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 03:02 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 03:02 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 03:02 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 03:02 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 03:02 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 03:02 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-26
94474 Matrix:
9/7/2023 7:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 03:02 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 03:02 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 03:02 V37679
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%09/09/23 03:021 MSA V37679
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%09/09/23 03:021 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.4 Limits: 70-130%09/09/23 03:021 MSA V37679
Surrogate: Toluene-d8 98.6 Limits: 70-130%09/09/23 03:021 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-27
94475 Matrix:
9/7/2023 8:17
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 03:26 6200BMSA
410 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 10:31 RSK-175TBL
<76.0 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 13:42 9056AKNC
26300 µg/L 650 2000Sulfate 1 09/08/23 13:42 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-27
94475 Matrix:
9/7/2023 8:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 03:26 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 03:26 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 03:26 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 03:26 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 03:26 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 03:26 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 03:26 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 03:26 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 03:26 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 03:26 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 03:26 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 03:26 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 03:26 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 03:26 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 03:26 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 03:26 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 03:26 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 03:26 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 03:26 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 03:26 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-27
94475 Matrix:
9/7/2023 8:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 03:26 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 03:26 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 03:26 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 03:26 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 03:26 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 03:26 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 03:26 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 03:26 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 03:26 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 03:26 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 03:26 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 03:26 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 03:26 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 03:26 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 03:26 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 03:26 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 03:26 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 03:26 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 03:26 V37679MSA
43.9 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 03:26 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 03:26 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-27
94475 Matrix:
9/7/2023 8:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 03:26 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 03:26 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 03:26 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 03:26 V37679MSA
2.57 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 03:26 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 03:26 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 03:26 V37679MSA
1.85 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 03:26 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 03:26 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 03:26 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 03:26 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 03:26 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 03:26 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 03:26 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 03:26 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 03:26 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 03:26 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 03:26 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 03:26 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 03:26 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 03:26 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-27
94475 Matrix:
9/7/2023 8:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 03:26 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 03:26 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 03:26 V37679
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/09/23 03:261 MSA V37679
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%09/09/23 03:261 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 91.2 Limits: 70-130%09/09/23 03:261 MSA V37679
Surrogate: Toluene-d8 98.2 Limits: 70-130%09/09/23 03:261 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-1
94476 Matrix:
9/7/2023 8:32
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 03:51 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%09/09/23 03:511 MSA V37679
Surrogate: Dibromofluoromethane 96.2 Limits: 70-130%09/09/23 03:511 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%09/09/23 03:511 MSA V37679
Surrogate: Toluene-d8 98.2 Limits: 70-130%09/09/23 03:511 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-1
94476 Matrix:
9/7/2023 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 03:51 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 03:51 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 03:51 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 03:51 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 03:51 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 03:51 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 03:51 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 03:51 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 03:51 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 03:51 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 03:51 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 03:51 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 03:51 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 03:51 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 03:51 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 03:51 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 03:51 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 03:51 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 03:51 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 03:51 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-1
94476 Matrix:
9/7/2023 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 03:51 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 03:51 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 03:51 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 03:51 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 03:51 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 03:51 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 03:51 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 03:51 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 03:51 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 03:51 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 03:51 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 03:51 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 03:51 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 03:51 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 03:51 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 03:51 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 03:51 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 03:51 V37679MSA
1.43 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 03:51 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 03:51 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 03:51 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-1
94476 Matrix:
9/7/2023 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 03:51 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 03:51 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 03:51 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 03:51 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 03:51 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 03:51 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 03:51 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 03:51 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 03:51 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 03:51 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 03:51 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 03:51 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 03:51 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 03:51 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 03:51 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 03:51 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 03:51 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 03:51 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 03:51 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 03:51 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 03:51 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-1
94476 Matrix:
9/7/2023 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 03:51 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 03:51 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 03:51 V37679
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%09/09/23 03:511 MSA V37679
Surrogate: Dibromofluoromethane 96.2 Limits: 70-130%09/09/23 03:511 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%09/09/23 03:511 MSA V37679
Surrogate: Toluene-d8 98.2 Limits: 70-130%09/09/23 03:511 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-21
94477 Matrix:
9/7/2023 8:48
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 04:16 6200BMSA
1140 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
568 µg/L 2.51 10.0Methane 1 09/12/23 12:53 RSK-175TBL
<76.0 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 13:54 9056AKNC
16300 µg/L 650 2000Sulfate 1 09/08/23 13:54 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-21
94477 Matrix:
9/7/2023 8:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 04:16 V37679MSA
4.18 µg/L 0.180 0.500Benzene 1 09/09/23 04:16 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 04:16 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 04:16 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 04:16 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 04:16 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 04:16 V37679MSA
1.04 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 04:16 V37679MSA
1.76 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 04:16 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 04:16 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 04:16 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 04:16 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 04:16 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 04:16 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 04:16 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 04:16 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 04:16 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 04:16 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 04:16 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 04:16 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 04:16 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 04:16 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 04:16 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-21
94477 Matrix:
9/7/2023 8:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 04:16 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 04:16 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 04:16 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 04:16 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 04:16 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 04:16 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 04:16 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 04:16 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 04:16 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 04:16 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 04:16 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 04:16 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 04:16 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 04:16 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 04:16 V37679MSA
32.8 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 04:16 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 04:16 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 04:16 V37679MSA
3.12 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 04:16 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 04:16 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 04:16 V37679MSA
0.611 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 04:16 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 04:16 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-21
94477 Matrix:
9/7/2023 8:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 04:16 V37679MSA
10.2 µg/L 0.470 1.00Naphthalene 1 09/09/23 04:16 V37679MSA
4.96 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 04:16 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 04:16 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 04:16 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 04:16 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 04:16 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 04:16 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 04:16 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 04:16 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 04:16 V37679MSA
0.314 J µg/L 0.220 0.500Toluene 1 09/09/23 04:16 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 04:16 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 04:16 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 04:16 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 04:16 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 04:16 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 04:16 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 04:16 V37679MSA
1.43 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 04:16 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 04:16 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 04:16 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 04:16 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-21
94477 Matrix:
9/7/2023 8:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
1.11 µg/L 0.210 0.500o-Xylene 1 09/09/23 04:16 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 04:16 V37679MSA
1.11 µg/L 0.210 0.500Xylene (Total)1 09/09/23 04:16 V37679
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%09/09/23 04:161 MSA V37679
Surrogate: Dibromofluoromethane 94.8 Limits: 70-130%09/09/23 04:161 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%09/09/23 04:161 MSA V37679
Surrogate: Toluene-d8 97.2 Limits: 70-130%09/09/23 04:161 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 31 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-20
94478 Matrix:
9/7/2023 9:09
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 04:40 6200BMSA
<50.0 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 10:44 RSK-175TBL
10500 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 14:07 9056AKNC
13500 µg/L 650 2000Sulfate 1 09/08/23 14:07 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-20
94478 Matrix:
9/7/2023 9:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 04:40 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 04:40 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 04:40 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 04:40 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 04:40 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 04:40 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 04:40 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 04:40 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 04:40 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 04:40 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 04:40 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 04:40 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 04:40 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 04:40 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 04:40 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 04:40 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 04:40 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 04:40 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 04:40 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 04:40 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-20
94478 Matrix:
9/7/2023 9:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 04:40 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 04:40 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 04:40 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 04:40 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 04:40 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 04:40 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 04:40 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 04:40 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 04:40 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 04:40 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 04:40 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 04:40 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 04:40 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 04:40 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 04:40 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 04:40 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 04:40 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 04:40 V37679MSA
1.27 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 04:40 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 04:40 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 04:40 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-20
94478 Matrix:
9/7/2023 9:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 04:40 V37679MSA
2.84 µg/L 0.470 1.00Naphthalene 1 09/09/23 04:40 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 04:40 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 04:40 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 04:40 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 04:40 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 04:40 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 04:40 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 04:40 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 04:40 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 04:40 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 04:40 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 04:40 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 04:40 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 04:40 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 04:40 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 04:40 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 04:40 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 04:40 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 04:40 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 04:40 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-20
94478 Matrix:
9/7/2023 9:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 04:40 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 04:40 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 04:40 V37679
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%09/09/23 04:401 MSA V37679
Surrogate: Dibromofluoromethane 95.2 Limits: 70-130%09/09/23 04:401 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.4 Limits: 70-130%09/09/23 04:401 MSA V37679
Surrogate: Toluene-d8 98.0 Limits: 70-130%09/09/23 04:401 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 36 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-19
94479 Matrix:
9/7/2023 9:24
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 05:05 6200BMSA
<50.0 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 10:57 RSK-175TBL
3140 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 14:19 9056AKNC
27500 µg/L 650 2000Sulfate 1 09/08/23 14:19 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-19
94479 Matrix:
9/7/2023 9:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 05:05 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 05:05 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 05:05 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 05:05 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 05:05 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 05:05 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 05:05 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 05:05 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 05:05 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 05:05 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 05:05 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 05:05 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 05:05 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 05:05 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 05:05 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 05:05 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 05:05 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 05:05 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 05:05 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 05:05 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 38 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-19
94479 Matrix:
9/7/2023 9:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 05:05 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 05:05 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 05:05 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 05:05 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 05:05 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 05:05 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 05:05 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 05:05 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 05:05 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 05:05 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 05:05 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 05:05 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 05:05 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 05:05 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 05:05 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 05:05 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 05:05 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 05:05 V37679MSA
1.36 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 05:05 V37679MSA
1.03 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 05:05 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 05:05 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 39 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-19
94479 Matrix:
9/7/2023 9:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 05:05 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 05:05 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 05:05 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 05:05 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 05:05 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 05:05 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 05:05 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 05:05 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 05:05 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 05:05 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 05:05 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 05:05 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 05:05 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 05:05 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 05:05 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 05:05 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 05:05 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 05:05 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 05:05 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 05:05 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 05:05 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-19
94479 Matrix:
9/7/2023 9:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 05:05 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 05:05 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 05:05 V37679
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%09/09/23 05:051 MSA V37679
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%09/09/23 05:051 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%09/09/23 05:051 MSA V37679
Surrogate: Toluene-d8 97.4 Limits: 70-130%09/09/23 05:051 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 41 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-18
94480 Matrix:
9/7/2023 9:45
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 05:30 6200BMSA
190 JH µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 11:10 RSK-175TBL
1110 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 14:31 9056AKNC
20500 µg/L 650 2000Sulfate 1 09/08/23 14:31 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-18
94480 Matrix:
9/7/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 05:30 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 05:30 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 05:30 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 05:30 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 05:30 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 05:30 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 05:30 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 05:30 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 05:30 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 05:30 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 05:30 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 05:30 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 05:30 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 05:30 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 05:30 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 05:30 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 05:30 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 05:30 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 05:30 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 05:30 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-18
94480 Matrix:
9/7/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 05:30 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 05:30 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 05:30 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 05:30 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 05:30 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 05:30 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 05:30 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 05:30 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 05:30 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 05:30 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 05:30 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 05:30 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 05:30 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 05:30 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 05:30 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 05:30 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 05:30 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 05:30 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 05:30 V37679MSA
0.216 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 05:30 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 05:30 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 44 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-18
94480 Matrix:
9/7/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 05:30 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 05:30 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 05:30 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 05:30 V37679MSA
1.81 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 05:30 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 05:30 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 05:30 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 05:30 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 05:30 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 05:30 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 05:30 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 05:30 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 05:30 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 05:30 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 05:30 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 05:30 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 05:30 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 05:30 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 05:30 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 05:30 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 05:30 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-18
94480 Matrix:
9/7/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 05:30 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 05:30 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 05:30 V37679
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%09/09/23 05:301 MSA V37679
Surrogate: Dibromofluoromethane 96.2 Limits: 70-130%09/09/23 05:301 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 70-130%09/09/23 05:301 MSA V37679
Surrogate: Toluene-d8 97.0 Limits: 70-130%09/09/23 05:301 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 46 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-24
94481 Matrix:
9/7/2023 10:02
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 05:55 6200BMSA
80.0 JH µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 12:40 RSK-175TBL
<76.0 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 14:44 9056AKNC
23400 µg/L 650 2000Sulfate 1 09/08/23 14:44 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 47 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-24
94481 Matrix:
9/7/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
1.91 J µg/L 1.80 10.0Acetone 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 05:55 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 05:55 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 05:55 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 05:55 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 05:55 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 05:55 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 05:55 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 05:55 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 05:55 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 05:55 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 05:55 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 05:55 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 05:55 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 05:55 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 05:55 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 05:55 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 05:55 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 05:55 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 05:55 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 05:55 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 48 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-24
94481 Matrix:
9/7/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 05:55 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 05:55 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 05:55 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 05:55 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 05:55 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 05:55 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 05:55 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 05:55 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 05:55 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 05:55 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 05:55 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 05:55 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 05:55 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 05:55 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 05:55 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 05:55 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 05:55 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 05:55 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 05:55 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 05:55 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 05:55 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 49 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-24
94481 Matrix:
9/7/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 05:55 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 05:55 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 05:55 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 05:55 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 05:55 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 05:55 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 05:55 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 05:55 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 05:55 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 05:55 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 05:55 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 05:55 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 05:55 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 05:55 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 05:55 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 05:55 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 05:55 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 05:55 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 05:55 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 05:55 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 05:55 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 50 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-24
94481 Matrix:
9/7/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 05:55 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 05:55 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 05:55 V37679
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%09/09/23 05:551 MSA V37679
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%09/09/23 05:551 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 70-130%09/09/23 05:551 MSA V37679
Surrogate: Toluene-d8 97.6 Limits: 70-130%09/09/23 05:551 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 51 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-33
94482 Matrix:
9/7/2023 10:19
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 06:20 6200BMSA
<50.0 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 11:23 RSK-175TBL
2450 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 14:56 9056AKNC
9940 µg/L 650 2000Sulfate 1 09/08/23 14:56 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 52 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-33
94482 Matrix:
9/7/2023 10:19
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 06:20 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 06:20 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 06:20 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 06:20 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 06:20 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 06:20 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 06:20 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 06:20 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 06:20 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 06:20 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 06:20 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 06:20 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 06:20 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 06:20 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 06:20 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 06:20 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 06:20 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 06:20 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 06:20 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 06:20 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 53 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-33
94482 Matrix:
9/7/2023 10:19
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 06:20 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 06:20 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 06:20 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 06:20 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 06:20 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 06:20 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 06:20 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 06:20 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 06:20 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 06:20 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 06:20 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 06:20 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 06:20 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 06:20 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 06:20 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 06:20 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 06:20 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 06:20 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 06:20 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 06:20 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 06:20 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 54 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-33
94482 Matrix:
9/7/2023 10:19
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 06:20 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 06:20 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 06:20 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 06:20 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 06:20 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 06:20 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 06:20 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 06:20 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 06:20 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 06:20 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 06:20 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 06:20 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 06:20 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 06:20 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 06:20 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 06:20 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 06:20 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 06:20 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 06:20 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 06:20 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 06:20 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 55 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-33
94482 Matrix:
9/7/2023 10:19
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 06:20 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 06:20 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 06:20 V37679
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%09/09/23 06:201 MSA V37679
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%09/09/23 06:201 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 70-130%09/09/23 06:201 MSA V37679
Surrogate: Toluene-d8 97.6 Limits: 70-130%09/09/23 06:201 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 56 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-31
94483 Matrix:
9/7/2023 10:36
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 06:45 6200BMSA
<50.0 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 11:36 RSK-175TBL
773 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 15:09 9056AKNC
16100 µg/L 650 2000Sulfate 1 09/08/23 15:09 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 57 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-31
94483 Matrix:
9/7/2023 10:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 06:45 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 06:45 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 06:45 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 06:45 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 06:45 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 06:45 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 06:45 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 06:45 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 06:45 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 06:45 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 06:45 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 06:45 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 06:45 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 06:45 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 06:45 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 06:45 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 06:45 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 06:45 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 06:45 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 06:45 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 58 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-31
94483 Matrix:
9/7/2023 10:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 06:45 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 06:45 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 06:45 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 06:45 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 06:45 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 06:45 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 06:45 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 06:45 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 06:45 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 06:45 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 06:45 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 06:45 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 06:45 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 06:45 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 06:45 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 06:45 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 06:45 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 06:45 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 06:45 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 06:45 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 06:45 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 59 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-31
94483 Matrix:
9/7/2023 10:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 06:45 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 06:45 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 06:45 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 06:45 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 06:45 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 06:45 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 06:45 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 06:45 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 06:45 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 06:45 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 06:45 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 06:45 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 06:45 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 06:45 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 06:45 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 06:45 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 06:45 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 06:45 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 06:45 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 06:45 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 06:45 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 60 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-31
94483 Matrix:
9/7/2023 10:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 06:45 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 06:45 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 06:45 V37679
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%09/09/23 06:451 MSA V37679
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%09/09/23 06:451 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 94.4 Limits: 70-130%09/09/23 06:451 MSA V37679
Surrogate: Toluene-d8 96.4 Limits: 70-130%09/09/23 06:451 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 61 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-9
94484 Matrix:
9/7/2023 10:53
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 07:09 6200BMSA
230 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 11:49 RSK-175TBL
92.0 J µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 15:21 9056AKNC
11300 µg/L 650 2000Sulfate 1 09/08/23 15:21 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 62 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-9
94484 Matrix:
9/7/2023 10:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 07:09 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 07:09 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 07:09 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 07:09 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 07:09 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 07:09 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 07:09 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 07:09 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 07:09 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 07:09 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 07:09 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 07:09 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 07:09 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 07:09 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 07:09 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 07:09 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 07:09 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 07:09 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 07:09 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 07:09 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 63 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-9
94484 Matrix:
9/7/2023 10:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 07:09 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 07:09 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 07:09 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 07:09 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 07:09 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 07:09 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 07:09 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 07:09 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 07:09 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 07:09 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 07:09 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 07:09 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 07:09 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 07:09 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 07:09 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 07:09 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 07:09 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 07:09 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 07:09 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 07:09 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 07:09 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 64 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-9
94484 Matrix:
9/7/2023 10:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 07:09 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 07:09 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 07:09 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 07:09 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 07:09 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 07:09 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 07:09 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 07:09 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 07:09 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 07:09 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 07:09 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 07:09 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 07:09 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 07:09 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 07:09 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 07:09 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 07:09 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 07:09 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 07:09 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 07:09 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 07:09 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 65 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:DMW-9
94484 Matrix:
9/7/2023 10:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 07:09 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 07:09 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 07:09 V37679
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%09/09/23 07:091 MSA V37679
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%09/09/23 07:091 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%09/09/23 07:091 MSA V37679
Surrogate: Toluene-d8 95.4 Limits: 70-130%09/09/23 07:091 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 66 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-7
94485 Matrix:
9/7/2023 11:14
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 07:34 6200BMSA
<50.0 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
5.92 J µg/L 2.51 10.0Methane 1 09/12/23 12:02 RSK-175TBL
4820 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 15:58 9056AKNC
15100 µg/L 650 2000Sulfate 1 09/08/23 15:58 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 67 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-7
94485 Matrix:
9/7/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 07:34 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 07:34 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 07:34 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 07:34 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 07:34 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 07:34 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 07:34 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 07:34 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 07:34 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 07:34 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 07:34 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 07:34 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 07:34 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 07:34 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 07:34 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 07:34 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 07:34 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 07:34 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 07:34 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 07:34 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 68 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-7
94485 Matrix:
9/7/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 07:34 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 07:34 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 07:34 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 07:34 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 07:34 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 07:34 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 07:34 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 07:34 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 07:34 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 07:34 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 07:34 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 07:34 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 07:34 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 07:34 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 07:34 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 07:34 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 07:34 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 07:34 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 07:34 V37679MSA
0.253 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 07:34 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 07:34 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 69 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-7
94485 Matrix:
9/7/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 07:34 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 07:34 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 07:34 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 07:34 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 07:34 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 07:34 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 07:34 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 07:34 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 07:34 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 07:34 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 07:34 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 07:34 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 07:34 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 07:34 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 07:34 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 07:34 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 07:34 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 07:34 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 07:34 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 07:34 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 07:34 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 70 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-7
94485 Matrix:
9/7/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 07:34 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 07:34 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 07:34 V37679
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%09/09/23 07:341 MSA V37679
Surrogate: Dibromofluoromethane 95.2 Limits: 70-130%09/09/23 07:341 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%09/09/23 07:341 MSA V37679
Surrogate: Toluene-d8 96.8 Limits: 70-130%09/09/23 07:341 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 71 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-15
94486 Matrix:
9/7/2023 11:29
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 07:59 6200BMSA
<50.0 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
<2.51 µg/L 2.51 10.0Methane 1 09/12/23 12:14 RSK-175TBL
3770 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 16:10 9056AKNC
48400 µg/L 650 2000Sulfate 1 09/08/23 16:10 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 72 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-15
94486 Matrix:
9/7/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
1.97 J µg/L 1.80 10.0Acetone 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 07:59 V37679MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 07:59 V37679MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 07:59 V37679MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 07:59 V37679MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 07:59 V37679MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 07:59 V37679MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 07:59 V37679MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 07:59 V37679MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 07:59 V37679MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 07:59 V37679MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 07:59 V37679MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 07:59 V37679MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 07:59 V37679MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 07:59 V37679MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 07:59 V37679MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 07:59 V37679MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 07:59 V37679MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 07:59 V37679MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 07:59 V37679MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 07:59 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 73 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-15
94486 Matrix:
9/7/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 07:59 V37679MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 07:59 V37679MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 07:59 V37679MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 07:59 V37679MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 07:59 V37679MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 07:59 V37679MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 07:59 V37679MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 07:59 V37679MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 07:59 V37679MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 07:59 V37679MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 07:59 V37679MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 07:59 V37679MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 07:59 V37679MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 07:59 V37679MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 07:59 V37679MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 07:59 V37679MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 07:59 V37679MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 07:59 V37679MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 07:59 V37679MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 07:59 V37679MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 07:59 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 74 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-15
94486 Matrix:
9/7/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 07:59 V37679MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/09/23 07:59 V37679MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 07:59 V37679MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 07:59 V37679MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 07:59 V37679MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 07:59 V37679MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 07:59 V37679MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 07:59 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 07:59 V37679MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 07:59 V37679MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 07:59 V37679MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 07:59 V37679MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 07:59 V37679MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 07:59 V37679MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 07:59 V37679MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 07:59 V37679MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 07:59 V37679MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 07:59 V37679MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 07:59 V37679MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 07:59 V37679MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 07:59 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 75 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-15
94486 Matrix:
9/7/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 07:59 V37679MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 07:59 V37679MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 07:59 V37679
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%09/09/23 07:591 MSA V37679
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%09/09/23 07:591 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 70-130%09/09/23 07:591 MSA V37679
Surrogate: Toluene-d8 96.2 Limits: 70-130%09/09/23 07:591 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 76 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-12
94487 Matrix:
9/7/2023 11:47
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 09/09/23 10:28 6200BMSA
5530 H µg/L 250 1000Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
2250 µg/L 25.1 100Methane 10 09/12/23 14:49 RSK-175TBL
<76.0 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 16:23 9056AKNC
766 J µg/L 650 2000Sulfate 1 09/08/23 16:23 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 77 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-12
94487 Matrix:
9/7/2023 11:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<180 µg/L 180 1000Acetone 100 09/09/23 10:28 V37679MSA
30.8 J µg/L 18.0 50.0Benzene 100 09/09/23 10:28 V37679MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/09/23 10:28 V37679MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/09/23 10:28 V37679MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/09/23 10:28 V37679MSA
<150 µg/L 150 500Bromoform 100 09/09/23 10:28 V37679MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/09/23 10:28 V37679MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 09/09/23 10:28 V37679MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/09/23 10:28 V37679MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/09/23 10:28 V37679MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/09/23 10:28 V37679MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/09/23 10:28 V37679MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/09/23 10:28 V37679MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/09/23 10:28 V37679MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/09/23 10:28 V37679MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 09/09/23 10:28 V37679MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/09/23 10:28 V37679MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/09/23 10:28 V37679MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/09/23 10:28 V37679MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/09/23 10:28 V37679MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 09/09/23 10:28 V37679MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/09/23 10:28 V37679MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/09/23 10:28 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 78 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-12
94487 Matrix:
9/7/2023 11:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/09/23 10:28 V37679MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/09/23 10:28 V37679MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 09/09/23 10:28 V37679MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/09/23 10:28 V37679MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/09/23 10:28 V37679MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/09/23 10:28 V37679MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/09/23 10:28 V37679MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/09/23 10:28 V37679MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/09/23 10:28 V37679MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/09/23 10:28 V37679MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/09/23 10:28 V37679MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/09/23 10:28 V37679MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/09/23 10:28 V37679MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/09/23 10:28 V37679MSA
<4200 µg/L 4200 20000Ethanol 100 09/09/23 10:28 V37679MSA
1380 µg/L 17.0 50.0Ethylbenzene 100 09/09/23 10:28 V37679MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/09/23 10:28 V37679MSA
<38.0 µg/L 38.0 1002-Hexanone 100 09/09/23 10:28 V37679MSA
42.6 J µg/L 18.0 50.0Isopropylbenzene 100 09/09/23 10:28 V37679MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/09/23 10:28 V37679MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/09/23 10:28 V37679MSA
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/09/23 10:28 V37679MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/09/23 10:28 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 79 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-12
94487 Matrix:
9/7/2023 11:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<33.0 µg/L 33.0 200Methylene Chloride 100 09/09/23 10:28 V37679MSA
434 µg/L 47.0 100Naphthalene 100 09/09/23 10:28 V37679MSA
92.8 µg/L 19.0 50.0n-Propylbenzene 100 09/09/23 10:28 V37679MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/09/23 10:28 V37679MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 09/09/23 10:28 V37679MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 09/09/23 10:28 V37679MSA
<190 µg/L 190 1000tert-Amyl Alcohol (TAA)100 09/09/23 10:28 V37679MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 09/09/23 10:28 V37679MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/09/23 10:28 V37679MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/09/23 10:28 V37679MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/09/23 10:28 V37679MSA
7290 µg/L 22.0 50.0Toluene 100 09/09/23 10:28 V37679MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/09/23 10:28 V37679MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/09/23 10:28 V37679MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/09/23 10:28 V37679MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/09/23 10:28 V37679MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/09/23 10:28 V37679MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/09/23 10:28 V37679MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/09/23 10:28 V37679MSA
814 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/09/23 10:28 V37679MSA
212 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/09/23 10:28 V37679MSA
<100 µg/L 100 500Vinyl Acetate 100 09/09/23 10:28 V37679MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 09/09/23 10:28 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 80 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-12
94487 Matrix:
9/7/2023 11:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
1560 µg/L 21.0 50.0o-Xylene 100 09/09/23 10:28 V37679MSA
3830 µg/L 42.0 100m,p-Xylene 100 09/09/23 10:28 V37679MSA
5390 µg/L 21.0 50.0Xylene (Total)100 09/09/23 10:28 V37679
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%09/09/23 10:28100 MSA V37679
Surrogate: Dibromofluoromethane 94.8 Limits: 70-130%09/09/23 10:28100 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 90.2 Limits: 70-130%09/09/23 10:28100 MSA V37679
Surrogate: Toluene-d8 98.0 Limits: 70-130%09/09/23 10:28100 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 81 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-11R
94488 Matrix:
9/7/2023 12:02
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 09/09/23 08:49 6200BMSA
2350 H µg/L 50.0 200Ferrous Iron 1 09/08/23 12:00 SM-3500-FE-BJMD
1400 µg/L 2.51 10.0Methane 1 09/12/23 13:06 RSK-175TBL
<76.0 µg/L 76.0 200Nitrate (NO3-N)1 09/08/23 16:35 9056AKNC
24900 µg/L 650 2000Sulfate 1 09/08/23 16:35 9056AKNC
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 82 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-11R
94488 Matrix:
9/7/2023 12:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<18.0 µg/L 18.0 100Acetone 10 09/09/23 08:49 V37679MSA
6.15 µg/L 1.80 5.00Benzene 10 09/09/23 08:49 V37679MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 09/09/23 08:49 V37679MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 09/09/23 08:49 V37679MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 09/09/23 08:49 V37679MSA
<15.0 µg/L 15.0 50.0Bromoform 10 09/09/23 08:49 V37679MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 09/09/23 08:49 V37679MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 09/09/23 08:49 V37679MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 09/09/23 08:49 V37679MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 09/09/23 08:49 V37679MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 09/09/23 08:49 V37679MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 09/09/23 08:49 V37679MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 09/09/23 08:49 V37679MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 09/09/23 08:49 V37679MSA
<2.20 µg/L 2.20 5.00Chloroform 10 09/09/23 08:49 V37679MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 09/09/23 08:49 V37679MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 09/09/23 08:49 V37679MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 09/09/23 08:49 V37679MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 09/09/23 08:49 V37679MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 09/09/23 08:49 V37679MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 09/09/23 08:49 V37679MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 09/09/23 08:49 V37679MSA
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 09/09/23 08:49 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 83 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-11R
94488 Matrix:
9/7/2023 12:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 09/09/23 08:49 V37679MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 09/09/23 08:49 V37679MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 09/09/23 08:49 V37679MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 09/09/23 08:49 V37679MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 09/09/23 08:49 V37679MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 09/09/23 08:49 V37679MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 09/09/23 08:49 V37679MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 09/09/23 08:49 V37679MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 09/09/23 08:49 V37679MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 09/09/23 08:49 V37679MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 09/09/23 08:49 V37679MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 09/09/23 08:49 V37679MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 09/09/23 08:49 V37679MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 09/09/23 08:49 V37679MSA
<420 µg/L 420 2000Ethanol 10 09/09/23 08:49 V37679MSA
104 µg/L 1.70 5.00Ethylbenzene 10 09/09/23 08:49 V37679MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 09/09/23 08:49 V37679MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 09/09/23 08:49 V37679MSA
5.90 µg/L 1.80 5.00Isopropylbenzene 10 09/09/23 08:49 V37679MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 09/09/23 08:49 V37679MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 09/09/23 08:49 V37679MSA
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/09/23 08:49 V37679MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 09/09/23 08:49 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 84 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-11R
94488 Matrix:
9/7/2023 12:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
<3.30 µg/L 3.30 20.0Methylene Chloride 10 09/09/23 08:49 V37679MSA
24.2 µg/L 4.70 10.0Naphthalene 10 09/09/23 08:49 V37679MSA
15.1 µg/L 1.90 5.00n-Propylbenzene 10 09/09/23 08:49 V37679MSA
<2.20 µg/L 2.20 5.00Styrene 10 09/09/23 08:49 V37679MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 09/09/23 08:49 V37679MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 09/09/23 08:49 V37679MSA
<19.0 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 09/09/23 08:49 V37679MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 09/09/23 08:49 V37679MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 09/09/23 08:49 V37679MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 09/09/23 08:49 V37679MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 09/09/23 08:49 V37679MSA
27.2 µg/L 2.20 5.00Toluene 10 09/09/23 08:49 V37679MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 09/09/23 08:49 V37679MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 09/09/23 08:49 V37679MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 09/09/23 08:49 V37679MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 09/09/23 08:49 V37679MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 09/09/23 08:49 V37679MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 09/09/23 08:49 V37679MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 09/09/23 08:49 V37679MSA
68.4 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 09/09/23 08:49 V37679MSA
2.77 J µg/L 1.80 5.001,3,5-Trimethylbenzene 10 09/09/23 08:49 V37679MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 09/09/23 08:49 V37679MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 09/09/23 08:49 V37679MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 85 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:MW-11R
94488 Matrix:
9/7/2023 12:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37678 09/08/23 14:00
15.4 µg/L 2.10 5.00o-Xylene 10 09/09/23 08:49 V37679MSA
21.8 µg/L 4.20 10.0m,p-Xylene 10 09/09/23 08:49 V37679MSA
37.2 µg/L 2.10 5.00Xylene (Total)10 09/09/23 08:49 V37679
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%09/09/23 08:4910 MSA V37679
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%09/09/23 08:4910 MSA V37679
Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 70-130%09/09/23 08:4910 MSA V37679
Surrogate: Toluene-d8 97.4 Limits: 70-130%09/09/23 08:4910 MSA V37679
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 86 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-3
94489 Matrix:
9/7/2023 12:10
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 06:52 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%09/09/23 06:521 MSA V37674
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/09/23 06:521 MSA V37674
Surrogate: 1,2-Dichloroethane - d4 87.2 Limits: 70-130%09/09/23 06:521 MSA V37674
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/09/23 06:521 MSA V37674
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 87 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-3
94489 Matrix:
9/7/2023 12:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 06:52 V37674MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 06:52 V37674MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 06:52 V37674MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 06:52 V37674MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 06:52 V37674MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 06:52 V37674MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 06:52 V37674MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 06:52 V37674MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 06:52 V37674MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 06:52 V37674MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 06:52 V37674MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 06:52 V37674MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 06:52 V37674MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 06:52 V37674MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 06:52 V37674MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 06:52 V37674MSA
<1.10 M µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 06:52 V37674MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 06:52 V37674MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 06:52 V37674MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 06:52 V37674MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 88 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-3
94489 Matrix:
9/7/2023 12:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 06:52 V37674MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 06:52 V37674MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 06:52 V37674MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 06:52 V37674MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 06:52 V37674MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 06:52 V37674MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 06:52 V37674MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 06:52 V37674MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 06:52 V37674MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 06:52 V37674MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 06:52 V37674MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 06:52 V37674MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 06:52 V37674MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 06:52 V37674MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 06:52 V37674MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 06:52 V37674MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 06:52 V37674MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 06:52 V37674MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 06:52 V37674MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 06:52 V37674MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 06:52 V37674MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 89 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-3
94489 Matrix:
9/7/2023 12:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 06:52 V37674MSA
<0.470 M µg/L 0.470 1.00Naphthalene 1 09/09/23 06:52 V37674MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 06:52 V37674MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 06:52 V37674MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 06:52 V37674MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 06:52 V37674MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 06:52 V37674MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 06:52 V37674MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 06:52 V37674MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 06:52 V37674MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 06:52 V37674MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 06:52 V37674MSA
<0.380 M µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 06:52 V37674MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 06:52 V37674MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 06:52 V37674MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 06:52 V37674MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 06:52 V37674MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 06:52 V37674MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 06:52 V37674MSA
<1.00 M µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 06:52 V37674MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 06:52 V37674MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 90 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-3
94489 Matrix:
9/7/2023 12:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 06:52 V37674MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 06:52 V37674MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 06:52 V37674
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%09/09/23 06:521 MSA V37674
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/09/23 06:521 MSA V37674
Surrogate: 1,2-Dichloroethane - d4 87.2 Limits: 70-130%09/09/23 06:521 MSA V37674
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/09/23 06:521 MSA V37674
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 91 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-4
94490 Matrix:
9/7/2023 12:17
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/09/23 07:18 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%09/09/23 07:181 MSA V37674
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/09/23 07:181 MSA V37674
Surrogate: 1,2-Dichloroethane - d4 88.2 Limits: 70-130%09/09/23 07:181 MSA V37674
Surrogate: Toluene-d8 99.0 Limits: 70-130%09/09/23 07:181 MSA V37674
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 92 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-4
94490 Matrix:
9/7/2023 12:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/09/23 07:18 V37674MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/09/23 07:18 V37674MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/09/23 07:18 V37674MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/09/23 07:18 V37674MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/09/23 07:18 V37674MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/09/23 07:18 V37674MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/09/23 07:18 V37674MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/09/23 07:18 V37674MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/09/23 07:18 V37674MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/09/23 07:18 V37674MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/09/23 07:18 V37674MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/09/23 07:18 V37674MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/09/23 07:18 V37674MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/09/23 07:18 V37674MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/09/23 07:18 V37674MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/09/23 07:18 V37674MSA
<1.10 M µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/09/23 07:18 V37674MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/09/23 07:18 V37674MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/09/23 07:18 V37674MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/09/23 07:18 V37674MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 93 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-4
94490 Matrix:
9/7/2023 12:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/09/23 07:18 V37674MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/09/23 07:18 V37674MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/09/23 07:18 V37674MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/09/23 07:18 V37674MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/09/23 07:18 V37674MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/09/23 07:18 V37674MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/09/23 07:18 V37674MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/09/23 07:18 V37674MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/09/23 07:18 V37674MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/09/23 07:18 V37674MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/09/23 07:18 V37674MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/09/23 07:18 V37674MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/09/23 07:18 V37674MSA
<42.0 µg/L 42.0 200Ethanol 1 09/09/23 07:18 V37674MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/09/23 07:18 V37674MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/09/23 07:18 V37674MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/09/23 07:18 V37674MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/09/23 07:18 V37674MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/09/23 07:18 V37674MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/09/23 07:18 V37674MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/09/23 07:18 V37674MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 94 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-4
94490 Matrix:
9/7/2023 12:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/09/23 07:18 V37674MSA
<0.470 M µg/L 0.470 1.00Naphthalene 1 09/09/23 07:18 V37674MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/09/23 07:18 V37674MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/09/23 07:18 V37674MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/09/23 07:18 V37674MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/09/23 07:18 V37674MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/09/23 07:18 V37674MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/09/23 07:18 V37674MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/09/23 07:18 V37674MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/09/23 07:18 V37674MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/09/23 07:18 V37674MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/09/23 07:18 V37674MSA
<0.380 M µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/09/23 07:18 V37674MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/09/23 07:18 V37674MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/09/23 07:18 V37674MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/09/23 07:18 V37674MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/09/23 07:18 V37674MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/09/23 07:18 V37674MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/09/23 07:18 V37674MSA
<1.00 M µg/L 1.00 5.00Vinyl Acetate 1 09/09/23 07:18 V37674MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/09/23 07:18 V37674MSA
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 95 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-251-0004
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2215 Received : 09/08/2023
YaYa #2
Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:SW-4
94490 Matrix:
9/7/2023 12:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37673 09/08/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/09/23 07:18 V37674MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/09/23 07:18 V37674MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/09/23 07:18 V37674
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%09/09/23 07:181 MSA V37674
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/09/23 07:181 MSA V37674
Surrogate: 1,2-Dichloroethane - d4 88.2 Limits: 70-130%09/09/23 07:181 MSA V37674
Surrogate: Toluene-d8 99.0 Limits: 70-130%09/09/23 07:181 MSA V37674
Qualifiers/
Definitions
Beyond holding timeHDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 96 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37673
Associated Lab Samples: 94489, 94490
LRB-V37673 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 06:2610.01.80<1.80µg/LAcetone
09/09/23 06:260.5000.180<0.180µg/LBenzene
09/09/23 06:260.5000.210<0.210µg/LBromobenzene
09/09/23 06:261.000.420<0.420µg/LBromochloromethane
09/09/23 06:260.5000.160<0.160µg/LBromodichloromethane
09/09/23 06:265.001.50<1.50µg/LBromoform
09/09/23 06:261.000.280<0.280µg/LBromomethane
09/09/23 06:260.5000.180<0.180µg/Ln-Butylbenzene
09/09/23 06:260.5000.200<0.200µg/Lsec-Butyl benzene
09/09/23 06:262.000.920<0.920µg/Ltert-Butyl benzene
09/09/23 06:260.5000.180<0.180µg/LCarbon Tetrachloride
09/09/23 06:260.5000.190<0.190µg/LChlorobenzene
09/09/23 06:260.5000.190<0.190µg/LChlorodibromomethane
09/09/23 06:261.000.430<0.430µg/LChloroethane
09/09/23 06:260.5000.220<0.220µg/LChloroform
09/09/23 06:260.5000.220<0.220µg/LChloromethane
09/09/23 06:260.5000.200<0.200µg/L2-Chlorotoluene
09/09/23 06:260.5000.200<0.200µg/L4-Chlorotoluene
09/09/23 06:260.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/09/23 06:262.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/09/23 06:260.5000.200<0.200µg/L1,2-Dibromoethane
09/09/23 06:260.5000.230<0.230µg/LDibromomethane
09/09/23 06:260.5000.220<0.220µg/L1,2-Dichlorobenzene
09/09/23 06:260.5000.190<0.190µg/L1,3-Dichlorobenzene
09/09/23 06:260.5000.210<0.210µg/L1,4-Dichlorobenzene
09/09/23 06:265.001.20<1.20µg/LDichlorodifluoromethane
09/09/23 06:260.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 15Date:09/13/2023 02:47 PM
Page 97 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37673
Associated Lab Samples: 94489, 94490
LRB-V37673 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 06:260.5000.150<0.150µg/L1,2-Dichloroethane
09/09/23 06:260.5000.150<0.150µg/L1,1-Dichloroethene
09/09/23 06:260.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/09/23 06:260.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/09/23 06:260.5000.190<0.190µg/L1,2-Dichloropropane
09/09/23 06:260.5000.130<0.130µg/L1,3-Dichloropropane
09/09/23 06:262.000.210<0.210µg/L2,2-Dichloropropane
09/09/23 06:260.5000.200<0.200µg/L1,1-Dichloropropene
09/09/23 06:260.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/09/23 06:260.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/09/23 06:2620042.0<42.0µg/LEthanol
09/09/23 06:260.5000.170<0.170µg/LEthylbenzene
09/09/23 06:263.000.350<0.350µg/LHexachlorobutadiene
09/09/23 06:261.000.380<0.380µg/L2-Hexanone
09/09/23 06:260.5000.180<0.180µg/LIsopropylbenzene
09/09/23 06:260.5000.089<0.089µg/L4-Isopropyl toluene
09/09/23 06:265.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/09/23 06:261.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/09/23 06:261.000.078<0.078µg/L4-Methyl-2-Pentanone
09/09/23 06:262.000.330<0.330µg/LMethylene Chloride
09/09/23 06:261.000.470<0.470µg/LNaphthalene
09/09/23 06:260.5000.190<0.190µg/Ln-Propylbenzene
09/09/23 06:260.5000.220<0.220µg/LStyrene
09/09/23 06:2610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/09/23 06:2610.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/09/23 06:2610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/09/23 06:2610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 15Date:09/13/2023 02:47 PM
Page 98 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37673
Associated Lab Samples: 94489, 94490
LRB-V37673 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 06:260.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/09/23 06:260.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/09/23 06:260.5000.220<0.220µg/LTetrachloroethene
09/09/23 06:260.5000.220<0.220µg/LToluene
09/09/23 06:260.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/09/23 06:260.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/09/23 06:260.5000.160<0.160µg/L1,1,1-Trichloroethane
09/09/23 06:260.5000.096<0.096µg/L1,1,2-Trichloroethane
09/09/23 06:260.5000.180<0.180µg/LTrichloroethene
09/09/23 06:260.5000.180<0.180µg/LTrichlorofluoromethane
09/09/23 06:260.5000.270<0.270µg/L1,2,3-Trichloropropane
09/09/23 06:260.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/09/23 06:260.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/09/23 06:265.001.00<1.00µg/LVinyl Acetate
09/09/23 06:260.5000.170<0.170µg/LVinyl Chloride
09/09/23 06:260.5000.210<0.210µg/Lo-Xylene
09/09/23 06:261.000.420<0.420µg/Lm,p-Xylene
09/09/23 06:2610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/09/23 06:264-Bromofluorobenzene (S)102 70-130
09/09/23 06:26Dibromofluoromethane (S)103 70-130
09/09/23 06:261,2-Dichloroethane - d4 (S)88.0 70-130
09/09/23 06:26Toluene-d8 (S)99.4 70-130
Page 3 of 15Date:09/13/2023 02:47 PM
Page 99 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37673
LCS-V37673 LCSD-V37673Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
26.3 65.766.226.540.0µg/LAcetone 40-160 0.7 20.0
20.7 10410420.820.0µg/LBenzene 70-130 0.4 20.0
19.8 99.097.519.520.0µg/LBromobenzene 70-130 1.5 20.0
21.0 10510520.920.0µg/LBromochloromethane 70-130 0.4 20.0
19.1 95.595.519.120.0µg/LBromodichloromethane 70-130 0.0 20.0
15.4 77.077.015.420.0µg/LBromoform 70-130 0.0 20.0
23.6 11811523.020.0µg/LBromomethane 60-140 2.5 20.0
20.9 10510520.920.0µg/Ln-Butylbenzene 70-130 0.0 20.0
20.9 10510120.220.0µg/Lsec-Butyl benzene 70-130 3.4 20.0
20.3 10210020.020.0µg/Ltert-Butyl benzene 70-130 1.4 20.0
21.0 10510721.320.0µg/LCarbon Tetrachloride 70-130 1.4 20.0
20.4 10210220.320.0µg/LChlorobenzene 70-130 0.4 20.0
18.6 93.094.018.820.0µg/LChlorodibromomethane 70-130 1.0 20.0
17.7 88.591.018.220.0µg/LChloroethane 60-140 2.7 20.0
21.4 10710420.720.0µg/LChloroform 70-130 3.3 20.0
17.8 89.088.017.620.0µg/LChloromethane 60-140 1.1 20.0
20.1 10199.019.820.0µg/L2-Chlorotoluene 70-130 1.5 20.0
19.7 98.597.019.420.0µg/L4-Chlorotoluene 70-130 1.5 20.0
19.6 98.096.519.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.5 20.0
13.8 69.0*78.515.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 12.8 20.0
17.6 88.091.518.320.0µg/L1,2-Dibromoethane 70-130 3.8 20.0
18.2 91.086.017.220.0µg/LDibromomethane 70-130 5.6 20.0
18.8 94.092.518.520.0µg/L1,2-Dichlorobenzene 70-130 1.6 20.0
20.2 10199.519.920.0µg/L1,3-Dichlorobenzene 70-130 1.4 20.0
19.4 97.095.519.120.0µg/L1,4-Dichlorobenzene 70-130 1.5 20.0
16.5 82.580.516.120.0µg/LDichlorodifluoromethane 60-140 2.4 20.0
Page 4 of 15* QC Fail Date:09/13/2023 02:47 PM
Page 100 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37673
LCS-V37673 LCSD-V37673Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.3 10710621.220.0µg/L1,1-Dichloroethane 70-130 0.4 20.0
16.9 84.584.516.920.0µg/L1,2-Dichloroethane 70-130 0.0 20.0
20.0 10095.519.120.0µg/L1,1-Dichloroethene 70-130 4.6 20.0
20.6 10310320.620.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
20.4 10299.019.820.0µg/Ltrans-1,2-Dichloroethene 70-130 2.9 20.0
19.9 99.510220.320.0µg/L1,2-Dichloropropane 70-130 1.9 20.0
18.0 90.092.018.420.0µg/L1,3-Dichloropropane 70-130 2.1 20.0
17.9 89.589.017.820.0µg/L2,2-Dichloropropane 70-130 0.5 20.0
22.4 11211322.620.0µg/L1,1-Dichloropropene 70-130 0.8 20.0
18.3 91.593.518.720.0µg/Lcis-1,3-Dichloropropene 70-130 2.1 20.0
18.1 90.588.517.720.0µg/Ltrans-1,3-Dichloropropene 70-130 2.2 20.0
383 76.679.4397500µg/LEthanol 60-140 3.5 20.0
18.6 93.095.519.120.0µg/LEthylbenzene 70-130 2.6 20.0
18.1 90.590.018.020.0µg/LHexachlorobutadiene 70-130 0.5 20.0
15.2 76.074.514.920.0µg/L2-Hexanone 60-140 1.9 20.0
21.0 10510420.820.0µg/LIsopropylbenzene 70-130 0.9 20.0
21.0 10510420.720.0µg/L4-Isopropyl toluene 70-130 1.4 20.0
16.9 84.582.016.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.0 20.0
18.5 92.590.018.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.7 20.0
15.1 75.569.513.920.0µg/L4-Methyl-2-Pentanone 60-140 8.2 20.0
20.7 10499.019.820.0µg/LMethylene Chloride 70-130 4.4 20.0
13.6 68.0*71.014.220.0µg/LNaphthalene 70-130 4.3 20.0
20.4 10210120.220.0µg/Ln-Propylbenzene 70-130 0.9 20.0
19.9 99.510320.620.0µg/LStyrene 70-130 3.4 20.0
39.3 98.299.239.740.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.0 20.0
26.4 66.063.725.540.0µg/Ltert-Butyl formate (TBF)40-140 3.4 20.0
Page 5 of 15* QC Fail Date:09/13/2023 02:47 PM
Page 101 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37674QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37673
LCS-V37673 LCSD-V37673Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
15.3 76.561.012.220.0µg/Ltert-Amyl Alcohol (TAA)40-140 22.5*20.0
37.6 94.092.737.140.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.3 20.0
19.9 99.510220.420.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.4 20.0
16.5 82.583.016.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.6 20.0
19.5 97.598.019.620.0µg/LTetrachloroethene 70-130 0.5 20.0
20.0 10097.519.520.0µg/LToluene 70-130 2.5 20.0
13.7 68.5*68.5*13.720.0µg/L1,2,3-Trichlorobenzene 70-130 0.0 20.0
15.1 75.579.515.920.0µg/L1,2,4-Trichlorobenzene 70-130 5.1 20.0
20.6 10310521.020.0µg/L1,1,1-Trichloroethane 70-130 1.9 20.0
18.8 94.091.518.320.0µg/L1,1,2-Trichloroethane 70-130 2.6 20.0
21.2 10610921.820.0µg/LTrichloroethene 70-130 2.7 20.0
18.7 93.594.518.920.0µg/LTrichlorofluoromethane 60-140 1.0 20.0
18.0 90.084.016.820.0µg/L1,2,3-Trichloropropane 70-130 6.8 20.0
21.0 10510320.520.0µg/L1,2,4-Trimethylbenzene 70-130 2.4 20.0
20.4 10210120.220.0µg/L1,3,5-Trimethylbenzene 70-130 0.9 20.0
11.7 58.5*58.5*11.720.0µg/LVinyl Acetate 60-140 0.0 20.0
19.6 98.099.519.920.0µg/LVinyl Chloride 60-140 1.5 20.0
19.5 97.597.519.520.0µg/Lo-Xylene 70-130 0.0 20.0
39.8 99.510240.840.0µg/Lm,p-Xylene 70-130 2.4 20.0
18.9 94.580.516.120.0µg/L3,3-Dimethyl-1-butanol 70-130 16.0 20.0
96.895.64-Bromofluorobenzene (S)70-130
101102Dibromofluoromethane (S)70-130
89.888.61,2-Dichloroethane - d4 (S)70-130
98.8101Toluene-d8 (S)70-130
Page 6 of 15* QC Fail Date:09/13/2023 02:47 PM
Page 102 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37678
Associated Lab Samples: 94473, 94474, 94475, 94476, 94477, 94478, 94479, 94480, 94481, 94482, 94483, 94484, 94485, 94486, 94487,
94488
LRB-V37678 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 01:4710.01.80<1.80µg/LAcetone
09/09/23 01:470.5000.180<0.180µg/LBenzene
09/09/23 01:470.5000.210<0.210µg/LBromobenzene
09/09/23 01:471.000.420<0.420µg/LBromochloromethane
09/09/23 01:470.5000.160<0.160µg/LBromodichloromethane
09/09/23 01:475.001.50<1.50µg/LBromoform
09/09/23 01:471.000.280<0.280µg/LBromomethane
09/09/23 01:470.5000.180<0.180µg/Ln-Butylbenzene
09/09/23 01:470.5000.200<0.200µg/Lsec-Butyl benzene
09/09/23 01:472.000.920<0.920µg/Ltert-Butyl benzene
09/09/23 01:470.5000.180<0.180µg/LCarbon Tetrachloride
09/09/23 01:470.5000.190<0.190µg/LChlorobenzene
09/09/23 01:470.5000.190<0.190µg/LChlorodibromomethane
09/09/23 01:471.000.430<0.430µg/LChloroethane
09/09/23 01:470.5000.220<0.220µg/LChloroform
09/09/23 01:470.5000.220<0.220µg/LChloromethane
09/09/23 01:470.5000.200<0.200µg/L2-Chlorotoluene
09/09/23 01:470.5000.200<0.200µg/L4-Chlorotoluene
09/09/23 01:470.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/09/23 01:472.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/09/23 01:470.5000.200<0.200µg/L1,2-Dibromoethane
09/09/23 01:470.5000.230<0.230µg/LDibromomethane
09/09/23 01:470.5000.220<0.220µg/L1,2-Dichlorobenzene
09/09/23 01:470.5000.190<0.190µg/L1,3-Dichlorobenzene
09/09/23 01:470.5000.210<0.210µg/L1,4-Dichlorobenzene
09/09/23 01:475.001.20<1.20µg/LDichlorodifluoromethane
09/09/23 01:470.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 15Date:09/13/2023 02:47 PM
Page 103 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37678
Associated Lab Samples: 94473, 94474, 94475, 94476, 94477, 94478, 94479, 94480, 94481, 94482, 94483, 94484, 94485, 94486, 94487,
94488
LRB-V37678 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 01:470.5000.150<0.150µg/L1,2-Dichloroethane
09/09/23 01:470.5000.150<0.150µg/L1,1-Dichloroethene
09/09/23 01:470.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/09/23 01:470.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/09/23 01:470.5000.190<0.190µg/L1,2-Dichloropropane
09/09/23 01:470.5000.130<0.130µg/L1,3-Dichloropropane
09/09/23 01:472.000.210<0.210µg/L2,2-Dichloropropane
09/09/23 01:470.5000.200<0.200µg/L1,1-Dichloropropene
09/09/23 01:470.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/09/23 01:470.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/09/23 01:4720042.0<42.0µg/LEthanol
09/09/23 01:470.5000.170<0.170µg/LEthylbenzene
09/09/23 01:473.000.350<0.350µg/LHexachlorobutadiene
09/09/23 01:471.000.380<0.380µg/L2-Hexanone
09/09/23 01:470.5000.180<0.180µg/LIsopropylbenzene
09/09/23 01:470.5000.089<0.089µg/L4-Isopropyl toluene
09/09/23 01:475.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/09/23 01:471.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/09/23 01:471.000.078<0.078µg/L4-Methyl-2-Pentanone
09/09/23 01:472.000.330<0.330µg/LMethylene Chloride
09/09/23 01:471.000.470<0.470µg/LNaphthalene
09/09/23 01:470.5000.190<0.190µg/Ln-Propylbenzene
09/09/23 01:470.5000.220<0.220µg/LStyrene
09/09/23 01:4710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/09/23 01:4710.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/09/23 01:4710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/09/23 01:4710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 15Date:09/13/2023 02:47 PM
Page 104 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37678
Associated Lab Samples: 94473, 94474, 94475, 94476, 94477, 94478, 94479, 94480, 94481, 94482, 94483, 94484, 94485, 94486, 94487,
94488
LRB-V37678 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 01:470.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/09/23 01:470.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/09/23 01:470.5000.220<0.220µg/LTetrachloroethene
09/09/23 01:470.5000.220<0.220µg/LToluene
09/09/23 01:470.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/09/23 01:470.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/09/23 01:470.5000.160<0.160µg/L1,1,1-Trichloroethane
09/09/23 01:470.5000.096<0.096µg/L1,1,2-Trichloroethane
09/09/23 01:470.5000.180<0.180µg/LTrichloroethene
09/09/23 01:470.5000.180<0.180µg/LTrichlorofluoromethane
09/09/23 01:470.5000.270<0.270µg/L1,2,3-Trichloropropane
09/09/23 01:470.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/09/23 01:470.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/09/23 01:475.001.00<1.00µg/LVinyl Acetate
09/09/23 01:470.5000.170<0.170µg/LVinyl Chloride
09/09/23 01:470.5000.210<0.210µg/Lo-Xylene
09/09/23 01:471.000.420<0.420µg/Lm,p-Xylene
09/09/23 01:4710.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/09/23 01:474-Bromofluorobenzene (S)98.2 70-130
09/09/23 01:47Dibromofluoromethane (S)95.2 70-130
09/09/23 01:471,2-Dichloroethane - d4 (S)91.8 70-130
09/09/23 01:47Toluene-d8 (S)97.2 70-130
Page 9 of 15Date:09/13/2023 02:47 PM
Page 105 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37678
LCS-V37678 LCSD-V37678Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
27.0 67.572.028.840.0µg/LAcetone 40-160 6.4 20.0
22.5 11311623.120.0µg/LBenzene 70-130 2.6 20.0
20.6 10310821.520.0µg/LBromobenzene 70-130 4.2 20.0
21.3 10711021.920.0µg/LBromochloromethane 70-130 2.7 20.0
20.8 10410721.420.0µg/LBromodichloromethane 70-130 2.8 20.0
19.0 95.010020.020.0µg/LBromoform 70-130 5.1 20.0
21.2 10610621.120.0µg/LBromomethane 60-140 0.4 20.0
21.3 10710821.620.0µg/Ln-Butylbenzene 70-130 1.3 20.0
20.6 10310621.220.0µg/Lsec-Butyl benzene 70-130 2.8 20.0
20.4 10210621.120.0µg/Ltert-Butyl benzene 70-130 3.3 20.0
21.8 10911422.720.0µg/LCarbon Tetrachloride 70-130 4.0 20.0
21.5 10811022.020.0µg/LChlorobenzene 70-130 2.2 20.0
20.4 10210521.020.0µg/LChlorodibromomethane 70-130 2.8 20.0
24.1 12112825.620.0µg/LChloroethane 60-140 6.0 20.0
21.3 10710921.720.0µg/LChloroform 70-130 1.8 20.0
21.5 10810420.720.0µg/LChloromethane 60-140 3.7 20.0
20.7 10410821.520.0µg/L2-Chlorotoluene 70-130 3.7 20.0
21.3 10710921.820.0µg/L4-Chlorotoluene 70-130 2.3 20.0
21.2 10610921.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.7 20.0
21.0 10510621.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.4 20.0
21.6 10811122.220.0µg/L1,2-Dibromoethane 70-130 2.7 20.0
20.6 10311122.120.0µg/LDibromomethane 70-130 7.0 20.0
21.2 10610821.620.0µg/L1,2-Dichlorobenzene 70-130 1.8 20.0
20.9 10510721.320.0µg/L1,3-Dichlorobenzene 70-130 1.8 20.0
20.6 10310721.420.0µg/L1,4-Dichlorobenzene 70-130 3.8 20.0
23.8 11912224.320.0µg/LDichlorodifluoromethane 60-140 2.0 20.0
Page 10 of 15Date:09/13/2023 02:47 PM
Page 106 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37678
LCS-V37678 LCSD-V37678Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.9 11011322.520.0µg/L1,1-Dichloroethane 70-130 2.7 20.0
20.1 10110520.920.0µg/L1,2-Dichloroethane 70-130 3.9 20.0
23.0 11512124.120.0µg/L1,1-Dichloroethene 70-130 4.6 20.0
22.1 11111522.920.0µg/Lcis-1,2-Dichloroethene 70-130 3.5 20.0
22.4 11211623.220.0µg/Ltrans-1,2-Dichloroethene 70-130 3.5 20.0
22.0 11011322.620.0µg/L1,2-Dichloropropane 70-130 2.6 20.0
20.8 10411021.920.0µg/L1,3-Dichloropropane 70-130 5.1 20.0
19.9 99.510020.020.0µg/L2,2-Dichloropropane 70-130 0.5 20.0
23.5 11812024.020.0µg/L1,1-Dichloropropene 70-130 2.1 20.0
21.1 10611122.220.0µg/Lcis-1,3-Dichloropropene 70-130 5.0 20.0
20.9 10510921.820.0µg/Ltrans-1,3-Dichloropropene 70-130 4.2 20.0
434 86.889.2446500µg/LEthanol 60-140 2.7 20.0
21.2 10611021.920.0µg/LEthylbenzene 70-130 3.2 20.0
20.2 10110621.120.0µg/LHexachlorobutadiene 70-130 4.3 20.0
18.0 90.094.018.820.0µg/L2-Hexanone 60-140 4.3 20.0
21.4 10711022.020.0µg/LIsopropylbenzene 70-130 2.7 20.0
21.0 10510821.620.0µg/L4-Isopropyl toluene 70-130 2.8 20.0
17.8 89.096.019.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 7.5 20.0
21.3 10711222.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 4.5 20.0
20.2 10110521.020.0µg/L4-Methyl-2-Pentanone 60-140 3.8 20.0
21.9 11011322.520.0µg/LMethylene Chloride 70-130 2.7 20.0
22.5 11311322.520.0µg/LNaphthalene 70-130 0.0 20.0
21.1 10611021.920.0µg/Ln-Propylbenzene 70-130 3.7 20.0
21.4 10711222.320.0µg/LStyrene 70-130 4.1 20.0
34.3 85.792.236.940.0µg/Ltert-Butyl Alcohol (TBA)40-140 7.3 20.0
37.4 93.510140.540.0µg/Ltert-Butyl formate (TBF)40-140 7.9 20.0
Page 11 of 15Date:09/13/2023 02:47 PM
Page 107 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37678
LCS-V37678 LCSD-V37678Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.3 10292.018.420.0µg/Ltert-Amyl Alcohol (TAA)40-140 9.8 20.0
44.2 11111445.640.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 3.1 20.0
21.4 10711021.920.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.3 20.0
19.3 96.510520.920.0µg/L1,1,2,2-Tetrachloroethane 70-130 7.9 20.0
21.1 10611122.220.0µg/LTetrachloroethene 70-130 5.0 20.0
22.2 11111623.220.0µg/LToluene 70-130 4.4 20.0
25.7 12912725.420.0µg/L1,2,3-Trichlorobenzene 70-130 1.1 20.0
22.5 11311522.920.0µg/L1,2,4-Trichlorobenzene 70-130 1.7 20.0
21.4 10711022.020.0µg/L1,1,1-Trichloroethane 70-130 2.7 20.0
21.8 10911422.820.0µg/L1,1,2-Trichloroethane 70-130 4.4 20.0
22.8 11411623.220.0µg/LTrichloroethene 70-130 1.7 20.0
21.9 11011522.920.0µg/LTrichlorofluoromethane 60-140 4.4 20.0
19.5 97.510621.120.0µg/L1,2,3-Trichloropropane 70-130 7.8 20.0
21.2 10610921.720.0µg/L1,2,4-Trimethylbenzene 70-130 2.3 20.0
21.0 10510821.620.0µg/L1,3,5-Trimethylbenzene 70-130 2.8 20.0
17.1 85.595.519.120.0µg/LVinyl Acetate 60-140 11.0 20.0
24.6 12312725.420.0µg/LVinyl Chloride 60-140 3.2 20.0
20.9 10510921.720.0µg/Lo-Xylene 70-130 3.7 20.0
45.3 11311847.040.0µg/Lm,p-Xylene 70-130 3.6 20.0
16.6 83.088.017.620.0µg/L3,3-Dimethyl-1-butanol 70-130 5.8 20.0
97.297.44-Bromofluorobenzene (S)70-130
95.896.4Dibromofluoromethane (S)70-130
94.093.81,2-Dichloroethane - d4 (S)70-130
97.698.0Toluene-d8 (S)70-130
Page 12 of 15Date:09/13/2023 02:47 PM
Page 108 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
Anions by Ion Chromatography
9056A
V37750QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-9056A (PREP)
QC Prep:V37749
Associated Lab Samples: 94474, 94475, 94477, 94478, 94479, 94480, 94481, 94482, 94483, 94484, 94485, 94486, 94487, 94488
LRB-V37749 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/08/23 13:0520076.0<76.0µg/LNitrate (NO3-N)
09/08/23 13:052000650<650µg/LSulfate
LCS-V37749Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10341104000µg/LNitrate (NO3-N)80-120
1114420040000µg/LSulfate 80-120
V 94487-MS-V37749 V 94487-MSD-V37749Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
4110 103409040004000<79.0µg/LNitrate (NO3-N)102 80-120 0.4 15
44400 109441004000040000766µg/LSulfate 108 80-120 0.6 15
V 94488-MS-V37749 V 94488-MSD-V37749Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
3990 100395040004000<76.0µg/LNitrate (NO3-N)99.0 80-120 1.0 15
68100 10867600400004000024900µg/LSulfate 107 80-120 0.7 15
Page 13 of 15Date:09/13/2023 02:47 PM
Page 109 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
QC Prep Batch Method:
RSK-175
RSK-175
V37713QC Analytical Batch(es):
Analysis Method:
Analysis Description:
RSK-175 (Prep)
QC Prep:V37712
Associated Lab Samples: 94474, 94475, 94477, 94478, 94479, 94480, 94481, 94482, 94483, 94484, 94485, 94486, 94487, 94488
LRB-V37712 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/12/23 10:0510.02.51<2.51µg/LMethane
LCS-V37712Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
114178156µg/LMethane 85-115
V 94474-DUP-V37712Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/12/23 13:450.0<10.0< 10.0µg/LMethane
Page 14 of 15Date:09/13/2023 02:47 PM
Page 110 of 114
Quality Control Data
23-251-0004Report No:
Project Description:
Client ID:Geological Resources, Inc.
YaYa #2
Ferrous Iron
SM-3500-FE-B
V37628QC Analytical Batch:
Analysis Method:
Analysis Description:
Associated Lab Samples: 94474, 94475, 94477, 94478, 94479, 94480, 94481, 94482, 94483, 94484, 94485, 94486, 94487, 94488
LRB Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/08/23 12:0020050.0<50.0µg/LFerrous Iron
LCSLaboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10420802000µg/LFerrous Iron 90-110
V 94478-MS V 94478-MSDMatrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2020 101197020002000<50.0µg/LFerrous Iron 99.0 80-120 2.5 20
Page 15 of 15Date:09/13/2023 02:47 PM
Page 111 of 114
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-251-0004
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 0.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:09/08/2023 10:25:54
Special precautions or instructions included?
Comments:
Page 112 of 114
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APPENDIX C
Contaminant Mass Calculations
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-7
MW-11R
MW-12MW-16
MW-22
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red. To Date Red.
MW-11R 581.00 2200.00 300.00 1180.00 182.00 221.00 4664.00 8.48
MW-12 3140.00 11900.00 840.00 3620.00 1370.00 880.00 21750.00 8.47
Average 1860.50 7050.00 570.00 2400.00 776.00 550.50 13207.00 8.48
MW-11R 31.70 343.00 78.10 306.00 0.00 22.20 781.00 7.35
MW-12 1870.00 8960.00 1020.00 4700.00 0.00 349.00 16899.00 7.37
Average 950.85 4651.50 549.05 2503.00 0.00 185.60 8840.00 7.36
MW-11R 90.90 477.00 167.00 553.00 0.00 124.00 1411.90 7.54
MW-12 1410.00 6450.00 1040.00 4240.00 102.00 317.00 13559.00 7.55
Average 750.45 3463.50 603.50 2396.50 51.00 220.50 7485.45 7.55
MW-11R 5000.00 260000.00 80000.00 50000.00 20000.00 6000.00 421000.00 10.15
MW-12 5000.00 260000.00 80000.00 50000.00 20000.00 6000.00 421000.00 11.85
Average 5000.00 260000.00 80000.00 50000.00 20000.00 6000.00 421000.00 11.00
MW-11R 37.80 75.90 50.70 173.00 8.80 18.50 364.70 10.40
MW-12 5000.00 260000.00 80000.00 50000.00 20000.00 6000.00 421000.00 10.46
Average 2518.90 130037.95 40025.35 25086.50 10004.40 3009.25 210682.35 10.43
MW-11R 769.00 9190.00 1180.00 5200.00 32.00 256.00 16627.00 9.35
MW-12 809.00 11600.00 1260.00 6180.00 30.30 324.00 20203.30 9.30
Average 789.00 10395.00 1220.00 5690.00 31.15 290.00 18415.15 9.33
MW-11R 3.00 19.10 13.00 88.10 0.36 6.20 129.76 3.82
MW-12 195.00 1610.00 432.00 1890.00 11.50 113.00 4251.50 3.84
Average 99.00 814.55 222.50 989.05 5.93 59.60 2190.63 3.83
MW-11R 16.60 299.00 147.00 654.00 0.00 85.10 1201.70 9.73
MW-12 617.00 5210.00 780.00 3770.00 23.70 171.00 10571.70 9.66
Average 316.80 2754.50 463.50 2212.00 11.85 128.05 5886.70 9.70
MW-11R 14.20 16.30 19.40 114.00 0.83 14.70 179.43 2.43
MW-12 157.00 3750.00 682.00 3430.00 6.70 206.00 8231.70 2.43
Average 85.60 1883.15 350.70 1772.00 3.77 110.35 4205.57 2.43
MW-11R 2.20 49.90 24.30 99.10 0.47 10.40 186.37 4.33
MW-12 210.00 4750.00 723.00 3330.00 0.00 197.00 9210.00 4.38
Average 106.10 2399.95 373.65 1714.55 0.24 103.70 4698.19 4.36
MW-11R 21.20 223.00 41.10 235.00 0.39 40.40 561.09 4.06
MW-12 99.30 6080.00 849.00 4620.00 0.00 314.00 11962.30 4.15
Average 60.25 3151.50 445.05 2427.50 0.20 177.20 6261.70 4.11
MW-11R 67.90 1720.00 440.00 1720.00 0.00 112.00 4059.90 4.00
MW-12 76.50 3250.00 587.00 2730.00 7.10 172.00 6822.60 4.00
Average 72.20 2485.00 513.50 2225.00 3.55 142.00 5441.25 4.00
MW-11R 3.3 21.2 98.9 132 0.00 38.8 294.20 2.62
MW-12 61.6 4,300 746 3,450 0.00 163 8720.60 2.66
Average 32.45 2160.60 422.45 1791.00 0.00 100.90 4507.40 2.64
MW-11R 26.20 272 144.00 369.00 0.00 42.60 853.80 6.72
MW-12 63.10 5330.00 1,020.00 3,850.00 0.00 268.00 10531.10 6.70
Average 44.65 2801.00 582.00 2109.50 0.00 155.30 5692.45 6.71
MW-11R 12.7 547 232 506 0.828 55.3 1353.83 7.02
MW-12 25.6 2317 758 3404.7 2.03 270 6777.33 7.17
Average 19.15 1432.00 495.00 1955.35 1.43 162.65 4065.58 7.10
MW-11R 6.15 27.2 104 37.2 0.000 24.2 198.75 7.19
MW-12 30.8 7290 1380 5390.0 0.00 434 14524.80 7.23
Average 18.48 3658.60 742.00 2713.60 0.00 229.10 7361.78 7.21
Date
Average Water
Column Height
(ft.)02/13/08 3.5301/06/10 4.6401/28/11 4.4610/18/11 1.0008/02/12 1.5702/19/13 2.68
01/20/13 8.17
09/11/14 2.31
03/10/15 9.57
12/15/15 7.65
06/08/16 7.90
12/06/16 8.0002/27/20 9.3609/15/20 5.2903/22/23 4.91
09/06/23 4.79
Notes:
• FP: Free Product• Area of the contaminant plume is calculated from Figure 6 • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
4,532.58 -1162.5%
501.22 … …
252,648 0.15 37,897
02/13/08
01/28/11
APPENDIX C
PERCENTAGE CALCULATIONS
YA YA # 2 (INCIDENT NO. 29195)
Baseline Event
1 2,534.71 12 8.48 3.52 8,922
359.03 18.7% 28.4%
01/06/10 4.64 441.60 11.9% 11.9%
501.22 --- ---441.60 11.9% 12%
Total Contaminant Mass
(g)
Percent Reduction Compared
to Previous Event Percent Reduction To Date
06/08/16
12/06/16
02/27/20
09/15/20
03/22/23
7.90 532.24 -37.6% -6.2%
8.00
3561.16 21.4%-611%
530.35 85.1%-6%
359.03 18.7% 28%4532.58 -1162.5% -804%
11.9% 6%
433.31 -196.6%14%
386.70 10.8% 23%
192.69 63.7% 62%
146.09 24.2% 71%
530.35 85.1% -5.8%
192.69
214.70 33.8% 57%
10/18/11
08/02/12
02/19/13
01/20/14
09/11/14
03/10/15
12/15/15
454.22 3.1% 9%
324.20 28.6% 35%
532.24 -37.6% -6%
468.65
433.31 -196.6%13.5%
7.65 386.70 10.8% 22.8%
3.53
4.46
1.00
8.17
9.57
63.7% 61.6%
2.31 146.09 24.2% 70.9%
-804.3%
1.57 3,561.16 21.4%-610.5%
2.68
09/06/23 4.79 379.65 -76.8%24.3%
Area 1
379.65 -76.8%24%
4.91 214.70 33.8% 57.2%
9.36 454.22 3.1% 9.4%
5.29 324.20 28.6% 35.3%
468.65 11.9% 6.5%
Page 1 of 1

APPENDIX D
Mann-Kendall Analyses
Groundwater Statistics Tool
UCL calculations and summary statistics for data sets that are normally distributed
Site Name Ya Ya #2
Operating Unit (OU)0
Type of Evaluation Remediation
Date of Evaluation 9/26/2023
Person performing analysis Eric Eubanks
Chemical of Concern Benzene
Well Name/Number MW-12
Date Units Date
Concentration Units µg/l
Confidence Level 95%
Number of results 11
Number < cleanup level 0
Are any potential outliers present?No
Mean of concentration 105
Standard deviation of concentration 76.4
t-value for UCL calculation 1.812
95% Upper Confidence Limit (UCL)
Method for calculating UCL
Value of 95% Upper Confidence Band
value at final sampling event
Trend calculation method
Cleanup level
Source of cleanup level
Is the trend decreasing or statistically
insignificant?
56.4
Yes
Ordinary Least Squares
When is the
concentration
predicted to exceed
the MCL?
Not applicable - slope is not
statistically increasing
147
Student's t UCL
1
MACs
Message: None.
0
50
100
150
200
250
1/20/2014 4/6/2017 6/21/2020 9/6/2023
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
l
)
Date
Trend Line
Detected Data Ordinary Least Squares
Cleanup Level Upper Confidence Band
Groundwater Statistics Tool
UCL calculations and summary statistics for data sets that are normally distributed
Site Name Ya Ya #2
Operating Unit (OU)0
Type of Evaluation Remediation
Date of Evaluation 9/26/2023
Person performing analysis Eric Eubanks
Chemical of Concern Toluene
Well Name/Number MW-12
Date Units Date
Concentration Units µg/l
Confidence Level 95%
Number of results 13
Number < cleanup level 0
Are any potential outliers present?No
Mean of concentration 4730
Standard deviation of concentration 2610
t-value for UCL calculation 1.782
95% Upper Confidence Limit (UCL)
Method for calculating UCL
Value of 95% Upper Confidence Band
value at final sampling event
Trend calculation method
Cleanup level
Source of cleanup level
Is the trend decreasing or statistically
insignificant?
7410
Yes
Ordinary Least Squares
When is the
concentration
predicted to exceed
the MCL?
Not applicable - slope is not
statistically increasing
6020
Student's t UCL
600
MACs
Message: None.
0
2000
4000
6000
8000
10000
12000
14000
2/22/2013 8/28/2016 3/3/2020 9/7/2023
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
l
)
Date
Trend Line
Detected Data Ordinary Least Squares
Cleanup Level Upper Confidence Band
Groundwater Statistics Tool
UCL calculations and summary statistics for data sets that are normally distributed
Site Name Ya Ya #2
Operating Unit (OU)0
Type of Evaluation Remediation
Date of Evaluation 9/26/2023
Person performing analysis Eric Eubanks
Chemical of Concern Ethylbenzene
Well Name/Number MW-12
Date Units Date
Concentration Units µg/l
Confidence Level 95%
Number of results 13
Number < cleanup level 1
Are any potential outliers present?No
Mean of concentration 817
Standard deviation of concentration 261
t-value for UCL calculation 1.782
95% Upper Confidence Limit (UCL)
Method for calculating UCL
Value of 95% Upper Confidence Band
value at final sampling event
Trend calculation method
Cleanup level
Source of cleanup level
Is the trend decreasing or statistically
insignificant?
1300
Yes
Ordinary Least Squares
When is the
concentration
predicted to exceed
the MCL?
Not applicable - slope is not
statistically increasing
946
Student's t UCL
500
MACs
Message: None.
0
200
400
600
800
1000
1200
1400
1600
2/22/2013 8/28/2016 3/3/2020 9/7/2023
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
l
)
Date
Trend Line
Detected Data Ordinary Least Squares
Cleanup Level Upper Confidence Band
Groundwater Statistics Tool
UCL calculations and summary statistics for data sets that are normally distributed
Site Name Ya Ya #2
Operating Unit (OU)0
Type of Evaluation Remediation
Date of Evaluation 9/26/2023
Person performing analysis Eric Eubanks
Chemical of Concern Xylenes
Well Name/Number MW-12
Date Units Date
Concentration Units µg/l
Confidence Level 95%
Number of results 13
Number < cleanup level 0
Are any potential outliers present?No
Mean of concentration 3690
Standard deviation of concentration 1140
t-value for UCL calculation 1.782
95% Upper Confidence Limit (UCL)
Method for calculating UCL
Value of 95% Upper Confidence Band
value at final sampling event
Trend calculation method
Cleanup level
Source of cleanup level
Is the trend decreasing or statistically
insignificant?
5340
Yes
Ordinary Least Squares
When is the
concentration
predicted to exceed
the MCL?
Not applicable - slope is not
statistically increasing
4250
Student's t UCL
500
MACs
Message: None.
0
1000
2000
3000
4000
5000
6000
7000
2/22/2013 8/28/2016 3/3/2020 9/7/2023
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
l
)
Date
Trend Line
Detected Data Ordinary Least Squares
Cleanup Level Upper Confidence Band
Groundwater Statistics Tool
UCL calculations and summary statistics for data sets that are normally distributed
Site Name Ya Ya #2
Operating Unit (OU)0
Type of Evaluation Remediation
Date of Evaluation 9/26/2023
Person performing analysis Eric Eubanks
Chemical of Concern Total BTEX
Well Name/Number MW-12
Date Units Date
Concentration Units µg/l
Confidence Level 95%
Number of results 13
Number < cleanup level 0
Are any potential outliers present?No
Mean of concentration 9440
Standard deviation of concentration 4090
t-value for UCL calculation 1.782
95% Upper Confidence Limit (UCL)
Method for calculating UCL
Value of 95% Upper Confidence Band
value at final sampling event
Trend calculation method
Cleanup level
Source of cleanup level
Is the trend decreasing or statistically
insignificant?
14100
Yes
Ordinary Least Squares
When is the
concentration
predicted to exceed
the MCL?
Not applicable - slope is not
statistically increasing
11500
Student's t UCL
1701
MACs
Message: None.
0
5000
10000
15000
20000
25000
2/22/2013 8/28/2016 3/3/2020 9/7/2023
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
l
)
Date
Trend Line
Detected Data Ordinary Least Squares
Cleanup Level Upper Confidence Band