AS-3693_28826_CA_MRP_20220421_ALL

MARCH 2022 - GROUNDWATER
MONITORING REPORT with
AFVR

For The
THE SPOT
2267 Smokey Park Highway Candler, North Carolina 28715

UST Incident # 28826

April 21, 2022
Singleton Environmental, Inc. Project No. SEI-1226

Singleton Environmental, Inc
Groundwater Monitoring Report with AFVR The Spot - Candler Candler, North Carolina

GROUNDWATER MONITORING REPORT with AFVR
April 21, 2022 Incident Number: 28826 Facility ID Number: 00-0-00004683 Site Name: The Spot 2267 Smokey Park Highway
Candler, NC 28705
Incident Number: 28826 Facility ID Number: 0-004683 UST Owner / Operator: Theodossis Business, LLC
Contact: Jimmy Theodossis 1100 McMinn Road Hendersonville, NC 28792 Telephone: [phone]
Consultant / Contractor: Singleton Environmental, Inc. PO Box 2012 Enka, NC 28728 Telephone: [phone]
Date Release Discovered: March 15, 2010 Estimated Quantity of Release: Unknown/unquantified Cause/Source of Release: Two 3,000-Gallon Gasoline USTs, One 6,000-Gallon
Gasoline UST, and One 3,000-Gallon Diesel UST.
Latitude: (35° 32’ 33.14” North)
Longitude: (82° 44’ 45.11” West) Signature and Seal of Certifying Professional Engineer: I, Christopher D. Singleton, a North Carolina Professional Geologist, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
____________________________________ Christopher D. Singleton, P.G. #1928
Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The
certification number of the company is C-443.
Groundwater Monitoring Report with AFVR The Spot - Candler Candler, North Carolina

Table of Contents
Introduction ................................................................................................................................1 Site History and Source Characterization…......................…………......................................... .....1
Summary of USTs …......................………….........................................................................1 Source of Release…......................…………...........................................................................1 Summary of Assessment Activities and Corrective Actions……......................................... ...1 Receptor Information…......................…………......................................... ..................................2
Site Geology and Hydrogeology…......................…………......................................... ..................2
AFVR Activities…......................…………...................................................................................2 Groundwater Sampling Activities…......................…………......................................... ................3 Free Product Removal …......................…………......................................... ................................4 Conclusions and Recommendations…..................…………......................................... ................4 Tables Table 1. Groundwater Levels Table 2. Groundwater Analytical Results
Table 3. AFVR Report Figures Figure 1. Site Vicinity Map
Figure 2. Site Map Figure 3. Groundwater Elevation Contour Map Figure 4. Groundwater Sampling Locations with MCLs and GCLs Appendices

Appendix A: Disposal Manifest Appendix B: Laboratory Analytical Report

Introduction

This report presents the results of the Groundwater Monitoring and AFVR event completed in March 2022 to evaluate the remedial progress of the groundwater contamination related to a petroleum release from the former underground storage tank (UST) system at The Spot, located at 2267 Smokey Park Hwy in Candler, North Carolina. Figure 1 shows the site location, and
Figure 2 presents a site map showing the location of the current UST system, monitoring wells, and soil sampling locations. Site History and Source Characterization
The following table summarizes information about the USTs at the site:

Tank No. Volume (gallons)
Contents (i.e., gasoline, diesel, kerosene, heating oil, waste oil, etc.)
Use (resale, heating building, distribution, farm or residential, etc.)
Date last used
Indicate whether UST has been removed or closed in place
Date of permanent closure (if applicable)
Was a release detected from this UST system? If yes, give date.
1 6,000 Gasoline Resale 3/15/10 Removed 3/15/10 Yes
2 3,000 Gasoline Resale 3/15/10 Removed 3/15/10 Yes
3 3,000 Gasoline Resale 3/15/10 Removed 3/15/10 Yes
4 3,000 Diesel Resale 3/15/10 Removed 3/15/10 Yes

Ownership of Tank: Theodossis Business, LLC Contact: Jimmy Theodossis 2267 Smokey Park Highway Candler, NC 28705
Telephone: [phone]
Source of Release
The source of the release is the former UST system removed in March 2010. The UST system
was used as a petroleum retail station. There are no other on-site or off-site petroleum or non-petroleum sources that are suspected to be contributing to the release. A new UST system was installed in April 2010. Summary of Assessment Activities and Corrective Actions
The petroleum release at the Site was confirmed during UST Closure activities in March 2010, LSA activities in February 2013 and CSA activities in October 2016. To date, eight groundwater monitoring wells (MW-1 through MW-8) have been installed at the
Site. Dissolved phase petroleum compounds above the State 2L standards have been detected in

monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-5. To date no free product has been
observed at the site. Receptor Information Singleton Environmental, Inc. personnel completed a water supply well survey near the site in February 2013 by searching surrounding properties for wells and water meter connections and interviewing local residents. 22 water supply wells were located within 1,000 feet of the site.
The following bullets summarize other receptor information regarding this site:
• Public water supply is not available near the site.

• The site is not located in a wellhead protection area.
• 22 water supply wells are located within 1,000 feet from the source area. The property containing the release is zoned commercial. The surrounding properties contain commercial and residential development. Site Geology and Hydrogeology

According to the Geologic Map of North Carolina (1985), the local geology consists of Muscovite Biotite Schist. A soil boring log is included in Appendix B. On March 30, 2022, the average depth to groundwater was 21.26 ft-bls. Groundwater flows south from the source area.
AFVR Activities
On March 7, 2022, SEI conducted an aggressive fluid and vapor recovery (AFVR) event at the
site. Fluids and vapors were extracted from monitoring well MW-1. The event began at 8:00 a.m. and ended at 4:00 p.m. Stinger depths were initially set at 25 feet below land surface (ft-bls) and lowered to 30 ft-bls two hours into the event.
A photoionization detector (PID) was used to measure effluent vapors from the system. Vacuum
pressure was measured 38.0 inches of Hg throughout the event.
SEI measured stack velocity using an averaging Pitot tube installed across the two-inch liquid-ring pump vapor discharge stack to determine flow in actual cubic feet per minute (ACFM). Progress employed the following equation to convert ACFM to standard cubic feet per minute
(SCFM):
SCFM=ACFM(TSTP / TActual)( PActual /PSTP)
• TSTP - Standard temperature (68oF = 528oR)
• TActual - Actual temperature (stack conditions (0F) +460oR)
• PActual - Actual pressure (stack conditions - observed gauge value in inches of water)

• PSTP - Standard pressure (29.92 inches of Hg = 646 inches of water)
The average liquid ring pump (LRP) stack temperature measured for each recovery location was
incorporated into the above equation to yield a correction factor applied to the data to calculate a
mass removal in vapor-phase. A summary AFVR report including average stack temperature, average vacuum applied, airflow effluent data, and estimated total emissions (in pounds) for the extraction location are presented in Table 3.
The fluids extracted from the wells were pumped into an on-site tanker truck. During the event SEI was able to evacuate approximately 171 gallons of contaminated groundwater. Based on total emission calculations performed by SEI the event removed approximately 78.18 pounds (or 10.27 gallons) of petroleum product as vapor from beneath the site. Just under two gallons of
product (1.6 gallons) were measured in the tank of the vacuum truck bringing the total gallons
recovered to 11.87 gallons (90.33 pounds).
The recovered fluids were transported off-site by Mountain Environmental Services for proper disposal. The disposal manifest is in Appendix A. Groundwater Sampling Activities
SEI was on site on March 30, 2022, to collect post-AFVR groundwater samples from the monitoring wells and water supply wells. Monitoring wells MW-1 through MW-8, and WSW-1 and WSW-2 were sampled as part of the sampling event. Prior to sampling, the monitoring wells were purged of three volumes of water and allowed to recharge prior to sampling. And the water supply wells were purged for approximately 20 minutes.
The groundwater samples were collected into laboratory-supplied bottles and placed into a cooler packed with ice. The cooler was delivered under chain-of-custody to Pace Analytical in Asheville, North Carolina for testing. Pace analyzed the groundwater samples for VOCs by
Standard Method 6200B. A summary of the groundwater sample analytical results are included
in Table 2.
• Laboratory analysis of the groundwater sample collected from monitoring wells WSW-1, WSW-2, MW-5, MW-6, and MW-7 did not detect any compounds above the laboratory
minimum detection limits.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-1 detected benzene, 1,2,4-trimethylbenzene, diisopropylether, ethylbenzene, MTBE,
naphthalene, toluene, n-propylbenzene, and total xylenes at concentrations exceeding
their respective NCAC 2L MCLS. The concentrations of benzene detected in the groundwater sample collected from monitoring well MW-1 exceeded the Gross Contamination Levels (GCLs).

• Laboratory analysis of the groundwater sample collected from monitoring well MW-2 detected benzene, 1,2-dichloroethane, and MTBE at concentrations their respective
NCAC 2L MCLs. None of the compounds exceeded the NCAC 2L GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-3 detected MTBE at concentrations exceeding the NCAC 2L MCLs. None of the
compounds exceeded the NCAC 2L GCLs.

• Laboratory analysis of the groundwater sample collected from monitoring well MW-4 detected 1,2,4-trimethylbenzene, EDB, 1,2-dichloroethane, benzene, diisopropylether, MTBE, methylene chloride, naphthalene, toluene, and total xylenes at concentrations
exceeding the NCAC 2L MCLs. None of the compounds exceeded the NCAC 2L GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-8 detected benzene and naphthalene at concentrations exceeding their respective NCAC 2L
MCLS. None of the compounds exceeded the NCAC 2L GCLs.
The laboratory analytical reports for the groundwater samples are provided in Appendix B. The laboratory test results are summarized on Table 2. A map depicting the contaminant plume is included on Figure 4.
Free Product Removal
Free product was not observed in the monitoring wells during this groundwater assessment,
however, approximately 1.6 gallons of product was observed in the vacuum truck tank after the event. CONCLUSIONS
Based on the results of the groundwater sampling event, SEI makes the following conclusions:
• Laboratory analysis of the groundwater sample collected from monitoring wells WSW-1, WSW-2, MW-5, MW-6, and MW-7 did not detect targeted compounds above their
respective NCAC 2L MCLS.
• Laboratory analysis of the groundwater samples collected from monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-8 detected targeted compounds above their respective NCAC 2L MCLS, and MW-1 still contains concentrations of benzene exceeded the
NCAC 2L GCLs.
• The contaminant plume has spread to monitoring well MW-8. Based on the remaining concentrations in select groundwater samples exceeding their respective NCAC 2L MCLS and GCLs, SEI recommends the following:

• SEI recommends groundwater monitoring in July 2022 to confirm the migration of the contaminant plume.

TABLES
MW Number Top of Casing Elevation
Top of Casing
to GW Depth Groundwater Elevation
MW-1 97.67 21.81 75.86
MW-2 96.31 21.27 75.04
MW-3 94.42 19.83 74.59
MW-4 94.77 19.92 74.85
MW-5 97.02 20.70 76.32
MW-6 98.85 22.48 76.37
MW-7 100 21.34 78.66
MW-8 92.98 22.73 70.25
Table 1
Groundwater Flow Mapping Elevation Details
Candler, NC
The Spot 3/30/22
1,2,4-
Trimeth
ylbenze
ne
EDB
1,2-Dichlor
oethan
e
1,3,5-
Trimeth
ylbenze
ne
Benzene
Diisopro
pyl
ether
Ethylbe
nzene
Isoprop
ylbenze
ne
(Cumen
e)
Methyl-
tert-
butyl
ether
Methylene
Chlorid
e
Naphth
alene Toluene m&p-
Xylene
n-
Propylb
enzene
o-
Xylene
Date
Collected
(mm/dd/yy)
Sample
Depth
(ft. BGS)
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
3/30/2022 1480 ND ND 369 9380 44 2100 66.5 213 ND 519 8340 5930 191 3340
12/20/2021 1190 ND ND 293 6820 232 1540 45.5 120 ND 350 4780 4000 154 2240
6/7/2021 3590 ND ND ND 9760 466 3060 135 308 ND 923 1100 10300 ND 4880
2/17/2021 1860 ND ND ND 10600 447 2330 77 256 ND 599 9490 6620 ND 3710
10/19/2020 2900 ND ND ND 10300 621 2760 117 329 217 779 12200 9210 ND 4630
12/4/2019 3660 ND ND 923 10400 612 3460 135 397 ND 792 14400 12000 456 5700
04/16/2019 1860 ND ND 447 12200 708 2650 76.7 373 ND 501 11700 8160 230 4310
3/30/2022 8.8 ND 1.3 5.8 49.8 25.1 ND 0.69 58.5 ND 4.4 ND 20.4 ND 26.6
12/20/2021 ND ND ND ND 692 19.2 ND 9.9 12.9 ND 13.6 ND ND ND 10.6
6/7/2021 3.3 ND ND ND 564 12.5 ND 10.7 7.4 ND 17.8 ND ND ND 43.3
2/17/2021 3.2 ND ND ND 816 18 ND 9.7 10.9 ND 17.5 ND ND ND 36.9
10/19/2020 37.2 ND ND ND 435 13.4 9.3 6.8 11.4 11.2 36.1 4.8 53 ND 144
12/4/2019 118 ND ND ND 778 26.1 12.6 5.7 28 ND 59.8 23.4 183 ND 370
04/16/2019 106 ND ND 25.7 759 29.0 29.0 7.6 29.7 ND 37.9 28.3 226 6.1 288
3/30/2022 ND ND ND ND ND 0.78 ND ND 46.2 ND ND ND ND ND ND
12/20/2021 ND ND ND ND 339 14.5 1.5 ND 3.7 ND ND 6 8 ND 3.3
6/7/2021 ND ND ND ND 211 8.6 1.7 ND 2.4 ND ND 7.6 6.6 ND 2.1
2/17/2021 ND ND ND ND 154 6.1 1.3 ND ND ND ND 4 4.3 ND 1.5
10/19/2020 ND ND ND ND 49.3 3 0.55 ND ND ND ND 2.6 1.8 ND 0.65
12/4/2019 ND ND ND ND ND 0.63 ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 454 9.3 32.6 123 219 100 181 14.2 567 22 152 763 1500 30.1 690
12/20/2021 1150 ND ND 228 138 ND 1820 ND ND ND 369 12300 6340 104 3330
2/17/2021 ND ND ND ND 7.7 ND ND ND ND ND ND 2 ND ND ND
10/19/2020 ND ND ND ND 0.58 ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND 0.84 ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Analytical Method
Sample ID
Constituent of Concern
MW-1
MW-2
MW-3
MW-4
Table # 2
Summary of Analytical Results - Water Samples
THE SPOT - CANDLER
NCDEQ's Incident # 28826
12/20/2021 1150 ND ND 228 138 ND 1820 ND ND ND 369 12300 6340 104 3330
6/7/2021 410 ND ND ND 58.8 ND 296 18.4 ND ND 113 2070 1360 ND 850
2/17/2021 458 ND ND ND 108 ND 551 22 ND ND 156 3310 1880 ND 1150
10/19/2020 900 ND ND ND 323 ND 1050 40 ND 126 307 7630 3700 ND 2120
12/4/2019 802 ND ND 184 1030 ND 1170 36.1 ND ND 253 8950 4300 86.2 2200
04/16/2019 653 ND ND 207 596 ND 797 30.5 ND ND 180 3000 2870 80.8 1410
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 30.9 ND ND 56.6 19.6 3.5 25.7 21.1 8.3 ND 67.2 7.2 21.1 42.5 173
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND 0.59 ND ND 0.75 ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND 2 ND ND 1.9 ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2020 ND ND ND ND ND 1.9 ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 NA ND ND NA NA NA NA NA NA NA NA NA NA NA NA
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
400 0.02 0.4 400 1 70 600 70 20 5 6 600 500 70 500
28500 50 400 25000 5000 70000 84500 25000 20000 5000 6000 260000 85500 30000 855002L Class GCL Standards
2L Class GA Standards
MW-5
MW-6
MW-7
MW-8
WSW-1
WSW-2
ft. BGS = feet below ground surface
mg/L = milligrams per liter
ug/L = micrograms per liter
Bold data above the MSCC (Soil to Groundwater)
NOTES:
ND = Not Detected
Elapsed
Time
(min)
Flow
(DSCFM)
PPM Measured
(ppm)
K
(#C-gas)PPMg
Cc:m
(mg/dsm^3)
Cc
(lb/dscf)
PMRc
(lb/hr)
PMRg
(lb/hour)
PMR
(lb)
1 4239.0 500 4 2,000 1064 0.00007 16.888 19.544 19.219
60 6864.0 154 4 616 328 0.00002 8.422 9.747 9.747
120 4698.0 161 4 644 342 0.00002 6.027 6.975 23.249
320 5690.0 138 4 552 294 0.00002 6.256 7.241 19.308
480 5820.0 124 4 496 264 0.00002 5.750 6.655 6.655
540 TOTAL EMISSIONS IN POUNDS 78.178
Calculations
PPMw = “wet” concentration
PPMd = “dry” concentration
PPMc = PPMv, volumetric concentration of VOC emissions as carbon, dry basis, at STP
Cc:m
Cc = Cc:m (62.43 x 10-9 lb-m3/mg-ft3), lb/dscf, mass concentration of VOC emissions as carbon, dry basis, at STP
PMRc = Cc (Qstd) (60 min/hr), lb/hr, pollutant mass removal rate of VOC’s as carbon
PMRg = (PMRc) (Mg/Mcg), lb/hr, pollutant mass removal rate of VOC’s as gasoline
K = number of carbons in calibration gas (methane K=1, propane K=3, hexane K=6)
Mc = 12.01 mg/mg-mole, molecular wt. of carbon
K3 = 24.07 dsm3/106 mg-mole, mass to volume conversion factor at STP
Cc = lb/dscf, mass concentration of VOC emissions as carbon, dry basis, at STP
Mg = 103 mg/mg-mole, molecular wt. of gasoline (value may vary depending on contaminant)
Mcg = 89 mg/mg-mole, weight of carbon in gasoline molecule
Average values for molecular weight of gasoline, weight of carbon in gasoline molecule, and the conversion of pounds of gasoline emissions to gallons
of liquid gasoline are from Automotive Fuels Reference Book, by K. Owens and T. Coley, Second Edition, 1995, published by the Society
of Automotive Engineers.
The Spot - Candler
NOTE: To convert lbs. of gasoline emissions to gallons of liquid gasoline, divide by 6.25 lbs/gal.
= PPMc (Mc/K3)
TABLE 3
AFVR RESULTS

FIGURES
ASHEVILLE QUADRANGLE NORTH CAROLINA 7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1 Site Map
The Spot – Candler, NC
THE SPOT
Singleton Environmental, Inc
Singleton Environmental, Inc
Singleton Environmental, Inc

APPENDIX A

AFVR Disposal Manifest

APPENDIX B
Laboratory Analytical Report
#=CL#
April 06, 2022
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92596442
92596442
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
The Spot
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 48
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92596442
The Spot
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 48
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92596442
The Spot
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92596442001 MW-1 SM 6200B 63 PASI-CSAS
92596442002 MW-2 SM 6200B 63 PASI-CSAS
92596442003 MW-3 SM 6200B 63 PASI-CSAS
92596442004 MW-4 SM 6200B 63 PASI-CSAS
92596442005 MW-5 SM 6200B 63 PASI-CSAS
92596442006 MW-6 SM 6200B 63 PASI-CSAS
92596442007 MW-7 SM 6200B 63 PASI-CSAS
92596442008 MW-8 SM 6200B 63 PASI-CSAS
92596442009 WSW-1 SM 6200B 63 PASI-CSAS
92596442010 WSW-2 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-1 Lab ID:92596442001 Collected:03/30/22 16:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 9380 ug/L 04/01/22 18:24 71-43-2 M125.0 50
Bromobenzene ND ug/L 04/01/22 18:24 108-86-125.0 50
Bromochloromethane ND ug/L 04/01/22 18:24 74-97-525.0 50
Bromodichloromethane ND ug/L 04/01/22 18:24 75-27-425.0 50
Bromoform ND ug/L 04/01/22 18:24 75-25-225.0 50
Bromomethane ND ug/L 04/01/22 18:24 74-83-925050
n-Butylbenzene ND ug/L 04/01/22 18:24 104-51-825.0 50
sec-Butylbenzene ND ug/L 04/01/22 18:24 135-98-825.0 50
tert-Butylbenzene ND ug/L 04/01/22 18:24 98-06-625.0 50
Carbon tetrachloride ND ug/L 04/01/22 18:24 56-23-5 M125.0 50
Chlorobenzene ND ug/L 04/01/22 18:24 108-90-725.0 50
Chloroethane ND ug/L 04/01/22 18:24 75-00-350.0 50
Chloroform ND ug/L 04/01/22 18:24 67-66-325.0 50
Chloromethane ND ug/L 04/01/22 18:24 74-87-350.0 50
2-Chlorotoluene ND ug/L 04/01/22 18:24 95-49-825.0 50
4-Chlorotoluene ND ug/L 04/01/22 18:24 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 18:24 96-12-850.0 50
Dibromochloromethane ND ug/L 04/01/22 18:24 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 18:24 106-93-425.0 50
Dibromomethane ND ug/L 04/01/22 18:24 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 04/01/22 18:24 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 04/01/22 18:24 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 04/01/22 18:24 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 04/01/22 18:24 75-71-8 IH,L1,M025.0 50
1,1-Dichloroethane ND ug/L 04/01/22 18:24 75-34-325.0 50
1,2-Dichloroethane ND ug/L 04/01/22 18:24 107-06-225.0 50
1,1-Dichloroethene ND ug/L 04/01/22 18:24 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 04/01/22 18:24 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 04/01/22 18:24 156-60-525.0 50
1,2-Dichloropropane ND ug/L 04/01/22 18:24 78-87-525.0 50
1,3-Dichloropropane ND ug/L 04/01/22 18:24 142-28-925.0 50
2,2-Dichloropropane ND ug/L 04/01/22 18:24 594-20-725.0 50
1,1-Dichloropropene ND ug/L 04/01/22 18:24 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 04/01/22 18:24 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 04/01/22 18:24 10061-02-625.0 50
Diisopropyl ether 404 ug/L 04/01/22 18:24 108-20-325.0 50
Ethylbenzene 2100 ug/L 04/01/22 18:24 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 04/01/22 18:24 87-68-310050
Isopropylbenzene (Cumene)66.5 ug/L 04/01/22 18:24 98-82-825.0 50
Methylene Chloride ND ug/L 04/01/22 18:24 75-09-210050
Methyl-tert-butyl ether 213 ug/L 04/01/22 18:24 1634-04-425.0 50
Naphthalene 519 ug/L 04/01/22 18:24 91-20-310050
n-Propylbenzene 191 ug/L 04/01/22 18:24 103-65-125.0 50
Styrene ND ug/L 04/01/22 18:24 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 18:24 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 18:24 79-34-525.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-1 Lab ID:92596442001 Collected:03/30/22 16:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 18:24 127-18-425.0 50
Toluene 8340 ug/L 04/01/22 18:24 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 04/01/22 18:24 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 04/01/22 18:24 120-82-110050
1,1,1-Trichloroethane ND ug/L 04/01/22 18:24 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 04/01/22 18:24 79-00-525.0 50
Trichloroethene ND ug/L 04/01/22 18:24 79-01-625.0 50
Trichlorofluoromethane ND ug/L 04/01/22 18:24 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 04/01/22 18:24 96-18-425.0 50
1,2,4-Trimethylbenzene 1480 ug/L 04/01/22 18:24 95-63-625.0 50
1,3,5-Trimethylbenzene 369 ug/L 04/01/22 18:24 108-67-825.0 50
Vinyl chloride ND ug/L 04/01/22 18:24 75-01-450.0 50
m&p-Xylene 5930 ug/L 04/01/22 18:24 179601-23-150.0 50
o-Xylene 3340 ug/L 04/01/22 18:24 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)103 %04/01/22 18:24 17060-07-070-130 50
4-Bromofluorobenzene (S)103 %04/01/22 18:24 460-00-470-130 50
Toluene-d8 (S)99 %04/01/22 18:24 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-2 Lab ID:92596442002 Collected:03/30/22 15:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 49.8 ug/L 04/04/22 23:24 71-43-20.50 1
Bromobenzene ND ug/L 04/04/22 23:24 108-86-10.50 1
Bromochloromethane ND ug/L 04/04/22 23:24 74-97-50.50 1
Bromodichloromethane ND ug/L 04/04/22 23:24 75-27-40.50 1
Bromoform ND ug/L 04/04/22 23:24 75-25-20.50 1
Bromomethane ND ug/L 04/04/22 23:24 74-83-95.0 1
n-Butylbenzene ND ug/L 04/04/22 23:24 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/04/22 23:24 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/04/22 23:24 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/04/22 23:24 56-23-50.50 1
Chlorobenzene ND ug/L 04/04/22 23:24 108-90-70.50 1
Chloroethane ND ug/L 04/04/22 23:24 75-00-31.0 1
Chloroform ND ug/L 04/04/22 23:24 67-66-30.50 1
Chloromethane ND ug/L 04/04/22 23:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/04/22 23:24 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/04/22 23:24 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/04/22 23:24 96-12-81.0 1
Dibromochloromethane ND ug/L 04/04/22 23:24 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/04/22 23:24 106-93-40.50 1
Dibromomethane ND ug/L 04/04/22 23:24 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/04/22 23:24 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/04/22 23:24 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/04/22 23:24 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/04/22 23:24 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/04/22 23:24 75-34-30.50 1
1,2-Dichloroethane 1.3 ug/L 04/04/22 23:24 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/04/22 23:24 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/04/22 23:24 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/04/22 23:24 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/04/22 23:24 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/04/22 23:24 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/04/22 23:24 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/04/22 23:24 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/04/22 23:24 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/04/22 23:24 10061-02-60.50 1
Diisopropyl ether 25.1 ug/L 04/04/22 23:24 108-20-30.50 1
Ethylbenzene ND ug/L 04/04/22 23:24 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/04/22 23:24 87-68-32.0 1
Isopropylbenzene (Cumene)0.69 ug/L 04/04/22 23:24 98-82-80.50 1
Methylene Chloride ND ug/L 04/04/22 23:24 75-09-22.0 1
Methyl-tert-butyl ether 58.5 ug/L 04/04/22 23:24 1634-04-40.50 1
Naphthalene 4.4 ug/L 04/04/22 23:24 91-20-32.0 1
n-Propylbenzene ND ug/L 04/04/22 23:24 103-65-10.50 1
Styrene ND ug/L 04/04/22 23:24 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/04/22 23:24 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/04/22 23:24 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-2 Lab ID:92596442002 Collected:03/30/22 15:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/04/22 23:24 127-18-40.50 1
Toluene ND ug/L 04/04/22 23:24 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/04/22 23:24 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/04/22 23:24 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/04/22 23:24 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/04/22 23:24 79-00-50.50 1
Trichloroethene ND ug/L 04/04/22 23:24 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/04/22 23:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/04/22 23:24 96-18-40.50 1
1,2,4-Trimethylbenzene 8.8 ug/L 04/04/22 23:24 95-63-60.50 1
1,3,5-Trimethylbenzene 5.8 ug/L 04/04/22 23:24 108-67-80.50 1
Vinyl chloride ND ug/L 04/04/22 23:24 75-01-41.0 1
m&p-Xylene 20.4 ug/L 04/04/22 23:24 179601-23-11.0 1
o-Xylene 26.6 ug/L 04/04/22 23:24 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %04/04/22 23:24 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %04/04/22 23:24 460-00-470-130 1
Toluene-d8 (S)100 %04/04/22 23:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-3 Lab ID:92596442003 Collected:03/30/22 14:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/04/22 23:42 71-43-20.50 1
Bromobenzene ND ug/L 04/04/22 23:42 108-86-10.50 1
Bromochloromethane ND ug/L 04/04/22 23:42 74-97-50.50 1
Bromodichloromethane ND ug/L 04/04/22 23:42 75-27-40.50 1
Bromoform ND ug/L 04/04/22 23:42 75-25-20.50 1
Bromomethane ND ug/L 04/04/22 23:42 74-83-95.0 1
n-Butylbenzene ND ug/L 04/04/22 23:42 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/04/22 23:42 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/04/22 23:42 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/04/22 23:42 56-23-50.50 1
Chlorobenzene ND ug/L 04/04/22 23:42 108-90-70.50 1
Chloroethane ND ug/L 04/04/22 23:42 75-00-31.0 1
Chloroform ND ug/L 04/04/22 23:42 67-66-30.50 1
Chloromethane ND ug/L 04/04/22 23:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/04/22 23:42 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/04/22 23:42 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/04/22 23:42 96-12-81.0 1
Dibromochloromethane ND ug/L 04/04/22 23:42 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/04/22 23:42 106-93-40.50 1
Dibromomethane ND ug/L 04/04/22 23:42 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/04/22 23:42 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/04/22 23:42 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/04/22 23:42 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/04/22 23:42 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/04/22 23:42 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/04/22 23:42 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/04/22 23:42 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/04/22 23:42 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/04/22 23:42 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/04/22 23:42 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/04/22 23:42 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/04/22 23:42 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/04/22 23:42 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/04/22 23:42 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/04/22 23:42 10061-02-60.50 1
Diisopropyl ether 0.78 ug/L 04/04/22 23:42 108-20-30.50 1
Ethylbenzene ND ug/L 04/04/22 23:42 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/04/22 23:42 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/04/22 23:42 98-82-80.50 1
Methylene Chloride ND ug/L 04/04/22 23:42 75-09-22.0 1
Methyl-tert-butyl ether 46.2 ug/L 04/04/22 23:42 1634-04-40.50 1
Naphthalene ND ug/L 04/04/22 23:42 91-20-32.0 1
n-Propylbenzene ND ug/L 04/04/22 23:42 103-65-10.50 1
Styrene ND ug/L 04/04/22 23:42 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/04/22 23:42 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/04/22 23:42 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-3 Lab ID:92596442003 Collected:03/30/22 14:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/04/22 23:42 127-18-40.50 1
Toluene ND ug/L 04/04/22 23:42 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/04/22 23:42 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/04/22 23:42 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/04/22 23:42 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/04/22 23:42 79-00-50.50 1
Trichloroethene ND ug/L 04/04/22 23:42 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/04/22 23:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/04/22 23:42 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/04/22 23:42 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/04/22 23:42 108-67-80.50 1
Vinyl chloride ND ug/L 04/04/22 23:42 75-01-41.0 1
m&p-Xylene ND ug/L 04/04/22 23:42 179601-23-11.0 1
o-Xylene ND ug/L 04/04/22 23:42 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)112 %04/04/22 23:42 17060-07-070-130 1
4-Bromofluorobenzene (S)105 %04/04/22 23:42 460-00-470-130 1
Toluene-d8 (S)100 %04/04/22 23:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-4 Lab ID:92596442004 Collected:03/30/22 14:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 219 ug/L 04/05/22 17:45 71-43-22.5 5
Bromobenzene ND ug/L 04/05/22 17:45 108-86-12.5 5
Bromochloromethane ND ug/L 04/05/22 17:45 74-97-52.5 5
Bromodichloromethane ND ug/L 04/05/22 17:45 75-27-42.5 5
Bromoform ND ug/L 04/05/22 17:45 75-25-22.5 5
Bromomethane ND ug/L 04/05/22 17:45 74-83-925.0 5
n-Butylbenzene ND ug/L 04/05/22 17:45 104-51-82.5 5
sec-Butylbenzene ND ug/L 04/05/22 17:45 135-98-82.5 5
tert-Butylbenzene ND ug/L 04/05/22 17:45 98-06-62.5 5
Carbon tetrachloride ND ug/L 04/05/22 17:45 56-23-5 L12.5 5
Chlorobenzene ND ug/L 04/05/22 17:45 108-90-72.5 5
Chloroethane ND ug/L 04/05/22 17:45 75-00-35.0 5
Chloroform ND ug/L 04/05/22 17:45 67-66-32.5 5
Chloromethane ND ug/L 04/05/22 17:45 74-87-35.0 5
2-Chlorotoluene ND ug/L 04/05/22 17:45 95-49-82.5 5
4-Chlorotoluene ND ug/L 04/05/22 17:45 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 04/05/22 17:45 96-12-85.0 5
Dibromochloromethane ND ug/L 04/05/22 17:45 124-48-12.5 5
1,2-Dibromoethane (EDB)9.3 ug/L 04/05/22 17:45 106-93-42.5 5
Dibromomethane ND ug/L 04/05/22 17:45 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 04/05/22 17:45 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 04/05/22 17:45 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 04/05/22 17:45 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 04/05/22 17:45 75-71-8 IH,L12.5 5
1,1-Dichloroethane ND ug/L 04/05/22 17:45 75-34-32.5 5
1,2-Dichloroethane 32.6 ug/L 04/05/22 17:45 107-06-22.5 5
1,1-Dichloroethene ND ug/L 04/05/22 17:45 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 04/05/22 17:45 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 04/05/22 17:45 156-60-52.5 5
1,2-Dichloropropane ND ug/L 04/05/22 17:45 78-87-52.5 5
1,3-Dichloropropane ND ug/L 04/05/22 17:45 142-28-92.5 5
2,2-Dichloropropane ND ug/L 04/05/22 17:45 594-20-72.5 5
1,1-Dichloropropene ND ug/L 04/05/22 17:45 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 04/05/22 17:45 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 04/05/22 17:45 10061-02-62.5 5
Diisopropyl ether 100 ug/L 04/05/22 17:45 108-20-32.5 5
Ethylbenzene 181 ug/L 04/05/22 17:45 100-41-42.5 5
Hexachloro-1,3-butadiene ND ug/L 04/05/22 17:45 87-68-310.0 5
Isopropylbenzene (Cumene)14.2 ug/L 04/05/22 17:45 98-82-82.5 5
Methylene Chloride 22.0 ug/L 04/05/22 17:45 75-09-210.0 5
Methyl-tert-butyl ether 567 ug/L 04/05/22 17:45 1634-04-42.5 5
Naphthalene 152 ug/L 04/05/22 17:45 91-20-310.0 5
n-Propylbenzene 30.1 ug/L 04/05/22 17:45 103-65-12.5 5
Styrene 3.5 ug/L 04/05/22 17:45 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 04/05/22 17:45 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 04/05/22 17:45 79-34-52.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-4 Lab ID:92596442004 Collected:03/30/22 14:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/05/22 17:45 127-18-42.5 5
Toluene 763 ug/L 04/05/22 17:45 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 04/05/22 17:45 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 04/05/22 17:45 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 04/05/22 17:45 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 04/05/22 17:45 79-00-52.5 5
Trichloroethene ND ug/L 04/05/22 17:45 79-01-62.5 5
Trichlorofluoromethane ND ug/L 04/05/22 17:45 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 04/05/22 17:45 96-18-42.5 5
1,2,4-Trimethylbenzene 454 ug/L 04/05/22 17:45 95-63-62.5 5
1,3,5-Trimethylbenzene 123 ug/L 04/05/22 17:45 108-67-82.5 5
Vinyl chloride ND ug/L 04/05/22 17:45 75-01-45.0 5
m&p-Xylene 1500 ug/L 04/05/22 17:45 179601-23-15.0 5
o-Xylene 690 ug/L 04/05/22 17:45 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)110 %04/05/22 17:45 17060-07-070-130 5
4-Bromofluorobenzene (S)100 %04/05/22 17:45 460-00-470-130 5
Toluene-d8 (S)103 %04/05/22 17:45 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-5 Lab ID:92596442005 Collected:03/30/22 15:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/05/22 16:51 71-43-20.50 1
Bromobenzene ND ug/L 04/05/22 16:51 108-86-10.50 1
Bromochloromethane ND ug/L 04/05/22 16:51 74-97-50.50 1
Bromodichloromethane ND ug/L 04/05/22 16:51 75-27-40.50 1
Bromoform ND ug/L 04/05/22 16:51 75-25-20.50 1
Bromomethane ND ug/L 04/05/22 16:51 74-83-95.0 1
n-Butylbenzene ND ug/L 04/05/22 16:51 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/05/22 16:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/05/22 16:51 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/05/22 16:51 56-23-5 L10.50 1
Chlorobenzene ND ug/L 04/05/22 16:51 108-90-70.50 1
Chloroethane ND ug/L 04/05/22 16:51 75-00-31.0 1
Chloroform ND ug/L 04/05/22 16:51 67-66-30.50 1
Chloromethane ND ug/L 04/05/22 16:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/05/22 16:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/05/22 16:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/05/22 16:51 96-12-81.0 1
Dibromochloromethane ND ug/L 04/05/22 16:51 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/05/22 16:51 106-93-40.50 1
Dibromomethane ND ug/L 04/05/22 16:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/05/22 16:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/05/22 16:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/05/22 16:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/05/22 16:51 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/05/22 16:51 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/05/22 16:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/05/22 16:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/05/22 16:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/05/22 16:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/05/22 16:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/05/22 16:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/05/22 16:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/05/22 16:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/05/22 16:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/05/22 16:51 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/05/22 16:51 108-20-30.50 1
Ethylbenzene ND ug/L 04/05/22 16:51 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/05/22 16:51 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/05/22 16:51 98-82-80.50 1
Methylene Chloride ND ug/L 04/05/22 16:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/05/22 16:51 1634-04-40.50 1
Naphthalene ND ug/L 04/05/22 16:51 91-20-32.0 1
n-Propylbenzene ND ug/L 04/05/22 16:51 103-65-10.50 1
Styrene ND ug/L 04/05/22 16:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/05/22 16:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/05/22 16:51 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-5 Lab ID:92596442005 Collected:03/30/22 15:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/05/22 16:51 127-18-40.50 1
Toluene ND ug/L 04/05/22 16:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/05/22 16:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/05/22 16:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/05/22 16:51 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/05/22 16:51 79-00-50.50 1
Trichloroethene ND ug/L 04/05/22 16:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/05/22 16:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/05/22 16:51 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/05/22 16:51 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/05/22 16:51 108-67-80.50 1
Vinyl chloride ND ug/L 04/05/22 16:51 75-01-41.0 1
m&p-Xylene ND ug/L 04/05/22 16:51 179601-23-11.0 1
o-Xylene ND ug/L 04/05/22 16:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %04/05/22 16:51 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %04/05/22 16:51 460-00-470-130 1
Toluene-d8 (S)101 %04/05/22 16:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-6 Lab ID:92596442006 Collected:03/30/22 13:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 22:54 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 22:54 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 22:54 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 22:54 75-27-40.50 1
Bromoform ND ug/L 04/01/22 22:54 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 22:54 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 22:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 22:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 22:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 22:54 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 22:54 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 22:54 75-00-31.0 1
Chloroform ND ug/L 04/01/22 22:54 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 22:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 22:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 22:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 22:54 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 22:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 22:54 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 22:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 22:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 22:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 22:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 22:54 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 22:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 22:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 22:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 22:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 22:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 22:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 22:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 22:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 22:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 22:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 22:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 22:54 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 22:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 22:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 22:54 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 22:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 22:54 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 22:54 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 22:54 103-65-10.50 1
Styrene ND ug/L 04/01/22 22:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 22:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 22:54 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-6 Lab ID:92596442006 Collected:03/30/22 13:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 22:54 127-18-40.50 1
Toluene ND ug/L 04/01/22 22:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 22:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 22:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 22:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 22:54 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 22:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 22:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 22:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 22:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 22:54 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 22:54 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 22:54 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 22:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %04/01/22 22:54 17060-07-070-130 1
4-Bromofluorobenzene (S)106 %04/01/22 22:54 460-00-470-130 1
Toluene-d8 (S)100 %04/01/22 22:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-7 Lab ID:92596442007 Collected:03/30/22 13:45 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 23:12 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 23:12 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 23:12 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 23:12 75-27-40.50 1
Bromoform ND ug/L 04/01/22 23:12 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 23:12 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 23:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 23:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 23:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 23:12 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 23:12 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 23:12 75-00-31.0 1
Chloroform ND ug/L 04/01/22 23:12 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 23:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 23:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 23:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 23:12 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 23:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 23:12 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 23:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 23:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 23:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 23:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 23:12 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 23:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 23:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 23:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 23:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 23:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 23:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 23:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 23:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 23:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 23:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 23:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 23:12 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 23:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 23:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 23:12 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 23:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 23:12 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 23:12 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 23:12 103-65-10.50 1
Styrene ND ug/L 04/01/22 23:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 23:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 23:12 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-7 Lab ID:92596442007 Collected:03/30/22 13:45 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 23:12 127-18-40.50 1
Toluene ND ug/L 04/01/22 23:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 23:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 23:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 23:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 23:12 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 23:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 23:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 23:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 23:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 23:12 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 23:12 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 23:12 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 23:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %04/01/22 23:12 17060-07-070-130 1
4-Bromofluorobenzene (S)103 %04/01/22 23:12 460-00-470-130 1
Toluene-d8 (S)102 %04/01/22 23:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-8 Lab ID:92596442008 Collected:03/30/22 16:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 19.6 ug/L 04/02/22 01:18 71-43-20.50 1
Bromobenzene ND ug/L 04/02/22 01:18 108-86-10.50 1
Bromochloromethane ND ug/L 04/02/22 01:18 74-97-50.50 1
Bromodichloromethane ND ug/L 04/02/22 01:18 75-27-40.50 1
Bromoform ND ug/L 04/02/22 01:18 75-25-20.50 1
Bromomethane ND ug/L 04/02/22 01:18 74-83-95.0 1
n-Butylbenzene ND ug/L 04/02/22 01:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/02/22 01:18 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/02/22 01:18 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/02/22 01:18 56-23-50.50 1
Chlorobenzene ND ug/L 04/02/22 01:18 108-90-70.50 1
Chloroethane ND ug/L 04/02/22 01:18 75-00-31.0 1
Chloroform ND ug/L 04/02/22 01:18 67-66-30.50 1
Chloromethane ND ug/L 04/02/22 01:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/02/22 01:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/02/22 01:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/02/22 01:18 96-12-81.0 1
Dibromochloromethane ND ug/L 04/02/22 01:18 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/02/22 01:18 106-93-40.50 1
Dibromomethane ND ug/L 04/02/22 01:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/02/22 01:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/02/22 01:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/02/22 01:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/02/22 01:18 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/02/22 01:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/02/22 01:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/02/22 01:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/02/22 01:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/02/22 01:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/02/22 01:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/02/22 01:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/02/22 01:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/02/22 01:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/02/22 01:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/02/22 01:18 10061-02-60.50 1
Diisopropyl ether 3.5 ug/L 04/02/22 01:18 108-20-30.50 1
Ethylbenzene 25.7 ug/L 04/02/22 01:18 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/02/22 01:18 87-68-32.0 1
Isopropylbenzene (Cumene)21.1 ug/L 04/02/22 01:18 98-82-80.50 1
Methylene Chloride ND ug/L 04/02/22 01:18 75-09-22.0 1
Methyl-tert-butyl ether 8.3 ug/L 04/02/22 01:18 1634-04-40.50 1
Naphthalene 67.2 ug/L 04/02/22 01:18 91-20-32.0 1
n-Propylbenzene 42.5 ug/L 04/02/22 01:18 103-65-10.50 1
Styrene ND ug/L 04/02/22 01:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/02/22 01:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/02/22 01:18 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
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Page 18 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-8 Lab ID:92596442008 Collected:03/30/22 16:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/02/22 01:18 127-18-40.50 1
Toluene 7.2 ug/L 04/02/22 01:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/02/22 01:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/02/22 01:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/02/22 01:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/02/22 01:18 79-00-50.50 1
Trichloroethene ND ug/L 04/02/22 01:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/02/22 01:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/02/22 01:18 96-18-40.50 1
1,2,4-Trimethylbenzene 30.9 ug/L 04/02/22 01:18 95-63-60.50 1
1,3,5-Trimethylbenzene 56.6 ug/L 04/02/22 01:18 108-67-80.50 1
Vinyl chloride ND ug/L 04/02/22 01:18 75-01-41.0 1
m&p-Xylene 21.1 ug/L 04/02/22 01:18 179601-23-11.0 1
o-Xylene 173 ug/L 04/02/22 01:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %04/02/22 01:18 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %04/02/22 01:18 460-00-470-130 1
Toluene-d8 (S)98 %04/02/22 01:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
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Asheville, NC 28804
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Page 19 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-1 Lab ID:92596442009 Collected:03/30/22 13:00 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 23:30 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 23:30 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 23:30 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 23:30 75-27-40.50 1
Bromoform ND ug/L 04/01/22 23:30 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 23:30 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 23:30 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 23:30 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 23:30 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 23:30 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 23:30 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 23:30 75-00-31.0 1
Chloroform ND ug/L 04/01/22 23:30 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 23:30 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 23:30 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 23:30 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 23:30 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 23:30 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 23:30 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 23:30 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 23:30 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 23:30 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 23:30 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 23:30 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 23:30 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 23:30 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 23:30 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 23:30 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 23:30 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 23:30 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 23:30 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 23:30 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 23:30 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 23:30 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 23:30 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 23:30 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 23:30 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 23:30 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 23:30 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 23:30 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 23:30 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 23:30 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 23:30 103-65-10.50 1
Styrene ND ug/L 04/01/22 23:30 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 23:30 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 23:30 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
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Page 20 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-1 Lab ID:92596442009 Collected:03/30/22 13:00 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 23:30 127-18-40.50 1
Toluene ND ug/L 04/01/22 23:30 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 23:30 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 23:30 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 23:30 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 23:30 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 23:30 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 23:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 23:30 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 23:30 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 23:30 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 23:30 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 23:30 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 23:30 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %04/01/22 23:30 17060-07-070-130 1
4-Bromofluorobenzene (S)109 %04/01/22 23:30 460-00-470-130 1
Toluene-d8 (S)102 %04/01/22 23:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-2 Lab ID:92596442010 Collected:03/30/22 13:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 23:48 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 23:48 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 23:48 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 23:48 75-27-40.50 1
Bromoform ND ug/L 04/01/22 23:48 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 23:48 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 23:48 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 23:48 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 23:48 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 23:48 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 23:48 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 23:48 75-00-31.0 1
Chloroform ND ug/L 04/01/22 23:48 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 23:48 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 23:48 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 23:48 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 23:48 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 23:48 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 23:48 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 23:48 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 23:48 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 23:48 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 23:48 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 23:48 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 23:48 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 23:48 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 23:48 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 23:48 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 23:48 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 23:48 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 23:48 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 23:48 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 23:48 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 23:48 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 23:48 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 23:48 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 23:48 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 23:48 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 23:48 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 23:48 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 23:48 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 23:48 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 23:48 103-65-10.50 1
Styrene ND ug/L 04/01/22 23:48 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 23:48 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 23:48 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-2 Lab ID:92596442010 Collected:03/30/22 13:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 23:48 127-18-40.50 1
Toluene ND ug/L 04/01/22 23:48 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 23:48 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 23:48 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 23:48 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 23:48 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 23:48 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 23:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 23:48 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 23:48 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 23:48 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 23:48 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 23:48 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 23:48 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %04/01/22 23:48 17060-07-070-130 1
4-Bromofluorobenzene (S)107 %04/01/22 23:48 460-00-470-130 1
Toluene-d8 (S)100 %04/01/22 23:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
688853
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3599706
Associated Lab Samples:92596442001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/01/22 10:18
1,1,1-Trichloroethane ug/L ND 0.50 04/01/22 10:18
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/01/22 10:18
1,1,2-Trichloroethane ug/L ND 0.50 04/01/22 10:18
1,1-Dichloroethane ug/L ND 0.50 04/01/22 10:18
1,1-Dichloroethene ug/L ND 0.50 04/01/22 10:18
1,1-Dichloropropene ug/L ND 0.50 04/01/22 10:18
1,2,3-Trichlorobenzene ug/L ND 2.0 04/01/22 10:18
1,2,3-Trichloropropane ug/L ND 0.50 04/01/22 10:18
1,2,4-Trichlorobenzene ug/L ND 2.0 04/01/22 10:18
1,2,4-Trimethylbenzene ug/L ND 0.50 04/01/22 10:18
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/01/22 10:18
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/01/22 10:18
1,2-Dichlorobenzene ug/L ND 0.50 04/01/22 10:18
1,2-Dichloroethane ug/L ND 0.50 04/01/22 10:18
1,2-Dichloropropane ug/L ND 0.50 04/01/22 10:18
1,3,5-Trimethylbenzene ug/L ND 0.50 04/01/22 10:18
1,3-Dichlorobenzene ug/L ND 0.50 04/01/22 10:18
1,3-Dichloropropane ug/L ND 0.50 04/01/22 10:18
1,4-Dichlorobenzene ug/L ND 0.50 04/01/22 10:18
2,2-Dichloropropane ug/L ND 0.50 04/01/22 10:18
2-Chlorotoluene ug/L ND 0.50 04/01/22 10:18
4-Chlorotoluene ug/L ND 0.50 04/01/22 10:18
Benzene ug/L ND 0.50 04/01/22 10:18
Bromobenzene ug/L ND 0.50 04/01/22 10:18
Bromochloromethane ug/L ND 0.50 04/01/22 10:18
Bromodichloromethane ug/L ND 0.50 04/01/22 10:18
Bromoform ug/L ND 0.50 04/01/22 10:18
Bromomethane ug/L ND 5.0 04/01/22 10:18
Carbon tetrachloride ug/L ND 0.50 04/01/22 10:18
Chlorobenzene ug/L ND 0.50 04/01/22 10:18
Chloroethane ug/L ND 1.0 04/01/22 10:18
Chloroform ug/L ND 0.50 04/01/22 10:18
Chloromethane ug/L ND 1.0 04/01/22 10:18
cis-1,2-Dichloroethene ug/L ND 0.50 04/01/22 10:18
cis-1,3-Dichloropropene ug/L ND 0.50 04/01/22 10:18
Dibromochloromethane ug/L ND 0.50 04/01/22 10:18
Dibromomethane ug/L ND 0.50 04/01/22 10:18
Dichlorodifluoromethane ug/L ND 0.50 IH04/01/22 10:18
Diisopropyl ether ug/L ND 0.50 04/01/22 10:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
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[phone]
Page 24 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3599706
Associated Lab Samples:92596442001
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/01/22 10:18
Hexachloro-1,3-butadiene ug/L ND 2.0 04/01/22 10:18
Isopropylbenzene (Cumene)ug/L ND 0.50 04/01/22 10:18
m&p-Xylene ug/L ND 1.0 04/01/22 10:18
Methyl-tert-butyl ether ug/L ND 0.50 04/01/22 10:18
Methylene Chloride ug/L ND 2.0 04/01/22 10:18
n-Butylbenzene ug/L ND 0.50 04/01/22 10:18
n-Propylbenzene ug/L ND 0.50 04/01/22 10:18
Naphthalene ug/L ND 2.0 04/01/22 10:18
o-Xylene ug/L ND 0.50 04/01/22 10:18
sec-Butylbenzene ug/L ND 0.50 04/01/22 10:18
Styrene ug/L ND 0.50 04/01/22 10:18
tert-Butylbenzene ug/L ND 0.50 04/01/22 10:18
Tetrachloroethene ug/L ND 0.50 04/01/22 10:18
Toluene ug/L ND 0.50 04/01/22 10:18
trans-1,2-Dichloroethene ug/L ND 0.50 04/01/22 10:18
trans-1,3-Dichloropropene ug/L ND 0.50 04/01/22 10:18
Trichloroethene ug/L ND 0.50 04/01/22 10:18
Trichlorofluoromethane ug/L ND 1.0 04/01/22 10:18
Vinyl chloride ug/L ND 1.0 04/01/22 10:18
1,2-Dichloroethane-d4 (S)%102 70-130 04/01/22 10:18
4-Bromofluorobenzene (S)%101 70-130 04/01/22 10:18
Toluene-d8 (S)%101 70-130 04/01/22 10:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3599707LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.650 107 60-140
1,1,1-Trichloroethane ug/L 51.250 102 60-140
1,1,2,2-Tetrachloroethane ug/L 54.050 108 60-140
1,1,2-Trichloroethane ug/L 51.050 102 60-140
1,1-Dichloroethane ug/L 46.850 94 60-140
1,1-Dichloroethene ug/L 51.450 103 60-140
1,1-Dichloropropene ug/L 49.950 100 60-140
1,2,3-Trichlorobenzene ug/L 56.050 112 60-140
1,2,3-Trichloropropane ug/L 52.950 106 60-140
1,2,4-Trichlorobenzene ug/L 57.350 115 60-140
1,2,4-Trimethylbenzene ug/L 52.450 105 60-140
1,2-Dibromo-3-chloropropane ug/L 49.750 99 60-140
1,2-Dibromoethane (EDB)ug/L 54.550 109 60-140
1,2-Dichlorobenzene ug/L 55.350 111 60-140
1,2-Dichloroethane ug/L 49.150 98 60-140
1,2-Dichloropropane ug/L 50.750 101 60-140
1,3,5-Trimethylbenzene ug/L 53.450 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3599707LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 57.750 115 60-140
1,3-Dichloropropane ug/L 53.350 107 60-140
1,4-Dichlorobenzene ug/L 53.850 108 60-140
2,2-Dichloropropane ug/L 54.950 110 60-140
2-Chlorotoluene ug/L 52.150 104 60-140
4-Chlorotoluene ug/L 54.350 109 60-140
Benzene ug/L 46.350 93 60-140
Bromobenzene ug/L 54.550 109 60-140
Bromochloromethane ug/L 42.550 85 60-140
Bromodichloromethane ug/L 52.450 105 60-140
Bromoform ug/L 49.950 100 60-140
Bromomethane ug/L 44.250 88 60-140
Carbon tetrachloride ug/L 60.650 121 60-140
Chlorobenzene ug/L 54.350 109 60-140
Chloroethane ug/L 49.750 99 60-140
Chloroform ug/L 49.650 99 60-140
Chloromethane ug/L 50.450 101 60-140
cis-1,2-Dichloroethene ug/L 47.350 95 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 54.750 109 60-140
Dibromomethane ug/L 52.950 106 60-140
Dichlorodifluoromethane ug/L 79.2 IH,L15015860-140
Diisopropyl ether ug/L 50.950 102 60-140
Ethylbenzene ug/L 52.250 104 60-140
Hexachloro-1,3-butadiene ug/L 58.850 118 60-140
Isopropylbenzene (Cumene)ug/L 51.650 103 60-140
m&p-Xylene ug/L 105100 105 60-140
Methyl-tert-butyl ether ug/L 52.150 104 60-140
Methylene Chloride ug/L 52.050 104 60-140
n-Butylbenzene ug/L 56.250 112 60-140
n-Propylbenzene ug/L 52.250 104 60-140
Naphthalene ug/L 57.050 114 60-140
o-Xylene ug/L 53.250 106 60-140
sec-Butylbenzene ug/L 54.250 108 60-140
Styrene ug/L 52.050 104 60-140
tert-Butylbenzene ug/L 46.250 92 60-140
Tetrachloroethene ug/L 54.950 110 60-140
Toluene ug/L 48.850 98 60-140
trans-1,2-Dichloroethene ug/L 48.750 97 60-140
trans-1,3-Dichloropropene ug/L 53.850 108 60-140
Trichloroethene ug/L 52.650 105 60-140
Trichlorofluoromethane ug/L 44.350 89 60-140
Vinyl chloride ug/L 51.750 103 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3599708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596442001
3599709
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 1000 112 60-140119 61000ND11201190
1,1,1-Trichloroethane ug/L 1000 115 60-140122 61000ND11501220
1,1,2,2-Tetrachloroethane ug/L 1000 109 60-140118 91000ND10901180
1,1,2-Trichloroethane ug/L 1000 109 60-140111 21000ND10901110
1,1-Dichloroethane ug/L 1000 102 60-140113 91000ND10201130
1,1-Dichloroethene ug/L 1000 121 60-140129 61000ND12101290
1,1-Dichloropropene ug/L 1000 119 60-140125 51000ND11901250
1,2,3-Trichlorobenzene ug/L 1000 106 60-140107 11000ND10601070
1,2,3-Trichloropropane ug/L 1000 105 60-140110 41000ND10501100
1,2,4-Trichlorobenzene ug/L 1000 111 60-140117 51000ND11101170
1,2,4-Trimethylbenzene ug/L 1000 105 60-140122 71000148025302700
1,2-Dibromo-3-chloropropane ug/L 1000 105 60-140102 31000ND10501020
1,2-Dibromoethane (EDB)ug/L 1000 116 60-140125 81000ND11601250
1,2-Dichlorobenzene ug/L 1000 107 60-140118 101000ND10701180
1,2-Dichloroethane ug/L 1000 102 60-140114 111000ND10201140
1,2-Dichloropropane ug/L 1000 112 60-140120 71000ND11201200
1,3,5-Trimethylbenzene ug/L 1000 111 60-140124 8100036914801610
1,3-Dichlorobenzene ug/L 1000 111 60-140118 61000ND11101180
1,3-Dichloropropane ug/L 1000 102 60-140113 111000ND10201130
1,4-Dichlorobenzene ug/L 1000 101 60-140112 111000ND10101120
2,2-Dichloropropane ug/L 1000 106 60-140118 111000ND10601180
2-Chlorotoluene ug/L 1000 111 60-140119 71000ND11101190
4-Chlorotoluene ug/L 1000 110 60-140116 51000ND11001160
Benzene ug/L E,M1100012660-140149 2100093801060010900
Bromobenzene ug/L 1000 105 60-140115 91000ND10501150
Bromochloromethane ug/L 1000 94 60-140104 101000ND9411040
Bromodichloromethane ug/L 1000 117 60-140116 11000ND11701160
Bromoform ug/L 1000 96 60-140105 91000ND9611050
Bromomethane ug/L 1000 61 60-14078 251000ND608783
Carbon tetrachloride ug/L M1100014060-140144 31000ND14001440
Chlorobenzene ug/L 1000 110 60-140122 101000ND11001220
Chloroethane ug/L 1000 134 60-140138 41000ND13401380
Chloroform ug/L 1000 107 60-140117 91000ND10701170
Chloromethane ug/L 1000 109 60-140120 91000ND10901200
cis-1,2-Dichloroethene ug/L 1000 104 60-140114 91000ND10401140
cis-1,3-Dichloropropene ug/L 1000 110 60-140121 101000ND11001210
Dibromochloromethane ug/L 1000 109 60-140119 91000ND10901190
Dibromomethane ug/L 1000 109 60-140120 91000ND10901200
Dichlorodifluoromethane ug/L IH,M0100023560-140224 51000ND23502240
Diisopropyl ether ug/L 1000 101 60-140114 9100040414101540
Ethylbenzene ug/L 1000 100 60-140116 51000210031003260
Hexachloro-1,3-butadiene ug/L 1000 126 60-140130 31000ND12601300
Isopropylbenzene (Cumene)ug/L 1000 112 60-140118 5100066.5 1190 1250
m&p-Xylene ug/L 2000 104 60-140127 62000593080008470
Methyl-tert-butyl ether ug/L 1000 109 60-140120 8100021313001420
Methylene Chloride ug/L 1000 117 60-140127 81000ND11701270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3599708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596442001
3599709
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 1000 124 60-140130 51000ND12401300
n-Propylbenzene ug/L 1000 110 60-140120 8100019112901390
Naphthalene ug/L 1000 97 60-140114 10100051914901650
o-Xylene ug/L 1000 103 60-140123 41000334043704570
sec-Butylbenzene ug/L 1000 120 60-140127 51000ND12001270
Styrene ug/L 1000 113 60-140115 21000ND11301150
tert-Butylbenzene ug/L 1000 98 60-140107 81000ND9791070
Tetrachloroethene ug/L 1000 123 60-140122 11000ND12301220
Toluene ug/L 1000 99 60-140126 31000834093309600
trans-1,2-Dichloroethene ug/L 1000 115 60-140120 41000ND11501200
trans-1,3-Dichloropropene ug/L 1000 106 60-140115 81000ND10601150
Trichloroethene ug/L 1000 114 60-140126 91000ND11401260
Trichlorofluoromethane ug/L 1000 131 60-140129 21000ND13101290
Vinyl chloride ug/L 1000 125 60-140130 41000ND12501300
1,2-Dichloroethane-d4 (S)%102 70-130103
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%101 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
688913
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442006, 92596442007, 92596442008, 92596442009, 92596442010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3600065
Associated Lab Samples:92596442006, 92596442007, 92596442008, 92596442009, 92596442010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/01/22 22:18
1,1,1-Trichloroethane ug/L ND 0.50 04/01/22 22:18
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/01/22 22:18
1,1,2-Trichloroethane ug/L ND 0.50 04/01/22 22:18
1,1-Dichloroethane ug/L ND 0.50 04/01/22 22:18
1,1-Dichloroethene ug/L ND 0.50 04/01/22 22:18
1,1-Dichloropropene ug/L ND 0.50 04/01/22 22:18
1,2,3-Trichlorobenzene ug/L ND 2.0 04/01/22 22:18
1,2,3-Trichloropropane ug/L ND 0.50 04/01/22 22:18
1,2,4-Trichlorobenzene ug/L ND 2.0 04/01/22 22:18
1,2,4-Trimethylbenzene ug/L ND 0.50 04/01/22 22:18
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/01/22 22:18
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/01/22 22:18
1,2-Dichlorobenzene ug/L ND 0.50 04/01/22 22:18
1,2-Dichloroethane ug/L ND 0.50 04/01/22 22:18
1,2-Dichloropropane ug/L ND 0.50 04/01/22 22:18
1,3,5-Trimethylbenzene ug/L ND 0.50 04/01/22 22:18
1,3-Dichlorobenzene ug/L ND 0.50 04/01/22 22:18
1,3-Dichloropropane ug/L ND 0.50 04/01/22 22:18
1,4-Dichlorobenzene ug/L ND 0.50 04/01/22 22:18
2,2-Dichloropropane ug/L ND 0.50 04/01/22 22:18
2-Chlorotoluene ug/L ND 0.50 04/01/22 22:18
4-Chlorotoluene ug/L ND 0.50 04/01/22 22:18
Benzene ug/L ND 0.50 04/01/22 22:18
Bromobenzene ug/L ND 0.50 04/01/22 22:18
Bromochloromethane ug/L ND 0.50 04/01/22 22:18
Bromodichloromethane ug/L ND 0.50 04/01/22 22:18
Bromoform ug/L ND 0.50 04/01/22 22:18
Bromomethane ug/L ND 5.0 04/01/22 22:18
Carbon tetrachloride ug/L ND 0.50 04/01/22 22:18
Chlorobenzene ug/L ND 0.50 04/01/22 22:18
Chloroethane ug/L ND 1.0 04/01/22 22:18
Chloroform ug/L ND 0.50 04/01/22 22:18
Chloromethane ug/L ND 1.0 04/01/22 22:18
cis-1,2-Dichloroethene ug/L ND 0.50 04/01/22 22:18
cis-1,3-Dichloropropene ug/L ND 0.50 04/01/22 22:18
Dibromochloromethane ug/L ND 0.50 04/01/22 22:18
Dibromomethane ug/L ND 0.50 04/01/22 22:18
Dichlorodifluoromethane ug/L ND 0.50 IH04/01/22 22:18
Diisopropyl ether ug/L ND 0.50 04/01/22 22:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3600065
Associated Lab Samples:92596442006, 92596442007, 92596442008, 92596442009, 92596442010
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/01/22 22:18
Hexachloro-1,3-butadiene ug/L ND 2.0 04/01/22 22:18
Isopropylbenzene (Cumene)ug/L ND 0.50 04/01/22 22:18
m&p-Xylene ug/L ND 1.0 04/01/22 22:18
Methyl-tert-butyl ether ug/L ND 0.50 04/01/22 22:18
Methylene Chloride ug/L ND 2.0 04/01/22 22:18
n-Butylbenzene ug/L ND 0.50 04/01/22 22:18
n-Propylbenzene ug/L ND 0.50 04/01/22 22:18
Naphthalene ug/L ND 2.0 04/01/22 22:18
o-Xylene ug/L ND 0.50 04/01/22 22:18
sec-Butylbenzene ug/L ND 0.50 04/01/22 22:18
Styrene ug/L ND 0.50 04/01/22 22:18
tert-Butylbenzene ug/L ND 0.50 04/01/22 22:18
Tetrachloroethene ug/L ND 0.50 04/01/22 22:18
Toluene ug/L ND 0.50 04/01/22 22:18
trans-1,2-Dichloroethene ug/L ND 0.50 04/01/22 22:18
trans-1,3-Dichloropropene ug/L ND 0.50 04/01/22 22:18
Trichloroethene ug/L ND 0.50 04/01/22 22:18
Trichlorofluoromethane ug/L ND 1.0 04/01/22 22:18
Vinyl chloride ug/L ND 1.0 04/01/22 22:18
1,2-Dichloroethane-d4 (S)%100 70-130 04/01/22 22:18
4-Bromofluorobenzene (S)%102 70-130 04/01/22 22:18
Toluene-d8 (S)%99 70-130 04/01/22 22:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3600066LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.250 110 60-140
1,1,1-Trichloroethane ug/L 53.450 107 60-140
1,1,2,2-Tetrachloroethane ug/L 54.550 109 60-140
1,1,2-Trichloroethane ug/L 53.850 108 60-140
1,1-Dichloroethane ug/L 47.850 96 60-140
1,1-Dichloroethene ug/L 50.650 101 60-140
1,1-Dichloropropene ug/L 51.150 102 60-140
1,2,3-Trichlorobenzene ug/L 51.250 102 60-140
1,2,3-Trichloropropane ug/L 49.750 99 60-140
1,2,4-Trichlorobenzene ug/L 56.150 112 60-140
1,2,4-Trimethylbenzene ug/L 51.650 103 60-140
1,2-Dibromo-3-chloropropane ug/L 52.750 105 60-140
1,2-Dibromoethane (EDB)ug/L 55.050 110 60-140
1,2-Dichlorobenzene ug/L 52.950 106 60-140
1,2-Dichloroethane ug/L 49.350 99 60-140
1,2-Dichloropropane ug/L 53.050 106 60-140
1,3,5-Trimethylbenzene ug/L 52.550 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3600066LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 54.750 109 60-140
1,3-Dichloropropane ug/L 51.750 103 60-140
1,4-Dichlorobenzene ug/L 52.550 105 60-140
2,2-Dichloropropane ug/L 53.250 106 60-140
2-Chlorotoluene ug/L 50.850 102 60-140
4-Chlorotoluene ug/L 52.150 104 60-140
Benzene ug/L 48.250 96 60-140
Bromobenzene ug/L 50.250 100 60-140
Bromochloromethane ug/L 43.950 88 60-140
Bromodichloromethane ug/L 53.750 107 60-140
Bromoform ug/L 51.250 102 60-140
Bromomethane ug/L 38.050 76 60-140
Carbon tetrachloride ug/L 62.950 126 60-140
Chlorobenzene ug/L 52.650 105 60-140
Chloroethane ug/L 55.350 111 60-140
Chloroform ug/L 49.650 99 60-140
Chloromethane ug/L 49.850 100 60-140
cis-1,2-Dichloroethene ug/L 47.750 95 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 55.250 110 60-140
Dibromomethane ug/L 54.450 109 60-140
Dichlorodifluoromethane ug/L 82.6 IH,L15016560-140
Diisopropyl ether ug/L 50.450 101 60-140
Ethylbenzene ug/L 51.750 103 60-140
Hexachloro-1,3-butadiene ug/L 57.650 115 60-140
Isopropylbenzene (Cumene)ug/L 51.450 103 60-140
m&p-Xylene ug/L 107100 107 60-140
Methyl-tert-butyl ether ug/L 52.050 104 60-140
Methylene Chloride ug/L 53.050 106 60-140
n-Butylbenzene ug/L 57.050 114 60-140
n-Propylbenzene ug/L 51.850 104 60-140
Naphthalene ug/L 53.150 106 60-140
o-Xylene ug/L 53.550 107 60-140
sec-Butylbenzene ug/L 52.650 105 60-140
Styrene ug/L 52.850 106 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 56.350 113 60-140
Toluene ug/L 50.550 101 60-140
trans-1,2-Dichloroethene ug/L 48.950 98 60-140
trans-1,3-Dichloropropene ug/L 54.150 108 60-140
Trichloroethene ug/L 54.550 109 60-140
Trichlorofluoromethane ug/L 48.950 98 60-140
Vinyl chloride ug/L 51.750 103 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3600067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596043003
3600068
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 104 60-140108 42000ND20802170
1,1,1-Trichloroethane ug/L 2000 106 60-140109 22000ND21202170
1,1,2,2-Tetrachloroethane ug/L 2000 103 60-140106 32000ND20602120
1,1,2-Trichloroethane ug/L 2000 101 60-140108 62000ND20302150
1,1-Dichloroethane ug/L 2000 102 60-140104 22000ND20402090
1,1-Dichloroethene ug/L 2000 109 60-140119 92000ND21702370
1,1-Dichloropropene ug/L 2000 113 60-140115 12000ND22602290
1,2,3-Trichlorobenzene ug/L 2000 103 60-140108 52000ND20702160
1,2,3-Trichloropropane ug/L 2000 104 60-14099 52000ND20801980
1,2,4-Trichlorobenzene ug/L 2000 106 60-140113 62000ND21202270
1,2,4-Trimethylbenzene ug/L 2000 100 60-140103 12000286048704910
1,2-Dibromo-3-chloropropane ug/L 2000 102 60-140105 32000ND20302100
1,2-Dibromoethane (EDB)ug/L 2000 109 60-140109 02000ND21802180
1,2-Dichlorobenzene ug/L 2000 107 60-140107 02000ND21402140
1,2-Dichloroethane ug/L 2000 103 60-140102 12000ND20502040
1,2-Dichloropropane ug/L 2000 104 60-140110 52000ND20902200
1,3,5-Trimethylbenzene ug/L 2000 114 60-140115 1200074930303050
1,3-Dichlorobenzene ug/L 2000 109 60-140115 52000ND21702290
1,3-Dichloropropane ug/L 2000 102 60-140111 92000ND20302220
1,4-Dichlorobenzene ug/L 2000 108 60-140106 12000ND21502130
2,2-Dichloropropane ug/L 2000 99 60-14093 62000ND19701860
2-Chlorotoluene ug/L 2000 106 60-140113 72000ND21102260
4-Chlorotoluene ug/L 2000 108 60-140109 12000ND21502170
Benzene ug/L 2000 96 60-140100 3200037923002370
Bromobenzene ug/L 2000 109 60-140107 22000ND21802140
Bromochloromethane ug/L 2000 96 60-14089 82000ND19201770
Bromodichloromethane ug/L 2000 103 60-140111 82000ND20502230
Bromoform ug/L 2000 92 60-14096 52000ND18401930
Bromomethane ug/L 2000 75 60-14084 112000ND15001670
Carbon tetrachloride ug/L 2000 122 60-140126 32000ND24502530
Chlorobenzene ug/L 2000 109 60-140107 32000ND21902130
Chloroethane ug/L 2000 118 60-140126 62000ND23602510
Chloroform ug/L 2000 106 60-140104 22000ND21202080
Chloromethane ug/L 2000 108 60-140111 22000ND21602220
cis-1,2-Dichloroethene ug/L 2000 102 60-140104 22000ND20302070
cis-1,3-Dichloropropene ug/L 2000 105 60-140108 32000ND20902160
Dibromochloromethane ug/L 2000 104 60-140106 22000ND20802110
Dibromomethane ug/L 2000 106 60-140115 82000ND21302310
Dichlorodifluoromethane ug/L IH,M0200015360-140182 172000ND30703640
Diisopropyl ether ug/L 2000 104 60-140101 22000ND20702030
Ethylbenzene ug/L 2000 106 60-140109 22000126033703430
Hexachloro-1,3-butadiene ug/L 2000 109 60-140120 92000ND21902400
Isopropylbenzene (Cumene)ug/L 2000 104 60-140108 4200011821902280
m&p-Xylene ug/L 4000 100 60-140110 44000546094609840
Methyl-tert-butyl ether ug/L 2000 109 60-140106 22000ND21702120
Methylene Chloride ug/L 2000 111 60-140117 52000ND22302330
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3600067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596043003
3600068
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 2000 111 60-140111 1200018524002410
n-Propylbenzene ug/L 2000 105 60-140107 1200031824202460
Naphthalene ug/L 2000 106 60-140111 4200033824502550
o-Xylene ug/L 2000 104 60-140111 32000263047004850
sec-Butylbenzene ug/L 2000 112 60-140117 42000ND22402330
Styrene ug/L 2000 108 60-140108 02000ND21502150
tert-Butylbenzene ug/L 2000 94 60-14096 22000ND18801920
Tetrachloroethene ug/L 2000 112 60-140113 12000ND22402260
Toluene ug/L 2000 68 60-14085 22000116001300013300
trans-1,2-Dichloroethene ug/L 2000 103 60-140104 22000ND20502080
trans-1,3-Dichloropropene ug/L 2000 100 60-140102 22000ND20002050
Trichloroethene ug/L 2000 113 60-140111 12000ND22602230
Trichlorofluoromethane ug/L 2000 106 60-140119 112000ND21302380
Vinyl chloride ug/L 2000 114 60-140121 62000ND22802420
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689213
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442002, 92596442003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3601549
Associated Lab Samples:92596442002, 92596442003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/04/22 21:36
1,1,1-Trichloroethane ug/L ND 0.50 04/04/22 21:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/04/22 21:36
1,1,2-Trichloroethane ug/L ND 0.50 04/04/22 21:36
1,1-Dichloroethane ug/L ND 0.50 04/04/22 21:36
1,1-Dichloroethene ug/L ND 0.50 04/04/22 21:36
1,1-Dichloropropene ug/L ND 0.50 04/04/22 21:36
1,2,3-Trichlorobenzene ug/L ND 2.0 04/04/22 21:36
1,2,3-Trichloropropane ug/L ND 0.50 04/04/22 21:36
1,2,4-Trichlorobenzene ug/L ND 2.0 04/04/22 21:36
1,2,4-Trimethylbenzene ug/L ND 0.50 04/04/22 21:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/04/22 21:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/04/22 21:36
1,2-Dichlorobenzene ug/L ND 0.50 04/04/22 21:36
1,2-Dichloroethane ug/L ND 0.50 04/04/22 21:36
1,2-Dichloropropane ug/L ND 0.50 04/04/22 21:36
1,3,5-Trimethylbenzene ug/L ND 0.50 04/04/22 21:36
1,3-Dichlorobenzene ug/L ND 0.50 04/04/22 21:36
1,3-Dichloropropane ug/L ND 0.50 04/04/22 21:36
1,4-Dichlorobenzene ug/L ND 0.50 04/04/22 21:36
2,2-Dichloropropane ug/L ND 0.50 04/04/22 21:36
2-Chlorotoluene ug/L ND 0.50 04/04/22 21:36
4-Chlorotoluene ug/L ND 0.50 04/04/22 21:36
Benzene ug/L ND 0.50 04/04/22 21:36
Bromobenzene ug/L ND 0.50 04/04/22 21:36
Bromochloromethane ug/L ND 0.50 04/04/22 21:36
Bromodichloromethane ug/L ND 0.50 04/04/22 21:36
Bromoform ug/L ND 0.50 04/04/22 21:36
Bromomethane ug/L ND 5.0 04/04/22 21:36
Carbon tetrachloride ug/L ND 0.50 04/04/22 21:36
Chlorobenzene ug/L ND 0.50 04/04/22 21:36
Chloroethane ug/L ND 1.0 04/04/22 21:36
Chloroform ug/L ND 0.50 04/04/22 21:36
Chloromethane ug/L ND 1.0 04/04/22 21:36
cis-1,2-Dichloroethene ug/L ND 0.50 04/04/22 21:36
cis-1,3-Dichloropropene ug/L ND 0.50 04/04/22 21:36
Dibromochloromethane ug/L ND 0.50 04/04/22 21:36
Dibromomethane ug/L ND 0.50 04/04/22 21:36
Dichlorodifluoromethane ug/L ND 0.50 IH04/04/22 21:36
Diisopropyl ether ug/L ND 0.50 04/04/22 21:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3601549
Associated Lab Samples:92596442002, 92596442003
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/04/22 21:36
Hexachloro-1,3-butadiene ug/L ND 2.0 04/04/22 21:36
Isopropylbenzene (Cumene)ug/L ND 0.50 04/04/22 21:36
m&p-Xylene ug/L ND 1.0 04/04/22 21:36
Methyl-tert-butyl ether ug/L ND 0.50 04/04/22 21:36
Methylene Chloride ug/L ND 2.0 04/04/22 21:36
n-Butylbenzene ug/L ND 0.50 04/04/22 21:36
n-Propylbenzene ug/L ND 0.50 04/04/22 21:36
Naphthalene ug/L ND 2.0 04/04/22 21:36
o-Xylene ug/L ND 0.50 04/04/22 21:36
sec-Butylbenzene ug/L ND 0.50 04/04/22 21:36
Styrene ug/L ND 0.50 04/04/22 21:36
tert-Butylbenzene ug/L ND 0.50 04/04/22 21:36
Tetrachloroethene ug/L ND 0.50 04/04/22 21:36
Toluene ug/L ND 0.50 04/04/22 21:36
trans-1,2-Dichloroethene ug/L ND 0.50 04/04/22 21:36
trans-1,3-Dichloropropene ug/L ND 0.50 04/04/22 21:36
Trichloroethene ug/L ND 0.50 04/04/22 21:36
Trichlorofluoromethane ug/L ND 1.0 04/04/22 21:36
Vinyl chloride ug/L ND 1.0 04/04/22 21:36
1,2-Dichloroethane-d4 (S)%108 70-130 04/04/22 21:36
4-Bromofluorobenzene (S)%107 70-130 04/04/22 21:36
Toluene-d8 (S)%101 70-130 04/04/22 21:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3601550LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 60-140
1,1,1-Trichloroethane ug/L 52.550 105 60-140
1,1,2,2-Tetrachloroethane ug/L 50.250 100 60-140
1,1,2-Trichloroethane ug/L 50.850 102 60-140
1,1-Dichloroethane ug/L 47.350 95 60-140
1,1-Dichloroethene ug/L 51.250 102 60-140
1,1-Dichloropropene ug/L 51.250 102 60-140
1,2,3-Trichlorobenzene ug/L 53.050 106 60-140
1,2,3-Trichloropropane ug/L 48.250 96 60-140
1,2,4-Trichlorobenzene ug/L 54.050 108 60-140
1,2,4-Trimethylbenzene ug/L 52.150 104 60-140
1,2-Dibromo-3-chloropropane ug/L 52.150 104 60-140
1,2-Dibromoethane (EDB)ug/L 52.050 104 60-140
1,2-Dichlorobenzene ug/L 52.450 105 60-140
1,2-Dichloroethane ug/L 47.650 95 60-140
1,2-Dichloropropane ug/L 50.950 102 60-140
1,3,5-Trimethylbenzene ug/L 52.250 104 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3601550LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 52.850 106 60-140
1,3-Dichloropropane ug/L 48.550 97 60-140
1,4-Dichlorobenzene ug/L 51.150 102 60-140
2,2-Dichloropropane ug/L 54.950 110 60-140
2-Chlorotoluene ug/L 49.950 100 60-140
4-Chlorotoluene ug/L 51.750 103 60-140
Benzene ug/L 45.950 92 60-140
Bromobenzene ug/L 49.550 99 60-140
Bromochloromethane ug/L 40.450 81 60-140
Bromodichloromethane ug/L 51.850 104 60-140
Bromoform ug/L 49.350 99 60-140
Bromomethane ug/L 46.950 94 60-140
Carbon tetrachloride ug/L 63.950 128 60-140
Chlorobenzene ug/L 48.750 97 60-140
Chloroethane ug/L 55.050 110 60-140
Chloroform ug/L 48.950 98 60-140
Chloromethane ug/L 53.650 107 60-140
cis-1,2-Dichloroethene ug/L 48.350 97 60-140
cis-1,3-Dichloropropene ug/L 52.550 105 60-140
Dibromochloromethane ug/L 50.950 102 60-140
Dibromomethane ug/L 52.850 106 60-140
Dichlorodifluoromethane ug/L 113 IH,L15022660-140
Diisopropyl ether ug/L 49.450 99 60-140
Ethylbenzene ug/L 47.450 95 60-140
Hexachloro-1,3-butadiene ug/L 58.050 116 60-140
Isopropylbenzene (Cumene)ug/L 47.250 94 60-140
m&p-Xylene ug/L 98.6100 99 60-140
Methyl-tert-butyl ether ug/L 51.650 103 60-140
Methylene Chloride ug/L 51.650 103 60-140
n-Butylbenzene ug/L 56.650 113 60-140
n-Propylbenzene ug/L 51.850 104 60-140
Naphthalene ug/L 55.550 111 60-140
o-Xylene ug/L 49.450 99 60-140
sec-Butylbenzene ug/L 54.550 109 60-140
Styrene ug/L 48.550 97 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 51.950 104 60-140
Toluene ug/L 47.250 94 60-140
trans-1,2-Dichloroethene ug/L 50.050 100 60-140
trans-1,3-Dichloropropene ug/L 52.350 105 60-140
Trichloroethene ug/L 50.650 101 60-140
Trichlorofluoromethane ug/L 53.050 106 60-140
Vinyl chloride ug/L 56.650 113 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3601551MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596441001
3601552
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 250 111 60-140113 2250ND277282
1,1,1-Trichloroethane ug/L 250 125 60-140114 9250ND312285
1,1,2,2-Tetrachloroethane ug/L 250 104 60-140104 0250ND260260
1,1,2-Trichloroethane ug/L 250 109 60-140107 2250ND272268
1,1-Dichloroethane ug/L 250 110 60-140104 5250ND279264
1,1-Dichloroethene ug/L 250 138 60-140121 13250ND345303
1,1-Dichloropropene ug/L 250 131 60-140113 14250ND328284
1,2,3-Trichlorobenzene ug/L 250 98 60-14098 0250ND249247
1,2,3-Trichloropropane ug/L 250 101 60-140105 4250ND252264
1,2,4-Trichlorobenzene ug/L 250 103 60-140104 1250ND261264
1,2,4-Trimethylbenzene ug/L 250 110 60-140106 4250ND281269
1,2-Dibromo-3-chloropropane ug/L 250 92 60-14097 5250ND231242
1,2-Dibromoethane (EDB)ug/L 250 111 60-140111 0250ND278277
1,2-Dichlorobenzene ug/L 250 110 60-140102 7250ND274256
1,2-Dichloroethane ug/L 250 111 60-140108 3250ND277269
1,2-Dichloropropane ug/L 250 119 60-140112 6250ND297280
1,3,5-Trimethylbenzene ug/L 250 115 60-140109 5250ND292277
1,3-Dichlorobenzene ug/L 250 110 60-140108 2250ND279275
1,3-Dichloropropane ug/L 250 107 60-140107 0250ND269268
1,4-Dichlorobenzene ug/L 250 101 60-140103 2250ND252257
2,2-Dichloropropane ug/L 250 117 60-140102 14250ND298260
2-Chlorotoluene ug/L 250 112 60-140107 4250ND279269
4-Chlorotoluene ug/L 250 109 60-140105 3250ND276268
Benzene ug/L 250 139 60-140104 5250146018101720
Bromobenzene ug/L 250 114 60-140108 6250ND286269
Bromochloromethane ug/L 250 113 60-140101 10250ND281254
Bromodichloromethane ug/L 250 114 60-140112 2250ND289284
Bromoform ug/L 250 95 60-14098 3250ND238246
Bromomethane ug/L 250 93 60-14090 3250ND232226
Carbon tetrachloride ug/L M125015860-140144 9250ND395361
Chlorobenzene ug/L 250 110 60-140112 2250ND275281
Chloroethane ug/L M125014160-140134 6250ND353334
Chloroform ug/L 250 116 60-140106 82506.4 296 272
Chloromethane ug/L 250 132 60-140120 9250ND329300
cis-1,2-Dichloroethene ug/L 250 109 60-140105 4250ND279269
cis-1,3-Dichloropropene ug/L 250 113 60-140115 2250ND283289
Dibromochloromethane ug/L 250 114 60-140117 2250ND286293
Dibromomethane ug/L 250 111 60-140121 9250ND277303
Dichlorodifluoromethane ug/L IH,M0,R125034460-140190 58250ND860475
Diisopropyl ether ug/L 250 111 60-140108 225034.1 310 303
Ethylbenzene ug/L 250 109 60-140107 2250ND278273
Hexachloro-1,3-butadiene ug/L 250 129 60-140125 3250ND323313
Isopropylbenzene (Cumene)ug/L 250 114 60-140110 325036.6 321 310
m&p-Xylene ug/L 500 116 60-140111 4500ND590568
Methyl-tert-butyl ether ug/L 250 114 60-140108 525023.1 309 294
Methylene Chloride ug/L 250 119 60-140113 525029.6 327 311
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3601551MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596441001
3601552
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 250 120 60-140111 82506.6 306 284
n-Propylbenzene ug/L 250 115 60-140109 6250ND288272
Naphthalene ug/L 250 92 60-14098 6250ND237251
o-Xylene ug/L 250 115 60-140107 72507.4 296 275
sec-Butylbenzene ug/L 250 123 60-140110 112507.4 315 283
Styrene ug/L 250 108 60-140105 3250ND272265
tert-Butylbenzene ug/L 250 104 60-14096 8250ND259239
Tetrachloroethene ug/L 250 116 60-140113 2250ND290283
Toluene ug/L 250 107 60-140105 2250ND272267
trans-1,2-Dichloroethene ug/L 250 124 60-140109 13250ND309272
trans-1,3-Dichloropropene ug/L 250 107 60-140108 1250ND268271
Trichloroethene ug/L 250 120 60-140109 925017.6 318 290
Trichlorofluoromethane ug/L M1,R125015660-140112 33250ND391280
Vinyl chloride ug/L M125014660-140118 21250ND365296
1,2-Dichloroethane-d4 (S)%108 70-130106
4-Bromofluorobenzene (S)%102 70-130102
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689413
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442004, 92596442005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3602443
Associated Lab Samples:92596442004, 92596442005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/05/22 11:45
1,1,1-Trichloroethane ug/L ND 0.50 04/05/22 11:45
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/05/22 11:45
1,1,2-Trichloroethane ug/L ND 0.50 04/05/22 11:45
1,1-Dichloroethane ug/L ND 0.50 04/05/22 11:45
1,1-Dichloroethene ug/L ND 0.50 04/05/22 11:45
1,1-Dichloropropene ug/L ND 0.50 04/05/22 11:45
1,2,3-Trichlorobenzene ug/L ND 2.0 04/05/22 11:45
1,2,3-Trichloropropane ug/L ND 0.50 04/05/22 11:45
1,2,4-Trichlorobenzene ug/L ND 2.0 04/05/22 11:45
1,2,4-Trimethylbenzene ug/L ND 0.50 04/05/22 11:45
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/05/22 11:45
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/05/22 11:45
1,2-Dichlorobenzene ug/L ND 0.50 04/05/22 11:45
1,2-Dichloroethane ug/L ND 0.50 04/05/22 11:45
1,2-Dichloropropane ug/L ND 0.50 04/05/22 11:45
1,3,5-Trimethylbenzene ug/L ND 0.50 04/05/22 11:45
1,3-Dichlorobenzene ug/L ND 0.50 04/05/22 11:45
1,3-Dichloropropane ug/L ND 0.50 04/05/22 11:45
1,4-Dichlorobenzene ug/L ND 0.50 04/05/22 11:45
2,2-Dichloropropane ug/L ND 0.50 04/05/22 11:45
2-Chlorotoluene ug/L ND 0.50 04/05/22 11:45
4-Chlorotoluene ug/L ND 0.50 04/05/22 11:45
Benzene ug/L ND 0.50 04/05/22 11:45
Bromobenzene ug/L ND 0.50 04/05/22 11:45
Bromochloromethane ug/L ND 0.50 04/05/22 11:45
Bromodichloromethane ug/L ND 0.50 04/05/22 11:45
Bromoform ug/L ND 0.50 04/05/22 11:45
Bromomethane ug/L ND 5.0 04/05/22 11:45
Carbon tetrachloride ug/L ND 0.50 04/05/22 11:45
Chlorobenzene ug/L ND 0.50 04/05/22 11:45
Chloroethane ug/L ND 1.0 04/05/22 11:45
Chloroform ug/L ND 0.50 04/05/22 11:45
Chloromethane ug/L ND 1.0 04/05/22 11:45
cis-1,2-Dichloroethene ug/L ND 0.50 04/05/22 11:45
cis-1,3-Dichloropropene ug/L ND 0.50 04/05/22 11:45
Dibromochloromethane ug/L ND 0.50 04/05/22 11:45
Dibromomethane ug/L ND 0.50 04/05/22 11:45
Dichlorodifluoromethane ug/L ND 0.50 IH04/05/22 11:45
Diisopropyl ether ug/L ND 0.50 04/05/22 11:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3602443
Associated Lab Samples:92596442004, 92596442005
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/05/22 11:45
Hexachloro-1,3-butadiene ug/L ND 2.0 04/05/22 11:45
Isopropylbenzene (Cumene)ug/L ND 0.50 04/05/22 11:45
m&p-Xylene ug/L ND 1.0 04/05/22 11:45
Methyl-tert-butyl ether ug/L ND 0.50 04/05/22 11:45
Methylene Chloride ug/L ND 2.0 04/05/22 11:45
n-Butylbenzene ug/L ND 0.50 04/05/22 11:45
n-Propylbenzene ug/L ND 0.50 04/05/22 11:45
Naphthalene ug/L ND 2.0 04/05/22 11:45
o-Xylene ug/L ND 0.50 04/05/22 11:45
sec-Butylbenzene ug/L ND 0.50 04/05/22 11:45
Styrene ug/L ND 0.50 04/05/22 11:45
tert-Butylbenzene ug/L ND 0.50 04/05/22 11:45
Tetrachloroethene ug/L ND 0.50 04/05/22 11:45
Toluene ug/L ND 0.50 04/05/22 11:45
trans-1,2-Dichloroethene ug/L ND 0.50 04/05/22 11:45
trans-1,3-Dichloropropene ug/L ND 0.50 04/05/22 11:45
Trichloroethene ug/L ND 0.50 04/05/22 11:45
Trichlorofluoromethane ug/L ND 1.0 04/05/22 11:45
Vinyl chloride ug/L ND 1.0 04/05/22 11:45
1,2-Dichloroethane-d4 (S)%108 70-130 04/05/22 11:45
4-Bromofluorobenzene (S)%106 70-130 04/05/22 11:45
Toluene-d8 (S)%98 70-130 04/05/22 11:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3602444LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.550 111 60-140
1,1,1-Trichloroethane ug/L 55.650 111 60-140
1,1,2,2-Tetrachloroethane ug/L 51.950 104 60-140
1,1,2-Trichloroethane ug/L 52.550 105 60-140
1,1-Dichloroethane ug/L 50.350 101 60-140
1,1-Dichloroethene ug/L 55.250 110 60-140
1,1-Dichloropropene ug/L 53.850 108 60-140
1,2,3-Trichlorobenzene ug/L 55.750 111 60-140
1,2,3-Trichloropropane ug/L 49.850 100 60-140
1,2,4-Trichlorobenzene ug/L 60.350 121 60-140
1,2,4-Trimethylbenzene ug/L 55.650 111 60-140
1,2-Dibromo-3-chloropropane ug/L 57.350 115 60-140
1,2-Dibromoethane (EDB)ug/L 54.150 108 60-140
1,2-Dichlorobenzene ug/L 55.350 111 60-140
1,2-Dichloroethane ug/L 51.850 104 60-140
1,2-Dichloropropane ug/L 54.150 108 60-140
1,3,5-Trimethylbenzene ug/L 56.850 114 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3602444LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 57.750 115 60-140
1,3-Dichloropropane ug/L 50.850 102 60-140
1,4-Dichlorobenzene ug/L 55.050 110 60-140
2,2-Dichloropropane ug/L 59.750 119 60-140
2-Chlorotoluene ug/L 56.750 113 60-140
4-Chlorotoluene ug/L 56.450 113 60-140
Benzene ug/L 47.150 94 60-140
Bromobenzene ug/L 53.650 107 60-140
Bromochloromethane ug/L 43.850 88 60-140
Bromodichloromethane ug/L 57.450 115 60-140
Bromoform ug/L 54.650 109 60-140
Bromomethane ug/L 50.550 101 60-140
Carbon tetrachloride ug/L 70.4 L15014160-140
Chlorobenzene ug/L 52.650 105 60-140
Chloroethane ug/L 59.650 119 60-140
Chloroform ug/L 51.950 104 60-140
Chloromethane ug/L 59.250 118 60-140
cis-1,2-Dichloroethene ug/L 51.150 102 60-140
cis-1,3-Dichloropropene ug/L 55.250 110 60-140
Dibromochloromethane ug/L 58.350 117 60-140
Dibromomethane ug/L 57.550 115 60-140
Dichlorodifluoromethane ug/L 109 IH,L15021860-140
Diisopropyl ether ug/L 51.650 103 60-140
Ethylbenzene ug/L 51.750 103 60-140
Hexachloro-1,3-butadiene ug/L 64.650 129 60-140
Isopropylbenzene (Cumene)ug/L 52.050 104 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 54.450 109 60-140
Methylene Chloride ug/L 54.950 110 60-140
n-Butylbenzene ug/L 60.650 121 60-140
n-Propylbenzene ug/L 56.350 113 60-140
Naphthalene ug/L 57.650 115 60-140
o-Xylene ug/L 53.350 107 60-140
sec-Butylbenzene ug/L 58.450 117 60-140
Styrene ug/L 53.050 106 60-140
tert-Butylbenzene ug/L 50.050 100 60-140
Tetrachloroethene ug/L 54.150 108 60-140
Toluene ug/L 49.750 99 60-140
trans-1,2-Dichloroethene ug/L 51.950 104 60-140
trans-1,3-Dichloropropene ug/L 56.150 112 60-140
Trichloroethene ug/L 54.850 110 60-140
Trichlorofluoromethane ug/L 56.850 114 60-140
Vinyl chloride ug/L 61.150 122 60-140
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
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[phone]
Page 41 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3602445MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596748028
3602446
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 108 60-140118 92000ND21602360
1,1,1-Trichloroethane ug/L 2000 114 60-140122 72000ND22802440
1,1,2,2-Tetrachloroethane ug/L 2000 102 60-140110 82000ND20402210
1,1,2-Trichloroethane ug/L 2000 104 60-140112 72000ND20802230
1,1-Dichloroethane ug/L 2000 103 60-140109 62000ND20602180
1,1-Dichloroethene ug/L 2000 115 60-140119 42000ND23002380
1,1-Dichloropropene ug/L 2000 111 60-140114 32000ND22302290
1,2,3-Trichlorobenzene ug/L 2000 101 60-140113 112000ND20102250
1,2,3-Trichloropropane ug/L 2000 102 60-140114 122000ND20302290
1,2,4-Trichlorobenzene ug/L 2000 109 60-140111 22000ND21702210
1,2,4-Trimethylbenzene ug/L 2000 104 60-140115 62000131033803600
1,2-Dibromo-3-chloropropane ug/L 2000 100 60-140100 02000ND20102010
1,2-Dibromoethane (EDB)ug/L 2000 107 60-140124 152000ND21402480
1,2-Dichlorobenzene ug/L 2000 106 60-140110 42000ND21102200
1,2-Dichloroethane ug/L 2000 108 60-140110 12000ND21702190
1,2-Dichloropropane ug/L 2000 108 60-140111 22000ND21702210
1,3,5-Trimethylbenzene ug/L 2000 107 60-140113 5200027524202530
1,3-Dichlorobenzene ug/L 2000 106 60-140109 22000ND21302180
1,3-Dichloropropane ug/L 2000 104 60-140115 92000ND20902290
1,4-Dichlorobenzene ug/L 2000 102 60-140105 32000ND20402090
2,2-Dichloropropane ug/L 2000 100 60-140109 92000ND20102190
2-Chlorotoluene ug/L 2000 109 60-140110 12000ND21702200
4-Chlorotoluene ug/L 2000 108 60-140110 22000ND21602210
Benzene ug/L 2000 83 60-140136 1020008340999011100
Bromobenzene ug/L 2000 105 60-140114 92000ND21002290
Bromochloromethane ug/L 2000 92 60-14097 62000ND18401950
Bromodichloromethane ug/L 2000 112 60-140122 92000ND22402440
Bromoform ug/L 2000 97 60-140108 112000ND19302160
Bromomethane ug/L 2000 76 60-14089 162000ND15201780
Carbon tetrachloride ug/L M0200014060-140142 22000ND27902840
Chlorobenzene ug/L 2000 106 60-140114 82000ND21102280
Chloroethane ug/L 2000 124 60-140124 02000ND24702470
Chloroform ug/L 2000 110 60-140110 12000ND22102190
Chloromethane ug/L 2000 111 60-140118 62000ND22302360
cis-1,2-Dichloroethene ug/L 2000 105 60-140110 42000ND21002190
cis-1,3-Dichloropropene ug/L 2000 110 60-140117 72000ND21902340
Dibromochloromethane ug/L 2000 113 60-140122 72000ND22602440
Dibromomethane ug/L 2000 117 60-140117 12000ND23502330
Dichlorodifluoromethane ug/L IH,M0200019360-140184 52000ND38603670
Diisopropyl ether ug/L 2000 106 60-140110 4200058.4 2180 2260
Ethylbenzene ug/L 2000 106 60-140122 92000147035803910
Hexachloro-1,3-butadiene ug/L 2000 115 60-140125 92000ND23002510
Isopropylbenzene (Cumene)ug/L 2000 106 60-140117 9200069.4 2190 2400
m&p-Xylene ug/L 4000 105 60-140126 114000281070107840
Methyl-tert-butyl ether ug/L 2000 113 60-140123 7200054428103010
Methylene Chloride ug/L 2000 114 60-140117 2200048027702820
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
Page 42 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3602445MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596748028
3602446
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 2000 114 60-140118 32000ND23202400
n-Propylbenzene ug/L 2000 107 60-140113 5200011222502380
Naphthalene ug/L 2000 99 60-140110 9200035323402560
o-Xylene ug/L 2000 107 60-140121 9200084429903260
sec-Butylbenzene ug/L 2000 110 60-140120 92000ND22002410
Styrene ug/L 2000 101 60-140110 82000ND20202190
tert-Butylbenzene ug/L 2000 97 60-140101 42000ND19502030
Tetrachloroethene ug/L 2000 108 60-140115 62000ND21602290
Toluene ug/L 2000 103 60-140118 82000155036103920
trans-1,2-Dichloroethene ug/L 2000 108 60-140116 72000ND21602320
trans-1,3-Dichloropropene ug/L 2000 101 60-140110 92000ND20202210
Trichloroethene ug/L 2000 111 60-140111 0200012723502350
Trichlorofluoromethane ug/L 2000 113 60-140123 82000ND22602450
Vinyl chloride ug/L 2000 117 60-140128 82000ND23502550
1,2-Dichloroethane-d4 (S)%105 70-130108
4-Bromofluorobenzene (S)%103 70-130103
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/06/2022 10:32 AM
Pace Analytical Services, LLC
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[phone]
Page 43 of 48
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92596442
The Spot
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92596442
The Spot
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92596442001 688853MW-1 SM 6200B
92596442002 689213MW-2 SM 6200B
92596442003 689213MW-3 SM 6200B
92596442004 689413MW-4 SM 6200B
92596442005 689413MW-5 SM 6200B
92596442006 688913MW-6 SM 6200B
92596442007 688913MW-7 SM 6200B
92596442008 688913MW-8 SM 6200B
92596442009 688913WSW-1 SM 6200B
92596442010 688913WSW-2 SM 6200B
REPORT OF LABORATORY ANALYSIS
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Page 45 of 48
Page 46 of 48
Page 47 of 48
Page 48 of 48
MARCH 2022 - GROUNDWATER
MONITORING REPORT with
AFVR

For The
THE SPOT
2267 Smokey Park Highway Candler, North Carolina 28715

UST Incident # 28826

April 29, 2022
Singleton Environmental, Inc. Project No. SEI-1226

Singleton Environmental, Inc
Groundwater Monitoring Report with AFVR The Spot - Candler Candler, North Carolina

GROUNDWATER MONITORING REPORT with AFVR
April 29, 2022 Incident Number: 28826 Facility ID Number: 00-0-00004683 Site Name: The Spot 2267 Smokey Park Highway
Candler, NC 28705
Incident Number: 28826 Facility ID Number: 0-004683 UST Owner / Operator: Theodossis Business, LLC
Contact: Jimmy Theodossis 1100 McMinn Road Hendersonville, NC 28792 Telephone: [phone]
Consultant / Contractor: Singleton Environmental, Inc. PO Box 2012 Enka, NC 28728 Telephone: [phone]
Date Release Discovered: March 15, 2010 Estimated Quantity of Release: Unknown/unquantified Cause/Source of Release: Two 3,000-Gallon Gasoline USTs, One 6,000-Gallon
Gasoline UST, and One 3,000-Gallon Diesel UST.
Latitude: (35° 32’ 33.14” North)
Longitude: (82° 44’ 45.11” West) Signature and Seal of Certifying Professional Engineer: I, Christopher D. Singleton, a North Carolina Professional Geologist, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
____________________________________ Christopher D. Singleton, P.G. #1928
Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The
certification number of the company is C-443.
Groundwater Monitoring Report with AFVR The Spot - Candler Candler, North Carolina

Table of Contents
Introduction ................................................................................................................................1 Site History and Source Characterization…......................…………......................................... .....1
Summary of USTs …......................………….........................................................................1 Source of Release…......................…………...........................................................................1 Summary of Assessment Activities and Corrective Actions……......................................... ...1 Receptor Information…......................…………......................................... ..................................2
Site Geology and Hydrogeology…......................…………......................................... ..................2
AFVR Activities…......................…………...................................................................................2 Groundwater Sampling Activities…......................…………......................................... ................3 Free Product Removal …......................…………......................................... ................................4 Conclusions and Recommendations…..................…………......................................... ................4 Tables Table 1. Groundwater Levels Table 2. Groundwater Analytical Results
Table 3. AFVR Report Figures Figure 1. Site Vicinity Map
Figure 2. Site Map Figure 3. Groundwater Elevation Contour Map Figure 4. Groundwater Sampling Locations with MCLs and GCLs Appendices

Appendix A: Disposal Manifest Appendix B: Laboratory Analytical Report

Introduction

This report presents the results of the Groundwater Monitoring and AFVR event completed in March 2022 to evaluate the remedial progress of the groundwater contamination related to a petroleum release from the former underground storage tank (UST) system at The Spot, located at 2267 Smokey Park Hwy in Candler, North Carolina. Figure 1 shows the site location, and
Figure 2 presents a site map showing the location of the current UST system, monitoring wells, and soil sampling locations. Site History and Source Characterization
The following table summarizes information about the USTs at the site:

Tank No. Volume (gallons)
Contents (i.e., gasoline, diesel, kerosene, heating oil, waste oil, etc.)
Use (resale, heating building, distribution, farm or residential, etc.)
Date last used
Indicate whether UST has been removed or closed in place
Date of permanent closure (if applicable)
Was a release detected from this UST system? If yes, give date.
1 6,000 Gasoline Resale 3/15/10 Removed 3/15/10 Yes
2 3,000 Gasoline Resale 3/15/10 Removed 3/15/10 Yes
3 3,000 Gasoline Resale 3/15/10 Removed 3/15/10 Yes
4 3,000 Diesel Resale 3/15/10 Removed 3/15/10 Yes

Ownership of Tank: Theodossis Business, LLC Contact: Jimmy Theodossis 2267 Smokey Park Highway Candler, NC 28705
Telephone: [phone]
Source of Release
The source of the release is the former UST system removed in March 2010. The UST system
was used as a petroleum retail station. There are no other on-site or off-site petroleum or non-petroleum sources that are suspected to be contributing to the release. A new UST system was installed in April 2010. Summary of Assessment Activities and Corrective Actions
The petroleum release at the Site was confirmed during UST Closure activities in March 2010, LSA activities in February 2013 and CSA activities in October 2016. To date, eight groundwater monitoring wells (MW-1 through MW-8) have been installed at the
Site. Dissolved phase petroleum compounds above the State 2L standards have been detected in

monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-5. To date no free product has been
observed at the site. Receptor Information Singleton Environmental, Inc. personnel completed a water supply well survey near the site in February 2013 by searching surrounding properties for wells and water meter connections and interviewing local residents. 22 water supply wells were located within 1,000 feet of the site.
The following bullets summarize other receptor information regarding this site:
• Public water supply is not available near the site.

• The site is not located in a wellhead protection area.
• 22 water supply wells are located within 1,000 feet from the source area. The property containing the release is zoned commercial. The surrounding properties contain commercial and residential development. Site Geology and Hydrogeology

According to the Geologic Map of North Carolina (1985), the local geology consists of Muscovite Biotite Schist. A soil boring log is included in Appendix B. On March 30, 2022, the average depth to groundwater was 21.26 ft-bls. Groundwater flows south from the source area.
AFVR Activities
On March 7, 2022, SEI conducted an aggressive fluid and vapor recovery (AFVR) event at the
site. Fluids and vapors were extracted from monitoring well MW-1. The event began at 8:00 a.m. and ended at 4:00 p.m. Stinger depths were initially set at 25 feet below land surface (ft-bls) and lowered to 30 ft-bls two hours into the event.
A photoionization detector (PID) was used to measure effluent vapors from the system. Vacuum
pressure was measured 38.0 inches of Hg throughout the event.
SEI measured stack velocity using an averaging Pitot tube installed across the two-inch liquid-ring pump vapor discharge stack to determine flow in actual cubic feet per minute (ACFM). Progress employed the following equation to convert ACFM to standard cubic feet per minute
(SCFM):
SCFM=ACFM(TSTP / TActual)( PActual /PSTP)
• TSTP - Standard temperature (68oF = 528oR)
• TActual - Actual temperature (stack conditions (0F) +460oR)
• PActual - Actual pressure (stack conditions - observed gauge value in inches of water)

• PSTP - Standard pressure (29.92 inches of Hg = 646 inches of water)
The average liquid ring pump (LRP) stack temperature measured for each recovery location was incorporated into the above equation to yield a correction factor applied to the data to calculate a mass removal in vapor-phase. A summary AFVR report including average stack temperature, average vacuum applied, airflow effluent data, and estimated total emissions (in pounds) for the
extraction location are presented in Table 3.

The fluids extracted from the wells were pumped into an on-site tanker truck. During the event SEI was able to evacuate approximately 171 gallons of contaminated groundwater. Based on total emission calculations performed by SEI the event removed approximately 78.18 pounds (or 10.27 gallons) of petroleum product as vapor from beneath the site. Just under two gallons of
product (1.6 gallons) were measured in the tank of the vacuum truck bringing the total gallons recovered to 11.87 gallons (90.33 pounds). The recovered fluids were transported off-site by Mountain Environmental Services for proper
disposal. The disposal manifest is in Appendix A.
Groundwater Sampling Activities
SEI was on site on March 30, 2022, to collect post-AFVR groundwater samples from the monitoring wells and water supply wells. Monitoring wells MW-1 through MW-8, and WSW-1 and WSW-2 were sampled as part of the sampling event. Prior to sampling, the monitoring wells
were purged of three volumes of water and allowed to recharge prior to sampling. And the water
supply wells were purged for approximately 20 minutes. The groundwater samples were collected into laboratory-supplied bottles and placed into a cooler packed with ice. The cooler was delivered under chain-of-custody to Pace Analytical in
Asheville, North Carolina for testing. Pace analyzed the groundwater samples for VOCs by Standard Method 6200B. A summary of the groundwater sample analytical results are included in Table 2.
• Laboratory analysis of the groundwater sample collected from monitoring wells WSW-1,
WSW-2, MW-6, MW-7, and MW-8 did not detect any compounds above the laboratory minimum detection limits.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-1
detected benzene, 1,2,4-trimethylbenzene, diisopropylether, ethylbenzene, MTBE, naphthalene, toluene, n-propylbenzene, and total xylenes at concentrations exceeding their respective NCAC 2L MCLS. The concentrations of benzene detected in the groundwater sample collected from monitoring well MW-1 exceeded the Gross Contamination Levels (GCLs).

• Laboratory analysis of the groundwater sample collected from monitoring well MW-2 detected benzene, MTBE, methylene chloride, and trichloroethene at concentrations their

respective NCAC 2L MCLs. None of the compounds exceeded the NCAC 2L GCLs, however, this is the first time trichloroethene has been detected at the site.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-3
detected benzene and methylene chloride at concentrations exceeding the NCAC 2L
MCLs. None of the compounds exceeded the NCAC 2L GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-4 detected benzene at concentrations exceeding the NCAC 2L MCLs. None of the compounds exceeded the NCAC 2L GCLs.
• Laboratory analysis of the groundwater sample collected from monitoring well MW-5
detected benzene, naphthalene, toluene, and total xylenes at concentrations exceeding
their respective NCAC 2L MCLS. None of the compounds exceeded the NCAC 2L
GCLs. The laboratory analytical reports for the groundwater samples are provided in Appendix B. The laboratory test results are summarized on Table 2. A map depicting the contaminant plume is
included on Figure 4.
Free Product Removal
Free product was not observed in the monitoring wells during this groundwater assessment, however, approximately 1.6 gallons of product was observed in the vacuum truck tank after the event. CONCLUSIONS
Based on the results of the groundwater sampling event, SEI makes the following conclusions:
• Laboratory analysis of the groundwater sample collected from monitoring wells WSW-1,
WSW-2, MW-6, MW-7, and MW-8 did not detect targeted compounds above their respective NCAC 2L MCLS.
• Laboratory analysis of the groundwater samples collected from monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-5 detected targeted compounds above their respective
NCAC 2L MCLS, and MW-1 still contains concentrations of benzene exceeded the NCAC 2L GCLs.
• Trichloroethen was detected at the site for the first time in MW-2.
Based on the remaining concentrations in select groundwater samples exceeding their respective
NCAC 2L MCLS and GCLs, SEI recommends the following:
• SEI recommends groundwater monitoring in July 2022 to confirm the migration of the contaminant plume.

TABLES
MW Number Top of Casing Elevation
Top of Casing
to GW Depth Groundwater Elevation
MW-1 97.67 21.81 75.86
MW-2 96.31 21.27 75.04
MW-3 94.42 19.83 74.59
MW-4 94.77 19.92 74.85
MW-5 97.02 20.70 76.32
MW-6 98.85 22.48 76.37
MW-7 100 21.34 78.66
MW-8 92.98 22.73 70.25
Table 1
Groundwater Flow Mapping Elevation Details
Candler, NC
The Spot 3/30/22
1,2,4-
Trimeth
ylbenze
ne
1,3,5-
Trimeth
ylbenze
ne
Benzene
Diisopro
pyl
ether
Ethylbe
nzene
Isoprop
ylbenze
ne
(Cumen
e)
Methyl-
tert-
butyl
ether
Methyl
ene Chlorid
e
Naphth
alene Toluene
Trichlor
oethene
m&p-
Xylene
n-
Propylb
enzene
o-
Xylene
Date
Collected
(mm/dd/yy)
Sample
Depth
(ft. BGS)
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
3/30/2022 1480 369 9380 404 2100 66.5 213 ND 519 8340 ND 5930 191 3340
12/20/2021 1190 293 6820 232 1540 45.5 120 ND 350 4780 ND 4000 154 2240
6/7/2021 3590 ND 9760 466 3060 135 308 ND 923 1100 ND 10300 ND 4880
2/17/2021 1860 ND 10600 447 2330 77 256 ND 599 9490 ND 6620 ND 3710
10/19/2020 2900 ND 10300 621 2760 117 329 217 779 12200 ND 9210 ND 4630
12/4/2019 3660 923 10400 612 3460 135 397 ND 792 14400 ND 12000 456 5700
04/16/2019 1860 447 12200 708 2650 76.7 373 ND 501 11700 ND 8160 230 4310
3/30/2022 ND ND 1460 34.1 ND 36.6 23.1 29.6 ND ND 17.6 ND ND 7.4
12/20/2021 ND ND 692 19.2 ND 9.9 12.9 ND 13.6 ND ND ND ND 10.6
6/7/2021 3.3 ND 564 12.5 ND 10.7 7.4 ND 17.8 ND ND ND ND 43.3
2/17/2021 3.2 ND 816 18 ND 9.7 10.9 ND 17.5 ND ND ND ND 36.9
10/19/2020 37.2 ND 435 13.4 9.3 6.8 11.4 11.2 36.1 4.8 ND 53 ND 144
12/4/2019 118 ND 778 26.1 12.6 5.7 28 ND 59.8 23.4 ND 183 ND 370
04/16/2019 106 25.7 759 29.0 29.0 7.6 29.7 ND 37.9 28.3 ND 226 6.1 288
3/30/2022 2.1 ND 320 11.9 2.4 ND 3.6 5.8 ND 5.7 ND 12.5 ND 5.7
12/20/2021 ND ND 339 14.5 1.5 ND 3.7 ND ND 6 ND 8 ND 3.3
6/7/2021 ND ND 211 8.6 1.7 ND 2.4 ND ND 7.6 ND 6.6 ND 2.1
2/17/2021 ND ND 154 6.1 1.3 ND ND ND ND 4 ND 4.3 ND 1.5
10/19/2020 ND ND 49.3 3 0.55 ND ND ND ND 2.6 ND 1.8 ND 0.65
12/4/2019 ND ND ND 0.63 ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND 17.6 ND 0.61 ND ND ND ND 3.5 ND 2.6 ND 0.99
12/20/2021 1150 228 138 ND 1820 ND ND ND 369 12300 ND 6340 104 3330
2/17/2021 ND ND 7.7 ND ND ND ND ND ND 2 ND ND ND ND
10/19/2020 ND ND 0.58 ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND 0.84 ND ND ND ND ND ND ND ND ND ND ND
Table # 2
Summary of Analytical Results - Water Samples
THE SPOT - CANDLER
NCDEQ's Incident # 28826
Analytical Method
Sample ID
Constituent of Concern
MW-1
MW-2
MW-3
MW-4
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 379 58.3 19.7 ND 269 19.2 ND ND 89.1 1330 ND 1020 26.3 639
12/20/2021 1150 ND 138 ND 1820 ND ND ND 369 12300 ND 6340 104 3330
6/7/2021 410 ND 58.8 ND 296 18.4 ND ND 113 2070 ND 1360 ND 850
2/17/2021 458 ND 108 ND 551 22 ND ND 156 3310 ND 1880 ND 1150
10/19/2020 900 ND 323 ND 1050 40 ND 126 307 7630 ND 3700 ND 2120
12/4/2019 802 184 1030 ND 1170 36.1 ND ND 253 8950 ND 4300 86.2 2200
04/16/2019 653 207 596 ND 797 30.5 ND ND 180 3000 ND 2870 80.8 1410
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND 0.59 ND ND 0.75 ND ND ND ND ND ND ND
2/17/2021 ND ND ND 2 ND ND 1.9 ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2020 ND ND ND 1.9 ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/4/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/30/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/20/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/7/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/17/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/19/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
MW-5
MW-6
MW-7
MW-8
WSW-1
WSW-2
12/4/2019 NA NA NA NA NA NA NA NA NA NA ND NA NA NA
04/16/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
400 400 1 70 600 70 20 5 6 600 3 500 70 500
28500 25000 5000 70000 84500 25000 20000 5000 6000 260000 3000 85500 30000 85500
2L Class GA Standards
ft. BGS = feet below ground surface
mg/L = milligrams per liter
ug/L = micrograms per liter
Bold data above the MSCC (Soil to Groundwater)
2L Class GCL Standards
NOTES:
ND = Not Detected
Elapsed
Time
(min)
Flow
(DSCFM)
PPM Measured
(ppm)
K
(#C-gas)PPMg
Cc:m
(mg/dsm^3)
Cc
(lb/dscf)
PMRc
(lb/hr)
PMRg
(lb/hour)
PMR
(lb)
1 4239.0 500 4 2,000 1064 0.00007 16.888 19.544 19.219
60 6864.0 154 4 616 328 0.00002 8.422 9.747 9.747
120 4698.0 161 4 644 342 0.00002 6.027 6.975 23.249
320 5690.0 138 4 552 294 0.00002 6.256 7.241 19.308
480 5820.0 124 4 496 264 0.00002 5.750 6.655 6.655
540 TOTAL EMISSIONS IN POUNDS 78.178
Calculations
PPMw = “wet” concentration
PPMd = “dry” concentration
PPMc = PPMv, volumetric concentration of VOC emissions as carbon, dry basis, at STP
Cc:m
Cc = Cc:m (62.43 x 10-9 lb-m3/mg-ft3), lb/dscf, mass concentration of VOC emissions as carbon, dry basis, at STP
PMRc = Cc (Qstd) (60 min/hr), lb/hr, pollutant mass removal rate of VOC’s as carbon
PMRg = (PMRc) (Mg/Mcg), lb/hr, pollutant mass removal rate of VOC’s as gasoline
K = number of carbons in calibration gas (methane K=1, propane K=3, hexane K=6)
Mc = 12.01 mg/mg-mole, molecular wt. of carbon
K3 = 24.07 dsm3/106 mg-mole, mass to volume conversion factor at STP
Cc = lb/dscf, mass concentration of VOC emissions as carbon, dry basis, at STP
Mg = 103 mg/mg-mole, molecular wt. of gasoline (value may vary depending on contaminant)
Mcg = 89 mg/mg-mole, weight of carbon in gasoline molecule
Average values for molecular weight of gasoline, weight of carbon in gasoline molecule, and the conversion of pounds of gasoline emissions to gallons
of liquid gasoline are from Automotive Fuels Reference Book, by K. Owens and T. Coley, Second Edition, 1995, published by the Society
of Automotive Engineers.
The Spot - Candler
NOTE: To convert lbs. of gasoline emissions to gallons of liquid gasoline, divide by 6.25 lbs/gal.
= PPMc (Mc/K3)
TABLE 3
AFVR RESULTS

FIGURES
ASHEVILLE QUADRANGLE NORTH CAROLINA 7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1 Site Map
The Spot – Candler, NC
THE SPOT
Singleton Environmental, Inc
Singleton Environmental, Inc
Singleton Environmental, Inc

APPENDIX A

AFVR Disposal Manifest

APPENDIX B
Laboratory Analytical Report
#=CL#
April 27, 2022
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92596442
92596442
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
The Spot
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
Revised Report. Multiple mis-labeled samples were discovered, leading to corrections with this data.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92596442
The Spot
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92596442
The Spot
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92596442001 MW-1 SM 6200B 63 PASI-CSAS
92596442002 MW-2 SM 6200B 63 PASI-CSAS
92596442003 MW-3 SM 6200B 63 PASI-CSAS
92596442004 MW-4 SM 6200B 63 PASI-CSAS
92596442005 MW-5 SM 6200B 63 PASI-CSAS
92596442006 MW-6 SM 6200B 63 PASI-CSAS
92596442007 MW-7 SM 6200B 63 PASI-CSAS
92596442008 MW-8 SM 6200B 63 PASI-CSAS
92596442009 WSW-1 SM 6200B 63 PASI-CSAS
92596442010 WSW-2 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-1 Lab ID:92596442001 Collected:03/30/22 16:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 9380 ug/L 04/01/22 18:24 71-43-2 M125.0 50
Bromobenzene ND ug/L 04/01/22 18:24 108-86-125.0 50
Bromochloromethane ND ug/L 04/01/22 18:24 74-97-525.0 50
Bromodichloromethane ND ug/L 04/01/22 18:24 75-27-425.0 50
Bromoform ND ug/L 04/01/22 18:24 75-25-225.0 50
Bromomethane ND ug/L 04/01/22 18:24 74-83-925050
n-Butylbenzene ND ug/L 04/01/22 18:24 104-51-825.0 50
sec-Butylbenzene ND ug/L 04/01/22 18:24 135-98-825.0 50
tert-Butylbenzene ND ug/L 04/01/22 18:24 98-06-625.0 50
Carbon tetrachloride ND ug/L 04/01/22 18:24 56-23-5 M125.0 50
Chlorobenzene ND ug/L 04/01/22 18:24 108-90-725.0 50
Chloroethane ND ug/L 04/01/22 18:24 75-00-350.0 50
Chloroform ND ug/L 04/01/22 18:24 67-66-325.0 50
Chloromethane ND ug/L 04/01/22 18:24 74-87-350.0 50
2-Chlorotoluene ND ug/L 04/01/22 18:24 95-49-825.0 50
4-Chlorotoluene ND ug/L 04/01/22 18:24 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 18:24 96-12-850.0 50
Dibromochloromethane ND ug/L 04/01/22 18:24 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 18:24 106-93-425.0 50
Dibromomethane ND ug/L 04/01/22 18:24 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 04/01/22 18:24 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 04/01/22 18:24 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 04/01/22 18:24 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 04/01/22 18:24 75-71-8 IH,L1,M025.0 50
1,1-Dichloroethane ND ug/L 04/01/22 18:24 75-34-325.0 50
1,2-Dichloroethane ND ug/L 04/01/22 18:24 107-06-225.0 50
1,1-Dichloroethene ND ug/L 04/01/22 18:24 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 04/01/22 18:24 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 04/01/22 18:24 156-60-525.0 50
1,2-Dichloropropane ND ug/L 04/01/22 18:24 78-87-525.0 50
1,3-Dichloropropane ND ug/L 04/01/22 18:24 142-28-925.0 50
2,2-Dichloropropane ND ug/L 04/01/22 18:24 594-20-725.0 50
1,1-Dichloropropene ND ug/L 04/01/22 18:24 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 04/01/22 18:24 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 04/01/22 18:24 10061-02-625.0 50
Diisopropyl ether 404 ug/L 04/01/22 18:24 108-20-325.0 50
Ethylbenzene 2100 ug/L 04/01/22 18:24 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 04/01/22 18:24 87-68-310050
Isopropylbenzene (Cumene)66.5 ug/L 04/01/22 18:24 98-82-825.0 50
Methylene Chloride ND ug/L 04/01/22 18:24 75-09-210050
Methyl-tert-butyl ether 213 ug/L 04/01/22 18:24 1634-04-425.0 50
Naphthalene 519 ug/L 04/01/22 18:24 91-20-310050
n-Propylbenzene 191 ug/L 04/01/22 18:24 103-65-125.0 50
Styrene ND ug/L 04/01/22 18:24 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 18:24 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 18:24 79-34-525.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-1 Lab ID:92596442001 Collected:03/30/22 16:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 18:24 127-18-425.0 50
Toluene 8340 ug/L 04/01/22 18:24 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 04/01/22 18:24 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 04/01/22 18:24 120-82-110050
1,1,1-Trichloroethane ND ug/L 04/01/22 18:24 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 04/01/22 18:24 79-00-525.0 50
Trichloroethene ND ug/L 04/01/22 18:24 79-01-625.0 50
Trichlorofluoromethane ND ug/L 04/01/22 18:24 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 04/01/22 18:24 96-18-425.0 50
1,2,4-Trimethylbenzene 1480 ug/L 04/01/22 18:24 95-63-625.0 50
1,3,5-Trimethylbenzene 369 ug/L 04/01/22 18:24 108-67-825.0 50
Vinyl chloride ND ug/L 04/01/22 18:24 75-01-450.0 50
m&p-Xylene 5930 ug/L 04/01/22 18:24 179601-23-150.0 50
o-Xylene 3340 ug/L 04/01/22 18:24 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)103 %04/01/22 18:24 17060-07-070-130 50
4-Bromofluorobenzene (S)103 %04/01/22 18:24 460-00-470-130 50
Toluene-d8 (S)99 %04/01/22 18:24 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-2 Lab ID:92596442002 Collected:03/30/22 15:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1460 ug/L 04/05/22 03:37 71-43-26.2 12.5
Bromobenzene ND ug/L 04/05/22 03:37 108-86-16.2 12.5
Bromochloromethane ND ug/L 04/05/22 03:37 74-97-56.2 12.5
Bromodichloromethane ND ug/L 04/05/22 03:37 75-27-46.2 12.5
Bromoform ND ug/L 04/05/22 03:37 75-25-26.2 12.5
Bromomethane ND ug/L 04/05/22 03:37 74-83-962.5 12.5
n-Butylbenzene 6.6 ug/L 04/05/22 03:37 104-51-86.2 12.5
sec-Butylbenzene 7.4 ug/L 04/05/22 03:37 135-98-86.2 12.5
tert-Butylbenzene ND ug/L 04/05/22 03:37 98-06-66.2 12.5
Carbon tetrachloride ND ug/L 04/05/22 03:37 56-23-56.2 12.5
Chlorobenzene ND ug/L 04/05/22 03:37 108-90-76.2 12.5
Chloroethane ND ug/L 04/05/22 03:37 75-00-312.5 12.5
Chloroform 6.4 ug/L 04/05/22 03:37 67-66-36.2 12.5
Chloromethane ND ug/L 04/05/22 03:37 74-87-312.5 12.5
2-Chlorotoluene ND ug/L 04/05/22 03:37 95-49-86.2 12.5
4-Chlorotoluene ND ug/L 04/05/22 03:37 106-43-46.2 12.5
1,2-Dibromo-3-chloropropane ND ug/L 04/05/22 03:37 96-12-812.5 12.5
Dibromochloromethane ND ug/L 04/05/22 03:37 124-48-16.2 12.5
1,2-Dibromoethane (EDB)ND ug/L 04/05/22 03:37 106-93-46.2 12.5
Dibromomethane ND ug/L 04/05/22 03:37 74-95-36.2 12.5
1,2-Dichlorobenzene ND ug/L 04/05/22 03:37 95-50-16.2 12.5
1,3-Dichlorobenzene ND ug/L 04/05/22 03:37 541-73-16.2 12.5
1,4-Dichlorobenzene ND ug/L 04/05/22 03:37 106-46-76.2 12.5
Dichlorodifluoromethane ND ug/L 04/05/22 03:37 75-71-8 L16.2 12.5
1,1-Dichloroethane ND ug/L 04/05/22 03:37 75-34-36.2 12.5
1,2-Dichloroethane ND ug/L 04/05/22 03:37 107-06-26.2 12.5
1,1-Dichloroethene ND ug/L 04/05/22 03:37 75-35-46.2 12.5
cis-1,2-Dichloroethene ND ug/L 04/05/22 03:37 156-59-26.2 12.5
trans-1,2-Dichloroethene ND ug/L 04/05/22 03:37 156-60-56.2 12.5
1,2-Dichloropropane ND ug/L 04/05/22 03:37 78-87-56.2 12.5
1,3-Dichloropropane ND ug/L 04/05/22 03:37 142-28-96.2 12.5
2,2-Dichloropropane ND ug/L 04/05/22 03:37 594-20-76.2 12.5
1,1-Dichloropropene ND ug/L 04/05/22 03:37 563-58-66.2 12.5
cis-1,3-Dichloropropene ND ug/L 04/05/22 03:37 10061-01-56.2 12.5
trans-1,3-Dichloropropene ND ug/L 04/05/22 03:37 10061-02-66.2 12.5
Diisopropyl ether 34.1 ug/L 04/05/22 03:37 108-20-36.2 12.5
Ethylbenzene ND ug/L 04/05/22 03:37 100-41-46.2 12.5
Hexachloro-1,3-butadiene ND ug/L 04/05/22 03:37 87-68-325.0 12.5
Isopropylbenzene (Cumene)36.6 ug/L 04/05/22 03:37 98-82-86.2 12.5
Methylene Chloride 29.6 ug/L 04/05/22 03:37 75-09-225.0 12.5
Methyl-tert-butyl ether 23.1 ug/L 04/05/22 03:37 1634-04-46.2 12.5
Naphthalene ND ug/L 04/05/22 03:37 91-20-325.0 12.5
n-Propylbenzene ND ug/L 04/05/22 03:37 103-65-16.2 12.5
Styrene ND ug/L 04/05/22 03:37 100-42-56.2 12.5
1,1,1,2-Tetrachloroethane ND ug/L 04/05/22 03:37 630-20-66.2 12.5
1,1,2,2-Tetrachloroethane ND ug/L 04/05/22 03:37 79-34-56.2 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-2 Lab ID:92596442002 Collected:03/30/22 15:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/05/22 03:37 127-18-46.2 12.5
Toluene ND ug/L 04/05/22 03:37 108-88-36.2 12.5
1,2,3-Trichlorobenzene ND ug/L 04/05/22 03:37 87-61-625.0 12.5
1,2,4-Trichlorobenzene ND ug/L 04/05/22 03:37 120-82-125.0 12.5
1,1,1-Trichloroethane ND ug/L 04/05/22 03:37 71-55-66.2 12.5
1,1,2-Trichloroethane ND ug/L 04/05/22 03:37 79-00-56.2 12.5
Trichloroethene 17.6 ug/L 04/05/22 03:37 79-01-66.2 12.5
Trichlorofluoromethane ND ug/L 04/05/22 03:37 75-69-412.5 12.5
1,2,3-Trichloropropane ND ug/L 04/05/22 03:37 96-18-46.2 12.5
1,2,4-Trimethylbenzene ND ug/L 04/05/22 03:37 95-63-66.2 12.5
1,3,5-Trimethylbenzene ND ug/L 04/05/22 03:37 108-67-86.2 12.5
Vinyl chloride ND ug/L 04/05/22 03:37 75-01-412.5 12.5
m&p-Xylene ND ug/L 04/05/22 03:37 179601-23-112.5 12.5
o-Xylene 7.4 ug/L 04/05/22 03:37 95-47-66.2 12.5
Surrogates
1,2-Dichloroethane-d4 (S)112 %04/05/22 03:37 17060-07-070-130 12.5
4-Bromofluorobenzene (S)107 %04/05/22 03:37 460-00-470-130 12.5
Toluene-d8 (S)102 %04/05/22 03:37 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-3 Lab ID:92596442003 Collected:03/30/22 14:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 320 ug/L 04/05/22 03:19 71-43-21.2 2.5
Bromobenzene ND ug/L 04/05/22 03:19 108-86-11.2 2.5
Bromochloromethane ND ug/L 04/05/22 03:19 74-97-51.2 2.5
Bromodichloromethane ND ug/L 04/05/22 03:19 75-27-41.2 2.5
Bromoform ND ug/L 04/05/22 03:19 75-25-21.2 2.5
Bromomethane ND ug/L 04/05/22 03:19 74-83-912.5 2.5
n-Butylbenzene ND ug/L 04/05/22 03:19 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 04/05/22 03:19 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 04/05/22 03:19 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 04/05/22 03:19 56-23-51.2 2.5
Chlorobenzene ND ug/L 04/05/22 03:19 108-90-71.2 2.5
Chloroethane ND ug/L 04/05/22 03:19 75-00-32.5 2.5
Chloroform ND ug/L 04/05/22 03:19 67-66-31.2 2.5
Chloromethane ND ug/L 04/05/22 03:19 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 04/05/22 03:19 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 04/05/22 03:19 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 04/05/22 03:19 96-12-82.5 2.5
Dibromochloromethane ND ug/L 04/05/22 03:19 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 04/05/22 03:19 106-93-41.2 2.5
Dibromomethane ND ug/L 04/05/22 03:19 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 04/05/22 03:19 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 04/05/22 03:19 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 04/05/22 03:19 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 04/05/22 03:19 75-71-8 L11.2 2.5
1,1-Dichloroethane ND ug/L 04/05/22 03:19 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 04/05/22 03:19 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 04/05/22 03:19 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 04/05/22 03:19 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 04/05/22 03:19 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 04/05/22 03:19 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 04/05/22 03:19 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 04/05/22 03:19 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 04/05/22 03:19 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 04/05/22 03:19 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 04/05/22 03:19 10061-02-61.2 2.5
Diisopropyl ether 11.9 ug/L 04/05/22 03:19 108-20-31.2 2.5
Ethylbenzene 2.4 ug/L 04/05/22 03:19 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 04/05/22 03:19 87-68-35.0 2.5
Isopropylbenzene (Cumene)ND ug/L 04/05/22 03:19 98-82-81.2 2.5
Methylene Chloride 5.8 ug/L 04/05/22 03:19 75-09-25.0 2.5
Methyl-tert-butyl ether 3.6 ug/L 04/05/22 03:19 1634-04-41.2 2.5
Naphthalene ND ug/L 04/05/22 03:19 91-20-35.0 2.5
n-Propylbenzene ND ug/L 04/05/22 03:19 103-65-11.2 2.5
Styrene ND ug/L 04/05/22 03:19 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 04/05/22 03:19 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 04/05/22 03:19 79-34-51.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-3 Lab ID:92596442003 Collected:03/30/22 14:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/05/22 03:19 127-18-41.2 2.5
Toluene 5.7 ug/L 04/05/22 03:19 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 04/05/22 03:19 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 04/05/22 03:19 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 04/05/22 03:19 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 04/05/22 03:19 79-00-51.2 2.5
Trichloroethene ND ug/L 04/05/22 03:19 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 04/05/22 03:19 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 04/05/22 03:19 96-18-41.2 2.5
1,2,4-Trimethylbenzene 2.1 ug/L 04/05/22 03:19 95-63-61.2 2.5
1,3,5-Trimethylbenzene ND ug/L 04/05/22 03:19 108-67-81.2 2.5
Vinyl chloride ND ug/L 04/05/22 03:19 75-01-42.5 2.5
m&p-Xylene 12.5 ug/L 04/05/22 03:19 179601-23-12.5 2.5
o-Xylene 5.7 ug/L 04/05/22 03:19 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)108 %04/05/22 03:19 17060-07-070-130 2.5
4-Bromofluorobenzene (S)102 %04/05/22 03:19 460-00-470-130 2.5
Toluene-d8 (S)100 %04/05/22 03:19 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-4 Lab ID:92596442004 Collected:03/30/22 14:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 17.6 ug/L 04/04/22 22:12 71-43-20.50 1
Bromobenzene ND ug/L 04/04/22 22:12 108-86-10.50 1
Bromochloromethane ND ug/L 04/04/22 22:12 74-97-50.50 1
Bromodichloromethane ND ug/L 04/04/22 22:12 75-27-40.50 1
Bromoform ND ug/L 04/04/22 22:12 75-25-20.50 1
Bromomethane ND ug/L 04/04/22 22:12 74-83-95.0 1
n-Butylbenzene ND ug/L 04/04/22 22:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/04/22 22:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/04/22 22:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/04/22 22:12 56-23-50.50 1
Chlorobenzene ND ug/L 04/04/22 22:12 108-90-70.50 1
Chloroethane ND ug/L 04/04/22 22:12 75-00-31.0 1
Chloroform ND ug/L 04/04/22 22:12 67-66-30.50 1
Chloromethane ND ug/L 04/04/22 22:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/04/22 22:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/04/22 22:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/04/22 22:12 96-12-81.0 1
Dibromochloromethane ND ug/L 04/04/22 22:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/04/22 22:12 106-93-40.50 1
Dibromomethane ND ug/L 04/04/22 22:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/04/22 22:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/04/22 22:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/04/22 22:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/04/22 22:12 75-71-8 L10.50 1
1,1-Dichloroethane ND ug/L 04/04/22 22:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/04/22 22:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/04/22 22:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/04/22 22:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/04/22 22:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/04/22 22:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/04/22 22:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/04/22 22:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/04/22 22:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/04/22 22:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/04/22 22:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/04/22 22:12 108-20-30.50 1
Ethylbenzene 0.61 ug/L 04/04/22 22:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/04/22 22:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/04/22 22:12 98-82-80.50 1
Methylene Chloride ND ug/L 04/04/22 22:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/04/22 22:12 1634-04-40.50 1
Naphthalene ND ug/L 04/04/22 22:12 91-20-32.0 1
n-Propylbenzene ND ug/L 04/04/22 22:12 103-65-10.50 1
Styrene ND ug/L 04/04/22 22:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/04/22 22:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/04/22 22:12 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-4 Lab ID:92596442004 Collected:03/30/22 14:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/04/22 22:12 127-18-40.50 1
Toluene 3.5 ug/L 04/04/22 22:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/04/22 22:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/04/22 22:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/04/22 22:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/04/22 22:12 79-00-50.50 1
Trichloroethene ND ug/L 04/04/22 22:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/04/22 22:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/04/22 22:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/04/22 22:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/04/22 22:12 108-67-80.50 1
Vinyl chloride ND ug/L 04/04/22 22:12 75-01-41.0 1
m&p-Xylene 2.6 ug/L 04/04/22 22:12 179601-23-11.0 1
o-Xylene 0.99 ug/L 04/04/22 22:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %04/04/22 22:12 17060-07-070-130 1
4-Bromofluorobenzene (S)106 %04/04/22 22:12 460-00-470-130 1
Toluene-d8 (S)101 %04/04/22 22:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-5 Lab ID:92596442005 Collected:03/30/22 15:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 19.7 ug/L 04/05/22 03:55 71-43-26.2 12.5
Bromobenzene ND ug/L 04/05/22 03:55 108-86-16.2 12.5
Bromochloromethane ND ug/L 04/05/22 03:55 74-97-56.2 12.5
Bromodichloromethane ND ug/L 04/05/22 03:55 75-27-46.2 12.5
Bromoform ND ug/L 04/05/22 03:55 75-25-26.2 12.5
Bromomethane ND ug/L 04/05/22 03:55 74-83-962.5 12.5
n-Butylbenzene ND ug/L 04/05/22 03:55 104-51-86.2 12.5
sec-Butylbenzene ND ug/L 04/05/22 03:55 135-98-86.2 12.5
tert-Butylbenzene ND ug/L 04/05/22 03:55 98-06-66.2 12.5
Carbon tetrachloride ND ug/L 04/05/22 03:55 56-23-56.2 12.5
Chlorobenzene ND ug/L 04/05/22 03:55 108-90-76.2 12.5
Chloroethane ND ug/L 04/05/22 03:55 75-00-312.5 12.5
Chloroform ND ug/L 04/05/22 03:55 67-66-36.2 12.5
Chloromethane ND ug/L 04/05/22 03:55 74-87-312.5 12.5
2-Chlorotoluene ND ug/L 04/05/22 03:55 95-49-86.2 12.5
4-Chlorotoluene ND ug/L 04/05/22 03:55 106-43-46.2 12.5
1,2-Dibromo-3-chloropropane ND ug/L 04/05/22 03:55 96-12-812.5 12.5
Dibromochloromethane ND ug/L 04/05/22 03:55 124-48-16.2 12.5
1,2-Dibromoethane (EDB)ND ug/L 04/05/22 03:55 106-93-46.2 12.5
Dibromomethane ND ug/L 04/05/22 03:55 74-95-36.2 12.5
1,2-Dichlorobenzene ND ug/L 04/05/22 03:55 95-50-16.2 12.5
1,3-Dichlorobenzene ND ug/L 04/05/22 03:55 541-73-16.2 12.5
1,4-Dichlorobenzene ND ug/L 04/05/22 03:55 106-46-76.2 12.5
Dichlorodifluoromethane ND ug/L 04/05/22 03:55 75-71-8 L16.2 12.5
1,1-Dichloroethane ND ug/L 04/05/22 03:55 75-34-36.2 12.5
1,2-Dichloroethane ND ug/L 04/05/22 03:55 107-06-26.2 12.5
1,1-Dichloroethene ND ug/L 04/05/22 03:55 75-35-46.2 12.5
cis-1,2-Dichloroethene ND ug/L 04/05/22 03:55 156-59-26.2 12.5
trans-1,2-Dichloroethene ND ug/L 04/05/22 03:55 156-60-56.2 12.5
1,2-Dichloropropane ND ug/L 04/05/22 03:55 78-87-56.2 12.5
1,3-Dichloropropane ND ug/L 04/05/22 03:55 142-28-96.2 12.5
2,2-Dichloropropane ND ug/L 04/05/22 03:55 594-20-76.2 12.5
1,1-Dichloropropene ND ug/L 04/05/22 03:55 563-58-66.2 12.5
cis-1,3-Dichloropropene ND ug/L 04/05/22 03:55 10061-01-56.2 12.5
trans-1,3-Dichloropropene ND ug/L 04/05/22 03:55 10061-02-66.2 12.5
Diisopropyl ether ND ug/L 04/05/22 03:55 108-20-36.2 12.5
Ethylbenzene 269 ug/L 04/05/22 03:55 100-41-46.2 12.5
Hexachloro-1,3-butadiene ND ug/L 04/05/22 03:55 87-68-325.0 12.5
Isopropylbenzene (Cumene)19.2 ug/L 04/05/22 03:55 98-82-86.2 12.5
Methylene Chloride ND ug/L 04/05/22 03:55 75-09-225.0 12.5
Methyl-tert-butyl ether ND ug/L 04/05/22 03:55 1634-04-46.2 12.5
Naphthalene 89.1 ug/L 04/05/22 03:55 91-20-325.0 12.5
n-Propylbenzene 26.3 ug/L 04/05/22 03:55 103-65-16.2 12.5
Styrene ND ug/L 04/05/22 03:55 100-42-56.2 12.5
1,1,1,2-Tetrachloroethane ND ug/L 04/05/22 03:55 630-20-66.2 12.5
1,1,2,2-Tetrachloroethane ND ug/L 04/05/22 03:55 79-34-56.2 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-5 Lab ID:92596442005 Collected:03/30/22 15:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/05/22 03:55 127-18-46.2 12.5
Toluene 1330 ug/L 04/05/22 03:55 108-88-36.2 12.5
1,2,3-Trichlorobenzene ND ug/L 04/05/22 03:55 87-61-625.0 12.5
1,2,4-Trichlorobenzene ND ug/L 04/05/22 03:55 120-82-125.0 12.5
1,1,1-Trichloroethane ND ug/L 04/05/22 03:55 71-55-66.2 12.5
1,1,2-Trichloroethane ND ug/L 04/05/22 03:55 79-00-56.2 12.5
Trichloroethene ND ug/L 04/05/22 03:55 79-01-66.2 12.5
Trichlorofluoromethane ND ug/L 04/05/22 03:55 75-69-412.5 12.5
1,2,3-Trichloropropane ND ug/L 04/05/22 03:55 96-18-46.2 12.5
1,2,4-Trimethylbenzene 379 ug/L 04/05/22 03:55 95-63-66.2 12.5
1,3,5-Trimethylbenzene 58.3 ug/L 04/05/22 03:55 108-67-86.2 12.5
Vinyl chloride ND ug/L 04/05/22 03:55 75-01-412.5 12.5
m&p-Xylene 1020 ug/L 04/05/22 03:55 179601-23-112.5 12.5
o-Xylene 639 ug/L 04/05/22 03:55 95-47-66.2 12.5
Surrogates
1,2-Dichloroethane-d4 (S)106 %04/05/22 03:55 17060-07-070-130 12.5
4-Bromofluorobenzene (S)100 %04/05/22 03:55 460-00-470-130 12.5
Toluene-d8 (S)102 %04/05/22 03:55 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-6 Lab ID:92596442006 Collected:03/30/22 13:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/04/22 22:30 71-43-20.50 1
Bromobenzene ND ug/L 04/04/22 22:30 108-86-10.50 1
Bromochloromethane ND ug/L 04/04/22 22:30 74-97-50.50 1
Bromodichloromethane ND ug/L 04/04/22 22:30 75-27-40.50 1
Bromoform ND ug/L 04/04/22 22:30 75-25-20.50 1
Bromomethane ND ug/L 04/04/22 22:30 74-83-95.0 1
n-Butylbenzene ND ug/L 04/04/22 22:30 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/04/22 22:30 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/04/22 22:30 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/04/22 22:30 56-23-50.50 1
Chlorobenzene ND ug/L 04/04/22 22:30 108-90-70.50 1
Chloroethane ND ug/L 04/04/22 22:30 75-00-31.0 1
Chloroform ND ug/L 04/04/22 22:30 67-66-30.50 1
Chloromethane ND ug/L 04/04/22 22:30 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/04/22 22:30 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/04/22 22:30 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/04/22 22:30 96-12-81.0 1
Dibromochloromethane ND ug/L 04/04/22 22:30 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/04/22 22:30 106-93-40.50 1
Dibromomethane ND ug/L 04/04/22 22:30 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/04/22 22:30 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/04/22 22:30 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/04/22 22:30 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/04/22 22:30 75-71-8 L10.50 1
1,1-Dichloroethane ND ug/L 04/04/22 22:30 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/04/22 22:30 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/04/22 22:30 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/04/22 22:30 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/04/22 22:30 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/04/22 22:30 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/04/22 22:30 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/04/22 22:30 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/04/22 22:30 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/04/22 22:30 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/04/22 22:30 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/04/22 22:30 108-20-30.50 1
Ethylbenzene ND ug/L 04/04/22 22:30 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/04/22 22:30 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/04/22 22:30 98-82-80.50 1
Methylene Chloride ND ug/L 04/04/22 22:30 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/04/22 22:30 1634-04-40.50 1
Naphthalene ND ug/L 04/04/22 22:30 91-20-32.0 1
n-Propylbenzene ND ug/L 04/04/22 22:30 103-65-10.50 1
Styrene ND ug/L 04/04/22 22:30 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/04/22 22:30 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/04/22 22:30 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-6 Lab ID:92596442006 Collected:03/30/22 13:15 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/04/22 22:30 127-18-40.50 1
Toluene ND ug/L 04/04/22 22:30 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/04/22 22:30 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/04/22 22:30 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/04/22 22:30 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/04/22 22:30 79-00-50.50 1
Trichloroethene ND ug/L 04/04/22 22:30 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/04/22 22:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/04/22 22:30 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/04/22 22:30 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/04/22 22:30 108-67-80.50 1
Vinyl chloride ND ug/L 04/04/22 22:30 75-01-41.0 1
m&p-Xylene ND ug/L 04/04/22 22:30 179601-23-11.0 1
o-Xylene ND ug/L 04/04/22 22:30 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %04/04/22 22:30 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %04/04/22 22:30 460-00-470-130 1
Toluene-d8 (S)100 %04/04/22 22:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-7 Lab ID:92596442007 Collected:03/30/22 13:45 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 13:54 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 13:54 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 13:54 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 13:54 75-27-40.50 1
Bromoform ND ug/L 04/01/22 13:54 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 13:54 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 13:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 13:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 13:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 13:54 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 13:54 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 13:54 75-00-31.0 1
Chloroform ND ug/L 04/01/22 13:54 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 13:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 13:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 13:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 13:54 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 13:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 13:54 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 13:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 13:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 13:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 13:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 13:54 75-71-8 L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 13:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 13:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 13:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 13:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 13:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 13:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 13:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 13:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 13:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 13:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 13:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 13:54 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 13:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 13:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 13:54 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 13:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 13:54 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 13:54 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 13:54 103-65-10.50 1
Styrene ND ug/L 04/01/22 13:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 13:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 13:54 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-7 Lab ID:92596442007 Collected:03/30/22 13:45 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 13:54 127-18-40.50 1
Toluene ND ug/L 04/01/22 13:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 13:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 13:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 13:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 13:54 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 13:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 13:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 13:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 13:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 13:54 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 13:54 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 13:54 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 13:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)108 %04/01/22 13:54 17060-07-070-130 1
4-Bromofluorobenzene (S)106 %04/01/22 13:54 460-00-470-130 1
Toluene-d8 (S)100 %04/01/22 13:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-8 Lab ID:92596442008 Collected:03/30/22 16:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/04/22 22:48 71-43-20.50 1
Bromobenzene ND ug/L 04/04/22 22:48 108-86-10.50 1
Bromochloromethane ND ug/L 04/04/22 22:48 74-97-50.50 1
Bromodichloromethane ND ug/L 04/04/22 22:48 75-27-40.50 1
Bromoform ND ug/L 04/04/22 22:48 75-25-20.50 1
Bromomethane ND ug/L 04/04/22 22:48 74-83-95.0 1
n-Butylbenzene ND ug/L 04/04/22 22:48 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/04/22 22:48 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/04/22 22:48 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/04/22 22:48 56-23-50.50 1
Chlorobenzene ND ug/L 04/04/22 22:48 108-90-70.50 1
Chloroethane ND ug/L 04/04/22 22:48 75-00-31.0 1
Chloroform ND ug/L 04/04/22 22:48 67-66-30.50 1
Chloromethane ND ug/L 04/04/22 22:48 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/04/22 22:48 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/04/22 22:48 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/04/22 22:48 96-12-81.0 1
Dibromochloromethane ND ug/L 04/04/22 22:48 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/04/22 22:48 106-93-40.50 1
Dibromomethane ND ug/L 04/04/22 22:48 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/04/22 22:48 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/04/22 22:48 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/04/22 22:48 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/04/22 22:48 75-71-8 L10.50 1
1,1-Dichloroethane ND ug/L 04/04/22 22:48 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/04/22 22:48 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/04/22 22:48 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/04/22 22:48 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/04/22 22:48 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/04/22 22:48 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/04/22 22:48 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/04/22 22:48 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/04/22 22:48 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/04/22 22:48 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/04/22 22:48 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/04/22 22:48 108-20-30.50 1
Ethylbenzene ND ug/L 04/04/22 22:48 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/04/22 22:48 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/04/22 22:48 98-82-80.50 1
Methylene Chloride ND ug/L 04/04/22 22:48 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/04/22 22:48 1634-04-40.50 1
Naphthalene ND ug/L 04/04/22 22:48 91-20-32.0 1
n-Propylbenzene ND ug/L 04/04/22 22:48 103-65-10.50 1
Styrene ND ug/L 04/04/22 22:48 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/04/22 22:48 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/04/22 22:48 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:MW-8 Lab ID:92596442008 Collected:03/30/22 16:40 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/04/22 22:48 127-18-40.50 1
Toluene ND ug/L 04/04/22 22:48 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/04/22 22:48 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/04/22 22:48 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/04/22 22:48 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/04/22 22:48 79-00-50.50 1
Trichloroethene ND ug/L 04/04/22 22:48 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/04/22 22:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/04/22 22:48 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/04/22 22:48 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/04/22 22:48 108-67-80.50 1
Vinyl chloride ND ug/L 04/04/22 22:48 75-01-41.0 1
m&p-Xylene ND ug/L 04/04/22 22:48 179601-23-11.0 1
o-Xylene ND ug/L 04/04/22 22:48 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %04/04/22 22:48 17060-07-070-130 1
4-Bromofluorobenzene (S)108 %04/04/22 22:48 460-00-470-130 1
Toluene-d8 (S)99 %04/04/22 22:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-1 Lab ID:92596442009 Collected:03/30/22 13:00 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 14:12 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 14:12 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 14:12 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 14:12 75-27-40.50 1
Bromoform ND ug/L 04/01/22 14:12 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 14:12 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 14:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 14:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 14:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 14:12 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 14:12 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 14:12 75-00-31.0 1
Chloroform ND ug/L 04/01/22 14:12 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 14:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 14:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 14:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 14:12 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 14:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 14:12 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 14:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 14:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 14:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 14:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 14:12 75-71-8 L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 14:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 14:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 14:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 14:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 14:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 14:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 14:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 14:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 14:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 14:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 14:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 14:12 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 14:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 14:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 14:12 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 14:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 14:12 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 14:12 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 14:12 103-65-10.50 1
Styrene ND ug/L 04/01/22 14:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 14:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 14:12 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-1 Lab ID:92596442009 Collected:03/30/22 13:00 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 14:12 127-18-40.50 1
Toluene ND ug/L 04/01/22 14:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 14:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 14:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 14:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 14:12 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 14:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 14:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 14:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 14:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 14:12 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 14:12 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 14:12 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 14:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %04/01/22 14:12 17060-07-070-130 1
4-Bromofluorobenzene (S)106 %04/01/22 14:12 460-00-470-130 1
Toluene-d8 (S)101 %04/01/22 14:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-2 Lab ID:92596442010 Collected:03/30/22 13:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/01/22 23:48 71-43-20.50 1
Bromobenzene ND ug/L 04/01/22 23:48 108-86-10.50 1
Bromochloromethane ND ug/L 04/01/22 23:48 74-97-50.50 1
Bromodichloromethane ND ug/L 04/01/22 23:48 75-27-40.50 1
Bromoform ND ug/L 04/01/22 23:48 75-25-20.50 1
Bromomethane ND ug/L 04/01/22 23:48 74-83-95.0 1
n-Butylbenzene ND ug/L 04/01/22 23:48 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/01/22 23:48 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/01/22 23:48 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/01/22 23:48 56-23-50.50 1
Chlorobenzene ND ug/L 04/01/22 23:48 108-90-70.50 1
Chloroethane ND ug/L 04/01/22 23:48 75-00-31.0 1
Chloroform ND ug/L 04/01/22 23:48 67-66-30.50 1
Chloromethane ND ug/L 04/01/22 23:48 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/01/22 23:48 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/01/22 23:48 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/01/22 23:48 96-12-81.0 1
Dibromochloromethane ND ug/L 04/01/22 23:48 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/01/22 23:48 106-93-40.50 1
Dibromomethane ND ug/L 04/01/22 23:48 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/01/22 23:48 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/01/22 23:48 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/01/22 23:48 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/01/22 23:48 75-71-8 IH,L10.50 1
1,1-Dichloroethane ND ug/L 04/01/22 23:48 75-34-30.50 1
1,2-Dichloroethane ND ug/L 04/01/22 23:48 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/01/22 23:48 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/01/22 23:48 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/01/22 23:48 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/01/22 23:48 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/01/22 23:48 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/01/22 23:48 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/01/22 23:48 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/01/22 23:48 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/01/22 23:48 10061-02-60.50 1
Diisopropyl ether ND ug/L 04/01/22 23:48 108-20-30.50 1
Ethylbenzene ND ug/L 04/01/22 23:48 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/01/22 23:48 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/01/22 23:48 98-82-80.50 1
Methylene Chloride ND ug/L 04/01/22 23:48 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 04/01/22 23:48 1634-04-40.50 1
Naphthalene ND ug/L 04/01/22 23:48 91-20-32.0 1
n-Propylbenzene ND ug/L 04/01/22 23:48 103-65-10.50 1
Styrene ND ug/L 04/01/22 23:48 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/01/22 23:48 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/01/22 23:48 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92596442
The Spot
Sample:WSW-2 Lab ID:92596442010 Collected:03/30/22 13:10 Received:03/31/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/01/22 23:48 127-18-40.50 1
Toluene ND ug/L 04/01/22 23:48 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/01/22 23:48 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/01/22 23:48 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/01/22 23:48 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/01/22 23:48 79-00-50.50 1
Trichloroethene ND ug/L 04/01/22 23:48 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/01/22 23:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/01/22 23:48 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/01/22 23:48 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/01/22 23:48 108-67-80.50 1
Vinyl chloride ND ug/L 04/01/22 23:48 75-01-41.0 1
m&p-Xylene ND ug/L 04/01/22 23:48 179601-23-11.0 1
o-Xylene ND ug/L 04/01/22 23:48 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %04/01/22 23:48 17060-07-070-130 1
4-Bromofluorobenzene (S)107 %04/01/22 23:48 460-00-470-130 1
Toluene-d8 (S)100 %04/01/22 23:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
688853
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442001, 92596442007, 92596442009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3599706
Associated Lab Samples:92596442001, 92596442007, 92596442009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/01/22 10:18
1,1,1-Trichloroethane ug/L ND 0.50 04/01/22 10:18
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/01/22 10:18
1,1,2-Trichloroethane ug/L ND 0.50 04/01/22 10:18
1,1-Dichloroethane ug/L ND 0.50 04/01/22 10:18
1,1-Dichloroethene ug/L ND 0.50 04/01/22 10:18
1,1-Dichloropropene ug/L ND 0.50 04/01/22 10:18
1,2,3-Trichlorobenzene ug/L ND 2.0 04/01/22 10:18
1,2,3-Trichloropropane ug/L ND 0.50 04/01/22 10:18
1,2,4-Trichlorobenzene ug/L ND 2.0 04/01/22 10:18
1,2,4-Trimethylbenzene ug/L ND 0.50 04/01/22 10:18
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/01/22 10:18
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/01/22 10:18
1,2-Dichlorobenzene ug/L ND 0.50 04/01/22 10:18
1,2-Dichloroethane ug/L ND 0.50 04/01/22 10:18
1,2-Dichloropropane ug/L ND 0.50 04/01/22 10:18
1,3,5-Trimethylbenzene ug/L ND 0.50 04/01/22 10:18
1,3-Dichlorobenzene ug/L ND 0.50 04/01/22 10:18
1,3-Dichloropropane ug/L ND 0.50 04/01/22 10:18
1,4-Dichlorobenzene ug/L ND 0.50 04/01/22 10:18
2,2-Dichloropropane ug/L ND 0.50 04/01/22 10:18
2-Chlorotoluene ug/L ND 0.50 04/01/22 10:18
4-Chlorotoluene ug/L ND 0.50 04/01/22 10:18
Benzene ug/L ND 0.50 04/01/22 10:18
Bromobenzene ug/L ND 0.50 04/01/22 10:18
Bromochloromethane ug/L ND 0.50 04/01/22 10:18
Bromodichloromethane ug/L ND 0.50 04/01/22 10:18
Bromoform ug/L ND 0.50 04/01/22 10:18
Bromomethane ug/L ND 5.0 04/01/22 10:18
Carbon tetrachloride ug/L ND 0.50 04/01/22 10:18
Chlorobenzene ug/L ND 0.50 04/01/22 10:18
Chloroethane ug/L ND 1.0 04/01/22 10:18
Chloroform ug/L ND 0.50 04/01/22 10:18
Chloromethane ug/L ND 1.0 04/01/22 10:18
cis-1,2-Dichloroethene ug/L ND 0.50 04/01/22 10:18
cis-1,3-Dichloropropene ug/L ND 0.50 04/01/22 10:18
Dibromochloromethane ug/L ND 0.50 04/01/22 10:18
Dibromomethane ug/L ND 0.50 04/01/22 10:18
Dichlorodifluoromethane ug/L ND 0.50 IH04/01/22 10:18
Diisopropyl ether ug/L ND 0.50 04/01/22 10:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3599706
Associated Lab Samples:92596442001, 92596442007, 92596442009
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/01/22 10:18
Hexachloro-1,3-butadiene ug/L ND 2.0 04/01/22 10:18
Isopropylbenzene (Cumene)ug/L ND 0.50 04/01/22 10:18
m&p-Xylene ug/L ND 1.0 04/01/22 10:18
Methyl-tert-butyl ether ug/L ND 0.50 04/01/22 10:18
Methylene Chloride ug/L ND 2.0 04/01/22 10:18
n-Butylbenzene ug/L ND 0.50 04/01/22 10:18
n-Propylbenzene ug/L ND 0.50 04/01/22 10:18
Naphthalene ug/L ND 2.0 04/01/22 10:18
o-Xylene ug/L ND 0.50 04/01/22 10:18
sec-Butylbenzene ug/L ND 0.50 04/01/22 10:18
Styrene ug/L ND 0.50 04/01/22 10:18
tert-Butylbenzene ug/L ND 0.50 04/01/22 10:18
Tetrachloroethene ug/L ND 0.50 04/01/22 10:18
Toluene ug/L ND 0.50 04/01/22 10:18
trans-1,2-Dichloroethene ug/L ND 0.50 04/01/22 10:18
trans-1,3-Dichloropropene ug/L ND 0.50 04/01/22 10:18
Trichloroethene ug/L ND 0.50 04/01/22 10:18
Trichlorofluoromethane ug/L ND 1.0 04/01/22 10:18
Vinyl chloride ug/L ND 1.0 04/01/22 10:18
1,2-Dichloroethane-d4 (S)%102 70-130 04/01/22 10:18
4-Bromofluorobenzene (S)%101 70-130 04/01/22 10:18
Toluene-d8 (S)%101 70-130 04/01/22 10:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3599707LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.650 107 60-140
1,1,1-Trichloroethane ug/L 51.250 102 60-140
1,1,2,2-Tetrachloroethane ug/L 54.050 108 60-140
1,1,2-Trichloroethane ug/L 51.050 102 60-140
1,1-Dichloroethane ug/L 46.850 94 60-140
1,1-Dichloroethene ug/L 51.450 103 60-140
1,1-Dichloropropene ug/L 49.950 100 60-140
1,2,3-Trichlorobenzene ug/L 56.050 112 60-140
1,2,3-Trichloropropane ug/L 52.950 106 60-140
1,2,4-Trichlorobenzene ug/L 57.350 115 60-140
1,2,4-Trimethylbenzene ug/L 52.450 105 60-140
1,2-Dibromo-3-chloropropane ug/L 49.750 99 60-140
1,2-Dibromoethane (EDB)ug/L 54.550 109 60-140
1,2-Dichlorobenzene ug/L 55.350 111 60-140
1,2-Dichloroethane ug/L 49.150 98 60-140
1,2-Dichloropropane ug/L 50.750 101 60-140
1,3,5-Trimethylbenzene ug/L 53.450 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3599707LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 57.750 115 60-140
1,3-Dichloropropane ug/L 53.350 107 60-140
1,4-Dichlorobenzene ug/L 53.850 108 60-140
2,2-Dichloropropane ug/L 54.950 110 60-140
2-Chlorotoluene ug/L 52.150 104 60-140
4-Chlorotoluene ug/L 54.350 109 60-140
Benzene ug/L 46.350 93 60-140
Bromobenzene ug/L 54.550 109 60-140
Bromochloromethane ug/L 42.550 85 60-140
Bromodichloromethane ug/L 52.450 105 60-140
Bromoform ug/L 49.950 100 60-140
Bromomethane ug/L 44.250 88 60-140
Carbon tetrachloride ug/L 60.650 121 60-140
Chlorobenzene ug/L 54.350 109 60-140
Chloroethane ug/L 49.750 99 60-140
Chloroform ug/L 49.650 99 60-140
Chloromethane ug/L 50.450 101 60-140
cis-1,2-Dichloroethene ug/L 47.350 95 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 54.750 109 60-140
Dibromomethane ug/L 52.950 106 60-140
Dichlorodifluoromethane ug/L 79.2 IH,L15015860-140
Diisopropyl ether ug/L 50.950 102 60-140
Ethylbenzene ug/L 52.250 104 60-140
Hexachloro-1,3-butadiene ug/L 58.850 118 60-140
Isopropylbenzene (Cumene)ug/L 51.650 103 60-140
m&p-Xylene ug/L 105100 105 60-140
Methyl-tert-butyl ether ug/L 52.150 104 60-140
Methylene Chloride ug/L 52.050 104 60-140
n-Butylbenzene ug/L 56.250 112 60-140
n-Propylbenzene ug/L 52.250 104 60-140
Naphthalene ug/L 57.050 114 60-140
o-Xylene ug/L 53.250 106 60-140
sec-Butylbenzene ug/L 54.250 108 60-140
Styrene ug/L 52.050 104 60-140
tert-Butylbenzene ug/L 46.250 92 60-140
Tetrachloroethene ug/L 54.950 110 60-140
Toluene ug/L 48.850 98 60-140
trans-1,2-Dichloroethene ug/L 48.750 97 60-140
trans-1,3-Dichloropropene ug/L 53.850 108 60-140
Trichloroethene ug/L 52.650 105 60-140
Trichlorofluoromethane ug/L 44.350 89 60-140
Vinyl chloride ug/L 51.750 103 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3599708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596442001
3599709
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 1000 112 60-140119 61000ND11201190
1,1,1-Trichloroethane ug/L 1000 115 60-140122 61000ND11501220
1,1,2,2-Tetrachloroethane ug/L 1000 109 60-140118 91000ND10901180
1,1,2-Trichloroethane ug/L 1000 109 60-140111 21000ND10901110
1,1-Dichloroethane ug/L 1000 102 60-140113 91000ND10201130
1,1-Dichloroethene ug/L 1000 121 60-140129 61000ND12101290
1,1-Dichloropropene ug/L 1000 119 60-140125 51000ND11901250
1,2,3-Trichlorobenzene ug/L 1000 106 60-140107 11000ND10601070
1,2,3-Trichloropropane ug/L 1000 105 60-140110 41000ND10501100
1,2,4-Trichlorobenzene ug/L 1000 111 60-140117 51000ND11101170
1,2,4-Trimethylbenzene ug/L 1000 105 60-140122 71000148025302700
1,2-Dibromo-3-chloropropane ug/L 1000 105 60-140102 31000ND10501020
1,2-Dibromoethane (EDB)ug/L 1000 116 60-140125 81000ND11601250
1,2-Dichlorobenzene ug/L 1000 107 60-140118 101000ND10701180
1,2-Dichloroethane ug/L 1000 102 60-140114 111000ND10201140
1,2-Dichloropropane ug/L 1000 112 60-140120 71000ND11201200
1,3,5-Trimethylbenzene ug/L 1000 111 60-140124 8100036914801610
1,3-Dichlorobenzene ug/L 1000 111 60-140118 61000ND11101180
1,3-Dichloropropane ug/L 1000 102 60-140113 111000ND10201130
1,4-Dichlorobenzene ug/L 1000 101 60-140112 111000ND10101120
2,2-Dichloropropane ug/L 1000 106 60-140118 111000ND10601180
2-Chlorotoluene ug/L 1000 111 60-140119 71000ND11101190
4-Chlorotoluene ug/L 1000 110 60-140116 51000ND11001160
Benzene ug/L E,M1100012660-140149 2100093801060010900
Bromobenzene ug/L 1000 105 60-140115 91000ND10501150
Bromochloromethane ug/L 1000 94 60-140104 101000ND9411040
Bromodichloromethane ug/L 1000 117 60-140116 11000ND11701160
Bromoform ug/L 1000 96 60-140105 91000ND9611050
Bromomethane ug/L 1000 61 60-14078 251000ND608783
Carbon tetrachloride ug/L M1100014060-140144 31000ND14001440
Chlorobenzene ug/L 1000 110 60-140122 101000ND11001220
Chloroethane ug/L 1000 134 60-140138 41000ND13401380
Chloroform ug/L 1000 107 60-140117 91000ND10701170
Chloromethane ug/L 1000 109 60-140120 91000ND10901200
cis-1,2-Dichloroethene ug/L 1000 104 60-140114 91000ND10401140
cis-1,3-Dichloropropene ug/L 1000 110 60-140121 101000ND11001210
Dibromochloromethane ug/L 1000 109 60-140119 91000ND10901190
Dibromomethane ug/L 1000 109 60-140120 91000ND10901200
Dichlorodifluoromethane ug/L IH,M0100023560-140224 51000ND23502240
Diisopropyl ether ug/L 1000 101 60-140114 9100040414101540
Ethylbenzene ug/L 1000 100 60-140116 51000210031003260
Hexachloro-1,3-butadiene ug/L 1000 126 60-140130 31000ND12601300
Isopropylbenzene (Cumene)ug/L 1000 112 60-140118 5100066.5 1190 1250
m&p-Xylene ug/L 2000 104 60-140127 62000593080008470
Methyl-tert-butyl ether ug/L 1000 109 60-140120 8100021313001420
Methylene Chloride ug/L 1000 117 60-140127 81000ND11701270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3599708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596442001
3599709
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 1000 124 60-140130 51000ND12401300
n-Propylbenzene ug/L 1000 110 60-140120 8100019112901390
Naphthalene ug/L 1000 97 60-140114 10100051914901650
o-Xylene ug/L 1000 103 60-140123 41000334043704570
sec-Butylbenzene ug/L 1000 120 60-140127 51000ND12001270
Styrene ug/L 1000 113 60-140115 21000ND11301150
tert-Butylbenzene ug/L 1000 98 60-140107 81000ND9791070
Tetrachloroethene ug/L 1000 123 60-140122 11000ND12301220
Toluene ug/L 1000 99 60-140126 31000834093309600
trans-1,2-Dichloroethene ug/L 1000 115 60-140120 41000ND11501200
trans-1,3-Dichloropropene ug/L 1000 106 60-140115 81000ND10601150
Trichloroethene ug/L 1000 114 60-140126 91000ND11401260
Trichlorofluoromethane ug/L 1000 131 60-140129 21000ND13101290
Vinyl chloride ug/L 1000 125 60-140130 41000ND12501300
1,2-Dichloroethane-d4 (S)%102 70-130103
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%101 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
688913
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3600065
Associated Lab Samples:92596442010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/01/22 22:18
1,1,1-Trichloroethane ug/L ND 0.50 04/01/22 22:18
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/01/22 22:18
1,1,2-Trichloroethane ug/L ND 0.50 04/01/22 22:18
1,1-Dichloroethane ug/L ND 0.50 04/01/22 22:18
1,1-Dichloroethene ug/L ND 0.50 04/01/22 22:18
1,1-Dichloropropene ug/L ND 0.50 04/01/22 22:18
1,2,3-Trichlorobenzene ug/L ND 2.0 04/01/22 22:18
1,2,3-Trichloropropane ug/L ND 0.50 04/01/22 22:18
1,2,4-Trichlorobenzene ug/L ND 2.0 04/01/22 22:18
1,2,4-Trimethylbenzene ug/L ND 0.50 04/01/22 22:18
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/01/22 22:18
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/01/22 22:18
1,2-Dichlorobenzene ug/L ND 0.50 04/01/22 22:18
1,2-Dichloroethane ug/L ND 0.50 04/01/22 22:18
1,2-Dichloropropane ug/L ND 0.50 04/01/22 22:18
1,3,5-Trimethylbenzene ug/L ND 0.50 04/01/22 22:18
1,3-Dichlorobenzene ug/L ND 0.50 04/01/22 22:18
1,3-Dichloropropane ug/L ND 0.50 04/01/22 22:18
1,4-Dichlorobenzene ug/L ND 0.50 04/01/22 22:18
2,2-Dichloropropane ug/L ND 0.50 04/01/22 22:18
2-Chlorotoluene ug/L ND 0.50 04/01/22 22:18
4-Chlorotoluene ug/L ND 0.50 04/01/22 22:18
Benzene ug/L ND 0.50 04/01/22 22:18
Bromobenzene ug/L ND 0.50 04/01/22 22:18
Bromochloromethane ug/L ND 0.50 04/01/22 22:18
Bromodichloromethane ug/L ND 0.50 04/01/22 22:18
Bromoform ug/L ND 0.50 04/01/22 22:18
Bromomethane ug/L ND 5.0 04/01/22 22:18
Carbon tetrachloride ug/L ND 0.50 04/01/22 22:18
Chlorobenzene ug/L ND 0.50 04/01/22 22:18
Chloroethane ug/L ND 1.0 04/01/22 22:18
Chloroform ug/L ND 0.50 04/01/22 22:18
Chloromethane ug/L ND 1.0 04/01/22 22:18
cis-1,2-Dichloroethene ug/L ND 0.50 04/01/22 22:18
cis-1,3-Dichloropropene ug/L ND 0.50 04/01/22 22:18
Dibromochloromethane ug/L ND 0.50 04/01/22 22:18
Dibromomethane ug/L ND 0.50 04/01/22 22:18
Dichlorodifluoromethane ug/L ND 0.50 IH04/01/22 22:18
Diisopropyl ether ug/L ND 0.50 04/01/22 22:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3600065
Associated Lab Samples:92596442010
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/01/22 22:18
Hexachloro-1,3-butadiene ug/L ND 2.0 04/01/22 22:18
Isopropylbenzene (Cumene)ug/L ND 0.50 04/01/22 22:18
m&p-Xylene ug/L ND 1.0 04/01/22 22:18
Methyl-tert-butyl ether ug/L ND 0.50 04/01/22 22:18
Methylene Chloride ug/L ND 2.0 04/01/22 22:18
n-Butylbenzene ug/L ND 0.50 04/01/22 22:18
n-Propylbenzene ug/L ND 0.50 04/01/22 22:18
Naphthalene ug/L ND 2.0 04/01/22 22:18
o-Xylene ug/L ND 0.50 04/01/22 22:18
sec-Butylbenzene ug/L ND 0.50 04/01/22 22:18
Styrene ug/L ND 0.50 04/01/22 22:18
tert-Butylbenzene ug/L ND 0.50 04/01/22 22:18
Tetrachloroethene ug/L ND 0.50 04/01/22 22:18
Toluene ug/L ND 0.50 04/01/22 22:18
trans-1,2-Dichloroethene ug/L ND 0.50 04/01/22 22:18
trans-1,3-Dichloropropene ug/L ND 0.50 04/01/22 22:18
Trichloroethene ug/L ND 0.50 04/01/22 22:18
Trichlorofluoromethane ug/L ND 1.0 04/01/22 22:18
Vinyl chloride ug/L ND 1.0 04/01/22 22:18
1,2-Dichloroethane-d4 (S)%100 70-130 04/01/22 22:18
4-Bromofluorobenzene (S)%102 70-130 04/01/22 22:18
Toluene-d8 (S)%99 70-130 04/01/22 22:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3600066LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.250 110 60-140
1,1,1-Trichloroethane ug/L 53.450 107 60-140
1,1,2,2-Tetrachloroethane ug/L 54.550 109 60-140
1,1,2-Trichloroethane ug/L 53.850 108 60-140
1,1-Dichloroethane ug/L 47.850 96 60-140
1,1-Dichloroethene ug/L 50.650 101 60-140
1,1-Dichloropropene ug/L 51.150 102 60-140
1,2,3-Trichlorobenzene ug/L 51.250 102 60-140
1,2,3-Trichloropropane ug/L 49.750 99 60-140
1,2,4-Trichlorobenzene ug/L 56.150 112 60-140
1,2,4-Trimethylbenzene ug/L 51.650 103 60-140
1,2-Dibromo-3-chloropropane ug/L 52.750 105 60-140
1,2-Dibromoethane (EDB)ug/L 55.050 110 60-140
1,2-Dichlorobenzene ug/L 52.950 106 60-140
1,2-Dichloroethane ug/L 49.350 99 60-140
1,2-Dichloropropane ug/L 53.050 106 60-140
1,3,5-Trimethylbenzene ug/L 52.550 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3600066LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 54.750 109 60-140
1,3-Dichloropropane ug/L 51.750 103 60-140
1,4-Dichlorobenzene ug/L 52.550 105 60-140
2,2-Dichloropropane ug/L 53.250 106 60-140
2-Chlorotoluene ug/L 50.850 102 60-140
4-Chlorotoluene ug/L 52.150 104 60-140
Benzene ug/L 48.250 96 60-140
Bromobenzene ug/L 50.250 100 60-140
Bromochloromethane ug/L 43.950 88 60-140
Bromodichloromethane ug/L 53.750 107 60-140
Bromoform ug/L 51.250 102 60-140
Bromomethane ug/L 38.050 76 60-140
Carbon tetrachloride ug/L 62.950 126 60-140
Chlorobenzene ug/L 52.650 105 60-140
Chloroethane ug/L 55.350 111 60-140
Chloroform ug/L 49.650 99 60-140
Chloromethane ug/L 49.850 100 60-140
cis-1,2-Dichloroethene ug/L 47.750 95 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 55.250 110 60-140
Dibromomethane ug/L 54.450 109 60-140
Dichlorodifluoromethane ug/L 82.6 IH,L15016560-140
Diisopropyl ether ug/L 50.450 101 60-140
Ethylbenzene ug/L 51.750 103 60-140
Hexachloro-1,3-butadiene ug/L 57.650 115 60-140
Isopropylbenzene (Cumene)ug/L 51.450 103 60-140
m&p-Xylene ug/L 107100 107 60-140
Methyl-tert-butyl ether ug/L 52.050 104 60-140
Methylene Chloride ug/L 53.050 106 60-140
n-Butylbenzene ug/L 57.050 114 60-140
n-Propylbenzene ug/L 51.850 104 60-140
Naphthalene ug/L 53.150 106 60-140
o-Xylene ug/L 53.550 107 60-140
sec-Butylbenzene ug/L 52.650 105 60-140
Styrene ug/L 52.850 106 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 56.350 113 60-140
Toluene ug/L 50.550 101 60-140
trans-1,2-Dichloroethene ug/L 48.950 98 60-140
trans-1,3-Dichloropropene ug/L 54.150 108 60-140
Trichloroethene ug/L 54.550 109 60-140
Trichlorofluoromethane ug/L 48.950 98 60-140
Vinyl chloride ug/L 51.750 103 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3600067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596043003
3600068
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 104 60-140108 42000ND20802170
1,1,1-Trichloroethane ug/L 2000 106 60-140109 22000ND21202170
1,1,2,2-Tetrachloroethane ug/L 2000 103 60-140106 32000ND20602120
1,1,2-Trichloroethane ug/L 2000 101 60-140108 62000ND20302150
1,1-Dichloroethane ug/L 2000 102 60-140104 22000ND20402090
1,1-Dichloroethene ug/L 2000 109 60-140119 92000ND21702370
1,1-Dichloropropene ug/L 2000 113 60-140115 12000ND22602290
1,2,3-Trichlorobenzene ug/L 2000 103 60-140108 52000ND20702160
1,2,3-Trichloropropane ug/L 2000 104 60-14099 52000ND20801980
1,2,4-Trichlorobenzene ug/L 2000 106 60-140113 62000ND21202270
1,2,4-Trimethylbenzene ug/L 2000 100 60-140103 12000286048704910
1,2-Dibromo-3-chloropropane ug/L 2000 102 60-140105 32000ND20302100
1,2-Dibromoethane (EDB)ug/L 2000 109 60-140109 02000ND21802180
1,2-Dichlorobenzene ug/L 2000 107 60-140107 02000ND21402140
1,2-Dichloroethane ug/L 2000 103 60-140102 12000ND20502040
1,2-Dichloropropane ug/L 2000 104 60-140110 52000ND20902200
1,3,5-Trimethylbenzene ug/L 2000 114 60-140115 1200074930303050
1,3-Dichlorobenzene ug/L 2000 109 60-140115 52000ND21702290
1,3-Dichloropropane ug/L 2000 102 60-140111 92000ND20302220
1,4-Dichlorobenzene ug/L 2000 108 60-140106 12000ND21502130
2,2-Dichloropropane ug/L 2000 99 60-14093 62000ND19701860
2-Chlorotoluene ug/L 2000 106 60-140113 72000ND21102260
4-Chlorotoluene ug/L 2000 108 60-140109 12000ND21502170
Benzene ug/L 2000 96 60-140100 3200037923002370
Bromobenzene ug/L 2000 109 60-140107 22000ND21802140
Bromochloromethane ug/L 2000 96 60-14089 82000ND19201770
Bromodichloromethane ug/L 2000 103 60-140111 82000ND20502230
Bromoform ug/L 2000 92 60-14096 52000ND18401930
Bromomethane ug/L 2000 75 60-14084 112000ND15001670
Carbon tetrachloride ug/L 2000 122 60-140126 32000ND24502530
Chlorobenzene ug/L 2000 109 60-140107 32000ND21902130
Chloroethane ug/L 2000 118 60-140126 62000ND23602510
Chloroform ug/L 2000 106 60-140104 22000ND21202080
Chloromethane ug/L 2000 108 60-140111 22000ND21602220
cis-1,2-Dichloroethene ug/L 2000 102 60-140104 22000ND20302070
cis-1,3-Dichloropropene ug/L 2000 105 60-140108 32000ND20902160
Dibromochloromethane ug/L 2000 104 60-140106 22000ND20802110
Dibromomethane ug/L 2000 106 60-140115 82000ND21302310
Dichlorodifluoromethane ug/L IH,M0200015360-140182 172000ND30703640
Diisopropyl ether ug/L 2000 104 60-140101 22000ND20702030
Ethylbenzene ug/L 2000 106 60-140109 22000126033703430
Hexachloro-1,3-butadiene ug/L 2000 109 60-140120 92000ND21902400
Isopropylbenzene (Cumene)ug/L 2000 104 60-140108 4200011821902280
m&p-Xylene ug/L 4000 100 60-140110 44000546094609840
Methyl-tert-butyl ether ug/L 2000 109 60-140106 22000ND21702120
Methylene Chloride ug/L 2000 111 60-140117 52000ND22302330
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3600067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596043003
3600068
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 2000 111 60-140111 1200018524002410
n-Propylbenzene ug/L 2000 105 60-140107 1200031824202460
Naphthalene ug/L 2000 106 60-140111 4200033824502550
o-Xylene ug/L 2000 104 60-140111 32000263047004850
sec-Butylbenzene ug/L 2000 112 60-140117 42000ND22402330
Styrene ug/L 2000 108 60-140108 02000ND21502150
tert-Butylbenzene ug/L 2000 94 60-14096 22000ND18801920
Tetrachloroethene ug/L 2000 112 60-140113 12000ND22402260
Toluene ug/L 2000 68 60-14085 22000116001300013300
trans-1,2-Dichloroethene ug/L 2000 103 60-140104 22000ND20502080
trans-1,3-Dichloropropene ug/L 2000 100 60-140102 22000ND20002050
Trichloroethene ug/L 2000 113 60-140111 12000ND22602230
Trichlorofluoromethane ug/L 2000 106 60-140119 112000ND21302380
Vinyl chloride ug/L 2000 114 60-140121 62000ND22802420
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689213
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92596442002, 92596442003, 92596442004, 92596442005, 92596442006, 92596442008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3601549
Associated Lab Samples:92596442002, 92596442003, 92596442004, 92596442005, 92596442006, 92596442008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/04/22 21:36
1,1,1-Trichloroethane ug/L ND 0.50 04/04/22 21:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/04/22 21:36
1,1,2-Trichloroethane ug/L ND 0.50 04/04/22 21:36
1,1-Dichloroethane ug/L ND 0.50 04/04/22 21:36
1,1-Dichloroethene ug/L ND 0.50 04/04/22 21:36
1,1-Dichloropropene ug/L ND 0.50 04/04/22 21:36
1,2,3-Trichlorobenzene ug/L ND 2.0 04/04/22 21:36
1,2,3-Trichloropropane ug/L ND 0.50 04/04/22 21:36
1,2,4-Trichlorobenzene ug/L ND 2.0 04/04/22 21:36
1,2,4-Trimethylbenzene ug/L ND 0.50 04/04/22 21:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/04/22 21:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/04/22 21:36
1,2-Dichlorobenzene ug/L ND 0.50 04/04/22 21:36
1,2-Dichloroethane ug/L ND 0.50 04/04/22 21:36
1,2-Dichloropropane ug/L ND 0.50 04/04/22 21:36
1,3,5-Trimethylbenzene ug/L ND 0.50 04/04/22 21:36
1,3-Dichlorobenzene ug/L ND 0.50 04/04/22 21:36
1,3-Dichloropropane ug/L ND 0.50 04/04/22 21:36
1,4-Dichlorobenzene ug/L ND 0.50 04/04/22 21:36
2,2-Dichloropropane ug/L ND 0.50 04/04/22 21:36
2-Chlorotoluene ug/L ND 0.50 04/04/22 21:36
4-Chlorotoluene ug/L ND 0.50 04/04/22 21:36
Benzene ug/L ND 0.50 04/04/22 21:36
Bromobenzene ug/L ND 0.50 04/04/22 21:36
Bromochloromethane ug/L ND 0.50 04/04/22 21:36
Bromodichloromethane ug/L ND 0.50 04/04/22 21:36
Bromoform ug/L ND 0.50 04/04/22 21:36
Bromomethane ug/L ND 5.0 04/04/22 21:36
Carbon tetrachloride ug/L ND 0.50 04/04/22 21:36
Chlorobenzene ug/L ND 0.50 04/04/22 21:36
Chloroethane ug/L ND 1.0 04/04/22 21:36
Chloroform ug/L ND 0.50 04/04/22 21:36
Chloromethane ug/L ND 1.0 04/04/22 21:36
cis-1,2-Dichloroethene ug/L ND 0.50 04/04/22 21:36
cis-1,3-Dichloropropene ug/L ND 0.50 04/04/22 21:36
Dibromochloromethane ug/L ND 0.50 04/04/22 21:36
Dibromomethane ug/L ND 0.50 04/04/22 21:36
Dichlorodifluoromethane ug/L ND 0.50 IH04/04/22 21:36
Diisopropyl ether ug/L ND 0.50 04/04/22 21:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3601549
Associated Lab Samples:92596442002, 92596442003, 92596442004, 92596442005, 92596442006, 92596442008
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 04/04/22 21:36
Hexachloro-1,3-butadiene ug/L ND 2.0 04/04/22 21:36
Isopropylbenzene (Cumene)ug/L ND 0.50 04/04/22 21:36
m&p-Xylene ug/L ND 1.0 04/04/22 21:36
Methyl-tert-butyl ether ug/L ND 0.50 04/04/22 21:36
Methylene Chloride ug/L ND 2.0 04/04/22 21:36
n-Butylbenzene ug/L ND 0.50 04/04/22 21:36
n-Propylbenzene ug/L ND 0.50 04/04/22 21:36
Naphthalene ug/L ND 2.0 04/04/22 21:36
o-Xylene ug/L ND 0.50 04/04/22 21:36
sec-Butylbenzene ug/L ND 0.50 04/04/22 21:36
Styrene ug/L ND 0.50 04/04/22 21:36
tert-Butylbenzene ug/L ND 0.50 04/04/22 21:36
Tetrachloroethene ug/L ND 0.50 04/04/22 21:36
Toluene ug/L ND 0.50 04/04/22 21:36
trans-1,2-Dichloroethene ug/L ND 0.50 04/04/22 21:36
trans-1,3-Dichloropropene ug/L ND 0.50 04/04/22 21:36
Trichloroethene ug/L ND 0.50 04/04/22 21:36
Trichlorofluoromethane ug/L ND 1.0 04/04/22 21:36
Vinyl chloride ug/L ND 1.0 04/04/22 21:36
1,2-Dichloroethane-d4 (S)%108 70-130 04/04/22 21:36
4-Bromofluorobenzene (S)%107 70-130 04/04/22 21:36
Toluene-d8 (S)%101 70-130 04/04/22 21:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3601550LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 60-140
1,1,1-Trichloroethane ug/L 52.550 105 60-140
1,1,2,2-Tetrachloroethane ug/L 50.250 100 60-140
1,1,2-Trichloroethane ug/L 50.850 102 60-140
1,1-Dichloroethane ug/L 47.350 95 60-140
1,1-Dichloroethene ug/L 51.250 102 60-140
1,1-Dichloropropene ug/L 51.250 102 60-140
1,2,3-Trichlorobenzene ug/L 53.050 106 60-140
1,2,3-Trichloropropane ug/L 48.250 96 60-140
1,2,4-Trichlorobenzene ug/L 54.050 108 60-140
1,2,4-Trimethylbenzene ug/L 52.150 104 60-140
1,2-Dibromo-3-chloropropane ug/L 52.150 104 60-140
1,2-Dibromoethane (EDB)ug/L 52.050 104 60-140
1,2-Dichlorobenzene ug/L 52.450 105 60-140
1,2-Dichloroethane ug/L 47.650 95 60-140
1,2-Dichloropropane ug/L 50.950 102 60-140
1,3,5-Trimethylbenzene ug/L 52.250 104 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3601550LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 52.850 106 60-140
1,3-Dichloropropane ug/L 48.550 97 60-140
1,4-Dichlorobenzene ug/L 51.150 102 60-140
2,2-Dichloropropane ug/L 54.950 110 60-140
2-Chlorotoluene ug/L 49.950 100 60-140
4-Chlorotoluene ug/L 51.750 103 60-140
Benzene ug/L 45.950 92 60-140
Bromobenzene ug/L 49.550 99 60-140
Bromochloromethane ug/L 40.450 81 60-140
Bromodichloromethane ug/L 51.850 104 60-140
Bromoform ug/L 49.350 99 60-140
Bromomethane ug/L 46.950 94 60-140
Carbon tetrachloride ug/L 63.950 128 60-140
Chlorobenzene ug/L 48.750 97 60-140
Chloroethane ug/L 55.050 110 60-140
Chloroform ug/L 48.950 98 60-140
Chloromethane ug/L 53.650 107 60-140
cis-1,2-Dichloroethene ug/L 48.350 97 60-140
cis-1,3-Dichloropropene ug/L 52.550 105 60-140
Dibromochloromethane ug/L 50.950 102 60-140
Dibromomethane ug/L 52.850 106 60-140
Dichlorodifluoromethane ug/L 113 IH,L15022660-140
Diisopropyl ether ug/L 49.450 99 60-140
Ethylbenzene ug/L 47.450 95 60-140
Hexachloro-1,3-butadiene ug/L 58.050 116 60-140
Isopropylbenzene (Cumene)ug/L 47.250 94 60-140
m&p-Xylene ug/L 98.6100 99 60-140
Methyl-tert-butyl ether ug/L 51.650 103 60-140
Methylene Chloride ug/L 51.650 103 60-140
n-Butylbenzene ug/L 56.650 113 60-140
n-Propylbenzene ug/L 51.850 104 60-140
Naphthalene ug/L 55.550 111 60-140
o-Xylene ug/L 49.450 99 60-140
sec-Butylbenzene ug/L 54.550 109 60-140
Styrene ug/L 48.550 97 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 51.950 104 60-140
Toluene ug/L 47.250 94 60-140
trans-1,2-Dichloroethene ug/L 50.050 100 60-140
trans-1,3-Dichloropropene ug/L 52.350 105 60-140
Trichloroethene ug/L 50.650 101 60-140
Trichlorofluoromethane ug/L 53.050 106 60-140
Vinyl chloride ug/L 56.650 113 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3601551MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596441001
3601552
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 250 111 60-140113 2250ND277282
1,1,1-Trichloroethane ug/L 250 125 60-140114 9250ND312285
1,1,2,2-Tetrachloroethane ug/L 250 104 60-140104 0250ND260260
1,1,2-Trichloroethane ug/L 250 109 60-140107 2250ND272268
1,1-Dichloroethane ug/L 250 112 60-140106 5250ND279264
1,1-Dichloroethene ug/L 250 138 60-140121 13250ND345303
1,1-Dichloropropene ug/L 250 131 60-140113 14250ND328284
1,2,3-Trichlorobenzene ug/L 250 99 60-14099 0250ND249247
1,2,3-Trichloropropane ug/L 250 101 60-140105 4250ND252264
1,2,4-Trichlorobenzene ug/L 250 105 60-140106 1250ND261264
1,2,4-Trimethylbenzene ug/L 250 109 60-140104 42508.8 281 269
1,2-Dibromo-3-chloropropane ug/L 250 92 60-14097 5250ND231242
1,2-Dibromoethane (EDB)ug/L 250 111 60-140111 0250ND278277
1,2-Dichlorobenzene ug/L 250 110 60-140102 7250ND274256
1,2-Dichloroethane ug/L 250 110 60-140107 32501.3 277 269
1,2-Dichloropropane ug/L 250 119 60-140112 6250ND297280
1,3,5-Trimethylbenzene ug/L 250 114 60-140108 52505.8 292 277
1,3-Dichlorobenzene ug/L 250 112 60-140110 2250ND279275
1,3-Dichloropropane ug/L 250 107 60-140107 0250ND269268
1,4-Dichlorobenzene ug/L 250 101 60-140103 2250ND252257
2,2-Dichloropropane ug/L 250 119 60-140104 14250ND298260
2-Chlorotoluene ug/L 250 112 60-140107 4250ND279269
4-Chlorotoluene ug/L 250 110 60-140107 3250ND276268
Benzene ug/L 250 705 60-140669 525049.8 1810 1720
Bromobenzene ug/L 250 114 60-140108 6250ND286269
Bromochloromethane ug/L 250 113 60-140101 10250ND281254
Bromodichloromethane ug/L 250 116 60-140114 2250ND289284
Bromoform ug/L 250 95 60-14098 3250ND238246
Bromomethane ug/L 250 93 60-14090 3250ND232226
Carbon tetrachloride ug/L M125015860-140144 9250ND395361
Chlorobenzene ug/L 250 110 60-140112 2250ND275281
Chloroethane ug/L M125014160-140134 6250ND353334
Chloroform ug/L 250 118 60-140109 8250ND296272
Chloromethane ug/L 250 132 60-140120 9250ND329300
cis-1,2-Dichloroethene ug/L 250 112 60-140108 4250ND279269
cis-1,3-Dichloropropene ug/L 250 113 60-140115 2250ND283289
Dibromochloromethane ug/L 250 114 60-140117 2250ND286293
Dibromomethane ug/L 250 111 60-140121 9250ND277303
Dichlorodifluoromethane ug/L IH,M0,R125034460-140190 58250ND860475
Diisopropyl ether ug/L 250 114 60-140111 225025.1 310 303
Ethylbenzene ug/L 250 111 60-140109 2250ND278273
Hexachloro-1,3-butadiene ug/L 250 129 60-140125 3250ND323313
Isopropylbenzene (Cumene)ug/L 250 128 60-140124 32500.69 321 310
m&p-Xylene ug/L 500 114 60-140109 450020.4 590 568
Methyl-tert-butyl ether ug/L 250 100 60-14094 525058.5 309 294
Methylene Chloride ug/L 250 131 60-140124 5250ND327311
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92596442
The Spot
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3601551MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92596441001
3601552
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 250 123 60-140114 8250ND306284
n-Propylbenzene ug/L 250 115 60-140109 6250ND288272
Naphthalene ug/L 250 93 60-14099 62504.4 237 251
o-Xylene ug/L 250 108 60-14099 725026.6 296 275
sec-Butylbenzene ug/L 250 126 60-140113 11250ND315283
Styrene ug/L 250 109 60-140106 3250ND272265
tert-Butylbenzene ug/L 250 104 60-14096 8250ND259239
Tetrachloroethene ug/L 250 116 60-140113 2250ND290283
Toluene ug/L 250 109 60-140107 2250ND272267
trans-1,2-Dichloroethene ug/L 250 124 60-140109 13250ND309272
trans-1,3-Dichloropropene ug/L 250 107 60-140108 1250ND268271
Trichloroethene ug/L 250 127 60-140116 9250ND318290
Trichlorofluoromethane ug/L M1,R125015660-140112 33250ND391280
Vinyl chloride ug/L M125014660-140118 21250ND365296
1,2-Dichloroethane-d4 (S)%108 70-130106
4-Bromofluorobenzene (S)%102 70-130102
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 43
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92596442
The Spot
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92596442
The Spot
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92596442001 688853MW-1 SM 6200B
92596442002 689213MW-2 SM 6200B
92596442003 689213MW-3 SM 6200B
92596442004 689213MW-4 SM 6200B
92596442005 689213MW-5 SM 6200B
92596442006 689213MW-6 SM 6200B
92596442007 688853MW-7 SM 6200B
92596442008 689213MW-8 SM 6200B
92596442009 688853WSW-1 SM 6200B
92596442010 688913WSW-2 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/27/2022 03:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 43
Page 41 of 43
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