AS-3647_28783_CA_MRP_20231127

CES of NC PLLC
1701 Shenandoah Avenue, NW Roanoke, VA 24017 540.343.6256 [office]
540.343.6259 [facsimile]

November 28, 2023 Ms. Maura Clark
NCDEQ / DWM / UST Section 2090 US Highway 70 Swannanoa, NC 28778
RE: Groundwater Monitoring Report Roadrunner #135 202 NC Highway 9 Black Mountain, North Carolina 28711 NCDEQ UST Incident No. 28783 CES Project No. 9.1130 Dear Ms. Clark: CES of NC, PLLC (CES) on behalf of GPM Southeast, LLC is submitting the enclosed “Groundwater
Monitoring Report” for the referenced site for your review and approval. This report summarizes groundwater monitoring activities conducted by CES in November of 2023. If you have any questions or comments pertaining to this project, please feel free to contact the undersigned at [phone].
Sincerely, CES OF NC, PLLC
Daniel Fisher, PMP Operations Manager cc: Mr. Rolfe Lann, GPM Southeast, LLC

GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783
Roadrunner #135

GROUNDWATER MONITORING REPORT
NOVEMBER 2023

ROADRUNNER #135 202 NC HIGHWAY 9 BLACK MOUNTAIN, NORTH CAROLINA 28711 FACILITY ID: 32291 UST INCIDENT NO.: 28783
CES PROJECT NUMBER: 9.1130 NOVEMBER 28, 2023
PREPARED BY: CES OF NC, PLLC 1701 Shenandoah Avenue, NW Roanoke, VA 24017 Phone: [phone]; Fax: [phone]
PREPARED FOR: GPM SOUTHEAST, LLC Mr. Rolfe Lann Vice President of Environmental 8565 Magellan Parkway, Suite 400 Richmond, Virginia 23227
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
Ms. Maura Clark Division of Waste Management Underground Storage Tank Section
2090 US Highway 70 Swannanoa, North Carolina 28788
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT i
GROUNDWATER MONITORING REPORT
SITE INFORMATION
Site Identification Date of Report: November 28, 2023 Site Name: Roadrunner #135 202 NC Highway 9
Black Mountain, North Carolina 28711 Facility I.D.: 00-0-0000032291 UST Incident Number: 28783 UST Number: AS-3647 Risk Rank: Intermediate (I 180 A) Latitude: 35.614272 Longitude: -82.319364 Source: UST Database Description of Geographical Data Point: Google Earth Site Contact Information UST Owner: GPM Southeast, LLC UST Operator: GPM Southeast, LLC Address: 8565 Magellan Pkwy, Ste 400 8565 Magellan Pkwy, Ste 400
Richmond, VA 23227 Richmond, VA 23227 Telephone: [phone] [phone] Email: [e-mail] [e-mail] Property Property Owner: BMRR, LLC Occupant: Roadrunner Market (Shell Gas) Address: 11 N. Market Street 202 NC Highway 9 Ashville, NC 28801 Black Mountain, NC 28711 Telephone: Not Available 828-669-5086 Email: Not Available Not Available Consultant: CES of NC, PLLC State License No. C-550 Address: 1701 Shenandoah Avenue, NW Roanoke, VA 24017
Telephone: [phone] Email: [e-mail] Laboratory: Pace Analytical Services, LLC State Certification No. 329 Address: 9800 Kincey Avenue, Ste 100 Huntersville, NC 28078 Telephone: [phone] Email: [e-mail] Release Information Date Discovered: November 12, 2009 Estimated Quantity: Undetermined Cause of Release: Assumed UST system Source of Release: Assumed UST system UST Information: Three (3) 10,000-gallon gasoline

GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT ii
EXECUTIVE SUMMARY
As required, the following executive summary provides the most pertinent information for this assessment.
For additional information please refer to subsequent sections of this report.
• CES of NC, PLLC (CES) was retained by GPM Southeast, LLC (GPM) to complete a limited groundwater monitoring event. The activities were requested in a “Notice of Regulatory Requirements” dated August 30, 2023, issued by the North Carolina Department of Environmental
Quality (NCDEQ). The services were provided in general accordance with the NCDEQ Underground Storage Tank (UST) Section “Assessment Guidelines” and “Corrective Action Guidelines”.

• Historical site activities include a Site Check and Initial Abatement Activities, a Limited Site Assessment (LSA), a Comprehensive Site Assessment (CSA), and multiple groundwater monitoring events. The previous groundwater monitoring event was performed in June of 2023, which indicated groundwater contamination remained above regulatory standards.

• CES personnel mobilized to the site on November 3, 2023, for completion of a limited groundwater monitoring event. Monitoring wells MW-1RA, MW-2, MW-3, MW-4, and MW-5 were sampled for volatile organic compounds (VOCs) by Standard Method 6200B. Free product was not encountered during the November 2023 monitoring event.

• Groundwater samples collected from site monitoring wells indicated groundwater impacts that exceeded the groundwater quality standards defined in Title 15A of the North Carolina Administrative Code (NCAC), subchapter 2L, Section .0202 (2L Standards) in monitoring wells MW-1RA, MW-3, MW-4, and MW-5 for benzene, toluene, ethylbenzene and xylenes (collectively
referred to as “BTEX”), methyl tert butyl ether (MTBE), and naphthalene. Samples from the November 2023 groundwater sampling event did not exceed the applicable gross contamination levels (GCL).

• Groundwater flow was generally interpreted to flow overall towards the south with an estimated horizontal hydraulic gradient of 0.0128 feet/foot during the November 2023 sampling event.
• The contaminant mass of BTEX is estimated to be 40.1 lbs.
• In conclusion, CES will complete the requested NCDEQ soil excavation activities and recommends conducting semi-annual groundwater monitoring for an additional year to monitor seasonal fluctuations and distribution trends.
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT iii
TABLE OF CONTENTS
Site Information ............................................................................................................................................. i
Executive Summary ...................................................................................................................................... ii List of Exhibits ............................................................................................................................................. iii List of Figures .............................................................................................................................................. iii
List of Tables ............................................................................................................................................... iv List of Appendices ....................................................................................................................................... iv 1.0 Introduction ...................................................................................................................................... 1 2.0 Site History and Characterization .................................................................................................... 1 2.1 Site Location ................................................................................................................................. 1 2.2 Current Facility Status .................................................................................................................. 1 2.3 Site History ................................................................................................................................... 1 2.4 Site Geology and Hydrogeology ................................................................................................... 2 3.0 Potential Receptor Information ........................................................................................................ 2 3.1 Water Supply Wells ...................................................................................................................... 3 3.2 Public Water Supplies ................................................................................................................... 3 3.3 Surface Water ................................................................................................................................ 3 3.4 Wellhead Protection Area ............................................................................................................. 3 3.5 Deep Aquifers in the Coastal Plain Physiographic Province ........................................................ 3
3.6 Subsurface Structures .................................................................................................................... 3 3.7 Property Owners and Occupants ................................................................................................... 3 3.8 Sensitive Land Use Features ......................................................................................................... 3
3.9 Surrounding Land Use .................................................................................................................. 3 4.0 Recent Activities .............................................................................................................................. 4 4.1 Groundwater Sampling ................................................................................................................. 4 4.2 Groundwater Occurrence and Flow Direction .............................................................................. 4 4.3 Laboratory Results ........................................................................................................................ 4 4.4 Estimated Extent of Contamination .............................................................................................. 5 4.5 Evaluation of Contaminant Mass ............................................................................................... 6 5.0 Conclusions and Recommendations ................................................................................................ 7 5.1 Conclusions ................................................................................................................................... 7 5.2 Recommendations ......................................................................................................................... 7 6.0 Statements and Certification ......................................................................................................... 8 7.0 Remarks ........................................................................................................................................... 9 8.0 References ........................................................................................................................................ 9
LIST OF EXHIBITS
Exhibit 1 – Maximum Detected Concentrations for Soil Compared to Cleanup Goals ............................... 5 Exhibit 2 – Summary of Maximum Groundwater Contaminant Concentrations .......................................... 6 LIST OF FIGURES
Figure 1 Site Location Map Figure 2 Site Map Figure 3 Site Vicinity Map Figure 4 Soil Analytical Results (6/28/2023) Figure 5 Potentiometric Map (11/3/2023) Figure 6A Estimated Horizontal Extent of Benzene Above 2L Standards
Figure 6B Estimated Horizontal Extent of Toluene Above 2L Standards Figure 6C Estimated Horizontal Extent of Ethylbenzene Above 2L Standards
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT iv
Figure 6D Estimated Horizontal Extent of Total Xylenes Above 2L Standards
Figure 6E Estimated Horizontal Extent of MTBE Above 2L Standards Figure 7 Cross Section Locations Figure 8A Cross Section A-A’
Figure 8B Cross Section B-B’ LIST OF TABLES
Table 1 UST System and Other Release Information Table 2 UST System Owner/Operator Information Table 3 Summary of Soil Analytical Results Table 4 Adjacent Properties and Receptor Data Table 5 Summary of Recent Groundwater Gauging and Well Construction Data Table 6 Summary of Groundwater Analytical Data Table 7 Natural Attenuation Groundwater Data Table 8 Determination of Contaminant Mass LIST OF APPENDICES
Appendix A Recent Correspondence Appendix B Laboratory Analytical Report(s) and Chain of Custody Documentation Appendix C Trend Graph
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 1
1.0 INTRODUCTION
The purpose of this report is to provide the details of groundwater monitoring activities associated with an
assumed release from a UST system at the Roadrunner #135 facility located at 202 NC Highway 9 in Black Mountain, North Carolina (site). The release was confirmed to the NCDEQ on December 3, 2009 and assigned Incident number 28783.
In correspondence dated August 30, 2023, the NCDEQ directed the responsible party, GPM, to proceed with groundwater monitoring activities. GPM retained CES for these environmental consulting services. The services were provided in general accordance with the NCDEQ UST Section “Assessment Guidelines” and “Corrective Action Guidelines”. 2.0 SITE HISTORY AND CHARACTERIZATION
Historically, the site has been owned and operated by Mountain Empire Oil Company (the predecessor by merger of GPM Southeast, LLC, known as GPM). The site has operated a UST system since at least 1990. Historical UST system information and owner/operator and other responsible party information is
summarized in Tables 1 & 2. As required, the following provides information relevant to site history and characterization. Detailed site history and characterization has been provided in previous reports.
2.1 SITE LOCATION The site is located at the southwest corner of the intersection of NC Highway 9 and Vance Avenue in Black Mountain, Buncombe County, North Carolina. Figure 1 is a topographic map depicting the site location and Figure 2 is a site map illustrating pertinent site features. The site vicinity is shown on Figure 3. 2.2 CURRENT FACILITY STATUS The property is owned by BMRR, LLC and is operated by GPM as Roadrunner #135, a convenience store and Shell-branded retail petroleum fuel outlet, which currently maintains three (3) 10,000-gallon gasoline USTs. GPM owns and operates the current registered USTs. According to GPM and based upon observation by CES personnel, the current UST system is in operation.
Improvements on site include a one-story convenience store building, four (4) double-sided petroleum product dispensers, and associated canopy with paved parking areas. 2.3 SITE HISTORY Mountain Environmental conducted Site Check soil boring and sampling activities at the site on November 12, 2009. Sampling activities were conducted as a result of an NCDEQ directive included with correspondence from Ms. Ter Spinner dated October 6, 2009. As part of the Site Check activities, five (5) soil samples were collected from locations around the UST basin on November 12, 2009. These samples
were collected from soil at a depth of approximately 3 to 5-feet below ground surface (bgs). All samples for this event were submitted for gasoline range organics (GRO) analysis. Results ranged from below reportable limits in sample S-5 to 5,030 mg/kg in sample S-4. An Initial Abatement Activities Report
(IAAR) was submitted in September 2010. Groundwater monitoring well MW-1 was installed as part of Limited Site Assessment (LSA) activities on
October 5, 2010. A subsequent soil sample immediately adjacent to MW-1 was collected from just above the water table on October 12, 2010. This sample was analyzed for volatile organic compounds (VOCs) by Environmental Protection Agency (EPA) Method 8260 and for volatile petroleum hydrocarbons (VPH) by the Massachusetts Department of Environmental Protection (MADEP) Method. Results indicated that VOC and VPH parameters exceeded the soil to groundwater maximum soil contaminant concentrations (MSCCs).
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 2
A groundwater sample was collected from monitoring well MW-1 on October 18, 2010. The sample was
analyzed for VOCs by EPA Method 6200B. Results indicated that ten (10) VOC parameters exceeded the groundwater quality standards defined in Title 15A of the North Carolina Administrative Code (NCAC), subchapter 2L, Section .0202 (2L Standards). In addition, benzene and methyl-tert-butyl ether (MTBE)
exceeded the GCLs at concentrations of 8,930 micrograms per liter (µg/L) and 47,800 µg/L, respectively. The LSA Report was submitted on November 30, 2010. Based on the receptor survey conducted as part of the LSA activities, the site was classified as an intermediate risk site due to the proximity of the Swannanoa River and the on-site dissolved benzene concentration exceeding the surface water standard by a factor of 10. As part of the Comprehensive Site Assessment (CSA) activities, an additional eight (8) monitoring wells, MW-2 through MW-9, were installed to assess the dissolved petroleum impact in groundwater at the site. Soil samples were collected at the five-foot sampling intervals for each monitoring well and analyzed for VOCs and VPH. VOCs were detected in the first five-foot interval from the borings for monitoring wells
MW-3 and MW-4. All other samples were below applicable standards. Groundwater sampling conducted for monitoring wells MW-1 through MW-9 on September 29, 2011, indicated VOC and VPH analytes present above the 2L Standards in MW-1, MW-3, MW-4, MW-5, and MW-6. The CSA Report was
submitted to NCDEQ on November 11, 2011. Historic soil data is summarized in Table 3 and depicted in Figure 4.
Multiple groundwater monitoring events have been conducted at the site since 2012 with free product occasionally present in monitoring well, MW-5. The previous groundwater monitoring event was performed in June of 2023 in which groundwater contamination remained above the 2L regulatory standards in MW-1R, MW-3, MW-4, and MW-5.
2.4 SITE GEOLOGY AND HYDROGEOLOGY The subject site is located in the Inner Piedmont Physiographic Province of western North Carolina. Mountain Environmental reviewed the Geologic Map of North Carolina (NC Department of Natural Resources and Community Development – 1985) for information regarding site bedrock geology. Bedrock at the subject property consists of rocks from the Asheville Metamorphic Suite. Rock types include ‘Metagraywacke – foliated to massive, locally conglomeratic; interlayered and gradational with mica schist,
muscovite-biotite gneiss and rare graphitic schist.’ Bedrock was not encountered during drilling activities. As reported in the CSA, the horizontal groundwater seepage velocity ranged from 0.019 feet per day (ft/day)
to 0.027 ft/day. This was estimated based upon an effective porosity of 0.35 and a hydraulic conductivity range of 0.52 to 0.74 ft/day. Hydraulic conductivity was determined through a series of rising head slug tests performed in monitoring wells, MW-3 and MW-5 and evaluated with the Bouwer and Rice equation.
These calculated hydraulic properties are indicative only of the areas immediately adjacent to the tested wells and may not reflect conditions throughout the upper portion of the regional aquifer, nor do they describe aquifer characteristics of the competent bedrock beneath the site.
3.0 POTENTIAL RECEPTOR INFORMATION
Potential receptors were evaluated based on available information and current site conditions as discussed below. Receptor information is summarized in Table 4 with receptor identification and location tied to the
site vicinity map included as Figure 3.

GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 3
3.1 WATER SUPPLY WELLS
During November 2010, Mountain Environmental personnel performed a water supply well survey and sensitive receptor update within a 1,000-foot radius of the site by mailing well survey forms to all property owners within a 500-foot radius of the site, visually observing surrounding properties for wells and water
meter connections and interviewing local residents. Based on the visual receptor survey and returned water supply well information sheet(s), no active water supply wells were identified within 1,000 feet of the source area. One (1) abandoned public water supply well owned by the Town of Black Mountain is located approximately 900-feet northwest of the source area. 3.2 PUBLIC WATER SUPPLIES Municipal water is available to the site and surrounding community by the Town of Black Mountain. 3.3 SURFACE WATER CES reviewed a USGS 7.5-minute quadrangle topographic map (Figure 1) to identify potential surface water bodies in the vicinity of the site. Site reconnaissance and topographic map review identified one (1)
surface water body within 1,500-feet of the site. The nearest surface water body is the Swannanoa River located approximately 420-feet south of the source area. 3.4 WELLHEAD PROTECTION AREA According to the NCDEQ Division of Water Resources Source Water Assessment Program (DWR SWAP) website, the source area is reportedly not located within an approved wellhead protection area.
3.5 DEEP AQUIFERS IN THE COASTAL PLAIN PHYSIOGRAPHIC PROVINCE The risk classification criteria specified in Title 15A of the NCAC, Subchapter 2L, Section .01159(d) requires an evaluation for the presence of unconfined or semi-confined deep aquifers in the Coastal Plain region of North Carolina, which may be used as a source of drinking water. According to the September 29, 2015 “Physiographic Provinces of NC” map, the site is not located within the Coastal Plain Physiographic Province. 3.6 SUBSURFACE STRUCTURES Subsurface water, sewer, and natural gas lines are present in the subsurface at the site. 3.7 PROPERTY OWNERS AND OCCUPANTS The site currently contains an active commercial convenience store with retail petroleum sales. Nine (9) contiguous properties are abutting the site as summarized in Table 4 and labeled on Figure 3. The site and
abutting properties are utilized for commercial purposes. 3.8 SENSITIVE LAND USE FEATURES
Sensitive land use features are defined by the NCDEQ as schools, daycare centers, nursing homes, hospitals, playgrounds, parks and recreation areas, churches, camps, and other places of public assembly. Based on the available information, the nearest specific sensitive land use feature is the trailhead for the River Walk
Park located approximately 920-feet east of the site. A public splash park is located approximately 1,350 feet north of the site. The Black Mountain Public Library and the Harwood Home for Funeral and Cremation Services are located approximately 1,000 feet northwest of the site while the Grace and Knowledge Community Church is located approximately 775 feet southwest of the site. 3.9 SURROUNDING LAND USE The subject site is a commercial service station and convenience store and is located in an area of Black Mountain that is commercially developed with retail shopping and dining facilities and some surrounding residential areas.
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 4
4.0 RECENT ACTIVITIES
CES has performed a limited groundwater monitoring event in accordance with the NCDEQ approved
pre-approval task authorization (PATA) 28783-24. A copy of the approved PATA form is included in Appendix A.
4.1 GROUNDWATER SAMPLING CES mobilized to the site on November 3, 2023, to conduct a groundwater monitoring event. Monitoring wells MW-1RA and MW-2 through MW-5 were located, accessed, and gauged for
equilibrated depth to water/depth to product (as applicable) and total well depth using an electronic oil-water interface probe. A summary of well construction and recent gauging data is included in Table 5. Following gauging, each monitoring well was purged of at least three (3) well volumes, or until dry, using dedicated disposable bailers. The bailer was gently lowered into the water column of the well and allowed to fill, then raised to the surface and evacuated. This process was repeated until the necessary volume of water had been removed from the well. To reduce the potential of cross contamination, new, clean, disposable nitrile gloves were worn during all phases of sample handing. Samples were placed into laboratory supplied containers pre-filled with appropriate preservatives, labeled with indelible ink, entered onto a chain-of-custody form, and immediately placed on wet ice in laboratory
supplied coolers maintained at approximately four (4) degrees Celsius pending transportation. The samples were transported under standard chain-of-custody protocol to Pace Analytical Services located in Huntersville, North Carolina, a North Carolina certified laboratory, for chemical analysis. The samples were analyzed for volatile organic compounds (VOCs) including MTBE, IPE, and EDB by Standard Method 6200B.
4.2 GROUNDWATER OCCURRENCE AND FLOW DIRECTION Depth to groundwater in the gauged monitoring wells ranged from 3.95-feet below top of casing (MW-5) to 7.33-feet below top of casing (MW-2). Groundwater elevations were calculated to range from 91.66-feet
(MW-2) to 90.19-feet (MW-5) relative to a common benchmark with an assumed elevation of 100.00 feet. A summary of groundwater gauging data is provided in Table 5. Based on this data, groundwater flow direction was generally interpreted to be overall towards the south as illustrated on Figure 5. The groundwater flow direction is generally consistent with historical assessments. The hydraulic gradient (i) was derived based on the referenced potentiometric map. The gradient was calculated based on the change in head over the horizontal distance between monitoring wells. For the purposes of the gradient calculations, MW-1RA was utilized as the up-gradient location and MW-5 is
utilized as the down-gradient location. Change in head (h): 91.30 (MW-1RA) to 90.19 (MW-5) = 1.11-feet
Horizontal distance (L): 86.396-feet i = h/L = (1.11-feet/86.396-feet) = 0.0128
4.3 LABORATORY RESULTS Laboratory analytical results were compared to the 2L Standards and GCLs. Upon review of the laboratory analytical report, the groundwater samples from monitoring wells MW-1R, MW-3, MW-4 and MW-5 contained concentrations of dissolved phase COCs at levels above 2L Standards.
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 5
A summary of laboratory results for groundwater samples is provided in Table 6. Isoconcentration maps
for BTEX and MTBE are provided in Figure 6A through Figure 6E. The laboratory analytical report and chain of custody documentation are provided in Appendix B.
A trend graph comparing the groundwater elevation to the benzene concentration in monitoring well MW-1/MW-1R/MW-1RA has been included as Appendix C.
4.4 ESTIMATED EXTENT OF CONTAMINATION Soil Soil sampling was conducted at the site on June 28, 2023, when soil samples were collected from nine (9) soil borings. Based on the June 2023 soil sampling, the extent of soil contamination above MSCCs is generally located in the vicinity of the pump islands and east of the UST basin, totaling approximately
13,200 square feet. (Figure 4). Based on historical soil analytical data, the extent of the soil contamination above MSCCs is generally located to the east of the pump islands and south and east of the UST basin. The depth of the soil contamination extends to at least 7-feet bgs, after which point an apparent smear zone is encountered. This equated to a volume of 78,400 cubic feet. Maximum detected concentrations (MDCs) of contaminants of
concern (COCs) and the applicable cleanup goals for soil are summarized below in Exhibit 1: Exhibit 1 – Maximum Detected Concentrations for Soil Compared to Cleanup Goals
COC STW MSCC
Red = above STW MSCC Highlighted = above Ind/Comm MSCC Free Product Free product was not detected during the November 2023 sampling event. Historically, free product has been detected in monitoring well MW-5 at a maximum thickness of 0.60-feet in September 2015 with the last occurrence being in March 2016.
Groundwater Historically, groundwater contamination above 2L Standards has been reported at the locations of MW-1, MW-3, MW-4, MW-5, and MW-6. According to current data, the total extent of groundwater contamination above 2L Standards comprises an approximate 16,780-square foot area beneath the site and likely includes portions of the currently active UST system. The vertical extent of groundwater contamination is unknown.
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 6
The contaminant plume appears to be oriented primarily in a north-south direction with the monitoring well
exhibiting the highest contaminant concentrations being MW-1RA.
During the most recent monitoring event, COCs in groundwater exceeded the 2L Standards at four (4) of
the five (5) locations monitored. The current maximum groundwater contaminant concentrations above regulatory standards observed during the recent reporting period compared to the historical maximum groundwater contaminant concentrations observed are summarized in Exhibit 2 below:
Exhibit 2 – Summary of Maximum Groundwater Contaminant Concentrations
Constituent 2L Standard GCL Maximum Location Maximum Location & Date
1 5,000 MW-1RA MW-1 – 6/5/2013
600 80,000 MW-1RA MW-1 – 6/5/2013
600 260,000 MW-1RA MW-1 – 10/4/2018
500 50,000 MW-1RA MW-1 – 11/3/2023
20 20,000 MW-1RA MW-1 – 6/5/2013 6 6,000 MW-1RA MW-5 – 5/15/2017 70 70,000 45.6 J MW-1RA MW-1 – 6/5/2013 70 30,500 MW-1RA MW-5 – 5/8/2018
70 26,100 MW-1RA MW-5 – 5/8/2018
400 28,500 MW-1RA MW-5 – 5/15/2017
400 24,100 MW-1RA MW-5 – 5/15/2017
Data presented in micrograms per liter (ug/L) Bold = Above 2L Standards Red = Above GCLs A cross section location map is included as Figure 7. Cross sections indicating the current extent of
contamination above regulatory limits and the assumed smear zone thickness based on historical water table elevations are included as Figures 8A and 8B. Estimated horizontal extents of dissolved BTEX and MTBE, are included as Figure 6A through Figure 6E, respectively.
4.5 EVALUATION OF CONTAMINANT MASS Contaminant mass was based on total BTEX. To determine contaminant mass, the average of total BTEX
concentrations from all monitoring well samples containing concentrations above 2L Standards and/or GCLs (affected monitoring wells) were calculated. Estimated horizontal extents of total BTEX contamination in groundwater (as discussed above) were determined by each individual contaminant’s estimated isoconcentration area as shown on Figures 6A through 6D. Approximate volumes were then calculated utilizing the estimated areas, average thickness of contamination as determined from the average water column in each affected monitoring well, and the estimated effective porosity (0.35) as reported in the CSA. The volumes were then multiplied by the individual contaminant concentrations to obtain a mass of each BTEX constituent in the surficial aquifer which was then converted to pounds (lbs.). Please note that this method assumes average isotropic concentrations of BTEX throughout the plume volume, therefore, this method presents a conservative estimate, and the actual BTEX mass may vary across different portions of the site. However, this method is considered effective for evaluation of trend data,
expansion/contraction of the plume, and overall site remediation progress. The current estimated mass of BTEX in groundwater was calculated to be approximately 40.1 lbs. or 18.2
kgs.
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 7
5.0 CONCLUSIONS AND RECOMMENDATIONS

5.1 CONCLUSIONS The following conclusions are presented based upon the data and site-specific information collected and presented in this report:
• Laboratory results from the groundwater monitoring event reported exceedances of 2L Standards in the samples collected from monitoring wells MW-1R, MW-3, MW-4, and MW-5. However, no exceedances to the applicable GCLs were observed during the November 2023 monitoring event.
• An evaluation of contaminant mass revealed the current estimated mass is 40.1-lbs.
• The presence of a surface body of water within 1,000-feet of the site and the occasional presence of benzene above GCLs contribute to the site’s risk ranking.
5.2 RECOMMENDATIONS CES recommends the following:
• Complete requested NCDEQ soil excavation activities to address the soil contamination above the Industrial/Commercial Cleanup Levels.
• Perform semi-annual groundwater sampling for an additional year to monitor seasonal fluctuations and distribution trends.
GROUNDWATER MONITORING REPORT
ROADRUNNER #135
BLACK MOUNTAIN, NORTH CAROLINA
INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 8
6.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. 11/30/2023 Will this report be submitted after
the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was
missing and why.

3 If applicable, will an of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error) YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and outline
proposed remedies. (This should be described in more detail in the report text above.)
Not applicable, milestones have not been determined for the site.
4 Does any known or suspected source zone soil contamination or free product remain outside of the
assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #6 or #7 is “YES”, generally describe in this cell any actions recommended to further
assess or clean up this known or suspected source. (This should be described in more detail in the report text above.)

6 Certification:
I, Rachel A. Raines, a Licensed Geologist for CES of NC, PLLC., do certify that the information contained in this report
is correct and accurate to the best of my knowledge.

Rachel A. Raines, NC PG#2739
Geologist

CES OF NC, PLLC. is licensed to practice geology in North Carolina. The certification number of the company o
corporation is C-550.

GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT 9
7.0 REMARKS
The recommendations contained in this report represent CES’s professional opinions based upon the
currently available information and are arrived at in accordance with currently accepted professional standards. This report is based upon a specific scope of work requested by the client. The contract between CES and its client outlines the scope of work, and only those tasks specifically authorized by that contract
or outlined in this report were performed. This report is intended only for the use of CES’s client and anyone else specifically identified in writing by CES as a user of this report. CES will not and cannot be liable for unauthorized reliance by any other third party. Other than as contained in this paragraph, CES makes no express or implied warranty as to the contents of this report. 8.0 REFERENCES
1. Limited Site Assessment Report, November 30, 2010. Mountain Environmental Group, Canton, NC. 2. Comprehensive Site Assessment Report, November 7, 2011. Mountain Environmental Group, Canton, NC. 3. Groundwater Monitoring Report, April 14, 2020. Appalachian Landslide Consultants, PLLC, Asheville, NC. 4. Groundwater Monitoring and Contaminant Transport Modeling Report, June 10, 2022. Appalachian Landslide Consultants, PLLC, Asheville, NC. 5. NC Source Water Assessment Program Mapping Applications website. North Carolina Department of Environmental Quality, Raleigh, NC. Accessed March 19, 2020.
https://deq.nc.gov/about/divisions/water-resources/drinking-water/drinking-water-protection-program/mapping-applications. 6. Geologic Map of North Carolina (digital version) website. North Carolina Geological Survey,
Raleigh, NC. Accessed March 19, 2020. https://ncdenr.maps.arcgis.com/apps/MapSeries/index.html?appid=0a7ccd9394734ff6aa2434d2528ddf12.
7. Physiographic Provinces of NC website, September 29, 2015. North Carolina Department of Environmental Quality, Raleigh, NC. Accessed March 19, 2020. https://www.arcgis.com/apps/MapSeries/index.html?appid=1316f4eb4e3349298c3bd0063ab8fb89.
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT

FIGURES

FIGURE 1
Site Location Map
Roadrunner #135
202 NC-9
Black Mountain, North Carolina
Black Mountain, North Carolina Project: Groundwater
Monitoring Report
Client: GPM Southeast, LLC
CES NC Job #: 9.1130
Date: 11/15/2023
Latitude:
35°36'51.6"N
Longitude:
82°19'09.9"W
U.S.G.S Topographic Maps of the Black
Mountain & Montreat Quadrangles,
North Carolina, 7.5 Minute Series (2022)
Scale: 1:24,000 Contour Interval: 40 Feet
Source:
National Geodetic Vertical
Datum 1988
Horizontal Datum:North American Datum 1983
Vertical Datum:
1701 Shenandoah Avenue, NW
Roanoke, VA 24017
540-343-6256 (office) 540-343-6259 (fax)
Site Location
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
FOC
FOC
FOC
FOC
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Site Map
Figure 2
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Natural Gas Line
Underground Electric Line
Fiber Optic Line
Telephone Line
FOC
G
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 175'350'700'
1 inch equals 350 feet
Roadrunner #135
Site Vicinity Map
Figure 3
Site
1
2
3
4
5
6
78
9
250 feet
500 feet
1000 feet
1500 feet
Map ID No. corresponds to Table 3 -
Adjacent Properties and Receptor Data
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
S-5
S-1
S-4
S-2
S-3
MW-1R
MW-1RA
SB-1
SB-2
SB-3
SB-4
SB-5
SB-6
SB-7
SB-8SB-9
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Soil Analytical Results (6/28/2023)
Figure 4
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Soil Sample Location (2009)
Dispenser Location
Catch Basin
Total Petroleum Hydrocarbons -
Gasoline Range Organics
Estimated Extent of Soils Exceeding
Soil to Groundwater MSCC
G
GRO
Units: mg/kg (milligrams per kilogram)
Bold indicates exceedance of
Soil to Groundwater MSCC
Bold & Shading indicates exceedance of
Ind/Comm Cleanup Level
Soil Boring Location (2023)
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Potentiometric Map (11/2/2023)
Figure 5
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Groundwater Elevation (feet)
Groundwater Elevation Contour (feet)
Groundwater Flow Direction
G
(91.30)
(91.30)
(91.66)
(91.60)
(90.35)
(90.19)
91.25
91.50
91.00
90.75
90.50
90.25
90.25
90.50
90.75
91.00
91.25
91.50
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Estimated Horizontal Extent of
Benzene above 2L Standards
Figure 6A
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Benzene Concentration
Estimated Benzene
Concentration Contour
G
Units: ug/L (micrograms per liter)
Sampling Date: 11/3/2023
Benzene 2L Standard: 1 ug/L
Benzene GCL: 5,000 ug/L
(4,670)
(<0.079)
(2,060)
(<0.079)
(503)
(NS)
(NS)
(NS)
(NS)
(4,670)1.0
1.0
1.0
Not Sampled(NS)
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Estimated Horizontal Extent of
Toluene above 2L Standards
Figure 6B
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Toluene Concentration
Estimated Toluene
Concentration Contour
G
Units: ug/L (micrograms per liter)
Sampling Date: 11/3/2023
Toluene 2L Standard: 600 ug/L
Toluene GCL: 260,000 ug/L
(22,400)
(<0.090)
(39.4)
(<0.090)
(39.7)
(NS)
(NS)
(NS)
(NS)
(93.02)
600
Not Sampled(NS)
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Estimated Horizontal Extent of
Ethylbenzene above 2L Standards
Figure 6C
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Ethylbenzene Concentration
Estimated Ethylbenzene
Concentration Contour
G
Units: ug/L (micrograms per liter)
Sampling Date: 11/3/2023
Ethylbenzene 2L Standard: 600 ug/L
Ethylbenzene GCL: 80,000 ug/L
(4,460)
(<0.081)
(403)
(<0.081)
(936)
(NS)
(NS)
(NS)
(NS)
(93.02)
600
600
Not Sampled(NS)
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Estimated Horizontal Extent of
Total Xylenes above 2L Standards
Figure 6D
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Total Xylenes Concentration
Estimated Total Xylenes
Concentration Contour
G
Units: ug/L (micrograms per liter)
Sampling Date: 11/3/2023
Total Xylenes 2L Standard: 500 ug/L
Total Xylenes GCL: 50,000 ug/L
(23,600)
(<0.094)
(125)
(<0.094)
(799)
(NS)
(NS)
(NS)
(NS)
(93.02)
500
500
Not Sampled(NS)
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Estimated Horizontal Extent of
MTBE above 2L Standards
Figure 6E
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Methyl-tert-butyl-ether
MTBE Concentration
Estimated MTBE
Concentration Contour
G
Units: ug/L (micrograms per liter)
Sampling Date: 11/3/2023
MTBE 2L Standard: 20 ug/L
MTBE GCL: 20,000 ug/L
(1,780)
(<0.053)
(22.4)
(111)
(442)
(NS)
(NS)
(NS)
(NS)
(93.02)
MTBE
20
20
Not Sampled(NS)
MW-1
MW-4
MW-6
MW-7
MW-9
MW-2
MW-3
MW-8
Roadrunner
#135
canopy
NC
-
9
Vance

A
v
e
n
u
e
Terry E
s
t
a
t
e

D
r
i
v
e
dumpsters
USTs
UST
vents
G
G G
G
MW-1R
MW-1RA
MW-5
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
0 20'40'80'
1 inch equals 40 feet
Roadrunner #135
Cross Section Locations
Figure 7
Legend
Approximate Property Lines
Monitoring Well (MW) Location
Dispenser Location
Catch Basin
Soil Boring Location - 2023
G
A
B
A'
B'
SB-1
SB-2
SB-3
SB-4
SB-5
SB-6
SB-7
SB-8SB-9
MW-2
MW-1RA
MW-4
MW-9
100
95
90
85
80
0 30 60 90 120 150 180 210 240 270
A
A'95
90
85
80
El
e
v
a
t
i
o
n

(
f
e
e
t
)
0 3015
0
2.5
5
Vertical Scale
(feet)
Horizontal Scale
(feet)
Silty Clay
Silty Clay/Sand
with Cobbles
Legend
Monitoring Well
Screen Interval
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
Roadrunner #135
Cross Section A-A'
Figure 8A
Estimated Extent of Soil Exceeding
Soil to Groundwater MSCCs
Estimated Extent of Groundwater
Exceeding 2L Standards
Water Leve
l

-

H
i
g
h
Water Level

-

L
o
w
Water Level - High
Water Level - Low
SB-1
SB-2 SB-4
SB-3
Approximate Soil Sample Location
90
85
80
0 40 80 120 160 200 240 280 320 360
MW-8
MW-3
MW-4
MW-5
MW-6 MW-7
B
B'
100
95
90
85
80
100
95
Ele
v
a
t
i
o
n

(
f
e
e
t
)
0 4020
0
2.5
5
Vertical Scale
(feet)
Horizontal Scale
(feet)
Silty Clay
Silty Clay/Sand
with Cobbles
Legend
Monitoring Well
Screen Interval
Water Level - High
Water Level - Low
CLIENT:
LOCATION:
Groundwater Monitoring Report
202 NC-9
Black Mountain, NC
GPM Southeast, LLC
Roadrunner #135
Cross Section B-B'
Figure 8B
Water Level - High
Water Level - Low
Estimated Extent of Soil Exceeding
Soil to Groundwater MSCCs
Estimated Extent of Groundwater
Exceeding 2L Standards
SB-7
SB-6
SB-3
SB-8
Approximate Soil Sample Location
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT

TABLES

TABLE 1
UST/AST SYSTEM AND OTHER RELEASE INFORMATION
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
UST ID
Number
Current/Last
Contents (in Construction
Details Associated Piping and Date Tank
Installed Status of UST associated with
1 Gasoline 10,000 11/1/1990 Active No
2 Gasoline 10,000 11/1/1990 Active No
3 Gasoline 10,000 11/1/1990 Active No
Incident
Number Discovered Released
28783 11/12/2009 Gasoline
Notes: - UST information provided by NCDEQ Registered Tanks Database
Discovery of Release
Unknown
TABLE 2
UST SYSTEM OWNER/OPERATOR INFORMATION
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
(mm/dd/yy to mm/dd/yy)
1, 2, 3 (Current)32291
28783
GPM Southeast, LLC 11/1/1990 - Present (current USTs)
8565 Magellan Parkway, Suite 400, Richmond, VA 23227 [phone]
8015
Sample ID
Date
Collected
Sample
BGS)Phase
S-1 11/12/2009 3-4'LSA 197 ------------------------------------------
S-4 11/12/2009
S-5 11/12/2009 4-5'LSA BRL ------------------------------------------
149 207 ----885 372 1,190 195 225 1,620 539 83.8 216 NA 216 NA 42.2 NA 42.2
MW-3 0.437 2.16 0.581 0.259 0.581 1.62 --0.34 2.77 0.423 0.56 0.34 51.5 143 NA 143 NA 27.6 NA 27.6
MW-4 3/29/2011 5'CSA NA 0.349 0.0412 0.125 0.0194 0.0067 0.0111 0.0855 0.398 0.0957 0.0588 0.0178 0.0395 0.012 4.6 15 NA 15 NA 2 NA 2
0.285 0.263 ----0.976 0.35 29.2 77.3 NA 77.3 NA 16.4 NA 16.4
MW-8 9/28/2011 5'CSA NA ------------------------------------------
4.09 36.9 7.89 1.31 J 3.68 J 221.1 <0.781 33.6 15.0 68.6 121 37.3 ----------------
0.557 1.19 <0.0533 <0.0528 0.0569 J 3.288 0.228 J <0.167 0.219 J 0.727 1.32 0.369 ----------------
0.0746 J 0.877 0.530 0.0934 J 0.154 J 6.29 0.323 2.07 0.689 0.902 6.19 1.85 ----------------
0.138 J 2.66 1.16 0.269 J 0.485 J 10.64 <0.110 4.97 2.06 0.554 14.0 3.78 ----------------
0.401 1.47 0.561 0.181 J 0.346 1.336 <0.0606 3.68 1.98 0.486 0.388 0.132 J ----------------
0.619 0.805 <0.0552 <0.0546 0.0802 J 2.603 <0.0575 0.231 J 0.194 J 0.765 0.560 0.225 J ----------------
0.0439 J 0.200 J 0.134 J <0.0554 0.0401 J 1.002 <0.0583 0.598 0.174 J 0.372 1.18 0.364 ----------------
0.149 J 2.00 0.624 0.142 J 0.312 J 12.01 <0.0711 1.67 1.23 4.39 8.24 2.20 ----------------
50 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A 24 0.0072 8 2.4 2.2 1.3 6 0.085 0.2 1.4 5.4 6.6 6.6 68 540 31 N/A N/A N/A N/A 31
N/A 210,000 59.4 297 11,600 23,300 23,300 46,700 1,810 27 23,300 18,600 2,330 2,330 9,340 23,300 7,000 N/A N/A N/A N/A 7,000
Notes:
Results in mg/kg (ppm).
ft BGS = feet below ground surface.Bold face type indicates exceedance of most stringent regulatory limit.
NA - Not Analyzed Shading indicates exceedance of Ind/Comm Cleanup Level
BRL - Below Reporting Limit Data from 2009-2011 as presented in the 2011 Comprehensive Site Assessment by Mountain Environmental Group.
To
t
a
l

C
9
-
C
2
2

A
r
o
m
a
t
i
c
s
MADEP Methods
TABLE 3
SUMMARY OF SOIL ANALYTICAL RESULTS
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
VOCs (8260)
n-
B
u
t
y
l
b
e
n
z
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
Analytical Method
Contaminant of Concern
TP
H
-
G
R
O
C1
9
-
C
3
6

A
l
i
p
h
a
t
i
c
s

(
E
P
H
)
C9
-
C
1
0

A
r
o
m
a
t
i
c
s

(
V
P
H
)
C1
1
-
C
2
2

A
r
o
m
a
t
i
c
s

(
E
P
H
)
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
8

A
r
o
m
a
t
i
c
s
To
t
a
l

C
9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
Ind/Comm Cleanup Level (mg/kg)
To
l
u
e
n
e
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Action Level (mg/kg)
Soil to Groundwater MSCC (mg/kg)
Et
h
y
l
b
e
n
z
e
n
e
Ac
e
t
o
n
e
Be
n
z
e
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e

(C
u
m
e
n
e
)
Me
t
h
y
l
-
t
e
r
t

B
u
t
y
l

E
t
h
e
r
Na
p
h
t
h
a
l
e
n
e
TABLE 4
ADJACENT PROPERTIES AND RECEPTOR DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
202 NC Hwy 9 11 N. Market Street
Black Mountain Asheville, NC 28801
200 NC Hwy 9 450 S. Orange Avenue, Ste 300
Black Mountain Orlando, FL 32801
205 NC Hwy 9 P.O. Box 460189
Black Mountain Dept. 203
Houston, TX 77056
Key West, FL 33040
Other Potential Receptors
(other public water supplies, reservoirs, water supply lines, surface water bodies, wellhead protection areas, recharge areas for deep aquifers, subsurface struc
NA Unknown
Site 061935509400000 BMRR, LLC N/A Public Water Service
Water Supply
Information
Map ID
No.
Parcel
Number/Map
Number
Property Owner Owner's Mailing Address Contact Phone
Number
1 061935429300000 National Retail Properties, LP c/o Hertz Equipment Rental N/A Public Water Service
3 061935910600000 Jennifer Shaffer, Gary and
Diane Onderdonk NA Unknown
2 061945331800000 Ingles Black Mountain Exchange, LLC c/o Ryan Tax Compliance Services, LLC NA Unknown
5 061934981600000 c/o Fontaine NA Unknown
4 061934990800000 Town of Black Mountain N/A Public Water ServiceN/A
NA
6 061934578000000 AFN ABSPROP002, LLC NA Unknown
N/A Public Water Service
Map ID
9 061934493700000
Location
BMRR #2, LLC c/o John G.
Kelso
7 061934690200000 Jerome & Diane Morris
061934580800000 Bruce & Sherry Cook, etal c/o
Marsha Pressley NA
A Swannanoa River South N/A 420-feet SN/A
Contact Name
Phone Number
NA
N/A
N/A
Public Water ServiceN/A N/A
8
ContactDescription Area (feet)
Property Address
N/A
NA
NA
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)
11/18/2010 8.00 --------89.91
4/1/2011 5.31 --------92.60
9/29/2011 7.01 --------90.90
4/4/2012 6.28 --------91.63
10/29/2012 6.57 --------91.34
6/5/2013 6.70 --------91.21
7/17/2014 6.33 --------91.58
2/25/2015 6.10 --------91.81
9/22/2015 7.37 --------90.54
3/23/2016 5.50 --------92.41
9/19/2016 6.64 --------91.27
5/15/2017 4.58 --------93.33
10/27/2017 4.61 --------93.30
5/8/2018 4.66 --------93.25
10/4/2018 4.99 --------92.92
5/10/2019 5.01 --------92.90
10/17/2019 5.10 --------92.81
4/1/2020 5.01 --------92.90
11/11/2020 4.98 --------92.93
5/6/2021 5.02 --------92.89
12/6/2021 5.22 --------92.69
4/20/2022 NG NG NG NG
MW-1R 5 - 15 97.68 11/16/2022 4.66 --------93.02
6/29/2023 4.88 --------93.16
11/3/2023 6.74 --------91.30
MW-1 5 - 15 97.91
MW-1RA 3 - 13 98.04
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

4/1/2011 5.57 --------93.42
9/29/2011 7.50 --------91.49
4/4/2012 6.47 --------92.52
10/29/2012 7.23 --------91.76
6/5/2013 5.06 --------93.93
7/17/2014 3.82 --------95.17
2/25/2015 6.45 --------92.54
9/22/2015 8.04 --------90.95
3/23/2016 5.89 --------93.10
9/19/2016 7.25 --------91.74
5/15/2017 4.93 --------94.06
10/27/2017 5.01 --------93.98
5/8/2018 5.09 --------93.90
10/4/2018 5.19 --------93.80
5/10/2019 5.22 --------93.77
10/17/2019 5.34 --------93.65
4/1/2020 4.97 --------94.02
11/11/2020 4.78 --------94.21
5/6/2021 4.81 --------94.18
12/6/2021 4.98 --------94.01
4/20/2022 6.05 --------92.94
11/16/2022 6.19 --------92.80
6/29/2023 5.25 --------93.74
11/3/2023 7.33 --------91.66
MW-2 5 - 15 98.99
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

4/1/2011 4.64 --------93.30
9/29/2011 6.41 --------91.53
4/4/2012 5.25 --------92.69
10/29/2012 5.56 --------92.38
6/5/2013 4.75 --------93.19
7/17/2014 6.29 --------91.65
2/25/2015 5.57 --------92.37
9/22/2015 6.92 --------91.02
3/23/2016 4.90 --------93.04
9/19/2016 5.98 --------91.96
5/15/2017 3.71 --------94.23
10/27/2017 3.73 --------94.21
5/8/2018 3.77 --------94.17
10/4/2018 4.01 --------93.93
5/10/2019 4.08 --------93.86
10/17/2019 4.19 --------93.75
4/1/2020 4.01 --------93.93
11/11/2020 3.97 --------93.97
5/6/2021 4.01 --------93.93
12/6/2021 4.33 --------93.61
4/20/2022 4.44 --------93.50
11/16/2022 4.01 --------93.93
6/29/2023 4.23 --------93.71
11/3/2023 6.34 --------91.60
MW-3 5 - 15 97.94
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

4/1/2011 4.11 --------91.83
9/29/2011 5.24 --------90.70
4/4/2012 4.24 --------91.70
10/29/2012 5.35 --------90.59
6/5/2013 4.99 --------90.95
7/17/2014 4.57 --------91.37
2/25/2015 4.34 --------91.60
9/22/2015 5.62 --------90.32
3/23/2016 3.84 --------92.10
9/19/2016 4.94 --------91.00
5/15/2017 2.88 --------93.06
10/27/2017 2.91 --------93.03
5/8/2018 2.99 --------92.95
10/4/2018 3.26 --------92.68
5/10/2019 3.3 --------92.64
10/17/2019 3.41 --------92.53
4/1/2020 3.99 --------91.95
11/11/2020 3.91 --------92.03
5/6/2021 3.96 --------91.98
12/6/2021 4.14 --------91.80
4/20/2022 4.21 --------91.73
11/16/2022 2.59 --------93.35
6/29/2023 3.11 --------92.83
11/3/2023 4.59 --------91.35
MW-4 5 - 15 95.94
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

4/1/2011 2.99 --------91.15
9/29/2011 4.22 --------89.92
4/4/2012 2.55 --------91.59
10/29/2012 4.23 --------89.91
6/5/2013 4.15 --------89.99
7/17/2014 3.69 --------90.45
2/25/2015 3.48 --------90.66
9/22/2015 5.21 5.81 0.60 88.48
3/23/2016 2.94 2.98 0.04 91.17
9/19/2016 4.03 --------90.11
5/15/2017 3.35 --------90.79
10/27/2017 3.35 --------90.79
5/8/2018 3.56 --------90.58
10/4/2018 3.74 --------90.40
5/10/2019 3.90 --------90.24
10/17/2019 3.98 --------90.16
4/1/2020 3.41 --------90.73
11/11/2020 3.36 --------90.78
5/6/2021 3.38 --------90.76
12/6/2021 3.99 --------90.15
4/20/2022 3.50 --------90.64
11/16/2022 2.05 --------92.09
6/29/2023 2.51 --------91.63
11/3/2023 3.95 --------90.19
MW-5 5 - 15 94.14
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

9/29/2011 8.18 --------83.38
4/4/2012 7.41 --------84.15
10/29/2012 NA --------NA
6/5/2013 NA --------NA
7/17/2014 7.99 --------83.57
2/25/2015 7.73 --------83.83
9/22/2015 8.73 --------82.83
3/23/2016 7.14 --------84.42
9/19/2016 8.21 --------83.35
5/15/2017 5.45 --------86.11
10/27/2017 5.47 --------86.09
5/8/2018 5.53 --------86.03
10/4/2018 5.89 --------85.67
5/10/2019 6.10 --------85.46
10/17/2019 5.99 --------85.57
4/1/2020 5.26 --------86.30
11/11/2020 5.21 --------86.35
5/6/2021 6.01 --------85.55
12/6/2021 6.14 --------85.42
4/20/2022 6.04 --------85.52
11/16/2022
6/29/2023 6.08 --------85.48
Could Not Locate
MW-6 5 - 15 91.56
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

9/29/2011 8.79 --------82.16
4/4/2012 8.23 --------82.72
10/29/2012 8.81 --------82.14
6/5/2013 8.01 --------82.94
7/17/2014 9.91 --------81.04
2/25/2015 8.52 --------82.43
9/22/2015 9.42 --------81.53
3/23/2016 8.14 --------82.81
9/19/2016 9.05 --------81.90
5/15/2017 6.06 --------84.89
10/27/2017 6.11 --------84.84
5/8/2018 6.33 --------84.62
10/4/2018 6.20 --------84.75
5/10/2019 6.29 --------84.66
10/17/2019 6.31 --------84.64
4/1/2020 5.99 --------84.96
11/11/2020 5.94 --------85.01
5/6/2021 5.90 --------85.05
12/6/2021 6.21 --------84.74
4/20/2022 6.74 --------84.21
11/16/2022 7.05 --------83.90
6/29/2023 7.33 --------83.62
MW-7 5 - 15 90.95
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

9/29/2011 8.92 --------92.44
4/4/2012 7.91 --------93.45
10/29/2012 8.86 --------92.50
6/5/2013 7.36 --------94.00
7/17/2014 8.28 --------93.08
2/25/2015 8.03 --------93.33
9/22/2015 9.45 --------91.91
3/23/2016 7.51 --------93.85
9/19/2016 8.70 --------92.66
5/15/2017 6.61 --------94.75
10/27/2017 6.70 --------94.66
5/8/2018 6.88 --------94.48
10/4/2018 8.09 --------93.27
5/10/2019 8.19 --------93.17
10/17/2019 7.94 --------93.42
4/1/2020 7.76 --------93.60
11/11/2020 7.71 --------93.65
5/6/2021 7.68 --------93.68
12/6/2021 7.71 --------93.65
4/20/2022 7.14 --------94.22
11/16/2022 7.04 --------94.32
6/29/2023 7.09 --------94.27
MW-8 5 - 15 101.36
TABLE 5
GROUNDWATER ELEVATION DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Well ID
Well Screen
(FT BGS)
Casing
Elevation Date
Depth to
Groundwater
(FT TOC)
Depth to
(FT TOC)
Product Groundwater
Elevation*
(FT)

9/29/2011 5.60 --------87.83
4/4/2012 4.21 --------89.22
10/29/2012 4.56 --------88.87
6/5/2013 4.57 --------88.86
7/17/2014 4.77 --------88.66
2/25/2015 4.46 --------88.97
9/22/2015 6.15 --------87.28
3/23/2016 4.14 --------89.29
9/19/2016 5.68 --------87.75
5/15/2017 3.75 --------89.68
10/27/2017 3.72 --------89.71
5/8/2018 3.77 --------89.66
10/4/2018 4.09 --------89.34
5/10/2019 4.12 --------89.31
10/17/2019 4.16 --------89.27
4/1/2020 3.99 --------89.44
11/11/2020 3.94 --------89.49
5/6/2021 3.90 --------89.53
12/6/2021 4.15 --------89.28
4/20/2022 3.76 --------89.67
11/16/2022 3.65 --------89.78
6/29/2023 3.92 --------89.51
Notes:
* Corrected for presence of free product where applicable using an assumed relative density of 75%.
FT - Feet (assigned reference to on-site benchmark equal to 100 feet)
FT TOC - Feet below top of well casing
FT BGS- Feet below ground surface
NA - Data not available
NG - Not gauged
MW-9 5 - 15 93.43
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Me
t
h
l
y
e
n
e

C
h
l
o
r
i
d
e
Me
t
h
y
l

t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
Di
i
s
o
p
r
o
p
y
l

E
t
h
e
r

(
I
P
E
)
Is
o
p
r
o
p
y
l

b
e
n
z
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
te
r
t
-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
Di
-
b
r
o
m
o
c
h
l
o
r
o
m
e
t
h
a
n
e
Br
o
m
o
d
i
c
h
l
o
r
o
m
e
t
h
a
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
10/18/2010 8,930 9,430 1,550 8,310 ND 47,800 420 ND ND ND 267 ND 91 ND ND ND 46 --1,100 825 NA NA NA NA NA NA
4/1/2011 5,030 7,810 1,390 6,470 ND 15,500 254 ND ND ND 95.2 40.1 135 ND ND ND ND ND 1,170 260 NA NA 29,300 41,900 3,480 NA
4/4/2012 12,800 23,000 3,140 12,140 ND 48,500 510 ND ND ND 224 72.8 210 ND ND ND ND ND 1,970 425 NA NA 83,000 63,700 7,840 NA
10/29/2012 15,800 22,900 3,530 14,990 ND 52,200 588 ND ND ND 386 ND 255 ND ND ND ND ND 2,150 468 NA NA NA 73,000 7,030 NA
6/5/2013 18,000 31,100 4,220 17,590 ND 56,100 ND ND ND ND 521 ND 349 ND ND ND ND ND 2,650 738 NA NA NA 63,100 ND NA
7/17/2014 14,100 8,540 2,880 12,590 54.7 35,400 655 ND <20 227 335 86.7 223 <10 <10 <10 <10 71.7 1,860 475 NA NA 72,500 56,500 5,440 NA
2/25/2015 12,600 8,610 2,960 11,970 <500 30,000 540 <250 <250 <125 353 <125 238 <125 <125 <125 <125 <125 1,870 490 NA NA 70,300 36,600 <5,000 NA
9/22/2015 11,600 3,040 2,590 9,716 <500 27,900 506 <250 <250 <125 265 <125 206 <125 <125 <125 <125 <125 1,770 451 NA NA NA NA <5,000 NA
3/23/2016 10,100 9,230 2,410 10,030 <400 19,100 416 <200 <200 <100 226 <100 145 <100 <100 <100 <100 <100 1,230 302 NA NA NA NA NA NA
9/19/2016 11,100 880 2,950 10,145 <250 19,100 648 <62.5 <62.5 <62.5 235 81.6 208 <62.5 <62.5 <62.5 <62.5 <62.5 1,810 441 NA NA NA NA NA NA
5/15/2017 112 33.2 37.6 104.7 <4.0 210 8.3 <1.0 <2.0 <1.0 2.4 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 22.2 <1.0 NA NA NA NA NA NA
10/27/2017 109 10.5 36.0 91.1 <2.0 92.9 8.5 <0.50 <1.0 <0.50 0.96 1.00 2.70 <0.50 <0.50 <0.50 <0.50 <0.50 19.8 5.7 NA NA NA NA NA NA
5/8/2018 0.64 <0.50 <0.50 <1.5 <2.0 5.3 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
10/4/2018 5,960 32,900 3,470 17,880 <400 <100 768 <100 <200 <100 <100 124 <100 <100 <100 <100 <100 <100 2,940 <100 NA NA NA NA NA NA
5/10/2019 2.0 <0.50 0.68 <1.50 <2.0 <0.50 <2.0 <5.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
10/17/2019 29.3 <0.50 17.9 3.3 <2.0 6.8 <2.0 <0.50 <1.0 <0.50 <0.50 0.85 2.4 <0.50 <0.50 <0.50 <0.50 <0.50 1.0 <0.50 NA NA NA NA NA NA
4/1/2020 16.8 <0.50 11.8 3.4 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 0.68 1.8 <0.50 <0.50 <0.50 <0.50 <0.50 0.9 <0.50 NA NA NA NA NA NA
11/11/2020 202 11.6 346 72.8 <5.0 24.7 129 <1.2 <2.5 <1.2 <1.2 55.5 181 <1.2 <1.2 <1.2 <1.2 <1.2 27.2 <1.2 NA NA NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
12/6/2021 362 259 407 62.6 <10 21.4 201 <2.5 <5.0 <2.5 <2.5 62.3 222 43.8 15.6 <2.5 <2.5 <2.5 17.3 36.8 NA NA 10,200 1,860 1,550 NA
4/20/2022 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 2.7 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
11/16/2022 6,600 2,300 3,500 8,900 1.4 4,300 650 <1.7 <1.0 <2.0 84 98 290 <1.5 <1.1 <1.9 <1.6 <2.6 1,300 310 <1.3 <2.0 NA NA NA NA
6/29/2023 2,620 7,870 2,740 15,160 <250 1,630 505 <50.0 <50.0 <50.0 43.0 J 58.1 184 <50.0 <50.0 <50.0 <50.0 <50.0 1,850 486 <50.0 <50.0 NA NA NA NA
11/3/2023 4,670 22,400 4,460 23,600 <378 1,780 848 <13.8 <35.0 <19.1 45.6 J 112 335 <13.3 <17.0 <17.1 <27.4 <34.2 2,850 689 <29.6 <34.0 NA NA NA NA
MW-1
Chemical Parameter
MW-1RA
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
4/1/2011 ND ND 1.5 1.8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7.2 2.5 NA NA 36.2 170 35.6 14.4
4/4/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA ND ND ND NA
10/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.69 ND NA NA ND ND ND NA
6/5/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA ND ND ND NA
7/17/2014 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
2/25/2015 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
9/22/2015 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
3/23/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
9/19/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 0.35 J <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
5/15/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0..50 <2.0 <0.5 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
10/27/2017 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
5/8/2018 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
10/4/2018 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 <0.50 1.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
5/10/2019 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 <0.5 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
10/17/2019 <0.50 <0.50 <0.50 <1.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
4/1/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
11/11/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
12/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA <50 <50 <50 NA
4/20/2022 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA
11/16/2022 <0.050 <0.053 <0.10 <0.268 <0.070 <0.12 <0.086 <0.083 <0.050 <0.10 <0.21 <0.13 <0.073 <0.074 <0.053 <0.094 <0.082 <0.13 <0.067 <0.10 <0.067 <0.10 NA NA NA NA
6/29/2023 <1.00 <1.00 <1.00 <10.0 <5.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA
11/3/2023 <0.079 <0.090 <0.081 <0.094 <1.9 <0.053 0.65 J 0.15 J <0.18 <0.096 <0.072 <0.11 <0.10 <0.066 <0.085 <0.086 <0.14 <0.17 <0.031 <0.071 <0.15 <0.17 NA NA NA NA
MW-2
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
4/1/2011 191 12.8 220 250.9 251.9 115 95 ND ND ND 1.6 70.6 214 ND ND ND ND ND 756 193 NA NA 3,950 11,500 2,630 ND
4/4/2012 119 6.6 120 52 53 81 45.8 ND ND ND 1.2 32.5 ND 27.3 ND ND 115 ND 188 21.8 NA NA ND ND ND NA
10/29/2012 274 12.7 179 103.8 104.8 227 77.1 ND ND ND 3.4 54.6 161 33.9 ND ND ND ND 242 24.6 NA NA 4,630 3,250 1,150 NA
6/5/2013 33.9 1.8 38 17.5 18.5 21.8 15.8 ND ND ND ND 11 42.7 10.2 4.3 5.3 ND ND 55 5.4 NA NA 1,480 1,110 430 NA
7/17/2014 234 18.8 229 152.5 <20.0 154 160 <2.5 <10.0 <5.0 <5 42.4 145 26.3 10.5 <5.0 <5.0 36.0 323 20 NA NA 1,810 2,630 895 NA
2/25/2015 340 188 171 106.6 <5.0 85.3 84.1 <2.5 3.2 <1.2 2.4 36.4 121 26.9 10.3 <1.2 <1.2 <1.2 217 15.4 NA NA 3,340 2,700 965 NA
9/22/2015 280 62.1 122 61.1 <5.0 93.2 58.4 <2.5 <2.5 <1.2 1.7 20.9 63.8 <1.2 4.2 <1.2 <1.2 <1.2 112 12.1 NA NA NA NA NA NA
3/23/2016 197 29.9 146 98.1 <2.0 39.8 57.9 <1 <1.0 <0.5 0.9 39.5 135 32.1 14 <0.50 <0.50 <0.50 110 5.5 NA NA NA NA NA NA
9/19/2016 649 40.3 271 284 <10 114 115 <5 <5.0 <2.5 2.8 39.3 133 <2.5 10.2 <2.5 <2.5 <2.5 262 19.0 NA NA NA NA NA NA
5/15/2017 160 10.3 84.9 144.8 <2.0 <0.50 14.4 <0.50 10.9 <0.50 <0.50 12.2 35.0 <0.50 <0.50 <0.50 <0.50 <0.50 54.1 <0.50 NA NA NA NA NA NA
10/27/2017 565 16.2 453 346.2 <10.0 77.3 143 <2.5 <5.0 <2.5 <2.5 41.5 138 21.0 8.80 <2.5 <2.5 <2.5 186 19.0 NA NA NA NA NA NA
5/8/2018 168 19.3 153 152.7 <2.0 13.7 50.3 <0.50 <1.0 <0.50 <0.50 17.4 57.2 <0.50 <0.50 <0.50 <0.50 <0.50 75.5 11.7 NA NA NA NA NA NA
10/4/2018 7.9 183 62.1 351 <2.0 <0.50 29.9 <0.50 2.2 <0.50 <0.50 4.9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 135 <0.50 NA NA NA NA NA NA
5/10/2019 495 47.8 617 269.3 <10 56.3 204 <25 <5.0 <2.5 2.9 70.6 218 <2.5 <2.5 <2.5 <2.5 <2.5 233 12.6 NA NA NA NA NA NA
10/17/2019 388 23.9 367 98.0 <8.0 <2.0 73.3 <2.0 <4.0 <2.0 <2.0 26.9 74.5 <2.0 <2.0 <2.0 <2.0 <2.0 53.1 <2.0 NA NA NA NA NA NA
4/1/2020 67.0 3.0 69.6 27.2 <2.0 <0.50 27.4 <0.50 <1.0 <0.50 <0.50 11.2 35.2 <0.50 <0.50 <0.50 <0.50 <0.50 14.7 <0.50 NA NA NA NA NA NA
11/11/2020 225 13.3 401 85.8 <8.0 26.2 138 <2.0 <4.0 <2.0 <2.0 62.7 199 <2.0 <2.0 <2.0 <2.0 <2.0 31.9 <2.0 NA NA NA NA NA NA
5/6/2021 220 29.9 369 91.8 <8.0 25.7 136 <2.0 <4.0 <2.0 <2.0 56.4 178 <2.0 <2.0 <2.0 <2.0 <2.0 59.8 <2.0 NA NA NA NA NA NA
12/6/2021 385 249 409 61.1 <10 21.8 192 <2.5 <5.0 <2.5 4.3 61.9 219 32.1 13.0 <2.5 <2.5 <2.5 10.6 33.8 NA NA 8,280 1,780 1,450 NA
4/20/2022 1,730 1,920 649 1,345 <25.0 23.8 157 <6.2 <12.5 <6.2 <6.2 67.4 208 <6.2 <6.2 <6.2 <6.2 <6.2 130 14.6 NA NA NA NA NA NA
11/16/2022 1,100 150 540 485 <0.35 30 170 <0.42 <0.25 <0.50 5.8 50 200 <0.37 14 <0.47 <0.41 <0.65 32 8.3 <0.34 <0.50 NA NA NA NA
6/29/2023 447 20.2 348 221 <10.0 13.9 106 <2.00 <2.00 <2.00 1.52 J 19.6 69.4 2.9 1.81 J <2.00 <2.00 <2.00 30 3.83 <2.00 <2.00 NA NA NA NA
11/3/2023 2,060 39.4 403 125 <37.8 22.4 165 <1.4 <3.5 <1.9 15.4 43.1 140 <1.3 <1.7 <1.7 <2.7 <3.4 15.0 <1.4 <3.0 <3.4 NA NA NA NA
MW-3
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
4/1/2011 801 64.6 1,020 2,762 ND 3,350 247 ND ND ND 19.3 88.7 204 ND ND ND ND ND 1,470 408 ND ND 7,180 36,100 5,390 11.2
4/4/2012 754 33.7 546 691 ND 4,130 96.6 ND ND ND 11.3 22.4 48.4 ND ND ND ND ND 195 52.1 ND ND 4,880 5,700 973 NA
10/29/2012 445 63.1 44.7 ND ND 4,990 ND ND ND ND 22.6 14 18.3 ND ND ND ND ND 24.7 ND ND ND 6,070 ND ND NA
6/5/2013 409 27.5 641 674.1 ND 2,830 111 ND ND ND 15.9 28.3 57.9 ND ND ND ND ND 161 50.9 ND ND 4,090 5,000 760 NA
7/17/2014 160 5 141 87.58 <2.0 2,080 51.4 <1.0 <1.0 <0.50 16.6 9.9 13.6 <0.50 2.2 <0.50 <0.50 <0.50 27.7 7.4 ND ND 1,590 951 253 NA
2/25/2015 9.9 <0.50 24.6 23.2 <2.0 43.4 4.8 <1.0 <1.0 <0.50 <0.50 0.84 2.4 <0.50 <0.50 <0.50 <0.50 <0.50 7.1 1.9 ND ND 81 141 <50.0 NA
9/22/2015 20.2 <5.0 <5.0 <15 <20.0 1,020 <20.0 <10.0 <10.0 <5.0 5.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 ND ND NA NA NA NA
3/23/2016 5.3 <0.50 <0.50 11.6 <2.0 16.6 3.3 <1.0 <1.0 <0.50 <0.50 0.72 2 <0.50 <0.50 <0.50 <0.50 <0.50 3.7 NA ND ND NA NA NA NA
9/19/2016 3.7 <0.50 <0.50 <1.5 <2.0 32 <2.0 0.32 J <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA ND ND NA NA NA NA
5/15/2017 2.1 <0.50 0.98 <1.5 <2.0 7.3 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/27/2017 1.3 <0.50 <0.50 <1.5 <2.0 19.2 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/8/2018 <0.50 <0.50 <0.50 <1.5 <2.0 6.6 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/4/2018 183 1,390 216 1,200 <25.0 <6.20 149 <6.20 <12.5 <6.20 <6.20 13.8 <6.20 <6.20 <6.20 <6.20 <6.20 <6.20 489 <6.20 ND ND NA NA NA NA
5/10/2019 1.4 <0.50 <0.50 <1.5 <2.0 12.2 <2.0 <5.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/17/2019 2.6 <0.50 0.84 <1.5 <2.0 11.9 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
4/1/2020 6.9 17 54.2 173 <2.0 <0.50 25.5 <0.50 <1.0 <0.50 <0.50 5.1 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 114 33.9 <0.50 <0.50 NA NA NA NA
11/11/2020 0.74 <0.50 <0.50 <1.5 <2.0 3.8 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 0.9 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
12/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 2.3 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
4/20/2022 <0.50 <0.50 <0.50 <1.5 <2.0 1.4 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.88 <0.50 <0.50 <0.50 <50 <50 <50 NA
11/16/2022 15 1.0 71 5.1 <0.070 50 19 <0.083 <0.050 <0.10 1.2 4.4 17 <0.074 1.1 <0.094 <0.082 <0.13 <0.067 2.2 <0.067 <0.10 NA NA NA NA
6/29/2023 14.6 <1.00 44.4 4.14 J <5.00 46.6 17.7 <1.00 <1.00 <1.00 0.687 J 1.68 6.43 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA
11/3/2023 <0.079 <0.090 <0.081 <0.094 <1.9 111 <0.10 <0.069 <0.18 <0.096 1.2 <0.11 <0.10 <0.066 <0.085 <0.086 <0.14 <0.17 <0.031 <0.071 <0.15 <0.17 NA NA NA NA
MW-4
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
4/1/2011 1,460 5,970 1,880 9,580 ND 2,210 527 ND ND ND 18.8 113 303 ND ND ND ND ND 2,730 2,530 ND ND 14,300 73,500 8,470 --
4/4/2012 202 998 442 2,115 ND 178 187 ND ND ND 4.6 39.6 111 ND ND ND ND ND 644 185 ND ND 5,020 13,700 2,570 NA
10/29/2012 2,180 8,210 3,120 14,430 ND 2,740 642 ND ND ND 22.8 133 314 ND ND ND ND ND 2,840 609 ND ND 37,800 73,900 8,750 NA
6/5/2013 2,790 8,260 2,330 10,670 ND 2,280 537 ND ND ND --80 218 ND ND ND ND ND 1,950 446 ND ND 34,500 57,000 --NA
7/17/2014 1,260 1,700 1,840 6,960 <10 1,520 580 ND 9.00 <2.5 <2.5 104 302 <2.5 <2.5 284 <2.5 13.4 2,020 573 ND ND 8,790 27,900 4,180 NA
2/25/2015 1,370 2,250 2,300 7,560 <40.0 1,150 538 ND <20.0 <10.0 <10.0 103 293 <10.0 <10.0 <10.0 <10.0 <10.0 1,950 500 ND ND 14,800 31,200 4,650 NA
9/22/2015 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/23/2016 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/19/2016 453 132 477 1,168 <10.0 863 213 <2.5 <5.0 <2.5 9 23 68 <2.5 <2.5 <2.5 <2.5 <2.5 502 105 ND ND NA NA NA NA
5/15/2017 1,530 1,170 3,290 11,050 <50.0 986 1,290 <12.5 35.2 <12.5 <12.5 231 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 4,970 1,420 ND ND NA NA NA NA
10/27/2017 ,1250 362 2,460 8,780 <50.0 874 903 <12.5 <25.0 <12.5 <12.5 157 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 4,080 1,140 ND ND NA NA NA NA
5/8/2018 1,690 2,220 3,410 12,080 <50.0 1,350 1,090 17.7 <25.0 <12.5 <12.5 202.0 649 <12.5 <12.5 <12.5 <12.5 <12.5 4,620 1,300 ND ND NA NA NA NA
10/4/2018 225 1,330 216 1,319 <20.0 <5.0 418 <5.0 <10.0 <5.0 <5.0 25.7 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 1,170 <5.0 ND ND NA NA NA NA
5/10/2019 1.5 <0.5 <0.5 <1.5 <2.0 13.5 <2.0 <5.0 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND ND NA NA NA NA
10/17/2019 1,440 430 1,390 4,482 <25.0 1,130 352 <6.2 <12.5 <6.2 <6.2 55.6 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 1,200 <6.2 <6.2 <6.2 NA NA NA NA
4/1/2020 1,260 1,650 2,650 8,380 <50.0 997 899 <12.5 <25.0 <12.5 <12.5 167 <12.5 <12.5 <12.5 <12.5 <12.5 <12.5 3,880 1,120 <12.5 <12.5 NA NA NA NA
11/11/2020 524 166 1,110 2,946 <2.0 378 237 <0.50 <1.0 <0.50 <0.50 55.9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1,120 301 <0.50 <0.50 NA NA NA NA
5/6/2021 737 497 1,460 3,768 <25.0 639 354 <6.2 <12.5 <6.2 <6.2 70.1 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 1,670 481 <6.2 <6.2 NA NA NA NA
12/6/2021 901 274 1,600 4,525 <25.0 578 404 <6.2 <12.5 <6.2 <6.2 78.9 229 <6.2 <6.2 <6.2 <6.2 <6.2 1,760 428 <6.2 <6.2 14,600 12,100 6,250 NA
4/20/2022 731 399 1,970 4,247 <40.0 492 531 <10.0 <20.0 <10.0 <10.0 127 398 <10.0 <10.0 <10.0 <10.0 <10.0 2,650 734 <10.0 <10.0 NA NA NA NA
11/16/2022 500 88 850 1,839 <0.070 420 260 <0.083 <0.050 <0.10 9.0 56 160 <0.074 8.8 <0.094 <0.082 <0.13 660 160 <0.067 <0.10 NA NA NA NA
6/29/2023 357 65 580 916 <25.0 457 168 <5.00 <5.00 <5.00 6.94 17.2 52.3 6.93 <5.00 <5.00 <5.00 <5.00 341 69.6 <5.00 <5.00 NA NA NA NA
11/3/2023 503 39.7 936 799 <9.4 442 351 <0.35 <0.88 <0.48 7.9 43.9 130 <0.33 <0.43 <0.43 <0.68 <0.86 459 66.3 <0.74 <0.85 NA NA NA NA
MW-5
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
9/29/2011 20.7 14.7 341 90.5 ND 41.6 136 ND ND ND ND 35.7 117 12.2 13.2 ND 3.7 ND 40.7 35.7 ND ND 1,280 3,380 532 --
4/4/2012 2.3 0.99 4.6 8.8 ND 26.4 3 ND ND ND ND 1.7 2.5 ND ND ND ND ND 4.3 5.3 ND ND 193 182 59.8 NA
10/29/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
6/5/2013 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
7/17/2014 6.7 4.3 163 163.0 <2.0 23.6 131 <1.0 <1.0 <0.50 <0.50 45.7 108 <0.50 9.3 <0.50 0.7 <0.50 1.3 2.1 ND ND 1,620 1,590 477 NA
2/25/2015 8.8 0.88 56.7 56.7 <2.0 22.6 74.8 <1.0 <1.0 <0.50 <0.50 39.9 78.5 <0.50 8.4 <0.50 <0.50 <0.50 <0.50 2.8 ND ND 1,460 1,320 473 NA
9/22/2015 3.0 1.2 50.9 50.9 <2.0 42.9 50.9 <1.0 <1.0 <0.50 <0.50 30 46.7 <0.50 8.2 <0.50 <0.50 <0.50 <0.50 0.88 ND ND NA NA NA NA
3/23/2016 <0.50 5 55.8 55.8 <2.0 5.7 33.1 <1.0 <1.0 <0.50 <0.50 11.1 22 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.0 ND ND NA NA NA NA
9/19/2016 2.7 0.28 J 12.3 12.3 <2.0 13.1 23.9 <0.50 <1.0 <0.50 <0.50 15.6 22.3 4.4 5.0 <0.50 <0.50 <0.50 <0.50 0.29 J ND ND NA NA NA NA
5/15/2017 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/27/2017 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/8/2018 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/4/2018 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 1.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/10/2019 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <5.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/17/2019 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 17.6 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.73 2.8 NA NA NA NA
4/1/2020 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/11/2020 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
12/6/2021 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 8.4 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.82 3.9 <50 <50 <50 NA
4/20/2022 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/16/2022
6/29/2023 <1.00 <1.00 <1.00 <10.0 <5.00 1.67 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA
Could Not Locate - No Sample
MW-6
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
9/29/2011 ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
4/4/2012 ND ND ND ND ND 3.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
10/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
6/5/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
7/17/2014 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND <0.50 <0.50 <0.50 NA
2/25/2015 <0.50 <0.50 <0.50 <1.5 <2.0 2.3 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND <0.50 <0.50 <0.50 NA
9/22/2015 <0.50 <0.50 <0.50 <1.5 <2.0 18.3 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA ND ND NA NA NA NA
3/23/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
9/19/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/15/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/27/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/8/2018 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/4/2018 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 2.1 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/10/2019 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <5.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/17/2019 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 15.7 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.7 2.7 NA NA NA NA
4/1/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/11/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
12/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 7.9 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.92 3.8 <50 <50 <50 NA
4/20/2022 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/16/2022 <0.050 <0.053 <0.10 <0.268 <0.070 <0.12 <0.086 <0.083 <0.050 <0.10 <0.21 <0.13 <0.073 <0.074 <0.053 <0.094 <0.082 <0.13 <0.067 <0.10 <0.067 <0.10 NA NA NA NA
6/29/2023 <1.00 <1.00 <1.00 <10.0 <5.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA
MW-7
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
9/29/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
4/4/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
10/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
6/5/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
7/17/2014 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND <0.50 <0.50 <0.50 NA
2/25/2015 <0.50 <0.50 <0.50 <1.5 <2.0 2.3 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND <0.50 <0.50 <0.50 NA
9/22/2015 <0.50 <0.50 <0.50 <1.5 <2.0 18.3 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA ND ND NA NA NA NA
3/23/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
9/19/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/15/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.8 <0.50 ND ND NA NA NA NA
10/27/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/8/2018 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/4/2018 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 3.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/10/2019 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <5.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/17/2019 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 32.7 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1 4.3 NA NA NA NA
4/1/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/11/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <2.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <2.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
12/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <50 <50 <50 NA
4/20/2022 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/16/2022 <0.050 <0.053 <0.10 <0.268 <0.070 <0.12 <0.086 <0.083 <0.050 <0.10 <0.21 <0.13 <0.073 <0.074 <0.053 <0.094 <0.082 <0.13 <0.067 <0.10 <0.067 <0.10 NA NA NA NA
6/29/2023 <1.00 <1.00 <1.00 <10.0 <5.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA
MW-8
TABLE 6
GROUNDWATER ANALYTICAL DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
,

T
o
t
a
l
Na
p
h
t
h
a
l
e
n
e
Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
4-
C
h
l
o
r
o
t
o
l
u
e
n
e
n-
B
u
t
y
l
b
e
n
z
e
n
e
s-
B
u
t
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
C5
-
C
8
Al
i
p
h
a
t
i
c
s
C9
-
C
1
8
Al
i
p
h
a
t
i
c
s
C9
-
C
2
2
Ar
o
m
a
t
i
c
s
Le
a
d
1 600 600 500 5 20 6 70 3 24 70 70 70 70 70 70 70 3 400 400 0.4 NE 400 700 200 15
5,000 260,000 80,000 50,000 5,000 20,000 6,000 7,000 3,000 24,000 70,000 30,500 26,100 5,900 8,800 14,750 70,000 3,000 28,500 24,100 400 NE NE NE NE 15,000
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Chemical Parameter
9/29/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
4/4/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
10/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
6/5/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
7/17/2014 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND <0.50 <0.50 <0.50 NA
2/25/2015 <0.50 <0.50 <0.50 <1.5 <2.0 2 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND <0.50 <0.50 <0.50 NA
9/22/2015 <0.50 <0.50 <0.50 <1.5 <2.0 18 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA ND ND NA NA NA NA
3/23/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
9/19/2016 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/15/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/27/2017 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/8/2018 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/4/2018 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 2.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
5/10/2019 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <5.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND ND NA NA NA NA
10/17/2019 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 32.1 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1 4.2 NA NA NA NA
4/1/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/11/2020 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <2.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
5/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <2.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
12/6/2021 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <2.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <50 <50 <50 NA
4/20/2022 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <2.0 <2.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
11/16/2022 <0.050 <0.053 <0.10 <0.268 <0.070 <0.12 <0.086 <0.083 <0.050 <0.10 <0.21 <0.13 <0.073 <0.074 <0.053 <0.094 <0.082 <0.13 <0.067 <0.10 <0.067 <0.10 NA NA NA NA
6/29/2023 <1.00 <1.00 <1.00 <10.0 <5.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA
Notes:
NCAC 2L Standard - North Carolina Administrative Code Groundwater Quality Standard
NE - Standard Not Established
Bold - Concentration exceeds North Carolina Groundwater Quality Standard (NCAC 2L Standard)
NS - Sample not collected from monitoring well; NA = not analyzed
J - Estimated concentration below laboratory reporting limit
"<" denotes analyte was not detected above laboratory method detection limits
MW-9
TABLE 7
NATURAL ATTENUATION GROUNDWATER DATA
Roadrunner #135
Black Mountain, Buncombe County, North Carolina
Incident No. 28783
Ir
o
n
Al
k
a
l
i
n
i
t
y
Su
l
f
a
t
e
Am
m
o
n
i
a

Ni
t
r
o
g
e
n
To
t
a
l

P
h
o
s
p
h
a
t
e
Ma
n
g
a
n
e
s
e
Ni
t
r
i
t
e

N
i
t
r
o
g
e
n
Ni
t
r
a
t
e

N
i
t
r
o
g
e
n
Me
t
h
a
n
e
Di
s
s
o
l
v
e
d

O
x
y
g
e
n
pH
Te
m
p
e
r
a
t
u
r
e
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L µS/cm oC mV
4/20/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/16/2022 1,680 131,000 524 <1,000 566 1,090 NA 2,500 <50 <50 <50 6,720 4.1 6.77 400 18.36 -65.3
6/29/2023 348 HF B 286 3.72 0.970 J 4.14 7.86 34100 6.38 0.0250 J <0.100 0.0250 J 4410 1.15 6.82 0.487 20.41 -102.5
4/20/2022 339,000 193,000 7,900 3,900 230 8,100 3,100 NA 670 <40 670 <10.0 0.52 5.39 119.1 15.8 186.8
11/16/2022 100 25,000 <200 3,700 132 J 111 J NA 141 <500 <50 <500 0.929 1.73 5.74 100 17.06 98.2
6/29/2023 0.458 HF B 15.9 1.06 9.66 <0.0500 1.06 812 0.297 0.377 <0.100 0.377 1.93 2.67 5.70 0.105 19.29 106.0
4/20/2020 59,800 130,000 1,700 <1,000 3,900 5,500 1,400 NA 44 69 <40 4,030 0.38 6.57 465.1 16.2 17.4
11/16/2022 1,010 89,100 2,550 <1,000 1,900 4,450 NA 1,630 <50 28.5 <50 7,660 3.06 6.65 203 14.63 -46.6
6/29/2023 1.13 HF B 113 2.22 <1.00 3.30 5.52 997 1.74 <0.0500 <0.100 <0.0500 6900 1.81 6.71 0.229 18.44 -52.9
4/20/2022 20,000 8,000 <500 <1,000 <100 <500 <50 NA 200 <40 200 125 1.49 6.07 43.9 16.7 7.3
11/16/2022 100 29,700 244 1,100 239 J 483 NA 352 283 <50 283 682 9.5 6.07 40 17.25 145.3
6/29/2023 0.345 HF B 33.0 <0.500 1.86 0.201 <0.500 1780 0.727 0.272 <0.100 0.272 450 3.43 6.06 0.110 19.87 65.3
4/20/2022 56,300 151,000 1,000 3,600 2,900 4,000 160 NA 55 62 <40 11,400 1.79 6.53 547.3 16.5 31.2
11/16/2022 14,800 30,800 2,070 3,420 622 2,690 NA 1,400 <50 <50 <50 4,770 3.21 3.64 189 16.49 -12.3
6/29/2023 2.48 HF B 90.7 7.21 1.18 1.11 8.32 2350 2.21 0.0460 J <0.100 0.0460 J 3350 1.98 6.52 0.313 19.13 -50.2
4/20/2022 438 <5,000 4,000 17,100.0 <100 4,000 2,400 NA 1,500 <40 1,500 <10.0 3.21 4.41 86.3 13.5 371.2
11/16/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
6/29/2023 29.8 HF B 6.96 3.64 14.0 0.0270 J 3.67 2220 0.558 1.06 <0.100 1.06 <1.00 5.14 5.10 0.072 16.02 147.9
4/20/2022 144,000 7,300 1,800 3,800 <100 1,800.0 2,800 NA 230 <40 230 <10.0 3.65 4.69 37.5 13.1 369.1
11/16/2022 0.624 25,600 <200 3,400 <250 132 J NA 21.3 156 <50 156 624 4.61 5.33 41 16.14 132.2
6/29/2023 8.20 HF B 13.7 <0.500 4.14 <0.0500 <0.500 110 0.458 0.348 <0.100 0.348 <1.00 3.85 5.23 0.37 15.14 164.5
4/20/2022 10,700 20,100 <500 86,500 <100 <500 470 NA 140 <40 140 <10.0 0.34 5.35 412.1 14.4 122.3
11/16/2022 <100 21,600 <200 78,300 170 J 103 J NA 1,150 <50 <50 <50 0.709 8.15 5.45 255 17.24 158.0
6/29/2023 70.5 HF B 23.9 0.291 J 74.3 0.0560 0.347 J 3940 5.07 0.256 <0.100 0.256 <1.00 2.84 5.57 0.305 16.84 149.2
4/20/2022 122,000 52,200 1,300 <1,000 100 1,300 1,600 NA 200 <40 200 <10.0 6.2 5.73 113.7 15.7 234.4
11/16/2022 <100 34,100 <200 9,210 175 J 219.0 NA 256 <50 <50 <50 136 2.57 6.02 134 17.53 56.1
6/29/2023 32.7 HF B 52.9 1.50 2.49 0.0850 1.58 <100 0.468 <0.0500 0.0255 J <0.0500 231 1.98 6.17 0.109 18.06 22.9
Notes:
NCAC 2L Standard - North Carolina Administrative Code Groundwater Quality Standard
NE - Standard Not Established
Bold - Concentration exceeds North Carolina Groundwater Quality Standard (NCAC 2L Standard)
NS - Sample not collected from monitoring well; NA = not analyzed
J - Estimated concentration below laboratory reporting limit
"<" denotes analyte was not detected above laboratory method detection limits
MW-9
Chemical Parameter
MW-2
MW-3
MW-4
MW-5
MW-6
MW-7
MW-8
Total Plume
Area1 Thickness2 Porosity3
ft^2 ft na ft^3 m^3 L ug/L ug kg lb.
11/3/2023 Benzene >2L 14,089 9.32 0.35 45,974 1,302 1,301,829 2,411 3,138,710,497 3.1 6.9
11/3/2023 Toluene >2L 2,593 8.26 0.35 7,498 212 212,307 22,400 4,755,685,258 4.8 10.5
11/3/2023 Ethylbenzene >2L 7,406 9.66 0.35 25,026 709 708,664 2,698 1,911,974,402 1.9 4.2
11/3/2023 Xylenes >2L 7,160 9.66 0.35 24,195 685 685,117 12,200 8,358,078,784 8.4 18.4
18.2 40.1
1. as calculated from Figures 6A-6E
2. average depth of impacted wells - DTW (saturated zone)
3. mean value from CSA
Sample
Date Constituent Volume Total Mass
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT

APPENDIX A
RECENT CORRESPONDENCE

Site Name City / County /Buncombe Incident #28783
Resp Pty Name / Contact /Incident Mgr Region ASH
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #23
Consultant / Project Mgr /Dan Fisher
Telephone / Fax Number /Task Authorization Number:24 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I-180A RRA Date:12/6/2018
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w
3r
d

P
t
y

D
e
d
?
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 5 /well Y $110.00 y $550.00 $550.00 /
4.090 #272 5 / sample Y $66.00 y $330.00 $330.00 /
4.091 1 /shipment Y $150.00 y $150.00 $150.00 /
6.090 1 / report Y $1,125.00 y $1,125.00 $1,125.00 /
12.050 1 / trip Y $250.00 y $250.00 $250.00 /
12.055 1 / trip Y $50.00 y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$2,455.00 $2,455.00 TOTAL:
Total Standard Costs (Not Third Party)$2,455.00 $2,455.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:10/18/23 by:(PM)(Reserved for RO)
RO Review: 10/18/23 by:(IM)Joint UST Preapproval Confirmed By:Date1
CO Review: 10/18/23 by:(STF)RP or Designee Receipt Confirmed By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DJF
Proposed
Units / Type
(Consultant)
Maura Clark
ActiveYES
TA-24 10/17/23-10/31/23
540-343-6259
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
NO
[e-mail]
Mountain Empire Oil Company Rolfe Lann
CES of NC, PLLC
DIRECTED COSTS
Black Mountain
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
540-343-6256
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
GPM 6035 (Roadrunner #135)
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and therationale for the proposed activities.If, following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this form to
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within12 monthsof the completion dateof the FIRST completed task toremainwithin the Statute ofLimitations. All ePATAs submitted within a claim are closed with that
claim, and may not be re-used in a separate submittal, even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
MC
TC
(Initials)
Maura Clark
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality - Division of Waste Management
10/18/2023
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT

APPENDIX B
LABORATORY REPORT(S) AND CHAIN OF CUSTODY DOCUMENTATION

#=CL#
November 13, 2023
LIMS USE: FR - ALLISON STREAMS
LIMS OBJECT ID: 92696826
92696826
Project:
Pace Project No.:
RE:
Allison Streams
Crawford Environmental
5104 Reagan Dr,
Suite 7
Charlotte, NC 28206
GPM 6035
Dear Allison Streams:
Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
704-977-0943
Enclosures
cc:James Coleman, Crawford Environmental
Carol Goss, Crawford Environmental Services, Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92696826
GPM 6035
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 35
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92696826
GPM 6035
Lab ID Sample ID Matrix Date Collected Date Received
92696826001 MW-1RA Water 11/03/23 09:35 11/03/23 13:52
92696826002 MW-2 Water 11/03/23 09:50 11/03/23 13:52
92696826003 MW-3 Water 11/03/23 10:10 11/03/23 13:52
92696826004 MW-4 Water 11/03/23 10:40 11/03/23 13:52
92696826005 MW-5 Water 11/03/23 11:00 11/03/23 13:52
92696826006 TRIP BLANK Water 11/03/23 13:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92696826
GPM 6035
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92696826001 MW-1RA SM 6200B 67 PASI-CLMB
92696826002 MW-2 SM 6200B 67 PASI-CSAS
92696826003 MW-3 SM 6200B 67 PASI-CLMB
92696826004 MW-4 SM 6200B 67 PASI-CSAS
92696826005 MW-5 SM 6200B 67 PASI-CLMB
92696826006 TRIP BLANK SM 6200B 67 PASI-CJJK
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-1RA Lab ID:92696826001 Collected:11/03/23 09:35 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Acetone ND ug/L 11/10/23 10:39 67-64-15000310200
Benzene 4670 ug/L 11/10/23 10:39 71-43-210015.7 200
Bromobenzene ND ug/L 11/10/23 10:39 108-86-110027.0 200
Bromochloromethane ND ug/L 11/10/23 10:39 74-97-510018.9 200
Bromodichloromethane ND ug/L 11/10/23 10:39 75-27-410034.0 200
Bromoform ND ug/L 11/10/23 10:39 75-25-210039.4 200
Bromomethane ND ug/L 11/10/23 10:39 74-83-9100044.4 200
2-Butanone (MEK)ND ug/L 11/10/23 10:39 78-93-3100062.2 200
n-Butylbenzene ND ug/L 11/10/23 10:39 104-51-810013.3 200
sec-Butylbenzene ND ug/L 11/10/23 10:39 135-98-810017.0 200
tert-Butylbenzene ND ug/L 11/10/23 10:39 98-06-610017.1 200
Carbon tetrachloride ND ug/L 11/10/23 10:39 56-23-510033.8 200
Chlorobenzene ND ug/L 11/10/23 10:39 108-90-710016.9 200
Chloroethane ND ug/L 11/10/23 10:39 75-00-320034.6 200
Chloroform ND ug/L 11/10/23 10:39 67-66-310013.8 200
Chloromethane ND ug/L 11/10/23 10:39 74-87-320035.0 200
2-Chlorotoluene ND ug/L 11/10/23 10:39 95-49-810025.8 200
4-Chlorotoluene ND ug/L 11/10/23 10:39 106-43-410019.1 200
Dibromochloromethane ND ug/L 11/10/23 10:39 124-48-110029.6 200
1,2-Dibromoethane (EDB)ND ug/L 11/10/23 10:39 106-93-410029.4 200
1,2-Dichlorobenzene ND ug/L 11/10/23 10:39 95-50-110018.8 200
1,3-Dichlorobenzene ND ug/L 11/10/23 10:39 541-73-110019.6 200
1,4-Dichlorobenzene ND ug/L 11/10/23 10:39 106-46-710017.9 200
Dichlorodifluoromethane ND ug/L 11/10/23 10:39 75-71-810024.6 200
1,1-Dichloroethane ND ug/L 11/10/23 10:39 75-34-310011.2 200
1,2-Dichloroethane ND ug/L 11/10/23 10:39 107-06-210021.2 200
1,1-Dichloroethene ND ug/L 11/10/23 10:39 75-35-410015.7 200
cis-1,2-Dichloroethene ND ug/L 11/10/23 10:39 156-59-210022.2 200
trans-1,2-Dichloroethene ND ug/L 11/10/23 10:39 156-60-510020.2 200
1,2-Dichloropropane ND ug/L 11/10/23 10:39 78-87-510027.2 200
1,3-Dichloropropane ND ug/L 11/10/23 10:39 142-28-910017.1 200
2,2-Dichloropropane ND ug/L 11/10/23 10:39 594-20-710024.4 200
1,1-Dichloropropene ND ug/L 11/10/23 10:39 563-58-610013.2 200
cis-1,3-Dichloropropene ND ug/L 11/10/23 10:39 10061-01-510017.9 200
trans-1,3-Dichloropropene ND ug/L 11/10/23 10:39 10061-02-610026.4 200
Diisopropyl ether 45.6J ug/L 11/10/23 10:39 108-20-310014.5 200
Ethylbenzene 4460 ug/L 11/10/23 10:39 100-41-410016.2 200
2-Hexanone ND ug/L 11/10/23 10:39 591-78-6100035.0 200
Isopropylbenzene (Cumene)112 ug/L 11/10/23 10:39 98-82-810021.2 200
p-Isopropyltoluene ND ug/L 11/10/23 10:39 99-87-610017.9 200
Methylene Chloride ND ug/L 11/10/23 10:39 75-09-2400378200
4-Methyl-2-pentanone (MIBK)ND ug/L 11/10/23 10:39 108-10-1100032.8 200
Methyl-tert-butyl ether 1780 ug/L 11/10/23 10:39 1634-04-410010.7 200
Naphthalene 848 ug/L 11/10/23 10:39 91-20-340020.2 200
n-Propylbenzene 335 ug/L 11/10/23 10:39 103-65-110021.0 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-1RA Lab ID:92696826001 Collected:11/03/23 09:35 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Styrene ND ug/L 11/10/23 10:39 100-42-510027.4 200
1,1,1,2-Tetrachloroethane ND ug/L 11/10/23 10:39 630-20-610018.2 200
1,1,2,2-Tetrachloroethane ND ug/L 11/10/23 10:39 79-34-510014.8 200
Tetrachloroethene ND ug/L 11/10/23 10:39 127-18-410017.1 200
Toluene 22400 ug/L 11/10/23 10:39 108-88-310018.0 200
1,2,3-Trichlorobenzene ND ug/L 11/10/23 10:39 87-61-640024.2 200
1,2,4-Trichlorobenzene ND ug/L 11/10/23 10:39 120-82-140031.2 200
1,1,1-Trichloroethane ND ug/L 11/10/23 10:39 71-55-610021.4 200
1,1,2-Trichloroethane ND ug/L 11/10/23 10:39 79-00-510019.1 200
Trichloroethene ND ug/L 11/10/23 10:39 79-01-610034.2 200
Trichlorofluoromethane ND ug/L 11/10/23 10:39 75-69-420028.8 200
1,2,3-Trichloropropane ND ug/L 11/10/23 10:39 96-18-410034.6 200
1,2,4-Trimethylbenzene 2850 ug/L 11/10/23 10:39 95-63-61006.1 200
1,3,5-Trimethylbenzene 689 ug/L 11/10/23 10:39 108-67-810014.3 200
Vinyl acetate ND ug/L 11/10/23 10:39 108-05-440021.4 200
Vinyl chloride ND ug/L 11/10/23 10:39 75-01-420029.8 200
Xylene (Total)23600 ug/L 11/10/23 10:39 1330-20-720018.7 200
m&p-Xylene 16400 ug/L 11/10/23 10:39 179601-23-120018.7 200
o-Xylene 7230 ug/L 11/10/23 10:39 95-47-610028.8 200
Surrogates
1,2-Dichloroethane-d4 (S)89 %11/10/23 10:39 17060-07-070-130 200
4-Bromofluorobenzene (S)98 %11/10/23 10:39 460-00-470-130 200
Toluene-d8 (S)103 %11/10/23 10:39 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-2 Lab ID:92696826002 Collected:11/03/23 09:50 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Acetone ND ug/L 11/07/23 18:25 67-64-125.0 1.6 1
Benzene ND ug/L 11/07/23 18:25 71-43-20.50 0.079 1
Bromobenzene ND ug/L 11/07/23 18:25 108-86-10.50 0.14 1
Bromochloromethane ND ug/L 11/07/23 18:25 74-97-50.50 0.094 1
Bromodichloromethane ND ug/L 11/07/23 18:25 75-27-40.50 0.17 1
Bromoform ND ug/L 11/07/23 18:25 75-25-20.50 0.20 1
Bromomethane ND ug/L 11/07/23 18:25 74-83-95.0 0.22 1
2-Butanone (MEK)ND ug/L 11/07/23 18:25 78-93-35.0 0.31 1
n-Butylbenzene ND ug/L 11/07/23 18:25 104-51-80.50 0.066 1
sec-Butylbenzene ND ug/L 11/07/23 18:25 135-98-80.50 0.085 1
tert-Butylbenzene ND ug/L 11/07/23 18:25 98-06-60.50 0.086 1
Carbon tetrachloride ND ug/L 11/07/23 18:25 56-23-50.50 0.17 1
Chlorobenzene ND ug/L 11/07/23 18:25 108-90-70.50 0.085 1
Chloroethane ND ug/L 11/07/23 18:25 75-00-3 M11.0 0.17 1
Chloroform 0.15J ug/L 11/07/23 18:25 67-66-30.50 0.069 1
Chloromethane ND ug/L 11/07/23 18:25 74-87-3 M11.0 0.18 1
2-Chlorotoluene ND ug/L 11/07/23 18:25 95-49-80.50 0.13 1
4-Chlorotoluene ND ug/L 11/07/23 18:25 106-43-40.50 0.096 1
Dibromochloromethane ND ug/L 11/07/23 18:25 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)ND ug/L 11/07/23 18:25 106-93-40.50 0.15 1
1,2-Dichlorobenzene ND ug/L 11/07/23 18:25 95-50-10.50 0.094 1
1,3-Dichlorobenzene ND ug/L 11/07/23 18:25 541-73-10.50 0.098 1
1,4-Dichlorobenzene ND ug/L 11/07/23 18:25 106-46-70.50 0.090 1
Dichlorodifluoromethane ND ug/L 11/07/23 18:25 75-71-80.50 0.12 1
1,1-Dichloroethane ND ug/L 11/07/23 18:25 75-34-30.50 0.056 1
1,2-Dichloroethane ND ug/L 11/07/23 18:25 107-06-20.50 0.11 1
1,1-Dichloroethene ND ug/L 11/07/23 18:25 75-35-4 M10.50 0.079 1
cis-1,2-Dichloroethene ND ug/L 11/07/23 18:25 156-59-20.50 0.11 1
trans-1,2-Dichloroethene ND ug/L 11/07/23 18:25 156-60-50.50 0.10 1
1,2-Dichloropropane ND ug/L 11/07/23 18:25 78-87-50.50 0.14 1
1,3-Dichloropropane ND ug/L 11/07/23 18:25 142-28-90.50 0.085 1
2,2-Dichloropropane ND ug/L 11/07/23 18:25 594-20-70.50 0.12 1
1,1-Dichloropropene ND ug/L 11/07/23 18:25 563-58-6 M10.50 0.066 1
cis-1,3-Dichloropropene ND ug/L 11/07/23 18:25 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene ND ug/L 11/07/23 18:25 10061-02-60.50 0.13 1
Diisopropyl ether ND ug/L 11/07/23 18:25 108-20-30.50 0.072 1
Ethylbenzene ND ug/L 11/07/23 18:25 100-41-40.50 0.081 1
2-Hexanone ND ug/L 11/07/23 18:25 591-78-65.0 0.18 1
Isopropylbenzene (Cumene)ND ug/L 11/07/23 18:25 98-82-8 M10.50 0.11 1
p-Isopropyltoluene ND ug/L 11/07/23 18:25 99-87-6 M10.50 0.089 1
Methylene Chloride ND ug/L 11/07/23 18:25 75-09-22.0 1.9 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/07/23 18:25 108-10-15.0 0.16 1
Methyl-tert-butyl ether ND ug/L 11/07/23 18:25 1634-04-40.50 0.053 1
Naphthalene 0.65J ug/L 11/07/23 18:25 91-20-32.0 0.10 1
n-Propylbenzene ND ug/L 11/07/23 18:25 103-65-10.50 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-2 Lab ID:92696826002 Collected:11/03/23 09:50 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Styrene ND ug/L 11/07/23 18:25 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane ND ug/L 11/07/23 18:25 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane ND ug/L 11/07/23 18:25 79-34-50.50 0.074 1
Tetrachloroethene ND ug/L 11/07/23 18:25 127-18-40.50 0.086 1
Toluene ND ug/L 11/07/23 18:25 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene ND ug/L 11/07/23 18:25 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene ND ug/L 11/07/23 18:25 120-82-12.0 0.16 1
1,1,1-Trichloroethane ND ug/L 11/07/23 18:25 71-55-60.50 0.11 1
1,1,2-Trichloroethane ND ug/L 11/07/23 18:25 79-00-50.50 0.096 1
Trichloroethene ND ug/L 11/07/23 18:25 79-01-60.50 0.17 1
Trichlorofluoromethane ND ug/L 11/07/23 18:25 75-69-41.0 0.14 1
1,2,3-Trichloropropane ND ug/L 11/07/23 18:25 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene ND ug/L 11/07/23 18:25 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene ND ug/L 11/07/23 18:25 108-67-80.50 0.071 1
Vinyl acetate ND ug/L 11/07/23 18:25 108-05-42.0 0.11 1
Vinyl chloride ND ug/L 11/07/23 18:25 75-01-4 M11.0 0.15 1
Xylene (Total)ND ug/L 11/07/23 18:25 1330-20-71.0 0.094 1
m&p-Xylene ND ug/L 11/07/23 18:25 179601-23-11.0 0.094 1
o-Xylene ND ug/L 11/07/23 18:25 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/07/23 18:25 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/07/23 18:25 460-00-470-130 1
Toluene-d8 (S)99 %11/07/23 18:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-3 Lab ID:92696826003 Collected:11/03/23 10:10 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Acetone ND ug/L 11/10/23 09:26 67-64-150031.0 20
Benzene 2060 ug/L 11/10/23 09:26 71-43-210.0 1.6 20
Bromobenzene ND ug/L 11/10/23 09:26 108-86-110.0 2.7 20
Bromochloromethane ND ug/L 11/10/23 09:26 74-97-510.0 1.9 20
Bromodichloromethane ND ug/L 11/10/23 09:26 75-27-410.0 3.4 20
Bromoform ND ug/L 11/10/23 09:26 75-25-210.0 3.9 20
Bromomethane ND ug/L 11/10/23 09:26 74-83-91004.4 20
2-Butanone (MEK)ND ug/L 11/10/23 09:26 78-93-31006.2 20
n-Butylbenzene ND ug/L 11/10/23 09:26 104-51-810.0 1.3 20
sec-Butylbenzene ND ug/L 11/10/23 09:26 135-98-810.0 1.7 20
tert-Butylbenzene ND ug/L 11/10/23 09:26 98-06-610.0 1.7 20
Carbon tetrachloride ND ug/L 11/10/23 09:26 56-23-510.0 3.4 20
Chlorobenzene ND ug/L 11/10/23 09:26 108-90-710.0 1.7 20
Chloroethane ND ug/L 11/10/23 09:26 75-00-320.0 3.5 20
Chloroform ND ug/L 11/10/23 09:26 67-66-310.0 1.4 20
Chloromethane ND ug/L 11/10/23 09:26 74-87-320.0 3.5 20
2-Chlorotoluene ND ug/L 11/10/23 09:26 95-49-810.0 2.6 20
4-Chlorotoluene ND ug/L 11/10/23 09:26 106-43-410.0 1.9 20
Dibromochloromethane ND ug/L 11/10/23 09:26 124-48-110.0 3.0 20
1,2-Dibromoethane (EDB)ND ug/L 11/10/23 09:26 106-93-410.0 2.9 20
1,2-Dichlorobenzene ND ug/L 11/10/23 09:26 95-50-110.0 1.9 20
1,3-Dichlorobenzene ND ug/L 11/10/23 09:26 541-73-110.0 2.0 20
1,4-Dichlorobenzene ND ug/L 11/10/23 09:26 106-46-710.0 1.8 20
Dichlorodifluoromethane ND ug/L 11/10/23 09:26 75-71-810.0 2.5 20
1,1-Dichloroethane ND ug/L 11/10/23 09:26 75-34-310.0 1.1 20
1,2-Dichloroethane ND ug/L 11/10/23 09:26 107-06-210.0 2.1 20
1,1-Dichloroethene ND ug/L 11/10/23 09:26 75-35-410.0 1.6 20
cis-1,2-Dichloroethene ND ug/L 11/10/23 09:26 156-59-210.0 2.2 20
trans-1,2-Dichloroethene ND ug/L 11/10/23 09:26 156-60-510.0 2.0 20
1,2-Dichloropropane ND ug/L 11/10/23 09:26 78-87-510.0 2.7 20
1,3-Dichloropropane ND ug/L 11/10/23 09:26 142-28-910.0 1.7 20
2,2-Dichloropropane ND ug/L 11/10/23 09:26 594-20-710.0 2.4 20
1,1-Dichloropropene ND ug/L 11/10/23 09:26 563-58-610.0 1.3 20
cis-1,3-Dichloropropene ND ug/L 11/10/23 09:26 10061-01-510.0 1.8 20
trans-1,3-Dichloropropene ND ug/L 11/10/23 09:26 10061-02-610.0 2.6 20
Diisopropyl ether 15.4 ug/L 11/10/23 09:26 108-20-310.0 1.4 20
Ethylbenzene 403 ug/L 11/10/23 09:26 100-41-410.0 1.6 20
2-Hexanone ND ug/L 11/10/23 09:26 591-78-61003.5 20
Isopropylbenzene (Cumene)43.1 ug/L 11/10/23 09:26 98-82-810.0 2.1 20
p-Isopropyltoluene ND ug/L 11/10/23 09:26 99-87-610.0 1.8 20
Methylene Chloride ND ug/L 11/10/23 09:26 75-09-240.0 37.8 20
4-Methyl-2-pentanone (MIBK)ND ug/L 11/10/23 09:26 108-10-11003.3 20
Methyl-tert-butyl ether 22.4 ug/L 11/10/23 09:26 1634-04-410.0 1.1 20
Naphthalene 165 ug/L 11/10/23 09:26 91-20-340.0 2.0 20
n-Propylbenzene 140 ug/L 11/10/23 09:26 103-65-110.0 2.1 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-3 Lab ID:92696826003 Collected:11/03/23 10:10 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Styrene ND ug/L 11/10/23 09:26 100-42-510.0 2.7 20
1,1,1,2-Tetrachloroethane ND ug/L 11/10/23 09:26 630-20-610.0 1.8 20
1,1,2,2-Tetrachloroethane ND ug/L 11/10/23 09:26 79-34-510.0 1.5 20
Tetrachloroethene ND ug/L 11/10/23 09:26 127-18-410.0 1.7 20
Toluene 39.4 ug/L 11/10/23 09:26 108-88-310.0 1.8 20
1,2,3-Trichlorobenzene ND ug/L 11/10/23 09:26 87-61-640.0 2.4 20
1,2,4-Trichlorobenzene ND ug/L 11/10/23 09:26 120-82-140.0 3.1 20
1,1,1-Trichloroethane ND ug/L 11/10/23 09:26 71-55-610.0 2.1 20
1,1,2-Trichloroethane ND ug/L 11/10/23 09:26 79-00-510.0 1.9 20
Trichloroethene ND ug/L 11/10/23 09:26 79-01-610.0 3.4 20
Trichlorofluoromethane ND ug/L 11/10/23 09:26 75-69-420.0 2.9 20
1,2,3-Trichloropropane ND ug/L 11/10/23 09:26 96-18-410.0 3.5 20
1,2,4-Trimethylbenzene 15.0 ug/L 11/10/23 09:26 95-63-610.0 0.61 20
1,3,5-Trimethylbenzene ND ug/L 11/10/23 09:26 108-67-810.0 1.4 20
Vinyl acetate ND ug/L 11/10/23 09:26 108-05-440.0 2.1 20
Vinyl chloride ND ug/L 11/10/23 09:26 75-01-420.0 3.0 20
Xylene (Total)125 ug/L 11/10/23 09:26 1330-20-720.0 1.9 20
m&p-Xylene 114 ug/L 11/10/23 09:26 179601-23-120.0 1.9 20
o-Xylene 11.0 ug/L 11/10/23 09:26 95-47-610.0 2.9 20
Surrogates
1,2-Dichloroethane-d4 (S)91 %11/10/23 09:26 17060-07-070-130 20
4-Bromofluorobenzene (S)98 %11/10/23 09:26 460-00-470-130 20
Toluene-d8 (S)104 %11/10/23 09:26 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-4 Lab ID:92696826004 Collected:11/03/23 10:40 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Acetone ND ug/L 11/07/23 18:44 67-64-125.0 1.6 1
Benzene ND ug/L 11/07/23 18:44 71-43-20.50 0.079 1
Bromobenzene ND ug/L 11/07/23 18:44 108-86-10.50 0.14 1
Bromochloromethane ND ug/L 11/07/23 18:44 74-97-50.50 0.094 1
Bromodichloromethane ND ug/L 11/07/23 18:44 75-27-40.50 0.17 1
Bromoform ND ug/L 11/07/23 18:44 75-25-20.50 0.20 1
Bromomethane ND ug/L 11/07/23 18:44 74-83-95.0 0.22 1
2-Butanone (MEK)ND ug/L 11/07/23 18:44 78-93-35.0 0.31 1
n-Butylbenzene ND ug/L 11/07/23 18:44 104-51-80.50 0.066 1
sec-Butylbenzene ND ug/L 11/07/23 18:44 135-98-80.50 0.085 1
tert-Butylbenzene ND ug/L 11/07/23 18:44 98-06-60.50 0.086 1
Carbon tetrachloride ND ug/L 11/07/23 18:44 56-23-50.50 0.17 1
Chlorobenzene ND ug/L 11/07/23 18:44 108-90-70.50 0.085 1
Chloroethane ND ug/L 11/07/23 18:44 75-00-31.0 0.17 1
Chloroform ND ug/L 11/07/23 18:44 67-66-30.50 0.069 1
Chloromethane ND ug/L 11/07/23 18:44 74-87-31.0 0.18 1
2-Chlorotoluene ND ug/L 11/07/23 18:44 95-49-80.50 0.13 1
4-Chlorotoluene ND ug/L 11/07/23 18:44 106-43-40.50 0.096 1
Dibromochloromethane ND ug/L 11/07/23 18:44 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)ND ug/L 11/07/23 18:44 106-93-40.50 0.15 1
1,2-Dichlorobenzene ND ug/L 11/07/23 18:44 95-50-10.50 0.094 1
1,3-Dichlorobenzene ND ug/L 11/07/23 18:44 541-73-10.50 0.098 1
1,4-Dichlorobenzene ND ug/L 11/07/23 18:44 106-46-70.50 0.090 1
Dichlorodifluoromethane ND ug/L 11/07/23 18:44 75-71-80.50 0.12 1
1,1-Dichloroethane ND ug/L 11/07/23 18:44 75-34-30.50 0.056 1
1,2-Dichloroethane ND ug/L 11/07/23 18:44 107-06-20.50 0.11 1
1,1-Dichloroethene ND ug/L 11/07/23 18:44 75-35-40.50 0.079 1
cis-1,2-Dichloroethene ND ug/L 11/07/23 18:44 156-59-20.50 0.11 1
trans-1,2-Dichloroethene ND ug/L 11/07/23 18:44 156-60-50.50 0.10 1
1,2-Dichloropropane ND ug/L 11/07/23 18:44 78-87-50.50 0.14 1
1,3-Dichloropropane ND ug/L 11/07/23 18:44 142-28-90.50 0.085 1
2,2-Dichloropropane ND ug/L 11/07/23 18:44 594-20-70.50 0.12 1
1,1-Dichloropropene ND ug/L 11/07/23 18:44 563-58-60.50 0.066 1
cis-1,3-Dichloropropene ND ug/L 11/07/23 18:44 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene ND ug/L 11/07/23 18:44 10061-02-60.50 0.13 1
Diisopropyl ether 1.2 ug/L 11/07/23 18:44 108-20-30.50 0.072 1
Ethylbenzene ND ug/L 11/07/23 18:44 100-41-40.50 0.081 1
2-Hexanone ND ug/L 11/07/23 18:44 591-78-65.0 0.18 1
Isopropylbenzene (Cumene)ND ug/L 11/07/23 18:44 98-82-80.50 0.11 1
p-Isopropyltoluene ND ug/L 11/07/23 18:44 99-87-60.50 0.089 1
Methylene Chloride ND ug/L 11/07/23 18:44 75-09-22.0 1.9 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/07/23 18:44 108-10-15.0 0.16 1
Methyl-tert-butyl ether 111 ug/L 11/07/23 18:44 1634-04-40.50 0.053 1
Naphthalene ND ug/L 11/07/23 18:44 91-20-32.0 0.10 1
n-Propylbenzene ND ug/L 11/07/23 18:44 103-65-10.50 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-4 Lab ID:92696826004 Collected:11/03/23 10:40 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Styrene ND ug/L 11/07/23 18:44 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane ND ug/L 11/07/23 18:44 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane ND ug/L 11/07/23 18:44 79-34-50.50 0.074 1
Tetrachloroethene ND ug/L 11/07/23 18:44 127-18-40.50 0.086 1
Toluene ND ug/L 11/07/23 18:44 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene ND ug/L 11/07/23 18:44 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene ND ug/L 11/07/23 18:44 120-82-12.0 0.16 1
1,1,1-Trichloroethane ND ug/L 11/07/23 18:44 71-55-60.50 0.11 1
1,1,2-Trichloroethane ND ug/L 11/07/23 18:44 79-00-50.50 0.096 1
Trichloroethene ND ug/L 11/07/23 18:44 79-01-60.50 0.17 1
Trichlorofluoromethane ND ug/L 11/07/23 18:44 75-69-41.0 0.14 1
1,2,3-Trichloropropane ND ug/L 11/07/23 18:44 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene ND ug/L 11/07/23 18:44 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene ND ug/L 11/07/23 18:44 108-67-80.50 0.071 1
Vinyl acetate ND ug/L 11/07/23 18:44 108-05-42.0 0.11 1
Vinyl chloride ND ug/L 11/07/23 18:44 75-01-41.0 0.15 1
Xylene (Total)ND ug/L 11/07/23 18:44 1330-20-71.0 0.094 1
m&p-Xylene ND ug/L 11/07/23 18:44 179601-23-11.0 0.094 1
o-Xylene ND ug/L 11/07/23 18:44 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/07/23 18:44 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/07/23 18:44 460-00-470-130 1
Toluene-d8 (S)99 %11/07/23 18:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-5 Lab ID:92696826005 Collected:11/03/23 11:00 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Acetone 84.9J ug/L 11/10/23 08:31 67-64-11257.8 5
Benzene 503 ug/L 11/10/23 08:31 71-43-22.5 0.39 5
Bromobenzene ND ug/L 11/10/23 08:31 108-86-12.5 0.68 5
Bromochloromethane ND ug/L 11/10/23 08:31 74-97-52.5 0.47 5
Bromodichloromethane ND ug/L 11/10/23 08:31 75-27-42.5 0.85 5
Bromoform ND ug/L 11/10/23 08:31 75-25-22.5 0.98 5
Bromomethane ND ug/L 11/10/23 08:31 74-83-925.0 1.1 5
2-Butanone (MEK)ND ug/L 11/10/23 08:31 78-93-325.0 1.6 5
n-Butylbenzene ND ug/L 11/10/23 08:31 104-51-82.5 0.33 5
sec-Butylbenzene ND ug/L 11/10/23 08:31 135-98-82.5 0.43 5
tert-Butylbenzene ND ug/L 11/10/23 08:31 98-06-62.5 0.43 5
Carbon tetrachloride ND ug/L 11/10/23 08:31 56-23-52.5 0.84 5
Chlorobenzene ND ug/L 11/10/23 08:31 108-90-72.5 0.42 5
Chloroethane ND ug/L 11/10/23 08:31 75-00-35.0 0.86 5
Chloroform ND ug/L 11/10/23 08:31 67-66-32.5 0.35 5
Chloromethane ND ug/L 11/10/23 08:31 74-87-35.0 0.88 5
2-Chlorotoluene ND ug/L 11/10/23 08:31 95-49-82.5 0.64 5
4-Chlorotoluene ND ug/L 11/10/23 08:31 106-43-42.5 0.48 5
Dibromochloromethane ND ug/L 11/10/23 08:31 124-48-12.5 0.74 5
1,2-Dibromoethane (EDB)ND ug/L 11/10/23 08:31 106-93-42.5 0.74 5
1,2-Dichlorobenzene ND ug/L 11/10/23 08:31 95-50-12.5 0.47 5
1,3-Dichlorobenzene ND ug/L 11/10/23 08:31 541-73-12.5 0.49 5
1,4-Dichlorobenzene ND ug/L 11/10/23 08:31 106-46-72.5 0.45 5
Dichlorodifluoromethane ND ug/L 11/10/23 08:31 75-71-82.5 0.62 5
1,1-Dichloroethane ND ug/L 11/10/23 08:31 75-34-32.5 0.28 5
1,2-Dichloroethane ND ug/L 11/10/23 08:31 107-06-22.5 0.53 5
1,1-Dichloroethene ND ug/L 11/10/23 08:31 75-35-42.5 0.39 5
cis-1,2-Dichloroethene ND ug/L 11/10/23 08:31 156-59-22.5 0.56 5
trans-1,2-Dichloroethene ND ug/L 11/10/23 08:31 156-60-52.5 0.50 5
1,2-Dichloropropane ND ug/L 11/10/23 08:31 78-87-52.5 0.68 5
1,3-Dichloropropane ND ug/L 11/10/23 08:31 142-28-92.5 0.43 5
2,2-Dichloropropane ND ug/L 11/10/23 08:31 594-20-72.5 0.61 5
1,1-Dichloropropene ND ug/L 11/10/23 08:31 563-58-62.5 0.33 5
cis-1,3-Dichloropropene ND ug/L 11/10/23 08:31 10061-01-52.5 0.45 5
trans-1,3-Dichloropropene ND ug/L 11/10/23 08:31 10061-02-62.5 0.66 5
Diisopropyl ether 7.9 ug/L 11/10/23 08:31 108-20-32.5 0.36 5
Ethylbenzene 936 ug/L 11/10/23 08:31 100-41-42.5 0.41 5
2-Hexanone ND ug/L 11/10/23 08:31 591-78-625.0 0.88 5
Isopropylbenzene (Cumene)43.9 ug/L 11/10/23 08:31 98-82-82.5 0.53 5
p-Isopropyltoluene ND ug/L 11/10/23 08:31 99-87-62.5 0.45 5
Methylene Chloride ND ug/L 11/10/23 08:31 75-09-210.0 9.4 5
4-Methyl-2-pentanone (MIBK)ND ug/L 11/10/23 08:31 108-10-125.0 0.82 5
Methyl-tert-butyl ether 442 ug/L 11/10/23 08:31 1634-04-42.5 0.27 5
Naphthalene 351 ug/L 11/10/23 08:31 91-20-310.0 0.50 5
n-Propylbenzene 130 ug/L 11/10/23 08:31 103-65-12.5 0.52 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:MW-5 Lab ID:92696826005 Collected:11/03/23 11:00 Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Styrene ND ug/L 11/10/23 08:31 100-42-52.5 0.68 5
1,1,1,2-Tetrachloroethane ND ug/L 11/10/23 08:31 630-20-62.5 0.46 5
1,1,2,2-Tetrachloroethane ND ug/L 11/10/23 08:31 79-34-52.5 0.37 5
Tetrachloroethene ND ug/L 11/10/23 08:31 127-18-42.5 0.43 5
Toluene 39.7 ug/L 11/10/23 08:31 108-88-32.5 0.45 5
1,2,3-Trichlorobenzene ND ug/L 11/10/23 08:31 87-61-610.0 0.60 5
1,2,4-Trichlorobenzene ND ug/L 11/10/23 08:31 120-82-110.0 0.78 5
1,1,1-Trichloroethane ND ug/L 11/10/23 08:31 71-55-62.5 0.54 5
1,1,2-Trichloroethane ND ug/L 11/10/23 08:31 79-00-52.5 0.48 5
Trichloroethene ND ug/L 11/10/23 08:31 79-01-62.5 0.86 5
Trichlorofluoromethane ND ug/L 11/10/23 08:31 75-69-45.0 0.72 5
1,2,3-Trichloropropane ND ug/L 11/10/23 08:31 96-18-42.5 0.86 5
1,2,4-Trimethylbenzene 459 ug/L 11/10/23 08:31 95-63-62.5 0.15 5
1,3,5-Trimethylbenzene 66.3 ug/L 11/10/23 08:31 108-67-82.5 0.36 5
Vinyl acetate ND ug/L 11/10/23 08:31 108-05-410.0 0.54 5
Vinyl chloride ND ug/L 11/10/23 08:31 75-01-45.0 0.74 5
Xylene (Total)799 ug/L 11/10/23 08:31 1330-20-75.0 0.47 5
m&p-Xylene 783 ug/L 11/10/23 08:31 179601-23-15.0 0.47 5
o-Xylene 15.7 ug/L 11/10/23 08:31 95-47-62.5 0.72 5
Surrogates
1,2-Dichloroethane-d4 (S)92 %11/10/23 08:31 17060-07-070-130 5
4-Bromofluorobenzene (S)97 %11/10/23 08:31 460-00-470-130 5
Toluene-d8 (S)103 %11/10/23 08:31 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:TRIP BLANK Lab ID:92696826006 Collected:Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Acetone 2.7J ug/L 11/07/23 15:54 67-64-1 C025.0 1.6 1
Benzene ND ug/L 11/07/23 15:54 71-43-20.50 0.079 1
Bromobenzene ND ug/L 11/07/23 15:54 108-86-10.50 0.14 1
Bromochloromethane ND ug/L 11/07/23 15:54 74-97-50.50 0.094 1
Bromodichloromethane ND ug/L 11/07/23 15:54 75-27-40.50 0.17 1
Bromoform ND ug/L 11/07/23 15:54 75-25-20.50 0.20 1
Bromomethane ND ug/L 11/07/23 15:54 74-83-95.0 0.22 1
2-Butanone (MEK)ND ug/L 11/07/23 15:54 78-93-35.0 0.31 1
n-Butylbenzene ND ug/L 11/07/23 15:54 104-51-80.50 0.066 1
sec-Butylbenzene ND ug/L 11/07/23 15:54 135-98-80.50 0.085 1
tert-Butylbenzene ND ug/L 11/07/23 15:54 98-06-60.50 0.086 1
Carbon tetrachloride ND ug/L 11/07/23 15:54 56-23-50.50 0.17 1
Chlorobenzene ND ug/L 11/07/23 15:54 108-90-70.50 0.085 1
Chloroethane ND ug/L 11/07/23 15:54 75-00-31.0 0.17 1
Chloroform ND ug/L 11/07/23 15:54 67-66-30.50 0.069 1
Chloromethane ND ug/L 11/07/23 15:54 74-87-31.0 0.18 1
2-Chlorotoluene ND ug/L 11/07/23 15:54 95-49-80.50 0.13 1
4-Chlorotoluene ND ug/L 11/07/23 15:54 106-43-40.50 0.096 1
Dibromochloromethane ND ug/L 11/07/23 15:54 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)ND ug/L 11/07/23 15:54 106-93-40.50 0.15 1
1,2-Dichlorobenzene ND ug/L 11/07/23 15:54 95-50-10.50 0.094 1
1,3-Dichlorobenzene ND ug/L 11/07/23 15:54 541-73-10.50 0.098 1
1,4-Dichlorobenzene ND ug/L 11/07/23 15:54 106-46-70.50 0.090 1
Dichlorodifluoromethane ND ug/L 11/07/23 15:54 75-71-80.50 0.12 1
1,1-Dichloroethane ND ug/L 11/07/23 15:54 75-34-30.50 0.056 1
1,2-Dichloroethane ND ug/L 11/07/23 15:54 107-06-20.50 0.11 1
1,1-Dichloroethene ND ug/L 11/07/23 15:54 75-35-40.50 0.079 1
cis-1,2-Dichloroethene ND ug/L 11/07/23 15:54 156-59-20.50 0.11 1
trans-1,2-Dichloroethene ND ug/L 11/07/23 15:54 156-60-50.50 0.10 1
1,2-Dichloropropane ND ug/L 11/07/23 15:54 78-87-50.50 0.14 1
1,3-Dichloropropane ND ug/L 11/07/23 15:54 142-28-90.50 0.085 1
2,2-Dichloropropane ND ug/L 11/07/23 15:54 594-20-70.50 0.12 1
1,1-Dichloropropene ND ug/L 11/07/23 15:54 563-58-60.50 0.066 1
cis-1,3-Dichloropropene ND ug/L 11/07/23 15:54 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene ND ug/L 11/07/23 15:54 10061-02-60.50 0.13 1
Diisopropyl ether ND ug/L 11/07/23 15:54 108-20-30.50 0.072 1
Ethylbenzene ND ug/L 11/07/23 15:54 100-41-40.50 0.081 1
2-Hexanone ND ug/L 11/07/23 15:54 591-78-65.0 0.18 1
Isopropylbenzene (Cumene)ND ug/L 11/07/23 15:54 98-82-80.50 0.11 1
p-Isopropyltoluene ND ug/L 11/07/23 15:54 99-87-60.50 0.089 1
Methylene Chloride ND ug/L 11/07/23 15:54 75-09-22.0 1.9 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/07/23 15:54 108-10-15.0 0.16 1
Methyl-tert-butyl ether ND ug/L 11/07/23 15:54 1634-04-40.50 0.053 1
Naphthalene ND ug/L 11/07/23 15:54 91-20-32.0 0.10 1
n-Propylbenzene ND ug/L 11/07/23 15:54 103-65-10.50 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696826
GPM 6035
Sample:TRIP BLANK Lab ID:92696826006 Collected:Received:11/03/23 13:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Styrene ND ug/L 11/07/23 15:54 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane ND ug/L 11/07/23 15:54 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane ND ug/L 11/07/23 15:54 79-34-50.50 0.074 1
Tetrachloroethene ND ug/L 11/07/23 15:54 127-18-40.50 0.086 1
Toluene ND ug/L 11/07/23 15:54 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene ND ug/L 11/07/23 15:54 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene ND ug/L 11/07/23 15:54 120-82-12.0 0.16 1
1,1,1-Trichloroethane ND ug/L 11/07/23 15:54 71-55-60.50 0.11 1
1,1,2-Trichloroethane ND ug/L 11/07/23 15:54 79-00-50.50 0.096 1
Trichloroethene ND ug/L 11/07/23 15:54 79-01-60.50 0.17 1
Trichlorofluoromethane ND ug/L 11/07/23 15:54 75-69-41.0 0.14 1
1,2,3-Trichloropropane ND ug/L 11/07/23 15:54 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene ND ug/L 11/07/23 15:54 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene ND ug/L 11/07/23 15:54 108-67-80.50 0.071 1
Vinyl acetate ND ug/L 11/07/23 15:54 108-05-42.0 0.11 1
Vinyl chloride ND ug/L 11/07/23 15:54 75-01-41.0 0.15 1
Xylene (Total)ND ug/L 11/07/23 15:54 1330-20-71.0 0.094 1
m&p-Xylene ND ug/L 11/07/23 15:54 179601-23-11.0 0.094 1
o-Xylene ND ug/L 11/07/23 15:54 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/07/23 15:54 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %11/07/23 15:54 460-00-470-130 1
Toluene-d8 (S)99 %11/07/23 15:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811308
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696826006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4200563
Associated Lab Samples:92696826006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/07/23 04:100.091
1,1,1-Trichloroethane ug/L ND 0.50 11/07/23 04:100.11
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/07/23 04:100.074
1,1,2-Trichloroethane ug/L ND 0.50 11/07/23 04:100.096
1,1-Dichloroethane ug/L ND 0.50 11/07/23 04:100.056
1,1-Dichloroethene ug/L ND 0.50 11/07/23 04:100.079
1,1-Dichloropropene ug/L ND 0.50 11/07/23 04:100.066
1,2,3-Trichlorobenzene ug/L ND 2.0 11/07/23 04:100.12
1,2,3-Trichloropropane ug/L ND 0.50 11/07/23 04:100.17
1,2,4-Trichlorobenzene ug/L ND 2.0 11/07/23 04:100.16
1,2,4-Trimethylbenzene ug/L ND 0.50 11/07/23 04:100.031
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/07/23 04:100.15
1,2-Dichlorobenzene ug/L ND 0.50 11/07/23 04:100.094
1,2-Dichloroethane ug/L ND 0.50 11/07/23 04:100.11
1,2-Dichloropropane ug/L ND 0.50 11/07/23 04:100.14
1,3,5-Trimethylbenzene ug/L ND 0.50 11/07/23 04:100.071
1,3-Dichlorobenzene ug/L ND 0.50 11/07/23 04:100.098
1,3-Dichloropropane ug/L ND 0.50 11/07/23 04:100.085
1,4-Dichlorobenzene ug/L ND 0.50 11/07/23 04:100.090
2,2-Dichloropropane ug/L ND 0.50 11/07/23 04:100.12
2-Butanone (MEK)ug/L ND 5.0 11/07/23 04:100.31
2-Chlorotoluene ug/L ND 0.50 11/07/23 04:100.13
2-Hexanone ug/L ND 5.0 11/07/23 04:100.18
4-Chlorotoluene ug/L ND 0.50 11/07/23 04:100.096
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/07/23 04:100.16
Acetone ug/L ND 25.0 11/07/23 04:101.6
Benzene ug/L ND 0.50 11/07/23 04:100.079
Bromobenzene ug/L ND 0.50 11/07/23 04:100.14
Bromochloromethane ug/L ND 0.50 11/07/23 04:100.094
Bromodichloromethane ug/L ND 0.50 11/07/23 04:100.17
Bromoform ug/L ND 0.50 11/07/23 04:100.20
Bromomethane ug/L ND 5.0 11/07/23 04:100.22
Carbon tetrachloride ug/L ND 0.50 11/07/23 04:100.17
Chlorobenzene ug/L ND 0.50 11/07/23 04:100.085
Chloroethane ug/L ND 1.0 11/07/23 04:100.17
Chloroform ug/L ND 0.50 11/07/23 04:100.069
Chloromethane ug/L ND 1.0 11/07/23 04:100.18
cis-1,2-Dichloroethene ug/L ND 0.50 11/07/23 04:100.11
cis-1,3-Dichloropropene ug/L ND 0.50 11/07/23 04:100.090
Dibromochloromethane ug/L ND 0.50 11/07/23 04:100.15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4200563
Associated Lab Samples:92696826006
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 0.50 11/07/23 04:100.12
Diisopropyl ether ug/L ND 0.50 11/07/23 04:100.072
Ethylbenzene ug/L ND 0.50 11/07/23 04:100.081
Isopropylbenzene (Cumene)ug/L ND 0.50 11/07/23 04:100.11
m&p-Xylene ug/L ND 1.0 11/07/23 04:100.094
Methyl-tert-butyl ether ug/L ND 0.50 11/07/23 04:100.053
Methylene Chloride ug/L ND 2.0 11/07/23 04:101.9
n-Butylbenzene ug/L ND 0.50 11/07/23 04:100.066
n-Propylbenzene ug/L ND 0.50 11/07/23 04:100.10
Naphthalene ug/L ND 2.0 11/07/23 04:100.10
o-Xylene ug/L ND 0.50 11/07/23 04:100.14
p-Isopropyltoluene ug/L ND 0.50 11/07/23 04:100.089
sec-Butylbenzene ug/L ND 0.50 11/07/23 04:100.085
Styrene ug/L ND 0.50 11/07/23 04:100.14
tert-Butylbenzene ug/L ND 0.50 11/07/23 04:100.086
Tetrachloroethene ug/L ND 0.50 11/07/23 04:100.086
Toluene ug/L ND 0.50 11/07/23 04:100.090
trans-1,2-Dichloroethene ug/L ND 0.50 11/07/23 04:100.10
trans-1,3-Dichloropropene ug/L ND 0.50 11/07/23 04:100.13
Trichloroethene ug/L ND 0.50 11/07/23 04:100.17
Trichlorofluoromethane ug/L ND 1.0 11/07/23 04:100.14
Vinyl acetate ug/L ND 2.0 11/07/23 04:100.11
Vinyl chloride ug/L ND 1.0 11/07/23 04:100.15
Xylene (Total)ug/L ND 1.0 11/07/23 04:100.094
1,2-Dichloroethane-d4 (S)%93 70-130 11/07/23 04:10
4-Bromofluorobenzene (S)%98 70-130 11/07/23 04:10
Toluene-d8 (S)%99 70-130 11/07/23 04:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200564LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.120 96 60-140
1,1,1-Trichloroethane ug/L 18.420 92 60-140
1,1,2,2-Tetrachloroethane ug/L 19.520 97 60-140
1,1,2-Trichloroethane ug/L 20.320 102 60-140
1,1-Dichloroethane ug/L 18.420 92 60-140
1,1-Dichloroethene ug/L 19.820 99 60-140
1,1-Dichloropropene ug/L 19.920 100 60-140
1,2,3-Trichlorobenzene ug/L 19.720 99 60-140
1,2,3-Trichloropropane ug/L 18.820 94 60-140
1,2,4-Trichlorobenzene ug/L 19.220 96 60-140
1,2,4-Trimethylbenzene ug/L 19.320 96 60-140
1,2-Dibromoethane (EDB)ug/L 19.420 97 60-140
1,2-Dichlorobenzene ug/L 20.020 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200564LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 18.220 91 60-140
1,2-Dichloropropane ug/L 19.020 95 60-140
1,3,5-Trimethylbenzene ug/L 19.020 95 60-140
1,3-Dichlorobenzene ug/L 20.020 100 60-140
1,3-Dichloropropane ug/L 18.620 93 60-140
1,4-Dichlorobenzene ug/L 19.320 97 60-140
2,2-Dichloropropane ug/L 17.320 86 60-140
2-Butanone (MEK)ug/L 35.840 90 60-140
2-Chlorotoluene ug/L 18.820 94 60-140
2-Hexanone ug/L 38.040 95 60-140
4-Chlorotoluene ug/L 18.820 94 60-140
4-Methyl-2-pentanone (MIBK)ug/L 37.540 94 60-140
Acetone ug/L 37.740 94 60-140
Benzene ug/L 19.420 97 60-140
Bromobenzene ug/L 19.620 98 60-140
Bromochloromethane ug/L 19.920 99 60-140
Bromodichloromethane ug/L 17.820 89 60-140
Bromoform ug/L 18.620 93 60-140
Bromomethane ug/L 13.920 70 60-140
Carbon tetrachloride ug/L 18.620 93 60-140
Chlorobenzene ug/L 19.520 98 60-140
Chloroethane ug/L 17.820 89 60-140
Chloroform ug/L 18.220 91 60-140
Chloromethane ug/L 20.120 101 60-140
cis-1,2-Dichloroethene ug/L 18.620 93 60-140
cis-1,3-Dichloropropene ug/L 18.020 90 60-140
Dibromochloromethane ug/L 19.020 95 60-140
Dichlorodifluoromethane ug/L 17.120 86 60-140
Diisopropyl ether ug/L 18.020 90 60-140
Ethylbenzene ug/L 18.520 93 60-140
Isopropylbenzene (Cumene)ug/L 19.520 97 60-140
m&p-Xylene ug/L 37.640 94 60-140
Methyl-tert-butyl ether ug/L 17.720 89 60-140
Methylene Chloride ug/L 19.720 99 60-140
n-Butylbenzene ug/L 19.620 98 60-140
n-Propylbenzene ug/L 18.620 93 60-140
Naphthalene ug/L 19.920 99 60-140
o-Xylene ug/L 19.320 97 60-140
p-Isopropyltoluene ug/L 19.420 97 60-140
sec-Butylbenzene ug/L 19.220 96 60-140
Styrene ug/L 19.420 97 60-140
tert-Butylbenzene ug/L 19.020 95 60-140
Tetrachloroethene ug/L 20.820 104 60-140
Toluene ug/L 18.820 94 60-140
trans-1,2-Dichloroethene ug/L 19.620 98 60-140
trans-1,3-Dichloropropene ug/L 17.920 89 60-140
Trichloroethene ug/L 19.320 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200564LABORATORY CONTROL SAMPLE:
LCSSpike
Trichlorofluoromethane ug/L 16.820 84 60-140
Vinyl acetate ug/L 36.840 92 60-140
Vinyl chloride ug/L 17.520 88 60-140
Xylene (Total)ug/L 56.960 95 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4200565MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696632006
4200566
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 69 60-14081 15 3020ND13.9 16.1
1,1,1-Trichloroethane ug/L 20 71 60-14081 13 3020ND14.3 16.2
1,1,2,2-Tetrachloroethane ug/L 20 69 60-14079 15 3020ND13.7 15.9
1,1,2-Trichloroethane ug/L 20 74 60-14084 13 3020ND14.8 16.8
1,1-Dichloroethane ug/L 20 73 60-14082 12 3020ND14.5 16.4
1,1-Dichloroethene ug/L 20 81 60-14092 12 3020ND16.3 18.3
1,1-Dichloropropene ug/L 20 80 60-14090 11 3020ND16.1 18.0
1,2,3-Trichlorobenzene ug/L 20 70 60-14076 8 3020ND14.1 15.2
1,2,3-Trichloropropane ug/L 20 68 60-14076 11 3020ND13.5 15.1
1,2,4-Trichlorobenzene ug/L 20 71 60-14079 11 3020ND14.1 15.7
1,2,4-Trimethylbenzene ug/L 20 72 60-14083 14 30200.15J 14.6 16.8
1,2-Dibromoethane (EDB)ug/L 20 70 60-14078 11 3020ND13.9 15.6
1,2-Dichlorobenzene ug/L 20 72 60-14083 14 3020ND14.4 16.6
1,2-Dichloroethane ug/L 20 69 60-14079 14 3020ND13.8 15.9
1,2-Dichloropropane ug/L 20 72 60-14083 13 3020ND14.4 16.5
1,3,5-Trimethylbenzene ug/L 20 71 60-14081 13 3020ND14.3 16.3
1,3-Dichlorobenzene ug/L 20 74 60-14084 13 3020ND14.8 16.8
1,3-Dichloropropane ug/L 20 68 60-14077 12 3020ND13.6 15.4
1,4-Dichlorobenzene ug/L 20 73 60-14081 11 3020ND14.6 16.3
2,2-Dichloropropane ug/L 20 73 60-14087 17 3020ND14.6 17.3
2-Butanone (MEK)ug/L 40 66 60-14075 14 3040ND26.3 30.2
2-Chlorotoluene ug/L 20 71 60-14081 13 3020ND14.2 16.3
2-Hexanone ug/L 40 66 60-14074 12 3040ND26.3 29.7
4-Chlorotoluene ug/L 20 72 60-14082 13 3020ND14.5 16.5
4-Methyl-2-pentanone
(MIBK)
ug/L 40 67 60-14075 11 3040ND27.0 30.1
Acetone ug/L 40 66 60-14071 8 3040ND27.7 29.9
Benzene ug/L 20 74 60-14084 12 30200.12J 15.0 16.9
Bromobenzene ug/L 20 71 60-14082 15 3020ND14.1 16.5
Bromochloromethane ug/L 20 73 60-14084 14 3020ND14.6 16.8
Bromodichloromethane ug/L 20 67 60-14075 11 3020ND13.4 15.0
Bromoform ug/L 20 63 60-14073 14 3020ND12.7 14.6
Bromomethane ug/L 20 70 60-14078 11 3020ND14.0 15.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4200565MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696632006
4200566
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 20 75 60-14083 11 3020ND14.9 16.7
Chlorobenzene ug/L 20 74 60-14082 10 3020ND14.8 16.3
Chloroethane ug/L 20 75 60-14085 13 3020ND14.9 17.0
Chloroform ug/L 20 69 60-14079 14 3020ND13.8 15.9
Chloromethane ug/L 20 79 60-14088 10 3020ND15.9 17.5
cis-1,2-Dichloroethene ug/L 20 73 60-14082 12 3020ND14.6 16.5
cis-1,3-Dichloropropene ug/L 20 68 60-14079 15 3020ND13.5 15.8
Dibromochloromethane ug/L 20 67 60-14077 14 3020ND13.4 15.4
Dichlorodifluoromethane ug/L 20 80 60-14088 10 3020ND16.0 17.6
Diisopropyl ether ug/L 20 66 60-14076 14 3020ND13.2 15.2
Ethylbenzene ug/L 20 71 60-14080 12 3020ND14.3 16.0
Isopropylbenzene
(Cumene)ug/L 20 75 60-14084 11 3020ND15.1 16.8
m&p-Xylene ug/L 40 71 60-14080 11 30400.36J 29.0 32.4
Methyl-tert-butyl ether ug/L 20 64 60-14072 12 3020ND12.7 14.4
Methylene Chloride ug/L 20 70 60-14078 11 3020ND14.3 15.9
n-Butylbenzene ug/L 20 80 60-14088 10 3020ND15.9 17.6
n-Propylbenzene ug/L 20 73 60-14083 13 3020ND14.6 16.6
Naphthalene ug/L 20 66 60-14074 12 30200.41J 13.6 15.3
o-Xylene ug/L 20 71 60-14080 12 30200.15J 14.4 16.1
p-Isopropyltoluene ug/L 20 76 60-14087 14 3020ND15.1 17.3
sec-Butylbenzene ug/L 20 76 60-14086 12 3020ND15.1 17.1
Styrene ug/L 20 71 60-14080 13 3020ND14.1 16.1
tert-Butylbenzene ug/L 20 61 60-14068 11 3020ND12.1 13.6
Tetrachloroethene ug/L 20 76 60-14084 11 3020ND15.1 16.8
Toluene ug/L 20 71 60-14079 10 30200.30J 14.6 16.1
trans-1,2-Dichloroethene ug/L 20 79 60-14087 9 30200.26J 16.0 17.6
trans-1,3-Dichloropropene ug/L 20 67 60-14076 13 3020ND13.4 15.1
Trichloroethene ug/L 20 75 60-14084 12 3020ND14.9 16.9
Trichlorofluoromethane ug/L 20 72 60-14080 12 3020ND14.3 16.1
Vinyl acetate ug/L 40 63 60-14071 11 3040ND25.3 28.3
Vinyl chloride ug/L 20 73 60-14082 12 3020ND14.6 16.5
Xylene (Total)ug/L 60 71 60-14080 11 30600.51J 43.3 48.6
1,2-Dichloroethane-d4 (S)%96 70-13093
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811311
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696826002, 92696826004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4200582
Associated Lab Samples:92696826002, 92696826004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/07/23 11:270.091
1,1,1-Trichloroethane ug/L ND 0.50 11/07/23 11:270.11
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/07/23 11:270.074
1,1,2-Trichloroethane ug/L ND 0.50 11/07/23 11:270.096
1,1-Dichloroethane ug/L ND 0.50 11/07/23 11:270.056
1,1-Dichloroethene ug/L ND 0.50 11/07/23 11:270.079
1,1-Dichloropropene ug/L ND 0.50 11/07/23 11:270.066
1,2,3-Trichlorobenzene ug/L ND 2.0 11/07/23 11:270.12
1,2,3-Trichloropropane ug/L ND 0.50 11/07/23 11:270.17
1,2,4-Trichlorobenzene ug/L ND 2.0 11/07/23 11:270.16
1,2,4-Trimethylbenzene ug/L ND 0.50 11/07/23 11:270.031
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/07/23 11:270.15
1,2-Dichlorobenzene ug/L ND 0.50 11/07/23 11:270.094
1,2-Dichloroethane ug/L ND 0.50 11/07/23 11:270.11
1,2-Dichloropropane ug/L ND 0.50 11/07/23 11:270.14
1,3,5-Trimethylbenzene ug/L ND 0.50 11/07/23 11:270.071
1,3-Dichlorobenzene ug/L ND 0.50 11/07/23 11:270.098
1,3-Dichloropropane ug/L ND 0.50 11/07/23 11:270.085
1,4-Dichlorobenzene ug/L ND 0.50 11/07/23 11:270.090
2,2-Dichloropropane ug/L ND 0.50 11/07/23 11:270.12
2-Butanone (MEK)ug/L ND 5.0 11/07/23 11:270.31
2-Chlorotoluene ug/L ND 0.50 11/07/23 11:270.13
2-Hexanone ug/L ND 5.0 11/07/23 11:270.18
4-Chlorotoluene ug/L ND 0.50 11/07/23 11:270.096
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/07/23 11:270.16
Acetone ug/L ND 25.0 11/07/23 11:271.6
Benzene ug/L ND 0.50 11/07/23 11:270.079
Bromobenzene ug/L ND 0.50 11/07/23 11:270.14
Bromochloromethane ug/L ND 0.50 11/07/23 11:270.094
Bromodichloromethane ug/L ND 0.50 11/07/23 11:270.17
Bromoform ug/L ND 0.50 11/07/23 11:270.20
Bromomethane ug/L ND 5.0 11/07/23 11:270.22
Carbon tetrachloride ug/L ND 0.50 11/07/23 11:270.17
Chlorobenzene ug/L ND 0.50 11/07/23 11:270.085
Chloroethane ug/L ND 1.0 11/07/23 11:270.17
Chloroform ug/L ND 0.50 11/07/23 11:270.069
Chloromethane ug/L ND 1.0 11/07/23 11:270.18
cis-1,2-Dichloroethene ug/L ND 0.50 11/07/23 11:270.11
cis-1,3-Dichloropropene ug/L ND 0.50 11/07/23 11:270.090
Dibromochloromethane ug/L ND 0.50 11/07/23 11:270.15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4200582
Associated Lab Samples:92696826002, 92696826004
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 0.50 11/07/23 11:270.12
Diisopropyl ether ug/L ND 0.50 11/07/23 11:270.072
Ethylbenzene ug/L ND 0.50 11/07/23 11:270.081
Isopropylbenzene (Cumene)ug/L ND 0.50 11/07/23 11:270.11
m&p-Xylene ug/L ND 1.0 11/07/23 11:270.094
Methyl-tert-butyl ether ug/L ND 0.50 11/07/23 11:270.053
Methylene Chloride ug/L ND 2.0 11/07/23 11:271.9
n-Butylbenzene ug/L ND 0.50 11/07/23 11:270.066
n-Propylbenzene ug/L ND 0.50 11/07/23 11:270.10
Naphthalene ug/L ND 2.0 11/07/23 11:270.10
o-Xylene ug/L ND 0.50 11/07/23 11:270.14
p-Isopropyltoluene ug/L ND 0.50 11/07/23 11:270.089
sec-Butylbenzene ug/L ND 0.50 11/07/23 11:270.085
Styrene ug/L ND 0.50 11/07/23 11:270.14
tert-Butylbenzene ug/L ND 0.50 11/07/23 11:270.086
Tetrachloroethene ug/L ND 0.50 11/07/23 11:270.086
Toluene ug/L ND 0.50 11/07/23 11:270.090
trans-1,2-Dichloroethene ug/L ND 0.50 11/07/23 11:270.10
trans-1,3-Dichloropropene ug/L ND 0.50 11/07/23 11:270.13
Trichloroethene ug/L ND 0.50 11/07/23 11:270.17
Trichlorofluoromethane ug/L ND 1.0 11/07/23 11:270.14
Vinyl acetate ug/L ND 2.0 11/07/23 11:270.11
Vinyl chloride ug/L ND 1.0 11/07/23 11:270.15
Xylene (Total)ug/L ND 1.0 11/07/23 11:270.094
1,2-Dichloroethane-d4 (S)%100 70-130 11/07/23 11:27
4-Bromofluorobenzene (S)%101 70-130 11/07/23 11:27
Toluene-d8 (S)%99 70-130 11/07/23 11:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200583LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.820 109 60-140
1,1,1-Trichloroethane ug/L 21.920 109 60-140
1,1,2,2-Tetrachloroethane ug/L 22.020 110 60-140
1,1,2-Trichloroethane ug/L 21.720 109 60-140
1,1-Dichloroethane ug/L 21.520 108 60-140
1,1-Dichloroethene ug/L 24.020 120 60-140
1,1-Dichloropropene ug/L 23.720 119 60-140
1,2,3-Trichlorobenzene ug/L 22.720 113 60-140
1,2,3-Trichloropropane ug/L 20.620 103 60-140
1,2,4-Trichlorobenzene ug/L 22.620 113 60-140
1,2,4-Trimethylbenzene ug/L 23.320 116 60-140
1,2-Dibromoethane (EDB)ug/L 22.220 111 60-140
1,2-Dichlorobenzene ug/L 22.220 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200583LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 21.020 105 60-140
1,2-Dichloropropane ug/L 22.220 111 60-140
1,3,5-Trimethylbenzene ug/L 23.220 116 60-140
1,3-Dichlorobenzene ug/L 22.020 110 60-140
1,3-Dichloropropane ug/L 21.520 108 60-140
1,4-Dichlorobenzene ug/L 21.320 106 60-140
2,2-Dichloropropane ug/L 22.420 112 60-140
2-Butanone (MEK)ug/L 43.240 108 60-140
2-Chlorotoluene ug/L 22.220 111 60-140
2-Hexanone ug/L 47.640 119 60-140
4-Chlorotoluene ug/L 22.420 112 60-140
4-Methyl-2-pentanone (MIBK)ug/L 44.040 110 60-140
Acetone ug/L 43.740 109 60-140
Benzene ug/L 21.820 109 60-140
Bromobenzene ug/L 21.320 106 60-140
Bromochloromethane ug/L 21.420 107 60-140
Bromodichloromethane ug/L 20.620 103 60-140
Bromoform ug/L 21.320 107 60-140
Bromomethane ug/L 17.320 86 60-140
Carbon tetrachloride ug/L 21.220 106 60-140
Chlorobenzene ug/L 21.220 106 60-140
Chloroethane ug/L 24.320 122 60-140
Chloroform ug/L 21.320 106 60-140
Chloromethane ug/L 27.920 140 60-140
cis-1,2-Dichloroethene ug/L 21.720 108 60-140
cis-1,3-Dichloropropene ug/L 22.020 110 60-140
Dibromochloromethane ug/L 21.320 106 60-140
Dichlorodifluoromethane ug/L 26.720 134 60-140
Diisopropyl ether ug/L 21.820 109 60-140
Ethylbenzene ug/L 21.720 108 60-140
Isopropylbenzene (Cumene)ug/L 23.520 117 60-140
m&p-Xylene ug/L 45.140 113 60-140
Methyl-tert-butyl ether ug/L 21.020 105 60-140
Methylene Chloride ug/L 21.120 105 60-140
n-Butylbenzene ug/L 23.920 120 60-140
n-Propylbenzene ug/L 22.120 110 60-140
Naphthalene ug/L 23.220 116 60-140
o-Xylene ug/L 23.320 116 60-140
p-Isopropyltoluene ug/L 24.120 121 60-140
sec-Butylbenzene ug/L 23.320 117 60-140
Styrene ug/L 23.720 119 60-140
tert-Butylbenzene ug/L 18.420 92 60-140
Tetrachloroethene ug/L 21.820 109 60-140
Toluene ug/L 20.820 104 60-140
trans-1,2-Dichloroethene ug/L 22.620 113 60-140
trans-1,3-Dichloropropene ug/L 22.120 110 60-140
Trichloroethene ug/L 21.520 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200583LABORATORY CONTROL SAMPLE:
LCSSpike
Trichlorofluoromethane ug/L 22.420 112 60-140
Vinyl acetate ug/L 46.340 116 60-140
Vinyl chloride ug/L 24.520 123 60-140
Xylene (Total)ug/L 68.460 114 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4200584MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696826002
4200585
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 134 60-140116 14 3020ND26.8 23.2
1,1,1-Trichloroethane ug/L 20 139 60-140119 15 3020ND27.8 23.8
1,1,2,2-Tetrachloroethane ug/L 20 129 60-140114 12 3020ND25.8 22.8
1,1,2-Trichloroethane ug/L 20 129 60-140114 13 3020ND25.8 22.7
1,1-Dichloroethane ug/L 20 134 60-140115 15 3020ND26.7 23.0
1,1-Dichloroethene ug/L M12015460-140131 16 3020ND30.8 26.3
1,1-Dichloropropene ug/L M12014960-140129 14 3020ND29.7 25.8
1,2,3-Trichlorobenzene ug/L 20 129 60-140117 10 3020ND25.7 23.3
1,2,3-Trichloropropane ug/L 20 121 60-140106 13 3020ND24.1 21.2
1,2,4-Trichlorobenzene ug/L 20 128 60-140113 13 3020ND25.6 22.6
1,2,4-Trimethylbenzene ug/L 20 139 60-140118 16 3020ND27.7 23.6
1,2-Dibromoethane (EDB)ug/L 20 131 60-140115 13 3020ND26.1 23.1
1,2-Dichlorobenzene ug/L 20 129 60-140112 14 3020ND25.7 22.3
1,2-Dichloroethane ug/L 20 123 60-140107 14 3020ND24.6 21.5
1,2-Dichloropropane ug/L 20 137 60-140119 14 3020ND27.3 23.8
1,3,5-Trimethylbenzene ug/L 20 139 60-140118 16 3020ND27.8 23.7
1,3-Dichlorobenzene ug/L 20 131 60-140113 14 3020ND26.1 22.6
1,3-Dichloropropane ug/L 20 128 60-140111 15 3020ND25.7 22.1
1,4-Dichlorobenzene ug/L 20 124 60-140107 15 3020ND24.7 21.4
2,2-Dichloropropane ug/L 20 136 60-140116 16 3020ND27.2 23.2
2-Butanone (MEK)ug/L 40 135 60-140118 14 3040ND53.9 47.0
2-Chlorotoluene ug/L 20 134 60-140115 15 3020ND26.7 23.0
2-Hexanone ug/L 40 138 60-140122 13 3040ND55.3 48.7
4-Chlorotoluene ug/L 20 133 60-140114 15 3020ND26.7 22.8
4-Methyl-2-pentanone
(MIBK)
ug/L 40 129 60-140114 12 3040ND51.6 45.6
Acetone ug/L 40 117 60-140107 9 3040ND46.8 42.9
Benzene ug/L 20 133 60-140115 14 3020ND26.7 23.1
Bromobenzene ug/L 20 127 60-140108 16 3020ND25.4 21.6
Bromochloromethane ug/L 20 129 60-140112 15 3020ND25.9 22.4
Bromodichloromethane ug/L 20 126 60-140109 15 3020ND25.2 21.8
Bromoform ug/L 20 127 60-140110 15 3020ND25.4 21.9
Bromomethane ug/L 20 116 60-140103 12 3020ND23.3 20.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4200584MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696826002
4200585
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 20 139 60-140120 14 3020ND27.7 24.1
Chlorobenzene ug/L 20 130 60-140112 15 3020ND26.0 22.4
Chloroethane ug/L M12014560-140125 15 3020ND29.0 25.1
Chloroform ug/L 20 130 60-140110 17 30200.15J 26.2 22.1
Chloromethane ug/L M12016760-140147 13 3020ND33.5 29.4
cis-1,2-Dichloroethene ug/L 20 134 60-140113 17 3020ND26.9 22.6
cis-1,3-Dichloropropene ug/L 20 128 60-140111 14 3020ND25.7 22.2
Dibromochloromethane ug/L 20 129 60-140112 14 3020ND25.8 22.3
Dichlorodifluoromethane ug/L 20 138 60-140117 16 3020ND27.6 23.5
Diisopropyl ether ug/L 20 132 60-140113 15 3020ND26.4 22.7
Ethylbenzene ug/L 20 131 60-140114 14 3020ND26.2 22.8
Isopropylbenzene
(Cumene)ug/L M12014360-140124 14 3020ND28.5 24.8
m&p-Xylene ug/L 40 135 60-140117 15 3040ND54.1 46.6
Methyl-tert-butyl ether ug/L 20 122 60-140107 13 3020ND24.4 21.4
Methylene Chloride ug/L 20 126 60-140108 15 3020ND25.2 21.6
n-Butylbenzene ug/L 20 140 60-140124 13 3020ND28.1 24.7
n-Propylbenzene ug/L 20 131 60-140114 14 3020ND26.3 22.9
Naphthalene ug/L 20 129 60-140115 11 30200.65J 26.4 23.6
o-Xylene ug/L 20 135 60-140118 14 3020ND27.0 23.5
p-Isopropyltoluene ug/L M12014560-140124 15 3020ND29.0 24.8
sec-Butylbenzene ug/L 20 139 60-140120 14 3020ND27.8 24.0
Styrene ug/L 20 140 60-140123 13 3020ND28.0 24.6
tert-Butylbenzene ug/L 20 112 60-14095 16 3020ND22.3 19.1
Tetrachloroethene ug/L 20 135 60-140117 14 3020ND26.9 23.5
Toluene ug/L 20 128 60-140112 14 3020ND25.7 22.4
trans-1,2-Dichloroethene ug/L 20 139 60-140120 15 3020ND27.8 23.9
trans-1,3-Dichloropropene ug/L 20 131 60-140114 15 3020ND26.3 22.7
Trichloroethene ug/L 20 133 60-140117 14 3020ND26.7 23.3
Trichlorofluoromethane ug/L 20 140 60-140120 16 3020ND28.0 24.0
Vinyl acetate ug/L 40 130 60-140112 15 3040ND52.0 45.0
Vinyl chloride ug/L M12014760-140126 16 3020ND29.4 25.1
Xylene (Total)ug/L 60 135 60-140117 14 3060ND81.1 70.2
1,2-Dichloroethane-d4 (S)%95 70-13095
4-Bromofluorobenzene (S)%102 70-130102
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811909
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696826001, 92696826003, 92696826005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4203833
Associated Lab Samples:92696826001, 92696826003, 92696826005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/10/23 04:350.091
1,1,1-Trichloroethane ug/L ND 0.50 11/10/23 04:350.11
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/10/23 04:350.074
1,1,2-Trichloroethane ug/L ND 0.50 11/10/23 04:350.096
1,1-Dichloroethane ug/L ND 0.50 11/10/23 04:350.056
1,1-Dichloroethene ug/L ND 0.50 11/10/23 04:350.079
1,1-Dichloropropene ug/L ND 0.50 11/10/23 04:350.066
1,2,3-Trichlorobenzene ug/L ND 2.0 11/10/23 04:350.12
1,2,3-Trichloropropane ug/L ND 0.50 11/10/23 04:350.17
1,2,4-Trichlorobenzene ug/L ND 2.0 11/10/23 04:350.16
1,2,4-Trimethylbenzene ug/L ND 0.50 11/10/23 04:350.031
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/10/23 04:350.15
1,2-Dichlorobenzene ug/L ND 0.50 11/10/23 04:350.094
1,2-Dichloroethane ug/L ND 0.50 11/10/23 04:350.11
1,2-Dichloropropane ug/L ND 0.50 11/10/23 04:350.14
1,3,5-Trimethylbenzene ug/L ND 0.50 11/10/23 04:350.071
1,3-Dichlorobenzene ug/L ND 0.50 11/10/23 04:350.098
1,3-Dichloropropane ug/L ND 0.50 11/10/23 04:350.085
1,4-Dichlorobenzene ug/L ND 0.50 11/10/23 04:350.090
2,2-Dichloropropane ug/L ND 0.50 11/10/23 04:350.12
2-Butanone (MEK)ug/L ND 5.0 11/10/23 04:350.31
2-Chlorotoluene ug/L ND 0.50 11/10/23 04:350.13
2-Hexanone ug/L ND 5.0 11/10/23 04:350.18
4-Chlorotoluene ug/L ND 0.50 11/10/23 04:350.096
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/10/23 04:350.16
Acetone ug/L ND 25.0 11/10/23 04:351.6
Benzene ug/L ND 0.50 11/10/23 04:350.079
Bromobenzene ug/L ND 0.50 11/10/23 04:350.14
Bromochloromethane ug/L ND 0.50 11/10/23 04:350.094
Bromodichloromethane ug/L ND 0.50 11/10/23 04:350.17
Bromoform ug/L ND 0.50 11/10/23 04:350.20
Bromomethane ug/L ND 5.0 11/10/23 04:350.22
Carbon tetrachloride ug/L ND 0.50 11/10/23 04:350.17
Chlorobenzene ug/L ND 0.50 11/10/23 04:350.085
Chloroethane ug/L ND 1.0 11/10/23 04:350.17
Chloroform ug/L ND 0.50 11/10/23 04:350.069
Chloromethane ug/L ND 1.0 11/10/23 04:350.18
cis-1,2-Dichloroethene ug/L ND 0.50 11/10/23 04:350.11
cis-1,3-Dichloropropene ug/L ND 0.50 11/10/23 04:350.090
Dibromochloromethane ug/L ND 0.50 11/10/23 04:350.15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4203833
Associated Lab Samples:92696826001, 92696826003, 92696826005
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 0.50 11/10/23 04:350.12
Diisopropyl ether ug/L ND 0.50 11/10/23 04:350.072
Ethylbenzene ug/L ND 0.50 11/10/23 04:350.081
Isopropylbenzene (Cumene)ug/L ND 0.50 11/10/23 04:350.11
m&p-Xylene ug/L ND 1.0 11/10/23 04:350.094
Methyl-tert-butyl ether ug/L ND 0.50 11/10/23 04:350.053
Methylene Chloride ug/L ND 2.0 11/10/23 04:351.9
n-Butylbenzene ug/L ND 0.50 11/10/23 04:350.066
n-Propylbenzene ug/L ND 0.50 11/10/23 04:350.10
Naphthalene ug/L ND 2.0 11/10/23 04:350.10
o-Xylene ug/L ND 0.50 11/10/23 04:350.14
p-Isopropyltoluene ug/L ND 0.50 11/10/23 04:350.089
sec-Butylbenzene ug/L ND 0.50 11/10/23 04:350.085
Styrene ug/L ND 0.50 11/10/23 04:350.14
tert-Butylbenzene ug/L ND 0.50 11/10/23 04:350.086
Tetrachloroethene ug/L ND 0.50 11/10/23 04:350.086
Toluene ug/L ND 0.50 11/10/23 04:350.090
trans-1,2-Dichloroethene ug/L ND 0.50 11/10/23 04:350.10
trans-1,3-Dichloropropene ug/L ND 0.50 11/10/23 04:350.13
Trichloroethene ug/L ND 0.50 11/10/23 04:350.17
Trichlorofluoromethane ug/L ND 1.0 11/10/23 04:350.14
Vinyl acetate ug/L ND 2.0 11/10/23 04:350.11
Vinyl chloride ug/L ND 1.0 11/10/23 04:350.15
Xylene (Total)ug/L ND 1.0 11/10/23 04:350.094
1,2-Dichloroethane-d4 (S)%90 70-130 11/10/23 04:35
4-Bromofluorobenzene (S)%96 70-130 11/10/23 04:35
Toluene-d8 (S)%106 70-130 11/10/23 04:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4203834LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.520 108 60-140
1,1,1-Trichloroethane ug/L 21.420 107 60-140
1,1,2,2-Tetrachloroethane ug/L 22.320 112 60-140
1,1,2-Trichloroethane ug/L 23.420 117 60-140
1,1-Dichloroethane ug/L 21.920 110 60-140
1,1-Dichloroethene ug/L 20.520 103 60-140
1,1-Dichloropropene ug/L 25.320 127 60-140
1,2,3-Trichlorobenzene ug/L 21.520 107 60-140
1,2,3-Trichloropropane ug/L 20.820 104 60-140
1,2,4-Trichlorobenzene ug/L 21.420 107 60-140
1,2,4-Trimethylbenzene ug/L 22.220 111 60-140
1,2-Dibromoethane (EDB)ug/L 23.420 117 60-140
1,2-Dichlorobenzene ug/L 22.020 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4203834LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 20.720 104 60-140
1,2-Dichloropropane ug/L 24.320 121 60-140
1,3,5-Trimethylbenzene ug/L 21.920 110 60-140
1,3-Dichlorobenzene ug/L 22.320 112 60-140
1,3-Dichloropropane ug/L 22.420 112 60-140
1,4-Dichlorobenzene ug/L 20.720 104 60-140
2,2-Dichloropropane ug/L 20.320 101 60-140
2-Butanone (MEK)ug/L 42.540 106 60-140
2-Chlorotoluene ug/L 21.620 108 60-140
2-Hexanone ug/L 46.940 117 60-140
4-Chlorotoluene ug/L 22.120 110 60-140
4-Methyl-2-pentanone (MIBK)ug/L 44.640 111 60-140
Acetone ug/L 43.940 110 60-140
Benzene ug/L 22.120 110 60-140
Bromobenzene ug/L 21.920 110 60-140
Bromochloromethane ug/L 23.520 117 60-140
Bromodichloromethane ug/L 21.420 107 60-140
Bromoform ug/L 21.220 106 60-140
Bromomethane ug/L 16.520 82 60-140
Carbon tetrachloride ug/L 20.820 104 60-140
Chlorobenzene ug/L 20.820 104 60-140
Chloroethane ug/L 19.320 96 60-140
Chloroform ug/L 20.920 104 60-140
Chloromethane ug/L 24.920 125 60-140
cis-1,2-Dichloroethene ug/L 21.520 108 60-140
cis-1,3-Dichloropropene ug/L 22.920 114 60-140
Dibromochloromethane ug/L 22.520 112 60-140
Dichlorodifluoromethane ug/L 25.120 125 60-140
Diisopropyl ether ug/L 24.220 121 60-140
Ethylbenzene ug/L 20.820 104 60-140
Isopropylbenzene (Cumene)ug/L 21.020 105 60-140
m&p-Xylene ug/L 40.940 102 60-140
Methyl-tert-butyl ether ug/L 19.620 98 60-140
Methylene Chloride ug/L 20.920 105 60-140
n-Butylbenzene ug/L 20.820 104 60-140
n-Propylbenzene ug/L 21.020 105 60-140
Naphthalene ug/L 23.720 119 60-140
o-Xylene ug/L 21.520 108 60-140
p-Isopropyltoluene ug/L 21.820 109 60-140
sec-Butylbenzene ug/L 21.020 105 60-140
Styrene ug/L 22.120 110 60-140
tert-Butylbenzene ug/L 21.620 108 60-140
Tetrachloroethene ug/L 21.220 106 60-140
Toluene ug/L 20.220 101 60-140
trans-1,2-Dichloroethene ug/L 22.120 111 60-140
trans-1,3-Dichloropropene ug/L 22.020 110 60-140
Trichloroethene ug/L 21.520 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4203834LABORATORY CONTROL SAMPLE:
LCSSpike
Trichlorofluoromethane ug/L 18.720 94 60-140
Vinyl acetate ug/L 39.440 99 60-140
Vinyl chloride ug/L 21.920 109 60-140
Xylene (Total)ug/L 62.460 104 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4203835MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697285001
4203836
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 117 60-140121 3 3020ND23.4 24.2
1,1,1-Trichloroethane ug/L 20 118 60-140124 5 3020ND23.5 24.7
1,1,2,2-Tetrachloroethane ug/L 20 118 60-140119 1 3020ND23.7 23.8
1,1,2-Trichloroethane ug/L 20 120 60-140124 3 3020ND24.0 24.8
1,1-Dichloroethane ug/L 20 120 60-140128 6 3020ND23.9 25.5
1,1-Dichloroethene ug/L 20 120 60-140126 5 3020ND24.0 25.1
1,1-Dichloropropene ug/L M12014660-140150 3 3020ND29.1 29.9
1,2,3-Trichlorobenzene ug/L 20 117 60-140120 2 3020ND23.4 24.0
1,2,3-Trichloropropane ug/L 20 111 60-140110 1 3020ND22.2 22.0
1,2,4-Trichlorobenzene ug/L 20 118 60-140121 2 3020ND23.7 24.1
1,2,4-Trimethylbenzene ug/L 20 123 60-140129 5 3020ND24.7 25.8
1,2-Dibromoethane (EDB)ug/L 20 125 60-140126 0 3020ND25.0 25.1
1,2-Dichlorobenzene ug/L 20 119 60-140120 0 3020ND23.9 24.0
1,2-Dichloroethane ug/L 20 108 60-140110 2 3020ND21.6 22.1
1,2-Dichloropropane ug/L 20 135 60-140139 3 3020ND27.0 27.8
1,3,5-Trimethylbenzene ug/L 20 122 60-140125 3 3020ND24.4 25.1
1,3-Dichlorobenzene ug/L 20 122 60-140123 1 3020ND24.3 24.7
1,3-Dichloropropane ug/L 20 120 60-140121 1 3020ND23.9 24.2
1,4-Dichlorobenzene ug/L 20 115 60-140119 3 3020ND23.1 23.7
2,2-Dichloropropane ug/L 20 121 60-140128 5 3020ND24.2 25.5
2-Butanone (MEK)ug/L 40 112 60-140111 1 3040ND45.0 44.6
2-Chlorotoluene ug/L 20 123 60-140124 1 3020ND24.5 24.8
2-Hexanone ug/L 40 128 60-140125 2 3040ND51.1 50.0
4-Chlorotoluene ug/L 20 123 60-140125 2 3020ND24.5 24.9
4-Methyl-2-pentanone
(MIBK)
ug/L 40 119 60-140119 0 3040ND47.5 47.4
Acetone ug/L 40 110 60-140112 2 3040ND44.0 44.8
Benzene ug/L 20 124 60-140129 3 3020ND24.9 25.7
Bromobenzene ug/L 20 118 60-140123 4 3020ND23.6 24.5
Bromochloromethane ug/L 20 128 60-140132 4 3020ND25.5 26.4
Bromodichloromethane ug/L 20 114 60-140119 4 3020ND22.8 23.7
Bromoform ug/L 20 112 60-140114 1 3020ND22.5 22.8
Bromomethane ug/L 20 72 60-14085 17 3020ND14.4 17.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696826
GPM 6035
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4203835MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697285001
4203836
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 20 124 60-140126 2 3020ND24.7 25.2
Chlorobenzene ug/L 20 116 60-140119 3 3020ND23.1 23.7
Chloroethane ug/L 20 108 60-140116 7 3020ND21.6 23.3
Chloroform ug/L 20 113 60-140119 5 3020ND22.6 23.8
Chloromethane ug/L M12013860-140147 7 3020ND27.5 29.4
cis-1,2-Dichloroethene ug/L 20 119 60-140123 4 3020ND23.7 24.7
cis-1,3-Dichloropropene ug/L 20 124 60-140125 1 3020ND24.8 25.1
Dibromochloromethane ug/L 20 121 60-140119 1 3020ND24.1 23.8
Dichlorodifluoromethane ug/L M12017860-140188 6 3020ND35.5 37.7
Diisopropyl ether ug/L 20 125 60-140125 0 3020ND25.0 25.0
Ethylbenzene ug/L 20 115 60-140121 5 3020ND22.9 24.1
Isopropylbenzene
(Cumene)ug/L 20 119 60-140123 3 3020ND23.8 24.5
m&p-Xylene ug/L 40 116 60-140120 3 3040ND46.6 48.0
Methyl-tert-butyl ether ug/L 20 101 60-14099 2 3020ND20.3 19.9
Methylene Chloride ug/L 20 109 60-140117 6 3020ND21.9 23.3
n-Butylbenzene ug/L 20 123 60-140127 3 3020ND24.7 25.4
n-Propylbenzene ug/L 20 120 60-140123 2 3020ND24.0 24.6
Naphthalene ug/L 20 127 60-140125 1 3020ND25.3 25.1
o-Xylene ug/L 20 118 60-140122 3 3020ND23.5 24.4
p-Isopropyltoluene ug/L 20 125 60-140129 3 3020ND25.0 25.7
sec-Butylbenzene ug/L 20 122 60-140126 3 3020ND24.5 25.2
Styrene ug/L 20 121 60-140124 3 3020ND24.2 24.9
tert-Butylbenzene ug/L 20 104 60-140108 4 3020ND20.7 21.6
Tetrachloroethene ug/L 20 117 60-140121 4 3020ND23.3 24.2
Toluene ug/L 20 114 60-140119 4 3020ND22.8 23.9
trans-1,2-Dichloroethene ug/L 20 123 60-140132 7 3020ND24.6 26.3
trans-1,3-Dichloropropene ug/L 20 118 60-140119 1 3020ND23.5 23.8
Trichloroethene ug/L 20 122 60-140125 3 3020ND24.3 25.1
Trichlorofluoromethane ug/L 20 119 60-140126 6 3020ND23.8 25.2
Vinyl acetate ug/L 40 103 60-140100 2 3040ND41.1 40.2
Vinyl chloride ug/L 20 130 60-140138 5 3020ND26.1 27.5
Xylene (Total)ug/L 60 117 60-140121 3 3060ND70.1 72.3
1,2-Dichloroethane-d4 (S)%90 70-13086
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92696826
GPM 6035
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Result confirmed by second analysis.C0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92696826
GPM 6035
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92696826001 811909MW-1RA SM 6200B
92696826002 811311MW-2 SM 6200B
92696826003 811909MW-3 SM 6200B
92696826004 811311MW-4 SM 6200B
92696826005 811909MW-5 SM 6200B
92696826006 811308TRIP BLANK SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/13/2023 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 35
Page 34 of 35
Page 35 of 35
GROUNDWATER MONITORING REPORT ROADRUNNER #135 BLACK MOUNTAIN, NORTH CAROLINA INCIDENT #28783

ROADRUNNER #135: GROUNDWATER MONITORING REPORT

APPENDIX C
TREND GRAPH

9/22/2015, 90.54
88.00
89.00
90.00
91.00
92.00
93.00
94.00
0
2,000
4,000
6,000
8,000
10,000
12,000
14,000
16,000
18,000
20,000
Gr
o
u
n
d
w
a
t
e
r

E
l
e
v
a
t
i
o
n

(
f
e
e
t
)
Be
n
z
e
n
e

C
o
n
c
e
n
t
r
a
t
i
o
n

(
u
g
/
L
)
Date
MW-1/MW-1R/MW-1RA
Benzene Concentration & Groundwater Elevation vs Time
Benzene Concentration (ug/L)Groundwater Elevation Average Groundwater Elevation