AS-3586_28724_M_ESA_20211216_Phase II

GEOTECHNICAL • CONSTRUCTION MATERIALS • ENVIRONMENTAL

PHASE II
ENVIRONMENTAL SITE ASSESSMENT

Caldwell County PIN 2774855555
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina

December 16, 2021
CVET Project No. 21-418

PREPARED FOR:

Piedmont Companies, Inc.
2671 East Main Street
Lincolnton, NC 28092

PREPARED BY:

CATAWBA VALLEY ENGINEERING AND TESTING, P.C.
HICKORY, NORTH CAROLINA

PO Box 747
Hickory, NC 28603

161 Lenoir Rhyne Blvd
Hickory, NC 28602

828 578 9972 O
828 322 1801 F

NC Firm No. C-3833
SC Firm No. 5201
Geotechnical Engineering
Environmental Services
CMT/Special Inspections
December 16, 2021

Mr. Guy Long
Piedmont Companies, Inc.
2671 East Main Street
Lincolnton, NC 28092

Re: Phase II Environmental Site Assessment
Caldwell County PIN 2774855555
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
Project Number: 21-418

Dear Piedmont Companies, Inc. (PCI),

Catawba Valley Engineering & Testing (CVET) is pleased to submit this Phase II
Environmental Site Assessment (ESA) Report for the above referenced property,
as authorized by PCI on November 4, 2021.

CVET appreciates the opportunity to provide our environmental engineering
services for this project. If you have any questions regarding the contents of this
report, or if we can provide additional services, please do not hesitate to contact
us.

Sincerely,

CATAWBA VALLEY ENGINEERING AND TESTING, P.C.

Nathan S. Simmons, P.G. David M. LeGrand, Jr., P.E.
Environmental Professional Owner/Principal Engineer
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

TABLE OF CONTENTS
1.0 BACKGROUND .......................................................................................................................... 1
2.0 SCOPE OF WORK ...................................................................................................................... 1
2.1 Ground Penetrating Radar (GPR) Survey ........................................................................ 1
2.2 Test Pit Exploration – Former Soil Treatment Cell .......................................................... 2
2.3 Groundwater Assessment ............................................................................................... 3
3.0 LABORATORY ANALYTICAL RESULTS ........................................................................................ 4
3.1 Soil Sampling .................................................................................................................. 4
3.2 Groundwater Sampling .................................................................................................. 4
4.0 DISCUSSION .............................................................................................................................. 4
5.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................................. 5
APPENDIX A – FIGURES
APPENDIX B – TABLES
APPENDIX C – LABORATORY ANALYTICAL REPORTS

Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

1

1.0 BACKGROUND

Based on information provided by PCI and information obtained from the Caldwell County GIS
Website, the property consists of one parcel of land totaling approximately 10.53 acres in size
(Appendix A – Figure 1).

On October 15, 2021, CVET submitted a Phase I ESA for the subject site. The report identified
the following recognized environmental condition (REC) and historical recognized environmental
condition (HREC):

 The subject site was formerly utilized as a textile manufacturing plant, dating back to at
least 1947. The potential for unknown or unreported USTs, buried waste, or other
potential environmental concerns cannot be ruled out.

 Contaminated soil and groundwater were identified in 2009, as the result of a leaking
20,000-gallon heating oil UST at the site. The incident was closed out by the NCDEQ in
2012, however, it is unclear if soil or groundwater were restored to levels below the
applicable screening standard. It is possible that impacted soil and groundwater may
remain at the subject property.

Based on the findings of the Phase I ESA Report, PCI contracted CVET to perform a Phase II ESA
at the subject property to address the items identified above.

2.0 SCOPE OF WORK

As part of this Phase II ESA, CVET performed the following scope of work:

2.1 Ground Penetrating Radar (GPR) Survey

On October 27 - 28, 2021, Ground Penetrating Radar Systems, LLC (GPRS) performed a GPR
survey across the subject site. The survey was performed to locate on-site utilities and also to
screen for potential USTs, buried waste, and other potential environmental concerns at the
subject site. All accessible areas were surveyed. Areas not surveyed include an area inhabited
by a homeless individual, steep topographic grades, and wooded/densely vegetated regions.

No obvious evidence of USTs or other potential environmental concerns were identified. On-site
utilities were located and are depicted in Appendix A – Figure 2. Some utilities or subsurface
features may be buried a depth beyond the range of the GPR equipment or in an area inaccessible
by GPR equipment.

Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

2

2.2 Test Pit Exploration – Former Soil Treatment Cell

On November 9, 2021, CVET mobilized to the site to complete exploratory test pits in the vicinity
of a former 20,000-gallon heating oil UST and in-situ soil treatment cell. The goal of the test pits
was to locate the former excavation and soil treatment area and determine if residual impact is
present. CVET completed a total of six test pits (TP-1, TP-2, TP-3, TP-4, TP-5, and TP-6), as
depicted in Appendix A – Figure 3. Evidence of the former UST excavation and soil treatment
cell was identified immediately in TP-1, as evidenced by the presence of straw and perforated
piping, which are known to have been a part of the soil treatment cell design. Moderate
hydrocarbon odors, resembling that of heating oil, and black soil staining were encountered in
TP-2. Additional test pits were completed in order to delineate the horizontal extent of the soil
treatment cell. A maximum depth of approximately 10-feet below ground surface (fbgs) was
attained with on-site excavation equipment. Test pit observations are described in the following
table:

Test
Pit ID
Approximate
Depth (fbgs)
Maximum
PID Reading
(ppm)
Field Observations
TP-1
0.0 – 4.0 0.5 Brown fill. No odors or staining.
4.0 – 8.5 0.0
Black and brown fill with straw, perforated piping,
and coal fragments. Light hydrocarbon odors
observed, no staining.
TP-2
0.0 – 5.0 5.0 Fill and building debris.
5.0 – 10.0 156.0
Dark brown fill, building debris, household trash,
straw, and perforated piping. Moderate hydrocarbon
odor and black staining.
TP-3 0.0 – 8.0 0.0 Red and brown fill. No odors or staining.
TP-4 0.0 – 5.0 0.0
Brown fill with partially weathered rock at base of
excavation and subsequent refusal depth. No odors
or staining.
TP-5 0.0 – 7.0 0.0
Dark brown to black fill, building debris, household
trash, coal fragments, and metal slag material. No
odors or staining.
TP-6 0.0 – 8.0 0.0 Red to brown fill, building debris, and perforated
piping. No odors or staining.

Soil from each test pit was screened for visual and olfactory evidence of impact and was also
screened utilizing a calibrated photo-ionizing detector (PID). Following completion of the test
pits, CVET returned to the pits and corresponding depth intervals appearing most likely to have
been impacted for the collection of four laboratory analytical samples (1-6’, 2-7’, 4-6’, and 5-6’),
as depicted in Appendix A - Figure 3. Samples were placed in laboratory supplied bottles and
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

3

were immediately placed on ice. Samples were submitted to Pace Analytical Laboratories of
Huntersville, North Carolina to be analyzed for a combination of volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), extractable petroleum hydrocarbons (EPH),
and volatile petroleum hydrocarbons (VPH).

Upon completion of the test pit exploration, each pit area was backfilled with the excavated soil,
compacted with the excavation equipment, and restored to its approximate original condition.

2.3 Groundwater Assessment

On December 9 - 10, 2021, CVET mobilized to the site for the installation of six temporary
groundwater monitoring wells, 1, 2, 3, 4, 5, and 6 (Appendix A – Figure 4). At each well location,
direct push technology was used to continuously screen the soil for potential evidence of impact,
to characterize general lithology, and to identify zones of preferential groundwater flow.
Monitoring well 1 was installed in the former UST excavation area/soil treatment cell and also
immediately adjacent to test pit TP-2, in which strong evidence of hydrocarbon impact was
previously observed. Monitoring wells 2, 3, 4, and 5 were completed in the vicinity of former
textile manufacturing building and former infrastructure. Additionally, monitoring well 6 was
installed to the south and down-gradient of most former textile manufacturing processes

Each boring was advanced until groundwater was encountered, following which, the boring was
extended beneath the water table. Well location 1 was installed with a screened interval that
spanned the water table to assess for petroleum impact. Petroleum compounds, such as those
that are suspected to be present in this area of the site, are considered light non-aqueous phase
liquids (LNAPLs), which are less dense than water. Transport and migration of these types of
compounds typically occurs along or near the water table surface. Well locations 2, 3, 4, 5, and
6 were installed to depth below the water table in which refusal or a relatively impermeable
geological unit was encountered. This depth represents the interface at which dense non-
aqueous phase liquids (DNAPLs) such as chlorinated solvents that may have been utilized in
former textile manufacturing processes are expected to be present. Of note, shallow rock and
subsequent drill rig refusal was encountered at well locations 2 and 3. A one-inch temporary PVC
monitoring well with 10 feet of slotted one-inch screen was installed in each open borehole.

Following installation, wells were allowed to equilibrate for approximately two hours, static
water levels were recorded, and wells were developed by purging at least three well volumes.
Groundwater was encountered at approximately 20-fbgs in well 1, at approximately 12-fbgs in
well 2, at approximately 22-fbgs in well 4, and at approximately 6-fbgs in well 6. Wells 3 and 5
were observed to be dry. Well development was performed to remove any fine grained sediment
that may have entered the well during installation, to promote hydraulic communication with
the surrounding materials, and to ensure that water is representative of the surrounding aquifer.
Following well development and removal of approximately three well volumes, as allowed by
well volume and recharge characteristics, groundwater sample were collected from wells 1, 2, 4,
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

4

and 6. Wells 3 and 5 were observed to be dry and no sample could be collected. A peristaltic
pump and new tubing was used to sample each well. The samples were immediately placed on
ice and were submitted to Pace Analytical Laboratories of Huntersville, North Carolina to be
analyzed for VOCs by EPA Method 8260 and SVOCs by EPA Method 8270. Wells 2 and 4 did not
provided sufficient sample volume to analyze for SVOCs.

One soil sample (S-1) was also collected during installation of well 1 (Appendix A – Figure 3), from
a depth of approximately 15-fbgs. No evidence of soil impact was observed during installation
of wells 2, 3, 4, 5, or 6, therefore no additional soil samples were collected for laboratory analysis.
Soil sample S-1 was placed on ice and submitted to Pace Analytical Laboratories of Huntersville,
North Carolina to be analyzed for VOCs and SVOCs. Following collection of soil and groundwater
samples, each well was abandoned in accordance with state and local regulations.

3.0 LABORATORY ANALYTICAL RESULTS

3.1 Soil Sampling

Based on laboratory analytical results for soil samples, benzene was detected at a concentration
above the NCDEQ Soil-to-Water (SW) Maximum Soil Contaminant Concentration (MSCC) in
samples 1-6’ and 2-7’, p-isopropyltoluene was detected at a concentration above the SW MSCC
in sample 2-7’, naphthalene was detected at a concentration above the SW MSCC is samples 1-
6’, 2-7’, and S-1, 1-methylnaphthalene was detected at a concentration above the SW MSCC in
sample S-1, and aromatics (C9-C22) were detected at a concentration above the SW MSCC in
sample 2-7’. No constituents were detected at a concentration above the Residential or
Commercial/Industrial MSCC. Laboratory results are summarized in Appendix A – Figure 3,
Appendix B – Table 1, and Appendix C.

3.2 Groundwater Sampling

Based on laboratory analytical results for groundwater samples, naphthalene and 1-
methylnaphthalene were detected at concentrations above the NCDEQ 2L groundwater standard
in sample 1. No 2L exceedances were identified in samples 2, 4, and 6. Laboratory results are
summarized in Appendix A – Figure 4, Appendix B – Table 2, and Appendix C.

4.0 DISCUSSION

Based on laboratory analytical results, it appears that petroleum impacted soil remains in the
vicinity of the former 20,000-gallon heating oil UST and associated soil treatment cell. It appears
that previous in-situ remediation of heating oil impacted soils has not adequately reduced soil
concentrations. Soil concentrations remain above the SW MSCC, but below the residential and
commercial/industrial MSCCs. Based on laboratory data and field observations, CVET estimates
that the horizontal extent of soil impact is approximately 800 square feet in size and extends to
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

5

a depth of approximately 25 feet in the center of the former UST basin. Of note, impacted soil
appeared to extend up to and beneath the water table, therefore, complete excavation and
removal of impacted soils may be difficult.

Based on groundwater assessment activities, it appears that petroleum impacted groundwater
remains in the vicinity of the former 20,000-gallon heating oil UST and associated soil treatment
cell. Concentrations are relatively low, although still in exceedance of the applicable NCDEQ 2L
groundwater standard.

5.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the results of this assessment, petroleum impacted soil remains in the vicinity of the
former 20,000-gallon heating oil UST and associated soil treatment cell. Impact was not
identified in any other areas of the site. Based on these findings, CVET recommends the
following:

 Submit the findings of this assessment to the NCDEQ immediately, via filing of a “UST-61
24-Hour Release and UST Leak Reporting Form.”

 Completion of a Phase I Limited Site Assessment (LSA) at the subject property, in order to
pursue closure of this incident. Of note, given that impacted soil and groundwater remain
at the subject site, closure of the incident would likely include site use restrictions and
filing of a Notice of Residual Petroleum (NORP) on the property deed. Based on soil and
groundwater concentrations identified in this Phase II ESA, site use limitations may
include a restriction on the use of groundwater at the site. Current soil concentrations
do not appear to trigger any site use restrictions at this time. However, subsequent LSA
findings will ultimately dictate closure and potential site use restrictions.

To the extent feasible, CVET has assessed for the presence of impacted soil and groundwater at
the subject site. Assessment was performed as allowed by site conditions/equipment limitations
and is not a guarantee of subsurface conditions. Bedrock and deeper aquifer conditions were
not evaluated. No other areas or aspects of the site were investigated.

Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

2

APPENDIX A – FIGURES

NSS 21-418
December 16, 2021 Figure 1
P.O.B. 747 NORTH CAROLINAHICKORY
TELE: 828-578-9972 FAX: [phone]
CATAWBA VALLEY
ENGINEERING & TESTING
Site Location Map
Powerhouse Road and Caldwell Street
Rhodhiss, North Carolina
Former 20,000-gallon UST
and Soil Treatment Cell
Drainage
Feature
NSS 21-418
December 16, 2021 Figure 2
P.O.B. 747 NORTH CAROLINAHICKORY
TELE: 828-578-9972 FAX: [phone]
CATAWBA VALLEY
ENGINEERING & TESTING
Utility Location Map
Powerhouse Road and Caldwell Street
Rhodhiss, North Carolina
NSS 21-418
December 16, 2021 Figure 3
P.O.B. 747 NORTH CAROLINAHICKORY
TELE: 828-578-9972 FAX: [phone]
CATAWBA VALLEY
ENGINEERING & TESTING
Soil Sample Location Map
Powerhouse Road and Caldwell Street
Rhodhiss, North Carolina
TP-6
TP-4
TP-5
TP-3
NSS 21-418
December 16, 2021 Figure 4
P.O.B. 747 NORTH CAROLINAHICKORY
TELE: 828-578-9972 FAX: [phone]
CATAWBA VALLEY
ENGINEERING & TESTING
Groundwater Sample Location Map
Powerhouse Road and Caldwell Street
Rhodhiss, North Carolina
Former 20,000-gallon
UST and Soil
Treatment Cell
Drainage
Feature
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

2

APPENDIX B – TABLES

Table 1 - Soil Analytical Results for Detected Constituents
Phase II ESA
Powerhouse Road
Rhodhiss, North Carolina
Area
Sample ID 1-6'2-7'4-6'5-6'S-1
Date 11/9/21 11/9/21 11/9/21 11/9/21 12/10/21
Detected Constituent CAS No.Soil-to-Water
MSCC (mg/kg)
Residential
MSCC (mg/kg)
Commercial-
Industrial MSCC
(mg/kg)
benzene 71-43-2 0.0072 12.0 59.4 0.0892 0.0121 < 0.00270 0.00640 J 0.00380 J
n-butylbenzene 104-51-8 2.40 782 11,600 0.0244 < 0.00290 < 0.00320 < 0.00570 < 0.00290
ethylbenzene 100-41-4 8.00 60.3 297 0.0823 0.0188 0.0071 0.0100 J 0.0159
sec-butylbenzene 135-98-8 2.20 1,560 23,300 < 0.00340 0.113 < 0.00300 < 000530 0.749
isopropylbenzene 98-82-8 1.30 1,560 23,300 0.0378 0.0093 < 0.00230 < 0.00410 0.0580
p-isopropyltoluene 99-87-6 0.12 1,560 23,300 0.0293 0.229 < 0.00330 < 0.00600 < 0.00300
napthalene 91-20-3 0.200 5.50 27.0 0.276 0.301 0.0405 0.0348 0.561
n-propylbenzene 103-65-1 1.400 1,560.00 23,300.0 0.0501 0.0265 < 0.00240 < 0.00430 < 0.00220
toluene 108-88-3 5.40 1,250 18,600 0.508 0.0567 0.0274 0.0599 0.0278
trichloroethene 79-01-6 0.017 7.82 71 0.00440 J < 0.00160 < 0.00180 < 0.00310 < 0.00160
1,2,4-trimethylbenzene 95-63-6 6.60 156 2,330 0.147 0.162 0.0229 0.0187 0.546
1,3,5-trimethylbenzene 108-67-8 6.60 156 2,330 < 0.00260 0.0763 0.00790 < 0.00410 0.372
Total xylenes 1330-20-7 6.00 3,120 46,700 0.723 0.132 0.0725 0.0846 0.104
1-Methylnaphthalene 90-12-0 0.054 22.8 112 < 0.132 < 0.697 < 1.26 < 0.684 0.282 J
2-Methylnaphthalene 91-57-6 1.50 62.5 934 < 0.150 < 0.793 < 1.44 < 0.778 0.357 J
aliphatics (C5 - C8)--68.0 625 9,340 --< 3.10 ------
aliphatics (C9 - C18)--540 1,560 23,300 --130.7 ------
aliphatics (C19 - C36)----31,200 467,000 --46.5 ------
aromatics (C9 - C22)--31.0 469 7,000 --84.2 ------
Notes:
Bolded and highlighted cells exceed the Commercial-Industrial MSCC
-- No standard available/Not analyzed
Bolded and highlighted cells exceed the Soil-to-Water MSCC
Bolded and highlighted cells exceed the Residential MSCC
mg/kg - milligrams per kilogram.
MSCC - Maximum Soil Contaminant Conncentration Levels as established by the NCDEQ
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.SVOCsVOC'sFormer Heating Oil Treatment Cell
Units in mg/kg
MADEP VPH and EPH
Table 2 - Groundwater Analytical Results for Detected Constituents
Phase II Environmental Site Assessment
Powerhouse Road
Rhodhiss, North Carolina
Sample ID 1 2 4 6
Area Former UST Basin/Soil
Treatment Cell
Down-Gradient of Former
Textile Processes
Date 12/10/2021 12/10/2021 12/10/2021 12/10/2021
Detected Constituent CAS No.NCDEQ 15A NCAC 2L
Groundwater Standard (ug/L)
NCDEQ Gross Contamination
Levels (ug/L)
Acetone 67-64-1 6,000 6,000,000 25.1 29.8 < 5.10 < 5.10
2-Butanone (MEK)78-93-3 4,000 4,000,000 5.10 11.1 < 4.00 < 4.00
Ethylbenzene 100-41-4 600 80,000 0.390 J < 0.300 < 0.300 < 0.300
Naphthalene 91-20-3 6 6,000 20.3 < 0.640 < 0.640 < 0.640
Toluene 108-88-3 600 260,000 0.500 J < 0.480 < 0.480 < 0.480
Total Xylenes 1330-20-7 500 50,000 2.50 J < 0.340 < 0.640 < 0.340
Fluorene 86-73-7 300 845 2.50 J ----< 1.70
1-Methylnaphthalene 90-12-0 1 1,000 19.1 ----< 1.70
2-Methylnaphthalene 91-57-6 30 12,000 22.2 ----< 1.60
Naphthalene 91-20-3 6 6,000 9.60 ----< 1.70
Phenanthrene 85-01-8 200 550 2.30 J ----< 1.70
Notes:
ug/L - micrograms per liter
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
Units in ug/L
Textile Manufacturing Building
SVOCsVOCs Bolded and highlighted cells exceed the NCDEQ gross contamination levels (GCLs)
Bolded and highlighted cells exceed the 15A NCAC 2L groundwater standard
VOC's - Volatile Organic Compounds
-- not analyzed due to insufficient groundwater volume and recharge
SVOC's - Semi Volatile Organic Compounds
NCDEQ - North Carolina Department of Environmental Quality
Powerhouse Road and Caldwell Street
Rhodhiss, Caldwell County, North Carolina
December 16, 2021
CVET Project No. 21-418

2

APPENDIX C – LABORATORY ANALYTICAL REPORTS

#=CL#
November 30, 2021
LIMS USE: FR - NATHAN SIMMONS
LIMS OBJECT ID: 92572495
92572495
Project:
Pace Project No.:
RE:
Nathan Simmons
Catawba Valley Engineering & Testing
161 Lenoir Rhyne Blvd SE
Hickory, NC 28603
21-418
Dear Nathan Simmons:
Enclosed are the analytical results for sample(s) received by the laboratory on November 15, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ryan Brumfield
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92572495
21-418
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92572495
21-418
Lab ID Sample ID Matrix Date Collected Date Received
92572495001 1-6'Solid 11/09/21 13:50 11/15/21 14:35
92572495002 4-6'Solid 11/09/21 14:30 11/15/21 14:35
92572495003 5-6'Solid 11/09/21 15:00 11/15/21 14:35
92572495004 2-7'Solid 11/09/21 14:00 11/15/21 14:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92572495
21-418
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92572495001 1-6'EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92572495002 4-6'EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92572495003 5-6'EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92572495004 2-7'MADEP EPH 8 PANJN
MADEP VPH 5 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:1-6'Lab ID:92572495001 Collected:11/09/21 13:50 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/16/21 17:01 83-32-911/16/21 11:203751321
Acenaphthylene ND ug/kg 11/16/21 17:01 208-96-811/16/21 11:203751321
Aniline ND ug/kg 11/16/21 17:01 62-53-311/16/21 11:203751471
Anthracene ND ug/kg 11/16/21 17:01 120-12-711/16/21 11:203751231
Benzo(a)anthracene ND ug/kg 11/16/21 17:01 56-55-311/16/21 11:203751251
Benzo(a)pyrene ND ug/kg 11/16/21 17:01 50-32-811/16/21 11:203751301
Benzo(b)fluoranthene ND ug/kg 11/16/21 17:01 205-99-211/16/21 11:203751251
Benzo(g,h,i)perylene ND ug/kg 11/16/21 17:01 191-24-211/16/21 11:203751461
Benzo(k)fluoranthene ND ug/kg 11/16/21 17:01 207-08-911/16/21 11:203751321
Benzoic Acid ND ug/kg 11/16/21 17:01 65-85-011/16/21 11:2018808061
Benzyl alcohol ND ug/kg 11/16/21 17:01 100-51-611/16/21 11:207512841
4-Bromophenylphenyl ether ND ug/kg 11/16/21 17:01 101-55-311/16/21 11:203751441
Butylbenzylphthalate ND ug/kg 11/16/21 17:01 85-68-711/16/21 11:203751581
4-Chloro-3-methylphenol ND ug/kg 11/16/21 17:01 59-50-711/16/21 11:207512641
4-Chloroaniline ND ug/kg 11/16/21 17:01 106-47-811/16/21 11:207512951
bis(2-Chloroethoxy)methane ND ug/kg 11/16/21 17:01 111-91-111/16/21 11:203751561
bis(2-Chloroethyl) ether ND ug/kg 11/16/21 17:01 111-44-411/16/21 11:203751411
2-Chloronaphthalene ND ug/kg 11/16/21 17:01 91-58-711/16/21 11:203751491
2-Chlorophenol ND ug/kg 11/16/21 17:01 95-57-811/16/21 11:203751411
4-Chlorophenylphenyl ether ND ug/kg 11/16/21 17:01 7005-72-311/16/21 11:203751401
Chrysene ND ug/kg 11/16/21 17:01 218-01-911/16/21 11:203751361
Dibenz(a,h)anthracene ND ug/kg 11/16/21 17:01 53-70-311/16/21 11:203751441
Dibenzofuran ND ug/kg 11/16/21 17:01 132-64-911/16/21 11:203751351
1,2-Dichlorobenzene ND ug/kg 11/16/21 17:01 95-50-111/16/21 11:203751351
1,3-Dichlorobenzene ND ug/kg 11/16/21 17:01 541-73-111/16/21 11:203751331
1,4-Dichlorobenzene ND ug/kg 11/16/21 17:01 106-46-711/16/21 11:203751431
3,3'-Dichlorobenzidine ND ug/kg 11/16/21 17:01 91-94-111/16/21 11:207512541
2,4-Dichlorophenol ND ug/kg 11/16/21 17:01 120-83-211/16/21 11:203751471
Diethylphthalate ND ug/kg 11/16/21 17:01 84-66-211/16/21 11:203751381
2,4-Dimethylphenol ND ug/kg 11/16/21 17:01 105-67-911/16/21 11:203751561
Dimethylphthalate ND ug/kg 11/16/21 17:01 131-11-311/16/21 11:203751361
Di-n-butylphthalate ND ug/kg 11/16/21 17:01 84-74-211/16/21 11:203751261
4,6-Dinitro-2-methylphenol ND ug/kg 11/16/21 17:01 534-52-111/16/21 11:207513501
2,4-Dinitrophenol ND ug/kg 11/16/21 17:01 51-28-511/16/21 11:20188011601
2,4-Dinitrotoluene ND ug/kg 11/16/21 17:01 121-14-211/16/21 11:203751441
2,6-Dinitrotoluene ND ug/kg 11/16/21 17:01 606-20-211/16/21 11:203751381
Di-n-octylphthalate ND ug/kg 11/16/21 17:01 117-84-011/16/21 11:203751481
bis(2-Ethylhexyl)phthalate ND ug/kg 11/16/21 17:01 117-81-711/16/21 11:203751461
Fluoranthene ND ug/kg 11/16/21 17:01 206-44-011/16/21 11:203751291
Fluorene ND ug/kg 11/16/21 17:01 86-73-711/16/21 11:203751321
Hexachloro-1,3-butadiene ND ug/kg 11/16/21 17:01 87-68-311/16/21 11:203751631
Hexachlorobenzene ND ug/kg 11/16/21 17:01 118-74-111/16/21 11:203751471
Hexachlorocyclopentadiene ND ug/kg 11/16/21 17:01 77-47-411/16/21 11:203752151
Hexachloroethane ND ug/kg 11/16/21 17:01 67-72-111/16/21 11:203751431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:1-6'Lab ID:92572495001 Collected:11/09/21 13:50 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 11/16/21 17:01 193-39-511/16/21 11:203751481
Isophorone ND ug/kg 11/16/21 17:01 78-59-111/16/21 11:203751671
1-Methylnaphthalene ND ug/kg 11/16/21 17:01 90-12-011/16/21 11:203751321
2-Methylnaphthalene ND ug/kg 11/16/21 17:01 91-57-611/16/21 11:203751501
2-Methylphenol(o-Cresol)ND ug/kg 11/16/21 17:01 95-48-711/16/21 11:203751541
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/16/21 17:01 15831-10-411/16/21 11:203751511
Naphthalene ND ug/kg 11/16/21 17:01 91-20-311/16/21 11:203751271
2-Nitroaniline ND ug/kg 11/16/21 17:01 88-74-411/16/21 11:2018803071
3-Nitroaniline ND ug/kg 11/16/21 17:01 99-09-211/16/21 11:2018802951
4-Nitroaniline ND ug/kg 11/16/21 17:01 100-01-611/16/21 11:207512851
Nitrobenzene ND ug/kg 11/16/21 17:01 98-95-311/16/21 11:203751741
2-Nitrophenol ND ug/kg 11/16/21 17:01 88-75-511/16/21 11:203751631
4-Nitrophenol ND ug/kg 11/16/21 17:01 100-02-711/16/21 11:2018807261
N-Nitrosodimethylamine ND ug/kg 11/16/21 17:01 62-75-911/16/21 11:203751261
N-Nitroso-di-n-propylamine ND ug/kg 11/16/21 17:01 621-64-711/16/21 11:203751411
N-Nitrosodiphenylamine ND ug/kg 11/16/21 17:01 86-30-611/16/21 11:203751331
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/16/21 17:01 108-60-111/16/21 11:203751791
Pentachlorophenol ND ug/kg 11/16/21 17:01 87-86-511/16/21 11:207513671
Phenanthrene ND ug/kg 11/16/21 17:01 85-01-811/16/21 11:203751231
Phenol ND ug/kg 11/16/21 17:01 108-95-211/16/21 11:203751671
Pyrene ND ug/kg 11/16/21 17:01 129-00-011/16/21 11:203751521
Pyridine ND ug/kg 11/16/21 17:01 110-86-111/16/21 11:203751181
1,2,4-Trichlorobenzene ND ug/kg 11/16/21 17:01 120-82-111/16/21 11:203751481
2,4,5-Trichlorophenol ND ug/kg 11/16/21 17:01 95-95-411/16/21 11:203751721
2,4,6-Trichlorophenol ND ug/kg 11/16/21 17:01 88-06-211/16/21 11:203751551
Surrogates
Nitrobenzene-d5 (S)67 %11/16/21 17:01 4165-60-011/16/21 11:2021-130 1
2-Fluorobiphenyl (S)81 %11/16/21 17:01 321-60-811/16/21 11:2019-130 1
Terphenyl-d14 (S)82 %11/16/21 17:01 1718-51-011/16/21 11:2015-130 1
Phenol-d6 (S)65 %11/16/21 17:01 13127-88-311/16/21 11:2018-130 1
2-Fluorophenol (S)60 %11/16/21 17:01 367-12-411/16/21 11:2018-130 1
2,4,6-Tribromophenol (S)88 %11/16/21 17:01 118-79-611/16/21 11:2018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/16/21 22:11 67-64-111/16/21 13:5315449.5 1
Benzene 89.2 ug/kg 11/16/21 22:11 71-43-211/16/21 13:537.7 3.1 1
Bromobenzene ND ug/kg 11/16/21 22:11 108-86-111/16/21 13:537.7 2.5 1
Bromochloromethane ND ug/kg 11/16/21 22:11 74-97-511/16/21 13:537.7 2.3 1
Bromodichloromethane ND ug/kg 11/16/21 22:11 75-27-411/16/21 13:537.7 3.0 1
Bromoform ND ug/kg 11/16/21 22:11 75-25-211/16/21 13:537.7 2.7 1
Bromomethane ND ug/kg 11/16/21 22:11 74-83-9 IK,L1,v111/16/21 13:5315.4 12.2 1
2-Butanone (MEK)ND ug/kg 11/16/21 22:11 78-93-311/16/21 13:5315437.0 1
n-Butylbenzene 24.4 ug/kg 11/16/21 22:11 104-51-811/16/21 13:537.7 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:1-6'Lab ID:92572495001 Collected:11/09/21 13:50 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene ND ug/kg 11/16/21 22:11 135-98-811/16/21 13:537.7 3.4 1
tert-Butylbenzene ND ug/kg 11/16/21 22:11 98-06-611/16/21 13:537.7 2.7 1
Carbon tetrachloride ND ug/kg 11/16/21 22:11 56-23-511/16/21 13:537.7 2.9 1
Chlorobenzene ND ug/kg 11/16/21 22:11 108-90-711/16/21 13:537.7 1.5 1
Chloroethane ND ug/kg 11/16/21 22:11 75-00-311/16/21 13:5315.4 5.9 1
Chloroform ND ug/kg 11/16/21 22:11 67-66-311/16/21 13:537.7 4.7 1
Chloromethane ND ug/kg 11/16/21 22:11 74-87-311/16/21 13:5315.4 6.5 1
2-Chlorotoluene ND ug/kg 11/16/21 22:11 95-49-811/16/21 13:537.7 2.7 1
4-Chlorotoluene ND ug/kg 11/16/21 22:11 106-43-411/16/21 13:537.7 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/16/21 22:11 96-12-811/16/21 13:537.7 3.0 1
Dibromochloromethane ND ug/kg 11/16/21 22:11 124-48-111/16/21 13:537.7 4.3 1
1,2-Dibromoethane (EDB)ND ug/kg 11/16/21 22:11 106-93-411/16/21 13:537.7 3.4 1
Dibromomethane ND ug/kg 11/16/21 22:11 74-95-311/16/21 13:537.7 1.6 1
1,2-Dichlorobenzene ND ug/kg 11/16/21 22:11 95-50-111/16/21 13:537.7 2.8 1
1,3-Dichlorobenzene ND ug/kg 11/16/21 22:11 541-73-111/16/21 13:537.7 2.4 1
1,4-Dichlorobenzene ND ug/kg 11/16/21 22:11 106-46-711/16/21 13:537.7 2.0 1
Dichlorodifluoromethane ND ug/kg 11/16/21 22:11 75-71-811/16/21 13:5315.4 3.3 1
1,1-Dichloroethane ND ug/kg 11/16/21 22:11 75-34-311/16/21 13:537.7 3.2 1
1,2-Dichloroethane ND ug/kg 11/16/21 22:11 107-06-211/16/21 13:537.7 5.1 1
1,1-Dichloroethene ND ug/kg 11/16/21 22:11 75-35-411/16/21 13:537.7 3.2 1
cis-1,2-Dichloroethene ND ug/kg 11/16/21 22:11 156-59-211/16/21 13:537.7 2.6 1
trans-1,2-Dichloroethene ND ug/kg 11/16/21 22:11 156-60-511/16/21 13:537.7 2.7 1
1,2-Dichloropropane ND ug/kg 11/16/21 22:11 78-87-511/16/21 13:537.7 2.3 1
1,3-Dichloropropane ND ug/kg 11/16/21 22:11 142-28-911/16/21 13:537.7 2.4 1
2,2-Dichloropropane ND ug/kg 11/16/21 22:11 594-20-711/16/21 13:537.7 2.5 1
1,1-Dichloropropene ND ug/kg 11/16/21 22:11 563-58-611/16/21 13:537.7 3.7 1
cis-1,3-Dichloropropene ND ug/kg 11/16/21 22:11 10061-01-511/16/21 13:537.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 11/16/21 22:11 10061-02-611/16/21 13:537.7 2.7 1
Diisopropyl ether ND ug/kg 11/16/21 22:11 108-20-311/16/21 13:537.7 2.1 1
Ethylbenzene 82.3 ug/kg 11/16/21 22:11 100-41-411/16/21 13:537.7 3.6 1
Hexachloro-1,3-butadiene ND ug/kg 11/16/21 22:11 87-68-311/16/21 13:5315.4 12.6 1
2-Hexanone ND ug/kg 11/16/21 22:11 591-78-611/16/21 13:5377.1 7.4 1
Isopropylbenzene (Cumene)37.8 ug/kg 11/16/21 22:11 98-82-811/16/21 13:537.7 2.6 1
p-Isopropyltoluene 29.3 ug/kg 11/16/21 22:11 99-87-611/16/21 13:537.7 3.8 1
Methylene Chloride ND ug/kg 11/16/21 22:11 75-09-211/16/21 13:5330.8 21.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/16/21 22:11 108-10-111/16/21 13:5377.1 7.4 1
Methyl-tert-butyl ether ND ug/kg 11/16/21 22:11 1634-04-411/16/21 13:537.7 2.9 1
Naphthalene 276 ug/kg 11/16/21 22:11 91-20-311/16/21 13:537.7 4.1 1
n-Propylbenzene 50.1 ug/kg 11/16/21 22:11 103-65-111/16/21 13:537.7 2.7 1
Styrene ND ug/kg 11/16/21 22:11 100-42-511/16/21 13:537.7 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/16/21 22:11 630-20-611/16/21 13:537.7 3.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/16/21 22:11 79-34-511/16/21 13:537.7 2.0 1
Tetrachloroethene ND ug/kg 11/16/21 22:11 127-18-411/16/21 13:537.7 2.4 1
Toluene 508 ug/kg 11/16/21 22:11 108-88-311/16/21 13:537.7 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:1-6'Lab ID:92572495001 Collected:11/09/21 13:50 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 11/16/21 22:11 87-61-611/16/21 13:537.7 6.2 1
1,2,4-Trichlorobenzene ND ug/kg 11/16/21 22:11 120-82-111/16/21 13:537.7 6.5 1
1,1,1-Trichloroethane ND ug/kg 11/16/21 22:11 71-55-611/16/21 13:537.7 4.0 1
1,1,2-Trichloroethane ND ug/kg 11/16/21 22:11 79-00-511/16/21 13:537.7 2.6 1
Trichloroethene 4.4J ug/kg 11/16/21 22:11 79-01-611/16/21 13:537.7 2.0 1
Trichlorofluoromethane ND ug/kg 11/16/21 22:11 75-69-411/16/21 13:537.7 4.2 1
1,2,3-Trichloropropane ND ug/kg 11/16/21 22:11 96-18-411/16/21 13:537.7 3.9 1
1,2,4-Trimethylbenzene 147 ug/kg 11/16/21 22:11 95-63-611/16/21 13:537.7 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 11/16/21 22:11 108-67-811/16/21 13:537.7 2.6 1
Vinyl acetate ND ug/kg 11/16/21 22:11 108-05-411/16/21 13:5377.1 5.6 1
Vinyl chloride ND ug/kg 11/16/21 22:11 75-01-411/16/21 13:5315.4 3.9 1
Xylene (Total)723 ug/kg 11/16/21 22:11 1330-20-711/16/21 13:5315.4 4.4 1
m&p-Xylene 443 ug/kg 11/16/21 22:11 179601-23-111/16/21 13:5315.4 5.3 1
o-Xylene 280 ug/kg 11/16/21 22:11 95-47-611/16/21 13:537.7 3.4 1
Surrogates
Toluene-d8 (S)100 %11/16/21 22:11 2037-26-511/16/21 13:5370-130 1
4-Bromofluorobenzene (S)100 %11/16/21 22:11 460-00-411/16/21 13:5369-134 1
1,2-Dichloroethane-d4 (S)104 %11/16/21 22:11 17060-07-011/16/21 13:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.4 %11/15/21 17:31 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:4-6'Lab ID:92572495002 Collected:11/09/21 14:30 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/17/21 19:32 83-32-911/16/21 11:203590126010
Acenaphthylene ND ug/kg 11/17/21 19:32 208-96-811/16/21 11:203590126010
Aniline ND ug/kg 11/17/21 19:32 62-53-311/16/21 11:203590140010
Anthracene ND ug/kg 11/17/21 19:32 120-12-711/16/21 11:203590118010
Benzo(a)anthracene ND ug/kg 11/17/21 19:32 56-55-311/16/21 11:203590120010
Benzo(a)pyrene ND ug/kg 11/17/21 19:32 50-32-811/16/21 11:203590124010
Benzo(b)fluoranthene ND ug/kg 11/17/21 19:32 205-99-211/16/21 11:203590120010
Benzo(g,h,i)perylene ND ug/kg 11/17/21 19:32 191-24-211/16/21 11:203590139010
Benzo(k)fluoranthene ND ug/kg 11/17/21 19:32 207-08-911/16/21 11:203590126010
Benzoic Acid ND ug/kg 11/17/21 19:32 65-85-011/16/21 11:2018000772010
Benzyl alcohol ND ug/kg 11/17/21 19:32 100-51-611/16/21 11:207190272010
4-Bromophenylphenyl ether ND ug/kg 11/17/21 19:32 101-55-311/16/21 11:203590138010
Butylbenzylphthalate ND ug/kg 11/17/21 19:32 85-68-711/16/21 11:203590151010
4-Chloro-3-methylphenol ND ug/kg 11/17/21 19:32 59-50-711/16/21 11:207190253010
4-Chloroaniline ND ug/kg 11/17/21 19:32 106-47-811/16/21 11:207190282010
bis(2-Chloroethoxy)methane ND ug/kg 11/17/21 19:32 111-91-111/16/21 11:203590149010
bis(2-Chloroethyl) ether ND ug/kg 11/17/21 19:32 111-44-411/16/21 11:203590135010
2-Chloronaphthalene ND ug/kg 11/17/21 19:32 91-58-711/16/21 11:203590143010
2-Chlorophenol ND ug/kg 11/17/21 19:32 95-57-811/16/21 11:203590135010
4-Chlorophenylphenyl ether ND ug/kg 11/17/21 19:32 7005-72-311/16/21 11:203590134010
Chrysene ND ug/kg 11/17/21 19:32 218-01-911/16/21 11:203590131010
Dibenz(a,h)anthracene ND ug/kg 11/17/21 19:32 53-70-311/16/21 11:203590138010
Dibenzofuran ND ug/kg 11/17/21 19:32 132-64-911/16/21 11:203590130010
1,2-Dichlorobenzene ND ug/kg 11/17/21 19:32 95-50-111/16/21 11:203590130010
1,3-Dichlorobenzene ND ug/kg 11/17/21 19:32 541-73-111/16/21 11:203590127010
1,4-Dichlorobenzene ND ug/kg 11/17/21 19:32 106-46-711/16/21 11:203590137010
3,3'-Dichlorobenzidine ND ug/kg 11/17/21 19:32 91-94-1 IL11/16/21 11:207190243010
2,4-Dichlorophenol ND ug/kg 11/17/21 19:32 120-83-211/16/21 11:203590140010
Diethylphthalate ND ug/kg 11/17/21 19:32 84-66-211/16/21 11:203590132010
2,4-Dimethylphenol ND ug/kg 11/17/21 19:32 105-67-911/16/21 11:203590149010
Dimethylphthalate ND ug/kg 11/17/21 19:32 131-11-311/16/21 11:203590131010
Di-n-butylphthalate ND ug/kg 11/17/21 19:32 84-74-211/16/21 11:203590121010
4,6-Dinitro-2-methylphenol ND ug/kg 11/17/21 19:32 534-52-1 v111/16/21 11:207190335010
2,4-Dinitrophenol ND ug/kg 11/17/21 19:32 51-28-5 v111/16/21 11:20180001110010
2,4-Dinitrotoluene ND ug/kg 11/17/21 19:32 121-14-211/16/21 11:203590138010
2,6-Dinitrotoluene ND ug/kg 11/17/21 19:32 606-20-211/16/21 11:203590132010
Di-n-octylphthalate ND ug/kg 11/17/21 19:32 117-84-011/16/21 11:203590142010
bis(2-Ethylhexyl)phthalate ND ug/kg 11/17/21 19:32 117-81-711/16/21 11:203590139010
Fluoranthene ND ug/kg 11/17/21 19:32 206-44-011/16/21 11:203590123010
Fluorene ND ug/kg 11/17/21 19:32 86-73-711/16/21 11:203590126010
Hexachloro-1,3-butadiene ND ug/kg 11/17/21 19:32 87-68-3 v111/16/21 11:203590156010
Hexachlorobenzene ND ug/kg 11/17/21 19:32 118-74-111/16/21 11:203590140010
Hexachlorocyclopentadiene ND ug/kg 11/17/21 19:32 77-47-411/16/21 11:203590206010
Hexachloroethane ND ug/kg 11/17/21 19:32 67-72-111/16/21 11:203590137010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:4-6'Lab ID:92572495002 Collected:11/09/21 14:30 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 11/17/21 19:32 193-39-511/16/21 11:203590142010
Isophorone ND ug/kg 11/17/21 19:32 78-59-111/16/21 11:203590160010
1-Methylnaphthalene ND ug/kg 11/17/21 19:32 90-12-011/16/21 11:203590126010
2-Methylnaphthalene ND ug/kg 11/17/21 19:32 91-57-611/16/21 11:203590144010
2-Methylphenol(o-Cresol)ND ug/kg 11/17/21 19:32 95-48-711/16/21 11:203590147010
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/17/21 19:32 15831-10-411/16/21 11:203590145010
Naphthalene ND ug/kg 11/17/21 19:32 91-20-311/16/21 11:203590122010
2-Nitroaniline ND ug/kg 11/17/21 19:32 88-74-411/16/21 11:2018000294010
3-Nitroaniline ND ug/kg 11/17/21 19:32 99-09-2 IL11/16/21 11:2018000282010
4-Nitroaniline ND ug/kg 11/17/21 19:32 100-01-611/16/21 11:207190273010
Nitrobenzene ND ug/kg 11/17/21 19:32 98-95-311/16/21 11:203590167010
2-Nitrophenol ND ug/kg 11/17/21 19:32 88-75-511/16/21 11:203590156010
4-Nitrophenol ND ug/kg 11/17/21 19:32 100-02-7 v111/16/21 11:2018000695010
N-Nitrosodimethylamine ND ug/kg 11/17/21 19:32 62-75-911/16/21 11:203590121010
N-Nitroso-di-n-propylamine ND ug/kg 11/17/21 19:32 621-64-711/16/21 11:203590135010
N-Nitrosodiphenylamine ND ug/kg 11/17/21 19:32 86-30-611/16/21 11:203590127010
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/17/21 19:32 108-60-1 v211/16/21 11:203590171010
Pentachlorophenol ND ug/kg 11/17/21 19:32 87-86-511/16/21 11:207190352010
Phenanthrene ND ug/kg 11/17/21 19:32 85-01-811/16/21 11:203590118010
Phenol ND ug/kg 11/17/21 19:32 108-95-2 v111/16/21 11:203590160010
Pyrene ND ug/kg 11/17/21 19:32 129-00-011/16/21 11:203590146010
Pyridine ND ug/kg 11/17/21 19:32 110-86-111/16/21 11:203590113010
1,2,4-Trichlorobenzene ND ug/kg 11/17/21 19:32 120-82-111/16/21 11:203590142010
2,4,5-Trichlorophenol ND ug/kg 11/17/21 19:32 95-95-411/16/21 11:203590164010
2,4,6-Trichlorophenol ND ug/kg 11/17/21 19:32 88-06-211/16/21 11:203590148010
Surrogates
Nitrobenzene-d5 (S)0 %11/17/21 19:32 4165-60-0 D3,S411/16/21 11:2021-130 10
2-Fluorobiphenyl (S)0 %11/17/21 19:32 321-60-8 S411/16/21 11:2019-130 10
Terphenyl-d14 (S)0 %11/17/21 19:32 1718-51-0 S411/16/21 11:2015-130 10
Phenol-d6 (S)0 %11/17/21 19:32 13127-88-3 S411/16/21 11:2018-130 10
2-Fluorophenol (S)0 %11/17/21 19:32 367-12-4 S411/16/21 11:2018-130 10
2,4,6-Tribromophenol (S)0 %11/17/21 19:32 118-79-611/16/21 11:2018-130 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/16/21 19:43 67-64-111/16/21 13:5313643.7 1
Benzene ND ug/kg 11/16/21 19:43 71-43-211/16/21 13:536.8 2.7 1
Bromobenzene ND ug/kg 11/16/21 19:43 108-86-111/16/21 13:536.8 2.2 1
Bromochloromethane ND ug/kg 11/16/21 19:43 74-97-511/16/21 13:536.8 2.0 1
Bromodichloromethane ND ug/kg 11/16/21 19:43 75-27-411/16/21 13:536.8 2.6 1
Bromoform ND ug/kg 11/16/21 19:43 75-25-211/16/21 13:536.8 2.4 1
Bromomethane ND ug/kg 11/16/21 19:43 74-83-9 IK,L1,v111/16/21 13:5313.6 10.8 1
2-Butanone (MEK)ND ug/kg 11/16/21 19:43 78-93-311/16/21 13:5313632.7 1
n-Butylbenzene ND ug/kg 11/16/21 19:43 104-51-811/16/21 13:536.8 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:4-6'Lab ID:92572495002 Collected:11/09/21 14:30 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene ND ug/kg 11/16/21 19:43 135-98-811/16/21 13:536.8 3.0 1
tert-Butylbenzene ND ug/kg 11/16/21 19:43 98-06-611/16/21 13:536.8 2.4 1
Carbon tetrachloride ND ug/kg 11/16/21 19:43 56-23-511/16/21 13:536.8 2.5 1
Chlorobenzene ND ug/kg 11/16/21 19:43 108-90-711/16/21 13:536.8 1.3 1
Chloroethane ND ug/kg 11/16/21 19:43 75-00-311/16/21 13:5313.6 5.3 1
Chloroform ND ug/kg 11/16/21 19:43 67-66-311/16/21 13:536.8 4.1 1
Chloromethane ND ug/kg 11/16/21 19:43 74-87-311/16/21 13:5313.6 5.7 1
2-Chlorotoluene ND ug/kg 11/16/21 19:43 95-49-811/16/21 13:536.8 2.4 1
4-Chlorotoluene ND ug/kg 11/16/21 19:43 106-43-411/16/21 13:536.8 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/16/21 19:43 96-12-811/16/21 13:536.8 2.6 1
Dibromochloromethane ND ug/kg 11/16/21 19:43 124-48-111/16/21 13:536.8 3.8 1
1,2-Dibromoethane (EDB)ND ug/kg 11/16/21 19:43 106-93-411/16/21 13:536.8 3.0 1
Dibromomethane ND ug/kg 11/16/21 19:43 74-95-311/16/21 13:536.8 1.5 1
1,2-Dichlorobenzene ND ug/kg 11/16/21 19:43 95-50-111/16/21 13:536.8 2.4 1
1,3-Dichlorobenzene ND ug/kg 11/16/21 19:43 541-73-111/16/21 13:536.8 2.1 1
1,4-Dichlorobenzene ND ug/kg 11/16/21 19:43 106-46-711/16/21 13:536.8 1.8 1
Dichlorodifluoromethane ND ug/kg 11/16/21 19:43 75-71-811/16/21 13:5313.6 3.0 1
1,1-Dichloroethane ND ug/kg 11/16/21 19:43 75-34-311/16/21 13:536.8 2.8 1
1,2-Dichloroethane ND ug/kg 11/16/21 19:43 107-06-211/16/21 13:536.8 4.5 1
1,1-Dichloroethene ND ug/kg 11/16/21 19:43 75-35-411/16/21 13:536.8 2.8 1
cis-1,2-Dichloroethene ND ug/kg 11/16/21 19:43 156-59-211/16/21 13:536.8 2.3 1
trans-1,2-Dichloroethene ND ug/kg 11/16/21 19:43 156-60-511/16/21 13:536.8 2.4 1
1,2-Dichloropropane ND ug/kg 11/16/21 19:43 78-87-511/16/21 13:536.8 2.0 1
1,3-Dichloropropane ND ug/kg 11/16/21 19:43 142-28-911/16/21 13:536.8 2.1 1
2,2-Dichloropropane ND ug/kg 11/16/21 19:43 594-20-711/16/21 13:536.8 2.2 1
1,1-Dichloropropene ND ug/kg 11/16/21 19:43 563-58-611/16/21 13:536.8 3.3 1
cis-1,3-Dichloropropene ND ug/kg 11/16/21 19:43 10061-01-511/16/21 13:536.8 1.9 1
trans-1,3-Dichloropropene ND ug/kg 11/16/21 19:43 10061-02-611/16/21 13:536.8 2.3 1
Diisopropyl ether ND ug/kg 11/16/21 19:43 108-20-311/16/21 13:536.8 1.8 1
Ethylbenzene 7.1 ug/kg 11/16/21 19:43 100-41-411/16/21 13:536.8 3.2 1
Hexachloro-1,3-butadiene ND ug/kg 11/16/21 19:43 87-68-311/16/21 13:5313.6 11.1 1
2-Hexanone ND ug/kg 11/16/21 19:43 591-78-611/16/21 13:5368.0 6.6 1
Isopropylbenzene (Cumene)ND ug/kg 11/16/21 19:43 98-82-811/16/21 13:536.8 2.3 1
p-Isopropyltoluene ND ug/kg 11/16/21 19:43 99-87-611/16/21 13:536.8 3.3 1
Methylene Chloride ND ug/kg 11/16/21 19:43 75-09-211/16/21 13:5327.2 18.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/16/21 19:43 108-10-111/16/21 13:5368.0 6.6 1
Methyl-tert-butyl ether ND ug/kg 11/16/21 19:43 1634-04-411/16/21 13:536.8 2.5 1
Naphthalene 40.5 ug/kg 11/16/21 19:43 91-20-311/16/21 13:536.8 3.6 1
n-Propylbenzene ND ug/kg 11/16/21 19:43 103-65-111/16/21 13:536.8 2.4 1
Styrene ND ug/kg 11/16/21 19:43 100-42-511/16/21 13:536.8 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/16/21 19:43 630-20-611/16/21 13:536.8 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/16/21 19:43 79-34-511/16/21 13:536.8 1.8 1
Tetrachloroethene ND ug/kg 11/16/21 19:43 127-18-411/16/21 13:536.8 2.2 1
Toluene 27.4 ug/kg 11/16/21 19:43 108-88-311/16/21 13:536.8 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:4-6'Lab ID:92572495002 Collected:11/09/21 14:30 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 11/16/21 19:43 87-61-611/16/21 13:536.8 5.5 1
1,2,4-Trichlorobenzene ND ug/kg 11/16/21 19:43 120-82-111/16/21 13:536.8 5.7 1
1,1,1-Trichloroethane ND ug/kg 11/16/21 19:43 71-55-611/16/21 13:536.8 3.5 1
1,1,2-Trichloroethane ND ug/kg 11/16/21 19:43 79-00-511/16/21 13:536.8 2.3 1
Trichloroethene ND ug/kg 11/16/21 19:43 79-01-611/16/21 13:536.8 1.8 1
Trichlorofluoromethane ND ug/kg 11/16/21 19:43 75-69-411/16/21 13:536.8 3.7 1
1,2,3-Trichloropropane ND ug/kg 11/16/21 19:43 96-18-411/16/21 13:536.8 3.4 1
1,2,4-Trimethylbenzene 22.9 ug/kg 11/16/21 19:43 95-63-611/16/21 13:536.8 1.9 1
1,3,5-Trimethylbenzene 7.9 ug/kg 11/16/21 19:43 108-67-811/16/21 13:536.8 2.3 1
Vinyl acetate ND ug/kg 11/16/21 19:43 108-05-411/16/21 13:5368.0 5.0 1
Vinyl chloride ND ug/kg 11/16/21 19:43 75-01-411/16/21 13:5313.6 3.5 1
Xylene (Total)72.5 ug/kg 11/16/21 19:43 1330-20-711/16/21 13:5313.6 3.9 1
m&p-Xylene 43.3 ug/kg 11/16/21 19:43 179601-23-111/16/21 13:5313.6 4.7 1
o-Xylene 29.1 ug/kg 11/16/21 19:43 95-47-611/16/21 13:536.8 3.0 1
Surrogates
Toluene-d8 (S)98 %11/16/21 19:43 2037-26-511/16/21 13:5370-130 1
4-Bromofluorobenzene (S)99 %11/16/21 19:43 460-00-411/16/21 13:5369-134 1
1,2-Dichloroethane-d4 (S)101 %11/16/21 19:43 17060-07-011/16/21 13:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 8.8 %11/15/21 17:31 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:5-6'Lab ID:92572495003 Collected:11/09/21 15:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/17/21 20:03 83-32-911/16/21 11:2019506845
Acenaphthylene ND ug/kg 11/17/21 20:03 208-96-811/16/21 11:2019506845
Aniline ND ug/kg 11/17/21 20:03 62-53-311/16/21 11:2019507615
Anthracene ND ug/kg 11/17/21 20:03 120-12-711/16/21 11:2019506375
Benzo(a)anthracene ND ug/kg 11/17/21 20:03 56-55-311/16/21 11:2019506495
Benzo(a)pyrene ND ug/kg 11/17/21 20:03 50-32-811/16/21 11:2019506725
Benzo(b)fluoranthene ND ug/kg 11/17/21 20:03 205-99-211/16/21 11:2019506495
Benzo(g,h,i)perylene ND ug/kg 11/17/21 20:03 191-24-211/16/21 11:2019507555
Benzo(k)fluoranthene ND ug/kg 11/17/21 20:03 207-08-911/16/21 11:2019506845
Benzoic Acid ND ug/kg 11/17/21 20:03 65-85-011/16/21 11:20973041805
Benzyl alcohol ND ug/kg 11/17/21 20:03 100-51-611/16/21 11:20389014705
4-Bromophenylphenyl ether ND ug/kg 11/17/21 20:03 101-55-311/16/21 11:2019507495
Butylbenzylphthalate ND ug/kg 11/17/21 20:03 85-68-711/16/21 11:2019508205
4-Chloro-3-methylphenol ND ug/kg 11/17/21 20:03 59-50-711/16/21 11:20389013705
4-Chloroaniline ND ug/kg 11/17/21 20:03 106-47-811/16/21 11:20389015305
bis(2-Chloroethoxy)methane ND ug/kg 11/17/21 20:03 111-91-111/16/21 11:2019508085
bis(2-Chloroethyl) ether ND ug/kg 11/17/21 20:03 111-44-411/16/21 11:2019507315
2-Chloronaphthalene ND ug/kg 11/17/21 20:03 91-58-711/16/21 11:2019507725
2-Chlorophenol ND ug/kg 11/17/21 20:03 95-57-811/16/21 11:2019507315
4-Chlorophenylphenyl ether ND ug/kg 11/17/21 20:03 7005-72-311/16/21 11:2019507255
Chrysene ND ug/kg 11/17/21 20:03 218-01-911/16/21 11:2019507085
Dibenz(a,h)anthracene ND ug/kg 11/17/21 20:03 53-70-311/16/21 11:2019507495
Dibenzofuran ND ug/kg 11/17/21 20:03 132-64-911/16/21 11:2019507025
1,2-Dichlorobenzene ND ug/kg 11/17/21 20:03 95-50-111/16/21 11:2019507025
1,3-Dichlorobenzene ND ug/kg 11/17/21 20:03 541-73-111/16/21 11:2019506905
1,4-Dichlorobenzene ND ug/kg 11/17/21 20:03 106-46-711/16/21 11:2019507435
3,3'-Dichlorobenzidine ND ug/kg 11/17/21 20:03 91-94-1 IL11/16/21 11:20389013105
2,4-Dichlorophenol ND ug/kg 11/17/21 20:03 120-83-211/16/21 11:2019507615
Diethylphthalate ND ug/kg 11/17/21 20:03 84-66-211/16/21 11:2019507145
2,4-Dimethylphenol ND ug/kg 11/17/21 20:03 105-67-911/16/21 11:2019508085
Dimethylphthalate ND ug/kg 11/17/21 20:03 131-11-311/16/21 11:2019507085
Di-n-butylphthalate ND ug/kg 11/17/21 20:03 84-74-211/16/21 11:2019506555
4,6-Dinitro-2-methylphenol ND ug/kg 11/17/21 20:03 534-52-1 v111/16/21 11:20389018205
2,4-Dinitrophenol ND ug/kg 11/17/21 20:03 51-28-5 v111/16/21 11:20973060105
2,4-Dinitrotoluene ND ug/kg 11/17/21 20:03 121-14-211/16/21 11:2019507495
2,6-Dinitrotoluene ND ug/kg 11/17/21 20:03 606-20-211/16/21 11:2019507145
Di-n-octylphthalate ND ug/kg 11/17/21 20:03 117-84-011/16/21 11:2019507675
bis(2-Ethylhexyl)phthalate ND ug/kg 11/17/21 20:03 117-81-711/16/21 11:2019507555
Fluoranthene ND ug/kg 11/17/21 20:03 206-44-011/16/21 11:2019506665
Fluorene ND ug/kg 11/17/21 20:03 86-73-711/16/21 11:2019506845
Hexachloro-1,3-butadiene ND ug/kg 11/17/21 20:03 87-68-3 v111/16/21 11:2019508435
Hexachlorobenzene ND ug/kg 11/17/21 20:03 118-74-111/16/21 11:2019507615
Hexachlorocyclopentadiene ND ug/kg 11/17/21 20:03 77-47-411/16/21 11:20195011105
Hexachloroethane ND ug/kg 11/17/21 20:03 67-72-111/16/21 11:2019507435
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:5-6'Lab ID:92572495003 Collected:11/09/21 15:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 11/17/21 20:03 193-39-511/16/21 11:2019507675
Isophorone ND ug/kg 11/17/21 20:03 78-59-111/16/21 11:2019508675
1-Methylnaphthalene ND ug/kg 11/17/21 20:03 90-12-011/16/21 11:2019506845
2-Methylnaphthalene ND ug/kg 11/17/21 20:03 91-57-611/16/21 11:2019507785
2-Methylphenol(o-Cresol)ND ug/kg 11/17/21 20:03 95-48-711/16/21 11:2019507965
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/17/21 20:03 15831-10-411/16/21 11:2019507845
Naphthalene ND ug/kg 11/17/21 20:03 91-20-311/16/21 11:2019506605
2-Nitroaniline ND ug/kg 11/17/21 20:03 88-74-411/16/21 11:20973015905
3-Nitroaniline ND ug/kg 11/17/21 20:03 99-09-2 IL11/16/21 11:20973015305
4-Nitroaniline ND ug/kg 11/17/21 20:03 100-01-611/16/21 11:20389014805
Nitrobenzene ND ug/kg 11/17/21 20:03 98-95-311/16/21 11:2019509025
2-Nitrophenol ND ug/kg 11/17/21 20:03 88-75-511/16/21 11:2019508435
4-Nitrophenol ND ug/kg 11/17/21 20:03 100-02-7 v111/16/21 11:20973037605
N-Nitrosodimethylamine ND ug/kg 11/17/21 20:03 62-75-911/16/21 11:2019506555
N-Nitroso-di-n-propylamine ND ug/kg 11/17/21 20:03 621-64-711/16/21 11:2019507315
N-Nitrosodiphenylamine ND ug/kg 11/17/21 20:03 86-30-611/16/21 11:2019506905
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/17/21 20:03 108-60-1 v211/16/21 11:2019509265
Pentachlorophenol ND ug/kg 11/17/21 20:03 87-86-511/16/21 11:20389019005
Phenanthrene ND ug/kg 11/17/21 20:03 85-01-811/16/21 11:2019506375
Phenol ND ug/kg 11/17/21 20:03 108-95-2 v111/16/21 11:2019508675
Pyrene ND ug/kg 11/17/21 20:03 129-00-011/16/21 11:2019507905
Pyridine ND ug/kg 11/17/21 20:03 110-86-111/16/21 11:2019506135
1,2,4-Trichlorobenzene ND ug/kg 11/17/21 20:03 120-82-111/16/21 11:2019507675
2,4,5-Trichlorophenol ND ug/kg 11/17/21 20:03 95-95-411/16/21 11:2019508905
2,4,6-Trichlorophenol ND ug/kg 11/17/21 20:03 88-06-211/16/21 11:2019508025
Surrogates
Nitrobenzene-d5 (S)98 %11/17/21 20:03 4165-60-0 D311/16/21 11:2021-130 5
2-Fluorobiphenyl (S)93 %11/17/21 20:03 321-60-811/16/21 11:2019-130 5
Terphenyl-d14 (S)120 %11/17/21 20:03 1718-51-011/16/21 11:2015-130 5
Phenol-d6 (S)89 %11/17/21 20:03 13127-88-311/16/21 11:2018-130 5
2-Fluorophenol (S)78 %11/17/21 20:03 367-12-411/16/21 11:2018-130 5
2,4,6-Tribromophenol (S)96 %11/17/21 20:03 118-79-611/16/21 11:2018-130 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/16/21 21:16 67-64-111/16/21 13:5324377.9 1
Benzene 6.4J ug/kg 11/16/21 21:16 71-43-211/16/21 13:5312.1 4.8 1
Bromobenzene ND ug/kg 11/16/21 21:16 108-86-111/16/21 13:5312.1 4.0 1
Bromochloromethane ND ug/kg 11/16/21 21:16 74-97-511/16/21 13:5312.1 3.6 1
Bromodichloromethane ND ug/kg 11/16/21 21:16 75-27-411/16/21 13:5312.1 4.7 1
Bromoform ND ug/kg 11/16/21 21:16 75-25-211/16/21 13:5312.1 4.3 1
Bromomethane ND ug/kg 11/16/21 21:16 74-83-9 IK,L1,v111/16/21 13:5324.3 19.2 1
2-Butanone (MEK)ND ug/kg 11/16/21 21:16 78-93-311/16/21 13:5324358.3 1
n-Butylbenzene ND ug/kg 11/16/21 21:16 104-51-811/16/21 13:5312.1 5.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:5-6'Lab ID:92572495003 Collected:11/09/21 15:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene ND ug/kg 11/16/21 21:16 135-98-811/16/21 13:5312.1 5.3 1
tert-Butylbenzene ND ug/kg 11/16/21 21:16 98-06-611/16/21 13:5312.1 4.3 1
Carbon tetrachloride ND ug/kg 11/16/21 21:16 56-23-511/16/21 13:5312.1 4.5 1
Chlorobenzene ND ug/kg 11/16/21 21:16 108-90-711/16/21 13:5312.1 2.3 1
Chloroethane ND ug/kg 11/16/21 21:16 75-00-311/16/21 13:5324.3 9.4 1
Chloroform ND ug/kg 11/16/21 21:16 67-66-311/16/21 13:5312.1 7.4 1
Chloromethane ND ug/kg 11/16/21 21:16 74-87-311/16/21 13:5324.3 10.2 1
2-Chlorotoluene ND ug/kg 11/16/21 21:16 95-49-811/16/21 13:5312.1 4.3 1
4-Chlorotoluene ND ug/kg 11/16/21 21:16 106-43-411/16/21 13:5312.1 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/16/21 21:16 96-12-811/16/21 13:5312.1 4.7 1
Dibromochloromethane ND ug/kg 11/16/21 21:16 124-48-111/16/21 13:5312.1 6.8 1
1,2-Dibromoethane (EDB)ND ug/kg 11/16/21 21:16 106-93-411/16/21 13:5312.1 5.3 1
Dibromomethane ND ug/kg 11/16/21 21:16 74-95-311/16/21 13:5312.1 2.6 1
1,2-Dichlorobenzene ND ug/kg 11/16/21 21:16 95-50-111/16/21 13:5312.1 4.4 1
1,3-Dichlorobenzene ND ug/kg 11/16/21 21:16 541-73-111/16/21 13:5312.1 3.8 1
1,4-Dichlorobenzene ND ug/kg 11/16/21 21:16 106-46-711/16/21 13:5312.1 3.2 1
Dichlorodifluoromethane ND ug/kg 11/16/21 21:16 75-71-811/16/21 13:5324.3 5.3 1
1,1-Dichloroethane ND ug/kg 11/16/21 21:16 75-34-311/16/21 13:5312.1 5.0 1
1,2-Dichloroethane ND ug/kg 11/16/21 21:16 107-06-211/16/21 13:5312.1 8.0 1
1,1-Dichloroethene ND ug/kg 11/16/21 21:16 75-35-411/16/21 13:5312.1 5.0 1
cis-1,2-Dichloroethene ND ug/kg 11/16/21 21:16 156-59-211/16/21 13:5312.1 4.2 1
trans-1,2-Dichloroethene ND ug/kg 11/16/21 21:16 156-60-511/16/21 13:5312.1 4.2 1
1,2-Dichloropropane ND ug/kg 11/16/21 21:16 78-87-511/16/21 13:5312.1 3.6 1
1,3-Dichloropropane ND ug/kg 11/16/21 21:16 142-28-911/16/21 13:5312.1 3.8 1
2,2-Dichloropropane ND ug/kg 11/16/21 21:16 594-20-711/16/21 13:5312.1 4.0 1
1,1-Dichloropropene ND ug/kg 11/16/21 21:16 563-58-611/16/21 13:5312.1 5.8 1
cis-1,3-Dichloropropene ND ug/kg 11/16/21 21:16 10061-01-511/16/21 13:5312.1 3.3 1
trans-1,3-Dichloropropene ND ug/kg 11/16/21 21:16 10061-02-611/16/21 13:5312.1 4.2 1
Diisopropyl ether ND ug/kg 11/16/21 21:16 108-20-311/16/21 13:5312.1 3.3 1
Ethylbenzene 10J ug/kg 11/16/21 21:16 100-41-411/16/21 13:5312.1 5.7 1
Hexachloro-1,3-butadiene ND ug/kg 11/16/21 21:16 87-68-311/16/21 13:5324.3 19.9 1
2-Hexanone ND ug/kg 11/16/21 21:16 591-78-611/16/21 13:5312111.7 1
Isopropylbenzene (Cumene)ND ug/kg 11/16/21 21:16 98-82-811/16/21 13:5312.1 4.1 1
p-Isopropyltoluene ND ug/kg 11/16/21 21:16 99-87-611/16/21 13:5312.1 6.0 1
Methylene Chloride ND ug/kg 11/16/21 21:16 75-09-211/16/21 13:5348.5 33.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/16/21 21:16 108-10-111/16/21 13:5312111.7 1
Methyl-tert-butyl ether ND ug/kg 11/16/21 21:16 1634-04-411/16/21 13:5312.1 4.5 1
Naphthalene 34.8 ug/kg 11/16/21 21:16 91-20-311/16/21 13:5312.1 6.4 1
n-Propylbenzene ND ug/kg 11/16/21 21:16 103-65-111/16/21 13:5312.1 4.3 1
Styrene ND ug/kg 11/16/21 21:16 100-42-511/16/21 13:5312.1 3.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/16/21 21:16 630-20-611/16/21 13:5312.1 4.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/16/21 21:16 79-34-511/16/21 13:5312.1 3.2 1
Tetrachloroethene ND ug/kg 11/16/21 21:16 127-18-411/16/21 13:5312.1 3.8 1
Toluene 59.9 ug/kg 11/16/21 21:16 108-88-311/16/21 13:5312.1 3.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:5-6'Lab ID:92572495003 Collected:11/09/21 15:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 11/16/21 21:16 87-61-611/16/21 13:5312.1 9.8 1
1,2,4-Trichlorobenzene ND ug/kg 11/16/21 21:16 120-82-111/16/21 13:5312.1 10.2 1
1,1,1-Trichloroethane ND ug/kg 11/16/21 21:16 71-55-611/16/21 13:5312.1 6.3 1
1,1,2-Trichloroethane ND ug/kg 11/16/21 21:16 79-00-511/16/21 13:5312.1 4.0 1
Trichloroethene ND ug/kg 11/16/21 21:16 79-01-611/16/21 13:5312.1 3.1 1
Trichlorofluoromethane ND ug/kg 11/16/21 21:16 75-69-411/16/21 13:5312.1 6.7 1
1,2,3-Trichloropropane ND ug/kg 11/16/21 21:16 96-18-411/16/21 13:5312.1 6.1 1
1,2,4-Trimethylbenzene 18.7 ug/kg 11/16/21 21:16 95-63-611/16/21 13:5312.1 3.3 1
1,3,5-Trimethylbenzene ND ug/kg 11/16/21 21:16 108-67-811/16/21 13:5312.1 4.1 1
Vinyl acetate ND ug/kg 11/16/21 21:16 108-05-411/16/21 13:531218.8 1
Vinyl chloride ND ug/kg 11/16/21 21:16 75-01-411/16/21 13:5324.3 6.2 1
Xylene (Total)84.6 ug/kg 11/16/21 21:16 1330-20-711/16/21 13:5324.3 6.9 1
m&p-Xylene 53.3 ug/kg 11/16/21 21:16 179601-23-111/16/21 13:5324.3 8.3 1
o-Xylene 31.3 ug/kg 11/16/21 21:16 95-47-611/16/21 13:5312.1 5.4 1
Surrogates
Toluene-d8 (S)100 %11/16/21 21:16 2037-26-511/16/21 13:5370-130 1
4-Bromofluorobenzene (S)99 %11/16/21 21:16 460-00-411/16/21 13:5369-134 1
1,2-Dichloroethane-d4 (S)102 %11/16/21 21:16 17060-07-011/16/21 13:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.9 %11/15/21 17:31 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:2-7'Lab ID:92572495004 Collected:11/09/21 14:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)103000 ug/kg 11/26/21 12:5111/22/21 04:25787026301
Aliphatic (C19-C36)46500 ug/kg 11/26/21 12:5111/22/21 04:25787026301
Aromatic (C11-C22)75700 ug/kg 11/26/21 16:3211/22/21 04:25787026301
Total Extractable Hydrocarbons 225000 ug/kg 11/26/21 16:32 TPH-TEH11/22/21 04:25787026301
Surrogates
o-Terphenyl (S)67.0 %11/26/21 16:32 84-15-111/22/21 04:2540.0-140 1
1-Chloro-octadecane (S)61.3 %11/26/21 12:51 3386-33-211/22/21 04:2540.0-140 1
2-Fluorobiphenyl (S)84.0 %11/26/21 16:32 321-60-811/22/21 04:2540.0-140 1
2-Bromonaphthalene (S)80.5 %11/26/21 16:32 580-13-211/22/21 04:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 11/15/21 17:51 N211/15/21 14:463.1 3.1 1
Aliphatic(C09-C12) Adjusted 27.7 mg/kg 11/15/21 17:51 N211/15/21 14:463.1 3.1 1
Aromatic (C09-C10)8.5 mg/kg 11/15/21 17:51 N211/15/21 14:463.1 3.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)110 %11/15/21 17:51 460-00-411/15/21 14:4670-130 1
4-Bromofluorobenzene (PID) (S)93 %11/15/21 17:51 460-00-411/15/21 14:4670-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 11/17/21 20:33 83-32-911/16/21 11:2019806975
Acenaphthylene ND ug/kg 11/17/21 20:33 208-96-811/16/21 11:2019806975
Aniline ND ug/kg 11/17/21 20:33 62-53-311/16/21 11:2019807755
Anthracene ND ug/kg 11/17/21 20:33 120-12-711/16/21 11:2019806495
Benzo(a)anthracene ND ug/kg 11/17/21 20:33 56-55-311/16/21 11:2019806615
Benzo(a)pyrene ND ug/kg 11/17/21 20:33 50-32-811/16/21 11:2019806855
Benzo(b)fluoranthene ND ug/kg 11/17/21 20:33 205-99-211/16/21 11:2019806615
Benzo(g,h,i)perylene ND ug/kg 11/17/21 20:33 191-24-211/16/21 11:2019807695
Benzo(k)fluoranthene ND ug/kg 11/17/21 20:33 207-08-911/16/21 11:2019806975
Benzoic Acid ND ug/kg 11/17/21 20:33 65-85-011/16/21 11:20991042605
Benzyl alcohol ND ug/kg 11/17/21 20:33 100-51-611/16/21 11:20396015005
4-Bromophenylphenyl ether ND ug/kg 11/17/21 20:33 101-55-311/16/21 11:2019807635
Butylbenzylphthalate ND ug/kg 11/17/21 20:33 85-68-711/16/21 11:2019808355
4-Chloro-3-methylphenol ND ug/kg 11/17/21 20:33 59-50-711/16/21 11:20396013905
4-Chloroaniline ND ug/kg 11/17/21 20:33 106-47-811/16/21 11:20396015605
bis(2-Chloroethoxy)methane ND ug/kg 11/17/21 20:33 111-91-111/16/21 11:2019808235
bis(2-Chloroethyl) ether ND ug/kg 11/17/21 20:33 111-44-411/16/21 11:2019807455
2-Chloronaphthalene ND ug/kg 11/17/21 20:33 91-58-711/16/21 11:2019807875
2-Chlorophenol ND ug/kg 11/17/21 20:33 95-57-811/16/21 11:2019807455
4-Chlorophenylphenyl ether ND ug/kg 11/17/21 20:33 7005-72-311/16/21 11:2019807395
Chrysene ND ug/kg 11/17/21 20:33 218-01-911/16/21 11:2019807215
Dibenz(a,h)anthracene ND ug/kg 11/17/21 20:33 53-70-311/16/21 11:2019807635
Dibenzofuran ND ug/kg 11/17/21 20:33 132-64-911/16/21 11:2019807155
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:2-7'Lab ID:92572495004 Collected:11/09/21 14:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 11/17/21 20:33 95-50-111/16/21 11:2019807155
1,3-Dichlorobenzene ND ug/kg 11/17/21 20:33 541-73-111/16/21 11:2019807035
1,4-Dichlorobenzene ND ug/kg 11/17/21 20:33 106-46-711/16/21 11:2019807575
3,3'-Dichlorobenzidine ND ug/kg 11/17/21 20:33 91-94-1 IL11/16/21 11:20396013405
2,4-Dichlorophenol ND ug/kg 11/17/21 20:33 120-83-211/16/21 11:2019807755
Diethylphthalate ND ug/kg 11/17/21 20:33 84-66-211/16/21 11:2019807275
2,4-Dimethylphenol ND ug/kg 11/17/21 20:33 105-67-911/16/21 11:2019808235
Dimethylphthalate ND ug/kg 11/17/21 20:33 131-11-311/16/21 11:2019807215
Di-n-butylphthalate ND ug/kg 11/17/21 20:33 84-74-211/16/21 11:2019806675
4,6-Dinitro-2-methylphenol ND ug/kg 11/17/21 20:33 534-52-1 v111/16/21 11:20396018505
2,4-Dinitrophenol ND ug/kg 11/17/21 20:33 51-28-5 v111/16/21 11:20991061305
2,4-Dinitrotoluene ND ug/kg 11/17/21 20:33 121-14-211/16/21 11:2019807635
2,6-Dinitrotoluene ND ug/kg 11/17/21 20:33 606-20-211/16/21 11:2019807275
Di-n-octylphthalate ND ug/kg 11/17/21 20:33 117-84-011/16/21 11:2019807815
bis(2-Ethylhexyl)phthalate ND ug/kg 11/17/21 20:33 117-81-711/16/21 11:2019807695
Fluoranthene ND ug/kg 11/17/21 20:33 206-44-011/16/21 11:2019806795
Fluorene ND ug/kg 11/17/21 20:33 86-73-711/16/21 11:2019806975
Hexachloro-1,3-butadiene ND ug/kg 11/17/21 20:33 87-68-3 v111/16/21 11:2019808595
Hexachlorobenzene ND ug/kg 11/17/21 20:33 118-74-111/16/21 11:2019807755
Hexachlorocyclopentadiene ND ug/kg 11/17/21 20:33 77-47-411/16/21 11:20198011405
Hexachloroethane ND ug/kg 11/17/21 20:33 67-72-111/16/21 11:2019807575
Indeno(1,2,3-cd)pyrene ND ug/kg 11/17/21 20:33 193-39-511/16/21 11:2019807815
Isophorone ND ug/kg 11/17/21 20:33 78-59-111/16/21 11:2019808835
1-Methylnaphthalene ND ug/kg 11/17/21 20:33 90-12-011/16/21 11:2019806975
2-Methylnaphthalene ND ug/kg 11/17/21 20:33 91-57-611/16/21 11:2019807935
2-Methylphenol(o-Cresol)ND ug/kg 11/17/21 20:33 95-48-711/16/21 11:2019808115
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/17/21 20:33 15831-10-411/16/21 11:2019807995
Naphthalene ND ug/kg 11/17/21 20:33 91-20-311/16/21 11:2019806735
2-Nitroaniline ND ug/kg 11/17/21 20:33 88-74-411/16/21 11:20991016205
3-Nitroaniline ND ug/kg 11/17/21 20:33 99-09-2 IL11/16/21 11:20991015605
4-Nitroaniline ND ug/kg 11/17/21 20:33 100-01-611/16/21 11:20396015105
Nitrobenzene ND ug/kg 11/17/21 20:33 98-95-311/16/21 11:2019809195
2-Nitrophenol ND ug/kg 11/17/21 20:33 88-75-511/16/21 11:2019808595
4-Nitrophenol ND ug/kg 11/17/21 20:33 100-02-7 v111/16/21 11:20991038305
N-Nitrosodimethylamine ND ug/kg 11/17/21 20:33 62-75-911/16/21 11:2019806675
N-Nitroso-di-n-propylamine ND ug/kg 11/17/21 20:33 621-64-711/16/21 11:2019807455
N-Nitrosodiphenylamine ND ug/kg 11/17/21 20:33 86-30-611/16/21 11:2019807035
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/17/21 20:33 108-60-1 v211/16/21 11:2019809435
Pentachlorophenol ND ug/kg 11/17/21 20:33 87-86-511/16/21 11:20396019405
Phenanthrene ND ug/kg 11/17/21 20:33 85-01-811/16/21 11:2019806495
Phenol ND ug/kg 11/17/21 20:33 108-95-2 v111/16/21 11:2019808835
Pyrene ND ug/kg 11/17/21 20:33 129-00-011/16/21 11:2019808055
Pyridine ND ug/kg 11/17/21 20:33 110-86-111/16/21 11:2019806255
1,2,4-Trichlorobenzene ND ug/kg 11/17/21 20:33 120-82-111/16/21 11:2019807815
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:2-7'Lab ID:92572495004 Collected:11/09/21 14:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 11/17/21 20:33 95-95-411/16/21 11:2019809075
2,4,6-Trichlorophenol ND ug/kg 11/17/21 20:33 88-06-211/16/21 11:2019808175
Surrogates
Nitrobenzene-d5 (S)48 %11/17/21 20:33 4165-60-0 D311/16/21 11:2021-130 5
2-Fluorobiphenyl (S)46 %11/17/21 20:33 321-60-811/16/21 11:2019-130 5
Terphenyl-d14 (S)55 %11/17/21 20:33 1718-51-011/16/21 11:2015-130 5
Phenol-d6 (S)38 %11/17/21 20:33 13127-88-311/16/21 11:2018-130 5
2-Fluorophenol (S)34 %11/17/21 20:33 367-12-411/16/21 11:2018-130 5
2,4,6-Tribromophenol (S)43 %11/17/21 20:33 118-79-611/16/21 11:2018-130 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 11/16/21 23:43 67-64-111/16/21 13:5312339.6 1
Benzene 12.1 ug/kg 11/16/21 23:43 71-43-211/16/21 13:536.2 2.5 1
Bromobenzene ND ug/kg 11/16/21 23:43 108-86-111/16/21 13:536.2 2.0 1
Bromochloromethane ND ug/kg 11/16/21 23:43 74-97-511/16/21 13:536.2 1.8 1
Bromodichloromethane ND ug/kg 11/16/21 23:43 75-27-411/16/21 13:536.2 2.4 1
Bromoform ND ug/kg 11/16/21 23:43 75-25-211/16/21 13:536.2 2.2 1
Bromomethane ND ug/kg 11/16/21 23:43 74-83-9 IK,L1,v111/16/21 13:5312.3 9.8 1
2-Butanone (MEK)ND ug/kg 11/16/21 23:43 78-93-311/16/21 13:5312329.6 1
n-Butylbenzene ND ug/kg 11/16/21 23:43 104-51-811/16/21 13:536.2 2.9 1
sec-Butylbenzene 113 ug/kg 11/16/21 23:43 135-98-811/16/21 13:536.2 2.7 1
tert-Butylbenzene ND ug/kg 11/16/21 23:43 98-06-611/16/21 13:536.2 2.2 1
Carbon tetrachloride ND ug/kg 11/16/21 23:43 56-23-511/16/21 13:536.2 2.3 1
Chlorobenzene ND ug/kg 11/16/21 23:43 108-90-711/16/21 13:536.2 1.2 1
Chloroethane ND ug/kg 11/16/21 23:43 75-00-311/16/21 13:5312.3 4.8 1
Chloroform ND ug/kg 11/16/21 23:43 67-66-311/16/21 13:536.2 3.8 1
Chloromethane ND ug/kg 11/16/21 23:43 74-87-311/16/21 13:5312.3 5.2 1
2-Chlorotoluene ND ug/kg 11/16/21 23:43 95-49-811/16/21 13:536.2 2.2 1
4-Chlorotoluene ND ug/kg 11/16/21 23:43 106-43-411/16/21 13:536.2 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/16/21 23:43 96-12-811/16/21 13:536.2 2.4 1
Dibromochloromethane ND ug/kg 11/16/21 23:43 124-48-111/16/21 13:536.2 3.5 1
1,2-Dibromoethane (EDB)ND ug/kg 11/16/21 23:43 106-93-411/16/21 13:536.2 2.7 1
Dibromomethane ND ug/kg 11/16/21 23:43 74-95-311/16/21 13:536.2 1.3 1
1,2-Dichlorobenzene ND ug/kg 11/16/21 23:43 95-50-111/16/21 13:536.2 2.2 1
1,3-Dichlorobenzene ND ug/kg 11/16/21 23:43 541-73-111/16/21 13:536.2 1.9 1
1,4-Dichlorobenzene ND ug/kg 11/16/21 23:43 106-46-711/16/21 13:536.2 1.6 1
Dichlorodifluoromethane ND ug/kg 11/16/21 23:43 75-71-811/16/21 13:5312.3 2.7 1
1,1-Dichloroethane ND ug/kg 11/16/21 23:43 75-34-311/16/21 13:536.2 2.5 1
1,2-Dichloroethane ND ug/kg 11/16/21 23:43 107-06-211/16/21 13:536.2 4.1 1
1,1-Dichloroethene ND ug/kg 11/16/21 23:43 75-35-411/16/21 13:536.2 2.5 1
cis-1,2-Dichloroethene ND ug/kg 11/16/21 23:43 156-59-211/16/21 13:536.2 2.1 1
trans-1,2-Dichloroethene ND ug/kg 11/16/21 23:43 156-60-511/16/21 13:536.2 2.2 1
1,2-Dichloropropane ND ug/kg 11/16/21 23:43 78-87-511/16/21 13:536.2 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:2-7'Lab ID:92572495004 Collected:11/09/21 14:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 11/16/21 23:43 142-28-911/16/21 13:536.2 1.9 1
2,2-Dichloropropane ND ug/kg 11/16/21 23:43 594-20-711/16/21 13:536.2 2.0 1
1,1-Dichloropropene ND ug/kg 11/16/21 23:43 563-58-611/16/21 13:536.2 3.0 1
cis-1,3-Dichloropropene ND ug/kg 11/16/21 23:43 10061-01-511/16/21 13:536.2 1.7 1
trans-1,3-Dichloropropene ND ug/kg 11/16/21 23:43 10061-02-611/16/21 13:536.2 2.1 1
Diisopropyl ether ND ug/kg 11/16/21 23:43 108-20-311/16/21 13:536.2 1.7 1
Ethylbenzene 18.8 ug/kg 11/16/21 23:43 100-41-411/16/21 13:536.2 2.9 1
Hexachloro-1,3-butadiene ND ug/kg 11/16/21 23:43 87-68-311/16/21 13:5312.3 10.1 1
2-Hexanone ND ug/kg 11/16/21 23:43 591-78-611/16/21 13:5361.7 6.0 1
Isopropylbenzene (Cumene)9.3 ug/kg 11/16/21 23:43 98-82-811/16/21 13:536.2 2.1 1
p-Isopropyltoluene 229 ug/kg 11/16/21 23:43 99-87-611/16/21 13:536.2 3.0 1
Methylene Chloride ND ug/kg 11/16/21 23:43 75-09-211/16/21 13:5324.7 16.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/16/21 23:43 108-10-111/16/21 13:5361.7 6.0 1
Methyl-tert-butyl ether ND ug/kg 11/16/21 23:43 1634-04-411/16/21 13:536.2 2.3 1
Naphthalene 301 ug/kg 11/16/21 23:43 91-20-311/16/21 13:536.2 3.2 1
n-Propylbenzene 26.5 ug/kg 11/16/21 23:43 103-65-111/16/21 13:536.2 2.2 1
Styrene ND ug/kg 11/16/21 23:43 100-42-511/16/21 13:536.2 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/16/21 23:43 630-20-611/16/21 13:536.2 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/16/21 23:43 79-34-511/16/21 13:536.2 1.6 1
Tetrachloroethene ND ug/kg 11/16/21 23:43 127-18-411/16/21 13:536.2 2.0 1
Toluene 56.7 ug/kg 11/16/21 23:43 108-88-311/16/21 13:536.2 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 11/16/21 23:43 87-61-611/16/21 13:536.2 5.0 1
1,2,4-Trichlorobenzene ND ug/kg 11/16/21 23:43 120-82-111/16/21 13:536.2 5.2 1
1,1,1-Trichloroethane ND ug/kg 11/16/21 23:43 71-55-611/16/21 13:536.2 3.2 1
1,1,2-Trichloroethane ND ug/kg 11/16/21 23:43 79-00-511/16/21 13:536.2 2.0 1
Trichloroethene ND ug/kg 11/16/21 23:43 79-01-611/16/21 13:536.2 1.6 1
Trichlorofluoromethane ND ug/kg 11/16/21 23:43 75-69-411/16/21 13:536.2 3.4 1
1,2,3-Trichloropropane ND ug/kg 11/16/21 23:43 96-18-411/16/21 13:536.2 3.1 1
1,2,4-Trimethylbenzene 162 ug/kg 11/16/21 23:43 95-63-611/16/21 13:536.2 1.7 1
1,3,5-Trimethylbenzene 76.3 ug/kg 11/16/21 23:43 108-67-811/16/21 13:536.2 2.1 1
Vinyl acetate ND ug/kg 11/16/21 23:43 108-05-411/16/21 13:5361.7 4.5 1
Vinyl chloride ND ug/kg 11/16/21 23:43 75-01-411/16/21 13:5312.3 3.1 1
Xylene (Total)132 ug/kg 11/16/21 23:43 1330-20-711/16/21 13:5312.3 3.5 1
m&p-Xylene 85.3 ug/kg 11/16/21 23:43 179601-23-111/16/21 13:5312.3 4.2 1
o-Xylene 46.5 ug/kg 11/16/21 23:43 95-47-611/16/21 13:536.2 2.7 1
Surrogates
Toluene-d8 (S)98 %11/16/21 23:43 2037-26-511/16/21 13:5370-130 1
4-Bromofluorobenzene (S)106 %11/16/21 23:43 460-00-411/16/21 13:5369-134 1
1,2-Dichloroethane-d4 (S)100 %11/16/21 23:43 17060-07-011/16/21 13:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.9 %11/15/21 17:32 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92572495
21-418
Sample:2-7'Lab ID:92572495004 Collected:11/09/21 14:00 Received:11/15/21 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.6 %11/18/21 18:3911/18/21 18:321
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1778290
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92572495004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3734702-1
Associated Lab Samples:92572495004
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)ug/kg ND 6500 11/26/21 09:322170
Aliphatic (C19-C36)ug/kg ND 6500 11/26/21 09:322170
Total Extractable Hydrocarbons ug/kg ND 6500 11/26/21 09:322170
1-Chloro-octadecane (S)%76.5 40.0-140 11/26/21 09:32
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3734702-4
Associated Lab Samples:92572495004
Matrix:Solid
AnalyzedMDL
Aromatic (C11-C22)ug/kg ND 6500 11/26/21 10:382170
Total Extractable Hydrocarbons ug/kg ND 6500 11/26/21 10:382170
o-Terphenyl (S)%66.4 40.0-140 11/26/21 10:38
2-Fluorobiphenyl (S)%81.2 40.0-140 11/26/21 10:38
2-Bromonaphthalene (S)%82 40.0-140 11/26/21 10:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3734702-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3734702-3
Aliphatic (C09-C18)ug/kg 2430039900 60.9 40.0-14059.623800 2.08 25
Aliphatic (C19-C36)ug/kg 4330053200 81.4 40.0-14080.642900 0.928 25
1-Chloro-octadecane (S)%81.6 40.0-14081.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3734702-5LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3734702-6
Aromatic (C11-C22)ug/kg 83100113000 73.5 40.0-14075.385100 2.38 25
o-Terphenyl (S)%67.7 40.0-14068.2
2-Fluorobiphenyl (S)%78.4 40.0-14077.6
2-Bromonaphthalene (S)%79.1 40.0-14078.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
659918
MADEP VPH
MADEP VPH
VPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92572495004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3458030
Associated Lab Samples:92572495004
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg ND 2.5 N211/15/21 13:362.5
Aromatic (C09-C10)mg/kg ND 2.5 N211/15/21 13:362.5
4-Bromofluorobenzene (FID) (S)%102 70-130 11/15/21 13:36
4-Bromofluorobenzene (PID) (S)%89 70-130 11/15/21 13:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3458031LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3458032
Aliphatic (C05-C08)mg/kg 13.5 N215.1 90 70-1309414.2 5 25
Aromatic (C09-C10)mg/kg 5.2 N2510370-1301035.2 1 25
4-Bromofluorobenzene (FID) (S)%104 70-130103
4-Bromofluorobenzene (PID) (S)%88 70-13087
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
660206
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3459385
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/16/21 18:121.9
1,1,1-Trichloroethane ug/kg ND 5.0 11/16/21 18:122.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/16/21 18:121.3
1,1,2-Trichloroethane ug/kg ND 5.0 11/16/21 18:121.7
1,1-Dichloroethane ug/kg ND 5.0 11/16/21 18:122.1
1,1-Dichloroethene ug/kg ND 5.0 11/16/21 18:122.1
1,1-Dichloropropene ug/kg ND 5.0 11/16/21 18:122.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/16/21 18:124.0
1,2,3-Trichloropropane ug/kg ND 5.0 11/16/21 18:122.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 11/16/21 18:124.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/16/21 18:121.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/16/21 18:121.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/16/21 18:122.2
1,2-Dichlorobenzene ug/kg ND 5.0 11/16/21 18:121.8
1,2-Dichloroethane ug/kg ND 5.0 11/16/21 18:123.3
1,2-Dichloropropane ug/kg ND 5.0 11/16/21 18:121.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/16/21 18:121.7
1,3-Dichlorobenzene ug/kg ND 5.0 11/16/21 18:121.6
1,3-Dichloropropane ug/kg ND 5.0 11/16/21 18:121.6
1,4-Dichlorobenzene ug/kg ND 5.0 11/16/21 18:121.3
2,2-Dichloropropane ug/kg ND 5.0 11/16/21 18:121.6
2-Butanone (MEK)ug/kg ND 100 11/16/21 18:1224.0
2-Chlorotoluene ug/kg ND 5.0 11/16/21 18:121.8
2-Hexanone ug/kg ND 50.0 11/16/21 18:124.8
4-Chlorotoluene ug/kg ND 5.0 11/16/21 18:120.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/16/21 18:124.8
Acetone ug/kg ND 100 11/16/21 18:1232.1
Benzene ug/kg ND 5.0 11/16/21 18:122.0
Bromobenzene ug/kg ND 5.0 11/16/21 18:121.6
Bromochloromethane ug/kg ND 5.0 11/16/21 18:121.5
Bromodichloromethane ug/kg ND 5.0 11/16/21 18:121.9
Bromoform ug/kg ND 5.0 11/16/21 18:121.8
Bromomethane ug/kg ND 10.0 IK,v111/16/21 18:127.9
Carbon tetrachloride ug/kg ND 5.0 11/16/21 18:121.9
Chlorobenzene ug/kg ND 5.0 11/16/21 18:120.96
Chloroethane ug/kg ND 10.0 11/16/21 18:123.9
Chloroform ug/kg ND 5.0 11/16/21 18:123.0
Chloromethane ug/kg ND 10.0 11/16/21 18:124.2
cis-1,2-Dichloroethene ug/kg ND 5.0 11/16/21 18:121.7
cis-1,3-Dichloropropene ug/kg ND 5.0 11/16/21 18:121.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3459385
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 11/16/21 18:122.8
Dibromomethane ug/kg ND 5.0 11/16/21 18:121.1
Dichlorodifluoromethane ug/kg ND 10.0 11/16/21 18:122.2
Diisopropyl ether ug/kg ND 5.0 11/16/21 18:121.4
Ethylbenzene ug/kg ND 5.0 11/16/21 18:122.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 11/16/21 18:128.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/16/21 18:121.7
m&p-Xylene ug/kg ND 10.0 11/16/21 18:123.4
Methyl-tert-butyl ether ug/kg ND 5.0 11/16/21 18:121.9
Methylene Chloride ug/kg ND 20.0 11/16/21 18:1213.7
n-Butylbenzene ug/kg ND 5.0 11/16/21 18:122.4
n-Propylbenzene ug/kg ND 5.0 11/16/21 18:121.8
Naphthalene ug/kg ND 5.0 11/16/21 18:122.6
o-Xylene ug/kg ND 5.0 11/16/21 18:122.2
p-Isopropyltoluene ug/kg ND 5.0 11/16/21 18:122.5
sec-Butylbenzene ug/kg ND 5.0 11/16/21 18:122.2
Styrene ug/kg ND 5.0 11/16/21 18:121.3
tert-Butylbenzene ug/kg ND 5.0 11/16/21 18:121.8
Tetrachloroethene ug/kg ND 5.0 11/16/21 18:121.6
Toluene ug/kg ND 5.0 11/16/21 18:121.4
trans-1,2-Dichloroethene ug/kg ND 5.0 11/16/21 18:121.8
trans-1,3-Dichloropropene ug/kg ND 5.0 11/16/21 18:121.7
Trichloroethene ug/kg ND 5.0 11/16/21 18:121.3
Trichlorofluoromethane ug/kg ND 5.0 11/16/21 18:122.8
Vinyl acetate ug/kg ND 50.0 11/16/21 18:123.6
Vinyl chloride ug/kg ND 10.0 11/16/21 18:122.5
Xylene (Total)ug/kg ND 10.0 11/16/21 18:122.8
1,2-Dichloroethane-d4 (S)%105 70-130 11/16/21 18:12
4-Bromofluorobenzene (S)%99 69-134 11/16/21 18:12
Toluene-d8 (S)%98 70-130 11/16/21 18:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3459386LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12101250 96 70-130
1,1,1-Trichloroethane ug/kg 12201250 97 70-130
1,1,2,2-Tetrachloroethane ug/kg 12301250 99 70-130
1,1,2-Trichloroethane ug/kg 12401250 99 70-130
1,1-Dichloroethane ug/kg 13001250 104 70-130
1,1-Dichloroethene ug/kg 13101250 105 70-130
1,1-Dichloropropene ug/kg 12201250 98 70-130
1,2,3-Trichlorobenzene ug/kg 12601250 100 65-130
1,2,3-Trichloropropane ug/kg 12401250 99 70-130
1,2,4-Trichlorobenzene ug/kg 12701250 102 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3459386LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12201250 98 70-130
1,2-Dibromo-3-chloropropane ug/kg 13501250 108 70-130
1,2-Dibromoethane (EDB)ug/kg 12501250 100 70-130
1,2-Dichlorobenzene ug/kg 12101250 97 70-130
1,2-Dichloroethane ug/kg 11601250 93 63-130
1,2-Dichloropropane ug/kg 12601250 101 70-130
1,3,5-Trimethylbenzene ug/kg 12401250 99 70-130
1,3-Dichlorobenzene ug/kg 11801250 94 70-130
1,3-Dichloropropane ug/kg 12101250 97 70-130
1,4-Dichlorobenzene ug/kg 12101250 97 70-130
2,2-Dichloropropane ug/kg 12201250 98 66-130
2-Butanone (MEK)ug/kg 25102500 101 70-130
2-Chlorotoluene ug/kg 12301250 98 70-130
2-Hexanone ug/kg 25702500 103 70-130
4-Chlorotoluene ug/kg 12001250 96 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24902500 100 70-130
Acetone ug/kg 23202500 93 69-130
Benzene ug/kg 12301250 99 70-130
Bromobenzene ug/kg 12401250 99 70-130
Bromochloromethane ug/kg 13001250 104 70-130
Bromodichloromethane ug/kg 12201250 97 69-130
Bromoform ug/kg 13001250 104 70-130
Bromomethane ug/kg 1700 IK,L1,v1125013652-130
Carbon tetrachloride ug/kg 12401250 99 70-130
Chlorobenzene ug/kg 11901250 95 70-130
Chloroethane ug/kg 14201250 114 65-130
Chloroform ug/kg 12301250 98 70-130
Chloromethane ug/kg 12401250 99 55-130
cis-1,2-Dichloroethene ug/kg 12601250 101 70-130
cis-1,3-Dichloropropene ug/kg 12601250 101 70-130
Dibromochloromethane ug/kg 12901250 103 70-130
Dibromomethane ug/kg 12901250 103 70-130
Dichlorodifluoromethane ug/kg 12801250 102 45-156
Diisopropyl ether ug/kg 12001250 96 70-130
Ethylbenzene ug/kg 11101250 89 70-130
Hexachloro-1,3-butadiene ug/kg 12301250 98 66-130
Isopropylbenzene (Cumene)ug/kg 12001250 96 70-130
m&p-Xylene ug/kg 23602500 95 70-130
Methyl-tert-butyl ether ug/kg 12101250 97 70-130
Methylene Chloride ug/kg 11301250 91 65-130
n-Butylbenzene ug/kg 12401250 99 67-130
n-Propylbenzene ug/kg 12001250 96 70-130
Naphthalene ug/kg 12001250 96 70-130
o-Xylene ug/kg 11801250 94 70-130
p-Isopropyltoluene ug/kg 12401250 99 67-130
sec-Butylbenzene ug/kg 12101250 97 69-130
Styrene ug/kg 12601250 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3459386LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11601250 93 67-130
Tetrachloroethene ug/kg 11801250 94 70-130
Toluene ug/kg 11801250 95 70-130
trans-1,2-Dichloroethene ug/kg 13301250 107 70-130
trans-1,3-Dichloropropene ug/kg 12201250 98 68-130
Trichloroethene ug/kg 12201250 98 70-130
Trichlorofluoromethane ug/kg 11901250 95 70-130
Vinyl acetate ug/kg 23902500 96 70-130
Vinyl chloride ug/kg 13201250 105 61-130
Xylene (Total)ug/kg 35403750 94 70-130
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3459388MATRIX SPIKE SAMPLE:
MSSpike
Result
92572501002
1,1,1,2-Tetrachloroethane ug/kg 389 M17105570-131ND
1,1,1-Trichloroethane ug/kg 381 M17105465-133ND
1,1,2,2-Tetrachloroethane ug/kg 378 M17105366-130ND
1,1,2-Trichloroethane ug/kg 385 M17105466-133ND
1,1-Dichloroethane ug/kg 403 M17105765-130ND
1,1-Dichloroethene ug/kg 390710 55 10-158ND
1,1-Dichloropropene ug/kg 370 M17105268-133ND
1,2,3-Trichlorobenzene ug/kg 367710 52 27-138ND
1,2,3-Trichloropropane ug/kg 373 M17105267-130ND
1,2,4-Trichlorobenzene ug/kg 358 M17105051-134ND
1,2,4-Trimethylbenzene ug/kg 381 M17105463-136ND
1,2-Dibromo-3-chloropropane ug/kg 344710 48 32-130ND
1,2-Dibromoethane (EDB)ug/kg 391 M17105570-130ND
1,2-Dichlorobenzene ug/kg 371 M17105269-130ND
1,2-Dichloroethane ug/kg 367 M17105259-130ND
1,2-Dichloropropane ug/kg 411 M17105870-130ND
1,3,5-Trimethylbenzene ug/kg 378 M17105365-137ND
1,3-Dichlorobenzene ug/kg 357 M17105070-130ND
1,3-Dichloropropane ug/kg 391 M17105570-130ND
1,4-Dichlorobenzene ug/kg 363 M17105168-130ND
2,2-Dichloropropane ug/kg 353710 50 32-130ND
2-Butanone (MEK)ug/kg 3201420 23 10-136ND
2-Chlorotoluene ug/kg 367 M17105269-141ND
2-Hexanone ug/kg 6511420 46 10-144ND
4-Chlorotoluene ug/kg 351 M17104970-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 7121420 50 25-143ND
Acetone ug/kg 3711420 26 10-130ND
Benzene ug/kg 404 M17105767-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3459388MATRIX SPIKE SAMPLE:
MSSpike
Result
92572501002
Bromobenzene ug/kg 373 M17105370-130ND
Bromochloromethane ug/kg 394 M17105569-134ND
Bromodichloromethane ug/kg 361 M17105164-130ND
Bromoform ug/kg 358 M17105062-130ND
Bromomethane ug/kg 269 IK,v17103820-176ND
Carbon tetrachloride ug/kg 369 M17105265-140ND
Chlorobenzene ug/kg 382 M17105470-130ND
Chloroethane ug/kg 88.1710 12 10-130ND
Chloroform ug/kg 387 M17105463-130ND
Chloromethane ug/kg 404 M17105758-130ND
cis-1,2-Dichloroethene ug/kg 398 M17105666-130ND
cis-1,3-Dichloropropene ug/kg 390 M17105567-130ND
Dibromochloromethane ug/kg 363 M17105167-130ND
Dibromomethane ug/kg 394 M17105563-131ND
Dichlorodifluoromethane ug/kg 362710 51 44-180ND
Diisopropyl ether ug/kg 367 M17105263-130ND
Ethylbenzene ug/kg 371 M17105266-130ND
Hexachloro-1,3-butadiene ug/kg 356 M17105064-150ND
Isopropylbenzene (Cumene)ug/kg 399 M17105669-135ND
m&p-Xylene ug/kg 750 M114205360-133ND
Methyl-tert-butyl ether ug/kg 359 M17105165-130ND
Methylene Chloride ug/kg 402 M17105761-130ND
n-Butylbenzene ug/kg 351 M17104965-140ND
n-Propylbenzene ug/kg 359 M17105067-140ND
Naphthalene ug/kg 364710 51 15-145ND
o-Xylene ug/kg 385 M17105466-133ND
p-Isopropyltoluene ug/kg 371 M17105256-147ND
sec-Butylbenzene ug/kg 381 M17105465-139ND
Styrene ug/kg 391 M17105570-132ND
tert-Butylbenzene ug/kg 377 M17105362-135ND
Tetrachloroethene ug/kg 358 M17105070-135ND
Toluene ug/kg 388 M17105567-130ND
trans-1,2-Dichloroethene ug/kg 398 M17105669-130ND
trans-1,3-Dichloropropene ug/kg 361 M17105162-130ND
Trichloroethene ug/kg 389 M17105570-135ND
Trichlorofluoromethane ug/kg 70.8710 10 10-130ND
Vinyl acetate ug/kg 689 M114204853-130ND
Vinyl chloride ug/kg 406 M17105761-148ND
Xylene (Total)ug/kg 1130 MS21305363-132ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92572270002
3459387SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK,v130ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92572270002
3459387SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%101102
4-Bromofluorobenzene (S)%9999
Toluene-d8 (S)%9998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
660043
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3458706
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 330 11/16/21 14:52130
1,2-Dichlorobenzene ug/kg ND 330 11/16/21 14:52119
1,3-Dichlorobenzene ug/kg ND 330 11/16/21 14:52117
1,4-Dichlorobenzene ug/kg ND 330 11/16/21 14:52126
1-Methylnaphthalene ug/kg ND 330 11/16/21 14:52116
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 v211/16/21 14:52157
2,4,5-Trichlorophenol ug/kg ND 330 11/16/21 14:52151
2,4,6-Trichlorophenol ug/kg ND 330 11/16/21 14:52136
2,4-Dichlorophenol ug/kg ND 330 11/16/21 14:52129
2,4-Dimethylphenol ug/kg ND 330 11/16/21 14:52137
2,4-Dinitrophenol ug/kg ND 1650 v111/16/21 14:521020
2,4-Dinitrotoluene ug/kg ND 330 11/16/21 14:52127
2,6-Dinitrotoluene ug/kg ND 330 11/16/21 14:52121
2-Chloronaphthalene ug/kg ND 330 11/16/21 14:52131
2-Chlorophenol ug/kg ND 330 11/16/21 14:52124
2-Methylnaphthalene ug/kg ND 330 11/16/21 14:52132
2-Methylphenol(o-Cresol)ug/kg ND 330 11/16/21 14:52135
2-Nitroaniline ug/kg ND 1650 11/16/21 14:52270
2-Nitrophenol ug/kg ND 330 11/16/21 14:52143
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 11/16/21 14:52133
3,3'-Dichlorobenzidine ug/kg ND 660 IL11/16/21 14:52223
3-Nitroaniline ug/kg ND 1650 11/16/21 14:52259
4,6-Dinitro-2-methylphenol ug/kg ND 660 11/16/21 14:52308
4-Bromophenylphenyl ether ug/kg ND 330 11/16/21 14:52127
4-Chloro-3-methylphenol ug/kg ND 660 11/16/21 14:52232
4-Chloroaniline ug/kg ND 660 11/16/21 14:52259
4-Chlorophenylphenyl ether ug/kg ND 330 11/16/21 14:52123
4-Nitroaniline ug/kg ND 660 11/16/21 14:52251
4-Nitrophenol ug/kg ND 1650 11/16/21 14:52638
Acenaphthene ug/kg ND 330 11/16/21 14:52116
Acenaphthylene ug/kg ND 330 11/16/21 14:52116
Aniline ug/kg ND 330 11/16/21 14:52129
Anthracene ug/kg ND 330 11/16/21 14:52108
Benzo(a)anthracene ug/kg ND 330 11/16/21 14:52110
Benzo(a)pyrene ug/kg ND 330 11/16/21 14:52114
Benzo(b)fluoranthene ug/kg ND 330 11/16/21 14:52110
Benzo(g,h,i)perylene ug/kg ND 330 v111/16/21 14:52128
Benzo(k)fluoranthene ug/kg ND 330 11/16/21 14:52116
Benzoic Acid ug/kg ND 1650 11/16/21 14:52709
Benzyl alcohol ug/kg ND 660 11/16/21 14:52250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3458706
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 330 11/16/21 14:52137
bis(2-Chloroethyl) ether ug/kg ND 330 11/16/21 14:52124
bis(2-Ethylhexyl)phthalate ug/kg ND 330 11/16/21 14:52128
Butylbenzylphthalate ug/kg ND 330 11/16/21 14:52139
Chrysene ug/kg ND 330 11/16/21 14:52120
Di-n-butylphthalate ug/kg ND 330 11/16/21 14:52111
Di-n-octylphthalate ug/kg ND 330 11/16/21 14:52130
Dibenz(a,h)anthracene ug/kg ND 330 11/16/21 14:52127
Dibenzofuran ug/kg ND 330 11/16/21 14:52119
Diethylphthalate ug/kg ND 330 11/16/21 14:52121
Dimethylphthalate ug/kg ND 330 11/16/21 14:52120
Fluoranthene ug/kg ND 330 11/16/21 14:52113
Fluorene ug/kg ND 330 11/16/21 14:52116
Hexachloro-1,3-butadiene ug/kg ND 330 11/16/21 14:52143
Hexachlorobenzene ug/kg ND 330 11/16/21 14:52129
Hexachlorocyclopentadiene ug/kg ND 330 11/16/21 14:52189
Hexachloroethane ug/kg ND 330 11/16/21 14:52126
Indeno(1,2,3-cd)pyrene ug/kg ND 330 11/16/21 14:52130
Isophorone ug/kg ND 330 11/16/21 14:52147
N-Nitroso-di-n-propylamine ug/kg ND 330 11/16/21 14:52124
N-Nitrosodimethylamine ug/kg ND 330 11/16/21 14:52111
N-Nitrosodiphenylamine ug/kg ND 330 11/16/21 14:52117
Naphthalene ug/kg ND 330 11/16/21 14:52112
Nitrobenzene ug/kg ND 330 11/16/21 14:52153
Pentachlorophenol ug/kg ND 660 11/16/21 14:52323
Phenanthrene ug/kg ND 330 11/16/21 14:52108
Phenol ug/kg ND 330 11/16/21 14:52147
Pyrene ug/kg ND 330 11/16/21 14:52134
Pyridine ug/kg ND 330 11/16/21 14:52104
2,4,6-Tribromophenol (S)%100 18-130 11/16/21 14:52
2-Fluorobiphenyl (S)%98 19-130 11/16/21 14:52
2-Fluorophenol (S)%71 18-130 11/16/21 14:52
Nitrobenzene-d5 (S)%80 21-130 11/16/21 14:52
Phenol-d6 (S)%74 18-130 11/16/21 14:52
Terphenyl-d14 (S)%108 15-130 11/16/21 14:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3458707LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14801670 89 47-130
1,2-Dichlorobenzene ug/kg 12801670 77 49-130
1,3-Dichlorobenzene ug/kg 12701670 76 48-130
1,4-Dichlorobenzene ug/kg 13201670 79 49-130
1-Methylnaphthalene ug/kg 15201670 91 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3458707LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 892 v316705438-130
2,4,5-Trichlorophenol ug/kg 17701670 106 49-130
2,4,6-Trichlorophenol ug/kg 16801670 101 50-130
2,4-Dichlorophenol ug/kg 15401670 93 51-130
2,4-Dimethylphenol ug/kg 14301670 86 53-130
2,4-Dinitrophenol ug/kg 10000 v1833012039-130
2,4-Dinitrotoluene ug/kg 17301670 104 53-130
2,6-Dinitrotoluene ug/kg 16801670 101 55-130
2-Chloronaphthalene ug/kg 15701670 94 48-130
2-Chlorophenol ug/kg 12701670 76 54-130
2-Methylnaphthalene ug/kg 15001670 90 57-130
2-Methylphenol(o-Cresol)ug/kg 13201670 79 50-130
2-Nitroaniline ug/kg 26203330 79 49-130
2-Nitrophenol ug/kg 15201670 91 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 13101670 78 50-130
3,3'-Dichlorobenzidine ug/kg 2730 IL33308247-130
3-Nitroaniline ug/kg 32203330 97 45-130
4,6-Dinitro-2-methylphenol ug/kg 32703330 98 50-142
4-Bromophenylphenyl ether ug/kg 16201670 97 55-130
4-Chloro-3-methylphenol ug/kg 29803330 90 52-130
4-Chloroaniline ug/kg 26503330 79 49-130
4-Chlorophenylphenyl ether ug/kg 18101670 109 53-130
4-Nitroaniline ug/kg 29803330 89 51-130
4-Nitrophenol ug/kg 72908330 88 40-130
Acenaphthene ug/kg 16901670 101 56-130
Acenaphthylene ug/kg 16901670 101 58-130
Aniline ug/kg 11601670 70 44-130
Anthracene ug/kg 14501670 87 60-130
Benzo(a)anthracene ug/kg 15201670 91 59-130
Benzo(a)pyrene ug/kg 19301670 116 57-130
Benzo(b)fluoranthene ug/kg 19701670 118 54-130
Benzo(g,h,i)perylene ug/kg 1860 v1167011159-130
Benzo(k)fluoranthene ug/kg 20601670 124 54-130
Benzoic Acid ug/kg 76408330 92 19-130
Benzyl alcohol ug/kg 26003330 78 50-130
bis(2-Chloroethoxy)methane ug/kg 12901670 78 55-130
bis(2-Chloroethyl) ether ug/kg 12801670 77 53-130
bis(2-Ethylhexyl)phthalate ug/kg 15701670 94 58-130
Butylbenzylphthalate ug/kg 16401670 98 46-138
Chrysene ug/kg 15501670 93 57-130
Di-n-butylphthalate ug/kg 14301670 86 57-130
Di-n-octylphthalate ug/kg 14901670 90 57-130
Dibenz(a,h)anthracene ug/kg 18701670 112 60-130
Dibenzofuran ug/kg 17201670 103 54-130
Diethylphthalate ug/kg 16901670 102 55-130
Dimethylphthalate ug/kg 16401670 99 57-130
Fluoranthene ug/kg 15201670 91 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3458707LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 17101670 102 56-130
Hexachloro-1,3-butadiene ug/kg 15801670 95 41-130
Hexachlorobenzene ug/kg 16301670 98 53-130
Hexachlorocyclopentadiene ug/kg 10901670 65 23-130
Hexachloroethane ug/kg 12401670 74 48-130
Indeno(1,2,3-cd)pyrene ug/kg 18001670 108 61-130
Isophorone ug/kg 13501670 81 49-130
N-Nitroso-di-n-propylamine ug/kg 12401670 75 52-130
N-Nitrosodimethylamine ug/kg 10801670 65 45-130
N-Nitrosodiphenylamine ug/kg 14201670 85 56-130
Naphthalene ug/kg 13701670 82 56-130
Nitrobenzene ug/kg 12901670 77 50-130
Pentachlorophenol ug/kg 30003330 90 33-130
Phenanthrene ug/kg 14801670 89 60-130
Phenol ug/kg 13301670 80 54-130
Pyrene ug/kg 17501670 105 61-130
Pyridine ug/kg 9641670 58 35-130
2,4,6-Tribromophenol (S)%108 18-130
2-Fluorobiphenyl (S)%102 19-130
2-Fluorophenol (S)%74 18-130
Nitrobenzene-d5 (S)%81 21-130
Phenol-d6 (S)%79 18-130
Terphenyl-d14 (S)%116 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3458708MATRIX SPIKE SAMPLE:
MSSpike
Result
92572445001
1,2,4-Trichlorobenzene ug/kg 16001920 83 22-130ND
1,2-Dichlorobenzene ug/kg 14101920 74 23-130ND
1,3-Dichlorobenzene ug/kg 14101920 74 26-130ND
1,4-Dichlorobenzene ug/kg 14501920 75 27-130ND
1-Methylnaphthalene ug/kg 16401920 86 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 965 v319205030-130ND
2,4,5-Trichlorophenol ug/kg 18801920 98 26-130ND
2,4,6-Trichlorophenol ug/kg 17601920 92 23-130ND
2,4-Dichlorophenol ug/kg 16201920 84 29-130ND
2,4-Dimethylphenol ug/kg 14901920 78 13-130ND
2,4-Dinitrophenol ug/kg 11100 v1960011510-131ND
2,4-Dinitrotoluene ug/kg 18301920 95 28-130ND
2,6-Dinitrotoluene ug/kg 18601920 97 36-130ND
2-Chloronaphthalene ug/kg 16601920 86 27-130ND
2-Chlorophenol ug/kg 13801920 72 29-130ND
2-Methylnaphthalene ug/kg 15801920 82 29-130ND
2-Methylphenol(o-Cresol)ug/kg 14001920 73 20-130ND
2-Nitroaniline ug/kg 28503830 74 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
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Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3458708MATRIX SPIKE SAMPLE:
MSSpike
Result
92572445001
2-Nitrophenol ug/kg 16201920 85 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 13701920 72 10-176ND
3,3'-Dichlorobenzidine ug/kg 3040 IL38307915-130ND
3-Nitroaniline ug/kg 35203830 92 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 36003830 94 15-132ND
4-Bromophenylphenyl ether ug/kg 17101920 89 35-130ND
4-Chloro-3-methylphenol ug/kg 31303830 82 30-130ND
4-Chloroaniline ug/kg 27403830 72 28-130ND
4-Chlorophenylphenyl ether ug/kg 19401920 101 32-130ND
4-Nitroaniline ug/kg 32703830 85 30-130ND
4-Nitrophenol ug/kg 80809600 84 17-130ND
Acenaphthene ug/kg 17901920 93 29-130ND
Acenaphthylene ug/kg 17901920 93 31-130ND
Aniline ug/kg 12501920 65 10-130ND
Anthracene ug/kg 15701920 82 33-130ND
Benzo(a)anthracene ug/kg 17001920 89 32-130ND
Benzo(a)pyrene ug/kg 21601920 113 32-130ND
Benzo(b)fluoranthene ug/kg 22401920 117 33-130ND
Benzo(g,h,i)perylene ug/kg 1980 v1192010328-130ND
Benzo(k)fluoranthene ug/kg 21901920 114 31-130ND
Benzoic Acid ug/kg 82209600 86 10-130ND
Benzyl alcohol ug/kg 27203830 71 31-130ND
bis(2-Chloroethoxy)methane ug/kg 13801920 72 30-130ND
bis(2-Chloroethyl) ether ug/kg 14001920 73 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 16801920 88 40-130ND
Butylbenzylphthalate ug/kg 17001920 89 40-130ND
Chrysene ug/kg 17301920 90 30-130ND
Di-n-butylphthalate ug/kg 15901920 83 41-130ND
Di-n-octylphthalate ug/kg 16501920 86 42-130ND
Dibenz(a,h)anthracene ug/kg 20101920 105 27-130ND
Dibenzofuran ug/kg 18301920 95 32-130ND
Diethylphthalate ug/kg 18801920 98 40-130ND
Dimethylphthalate ug/kg 18101920 94 37-130ND
Fluoranthene ug/kg 17801920 93 26-130ND
Fluorene ug/kg 18401920 96 31-130ND
Hexachloro-1,3-butadiene ug/kg 17101920 89 20-130ND
Hexachlorobenzene ug/kg 17401920 91 29-130ND
Hexachlorocyclopentadiene ug/kg 11301920 59 10-130ND
Hexachloroethane ug/kg 13601920 71 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 19601920 102 28-130ND
Isophorone ug/kg 14001920 73 32-130ND
N-Nitroso-di-n-propylamine ug/kg 13201920 69 31-130ND
N-Nitrosodimethylamine ug/kg 12001920 63 20-130ND
N-Nitrosodiphenylamine ug/kg 15201920 79 32-130ND
Naphthalene ug/kg 14701920 76 30-130ND
Nitrobenzene ug/kg 14201920 74 25-130ND
Pentachlorophenol ug/kg 32803830 85 10-130ND
REPORT OF LABORATORY ANALYSIS
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Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3458708MATRIX SPIKE SAMPLE:
MSSpike
Result
92572445001
Phenanthrene ug/kg 16501920 86 34-130ND
Phenol ug/kg 14201920 74 14-130ND
Pyrene ug/kg 18201920 95 31-130ND
Pyridine ug/kg 10701920 56 10-130ND
2,4,6-Tribromophenol (S)%95 18-130
2-Fluorobiphenyl (S)%86 19-130
2-Fluorophenol (S)%65 18-130
Nitrobenzene-d5 (S)%71 21-130
Phenol-d6 (S)%68 18-130
Terphenyl-d14 (S)%97 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92572495001
3458709SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND v230ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND v130ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND IL30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92572495001
3458709SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND v130ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%8388
2-Fluorobiphenyl (S)%7681
2-Fluorophenol (S)%5560
Nitrobenzene-d5 (S)%6367
Phenol-d6 (S)%5965
Terphenyl-d14 (S)%8882
REPORT OF LABORATORY ANALYSIS
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Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
659981
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92572495001, 92572495002, 92572495003, 92572495004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92572480003
3458470SAMPLE DUPLICATE:
Percent Moisture %12.5 N212512.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92572525001
3458471SAMPLE DUPLICATE:
Percent Moisture %7.8 N22257.9
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92572495
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1776515
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92572495004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3731687-1
Associated Lab Samples:92572495004
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 11/18/21 18:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3731687-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
REPORT OF LABORATORY ANALYSIS
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Page 39 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92572495
21-418
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 40 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92572495
21-418
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92572495004 1778290 17782902-7'MA DEP/NJ DEP MADEP EPH
92572495004 659918 6599412-7'MADEP VPH MADEP VPH
92572495001 660043 6603711-6'EPA 3546 EPA 8270E
92572495002 660043 6603714-6'EPA 3546 EPA 8270E
92572495003 660043 6603715-6'EPA 3546 EPA 8270E
92572495004 660043 6603712-7'EPA 3546 EPA 8270E
92572495001 660206 6602771-6'EPA 5035A/5030B EPA 8260D
92572495002 660206 6602774-6'EPA 5035A/5030B EPA 8260D
92572495003 660206 6602775-6'EPA 5035A/5030B EPA 8260D
92572495004 660206 6602772-7'EPA 5035A/5030B EPA 8260D
92572495001 6599811-6'SW-846
92572495002 6599814-6'SW-846
92572495003 6599815-6'SW-846
92572495004 6599812-7'SW-846
92572495004 1776515 17765152-7'SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/30/2021 04:15 PM
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Page 41 of 44
Page 42 of 44
Page 43 of 44
Page 44 of 44
#=CL#
December 16, 2021
LIMS USE: FR - NATHAN SIMMONS
LIMS OBJECT ID: 92577240
92577240
Project:
Pace Project No.:
RE:
Nathan Simmons
Catawba Valley Engineering & Testing
161 Lenoir Rhyne Blvd SE
Hickory, NC 28603
21-418
Dear Nathan Simmons:
Enclosed are the analytical results for sample(s) received by the laboratory on December 10, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ryan Brumfield
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 54
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92577240
21-418
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 54
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92577240
21-418
Lab ID Sample ID Matrix Date Collected Date Received
92577240001 1 Water 12/10/21 10:00 12/10/21 13:10
92577240002 6 Water 12/10/21 11:00 12/10/21 13:10
92577240003 2 Water 12/10/21 10:15 12/10/21 13:10
92577240004 4 Water 12/10/21 10:30 12/10/21 13:10
92577240005 S-1 Solid 12/09/21 13:30 12/10/21 13:10
REPORT OF LABORATORY ANALYSIS
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Page 3 of 54
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92577240
21-418
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92577240001 1 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92577240002 6 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92577240003 2 EPA 8260D 63 PASI-CSAS
92577240004 4 EPA 8260D 63 PASI-CSAS
92577240005 S-1 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:1 Lab ID:92577240001 Collected:12/10/21 10:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 12/13/21 13:28 83-32-912/13/21 05:119.1 1.8 1
Acenaphthylene ND ug/L 12/13/21 13:28 208-96-812/13/21 05:119.1 1.8 1
Aniline ND ug/L 12/13/21 13:28 62-53-312/13/21 05:119.1 1.5 1
Anthracene ND ug/L 12/13/21 13:28 120-12-712/13/21 05:119.1 2.1 1
Benzo(a)anthracene ND ug/L 12/13/21 13:28 56-55-312/13/21 05:119.1 2.4 1
Benzo(a)pyrene ND ug/L 12/13/21 13:28 50-32-812/13/21 05:119.1 2.5 1
Benzo(b)fluoranthene ND ug/L 12/13/21 13:28 205-99-212/13/21 05:119.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 12/13/21 13:28 191-24-212/13/21 05:119.1 2.6 1
Benzo(k)fluoranthene ND ug/L 12/13/21 13:28 207-08-912/13/21 05:119.1 2.5 1
Benzoic Acid ND ug/L 12/13/21 13:28 65-85-012/13/21 05:1145.5 3.1 1
Benzyl alcohol ND ug/L 12/13/21 13:28 100-51-612/13/21 05:1118.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 12/13/21 13:28 101-55-312/13/21 05:119.1 1.6 1
Butylbenzylphthalate ND ug/L 12/13/21 13:28 85-68-712/13/21 05:119.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 12/13/21 13:28 59-50-712/13/21 05:119.1 3.0 1
4-Chloroaniline ND ug/L 12/13/21 13:28 106-47-812/13/21 05:1118.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 12/13/21 13:28 111-91-112/13/21 05:119.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 12/13/21 13:28 111-44-412/13/21 05:119.1 1.7 1
2-Chloronaphthalene ND ug/L 12/13/21 13:28 91-58-712/13/21 05:119.1 1.6 1
2-Chlorophenol ND ug/L 12/13/21 13:28 95-57-812/13/21 05:119.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 12/13/21 13:28 7005-72-312/13/21 05:119.1 1.8 1
Chrysene ND ug/L 12/13/21 13:28 218-01-912/13/21 05:119.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 12/13/21 13:28 53-70-312/13/21 05:119.1 2.7 1
Dibenzofuran ND ug/L 12/13/21 13:28 132-64-912/13/21 05:119.1 1.9 1
1,2-Dichlorobenzene ND ug/L 12/13/21 13:28 95-50-112/13/21 05:119.1 1.6 1
1,3-Dichlorobenzene ND ug/L 12/13/21 13:28 541-73-112/13/21 05:119.1 1.5 1
1,4-Dichlorobenzene ND ug/L 12/13/21 13:28 106-46-712/13/21 05:119.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 12/13/21 13:28 91-94-112/13/21 05:1118.2 7.4 1
2,4-Dichlorophenol ND ug/L 12/13/21 13:28 120-83-212/13/21 05:119.1 1.3 1
Diethylphthalate ND ug/L 12/13/21 13:28 84-66-212/13/21 05:119.1 1.9 1
2,4-Dimethylphenol ND ug/L 12/13/21 13:28 105-67-912/13/21 05:119.1 1.5 1
Dimethylphthalate ND ug/L 12/13/21 13:28 131-11-312/13/21 05:119.1 1.9 1
Di-n-butylphthalate ND ug/L 12/13/21 13:28 84-74-212/13/21 05:119.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 12/13/21 13:28 534-52-112/13/21 05:1118.2 3.1 1
2,4-Dinitrophenol ND ug/L 12/13/21 13:28 51-28-512/13/21 05:1145.5 23.6 1
2,4-Dinitrotoluene ND ug/L 12/13/21 13:28 121-14-212/13/21 05:119.1 1.5 1
2,6-Dinitrotoluene ND ug/L 12/13/21 13:28 606-20-212/13/21 05:119.1 1.6 1
Di-n-octylphthalate ND ug/L 12/13/21 13:28 117-84-012/13/21 05:119.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/13/21 13:28 117-81-712/13/21 05:115.5 3.4 1
Fluoranthene ND ug/L 12/13/21 13:28 206-44-012/13/21 05:119.1 2.0 1
Fluorene 2.5J ug/L 12/13/21 13:28 86-73-712/13/21 05:119.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 12/13/21 13:28 87-68-312/13/21 05:119.1 1.6 1
Hexachlorobenzene ND ug/L 12/13/21 13:28 118-74-112/13/21 05:119.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 12/13/21 13:28 77-47-412/13/21 05:119.1 1.4 1
Hexachloroethane ND ug/L 12/13/21 13:28 67-72-112/13/21 05:119.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 12/13/21 13:28 193-39-512/13/21 05:119.1 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:1 Lab ID:92577240001 Collected:12/10/21 10:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 12/13/21 13:28 78-59-112/13/21 05:119.1 1.5 1
1-Methylnaphthalene 19.1 ug/L 12/13/21 13:28 90-12-012/13/21 05:119.1 1.8 1
2-Methylnaphthalene 22.2 ug/L 12/13/21 13:28 91-57-612/13/21 05:119.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 12/13/21 13:28 95-48-712/13/21 05:119.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/13/21 13:28 15831-10-412/13/21 05:119.1 1.1 1
Naphthalene 9.6 ug/L 12/13/21 13:28 91-20-312/13/21 05:119.1 1.9 1
2-Nitroaniline ND ug/L 12/13/21 13:28 88-74-412/13/21 05:1118.2 2.7 1
3-Nitroaniline ND ug/L 12/13/21 13:28 99-09-212/13/21 05:1118.2 3.4 1
4-Nitroaniline ND ug/L 12/13/21 13:28 100-01-612/13/21 05:1118.2 4.6 1
Nitrobenzene ND ug/L 12/13/21 13:28 98-95-312/13/21 05:119.1 1.7 1
2-Nitrophenol ND ug/L 12/13/21 13:28 88-75-512/13/21 05:119.1 1.3 1
4-Nitrophenol ND ug/L 12/13/21 13:28 100-02-712/13/21 05:1145.5 6.0 1
N-Nitrosodimethylamine ND ug/L 12/13/21 13:28 62-75-912/13/21 05:119.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 12/13/21 13:28 621-64-712/13/21 05:119.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 12/13/21 13:28 86-30-612/13/21 05:119.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 12/13/21 13:28 108-60-112/13/21 05:119.1 1.0 1
Pentachlorophenol ND ug/L 12/13/21 13:28 87-86-512/13/21 05:1118.2 3.4 1
Phenanthrene 2.3J ug/L 12/13/21 13:28 85-01-812/13/21 05:119.1 1.8 1
Phenol ND ug/L 12/13/21 13:28 108-95-212/13/21 05:119.1 1.2 1
Pyrene ND ug/L 12/13/21 13:28 129-00-012/13/21 05:119.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 12/13/21 13:28 120-82-112/13/21 05:119.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 12/13/21 13:28 95-95-412/13/21 05:119.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 12/13/21 13:28 88-06-212/13/21 05:119.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)71 %12/13/21 13:28 4165-60-012/13/21 05:1110-144 1
2-Fluorobiphenyl (S)60 %12/13/21 13:28 321-60-812/13/21 05:1110-130 1
Terphenyl-d14 (S)71 %12/13/21 13:28 1718-51-012/13/21 05:1134-163 1
Phenol-d6 (S)47 %12/13/21 13:28 13127-88-312/13/21 05:1110-130 1
2-Fluorophenol (S)60 %12/13/21 13:28 367-12-412/13/21 05:1110-130 1
2,4,6-Tribromophenol (S)82 %12/13/21 13:28 118-79-612/13/21 05:1110-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 25.1 ug/L 12/14/21 02:56 67-64-125.0 5.1 1
Benzene ND ug/L 12/14/21 02:56 71-43-21.0 0.34 1
Bromobenzene ND ug/L 12/14/21 02:56 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 12/14/21 02:56 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 12/14/21 02:56 75-27-41.0 0.31 1
Bromoform ND ug/L 12/14/21 02:56 75-25-21.0 0.34 1
Bromomethane ND ug/L 12/14/21 02:56 74-83-92.0 1.7 1
2-Butanone (MEK)5.1 ug/L 12/14/21 02:56 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 12/14/21 02:56 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 12/14/21 02:56 108-90-71.0 0.28 1
Chloroethane ND ug/L 12/14/21 02:56 75-00-3 IL1.0 0.65 1
Chloroform ND ug/L 12/14/21 02:56 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:1 Lab ID:92577240001 Collected:12/10/21 10:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 12/14/21 02:56 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/14/21 02:56 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 12/14/21 02:56 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/21 02:56 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 12/14/21 02:56 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/21 02:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/14/21 02:56 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 12/14/21 02:56 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 12/14/21 02:56 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 12/14/21 02:56 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 12/14/21 02:56 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 12/14/21 02:56 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 12/14/21 02:56 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 12/14/21 02:56 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/14/21 02:56 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/14/21 02:56 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 12/14/21 02:56 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 12/14/21 02:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/14/21 02:56 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 12/14/21 02:56 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/14/21 02:56 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/14/21 02:56 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 12/14/21 02:56 108-20-31.0 0.31 1
Ethylbenzene 0.39J ug/L 12/14/21 02:56 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/14/21 02:56 87-68-32.0 1.5 1
2-Hexanone ND ug/L 12/14/21 02:56 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 12/14/21 02:56 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 12/14/21 02:56 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/14/21 02:56 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 12/14/21 02:56 1634-04-41.0 0.42 1
Naphthalene 20.3 ug/L 12/14/21 02:56 91-20-31.0 0.64 1
Styrene ND ug/L 12/14/21 02:56 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/21 02:56 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/14/21 02:56 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/14/21 02:56 127-18-41.0 0.29 1
Toluene 0.50J ug/L 12/14/21 02:56 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 12/14/21 02:56 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/14/21 02:56 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/14/21 02:56 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 12/14/21 02:56 79-00-51.0 0.32 1
Trichloroethene ND ug/L 12/14/21 02:56 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 12/14/21 02:56 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/14/21 02:56 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 12/14/21 02:56 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 12/14/21 02:56 75-01-41.0 0.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:1 Lab ID:92577240001 Collected:12/10/21 10:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)2.5 ug/L 12/14/21 02:56 1330-20-71.0 0.34 1
m&p-Xylene 1.5J ug/L 12/14/21 02:56 179601-23-12.0 0.71 1
o-Xylene 0.97J ug/L 12/14/21 02:56 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)103 %12/14/21 02:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %12/14/21 02:56 17060-07-070-130 1
Toluene-d8 (S)102 %12/14/21 02:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:6 Lab ID:92577240002 Collected:12/10/21 11:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 12/13/21 13:57 83-32-912/13/21 05:118.3 1.7 1
Acenaphthylene ND ug/L 12/13/21 13:57 208-96-812/13/21 05:118.3 1.6 1
Aniline ND ug/L 12/13/21 13:57 62-53-312/13/21 05:118.3 1.4 1
Anthracene ND ug/L 12/13/21 13:57 120-12-712/13/21 05:118.3 1.9 1
Benzo(a)anthracene ND ug/L 12/13/21 13:57 56-55-312/13/21 05:118.3 2.2 1
Benzo(a)pyrene ND ug/L 12/13/21 13:57 50-32-812/13/21 05:118.3 2.3 1
Benzo(b)fluoranthene ND ug/L 12/13/21 13:57 205-99-212/13/21 05:118.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 12/13/21 13:57 191-24-212/13/21 05:118.3 2.4 1
Benzo(k)fluoranthene ND ug/L 12/13/21 13:57 207-08-912/13/21 05:118.3 2.3 1
Benzoic Acid ND ug/L 12/13/21 13:57 65-85-012/13/21 05:1141.7 2.8 1
Benzyl alcohol ND ug/L 12/13/21 13:57 100-51-612/13/21 05:1116.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 12/13/21 13:57 101-55-312/13/21 05:118.3 1.5 1
Butylbenzylphthalate ND ug/L 12/13/21 13:57 85-68-712/13/21 05:118.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 12/13/21 13:57 59-50-712/13/21 05:118.3 2.8 1
4-Chloroaniline ND ug/L 12/13/21 13:57 106-47-812/13/21 05:1116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 12/13/21 13:57 111-91-112/13/21 05:118.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 12/13/21 13:57 111-44-412/13/21 05:118.3 1.6 1
2-Chloronaphthalene ND ug/L 12/13/21 13:57 91-58-712/13/21 05:118.3 1.4 1
2-Chlorophenol ND ug/L 12/13/21 13:57 95-57-812/13/21 05:118.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 12/13/21 13:57 7005-72-312/13/21 05:118.3 1.7 1
Chrysene ND ug/L 12/13/21 13:57 218-01-912/13/21 05:118.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 12/13/21 13:57 53-70-312/13/21 05:118.3 2.5 1
Dibenzofuran ND ug/L 12/13/21 13:57 132-64-912/13/21 05:118.3 1.8 1
1,2-Dichlorobenzene ND ug/L 12/13/21 13:57 95-50-112/13/21 05:118.3 1.5 1
1,3-Dichlorobenzene ND ug/L 12/13/21 13:57 541-73-112/13/21 05:118.3 1.3 1
1,4-Dichlorobenzene ND ug/L 12/13/21 13:57 106-46-712/13/21 05:118.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 12/13/21 13:57 91-94-112/13/21 05:1116.7 6.8 1
2,4-Dichlorophenol ND ug/L 12/13/21 13:57 120-83-212/13/21 05:118.3 1.2 1
Diethylphthalate ND ug/L 12/13/21 13:57 84-66-212/13/21 05:118.3 1.7 1
2,4-Dimethylphenol ND ug/L 12/13/21 13:57 105-67-912/13/21 05:118.3 1.4 1
Dimethylphthalate ND ug/L 12/13/21 13:57 131-11-312/13/21 05:118.3 1.8 1
Di-n-butylphthalate ND ug/L 12/13/21 13:57 84-74-212/13/21 05:118.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 12/13/21 13:57 534-52-112/13/21 05:1116.7 2.8 1
2,4-Dinitrophenol ND ug/L 12/13/21 13:57 51-28-512/13/21 05:1141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 12/13/21 13:57 121-14-212/13/21 05:118.3 1.4 1
2,6-Dinitrotoluene ND ug/L 12/13/21 13:57 606-20-212/13/21 05:118.3 1.4 1
Di-n-octylphthalate ND ug/L 12/13/21 13:57 117-84-012/13/21 05:118.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/13/21 13:57 117-81-712/13/21 05:115.0 3.1 1
Fluoranthene ND ug/L 12/13/21 13:57 206-44-012/13/21 05:118.3 1.8 1
Fluorene ND ug/L 12/13/21 13:57 86-73-712/13/21 05:118.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 12/13/21 13:57 87-68-312/13/21 05:118.3 1.5 1
Hexachlorobenzene ND ug/L 12/13/21 13:57 118-74-112/13/21 05:118.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 12/13/21 13:57 77-47-412/13/21 05:118.3 1.3 1
Hexachloroethane ND ug/L 12/13/21 13:57 67-72-112/13/21 05:118.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 12/13/21 13:57 193-39-512/13/21 05:118.3 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:6 Lab ID:92577240002 Collected:12/10/21 11:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 12/13/21 13:57 78-59-112/13/21 05:118.3 1.4 1
1-Methylnaphthalene ND ug/L 12/13/21 13:57 90-12-012/13/21 05:118.3 1.7 1
2-Methylnaphthalene ND ug/L 12/13/21 13:57 91-57-612/13/21 05:118.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 12/13/21 13:57 95-48-712/13/21 05:118.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/13/21 13:57 15831-10-412/13/21 05:118.3 1.0 1
Naphthalene ND ug/L 12/13/21 13:57 91-20-312/13/21 05:118.3 1.7 1
2-Nitroaniline ND ug/L 12/13/21 13:57 88-74-412/13/21 05:1116.7 2.5 1
3-Nitroaniline ND ug/L 12/13/21 13:57 99-09-212/13/21 05:1116.7 3.1 1
4-Nitroaniline ND ug/L 12/13/21 13:57 100-01-612/13/21 05:1116.7 4.2 1
Nitrobenzene ND ug/L 12/13/21 13:57 98-95-312/13/21 05:118.3 1.6 1
2-Nitrophenol ND ug/L 12/13/21 13:57 88-75-512/13/21 05:118.3 1.2 1
4-Nitrophenol ND ug/L 12/13/21 13:57 100-02-712/13/21 05:1141.7 5.5 1
N-Nitrosodimethylamine ND ug/L 12/13/21 13:57 62-75-912/13/21 05:118.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 12/13/21 13:57 621-64-712/13/21 05:118.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 12/13/21 13:57 86-30-612/13/21 05:118.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 12/13/21 13:57 108-60-112/13/21 05:118.3 0.96 1
Pentachlorophenol ND ug/L 12/13/21 13:57 87-86-512/13/21 05:1116.7 3.1 1
Phenanthrene ND ug/L 12/13/21 13:57 85-01-812/13/21 05:118.3 1.7 1
Phenol ND ug/L 12/13/21 13:57 108-95-212/13/21 05:118.3 1.1 1
Pyrene ND ug/L 12/13/21 13:57 129-00-012/13/21 05:118.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 12/13/21 13:57 120-82-112/13/21 05:118.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 12/13/21 13:57 95-95-412/13/21 05:118.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 12/13/21 13:57 88-06-212/13/21 05:118.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)85 %12/13/21 13:57 4165-60-012/13/21 05:1110-144 1
2-Fluorobiphenyl (S)68 %12/13/21 13:57 321-60-812/13/21 05:1110-130 1
Terphenyl-d14 (S)76 %12/13/21 13:57 1718-51-012/13/21 05:1134-163 1
Phenol-d6 (S)44 %12/13/21 13:57 13127-88-312/13/21 05:1110-130 1
2-Fluorophenol (S)59 %12/13/21 13:57 367-12-412/13/21 05:1110-130 1
2,4,6-Tribromophenol (S)89 %12/13/21 13:57 118-79-612/13/21 05:1110-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 12/14/21 03:14 67-64-125.0 5.1 1
Benzene ND ug/L 12/14/21 03:14 71-43-21.0 0.34 1
Bromobenzene ND ug/L 12/14/21 03:14 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 12/14/21 03:14 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 12/14/21 03:14 75-27-41.0 0.31 1
Bromoform ND ug/L 12/14/21 03:14 75-25-21.0 0.34 1
Bromomethane ND ug/L 12/14/21 03:14 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 12/14/21 03:14 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 12/14/21 03:14 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 12/14/21 03:14 108-90-71.0 0.28 1
Chloroethane ND ug/L 12/14/21 03:14 75-00-3 IL1.0 0.65 1
Chloroform ND ug/L 12/14/21 03:14 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:6 Lab ID:92577240002 Collected:12/10/21 11:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 12/14/21 03:14 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/14/21 03:14 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 12/14/21 03:14 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/21 03:14 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 12/14/21 03:14 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/21 03:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/14/21 03:14 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 12/14/21 03:14 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 12/14/21 03:14 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 12/14/21 03:14 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 12/14/21 03:14 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 12/14/21 03:14 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 12/14/21 03:14 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 12/14/21 03:14 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/14/21 03:14 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/14/21 03:14 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 12/14/21 03:14 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 12/14/21 03:14 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/14/21 03:14 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 12/14/21 03:14 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/14/21 03:14 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/14/21 03:14 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 12/14/21 03:14 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 12/14/21 03:14 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/14/21 03:14 87-68-32.0 1.5 1
2-Hexanone ND ug/L 12/14/21 03:14 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 12/14/21 03:14 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 12/14/21 03:14 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/14/21 03:14 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 12/14/21 03:14 1634-04-41.0 0.42 1
Naphthalene ND ug/L 12/14/21 03:14 91-20-31.0 0.64 1
Styrene ND ug/L 12/14/21 03:14 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/21 03:14 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/14/21 03:14 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/14/21 03:14 127-18-41.0 0.29 1
Toluene ND ug/L 12/14/21 03:14 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 12/14/21 03:14 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/14/21 03:14 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/14/21 03:14 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 12/14/21 03:14 79-00-51.0 0.32 1
Trichloroethene ND ug/L 12/14/21 03:14 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 12/14/21 03:14 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/14/21 03:14 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 12/14/21 03:14 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 12/14/21 03:14 75-01-41.0 0.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:6 Lab ID:92577240002 Collected:12/10/21 11:00 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 12/14/21 03:14 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 12/14/21 03:14 179601-23-12.0 0.71 1
o-Xylene ND ug/L 12/14/21 03:14 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)103 %12/14/21 03:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %12/14/21 03:14 17060-07-070-130 1
Toluene-d8 (S)99 %12/14/21 03:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:2 Lab ID:92577240003 Collected:12/10/21 10:15 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 29.8 ug/L 12/14/21 03:32 67-64-125.0 5.1 1
Benzene ND ug/L 12/14/21 03:32 71-43-21.0 0.34 1
Bromobenzene ND ug/L 12/14/21 03:32 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 12/14/21 03:32 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 12/14/21 03:32 75-27-41.0 0.31 1
Bromoform ND ug/L 12/14/21 03:32 75-25-21.0 0.34 1
Bromomethane ND ug/L 12/14/21 03:32 74-83-92.0 1.7 1
2-Butanone (MEK)11.1 ug/L 12/14/21 03:32 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 12/14/21 03:32 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 12/14/21 03:32 108-90-71.0 0.28 1
Chloroethane ND ug/L 12/14/21 03:32 75-00-3 IL1.0 0.65 1
Chloroform ND ug/L 12/14/21 03:32 67-66-31.0 0.43 1
Chloromethane ND ug/L 12/14/21 03:32 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/14/21 03:32 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 12/14/21 03:32 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/21 03:32 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 12/14/21 03:32 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/21 03:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/14/21 03:32 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 12/14/21 03:32 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 12/14/21 03:32 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 12/14/21 03:32 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 12/14/21 03:32 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 12/14/21 03:32 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 12/14/21 03:32 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 12/14/21 03:32 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/14/21 03:32 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/14/21 03:32 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 12/14/21 03:32 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 12/14/21 03:32 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/14/21 03:32 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 12/14/21 03:32 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/14/21 03:32 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/14/21 03:32 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 12/14/21 03:32 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 12/14/21 03:32 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/14/21 03:32 87-68-32.0 1.5 1
2-Hexanone ND ug/L 12/14/21 03:32 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 12/14/21 03:32 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 12/14/21 03:32 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/14/21 03:32 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 12/14/21 03:32 1634-04-41.0 0.42 1
Naphthalene ND ug/L 12/14/21 03:32 91-20-31.0 0.64 1
Styrene ND ug/L 12/14/21 03:32 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/21 03:32 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:2 Lab ID:92577240003 Collected:12/10/21 10:15 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 12/14/21 03:32 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/14/21 03:32 127-18-41.0 0.29 1
Toluene ND ug/L 12/14/21 03:32 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 12/14/21 03:32 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/14/21 03:32 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/14/21 03:32 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 12/14/21 03:32 79-00-51.0 0.32 1
Trichloroethene ND ug/L 12/14/21 03:32 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 12/14/21 03:32 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/14/21 03:32 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 12/14/21 03:32 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 12/14/21 03:32 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 12/14/21 03:32 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 12/14/21 03:32 179601-23-12.0 0.71 1
o-Xylene ND ug/L 12/14/21 03:32 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)102 %12/14/21 03:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %12/14/21 03:32 17060-07-070-130 1
Toluene-d8 (S)100 %12/14/21 03:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:4 Lab ID:92577240004 Collected:12/10/21 10:30 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 12/14/21 03:50 67-64-125.0 5.1 1
Benzene ND ug/L 12/14/21 03:50 71-43-21.0 0.34 1
Bromobenzene ND ug/L 12/14/21 03:50 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 12/14/21 03:50 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 12/14/21 03:50 75-27-41.0 0.31 1
Bromoform ND ug/L 12/14/21 03:50 75-25-21.0 0.34 1
Bromomethane ND ug/L 12/14/21 03:50 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 12/14/21 03:50 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 12/14/21 03:50 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 12/14/21 03:50 108-90-71.0 0.28 1
Chloroethane ND ug/L 12/14/21 03:50 75-00-3 IL1.0 0.65 1
Chloroform ND ug/L 12/14/21 03:50 67-66-31.0 0.43 1
Chloromethane ND ug/L 12/14/21 03:50 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/14/21 03:50 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 12/14/21 03:50 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/21 03:50 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 12/14/21 03:50 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/21 03:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/14/21 03:50 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 12/14/21 03:50 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 12/14/21 03:50 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 12/14/21 03:50 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 12/14/21 03:50 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 12/14/21 03:50 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 12/14/21 03:50 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 12/14/21 03:50 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/14/21 03:50 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/14/21 03:50 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 12/14/21 03:50 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 12/14/21 03:50 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/14/21 03:50 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 12/14/21 03:50 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/14/21 03:50 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/14/21 03:50 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 12/14/21 03:50 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 12/14/21 03:50 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/14/21 03:50 87-68-32.0 1.5 1
2-Hexanone ND ug/L 12/14/21 03:50 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 12/14/21 03:50 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 12/14/21 03:50 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/14/21 03:50 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 12/14/21 03:50 1634-04-41.0 0.42 1
Naphthalene ND ug/L 12/14/21 03:50 91-20-31.0 0.64 1
Styrene ND ug/L 12/14/21 03:50 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/21 03:50 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:4 Lab ID:92577240004 Collected:12/10/21 10:30 Received:12/10/21 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 12/14/21 03:50 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/14/21 03:50 127-18-41.0 0.29 1
Toluene ND ug/L 12/14/21 03:50 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 12/14/21 03:50 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/14/21 03:50 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/14/21 03:50 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 12/14/21 03:50 79-00-51.0 0.32 1
Trichloroethene ND ug/L 12/14/21 03:50 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 12/14/21 03:50 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/14/21 03:50 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 12/14/21 03:50 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 12/14/21 03:50 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 12/14/21 03:50 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 12/14/21 03:50 179601-23-12.0 0.71 1
o-Xylene ND ug/L 12/14/21 03:50 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)104 %12/14/21 03:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %12/14/21 03:50 17060-07-070-130 1
Toluene-d8 (S)100 %12/14/21 03:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:S-1 Lab ID:92577240005 Collected:12/09/21 13:30 Received:12/10/21 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 12/15/21 10:57 83-32-912/11/21 13:483961391
Acenaphthylene ND ug/kg 12/15/21 10:57 208-96-812/11/21 13:483961391
Aniline ND ug/kg 12/15/21 10:57 62-53-312/11/21 13:483961551
Anthracene ND ug/kg 12/15/21 10:57 120-12-712/11/21 13:483961301
Benzo(a)anthracene ND ug/kg 12/15/21 10:57 56-55-312/11/21 13:483961321
Benzo(a)pyrene ND ug/kg 12/15/21 10:57 50-32-812/11/21 13:483961371
Benzo(b)fluoranthene ND ug/kg 12/15/21 10:57 205-99-212/11/21 13:483961321
Benzo(g,h,i)perylene ND ug/kg 12/15/21 10:57 191-24-212/11/21 13:483961541
Benzo(k)fluoranthene ND ug/kg 12/15/21 10:57 207-08-912/11/21 13:483961391
Benzoic Acid ND ug/kg 12/15/21 10:57 65-85-012/11/21 13:4819808511
Benzyl alcohol ND ug/kg 12/15/21 10:57 100-51-612/11/21 13:487923001
4-Bromophenylphenyl ether ND ug/kg 12/15/21 10:57 101-55-312/11/21 13:483961521
Butylbenzylphthalate ND ug/kg 12/15/21 10:57 85-68-712/11/21 13:483961671
4-Chloro-3-methylphenol ND ug/kg 12/15/21 10:57 59-50-712/11/21 13:487922791
4-Chloroaniline ND ug/kg 12/15/21 10:57 106-47-812/11/21 13:487923111
bis(2-Chloroethoxy)methane ND ug/kg 12/15/21 10:57 111-91-112/11/21 13:483961651
bis(2-Chloroethyl) ether ND ug/kg 12/15/21 10:57 111-44-412/11/21 13:483961491
2-Chloronaphthalene ND ug/kg 12/15/21 10:57 91-58-712/11/21 13:483961571
2-Chlorophenol ND ug/kg 12/15/21 10:57 95-57-812/11/21 13:483961491
4-Chlorophenylphenyl ether ND ug/kg 12/15/21 10:57 7005-72-312/11/21 13:483961481
Chrysene ND ug/kg 12/15/21 10:57 218-01-912/11/21 13:483961441
Dibenz(a,h)anthracene ND ug/kg 12/15/21 10:57 53-70-312/11/21 13:483961521
Dibenzofuran ND ug/kg 12/15/21 10:57 132-64-912/11/21 13:483961431
1,2-Dichlorobenzene ND ug/kg 12/15/21 10:57 95-50-112/11/21 13:483961431
1,3-Dichlorobenzene ND ug/kg 12/15/21 10:57 541-73-112/11/21 13:483961401
1,4-Dichlorobenzene ND ug/kg 12/15/21 10:57 106-46-712/11/21 13:483961511
3,3'-Dichlorobenzidine ND ug/kg 12/15/21 10:57 91-94-1 IL12/11/21 13:487922681
2,4-Dichlorophenol ND ug/kg 12/15/21 10:57 120-83-212/11/21 13:483961551
Diethylphthalate ND ug/kg 12/15/21 10:57 84-66-212/11/21 13:483961451
2,4-Dimethylphenol ND ug/kg 12/15/21 10:57 105-67-912/11/21 13:483961651
Dimethylphthalate ND ug/kg 12/15/21 10:57 131-11-312/11/21 13:483961441
Di-n-butylphthalate ND ug/kg 12/15/21 10:57 84-74-212/11/21 13:483961331
4,6-Dinitro-2-methylphenol ND ug/kg 12/15/21 10:57 534-52-1 v112/11/21 13:487923701
2,4-Dinitrophenol ND ug/kg 12/15/21 10:57 51-28-5 v112/11/21 13:48198012201
2,4-Dinitrotoluene ND ug/kg 12/15/21 10:57 121-14-212/11/21 13:483961521
2,6-Dinitrotoluene ND ug/kg 12/15/21 10:57 606-20-212/11/21 13:483961451
Di-n-octylphthalate ND ug/kg 12/15/21 10:57 117-84-012/11/21 13:483961561
bis(2-Ethylhexyl)phthalate ND ug/kg 12/15/21 10:57 117-81-712/11/21 13:483961541
Fluoranthene ND ug/kg 12/15/21 10:57 206-44-012/11/21 13:483961361
Fluorene ND ug/kg 12/15/21 10:57 86-73-712/11/21 13:483961391
Hexachloro-1,3-butadiene ND ug/kg 12/15/21 10:57 87-68-3 v112/11/21 13:483961721
Hexachlorobenzene ND ug/kg 12/15/21 10:57 118-74-112/11/21 13:483961551
Hexachlorocyclopentadiene ND ug/kg 12/15/21 10:57 77-47-412/11/21 13:483962271
Hexachloroethane ND ug/kg 12/15/21 10:57 67-72-112/11/21 13:483961511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:S-1 Lab ID:92577240005 Collected:12/09/21 13:30 Received:12/10/21 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 12/15/21 10:57 193-39-512/11/21 13:483961561
Isophorone ND ug/kg 12/15/21 10:57 78-59-112/11/21 13:483961771
1-Methylnaphthalene 282J ug/kg 12/15/21 10:57 90-12-012/11/21 13:483961391
2-Methylnaphthalene 357J ug/kg 12/15/21 10:57 91-57-612/11/21 13:483961581
2-Methylphenol(o-Cresol)ND ug/kg 12/15/21 10:57 95-48-712/11/21 13:483961621
3&4-Methylphenol(m&p Cresol)ND ug/kg 12/15/21 10:57 15831-10-412/11/21 13:483961601
Naphthalene ND ug/kg 12/15/21 10:57 91-20-312/11/21 13:483961341
2-Nitroaniline ND ug/kg 12/15/21 10:57 88-74-412/11/21 13:4819803241
3-Nitroaniline ND ug/kg 12/15/21 10:57 99-09-2 IL12/11/21 13:4819803111
4-Nitroaniline ND ug/kg 12/15/21 10:57 100-01-612/11/21 13:487923011
Nitrobenzene ND ug/kg 12/15/21 10:57 98-95-312/11/21 13:483961841
2-Nitrophenol ND ug/kg 12/15/21 10:57 88-75-512/11/21 13:483961721
4-Nitrophenol ND ug/kg 12/15/21 10:57 100-02-712/11/21 13:4819807661
N-Nitrosodimethylamine ND ug/kg 12/15/21 10:57 62-75-912/11/21 13:483961331
N-Nitroso-di-n-propylamine ND ug/kg 12/15/21 10:57 621-64-712/11/21 13:483961491
N-Nitrosodiphenylamine ND ug/kg 12/15/21 10:57 86-30-612/11/21 13:483961401
2,2'-Oxybis(1-chloropropane)ND ug/kg 12/15/21 10:57 108-60-112/11/21 13:483961891
Pentachlorophenol ND ug/kg 12/15/21 10:57 87-86-512/11/21 13:487923881
Phenanthrene ND ug/kg 12/15/21 10:57 85-01-812/11/21 13:483961301
Phenol ND ug/kg 12/15/21 10:57 108-95-212/11/21 13:483961771
Pyrene ND ug/kg 12/15/21 10:57 129-00-012/11/21 13:483961611
Pyridine ND ug/kg 12/15/21 10:57 110-86-112/11/21 13:483961251
1,2,4-Trichlorobenzene ND ug/kg 12/15/21 10:57 120-82-112/11/21 13:483961561
2,4,5-Trichlorophenol ND ug/kg 12/15/21 10:57 95-95-412/11/21 13:483961811
2,4,6-Trichlorophenol ND ug/kg 12/15/21 10:57 88-06-212/11/21 13:483961631
Surrogates
Nitrobenzene-d5 (S)65 %12/15/21 10:57 4165-60-012/11/21 13:4821-130 1
2-Fluorobiphenyl (S)66 %12/15/21 10:57 321-60-812/11/21 13:4819-130 1
Terphenyl-d14 (S)50 %12/15/21 10:57 1718-51-012/11/21 13:4815-130 1
Phenol-d6 (S)60 %12/15/21 10:57 13127-88-312/11/21 13:4818-130 1
2-Fluorophenol (S)62 %12/15/21 10:57 367-12-412/11/21 13:4818-130 1
2,4,6-Tribromophenol (S)65 %12/15/21 10:57 118-79-612/11/21 13:4818-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 12/12/21 22:17 67-64-112/12/21 15:1112139.0 1
Benzene 3.8J ug/kg 12/12/21 22:17 71-43-212/12/21 15:116.1 2.4 1
Bromobenzene ND ug/kg 12/12/21 22:17 108-86-112/12/21 15:116.1 2.0 1
Bromochloromethane ND ug/kg 12/12/21 22:17 74-97-512/12/21 15:116.1 1.8 1
Bromodichloromethane ND ug/kg 12/12/21 22:17 75-27-412/12/21 15:116.1 2.3 1
Bromoform ND ug/kg 12/12/21 22:17 75-25-2 v112/12/21 15:116.1 2.1 1
Bromomethane ND ug/kg 12/12/21 22:17 74-83-9 IK12/12/21 15:1112.1 9.6 1
2-Butanone (MEK)ND ug/kg 12/12/21 22:17 78-93-312/12/21 15:1112129.1 1
n-Butylbenzene ND ug/kg 12/12/21 22:17 104-51-812/12/21 15:116.1 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:S-1 Lab ID:92577240005 Collected:12/09/21 13:30 Received:12/10/21 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene 749 ug/kg 12/12/21 22:17 135-98-812/12/21 15:116.1 2.7 1
tert-Butylbenzene ND ug/kg 12/12/21 22:17 98-06-612/12/21 15:116.1 2.2 1
Carbon tetrachloride ND ug/kg 12/12/21 22:17 56-23-512/12/21 15:116.1 2.3 1
Chlorobenzene ND ug/kg 12/12/21 22:17 108-90-712/12/21 15:116.1 1.2 1
Chloroethane ND ug/kg 12/12/21 22:17 75-00-312/12/21 15:1112.1 4.7 1
Chloroform ND ug/kg 12/12/21 22:17 67-66-3 v212/12/21 15:116.1 3.7 1
Chloromethane ND ug/kg 12/12/21 22:17 74-87-312/12/21 15:1112.1 5.1 1
2-Chlorotoluene ND ug/kg 12/12/21 22:17 95-49-812/12/21 15:116.1 2.1 1
4-Chlorotoluene ND ug/kg 12/12/21 22:17 106-43-412/12/21 15:116.1 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 12/12/21 22:17 96-12-812/12/21 15:116.1 2.4 1
Dibromochloromethane ND ug/kg 12/12/21 22:17 124-48-112/12/21 15:116.1 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 12/12/21 22:17 106-93-412/12/21 15:116.1 2.7 1
Dibromomethane ND ug/kg 12/12/21 22:17 74-95-312/12/21 15:116.1 1.3 1
1,2-Dichlorobenzene ND ug/kg 12/12/21 22:17 95-50-112/12/21 15:116.1 2.2 1
1,3-Dichlorobenzene ND ug/kg 12/12/21 22:17 541-73-112/12/21 15:116.1 1.9 1
1,4-Dichlorobenzene ND ug/kg 12/12/21 22:17 106-46-712/12/21 15:116.1 1.6 1
Dichlorodifluoromethane ND ug/kg 12/12/21 22:17 75-71-812/12/21 15:1112.1 2.6 1
1,1-Dichloroethane ND ug/kg 12/12/21 22:17 75-34-312/12/21 15:116.1 2.5 1
1,2-Dichloroethane ND ug/kg 12/12/21 22:17 107-06-212/12/21 15:116.1 4.0 1
1,1-Dichloroethene ND ug/kg 12/12/21 22:17 75-35-412/12/21 15:116.1 2.5 1
cis-1,2-Dichloroethene ND ug/kg 12/12/21 22:17 156-59-212/12/21 15:116.1 2.1 1
trans-1,2-Dichloroethene ND ug/kg 12/12/21 22:17 156-60-512/12/21 15:116.1 2.1 1
1,2-Dichloropropane ND ug/kg 12/12/21 22:17 78-87-512/12/21 15:116.1 1.8 1
1,3-Dichloropropane ND ug/kg 12/12/21 22:17 142-28-912/12/21 15:116.1 1.9 1
2,2-Dichloropropane ND ug/kg 12/12/21 22:17 594-20-712/12/21 15:116.1 2.0 1
1,1-Dichloropropene ND ug/kg 12/12/21 22:17 563-58-612/12/21 15:116.1 2.9 1
cis-1,3-Dichloropropene ND ug/kg 12/12/21 22:17 10061-01-512/12/21 15:116.1 1.7 1
trans-1,3-Dichloropropene ND ug/kg 12/12/21 22:17 10061-02-612/12/21 15:116.1 2.1 1
Diisopropyl ether ND ug/kg 12/12/21 22:17 108-20-312/12/21 15:116.1 1.6 1
Ethylbenzene 15.9 ug/kg 12/12/21 22:17 100-41-412/12/21 15:116.1 2.8 1
Hexachloro-1,3-butadiene ND ug/kg 12/12/21 22:17 87-68-312/12/21 15:1112.1 9.9 1
2-Hexanone ND ug/kg 12/12/21 22:17 591-78-612/12/21 15:1160.7 5.9 1
Isopropylbenzene (Cumene)58.0 ug/kg 12/12/21 22:17 98-82-812/12/21 15:116.1 2.1 1
p-Isopropyltoluene ND ug/kg 12/12/21 22:17 99-87-612/12/21 15:116.1 3.0 1
Methylene Chloride ND ug/kg 12/12/21 22:17 75-09-212/12/21 15:1124.3 16.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 12/12/21 22:17 108-10-112/12/21 15:1160.7 5.9 1
Methyl-tert-butyl ether ND ug/kg 12/12/21 22:17 1634-04-412/12/21 15:116.1 2.3 1
Naphthalene 561 ug/kg 12/12/21 22:17 91-20-312/12/21 15:116.1 3.2 1
n-Propylbenzene ND ug/kg 12/12/21 22:17 103-65-112/12/21 15:116.1 2.2 1
Styrene ND ug/kg 12/12/21 22:17 100-42-512/12/21 15:116.1 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 12/12/21 22:17 630-20-612/12/21 15:116.1 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 12/12/21 22:17 79-34-512/12/21 15:116.1 1.6 1
Tetrachloroethene ND ug/kg 12/12/21 22:17 127-18-412/12/21 15:116.1 1.9 1
Toluene 27.8 ug/kg 12/12/21 22:17 108-88-312/12/21 15:116.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92577240
21-418
Sample:S-1 Lab ID:92577240005 Collected:12/09/21 13:30 Received:12/10/21 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 12/12/21 22:17 87-61-612/12/21 15:116.1 4.9 1
1,2,4-Trichlorobenzene ND ug/kg 12/12/21 22:17 120-82-112/12/21 15:116.1 5.1 1
1,1,1-Trichloroethane ND ug/kg 12/12/21 22:17 71-55-612/12/21 15:116.1 3.2 1
1,1,2-Trichloroethane ND ug/kg 12/12/21 22:17 79-00-512/12/21 15:116.1 2.0 1
Trichloroethene ND ug/kg 12/12/21 22:17 79-01-612/12/21 15:116.1 1.6 1
Trichlorofluoromethane ND ug/kg 12/12/21 22:17 75-69-412/12/21 15:116.1 3.3 1
1,2,3-Trichloropropane ND ug/kg 12/12/21 22:17 96-18-412/12/21 15:116.1 3.1 1
1,2,4-Trimethylbenzene 546 ug/kg 12/12/21 22:17 95-63-612/12/21 15:116.1 1.7 1
1,3,5-Trimethylbenzene 372 ug/kg 12/12/21 22:17 108-67-812/12/21 15:116.1 2.0 1
Vinyl acetate ND ug/kg 12/12/21 22:17 108-05-412/12/21 15:1160.7 4.4 1
Vinyl chloride ND ug/kg 12/12/21 22:17 75-01-412/12/21 15:1112.1 3.1 1
Xylene (Total)104 ug/kg 12/12/21 22:17 1330-20-712/12/21 15:1112.1 3.5 1
m&p-Xylene 66.1 ug/kg 12/12/21 22:17 179601-23-112/12/21 15:1112.1 4.2 1
o-Xylene 38.1 ug/kg 12/12/21 22:17 95-47-612/12/21 15:116.1 2.7 1
Surrogates
Toluene-d8 (S)98 %12/12/21 22:17 2037-26-512/12/21 15:1170-130 1
4-Bromofluorobenzene (S)113 %12/12/21 22:17 460-00-412/12/21 15:1169-134 1
1,2-Dichloroethane-d4 (S)91 %12/12/21 22:17 17060-07-012/12/21 15:1170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.6 %12/13/21 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
665553
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92577240005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3486721
Associated Lab Samples:92577240005
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 12/12/21 18:151.9
1,1,1-Trichloroethane ug/kg ND 5.0 12/12/21 18:152.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 12/12/21 18:151.3
1,1,2-Trichloroethane ug/kg ND 5.0 12/12/21 18:151.7
1,1-Dichloroethane ug/kg ND 5.0 12/12/21 18:152.1
1,1-Dichloroethene ug/kg ND 5.0 12/12/21 18:152.1
1,1-Dichloropropene ug/kg ND 5.0 12/12/21 18:152.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 12/12/21 18:154.0
1,2,3-Trichloropropane ug/kg ND 5.0 12/12/21 18:152.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 12/12/21 18:154.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 12/12/21 18:151.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 12/12/21 18:151.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 12/12/21 18:152.2
1,2-Dichlorobenzene ug/kg ND 5.0 12/12/21 18:151.8
1,2-Dichloroethane ug/kg ND 5.0 12/12/21 18:153.3
1,2-Dichloropropane ug/kg ND 5.0 12/12/21 18:151.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 12/12/21 18:151.7
1,3-Dichlorobenzene ug/kg ND 5.0 12/12/21 18:151.6
1,3-Dichloropropane ug/kg ND 5.0 12/12/21 18:151.6
1,4-Dichlorobenzene ug/kg ND 5.0 12/12/21 18:151.3
2,2-Dichloropropane ug/kg ND 5.0 12/12/21 18:151.6
2-Butanone (MEK)ug/kg ND 100 12/12/21 18:1524.0
2-Chlorotoluene ug/kg ND 5.0 12/12/21 18:151.8
2-Hexanone ug/kg ND 50.0 12/12/21 18:154.8
4-Chlorotoluene ug/kg ND 5.0 12/12/21 18:150.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 12/12/21 18:154.8
Acetone ug/kg ND 100 12/12/21 18:1532.1
Benzene ug/kg ND 5.0 12/12/21 18:152.0
Bromobenzene ug/kg ND 5.0 12/12/21 18:151.6
Bromochloromethane ug/kg ND 5.0 12/12/21 18:151.5
Bromodichloromethane ug/kg ND 5.0 12/12/21 18:151.9
Bromoform ug/kg ND 5.0 v112/12/21 18:151.8
Bromomethane ug/kg ND 10.0 IK12/12/21 18:157.9
Carbon tetrachloride ug/kg ND 5.0 12/12/21 18:151.9
Chlorobenzene ug/kg ND 5.0 12/12/21 18:150.96
Chloroethane ug/kg ND 10.0 12/12/21 18:153.9
Chloroform ug/kg ND 5.0 v212/12/21 18:153.0
Chloromethane ug/kg ND 10.0 12/12/21 18:154.2
cis-1,2-Dichloroethene ug/kg ND 5.0 12/12/21 18:151.7
cis-1,3-Dichloropropene ug/kg ND 5.0 12/12/21 18:151.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3486721
Associated Lab Samples:92577240005
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 12/12/21 18:152.8
Dibromomethane ug/kg ND 5.0 12/12/21 18:151.1
Dichlorodifluoromethane ug/kg ND 10.0 12/12/21 18:152.2
Diisopropyl ether ug/kg ND 5.0 12/12/21 18:151.4
Ethylbenzene ug/kg ND 5.0 12/12/21 18:152.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 12/12/21 18:158.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 12/12/21 18:151.7
m&p-Xylene ug/kg ND 10.0 12/12/21 18:153.4
Methyl-tert-butyl ether ug/kg ND 5.0 12/12/21 18:151.9
Methylene Chloride ug/kg ND 20.0 12/12/21 18:1513.7
n-Butylbenzene ug/kg ND 5.0 12/12/21 18:152.4
n-Propylbenzene ug/kg ND 5.0 12/12/21 18:151.8
Naphthalene ug/kg ND 5.0 12/12/21 18:152.6
o-Xylene ug/kg ND 5.0 12/12/21 18:152.2
p-Isopropyltoluene ug/kg ND 5.0 12/12/21 18:152.5
sec-Butylbenzene ug/kg ND 5.0 12/12/21 18:152.2
Styrene ug/kg ND 5.0 12/12/21 18:151.3
tert-Butylbenzene ug/kg ND 5.0 12/12/21 18:151.8
Tetrachloroethene ug/kg ND 5.0 12/12/21 18:151.6
Toluene ug/kg ND 5.0 12/12/21 18:151.4
trans-1,2-Dichloroethene ug/kg ND 5.0 12/12/21 18:151.8
trans-1,3-Dichloropropene ug/kg ND 5.0 12/12/21 18:151.7
Trichloroethene ug/kg ND 5.0 12/12/21 18:151.3
Trichlorofluoromethane ug/kg ND 5.0 12/12/21 18:152.8
Vinyl acetate ug/kg ND 50.0 12/12/21 18:153.6
Vinyl chloride ug/kg ND 10.0 12/12/21 18:152.5
Xylene (Total)ug/kg ND 10.0 12/12/21 18:152.8
1,2-Dichloroethane-d4 (S)%96 70-130 12/12/21 18:15
4-Bromofluorobenzene (S)%105 69-134 12/12/21 18:15
Toluene-d8 (S)%99 70-130 12/12/21 18:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486722LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13201250 105 70-130
1,1,1-Trichloroethane ug/kg 10601250 84 70-130
1,1,2,2-Tetrachloroethane ug/kg 12601250 101 70-130
1,1,2-Trichloroethane ug/kg 12001250 96 70-130
1,1-Dichloroethane ug/kg 11101250 89 70-130
1,1-Dichloroethene ug/kg 10901250 87 70-130
1,1-Dichloropropene ug/kg 10601250 85 70-130
1,2,3-Trichlorobenzene ug/kg 13001250 104 65-130
1,2,3-Trichloropropane ug/kg 12801250 102 70-130
1,2,4-Trichlorobenzene ug/kg 13001250 104 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486722LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13001250 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 12701250 102 70-130
1,2-Dibromoethane (EDB)ug/kg 12601250 101 70-130
1,2-Dichlorobenzene ug/kg 12701250 102 70-130
1,2-Dichloroethane ug/kg 10801250 86 63-130
1,2-Dichloropropane ug/kg 12601250 101 70-130
1,3,5-Trimethylbenzene ug/kg 13201250 106 70-130
1,3-Dichlorobenzene ug/kg 12901250 103 70-130
1,3-Dichloropropane ug/kg 12401250 99 70-130
1,4-Dichlorobenzene ug/kg 12601250 101 70-130
2,2-Dichloropropane ug/kg 11101250 89 66-130
2-Butanone (MEK)ug/kg 23402500 94 70-130
2-Chlorotoluene ug/kg 13201250 106 70-130
2-Hexanone ug/kg 29002500 116 70-130
4-Chlorotoluene ug/kg 12701250 101 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 27502500 110 70-130
Acetone ug/kg 24702500 99 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 12501250 100 70-130
Bromochloromethane ug/kg 10801250 87 70-130
Bromodichloromethane ug/kg 12801250 102 69-130
Bromoform ug/kg 1500 v1125012070-130
Bromomethane ug/kg 1230 IK12509952-130
Carbon tetrachloride ug/kg 12101250 97 70-130
Chlorobenzene ug/kg 12401250 100 70-130
Chloroethane ug/kg 11601250 93 65-130
Chloroform ug/kg 999 v312508070-130
Chloromethane ug/kg 11601250 93 55-130
cis-1,2-Dichloroethene ug/kg 11101250 88 70-130
cis-1,3-Dichloropropene ug/kg 12701250 102 70-130
Dibromochloromethane ug/kg 13701250 109 70-130
Dibromomethane ug/kg 12701250 102 70-130
Dichlorodifluoromethane ug/kg 11801250 95 45-156
Diisopropyl ether ug/kg 12001250 96 70-130
Ethylbenzene ug/kg 12101250 97 70-130
Hexachloro-1,3-butadiene ug/kg 12201250 98 66-130
Isopropylbenzene (Cumene)ug/kg 13101250 105 70-130
m&p-Xylene ug/kg 25902500 103 70-130
Methyl-tert-butyl ether ug/kg 10501250 84 70-130
Methylene Chloride ug/kg 12201250 98 65-130
n-Butylbenzene ug/kg 13001250 104 67-130
n-Propylbenzene ug/kg 12901250 103 70-130
Naphthalene ug/kg 12801250 102 70-130
o-Xylene ug/kg 13101250 105 70-130
p-Isopropyltoluene ug/kg 12701250 102 67-130
sec-Butylbenzene ug/kg 12901250 103 69-130
Styrene ug/kg 13801250 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486722LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12701250 101 67-130
Tetrachloroethene ug/kg 12401250 100 70-130
Toluene ug/kg 11901250 95 70-130
trans-1,2-Dichloroethene ug/kg 11001250 88 70-130
trans-1,3-Dichloropropene ug/kg 13001250 104 68-130
Trichloroethene ug/kg 11601250 93 70-130
Trichlorofluoromethane ug/kg 10701250 86 70-130
Vinyl acetate ug/kg 28102500 112 70-130
Vinyl chloride ug/kg 10901250 87 61-130
Xylene (Total)ug/kg 38903750 104 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%103 69-134
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3486724MATRIX SPIKE SAMPLE:
MSSpike
Result
92577299002
1,1,1,2-Tetrachloroethane ug/kg 12101300 93 70-131ND
1,1,1-Trichloroethane ug/kg 11201300 86 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 11901300 92 66-130ND
1,1,2-Trichloroethane ug/kg 12101300 93 66-133ND
1,1-Dichloroethane ug/kg 11701300 90 65-130ND
1,1-Dichloroethene ug/kg 12201300 94 10-158ND
1,1-Dichloropropene ug/kg 11901300 92 68-133ND
1,2,3-Trichlorobenzene ug/kg 14001300 108 27-138ND
1,2,3-Trichloropropane ug/kg 11801300 91 67-130ND
1,2,4-Trichlorobenzene ug/kg 14101300 108 51-134ND
1,2,4-Trimethylbenzene ug/kg 15401300 118 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 10501300 81 32-130ND
1,2-Dibromoethane (EDB)ug/kg 12501300 96 70-130ND
1,2-Dichlorobenzene ug/kg 13001300 100 69-130ND
1,2-Dichloroethane ug/kg 10101300 78 59-130ND
1,2-Dichloropropane ug/kg 12901300 99 70-130ND
1,3,5-Trimethylbenzene ug/kg 14701300 113 65-137ND
1,3-Dichlorobenzene ug/kg 13601300 104 70-130ND
1,3-Dichloropropane ug/kg 12601300 97 70-130ND
1,4-Dichlorobenzene ug/kg 12601300 97 68-130ND
2,2-Dichloropropane ug/kg 10701300 82 32-130ND
2-Butanone (MEK)ug/kg 21102600 81 10-136ND
2-Chlorotoluene ug/kg 13601300 105 69-141ND
2-Hexanone ug/kg 25402600 98 10-144ND
4-Chlorotoluene ug/kg 13001300 100 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 24102600 93 25-143ND
Acetone ug/kg 18302600 70 10-130ND
Benzene ug/kg 12901300 99 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3486724MATRIX SPIKE SAMPLE:
MSSpike
Result
92577299002
Bromobenzene ug/kg 12501300 96 70-130ND
Bromochloromethane ug/kg 10901300 84 69-134ND
Bromodichloromethane ug/kg 10801300 83 64-130ND
Bromoform ug/kg 1050 v113008062-130ND
Bromomethane ug/kg 818 IK13006320-176ND
Carbon tetrachloride ug/kg 10801300 83 65-140ND
Chlorobenzene ug/kg 13301300 103 70-130ND
Chloroethane ug/kg 4671300 36 10-130ND
Chloroform ug/kg 1040 v313008063-130ND
Chloromethane ug/kg 13301300 103 58-130ND
cis-1,2-Dichloroethene ug/kg 11501300 89 66-130ND
cis-1,3-Dichloropropene ug/kg 12001300 92 67-130ND
Dibromochloromethane ug/kg 10701300 83 67-130ND
Dibromomethane ug/kg 12201300 94 63-131ND
Dichlorodifluoromethane ug/kg 12301300 94 44-180ND
Diisopropyl ether ug/kg 12201300 94 63-130ND
Ethylbenzene ug/kg 13401300 103 66-130ND
Hexachloro-1,3-butadiene ug/kg 15101300 116 64-150ND
Isopropylbenzene (Cumene)ug/kg 14701300 113 69-135ND
m&p-Xylene ug/kg 28702600 110 60-133ND
Methyl-tert-butyl ether ug/kg 10801300 83 65-130ND
Methylene Chloride ug/kg 12101300 93 61-130ND
n-Butylbenzene ug/kg 14701300 113 65-140ND
n-Propylbenzene ug/kg 14201300 109 67-140ND
Naphthalene ug/kg 13601300 105 15-145ND
o-Xylene ug/kg 14201300 109 66-133ND
p-Isopropyltoluene ug/kg 14401300 110 56-147ND
sec-Butylbenzene ug/kg 14801300 113 65-139ND
Styrene ug/kg 13801300 106 70-132ND
tert-Butylbenzene ug/kg 14201300 109 62-135ND
Tetrachloroethene ug/kg 14201300 109 70-135ND
Toluene ug/kg 12901300 100 67-130ND
trans-1,2-Dichloroethene ug/kg 12201300 94 69-130ND
trans-1,3-Dichloropropene ug/kg 11601300 89 62-130ND
Trichloroethene ug/kg 12901300 99 70-135ND
Trichlorofluoromethane ug/kg 5851300 45 10-130ND
Vinyl acetate ug/kg 25202600 97 53-130ND
Vinyl chloride ug/kg 11701300 90 61-148ND
Xylene (Total)ug/kg 42903900 110 63-132ND
1,2-Dichloroethane-d4 (S)%83 70-130
4-Bromofluorobenzene (S)%103 69-134
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92577299001
3486723SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND v130ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND v230ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92577299001
3486723SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9090
4-Bromofluorobenzene (S)%103101
Toluene-d8 (S)%9899
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
665749
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92577240001, 92577240002, 92577240003, 92577240004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3487778
Associated Lab Samples:92577240001, 92577240002, 92577240003, 92577240004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/14/21 02:380.31
1,1,1-Trichloroethane ug/L ND 1.0 12/14/21 02:380.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/14/21 02:380.22
1,1,2-Trichloroethane ug/L ND 1.0 12/14/21 02:380.32
1,1-Dichloroethane ug/L ND 1.0 12/14/21 02:380.37
1,1-Dichloroethene ug/L ND 1.0 12/14/21 02:380.35
1,1-Dichloropropene ug/L ND 1.0 12/14/21 02:380.43
1,2,3-Trichlorobenzene ug/L ND 1.0 12/14/21 02:380.81
1,2,3-Trichloropropane ug/L ND 1.0 12/14/21 02:380.26
1,2,4-Trichlorobenzene ug/L ND 1.0 12/14/21 02:380.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 12/14/21 02:380.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/14/21 02:380.27
1,2-Dichlorobenzene ug/L ND 1.0 12/14/21 02:380.34
1,2-Dichloroethane ug/L ND 1.0 12/14/21 02:380.32
1,2-Dichloropropane ug/L ND 1.0 12/14/21 02:380.36
1,3-Dichlorobenzene ug/L ND 1.0 12/14/21 02:380.34
1,3-Dichloropropane ug/L ND 1.0 12/14/21 02:380.28
1,4-Dichlorobenzene ug/L ND 1.0 12/14/21 02:380.33
2,2-Dichloropropane ug/L ND 1.0 12/14/21 02:380.39
2-Butanone (MEK)ug/L ND 5.0 12/14/21 02:384.0
2-Chlorotoluene ug/L ND 1.0 12/14/21 02:380.32
2-Hexanone ug/L ND 5.0 12/14/21 02:380.48
4-Chlorotoluene ug/L ND 1.0 12/14/21 02:380.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 12/14/21 02:382.7
Acetone ug/L ND 25.0 12/14/21 02:385.1
Benzene ug/L ND 1.0 12/14/21 02:380.34
Bromobenzene ug/L ND 1.0 12/14/21 02:380.29
Bromochloromethane ug/L ND 1.0 12/14/21 02:380.47
Bromodichloromethane ug/L ND 1.0 12/14/21 02:380.31
Bromoform ug/L ND 1.0 12/14/21 02:380.34
Bromomethane ug/L ND 2.0 12/14/21 02:381.7
Carbon tetrachloride ug/L ND 1.0 12/14/21 02:380.33
Chlorobenzene ug/L ND 1.0 12/14/21 02:380.28
Chloroethane ug/L ND 1.0 IL12/14/21 02:380.65
Chloroform ug/L ND 1.0 12/14/21 02:380.43
Chloromethane ug/L ND 1.0 12/14/21 02:380.54
cis-1,2-Dichloroethene ug/L ND 1.0 12/14/21 02:380.38
cis-1,3-Dichloropropene ug/L ND 1.0 12/14/21 02:380.36
Dibromochloromethane ug/L ND 1.0 12/14/21 02:380.36
Dibromomethane ug/L ND 1.0 12/14/21 02:380.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3487778
Associated Lab Samples:92577240001, 92577240002, 92577240003, 92577240004
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 12/14/21 02:380.35
Diisopropyl ether ug/L ND 1.0 12/14/21 02:380.31
Ethylbenzene ug/L ND 1.0 12/14/21 02:380.30
Hexachloro-1,3-butadiene ug/L ND 2.0 12/14/21 02:381.5
m&p-Xylene ug/L ND 2.0 12/14/21 02:380.71
Methyl-tert-butyl ether ug/L ND 1.0 12/14/21 02:380.42
Methylene Chloride ug/L ND 5.0 12/14/21 02:382.0
Naphthalene ug/L ND 1.0 12/14/21 02:380.64
o-Xylene ug/L ND 1.0 12/14/21 02:380.34
p-Isopropyltoluene ug/L ND 1.0 12/14/21 02:380.41
Styrene ug/L ND 1.0 12/14/21 02:380.29
Tetrachloroethene ug/L ND 1.0 12/14/21 02:380.29
Toluene ug/L ND 1.0 12/14/21 02:380.48
trans-1,2-Dichloroethene ug/L ND 1.0 12/14/21 02:380.40
trans-1,3-Dichloropropene ug/L ND 1.0 12/14/21 02:380.36
Trichloroethene ug/L ND 1.0 12/14/21 02:380.38
Trichlorofluoromethane ug/L ND 1.0 12/14/21 02:380.30
Vinyl acetate ug/L ND 2.0 12/14/21 02:381.3
Vinyl chloride ug/L ND 1.0 12/14/21 02:380.39
Xylene (Total)ug/L ND 1.0 12/14/21 02:380.34
1,2-Dichloroethane-d4 (S)%108 70-130 12/14/21 02:38
4-Bromofluorobenzene (S)%101 70-130 12/14/21 02:38
Toluene-d8 (S)%101 70-130 12/14/21 02:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3487779LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.050 108 70-130
1,1,1-Trichloroethane ug/L 57.250 114 70-130
1,1,2,2-Tetrachloroethane ug/L 51.850 104 70-130
1,1,2-Trichloroethane ug/L 57.450 115 70-130
1,1-Dichloroethane ug/L 56.550 113 70-130
1,1-Dichloroethene ug/L 58.050 116 70-132
1,1-Dichloropropene ug/L 57.650 115 70-131
1,2,3-Trichlorobenzene ug/L 54.250 108 70-134
1,2,3-Trichloropropane ug/L 48.350 97 70-130
1,2,4-Trichlorobenzene ug/L 54.350 109 70-130
1,2-Dibromo-3-chloropropane ug/L 47.850 96 70-132
1,2-Dibromoethane (EDB)ug/L 53.250 106 70-130
1,2-Dichlorobenzene ug/L 56.550 113 70-130
1,2-Dichloroethane ug/L 55.450 111 70-130
1,2-Dichloropropane ug/L 57.050 114 70-130
1,3-Dichlorobenzene ug/L 56.650 113 70-130
1,3-Dichloropropane ug/L 53.250 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3487779LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 57.050 114 70-130
2,2-Dichloropropane ug/L 54.650 109 70-130
2-Butanone (MEK)ug/L 85.2100 85 70-133
2-Chlorotoluene ug/L 57.150 114 70-130
2-Hexanone ug/L 87.4100 87 70-130
4-Chlorotoluene ug/L 54.450 109 70-130
4-Methyl-2-pentanone (MIBK)ug/L 94.8100 95 70-130
Acetone ug/L 87.8100 88 70-144
Benzene ug/L 56.650 113 70-130
Bromobenzene ug/L 56.650 113 70-130
Bromochloromethane ug/L 57.650 115 70-130
Bromodichloromethane ug/L 57.550 115 70-130
Bromoform ug/L 50.250 100 70-131
Bromomethane ug/L 50.650 101 30-177
Carbon tetrachloride ug/L 56.150 112 70-130
Chlorobenzene ug/L 56.550 113 70-130
Chloroethane ug/L 47.2 IL509446-131
Chloroform ug/L 56.950 114 70-130
Chloromethane ug/L 51.350 103 49-130
cis-1,2-Dichloroethene ug/L 57.350 115 70-130
cis-1,3-Dichloropropene ug/L 56.550 113 70-130
Dibromochloromethane ug/L 54.750 109 70-130
Dibromomethane ug/L 54.150 108 70-130
Dichlorodifluoromethane ug/L 52.350 105 52-134
Diisopropyl ether ug/L 53.650 107 70-131
Ethylbenzene ug/L 56.650 113 70-130
Hexachloro-1,3-butadiene ug/L 53.050 106 70-131
m&p-Xylene ug/L 112100 112 70-130
Methyl-tert-butyl ether ug/L 55.650 111 70-130
Methylene Chloride ug/L 52.150 104 68-130
Naphthalene ug/L 52.650 105 70-133
o-Xylene ug/L 57.250 114 70-130
p-Isopropyltoluene ug/L 56.850 114 70-130
Styrene ug/L 57.450 115 70-130
Tetrachloroethene ug/L 51.550 103 70-130
Toluene ug/L 58.050 116 70-130
trans-1,2-Dichloroethene ug/L 58.150 116 70-130
trans-1,3-Dichloropropene ug/L 56.150 112 70-130
Trichloroethene ug/L 56.850 114 70-130
Trichlorofluoromethane ug/L 50.950 102 61-130
Vinyl acetate ug/L 119100 119 70-140
Vinyl chloride ug/L 55.750 111 59-142
Xylene (Total)ug/L 170150 113 70-130
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3487780MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92577080017
3487781
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 100 121 70-135119 2 30100ND121119
1,1,1-Trichloroethane ug/L 100 126 70-148124 2 30100ND126124
1,1,2,2-Tetrachloroethane ug/L 100 112 70-131110 2 30100ND112110
1,1,2-Trichloroethane ug/L 100 124 70-136118 5 30100ND124118
1,1-Dichloroethane ug/L 100 123 70-147121 2 30100ND123121
1,1-Dichloroethene ug/L 100 126 70-158121 4 30100ND126121
1,1-Dichloropropene ug/L 100 126 70-149123 2 30100ND126123
1,2,3-Trichlorobenzene ug/L 100 125 68-140125 0 30100ND125125
1,2,3-Trichloropropane ug/L 100 103 67-137106 3 30100ND103106
1,2,4-Trichlorobenzene ug/L 100 127 70-139127 0 30100ND127127
1,2-Dibromo-3-
chloropropane ug/L 100 97 69-136101 4 30100ND97.1 101
1,2-Dibromoethane (EDB)ug/L 100 117 70-137118 1 30100ND117118
1,2-Dichlorobenzene ug/L 100 121 70-133122 0 30100ND121122
1,2-Dichloroethane ug/L 100 119 67-138117 2 30100ND122119
1,2-Dichloropropane ug/L 100 123 70-138121 1 30100ND123121
1,3-Dichlorobenzene ug/L 100 125 70-133123 2 30100ND125123
1,3-Dichloropropane ug/L 100 118 70-136117 1 30100ND118117
1,4-Dichlorobenzene ug/L 100 125 70-133124 1 30100ND125124
2,2-Dichloropropane ug/L 100 128 52-155124 3 30100ND128124
2-Butanone (MEK)ug/L 200 92 61-14797 4 30200ND185193
2-Chlorotoluene ug/L 100 126 70-141127 1 30100ND126127
2-Hexanone ug/L 200 95 67-13998 4 30200ND189197
4-Chlorotoluene ug/L 100 117 70-135119 2 30100ND117119
4-Methyl-2-pentanone
(MIBK)ug/L 200 103 67-136104 1 30200ND206209
Acetone ug/L 200 96 55-15993 3 30200ND191185
Benzene ug/L 100 124 67-150118 5 30100ND124118
Bromobenzene ug/L 100 125 70-134125 0 30100ND125125
Bromochloromethane ug/L 100 117 70-146119 1 30100ND117119
Bromodichloromethane ug/L 100 124 70-138120 3 30100ND124120
Bromoform ug/L 100 105 57-138104 1 30100ND105104
Bromomethane ug/L 100 109 10-200112 2 30100ND109112
Carbon tetrachloride ug/L 100 122 70-147118 3 30100ND122118
Chlorobenzene ug/L 100 126 70-137125 1 30100ND126125
Chloroethane ug/L IL10013151-166128 2 30100ND131128
Chloroform ug/L 100 121 70-144121 0 30100ND121121
Chloromethane ug/L 100 93 24-16194 0 30100ND93.4 93.8
cis-1,2-Dichloroethene ug/L 100 124 67-148122 2 30100ND124122
cis-1,3-Dichloropropene ug/L 100 120 70-142119 1 30100ND120119
Dibromochloromethane ug/L 100 113 68-138116 3 30100ND113116
Dibromomethane ug/L 100 111 70-134112 1 30100ND111112
Dichlorodifluoromethane ug/L 100 88 43-15586 3 30100ND87.8 85.6
Diisopropyl ether ug/L 100 116 65-146116 1 301009.8 126 126
Ethylbenzene ug/L 100 127 68-143126 1 30100ND127126
Hexachloro-1,3-butadiene ug/L 100 139 62-151135 3 30100ND139135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3487780MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92577080017
3487781
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 200 126 53-157126 0 30200ND252251
Methyl-tert-butyl ether ug/L 100 88 59-15667 3 30100696785763
Methylene Chloride ug/L 100 107 64-148107 0 30100ND114114
Naphthalene ug/L 100 112 57-150113 0 30100ND112113
o-Xylene ug/L 100 126 68-143124 1 30100ND126124
p-Isopropyltoluene ug/L 100 133 70-141131 2 30100ND133131
Styrene ug/L 100 123 70-136121 2 30100ND123121
Tetrachloroethene ug/L 100 117 70-139117 0 30100ND117117
Toluene ug/L 100 126 47-157124 1 30100ND126124
trans-1,2-Dichloroethene ug/L 100 124 70-149123 1 30100ND124123
trans-1,3-Dichloropropene ug/L 100 122 70-138119 3 30100ND122119
Trichloroethene ug/L 100 118 70-149117 1 30100ND118117
Trichlorofluoromethane ug/L 100 113 61-154112 1 30100ND113112
Vinyl acetate ug/L 200 124 48-156124 0 30200ND249248
Vinyl chloride ug/L 100 113 55-172113 1 30100ND113113
Xylene (Total)ug/L 300 126 66-145125 1 30300ND379376
1,2-Dichloroethane-d4 (S)%96 70-13098
4-Bromofluorobenzene (S)%103 70-130102
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
665576
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92577240001, 92577240002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3486790
Associated Lab Samples:92577240001, 92577240002
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 12/13/21 12:301.7
1,2-Dichlorobenzene ug/L ND 10.0 12/13/21 12:301.8
1,3-Dichlorobenzene ug/L ND 10.0 12/13/21 12:301.6
1,4-Dichlorobenzene ug/L ND 10.0 12/13/21 12:301.7
1-Methylnaphthalene ug/L ND 10.0 12/13/21 12:302.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 12/13/21 12:301.2
2,4,5-Trichlorophenol ug/L ND 10.0 12/13/21 12:301.4
2,4,6-Trichlorophenol ug/L ND 10.0 12/13/21 12:301.6
2,4-Dichlorophenol ug/L ND 10.0 12/13/21 12:301.4
2,4-Dimethylphenol ug/L ND 10.0 12/13/21 12:301.7
2,4-Dinitrophenol ug/L ND 50.0 12/13/21 12:3026.0
2,4-Dinitrotoluene ug/L ND 10.0 12/13/21 12:301.6
2,6-Dinitrotoluene ug/L ND 10.0 12/13/21 12:301.7
2-Chloronaphthalene ug/L ND 10.0 12/13/21 12:301.7
2-Chlorophenol ug/L ND 10.0 12/13/21 12:301.2
2-Methylnaphthalene ug/L ND 10.0 12/13/21 12:301.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 12/13/21 12:301.9
2-Nitroaniline ug/L ND 20.0 12/13/21 12:303.0
2-Nitrophenol ug/L ND 10.0 12/13/21 12:301.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 12/13/21 12:301.2
3,3'-Dichlorobenzidine ug/L ND 20.0 12/13/21 12:308.1
3-Nitroaniline ug/L ND 20.0 12/13/21 12:303.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 12/13/21 12:303.4
4-Bromophenylphenyl ether ug/L ND 10.0 12/13/21 12:301.8
4-Chloro-3-methylphenol ug/L ND 10.0 12/13/21 12:303.3
4-Chloroaniline ug/L ND 20.0 12/13/21 12:303.6
4-Chlorophenylphenyl ether ug/L ND 10.0 12/13/21 12:302.0
4-Nitroaniline ug/L ND 20.0 12/13/21 12:305.1
4-Nitrophenol ug/L ND 50.0 12/13/21 12:306.6
Acenaphthene ug/L ND 10.0 12/13/21 12:302.0
Acenaphthylene ug/L ND 10.0 12/13/21 12:302.0
Aniline ug/L ND 10.0 12/13/21 12:301.6
Anthracene ug/L ND 10.0 12/13/21 12:302.3
Benzo(a)anthracene ug/L ND 10.0 12/13/21 12:302.7
Benzo(a)pyrene ug/L ND 10.0 12/13/21 12:302.8
Benzo(b)fluoranthene ug/L ND 10.0 12/13/21 12:302.6
Benzo(g,h,i)perylene ug/L ND 10.0 12/13/21 12:302.8
Benzo(k)fluoranthene ug/L ND 10.0 12/13/21 12:302.7
Benzoic Acid ug/L ND 50.0 12/13/21 12:303.4
Benzyl alcohol ug/L ND 20.0 12/13/21 12:302.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3486790
Associated Lab Samples:92577240001, 92577240002
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 12/13/21 12:301.8
bis(2-Chloroethyl) ether ug/L ND 10.0 12/13/21 12:301.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 12/13/21 12:303.7
Butylbenzylphthalate ug/L ND 10.0 12/13/21 12:303.1
Chrysene ug/L ND 10.0 12/13/21 12:302.8
Di-n-butylphthalate ug/L ND 10.0 12/13/21 12:302.2
Di-n-octylphthalate ug/L ND 10.0 12/13/21 12:303.9
Dibenz(a,h)anthracene ug/L ND 10.0 12/13/21 12:303.0
Dibenzofuran ug/L ND 10.0 12/13/21 12:302.1
Diethylphthalate ug/L ND 10.0 12/13/21 12:302.0
Dimethylphthalate ug/L ND 10.0 12/13/21 12:302.1
Fluoranthene ug/L ND 10.0 12/13/21 12:302.2
Fluorene ug/L ND 10.0 12/13/21 12:302.1
Hexachloro-1,3-butadiene ug/L ND 10.0 12/13/21 12:301.8
Hexachlorobenzene ug/L ND 10.0 12/13/21 12:302.2
Hexachlorocyclopentadiene ug/L ND 10.0 12/13/21 12:301.6
Hexachloroethane ug/L ND 10.0 12/13/21 12:301.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 12/13/21 12:302.9
Isophorone ug/L ND 10.0 12/13/21 12:301.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 12/13/21 12:301.3
N-Nitrosodimethylamine ug/L ND 10.0 12/13/21 12:301.9
N-Nitrosodiphenylamine ug/L ND 10.0 12/13/21 12:303.0
Naphthalene ug/L ND 10.0 12/13/21 12:302.1
Nitrobenzene ug/L ND 10.0 12/13/21 12:301.9
Pentachlorophenol ug/L ND 20.0 12/13/21 12:303.8
Phenanthrene ug/L ND 10.0 12/13/21 12:302.0
Phenol ug/L ND 10.0 12/13/21 12:301.4
Pyrene ug/L ND 10.0 12/13/21 12:302.2
2,4,6-Tribromophenol (S)%95 10-144 12/13/21 12:30
2-Fluorobiphenyl (S)%76 10-130 12/13/21 12:30
2-Fluorophenol (S)%64 10-130 12/13/21 12:30
Nitrobenzene-d5 (S)%88 10-144 12/13/21 12:30
Phenol-d6 (S)%46 10-130 12/13/21 12:30
Terphenyl-d14 (S)%79 34-163 12/13/21 12:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486791LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 29.450 59 18-130
1,2-Dichlorobenzene ug/L 28.050 56 20-130
1,3-Dichlorobenzene ug/L 27.050 54 18-130
1,4-Dichlorobenzene ug/L 27.250 54 18-130
1-Methylnaphthalene ug/L 37.150 74 29-130
2,2'-Oxybis(1-chloropropane)ug/L 42.350 85 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486791LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 48.050 96 35-130
2,4,6-Trichlorophenol ug/L 49.350 99 31-130
2,4-Dichlorophenol ug/L 48.550 97 35-130
2,4-Dimethylphenol ug/L 47.650 95 34-130
2,4-Dinitrophenol ug/L 255250 102 10-153
2,4-Dinitrotoluene ug/L 52.850 106 37-136
2,6-Dinitrotoluene ug/L 51.750 103 33-136
2-Chloronaphthalene ug/L 39.050 78 26-130
2-Chlorophenol ug/L 42.350 85 37-130
2-Methylnaphthalene ug/L 36.950 74 29-130
2-Methylphenol(o-Cresol)ug/L 44.550 89 35-130
2-Nitroaniline ug/L 93.9100 94 37-130
2-Nitrophenol ug/L 50.350 101 32-130
3&4-Methylphenol(m&p Cresol)ug/L 43.150 86 34-130
3,3'-Dichlorobenzidine ug/L 92.7100 93 34-136
3-Nitroaniline ug/L 103100 103 37-138
4,6-Dinitro-2-methylphenol ug/L 101100 101 21-157
4-Bromophenylphenyl ether ug/L 46.050 92 38-130
4-Chloro-3-methylphenol ug/L 96.9100 97 37-130
4-Chloroaniline ug/L 92.7100 93 38-130
4-Chlorophenylphenyl ether ug/L 44.750 89 33-130
4-Nitroaniline ug/L 105100 105 42-137
4-Nitrophenol ug/L 150250 60 10-130
Acenaphthene ug/L 43.050 86 33-130
Acenaphthylene ug/L 44.350 89 35-130
Aniline ug/L 34.050 68 22-130
Anthracene ug/L 46.150 92 48-130
Benzo(a)anthracene ug/L 48.050 96 48-137
Benzo(a)pyrene ug/L 49.550 99 49-138
Benzo(b)fluoranthene ug/L 47.850 96 52-138
Benzo(g,h,i)perylene ug/L 48.250 96 48-140
Benzo(k)fluoranthene ug/L 48.750 97 48-139
Benzoic Acid ug/L 136250 54 10-130
Benzyl alcohol ug/L 94.5100 94 35-130
bis(2-Chloroethoxy)methane ug/L 48.650 97 34-130
bis(2-Chloroethyl) ether ug/L 46.950 94 36-130
bis(2-Ethylhexyl)phthalate ug/L 47.350 95 32-165
Butylbenzylphthalate ug/L 47.850 96 34-161
Chrysene ug/L 46.750 93 47-131
Di-n-butylphthalate ug/L 47.150 94 39-144
Di-n-octylphthalate ug/L 48.550 97 30-170
Dibenz(a,h)anthracene ug/L 49.750 99 49-138
Dibenzofuran ug/L 45.350 91 33-130
Diethylphthalate ug/L 45.550 91 38-131
Dimethylphthalate ug/L 45.550 91 37-130
Fluoranthene ug/L 48.150 96 46-137
Fluorene ug/L 45.850 92 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486791LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 24.750 49 11-130
Hexachlorobenzene ug/L 46.250 92 38-130
Hexachlorocyclopentadiene ug/L 26.650 53 10-130
Hexachloroethane ug/L 25.450 51 14-130
Indeno(1,2,3-cd)pyrene ug/L 47.450 95 41-130
Isophorone ug/L 46.550 93 33-130
N-Nitroso-di-n-propylamine ug/L 48.550 97 36-130
N-Nitrosodimethylamine ug/L 35.550 71 34-130
N-Nitrosodiphenylamine ug/L 46.050 92 37-130
Naphthalene ug/L 33.950 68 30-130
Nitrobenzene ug/L 47.850 96 36-130
Pentachlorophenol ug/L 104100 104 23-149
Phenanthrene ug/L 46.750 93 44-130
Phenol ug/L 27.150 54 18-130
Pyrene ug/L 47.450 95 47-134
2,4,6-Tribromophenol (S)%108 10-144
2-Fluorobiphenyl (S)%83 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%100 10-144
Phenol-d6 (S)%55 10-130
Terphenyl-d14 (S)%75 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3486792MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92576696004
3486793
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 34 10-13034 0 3050ND17.0 17.0
1,2-Dichlorobenzene ug/L 50 34 10-13037 8 3050ND17.0 18.4
1,3-Dichlorobenzene ug/L 50 32 10-13033 1 3050ND16.1 16.3
1,4-Dichlorobenzene ug/L 50 32 10-13034 6 3050ND16.1 17.0
1-Methylnaphthalene ug/L 50 45 10-13050 9 3050ND22.7 24.9
2,2'-Oxybis(1-
chloropropane)
ug/L 50 50 12-14253 7 3050ND24.8 26.6
2,4,5-Trichlorophenol ug/L 50 64 10-14364 1 3050ND32.0 31.8
2,4,6-Trichlorophenol ug/L 50 61 10-14761 1 3050ND30.6 30.4
2,4-Dichlorophenol ug/L 50 55 10-13858 7 3050ND27.3 29.2
2,4-Dimethylphenol ug/L 50 54 25-13059 8 3050ND27.2 29.4
2,4-Dinitrophenol ug/L R12505010-16583 49 30250ND126207
2,4-Dinitrotoluene ug/L 50 88 29-14891 4 3050ND43.8 45.6
2,6-Dinitrotoluene ug/L 50 74 26-14677 5 3050ND36.8 38.6
2-Chloronaphthalene ug/L 50 47 11-13047 0 3050ND23.4 23.5
2-Chlorophenol ug/L 50 51 10-13354 6 3050ND25.3 26.8
2-Methylnaphthalene ug/L 50 45 13-13049 10 3050ND22.4 24.6
2-Methylphenol(o-Cresol)ug/L 50 50 20-13053 5 3050ND25.0 26.4
2-Nitroaniline ug/L 100 62 24-13664 3 30100ND62.2 64.2
REPORT OF LABORATORY ANALYSIS
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Page 36 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3486792MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92576696004
3486793
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 50 60 10-15363 5 3050ND30.1 31.6
3&4-Methylphenol(m&p
Cresol)ug/L 50 46 16-13051 10 3050ND23.2 25.7
3,3'-Dichlorobenzidine ug/L 100 79 10-15374 6 30100ND79.0 74.2
3-Nitroaniline ug/L 100 70 22-15174 6 30100ND70.2 74.4
4,6-Dinitro-2-methylphenol ug/L 100 79 10-18083 5 30100ND78.8 82.6
4-Bromophenylphenyl ether ug/L 50 68 25-13065 5 3050ND34.0 32.5
4-Chloro-3-methylphenol ug/L 100 64 25-13370 9 30100ND64.1 70.3
4-Chloroaniline ug/L 100 50 14-13254 8 30100ND50.3 54.5
4-Chlorophenylphenyl ether ug/L 50 62 19-13066 7 3050ND30.8 33.0
4-Nitroaniline ug/L 100 81 29-15085 5 30100ND81.5 85.5
4-Nitrophenol ug/L 250 47 10-13052 11 30250ND117130
Acenaphthene ug/L 50 54 16-13058 6 3050ND27.1 28.8
Acenaphthylene ug/L 50 56 15-13759 5 3050ND27.9 29.5
Aniline ug/L 50 41 10-13037 9 3050ND20.5 18.7
Anthracene ug/L 50 74 37-13673 2 3050ND37.2 36.6
Benzo(a)anthracene ug/L 50 82 40-14582 0 3050ND40.8 41.0
Benzo(a)pyrene ug/L 50 83 41-14681 2 3050ND41.5 40.6
Benzo(b)fluoranthene ug/L 50 80 39-15183 4 3050ND39.8 41.6
Benzo(g,h,i)perylene ug/L 50 81 40-14782 2 3050ND40.5 41.1
Benzo(k)fluoranthene ug/L 50 77 40-14674 3 3050ND38.3 37.2
Benzoic Acid ug/L 250 13 10-13042 30250ND32.5J 104
Benzyl alcohol ug/L 100 53 25-13056 6 30100ND53.0 56.4
bis(2-
Chloroethoxy)methane
ug/L 50 51 23-13055 9 3050ND25.4 27.7
bis(2-Chloroethyl) ether ug/L 50 52 25-13058 10 3050ND26.1 29.0
bis(2-Ethylhexyl)phthalate ug/L 50 84 28-16684 0 3050ND41.8 41.9
Butylbenzylphthalate ug/L 50 84 33-16584 0 3050ND42.1 42.1
Chrysene ug/L 50 79 38-14181 2 3050ND39.6 40.3
Di-n-butylphthalate ug/L 50 84 32-15384 0 3050ND42.1 42.0
Di-n-octylphthalate ug/L 50 93 30-17594 1 3050ND46.4 47.0
Dibenz(a,h)anthracene ug/L 50 80 39-14881 2 3050ND39.9 40.6
Dibenzofuran ug/L 50 61 20-13063 3 3050ND30.5 31.6
Diethylphthalate ug/L 50 77 28-14281 5 30502.74J 41.0 43.0
Dimethylphthalate ug/L 50 70 26-13672 4 3050ND34.9 36.2
Fluoranthene ug/L 50 84 39-14385 1 3050ND41.8 42.3
Fluorene ug/L 50 65 24-13267 4 3050ND32.3 33.7
Hexachloro-1,3-butadiene ug/L 50 28 10-13029 3 3050ND14.1 14.6
Hexachlorobenzene ug/L 50 70 29-13067 4 3050ND34.8 33.5
Hexachlorocyclopentadiene ug/L 50 30 10-13030 1 3050ND14.9 15.0
Hexachloroethane ug/L 50 29 10-13031 6 3050ND14.4 15.3
Indeno(1,2,3-cd)pyrene ug/L 50 77 39-14879 3 3050ND38.7 39.7
Isophorone ug/L 50 56 23-13062 10 3050ND27.9 31.0
N-Nitroso-di-n-propylamine ug/L 50 56 25-13063 11 3050ND28.2 31.4
N-Nitrosodimethylamine ug/L 50 44 22-13046 5 3050ND21.8 22.9
N-Nitrosodiphenylamine ug/L 50 70 26-13468 2 3050ND34.9 34.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
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Page 37 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3486792MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92576696004
3486793
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 50 40 14-13042 5 3050ND20.0 21.0
Nitrobenzene ug/L 50 52 25-13055 4 3050ND26.2 27.3
Pentachlorophenol ug/L 100 65 10-17570 7 30100ND65.1 70.0
Phenanthrene ug/L 50 75 36-13373 2 3050ND37.4 36.7
Phenol ug/L 50 33 10-13035 5 3050ND16.6 17.5
Pyrene ug/L 50 80 40-14378 2 3050ND39.8 39.1
2,4,6-Tribromophenol (S)%73 10-14468
2-Fluorobiphenyl (S)%44 10-13047
2-Fluorophenol (S)%39 10-13042
Nitrobenzene-d5 (S)%52 10-14456
Phenol-d6 (S)%32 10-13033
Terphenyl-d14 (S)%59 34-16359
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
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Page 38 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
665495
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92577240005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3486527
Associated Lab Samples:92577240005
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 326 12/15/21 10:49128
1,2-Dichlorobenzene ug/kg ND 326 12/15/21 10:49117
1,3-Dichlorobenzene ug/kg ND 326 12/15/21 10:49115
1,4-Dichlorobenzene ug/kg ND 326 12/15/21 10:49124
1-Methylnaphthalene ug/kg ND 326 12/15/21 10:49114
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 12/15/21 10:49155
2,4,5-Trichlorophenol ug/kg ND 326 12/15/21 10:49149
2,4,6-Trichlorophenol ug/kg ND 326 12/15/21 10:49134
2,4-Dichlorophenol ug/kg ND 326 12/15/21 10:49127
2,4-Dimethylphenol ug/kg ND 326 12/15/21 10:49135
2,4-Dinitrophenol ug/kg ND 1630 12/15/21 10:491010
2,4-Dinitrotoluene ug/kg ND 326 12/15/21 10:49125
2,6-Dinitrotoluene ug/kg ND 326 12/15/21 10:49119
2-Chloronaphthalene ug/kg ND 326 12/15/21 10:49129
2-Chlorophenol ug/kg ND 326 12/15/21 10:49122
2-Methylnaphthalene ug/kg ND 326 12/15/21 10:49130
2-Methylphenol(o-Cresol)ug/kg ND 326 12/15/21 10:49133
2-Nitroaniline ug/kg ND 1630 12/15/21 10:49266
2-Nitrophenol ug/kg ND 326 12/15/21 10:49141
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 12/15/21 10:49131
3,3'-Dichlorobenzidine ug/kg ND 651 IL12/15/21 10:49220
3-Nitroaniline ug/kg ND 1630 IL12/15/21 10:49256
4,6-Dinitro-2-methylphenol ug/kg ND 651 12/15/21 10:49304
4-Bromophenylphenyl ether ug/kg ND 326 12/15/21 10:49125
4-Chloro-3-methylphenol ug/kg ND 651 12/15/21 10:49229
4-Chloroaniline ug/kg ND 651 IL12/15/21 10:49256
4-Chlorophenylphenyl ether ug/kg ND 326 12/15/21 10:49121
4-Nitroaniline ug/kg ND 651 12/15/21 10:49248
4-Nitrophenol ug/kg ND 1630 12/15/21 10:49630
Acenaphthene ug/kg ND 326 12/15/21 10:49114
Acenaphthylene ug/kg ND 326 12/15/21 10:49114
Aniline ug/kg ND 326 12/15/21 10:49127
Anthracene ug/kg ND 326 12/15/21 10:49107
Benzo(a)anthracene ug/kg ND 326 12/15/21 10:49109
Benzo(a)pyrene ug/kg ND 326 12/15/21 10:49112
Benzo(b)fluoranthene ug/kg ND 326 12/15/21 10:49109
Benzo(g,h,i)perylene ug/kg ND 326 12/15/21 10:49126
Benzo(k)fluoranthene ug/kg ND 326 12/15/21 10:49114
Benzoic Acid ug/kg ND 1630 12/15/21 10:49700
Benzyl alcohol ug/kg ND 651 12/15/21 10:49247
REPORT OF LABORATORY ANALYSIS
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Page 39 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3486527
Associated Lab Samples:92577240005
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 326 12/15/21 10:49135
bis(2-Chloroethyl) ether ug/kg ND 326 12/15/21 10:49122
bis(2-Ethylhexyl)phthalate ug/kg ND 326 12/15/21 10:49126
Butylbenzylphthalate ug/kg ND 326 12/15/21 10:49137
Chrysene ug/kg ND 326 12/15/21 10:49118
Di-n-butylphthalate ug/kg ND 326 12/15/21 10:49110
Di-n-octylphthalate ug/kg ND 326 12/15/21 10:49128
Dibenz(a,h)anthracene ug/kg ND 326 12/15/21 10:49125
Dibenzofuran ug/kg ND 326 12/15/21 10:49117
Diethylphthalate ug/kg ND 326 12/15/21 10:49119
Dimethylphthalate ug/kg ND 326 12/15/21 10:49118
Fluoranthene ug/kg ND 326 12/15/21 10:49112
Fluorene ug/kg ND 326 12/15/21 10:49114
Hexachloro-1,3-butadiene ug/kg ND 326 12/15/21 10:49141
Hexachlorobenzene ug/kg ND 326 12/15/21 10:49127
Hexachlorocyclopentadiene ug/kg ND 326 12/15/21 10:49187
Hexachloroethane ug/kg ND 326 12/15/21 10:49124
Indeno(1,2,3-cd)pyrene ug/kg ND 326 12/15/21 10:49128
Isophorone ug/kg ND 326 12/15/21 10:49145
N-Nitroso-di-n-propylamine ug/kg ND 326 12/15/21 10:49122
N-Nitrosodimethylamine ug/kg ND 326 12/15/21 10:49110
N-Nitrosodiphenylamine ug/kg ND 326 12/15/21 10:49115
Naphthalene ug/kg ND 326 12/15/21 10:49111
Nitrobenzene ug/kg ND 326 12/15/21 10:49151
Pentachlorophenol ug/kg ND 651 12/15/21 10:49319
Phenanthrene ug/kg ND 326 12/15/21 10:49107
Phenol ug/kg ND 326 12/15/21 10:49145
Pyrene ug/kg ND 326 12/15/21 10:49132
Pyridine ug/kg ND 326 12/15/21 10:49103
2,4,6-Tribromophenol (S)%66 18-130 12/15/21 10:49
2-Fluorobiphenyl (S)%61 19-130 12/15/21 10:49
2-Fluorophenol (S)%62 18-130 12/15/21 10:49
Nitrobenzene-d5 (S)%59 21-130 12/15/21 10:49
Phenol-d6 (S)%60 18-130 12/15/21 10:49
Terphenyl-d14 (S)%58 15-130 12/15/21 10:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486528LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10401640 63 47-130
1,2-Dichlorobenzene ug/kg 10301640 62 49-130
1,3-Dichlorobenzene ug/kg 10301640 62 48-130
1,4-Dichlorobenzene ug/kg 10201640 62 49-130
1-Methylnaphthalene ug/kg 10801640 66 54-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
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Huntersville, NC 28078
[phone]
Page 40 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486528LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 9501640 58 38-130
2,4,5-Trichlorophenol ug/kg 11401640 69 49-130
2,4,6-Trichlorophenol ug/kg 10901640 66 50-130
2,4-Dichlorophenol ug/kg 10901640 66 51-130
2,4-Dimethylphenol ug/kg 11001640 67 53-130
2,4-Dinitrophenol ug/kg 53908220 66 39-130
2,4-Dinitrotoluene ug/kg 11001640 67 53-130
2,6-Dinitrotoluene ug/kg 11501640 70 55-130
2-Chloronaphthalene ug/kg 11001640 67 48-130
2-Chlorophenol ug/kg 10201640 62 54-130
2-Methylnaphthalene ug/kg 10801640 66 57-130
2-Methylphenol(o-Cresol)ug/kg 10401640 63 50-130
2-Nitroaniline ug/kg 21303290 65 49-130
2-Nitrophenol ug/kg 10501640 64 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 9871640 60 50-130
3,3'-Dichlorobenzidine ug/kg 2100 IL32906447-130
3-Nitroaniline ug/kg 1890 IL32905845-130
4,6-Dinitro-2-methylphenol ug/kg 23303290 71 50-142
4-Bromophenylphenyl ether ug/kg 11901640 72 55-130
4-Chloro-3-methylphenol ug/kg 21303290 65 52-130
4-Chloroaniline ug/kg 2000 IL32906149-130
4-Chlorophenylphenyl ether ug/kg 11001640 67 53-130
4-Nitroaniline ug/kg 20503290 62 51-130
4-Nitrophenol ug/kg 51208220 62 40-130
Acenaphthene ug/kg 10801640 66 56-130
Acenaphthylene ug/kg 11101640 68 58-130
Aniline ug/kg 9551640 58 44-130
Anthracene ug/kg 11101640 68 60-130
Benzo(a)anthracene ug/kg 11901640 72 59-130
Benzo(a)pyrene ug/kg 14101640 86 57-130
Benzo(b)fluoranthene ug/kg 14001640 85 54-130
Benzo(g,h,i)perylene ug/kg 13901640 84 59-130
Benzo(k)fluoranthene ug/kg 14501640 88 54-130
Benzoic Acid ug/kg 54508220 66 19-130
Benzyl alcohol ug/kg 20603290 63 50-130
bis(2-Chloroethoxy)methane ug/kg 10501640 64 55-130
bis(2-Chloroethyl) ether ug/kg 10201640 62 53-130
bis(2-Ethylhexyl)phthalate ug/kg 11801640 72 58-130
Butylbenzylphthalate ug/kg 12301640 75 46-138
Chrysene ug/kg 12201640 74 57-130
Di-n-butylphthalate ug/kg 11501640 70 57-130
Di-n-octylphthalate ug/kg 11801640 72 57-130
Dibenz(a,h)anthracene ug/kg 13601640 83 60-130
Dibenzofuran ug/kg 11101640 67 54-130
Diethylphthalate ug/kg 11301640 68 55-130
Dimethylphthalate ug/kg 11501640 70 57-130
Fluoranthene ug/kg 11401640 69 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
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Huntersville, NC 28078
[phone]
Page 41 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3486528LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 10801640 66 56-130
Hexachloro-1,3-butadiene ug/kg 10701640 65 41-130
Hexachlorobenzene ug/kg 12401640 76 53-130
Hexachlorocyclopentadiene ug/kg 10001640 61 23-130
Hexachloroethane ug/kg 10101640 62 48-130
Indeno(1,2,3-cd)pyrene ug/kg 13101640 80 61-130
Isophorone ug/kg 10601640 65 49-130
N-Nitroso-di-n-propylamine ug/kg 9751640 59 52-130
N-Nitrosodimethylamine ug/kg 10101640 61 45-130
N-Nitrosodiphenylamine ug/kg 11401640 70 56-130
Naphthalene ug/kg 10301640 62 56-130
Nitrobenzene ug/kg 10301640 63 50-130
Pentachlorophenol ug/kg 22203290 68 33-130
Phenanthrene ug/kg 11601640 71 60-130
Phenol ug/kg 9961640 61 54-130
Pyrene ug/kg 12801640 78 61-130
Pyridine ug/kg 9361640 57 35-130
2,4,6-Tribromophenol (S)%75 18-130
2-Fluorobiphenyl (S)%63 19-130
2-Fluorophenol (S)%62 18-130
Nitrobenzene-d5 (S)%59 21-130
Phenol-d6 (S)%59 18-130
Terphenyl-d14 (S)%57 15-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
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[phone]
Page 42 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92577240
21-418
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
665715
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92577240005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92576103011
3487500SAMPLE DUPLICATE:
Percent Moisture %98.7 N202598.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92577369002
3487600SAMPLE DUPLICATE:
Percent Moisture %20.4 N2102518.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2021 03:00 PM
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Page 43 of 54
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92577240
21-418
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 44 of 54
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92577240
21-418
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92577240001 665576 6656791EPA 3510C EPA 8270E
92577240002 665576 6656796EPA 3510C EPA 8270E
92577240005 665495 665584S-1 EPA 3546 EPA 8270E
92577240005 665553 665559S-1 EPA 5035A/5030B EPA 8260D
92577240001 6657491EPA 8260D
92577240002 6657496EPA 8260D
92577240003 6657492EPA 8260D
92577240004 6657494EPA 8260D
92577240005 665715S-1 SW-846
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 45 of 54
LIMS OBJECT ID: 92577240
LIMS USE: SRF Sample Receipt Form
Charlotte
Pace Analytical Services, LLC
Workorder:
Report Version:
Client Work ID:
Client:
Min Sample Due:
Max Sample Due:
Login Summary
92577240
D Catawba Valley Engineering & Testing
21-418
12/15/2021 19:00
12/15/2021 19:00
Profile:6933
SamplingProfile Desc:
Lab ID Sample ID Collected Matrix
Report
Location Due DateProp.Received
Turn
Code
92577240001 1 WT J2F NC12/10/21 10:00 12/15/2112/10/21 13:10 W003
92577240002 6 WT J2F NC12/10/21 11:00 12/15/2112/10/21 13:10 W003
92577240003 2 WT J2F NC12/10/21 10:15 12/15/2112/10/21 13:10 W003
92577240004 4 WT J2F NC12/10/21 10:30 12/15/2112/10/21 13:10 W003
92577240005 S-1 SL J2F NC12/09/21 13:30 12/15/21
Percent MoistureNon-Certified Cmps:
12/10/21 13:10 W003
Wednesday, December 15, 2021 1:41:12 PM Page 1 of 6Page 46 of 54
LIMS OBJECT ID: 92577240
LIMS USE: SRF Sample Receipt Form
Charlotte
Pace Analytical Services, LLC
Charge Summary
Bill To:Nathan Simmons
Catawba Valley Engineering & Testing
161 Lenoir Rhyne Blvd SE
Hickory, NC 28603
Client PO:
A/R Acct:92-618501
Text to appear on Invoice:
Workorder:92577240
Michele Childers ([e-mail])Invoice CC:
Tax Status:Nonexempt, Sales Tax May Apply
Qty Description Method MatrixUnit Price TotalCmps
4 8260D MSV Low Level WaterEaEPA 8260D $126.00 $504.0060
1 8260D/5035A/5030B Volatiles SolidEaEPA 8260D $130.00 $130.0067
1 8270E MSSV Microwave SolidEaEPA 8270E $262.50 $262.5069
2 8270E RVE WaterEaEPA 8270E $294.00 $588.0068
1 Dry Weight SolidEaSW-846 $0.00 $0.001
1 Environmental Impact Fee WaterEaMiscellaneous $12.00 $12.000
1 Sampling Media SolidEaMiscellaneous $10.00 $10.000
$1,506.50Total before Taxes:
Estimated Tax (0.00%):$0.00
Grand Total:$1,506.50
Wednesday, December 15, 2021 1:41:12 PM Page 2 of 6Page 47 of 54
LIMS OBJECT ID: 92577240
LIMS USE: SRF Sample Receipt Form
Charlotte
Pace Analytical Services, LLC
Sample Acknowledgement Recipients:
Catawba Valley Engineering & Testing
Nathan Simmons
161 Lenoir Rhyne Blvd SE
Hickory, NC 28603
Email: [e-mail]
Bill to:
Catawba Valley Engineering & Testing
Nathan Simmons
161 Lenoir Rhyne Blvd SE
Hickory, NC 28603
Email: [e-mail]
Inv CC:
Michele Childers ([e-mail])
Final Report Recipients:
Catawba Valley Engineering & Testing
Nathan Simmons (Primary)
161 Lenoir Rhyne Blvd SE
Hickory, NC 28603
Email: [e-mail]
Line Item Descriptions:
[1] Price Guide SL
[2] Price Guide WT
Client P O No:
Phone:
Project Manager:
Client Project ID:
Lab Project No:
Project Deliverables Type:
Project Report Due Date:
Profile:
[phone]
Ryan Brumfield
21-418
92577240
Standard Report
12/15/21
6933 (Autoreleased)
Automated EDD
FR Only no EDD (0)EDD #:
Publish (P)Publish or Review?:
Yes (Y)Email Client ?:
Yes (Y)Include FR ?:
Summary Level w/o Samp Info (SL)Auto Invoice:
Yes, auto email (Y)Email Invoice?:
Yes, print invoice (Y)Print Final Invoice?:
FR Only no EDD (0)Multiple EDD #2:
FR Only no EDD (0)Multiple EDD #3:
FR Only no EDD (0)Multiple EDD #4:
FR Only no EDD (0)Multiple EDD #5:
Lab Smp ID:
Proj Smp No:
Client Smp ID:
Matrix:Type:Line Item:
92577240001
1
Collected:
Received:
12/10/21 10:00
12/10/21 13:10
1
Water PS 2 Lab:
Location:NC
Auxillary Data:NOTE
Subout info:SI-33GCV = VPH to Pace National Notes for Login:
PARAMETER METHOD UNIT PRICE WR SPL %EARLIEST HOLD
8260D WLL - 8260D MSV Low Level 200EPA 8260D $126.0012/24/21 23:59
60Compound Count:
8270E RV - 8270E RVE 200EPA 8270E $294.0012/17/21 23:59
68Compound Count:
ECENVIMP - Environmental Impact Fee Miscellaneous Charges $12.00
Sub Total - Sample 3485749 $432.00
Lab Smp ID:
Proj Smp No:
Client Smp ID:
Matrix:Type:Line Item:
92577240002
2
Collected:
Received:
12/10/21 11:00
12/10/21 13:10
6
Water PS 2 Lab:
Location:NC
Auxillary Data:NOTE
Subout info:SI-33GCV = VPH to Pace National Notes for Login:
Wednesday, December 15, 2021 1:41:12 PM Page 3 of 6Page 48 of 54
LIMS OBJECT ID: 92577240
LIMS USE: SRF Sample Receipt Form
Charlotte
Pace Analytical Services, LLC
PARAMETER METHOD UNIT PRICE WR SPL %EARLIEST HOLD
8260D WLL - 8260D MSV Low Level EPA 8260D $126.0012/24/21 23:59
60Compound Count:
8270E RV - 8270E RVE EPA 8270E $294.0012/17/21 23:59
68Compound Count:
Sub Total - Sample 3485752 $420.00
Lab Smp ID:
Proj Smp No:
Client Smp ID:
Matrix:Type:Line Item:
92577240003
3
Collected:
Received:
12/10/21 10:15
12/10/21 13:10
2
Water PS 2 Lab:
Location:NC
Auxillary Data:NOTE
Subout info:SI-33GCV = VPH to Pace National Notes for Login:
PARAMETER METHOD UNIT PRICE WR SPL %EARLIEST HOLD
8260D WLL - 8260D MSV Low Level EPA 8260D $126.0012/24/21 23:59
60Compound Count:
Sub Total - Sample 3485754 $126.00
Lab Smp ID:
Proj Smp No:
Client Smp ID:
Matrix:Type:Line Item:
92577240004
4
Collected:
Received:
12/10/21 10:30
12/10/21 13:10
4
Water PS 2 Lab:
Location:NC
Auxillary Data:NOTE
Subout info:SI-33GCV = VPH to Pace National Notes for Login:
PARAMETER METHOD UNIT PRICE WR SPL %EARLIEST HOLD
8260D WLL - 8260D MSV Low Level EPA 8260D $126.0012/24/21 23:59
60Compound Count:
Sub Total - Sample 3485755 $126.00
Lab Smp ID:
Proj Smp No:
Client Smp ID:
Matrix:Type:Line Item:
92577240005
5
Collected:
Received:
12/09/21 13:30
12/10/21 13:10
S-1
Solid PS 1 Lab:
Location:NC
Auxillary Data:ICOM
Add a IRWO comment.:IR40: Reactive Sulfide, Ignitability, pH
Subout info:SI-33GCV = VPH to Pace National
Notes for Login:Fecal Coliform - ENCO Cary, NC (PACE
to Courier to lab) 102 Woodwinds Ct A
Cary, NC 27511
Add a IRWO comment.:
Add a IRWO comment.:
Add a IRWO comment.:
Add a IRWO comment.:
PARAMETER METHOD UNIT PRICE WR SPL %EARLIEST HOLD
8260D SM - 8260D/5035A/5030B Volatiles 200EPA 8260D $130.0012/23/21 23:59
67Compound Count:
8270E SMW - 8270E MSSV Microwave 175EPA 8270E $262.5012/23/21 23:59
69Compound Count:
DRY WEIGHT - Dry Weight SW-846 $0.0001/09/22 17:00
1Compound Count:
SCSAMMED - Sampling Media Miscellaneous Charges $10.00
Wednesday, December 15, 2021 1:41:14 PM Page 4 of 6Page 49 of 54
LIMS OBJECT ID: 92577240
LIMS USE: SRF Sample Receipt Form
Charlotte
Pace Analytical Services, LLC
PARAMETER METHOD UNIT PRICE WR SPL %EARLIEST HOLD
Sub Total - Sample 3485760 $402.50
Total Before Taxes - Project 92577240
Unit Pricing above does not reflect associated shipping, bottle, sample disposal and other miscellaneous charges. Prices are
subject to change without notice. Contact your Project Manager for further information.
$1,506.50
Estimated Tax (0.00%)$0.00
Wednesday, December 15, 2021 1:41:17 PM Page 5 of 6Page 50 of 54
LIMS OBJECT ID: 92577240
LIMS USE: SRF Sample Receipt Form
Charlotte
Pace Analytical Services, LLC
Containers
Lab ID Container ID Type UtilizationLocation
92577240001 AG0U1/2 AG0U 8270E RV92577240001Charlotte
92577240001 AG0U2/2 AG0U Charlotte
92577240001 DG9H1/3 DG9H 8260D WLLCharlotte
92577240001 DG9H2/3 DG9H Charlotte
92577240001 DG9H3/3 DG9H Charlotte
92577240001 NONE1/1 NONE ECENVIMP
92577240002 AG0U1/2 AG0U 8270E RV92577240002Charlotte
92577240002 AG0U2/2 AG0U Charlotte
92577240002 DG9H1/3 DG9H 8260D WLLCharlotte
92577240002 DG9H2/3 DG9H Charlotte
92577240002 DG9H3/3 DG9H Charlotte
92577240003 DG9H1/3 DG9H 8260D WLL92577240003Charlotte
92577240003 DG9H2/3 DG9H Charlotte
92577240003 DG9H3/3 DG9H Charlotte
92577240004 DG9H1/3 DG9H 8260D WLL92577240004Charlotte
92577240004 DG9H2/3 DG9H Charlotte
92577240004 DG9H3/3 DG9H Charlotte
92577240005 V/GK1/3 V/GK 8260D SM,DRY WEIGHT92577240005Charlotte
92577240005 V/GK2/3 V/GK Charlotte
92577240005 V/GK3/3 V/GK Charlotte
92577240005 WGFU1/1 WGFU 8270E SM,SCSAMMEDCharlotte
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