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Home My WebLink AboutAS-3505_28649_CA_RMR_20160308_ALL ACTIVE REMEDIATION MONITORING REPORT Cajah’s Mountain Superette 1990 Connelly Springs Road Lenoir, Caldwell County, North Carolina 28645 Facility ID No. 0-004593 NCDEQ Incident No. 28649 Risk Classification: High (H190D) ATC Project No. CARCAJA March 8, 2016 7606 Whitehall Executive Center Drive, Suite 800 Charlotte, NC 28273 Tel: 704-529-3200 Fax: 704-529-3272 www.atcgroupservices.com N.C. Engineering License No. C-1598 March 8, 2016 Mr. Dan Murphy North Carolina Department of Environmental Quality Asheville Regional Office Division of Waste Management - UST Section 2090 US Highway 70 Swannanoa, North Carolina 28778 RE: Active Remediation Monitoring Report Cajah’s Mountain Superette 1990 Connelly Springs Road Lenoir, Caldwell County, North Carolina 28645 Facility ID No. 0-004593 NCDEQ Incident No. 28649 Risk Classification: High (H190D) ATC Project No. CARCAJA Dear Mr. Murphy: ATC Associates of North Carolina, P.C., on behalf of Cary Oil Company, is submitting the enclosed Active Remediation Monitoring Report for the Cajah’s Mountain Superette site. This report includes information pertaining to operation and maintenance of the on-site and off-site air sparge and soil vapor extraction systems and data from a groundwater monitoring event conducted in January 2016. If you have any questions or require additional information, please contact us at (704) 529-3200. Sincerely, ATC Associates of North Carolina, P.C. Christine E. Schaefer Project Manager cc: Mr. Glenn Petti – Cary Oil Company Active Remediation Monitoring Report Cajah’s Mountain Superette 1990 Connelly Springs Road Lenoir, Caldwell County, North Carolina 28645 Facility ID No. 0-004593 NCDEQ Incident No. 28649 Risk Classification: High (H190D) ATC Project No. CARCAJA Prepared By: Submitted To: North Carolina Department of Environmental Quality Christine E. Schaefer Asheville Regional Office Project Manager Division of Waste Management - UST Section 2090 US Highway 70 Swannanoa, North Carolina 28778 ___________________________ Submitted By: David A. Hunter, P.G. NC Licensed Geologist No.1171 ATC Associates of North Carolina, P.C. 7606 Whitehall Executive Center Drive Suite 800 Charlotte, North Carolina 28273 Phone: (704) 529-3200 Fax: (704) 529-3272 On Behalf Of: Cary Oil Company 110 Mackenan Drive, Suite 300 Cary, North Carolina 27511 Phone: (919) 462-3194 March 8, 2016 Site Identification: Date of Report: March 8, 2016 Facility I.D.: 0-004593 UST Incident Number (if known): 28649 Site Risk: High Site Rank: H190D Land Use Category: Commercial Site Name: Cajah’s Mountain Superette Site Street Address: 1990 Connelly Springs Road City/Town: Lenoir Zip Code: 28645 County: Caldwell Description of Geographical Data Point (e.g., diesel fill port): Former Tank Basin Location Method (GPS, topographical map, other): Google Earth Latitude (decimal degrees): 35.83749120° N Longitude (decimal degrees): 81.5387323° W Information about Contacts Associated with the Leaking UST System: UST Owner: Cary Oil Company Address: 110 Mackenan Drive, Suite 300, Cary, NC 27511 Phone: (919) 462-3194 Property Owner: Mary Lindsay Address: 127 Dell Circle, Hudson, NC 28638 Phone: (828) 728-2674 Property Occupant: Mooresridge Catering (Walter Moore) Address: 1990 Connelly Springs Road, Lenoir, NC 28645 Phone: (828) 728-0859 Consultant/Contractor: ATC Associates of North Carolina, P.C. Address: 7606 Whitehall Executive Center Dr., Charlotte, NC 28273 Phone: (704) 529-3200 Analytical Laboratory: Pace Analytical Services, Inc. State Certification No.: 5342 Address: 9800 Kincey Avenue, Suite 100, Huntersville, NC 28078 Phone: (704) 875-9092 Information about Release: Date Discovered: August 28, 2008 Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release (Dispenser/Piping/UST): Unknown Sizes and contents of UST system(s) from which the release occurred: Two 8,000-gallon gasoline USTs and one 4,000-gallon gasoline UST and associated dispensers Information about the Monitoring Report: Date of Groundwater Monitoring Event: January 19 and 20, 2016 Period of Time Reported: 11/1/15 – 1/31/16 Type of Monitoring Report: Subsequent Active Remediation Monitoring Report I, David A. Hunter, a Professional Engineer/Licensed Geologist (circle one) for ATC Associates of North Carolina, P.C., do certify that the information contained in this report is correct and accurate to the best of my knowledge. ATC Associates of North Carolina, P.C. is licensed to practice geology/engineering (circle one or both) in North Carolina. The certification number issued by the North Carolina Board for Licensing of Geologists is C- 274. The certification number issued by the North Carolina Board of Examiners for Engineers and Surveyors is C-1598. TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY ............................................................................................................. 1 2.0 SUPPORTING INFORMATION AND CAP IMPLEMENTATION ......................................... 2 3.0 GROUNDWATER INVESTIGATION ......................................................................................... 3 3.1 Fluid Measurements and Free Product Conditions .............................................................. 3 3.2 Groundwater Monitoring ...................................................................................................... 4 4.0 REMEDIATION SYSTEM PERFORMANCE ............................................................................ 5 5.0 CONCLUSIONS AND RECOMMENDATIONS ......................................................................... 6 6.0 REPORT LIMITATIONS .............................................................................................................. 7 TABLES Table 1 Site History Table 2 Public and Private Water Supply Well and Other Receptor Information Table 3 Property Owners/Occupants and Land Use Information Table 4 Summary of Groundwater Sampling Results Table 5 Historical Groundwater Sampling Results Table 6 Monitored Natural Attenuation Parameters Table 7 Monitoring Well Construction and Groundwater Elevation Information Table 8 Groundwater Sampling Water Quality Parameters Table 9 Vertical Hydraulic Gradient Evaluations Table 10 Free Product Recovery Information Table 11 SVE System Cumulative Recovery FIGURES Figure 1 Site Topographic Map Figure 2 Site Map Figure 3 Site Vicinity Map Figure 4 Groundwater Elevation Contour Map Figure 5 Dissolved Benzene Isoconcentration Contour Map Figure 6 Dissolved MTBE Isoconcentration Contour Map APPENDICES Appendix A Standard Operating Procedures Appendix B Laboratory Analytical Reports Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 1 1.0 EXECUTIVE SUMMARY Cary Oil Company (Cary Oil) retained ATC Associates of North Carolina, P.C. (ATC) to prepare an Active Remediation Monitoring Report for the project site located at 1990 Connelly Springs Road in Lenoir, Caldwell County, North Carolina. Figure 1 shows the site and vicinity on part of a United States Geological Survey (USGS) site topographic map. This report documents remedial system operation and maintenance activities and the results of a groundwater monitoring event conducted in January 2016. According to groundwater analytical results obtained from the monitoring event performed on January 19 and 20, 2016, concentrations of petroleum contaminants of concern, excluding lead, were detected above the associated North Carolina NCAC 2L.0202 standards (2L standards) in nine site monitoring wells. Free product was not observed in site wells during the January 2016 monitoring event. Monitoring well MW-6 was not sampled due to the presence of mud and sediment in the well. The risk classification for the site has been designated as “High” and ranked H190D by the North Carolina Department of Environmental Quality (NCDEQ). Therefore, groundwater contamination must be remediated to concentration levels which are equal to or less than the associated 2L standards. As outlined in the October 31, 2012, Corrective Action Plan (CAP), high vacuum extraction through the implementation of Aggressive Fluid/Vapor Recovery (AFVR) technology appeared to be the most feasible and cost effective option for recovering remaining free product on-site. Air sparge and soil vapor extraction (AS/SVE) were the chosen corrective action technologies for shallow petroleum-impacted groundwater at this site based on site conditions and technical considerations. Natural attenuation was determined to be the most feasible and cost effective remedial option for reducing groundwater contaminant concentrations in portions of the intermediate and deep zones of the unconfined aquifer. Air sparge and soil vapor extraction wells were installed at the site on December 30, 2013, through January 15, 2014. The on-site and off-site system installations were completed on January 13, 2014, through January 24, 2014. System startup activities were conducted on March 26, 2014. However, due to noise concerns, the off-site system was turned off until April 9, 2014, when the telemetry was programmed to operate the system from 8:00 am to 8:00 pm. Efforts have been made to reduce excessive noise that originates from the building but minimal reductions have been observed. Following free product recovery from the source area, air sparge wells AS-1 through AS-3 were activated in October 2015. On-site system run-time was 91.9% from Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 2 November 24, 2015, to January 28, 2016. Off-site system run-time was 42.5% from November 24, 2015, to January 28, 2016 (the system is programmed to shut down during nighttime hours). Based on laboratory analytical results from quarterly effluent air sampling, approximately 605.2 and 0.2043 pounds of total BTEX have been recovered by the on-site and off-site SVE systems, respectively, from startup through December 15, 2015. Additional system performance information is included in Section 4.0. 2.0 SUPPORTING INFORMATION AND CAP IMPLEMENTATION Soil impact was identified during UST removals in August 2008, and NCDEQ subsequently requested site assessment. Between 2009 and 2013, site assessment, Aggressive Fluid/Vapor Recovery (AFVR) events for free product recovery, and a CAP with pilot testing were completed related to the Cajah’s release. Monitoring wells installed as part of assessment activities are indicated on Figure 2. Free product recovery efforts in the form of AFVR events, conducted between March 2012 and December 2013, recovered approximate totals of 44 gallons of liquid phase product, 54.17 gallons of vaporized product, and 1,870 gallons of petroleum contact water from well MW-8. Historical free product recovery information is summarized in Table 10. Adsorbent socks were installed and changed as necessary in well MW-8 beginning in February 2015 to recover remaining free product. The sock was removed in early July 2015, and the well has not indicated free product during subsequent groundwater monitoring events. Baton Water Corporation and the Town of Lenoir supply public water in the site vicinity. Twenty-one (21) private water supply wells have been identified within approximately 1,500 feet of the site. Water supply well information for the area is summarized in Table 2, and supply well locations relative to the source area are depicted on Figure 3. Historical analytical results from sampled supply wells are included in Table 5. Based on results of the CAP and pilot testing, ATC found that AFVR, AS/SVE technologies, and natural attenuation appeared to be the most feasible and cost effective remedial options for recovering free product and reducing groundwater contaminant concentrations associated with Incident No. 28649. Due to potential complications associated with horizontal boring under Connelly Springs Road and potential to affect underground utilities, two separate AS/SVE remediation systems were recommended to reduce groundwater concentrations on-site and in the immediate vicinity and on the east side of Connelly Springs Road. Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 3 With the exception of one SVE well installed as part of the pilot test in 2012, the systems were installed during the period of December 2013 through January 2014. The on-site and off-site air sparge systems consist of six and eight air sparge wells, respectively, rotary claw air compressors, and schedule 80 PVC piping for transferring compressed air from the remediation systems to the air sparge wells. The on-site and off-site vapor extraction systems consist of nine and five vapor extraction wells, respectively, regenerative vacuum blowers, condensate collection vessels, and schedule 40 PVC piping for transferring extracted vapors from the vapor extraction wells to the remediation systems. System startup activities were conducted on March 26, 2014. However, due to noise concerns, the off-site system was turned off until April 9, 2014, when the telemetry was programmed to operate the system from 8:00 am to 8:00 pm. Efforts have been made to reduce excessive noise that originates from the building, but minimal reductions have been observed. Monitoring well MW-8 was gauged on March 26, 2014, prior to system startup, and contained 0.43 feet of free product. On-site air sparge wells AS-1 through AS-3 were left off, by means of closed system manifold valves, until free product could be sufficiently recovered from the area. Following installations of adsorbent product socks, free product has been sufficiently reduced, and operation of AS-1 through AS-3 began in October 2015. For a detailed description of site environmental information, please refer to an earlier ARMR or the CAP. 3.0 GROUNDWATER INVESTIGATION 3.1 Fluid Measurements and Free Product Conditions On January 19 and 20, 2016, an oil/water interface probe was used to check for the presence of free product and measure static water levels at monitoring wells MW-1, MW-2, MW-5, MW-6, MW-7, MW-8, MW-11, MW-12, MW-14, MW-18, MW-22, IMW-1, IMW-2, and DMW-1 through DMW-5. Product was not observed in site monitoring wells. Mud and sediment were encountered from a depth of approximately 32 feet below TOC to the bottom of the screen in well MW-6. Groundwater elevations were determined in reference to the surveyed top of well casing elevations. Relevant field methods are summarized in Appendix A. Groundwater elevations were calculated based on the January 19 and 20, 2016, gauging data, and a summary of historical groundwater elevation data are included in Table 7. A groundwater elevation contour map, based on the January 2016 static water level data, is included as Figure 4. Groundwater flow direction across the site is generally towards the east-southeast with an estimated horizontal hydraulic gradient of 0.021 across the center of plume mass, based on January 2016 elevation data. Vertical gradient information is provided in Table 9, which shows predominantly downward migration between water zones in wells gauged across the site. However, the depth to water measured in well Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 4 DMW-5 in January 2016 does not appear representative of actual water table conditions and vertical gradient calculations associated with this well are therefore potentially inaccurate. 3.2 Groundwater Monitoring Groundwater samples were obtained from monitoring wells MW-1, MW-2, MW-5, MW-7, MW-8, MW-11, MW-12, MW-14, MW-18, MW-22, IMW-1, IMW-2, and DMW-1 through DMW-5, and water supply wells PW-1 and PW-18 on January 19 and 20, 2016. Based on historical impact and contaminant distribution, additional water supply wells were proposed for sample collection. However, available phone numbers for the property owners were disconnected, and letters requesting access for sampling were not acknowledged. Except for locations that were sampled, no one answered the doors at the residences during the sampling event. Prior to sampling, each monitoring well was purged of three standing water columns, or until the well was purged dry. Measurements of dissolved oxygen, pH, oxidation reduction potential, specific conductivity, and temperature were collected from each well volume purged. The water quality readings are provided in Table 8. Samples were then collected with new disposable bailers and poured directly into laboratory- provided containers with appropriate preservatives. Samples were also collected with new disposable bailers directly from the water supply wells as the wells were not in operation and pumps had been removed. The samples were then placed in a chilled cooler and submitted to North Carolina-accredited Pace Analytical Services, Inc. of Huntersville, North Carolina, using proper chain-of-custody procedures for laboratory analyses. Groundwater samples from the site monitoring well network were analyzed for volatile organic compounds by EPA Method 6200B including BTEX, MTBE, and isopropyl ether (IPE) and by EPA Method 6010 for lead. The intermediate and deep monitoring wells were also analyzed for natural attenuation parameters including nitrate, ferrous iron, sulfate, methane, and manganese. Samples collected from the water supply wells were analyzed by EPA Method 6200B. Samples have also historically been analyzed by Massachusetts Department of Environmental Protection (MADEP) volatile petroleum hydrocarbons (VPH) and EPA Method 504.1 for ethylene dibromide (EDB). Under the direction of the NCDEQ, the MADEP analysis was not performed starting in July 2015, and the EPA Method 504.1 analysis was not performed starting in January 2016. Although EDB is reported under EPA Method 6200B, the Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 5 analysis cannot attain the reduced detection limit required by the 2L standard. Confirmation sampling that incorporates MADEP VPH and EPA Method 504.1 analysis will be performed prior to site closure. According to the analytical results, concentrations of petroleum hydrocarbons were detected above the associated 2L standards in monitoring wells MW-2, MW-7, MW-8, MW-11, MW-12, MW-14, MW-18, IMW-1, and DMW-1. Concentrations of lead were reported above the 2L standard in wells MW-1, MW-2, MW-5, MW-7, MW-8, MW-11, MW-12, MW-14, and MW-22. However, the occurrence of lead in the aquifer seems disassociated with the contaminant plume and is likely naturally occurring. Based on current and historical analytical results, groundwater contamination above NCDEQ 2L standards is generally located in front of the on-site building in the vicinity of the former UST system and migrates downgradient to the east-southeast across Connelly Springs Road towards IMW-1 and slightly to the southwest towards wells MW-9 and DMW-2. Natural attenuation sampling indicates an environment conducive to potential bioremediation in the intermediate and deep aquifer zones. Generally, measured dissolved oxygen concentrations are consistently above anoxic and hypoxic conditions, indicating a potential for aerobic activity. Petroleum compound concentrations have generally shown an increasing trend in downgradient, intermediate well IMW-1, until January 2016 when concentrations decreased. Impact in this well should continue to be monitored and remedial system adjustments should be made as deemed necessary. Impact in on-site, deep well DMW-1 is generally decreasing with time. Contaminants of concern in other intermediate and deep wells remain minimal. Groundwater analytical results obtained in January 2016 are summarized in Table 4. Isoconcentration contour maps for dissolved benzene and MTBE are included as Figures 5 and 6, respectively. Please note that the figures display contours of vertical maximum impact due to the prevalence of impact from intermediate zone wells. Historical summaries of groundwater analytical results are provided in Table 5 and Table 6. Copies of the January 2016 laboratory analytical reports and chain-of-custody forms are included in Appendix B. 4.0 REMEDIATION SYSTEM PERFORMANCE System startup activities were conducted on March 26, 2014. However, due to noise concerns, the off-site system was turned off until April 9, 2014, when the telemetry was programmed to operate the system from Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 6 8:00 am to 8:00 pm. Efforts have been made to reduce excessive noise that originates from the building but minimal reductions have been observed. Due to bad motor windings, the off-site SVE blower was replaced under warranty by the system fabricator on October 15, 2014. Air sparge wells AS-1 through AS-3 were left off, by means of closed system manifold valves, until free product could be sufficiently recovered from the on-site source area. Following free product recovery using adsorbent product socks, air sparge wells AS-1 through AS-3 were activated in October 2015. System operation and maintenance (O&M) visits were conducted twice per month from November 2015 through January 2016 to check system components and perform routine maintenance. On-site system run- time was 91.9% from November 24, 2015, to January 28, 2016. During system operation, vacuum readings for each well point at the on-site SVE manifold were set at approximately 49 inches of water. Pressure readings for each well point at the on-site AS manifold were set at approximately nine psi. Off-site system run-time was 42.5% from November 24, 2015, to January 28, 2016 (the system is programmed to shut down during nighttime hours). During system operation, vacuum readings for each well point at the off-site SVE manifold were set at approximately 51 inches of water. Pressure readings for each well point at the off-site AS manifold were set at approximately 11 psi. Effluent air samples were collected from the on-site and off-site SVE systems on December 15, 2015, to evaluate petroleum vapor removal and to assist with system optimization efforts. The air samples were submitted to Accutest Laboratories for analysis by EPA Method TO-18. The laboratory analytical report is provided in Appendix B. Table 11 shows SVE cumulative recovery calculations based on system effluent sampling data. Assuming consistent recovery during each day of operation between sampling dates, approximately 605.2 and 0.2043 pounds of total BTEX have been recovered by the on-site and off-site SVE systems, respectively, from startup through December 15, 2015. 5.0 CONCLUSIONS AND RECOMMENDATIONS A groundwater monitoring event was conducted at the Cajah’s Mountain Superette site on January 19 and 20, 2016, to obtain current groundwater data. Recent and historical results indicate groundwater contamination above NCDEQ 2L standards is generally located in front of the on-site building in the vicinity of the former UST system and migrates downgradient to the east-southeast across Connelly Springs Road towards well IMW-1 and slightly to the southwest towards wells MW-9 and DMW-2. Cajah’s Mountain Superette March 8, 2016 Active Remediation Monitoring Report Page 7 System startup activities were conducted at the site on March 26, 2014, and O&M visits are being conducted twice per month, as proposed in the CAP. Adsorbent socks were installed and changed as necessary in well MW-8 beginning in February 2015 to recover remaining free product. The sock was removed in early July 2015, and the well has not indicated free product during subsequent groundwater monitoring events. Air sparge wells AS-1 through AS-3 were therefore started in October 2015. Additional groundwater monitoring and operation and maintenance of the site systems are recommended, as outlined in the CAP. 6.0 REPORT LIMITATIONS This investigation is intended to be a non-biased assessment of on-site environmental conditions proximate to the location of the former and/or current UST system. Subsurface investigative and remedial methodologies were performed in general accordance with applicable state and federal regulatory requirements. The information presented in this report is based upon site-specific observations, generally accepted geological and environmental consulting practices, and analytical results for environmental samples collected at the time of the field investigation was performed. The data presented in this report are believed to represent subsurface conditions at the facility; however, data may not be completely representative of subsurface conditions at every location. ATC assumes no liability arising from environmental impact to, or from, the site, regardless of the date of impact occurrence or findings. TABLES Table 1 Site History Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Zip Telephone Number 27511 (919) 462-3194 Zip Telephone Number 27511 (919) 462-3194 1 Gasoline None 4,000 Fiberglass 24' x 64" Fiberglass Reinforced Plastic Early 1980s Removed 8/14/08 Yes 2 Gasoline None 8,000 Fiberglass 8' x 21.4" Fiberglass Reinforced Plastic Early 1980s Removed 8/14/08 Yes 3 Gasoline None 8,000 Fiberglass 8' x 21.4" Fiberglass Reinforced Plastic Early 1980s Removed 8/14/08 Yes UST ID Number Current/Last Contents Previous Contents Capacity (gallons) Release confirmed during 8/14/08 excavation Tank Dimensions Description of Associated Piping and Pumps Date Tank Installed Status of Tank Was Release Associated With UST System? Date of Release Description of Release 28649 Gasoline 8/14/08 Incident Number Material Released Construction Details 0-004593 Name of Owner Dates of Ownership (m/dd/yy) to (m/dd/yy) UST ID Number(s) Facility ID Number 4/2005 to 8/14/2008 Name of Operator Street Address Dates of Operation (m/dd/yy) to (m/dd/yy) Cary Oil Company Cary NC 110 Mackenan Drive, Suite 300 City State UST ID Number(s) Facility ID Number 1, 2, and 3 0-004593 Street Address 110 Mackenan Drive, Suite 300 Cary Oil Company City State Cary NC 4/2005 to 8/14/2008 1, 2, and 3 Table 2 Public and Private Water Supply Well and Other Receptor Information Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 PW-1 Jimmie & Louise Beane / 1511 Bradshaw Terrace, Lenoir, NC 28645 1511 Bradshaw Terrace Lenoir 828-728-9368 Not in use Unknown Unknown 400 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-2 CitiMortgage, Inc. / 1000 Technology Drive, O'Fallon, MO 63368 1433 Brandon Road Lenoir NA In use for potable water by next- door Price & Shell Unknown Unknown 450 Downgradient Well services more than one residence (Price & Shell) PW-3 Henry & Linda Johnson / 1535 Bradshaw Terrace, Lenoir, NC 28645 1535 Bradshaw Terrace Lenoir 828-728-5256 Not in use Unknown Unknown 775 Downgradient Not accessible - According to Mr. Johnson, well has been filled over the years with sticks and rocks, and water is not accessible PW-4 Clifford & Jeanie Stewart / 319 Welcome Ave., Greenville, SC 29611 1554 Bradshaw Terrace Lenoir NA Not in use Unknown Unknown 1,100 Downgradient PW-5 Poarch Dixie Land Tate Azor / 1490 Land Street, Lenoir, NC 28645 1497 Land Street Lenoir NA Not in use Approx. 40-45' Unknown 1,000 Sidegradient PW-6 Ryan & Shirley Rozzelle / 186 Mountain Oak Lane, Hickory, NC 28601 1418 Brandon Road Lenoir 828-495-3456 Unknown Unknown Unknown 850 Sidegradient Current well use unknown; Property provided municipal water by Baton Water Corporation PW-7 Helen Sullivan / 904 Second St. NE, Apt. 234, Hickory, NC 28601 Justin Lane (No address number) Lenoir 828-728-2757 Not in use Unknown Unknown 1,200 Sidegradient Well operational but not in use and property provided municipal water by Baton Water Corporation PW-8 Brandon Apartments (Keith and Patricia Williams) / 1415 N. Catwaba Church Avenue, Lenoir, NC 28645 3715 Panda Lane Lenoir 828-728-9167 Not in use Unknown Unknown 1,000 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-9 Randy & Joyce Kestner / 4593 Horseshoe Bend Road, Hudson, NC 28638 3725 Happy Horse Lane Lenoir NA In use for potable water Unknown Unknown 1,100 Downgradient PW-10 Berry Kaylor / 3965 Greenwood Drive, Lenoir, NC 28645 3965 Greenwood Drive Lenoir 828-728-6946 Not in use Unknown Unknown 1,475 Sidegradient PW-11 Sherri Barnwell / 1499 Union Grove Road, Lenoir, NC 28645 1499 Union Grove Road Lenoir 828-728-3412 Not in use Unknown Unknown 1,300 Sidegradient Well not operational and property provided municipal water by Baton Water Corporation PW-12 Roger & Penny Triplett / 1740 Taylorsville Road SE, Lenoir, NC 28645 1512 Union Grove Road Lenoir NA Not in use Unknown Unknown 1,100 Sidegradient Property provided municipal water by Baton Water Corporation PW-13 William Rudicil / 1520 Union Grove Road, Lenoir, NC 28645 1520 Union Grove Road Lenoir NA Not in use Unknown Unknown 1,190 Sidegradient Property provided municipal water by Baton Water Corporation PW-14 Karen Sanders / 1522 Union Grove Road, Lenoir, NC 28645 1522 Union Grove Road Lenoir 828-726-1420 Not in use Unknown Unknown 1,210 Sidegradient PW-15 Arnold & Wanda Correll / 1528 Bradshaw Terrace, Lenoir, NC 28645 1528 Bradshaw Terrace Lenoir 828-728-7497 In use for outdoor/irrigation water Approx. 90 Unknown 525 Downgradient Well depth estimated by Mr. Correll; Property provided municipal water by Baton Water Corporation; Well only supplies water to outside spigots; Well not operational during winter PW-16 Theohary & Linda Smargian / PO Box 967, Hudson, NC 28638 1518 Bradshaw Terrace Lenoir NA Not in use Approx. 176* Unknown 400 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-17 Douglas & Katherine Hawkins / 1980 Connelly Springs Road, Lenoir, NC 28645 1980 Connelly Springs Road Lenoir NA Not in use Unknown Unknown 150 Sidegradient Well installed in 1961; Mary Lindsay (subject property owner) is POA; well is beneath house and not accessible PW-18 Jimmie & Louise Beane** / 1511 Bradshaw Terrace, Lenoir, NC 28645 1514 Bradshaw Terrace Lenoir NA Not in use Unknown Unknown 240 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-20 Cajah's Mt Park LLC (Steve Hamby) / PO Box 1114, Hudson, NC 28638 0 Connellly Springs Road (Cajah's Mountain Mobile Home Park)Lenoir NA Not In use Unknown Unknown 325 Sidegradient No access to well, well reportedly not operational, and property provided municipal water by Baton Water Corporation PW-21 Paula Fetherbay c/o Paula St. Clair / 1975 Connelly Springs Road, Lenoir, NC 28645 1975 Connelly Springs Road Lenoir NA In use for potable water Unknown Unknown 375 Sidegradient PW-22 Daniel Ace / 3733 Happy Horse Lane, Lenoir, NC 28645 3733 Happy Horse Lane Lenoir NA Reportedly, in use for potable water Unknown Unknown 1,100 Downgradient N/A East N/A N/A Surface water 700 Downgradient Stream was not identified on USGS topographic map, but was depicted on Caldwell County Geographic Information website, and could not be located during field activities. N/A West N/A N/A Surface water 500 Downgradient Stream was not identified on USGS topographic map, but was depicted on Caldwell County Geographic Information website. * On 7/26/10, due to difficulty encountered gauging depth of the two foot diameter well with an o/w interface meter, it was estimated that depth of PW-16 was approximately 176 ft bgs, as the meter appeared to reach bottom at that depth. ** residential property is currently leased; The Beane's are the owner for the residential property NA = Not Available Potable Well ID Well Depth (ft bgs) Receptor ID Location Contact Property Owner Contact Information Property Address City Phone Number Well Screen Interval (ft) Well Use Comment Approx. distance from source area of release (ft) Up/Down/ or Crossgradient* Approx. distance from source area of release (ft) Up/Down/Crossgradient/Ot her Comment Unnamed intermittent stream Unnamed intermittent stream Description Phone Number Usage Table 3 Property Owners/Occupants and Land Use Information Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Site Mary Lindsay 2746795343 1990 Connelly Springs Road 127 Dell Circle, Hudson, NC Lenoir, NC Adjacent to North 2746794580 1980 Connelly Springs Road Douglas & Katherine Hawkins R-20 / Residence Lenoir, NC Adjacent Northeast (opposite Connelly Springs Road) 2746890460 1989 Connelly Springs Road Philip and Debbie Yott RA-20 / Residence Lenoir, NC Adjacent East (opposite Connelly Springs Road)Chuck and Mattie Triplett 2746799380 1995 Connelly Springs Road 1130 Rosedale Drive SW, Lenoir, NC RA-20 / Residence Lenoir, NC Adjacent Southeast (opposite Connelly Springs Road)Cajah's Mountain Park LLC 2746890106 1999 Connelly Springs Road PO Box 1114, Hudson, NC RA-20 / Mobile home park Lenoir, NC Adjacent to South 2746795237 1998 Connelly Springs Road Moore Family Partnership LLC Lenoir, NC Adjacent to West Jimmie and Louise Beane 2746793289 1514 Bradshaw Terrace 1511 Bradshaw Terrace, Lenoir, NC RA-20 / Residence Lenoir, NC Updated as of 3/18/2015. R-20 and RA-20 refer to residential zoning B-1 refers to business zoning B-1 / Frosty Frez Restaurant and separate associated office building Tax Parcel Pin # (and well ID # if applicable)Property Location and Address Owner's Name and Address (if different) Zoning/Land Use R-20 / Catering business (former gas station) Table 4 Summary of Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 EPA METHOD 6200B C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class (Target analytes reported above method detection limits) C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e Et h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X L e a d MW-1 1/20/2016 NA NA NA <0.50 <0.50 0.27 J <0.50 14.8 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 43.4 MW-2 1/20/2016 NA NA NA 0.88 0.35 J <0.50 <0.50 2.7 <1.0 <0.50 <0.50 <0.50 0.62 0.58 12.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA 0.26 J <0.50 <2.0 16.1 <0.50 <0.50 2.6 18.7 61.8 MW-5 1/20/2016 NA NA NA <0.50 0.87 <0.50 <0.50 0.58 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.39 J 6.5 1.9 5.18 J 13.97 J 36.8 MW-6 1/19/2016 MW-7 1/20/2016 NA NA NA 34.2 14.7 <1.2 <1.2 4.0 <2.5 <1.2 <1.2 <1.2 5.9 3.8 125 <1.2 3.0 0.70 J <1.2 <1.2 NA 1.5 <1.2 7.5 276 17.2 4.3 89.2 386.7 38.7 MW-8 1/20/2016 NA NA NA 5,330 1,290 <125 <125 <125 <250 <125 <125 <125 <125 189 <125 <125 626 <125 <125 <125 NA <125 <125 1,320 1,800 21,500 3,040 19,530 45,870 54.1 MW-11 1/20/2016 NA NA NA 2,530 594 <125 <125 <125 <250 <125 <125 <125 94.8 J 105 J 2,510 <125 322 <125 <125 <125 NA <125 <125 642 5,450 23,900 2,920 16,260 48,530 54.8 MW-12 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 3.2 <0.50 188 <0.50 <0.50 0.68 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 29.3 MW-14 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 4.1 <0.50 122 <0.50 <0.50 1.0 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 40.7 MW-18 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 0.33 J <1.0 <0.50 <0.50 <0.50 2.2 <0.50 2.8 <0.50 <0.50 1.3 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 14.4 MW-22 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.32 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 21.4 J IMW-1 1/19/2016 NA NA NA 1.4 1.0 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 11.8 0.86 61.6 <0.50 <0.50 3.2 <0.50 <0.50 NA <0.50 <0.50 4.8 144 0.44 J 0.80 17.0 162.24 J 9.1 IMW-2 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.55 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <5.0 DMW-1 1/20/2016 NA NA NA <0.50 <0.50 0.67 <0.50 10.9 <1.0 <0.50 <0.50 <0.50 1.3 <0.50 101 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 8.7 DMW-2 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <5.0 DMW-3 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <5.0 DMW-4 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.78 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.57 <0.50 <0.50 0.28 J 0.85 J <5.0 DMW-5 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.28 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <5.0 PW-1 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA PW-2 1/20/2016 PW-9 1/20/2016 PW-16 1/20/2016 PW-18 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.50 ND NA PW-22 1/20/2016 400 700 200 400 400 NE 4 70 3 0.4 NE 0.02 70 70 20 70 70 0.4 3 0.7 25 70 70 6 1 600 600 500 N/A 15 NE NE NE 28,500 25,000 NE 4000 70,000 3,000 400 NE 50 70,000 25,000 20,000 6,900 30,000 400 3,000 700 11,700 8,500 70,000 6,000 5,000 260,000 84,500 85,500 N/A 15,000 1. All measurements are in micrograms per liter (ug/L). 7. NE = Not Established. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. (Amended Effective April 16, 2012) 8. VPH = Volatile Petroleum Hydrocarbons: C5-C8 and C9-C18 aliphatic chains, and C9-C22 aromatic chain 3. "<" or ND = Not detected above method detection limit or laboratory reporting limit. 9. Analytical table indicates target analyte concentrations reported above method detection limits. 4. GCL = Gross Contaminant Level established by NCDEQ. 10. NA = Not Analyzed for specified parameter 5. Target analyte concentrations detected above 2L Groundwater Standards are bolded. 11. N/A = Not Applicable 6. Target analyte concentrations detected above GCLs are bolded and italicized. 12. J = Estimated value below the laboratory reporting limit but above the method detection limit. Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access GCLs NC 2L GW Standards EPA METHOD 6010 Not Sampled Due to Mud/Sediment in Well SAMPLE I.D.DATE SAMPLED MADEP VPH Page 1 of 1 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d 12/10/2008 180 1.6 42 3.1 1.6 0.65 <0.1 11 3.3 <0.1 <0.1 *<0.022 0.24 0.34 65 0.4 0.63 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 10 2.5 1.2 3.3 17.0 <0.022 110 11/17/2009 1,300 35 61 2.9 2.1 <0.1 <0.1 13 <0.1 <0.1 <0.1 *<0.022 <0.1 0.46 18 0.7 0.83 <0.2 <0.1 <0.2 0.53 <0.1 <0.1 <0.1 17 5.1 0.75 9.5 32.4 <0.022 149 2/3/2012 1,180 488 137 19.1 7.6 <0.50 <0.50 5.2 <1.0 <0.50 <0.50 *<0.020 <0.50 2.2 3.7 1.6 5.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.1 26.6 18.1 6.9 41.0 92.6 <0.020 36.6 8/22/2012 1,570 125 135 3.4 5.4 <0.12 <0.12 7.0 <0.20 <0.10 NA *0.020 0.22 J 3.5 6.1 1.4 6.4 <0.16 <0.18 <0.14 0.50 1.5 <0.10 <0.10 49.2 13.9 2.5 26.8 92.4 0.020 20.0 1/23/2014 549 <50.0 <50.0 1.5 1.7 <0.50 <0.50 8.1 <1.0 <0.50 <0.50 *<0.020 <0.50 1.1 0.75 0.53 0.96 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 11.4 0.54 <0.50 5.3 17.2 <0.020 10.0 7/18/2014 785 542 117 16.3 8.8 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 0.62 5.5 5.0 2.9 6.0 <0.50 <0.50 <0.50 NA 2.4 <0.50 <2.0 37.4 4.7 2.8 44.0 88.9 <0.020 47.0 1/14/2015 163 131 <50.0 <0.50 0.57 <0.50 <0.50 9.4 <1.0 <0.50 <0.50 *<0.020 <0.50 1.1 0.77 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.53 <0.50 <2.0 8.2 <0.50 <0.50 3.6 11.8 <0.020 37.4 7/22/2015 NA NA NA 0.98 1.40 <0.50 <0.50 8.5 <1.0 <0.50 <0.50 *<0.020 <0.50 0.93 0.81 <0.50 0.45 J <0.50 <0.50 <0.50 NA 0.49 J <0.50 <2.0 6.9 <0.50 <0.50 3.9 10.8 <0.020 6.8 1/20/2016 NA NA NA <0.50 <0.50 0.27 J <0.50 14.8 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 43.4 3/13/2009 605 540 <100 29.3 10.7 1.8 <0.1 16.2 <1.0 <0.1 <0.1 *<0.02 2.8 1.7 72.1 1.1 3.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 151 80.8 11.6 116.1 360 <0.02 22.7 11/17/2009 2,600 460 660 110 38 <0.1 <0.1 16 <0.1 <0.1 <0.1 *<0.023 <0.1 3.9 340 <0.1 6.3 0.74 <0.1 <0.2 3.2 <0.1 <0.1 3.8 630 170 16 320 1,136 <0.023 22.4 2/3/2012 1,980 1,450 213 79.1 28.3 0.74 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 6.1 5.7 135 <0.50 10.9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 3.7 336 79.3 32.7 233 681 <0.020 31.5 8/22/2012 3,660 1,180 1,180 126 53.2 <2.3 <2.4 14.1 <3.9 <2.0 NA *0.042 15.3 4.4 J 389 <2.0 7.4 J <3.3 <3.6 <2.7 <2.0 <2.0 <2.0 7.2 J 939 89.7 18.3 447 1,494 0.042 29.4 1/24/2014 2,020 445 <250 52.0 18.9 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *<0.020 8.1 1.6 222 <1.0 1.3 <1.0 <1.0 <1.0 NA <1.0 <1.0 5.9 272 20.7 2.5 135.3 430.5 <0.020 <5.0 7/17/2014 2,350 696 <250 19.7 23.1 <1.2 <1.2 <1.2 <2.5 <1.2 <1.2 *<0.020 17.3 2.8 444 <1.2 2.2 <1.2 <1.2 <1.2 NA <1.2 <1.2 14.2 499 19.7 5.1 187.4 711.2 <0.020 11.7 1/14/2015 613 345 94.2 <2.5 16.8 <2.5 <2.5 5.7 <5.0 <2.5 <2.5 *<0.020 10.0 <2.5 274 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 14.1 345 10.9 3.9 68.9 428.7 <0.020 15.8 7/22/2015 NA NA NA 3.3 2.1 <1.2 <1.2 3.4 <2.5 <1.2 <1.2 *<0.020 7.1 1.4 197 <1.2 0.74 J 0.73 J <1.2 <1.2 NA <1.2 <1.2 7.1 143 2.4 1.4 12.8 159.6 <0.020 8.9 1/20/2016 NA NA NA 0.88 0.35 J <0.50 <0.50 2.7 <1.0 <0.50 <0.50 <0.50 0.62 0.58 12.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA 0.26 J <0.50 <2.0 16.1 <0.50 <0.50 2.6 18.7 NA 61.8 3/13/2009 <100 <100 <100 <0.50 <0.50 <0.50 <0.1 0.68 <1.0 <0.1 <0.1 *<0.02 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND <0.02 19.5 11/17/2009 <30 <10 <35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 ND <0.022 165 2/3/2012 <50.0 <50.0 <50.0 <0.50 <0.50 2.5 <0.50 11.9 <1.0 0.71 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 161 8/23/2012 <35 <35 <35 <0.10 <0.10 2.3 0.12 17.1 <0.20 0.27 J NA *<0.0091 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0091 100 1/23/2014 <50.0 <50.0 <50.0 <0.50 <0.50 1.4 <0.50 18.2 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 148 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 2.1 <0.50 22.7 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 174 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 1.5 <0.50 22.6 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 108 7/22/2015 NA NA NA <0.50 <0.50 0.97 <0.50 17.5 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 51.9 3/13/2009 <100 <100 <100 <0.50 <0.50 <0.50 <0.1 <0.50 <1.0 <0.1 <0.1 *<0.02 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.60 <0.50 <0.50 0.6 <0.02 25.9 11/17/2009 <30 <10 <35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 0.5 <0.2 0.41 1.0 <0.022 185 2/3/2012 <50.0 <50.0 <50.0 <0.50 <0.50 1.2 <0.50 6.0 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 61.9 8/22/2012 94.8 J <35 <35 <0.10 <0.10 1.7 <0.12 8.5 <0.20 0.36 J NA *<0.0097 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 47.9 1/23/2014 <50.0 <50.0 <50.0 <0.50 <0.50 0.58 <0.50 11.6 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 31.4 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 17.7 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 17.5 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 0.59 <0.50 14.8 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 13.2 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 7.7 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 26.7 11/17/2009 800 50 130 12 3.7 <0.1 <0.1 7.7 <0.1 <0.1 <0.1 *<0.022 <0.1 0.87 1.7 <0.1 1.4 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 1.1 35 88 9.9 61 193.9 <0.022 <10 2/3/2012 156 155 <50.0 4.7 1.0 <0.50 <0.50 1.4 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 4.2 <0.50 3.8 1.3 8.3 13.4 <0.020 35.0 8/22/2012 146 <35 <35 <0.10 <0.10 <0.12 <0.12 0.73 <0.20 <0.10 NA *<0.0095 <0.11 0.18 J <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.36 J <0.13 <0.15 0.63 J 0.99 <0.0095 <5.0 1/24/2014 131 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 32.9 7/18/2014 55.2 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 9.2 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 1.3 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 18.9 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 1.2 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 79.4 1/20/2016 NA NA NA <0.50 0.87 <0.50 <0.50 0.58 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.39 J 6.5 1.9 5.18 J 13.97 J NA 36.8 Table 5 MW-4 MW-1 MW-2 MW-5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. MW-3 Page 1 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 11/17/2009 1,200 990 410 23 4 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.023 3 3.7 130 0.79 7.2 0.34 <0.1 <0.2 1.9 0.9 <0.1 1.2 370 180 39 168 757 <0.023 45.2 2/2/2012 790 479 69.3 13.3 4.9 <0.50 <0.50 2.5 <1.0 <0.50 <0.50 *<0.020 <0.50 1.6 5.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 112 36.2 13.8 61.7 223.7 <0.020 92.3 8/22/2012 1,060 331 320 20.8 9.2 <0.59 <0.59 2.0 J <0.98 <0.51 NA *0.062 2.4 J 2.6 4.9 0.69 J 4.9 <0.82 <0.90 <0.69 0.63 J 1.2 J <0.50 2.0 J 226 77.1 24.9 122.1 450.1 0.062 18.1 1/23/2014 282 54.0 <50.0 3.6 1.5 <0.50 <0.50 2.4 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 1.0 <0.50 0.57 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 21.1 5.7 3.0 12.2 42.0 <0.020 41.2 7/17/2014 1/13/2015 7/22/2015 1/19/2016 11/17/2009 4,200 550 1,000 100 31 <0.1 <0.1 12 <0.1 <0.1 <0.1 *<0.023 12 7.4 290 3.2 9.3 1.4 <0.1 <0.2 2.6 <0.1 0.58 5.4 920 890 78 520 2,408 <0.023 <10 2/2/2012 1,840 1,840 428 88.7 31.0 <0.50 <0.50 15.0 <1.0 <0.50 <0.50 *<0.020 4.0 5.9 95.0 <0.50 8.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 4.1 252 131 15.4 291.6 690 <0.020 52.5 8/22/2012 2,250 784 753 110 32.1 <1.2 <1.2 11.7 <2.0 <1.0 NA *0.058 9.4 5.8 196 2.9 J 10.9 <1.6 <1.8 <1.4 1.3 J 2.0 J <1.0 4.3 J 463 275 43.5 418 1,199.5 0.058 <5.0 1/23/2014 3,790 1,880 <500 195 64.3 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *0.052 11.4 12.6 170 <5.0 26.7 <5.0 <5.0 <5.0 NA <5.0 <5.0 <20.0 811 952 132 814 2,709 0.052 73.2 7/18/2014 3,140 1,800 <500 148 47.3 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *0.085 6.1 9.4 68.1 <5.0 19.9 <5.0 <5.0 <5.0 NA <5.0 <5.0 <20.0 520 1,040 137 720 2,417 0.085 19.2 1/14/2015 2,930 2,610 <2,500 179 54.7 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *<0.020 9.8 10.9 112 <5.0 23.2 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <20.0 650 934 126 734 2,444 <0.020 216 7/22/2015 NA NA NA 101 39.9 <2.5 <2.5 4.6 <5.0 <2.5 <2.5 *0.085 9.8 7.8 134 <2.5 14.2 1.8 J <2.5 <2.5 NA 2.7 <2.5 7.4 J 434 401 59.4 387 1,281 0.085 23.5 1/20/2016 NA NA NA 34.2 14.7 <1.2 <1.2 4.0 <2.5 <1.2 <1.2 <1.2 5.9 3.8 125 <1.2 3.0 0.70 J <1.2 <1.2 NA 1.5 <1.2 7.5 276 17.2 4.3 89.2 386.7 NA 38.7 11/17/2009 31,000 4,100 8,700 580 130 <5 <0.1 <5 <5 <0.1 <0.1 *2.8 <5 25 <10 <5 61 39 27 27 <5 <5 29 130 1,900 17,000 900 4,600 24,400 2.8 <10 2/2/2012 8/22/2012 1/20/2014 7/17/2014 1/13/2015 7/22/2015 NA NA NA 4,130 2,480 <12.5 <12.5 <12.5 <25.0 <12.5 <12.5 *20.0 <12.5 335 77.2 434 1,220 <12.5 <12.5 <12.5 NA <12.5 83.3 2,330 6,810 36,100 4,160 19,240 66,310 20.0 8.9 1/20/2016 NA NA NA 5,330 1,290 <125 <125 <125 <250 <125 <125 <125 <125 189 <125 <125 626 <125 <125 <125 NA <125 <125 1,320 1,800 21,500 3,040 19,530 45,870 NA 54.1 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.021 23.7 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 1.6 <0.50 1.1 2.7 <0.019 6.4 8/22/2012 784 186 218 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 NA *<0.0094 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.15 <0.10 0.26 J <0.10 <0.22 0.26 <0.0094 <5.0 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 31.5 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 50.0 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 56.7 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 15.4 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 0.12 1.4 <0.1 0.29 1.8 <0.021 <10 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 0.83 <0.50 <1.5 0.83 <0.020 4.9 J 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 20.2 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 21.3 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 17.3 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 9.0 Not Sampled Due to Mud in Well MW-7 MW-8 MW-9 Not Sampled Due to Mud in Well Not Sampled Due to Presence of Free Product MW-10 Not Sampled Due to Mud/Sediment in Well Not Sampled Due to Presence of Free Product Not Sampled Due To Presence Of Free Product Not Sampled Due To Presence Of Free Product Not Sampled Due To Presence Of Free Product Not Sampled Due to Mud/Sediment in Well MW-6 Page 2 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 7/28/2010 75,000 5,700 24,000 1,800 520 <50 <0.1 <50 <50 <0.1 <0.1 *3.1 190 110 5,600 <50 270 <100 <50 <100 <50 <50 84 700 15,000 37,000 2,800 14,100 68,900 3.1 19.3 2/2/2012 56,300 68,400 <10,000 2,090 492 <0.50 <0.50 <0.50 <1.0 0.73 <0.50 *4.1 151 116 2,590 <0.50 273 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 565 9,890 27,100 2,980 15,290 55,260 4.1 18.1 8/23/2012 17,700 8,370 4,730 2,150 528 <120 <120 <160 <200 <100 NA *2.4 131 J <100 3,210 <100 309 J <160 <180 <140 <100 <100 <100 616 8,720 31,700 3,140 17,310 60,870 2.4 19.5 1/22/2014 71,500 47,800 5,070 2,130 489 <125 <125 <125 <250 <125 <125 *2.7 <125 <125 1,960 <125 265 <125 <125 <125 NA <125 <125 538 7,860 30,300 2,650 14,460 55,270 2.7 55.7 7/17/2014 54,100 33,200 <5,000 1,540 360 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *0.93 57.6 69.4 1,210 <5.0 187 <5.0 <5.0 <5.0 NA <5.0 44.4 510 5,350 19,300 1,900 10,410 36,960 0.93 39.7 1/13/2015 54,700 59,600 <10,000 2,860 644 <100 <100 <100 <200 <100 <100 *2.5 <100 124 1,400 <100 361 <100 <100 <100 <100 <100 <100 739 6,650 28,100 3,200 17,760 55,710 2.5 48.5 7/21/2015 NA NA NA 2,270 568 <125 <125 <125 <250 <125 <125 *2.4 83.9 J 103 J 1,870 <125 307 <125 <125 <125 NA <125 67.8 J 728 5,630 26,000 2,960 15,150 49,740 2.4 14.9 1/20/2016 NA NA NA 2,530 594 <125 <125 <125 <250 <125 <125 <125 94.8 J 105 J 2,510 <125 322 <125 <125 <125 NA <125 <125 642 5,450 23,900 2,920 16,260 48,530 NA 54.8 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 2.7 2.7 <0.021 15.2 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <4.0 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0094 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0094 11.8 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 11.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.96 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 58.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.10 0.58 <0.50 46.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 0.10 437 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.23 3.5 <0.50 207 <0.50 <0.50 1.1 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 0.23 45.7 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 3.2 <0.50 188 <0.50 <0.50 0.68 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 29.3 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 4.5 J 8/24/2012 163 50.8 J <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 <5.0 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 5.9 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 12.8 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 5.5 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 4.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 11.4 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0092 <0.11 <0.10 1.7 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0092 14.5 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 21.1 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 12.4 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 117 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 2.9 <0.50 33.5 <0.50 <0.50 0.68 <0.50 <0.50 NA <0.50 <0.50 <2.0 1.1 <0.50 <0.50 <1.5 ND <0.020 7.7 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 4.1 <0.50 122 <0.50 <0.50 1.0 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 40.7 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 <5.0 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 10.6 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 41.7 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 152 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 98.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 233 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 30.7 MW-13 MW-11 MW-12 MW-14 MW-15 MW-16 Page 3 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 8.0 8/24/2012 78.4 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 16.3 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 95.6 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 91.4 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 139 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.33 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 21.7 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 0.60 <0.50 <1.5 0.60 <0.020 28.2 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 0.39 J <0.10 1.2 <0.10 <0.11 <0.16 <0.18 <0.14 0.72 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 42.6 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 2.1 <0.50 1.7 <0.50 <0.50 0.81 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 79.3 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 1.7 <0.50 <0.50 0.63 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 50.9 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.023 2.0 <0.50 1.0 <0.50 <0.50 1.2 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 0.023 109 7/21/2015 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 0.33 J <1.0 <0.50 <0.50 <0.50 2.2 <0.50 2.8 <0.50 <0.50 1.3 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 14.4 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <20.0 8/23/2012 <35 <35 41.6 J <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 0.30 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 25.3 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.019 139 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 54.5 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 112 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <100 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 15.6 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 0.21 J <0.20 <0.10 NA *<0.0097 0.14 J <0.10 0.38 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 8.2 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 41.7 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 26.8 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 64.3 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 24.4 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <4.0 8/24/2012 60.8 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 2.5 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 <5.0 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 3.4 J 4/3/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *0.024 1.7 <0.10 47.4 <0.10 <0.11 0.64 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND 0.024 29.9 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0097 0.80 <0.10 24.0 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 7.5 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 8.9 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 *<0.020 <0.50 <0.50 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 66.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 2.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 109 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.49 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 7.2 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.32 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 21.4 J 2/2/2012 309 406 <50.0 25.0 <0.50 0.67 <0.50 1.1 <1.0 0.74 <0.50 *0.42 16.5 2.6 84.6 <0.50 3.1 3.6 <0.50 <0.50 <0.50 <0.50 <0.50 10.8 260 71.1 21.8 215 567.9 0.42 <4.0 8/23/2012 2,300 865 477 76.3 <2.0 <2.3 <2.4 <3.2 <3.9 <2.0 NA *1.1 51.9 7.3 J 251 <2.0 11.6 12.3 <3.6 <2.7 <2.0 <2.0 <2.0 31.3 967 266 82.1 638 1,953.1 1.1 <5.0 1/22/2014 3,060 2,060 <1,000 110 <5.0 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *1.5 61.0 8.9 247 <5.0 12.2 16.5 <5.0 <5.0 NA <5.0 <5.0 42.3 1,470 65.2 85.8 796 2,417.0 1.5 <5.0 7/17/2014 4,160 2,360 <1,250 112 9.8 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *1.5 74.9 11.5 292 1.8 15.1 21.3 <0.50 <0.50 NA <0.50 <0.50 53.1 1,360 78.5 118 785 2,341.5 1.5 <5.0 1/13/2015 5,250 5,210 <5,000 104 8.6 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *1.4 57.8 9.4 282 <5.0 12.4 16.3 <5.0 <5.0 <5.0 <5.0 <5.0 47.4 1,360 23.4 88.5 783 2,254.9 1.4 <5.0 7/21/2015 NA NA NA 71.1 6.6 <5.0 <5.0 <5.0 14.1 <5.0 <5.0 *1.6 54.3 9.8 311 <5.0 12.0 17.8 <5.0 <5.0 NA <5.0 <5.0 47.2 1,550 17.6 78.0 691 2,336.6 1.6 2.5 J 1/19/2016 NA NA NA 1.4 1.0 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 11.8 0.86 61.6 <0.50 <0.50 3.2 <0.50 <0.50 NA <0.50 <0.50 4.8 144 0.44 J 0.80 17.0 162.24 J NA 9.1 MW-21 MW-17 MW-19 MW-18 MW-20 Not Sampled - Aboveground Pool Obstructing Well IMW-1 MW-22 Page 4 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 4/3/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *0.0096 J 0.91 <0.10 1.2 <0.10 <0.11 <0.12 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND 0.0096 J <5.0 8/23/2012 61.0 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 0.42 J <0.10 0.60 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 <5.0 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 0.65 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.55 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 11/17/2009 1,300 180 230 41 <0.1 <0.1 <0.1 7.9 <0.1 <0.1 <0.1 *<0.022 2.3 2.6 450 1.2 3.2 <0.2 <0.1 <0.2 2.1 <0.1 <0.1 3.4 140 0.41 3 21.8 165.6 <0.022 <10 2/3/2012 1,510 502 90 31.1 <0.50 <0.50 <0.50 15.7 <1.0 <0.50 <0.50 *0.023 2.7 2.8 490 1.6 2.1 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 3.7 134 0.61 1.0 54.2 189.8 0.023 11.7 8/22/2012 757 160 181 11.9 <1.0 <1.2 <1.2 7.9 <2.0 <1.0 NA *0.026 2.1 J 1.1 J 349 <1.0 <1.1 <1.6 <1.8 <1.4 <1.0 <1.0 <1.0 1.5 J 57.9 11.8 <1.5 28.3 98.0 0.026 <5.0 1/23/2014 251 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 4.1 <1.0 <0.50 <0.50 *<0.020 1.2 <0.50 325 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 8.8 7/17/2014 273 <50.0 <50.0 <0.50 <0.50 1.1 <0.50 16.4 <1.0 <0.50 <0.50 *<0.020 1.8 <0.50 448 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/14/2015 123 <50.0 <50.0 <1.0 <1.0 <1.0 <1.0 10.3 <2.0 <1.0 <1.0 *<0.020 1.4 <1.0 174 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <4.0 <1.0 <1.0 <1.0 <3.0 ND <0.020 9.7 7/22/2015 NA NA NA <0.50 <0.50 0.88 <0.50 12.9 <1.0 <0.50 <0.50 *<0.020 1.4 <0.50 118 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 8.0 1/20/2016 NA NA NA <0.50 <0.50 0.67 <0.50 10.9 <1.0 <0.50 <0.50 <0.50 1.3 <0.50 101 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 8.7 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 1.4 2 <0.1 3.1 6.5 <0.021 <10 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 1.3 6.9 0.77 3.7 12.7 <0.020 <4.0 8/22/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 0.28 J <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 <5.0 1/22/2014 399 <50.0 <50.0 0.62 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 5.5 <0.50 <0.50 3.84 3.84 <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 10.0 1/14/2015 85.8 74.8 <50.0 3.5 0.69 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.028 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 39.1 9.7 1.9 25.6 76.3 0.028 5.8 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 2/3/2012 <50.0 69.9 <50.0 0.69 <0.50 <0.50 <0.50 0.66 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 25.8 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 1.7 1.5 <0.50 2.4 5.6 <0.021 4.2 J 8/22/2012 58.4 J <35 <35 0.17 J <0.10 <0.12 <0.12 <0.16 1.4 <0.10 NA *<0.0095 0.22 J <0.10 33.2 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.52 0.46 J <0.15 0.26 J 1.24 <0.0095 <5.0 1/23/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 27.1 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.30 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 0.55 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 25.1 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 1.0 1.0 <0.020 <5.0 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 0.41 J <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.56 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 2/2/2012 <50.0 116 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <4.0 8/23/2012 47.4 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 1.4 <0.10 NA *<0.0094 <0.11 <0.10 0.18 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 0.16 J 0.23 J 0.22 J <0.15 <0.30 0.45 <0.0094 <5.0 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 2.4 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 1.5 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.64 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 6.3 5.0 <0.50 7.2 18.50 <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.39 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.78 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.57 <0.50 <0.50 0.28 J 0.85 J NA <5.0 4/3/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 0.18 J <0.10 3.1 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.58 <0.13 <0.15 <0.30 0.58 <0.0095 <5.0 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 0.52 <0.10 NA *<0.0095 0.26 J <0.10 5.2 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.79 <0.13 <0.15 <0.30 0.79 <0.0095 <5.0 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.55 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 3.4 J 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.28 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 DMW-4 DMW-5 IMW-2 DMW-1 DMW-2 DMW-3 Page 5 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 *<0.023 <0.1 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 0.84 0.12 <0.1 <0.1 2.7 2.8 <0.023 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 <0.1 0.97 <0.1 <0.1 *<0.021 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.021 NA 8/29/2012 39.6 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA NA 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 0.31 <0.2 <0.1 <0.1 *<0.021 <0.1 <0.2 6 <0.1 <0.1 0.12 <0.1 <0.2 <10 <0.1 <0.1 0.34 0.12 <0.1 <0.1 <0.1 0.12 <0.021 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.22 1.5 <0.1 <0.1 *<0.02 <0.5 <0.2 2.5 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.02 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 1.6 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 3.7 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/24/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.4 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/16/2014 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.4 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.0 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/20/2016 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 1/15/2015 7/22/2015 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.4 0.33 <0.1 <0.1 *<0.022 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 0.44 J <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/24/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/16/2014 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 0.34 J <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA PW-7 5/5/2011 <30 <40 <10 <0.1 <0.1 4.2 3.5 3.2 0.19 7.2 0.1 *<0.021 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.021 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 <0.1 0.93 <0.1 <0.1 *<0.022 <0.5 <0.2 0.64 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 8/24/2012 42.9 J <35 <35 <0.10 <0.10 <0.12 <0.12 0.20 J <0.20 <0.10 NA *<0.0096 0.30 J <0.10 0.40 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/24/2014 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/20/2016 PW-10 1/15/2015 PW-11 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 0.54 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 NA 1/15/2015 7/22/2015 1/15/2015 7/22/2015 Not Sampled - No One Home, No Access PW-4 PW-5 Not Sampled - No One Home, No Access PW-12 PW-1 PW-6 Not Sampled - Well House Partialy Collapsed and Multiple Hazards to Access Sample Port Not Sampled - No One Home and Outside Water Turned Off Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled; Outside Spigots Winterized and No One Home Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access PW-2 Not Sampled - No One Home, No Access PW-9 Not Sampled - No One Home, No AccessPW-13 Page 6 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. PW-14 1/15/2015 11/17/2009 <30 <10 <35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 ND <0.022 NA 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 1.3 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 1.2 <0.1 <0.1 <0.2 <0.1 ND <0.022 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 1.2 0.78 <0.1 <0.1 *<0.022 <0.5 <0.2 0.25 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 7/22/2015 11/17/2009 440 80 220 9.6 2.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *NA <0.1 0.5 <0.1 <0.1 1.1 <0.1 <0.1 <0.2 <0.1 <0.1 0.46 2.7 12 170 16 81 ND NA NA 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 1.4 4.3 <0.2 3.9 ND <0.021 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.21 0.3 <0.1 <0.1 *<0.022 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0094 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0094 NA 1/20/2016 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 ND <0.022 NA 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.50 ND NA NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.10 1.7 <0.1 <0.1 *<0.023 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.023 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0097 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 NA 1/27/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.90 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 0.85 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 NA 1/24/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/20/2016 400 700 200 400 400 NE 4 70 3 0.4 NE 0.02 70 70 20 70 70 0.4 3 0.7 25 70 70 6 1 600 600 500 N/A 0.02 15 NE NE NE 28,500 25,000 NE 4000 70,000 3,000 400 NE 50 70,000 25,000 20,000 6,900 30,000 400 3,000 700 11,700 8,500 70,000 6,000 5,000 260,000 84,500 85,500 N/A 50 15,000 1. All measurements are in micrograms per liter (ug/L).9. Analytical table indicates target analyte concentrations reported above method detection limits. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. (Amended Effective April 16, 2012) 10. NA = Not Analyzed for specified parameter 3. "<" or ND = Not detected above method detection limit or laboratory reporting limit. 11. N/A = Not Applicable 4. GCL = Gross Contaminant Level established by NCDEQ. 12. J = Estimated value below the laboratory reporting limit but above the method detection limit. 5. Target analyte concentrations detected above 2L Groundwater Standards are bolded. 6. Target analyte concentrations detected above GCLs are bolded and italicized. 7. NE = Not Established. 14. * = Value reported under EPA Method 504.1. PW-21 GCLs NC 2L GW Standards PW-18 8. VPH = Volatile Petroleum Hydrocarbons: C5-C8 and C9-C18 aliphatic chains, and C9-C22 aromatic chain Not Sampled - Well Not Operational During Winter 13. Methylene chloride, a known laboratory contaminant, was reported at 0.2 ug/L for water collected from PW-16 on July 26, 2010; and at 0.51 ug/L for water collected from PW-7 on May 5, 2011. Not Sampled - No One Home, No Access PW-16 Not Sampled - No One Home, No Access PW-22 PW-15 Not Sampled - Owner Refused Access Not Sampled - Owner Refused Access Page 7 of 7 Table 6 Monitored Natural Attenuation Parameters Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number 28649 Sample I.D.Date Sampled Dissolved Oxygen Nitrate Manganese Ferrous Iron Sulfate Methane 8/23/2012 3.22 0.17 0.832 <0.10 <2.0 0.00501 1/22/2014 5.87 0.038 2.12 <0.50 <2.0 0.0091 7/17/2014 6.08 0.040 1.88 <0.50 <2.0 0.0088 1/13/2015 2.93 0.080 1.99 0.87 <2.0 0.0077 7/21/2015 2.05 0.066 2.89 1.2 1.6 J 0.0090 J 1/19/2016 1.49 0.34 0.964 <0.50 1.4 J 0.0027 J 8/23/2012 3.56 <0.10 0.0994 0.34 2.0 0.00427 1/22/2014 7.22 0.023 0.0086 <0.50 3.6 <0.0066 7/17/2014 4.05 <0.020 0.0091 <0.50 3.9 <0.0066 1/13/2015 3.05 0.069 <0.0050 <0.50 5.8 <0.0066 7/22/2015 5.48 0.017 J 0.0486 <0.50 3.8 0.0021 J 1/19/2016 3.39 0.053 0.0206 <0.50 7.4 0.0019 J 8/22/2012 3.09 0.80 0.214 0.33 6.3 0.00517 1/23/2014 10.11 1.2 0.188 <0.50 5.9 <0.0066 7/17/2014 12.17 1.2 0.253 <0.50 <2.0 <0.0066 1/14/2015 5.49 1.3 0.405 1.0 <2.0 <0.0066 7/22/2015 5.70 1.1 0.444 <0.50 1.5 J <0.0100 1/20/2016 2.26 1.1 0.290 <0.50 1.5 J 0.0015 J 8/22/2012 1.31 <0.10 0.510 0.48 <2.0 0.0237 1/22/2014 1.09 0.061 0.399 <0.50 <2.0 0.512 7/17/2014 11.37 0.057 0.586 <0.50 14.4 0.288 1/14/2015 1.99 0.23 0.509 0.80 9.2 1.58 7/22/2015 1.31 0.58 0.371 <0.50 7.5 0.0020 J 1/20/2016 1.35 <0.020 0.363 <0.50 1.8 J 4.49 8/22/2012 2.30 <1.0 <0.015 <0.10 <20 0.00180 1/23/2014 4.98 <0.020 <0.0050 <0.50 5.1 <0.0066 7/17/2014 3.32 <0.020 <0.0050 <0.50 12.6 0.01470 1/14/2015 5.06 0.48 0.0203 <0.50 6.2 <0.0066 7/22/2015 2.02 <0.020 0.0199 <0.50 11.3 0.0020 J 1/20/2016 1.91 0.21 0.0165 <0.50 5.8 0.0019 J 8/23/2012 1.67 <2.5 0.0171 <0.10 <50 0.0047 1/21/2014 4.52 <0.020 0.0150 <0.50 10 0.0206 7/17/2014 7.24 <0.020 0.0071 <0.50 9.9 0.0652 1/13/2015 2.45 <0.020 <0.0050 <0.50 10.4 0.0330 7/21/2015 1.91 <0.020 0.0156 0.70 9.5 <0.0100 1/19/2016 1.41 <0.020 0.0205 <0.50 15.2 0.0352 8/23/2012 1.65 0.11 0.0532 0.52 7.6 0.00126 1/22/2014 4.77 <0.020 0.0206 0.83 8.0 <0.0066 7/17/2014 3.59 0.022 0.0161 <0.50 6.6 <0.0066 1/13/2015 3.16 0.095 0.0059 <0.50 5.9 <0.0066 7/21/2015 2.63 0.050 0.0478 <0.50 5.4 0.0015 J 1/19/2016 1.63 0.089 0.0176 <0.50 6.0 0.0017 J 1. All concentrations are in milligrams per liter (mg/L). 2. "<" = Not detected above laboratory reporting limit. 3. Dissolved oxygen readings collected in the field with water quality equipment. 4. Values in bold indicate levels greater than the laboratory reporting limit. DMW-4 DMW-5 IMW-1 IMW-2 DMW-1 DMW-2 DMW-3 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 3/13/2008 36.00 -- 64.00 7/28/2010 32.50 -- 67.50 2/2/2012 35.97 -- 64.03 8/22/2012 35.92 -- 64.08 1/20/2014 32.42 -- 67.58 7/16/2014 32.68 -- 67.32 1/13/2015 34.14 -- 65.86 7/22/2015 34.27 --65.73 1/20/2016 33.23 --66.77 3/13/2009 35.66 -- 63.90 7/28/2010 NM -- N/A 2/2/2012 35.70 -- 63.86 8/22/2012 35.55 -- 64.01 1/20/2014 32.31 -- 67.25 7/16/2014 32.15 -- 67.41 1/13/2015 34.05 -- 65.51 7/22/2015 33.98 --65.58 1/20/2016 33.04 --66.52 3/13/2009 26.92 -- 63.27 7/28/2010 NM -- N/A 2/2/2012 26.70 -- 63.49 8/22/2012 26.75 -- 63.44 1/20/2014 23.13 -- 67.06 7/16/2014 23.31 -- 66.88 1/13/2015 24.81 -- 65.38 7/22/2015 25.35 --64.84 3/13/2009 27.85 -- 64.32 7/28/2010 24.65 -- 67.52 2/2/2012 27.75 -- 64.42 8/22/2012 27.83 -- 64.34 1/20/2014 24.09 -- 68.08 7/16/2014 24.54 -- 67.63 1/13/2015 25.95 -- 66.22 7/22/2015 26.44 --65.73 11/16/2009 36.05 -- 64.13 7/28/2010 32.58 -- 67.60 2/2/2012 35.97 -- 64.21 8/22/2012 35.93 -- 64.25 1/20/2014 32.38 -- 67.80 7/16/2014 32.53 -- 67.65 1/13/2015 34.28 -- 65.90 7/22/2015 34.24 --65.94 1/20/2016 33.11 --67.07 11/16/2009 35.85 -- 63.86 7/28/2010 32.30 -- 67.41 2/2/2012 35.82 -- 63.89 8/22/2012 35.73 -- 63.98 1/20/2014 32.50 -- 67.21 7/16/2014 Mud -- Mud 1/13/2015 Mud -- Mud 7/22/2015 Mud -- Mud 1/20/2016 Mud -- Mud 11/16/2009 34.86 -- 63.64 7/28/2010 31.20 -- 67.30 2/2/2012 34.88 -- 63.62 8/22/2012 34.71 -- 63.79 1/20/2014 31.66 -- 66.84 7/16/2014 30.87 -- 67.63 1/13/2015 33.66 -- 64.84 7/22/2015 33.21 --65.29 1/20/2016 32.34 --66.16 0.010 46 31-46 99.56 0.010 44 29-44 98.50 MW-6 11/4/2009 2 0.010 45 25-45 99.71 0.010 35 20-35 100.1830-45450.010211/5/2009 MW-1 12/4/2008 2 0.010 48 33-48 100.00 MW-2 3/10/2009 2 90.19 MW-4 3/10/2009 2 0.010 40 25-40 92.17 MW-3 3/10/2009 2 MW-5 MW-7 11/5/2009 2 Page 1 of 4 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 11/16/2009 34.60 -- 63.86 7/28/2010 30.10 -- 68.36 2/2/2012 36.94 2.97 64.07 8/22/2012 34.92 0.53 63.99 1/20/2014 31.51 0.44 67.33 7/16/2014 31.30 0.12 67.26 1/13/2015 33.18 0.12 65.38 7/22/2015 32.85 --65.61 1/20/2016 31.92 --66.54 7/28/2010 24.17 -- 66.65 2/2/2012 26.65 -- 64.17 8/22/2012 26.73 -- 64.09 1/20/2014 23.04 -- 67.78 7/16/2014 23.99 -- 66.83 1/13/2015 25.05 -- 65.77 7/22/2015 25.98 --64.84 7/28/2010 32.16 -- 66.18 2/2/2012 36.35 -- 61.99 8/22/2012 34.86 -- 63.48 1/20/2014 32.03 -- 66.31 7/16/2014 31.99 -- 66.35 1/13/2015 33.66 -- 64.68 7/22/2015 33.79 --64.55 7/28/2010 31.27 -- 66.49 2/2/2012 35.41 -- 62.35 8/22/2012 34.13 -- 63.63 1/20/2014 31.27 -- 66.49 7/16/2014 30.99 -- 66.77 1/13/2015 33.03 -- 64.73 7/21/2015 32.64 --65.12 1/20/2016 32.16 --65.60 7/28/2010 31.59 -- 66.17 2/2/2012 35.50 -- 62.26 8/22/2012 34.29 -- 63.47 1/20/2014 31.59 -- 66.17 7/16/2014 31.61 -- 66.15 1/13/2015 32.18 -- 65.58 7/21/2015 31.17 --66.59 1/19/2016 31.31 --66.45 2/2/2012 37.08 -- 63.34 8/22/2012 36.83 -- 63.59 1/20/2014 33.24 -- 67.18 7/16/2014 33.69 -- 66.73 1/13/2015 35.62 -- 64.80 7/21/2015 35.48 --64.94 2/2/2012 34.50 -- 60.76 8/22/2012 34.22 -- 61.04 1/20/2014 31.60 -- 63.66 7/16/2014 31.65 -- 63.61 1/13/2015 33.19 -- 62.07 7/21/2015 31.70 --63.56 1/19/2016 31.26 --64.00 2/2/2012 35.00 -- 58.57 8/22/2012 34.11 -- 59.46 1/20/2014 31.93 -- 61.64 7/16/2014 31.28 -- 62.29 1/13/2015 33.53 -- 60.04 7/21/2015 33.53 --60.04 40 25-40 97.33 MW-11 7/27/2010 2 0.010 40 25-40 97.76 MW-12 7/27/2010 2 0.010 100.422 0.010 45 30-45 MW-14 1/26/2012 2 0.010 MW-15 1/24/2012 2 0.010 43 28-43 90.82 MW-10 7/27/2010 2 0.010 40 25-40 98.34 MW-9 7/27/2010 2 0.010 30 15-30 93.57 43 98.4629-44440.010211/5/2009MW-8 28-43 95.26 MW-13 1/23/2012 Page 2 of 4 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 2/2/2012 26.23 -- 60.28 8/22/2012 26.46 -- 60.05 1/20/2014 22.83 -- 63.68 7/16/2014 23.03 -- 63.48 1/13/2015 25.14 -- 61.37 7/21/2015 25.54 --60.97 2/2/2012 24.08 -- 57.87 8/22/2012 24.15 -- 57.80 1/20/2014 21.16 -- 60.79 7/16/2014 21.38 -- 60.57 1/13/2015 23.01 -- 58.94 7/21/2015 23.43 --58.52 2/2/2012 24.99 -- 48.37 8/22/2012 25.67 -- 47.69 1/20/2014 22.24 -- 51.12 7/16/2014 22.94 -- 50.42 1/13/2015 23.77 -- 49.59 7/21/2015 1/19/2016 21.85 --51.51 2/2/2012 32.48 -- 46.04 8/22/2012 31.98 -- 46.54 1/20/2014 28.70 -- 49.82 7/16/2014 28.77 -- 49.75 1/13/2015 30.65 -- 47.87 7/21/2015 31.40 --47.12 2/2/2012 40.39 -- 45.11 8/22/2012 39.79 -- 45.71 1/20/2014 36.62 -- 48.88 7/16/2014 35.89 -- 49.61 1/13/2015 38.81 -- 46.69 7/21/2015 38.83 --46.67 2/2/2012 38.61 -- 43.88 8/22/2012 37.19 -- 45.30 1/20/2014 35.66 -- 46.83 7/16/2014 35.39 -- 47.10 1/13/2015 37.84 -- 44.65 7/21/2015 36.18 --46.31 4/3/2012 24.97 -- 60.42 8/22/2012 24.99 -- 60.40 1/20/2014 22.45 -- 62.94 7/16/2014 22.65 -- 62.74 1/13/2015 23.82 -- 61.57 7/21/2015 24.18 --61.21 1/19/2016 22.77 --62.62 2/2/2012 34.58 -- 60.77 8/22/2012 35.95 -- 59.40 1/20/2014 31.81 -- 63.54 7/16/2014 31.68 -- 63.67 1/13/2015 33.05 -- 62.30 7/21/2015 32.84 --62.51 1/19/2016 32.41 --62.94 4/3/2012 32.81 -- 52.28 8/22/2012 27.14 -- 57.95 1/20/2014 24.41 -- 60.68 7/16/2014 24.25 -- 60.84 1/13/2015 26.05 -- 59.04 7/22/2015 26.48 --58.61 1/19/2016 26.70 --58.39 Well Obstructed by Aboveground Pool MW-19 1/23/2012 2 2 0.010 80 70-80 85.09 95.3559-64640.010 20-35 86.51 85.3918-3333 30 15-30 73.36 78.52 MW-16 1/23/2012 MW-17 1/24/2012 2 0.010 0.010 MW-21 1/24/2012 21/26/2012 3/23/2012 & 3/30/2012IMW-2 IMW-1 0.01023/23/2012MW-22 1/23/2012MW-18 2 2 39 24-39 0.010 29 14-29 81.95 2 0.010 35 0.010 47.5 32.5-47.5 82.49 MW-20 1/26/2012 2 0.010 47 32-47 85.50 Page 3 of 4 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 11/16/2009 36.24 -- 63.97 7/28/2010 33.10 -- 67.11 2/2/2012 36.20 -- 64.01 8/22/2012 36.18 -- 64.03 1/20/2014 32.52 -- 67.69 7/16/2014 32.94 -- 67.27 1/13/2015 34.49 -- 65.72 7/22/2015 34.63 --65.58 1/20/2016 33.40 --66.81 7/28/2010 24.73 -- 66.12 2/2/2012 28.58 -- 62.27 8/22/2012 27.34 -- 63.51 1/20/2014 23.87 -- 66.98 7/16/2014 24.46 -- 66.39 1/13/2015 25.34 -- 65.51 7/22/2015 26.54 --64.31 1/20/2016 23.87 --66.98 2/2/2012 45.90 -- 53.25 8/22/2012 36.05 -- 63.10 1/20/2014 31.25 -- 67.90 7/16/2014 32.45 -- 66.70 1/13/2015 33.98 -- 65.17 7/22/2015 33.91 --65.24 1/20/2016 32.90 --66.25 2/2/2012 36.41 -- 50.57 8/22/2012 36.30 -- 50.68 1/20/2014 32.53 -- 54.45 7/16/2014 32.23 -- 54.75 1/13/2015 34.36 -- 52.62 7/21/2015 34.73 --52.25 1/19/2016 34.16 --52.82 4/3/2012 33.08 -- 52.17 8/22/2012 25.88 -- 59.37 1/20/2014 22.47 -- 62.78 7/16/2014 22.81 -- 62.44 1/13/2015 24.25 -- 61.00 7/21/2015 24.73 --60.52 1/19/2016 41.18 --44.07 Note: * Elevations are based on an assumed TOC datum of 100.00 feet at MW-1. If free product is present in well, groundwater elevation is calculated by [Top of Casing Elevation-Depth to Water]+[free product thickness x 0.8581] 2 0.010 130 110-130 86.981/27/2012- 1/31/2012DMW-4 DMW-3 DMW-2 7/26/2010- 7/27/2010 1/26/2012- 1/30/2012 2 2 0.0102DMW-1 11/4/2009- 11/5/2009 75 70-75 130 110-130 85.25 0.010 0.010 95 90-95 90.85 99.15118-123123 100.21 DMW-5 3/29/2012- 3/30/2012 2 0.010 Page 4 of 4 Table 8 Groundwater Sampling Water Quality Parameter Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Temperature (°C) Conductivity (mS/cm) Dissolved Oxygen (mg/L) H (standard units) Oxidation Reduction Potential (mV) MW-1 12/4/2008 1/20/2016 48 100.00 12.87 0.069 1.74 5.40 290.0 MW-2 3/10/2009 1/20/2016 46 99.56 14.31 0.065 1.40 5.77 162.0 MW-5 11/5/2009 1/20/2016 45 100.18 12.32 0.080 2.23 5.27 295.0 MW-6 11/4/2009 1/19/2016 45 99.71 MW-7 11/5/2009 1/20/2016 44 98.50 13.91 0.066 1.38 5.38 157.0 MW-8 11/5/2009 1/20/2016 44 98.46 MW-11 7/27/2010 1/20/2016 40 97.76 11.67 0.435 1.72 4.62 336.0 MW-12 7/27/2010 1/19/2016 40 97.33 13.75 0.231 3.01 4.42 289.0 MW-14 1/26/2012 1/19/2016 43 95.26 13.82 0.059 3.35 5.22 253.0 MW-18 1/23/2012 1/19/2016 30 73.36 11.41 0.107 3.26 6.01 92.0 MW-22 3/23/2012 1/19/2016 33 85.39 11.84 0.075 2.85 5.09 191.0 IMW-1 1/26/2012 1/19/2016 64 95.35 13.16 0.074 1.49 5.04 265.0 IMW-2 3/23&30/2012 1/19/2016 80 85.09 11.98 0.154 3.39 9.62 133.0 DMW-1 11/4-5/2009 1/20/2016 75 100.21 11.80 0.085 2.26 5.80 288.0 DMW-2 7/26-27/2010 1/20/2016 95 90.85 11.89 0.123 1.35 9.48 23.0 DMW-3 1/26-30/2012 1/20/2016 123 99.15 11.99 0.110 1.91 8.29 258.0 DMW-4 1/27-31/2012 1/19/2016 130 86.98 13.12 1.910 1.41 13.09 -320.0 DMW-5 3/29-30/2012 1/19/2016 130 85.25 11.65 0.178 1.63 10.07 101.0 PW-1 unknown 1/20/2016 unknown unknown 11.75 0.143 1.90 7.92 121.0 PW-18 unknown 1/20/2016 unknown unknown 11.53 0.095 1.64 7.63 139.0 Note: MW-1 top of casing assumed to be 100.00 feet for well elevation survey Not Measured Due To Mud/Sediment in Well Sheen/Strong Odor (Sample Only) Top of Casing Elevation (feet) Water Quality Parameters Well ID Date of Installation Date Liquid Gauged Total Depth (feet) Groundwater Elevation Difference Elevation at Midpoint of Screen/Water Column Difference (feet) (feet) (feet) (feet) MW-2 66.52 60.04 Upward DMW-1 66.81 -5.69 ↑ MW-2 66.52 60.04 Downward DMW-3 66.25 -54.25 ↓ DMW-1 66.81 -5.69 Downward DMW-3 66.25 -54.25 ↓ MW-14 64.00 58.13 Downward IMW-1 62.94 1.44 ↓ MW-22 62.62 57.51 Downward IMW-2 58.39 -16.61 ↓ MW-22 62.62 57.51 Downward DMW-5 44.07 -75.93 ↓ IMW-2 58.39 -16.61 Downward DMW-5 44.07 -75.93 ↓ Water level data collected on 1/19/2016 and 1/20/2016. N/A = Not Applicable 14.32 59.32 -0.2414 Vertical gradients calculated using the midpoint of the screen for IMW and DMW wells and the midpoint of the water column for the MW wells. Table 9 Vertical Hydraulic Gradient Evaluations Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina 18.55 133.44 0.1390 4.23 74.12 0.0571 1.06 56.69 0.0187 -0.29 65.73 -0.0044 0.56 48.56 0.0115 0.27 114.29 0.0024 Facility ID Number 0-004593 Incident Number: 28649 Well Pair Vertical Gradient Table 10 Free Product Recovery Information Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number 28649 Date Well ID Free Product Recovery Method Product Thickness Before Recovery (Feet) Product Thickness After Recovery (Feet) Amount of Vaporized Product (Gallons) Amount of Liquid (Water and Product) (Gallons) Amount of Liquid Product (Gallons) Total Amount of Product Recovered (Gallons) 3/28/2012 MW-8 AFVR 2.15 0.01 6.76 226 44 50.76 6/28/2012 MW-8 AFVR 0.48 0.00 6.07 231 0.00 6.07 9/28/2012 MW-8 AFVR 0.26 0.00 8.68 231 0.00 8.68 12/13/2012 MW-8 AFVR 0.69 0.00 12.79 226 0.00 12.79 3/14/2013 MW-8 AFVR 0.31 0.00 5.34 231 0.00 5.34 7/24/2013 MW-8 AFVR 0.94 0.00 2.97 189 0.00 2.97 9/16/2013 MW-8 AFVR 0.61 0.00 5.34 270 0.00 5.34 12/18/2013 MW-8 AFVR 1.12 0.00 6.22 310 0.00 6.22 AFVR = Aggressive Fluid/Vapor Recovery 12/13/2012 3/14/2013 7/24/2013 9/16/2013 12/18/2013 78.30 83.64 86.61 91.95 98.17 12.79 5.34 2.97 5.34 6.22 56.83 9/28/2012 8.68 65.51 Date of Recovery Event Total Volume of Free Product Recovered from Site During Current Recovery Event (Gallons) Cumulative Total Volume Recovered to Date from All Recovery Events (Gallons) 3/28/2012 50.76 50.76 6/28/2012 6.07 Date Cross-Sectional Area of Pipe Conversion Factor3 Days of Operation Cumulative Recovery (ft2) (lb-m3/mg-ft3)(lb/hr) (lb/day) (days) (lbs) 04/04/14* 0.08700 1,116 97.09 413 0.00000006243 0.1502 3.60 9.00 32.44 07/10/14 0.08700 1,116 97.09 6.04 0.00000006243 0.0022 0.05 97.00 37.56 10/27/14 0.08700 714 62.12 281.0 0.00000006243 0.0654 1.57 109.00 208.6 03/04/15 0.08700 719 62.55 313.0 0.00000006243 0.0733 1.760 128.00 433.9 06/18/15* 0.08700 763 66.38 26.30 0.00000006243 0.0065 0.1569 106.00 450.5 10/29/15 0.08700 603 52.46 275.0 0.00000006243 0.05404 1.2970 32.00 492.0 12/15/15 0.08700 647 56.29 476.0 0.00000006243 0.10036 2.4087 47.00 605.2 04/04/14* 0.08700 626 54.46 0.64 0.00000006243 0.0001 0.003 9.00 0.02820 07/10/14 10/27/14 0.08700 575 50.03 0.45 0.00000006243 0.0001 0.002 87.00 0.2043 03/04/15 0.08700 523 45.50 0.00 0.00000006243 0.0000 0.000 128.00 0.2043 06/18/15* 0.08700 731 63.60 0.00 0.00000006243 0.0000 0.000 106.00 0.2043 10/29/15 0.08700 528 45.94 0.00 0.00000006243 0.0000 0.000 55.00 0.2043 12/15/15 0.08700 368 32.02 0.00 0.00000006243 0.0000 0.000 47.00 0.2043 Notes: * Effluent velocity inferred; reading not collected 4. Mass removal rate = (air flow rate) x (total BTEX) x (conversion factor) x (60 min/hr or 1,440 min/day) 1. Air flow rate = (cross-sectional area) x (effluent velocity) 2. Total BTEX concentrations in effluent air are based on EPA Method 18 laboratory data 3. Conversion factor to convert units of concentration from mg/m3 to lb/ft3 On-Site System Table 11 SVE System Cumulative Recovery Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 No Sample Collected; System Down Incident Number 28649 Effluent Velocity (ft/min) Air Flow Rate1 (ft3/min) Total BTEX2 (mg/m3) Mass Removal Rate4 Off-Site System FIGURES SITE PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E DC S A I D SITE HAMBY/CAJAH'SMT PARK TRIPLETT HAMBY/CAJAH' MT PARK WILLIAMS/BRANDON APARTMENTS PRICE CHURCH SHELL CHURCH PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E PW-21 PW-20 PW-22 PW-8 PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E APPENDIX A STANDARD OPERATING PROCEDURES 23BGroundwater Levels Groundwater level measurements were obtained by using an electronic sounding/interface detection device which registers when a probe makes contact with petroleum product and/or water. Depth to groundwater measurements were obtained by lowering the device into the well until it indicated that the water surface had been encountered, at which point a measurement was taken at the top of the riser pipe or top of casing. Measurements were recorded to the nearest 0.01 foot. 24BGroundwater Sampling Groundwater samples were collected using a new, dedicated plastic bailer or pre-decontaminated submersible pump with associated new tubing. Before obtaining a sample, a minimum of three well volumes of groundwater were evacuated to ensure collection of a sample representative of the in-situ groundwater conditions. A sample was collected using a dedicated bailer, or via outflow for the tubing connected to the submersible pump and transferred to containers supplied by the laboratory, and placed in an ice-filled cooler. Chain-of-custody forms were completed and accompanied the samples to the laboratory. The submersible pump system was decontaminated between wells using alconox, deionized water, and alcohol. 25BChemical Analysis Chemical analyses for groundwater were performed by Pace Analytical Services, Inc. in Huntersville, North Carolina. Extractions and analyses were performed in accordance with standard Environmental Protection Agency (EPA) methodology. The groundwater samples were analyzed for volatile organic compounds by EPA Method 6200B including BTEX (benzene, toluene, ethylbenzene, and total xylenes), methyl-tert butyl ether (MTBE), and isopropyl ether (IPE) and for lead by EPA Method 6010. APPENDIX B LABORATORY ANALYTICAL REPORTS #=CL# January 26, 2016 LIMS USE: FR - CHRISTINE LIMS OBJECT ID: 92283542 92283542 Project: Pace Project No.: RE: Christine Schaefer ATC Group Services LLC 7606 Whitehall Executive Cente Suite 800 Charlotte, NC 28273 CAJAHS MOUNTAIN Dear Christine Schaefer: Enclosed are the analytical results for sample(s) received by the laboratory on January 19, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Dale Ingram dale.ingram@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 37 #=CP# CERTIFICATIONS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Minnesota Certification IDs 1700 Elm Street SE Suite 200, Minneapolis, MN 55414525 N 8th Street, Salina, KS 67401 A2LA Certification #: 2926.01Alaska Certification #: UST-078Alaska Certification #MN00064 Alabama Certification #40770Arizona Certification #: AZ-0014 Arkansas Certification #: 88-0680California Certification #: 01155CAColorado Certification #Pace Connecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-L Florida/NELAP Certification #: E87605Guam Certification #:14-008rGeorgia Certification #: 959 Georgia EPD #: PaceIdaho Certification #: MN00064 Hawaii Certification #MN00064Illinois Certification #: 200011Indiana Certification#C-MN-01 Iowa Certification #: 368Kansas Certification #: E-10167 Kentucky Dept of Envi. Protection - DW #90062Kentucky Dept of Envi. 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Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 37 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Lab ID Sample ID Matrix Date Collected Date Received 92283542001 IMW-1 Water 01/19/16 14:25 01/19/16 16:32 92283542002 IMW-2 Water 01/19/16 12:30 01/19/16 16:32 92283542003 DMW-4 Water 01/19/16 10:20 01/19/16 16:32 92283542004 DMW-5 Water 01/19/16 12:00 01/19/16 16:32 92283542005 MW-12 Water 01/19/16 15:05 01/19/16 16:32 92283542006 MW-14 Water 01/19/16 14:45 01/19/16 16:32 92283542007 MW-18 Water 01/19/16 11:20 01/19/16 16:32 92283542008 MW-22 Water 01/19/16 13:00 01/19/16 16:32 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 37 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92283542001 IMW-1 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283542002 IMW-2 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283542003 DMW-4 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283542004 DMW-5 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283542005 MW-12 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283542006 MW-14 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283542007 MW-18 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283542008 MW-22 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:IMW-1 Lab ID:92283542001 Collected:01/19/16 14:25 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 2.7J ug/L 01/21/16 18:41 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 9.1 ug/L 01/21/16 17:47 7439-92-101/20/16 17:305.0 2.5 1 Manganese 964 ug/L 01/21/16 17:47 7439-96-501/20/16 17:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 144 ug/L 01/21/16 12:08 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 12:08 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 12:08 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 12:08 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 12:08 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 12:08 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 12:08 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 12:08 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 12:08 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 12:08 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 12:08 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 12:08 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 12:08 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 12:08 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 12:08 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 12:08 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 12:08 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 12:08 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 12:08 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 12:08 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 12:08 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 12:08 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 12:08 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 12:08 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 12:08 75-34-30.50 0.25 1 1,2-Dichloroethane 3.2 ug/L 01/21/16 12:08 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 12:08 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 12:08 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 12:08 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 12:08 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 12:08 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 12:08 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 12:08 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 12:08 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 12:08 10061-02-60.50 0.25 1 Diisopropyl ether 11.8 ug/L 01/21/16 12:08 108-20-30.50 0.25 1 Ethylbenzene 0.80 ug/L 01/21/16 12:08 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 12:08 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)0.86 ug/L 01/21/16 12:08 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:IMW-1 Lab ID:92283542001 Collected:01/19/16 14:25 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride <2.0 ug/L 01/21/16 12:08 75-09-22.0 1.0 1 Methyl-tert-butyl ether 61.6 ug/L 01/21/16 12:08 1634-04-40.50 0.25 1 Naphthalene 4.8 ug/L 01/21/16 12:08 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 12:08 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/21/16 12:08 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 12:08 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 12:08 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 12:08 127-18-40.50 0.25 1 Toluene 0.44J ug/L 01/21/16 12:08 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 12:08 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 12:08 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 12:08 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 12:08 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 12:08 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 12:08 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 12:08 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 1.4 ug/L 01/21/16 12:08 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 1.0 ug/L 01/21/16 12:08 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 12:08 75-01-41.0 0.25 1 m&p-Xylene 4.8 ug/L 01/21/16 12:08 179601-23-11.0 0.50 1 o-Xylene 12.2 ug/L 01/21/16 12:08 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)93 %01/21/16 12:08 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/21/16 12:08 460-00-470-130 1 Toluene-d8 (S)99 %01/21/16 12:08 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 1.4J mg/L 01/21/16 16:31 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 0.34 mg/L 01/20/16 15:540.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:IMW-2 Lab ID:92283542002 Collected:01/19/16 12:30 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 1.9J ug/L 01/21/16 18:50 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 01/21/16 17:50 7439-92-101/20/16 17:305.0 2.5 1 Manganese 20.6 ug/L 01/21/16 17:50 7439-96-501/20/16 17:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 02:55 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 02:55 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 02:55 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 02:55 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 02:55 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 02:55 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 02:55 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 02:55 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 02:55 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 02:55 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 02:55 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 02:55 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 02:55 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 02:55 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 02:55 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 02:55 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 02:55 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 02:55 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 02:55 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 02:55 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 02:55 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 02:55 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 02:55 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 02:55 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 02:55 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/21/16 02:55 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 02:55 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 02:55 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 02:55 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 02:55 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 02:55 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 02:55 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 02:55 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 02:55 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 02:55 10061-02-60.50 0.25 1 Diisopropyl ether 0.55 ug/L 01/21/16 02:55 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 02:55 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 02:55 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 02:55 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:IMW-2 Lab ID:92283542002 Collected:01/19/16 12:30 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride <2.0 ug/L 01/21/16 02:55 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/21/16 02:55 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 02:55 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 02:55 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/21/16 02:55 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 02:55 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 02:55 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 02:55 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 02:55 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 02:55 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 02:55 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 02:55 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 02:55 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 02:55 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 02:55 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 02:55 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 02:55 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 02:55 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 02:55 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 02:55 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 02:55 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)96 %01/21/16 02:55 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %01/21/16 02:55 460-00-470-130 1 Toluene-d8 (S)99 %01/21/16 02:55 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 7.4 mg/L 01/21/16 16:45 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 0.053 mg/L 01/20/16 15:530.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:DMW-4 Lab ID:92283542003 Collected:01/19/16 10:20 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 35.2 ug/L 01/21/16 18:58 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 01/21/16 17:53 7439-92-101/20/16 17:305.0 2.5 1 Manganese 20.5 ug/L 01/21/16 17:53 7439-96-501/20/16 17:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 0.57 ug/L 01/21/16 03:12 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 03:12 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 03:12 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 03:12 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 03:12 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 03:12 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 03:12 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 03:12 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 03:12 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 03:12 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 03:12 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 03:12 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 03:12 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 03:12 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 03:12 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 03:12 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 03:12 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 03:12 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 03:12 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 03:12 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 03:12 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 03:12 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 03:12 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 03:12 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 03:12 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/21/16 03:12 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 03:12 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 03:12 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 03:12 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 03:12 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 03:12 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 03:12 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 03:12 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 03:12 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 03:12 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/21/16 03:12 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 03:12 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 03:12 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 03:12 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:DMW-4 Lab ID:92283542003 Collected:01/19/16 10:20 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride <2.0 ug/L 01/21/16 03:12 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.78 ug/L 01/21/16 03:12 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 03:12 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 03:12 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/21/16 03:12 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 03:12 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 03:12 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 03:12 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 03:12 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 03:12 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 03:12 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 03:12 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 03:12 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 03:12 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 03:12 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 03:12 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 03:12 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 03:12 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 03:12 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 03:12 179601-23-11.0 0.50 1 o-Xylene 0.28J ug/L 01/21/16 03:12 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)94 %01/21/16 03:12 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %01/21/16 03:12 460-00-470-130 1 Toluene-d8 (S)99 %01/21/16 03:12 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 15.2 mg/L 01/21/16 17:25 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate <0.020 mg/L 01/20/16 15:510.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:DMW-5 Lab ID:92283542004 Collected:01/19/16 12:00 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 1.7J ug/L 01/21/16 19:06 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 01/21/16 17:57 7439-92-101/20/16 17:305.0 2.5 1 Manganese 17.6 ug/L 01/21/16 17:57 7439-96-501/20/16 17:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 03:29 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 03:29 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 03:29 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 03:29 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 03:29 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 03:29 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 03:29 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 03:29 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 03:29 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 03:29 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 03:29 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 03:29 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 03:29 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 03:29 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 03:29 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 03:29 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 03:29 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 03:29 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 03:29 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 03:29 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 03:29 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 03:29 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 03:29 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 03:29 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 03:29 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/21/16 03:29 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 03:29 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 03:29 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 03:29 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 03:29 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 03:29 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 03:29 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 03:29 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 03:29 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 03:29 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/21/16 03:29 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 03:29 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 03:29 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 03:29 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:DMW-5 Lab ID:92283542004 Collected:01/19/16 12:00 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride <2.0 ug/L 01/21/16 03:29 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.28J ug/L 01/21/16 03:29 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 03:29 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 03:29 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/21/16 03:29 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 03:29 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 03:29 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 03:29 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 03:29 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 03:29 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 03:29 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 03:29 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 03:29 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 03:29 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 03:29 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 03:29 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 03:29 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 03:29 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 03:29 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 03:29 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 03:29 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)94 %01/21/16 03:29 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %01/21/16 03:29 460-00-470-130 1 Toluene-d8 (S)100 %01/21/16 03:29 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 6.0 mg/L 01/21/16 17:39 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 0.089 mg/L 01/20/16 15:520.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-12 Lab ID:92283542005 Collected:01/19/16 15:05 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 29.3 ug/L 01/25/16 14:30 7439-92-101/20/16 17:3025.0 12.5 5 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 12:24 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 12:24 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 12:24 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 12:24 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 12:24 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 12:24 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 12:24 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 12:24 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 12:24 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 12:24 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 12:24 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 12:24 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 12:24 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 12:24 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 12:24 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 12:24 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 12:24 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 12:24 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 12:24 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 12:24 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 12:24 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 12:24 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 12:24 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 12:24 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 12:24 75-34-30.50 0.25 1 1,2-Dichloroethane 0.68 ug/L 01/21/16 12:24 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 12:24 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 12:24 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 12:24 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 12:24 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 12:24 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 12:24 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 12:24 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 12:24 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 12:24 10061-02-60.50 0.25 1 Diisopropyl ether 3.2 ug/L 01/21/16 12:24 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 12:24 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 12:24 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 12:24 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/21/16 12:24 75-09-22.0 1.0 1 Methyl-tert-butyl ether 188 ug/L 01/21/16 12:24 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 12:24 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 12:24 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-12 Lab ID:92283542005 Collected:01/19/16 15:05 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/21/16 12:24 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 12:24 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 12:24 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 12:24 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 12:24 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 12:24 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 12:24 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 12:24 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 12:24 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 12:24 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 12:24 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 12:24 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 12:24 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 12:24 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 12:24 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 12:24 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 12:24 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)95 %01/21/16 12:24 17060-07-070-130 1 4-Bromofluorobenzene (S)103 %01/21/16 12:24 460-00-470-130 1 Toluene-d8 (S)101 %01/21/16 12:24 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-14 Lab ID:92283542006 Collected:01/19/16 14:45 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 40.7 ug/L 01/25/16 14:33 7439-92-101/20/16 17:3025.0 12.5 5 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 03:45 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 03:45 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 03:45 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 03:45 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 03:45 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 03:45 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 03:45 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 03:45 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 03:45 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 03:45 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 03:45 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 03:45 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 03:45 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 03:45 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 03:45 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 03:45 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 03:45 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 03:45 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 03:45 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 03:45 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 03:45 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 03:45 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 03:45 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 03:45 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 03:45 75-34-30.50 0.25 1 1,2-Dichloroethane 1.0 ug/L 01/21/16 03:45 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 03:45 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 03:45 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 03:45 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 03:45 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 03:45 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 03:45 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 03:45 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 03:45 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 03:45 10061-02-60.50 0.25 1 Diisopropyl ether 4.1 ug/L 01/21/16 03:45 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 03:45 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 03:45 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 03:45 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/21/16 03:45 75-09-22.0 1.0 1 Methyl-tert-butyl ether 122 ug/L 01/21/16 03:45 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 03:45 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 03:45 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-14 Lab ID:92283542006 Collected:01/19/16 14:45 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/21/16 03:45 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 03:45 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 03:45 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 03:45 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 03:45 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 03:45 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 03:45 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 03:45 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 03:45 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 03:45 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 03:45 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 03:45 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 03:45 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 03:45 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 03:45 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 03:45 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 03:45 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)96 %01/21/16 03:45 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %01/21/16 03:45 460-00-470-130 1 Toluene-d8 (S)98 %01/21/16 03:45 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-18 Lab ID:92283542007 Collected:01/19/16 11:20 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 14.4 ug/L 01/21/16 18:06 7439-92-101/20/16 17:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 16:19 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 16:19 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 16:19 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 16:19 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 16:19 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 16:19 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 16:19 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 16:19 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 16:19 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 16:19 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 16:19 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 16:19 75-00-31.0 0.50 1 Chloroform 0.33J ug/L 01/21/16 16:19 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 16:19 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 16:19 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 16:19 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 16:19 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 16:19 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 16:19 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 16:19 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 16:19 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 16:19 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 16:19 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 16:19 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 16:19 75-34-30.50 0.25 1 1,2-Dichloroethane 1.3 ug/L 01/21/16 16:19 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 16:19 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 16:19 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 16:19 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 16:19 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 16:19 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 16:19 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 16:19 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 16:19 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 16:19 10061-02-60.50 0.25 1 Diisopropyl ether 2.2 ug/L 01/21/16 16:19 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 16:19 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 16:19 87-68-3 L32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 16:19 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/21/16 16:19 75-09-22.0 1.0 1 Methyl-tert-butyl ether 2.8 ug/L 01/21/16 16:19 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 16:19 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 16:19 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-18 Lab ID:92283542007 Collected:01/19/16 11:20 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/21/16 16:19 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 16:19 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 16:19 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 16:19 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 16:19 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 16:19 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 16:19 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 16:19 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 16:19 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 16:19 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 16:19 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 16:19 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 16:19 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 16:19 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 16:19 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 16:19 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 16:19 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)97 %01/21/16 16:19 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %01/21/16 16:19 460-00-470-130 1 Toluene-d8 (S)98 %01/21/16 16:19 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-22 Lab ID:92283542008 Collected:01/19/16 13:00 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 21.4J ug/L 01/21/16 18:12 7439-92-101/20/16 17:3025.0 12.5 5 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 16:35 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 16:35 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 16:35 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/21/16 16:35 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 16:35 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 16:35 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 16:35 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 16:35 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 16:35 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 16:35 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 16:35 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 16:35 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/21/16 16:35 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 16:35 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 16:35 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 16:35 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 16:35 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 16:35 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 16:35 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 16:35 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 16:35 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 16:35 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 16:35 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 16:35 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 16:35 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/21/16 16:35 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 16:35 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 16:35 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 16:35 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 16:35 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 16:35 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 16:35 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 16:35 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 16:35 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 16:35 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/21/16 16:35 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 16:35 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 16:35 87-68-3 L32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 16:35 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/21/16 16:35 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.32J ug/L 01/21/16 16:35 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 16:35 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 16:35 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 37 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Sample:MW-22 Lab ID:92283542008 Collected:01/19/16 13:00 Received:01/19/16 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/21/16 16:35 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 16:35 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 16:35 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 16:35 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 16:35 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 16:35 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 16:35 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 16:35 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 16:35 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 16:35 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 16:35 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 16:35 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 16:35 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 16:35 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 16:35 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 16:35 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 16:35 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)97 %01/21/16 16:35 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/21/16 16:35 460-00-470-130 1 Toluene-d8 (S)98 %01/21/16 16:35 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: AIR/25065 RSK 175 RSK 175 RSK 175 AIR HEADSPACE Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2178463 Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Matrix:Water AnalyzedMDL Methane ug/L 1.7J 10.0 01/21/16 16:220.63 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2178464LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result 2178465 Methane ug/L 60.660.7 100 85-11510261.6 2 20 Parameter Units Dup Result Max RPD QualifiersRPDResult 92283470006 2179324SAMPLE DUPLICATE: Methane ug/L 2.0J 20ND Parameter Units Dup Result Max RPD QualifiersRPDResult 92283470015 2179325SAMPLE DUPLICATE: Methane ug/L 1.4J 20ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/20511 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004, 92283542005, 92283542006, 92283542007, 92283542008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1650969 Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004, 92283542005, 92283542006, 92283542007, 92283542008 Matrix:Water AnalyzedMDL Lead ug/L <5.0 5.0 01/21/16 16:392.5 Manganese ug/L <5.0 5.0 01/21/16 16:392.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1650970LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 482500 96 80-120 Manganese ug/L 479500 96 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1650971MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283522005 1650972 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Lead ug/L 500 95 75-12595 0 20500ND473473 Manganese ug/L 500 95 75-12594 1 2050018.1 494 487 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/35236 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92283542002, 92283542003, 92283542004, 92283542006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651275 Associated Lab Samples:92283542002, 92283542003, 92283542004, 92283542006 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 01/21/16 00:250.25 1,1,1-Trichloroethane ug/L <0.50 0.50 01/21/16 00:250.25 1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 01/21/16 00:250.25 1,1,2-Trichloroethane ug/L <0.50 0.50 01/21/16 00:250.25 1,1-Dichloroethane ug/L <0.50 0.50 01/21/16 00:250.25 1,1-Dichloroethene ug/L <0.50 0.50 01/21/16 00:250.25 1,1-Dichloropropene ug/L <0.50 0.50 01/21/16 00:250.25 1,2,3-Trichlorobenzene ug/L <2.0 2.0 01/21/16 00:251.0 1,2,3-Trichloropropane ug/L <0.50 0.50 01/21/16 00:250.25 1,2,4-Trichlorobenzene ug/L <2.0 2.0 01/21/16 00:251.0 1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 01/21/16 00:250.50 1,2-Dibromoethane (EDB)ug/L <0.50 0.50 01/21/16 00:250.25 1,2-Dichlorobenzene ug/L <0.50 0.50 01/21/16 00:250.25 1,2-Dichloroethane ug/L <0.50 0.50 01/21/16 00:250.25 1,2-Dichloropropane ug/L <0.50 0.50 01/21/16 00:250.25 1,3,5-Trimethylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 1,3-Dichlorobenzene ug/L <0.50 0.50 01/21/16 00:250.25 1,3-Dichloropropane ug/L <0.50 0.50 01/21/16 00:250.25 1,4-Dichlorobenzene ug/L <0.50 0.50 01/21/16 00:250.25 2,2-Dichloropropane ug/L <0.50 0.50 01/21/16 00:250.25 2-Chlorotoluene ug/L <0.50 0.50 01/21/16 00:250.25 4-Chlorotoluene ug/L <0.50 0.50 01/21/16 00:250.25 Benzene ug/L <0.50 0.50 01/21/16 00:250.25 Bromobenzene ug/L <0.50 0.50 01/21/16 00:250.25 Bromochloromethane ug/L <0.50 0.50 01/21/16 00:250.25 Bromodichloromethane ug/L <0.50 0.50 01/21/16 00:250.25 Bromoform ug/L <0.50 0.50 01/21/16 00:250.25 Bromomethane ug/L <5.0 5.0 01/21/16 00:250.50 Carbon tetrachloride ug/L <0.50 0.50 01/21/16 00:250.25 Chlorobenzene ug/L <0.50 0.50 01/21/16 00:250.25 Chloroethane ug/L <1.0 1.0 01/21/16 00:250.50 Chloroform ug/L <0.50 0.50 01/21/16 00:250.25 Chloromethane ug/L <1.0 1.0 01/21/16 00:250.50 cis-1,2-Dichloroethene ug/L <0.50 0.50 01/21/16 00:250.25 cis-1,3-Dichloropropene ug/L <0.50 0.50 01/21/16 00:250.25 Dibromochloromethane ug/L <0.50 0.50 01/21/16 00:250.25 Dibromomethane ug/L <0.50 0.50 01/21/16 00:250.25 Dichlorodifluoromethane ug/L <0.50 0.50 01/21/16 00:250.25 Diisopropyl ether ug/L <0.50 0.50 01/21/16 00:250.25 Ethylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651275 Associated Lab Samples:92283542002, 92283542003, 92283542004, 92283542006 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <2.0 2.0 01/21/16 00:251.0 Isopropylbenzene (Cumene)ug/L <0.50 0.50 01/21/16 00:250.25 m&p-Xylene ug/L <1.0 1.0 01/21/16 00:250.50 Methyl-tert-butyl ether ug/L <0.50 0.50 01/21/16 00:250.25 Methylene Chloride ug/L <2.0 2.0 01/21/16 00:251.0 n-Butylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 n-Propylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 Naphthalene ug/L <2.0 2.0 01/21/16 00:251.0 o-Xylene ug/L <0.50 0.50 01/21/16 00:250.25 sec-Butylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 Styrene ug/L <0.50 0.50 01/21/16 00:250.25 tert-Butylbenzene ug/L <0.50 0.50 01/21/16 00:250.25 Tetrachloroethene ug/L <0.50 0.50 01/21/16 00:250.25 Toluene ug/L <0.50 0.50 01/21/16 00:250.25 trans-1,2-Dichloroethene ug/L <0.50 0.50 01/21/16 00:250.25 trans-1,3-Dichloropropene ug/L <0.50 0.50 01/21/16 00:250.25 Trichloroethene ug/L <0.50 0.50 01/21/16 00:250.25 Trichlorofluoromethane ug/L <1.0 1.0 01/21/16 00:250.50 Vinyl chloride ug/L <1.0 1.0 01/21/16 00:250.25 1,2-Dichloroethane-d4 (S)%94 70-130 01/21/16 00:25 4-Bromofluorobenzene (S)%101 70-130 01/21/16 00:25 Toluene-d8 (S)%99 70-130 01/21/16 00:25 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651276LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 55.450 111 60-140 1,1,1-Trichloroethane ug/L 54.950 110 60-140 1,1,2,2-Tetrachloroethane ug/L 53.350 107 60-140 1,1,2-Trichloroethane ug/L 50.050 100 60-140 1,1-Dichloroethane ug/L 50.750 101 60-140 1,1-Dichloroethene ug/L 54.050 108 60-140 1,1-Dichloropropene ug/L 53.450 107 60-140 1,2,3-Trichlorobenzene ug/L 52.250 104 60-140 1,2,3-Trichloropropane ug/L 52.550 105 60-140 1,2,4-Trichlorobenzene ug/L 52.950 106 60-140 1,2,4-Trimethylbenzene ug/L 57.150 114 60-140 1,2-Dibromo-3-chloropropane ug/L 51.950 104 60-140 1,2-Dibromoethane (EDB)ug/L 56.850 114 60-140 1,2-Dichlorobenzene ug/L 51.850 104 60-140 1,2-Dichloroethane ug/L 42.950 86 60-140 1,2-Dichloropropane ug/L 51.750 103 60-140 1,3,5-Trimethylbenzene ug/L 58.250 116 60-140 1,3-Dichlorobenzene ug/L 52.550 105 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651276LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 52.550 105 60-140 1,4-Dichlorobenzene ug/L 50.750 101 60-140 2,2-Dichloropropane ug/L 52.250 104 60-140 2-Chlorotoluene ug/L 54.350 109 60-140 4-Chlorotoluene ug/L 53.850 108 60-140 Benzene ug/L 53.150 106 60-140 Bromobenzene ug/L 53.050 106 60-140 Bromochloromethane ug/L 49.750 99 60-140 Bromodichloromethane ug/L 53.350 107 60-140 Bromoform ug/L 37.950 76 60-140 Bromomethane ug/L 48.050 96 60-140 Carbon tetrachloride ug/L 59.550 119 60-140 Chlorobenzene ug/L 50.550 101 60-140 Chloroethane ug/L 48.850 98 60-140 Chloroform ug/L 48.350 97 60-140 Chloromethane ug/L 43.250 86 60-140 cis-1,2-Dichloroethene ug/L 50.150 100 60-140 cis-1,3-Dichloropropene ug/L 57.650 115 60-140 Dibromochloromethane ug/L 44.250 88 60-140 Dibromomethane ug/L 50.750 101 60-140 Dichlorodifluoromethane ug/L 39.850 80 60-140 Diisopropyl ether ug/L 52.750 105 60-140 Ethylbenzene ug/L 52.750 105 60-140 Hexachloro-1,3-butadiene ug/L 67.950 136 60-140 Isopropylbenzene (Cumene)ug/L 56.150 112 60-140 m&p-Xylene ug/L 107100 107 60-140 Methyl-tert-butyl ether ug/L 53.250 106 60-140 Methylene Chloride ug/L 47.450 95 60-140 n-Butylbenzene ug/L 57.750 115 60-140 n-Propylbenzene ug/L 55.750 111 60-140 Naphthalene ug/L 56.750 113 60-140 o-Xylene ug/L 55.750 111 60-140 sec-Butylbenzene ug/L 57.150 114 60-140 Styrene ug/L 58.250 116 60-140 tert-Butylbenzene ug/L 48.350 97 60-140 Tetrachloroethene ug/L 51.550 103 60-140 Toluene ug/L 50.550 101 60-140 trans-1,2-Dichloroethene ug/L 50.950 102 60-140 trans-1,3-Dichloropropene ug/L 55.950 112 60-140 Trichloroethene ug/L 50.150 100 60-140 Trichlorofluoromethane ug/L 54.150 108 60-140 Vinyl chloride ug/L 51.550 103 60-140 1,2-Dichloroethane-d4 (S)%94 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1651277MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283514001 1651278 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 115 60-140111 4 3020ND23.0 22.2 1,1,1-Trichloroethane ug/L 20 124 60-140117 6 3020ND24.8 23.5 1,1,2,2-Tetrachloroethane ug/L 20 115 60-140109 5 3020ND22.9 21.8 1,1,2-Trichloroethane ug/L 20 109 60-140102 7 3020ND21.9 20.4 1,1-Dichloroethane ug/L 20 116 60-140112 4 3020ND23.2 22.4 1,1-Dichloroethene ug/L 20 128 60-140122 5 3020ND25.6 24.4 1,1-Dichloropropene ug/L 20 121 60-140118 3 3020ND24.3 23.7 1,2,3-Trichlorobenzene ug/L 20 108 60-140107 1 3020ND21.6 21.4 1,2,3-Trichloropropane ug/L 20 117 60-140109 6 3020ND23.3 21.9 1,2,4-Trichlorobenzene ug/L 20 104 60-140106 2 3020ND20.8 21.2 1,2,4-Trimethylbenzene ug/L 20 138 60-140119 9 302018.9 46.5 42.6 1,2-Dibromo-3- chloropropane ug/L 20 118 60-140112 5 3020ND23.6 22.4 1,2-Dibromoethane (EDB)ug/L 20 121 60-140115 4 3020ND24.1 23.1 1,2-Dichlorobenzene ug/L 20 115 60-140109 5 3020ND22.9 21.7 1,2-Dichloroethane ug/L 20 94 60-14089 5 3020ND18.9 18.0 1,2-Dichloropropane ug/L 20 114 60-140110 4 3020ND22.7 21.9 1,3,5-Trimethylbenzene ug/L 20 123 60-140119 3 30202.2 26.7 25.9 1,3-Dichlorobenzene ug/L 20 112 60-140109 3 3020ND22.4 21.8 1,3-Dichloropropane ug/L 20 114 60-140107 6 3020ND22.8 21.5 1,4-Dichlorobenzene ug/L 20 110 60-140107 3 3020ND22.1 21.4 2,2-Dichloropropane ug/L 20 106 60-140103 4 3020ND21.3 20.5 2-Chlorotoluene ug/L 20 117 60-140102 14 3020ND23.4 20.4 4-Chlorotoluene ug/L 20 118 60-140113 4 3020ND23.6 22.7 Benzene ug/L 20 120 60-140116 4 30201.9 25.9 25.0 Bromobenzene ug/L 20 115 60-140112 2 3020ND23.0 22.4 Bromochloromethane ug/L 20 110 60-140107 3 3020ND22.0 21.4 Bromodichloromethane ug/L 20 109 60-140106 3 3020ND21.9 21.2 Bromoform ug/L 20 81 60-14077 4 3020ND16.1 15.5 Bromomethane ug/L 20 96 60-14096 0 3020ND19.3 19.3 Carbon tetrachloride ug/L 20 129 60-140124 4 3020ND25.8 24.8 Chlorobenzene ug/L 20 115 60-140108 6 3020ND23.0 21.6 Chloroethane ug/L 20 119 60-140112 6 3020ND23.8 22.5 Chloroform ug/L 20 110 60-140106 3 3020ND22.2 21.5 Chloromethane ug/L 20 104 60-140102 1 3020ND20.7 20.4 cis-1,2-Dichloroethene ug/L 20 114 60-140108 5 3020ND22.7 21.6 cis-1,3-Dichloropropene ug/L 20 112 60-140110 2 3020ND22.4 21.9 Dibromochloromethane ug/L 20 93 60-14089 4 3020ND18.5 17.8 Dibromomethane ug/L 20 110 60-140106 4 3020ND22.0 21.2 Dichlorodifluoromethane ug/L 20 96 60-14093 3 3020ND19.2 18.6 Diisopropyl ether ug/L 20 115 60-140111 3 3020ND23.2 22.4 Ethylbenzene ug/L 20 119 60-140113 4 30201.7 25.5 24.4 Hexachloro-1,3-butadiene ug/L 20 130 60-140128 2 3020ND25.9 25.5 Isopropylbenzene (Cumene)ug/L 20 122 60-140117 3 30202.5 26.8 26.0 m&p-Xylene ug/L 40 121 60-140115 5 30402.4 50.6 48.2 Methyl-tert-butyl ether ug/L 20 112 60-140109 2 3020ND22.5 22.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1651277MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283514001 1651278 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 106 60-140101 5 3020ND21.1 20.1 n-Butylbenzene ug/L 20 130 60-140126 2 3020ND25.9 25.3 n-Propylbenzene ug/L 20 121 60-140116 4 30203.7 27.8 26.8 Naphthalene ug/L 20 135 60-140131 3 3020ND27.0 26.2 o-Xylene ug/L 20 123 60-140118 4 30200.96 25.6 24.5 sec-Butylbenzene ug/L 20 112 60-140110 1 30206.3 28.8 28.4 Styrene ug/L 20 125 60-140120 4 3020ND25.0 24.0 tert-Butylbenzene ug/L 20 99 60-14099 0 3020ND19.9 19.8 Tetrachloroethene ug/L 20 112 60-140108 3 3020ND22.4 21.6 Toluene ug/L 20 116 60-140109 6 3020ND23.6 22.2 trans-1,2-Dichloroethene ug/L 20 119 60-140113 4 3020ND23.7 22.7 trans-1,3-Dichloropropene ug/L 20 113 60-140109 4 3020ND22.7 21.9 Trichloroethene ug/L 20 115 60-140108 6 3020ND22.9 21.6 Trichlorofluoromethane ug/L 20 131 60-140124 6 3020ND26.2 24.7 Vinyl chloride ug/L 20 122 60-140122 0 3020ND24.4 24.3 1,2-Dichloroethane-d4 (S)%92 70-13094 4-Bromofluorobenzene (S)%100 70-130100 Toluene-d8 (S)%99 70-13099 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/35241 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92283542001, 92283542005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651591 Associated Lab Samples:92283542001, 92283542005 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 01/21/16 08:130.25 1,1,1-Trichloroethane ug/L <0.50 0.50 01/21/16 08:130.25 1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 01/21/16 08:130.25 1,1,2-Trichloroethane ug/L <0.50 0.50 01/21/16 08:130.25 1,1-Dichloroethane ug/L <0.50 0.50 01/21/16 08:130.25 1,1-Dichloroethene ug/L <0.50 0.50 01/21/16 08:130.25 1,1-Dichloropropene ug/L <0.50 0.50 01/21/16 08:130.25 1,2,3-Trichlorobenzene ug/L <2.0 2.0 01/21/16 08:131.0 1,2,3-Trichloropropane ug/L <0.50 0.50 01/21/16 08:130.25 1,2,4-Trichlorobenzene ug/L <2.0 2.0 01/21/16 08:131.0 1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 01/21/16 08:130.50 1,2-Dibromoethane (EDB)ug/L <0.50 0.50 01/21/16 08:130.25 1,2-Dichlorobenzene ug/L <0.50 0.50 01/21/16 08:130.25 1,2-Dichloroethane ug/L <0.50 0.50 01/21/16 08:130.25 1,2-Dichloropropane ug/L <0.50 0.50 01/21/16 08:130.25 1,3,5-Trimethylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 1,3-Dichlorobenzene ug/L <0.50 0.50 01/21/16 08:130.25 1,3-Dichloropropane ug/L <0.50 0.50 01/21/16 08:130.25 1,4-Dichlorobenzene ug/L <0.50 0.50 01/21/16 08:130.25 2,2-Dichloropropane ug/L <0.50 0.50 01/21/16 08:130.25 2-Chlorotoluene ug/L <0.50 0.50 01/21/16 08:130.25 4-Chlorotoluene ug/L <0.50 0.50 01/21/16 08:130.25 Benzene ug/L <0.50 0.50 01/21/16 08:130.25 Bromobenzene ug/L <0.50 0.50 01/21/16 08:130.25 Bromochloromethane ug/L <0.50 0.50 01/21/16 08:130.25 Bromodichloromethane ug/L <0.50 0.50 01/21/16 08:130.25 Bromoform ug/L <0.50 0.50 01/21/16 08:130.25 Bromomethane ug/L <5.0 5.0 01/21/16 08:130.50 Carbon tetrachloride ug/L <0.50 0.50 01/21/16 08:130.25 Chlorobenzene ug/L <0.50 0.50 01/21/16 08:130.25 Chloroethane ug/L <1.0 1.0 01/21/16 08:130.50 Chloroform ug/L <0.50 0.50 01/21/16 08:130.25 Chloromethane ug/L <1.0 1.0 01/21/16 08:130.50 cis-1,2-Dichloroethene ug/L <0.50 0.50 01/21/16 08:130.25 cis-1,3-Dichloropropene ug/L <0.50 0.50 01/21/16 08:130.25 Dibromochloromethane ug/L <0.50 0.50 01/21/16 08:130.25 Dibromomethane ug/L <0.50 0.50 01/21/16 08:130.25 Dichlorodifluoromethane ug/L <0.50 0.50 01/21/16 08:130.25 Diisopropyl ether ug/L <0.50 0.50 01/21/16 08:130.25 Ethylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651591 Associated Lab Samples:92283542001, 92283542005 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <2.0 2.0 01/21/16 08:131.0 Isopropylbenzene (Cumene)ug/L <0.50 0.50 01/21/16 08:130.25 m&p-Xylene ug/L <1.0 1.0 01/21/16 08:130.50 Methyl-tert-butyl ether ug/L <0.50 0.50 01/21/16 08:130.25 Methylene Chloride ug/L <2.0 2.0 01/21/16 08:131.0 n-Butylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 n-Propylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 Naphthalene ug/L <2.0 2.0 01/21/16 08:131.0 o-Xylene ug/L <0.50 0.50 01/21/16 08:130.25 sec-Butylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 Styrene ug/L <0.50 0.50 01/21/16 08:130.25 tert-Butylbenzene ug/L <0.50 0.50 01/21/16 08:130.25 Tetrachloroethene ug/L <0.50 0.50 01/21/16 08:130.25 Toluene ug/L <0.50 0.50 01/21/16 08:130.25 trans-1,2-Dichloroethene ug/L <0.50 0.50 01/21/16 08:130.25 trans-1,3-Dichloropropene ug/L <0.50 0.50 01/21/16 08:130.25 Trichloroethene ug/L <0.50 0.50 01/21/16 08:130.25 Trichlorofluoromethane ug/L <1.0 1.0 01/21/16 08:130.50 Vinyl chloride ug/L <1.0 1.0 01/21/16 08:130.25 1,2-Dichloroethane-d4 (S)%94 70-130 01/21/16 08:13 4-Bromofluorobenzene (S)%102 70-130 01/21/16 08:13 Toluene-d8 (S)%100 70-130 01/21/16 08:13 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651592LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 55.750 111 60-140 1,1,1-Trichloroethane ug/L 55.850 112 60-140 1,1,2,2-Tetrachloroethane ug/L 54.650 109 60-140 1,1,2-Trichloroethane ug/L 51.150 102 60-140 1,1-Dichloroethane ug/L 52.350 105 60-140 1,1-Dichloroethene ug/L 55.250 110 60-140 1,1-Dichloropropene ug/L 54.950 110 60-140 1,2,3-Trichlorobenzene ug/L 52.950 106 60-140 1,2,3-Trichloropropane ug/L 53.450 107 60-140 1,2,4-Trichlorobenzene ug/L 52.250 104 60-140 1,2,4-Trimethylbenzene ug/L 58.250 116 60-140 1,2-Dibromo-3-chloropropane ug/L 52.050 104 60-140 1,2-Dibromoethane (EDB)ug/L 57.250 114 60-140 1,2-Dichlorobenzene ug/L 52.450 105 60-140 1,2-Dichloroethane ug/L 42.750 85 60-140 1,2-Dichloropropane ug/L 53.550 107 60-140 1,3,5-Trimethylbenzene ug/L 58.550 117 60-140 1,3-Dichlorobenzene ug/L 53.050 106 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651592LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 53.550 107 60-140 1,4-Dichlorobenzene ug/L 51.550 103 60-140 2,2-Dichloropropane ug/L 48.550 97 60-140 2-Chlorotoluene ug/L 55.550 111 60-140 4-Chlorotoluene ug/L 55.350 111 60-140 Benzene ug/L 55.150 110 60-140 Bromobenzene ug/L 52.250 104 60-140 Bromochloromethane ug/L 50.050 100 60-140 Bromodichloromethane ug/L 54.550 109 60-140 Bromoform ug/L 39.650 79 60-140 Bromomethane ug/L 51.450 103 60-140 Carbon tetrachloride ug/L 60.050 120 60-140 Chlorobenzene ug/L 51.450 103 60-140 Chloroethane ug/L 51.450 103 60-140 Chloroform ug/L 49.250 98 60-140 Chloromethane ug/L 45.850 92 60-140 cis-1,2-Dichloroethene ug/L 51.550 103 60-140 cis-1,3-Dichloropropene ug/L 57.450 115 60-140 Dibromochloromethane ug/L 44.050 88 60-140 Dibromomethane ug/L 50.950 102 60-140 Dichlorodifluoromethane ug/L 38.250 76 60-140 Diisopropyl ether ug/L 53.350 107 60-140 Ethylbenzene ug/L 53.950 108 60-140 Hexachloro-1,3-butadiene ug/L 67.850 136 60-140 Isopropylbenzene (Cumene)ug/L 57.550 115 60-140 m&p-Xylene ug/L 109100 109 60-140 Methyl-tert-butyl ether ug/L 53.150 106 60-140 Methylene Chloride ug/L 47.650 95 60-140 n-Butylbenzene ug/L 57.550 115 60-140 n-Propylbenzene ug/L 56.350 113 60-140 Naphthalene ug/L 57.450 115 60-140 o-Xylene ug/L 57.050 114 60-140 sec-Butylbenzene ug/L 57.350 115 60-140 Styrene ug/L 59.950 120 60-140 tert-Butylbenzene ug/L 48.850 98 60-140 Tetrachloroethene ug/L 52.450 105 60-140 Toluene ug/L 51.950 104 60-140 trans-1,2-Dichloroethene ug/L 52.550 105 60-140 trans-1,3-Dichloropropene ug/L 56.350 113 60-140 Trichloroethene ug/L 50.950 102 60-140 Trichlorofluoromethane ug/L 54.150 108 60-140 Vinyl chloride ug/L 54.050 108 60-140 1,2-Dichloroethane-d4 (S)%93 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/42669 SM 3500-Fe B SM 3500-Fe B Iron, Ferrous Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1653004 Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Matrix:Water AnalyzedMDL Iron, Ferrous mg/L <0.50 0.50 N201/25/16 17:050.50 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1653005LABORATORY CONTROL SAMPLE: LCSSpike Iron, Ferrous mg/L 1.6 N21.5 108 90-110 Parameter Units Dup Result Max RPD QualifiersRPDResult 92283542003 1653006SAMPLE DUPLICATE: Iron, Ferrous mg/L <0.50 H1,N210<0.50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/26180 EPA 300.0 EPA 300.0 300.0 IC Anions Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651465 Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Matrix:Water AnalyzedMDL Sulfate mg/L <2.0 2.0 01/21/16 11:041.0 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651466LABORATORY CONTROL SAMPLE: LCSSpike Sulfate mg/L 18.820 94 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 1651467MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283437001 1651468 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Sulfate mg/L M620-280 90-110-25 2 1020334032903340 Parameter Units MS Result % Rec Limits Qual% RecConc. 1651469MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283542002 1651470 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Sulfate mg/L 20 98 90-11099 1 10207.4 26.9 27.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 37 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/26168 EPA 353.2 EPA 353.2 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651186 Associated Lab Samples:92283542001, 92283542002, 92283542003, 92283542004 Matrix:Water AnalyzedMDL Nitrogen, Nitrate mg/L <0.020 0.020 01/20/16 15:390.010 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651187LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 2.52.5 101 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 1651188MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283452001 1651189 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Nitrogen, Nitrate mg/L 2.5 95 90-11096 1 102.5ND 2.4 2.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 37 #=QL# QUALIFIERS Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C Pace Analytical Services - MinneapolisPASI-M ANALYTE QUALIFIERS Analysis conducted outside the EPA method holding time.H1 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6 The lab does not hold TNI accreditation for this parameter.N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 37 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92283542 CAJAHS MOUNTAIN Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92283542001 AIR/25065IMW-1 RSK 175 92283542002 AIR/25065IMW-2 RSK 175 92283542003 AIR/25065DMW-4 RSK 175 92283542004 AIR/25065DMW-5 RSK 175 92283542001 MPRP/20511 ICP/18508IMW-1 EPA 3010A EPA 6010 92283542002 MPRP/20511 ICP/18508IMW-2 EPA 3010A EPA 6010 92283542003 MPRP/20511 ICP/18508DMW-4 EPA 3010A EPA 6010 92283542004 MPRP/20511 ICP/18508DMW-5 EPA 3010A EPA 6010 92283542005 MPRP/20511 ICP/18508MW-12 EPA 3010A EPA 6010 92283542006 MPRP/20511 ICP/18508MW-14 EPA 3010A EPA 6010 92283542007 MPRP/20511 ICP/18508MW-18 EPA 3010A EPA 6010 92283542008 MPRP/20511 ICP/18508MW-22 EPA 3010A EPA 6010 92283542001 MSV/35241IMW-1 SM 6200B 92283542002 MSV/35236IMW-2 SM 6200B 92283542003 MSV/35236DMW-4 SM 6200B 92283542004 MSV/35236DMW-5 SM 6200B 92283542005 MSV/35241MW-12 SM 6200B 92283542006 MSV/35236MW-14 SM 6200B 92283542007 MSV/35255MW-18 SM 6200B 92283542008 MSV/35255MW-22 SM 6200B 92283542001 WET/42669IMW-1 SM 3500-Fe B 92283542002 WET/42669IMW-2 SM 3500-Fe B 92283542003 WET/42669DMW-4 SM 3500-Fe B 92283542004 WET/42669DMW-5 SM 3500-Fe B 92283542001 WETA/26180IMW-1 EPA 300.0 92283542002 WETA/26180IMW-2 EPA 300.0 92283542003 WETA/26180DMW-4 EPA 300.0 92283542004 WETA/26180DMW-5 EPA 300.0 92283542001 WETA/26168IMW-1 EPA 353.2 92283542002 WETA/26168IMW-2 EPA 353.2 92283542003 WETA/26168DMW-4 EPA 353.2 92283542004 WETA/26168DMW-5 EPA 353.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/26/2016 03:37 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 37 Page 36 of 37 Page 37 of 37 #=CL# January 29, 2016 LIMS USE: FR - CHRISTINE LIMS OBJECT ID: 92283758 92283758 Project: Pace Project No.: RE: Christine Schaefer ATC Group Services LLC 7606 Whitehall Executive Cente Suite 800 Charlotte, NC 28273 CAJAH'S MOUNTAIN Dear Christine Schaefer: Enclosed are the analytical results for sample(s) received by the laboratory on January 20, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Dale Ingram dale.ingram@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 45 #=CP# CERTIFICATIONS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Minnesota Certification IDs 1700 Elm Street SE Suite 200, Minneapolis, MN 55414525 N 8th Street, Salina, KS 67401 A2LA Certification #: 2926.01Alaska Certification #: UST-078Alaska Certification #MN00064 Alabama Certification #40770Arizona Certification #: AZ-0014 Arkansas Certification #: 88-0680California Certification #: 01155CAColorado Certification #Pace Connecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-L Florida/NELAP Certification #: E87605Guam Certification #:14-008rGeorgia Certification #: 959 Georgia EPD #: PaceIdaho Certification #: MN00064 Hawaii Certification #MN00064Illinois Certification #: 200011Indiana Certification#C-MN-01 Iowa Certification #: 368Kansas Certification #: E-10167 Kentucky Dept of Envi. Protection - DW #90062Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086 Louisiana DHH #: LA140001Maine Certification #: 2013011 Maryland Certification #: 322Michigan DEPH Certification #: 9909 Minnesota Certification #: 027-053-137Mississippi Certification #: Pace Montana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: Pace New Jersey Certification #: MN-002New York Certification #: 11647 North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036 Ohio EPA #: 4150Ohio VAP Certification #: CL101 Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001 Pennsylvania Certification #: 68-00563Puerto Rico Certification Saipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192 Tennessee Certification #: 02818Utah Certification #: MN000642013-4 Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486 West Virginia Certification #: 382West Virginia DHHR #:9952C Wisconsin Certification #: 999407970 Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84 West Virginia Certification #: 357Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 45 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Lab ID Sample ID Matrix Date Collected Date Received 92283758001 DMW-1 Water 01/20/16 11:30 01/20/16 17:10 92283758002 DMW-2 Water 01/20/16 13:25 01/20/16 17:10 92283758003 DMW-3 Water 01/20/16 12:00 01/20/16 17:10 92283758004 MW-1 Water 01/20/16 11:00 01/20/16 17:10 92283758005 MW-2 Water 01/20/16 14:25 01/20/16 17:10 92283758006 MW-5 Water 01/20/16 10:35 01/20/16 17:10 92283758007 MW-7 Water 01/20/16 13:55 01/20/16 17:10 92283758008 MW-8 Water 01/20/16 14:45 01/20/16 17:10 92283758009 MW-11 Water 01/20/16 10:15 01/20/16 17:10 92283758010 PW-1 Water 01/20/16 15:00 01/20/16 17:10 92283758011 PW-18 Water 01/20/16 15:20 01/20/16 17:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 45 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92283758001 DMW-1 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283758002 DMW-2 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283758003 DMW-3 RSK 175 1 PASI-MSTV EPA 6010 2 PASI-ACDF SM 6200B 63 PASI-CCAH SM 3500-Fe B 1 PASI-AWRC EPA 300.0 1 PASI-AMDW EPA 353.2 1 PASI-ADMN 92283758004 MW-1 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283758005 MW-2 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283758006 MW-5 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283758007 MW-7 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283758008 MW-8 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283758009 MW-11 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92283758010 PW-1 SM 6200B 63 PASI-CCAH 92283758011 PW-18 SM 6200B 63 PASI-CCAH REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:DMW-1 Lab ID:92283758001 Collected:01/20/16 11:30 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 1.5J ug/L 01/22/16 12:23 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 8.7 ug/L 01/26/16 21:29 7439-92-101/26/16 09:555.0 2.5 1 Manganese 290 ug/L 01/26/16 21:29 7439-96-501/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/21/16 23:50 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/21/16 23:50 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/21/16 23:50 74-97-50.50 0.25 1 Bromodichloromethane 0.67 ug/L 01/21/16 23:50 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/21/16 23:50 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/21/16 23:50 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/21/16 23:50 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/21/16 23:50 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/21/16 23:50 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/21/16 23:50 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/21/16 23:50 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/21/16 23:50 75-00-31.0 0.50 1 Chloroform 10.9 ug/L 01/21/16 23:50 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/21/16 23:50 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/21/16 23:50 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/21/16 23:50 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/21/16 23:50 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/21/16 23:50 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/21/16 23:50 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/21/16 23:50 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/21/16 23:50 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/21/16 23:50 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/21/16 23:50 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/21/16 23:50 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/21/16 23:50 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/21/16 23:50 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/21/16 23:50 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/21/16 23:50 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/21/16 23:50 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/21/16 23:50 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/21/16 23:50 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/21/16 23:50 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/21/16 23:50 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/21/16 23:50 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/21/16 23:50 10061-02-60.50 0.25 1 Diisopropyl ether 1.3 ug/L 01/21/16 23:50 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/21/16 23:50 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/21/16 23:50 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/21/16 23:50 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:DMW-1 Lab ID:92283758001 Collected:01/20/16 11:30 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride 1.3J ug/L 01/21/16 23:50 75-09-2 C92.0 1.0 1 Methyl-tert-butyl ether 101 ug/L 01/21/16 23:50 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/21/16 23:50 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/21/16 23:50 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/21/16 23:50 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/21/16 23:50 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/21/16 23:50 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/21/16 23:50 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/21/16 23:50 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/21/16 23:50 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/21/16 23:50 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/21/16 23:50 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/21/16 23:50 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/21/16 23:50 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/21/16 23:50 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/21/16 23:50 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/21/16 23:50 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/21/16 23:50 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/21/16 23:50 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/21/16 23:50 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/21/16 23:50 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)95 %01/21/16 23:50 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/21/16 23:50 460-00-470-130 1 Toluene-d8 (S)100 %01/21/16 23:50 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 1.5J mg/L 01/25/16 12:15 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 1.1 mg/L 01/21/16 10:090.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:DMW-2 Lab ID:92283758002 Collected:01/20/16 13:25 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 4490 ug/L 01/22/16 12:39 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 01/26/16 21:32 7439-92-101/26/16 09:555.0 2.5 1 Manganese 363 ug/L 01/26/16 21:32 7439-96-501/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/22/16 00:07 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/22/16 00:07 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/22/16 00:07 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/22/16 00:07 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/22/16 00:07 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/22/16 00:07 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/22/16 00:07 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/22/16 00:07 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/22/16 00:07 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/22/16 00:07 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/22/16 00:07 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/22/16 00:07 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/22/16 00:07 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/22/16 00:07 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/22/16 00:07 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/22/16 00:07 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/22/16 00:07 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/22/16 00:07 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/22/16 00:07 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/22/16 00:07 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/22/16 00:07 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/22/16 00:07 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/22/16 00:07 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/22/16 00:07 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/22/16 00:07 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/22/16 00:07 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/22/16 00:07 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:07 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:07 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/22/16 00:07 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/22/16 00:07 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/22/16 00:07 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/22/16 00:07 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:07 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:07 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/22/16 00:07 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/22/16 00:07 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/22/16 00:07 87-68-3 M12.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/22/16 00:07 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:DMW-2 Lab ID:92283758002 Collected:01/20/16 13:25 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride 1.1J ug/L 01/22/16 00:07 75-09-2 C92.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/22/16 00:07 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/22/16 00:07 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/22/16 00:07 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/22/16 00:07 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:07 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:07 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/22/16 00:07 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/22/16 00:07 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/22/16 00:07 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/22/16 00:07 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/22/16 00:07 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/22/16 00:07 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/22/16 00:07 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/22/16 00:07 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/22/16 00:07 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/22/16 00:07 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/22/16 00:07 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/22/16 00:07 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/22/16 00:07 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/22/16 00:07 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)96 %01/22/16 00:07 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/22/16 00:07 460-00-470-130 1 Toluene-d8 (S)99 %01/22/16 00:07 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 1.8J mg/L 01/25/16 18:01 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate <0.020 mg/L 01/21/16 10:190.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:DMW-3 Lab ID:92283758003 Collected:01/20/16 12:00 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: RSK 175RSK 175 AIR Headspace Methane 1.9J ug/L 01/22/16 12:47 74-82-810.0 0.63 1 Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 01/26/16 21:35 7439-92-101/26/16 09:555.0 2.5 1 Manganese 16.5 ug/L 01/26/16 21:35 7439-96-501/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/22/16 00:24 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/22/16 00:24 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/22/16 00:24 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/22/16 00:24 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/22/16 00:24 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/22/16 00:24 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/22/16 00:24 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/22/16 00:24 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/22/16 00:24 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/22/16 00:24 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/22/16 00:24 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/22/16 00:24 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/22/16 00:24 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/22/16 00:24 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/22/16 00:24 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/22/16 00:24 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/22/16 00:24 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/22/16 00:24 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/22/16 00:24 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/22/16 00:24 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/22/16 00:24 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/22/16 00:24 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/22/16 00:24 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/22/16 00:24 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/22/16 00:24 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/22/16 00:24 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/22/16 00:24 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:24 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:24 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/22/16 00:24 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/22/16 00:24 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/22/16 00:24 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/22/16 00:24 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:24 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:24 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/22/16 00:24 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/22/16 00:24 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/22/16 00:24 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/22/16 00:24 98-82-80.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:DMW-3 Lab ID:92283758003 Collected:01/20/16 12:00 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Methylene Chloride <2.0 ug/L 01/22/16 00:24 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/22/16 00:24 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/22/16 00:24 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/22/16 00:24 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/22/16 00:24 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:24 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:24 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/22/16 00:24 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/22/16 00:24 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/22/16 00:24 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/22/16 00:24 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/22/16 00:24 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/22/16 00:24 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/22/16 00:24 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/22/16 00:24 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/22/16 00:24 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/22/16 00:24 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/22/16 00:24 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/22/16 00:24 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/22/16 00:24 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/22/16 00:24 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %01/22/16 00:24 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %01/22/16 00:24 460-00-470-130 1 Toluene-d8 (S)98 %01/22/16 00:24 2037-26-570-130 1 Analytical Method: SM 3500-Fe BIron, Ferrous Iron, Ferrous <0.50 mg/L 01/25/16 17:05 H1,N20.50 0.50 1 Analytical Method: EPA 300.0300.0 IC Anions 28 Days Sulfate 5.8 mg/L 01/25/16 18:14 14808-79-82.0 1.0 1 Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 0.21 mg/L 01/21/16 10:180.020 0.010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-1 Lab ID:92283758004 Collected:01/20/16 11:00 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 43.4 ug/L 01/26/16 21:38 7439-92-101/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/22/16 00:40 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/22/16 00:40 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/22/16 00:40 74-97-50.50 0.25 1 Bromodichloromethane 0.27J ug/L 01/22/16 00:40 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/22/16 00:40 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/22/16 00:40 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/22/16 00:40 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/22/16 00:40 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/22/16 00:40 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/22/16 00:40 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/22/16 00:40 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/22/16 00:40 75-00-31.0 0.50 1 Chloroform 14.8 ug/L 01/22/16 00:40 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/22/16 00:40 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/22/16 00:40 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/22/16 00:40 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/22/16 00:40 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/22/16 00:40 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/22/16 00:40 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/22/16 00:40 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/22/16 00:40 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/22/16 00:40 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/22/16 00:40 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/22/16 00:40 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/22/16 00:40 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/22/16 00:40 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/22/16 00:40 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:40 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:40 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/22/16 00:40 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/22/16 00:40 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/22/16 00:40 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/22/16 00:40 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:40 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:40 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/22/16 00:40 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/22/16 00:40 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/22/16 00:40 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/22/16 00:40 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/22/16 00:40 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/22/16 00:40 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/22/16 00:40 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/22/16 00:40 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-1 Lab ID:92283758004 Collected:01/20/16 11:00 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/22/16 00:40 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:40 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:40 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/22/16 00:40 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/22/16 00:40 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/22/16 00:40 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/22/16 00:40 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/22/16 00:40 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/22/16 00:40 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/22/16 00:40 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/22/16 00:40 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/22/16 00:40 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/22/16 00:40 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/22/16 00:40 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/22/16 00:40 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/22/16 00:40 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/22/16 00:40 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)95 %01/22/16 00:40 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/22/16 00:40 460-00-470-130 1 Toluene-d8 (S)98 %01/22/16 00:40 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-2 Lab ID:92283758005 Collected:01/20/16 14:25 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 61.8 ug/L 01/26/16 21:51 7439-92-101/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 16.1 ug/L 01/28/16 20:07 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/28/16 20:07 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/28/16 20:07 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/28/16 20:07 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/28/16 20:07 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/28/16 20:07 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/28/16 20:07 104-51-80.50 0.25 1 sec-Butylbenzene 0.26J ug/L 01/28/16 20:07 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/28/16 20:07 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/28/16 20:07 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/28/16 20:07 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/28/16 20:07 75-00-31.0 0.50 1 Chloroform 2.7 ug/L 01/28/16 20:07 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/28/16 20:07 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/28/16 20:07 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/28/16 20:07 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/28/16 20:07 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/28/16 20:07 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/28/16 20:07 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/28/16 20:07 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/28/16 20:07 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/28/16 20:07 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/28/16 20:07 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/28/16 20:07 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/28/16 20:07 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/28/16 20:07 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/28/16 20:07 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/28/16 20:07 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/28/16 20:07 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/28/16 20:07 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/28/16 20:07 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/28/16 20:07 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/28/16 20:07 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/28/16 20:07 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/28/16 20:07 10061-02-60.50 0.25 1 Diisopropyl ether 0.62 ug/L 01/28/16 20:07 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/28/16 20:07 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/28/16 20:07 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)0.58 ug/L 01/28/16 20:07 98-82-80.50 0.25 1 Methylene Chloride 1.3J ug/L 01/28/16 20:07 75-09-2 C92.0 1.0 1 Methyl-tert-butyl ether 12.6 ug/L 01/28/16 20:07 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/28/16 20:07 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/28/16 20:07 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-2 Lab ID:92283758005 Collected:01/20/16 14:25 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/28/16 20:07 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/28/16 20:07 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/28/16 20:07 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/28/16 20:07 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/28/16 20:07 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/28/16 20:07 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/28/16 20:07 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/28/16 20:07 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/28/16 20:07 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/28/16 20:07 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/28/16 20:07 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/28/16 20:07 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 0.88 ug/L 01/28/16 20:07 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 0.35J ug/L 01/28/16 20:07 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/28/16 20:07 75-01-41.0 0.25 1 m&p-Xylene 1.3 ug/L 01/28/16 20:07 179601-23-11.0 0.50 1 o-Xylene 1.3 ug/L 01/28/16 20:07 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %01/28/16 20:07 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %01/28/16 20:07 460-00-470-130 1 Toluene-d8 (S)101 %01/28/16 20:07 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-5 Lab ID:92283758006 Collected:01/20/16 10:35 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 36.8 ug/L 01/26/16 21:54 7439-92-101/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 0.39J ug/L 01/22/16 00:57 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/22/16 00:57 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/22/16 00:57 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/22/16 00:57 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/22/16 00:57 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/22/16 00:57 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/22/16 00:57 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/22/16 00:57 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/22/16 00:57 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/22/16 00:57 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/22/16 00:57 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/22/16 00:57 75-00-31.0 0.50 1 Chloroform 0.58 ug/L 01/22/16 00:57 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/22/16 00:57 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/22/16 00:57 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/22/16 00:57 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/22/16 00:57 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/22/16 00:57 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/22/16 00:57 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/22/16 00:57 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/22/16 00:57 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/22/16 00:57 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/22/16 00:57 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/22/16 00:57 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/22/16 00:57 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/22/16 00:57 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/22/16 00:57 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:57 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/22/16 00:57 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/22/16 00:57 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/22/16 00:57 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/22/16 00:57 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/22/16 00:57 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:57 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/22/16 00:57 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/22/16 00:57 108-20-30.50 0.25 1 Ethylbenzene 1.9 ug/L 01/22/16 00:57 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/22/16 00:57 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/22/16 00:57 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/22/16 00:57 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/22/16 00:57 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/22/16 00:57 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/22/16 00:57 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-5 Lab ID:92283758006 Collected:01/20/16 10:35 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 01/22/16 00:57 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:57 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/22/16 00:57 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 01/22/16 00:57 127-18-40.50 0.25 1 Toluene 6.5 ug/L 01/22/16 00:57 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/22/16 00:57 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/22/16 00:57 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/22/16 00:57 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/22/16 00:57 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/22/16 00:57 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/22/16 00:57 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/22/16 00:57 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/22/16 00:57 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 0.87 ug/L 01/22/16 00:57 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/22/16 00:57 75-01-41.0 0.25 1 m&p-Xylene 0.98J ug/L 01/22/16 00:57 179601-23-11.0 0.50 1 o-Xylene 4.2 ug/L 01/22/16 00:57 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)96 %01/22/16 00:57 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/22/16 00:57 460-00-470-130 1 Toluene-d8 (S)100 %01/22/16 00:57 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-7 Lab ID:92283758007 Collected:01/20/16 13:55 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 38.7 ug/L 01/26/16 21:57 7439-92-101/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 276 ug/L 01/28/16 20:24 71-43-21.2 0.62 2.5 Bromobenzene <1.2 ug/L 01/28/16 20:24 108-86-11.2 0.62 2.5 Bromochloromethane <1.2 ug/L 01/28/16 20:24 74-97-51.2 0.62 2.5 Bromodichloromethane <1.2 ug/L 01/28/16 20:24 75-27-41.2 0.62 2.5 Bromoform <1.2 ug/L 01/28/16 20:24 75-25-21.2 0.62 2.5 Bromomethane <12.5 ug/L 01/28/16 20:24 74-83-912.5 1.2 2.5 n-Butylbenzene <1.2 ug/L 01/28/16 20:24 104-51-81.2 0.62 2.5 sec-Butylbenzene 1.5 ug/L 01/28/16 20:24 135-98-81.2 0.62 2.5 tert-Butylbenzene <1.2 ug/L 01/28/16 20:24 98-06-61.2 0.62 2.5 Carbon tetrachloride <1.2 ug/L 01/28/16 20:24 56-23-51.2 0.62 2.5 Chlorobenzene <1.2 ug/L 01/28/16 20:24 108-90-71.2 0.62 2.5 Chloroethane <2.5 ug/L 01/28/16 20:24 75-00-32.5 1.2 2.5 Chloroform 4.0 ug/L 01/28/16 20:24 67-66-31.2 0.62 2.5 Chloromethane <2.5 ug/L 01/28/16 20:24 74-87-32.5 1.2 2.5 2-Chlorotoluene <1.2 ug/L 01/28/16 20:24 95-49-81.2 0.62 2.5 4-Chlorotoluene <1.2 ug/L 01/28/16 20:24 106-43-41.2 0.62 2.5 1,2-Dibromo-3-chloropropane <2.5 ug/L 01/28/16 20:24 96-12-82.5 1.2 2.5 Dibromochloromethane <1.2 ug/L 01/28/16 20:24 124-48-11.2 0.62 2.5 1,2-Dibromoethane (EDB)<1.2 ug/L 01/28/16 20:24 106-93-41.2 0.62 2.5 Dibromomethane <1.2 ug/L 01/28/16 20:24 74-95-31.2 0.62 2.5 1,2-Dichlorobenzene <1.2 ug/L 01/28/16 20:24 95-50-11.2 0.62 2.5 1,3-Dichlorobenzene <1.2 ug/L 01/28/16 20:24 541-73-11.2 0.62 2.5 1,4-Dichlorobenzene <1.2 ug/L 01/28/16 20:24 106-46-71.2 0.62 2.5 Dichlorodifluoromethane <1.2 ug/L 01/28/16 20:24 75-71-81.2 0.62 2.5 1,1-Dichloroethane <1.2 ug/L 01/28/16 20:24 75-34-31.2 0.62 2.5 1,2-Dichloroethane 0.70J ug/L 01/28/16 20:24 107-06-21.2 0.62 2.5 1,1-Dichloroethene <1.2 ug/L 01/28/16 20:24 75-35-41.2 0.62 2.5 cis-1,2-Dichloroethene <1.2 ug/L 01/28/16 20:24 156-59-21.2 0.62 2.5 trans-1,2-Dichloroethene <1.2 ug/L 01/28/16 20:24 156-60-51.2 0.62 2.5 1,2-Dichloropropane <1.2 ug/L 01/28/16 20:24 78-87-51.2 0.62 2.5 1,3-Dichloropropane <1.2 ug/L 01/28/16 20:24 142-28-91.2 0.62 2.5 2,2-Dichloropropane <1.2 ug/L 01/28/16 20:24 594-20-71.2 0.62 2.5 1,1-Dichloropropene <1.2 ug/L 01/28/16 20:24 563-58-61.2 0.62 2.5 cis-1,3-Dichloropropene <1.2 ug/L 01/28/16 20:24 10061-01-51.2 0.62 2.5 trans-1,3-Dichloropropene <1.2 ug/L 01/28/16 20:24 10061-02-61.2 0.62 2.5 Diisopropyl ether 5.9 ug/L 01/28/16 20:24 108-20-31.2 0.62 2.5 Ethylbenzene 4.3 ug/L 01/28/16 20:24 100-41-41.2 0.62 2.5 Hexachloro-1,3-butadiene <5.0 ug/L 01/28/16 20:24 87-68-35.0 2.5 2.5 Isopropylbenzene (Cumene)3.8 ug/L 01/28/16 20:24 98-82-81.2 0.62 2.5 Methylene Chloride 4.4J ug/L 01/28/16 20:24 75-09-2 C95.0 2.5 2.5 Methyl-tert-butyl ether 125 ug/L 01/28/16 20:24 1634-04-41.2 0.62 2.5 Naphthalene 7.5 ug/L 01/28/16 20:24 91-20-35.0 2.5 2.5 n-Propylbenzene 3.0 ug/L 01/28/16 20:24 103-65-11.2 0.62 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-7 Lab ID:92283758007 Collected:01/20/16 13:55 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <1.2 ug/L 01/28/16 20:24 100-42-51.2 0.62 2.5 1,1,1,2-Tetrachloroethane <1.2 ug/L 01/28/16 20:24 630-20-61.2 0.62 2.5 1,1,2,2-Tetrachloroethane <1.2 ug/L 01/28/16 20:24 79-34-51.2 0.62 2.5 Tetrachloroethene <1.2 ug/L 01/28/16 20:24 127-18-41.2 0.62 2.5 Toluene 17.2 ug/L 01/28/16 20:24 108-88-31.2 0.62 2.5 1,2,3-Trichlorobenzene <5.0 ug/L 01/28/16 20:24 87-61-65.0 2.5 2.5 1,2,4-Trichlorobenzene <5.0 ug/L 01/28/16 20:24 120-82-15.0 2.5 2.5 1,1,1-Trichloroethane <1.2 ug/L 01/28/16 20:24 71-55-61.2 0.62 2.5 1,1,2-Trichloroethane <1.2 ug/L 01/28/16 20:24 79-00-51.2 0.62 2.5 Trichloroethene <1.2 ug/L 01/28/16 20:24 79-01-61.2 0.62 2.5 Trichlorofluoromethane <2.5 ug/L 01/28/16 20:24 75-69-42.5 1.2 2.5 1,2,3-Trichloropropane <1.2 ug/L 01/28/16 20:24 96-18-41.2 0.62 2.5 1,2,4-Trimethylbenzene 34.2 ug/L 01/28/16 20:24 95-63-61.2 0.62 2.5 1,3,5-Trimethylbenzene 14.7 ug/L 01/28/16 20:24 108-67-81.2 0.62 2.5 Vinyl chloride <2.5 ug/L 01/28/16 20:24 75-01-42.5 0.62 2.5 m&p-Xylene 31.8 ug/L 01/28/16 20:24 179601-23-12.5 1.2 2.5 o-Xylene 57.4 ug/L 01/28/16 20:24 95-47-61.2 0.62 2.5 Surrogates 1,2-Dichloroethane-d4 (S)104 %01/28/16 20:24 17060-07-070-130 2.5 4-Bromofluorobenzene (S)96 %01/28/16 20:24 460-00-470-130 2.5 Toluene-d8 (S)102 %01/28/16 20:24 2037-26-570-130 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-8 Lab ID:92283758008 Collected:01/20/16 14:45 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 54.1 ug/L 01/26/16 22:00 7439-92-101/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 1800 ug/L 01/22/16 03:27 71-43-212562.5 250 Bromobenzene <125 ug/L 01/22/16 03:27 108-86-112562.5 250 Bromochloromethane <125 ug/L 01/22/16 03:27 74-97-512562.5 250 Bromodichloromethane <125 ug/L 01/22/16 03:27 75-27-412562.5 250 Bromoform <125 ug/L 01/22/16 03:27 75-25-212562.5 250 Bromomethane <1250 ug/L 01/22/16 03:27 74-83-91250125250 n-Butylbenzene <125 ug/L 01/22/16 03:27 104-51-812562.5 250 sec-Butylbenzene <125 ug/L 01/22/16 03:27 135-98-812562.5 250 tert-Butylbenzene <125 ug/L 01/22/16 03:27 98-06-612562.5 250 Carbon tetrachloride <125 ug/L 01/22/16 03:27 56-23-512562.5 250 Chlorobenzene <125 ug/L 01/22/16 03:27 108-90-712562.5 250 Chloroethane <250 ug/L 01/22/16 03:27 75-00-3250125250 Chloroform <125 ug/L 01/22/16 03:27 67-66-312562.5 250 Chloromethane <250 ug/L 01/22/16 03:27 74-87-3250125250 2-Chlorotoluene <125 ug/L 01/22/16 03:27 95-49-812562.5 250 4-Chlorotoluene <125 ug/L 01/22/16 03:27 106-43-412562.5 250 1,2-Dibromo-3-chloropropane <250 ug/L 01/22/16 03:27 96-12-8250125250 Dibromochloromethane <125 ug/L 01/22/16 03:27 124-48-112562.5 250 1,2-Dibromoethane (EDB)<125 ug/L 01/22/16 03:27 106-93-412562.5 250 Dibromomethane <125 ug/L 01/22/16 03:27 74-95-312562.5 250 1,2-Dichlorobenzene <125 ug/L 01/22/16 03:27 95-50-112562.5 250 1,3-Dichlorobenzene <125 ug/L 01/22/16 03:27 541-73-112562.5 250 1,4-Dichlorobenzene <125 ug/L 01/22/16 03:27 106-46-712562.5 250 Dichlorodifluoromethane <125 ug/L 01/22/16 03:27 75-71-812562.5 250 1,1-Dichloroethane <125 ug/L 01/22/16 03:27 75-34-312562.5 250 1,2-Dichloroethane <125 ug/L 01/22/16 03:27 107-06-212562.5 250 1,1-Dichloroethene <125 ug/L 01/22/16 03:27 75-35-412562.5 250 cis-1,2-Dichloroethene <125 ug/L 01/22/16 03:27 156-59-212562.5 250 trans-1,2-Dichloroethene <125 ug/L 01/22/16 03:27 156-60-512562.5 250 1,2-Dichloropropane <125 ug/L 01/22/16 03:27 78-87-512562.5 250 1,3-Dichloropropane <125 ug/L 01/22/16 03:27 142-28-912562.5 250 2,2-Dichloropropane <125 ug/L 01/22/16 03:27 594-20-712562.5 250 1,1-Dichloropropene <125 ug/L 01/22/16 03:27 563-58-612562.5 250 cis-1,3-Dichloropropene <125 ug/L 01/22/16 03:27 10061-01-512562.5 250 trans-1,3-Dichloropropene <125 ug/L 01/22/16 03:27 10061-02-612562.5 250 Diisopropyl ether <125 ug/L 01/22/16 03:27 108-20-312562.5 250 Ethylbenzene 3040 ug/L 01/22/16 03:27 100-41-412562.5 250 Hexachloro-1,3-butadiene <500 ug/L 01/22/16 03:27 87-68-3500250250 Isopropylbenzene (Cumene)189 ug/L 01/22/16 03:27 98-82-812562.5 250 Methylene Chloride <500 ug/L 01/22/16 03:27 75-09-2500250250 Methyl-tert-butyl ether <125 ug/L 01/22/16 03:27 1634-04-412562.5 250 Naphthalene 1320 ug/L 01/22/16 03:27 91-20-3500250250 n-Propylbenzene 626 ug/L 01/22/16 03:27 103-65-112562.5 250 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-8 Lab ID:92283758008 Collected:01/20/16 14:45 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <125 ug/L 01/22/16 03:27 100-42-512562.5 250 1,1,1,2-Tetrachloroethane <125 ug/L 01/22/16 03:27 630-20-612562.5 250 1,1,2,2-Tetrachloroethane <125 ug/L 01/22/16 03:27 79-34-512562.5 250 Tetrachloroethene <125 ug/L 01/22/16 03:27 127-18-412562.5 250 Toluene 21500 ug/L 01/22/16 03:27 108-88-312562.5 250 1,2,3-Trichlorobenzene <500 ug/L 01/22/16 03:27 87-61-6500250250 1,2,4-Trichlorobenzene <500 ug/L 01/22/16 03:27 120-82-1500250250 1,1,1-Trichloroethane <125 ug/L 01/22/16 03:27 71-55-612562.5 250 1,1,2-Trichloroethane <125 ug/L 01/22/16 03:27 79-00-512562.5 250 Trichloroethene <125 ug/L 01/22/16 03:27 79-01-612562.5 250 Trichlorofluoromethane <250 ug/L 01/22/16 03:27 75-69-4250125250 1,2,3-Trichloropropane <125 ug/L 01/22/16 03:27 96-18-412562.5 250 1,2,4-Trimethylbenzene 5330 ug/L 01/22/16 03:27 95-63-612562.5 250 1,3,5-Trimethylbenzene 1290 ug/L 01/22/16 03:27 108-67-812562.5 250 Vinyl chloride <250 ug/L 01/22/16 03:27 75-01-425062.5 250 m&p-Xylene 13100 ug/L 01/22/16 03:27 179601-23-1250125250 o-Xylene 6430 ug/L 01/22/16 03:27 95-47-612562.5 250 Surrogates 1,2-Dichloroethane-d4 (S)99 %01/22/16 03:27 17060-07-070-130 250 4-Bromofluorobenzene (S)104 %01/22/16 03:27 460-00-470-130 250 Toluene-d8 (S)100 %01/22/16 03:27 2037-26-570-130 250 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-11 Lab ID:92283758009 Collected:01/20/16 10:15 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 54.8 ug/L 01/26/16 22:03 7439-92-101/26/16 09:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 5450 ug/L 01/22/16 03:44 71-43-212562.5 250 Bromobenzene <125 ug/L 01/22/16 03:44 108-86-112562.5 250 Bromochloromethane <125 ug/L 01/22/16 03:44 74-97-512562.5 250 Bromodichloromethane <125 ug/L 01/22/16 03:44 75-27-412562.5 250 Bromoform <125 ug/L 01/22/16 03:44 75-25-212562.5 250 Bromomethane <1250 ug/L 01/22/16 03:44 74-83-91250125250 n-Butylbenzene <125 ug/L 01/22/16 03:44 104-51-812562.5 250 sec-Butylbenzene <125 ug/L 01/22/16 03:44 135-98-812562.5 250 tert-Butylbenzene <125 ug/L 01/22/16 03:44 98-06-612562.5 250 Carbon tetrachloride <125 ug/L 01/22/16 03:44 56-23-512562.5 250 Chlorobenzene <125 ug/L 01/22/16 03:44 108-90-712562.5 250 Chloroethane <250 ug/L 01/22/16 03:44 75-00-3250125250 Chloroform <125 ug/L 01/22/16 03:44 67-66-312562.5 250 Chloromethane <250 ug/L 01/22/16 03:44 74-87-3250125250 2-Chlorotoluene <125 ug/L 01/22/16 03:44 95-49-812562.5 250 4-Chlorotoluene <125 ug/L 01/22/16 03:44 106-43-412562.5 250 1,2-Dibromo-3-chloropropane <250 ug/L 01/22/16 03:44 96-12-8250125250 Dibromochloromethane <125 ug/L 01/22/16 03:44 124-48-112562.5 250 1,2-Dibromoethane (EDB)<125 ug/L 01/22/16 03:44 106-93-412562.5 250 Dibromomethane <125 ug/L 01/22/16 03:44 74-95-312562.5 250 1,2-Dichlorobenzene <125 ug/L 01/22/16 03:44 95-50-112562.5 250 1,3-Dichlorobenzene <125 ug/L 01/22/16 03:44 541-73-112562.5 250 1,4-Dichlorobenzene <125 ug/L 01/22/16 03:44 106-46-712562.5 250 Dichlorodifluoromethane <125 ug/L 01/22/16 03:44 75-71-812562.5 250 1,1-Dichloroethane <125 ug/L 01/22/16 03:44 75-34-312562.5 250 1,2-Dichloroethane <125 ug/L 01/22/16 03:44 107-06-212562.5 250 1,1-Dichloroethene <125 ug/L 01/22/16 03:44 75-35-412562.5 250 cis-1,2-Dichloroethene <125 ug/L 01/22/16 03:44 156-59-212562.5 250 trans-1,2-Dichloroethene <125 ug/L 01/22/16 03:44 156-60-512562.5 250 1,2-Dichloropropane <125 ug/L 01/22/16 03:44 78-87-512562.5 250 1,3-Dichloropropane <125 ug/L 01/22/16 03:44 142-28-912562.5 250 2,2-Dichloropropane <125 ug/L 01/22/16 03:44 594-20-712562.5 250 1,1-Dichloropropene <125 ug/L 01/22/16 03:44 563-58-612562.5 250 cis-1,3-Dichloropropene <125 ug/L 01/22/16 03:44 10061-01-512562.5 250 trans-1,3-Dichloropropene <125 ug/L 01/22/16 03:44 10061-02-612562.5 250 Diisopropyl ether 94.8J ug/L 01/22/16 03:44 108-20-312562.5 250 Ethylbenzene 2920 ug/L 01/22/16 03:44 100-41-412562.5 250 Hexachloro-1,3-butadiene <500 ug/L 01/22/16 03:44 87-68-3500250250 Isopropylbenzene (Cumene)105J ug/L 01/22/16 03:44 98-82-812562.5 250 Methylene Chloride <500 ug/L 01/22/16 03:44 75-09-2500250250 Methyl-tert-butyl ether 2510 ug/L 01/22/16 03:44 1634-04-412562.5 250 Naphthalene 642 ug/L 01/22/16 03:44 91-20-3500250250 n-Propylbenzene 322 ug/L 01/22/16 03:44 103-65-112562.5 250 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:MW-11 Lab ID:92283758009 Collected:01/20/16 10:15 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <125 ug/L 01/22/16 03:44 100-42-512562.5 250 1,1,1,2-Tetrachloroethane <125 ug/L 01/22/16 03:44 630-20-612562.5 250 1,1,2,2-Tetrachloroethane <125 ug/L 01/22/16 03:44 79-34-512562.5 250 Tetrachloroethene <125 ug/L 01/22/16 03:44 127-18-412562.5 250 Toluene 23900 ug/L 01/22/16 03:44 108-88-312562.5 250 1,2,3-Trichlorobenzene <500 ug/L 01/22/16 03:44 87-61-6500250250 1,2,4-Trichlorobenzene <500 ug/L 01/22/16 03:44 120-82-1500250250 1,1,1-Trichloroethane <125 ug/L 01/22/16 03:44 71-55-612562.5 250 1,1,2-Trichloroethane <125 ug/L 01/22/16 03:44 79-00-512562.5 250 Trichloroethene <125 ug/L 01/22/16 03:44 79-01-612562.5 250 Trichlorofluoromethane <250 ug/L 01/22/16 03:44 75-69-4250125250 1,2,3-Trichloropropane <125 ug/L 01/22/16 03:44 96-18-412562.5 250 1,2,4-Trimethylbenzene 2530 ug/L 01/22/16 03:44 95-63-612562.5 250 1,3,5-Trimethylbenzene 594 ug/L 01/22/16 03:44 108-67-812562.5 250 Vinyl chloride <250 ug/L 01/22/16 03:44 75-01-425062.5 250 m&p-Xylene 11000 ug/L 01/22/16 03:44 179601-23-1250125250 o-Xylene 5260 ug/L 01/22/16 03:44 95-47-612562.5 250 Surrogates 1,2-Dichloroethane-d4 (S)97 %01/22/16 03:44 17060-07-070-130 250 4-Bromofluorobenzene (S)104 %01/22/16 03:44 460-00-470-130 250 Toluene-d8 (S)99 %01/22/16 03:44 2037-26-570-130 250 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:PW-1 Lab ID:92283758010 Collected:01/20/16 15:00 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/22/16 04:51 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/22/16 04:51 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/22/16 04:51 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/22/16 04:51 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/22/16 04:51 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/22/16 04:51 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/22/16 04:51 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/22/16 04:51 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/22/16 04:51 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/22/16 04:51 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/22/16 04:51 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/22/16 04:51 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/22/16 04:51 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/22/16 04:51 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/22/16 04:51 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/22/16 04:51 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/22/16 04:51 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/22/16 04:51 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/22/16 04:51 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/22/16 04:51 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/22/16 04:51 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/22/16 04:51 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/22/16 04:51 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/22/16 04:51 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/22/16 04:51 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/22/16 04:51 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/22/16 04:51 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/22/16 04:51 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/22/16 04:51 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/22/16 04:51 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/22/16 04:51 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/22/16 04:51 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/22/16 04:51 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/22/16 04:51 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/22/16 04:51 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/22/16 04:51 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/22/16 04:51 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/22/16 04:51 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/22/16 04:51 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/22/16 04:51 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/22/16 04:51 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/22/16 04:51 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/22/16 04:51 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/22/16 04:51 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/22/16 04:51 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/22/16 04:51 79-34-50.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:PW-1 Lab ID:92283758010 Collected:01/20/16 15:00 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Tetrachloroethene <0.50 ug/L 01/22/16 04:51 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/22/16 04:51 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/22/16 04:51 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/22/16 04:51 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/22/16 04:51 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/22/16 04:51 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/22/16 04:51 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/22/16 04:51 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/22/16 04:51 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/22/16 04:51 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/22/16 04:51 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/22/16 04:51 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/22/16 04:51 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/22/16 04:51 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)97 %01/22/16 04:51 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %01/22/16 04:51 460-00-470-130 1 Toluene-d8 (S)99 %01/22/16 04:51 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:PW-18 Lab ID:92283758011 Collected:01/20/16 15:20 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 01/22/16 05:08 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 01/22/16 05:08 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 01/22/16 05:08 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 01/22/16 05:08 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 01/22/16 05:08 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 01/22/16 05:08 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 01/22/16 05:08 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 01/22/16 05:08 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 01/22/16 05:08 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 01/22/16 05:08 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 01/22/16 05:08 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 01/22/16 05:08 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 01/22/16 05:08 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 01/22/16 05:08 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 01/22/16 05:08 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 01/22/16 05:08 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 01/22/16 05:08 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 01/22/16 05:08 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 01/22/16 05:08 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 01/22/16 05:08 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 01/22/16 05:08 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 01/22/16 05:08 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 01/22/16 05:08 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 01/22/16 05:08 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 01/22/16 05:08 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 01/22/16 05:08 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 01/22/16 05:08 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 01/22/16 05:08 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 01/22/16 05:08 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 01/22/16 05:08 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 01/22/16 05:08 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 01/22/16 05:08 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 01/22/16 05:08 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 01/22/16 05:08 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 01/22/16 05:08 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 01/22/16 05:08 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 01/22/16 05:08 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 01/22/16 05:08 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 01/22/16 05:08 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 01/22/16 05:08 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 01/22/16 05:08 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 01/22/16 05:08 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 01/22/16 05:08 103-65-10.50 0.25 1 Styrene <0.50 ug/L 01/22/16 05:08 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 01/22/16 05:08 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 01/22/16 05:08 79-34-50.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 45 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Sample:PW-18 Lab ID:92283758011 Collected:01/20/16 15:20 Received:01/20/16 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Tetrachloroethene <0.50 ug/L 01/22/16 05:08 127-18-40.50 0.25 1 Toluene <0.50 ug/L 01/22/16 05:08 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 01/22/16 05:08 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 01/22/16 05:08 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 01/22/16 05:08 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 01/22/16 05:08 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 01/22/16 05:08 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 01/22/16 05:08 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 01/22/16 05:08 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 01/22/16 05:08 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 01/22/16 05:08 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 01/22/16 05:08 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 01/22/16 05:08 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 01/22/16 05:08 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)99 %01/22/16 05:08 17060-07-070-130 1 4-Bromofluorobenzene (S)103 %01/22/16 05:08 460-00-470-130 1 Toluene-d8 (S)99 %01/22/16 05:08 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: AIR/25074 RSK 175 RSK 175 RSK 175 AIR HEADSPACE Associated Lab Samples:92283758001, 92283758002, 92283758003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2179438 Associated Lab Samples:92283758001, 92283758002, 92283758003 Matrix:Water AnalyzedMDL Methane ug/L 1.7J 10.0 01/22/16 12:150.63 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2179439LABORATORY CONTROL SAMPLE & LCSD: LCSSpike LCSD % Rec RPD Max RPD LCSD Result 2179440 Methane ug/L 60.960.7 100 85-1159154.9 10 20 Parameter Units Dup Result Max RPD QualifiersRPDResult 92283758001 2179569SAMPLE DUPLICATE: Methane ug/L 1.3J 201.5J Parameter Units Dup Result Max RPD QualifiersRPDResult 92283899007 2179570SAMPLE DUPLICATE: Methane ug/L 2.7J 20ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/20524 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92283758001, 92283758002, 92283758003, 92283758004, 92283758005, 92283758006, 92283758007, 92283758008, 92283758009 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1652909 Associated Lab Samples:92283758001, 92283758002, 92283758003, 92283758004, 92283758005, 92283758006, 92283758007, 92283758008, 92283758009 Matrix:Water AnalyzedMDL Lead ug/L <5.0 5.0 01/26/16 21:112.5 Manganese ug/L <5.0 5.0 01/26/16 21:112.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1652910LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 412500 82 80-120 Manganese ug/L 403500 81 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1652911MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283533001 1652912 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Lead ug/L M15007575-12572 3 20500ND375362 Manganese ug/L 500 81 75-12578 3 2050018.8 422 411 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/35256 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92283758001, 92283758002, 92283758003, 92283758004, 92283758006, 92283758008, 92283758009, 92283758010, 92283758011 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1652020 Associated Lab Samples:92283758001, 92283758002, 92283758003, 92283758004, 92283758006, 92283758008, 92283758009, 92283758010, 92283758011 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 01/21/16 23:330.25 1,1,1-Trichloroethane ug/L <0.50 0.50 01/21/16 23:330.25 1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 01/21/16 23:330.25 1,1,2-Trichloroethane ug/L <0.50 0.50 01/21/16 23:330.25 1,1-Dichloroethane ug/L <0.50 0.50 01/21/16 23:330.25 1,1-Dichloroethene ug/L <0.50 0.50 01/21/16 23:330.25 1,1-Dichloropropene ug/L <0.50 0.50 01/21/16 23:330.25 1,2,3-Trichlorobenzene ug/L <2.0 2.0 01/21/16 23:331.0 1,2,3-Trichloropropane ug/L <0.50 0.50 01/21/16 23:330.25 1,2,4-Trichlorobenzene ug/L <2.0 2.0 01/21/16 23:331.0 1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 01/21/16 23:330.50 1,2-Dibromoethane (EDB)ug/L <0.50 0.50 01/21/16 23:330.25 1,2-Dichlorobenzene ug/L <0.50 0.50 01/21/16 23:330.25 1,2-Dichloroethane ug/L <0.50 0.50 01/21/16 23:330.25 1,2-Dichloropropane ug/L <0.50 0.50 01/21/16 23:330.25 1,3,5-Trimethylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 1,3-Dichlorobenzene ug/L <0.50 0.50 01/21/16 23:330.25 1,3-Dichloropropane ug/L <0.50 0.50 01/21/16 23:330.25 1,4-Dichlorobenzene ug/L <0.50 0.50 01/21/16 23:330.25 2,2-Dichloropropane ug/L <0.50 0.50 01/21/16 23:330.25 2-Chlorotoluene ug/L <0.50 0.50 01/21/16 23:330.25 4-Chlorotoluene ug/L <0.50 0.50 01/21/16 23:330.25 Benzene ug/L <0.50 0.50 01/21/16 23:330.25 Bromobenzene ug/L <0.50 0.50 01/21/16 23:330.25 Bromochloromethane ug/L <0.50 0.50 01/21/16 23:330.25 Bromodichloromethane ug/L <0.50 0.50 01/21/16 23:330.25 Bromoform ug/L <0.50 0.50 01/21/16 23:330.25 Bromomethane ug/L <5.0 5.0 01/21/16 23:330.50 Carbon tetrachloride ug/L <0.50 0.50 01/21/16 23:330.25 Chlorobenzene ug/L <0.50 0.50 01/21/16 23:330.25 Chloroethane ug/L <1.0 1.0 01/21/16 23:330.50 Chloroform ug/L <0.50 0.50 01/21/16 23:330.25 Chloromethane ug/L <1.0 1.0 01/21/16 23:330.50 cis-1,2-Dichloroethene ug/L <0.50 0.50 01/21/16 23:330.25 cis-1,3-Dichloropropene ug/L <0.50 0.50 01/21/16 23:330.25 Dibromochloromethane ug/L <0.50 0.50 01/21/16 23:330.25 Dibromomethane ug/L <0.50 0.50 01/21/16 23:330.25 Dichlorodifluoromethane ug/L <0.50 0.50 01/21/16 23:330.25 Diisopropyl ether ug/L <0.50 0.50 01/21/16 23:330.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1652020 Associated Lab Samples:92283758001, 92283758002, 92283758003, 92283758004, 92283758006, 92283758008, 92283758009, 92283758010, 92283758011 Matrix:Water AnalyzedMDL Ethylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 Hexachloro-1,3-butadiene ug/L <2.0 2.0 01/21/16 23:331.0 Isopropylbenzene (Cumene)ug/L <0.50 0.50 01/21/16 23:330.25 m&p-Xylene ug/L <1.0 1.0 01/21/16 23:330.50 Methyl-tert-butyl ether ug/L <0.50 0.50 01/21/16 23:330.25 Methylene Chloride ug/L <2.0 2.0 01/21/16 23:331.0 n-Butylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 n-Propylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 Naphthalene ug/L <2.0 2.0 01/21/16 23:331.0 o-Xylene ug/L <0.50 0.50 01/21/16 23:330.25 sec-Butylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 Styrene ug/L <0.50 0.50 01/21/16 23:330.25 tert-Butylbenzene ug/L <0.50 0.50 01/21/16 23:330.25 Tetrachloroethene ug/L <0.50 0.50 01/21/16 23:330.25 Toluene ug/L <0.50 0.50 01/21/16 23:330.25 trans-1,2-Dichloroethene ug/L <0.50 0.50 01/21/16 23:330.25 trans-1,3-Dichloropropene ug/L <0.50 0.50 01/21/16 23:330.25 Trichloroethene ug/L <0.50 0.50 01/21/16 23:330.25 Trichlorofluoromethane ug/L <1.0 1.0 01/21/16 23:330.50 Vinyl chloride ug/L <1.0 1.0 01/21/16 23:330.25 1,2-Dichloroethane-d4 (S)%95 70-130 01/21/16 23:33 4-Bromofluorobenzene (S)%101 70-130 01/21/16 23:33 Toluene-d8 (S)%99 70-130 01/21/16 23:33 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1652021LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 47.750 95 60-140 1,1,1-Trichloroethane ug/L 47.650 95 60-140 1,1,2,2-Tetrachloroethane ug/L 46.150 92 60-140 1,1,2-Trichloroethane ug/L 44.050 88 60-140 1,1-Dichloroethane ug/L 45.350 91 60-140 1,1-Dichloroethene ug/L 47.250 94 60-140 1,1-Dichloropropene ug/L 46.150 92 60-140 1,2,3-Trichlorobenzene ug/L 44.050 88 60-140 1,2,3-Trichloropropane ug/L 45.650 91 60-140 1,2,4-Trichlorobenzene ug/L 43.650 87 60-140 1,2,4-Trimethylbenzene ug/L 49.650 99 60-140 1,2-Dibromo-3-chloropropane ug/L 44.950 90 60-140 1,2-Dibromoethane (EDB)ug/L 49.550 99 60-140 1,2-Dichlorobenzene ug/L 45.450 91 60-140 1,2-Dichloroethane ug/L 38.350 77 60-140 1,2-Dichloropropane ug/L 45.250 90 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1652021LABORATORY CONTROL SAMPLE: LCSSpike 1,3,5-Trimethylbenzene ug/L 50.350 101 60-140 1,3-Dichlorobenzene ug/L 45.650 91 60-140 1,3-Dichloropropane ug/L 46.250 92 60-140 1,4-Dichlorobenzene ug/L 44.450 89 60-140 2,2-Dichloropropane ug/L 43.850 88 60-140 2-Chlorotoluene ug/L 47.650 95 60-140 4-Chlorotoluene ug/L 47.850 96 60-140 Benzene ug/L 46.550 93 60-140 Bromobenzene ug/L 47.150 94 60-140 Bromochloromethane ug/L 44.250 88 60-140 Bromodichloromethane ug/L 47.250 94 60-140 Bromoform ug/L 33.650 67 60-140 Bromomethane ug/L 45.350 91 60-140 Carbon tetrachloride ug/L 50.350 101 60-140 Chlorobenzene ug/L 44.150 88 60-140 Chloroethane ug/L 44.250 88 60-140 Chloroform ug/L 42.750 85 60-140 Chloromethane ug/L 43.150 86 60-140 cis-1,2-Dichloroethene ug/L 44.750 89 60-140 cis-1,3-Dichloropropene ug/L 50.150 100 60-140 Dibromochloromethane ug/L 38.950 78 60-140 Dibromomethane ug/L 44.050 88 60-140 Dichlorodifluoromethane ug/L 39.250 78 60-140 Diisopropyl ether ug/L 47.350 95 60-140 Ethylbenzene ug/L 45.650 91 60-140 Hexachloro-1,3-butadiene ug/L 56.550 113 60-140 Isopropylbenzene (Cumene)ug/L 47.950 96 60-140 m&p-Xylene ug/L 93.0100 93 60-140 Methyl-tert-butyl ether ug/L 47.450 95 60-140 Methylene Chloride ug/L 41.750 83 60-140 n-Butylbenzene ug/L 48.350 97 60-140 n-Propylbenzene ug/L 48.150 96 60-140 Naphthalene ug/L 47.750 95 60-140 o-Xylene ug/L 48.050 96 60-140 sec-Butylbenzene ug/L 47.550 95 60-140 Styrene ug/L 50.950 102 60-140 tert-Butylbenzene ug/L 41.550 83 60-140 Tetrachloroethene ug/L 43.450 87 60-140 Toluene ug/L 44.450 89 60-140 trans-1,2-Dichloroethene ug/L 44.750 89 60-140 trans-1,3-Dichloropropene ug/L 49.150 98 60-140 Trichloroethene ug/L 43.450 87 60-140 Trichlorofluoromethane ug/L 45.950 92 60-140 Vinyl chloride ug/L 47.450 95 60-140 1,2-Dichloroethane-d4 (S)%95 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1652022MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283758002 1652023 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 118 60-140117 1 3020<0.50 23.6 23.4 1,1,1-Trichloroethane ug/L 20 128 60-140128 0 3020<0.50 25.7 25.7 1,1,2,2-Tetrachloroethane ug/L 20 109 60-140113 4 3020<0.50 21.9 22.7 1,1,2-Trichloroethane ug/L 20 108 60-140109 1 3020<0.50 21.6 21.8 1,1-Dichloroethane ug/L 20 119 60-140119 0 3020<0.50 23.7 23.7 1,1-Dichloroethene ug/L 20 133 60-140132 1 3020<0.50 26.7 26.4 1,1-Dichloropropene ug/L 20 125 60-140126 1 3020<0.50 24.9 25.2 1,2,3-Trichlorobenzene ug/L 20 102 60-140115 12 3020<2.0 20.4 23.0 1,2,3-Trichloropropane ug/L 20 109 60-140114 4 3020<0.50 21.9 22.8 1,2,4-Trichlorobenzene ug/L 20 102 60-140110 8 3020<2.0 20.4 22.0 1,2,4-Trimethylbenzene ug/L 20 124 60-140123 0 3020<0.50 24.8 24.7 1,2-Dibromo-3- chloropropane ug/L 20 88 60-14099 11 3020<1.0 17.7 19.7 1,2-Dibromoethane (EDB)ug/L 20 120 60-140121 1 3020<0.50 24.0 24.2 1,2-Dichlorobenzene ug/L 20 112 60-140111 0 3020<0.50 22.4 22.3 1,2-Dichloroethane ug/L 20 96 60-14096 0 3020<0.50 19.4 19.4 1,2-Dichloropropane ug/L 20 117 60-140116 1 3020<0.50 23.4 23.2 1,3,5-Trimethylbenzene ug/L 20 127 60-140126 1 3020<0.50 25.4 25.2 1,3-Dichlorobenzene ug/L 20 115 60-140115 0 3020<0.50 23.0 23.0 1,3-Dichloropropane ug/L 20 116 60-140114 1 3020<0.50 23.1 22.8 1,4-Dichlorobenzene ug/L 20 112 60-140113 1 3020<0.50 22.5 22.6 2,2-Dichloropropane ug/L 20 112 60-140113 1 3020<0.50 22.4 22.7 2-Chlorotoluene ug/L 20 121 60-140123 1 3020<0.50 24.2 24.5 4-Chlorotoluene ug/L 20 122 60-140120 1 3020<0.50 24.3 24.0 Benzene ug/L 20 123 60-140122 1 3020<0.50 24.6 24.4 Bromobenzene ug/L 20 124 60-140115 8 3020<0.50 24.7 22.9 Bromochloromethane ug/L 20 112 60-140111 0 3020<0.50 22.3 22.2 Bromodichloromethane ug/L 20 113 60-140111 2 3020<0.50 22.6 22.1 Bromoform ug/L 20 73 60-14077 6 3020<0.50 14.6 15.5 Bromomethane ug/L 20 77 60-14074 4 3020<5.0 15.4 14.7 Carbon tetrachloride ug/L 20 137 60-140135 2 3020<0.50 27.4 27.0 Chlorobenzene ug/L 20 117 60-140114 3 3020<0.50 23.4 22.8 Chloroethane ug/L 20 135 60-140116 15 3020<1.0 27.0 23.2 Chloroform ug/L 20 110 60-140112 1 3020<0.50 22.1 22.4 Chloromethane ug/L 20 114 60-140109 5 3020<1.0 23.0 21.9 cis-1,2-Dichloroethene ug/L 20 116 60-140116 0 3020<0.50 23.2 23.2 cis-1,3-Dichloropropene ug/L 20 104 60-140106 1 3020<0.50 20.9 21.1 Dibromochloromethane ug/L 20 90 60-14091 1 3020<0.50 18.0 18.3 Dibromomethane ug/L 20 110 60-140109 1 3020<0.50 22.0 21.8 Dichlorodifluoromethane ug/L 20 117 60-140119 1 3020<0.50 23.5 23.8 Diisopropyl ether ug/L 20 117 60-140119 2 3020<0.50 23.4 23.9 Ethylbenzene ug/L 20 122 60-140121 1 3020<0.50 24.4 24.1 Hexachloro-1,3-butadiene ug/L M12014360-140151 5 3020<2.0 28.7 30.1 Isopropylbenzene (Cumene)ug/L 20 126 60-140124 1 3020<0.50 25.2 24.9 m&p-Xylene ug/L 40 125 60-140122 2 3040<1.0 50.0 48.9 Methyl-tert-butyl ether ug/L 20 114 60-140117 3 3020<0.50 22.9 23.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1652022MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283758002 1652023 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 106 60-140107 1 30201.1J 22.3 22.5 n-Butylbenzene ug/L 20 118 60-140118 0 3020<0.50 23.5 23.6 n-Propylbenzene ug/L 20 124 60-140123 1 3020<0.50 24.8 24.6 Naphthalene ug/L 20 102 60-140120 16 3020<2.0 20.4 24.0 o-Xylene ug/L 20 125 60-140124 1 3020<0.50 25.0 24.7 sec-Butylbenzene ug/L 20 122 60-140121 1 3020<0.50 24.4 24.2 Styrene ug/L 20 125 60-140123 1 3020<0.50 25.0 24.6 tert-Butylbenzene ug/L 20 105 60-140104 1 3020<0.50 21.0 20.8 Tetrachloroethene ug/L 20 119 60-140116 3 3020<0.50 23.8 23.2 Toluene ug/L 20 119 60-140116 3 3020<0.50 23.9 23.2 trans-1,2-Dichloroethene ug/L 20 122 60-140121 1 3020<0.50 24.4 24.2 trans-1,3-Dichloropropene ug/L 20 103 60-140106 3 3020<0.50 20.5 21.1 Trichloroethene ug/L 20 117 60-140116 1 3020<0.50 23.4 23.2 Trichlorofluoromethane ug/L 20 140 60-140136 3 3020<1.0 28.0 27.1 Vinyl chloride ug/L 20 130 60-140134 3 3020<1.0 26.0 26.8 1,2-Dichloroethane-d4 (S)%94 70-13096 4-Bromofluorobenzene (S)%101 70-130103 Toluene-d8 (S)%99 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/35294 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92283758005, 92283758007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1653738 Associated Lab Samples:92283758005, 92283758007 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 01/28/16 15:020.25 1,1,1-Trichloroethane ug/L <0.50 0.50 01/28/16 15:020.25 1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 01/28/16 15:020.25 1,1,2-Trichloroethane ug/L <0.50 0.50 01/28/16 15:020.25 1,1-Dichloroethane ug/L <0.50 0.50 01/28/16 15:020.25 1,1-Dichloroethene ug/L <0.50 0.50 01/28/16 15:020.25 1,1-Dichloropropene ug/L <0.50 0.50 01/28/16 15:020.25 1,2,3-Trichlorobenzene ug/L <2.0 2.0 01/28/16 15:021.0 1,2,3-Trichloropropane ug/L <0.50 0.50 01/28/16 15:020.25 1,2,4-Trichlorobenzene ug/L <2.0 2.0 01/28/16 15:021.0 1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 01/28/16 15:020.50 1,2-Dibromoethane (EDB)ug/L <0.50 0.50 01/28/16 15:020.25 1,2-Dichlorobenzene ug/L <0.50 0.50 01/28/16 15:020.25 1,2-Dichloroethane ug/L <0.50 0.50 01/28/16 15:020.25 1,2-Dichloropropane ug/L <0.50 0.50 01/28/16 15:020.25 1,3,5-Trimethylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 1,3-Dichlorobenzene ug/L <0.50 0.50 01/28/16 15:020.25 1,3-Dichloropropane ug/L <0.50 0.50 01/28/16 15:020.25 1,4-Dichlorobenzene ug/L <0.50 0.50 01/28/16 15:020.25 2,2-Dichloropropane ug/L <0.50 0.50 01/28/16 15:020.25 2-Chlorotoluene ug/L <0.50 0.50 01/28/16 15:020.25 4-Chlorotoluene ug/L <0.50 0.50 01/28/16 15:020.25 Benzene ug/L <0.50 0.50 01/28/16 15:020.25 Bromobenzene ug/L <0.50 0.50 01/28/16 15:020.25 Bromochloromethane ug/L <0.50 0.50 01/28/16 15:020.25 Bromodichloromethane ug/L <0.50 0.50 01/28/16 15:020.25 Bromoform ug/L <0.50 0.50 01/28/16 15:020.25 Bromomethane ug/L <5.0 5.0 01/28/16 15:020.50 Carbon tetrachloride ug/L <0.50 0.50 01/28/16 15:020.25 Chlorobenzene ug/L <0.50 0.50 01/28/16 15:020.25 Chloroethane ug/L <1.0 1.0 01/28/16 15:020.50 Chloroform ug/L <0.50 0.50 01/28/16 15:020.25 Chloromethane ug/L <1.0 1.0 01/28/16 15:020.50 cis-1,2-Dichloroethene ug/L <0.50 0.50 01/28/16 15:020.25 cis-1,3-Dichloropropene ug/L <0.50 0.50 01/28/16 15:020.25 Dibromochloromethane ug/L <0.50 0.50 01/28/16 15:020.25 Dibromomethane ug/L <0.50 0.50 01/28/16 15:020.25 Dichlorodifluoromethane ug/L <0.50 0.50 01/28/16 15:020.25 Diisopropyl ether ug/L <0.50 0.50 01/28/16 15:020.25 Ethylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1653738 Associated Lab Samples:92283758005, 92283758007 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <2.0 2.0 01/28/16 15:021.0 Isopropylbenzene (Cumene)ug/L <0.50 0.50 01/28/16 15:020.25 m&p-Xylene ug/L <1.0 1.0 01/28/16 15:020.50 Methyl-tert-butyl ether ug/L <0.50 0.50 01/28/16 15:020.25 Methylene Chloride ug/L <2.0 2.0 01/28/16 15:021.0 n-Butylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 n-Propylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 Naphthalene ug/L <2.0 2.0 01/28/16 15:021.0 o-Xylene ug/L <0.50 0.50 01/28/16 15:020.25 sec-Butylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 Styrene ug/L <0.50 0.50 01/28/16 15:020.25 tert-Butylbenzene ug/L <0.50 0.50 01/28/16 15:020.25 Tetrachloroethene ug/L <0.50 0.50 01/28/16 15:020.25 Toluene ug/L <0.50 0.50 01/28/16 15:020.25 trans-1,2-Dichloroethene ug/L <0.50 0.50 01/28/16 15:020.25 trans-1,3-Dichloropropene ug/L <0.50 0.50 01/28/16 15:020.25 Trichloroethene ug/L <0.50 0.50 01/28/16 15:020.25 Trichlorofluoromethane ug/L <1.0 1.0 01/28/16 15:020.50 Vinyl chloride ug/L <1.0 1.0 01/28/16 15:020.25 1,2-Dichloroethane-d4 (S)%103 70-130 01/28/16 15:02 4-Bromofluorobenzene (S)%97 70-130 01/28/16 15:02 Toluene-d8 (S)%102 70-130 01/28/16 15:02 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1653739LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 46.850 94 60-140 1,1,1-Trichloroethane ug/L 46.350 93 60-140 1,1,2,2-Tetrachloroethane ug/L 47.350 95 60-140 1,1,2-Trichloroethane ug/L 47.150 94 60-140 1,1-Dichloroethane ug/L 44.550 89 60-140 1,1-Dichloroethene ug/L 45.750 91 60-140 1,1-Dichloropropene ug/L 46.650 93 60-140 1,2,3-Trichlorobenzene ug/L 46.850 94 60-140 1,2,3-Trichloropropane ug/L 45.950 92 60-140 1,2,4-Trichlorobenzene ug/L 47.250 94 60-140 1,2,4-Trimethylbenzene ug/L 46.650 93 60-140 1,2-Dibromo-3-chloropropane ug/L 49.350 99 60-140 1,2-Dibromoethane (EDB)ug/L 49.350 99 60-140 1,2-Dichlorobenzene ug/L 45.650 91 60-140 1,2-Dichloroethane ug/L 42.150 84 60-140 1,2-Dichloropropane ug/L 45.850 92 60-140 1,3,5-Trimethylbenzene ug/L 46.150 92 60-140 1,3-Dichlorobenzene ug/L 46.850 94 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1653739LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 47.050 94 60-140 1,4-Dichlorobenzene ug/L 45.850 92 60-140 2,2-Dichloropropane ug/L 46.250 92 60-140 2-Chlorotoluene ug/L 45.750 91 60-140 4-Chlorotoluene ug/L 46.950 94 60-140 Benzene ug/L 47.250 94 60-140 Bromobenzene ug/L 46.650 93 60-140 Bromochloromethane ug/L 45.350 91 60-140 Bromodichloromethane ug/L 48.750 97 60-140 Bromoform ug/L 47.250 94 60-140 Bromomethane ug/L 48.650 97 60-140 Carbon tetrachloride ug/L 48.750 97 60-140 Chlorobenzene ug/L 45.950 92 60-140 Chloroethane ug/L 47.150 94 60-140 Chloroform ug/L 44.650 89 60-140 Chloromethane ug/L 46.250 92 60-140 cis-1,2-Dichloroethene ug/L 45.050 90 60-140 cis-1,3-Dichloropropene ug/L 48.950 98 60-140 Dibromochloromethane ug/L 49.050 98 60-140 Dibromomethane ug/L 46.950 94 60-140 Dichlorodifluoromethane ug/L 43.050 86 60-140 Diisopropyl ether ug/L 46.150 92 60-140 Ethylbenzene ug/L 46.150 92 60-140 Hexachloro-1,3-butadiene ug/L 47.150 94 60-140 Isopropylbenzene (Cumene)ug/L 44.750 89 60-140 m&p-Xylene ug/L 90.9100 91 60-140 Methyl-tert-butyl ether ug/L 48.550 97 60-140 Methylene Chloride ug/L 44.350 89 60-140 n-Butylbenzene ug/L 47.650 95 60-140 n-Propylbenzene ug/L 45.950 92 60-140 Naphthalene ug/L 47.050 94 60-140 o-Xylene ug/L 45.150 90 60-140 sec-Butylbenzene ug/L 45.350 91 60-140 Styrene ug/L 46.450 93 60-140 tert-Butylbenzene ug/L 37.950 76 60-140 Tetrachloroethene ug/L 44.050 88 60-140 Toluene ug/L 46.350 93 60-140 trans-1,2-Dichloroethene ug/L 45.750 91 60-140 trans-1,3-Dichloropropene ug/L 48.650 97 60-140 Trichloroethene ug/L 45.350 91 60-140 Trichlorofluoromethane ug/L 48.350 97 60-140 Vinyl chloride ug/L 47.650 95 60-140 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1656344MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283830006 1656345 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 99 60-14098 1 3020ND19.9 19.6 1,1,1-Trichloroethane ug/L 20 107 60-140109 2 3020ND21.4 21.7 1,1,2,2-Tetrachloroethane ug/L 20 97 60-14095 2 3020ND19.4 19.1 1,1,2-Trichloroethane ug/L 20 99 60-14098 1 3020ND19.8 19.6 1,1-Dichloroethane ug/L 20 100 60-14099 1 3020ND20.0 19.9 1,1-Dichloroethene ug/L 20 108 60-140108 0 3020ND21.6 21.6 1,1-Dichloropropene ug/L 20 110 60-140108 1 3020ND21.9 21.6 1,2,3-Trichlorobenzene ug/L 20 96 60-14094 2 3020ND19.2 18.7 1,2,3-Trichloropropane ug/L 20 99 60-14097 2 3020ND19.7 19.4 1,2,4-Trichlorobenzene ug/L 20 98 60-140100 2 3020ND19.6 19.9 1,2,4-Trimethylbenzene ug/L 20 103 60-140102 1 3020ND20.6 20.3 1,2-Dibromo-3- chloropropane ug/L 20 98 60-14090 9 3020ND19.6 18.0 1,2-Dibromoethane (EDB)ug/L 20 101 60-140100 2 3020ND20.2 19.9 1,2-Dichlorobenzene ug/L 20 98 60-14096 2 3020ND19.6 19.3 1,2-Dichloroethane ug/L 20 90 60-14088 2 3020ND18.2 17.8 1,2-Dichloropropane ug/L 20 95 60-14097 2 3020ND19.0 19.4 1,3,5-Trimethylbenzene ug/L 20 103 60-140102 1 3020ND20.6 20.3 1,3-Dichlorobenzene ug/L 20 102 60-140103 0 3020ND20.5 20.5 1,3-Dichloropropane ug/L 20 99 60-14098 1 3020ND19.8 19.6 1,4-Dichlorobenzene ug/L 20 101 60-14099 2 3020ND20.3 19.9 2,2-Dichloropropane ug/L 20 107 60-140108 1 3020ND21.3 21.6 2-Chlorotoluene ug/L 20 102 60-140100 2 3020ND20.4 20.0 4-Chlorotoluene ug/L 20 104 60-140101 2 3020ND20.7 20.3 Benzene ug/L 20 103 60-140104 1 3020ND20.6 20.7 Bromobenzene ug/L 20 100 60-14098 2 3020ND20.0 19.6 Bromochloromethane ug/L 20 98 60-14096 2 3020ND19.6 19.1 Bromodichloromethane ug/L 20 98 60-140100 1 3020ND19.7 19.9 Bromoform ug/L 20 79 60-14079 0 3020ND15.8 15.8 Bromomethane ug/L 20 114 60-140112 3 3020ND22.9 22.3 Carbon tetrachloride ug/L 20 107 60-140109 2 3020ND21.5 21.9 Chlorobenzene ug/L 20 103 60-140102 1 3020ND20.6 20.5 Chloroethane ug/L 20 110 60-140107 3 3020ND22.1 21.3 Chloroform ug/L 20 102 60-14099 2 3020ND20.3 19.9 Chloromethane ug/L 20 91 60-14095 4 3020ND18.2 18.9 cis-1,2-Dichloroethene ug/L 20 101 60-14098 2 3020ND20.1 19.6 cis-1,3-Dichloropropene ug/L 20 97 60-14099 3 3020ND19.3 19.8 Dibromochloromethane ug/L 20 93 60-14093 0 3020ND18.6 18.6 Dibromomethane ug/L 20 98 60-14097 1 3020ND19.6 19.4 Dichlorodifluoromethane ug/L 20 97 60-14098 0 3020ND19.5 19.5 Diisopropyl ether ug/L 20 96 60-14094 2 3020ND19.1 18.7 Ethylbenzene ug/L 20 103 60-140103 1 3020ND20.7 20.5 Hexachloro-1,3-butadiene ug/L 20 104 60-14098 5 3020ND20.7 19.7 Isopropylbenzene (Cumene)ug/L 20 102 60-140101 1 3020ND20.3 20.2 m&p-Xylene ug/L 40 103 60-140101 1 3040ND41.1 40.6 Methyl-tert-butyl ether ug/L 20 103 60-140100 3 3020ND20.6 19.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1656344MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283830006 1656345 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 96 60-14096 1 3020ND19.4 19.3 n-Butylbenzene ug/L 20 110 60-140108 2 3020ND22.0 21.7 n-Propylbenzene ug/L 20 104 60-140103 1 3020ND20.9 20.7 Naphthalene ug/L 20 100 60-14098 2 3020ND20.0 19.5 o-Xylene ug/L 20 98 60-14098 0 3020ND19.6 19.6 sec-Butylbenzene ug/L 20 105 60-140104 0 3020ND20.9 20.8 Styrene ug/L 20 99 60-14098 1 3020ND19.9 19.6 tert-Butylbenzene ug/L 20 86 60-14085 0 3020ND17.1 17.1 Tetrachloroethene ug/L 20 104 60-140100 4 3020ND20.8 19.9 Toluene ug/L 20 102 60-140104 2 3020ND20.4 20.8 trans-1,2-Dichloroethene ug/L 20 105 60-140104 1 3020ND21.1 20.8 trans-1,3-Dichloropropene ug/L 20 96 60-14094 2 3020ND19.1 18.8 Trichloroethene ug/L 20 101 60-140102 0 3020ND20.3 20.4 Trichlorofluoromethane ug/L 20 116 60-140116 1 3020ND23.1 23.3 Vinyl chloride ug/L 20 111 60-140110 0 3020ND22.1 22.1 1,2-Dichloroethane-d4 (S)%101 70-13099 4-Bromofluorobenzene (S)%99 70-13098 Toluene-d8 (S)%101 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/42669 SM 3500-Fe B SM 3500-Fe B Iron, Ferrous Associated Lab Samples:92283758001, 92283758002, 92283758003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1653004 Associated Lab Samples:92283758001, 92283758002, 92283758003 Matrix:Water AnalyzedMDL Iron, Ferrous mg/L <0.50 0.50 N201/25/16 17:050.50 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1653005LABORATORY CONTROL SAMPLE: LCSSpike Iron, Ferrous mg/L 1.6 N21.5 108 90-110 Parameter Units Dup Result Max RPD QualifiersRPDResult 92283542003 1653006SAMPLE DUPLICATE: Iron, Ferrous mg/L <0.50 H1,N210<0.50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/26197 EPA 300.0 EPA 300.0 300.0 IC Anions Associated Lab Samples:92283758001, 92283758002, 92283758003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1652562 Associated Lab Samples:92283758001, 92283758002, 92283758003 Matrix:Water AnalyzedMDL Sulfate mg/L <2.0 2.0 01/25/16 11:471.0 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1652563LABORATORY CONTROL SAMPLE: LCSSpike Sulfate mg/L 19.020 95 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 1652564MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283758001 1652565 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Sulfate mg/L 20 106 90-110105 1 10201.5J 22.7 22.5 Parameter Units MS Result % Rec Limits Qual% RecConc. 1652566MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283758002 1652567 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Sulfate mg/L 20 94 90-11094 0 10201.8J 20.7 20.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 45 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/26181 EPA 353.2 EPA 353.2 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples:92283758001, 92283758002, 92283758003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1651538 Associated Lab Samples:92283758001, 92283758002, 92283758003 Matrix:Water AnalyzedMDL Nitrogen, Nitrate mg/L <0.020 0.020 01/21/16 09:470.010 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1651539LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 2.42.5 95 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 1651540MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283613014 1651541 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Nitrogen, Nitrate mg/L 2.5 95 90-11094 1 102.50.085 2.5 2.4 Parameter Units MS Result % Rec Limits Qual% RecConc. 1651542MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92283758001 1651543 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Nitrogen, Nitrate mg/L 2.5 92 90-11091 1 102.51.1 3.4 3.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 45 #=QL# QUALIFIERS Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C Pace Analytical Services - MinneapolisPASI-M ANALYTE QUALIFIERS Common Laboratory Contaminant.C9 Analysis conducted outside the EPA method holding time.H1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 The lab does not hold TNI accreditation for this parameter.N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 45 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92283758 CAJAH'S MOUNTAIN Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92283758001 AIR/25074DMW-1 RSK 175 92283758002 AIR/25074DMW-2 RSK 175 92283758003 AIR/25074DMW-3 RSK 175 92283758001 MPRP/20524 ICP/18522DMW-1 EPA 3010A EPA 6010 92283758002 MPRP/20524 ICP/18522DMW-2 EPA 3010A EPA 6010 92283758003 MPRP/20524 ICP/18522DMW-3 EPA 3010A EPA 6010 92283758004 MPRP/20524 ICP/18522MW-1 EPA 3010A EPA 6010 92283758005 MPRP/20524 ICP/18522MW-2 EPA 3010A EPA 6010 92283758006 MPRP/20524 ICP/18522MW-5 EPA 3010A EPA 6010 92283758007 MPRP/20524 ICP/18522MW-7 EPA 3010A EPA 6010 92283758008 MPRP/20524 ICP/18522MW-8 EPA 3010A EPA 6010 92283758009 MPRP/20524 ICP/18522MW-11 EPA 3010A EPA 6010 92283758001 MSV/35256DMW-1 SM 6200B 92283758002 MSV/35256DMW-2 SM 6200B 92283758003 MSV/35256DMW-3 SM 6200B 92283758004 MSV/35256MW-1 SM 6200B 92283758005 MSV/35294MW-2 SM 6200B 92283758006 MSV/35256MW-5 SM 6200B 92283758007 MSV/35294MW-7 SM 6200B 92283758008 MSV/35256MW-8 SM 6200B 92283758009 MSV/35256MW-11 SM 6200B 92283758010 MSV/35256PW-1 SM 6200B 92283758011 MSV/35256PW-18 SM 6200B 92283758001 WET/42669DMW-1 SM 3500-Fe B 92283758002 WET/42669DMW-2 SM 3500-Fe B 92283758003 WET/42669DMW-3 SM 3500-Fe B 92283758001 WETA/26197DMW-1 EPA 300.0 92283758002 WETA/26197DMW-2 EPA 300.0 92283758003 WETA/26197DMW-3 EPA 300.0 92283758001 WETA/26181DMW-1 EPA 353.2 92283758002 WETA/26181DMW-2 EPA 353.2 92283758003 WETA/26181DMW-3 EPA 353.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 01/29/2016 03:35 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 45 Page 44 of 45 Page 45 of 45 12/23/15 Technical Report for Cardno ATC Associates, Inc Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC 89.03451.1018 Accutest Job Number: FA30067 Sampling Date: 12/15/15 Report to: Cardno ATC Associates 4020 Old Pineville Rd Charlotte, NC 28217 Michael.d.shaw@cardno.com; christine.dupuis@atcassociates.com ATTN: Christine Dupuis Total number of pages in report: Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001) DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177), AK, AR, GA, KY, MA, NV, OK, UT, WA This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. Southeast 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407-425-6700 fax: 407-425-0707 http://www.accutest.com Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Southeast 12/23/15 e-Hardcopy 2.0 Automated Report 15 Accutest Laboratories is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. 1 of 15 FA30067 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................5 3.1: FA30067-1: INFF ON SITE .........................................................................................6 3.2: FA30067-2: INFF OFF SITE ........................................................................................7 Section 4: Misc. Forms ............................................................................................................8 4.1: Chain of Custody ...........................................................................................................9 Section 5: GC Volatiles - QC Data Summaries .....................................................................12 5.1: Method Blank Summary ................................................................................................13 5.2: Blank Spike Summary ...................................................................................................14 5.3: Duplicate Summary .......................................................................................................15 1 2 3 4 5 2 of 15 FA30067 Accutest Laboratories Sample Summary Cardno ATC Associates, Inc Job No:FA30067 Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Project No: 89.03451.1018 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA30067-1 12/15/15 16:00 JV 12/17/15 AIR Air INFF ON SITE FA30067-2 12/15/15 16:15 JV 12/17/15 AIR Air INFF OFF SITE 3 of 15 FA30067 1 Summary of Hits Page 1 of 1 Job Number:FA30067 Account:Cardno ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Collected:12/15/15 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA30067-1 INFF ON SITE Benzene 5.9 0.50 0.10 ppmv EPA TO-3 Toluene 51.6 0.50 0.10 ppmv EPA TO-3 Ethylbenzene 10.6 0.50 0.10 ppmv EPA TO-3 Xylenes (total)49.9 1.5 0.30 ppmv EPA TO-3 TPH as Equiv Pentane 704 5.0 1.0 ppmv EPA TO-3 Benzene 19 1.6 0.32 mg/m3 EPA TO-3 Toluene 194 1.9 0.38 mg/m3 EPA TO-3 Ethylbenzene 46.0 2.2 0.43 mg/m3 EPA TO-3 Xylenes (total)217 6.5 1.3 mg/m3 EPA TO-3 TPH as Equiv Pentane 2070 15 2.9 mg/m3 EPA TO-3 FA30067-2 INFF OFF SITE No hits reported in this sample. 4 of 15 FA30067 2 Accutest Laboratories Sample Results Report of Analysis Southeast Section 3 5 of 15 FA30067 3 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID:INFF ON SITE Lab Sample ID:FA30067-1 Date Sampled:12/15/15 Matrix:AIR - Air Date Received:12/17/15 Method:EPA TO-3 Percent Solids:n/a Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 HH052726.D 1 12/17/15 SH n/a n/a GHH2923 Run #2 Initial Volume Run #1 0.50 ml Run #2 Purgeable Aromatics CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units 71-43-2 78.11 Benzene 5.9 0.50 0.10 ppmv 19 1.6 0.32 mg/m3 108-88-3 92.14 Toluene 51.6 0.50 0.10 ppmv 194 1.9 0.38 mg/m3 100-41-4 106.2 Ethylbenzene 10.6 0.50 0.10 ppmv 46.0 2.2 0.43 mg/m3 1330-20-7 106.2 Xylenes (total)49.9 1.5 0.30 ppmv 217 6.5 1.3 mg/m3 1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3 72 TPH as Equiv Pentane 704 5.0 1.0 ppmv 2070 15 2.9 mg/m3 CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 116%54-142% 460-00-4 4-Bromofluorobenzene 118%54-142% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 15 FA30067 3 3. 1 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID:INFF OFF SITE Lab Sample ID:FA30067-2 Date Sampled:12/15/15 Matrix:AIR - Air Date Received:12/17/15 Method:EPA TO-3 Percent Solids:n/a Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 HH052727.D 1 12/17/15 SH n/a n/a GHH2923 Run #2 Initial Volume Run #1 0.50 ml Run #2 Purgeable Aromatics CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units 71-43-2 78.11 Benzene ND 0.50 0.10 ppmv ND 1.6 0.32 mg/m3 108-88-3 92.14 Toluene ND 0.50 0.10 ppmv ND 1.9 0.38 mg/m3 100-41-4 106.2 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 0.43 mg/m3 1330-20-7 106.2 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 1.3 mg/m3 1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3 72 TPH as Equiv Pentane ND 5.0 1.0 ppmv ND 15 2.9 mg/m3 CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 99%54-142% 460-00-4 4-Bromofluorobenzene 108%54-142% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 15 FA30067 3 3. 2 Accutest Laboratories Misc. Forms Custody Documents and Other Forms Includes the following where applicable: Chain of Custody Southeast Section 4 8 of 15 FA30067 4 FA30067: Chain of Custody Page 1 of 3 9 of 15 FA30067 4 4. 1 FA30067: Chain of Custody Page 2 of 3 10 of 15 FA30067 4 4. 1 FA30067: Chain of Custody Page 3 of 3 11 of 15 FA30067 4 4. 1 Accutest Laboratories GC Volatiles QC Data Summaries Includes the following where applicable: Method Blank Summaries Blank Spike Summaries Matrix Spike and Duplicate Summaries Southeast Section 5 12 of 15 FA30067 5 Method Blank Summary Page 1 of 1 Job Number:FA30067 Account:ATCNCC Cardno ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GHH2923-MB HH052712.D 1 12/17/15 SH n/a n/a GHH2923 The QC reported here applies to the following samples:Method: EPA TO-3 FA30067-1, FA30067-2 CAS No.Compound Result RL MDL Units Q Result RL Units 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 mg/m3 71-43-2 Benzene ND 0.50 0.10 ppmv ND 1.6 mg/m3 108-88-3 Toluene ND 0.50 0.10 ppmv ND 1.9 mg/m3 100-41-4 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 mg/m3 1330-20-7 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 mg/m3 TPH as Equiv Pentane ND 5.0 1.0 ppmv ND 15 mg/m3 CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 102%54-142% 460-00-4 4-Bromofluorobenzene 112%54-142% 13 of 15 FA30067 5 5. 1 . 1 Blank Spike Summary Page 1 of 1 Job Number:FA30067 Account:ATCNCC Cardno ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GHH2923-BS HH052711.D 1 12/17/15 SH n/a n/a GHH2923 The QC reported here applies to the following samples:Method: EPA TO-3 FA30067-1, FA30067-2 Spike BSP BSP CAS No.Compound ppmv ppmv %Limits 1634-04-4 Methyl Tert Butyl Ether 10 8.1 81 60-111 71-43-2 Benzene 10 9.3 93 64-111 108-88-3 Toluene 10 9.3 93 60-112 100-41-4 Ethylbenzene 10 8.2 82 59-112 1330-20-7 Xylenes (total)30 25.5 85 58-110 TPH as Equiv Pentane 135 103 76 66-116 CAS No.Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 90%54-142% 460-00-4 4-Bromofluorobenzene 107%54-142% * = Outside of Control Limits. 14 of 15 FA30067 5 5. 2 . 1 Duplicate Summary Page 1 of 1 Job Number:FA30067 Account:ATCNCC Cardno ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA30050-2DUP HH052720.D 1 12/17/15 SH n/a n/a GHH2923 FA30050-2 HH052719.D 1 12/17/15 SH n/a n/a GHH2923 The QC reported here applies to the following samples:Method: EPA TO-3 FA30067-1, FA30067-2 FA30050-2 DUP CAS No.Compound ppmv Q ppmv Q RPD Limits 1634-04-4 Methyl Tert Butyl Ether 0.50 U ND nc 10 71-43-2 Benzene 0.50 U ND nc 11 108-88-3 Toluene 0.50 U ND nc 14 100-41-4 Ethylbenzene 0.50 U ND nc 13 1330-20-7 Xylenes (total)1.5 U ND nc 15 TPH as Equiv Pentane 40.8 40.8 0 28 CAS No.Surrogate Recoveries DUP FA30050-2 Limits 460-00-4 4-Bromofluorobenzene 103%104%54-142% 460-00-4 4-Bromofluorobenzene 113%113%54-142% * = Outside of Control Limits. 15 of 15 FA30067 5 5. 3 . 1 ACTIVE REMEDIATION MONITORING REPORT Cajah’s Mountain Superette 1990 Connelly Springs Road Lenoir, Caldwell County, North Carolina 28645 Facility ID No. 0-004593 NCDEQ Incident No. 28649 Risk Classification: High (H190D) ATC Project No. CARCAJA August 31, 2016 7606 Whitehall Executive Center Drive, Suite 800 Charlotte, NC 28273 Tel: 704-529-3200 Fax: 704-529-3272 www.atcgroupservices.com N.C. Engineering License No. C-1598 August 31, 2016 Mr. Dan Murphy North Carolina Department of Environmental Quality Asheville Regional Office Division of Waste Management - UST Section 2090 US Highway 70 Swannanoa, North Carolina 28778 RE: Active Remediation Monitoring Report Cajah’s Mountain Superette 1990 Connelly Springs Road Lenoir, Caldwell County, North Carolina 28645 Facility ID No. 0-004593 NCDEQ Incident No. 28649 Risk Classification: High (H190D) ATC Project No. CARCAJA Dear Mr. Murphy: ATC Associates of North Carolina, P.C., on behalf of Cary Oil Company, is submitting the enclosed Active Remediation Monitoring Report for the Cajah’s Mountain Superette site. This report includes information pertaining to operation and maintenance of the on-site and off-site air sparge and soil vapor extraction systems and data from a groundwater monitoring event conducted in July 2016. If you have any questions or require additional information, please contact us at (704) 529-3200. Sincerely, ATC Associates of North Carolina, P.C. Christine E. Schaefer Project Manager cc: Mr. Glenn Petti – Cary Oil Company Site Identification: Date of Report: August 31, 2016 Facility I.D.: 0-004593 UST Incident Number (if known): 28649 Site Risk: High Site Rank: H190D Land Use Category: Commercial Site Name: Cajah’s Mountain Superette Site Street Address: 1990 Connelly Springs Road City/Town: Lenoir Zip Code: 28645 County: Caldwell Description of Geographical Data Point (e.g., diesel fill port): Former Tank Basin Location Method (GPS, topographical map, other): Google Earth Latitude (decimal degrees): 35.83749120° N Longitude (decimal degrees): 81.5387323° W Information about Contacts Associated with the Leaking UST System: UST Owner: Cary Oil Company Address: 110 MacKenan Drive, Suite 300, Cary, NC 27511 Phone: (919) 462-3194 Property Owner: Mary Lindsay Address: 127 Dell Circle, Hudson, NC 28638 Phone: (828) 728-2674 Property Occupant: Mooresridge Catering (Walter Moore) Address: 1990 Connelly Springs Road, Lenoir, NC 28645 Phone: (828) 728-0859 Consultant/Contractor: ATC Associates of North Carolina, P.C. Address: 7606 Whitehall Executive Center Dr., Charlotte, NC 28273 Phone: (704) 529-3200 Analytical Laboratory: Pace Analytical Services, Inc. State Certification No.: 5342 Address: 9800 Kincey Avenue, Suite 100, Huntersville, NC 28078 Phone: (704) 875-9092 Information about Release: Date Discovered: August 28, 2008 Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release (Dispenser/Piping/UST): Unknown Sizes and contents of UST system(s) from which the release occurred: Two 8,000-gallon gasoline USTs and one 4,000-gallon gasoline UST and associated dispensers Information about the Monitoring Report: Date of Groundwater Monitoring Event: July 19 and 20, 2016 Period of Time Reported: 5/1/16 – 7/31/16 Type of Monitoring Report: Subsequent Active Remediation Monitoring Report I, David A. Hunter, a Professional Engineer/Licensed Geologist (circle one) for ATC Associates of North Carolina, P.C., do certify that the information contained in this report is correct and accurate to the best of my knowledge. ATC Associates of North Carolina, P.C. is licensed to practice geology/engineering (circle one or both) in North Carolina. The certification number issued by the North Carolina Board for Licensing of Geologists is C- 274. The certification number issued by the North Carolina Board of Examiners for Engineers and Surveyors is C-1598. TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY ............................................................................................................. 1 2.0 SUPPORTING INFORMATION AND CAP IMPLEMENTATION ......................................... 2 3.0 GROUNDWATER INVESTIGATION ......................................................................................... 3 3.1 Fluid Measurements and Free Product Conditions .............................................................. 3 3.2 Groundwater Monitoring ...................................................................................................... 4 4.0 REMEDIATION SYSTEM PERFORMANCE ............................................................................ 5 5.0 CONCLUSIONS AND RECOMMENDATIONS ......................................................................... 6 6.0 REPORT LIMITATIONS .............................................................................................................. 7 TABLES Table 1 Site History Table 2 Public and Private Water Supply Well and Other Receptor Information Table 3 Property Owners/Occupants and Land Use Information Table 4 Summary of Groundwater Sampling Results Table 5 Historical Groundwater Sampling Results Table 6 Monitored Natural Attenuation Parameters Table 7 Monitoring Well Construction and Groundwater Elevation Information Table 8 Groundwater Sampling Water Quality Parameters Table 9 Vertical Hydraulic Gradient Evaluations Table 10 Free Product Recovery Information Table 11 SVE System Cumulative Recovery FIGURES Figure 1 Site Topographic Map Figure 2 Site Map Figure 3 Site Vicinity Map Figure 4 Groundwater Elevation Contour Map Figure 5 Dissolved Benzene Isoconcentration Contour Map Figure 6 Dissolved MTBE Isoconcentration Contour Map APPENDICES Appendix A Standard Operating Procedures Appendix B Laboratory Analytical Reports Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 1 1.0 EXECUTIVE SUMMARY Cary Oil Company (Cary Oil) retained ATC Associates of North Carolina, P.C. (ATC) to prepare an Active Remediation Monitoring Report for the project site located at 1990 Connelly Springs Road in Lenoir, Caldwell County, North Carolina. Figure 1 shows the site and vicinity on part of a United States Geological Survey (USGS) site topographic map. This report documents remedial system operation and maintenance activities and the results of a groundwater monitoring event conducted in July 2016. According to groundwater analytical results obtained from the monitoring event performed on July 19 and 20, 2016, concentrations of petroleum contaminants of concern, excluding lead, were detected above the associated North Carolina NCAC 2L.0202 standards (2L standards) in nine site monitoring wells. Free product was not observed in site wells during the July 2016 monitoring event. Monitoring well MW-6 was not sampled due to the presence of sediment in the well. The risk classification for the site has been designated as “High” and ranked H190D by the North Carolina Department of Environmental Quality (NCDEQ). Therefore, groundwater contamination must be remediated to concentration levels which are equal to or less than the associated 2L standards. As outlined in the October 31, 2012, Corrective Action Plan (CAP), high vacuum extraction through the implementation of Aggressive Fluid/Vapor Recovery (AFVR) technology appeared to be the most feasible and cost effective option for recovering remaining free product on-site. Air sparge and soil vapor extraction (AS/SVE) were the chosen corrective action technologies for shallow petroleum-impacted groundwater at this site based on site conditions and technical considerations. Natural attenuation was determined to be the most feasible and cost effective remedial option for reducing groundwater contaminant concentrations in portions of the intermediate and deep zones of the unconfined aquifer. Air sparge and soil vapor extraction wells were installed at the site on December 30, 2013, through January 15, 2014. The on-site and off-site system installations were completed on January 13, 2014, through January 24, 2014. System startup activities were conducted on March 26, 2014. However, due to noise concerns, the off-site system was turned off until April 9, 2014, when the telemetry was programmed to operate the system from 8:00 am to 8:00 pm. Efforts have been made to reduce excessive noise that originates from the building but minimal reductions have been observed. Following free product recovery from the source area, air sparge wells AS-1 through AS-3 were activated in October 2015. On-site system run-time was 58% from May 11 to Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 2 July 26, 2016. Off-site system run-time was 28% from May 11 to July 26, 2016 (the system is programmed to shut down during nighttime hours). Downtime was generally attributable to warm weather and subsequent elevated system building temperatures that led to high temperature alarms. Based on laboratory analytical results from quarterly effluent air sampling, approximately 799.8 and 0.2043 pounds of total BTEX have been recovered by the on-site and off-site SVE systems, respectively, from startup through June 27, 2016. Additional system performance information is included in Section 4.0. 2.0 SUPPORTING INFORMATION AND CAP IMPLEMENTATION Soil impact was identified during underground storage tank removals in August 2008, and NCDEQ subsequently requested site assessment. Between 2009 and 2013, site assessment, AFVR events for free product recovery, and a CAP with pilot testing were completed related to the Cajah’s release. Monitoring wells installed as part of assessment activities are indicated on Figure 2. Free product recovery efforts in the form of AFVR events, conducted between March 2012 and December 2013, recovered approximate totals of 44 gallons of liquid phase product, 54.17 gallons of vaporized product, and 1,870 gallons of petroleum contact water from well MW-8. Historical free product recovery information is summarized in Table 10. Adsorbent socks were installed and changed as necessary in well MW-8 beginning in February 2015 to recover remaining free product. The sock was removed in early July 2015, and the well has not indicated free product during subsequent groundwater monitoring events. Baton Water Corporation and the Town of Lenoir supply public water in the site vicinity. Twenty-one (21) private water supply wells have been identified within approximately 1,500 feet of the site. Water supply well information for the area is summarized in Table 2, and supply well locations relative to the source area are depicted on Figure 3. Historical analytical results from sampled supply wells are included in Table 5. Based on results of the CAP and pilot testing, ATC found that AFVR, AS/SVE technologies, and natural attenuation appeared to be the most feasible and cost effective remedial options for recovering free product and reducing groundwater contaminant concentrations associated with Incident No. 28649. Due to potential complications associated with horizontal boring under Connelly Springs Road and potential to affect underground utilities, two separate AS/SVE remediation systems were recommended to reduce groundwater concentrations on-site and in the immediate vicinity and on the east side of Connelly Springs Road. Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 3 With the exception of one SVE well installed as part of the pilot test in 2012, the systems were installed during the period of December 2013 through January 2014. The on-site and off-site air sparge systems consist of six and eight air sparge wells, respectively, rotary claw air compressors, and schedule 80 PVC piping for transferring compressed air from the remediation systems to the air sparge wells. The on-site and off-site vapor extraction systems consist of nine and five vapor extraction wells, respectively, regenerative vacuum blowers, condensate collection vessels, and schedule 40 PVC piping for transferring extracted vapors from the vapor extraction wells to the remediation systems. System startup activities were conducted on March 26, 2014. However, due to noise concerns, the off-site system was turned off until April 9, 2014, when the telemetry was programmed to operate the system from 8:00 am to 8:00 pm. Efforts have been made to reduce excessive noise that originates from the building, but minimal reductions have been observed. Monitoring well MW-8 was gauged on March 26, 2014, prior to system startup, and contained 0.43 feet of free product. On-site air sparge wells AS-1 through AS-3 were left off, by means of closed system manifold valves, until free product could be sufficiently recovered from the area. Following installations of adsorbent product socks, free product has been sufficiently reduced, and operation of AS-1 through AS-3 began in October 2015. For a detailed description of site environmental information, please refer to an earlier ARMR or the CAP. 3.0 GROUNDWATER INVESTIGATION 3.1 Fluid Measurements and Free Product Conditions On July 19 and 20, 2016, an oil/water interface probe was used to check for the presence of free product and measure static water levels at monitoring wells MW-1, MW-2, MW-5, MW-6, MW-7, MW-8, MW-11, MW-12, MW-14, MW-18, MW-22, IMW-1, IMW-2, and DMW-1 through DMW-5. Product was not observed in site monitoring wells. Sediment was encountered from a depth of approximately 32 feet below TOC to the bottom of the screen in well MW-6. Groundwater elevations were determined in reference to the surveyed top of well casing elevations. Relevant field methods are summarized in Appendix A. Groundwater elevations were calculated based on the July 19 and 20, 2016, gauging data, and a summary of historical groundwater elevation data are included in Table 7. A groundwater elevation contour map, based on the July 2016 static water level data, is included as Figure 4. Groundwater flow direction across the site is generally towards the east-southeast with an estimated horizontal hydraulic gradient of 0.023 across the center of plume mass, based on July 2016 elevation data. Vertical gradient information is provided in Table 9, which shows downward migration between shallower wells MW-2 and DMW-1 with deeper well DMW-3 in front of the on-site building. An upward Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 4 gradient between wells MW-2 and DMW-1 was seen in the same area. Downward migration was seen between shallow well MW-22 with both intermediate and deep aquifer zones in IMW-2 and DMW-5, while an upward gradient was observed between intermediate and deep wells IMW-2 and DMW-5. An upward gradient was observed between wells MW-14 and IMW-1. 3.2 Groundwater Monitoring Groundwater samples were obtained from monitoring wells MW-1, MW-2, MW-5, MW-7, MW-8, MW-11, MW-12, MW-14, MW-18, MW-22, IMW-1, IMW-2, and DMW-1 through DMW-5 on July 19 and 20, 2016. Due to historically consistent lack of property owner response to requests for sampling, water supply wells were not proposed for sample collection during the July 2016 monitoring event. Water supply well sampling attempts may be re-evaluated by ATC and the NCDEQ in the future. Prior to sampling, each monitoring well was purged of three standing water columns, or until the well was purged dry. Measurements of dissolved oxygen, pH, oxidation reduction potential, specific conductivity, and temperature were collected from each well volume purged. The water quality readings are provided in Table 8. Samples were then collected with new disposable bailers and poured directly into laboratory- provided containers with appropriate preservatives. The samples were then placed in a chilled cooler and submitted to North Carolina-accredited Pace Analytical Services, Inc. of Huntersville, North Carolina, using proper chain-of-custody procedures for laboratory analyses. Groundwater samples from the site monitoring well network were analyzed for volatile organic compounds by EPA Method 6200B including BTEX, MTBE, and isopropyl ether (IPE) and by EPA Method 6010 for lead. Samples have also historically been analyzed by Massachusetts Department of Environmental Protection (MADEP) volatile petroleum hydrocarbons (VPH) and EPA Method 504.1 for ethylene dibromide (EDB). Under the direction of the NCDEQ, the MADEP analysis was not performed starting in July 2015, and the EPA Method 504.1 analysis was not performed starting in January 2016. Although EDB is reported under EPA Method 6200B, the analysis cannot attain the reduced detection limit required by the 2L standard. Confirmation sampling that incorporates MADEP VPH and EPA Method 504.1 analysis will be performed prior to site closure. The intermediate and deep monitoring wells were also historically analyzed for natural attenuation parameters including nitrate, ferrous iron, sulfate, methane, and manganese. These analytes were not pre-approved for trust fund reimbursement, and were therefore not analyzed, in July 2016. Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 5 According to the analytical results, concentrations of petroleum hydrocarbons were detected above the associated 2L standards in monitoring wells MW-1, MW-2, MW-5, MW-7, MW-8, MW-11, MW-18, IMW- 1, and DMW-1. Concentrations of lead were reported above the 2L standard in wells MW-1, MW-2, MW-7, MW-8, MW-11, MW-12, MW-14, MW-18, MW-22, and IMW-1. However, the occurrence of lead in the aquifer seems generally disassociated with the contaminant plume and is likely naturally occurring. The lead results may also be a result of bias based on sediment inclusion in the samples. Based on current and historical analytical results, groundwater contamination above NCDEQ 2L standards is generally located in front of the on-site building in the vicinity of the former UST system and migrates downgradient to the east- southeast across Connelly Springs Road towards IMW-1 and slightly to the southwest towards wells MW-9 and DMW-2. Historical natural attenuation sampling indicates an environment conducive to potential bioremediation in the intermediate and deep aquifer zones. Generally, measured dissolved oxygen concentrations are consistently above anoxic and hypoxic conditions, indicating a potential for aerobic activity. Petroleum compound concentrations had generally shown an increasing trend in downgradient, intermediate well IMW-1, until January 2016 when concentrations began decreasing. Impact in this well should continue to be monitored and remedial system adjustments should be made as deemed necessary. Impact in on-site, deep well DMW-1 is generally decreasing with time. Contaminants of concern in other intermediate and deep wells remain minimal. Groundwater analytical results obtained in July 2016 are summarized in Table 4. Isoconcentration contour maps for dissolved benzene and MTBE are included as Figures 5 and 6, respectively. Please note that the figures display contours of vertical maximum impact due to the prevalence of impact from intermediate zone wells. Historical summaries of groundwater analytical results are provided in Table 5 and Table 6. Copies of the July 2016 laboratory analytical report and chain-of-custody forms are included in Appendix B. 4.0 REMEDIATION SYSTEM PERFORMANCE System startup activities were conducted on March 26, 2014. However, due to noise concerns, the off-site system was turned off until April 9, 2014, when the telemetry was programmed to operate the system from 8:00 am to 8:00 pm. Efforts have been made to reduce excessive noise that originates from the building, but Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 6 minimal reductions have been observed. Due to bad motor windings, the off-site SVE blower was replaced under warranty by the system fabricator on October 15, 2014. Air sparge wells AS-1 through AS-3 were left off, by means of closed system manifold valves, until free product could be sufficiently recovered from the on-site source area. Following free product recovery using adsorbent product socks, air sparge wells AS-1 through AS-3 were activated in October 2015. System operation and maintenance (O&M) visits were conducted twice per month from May through July 2016 to check system components and perform routine maintenance. On-site system run-time was 58% from May 11 to July 26, 2016. During system operation, vacuum readings for each well point at the on-site SVE manifold were set at approximately 50 inches of water. Pressure readings for each well point at the on-site AS manifold were set at approximately 11 psi. Off-site wells AS-9 through AS-12 were shut down in April 2016 to provide more sparge pressure to the west side of the property where higher dissolved concentrations exist. Off-site system run-time was 28% from May 11 to July 26, 2016 (the system is programmed to shut down during nighttime hours). System downtime due to overheating also occurred. During system operation, vacuum readings for each well point at the off- site SVE manifold were set at approximately 52 inches of water. Pressure readings for each well point at the off-site AS manifold were set at approximately 13 psi. Effluent air samples were collected from the on-site and off-site SVE systems on June 27, 2016, to evaluate petroleum vapor removal and to assist with system optimization efforts. The air samples were submitted to Accutest Laboratories for analysis by EPA Method TO-18. The laboratory analytical report is provided in Appendix B. Table 11 shows SVE cumulative recovery calculations based on system effluent sampling data. Assuming consistent recovery during each day of operation between sampling dates, approximately 799.8 and 0.2043 pounds of total BTEX have been recovered by the on-site and off-site SVE systems, respectively, from startup through June 27, 2016. 5.0 CONCLUSIONS AND RECOMMENDATIONS A groundwater monitoring event was conducted at the Cajah’s Mountain Superette site on July 19 and 20, 2016, to obtain current groundwater data. Recent and historical results indicate groundwater contamination above NCDEQ 2L standards is generally located in front of the on-site building in the vicinity of the former UST system and migrates downgradient to the east-southeast across Connelly Cajah’s Mountain Superette August 31, 2016 Active Remediation Monitoring Report Page 7 Springs Road towards well IMW-1 and slightly to the southwest towards wells MW-9 and DMW-2. System startup activities were conducted at the site on March 26, 2014, and O&M visits are being conducted twice per month, as proposed in the CAP. Adjustments to the off-site SVE system were made in April 2016 to focus efforts on the western portion of the off-site property. Significantly lower contaminant concentrations were subsequently observed in off-site well MW-11 in July 2016. Well MW- 11 has historically contained the highest off-site shallow aquifer impact concentrations. Additional groundwater monitoring and operation and maintenance of the site systems are recommended, as outlined in the CAP. 6.0 REPORT LIMITATIONS This investigation is intended to be a non-biased assessment of on-site environmental conditions proximate to the location of the former and/or current UST system. Subsurface investigative and remedial methodologies were performed in general accordance with applicable state and federal regulatory requirements. The information presented in this report is based upon site-specific observations, generally accepted geological and environmental consulting practices, and analytical results for environmental samples collected at the time of the field investigation was performed. The data presented in this report are believed to represent subsurface conditions at the facility; however, data may not be completely representative of subsurface conditions at every location. ATC assumes no liability arising from environmental impact to, or from, the site, regardless of the date of impact occurrence or findings. TABLES Table 1 Site History Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Zip Telephone Number 27511 (919) 462-3194 Zip Telephone Number 27511 (919) 462-3194 1 Gasoline None 4,000 Fiberglass 24' x 64" Fiberglass Reinforced Plastic Early 1980s Removed 8/14/08 Yes 2 Gasoline None 8,000 Fiberglass 8' x 21.4" Fiberglass Reinforced Plastic Early 1980s Removed 8/14/08 Yes 3 Gasoline None 8,000 Fiberglass 8' x 21.4" Fiberglass Reinforced Plastic Early 1980s Removed 8/14/08 Yes UST ID Number Current/Last Contents Previous Contents Capacity (gallons) Release confirmed during 8/14/08 excavation Tank Dimensions Description of Associated Piping and Pumps Date Tank Installed Status of Tank Was Release Associated With UST System? Date of Release Description of Release 28649 Gasoline 8/14/08 Incident Number Material Released Construction Details 0-004593 Name of Owner Dates of Ownership (m/dd/yy) to (m/dd/yy) UST ID Number(s) Facility ID Number 4/2005 to 8/14/2008 Name of Operator Street Address Dates of Operation (m/dd/yy) to (m/dd/yy) Cary Oil Company Cary NC 110 MacKenan Drive, Suite 300 City State UST ID Number(s) Facility ID Number 1, 2, and 3 0-004593 Street Address 110 MacKenan Drive, Suite 300 Cary Oil Company City State Cary NC 4/2005 to 8/14/2008 1, 2, and 3 Table 2 Public and Private Water Supply Well and Other Receptor Information Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 PW-1 Jimmie & Louise Beane / 1511 Bradshaw Terrace, Lenoir, NC 28645 1511 Bradshaw Terrace Lenoir 828-728-9368 Not in use Unknown Unknown 400 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-2 CitiMortgage, Inc. / 1000 Technology Drive, O'Fallon, MO 63368 1433 Brandon Road Lenoir NA In use for potable water by next- door Price & Shell Unknown Unknown 450 Downgradient Well services more than one residence (Price & Shell) PW-3 Henry & Linda Johnson / 1535 Bradshaw Terrace, Lenoir, NC 28645 1535 Bradshaw Terrace Lenoir 828-728-5256 Not in use Unknown Unknown 775 Downgradient Not accessible - According to Mr. Johnson, well has been filled over the years with sticks and rocks, and water is not accessible PW-4 Clifford & Jeanie Stewart / 319 Welcome Ave., Greenville, SC 29611 1554 Bradshaw Terrace Lenoir NA Not in use Unknown Unknown 1,100 Downgradient PW-5 Poarch Dixie Land Tate Azor / 1490 Land Street, Lenoir, NC 28645 1497 Land Street Lenoir NA Not in use Approx. 40-45' Unknown 1,000 Sidegradient PW-6 Ryan & Shirley Rozzelle / 186 Mountain Oak Lane, Hickory, NC 28601 1418 Brandon Road Lenoir 828-495-3456 Unknown Unknown Unknown 850 Sidegradient Current well use unknown; Property provided municipal water by Baton Water Corporation PW-7 Helen Sullivan / 904 Second St. NE, Apt. 234, Hickory, NC 28601 Justin Lane (No address number) Lenoir 828-728-2757 Not in use Unknown Unknown 1,200 Sidegradient Well operational but not in use and property provided municipal water by Baton Water Corporation PW-8 Brandon Apartments (Keith and Patricia Williams) / 1415 N. Catwaba Church Avenue, Lenoir, NC 28645 3715 Panda Lane Lenoir 828-728-9167 Not in use Unknown Unknown 1,000 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-9 Randy & Joyce Kestner / 4593 Horseshoe Bend Road, Hudson, NC 28638 3725 Happy Horse Lane Lenoir NA In use for potable water Unknown Unknown 1,100 Downgradient PW-10 Berry Kaylor / 3965 Greenwood Drive, Lenoir, NC 28645 3965 Greenwood Drive Lenoir 828-728-6946 Not in use Unknown Unknown 1,475 Sidegradient PW-11 Sherri Barnwell / 1499 Union Grove Road, Lenoir, NC 28645 1499 Union Grove Road Lenoir 828-728-3412 Not in use Unknown Unknown 1,300 Sidegradient Well not operational and property provided municipal water by Baton Water Corporation PW-12 Roger & Penny Triplett / 1740 Taylorsville Road SE, Lenoir, NC 28645 1512 Union Grove Road Lenoir NA Not in use Unknown Unknown 1,100 Sidegradient Property provided municipal water by Baton Water Corporation PW-13 William Rudicil / 1520 Union Grove Road, Lenoir, NC 28645 1520 Union Grove Road Lenoir NA Not in use Unknown Unknown 1,190 Sidegradient Property provided municipal water by Baton Water Corporation PW-14 Karen Sanders / 1522 Union Grove Road, Lenoir, NC 28645 1522 Union Grove Road Lenoir 828-726-1420 Not in use Unknown Unknown 1,210 Sidegradient PW-15 Arnold & Wanda Correll / 1528 Bradshaw Terrace, Lenoir, NC 28645 1528 Bradshaw Terrace Lenoir 828-728-7497 In use for outdoor/irrigation water Approx. 90 Unknown 525 Downgradient Well depth estimated by Mr. Correll; Property provided municipal water by Baton Water Corporation; Well only supplies water to outside spigots; Well not operational during winter PW-16 Theohary & Linda Smargian / PO Box 967, Hudson, NC 28638 1518 Bradshaw Terrace Lenoir NA Not in use Approx. 176* Unknown 400 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-17 Douglas & Katherine Hawkins / 1980 Connelly Springs Road, Lenoir, NC 28645 1980 Connelly Springs Road Lenoir NA Not in use Unknown Unknown 150 Sidegradient Well installed in 1961; Mary Lindsay (subject property owner) is POA; well is beneath house and not accessible PW-18 Jimmie & Louise Beane** / 1511 Bradshaw Terrace, Lenoir, NC 28645 1514 Bradshaw Terrace Lenoir NA Not in use Unknown Unknown 240 Downgradient Well not operational and property provided municipal water by Baton Water Corporation PW-20 Cajah's Mt Park LLC (Steve Hamby) / PO Box 1114, Hudson, NC 28638 0 Connellly Springs Road (Cajah's Mountain Mobile Home Park)Lenoir NA Not In use Unknown Unknown 325 Sidegradient No access to well, well reportedly not operational, and property provided municipal water by Baton Water Corporation PW-21 Paula Fetherbay c/o Paula St. Clair / 1975 Connelly Springs Road, Lenoir, NC 28645 1975 Connelly Springs Road Lenoir NA In use for potable water Unknown Unknown 375 Sidegradient PW-22 Daniel Ace / 3733 Happy Horse Lane, Lenoir, NC 28645 3733 Happy Horse Lane Lenoir NA Reportedly, in use for potable water Unknown Unknown 1,100 Downgradient N/A East N/A N/A Surface water 700 Downgradient Stream was not identified on USGS topographic map, but was depicted on Caldwell County Geographic Information website, and could not be located during field activities. N/A West N/A N/A Surface water 500 Downgradient Stream was not identified on USGS topographic map, but was depicted on Caldwell County Geographic Information website. * On 7/26/10, due to difficulty encountered gauging depth of the two foot diameter well with an o/w interface meter, it was estimated that depth of PW-16 was approximately 176 ft bgs, as the meter appeared to reach bottom at that depth. ** residential property is currently leased; The Beanes are the owner for the residential property NA = Not Available Potable Well ID Well Depth (ft bgs) Receptor ID Location Contact Property Owner Contact Information Property Address City Phone Number Well Screen Interval (ft) Well Use Comment Approx. distance from source area of release (ft) Up/Down/ or Crossgradient* Approx. distance from source area of release (ft) Up/Down/Crossgradient/Ot her Comment Unnamed intermittent stream Unnamed intermittent stream Description Phone Number Usage Table 3 Property Owners/Occupants and Land Use Information Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Site Mary Lindsay 2746795343 1990 Connelly Springs Road 127 Dell Circle, Hudson, NC Lenoir, NC Adjacent to North 2746794580 1980 Connelly Springs Road Douglas & Katherine Hawkins R-20 / Residence Lenoir, NC Adjacent Northeast (opposite Connelly Springs Road) 2746890460 1989 Connelly Springs Road Philip and Debbie Yott RA-20 / Residence Lenoir, NC Adjacent East (opposite Connelly Springs Road)Chuck and Mattie Triplett 2746799380 1995 Connelly Springs Road 1130 Rosedale Drive SW, Lenoir, NC RA-20 / Residence Lenoir, NC Adjacent Southeast (opposite Connelly Springs Road)Cajah's Mountain Park LLC 2746890106 1999 Connelly Springs Road PO Box 1114, Hudson, NC RA-20 / Mobile home park Lenoir, NC Adjacent to South 2746795237 1998 Connelly Springs Road Moore Family Partnership LLC Lenoir, NC Adjacent to West Jimmie and Louise Beane 2746793289 1514 Bradshaw Terrace 1511 Bradshaw Terrace, Lenoir, NC RA-20 / Residence Lenoir, NC Updated as of 3/18/2015. R-20 and RA-20 refer to residential zoning B-1 refers to business zoning B-1 / Frosty Frez Restaurant and separate associated office building Tax Parcel Pin # (and well ID # if applicable)Property Location and Address Owner's Name and Address (if different) Zoning/Land Use R-20 / Catering business (former gas station) Table 4 Summary of Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 EPA METHOD 6200B C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class (Target analytes reported above method detection limits) C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e Et h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X L e a d MW-1 7/20/2016 NA NA NA 1.9 3.7 <0.50 <0.50 4.4 <1.0 <0.50 <0.50 <0.50 <0.50 0.78 5.8 <0.50 0.42 J <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 8.1 14.1 9.0 28.2 59.4 20.5 MW-2 7/20/2016 NA NA NA 0.34 J <0.50 <0.50 <0.50 5.1 <1.0 <0.50 <0.50 <0.50 <0.50 0.46 J 4.4 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 6.9 <0.50 <0.50 1.35 J 8.25 J 37.1 MW-5 7/20/2016 NA NA NA 4.7 6.5 <0.50 <0.50 0.68 <1.0 <0.50 <0.50 <0.50 <0.50 1.7 <0.50 <0.50 0.41 J <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 1.2 3.3 4.1 103.0 111.6 13.6 MW-6 7/19/2016 MW-7 7/20/2016 NA NA NA 71.4 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 12.2 4.1 132 <1.0 6.5 1.2 <1.0 <1.0 NA <1.0 <1.0 13.5 235 152 38.6 266 691.6 67.3 MW-8 7/20/2016 NA NA NA 5,350 1,500 <62.5 <62.5 <62.5 <125 <62.5 <62.5 <62.5 <62.5 204 208 259 708 <62.5 <62.5 <62.5 NA <62.5 55.8 J 1,280 4,950 24,600 2,610 15,440 47,600 48.7 MW-11 7/19/2016 NA NA NA 851 201 <20.0 <20.0 <20.0 <40.0 <20.0 <20.0 <20.0 <20.0 34.1 138 <20.0 105 <20.0 <20.0 <20.0 NA <20.0 13.4 J 229 693 4,110 686 3,870 9,359 23.2 MW-12 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 6.4 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 50.5 MW-14 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 1.6 <0.50 14.2 <0.50 <0.50 0.29 J <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 92.6 MW-18 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.62 <0.50 <0.50 0.60 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 54.9 MW-22 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.41 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 56.3 IMW-1 7/19/2016 NA NA NA 1.7 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 0.25 J 23.6 0.63 150 <0.50 0.56 6.1 <0.50 <0.50 NA <0.50 <0.50 6.0 155 <0.50 4.2 12.1 171.3 15.4 IMW-2 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.51 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <5.0 DMW-1 7/20/2016 NA NA NA <0.50 <0.50 0.83 <0.50 11.3 <1.0 <0.50 <0.50 <0.50 0.84 <0.50 44.5 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.60 <0.50 <0.50 <1.5 0.60 12.9 DMW-2 7/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 4.4 J DMW-3 7/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 4.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <5.0 DMW-4 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.40 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 12.4 DMW-5 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.30 J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 13.7 400 700 200 400 400 0.6 4 70 3 0.4 NE 0.02 70 70 20 70 70 0.4 3 0.7 25 70 70 6 1 600 600 500 N/A 15 NE NE NE 28,500 25,000 NE 4,000 70,000 3,000 400 NE 50 70,000 25,000 20,000 6,900 30,000 400 3,000 700 11,700 8,500 70,000 6,000 5,000 260,000 84,500 85,500 N/A 15,000 1. All measurements are in micrograms per liter (ug/L). 7. NE = Not Established. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. (Amended Effective April 16, 2012) 8. VPH = Volatile Petroleum Hydrocarbons: C5-C8 and C9-C18 aliphatic chains, and C9-C22 aromatic chain 3. "<" or ND = Not detected above method detection limit or laboratory reporting limit. 9. Analytical table indicates target analyte concentrations reported above method detection limits. 4. GCL = Gross Contaminant Level established by NCDEQ. 10. NA = Not Analyzed for specified parameter 5. Target analyte concentrations detected above 2L Groundwater Standards are bolded. 11. N/A = Not Applicable 6. Target analyte concentrations detected above GCLs are bolded and italicized. 12. J = Estimated value below the laboratory reporting limit but above the method detection limit. GCLs NC 2L GW Standards Not Sampled Due to Mud/Sediment in Well EPA METHOD 6010 SAMPLE I.D.DATE SAMPLED MADEP VPH Page 1 of 1 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d 12/10/2008 180 1.6 42 3.1 1.6 0.65 <0.1 11 3.3 <0.1 <0.1 *<0.022 0.24 0.34 65 0.4 0.63 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 10 2.5 1.2 3.3 17.0 <0.022 110 11/17/2009 1,300 35 61 2.9 2.1 <0.1 <0.1 13 <0.1 <0.1 <0.1 *<0.022 <0.1 0.46 18 0.7 0.83 <0.2 <0.1 <0.2 0.53 <0.1 <0.1 <0.1 17 5.1 0.75 9.5 32.4 <0.022 149 2/3/2012 1,180 488 137 19.1 7.6 <0.50 <0.50 5.2 <1.0 <0.50 <0.50 *<0.020 <0.50 2.2 3.7 1.6 5.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.1 26.6 18.1 6.9 41.0 92.6 <0.020 36.6 8/22/2012 1,570 125 135 3.4 5.4 <0.12 <0.12 7.0 <0.20 <0.10 NA *0.020 0.22 J 3.5 6.1 1.4 6.4 <0.16 <0.18 <0.14 0.50 1.5 <0.10 <0.10 49.2 13.9 2.5 26.8 92.4 0.020 20.0 1/23/2014 549 <50.0 <50.0 1.5 1.7 <0.50 <0.50 8.1 <1.0 <0.50 <0.50 *<0.020 <0.50 1.1 0.75 0.53 0.96 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 11.4 0.54 <0.50 5.3 17.2 <0.020 10.0 7/18/2014 785 542 117 16.3 8.8 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 0.62 5.5 5.0 2.9 6.0 <0.50 <0.50 <0.50 NA 2.4 <0.50 <2.0 37.4 4.7 2.8 44.0 88.9 <0.020 47.0 1/14/2015 163 131 <50.0 <0.50 0.57 <0.50 <0.50 9.4 <1.0 <0.50 <0.50 *<0.020 <0.50 1.1 0.77 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.53 <0.50 <2.0 8.2 <0.50 <0.50 3.6 11.8 <0.020 37.4 7/22/2015 NA NA NA 0.98 1.40 <0.50 <0.50 8.5 <1.0 <0.50 <0.50 *<0.020 <0.50 0.93 0.81 <0.50 0.45 J <0.50 <0.50 <0.50 NA 0.49 J <0.50 <2.0 6.9 <0.50 <0.50 3.9 10.8 <0.020 6.8 1/20/2016 NA NA NA <0.50 <0.50 0.27 J <0.50 14.8 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 43.4 7/20/2016 NA NA NA 1.9 3.7 <0.50 <0.50 4.4 <1.0 <0.50 <0.50 <0.50 <0.50 0.78 5.8 <0.50 0.42 J <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 8.1 14.1 9.0 28.2 59.4 NA 20.5 3/13/2009 605 540 <100 29.3 10.7 1.8 <0.1 16.2 <1.0 <0.1 <0.1 *<0.02 2.8 1.7 72.1 1.1 3.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 151 80.8 11.6 116.1 360 <0.02 22.7 11/17/2009 2,600 460 660 110 38 <0.1 <0.1 16 <0.1 <0.1 <0.1 *<0.023 <0.1 3.9 340 <0.1 6.3 0.74 <0.1 <0.2 3.2 <0.1 <0.1 3.8 630 170 16 320 1,136 <0.023 22.4 2/3/2012 1,980 1,450 213 79.1 28.3 0.74 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 6.1 5.7 135 <0.50 10.9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 3.7 336 79.3 32.7 233 681 <0.020 31.5 8/22/2012 3,660 1,180 1,180 126 53.2 <2.3 <2.4 14.1 <3.9 <2.0 NA *0.042 15.3 4.4 J 389 <2.0 7.4 J <3.3 <3.6 <2.7 <2.0 <2.0 <2.0 7.2 J 939 89.7 18.3 447 1,494 0.042 29.4 1/24/2014 2,020 445 <250 52.0 18.9 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *<0.020 8.1 1.6 222 <1.0 1.3 <1.0 <1.0 <1.0 NA <1.0 <1.0 5.9 272 20.7 2.5 135.3 430.5 <0.020 <5.0 7/17/2014 2,350 696 <250 19.7 23.1 <1.2 <1.2 <1.2 <2.5 <1.2 <1.2 *<0.020 17.3 2.8 444 <1.2 2.2 <1.2 <1.2 <1.2 NA <1.2 <1.2 14.2 499 19.7 5.1 187.4 711.2 <0.020 11.7 1/14/2015 613 345 94.2 <2.5 16.8 <2.5 <2.5 5.7 <5.0 <2.5 <2.5 *<0.020 10.0 <2.5 274 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 14.1 345 10.9 3.9 68.9 428.7 <0.020 15.8 7/22/2015 NA NA NA 3.3 2.1 <1.2 <1.2 3.4 <2.5 <1.2 <1.2 *<0.020 7.1 1.4 197 <1.2 0.74 J 0.73 J <1.2 <1.2 NA <1.2 <1.2 7.1 143 2.4 1.4 12.8 159.6 <0.020 8.9 1/20/2016 NA NA NA 0.88 0.35 J <0.50 <0.50 2.7 <1.0 <0.50 <0.50 <0.50 0.62 0.58 12.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA 0.26 J <0.50 <2.0 16.1 <0.50 <0.50 2.6 18.7 NA 61.8 7/20/2016 NA NA NA 0.34 J <0.50 <0.50 <0.50 5.1 <1.0 <0.50 <0.50 <0.50 <0.50 0.46 J 4.4 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 6.9 <0.50 <0.50 1.35 J 8.25 J NA 37.1 3/13/2009 <100 <100 <100 <0.50 <0.50 <0.50 <0.1 0.68 <1.0 <0.1 <0.1 *<0.02 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ND <0.02 19.5 11/17/2009 <30 <10 <35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 ND <0.022 165 2/3/2012 <50.0 <50.0 <50.0 <0.50 <0.50 2.5 <0.50 11.9 <1.0 0.71 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 161 8/23/2012 <35 <35 <35 <0.10 <0.10 2.3 0.12 17.1 <0.20 0.27 J NA *<0.0091 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0091 100 1/23/2014 <50.0 <50.0 <50.0 <0.50 <0.50 1.4 <0.50 18.2 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 148 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 2.1 <0.50 22.7 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 174 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 1.5 <0.50 22.6 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 108 7/22/2015 NA NA NA <0.50 <0.50 0.97 <0.50 17.5 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 51.9 3/13/2009 <100 <100 <100 <0.50 <0.50 <0.50 <0.1 <0.50 <1.0 <0.1 <0.1 *<0.02 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.60 <0.50 <0.50 0.6 <0.02 25.9 11/17/2009 <30 <10 <35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 0.5 <0.2 0.41 1.0 <0.022 185 2/3/2012 <50.0 <50.0 <50.0 <0.50 <0.50 1.2 <0.50 6.0 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 61.9 8/22/2012 94.8 J <35 <35 <0.10 <0.10 1.7 <0.12 8.5 <0.20 0.36 J NA *<0.0097 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 47.9 1/23/2014 <50.0 <50.0 <50.0 <0.50 <0.50 0.58 <0.50 11.6 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 31.4 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 17.7 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 17.5 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 0.59 <0.50 14.8 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 13.2 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 7.7 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 26.7 11/17/2009 800 50 130 12 3.7 <0.1 <0.1 7.7 <0.1 <0.1 <0.1 *<0.022 <0.1 0.87 1.7 <0.1 1.4 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 1.1 35 88 9.9 61 193.9 <0.022 <10 2/3/2012 156 155 <50.0 4.7 1.0 <0.50 <0.50 1.4 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 4.2 <0.50 3.8 1.3 8.3 13.4 <0.020 35.0 8/22/2012 146 <35 <35 <0.10 <0.10 <0.12 <0.12 0.73 <0.20 <0.10 NA *<0.0095 <0.11 0.18 J <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.36 J <0.13 <0.15 0.63 J 0.99 <0.0095 <5.0 1/24/2014 131 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 32.9 7/18/2014 55.2 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 9.2 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 1.3 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 18.9 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 1.2 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 79.4 1/20/2016 NA NA NA <0.50 0.87 <0.50 <0.50 0.58 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.39 J 6.5 1.9 5.18 J 13.97 J NA 36.8 7/20/2016 NA NA NA 4.7 6.5 <0.50 <0.50 0.68 <1.0 <0.50 <0.50 <0.50 <0.50 1.7 <0.50 <0.50 0.41 J <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 1.2 3.3 4.1 103.0 111.6 NA 13.6 MW-4 MW-5 Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. MW-1 MW-2 MW-3 Page 1 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 11/17/2009 1,200 990 410 23 4 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.023 3 3.7 130 0.79 7.2 0.34 <0.1 <0.2 1.9 0.9 <0.1 1.2 370 180 39 168 757 <0.023 45.2 2/2/2012 790 479 69.3 13.3 4.9 <0.50 <0.50 2.5 <1.0 <0.50 <0.50 *<0.020 <0.50 1.6 5.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 112 36.2 13.8 61.7 223.7 <0.020 92.3 8/22/2012 1,060 331 320 20.8 9.2 <0.59 <0.59 2.0 J <0.98 <0.51 NA *0.062 2.4 J 2.6 4.9 0.69 J 4.9 <0.82 <0.90 <0.69 0.63 J 1.2 J <0.50 2.0 J 226 77.1 24.9 122.1 450.1 0.062 18.1 1/23/2014 282 54.0 <50.0 3.6 1.5 <0.50 <0.50 2.4 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 1.0 <0.50 0.57 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 21.1 5.7 3.0 12.2 42.0 <0.020 41.2 7/17/2014 1/13/2015 7/22/2015 1/19/2016 7/19/2016 11/17/2009 4,200 550 1,000 100 31 <0.1 <0.1 12 <0.1 <0.1 <0.1 *<0.023 12 7.4 290 3.2 9.3 1.4 <0.1 <0.2 2.6 <0.1 0.58 5.4 920 890 78 520 2,408 <0.023 <10 2/2/2012 1,840 1,840 428 88.7 31.0 <0.50 <0.50 15.0 <1.0 <0.50 <0.50 *<0.020 4.0 5.9 95.0 <0.50 8.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 4.1 252 131 15.4 291.6 690 <0.020 52.5 8/22/2012 2,250 784 753 110 32.1 <1.2 <1.2 11.7 <2.0 <1.0 NA *0.058 9.4 5.8 196 2.9 J 10.9 <1.6 <1.8 <1.4 1.3 J 2.0 J <1.0 4.3 J 463 275 43.5 418 1,199.5 0.058 <5.0 1/23/2014 3,790 1,880 <500 195 64.3 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *0.052 11.4 12.6 170 <5.0 26.7 <5.0 <5.0 <5.0 NA <5.0 <5.0 <20.0 811 952 132 814 2,709 0.052 73.2 7/18/2014 3,140 1,800 <500 148 47.3 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *0.085 6.1 9.4 68.1 <5.0 19.9 <5.0 <5.0 <5.0 NA <5.0 <5.0 <20.0 520 1,040 137 720 2,417 0.085 19.2 1/14/2015 2,930 2,610 <2,500 179 54.7 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *<0.020 9.8 10.9 112 <5.0 23.2 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <20.0 650 934 126 734 2,444 <0.020 216 7/22/2015 NA NA NA 101 39.9 <2.5 <2.5 4.6 <5.0 <2.5 <2.5 *0.085 9.8 7.8 134 <2.5 14.2 1.8 J <2.5 <2.5 NA 2.7 <2.5 7.4 J 434 401 59.4 387 1,281 0.085 23.5 1/20/2016 NA NA NA 34.2 14.7 <1.2 <1.2 4.0 <2.5 <1.2 <1.2 <1.2 5.9 3.8 125 <1.2 3.0 0.70 J <1.2 <1.2 NA 1.5 <1.2 7.5 276 17.2 4.3 89.2 386.7 NA 38.7 7/20/2016 NA NA NA 71.4 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 12.2 4.1 132 <1.0 6.5 1.2 <1.0 <1.0 NA <1.0 <1.0 13.5 235 152 38.6 266 691.6 NA 67.3 11/17/2009 31,000 4,100 8,700 580 130 <5 <0.1 <5 <5 <0.1 <0.1 *2.8 <5 25 <10 <5 61 39 27 27 <5 <5 29 130 1,900 17,000 900 4,600 24,400 2.8 <10 2/2/2012 8/22/2012 1/20/2014 7/17/2014 1/13/2015 7/22/2015 NA NA NA 4,130 2,480 <12.5 <12.5 <12.5 <25.0 <12.5 <12.5 *20.0 <12.5 335 77.2 434 1,220 <12.5 <12.5 <12.5 NA <12.5 83.3 2,330 6,810 36,100 4,160 19,240 66,310 20.0 8.9 1/20/2016 NA NA NA 5,330 1,290 <125 <125 <125 <250 <125 <125 <125 <125 189 <125 <125 626 <125 <125 <125 NA <125 <125 1,320 1,800 21,500 3,040 19,530 45,870 NA 54.1 7/20/2016 NA NA NA 5,350 1,500 <62.5 <62.5 <62.5 <125 <62.5 <62.5 <62.5 <62.5 204 208 259 708 <62.5 <62.5 <62.5 NA <62.5 55.8 J 1,280 4,950 24,600 2,610 15,440 47,600 NA 48.7 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.021 23.7 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 1.6 <0.50 1.1 2.7 <0.019 6.4 8/22/2012 784 186 218 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 NA *<0.0094 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.15 <0.10 0.26 J <0.10 <0.22 0.26 <0.0094 <5.0 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 31.5 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 50.0 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 56.7 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 15.4 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 0.12 1.4 <0.1 0.29 1.8 <0.021 <10 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 0.83 <0.50 <1.5 0.83 <0.020 4.9 J 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 20.2 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 21.3 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 17.3 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 9.0 MW-9 MW-6 MW-7 MW-8 Not Sampled Due to Mud in Well Not Sampled Due to Mud in Well Not Sampled Due to Presence of Free Product MW-10 Not Sampled Due to Mud/Sediment in Well Not Sampled Due to Presence of Free Product Not Sampled Due To Presence Of Free Product Not Sampled Due To Presence Of Free Product Not Sampled Due To Presence Of Free Product Not Sampled Due to Mud/Sediment in Well Not Sampled Due to Mud/Sediment in Well Page 2 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 7/28/2010 75,000 5,700 24,000 1,800 520 <50 <0.1 <50 <50 <0.1 <0.1 *3.1 190 110 5,600 <50 270 <100 <50 <100 <50 <50 84 700 15,000 37,000 2,800 14,100 68,900 3.1 19.3 2/2/2012 56,300 68,400 <10,000 2,090 492 <0.50 <0.50 <0.50 <1.0 0.73 <0.50 *4.1 151 116 2,590 <0.50 273 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 565 9,890 27,100 2,980 15,290 55,260 4.1 18.1 8/23/2012 17,700 8,370 4,730 2,150 528 <120 <120 <160 <200 <100 NA *2.4 131 J <100 3,210 <100 309 J <160 <180 <140 <100 <100 <100 616 8,720 31,700 3,140 17,310 60,870 2.4 19.5 1/22/2014 71,500 47,800 5,070 2,130 489 <125 <125 <125 <250 <125 <125 *2.7 <125 <125 1,960 <125 265 <125 <125 <125 NA <125 <125 538 7,860 30,300 2,650 14,460 55,270 2.7 55.7 7/17/2014 54,100 33,200 <5,000 1,540 360 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *0.93 57.6 69.4 1,210 <5.0 187 <5.0 <5.0 <5.0 NA <5.0 44.4 510 5,350 19,300 1,900 10,410 36,960 0.93 39.7 1/13/2015 54,700 59,600 <10,000 2,860 644 <100 <100 <100 <200 <100 <100 *2.5 <100 124 1,400 <100 361 <100 <100 <100 <100 <100 <100 739 6,650 28,100 3,200 17,760 55,710 2.5 48.5 7/21/2015 NA NA NA 2,270 568 <125 <125 <125 <250 <125 <125 *2.4 83.9 J 103 J 1,870 <125 307 <125 <125 <125 NA <125 67.8 J 728 5,630 26,000 2,960 15,150 49,740 2.4 14.9 1/20/2016 NA NA NA 2,530 594 <125 <125 <125 <250 <125 <125 <125 94.8 J 105 J 2,510 <125 322 <125 <125 <125 NA <125 <125 642 5,450 23,900 2,920 16,260 48,530 NA 54.8 7/19/2016 NA NA NA 851 201 <20.0 <20.0 <20.0 <40.0 <20.0 <20.0 <20.0 <20.0 34.1 138 <20.0 105 <20.0 <20.0 <20.0 NA <20.0 13.4 J 229 693 4,110 686 3,870 9,359 NA 23.2 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 2.7 2.7 <0.021 15.2 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <4.0 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0094 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0094 11.8 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 11.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.96 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 58.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.10 0.58 <0.50 46.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 0.10 437 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.23 3.5 <0.50 207 <0.50 <0.50 1.1 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 0.23 45.7 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 3.2 <0.50 188 <0.50 <0.50 0.68 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 29.3 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 6.4 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 50.5 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 4.5 J 8/24/2012 163 50.8 J <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 <5.0 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 5.9 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 12.8 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 5.5 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 4.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 11.4 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0092 <0.11 <0.10 1.7 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0092 14.5 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 21.1 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 12.4 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 117 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 2.9 <0.50 33.5 <0.50 <0.50 0.68 <0.50 <0.50 NA <0.50 <0.50 <2.0 1.1 <0.50 <0.50 <1.5 ND <0.020 7.7 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 4.1 <0.50 122 <0.50 <0.50 1.0 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 40.7 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 1.6 <0.50 14.2 <0.50 <0.50 0.29 J <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 92.6 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 <5.0 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 10.6 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 41.7 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 152 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 98.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 233 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 30.7 MW-13 MW-12 MW-14 MW-15 MW-16 MW-11 Page 3 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 8.0 8/24/2012 78.4 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 16.3 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 95.6 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 91.4 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 139 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.33 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 21.7 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 0.60 <0.50 <1.5 0.60 <0.020 28.2 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 0.39 J <0.10 1.2 <0.10 <0.11 <0.16 <0.18 <0.14 0.72 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 42.6 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 2.1 <0.50 1.7 <0.50 <0.50 0.81 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 79.3 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 1.7 <0.50 <0.50 0.63 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 50.9 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.023 2.0 <0.50 1.0 <0.50 <0.50 1.2 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND 0.023 109 7/21/2015 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 0.33 J <1.0 <0.50 <0.50 <0.50 2.2 <0.50 2.8 <0.50 <0.50 1.3 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 14.4 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.62 <0.50 <0.50 0.60 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 54.9 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <20.0 8/23/2012 <35 <35 41.6 J <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 0.30 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 25.3 1/20/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.019 139 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 54.5 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 112 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <100 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 15.6 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 0.21 J <0.20 <0.10 NA *<0.0097 0.14 J <0.10 0.38 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 8.2 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 41.7 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 26.8 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 64.3 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.021 24.4 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <4.0 8/24/2012 60.8 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 2.5 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 <5.0 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/16/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 3.4 J 4/3/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *0.024 1.7 <0.10 47.4 <0.10 <0.11 0.64 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND 0.024 29.9 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0097 0.80 <0.10 24.0 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 7.5 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 8.9 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 *<0.020 <0.50 <0.50 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 66.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 2.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 109 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.49 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 7.2 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.32 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 21.4 J 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.41 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 56.3 2/2/2012 309 406 <50.0 25.0 <0.50 0.67 <0.50 1.1 <1.0 0.74 <0.50 *0.42 16.5 2.6 84.6 <0.50 3.1 3.6 <0.50 <0.50 <0.50 <0.50 <0.50 10.8 260 71.1 21.8 215 567.9 0.42 <4.0 8/23/2012 2,300 865 477 76.3 <2.0 <2.3 <2.4 <3.2 <3.9 <2.0 NA *1.1 51.9 7.3 J 251 <2.0 11.6 12.3 <3.6 <2.7 <2.0 <2.0 <2.0 31.3 967 266 82.1 638 1,953.1 1.1 <5.0 1/22/2014 3,060 2,060 <1,000 110 <5.0 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *1.5 61.0 8.9 247 <5.0 12.2 16.5 <5.0 <5.0 NA <5.0 <5.0 42.3 1,470 65.2 85.8 796 2,417.0 1.5 <5.0 7/17/2014 4,160 2,360 <1,250 112 9.8 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *1.5 74.9 11.5 292 1.8 15.1 21.3 <0.50 <0.50 NA <0.50 <0.50 53.1 1,360 78.5 118 785 2,341.5 1.5 <5.0 1/13/2015 5,250 5,210 <5,000 104 8.6 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 *1.4 57.8 9.4 282 <5.0 12.4 16.3 <5.0 <5.0 <5.0 <5.0 <5.0 47.4 1,360 23.4 88.5 783 2,254.9 1.4 <5.0 7/21/2015 NA NA NA 71.1 6.6 <5.0 <5.0 <5.0 14.1 <5.0 <5.0 *1.6 54.3 9.8 311 <5.0 12.0 17.8 <5.0 <5.0 NA <5.0 <5.0 47.2 1,550 17.6 78.0 691 2,336.6 1.6 2.5 J 1/19/2016 NA NA NA 1.4 1.0 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 11.8 0.86 61.6 <0.50 <0.50 3.2 <0.50 <0.50 NA <0.50 <0.50 4.8 144 0.44 J 0.80 17.0 162.24 J NA 9.1 7/19/2016 NA NA NA 1.7 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 0.25 J 23.6 0.63 150 <0.50 0.56 6.1 <0.50 <0.50 NA <0.50 <0.50 6.0 155 <0.50 4.2 12.1 171.3 NA 15.4 MW-22 IMW-1 MW-21 MW-18 MW-17 MW-20 Not Sampled - Aboveground Pool Obstructing Well MW-19 Page 4 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 4/3/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *0.0096 J 0.91 <0.10 1.2 <0.10 <0.11 <0.12 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND 0.0096 J <5.0 8/23/2012 61.0 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 0.42 J <0.10 0.60 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 <5.0 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 0.65 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.55 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.51 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 11/17/2009 1,300 180 230 41 <0.1 <0.1 <0.1 7.9 <0.1 <0.1 <0.1 *<0.022 2.3 2.6 450 1.2 3.2 <0.2 <0.1 <0.2 2.1 <0.1 <0.1 3.4 140 0.41 3 21.8 165.6 <0.022 <10 2/3/2012 1,510 502 90 31.1 <0.50 <0.50 <0.50 15.7 <1.0 <0.50 <0.50 *0.023 2.7 2.8 490 1.6 2.1 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 3.7 134 0.61 1.0 54.2 189.8 0.023 11.7 8/22/2012 757 160 181 11.9 <1.0 <1.2 <1.2 7.9 <2.0 <1.0 NA *0.026 2.1 J 1.1 J 349 <1.0 <1.1 <1.6 <1.8 <1.4 <1.0 <1.0 <1.0 1.5 J 57.9 11.8 <1.5 28.3 98.0 0.026 <5.0 1/23/2014 251 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 4.1 <1.0 <0.50 <0.50 *<0.020 1.2 <0.50 325 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 8.8 7/17/2014 273 <50.0 <50.0 <0.50 <0.50 1.1 <0.50 16.4 <1.0 <0.50 <0.50 *<0.020 1.8 <0.50 448 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/14/2015 123 <50.0 <50.0 <1.0 <1.0 <1.0 <1.0 10.3 <2.0 <1.0 <1.0 *<0.020 1.4 <1.0 174 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <4.0 <1.0 <1.0 <1.0 <3.0 ND <0.020 9.7 7/22/2015 NA NA NA <0.50 <0.50 0.88 <0.50 12.9 <1.0 <0.50 <0.50 *<0.020 1.4 <0.50 118 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 8.0 1/20/2016 NA NA NA <0.50 <0.50 0.67 <0.50 10.9 <1.0 <0.50 <0.50 <0.50 1.3 <0.50 101 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 8.7 7/20/2016 NA NA NA <0.50 <0.50 0.83 <0.50 11.3 <1.0 <0.50 <0.50 <0.50 0.84 <0.50 44.5 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.60 <0.50 <0.50 <1.5 0.60 NA 12.9 7/28/2010 <30 <35 <5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 1.4 2 <0.1 3.1 6.5 <0.021 <10 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 1.3 6.9 0.77 3.7 12.7 <0.020 <4.0 8/22/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 0.28 J <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 <5.0 1/22/2014 399 <50.0 <50.0 0.62 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 5.5 <0.50 <0.50 3.84 3.84 <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 10.0 1/14/2015 85.8 74.8 <50.0 3.5 0.69 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *0.028 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 39.1 9.7 1.9 25.6 76.3 0.028 5.8 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 7/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 4.4 J 2/3/2012 <50.0 69.9 <50.0 0.69 <0.50 <0.50 <0.50 0.66 <1.0 <0.50 <0.50 *<0.021 <0.50 <0.50 25.8 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 1.7 1.5 <0.50 2.4 5.6 <0.021 4.2 J 8/22/2012 58.4 J <35 <35 0.17 J <0.10 <0.12 <0.12 <0.16 1.4 <0.10 NA *<0.0095 0.22 J <0.10 33.2 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.52 0.46 J <0.15 0.26 J 1.24 <0.0095 <5.0 1/23/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 27.1 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.30 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 0.55 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 25.1 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 1.0 1.0 <0.020 <5.0 1/14/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 0.41 J <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.56 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 7/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 4.6 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 2/2/2012 <50.0 116 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <4.0 8/23/2012 47.4 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 1.4 <0.10 NA *<0.0094 <0.11 <0.10 0.18 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 0.16 J 0.23 J 0.22 J <0.15 <0.30 0.45 <0.0094 <5.0 1/21/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 2.4 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 1.5 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.64 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 6.3 5.0 <0.50 7.2 18.50 <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.39 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.78 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 0.57 <0.50 <0.50 0.28 J 0.85 J NA <5.0 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.40 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 12.4 DMW-3 DMW-4 IMW-2 DMW-1 DMW-2 Page 5 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. 4/3/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 0.18 J <0.10 3.1 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.58 <0.13 <0.15 <0.30 0.58 <0.0095 <5.0 8/23/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 0.52 <0.10 NA *<0.0095 0.26 J <0.10 5.2 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 0.79 <0.13 <0.15 <0.30 0.79 <0.0095 <5.0 1/22/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/17/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.55 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 1/13/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 <5.0 7/21/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 3.4 J 1/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.28 J <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA <5.0 7/19/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 0.30 J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA 13.7 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 *<0.023 <0.1 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 0.84 0.12 <0.1 <0.1 2.7 2.8 <0.023 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 <0.1 0.97 <0.1 <0.1 *<0.021 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.021 NA 8/29/2012 39.6 J <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND NA NA 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 0.31 <0.2 <0.1 <0.1 *<0.021 <0.1 <0.2 6 <0.1 <0.1 0.12 <0.1 <0.2 <10 <0.1 <0.1 0.34 0.12 <0.1 <0.1 <0.1 0.12 <0.021 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.22 1.5 <0.1 <0.1 *<0.02 <0.5 <0.2 2.5 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.02 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 1.6 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 3.7 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/24/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.4 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/16/2014 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.4 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 3.0 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/20/2016 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 1/15/2015 7/22/2015 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.4 0.33 <0.1 <0.1 *<0.022 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 0.44 J <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/24/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/16/2014 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 0.34 J <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA PW-7 5/5/2011 <30 <40 <10 <0.1 <0.1 4.2 3.5 3.2 0.19 7.2 0.1 *<0.021 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.021 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 <0.1 0.93 <0.1 <0.1 *<0.022 <0.5 <0.2 0.64 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 8/24/2012 42.9 J <35 <35 <0.10 <0.10 <0.12 <0.12 0.20 J <0.20 <0.10 NA *<0.0096 0.30 J <0.10 0.40 J <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/24/2014 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/20/2016 PW-10 1/15/2015 PW-11 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0093 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0093 NA 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 0.54 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 NA 1/15/2015 7/22/2015 1/15/2015 7/22/2015 DMW-5 PW-12 PW-6 PW-1 Not Sampled - No One Home, No Access PW-4 PW-5 Not Sampled - No One Home, No Access Not Sampled - Well House Partialy Collapsed and Multiple Hazards to Access Sample Port Not Sampled - No One Home and Outside Water Turned Off Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled; Outside Spigots Winterized and No One Home Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access Not Sampled - No One Home, No Access PW-2 Not Sampled - No One Home, No Access PW-9 Not Sampled - No One Home, No AccessPW-13 Page 6 of 7 Historical Groundwater Sampling Results Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 C5-C8 Aliphatics Carbon Fraction Class C9-C18 Aliphatics Carbon Fraction Class C9-C22 Aromatics Carbon Fraction Class C 5 - C 8 C9 - C 1 2 C 9 - C 1 0 1 , 2 , 4 - T r i m e t h y l b e n z e n e 1 , 3 , 5 - T r i m e t h y l b e n z e n e B r o m o d i c h l o r o m e t h a n e B r o m o f o r m C h l o r o f o r m C h l o r o m e t h a n e D i b r o m o c h l o r o m e t h a n e D i b r o m o m e t h a n e E t h y l e n e D i b r o m i d e ( E D B ) I s o p r o p y l E t h e r I s o p r o p y l b e n z e n e M e t h y l t e r t b u t y l e t h e r ( M T B E ) n - B u t y l b e n z e n e n - P r o p y l b e n z e n e 1 , 2 , - D i c h l o r o e t h a n e T r i c h l o r o e t h y l e n e ( T C E ) T e t r a c h l o r o e t h y l e n e ( P C E ) p - I s o p r o p y l t o l u e n e s e c - B u t y l b e n z e n e S t y r e n e N a p h t h a l e n e B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s T o t a l B T E X E t h y l e n e D i b r o m i d e ( E D B ) L e a d Table 5 EPA METHOD 6010 DATE SAMPLED EPA METHOD 504.1 EPA METHOD 6200B (Target analytes reported above method detection limits) MADEP VPH SAMPLE I.D. PW-14 1/15/2015 11/17/2009 <30 <10 <35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 ND <0.022 NA 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 1.3 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 1.2 <0.1 <0.1 <0.2 <0.1 ND <0.022 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 1.2 0.78 <0.1 <0.1 *<0.022 <0.5 <0.2 0.25 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 7/22/2015 11/17/2009 440 80 220 9.6 2.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *NA <0.1 0.5 <0.1 <0.1 1.1 <0.1 <0.1 <0.2 <0.1 <0.1 0.46 2.7 12 170 16 81 ND NA NA 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.021 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 1.4 4.3 <0.2 3.9 ND <0.021 NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.21 0.3 <0.1 <0.1 *<0.022 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.022 NA 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0094 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0094 NA 1/20/2016 7/26/2010 NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 *<0.022 <0.1 <0.1 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 ND <0.022 NA 8/29/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0096 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0096 NA 1/20/2016 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.50 ND NA NA 5/5/2011 <30 <40 <10 <0.1 <0.1 <0.1 <0.1 0.10 1.7 <0.1 <0.1 *<0.023 <0.5 <0.2 <0.2 <0.1 <0.1 <0.2 <0.1 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 ND <0.023 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0097 <0.11 <0.10 <0.13 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0097 NA 1/27/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 2/2/2012 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 0.90 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 8/24/2012 <35 <35 <35 <0.10 <0.10 <0.12 <0.12 <0.16 <0.20 <0.10 NA *<0.0095 <0.11 <0.10 0.85 <0.10 <0.11 <0.16 <0.18 <0.14 <0.10 <0.10 <0.10 <0.10 <0.13 <0.13 <0.15 <0.30 ND <0.0095 NA 1/24/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/18/2014 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/15/2015 <50.0 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 7/22/2015 NA NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 *<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <1.5 ND <0.020 NA 1/20/2016 400 700 200 400 400 0.6 4 70 3 0.4 NE 0.02 70 70 20 70 70 0.4 3 0.7 25 70 70 6 1 600 600 500 N/A 0.02 15 NE NE NE 28,500 25,000 NE 4000 70,000 3,000 400 NE 50 70,000 25,000 20,000 6,900 30,000 400 3,000 700 11,700 8,500 70,000 6,000 5,000 260,000 84,500 85,500 N/A 50 15,000 1. All measurements are in micrograms per liter (ug/L).9. Analytical table indicates target analyte concentrations reported above method detection limits. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. (Amended Effective April 16, 2012) 10. NA = Not Analyzed for specified parameter 3. "<" or ND = Not detected above method detection limit or laboratory reporting limit. 11. N/A = Not Applicable 4. GCL = Gross Contaminant Level established by NCDEQ. 12. J = Estimated value below the laboratory reporting limit but above the method detection limit. 5. Target analyte concentrations detected above 2L Groundwater Standards are bolded. 6. Target analyte concentrations detected above GCLs are bolded and italicized. 7. NE = Not Established. 14. * = Value reported under EPA Method 504.1. PW-18 GCLs NC 2L GW Standards 8. VPH = Volatile Petroleum Hydrocarbons: C5-C8 and C9-C18 aliphatic chains, and C9-C22 aromatic chain Not Sampled - Well Not Operational During Winter PW-21 13. Methylene chloride, a known laboratory contaminant, was reported at 0.2 ug/L for water collected from PW-16 on July 26, 2010; and at 0.51 ug/L for water collected from PW-7 on May 5, 2011. Not Sampled - No One Home, No Access PW-16 Not Sampled - No One Home, No Access PW-22 PW-15 Not Sampled - Owner Refused Access Not Sampled - Owner Refused Access Page 7 of 7 Table 6 Monitored Natural Attenuation Parameters Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number 28649 Sample I.D.Date Sampled Dissolved Oxygen Nitrate Manganese Ferrous Iron Sulfate Methane 8/23/2012 3.22 0.17 0.832 <0.10 <2.0 0.00501 1/22/2014 5.87 0.038 2.12 <0.50 <2.0 0.0091 7/17/2014 6.08 0.040 1.88 <0.50 <2.0 0.0088 1/13/2015 2.93 0.080 1.99 0.87 <2.0 0.0077 7/21/2015 2.05 0.066 2.89 1.2 1.6 J 0.0090 J 1/19/2016 1.49 0.34 0.964 <0.50 1.4 J 0.0027 J 7/19/2016 5.01 NA NA NA NA NA 8/23/2012 3.56 <0.10 0.0994 0.34 2.0 0.00427 1/22/2014 7.22 0.023 0.0086 <0.50 3.6 <0.0066 7/17/2014 4.05 <0.020 0.0091 <0.50 3.9 <0.0066 1/13/2015 3.05 0.069 <0.0050 <0.50 5.8 <0.0066 7/22/2015 5.48 0.017 J 0.0486 <0.50 3.8 0.0021 J 1/19/2016 3.39 0.053 0.0206 <0.50 7.4 0.0019 J 7/19/2016 6.10 NA NA NA NA NA 8/22/2012 3.09 0.80 0.214 0.33 6.3 0.00517 1/23/2014 10.11 1.2 0.188 <0.50 5.9 <0.0066 7/17/2014 12.17 1.2 0.253 <0.50 <2.0 <0.0066 1/14/2015 5.49 1.3 0.405 1.0 <2.0 <0.0066 7/22/2015 5.70 1.1 0.444 <0.50 1.5 J <0.0100 1/20/2016 2.26 1.1 0.290 <0.50 1.5 J 0.0015 J 7/20/2016 5.40 NA NA NA NA NA 8/22/2012 1.31 <0.10 0.510 0.48 <2.0 0.0237 1/22/2014 1.09 0.061 0.399 <0.50 <2.0 0.512 7/17/2014 11.37 0.057 0.586 <0.50 14.4 0.288 1/14/2015 1.99 0.23 0.509 0.80 9.2 1.58 7/22/2015 1.31 0.58 0.371 <0.50 7.5 0.0020 J 1/20/2016 1.35 <0.020 0.363 <0.50 1.8 J 4.49 7/20/2016 4.52 NA NA NA NA NA 8/22/2012 2.30 <1.0 <0.015 <0.10 <20 0.00180 1/23/2014 4.98 <0.020 <0.0050 <0.50 5.1 <0.0066 7/17/2014 3.32 <0.020 <0.0050 <0.50 12.6 0.01470 1/14/2015 5.06 0.48 0.0203 <0.50 6.2 <0.0066 7/22/2015 2.02 <0.020 0.0199 <0.50 11.3 0.0020 J 1/20/2016 1.91 0.21 0.0165 <0.50 5.8 0.0019 J 7/20/2016 4.69 NA NA NA NA NA 8/23/2012 1.67 <2.5 0.0171 <0.10 <50 0.0047 1/21/2014 4.52 <0.020 0.0150 <0.50 10 0.0206 7/17/2014 7.24 <0.020 0.0071 <0.50 9.9 0.0652 1/13/2015 2.45 <0.020 <0.0050 <0.50 10.4 0.0330 7/21/2015 1.91 <0.020 0.0156 0.70 9.5 <0.0100 1/19/2016 1.41 <0.020 0.0205 <0.50 15.2 0.0352 7/19/2016 4.31 NA NA NA NA NA 8/23/2012 1.65 0.11 0.0532 0.52 7.6 0.00126 1/22/2014 4.77 <0.020 0.0206 0.83 8.0 <0.0066 7/17/2014 3.59 0.022 0.0161 <0.50 6.6 <0.0066 1/13/2015 3.16 0.095 0.0059 <0.50 5.9 <0.0066 7/21/2015 2.63 0.050 0.0478 <0.50 5.4 0.0015 J 1/19/2016 1.63 0.089 0.0176 <0.50 6.0 0.0017 J 7/19/2016 7.82 NA NA NA NA NA 1. All concentrations are in milligrams per liter (mg/L). 2. "<" = Not detected above laboratory reporting limit. 3. Dissolved oxygen readings collected in the field with water quality equipment. 4. Values in bold indicate levels greater than the laboratory reporting limit. 5. NA = Not Analyzed. DMW-4 DMW-5 IMW-1 IMW-2 DMW-1 DMW-2 DMW-3 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 3/13/2008 36.00 -- 64.00 7/28/2010 32.50 -- 67.50 2/2/2012 35.97 -- 64.03 8/22/2012 35.92 -- 64.08 1/20/2014 32.42 -- 67.58 7/16/2014 32.68 -- 67.32 1/13/2015 34.14 -- 65.86 7/22/2015 34.27 --65.73 1/20/2016 33.23 --66.77 7/20/2016 32.90 --67.10 3/13/2009 35.66 -- 63.90 7/28/2010 NM -- N/A 2/2/2012 35.70 -- 63.86 8/22/2012 35.55 -- 64.01 1/20/2014 32.31 -- 67.25 7/16/2014 32.15 -- 67.41 1/13/2015 34.05 -- 65.51 7/22/2015 33.98 --65.58 1/20/2016 33.04 --66.52 7/20/2016 32.66 --66.90 3/13/2009 26.92 -- 63.27 7/28/2010 NM -- N/A 2/2/2012 26.70 -- 63.49 8/22/2012 26.75 -- 63.44 1/20/2014 23.13 -- 67.06 7/16/2014 23.31 -- 66.88 1/13/2015 24.81 -- 65.38 7/22/2015 25.35 --64.84 3/13/2009 27.85 -- 64.32 7/28/2010 24.65 -- 67.52 2/2/2012 27.75 -- 64.42 8/22/2012 27.83 -- 64.34 1/20/2014 24.09 -- 68.08 7/16/2014 24.54 -- 67.63 1/13/2015 25.95 -- 66.22 7/22/2015 26.44 --65.73 11/16/2009 36.05 -- 64.13 7/28/2010 32.58 -- 67.60 2/2/2012 35.97 -- 64.21 8/22/2012 35.93 -- 64.25 1/20/2014 32.38 -- 67.80 7/16/2014 32.53 -- 67.65 1/13/2015 34.28 -- 65.90 7/22/2015 34.24 --65.94 1/20/2016 33.11 --67.07 7/20/2016 32.84 --67.34 11/16/2009 35.85 -- 63.86 7/28/2010 32.30 -- 67.41 2/2/2012 35.82 -- 63.89 8/22/2012 35.73 -- 63.98 1/20/2014 32.50 -- 67.21 7/16/2014 Mud -- Mud 1/13/2015 Mud -- Mud 7/22/2015 Mud -- Mud 1/20/2016 Mud -- Mud 7/20/2016 Mud -- Mud 11/16/2009 34.86 -- 63.64 7/28/2010 31.20 -- 67.30 2/2/2012 34.88 -- 63.62 8/22/2012 34.71 -- 63.79 1/20/2014 31.66 -- 66.84 7/16/2014 30.87 -- 67.63 1/13/2015 33.66 -- 64.84 7/22/2015 33.21 --65.29 1/20/2016 32.34 --66.16 7/20/2016 31.92 --66.58 100.18 MW-6 11/4/2009 2 0.010 45 25-45 99.71 MW-7 11/5/2009 2 0.010 44 29-44 98.50 MW-1 12/4/2008 2 0.010 48 33-48 100.00 MW-2 3/10/2009 2 0.010 46 31-46 99.56 0.010 35 20-35 MW-5 11/5/2009 2 0.010 45 30-45 90.19 MW-4 3/10/2009 2 0.010 40 25-40 92.17 MW-3 3/10/2009 2 Page 1 of 4 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 11/16/2009 34.60 -- 63.86 7/28/2010 30.10 -- 68.36 2/2/2012 36.94 2.97 64.07 8/22/2012 34.92 0.53 63.99 1/20/2014 31.51 0.44 67.33 7/16/2014 31.30 0.12 67.26 1/13/2015 33.18 0.12 65.38 7/22/2015 32.85 --65.61 1/20/2016 31.92 --66.54 7/20/2016 31.55 --66.91 7/28/2010 24.17 -- 66.65 2/2/2012 26.65 -- 64.17 8/22/2012 26.73 -- 64.09 1/20/2014 23.04 -- 67.78 7/16/2014 23.99 -- 66.83 1/13/2015 25.05 -- 65.77 7/22/2015 25.98 --64.84 7/28/2010 32.16 -- 66.18 2/2/2012 36.35 -- 61.99 8/22/2012 34.86 -- 63.48 1/20/2014 32.03 -- 66.31 7/16/2014 31.99 -- 66.35 1/13/2015 33.66 -- 64.68 7/22/2015 33.79 --64.55 7/28/2010 31.27 -- 66.49 2/2/2012 35.41 -- 62.35 8/22/2012 34.13 -- 63.63 1/20/2014 31.27 -- 66.49 7/16/2014 30.99 -- 66.77 1/13/2015 33.03 -- 64.73 7/21/2015 32.64 --65.12 1/20/2016 32.16 --65.60 7/19/2016 31.36 --66.40 7/28/2010 31.59 -- 66.17 2/2/2012 35.50 -- 62.26 8/22/2012 34.29 -- 63.47 1/20/2014 31.59 -- 66.17 7/16/2014 31.61 -- 66.15 1/13/2015 32.18 -- 65.58 7/21/2015 31.17 --66.59 1/19/2016 31.31 --66.45 7/19/2016 31.95 --65.81 2/2/2012 37.08 -- 63.34 8/22/2012 36.83 -- 63.59 1/20/2014 33.24 -- 67.18 7/16/2014 33.69 -- 66.73 1/13/2015 35.62 -- 64.80 7/21/2015 35.48 --64.94 2/2/2012 34.50 -- 60.76 8/22/2012 34.22 -- 61.04 1/20/2014 31.60 -- 63.66 7/16/2014 31.65 -- 63.61 1/13/2015 33.19 -- 62.07 7/21/2015 31.70 --63.56 1/19/2016 31.26 --64.00 7/19/2016 34.94 --60.32 2/2/2012 35.00 -- 58.57 8/22/2012 34.11 -- 59.46 1/20/2014 31.93 -- 61.64 7/16/2014 31.28 -- 62.29 1/13/2015 33.53 -- 60.04 7/21/2015 33.53 --60.04 98.46 0.010 40 25-40 97.33 MW-14 1/26/2012 2 0.010 43 28-43 95.26 97.76 MW-12 7/27/2010 2 90.82 0.010 40 25-40 98.34 MW-9 7/27/2010 2 MW-11 7/27/2010 2 0.010 40 25-40 MW-8 11/5/2009 2 0.010 44 29-44 MW-10 7/27/2010 2 100.422 0.010 45 30-45 MW-15 1/24/2012 2 0.010 43 28-43 93.57 0.010 30 15-30 MW-13 1/23/2012 Page 2 of 4 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 2/2/2012 26.23 -- 60.28 8/22/2012 26.46 -- 60.05 1/20/2014 22.83 -- 63.68 7/16/2014 23.03 -- 63.48 1/13/2015 25.14 -- 61.37 7/21/2015 25.54 --60.97 2/2/2012 24.08 -- 57.87 8/22/2012 24.15 -- 57.80 1/20/2014 21.16 -- 60.79 7/16/2014 21.38 -- 60.57 1/13/2015 23.01 -- 58.94 7/21/2015 23.43 --58.52 2/2/2012 24.99 -- 48.37 8/22/2012 25.67 -- 47.69 1/20/2014 22.24 -- 51.12 7/16/2014 22.94 -- 50.42 1/13/2015 23.77 -- 49.59 7/21/2015 1/19/2016 21.85 --51.51 7/19/2016 23.12 --52.51 2/2/2012 32.48 -- 46.04 8/22/2012 31.98 -- 46.54 1/20/2014 28.70 -- 49.82 7/16/2014 28.77 -- 49.75 1/13/2015 30.65 -- 47.87 7/21/2015 31.40 --47.12 2/2/2012 40.39 -- 45.11 8/22/2012 39.79 -- 45.71 1/20/2014 36.62 -- 48.88 7/16/2014 35.89 -- 49.61 1/13/2015 38.81 -- 46.69 7/21/2015 38.83 --46.67 2/2/2012 38.61 -- 43.88 8/22/2012 37.19 -- 45.30 1/20/2014 35.66 -- 46.83 7/16/2014 35.39 -- 47.10 1/13/2015 37.84 -- 44.65 7/21/2015 36.18 --46.31 4/3/2012 24.97 -- 60.42 8/22/2012 24.99 -- 60.40 1/20/2014 22.45 -- 62.94 7/16/2014 22.65 -- 62.74 1/13/2015 23.82 -- 61.57 7/21/2015 24.18 --61.21 1/19/2016 22.77 --62.62 7/19/2016 22.93 --62.46 2/2/2012 34.58 -- 60.77 8/22/2012 35.95 -- 59.40 1/20/2014 31.81 -- 63.54 7/16/2014 31.68 -- 63.67 1/13/2015 33.05 -- 62.30 7/21/2015 32.84 --62.51 1/19/2016 32.41 --62.94 7/19/2016 32.06 --63.29 4/3/2012 32.81 -- 52.28 8/22/2012 27.14 -- 57.95 1/20/2014 24.41 -- 60.68 7/16/2014 24.25 -- 60.84 1/13/2015 26.05 -- 59.04 7/22/2015 26.48 --58.61 1/19/2016 26.70 --58.39 7/19/2016 24.62 --60.47 IMW-1 1/26/2012 2 0.010 64 59-64 95.35 IMW-2 3/23/2012 & 3/30/2012 2 0.010 80 70-80 85.09 47 32-47 85.50 MW-21 1/24/2012 2 MW-20 1/26/2012 2 0.010 MW-22 3/23/2012 2 0.010 33 18-33 85.39 47.5 32.5-47.5 82.49 Well Obstructed by Aboveground Pool MW-19 1/23/2012 2 20-35 86.51 78.52 MW-16 30 15-30 73.36 1/23/2012 MW-17 1/24/2012 2 0.010 0.010 MW-18 1/23/2012 2 0.010 39 24-39 29 14-29 81.95 2 0.010 35 0.010 Page 3 of 4 Table 7Monitoring Well Construction and Groundwater Elevation Informati Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Well ID Date of Installation Date Liquid Gauged Well Diameter (inches) Screen Slot (inches) Total Depth (feet) Screened Interval (feet) Top of Casing Elevation (feet) Depth to Groundwater (feet) Free Product Thickness (feet) Groundwater Elevation (feet) 11/16/2009 36.24 -- 63.97 7/28/2010 33.10 -- 67.11 2/2/2012 36.20 -- 64.01 8/22/2012 36.18 -- 64.03 1/20/2014 32.52 -- 67.69 7/16/2014 32.94 -- 67.27 1/13/2015 34.49 -- 65.72 7/22/2015 34.63 --65.58 1/20/2016 33.40 --66.81 7/20/2016 33.15 --67.06 7/28/2010 24.73 -- 66.12 2/2/2012 28.58 -- 62.27 8/22/2012 27.34 -- 63.51 1/20/2014 23.87 -- 66.98 7/16/2014 24.46 -- 66.39 1/13/2015 25.34 -- 65.51 7/22/2015 26.54 --64.31 1/20/2016 23.87 --66.98 7/20/2016 24.69 --66.16 2/2/2012 45.90 -- 53.25 8/22/2012 36.05 -- 63.10 1/20/2014 31.25 -- 67.90 7/16/2014 32.45 -- 66.70 1/13/2015 33.98 -- 65.17 7/22/2015 33.91 --65.24 1/20/2016 32.90 --66.25 7/20/2016 32.83 --66.32 2/2/2012 36.41 -- 50.57 8/22/2012 36.30 -- 50.68 1/20/2014 32.53 -- 54.45 7/16/2014 32.23 -- 54.75 1/13/2015 34.36 -- 52.62 7/21/2015 34.73 --52.25 1/19/2016 34.16 --52.82 7/19/2016 32.41 --54.57 4/3/2012 33.08 -- 52.17 8/22/2012 25.88 -- 59.37 1/20/2014 22.47 -- 62.78 7/16/2014 22.81 -- 62.44 1/13/2015 24.25 -- 61.00 7/21/2015 24.73 --60.52 1/19/2016 41.18 --44.07 7/19/2016 23.09 --62.16 Note: * Elevations are based on an assumed TOC datum of 100.00 feet at MW-1. If free product is present in well, groundwater elevation is calculated by [Top of Casing Elevation-Depth to Water]+[free product thickness x 0.8581] DMW-5 3/29/2012- 3/30/2012 2 0.010 130 110-130 85.25 DMW-3 1/26/2012- 1/30/2012 2 0.010 123 118-123 99.15 DMW-4 1/27/2012- 1/31/2012 2 0.010 130 110-130 86.98 DMW-1 11/4/2009- 11/5/2009 2 0.010 75 70-75 100.21 DMW-2 7/26/2010- 7/27/2010 2 0.010 95 90-95 90.85 Page 4 of 4 Table 8 Groundwater Sampling Water Quality Parameter Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number: 28649 Temperature (°C) Conductivity (mS/cm) Dissolved Oxygen (mg/L) H (standard units) Oxidation Reduction Potential (mV) MW-1 12/4/2008 7/20/2016 48 100.00 22.54 0.074 5.38 6.11 77 MW-2 3/10/2009 7/20/2016 46 99.56 23.18 0.121 5.13 5.70 -110 MW-5 11/5/2009 7/20/2016 45 100.18 22.75 0.110 4.66 5.96 138 MW-6 11/4/2009 7/20/2016 45 99.71 MW-7 11/5/2009 7/20/2016 44 98.50 21.22 0.094 7.35 6.78 110 MW-8 11/5/2009 7/20/2016 44 98.46 MW-11 7/27/2010 7/19/2016 40 97.76 22.93 0.169 5.38 7.14 117 MW-12 7/27/2010 7/19/2016 40 97.33 22.74 0.088 6.96 6.33 95 MW-14 1/26/2012 7/19/2016 43 95.26 21.18 0.076 5.37 6.81 -113 MW-18 1/23/2012 7/19/2016 30 73.36 20.89 0.068 6.90 12.09 -137 MW-22 3/23/2012 7/19/2016 33 85.39 21.84 0.089 6.78 7.03 67 IMW-1 1/26/2012 7/19/2016 64 95.35 21.64 0.114 5.01 6.95 89 IMW-2 3/23&30/2012 7/19/2016 80 85.09 22.04 0.171 6.10 8.22 -63 DMW-1 11/4-5/2009 7/20/2016 75 100.21 19.55 0.244 5.40 7.31 -88 DMW-2 7/26-27/2010 7/20/2016 95 90.85 19.27 0.231 4.52 6.05 -41 DMW-3 1/26-30/2012 7/20/2016 123 99.15 18.89 0.058 4.69 8.22 -137 DMW-4 1/27-31/2012 7/19/2016 130 86.98 22.70 0.779 4.31 12.28 -534 DMW-5 3/29-30/2012 7/19/2016 130 85.25 21.77 0.152 7.82 9.27 -54 Note: MW-1 top of casing assumed to be 100.00 feet for well elevation survey Not Measured Due To Mud/Sediment in Well Sheen/Strong Odor (Sample Only) Top of Casing Elevation (feet) Water Quality Parameters Well ID Date of Installation Date Liquid Gauged Total Depth (feet) Groundwater Elevation Difference Elevation at Midpoint of Screen/Water Column Difference (feet) (feet) (feet) (feet) MW-2 66.90 60.23 Upward DMW-1 67.06 -5.44 ↑ MW-2 66.90 60.23 Downward DMW-3 66.32 -54.18 ↓ DMW-1 67.06 -5.44 Downward DMW-3 66.32 -54.18 ↓ MW-14 60.32 56.29 Upward IMW-1 63.29 1.79 ↑ MW-22 62.46 57.43 Downward IMW-2 60.47 -14.53 ↓ MW-22 62.46 57.43 Downward DMW-5 62.16 -57.84 ↓ IMW-2 60.47 -14.53 Upward DMW-5 62.16 -57.84 ↑ Water level data collected on 7/19/2016 and 7/20/2016. N/A = Not Applicable -1.69 43.31 0.0390 Vertical gradients calculated using the midpoint of the screen for IMW and DMW wells and the midpoint of the water column for the MW wells. Table 9 Vertical Hydraulic Gradient Evaluations Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina 0.30 115.27 0.0026 1.99 71.96 0.0277 -2.97 54.50 -0.0545 -0.16 65.67 -0.0024 0.74 48.74 0.0152 0.58 114.41 0.0051 Facility ID Number 0-004593 Incident Number: 28649 Well Pair Vertical Gradient Table 10 Free Product Recovery Information Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number 28649 Date Well ID Free Product Recovery Method Product Thickness Before Recovery (Feet) Product Thickness After Recovery (Feet) Amount of Vaporized Product (Gallons) Amount of Liquid (Water and Product) (Gallons) Amount of Liquid Product (Gallons) Total Amount of Product Recovered (Gallons) 3/28/2012 MW-8 AFVR 2.15 0.01 6.76 226 44 50.76 6/28/2012 MW-8 AFVR 0.48 0.00 6.07 231 0.00 6.07 9/28/2012 MW-8 AFVR 0.26 0.00 8.68 231 0.00 8.68 12/13/2012 MW-8 AFVR 0.69 0.00 12.79 226 0.00 12.79 3/14/2013 MW-8 AFVR 0.31 0.00 5.34 231 0.00 5.34 7/24/2013 MW-8 AFVR 0.94 0.00 2.97 189 0.00 2.97 9/16/2013 MW-8 AFVR 0.61 0.00 5.34 270 0.00 5.34 12/18/2013 MW-8 AFVR 1.12 0.00 6.22 310 0.00 6.22 AFVR = Aggressive Fluid/Vapor Recovery 12/13/2012 3/14/2013 7/24/2013 9/16/2013 12/18/2013 78.30 83.64 86.61 91.95 98.17 12.79 5.34 2.97 5.34 6.22 56.83 9/28/2012 8.68 65.51 Date of Recovery Event Total Volume of Free Product Recovered from Site During Current Recovery Event (Gallons) Cumulative Total Volume Recovered to Date from All Recovery Events (Gallons) 3/28/2012 50.76 50.76 6/28/2012 6.07 Date Cross-Sectional Area of Pipe Conversion Factor3 Days of Operation Cumulative Recovery (ft2) (lb-m3/mg-ft3)(lb/hr) (lb/day) (days) (lbs) 04/04/14* 0.08700 1,116 97.09 413 0.00000006243 0.1502 3.60 9.00 32.44 07/10/14 0.08700 1,116 97.09 6.04 0.00000006243 0.0022 0.05 97.00 37.56 10/27/14 0.08700 714 62.12 281.0 0.00000006243 0.0654 1.57 109.00 208.6 03/04/15 0.08700 719 62.55 313.0 0.00000006243 0.0733 1.760 128.00 433.9 06/18/15* 0.08700 763 66.38 26.30 0.00000006243 0.0065 0.1569 106.00 450.5 10/29/15 0.08700 603 52.46 275.0 0.00000006243 0.05404 1.2970 32.00 492.0 12/15/15 0.08700 647 56.29 476.0 0.00000006243 0.10036 2.4087 47.00 605.2 03/31/16 0.08700 588 51.16 178.8 0.00000006243 0.03426 0.8223 107.00 693.2 06/27/16 0.08700 1,269 110.4 162.7 0.00000006243 0.06728 1.615 66.00 799.8 04/04/14* 0.08700 626 54.46 0.64 0.00000006243 0.0001 0.003 9.00 0.02820 07/10/14 10/27/14 0.08700 575 50.03 0.45 0.00000006243 0.0001 0.002 87.00 0.2043 03/04/15 0.08700 523 45.50 0.00 0.00000006243 0.0000 0.000 128.00 0.2043 06/18/15* 0.08700 731 63.60 0.00 0.00000006243 0.0000 0.000 106.00 0.2043 10/29/15 0.08700 528 45.94 0.00 0.00000006243 0.0000 0.000 55.00 0.2043 12/15/15 0.08700 368 32.02 0.00 0.00000006243 0.0000 0.000 47.00 0.2043 03/31/16 0.08700 645 56.12 0.00 0.00000006243 0.0000 0.000 107.00 0.2043 06/27/16 0.08700 720 62.64 0.00 0.00000006243 0.0000 0.000 71.00 0.2043 Notes: * Effluent velocity inferred; reading not collected 3. Conversion factor to convert units of concentration from m /m3 to lb/ft3 4. Mass removal rate = (air flow rate) x (total BTEX) x (conversion factor) x (60 min/hr or 1,440 min/day) 2. Total BTEX concentrations in effluent air are based on EPA Method 18 laboratory data 1. Air flow rate = (cross-sectional area) x (effluent velocity) On-Site System Off-Site System No Sample Collected; System Down Table 11 SVE System Cumulative Recovery Cajah's Mountain Superette 1990 Connelly Springs Road Lenoir, North Carolina Facility ID Number 0-004593 Incident Number 28649 Effluent Velocity (ft/min) Air Flow Rate1 (ft3/min) Total BTEX2 (mg/m3) Mass Removal Rate4 FIGURES SITE PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E DC S A I D SITE HAMBY/CAJAH'SMT PARK TRIPLETT HAMBY/CAJAH' MT PARK WILLIAMS/BRANDON APARTMENTS PRICE CHURCH SHELL CHURCH PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E PW-21 PW-20 PW-22 PW-8 PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E SITE HAMBY/CAJAH'SMT PARK TRIPLETT HAMBY/CAJAH' MT PARK WILLIAMS/BRANDON APARTMENTS PRICE CHURCH SHELL CHURCH PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E Gr o u n d w a t e r d a t a c o l l e c t e d o n J u l y 1 9 a n d 2 0 , 20 1 6 . NM = N o t M e a s u r e d *M W - 2 2 , D M W , a n d I M W w e l l s n o t u s e d i n co n t o u r i n g . SITE HAMBY/CAJAH'SMT PARK TRIPLETT HAMBY/CAJAH' MT PARK WILLIAMS/BRANDON APARTMENTS PRICE CHURCH SHELL CHURCH PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E Gr o u n d w a t e r d a t a c o l l e c t e d o n J u l y 1 9 a n d 2 0 , 20 1 6 . Ve r t i c a l m a x i m u m i m p a c t c o n t o u r e d . NS = N o t S a m p l e d NC D E Q 2 L S t a n d a r d = 1 u g / L SITE HAMBY/CAJAH'SMT PARK TRIPLETT HAMBY/CAJAH' MT PARK WILLIAMS/BRANDON APARTMENTS PRICE CHURCH SHELL CHURCH PR O J E C T N O . NO T E S : DA T E TI T L E SC A L E RE V . B Y PR E P . B Y CA D F I L E Gr o u n d w a t e r d a t a c o l l e c t e d o n J u l y 1 9 an d 2 0 , 2 0 1 6 . Ve r t i c a l m a x i m u m i m p a c t c o n t o u r e d . NS = N o t S a m p l e d NC D E Q 2 L S t a n d a r d = 2 0 u g / L APPENDIX A STANDARD OPERATING PROCEDURES 23BGroundwater Levels Groundwater level measurements were obtained by using an electronic sounding/interface detection device which registers when a probe makes contact with petroleum product and/or water. Depth to groundwater measurements were obtained by lowering the device into the well until it indicated that the water surface had been encountered, at which point a measurement was taken at the top of the riser pipe or top of casing. Measurements were recorded to the nearest 0.01 foot. 24BGroundwater Sampling Groundwater samples were collected using a new, dedicated plastic bailer or pre-decontaminated submersible pump with associated new tubing. Before obtaining a sample, a minimum of three well volumes of groundwater were evacuated to ensure collection of a sample representative of the in-situ groundwater conditions. A sample was collected using a dedicated bailer, or via outflow for the tubing connected to the submersible pump and transferred to containers supplied by the laboratory, and placed in an ice-filled cooler. Chain-of-custody forms were completed and accompanied the samples to the laboratory. The submersible pump system was decontaminated between wells using alconox, deionized water, and alcohol. 25BChemical Analysis Chemical analyses for groundwater were performed by Pace Analytical Services, Inc. in Huntersville, North Carolina. Extractions and analyses were performed in accordance with standard Environmental Protection Agency (EPA) methodology. The groundwater samples were analyzed for volatile organic compounds by EPA Method 6200B including BTEX (benzene, toluene, ethylbenzene, and total xylenes), methyl-tert butyl ether (MTBE), and isopropyl ether (IPE) and for lead by EPA Method 6010. APPENDIX B LABORATORY ANALYTICAL REPORTS #=CL# July 26, 2016 LIMS USE: FR - CHRISTINE LIMS OBJECT ID: 92305873 92305873 Project: Pace Project No.: RE: Christine Schaefer ATC Group Services LLC 7606 Whitehall Executive Cente Suite 800 Charlotte, NC 28273 CAJAH'S MOUNTAIN SUPERETTE Dear Christine Schaefer: Enclosed are the analytical results for sample(s) received by the laboratory on July 20, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey.carter@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 55 #=CP# CERTIFICATIONS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 55 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Lab ID Sample ID Matrix Date Collected Date Received 92305873001 MW-1 Water 07/20/16 13:10 07/20/16 15:05 92305873002 MW-2 Water 07/20/16 13:40 07/20/16 15:05 92305873003 MW-5 Water 07/20/16 12:35 07/20/16 15:05 92305873004 MW-7 Water 07/20/16 11:40 07/20/16 15:05 92305873005 MW-8 Water 07/20/16 14:15 07/20/16 15:05 92305873006 MW-11 Water 07/19/16 14:40 07/20/16 15:05 92305873007 MW-12 Water 07/19/16 14:15 07/20/16 15:05 92305873008 MW-14 Water 07/19/16 13:00 07/20/16 15:05 92305873009 MW-18 Water 07/19/16 10:20 07/20/16 15:05 92305873010 MW-22 Water 07/19/16 12:15 07/20/16 15:05 92305873011 IMW-1 Water 07/19/16 13:40 07/20/16 15:05 92305873012 IMW-2 Water 07/19/16 11:50 07/20/16 15:05 92305873013 DMW-1 Water 07/20/16 11:05 07/20/16 15:05 92305873014 DMW-2 Water 07/20/16 09:15 07/20/16 15:05 92305873015 DMW-3 Water 07/20/16 10:10 07/20/16 15:05 92305873016 DMW-4 Water 07/19/16 09:45 07/20/16 15:05 92305873017 DMW-5 Water 07/19/16 11:15 07/20/16 15:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 55 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92305873001 MW-1 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873002 MW-2 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873003 MW-5 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873004 MW-7 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873005 MW-8 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873006 MW-11 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873007 MW-12 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873008 MW-14 EPA 6010 1 PASI-ASH1 SM 6200B 63 PASI-CNB 92305873009 MW-18 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873010 MW-22 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873011 IMW-1 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873012 IMW-2 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873013 DMW-1 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873014 DMW-2 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873015 DMW-3 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873016 DMW-4 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB 92305873017 DMW-5 EPA 6010 1 PASI-AJMW SM 6200B 63 PASI-CNB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-1 Lab ID:92305873001 Collected:07/20/16 13:10 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 20.5 ug/L 07/23/16 22:15 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 8.1 ug/L 07/21/16 18:45 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 18:45 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 18:45 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 18:45 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 18:45 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 18:45 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 18:45 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 18:45 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 18:45 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 18:45 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 18:45 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 18:45 75-00-31.0 0.50 1 Chloroform 4.4 ug/L 07/21/16 18:45 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 18:45 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 18:45 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 18:45 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 18:45 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 18:45 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 18:45 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 18:45 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 18:45 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 18:45 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 18:45 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 18:45 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 18:45 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 18:45 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 18:45 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 18:45 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 18:45 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 18:45 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 18:45 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 18:45 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 18:45 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 18:45 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 18:45 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 18:45 108-20-30.50 0.25 1 Ethylbenzene 9.0 ug/L 07/21/16 18:45 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 18:45 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)0.78 ug/L 07/21/16 18:45 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 18:45 75-09-22.0 1.0 1 Methyl-tert-butyl ether 5.8 ug/L 07/21/16 18:45 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 18:45 91-20-32.0 1.0 1 n-Propylbenzene 0.42J ug/L 07/21/16 18:45 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-1 Lab ID:92305873001 Collected:07/20/16 13:10 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 18:45 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 18:45 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 18:45 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 18:45 127-18-40.50 0.25 1 Toluene 14.1 ug/L 07/21/16 18:45 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 18:45 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 18:45 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 18:45 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 18:45 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 18:45 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 18:45 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 18:45 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 1.9 ug/L 07/21/16 18:45 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 3.7 ug/L 07/21/16 18:45 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 18:45 75-01-41.0 0.25 1 m&p-Xylene 17.0 ug/L 07/21/16 18:45 179601-23-11.0 0.50 1 o-Xylene 11.2 ug/L 07/21/16 18:45 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %07/21/16 18:45 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %07/21/16 18:45 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 18:45 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-2 Lab ID:92305873002 Collected:07/20/16 13:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 37.1 ug/L 07/23/16 19:27 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 6.9 ug/L 07/21/16 19:02 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 19:02 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 19:02 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 19:02 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 19:02 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 19:02 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 19:02 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 19:02 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 19:02 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 19:02 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 19:02 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 19:02 75-00-31.0 0.50 1 Chloroform 5.1 ug/L 07/21/16 19:02 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 19:02 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 19:02 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 19:02 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 19:02 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 19:02 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 19:02 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 19:02 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 19:02 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 19:02 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 19:02 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 19:02 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 19:02 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 19:02 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 19:02 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:02 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:02 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 19:02 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 19:02 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 19:02 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 19:02 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:02 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:02 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 19:02 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 19:02 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 19:02 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)0.46J ug/L 07/21/16 19:02 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 19:02 75-09-22.0 1.0 1 Methyl-tert-butyl ether 4.4 ug/L 07/21/16 19:02 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 19:02 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 19:02 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-2 Lab ID:92305873002 Collected:07/20/16 13:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 19:02 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:02 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:02 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 19:02 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 19:02 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 19:02 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 19:02 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 19:02 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 19:02 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 19:02 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 19:02 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 19:02 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 0.34J ug/L 07/21/16 19:02 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 19:02 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 19:02 75-01-41.0 0.25 1 m&p-Xylene 0.58J ug/L 07/21/16 19:02 179601-23-11.0 0.50 1 o-Xylene 0.77 ug/L 07/21/16 19:02 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %07/21/16 19:02 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %07/21/16 19:02 460-00-470-130 1 Toluene-d8 (S)100 %07/21/16 19:02 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-5 Lab ID:92305873003 Collected:07/20/16 12:35 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 13.6 ug/L 07/23/16 19:36 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 1.2 ug/L 07/21/16 19:19 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 19:19 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 19:19 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 19:19 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 19:19 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 19:19 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 19:19 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 19:19 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 19:19 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 19:19 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 19:19 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 19:19 75-00-31.0 0.50 1 Chloroform 0.68 ug/L 07/21/16 19:19 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 19:19 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 19:19 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 19:19 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 19:19 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 19:19 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 19:19 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 19:19 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 19:19 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 19:19 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 19:19 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 19:19 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 19:19 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 19:19 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 19:19 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:19 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:19 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 19:19 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 19:19 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 19:19 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 19:19 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:19 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:19 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 19:19 108-20-30.50 0.25 1 Ethylbenzene 4.1 ug/L 07/21/16 19:19 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 19:19 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)1.7 ug/L 07/21/16 19:19 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 19:19 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 07/21/16 19:19 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 19:19 91-20-32.0 1.0 1 n-Propylbenzene 0.41J ug/L 07/21/16 19:19 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-5 Lab ID:92305873003 Collected:07/20/16 12:35 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 19:19 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:19 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:19 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 19:19 127-18-40.50 0.25 1 Toluene 3.3 ug/L 07/21/16 19:19 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 19:19 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 19:19 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 19:19 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 19:19 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 19:19 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 19:19 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 19:19 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 4.7 ug/L 07/21/16 19:19 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 6.5 ug/L 07/21/16 19:19 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 19:19 75-01-41.0 0.25 1 m&p-Xylene 67.5 ug/L 07/21/16 19:19 179601-23-11.0 0.50 1 o-Xylene 35.5 ug/L 07/21/16 19:19 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)99 %07/21/16 19:19 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %07/21/16 19:19 460-00-470-130 1 Toluene-d8 (S)102 %07/21/16 19:19 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-7 Lab ID:92305873004 Collected:07/20/16 11:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 67.3 ug/L 07/23/16 19:39 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 235 ug/L 07/21/16 23:17 71-43-21.0 0.50 2 Bromobenzene <1.0 ug/L 07/21/16 23:17 108-86-11.0 0.50 2 Bromochloromethane <1.0 ug/L 07/21/16 23:17 74-97-51.0 0.50 2 Bromodichloromethane <1.0 ug/L 07/21/16 23:17 75-27-41.0 0.50 2 Bromoform <1.0 ug/L 07/21/16 23:17 75-25-21.0 0.50 2 Bromomethane <10.0 ug/L 07/21/16 23:17 74-83-910.0 1.0 2 n-Butylbenzene <1.0 ug/L 07/21/16 23:17 104-51-81.0 0.50 2 sec-Butylbenzene <1.0 ug/L 07/21/16 23:17 135-98-81.0 0.50 2 tert-Butylbenzene <1.0 ug/L 07/21/16 23:17 98-06-61.0 0.50 2 Carbon tetrachloride <1.0 ug/L 07/21/16 23:17 56-23-51.0 0.50 2 Chlorobenzene <1.0 ug/L 07/21/16 23:17 108-90-71.0 0.50 2 Chloroethane <2.0 ug/L 07/21/16 23:17 75-00-32.0 1.0 2 Chloroform <1.0 ug/L 07/21/16 23:17 67-66-31.0 0.50 2 Chloromethane <2.0 ug/L 07/21/16 23:17 74-87-32.0 1.0 2 2-Chlorotoluene <1.0 ug/L 07/21/16 23:17 95-49-81.0 0.50 2 4-Chlorotoluene <1.0 ug/L 07/21/16 23:17 106-43-41.0 0.50 2 1,2-Dibromo-3-chloropropane <2.0 ug/L 07/21/16 23:17 96-12-82.0 1.0 2 Dibromochloromethane <1.0 ug/L 07/21/16 23:17 124-48-11.0 0.50 2 1,2-Dibromoethane (EDB)<1.0 ug/L 07/21/16 23:17 106-93-41.0 0.50 2 Dibromomethane <1.0 ug/L 07/21/16 23:17 74-95-31.0 0.50 2 1,2-Dichlorobenzene <1.0 ug/L 07/21/16 23:17 95-50-11.0 0.50 2 1,3-Dichlorobenzene <1.0 ug/L 07/21/16 23:17 541-73-11.0 0.50 2 1,4-Dichlorobenzene <1.0 ug/L 07/21/16 23:17 106-46-71.0 0.50 2 Dichlorodifluoromethane <1.0 ug/L 07/21/16 23:17 75-71-81.0 0.50 2 1,1-Dichloroethane <1.0 ug/L 07/21/16 23:17 75-34-31.0 0.50 2 1,2-Dichloroethane 1.2 ug/L 07/21/16 23:17 107-06-21.0 0.50 2 1,1-Dichloroethene <1.0 ug/L 07/21/16 23:17 75-35-41.0 0.50 2 cis-1,2-Dichloroethene <1.0 ug/L 07/21/16 23:17 156-59-21.0 0.50 2 trans-1,2-Dichloroethene <1.0 ug/L 07/21/16 23:17 156-60-51.0 0.50 2 1,2-Dichloropropane <1.0 ug/L 07/21/16 23:17 78-87-51.0 0.50 2 1,3-Dichloropropane <1.0 ug/L 07/21/16 23:17 142-28-91.0 0.50 2 2,2-Dichloropropane <1.0 ug/L 07/21/16 23:17 594-20-71.0 0.50 2 1,1-Dichloropropene <1.0 ug/L 07/21/16 23:17 563-58-61.0 0.50 2 cis-1,3-Dichloropropene <1.0 ug/L 07/21/16 23:17 10061-01-51.0 0.50 2 trans-1,3-Dichloropropene <1.0 ug/L 07/21/16 23:17 10061-02-61.0 0.50 2 Diisopropyl ether 12.2 ug/L 07/21/16 23:17 108-20-31.0 0.50 2 Ethylbenzene 38.6 ug/L 07/21/16 23:17 100-41-41.0 0.50 2 Hexachloro-1,3-butadiene <4.0 ug/L 07/21/16 23:17 87-68-34.0 2.0 2 Isopropylbenzene (Cumene)4.1 ug/L 07/21/16 23:17 98-82-81.0 0.50 2 Methylene Chloride <4.0 ug/L 07/21/16 23:17 75-09-24.0 2.0 2 Methyl-tert-butyl ether 132 ug/L 07/21/16 23:17 1634-04-41.0 0.50 2 Naphthalene 13.5 ug/L 07/21/16 23:17 91-20-34.0 2.0 2 n-Propylbenzene 6.5 ug/L 07/21/16 23:17 103-65-11.0 0.50 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-7 Lab ID:92305873004 Collected:07/20/16 11:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <1.0 ug/L 07/21/16 23:17 100-42-51.0 0.50 2 1,1,1,2-Tetrachloroethane <1.0 ug/L 07/21/16 23:17 630-20-61.0 0.50 2 1,1,2,2-Tetrachloroethane <1.0 ug/L 07/21/16 23:17 79-34-51.0 0.50 2 Tetrachloroethene <1.0 ug/L 07/21/16 23:17 127-18-41.0 0.50 2 Toluene 152 ug/L 07/21/16 23:17 108-88-31.0 0.50 2 1,2,3-Trichlorobenzene <4.0 ug/L 07/21/16 23:17 87-61-64.0 2.0 2 1,2,4-Trichlorobenzene <4.0 ug/L 07/21/16 23:17 120-82-14.0 2.0 2 1,1,1-Trichloroethane <1.0 ug/L 07/21/16 23:17 71-55-61.0 0.50 2 1,1,2-Trichloroethane <1.0 ug/L 07/21/16 23:17 79-00-51.0 0.50 2 Trichloroethene <1.0 ug/L 07/21/16 23:17 79-01-61.0 0.50 2 Trichlorofluoromethane <2.0 ug/L 07/21/16 23:17 75-69-42.0 1.0 2 1,2,3-Trichloropropane <1.0 ug/L 07/21/16 23:17 96-18-41.0 0.50 2 1,2,4-Trimethylbenzene 71.4 ug/L 07/21/16 23:17 95-63-61.0 0.50 2 1,3,5-Trimethylbenzene <1.0 ug/L 07/21/16 23:17 108-67-81.0 0.50 2 Vinyl chloride <2.0 ug/L 07/21/16 23:17 75-01-42.0 0.50 2 m&p-Xylene 112 ug/L 07/21/16 23:17 179601-23-12.0 1.0 2 o-Xylene 154 ug/L 07/21/16 23:17 95-47-61.0 0.50 2 Surrogates 1,2-Dichloroethane-d4 (S)100 %07/21/16 23:17 17060-07-070-130 2 4-Bromofluorobenzene (S)97 %07/21/16 23:17 460-00-470-130 2 Toluene-d8 (S)100 %07/21/16 23:17 2037-26-570-130 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-8 Lab ID:92305873005 Collected:07/20/16 14:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 48.7 ug/L 07/23/16 19:43 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 4950 ug/L 07/21/16 23:34 71-43-262.5 31.2 125 Bromobenzene <62.5 ug/L 07/21/16 23:34 108-86-162.5 31.2 125 Bromochloromethane <62.5 ug/L 07/21/16 23:34 74-97-562.5 31.2 125 Bromodichloromethane <62.5 ug/L 07/21/16 23:34 75-27-462.5 31.2 125 Bromoform <62.5 ug/L 07/21/16 23:34 75-25-262.5 31.2 125 Bromomethane <625 ug/L 07/21/16 23:34 74-83-962562.5 125 n-Butylbenzene 259 ug/L 07/21/16 23:34 104-51-862.5 31.2 125 sec-Butylbenzene <62.5 ug/L 07/21/16 23:34 135-98-862.5 31.2 125 tert-Butylbenzene <62.5 ug/L 07/21/16 23:34 98-06-662.5 31.2 125 Carbon tetrachloride <62.5 ug/L 07/21/16 23:34 56-23-562.5 31.2 125 Chlorobenzene <62.5 ug/L 07/21/16 23:34 108-90-762.5 31.2 125 Chloroethane <125 ug/L 07/21/16 23:34 75-00-312562.5 125 Chloroform <62.5 ug/L 07/21/16 23:34 67-66-362.5 31.2 125 Chloromethane <125 ug/L 07/21/16 23:34 74-87-312562.5 125 2-Chlorotoluene <62.5 ug/L 07/21/16 23:34 95-49-862.5 31.2 125 4-Chlorotoluene <62.5 ug/L 07/21/16 23:34 106-43-462.5 31.2 125 1,2-Dibromo-3-chloropropane <125 ug/L 07/21/16 23:34 96-12-812562.5 125 Dibromochloromethane <62.5 ug/L 07/21/16 23:34 124-48-162.5 31.2 125 1,2-Dibromoethane (EDB)<62.5 ug/L 07/21/16 23:34 106-93-462.5 31.2 125 Dibromomethane <62.5 ug/L 07/21/16 23:34 74-95-362.5 31.2 125 1,2-Dichlorobenzene <62.5 ug/L 07/21/16 23:34 95-50-162.5 31.2 125 1,3-Dichlorobenzene <62.5 ug/L 07/21/16 23:34 541-73-162.5 31.2 125 1,4-Dichlorobenzene <62.5 ug/L 07/21/16 23:34 106-46-762.5 31.2 125 Dichlorodifluoromethane <62.5 ug/L 07/21/16 23:34 75-71-862.5 31.2 125 1,1-Dichloroethane <62.5 ug/L 07/21/16 23:34 75-34-362.5 31.2 125 1,2-Dichloroethane <62.5 ug/L 07/21/16 23:34 107-06-262.5 31.2 125 1,1-Dichloroethene <62.5 ug/L 07/21/16 23:34 75-35-462.5 31.2 125 cis-1,2-Dichloroethene <62.5 ug/L 07/21/16 23:34 156-59-262.5 31.2 125 trans-1,2-Dichloroethene <62.5 ug/L 07/21/16 23:34 156-60-562.5 31.2 125 1,2-Dichloropropane <62.5 ug/L 07/21/16 23:34 78-87-562.5 31.2 125 1,3-Dichloropropane <62.5 ug/L 07/21/16 23:34 142-28-962.5 31.2 125 2,2-Dichloropropane <62.5 ug/L 07/21/16 23:34 594-20-762.5 31.2 125 1,1-Dichloropropene <62.5 ug/L 07/21/16 23:34 563-58-662.5 31.2 125 cis-1,3-Dichloropropene <62.5 ug/L 07/21/16 23:34 10061-01-562.5 31.2 125 trans-1,3-Dichloropropene <62.5 ug/L 07/21/16 23:34 10061-02-662.5 31.2 125 Diisopropyl ether <62.5 ug/L 07/21/16 23:34 108-20-362.5 31.2 125 Ethylbenzene 2610 ug/L 07/21/16 23:34 100-41-462.5 31.2 125 Hexachloro-1,3-butadiene <250 ug/L 07/21/16 23:34 87-68-3250125125 Isopropylbenzene (Cumene)204 ug/L 07/21/16 23:34 98-82-862.5 31.2 125 Methylene Chloride <250 ug/L 07/21/16 23:34 75-09-2250125125 Methyl-tert-butyl ether 208 ug/L 07/21/16 23:34 1634-04-462.5 31.2 125 Naphthalene 1280 ug/L 07/21/16 23:34 91-20-3250125125 n-Propylbenzene 708 ug/L 07/21/16 23:34 103-65-162.5 31.2 125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-8 Lab ID:92305873005 Collected:07/20/16 14:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene 55.8J ug/L 07/21/16 23:34 100-42-562.5 31.2 125 1,1,1,2-Tetrachloroethane <62.5 ug/L 07/21/16 23:34 630-20-662.5 31.2 125 1,1,2,2-Tetrachloroethane <62.5 ug/L 07/21/16 23:34 79-34-562.5 31.2 125 Tetrachloroethene <62.5 ug/L 07/21/16 23:34 127-18-462.5 31.2 125 Toluene 24600 ug/L 07/21/16 23:34 108-88-362.5 31.2 125 1,2,3-Trichlorobenzene <250 ug/L 07/21/16 23:34 87-61-6250125125 1,2,4-Trichlorobenzene <250 ug/L 07/21/16 23:34 120-82-1250125125 1,1,1-Trichloroethane <62.5 ug/L 07/21/16 23:34 71-55-662.5 31.2 125 1,1,2-Trichloroethane <62.5 ug/L 07/21/16 23:34 79-00-562.5 31.2 125 Trichloroethene <62.5 ug/L 07/21/16 23:34 79-01-662.5 31.2 125 Trichlorofluoromethane <125 ug/L 07/21/16 23:34 75-69-412562.5 125 1,2,3-Trichloropropane <62.5 ug/L 07/21/16 23:34 96-18-462.5 31.2 125 1,2,4-Trimethylbenzene 5350 ug/L 07/21/16 23:34 95-63-662.5 31.2 125 1,3,5-Trimethylbenzene 1500 ug/L 07/21/16 23:34 108-67-862.5 31.2 125 Vinyl chloride <125 ug/L 07/21/16 23:34 75-01-412531.2 125 m&p-Xylene 10400 ug/L 07/21/16 23:34 179601-23-112562.5 125 o-Xylene 5040 ug/L 07/21/16 23:34 95-47-662.5 31.2 125 Surrogates 1,2-Dichloroethane-d4 (S)101 %07/21/16 23:34 17060-07-070-130 125 4-Bromofluorobenzene (S)100 %07/21/16 23:34 460-00-470-130 125 Toluene-d8 (S)100 %07/21/16 23:34 2037-26-570-130 125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-11 Lab ID:92305873006 Collected:07/19/16 14:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 23.2 ug/L 07/23/16 19:46 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 693 ug/L 07/22/16 14:57 71-43-220.0 10.0 40 Bromobenzene <20.0 ug/L 07/22/16 14:57 108-86-120.0 10.0 40 Bromochloromethane <20.0 ug/L 07/22/16 14:57 74-97-520.0 10.0 40 Bromodichloromethane <20.0 ug/L 07/22/16 14:57 75-27-420.0 10.0 40 Bromoform <20.0 ug/L 07/22/16 14:57 75-25-220.0 10.0 40 Bromomethane <200 ug/L 07/22/16 14:57 74-83-920020.0 40 n-Butylbenzene <20.0 ug/L 07/22/16 14:57 104-51-820.0 10.0 40 sec-Butylbenzene <20.0 ug/L 07/22/16 14:57 135-98-820.0 10.0 40 tert-Butylbenzene <20.0 ug/L 07/22/16 14:57 98-06-620.0 10.0 40 Carbon tetrachloride <20.0 ug/L 07/22/16 14:57 56-23-520.0 10.0 40 Chlorobenzene <20.0 ug/L 07/22/16 14:57 108-90-720.0 10.0 40 Chloroethane <40.0 ug/L 07/22/16 14:57 75-00-340.0 20.0 40 Chloroform <20.0 ug/L 07/22/16 14:57 67-66-320.0 10.0 40 Chloromethane <40.0 ug/L 07/22/16 14:57 74-87-340.0 20.0 40 2-Chlorotoluene <20.0 ug/L 07/22/16 14:57 95-49-820.0 10.0 40 4-Chlorotoluene <20.0 ug/L 07/22/16 14:57 106-43-420.0 10.0 40 1,2-Dibromo-3-chloropropane <40.0 ug/L 07/22/16 14:57 96-12-840.0 20.0 40 Dibromochloromethane <20.0 ug/L 07/22/16 14:57 124-48-120.0 10.0 40 1,2-Dibromoethane (EDB)<20.0 ug/L 07/22/16 14:57 106-93-420.0 10.0 40 Dibromomethane <20.0 ug/L 07/22/16 14:57 74-95-320.0 10.0 40 1,2-Dichlorobenzene <20.0 ug/L 07/22/16 14:57 95-50-120.0 10.0 40 1,3-Dichlorobenzene <20.0 ug/L 07/22/16 14:57 541-73-120.0 10.0 40 1,4-Dichlorobenzene <20.0 ug/L 07/22/16 14:57 106-46-720.0 10.0 40 Dichlorodifluoromethane <20.0 ug/L 07/22/16 14:57 75-71-820.0 10.0 40 1,1-Dichloroethane <20.0 ug/L 07/22/16 14:57 75-34-320.0 10.0 40 1,2-Dichloroethane <20.0 ug/L 07/22/16 14:57 107-06-220.0 10.0 40 1,1-Dichloroethene <20.0 ug/L 07/22/16 14:57 75-35-420.0 10.0 40 cis-1,2-Dichloroethene <20.0 ug/L 07/22/16 14:57 156-59-220.0 10.0 40 trans-1,2-Dichloroethene <20.0 ug/L 07/22/16 14:57 156-60-520.0 10.0 40 1,2-Dichloropropane <20.0 ug/L 07/22/16 14:57 78-87-520.0 10.0 40 1,3-Dichloropropane <20.0 ug/L 07/22/16 14:57 142-28-920.0 10.0 40 2,2-Dichloropropane <20.0 ug/L 07/22/16 14:57 594-20-720.0 10.0 40 1,1-Dichloropropene <20.0 ug/L 07/22/16 14:57 563-58-620.0 10.0 40 cis-1,3-Dichloropropene <20.0 ug/L 07/22/16 14:57 10061-01-520.0 10.0 40 trans-1,3-Dichloropropene <20.0 ug/L 07/22/16 14:57 10061-02-620.0 10.0 40 Diisopropyl ether <20.0 ug/L 07/22/16 14:57 108-20-320.0 10.0 40 Ethylbenzene 686 ug/L 07/22/16 14:57 100-41-420.0 10.0 40 Hexachloro-1,3-butadiene <80.0 ug/L 07/22/16 14:57 87-68-380.0 40.0 40 Isopropylbenzene (Cumene)34.1 ug/L 07/22/16 14:57 98-82-820.0 10.0 40 Methylene Chloride <80.0 ug/L 07/22/16 14:57 75-09-280.0 40.0 40 Methyl-tert-butyl ether 138 ug/L 07/22/16 14:57 1634-04-420.0 10.0 40 Naphthalene 229 ug/L 07/22/16 14:57 91-20-380.0 40.0 40 n-Propylbenzene 105 ug/L 07/22/16 14:57 103-65-120.0 10.0 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-11 Lab ID:92305873006 Collected:07/19/16 14:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene 13.4J ug/L 07/22/16 14:57 100-42-520.0 10.0 40 1,1,1,2-Tetrachloroethane <20.0 ug/L 07/22/16 14:57 630-20-620.0 10.0 40 1,1,2,2-Tetrachloroethane <20.0 ug/L 07/22/16 14:57 79-34-520.0 10.0 40 Tetrachloroethene <20.0 ug/L 07/22/16 14:57 127-18-420.0 10.0 40 Toluene 4110 ug/L 07/22/16 14:57 108-88-320.0 10.0 40 1,2,3-Trichlorobenzene <80.0 ug/L 07/22/16 14:57 87-61-680.0 40.0 40 1,2,4-Trichlorobenzene <80.0 ug/L 07/22/16 14:57 120-82-180.0 40.0 40 1,1,1-Trichloroethane <20.0 ug/L 07/22/16 14:57 71-55-620.0 10.0 40 1,1,2-Trichloroethane <20.0 ug/L 07/22/16 14:57 79-00-520.0 10.0 40 Trichloroethene <20.0 ug/L 07/22/16 14:57 79-01-620.0 10.0 40 Trichlorofluoromethane <40.0 ug/L 07/22/16 14:57 75-69-440.0 20.0 40 1,2,3-Trichloropropane <20.0 ug/L 07/22/16 14:57 96-18-420.0 10.0 40 1,2,4-Trimethylbenzene 851 ug/L 07/22/16 14:57 95-63-620.0 10.0 40 1,3,5-Trimethylbenzene 201 ug/L 07/22/16 14:57 108-67-820.0 10.0 40 Vinyl chloride <40.0 ug/L 07/22/16 14:57 75-01-440.0 10.0 40 m&p-Xylene 2670 ug/L 07/22/16 14:57 179601-23-140.0 20.0 40 o-Xylene 1200 ug/L 07/22/16 14:57 95-47-620.0 10.0 40 Surrogates 1,2-Dichloroethane-d4 (S)100 %07/22/16 14:57 17060-07-070-130 40 4-Bromofluorobenzene (S)98 %07/22/16 14:57 460-00-470-130 40 Toluene-d8 (S)99 %07/22/16 14:57 2037-26-570-130 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-12 Lab ID:92305873007 Collected:07/19/16 14:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 50.5 ug/L 07/23/16 19:49 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/22/16 00:08 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/22/16 00:08 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/22/16 00:08 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/22/16 00:08 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/22/16 00:08 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/22/16 00:08 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/22/16 00:08 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/22/16 00:08 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/22/16 00:08 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/22/16 00:08 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/22/16 00:08 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/22/16 00:08 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/22/16 00:08 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/22/16 00:08 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/22/16 00:08 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/22/16 00:08 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/22/16 00:08 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/22/16 00:08 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/22/16 00:08 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/22/16 00:08 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/22/16 00:08 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/22/16 00:08 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/22/16 00:08 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/22/16 00:08 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/22/16 00:08 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/22/16 00:08 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/22/16 00:08 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/22/16 00:08 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/22/16 00:08 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/22/16 00:08 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/22/16 00:08 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/22/16 00:08 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/22/16 00:08 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/22/16 00:08 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/22/16 00:08 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/22/16 00:08 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/22/16 00:08 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/22/16 00:08 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/22/16 00:08 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/22/16 00:08 75-09-22.0 1.0 1 Methyl-tert-butyl ether 6.4 ug/L 07/22/16 00:08 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/22/16 00:08 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/22/16 00:08 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-12 Lab ID:92305873007 Collected:07/19/16 14:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/22/16 00:08 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/22/16 00:08 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/22/16 00:08 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/22/16 00:08 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/22/16 00:08 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/22/16 00:08 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/22/16 00:08 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/22/16 00:08 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/22/16 00:08 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/22/16 00:08 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/22/16 00:08 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/22/16 00:08 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/22/16 00:08 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/22/16 00:08 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/22/16 00:08 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/22/16 00:08 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/22/16 00:08 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %07/22/16 00:08 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %07/22/16 00:08 460-00-470-130 1 Toluene-d8 (S)100 %07/22/16 00:08 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-14 Lab ID:92305873008 Collected:07/19/16 13:00 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 92.6 ug/L 07/26/16 11:13 7439-92-107/22/16 17:5525.0 12.5 5 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 23:00 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 23:00 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 23:00 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 23:00 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 23:00 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 23:00 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 23:00 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 23:00 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 23:00 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 23:00 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 23:00 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 23:00 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 23:00 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 23:00 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 23:00 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 23:00 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 23:00 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 23:00 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 23:00 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 23:00 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 23:00 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 23:00 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 23:00 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 23:00 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 23:00 75-34-30.50 0.25 1 1,2-Dichloroethane 0.29J ug/L 07/21/16 23:00 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 23:00 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 23:00 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 23:00 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 23:00 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 23:00 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 23:00 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 23:00 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 23:00 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 23:00 10061-02-60.50 0.25 1 Diisopropyl ether 1.6 ug/L 07/21/16 23:00 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 23:00 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 23:00 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 23:00 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 23:00 75-09-22.0 1.0 1 Methyl-tert-butyl ether 14.2 ug/L 07/21/16 23:00 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 23:00 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 23:00 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-14 Lab ID:92305873008 Collected:07/19/16 13:00 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 23:00 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 23:00 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 23:00 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 23:00 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 23:00 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 23:00 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 23:00 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 23:00 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 23:00 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 23:00 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 23:00 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 23:00 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 23:00 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 23:00 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 23:00 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 23:00 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 23:00 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)97 %07/21/16 23:00 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %07/21/16 23:00 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 23:00 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-18 Lab ID:92305873009 Collected:07/19/16 10:20 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 54.9 ug/L 07/23/16 20:04 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 19:36 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 19:36 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 19:36 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 19:36 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 19:36 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 19:36 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 19:36 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 19:36 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 19:36 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 19:36 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 19:36 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 19:36 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 19:36 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 19:36 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 19:36 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 19:36 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 19:36 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 19:36 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 19:36 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 19:36 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 19:36 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 19:36 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 19:36 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 19:36 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 19:36 75-34-30.50 0.25 1 1,2-Dichloroethane 0.60 ug/L 07/21/16 19:36 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 19:36 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:36 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:36 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 19:36 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 19:36 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 19:36 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 19:36 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:36 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:36 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 19:36 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 19:36 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 19:36 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 19:36 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 19:36 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.62 ug/L 07/21/16 19:36 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 19:36 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 19:36 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-18 Lab ID:92305873009 Collected:07/19/16 10:20 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 19:36 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:36 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:36 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 19:36 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 19:36 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 19:36 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 19:36 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 19:36 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 19:36 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 19:36 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 19:36 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 19:36 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 19:36 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 19:36 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 19:36 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 19:36 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 19:36 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %07/21/16 19:36 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %07/21/16 19:36 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 19:36 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-22 Lab ID:92305873010 Collected:07/19/16 12:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 56.3 ug/L 07/23/16 20:07 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 19:53 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 19:53 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 19:53 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 19:53 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 19:53 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 19:53 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 19:53 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 19:53 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 19:53 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 19:53 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 19:53 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 19:53 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 19:53 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 19:53 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 19:53 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 19:53 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 19:53 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 19:53 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 19:53 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 19:53 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 19:53 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 19:53 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 19:53 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 19:53 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 19:53 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 19:53 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 19:53 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:53 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 19:53 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 19:53 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 19:53 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 19:53 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 19:53 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:53 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 19:53 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 19:53 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 19:53 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 19:53 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 19:53 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 19:53 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.41J ug/L 07/21/16 19:53 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 19:53 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 19:53 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:MW-22 Lab ID:92305873010 Collected:07/19/16 12:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 19:53 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:53 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 19:53 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 19:53 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 19:53 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 19:53 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 19:53 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 19:53 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 19:53 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 19:53 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 19:53 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 19:53 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 19:53 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 19:53 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 19:53 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 19:53 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 19:53 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)99 %07/21/16 19:53 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %07/21/16 19:53 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 19:53 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:IMW-1 Lab ID:92305873011 Collected:07/19/16 13:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 15.4 ug/L 07/23/16 20:10 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 155 ug/L 07/21/16 22:26 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 22:26 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 22:26 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 22:26 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 22:26 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 22:26 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 22:26 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 22:26 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 22:26 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 22:26 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 22:26 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 22:26 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 22:26 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 22:26 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 22:26 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 22:26 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 22:26 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 22:26 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)0.25J ug/L 07/21/16 22:26 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 22:26 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 22:26 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 22:26 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 22:26 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 22:26 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 22:26 75-34-30.50 0.25 1 1,2-Dichloroethane 6.1 ug/L 07/21/16 22:26 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 22:26 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 22:26 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 22:26 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 22:26 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 22:26 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 22:26 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 22:26 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 22:26 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 22:26 10061-02-60.50 0.25 1 Diisopropyl ether 23.6 ug/L 07/21/16 22:26 108-20-30.50 0.25 1 Ethylbenzene 4.2 ug/L 07/21/16 22:26 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 22:26 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)0.63 ug/L 07/21/16 22:26 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 22:26 75-09-22.0 1.0 1 Methyl-tert-butyl ether 150 ug/L 07/21/16 22:26 1634-04-40.50 0.25 1 Naphthalene 6.0 ug/L 07/21/16 22:26 91-20-32.0 1.0 1 n-Propylbenzene 0.56 ug/L 07/21/16 22:26 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:IMW-1 Lab ID:92305873011 Collected:07/19/16 13:40 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 22:26 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 22:26 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 22:26 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 22:26 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 22:26 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 22:26 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 22:26 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 22:26 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 22:26 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 22:26 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 22:26 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 22:26 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 1.7 ug/L 07/21/16 22:26 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 22:26 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 22:26 75-01-41.0 0.25 1 m&p-Xylene 9.9 ug/L 07/21/16 22:26 179601-23-11.0 0.50 1 o-Xylene 2.2 ug/L 07/21/16 22:26 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %07/21/16 22:26 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %07/21/16 22:26 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 22:26 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:IMW-2 Lab ID:92305873012 Collected:07/19/16 11:50 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 07/23/16 20:14 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 20:10 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 20:10 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 20:10 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 20:10 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 20:10 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 20:10 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 20:10 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 20:10 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 20:10 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 20:10 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 20:10 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 20:10 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 20:10 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 20:10 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 20:10 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 20:10 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 20:10 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 20:10 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 20:10 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 20:10 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 20:10 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 20:10 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 20:10 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 20:10 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 20:10 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 20:10 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 20:10 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 20:10 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 20:10 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 20:10 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 20:10 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 20:10 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 20:10 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 20:10 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 20:10 10061-02-60.50 0.25 1 Diisopropyl ether 0.51 ug/L 07/21/16 20:10 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 20:10 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 20:10 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 20:10 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 20:10 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 07/21/16 20:10 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 20:10 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 20:10 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:IMW-2 Lab ID:92305873012 Collected:07/19/16 11:50 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 20:10 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 20:10 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 20:10 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 20:10 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 20:10 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 20:10 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 20:10 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 20:10 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 20:10 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 20:10 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 20:10 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 20:10 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 20:10 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 20:10 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 20:10 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 20:10 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 20:10 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)101 %07/21/16 20:10 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %07/21/16 20:10 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 20:10 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-1 Lab ID:92305873013 Collected:07/20/16 11:05 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 12.9 ug/L 07/23/16 20:17 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 0.60 ug/L 07/21/16 22:43 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 22:43 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 22:43 74-97-50.50 0.25 1 Bromodichloromethane 0.83 ug/L 07/21/16 22:43 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 22:43 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 22:43 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 22:43 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 22:43 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 22:43 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 22:43 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 22:43 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 22:43 75-00-31.0 0.50 1 Chloroform 11.3 ug/L 07/21/16 22:43 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 22:43 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 22:43 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 22:43 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 22:43 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 22:43 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 22:43 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 22:43 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 22:43 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 22:43 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 22:43 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 22:43 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 22:43 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 22:43 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 22:43 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 22:43 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 22:43 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 22:43 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 22:43 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 22:43 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 22:43 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 22:43 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 22:43 10061-02-60.50 0.25 1 Diisopropyl ether 0.84 ug/L 07/21/16 22:43 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 22:43 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 22:43 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 22:43 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 22:43 75-09-22.0 1.0 1 Methyl-tert-butyl ether 44.5 ug/L 07/21/16 22:43 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 22:43 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 22:43 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-1 Lab ID:92305873013 Collected:07/20/16 11:05 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 22:43 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 22:43 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 22:43 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 22:43 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 22:43 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 22:43 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 22:43 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 22:43 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 22:43 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 22:43 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 22:43 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 22:43 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 22:43 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 22:43 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 22:43 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 22:43 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 22:43 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)101 %07/21/16 22:43 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %07/21/16 22:43 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 22:43 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-2 Lab ID:92305873014 Collected:07/20/16 09:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 4.4J ug/L 07/23/16 20:20 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 20:27 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 20:27 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 20:27 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 20:27 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 20:27 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 20:27 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 20:27 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 20:27 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 20:27 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 20:27 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 20:27 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 20:27 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 20:27 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 20:27 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 20:27 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 20:27 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 20:27 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 20:27 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 20:27 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 20:27 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 20:27 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 20:27 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 20:27 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 20:27 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 20:27 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 20:27 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 20:27 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 20:27 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 20:27 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 20:27 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 20:27 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 20:27 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 20:27 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 20:27 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 20:27 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 20:27 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 20:27 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 20:27 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 20:27 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 20:27 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 07/21/16 20:27 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 20:27 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 20:27 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-2 Lab ID:92305873014 Collected:07/20/16 09:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 20:27 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 20:27 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 20:27 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 20:27 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 20:27 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 20:27 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 20:27 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 20:27 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 20:27 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 20:27 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 20:27 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 20:27 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 20:27 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 20:27 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 20:27 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 20:27 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 20:27 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %07/21/16 20:27 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %07/21/16 20:27 460-00-470-130 1 Toluene-d8 (S)100 %07/21/16 20:27 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-3 Lab ID:92305873015 Collected:07/20/16 10:10 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead <5.0 ug/L 07/23/16 20:23 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 20:44 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 20:44 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 20:44 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 20:44 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 20:44 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 20:44 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 20:44 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 20:44 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 20:44 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 20:44 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 20:44 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 20:44 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 20:44 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 20:44 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 20:44 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 20:44 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 20:44 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 20:44 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 20:44 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 20:44 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 20:44 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 20:44 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 20:44 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 20:44 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 20:44 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 20:44 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 20:44 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 20:44 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 20:44 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 20:44 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 20:44 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 20:44 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 20:44 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 20:44 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 20:44 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 20:44 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 20:44 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 20:44 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 20:44 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 20:44 75-09-22.0 1.0 1 Methyl-tert-butyl ether 4.6 ug/L 07/21/16 20:44 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 20:44 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 20:44 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-3 Lab ID:92305873015 Collected:07/20/16 10:10 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 20:44 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 20:44 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 20:44 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 20:44 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 20:44 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 20:44 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 20:44 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 20:44 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 20:44 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 20:44 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 20:44 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 20:44 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 20:44 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 20:44 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 20:44 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 20:44 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 20:44 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %07/21/16 20:44 17060-07-070-130 1 4-Bromofluorobenzene (S)95 %07/21/16 20:44 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 20:44 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-4 Lab ID:92305873016 Collected:07/19/16 09:45 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 12.4 ug/L 07/23/16 20:26 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 21:01 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 21:01 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 21:01 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 21:01 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 21:01 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 21:01 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 21:01 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 21:01 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 21:01 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 21:01 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 21:01 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 21:01 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 21:01 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 21:01 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 21:01 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 21:01 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 21:01 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 21:01 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 21:01 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 21:01 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 21:01 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 21:01 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 21:01 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 21:01 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 21:01 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 21:01 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 21:01 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 21:01 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 21:01 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 21:01 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 21:01 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 21:01 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 21:01 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 21:01 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 21:01 10061-02-60.50 0.25 1 Diisopropyl ether <0.50 ug/L 07/21/16 21:01 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 21:01 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 21:01 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 21:01 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 21:01 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.40J ug/L 07/21/16 21:01 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 21:01 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 21:01 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-4 Lab ID:92305873016 Collected:07/19/16 09:45 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 21:01 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 21:01 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 21:01 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 21:01 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 21:01 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 21:01 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 21:01 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 21:01 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 21:01 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 21:01 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 21:01 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 21:01 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 21:01 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 21:01 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 21:01 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 21:01 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 21:01 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %07/21/16 21:01 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %07/21/16 21:01 460-00-470-130 1 Toluene-d8 (S)101 %07/21/16 21:01 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-5 Lab ID:92305873017 Collected:07/19/16 11:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Lead 13.7 ug/L 07/23/16 20:29 7439-92-107/22/16 17:555.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.50 ug/L 07/21/16 21:18 71-43-20.50 0.25 1 Bromobenzene <0.50 ug/L 07/21/16 21:18 108-86-10.50 0.25 1 Bromochloromethane <0.50 ug/L 07/21/16 21:18 74-97-50.50 0.25 1 Bromodichloromethane <0.50 ug/L 07/21/16 21:18 75-27-40.50 0.25 1 Bromoform <0.50 ug/L 07/21/16 21:18 75-25-20.50 0.25 1 Bromomethane <5.0 ug/L 07/21/16 21:18 74-83-95.0 0.50 1 n-Butylbenzene <0.50 ug/L 07/21/16 21:18 104-51-80.50 0.25 1 sec-Butylbenzene <0.50 ug/L 07/21/16 21:18 135-98-80.50 0.25 1 tert-Butylbenzene <0.50 ug/L 07/21/16 21:18 98-06-60.50 0.25 1 Carbon tetrachloride <0.50 ug/L 07/21/16 21:18 56-23-50.50 0.25 1 Chlorobenzene <0.50 ug/L 07/21/16 21:18 108-90-70.50 0.25 1 Chloroethane <1.0 ug/L 07/21/16 21:18 75-00-31.0 0.50 1 Chloroform <0.50 ug/L 07/21/16 21:18 67-66-30.50 0.25 1 Chloromethane <1.0 ug/L 07/21/16 21:18 74-87-31.0 0.50 1 2-Chlorotoluene <0.50 ug/L 07/21/16 21:18 95-49-80.50 0.25 1 4-Chlorotoluene <0.50 ug/L 07/21/16 21:18 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <1.0 ug/L 07/21/16 21:18 96-12-81.0 0.50 1 Dibromochloromethane <0.50 ug/L 07/21/16 21:18 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.50 ug/L 07/21/16 21:18 106-93-40.50 0.25 1 Dibromomethane <0.50 ug/L 07/21/16 21:18 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.50 ug/L 07/21/16 21:18 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.50 ug/L 07/21/16 21:18 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.50 ug/L 07/21/16 21:18 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.50 ug/L 07/21/16 21:18 75-71-80.50 0.25 1 1,1-Dichloroethane <0.50 ug/L 07/21/16 21:18 75-34-30.50 0.25 1 1,2-Dichloroethane <0.50 ug/L 07/21/16 21:18 107-06-20.50 0.25 1 1,1-Dichloroethene <0.50 ug/L 07/21/16 21:18 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.50 ug/L 07/21/16 21:18 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.50 ug/L 07/21/16 21:18 156-60-50.50 0.25 1 1,2-Dichloropropane <0.50 ug/L 07/21/16 21:18 78-87-50.50 0.25 1 1,3-Dichloropropane <0.50 ug/L 07/21/16 21:18 142-28-90.50 0.25 1 2,2-Dichloropropane <0.50 ug/L 07/21/16 21:18 594-20-70.50 0.25 1 1,1-Dichloropropene <0.50 ug/L 07/21/16 21:18 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.50 ug/L 07/21/16 21:18 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.50 ug/L 07/21/16 21:18 10061-02-60.50 0.25 1 Diisopropyl ether 0.30J ug/L 07/21/16 21:18 108-20-30.50 0.25 1 Ethylbenzene <0.50 ug/L 07/21/16 21:18 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <2.0 ug/L 07/21/16 21:18 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.50 ug/L 07/21/16 21:18 98-82-80.50 0.25 1 Methylene Chloride <2.0 ug/L 07/21/16 21:18 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.50 ug/L 07/21/16 21:18 1634-04-40.50 0.25 1 Naphthalene <2.0 ug/L 07/21/16 21:18 91-20-32.0 1.0 1 n-Propylbenzene <0.50 ug/L 07/21/16 21:18 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 55 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Sample:DMW-5 Lab ID:92305873017 Collected:07/19/16 11:15 Received:07/20/16 15:05 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B6200B MSV Styrene <0.50 ug/L 07/21/16 21:18 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.50 ug/L 07/21/16 21:18 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.50 ug/L 07/21/16 21:18 79-34-50.50 0.25 1 Tetrachloroethene <0.50 ug/L 07/21/16 21:18 127-18-40.50 0.25 1 Toluene <0.50 ug/L 07/21/16 21:18 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <2.0 ug/L 07/21/16 21:18 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <2.0 ug/L 07/21/16 21:18 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.50 ug/L 07/21/16 21:18 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.50 ug/L 07/21/16 21:18 79-00-50.50 0.25 1 Trichloroethene <0.50 ug/L 07/21/16 21:18 79-01-60.50 0.25 1 Trichlorofluoromethane <1.0 ug/L 07/21/16 21:18 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.50 ug/L 07/21/16 21:18 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.50 ug/L 07/21/16 21:18 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.50 ug/L 07/21/16 21:18 108-67-80.50 0.25 1 Vinyl chloride <1.0 ug/L 07/21/16 21:18 75-01-41.0 0.25 1 m&p-Xylene <1.0 ug/L 07/21/16 21:18 179601-23-11.0 0.50 1 o-Xylene <0.50 ug/L 07/21/16 21:18 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %07/21/16 21:18 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %07/21/16 21:18 460-00-470-130 1 Toluene-d8 (S)102 %07/21/16 21:18 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322121 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92305873001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1785294 Associated Lab Samples:92305873001 Matrix:Water AnalyzedMDL Lead ug/L <5.0 5.0 07/23/16 20:452.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785295LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 499500 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1785296MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305714001 1785297 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Lead ug/L 500 98 75-12599 0 20500ND492494 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322122 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92305873002, 92305873003, 92305873004, 92305873005, 92305873006, 92305873007, 92305873008, 92305873009, 92305873010, 92305873011, 92305873012, 92305873013, 92305873014, 92305873015, 92305873016, 92305873017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1785298 Associated Lab Samples:92305873002, 92305873003, 92305873004, 92305873005, 92305873006, 92305873007, 92305873008, 92305873009, 92305873010, 92305873011, 92305873012, 92305873013, 92305873014, 92305873015, 92305873016, 92305873017 Matrix:Water AnalyzedMDL Lead ug/L <5.0 5.0 07/23/16 19:122.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785299LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 447500 89 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1785300MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305873002 1785301 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Lead ug/L 500 100 75-125102 2 2050037.1 535 546 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322096 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92305873001, 92305873002, 92305873003, 92305873004, 92305873005, 92305873007, 92305873008, 92305873009, 92305873010, 92305873011, 92305873012, 92305873013, 92305873014, 92305873015, 92305873016, 92305873017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1785061 Associated Lab Samples:92305873001, 92305873002, 92305873003, 92305873004, 92305873005, 92305873007, 92305873008, 92305873009, 92305873010, 92305873011, 92305873012, 92305873013, 92305873014, 92305873015, 92305873016, 92305873017 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 07/21/16 18:280.25 1,1,1-Trichloroethane ug/L <0.50 0.50 07/21/16 18:280.25 1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 07/21/16 18:280.25 1,1,2-Trichloroethane ug/L <0.50 0.50 07/21/16 18:280.25 1,1-Dichloroethane ug/L <0.50 0.50 07/21/16 18:280.25 1,1-Dichloroethene ug/L <0.50 0.50 07/21/16 18:280.25 1,1-Dichloropropene ug/L <0.50 0.50 07/21/16 18:280.25 1,2,3-Trichlorobenzene ug/L <2.0 2.0 07/21/16 18:281.0 1,2,3-Trichloropropane ug/L <0.50 0.50 07/21/16 18:280.25 1,2,4-Trichlorobenzene ug/L <2.0 2.0 07/21/16 18:281.0 1,2,4-Trimethylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 07/21/16 18:280.50 1,2-Dibromoethane (EDB)ug/L <0.50 0.50 07/21/16 18:280.25 1,2-Dichlorobenzene ug/L <0.50 0.50 07/21/16 18:280.25 1,2-Dichloroethane ug/L <0.50 0.50 07/21/16 18:280.25 1,2-Dichloropropane ug/L <0.50 0.50 07/21/16 18:280.25 1,3,5-Trimethylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 1,3-Dichlorobenzene ug/L <0.50 0.50 07/21/16 18:280.25 1,3-Dichloropropane ug/L <0.50 0.50 07/21/16 18:280.25 1,4-Dichlorobenzene ug/L <0.50 0.50 07/21/16 18:280.25 2,2-Dichloropropane ug/L <0.50 0.50 07/21/16 18:280.25 2-Chlorotoluene ug/L <0.50 0.50 07/21/16 18:280.25 4-Chlorotoluene ug/L <0.50 0.50 07/21/16 18:280.25 Benzene ug/L <0.50 0.50 07/21/16 18:280.25 Bromobenzene ug/L <0.50 0.50 07/21/16 18:280.25 Bromochloromethane ug/L <0.50 0.50 07/21/16 18:280.25 Bromodichloromethane ug/L <0.50 0.50 07/21/16 18:280.25 Bromoform ug/L <0.50 0.50 07/21/16 18:280.25 Bromomethane ug/L <5.0 5.0 07/21/16 18:280.50 Carbon tetrachloride ug/L <0.50 0.50 07/21/16 18:280.25 Chlorobenzene ug/L <0.50 0.50 07/21/16 18:280.25 Chloroethane ug/L <1.0 1.0 07/21/16 18:280.50 Chloroform ug/L <0.50 0.50 07/21/16 18:280.25 Chloromethane ug/L <1.0 1.0 07/21/16 18:280.50 cis-1,2-Dichloroethene ug/L <0.50 0.50 07/21/16 18:280.25 cis-1,3-Dichloropropene ug/L <0.50 0.50 07/21/16 18:280.25 Dibromochloromethane ug/L <0.50 0.50 07/21/16 18:280.25 Dibromomethane ug/L <0.50 0.50 07/21/16 18:280.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1785061 Associated Lab Samples:92305873001, 92305873002, 92305873003, 92305873004, 92305873005, 92305873007, 92305873008, 92305873009, 92305873010, 92305873011, 92305873012, 92305873013, 92305873014, 92305873015, 92305873016, 92305873017 Matrix:Water AnalyzedMDL Dichlorodifluoromethane ug/L <0.50 0.50 07/21/16 18:280.25 Diisopropyl ether ug/L <0.50 0.50 07/21/16 18:280.25 Ethylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 Hexachloro-1,3-butadiene ug/L <2.0 2.0 07/21/16 18:281.0 Isopropylbenzene (Cumene)ug/L <0.50 0.50 07/21/16 18:280.25 m&p-Xylene ug/L <1.0 1.0 07/21/16 18:280.50 Methyl-tert-butyl ether ug/L <0.50 0.50 07/21/16 18:280.25 Methylene Chloride ug/L <2.0 2.0 07/21/16 18:281.0 n-Butylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 n-Propylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 Naphthalene ug/L <2.0 2.0 07/21/16 18:281.0 o-Xylene ug/L <0.50 0.50 07/21/16 18:280.25 sec-Butylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 Styrene ug/L <0.50 0.50 07/21/16 18:280.25 tert-Butylbenzene ug/L <0.50 0.50 07/21/16 18:280.25 Tetrachloroethene ug/L <0.50 0.50 07/21/16 18:280.25 Toluene ug/L <0.50 0.50 07/21/16 18:280.25 trans-1,2-Dichloroethene ug/L <0.50 0.50 07/21/16 18:280.25 trans-1,3-Dichloropropene ug/L <0.50 0.50 07/21/16 18:280.25 Trichloroethene ug/L <0.50 0.50 07/21/16 18:280.25 Trichlorofluoromethane ug/L <1.0 1.0 07/21/16 18:280.50 Vinyl chloride ug/L <1.0 1.0 07/21/16 18:280.25 1,2-Dichloroethane-d4 (S)%98 70-130 07/21/16 18:28 4-Bromofluorobenzene (S)%97 70-130 07/21/16 18:28 Toluene-d8 (S)%100 70-130 07/21/16 18:28 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785062LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 42.950 86 60-140 1,1,1-Trichloroethane ug/L 44.850 90 60-140 1,1,2,2-Tetrachloroethane ug/L 41.450 83 60-140 1,1,2-Trichloroethane ug/L 42.650 85 60-140 1,1-Dichloroethane ug/L 42.750 85 60-140 1,1-Dichloroethene ug/L 47.250 94 60-140 1,1-Dichloropropene ug/L 45.450 91 60-140 1,2,3-Trichlorobenzene ug/L 43.850 88 60-140 1,2,3-Trichloropropane ug/L 40.850 82 60-140 1,2,4-Trichlorobenzene ug/L 44.750 89 60-140 1,2,4-Trimethylbenzene ug/L 44.050 88 60-140 1,2-Dibromo-3-chloropropane ug/L 44.250 88 60-140 1,2-Dibromoethane (EDB)ug/L 43.350 87 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785062LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dichlorobenzene ug/L 42.950 86 60-140 1,2-Dichloroethane ug/L 40.050 80 60-140 1,2-Dichloropropane ug/L 42.750 85 60-140 1,3,5-Trimethylbenzene ug/L 43.150 86 60-140 1,3-Dichlorobenzene ug/L 43.450 87 60-140 1,3-Dichloropropane ug/L 41.050 82 60-140 1,4-Dichlorobenzene ug/L 43.550 87 60-140 2,2-Dichloropropane ug/L 46.050 92 60-140 2-Chlorotoluene ug/L 43.150 86 60-140 4-Chlorotoluene ug/L 43.850 88 60-140 Benzene ug/L 43.050 86 60-140 Bromobenzene ug/L 46.950 94 60-140 Bromochloromethane ug/L 43.050 86 60-140 Bromodichloromethane ug/L 42.250 84 60-140 Bromoform ug/L 42.150 84 60-140 Bromomethane ug/L 48.650 97 60-140 Carbon tetrachloride ug/L 46.150 92 60-140 Chlorobenzene ug/L 43.550 87 60-140 Chloroethane ug/L 47.250 94 60-140 Chloroform ug/L 42.750 85 60-140 Chloromethane ug/L 35.750 71 60-140 cis-1,2-Dichloroethene ug/L 44.050 88 60-140 cis-1,3-Dichloropropene ug/L 44.950 90 60-140 Dibromochloromethane ug/L 42.250 84 60-140 Dibromomethane ug/L 42.750 85 60-140 Dichlorodifluoromethane ug/L 45.250 90 60-140 Diisopropyl ether ug/L 46.250 92 60-140 Ethylbenzene ug/L 43.150 86 60-140 Hexachloro-1,3-butadiene ug/L 44.150 88 60-140 Isopropylbenzene (Cumene)ug/L 43.250 86 60-140 m&p-Xylene ug/L 84.7100 85 60-140 Methyl-tert-butyl ether ug/L 46.450 93 60-140 Methylene Chloride ug/L 49.550 99 60-140 n-Butylbenzene ug/L 45.550 91 60-140 n-Propylbenzene ug/L 42.350 85 60-140 Naphthalene ug/L 43.950 88 60-140 o-Xylene ug/L 42.350 85 60-140 sec-Butylbenzene ug/L 43.150 86 60-140 Styrene ug/L 44.950 90 60-140 tert-Butylbenzene ug/L 35.450 71 60-140 Tetrachloroethene ug/L 41.850 84 60-140 Toluene ug/L 42.450 85 60-140 trans-1,2-Dichloroethene ug/L 44.650 89 60-140 trans-1,3-Dichloropropene ug/L 43.250 86 60-140 Trichloroethene ug/L 42.550 85 60-140 Trichlorofluoromethane ug/L 44.150 88 60-140 Vinyl chloride ug/L 45.850 92 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785062LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dichloroethane-d4 (S)%102 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%100 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 1785063MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305873001 1785064 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 89 60-14091 2 3020<0.50 17.8 18.1 1,1,1-Trichloroethane ug/L 20 101 60-140101 0 3020<0.50 20.2 20.2 1,1,2,2-Tetrachloroethane ug/L 20 83 60-14084 2 3020<0.50 16.6 16.9 1,1,2-Trichloroethane ug/L 20 87 60-14090 3 3020<0.50 17.4 18.0 1,1-Dichloroethane ug/L 20 95 60-14095 0 3020<0.50 18.9 19.0 1,1-Dichloroethene ug/L 20 104 60-140104 0 3020<0.50 20.8 20.8 1,1-Dichloropropene ug/L 20 94 60-14095 1 3020<0.50 18.7 19.0 1,2,3-Trichlorobenzene ug/L 20 88 60-14092 4 3020<2.0 17.6 18.4 1,2,3-Trichloropropane ug/L 20 84 60-14086 3 3020<0.50 16.7 17.2 1,2,4-Trichlorobenzene ug/L 20 91 60-14094 4 3020<2.0 18.1 18.8 1,2,4-Trimethylbenzene ug/L 20 94 60-14094 1 30201.9 20.8 20.6 1,2-Dibromo-3- chloropropane ug/L 20 86 60-14090 5 3020<1.0 17.1 18.0 1,2-Dibromoethane (EDB)ug/L 20 89 60-14092 2 3020<0.50 17.9 18.3 1,2-Dichlorobenzene ug/L 20 93 60-14093 0 3020<0.50 18.7 18.6 1,2-Dichloroethane ug/L 20 83 60-14084 1 3020<0.50 16.8 17.0 1,2-Dichloropropane ug/L 20 87 60-14088 1 3020<0.50 17.4 17.6 1,3,5-Trimethylbenzene ug/L 20 94 60-14093 1 30203.7 22.5 22.4 1,3-Dichlorobenzene ug/L 20 91 60-14091 1 3020<0.50 18.3 18.2 1,3-Dichloropropane ug/L 20 84 60-14086 2 3020<0.50 16.7 17.1 1,4-Dichlorobenzene ug/L 20 91 60-14091 1 3020<0.50 18.1 18.3 2,2-Dichloropropane ug/L 20 90 60-14091 1 3020<0.50 18.0 18.2 2-Chlorotoluene ug/L 20 95 60-14091 4 3020<0.50 18.9 18.3 4-Chlorotoluene ug/L 20 93 60-14092 1 3020<0.50 18.6 18.5 Benzene ug/L 20 92 60-14095 2 30208.1 26.6 27.1 Bromobenzene ug/L 20 94 60-14096 2 3020<0.50 18.8 19.2 Bromochloromethane ug/L 20 91 60-14093 2 3020<0.50 18.2 18.6 Bromodichloromethane ug/L 20 90 60-14093 3 3020<0.50 18.1 18.6 Bromoform ug/L 20 79 60-14083 4 3020<0.50 15.9 16.5 Bromomethane ug/L 20 80 60-14084 5 3020<5.0 16.0 16.7 Carbon tetrachloride ug/L 20 101 60-140102 2 3020<0.50 20.2 20.5 Chlorobenzene ug/L 20 93 60-14094 1 3020<0.50 18.7 18.8 Chloroethane ug/L 20 99 60-140103 4 3020<1.0 19.8 20.6 Chloroform ug/L 20 95 60-14096 1 30204.4 23.3 23.6 Chloromethane ug/L 20 97 60-14097 0 3020<1.0 19.4 19.4 cis-1,2-Dichloroethene ug/L 20 95 60-14095 0 3020<0.50 19.0 18.9 cis-1,3-Dichloropropene ug/L 20 86 60-14090 5 3020<0.50 17.2 18.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1785063MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305873001 1785064 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Dibromochloromethane ug/L 20 85 60-14087 2 3020<0.50 17.0 17.3 Dibromomethane ug/L 20 88 60-14090 2 3020<0.50 17.5 17.9 Dichlorodifluoromethane ug/L 20 101 60-140103 1 3020<0.50 20.3 20.6 Diisopropyl ether ug/L 20 99 60-14094 5 3020<0.50 19.9 18.8 Ethylbenzene ug/L 20 94 60-14093 1 30209.0 27.9 27.7 Hexachloro-1,3-butadiene ug/L 20 91 60-14098 7 3020<2.0 18.3 19.5 Isopropylbenzene (Cumene)ug/L 20 94 60-14094 0 30200.78 19.7 19.6 m&p-Xylene ug/L 40 90 60-14091 0 304017.0 53.2 53.4 Methyl-tert-butyl ether ug/L 20 97 60-14093 4 30205.8 25.3 24.3 Methylene Chloride ug/L 20 89 60-14088 1 3020<2.0 17.7 17.6 n-Butylbenzene ug/L 20 96 60-14097 1 3020<0.50 19.2 19.4 n-Propylbenzene ug/L 20 94 60-14093 0 30200.42J 19.1 19.1 Naphthalene ug/L 20 83 60-14086 4 3020<2.0 16.8 17.4 o-Xylene ug/L 20 90 60-14089 1 302011.2 29.2 29.1 sec-Butylbenzene ug/L 20 95 60-14096 0 3020<0.50 19.1 19.1 Styrene ug/L 20 97 60-14096 0 3020<0.50 19.3 19.3 tert-Butylbenzene ug/L 20 79 60-14078 1 3020<0.50 15.8 15.6 Tetrachloroethene ug/L 20 90 60-14089 0 3020<0.50 17.9 17.9 Toluene ug/L 20 87 60-14084 2 302014.1 31.4 30.9 trans-1,2-Dichloroethene ug/L 20 97 60-14098 1 3020<0.50 19.3 19.5 trans-1,3-Dichloropropene ug/L 20 84 60-14087 3 3020<0.50 16.8 17.3 Trichloroethene ug/L 20 92 60-14094 3 3020<0.50 18.4 18.9 Trichlorofluoromethane ug/L 20 106 60-140104 2 3020<1.0 21.2 20.7 Vinyl chloride ug/L 20 94 60-14097 2 3020<1.0 18.9 19.4 1,2-Dichloroethane-d4 (S)%101 70-13099 4-Bromofluorobenzene (S)%100 70-130100 Toluene-d8 (S)%100 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322232 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92305873006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1785600 Associated Lab Samples:92305873006 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 07/22/16 12:240.25 1,1,1-Trichloroethane ug/L <0.50 0.50 07/22/16 12:240.25 1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 07/22/16 12:240.25 1,1,2-Trichloroethane ug/L <0.50 0.50 07/22/16 12:240.25 1,1-Dichloroethane ug/L <0.50 0.50 07/22/16 12:240.25 1,1-Dichloroethene ug/L <0.50 0.50 07/22/16 12:240.25 1,1-Dichloropropene ug/L <0.50 0.50 07/22/16 12:240.25 1,2,3-Trichlorobenzene ug/L <2.0 2.0 07/22/16 12:241.0 1,2,3-Trichloropropane ug/L <0.50 0.50 07/22/16 12:240.25 1,2,4-Trichlorobenzene ug/L <2.0 2.0 07/22/16 12:241.0 1,2,4-Trimethylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 07/22/16 12:240.50 1,2-Dibromoethane (EDB)ug/L <0.50 0.50 07/22/16 12:240.25 1,2-Dichlorobenzene ug/L <0.50 0.50 07/22/16 12:240.25 1,2-Dichloroethane ug/L <0.50 0.50 07/22/16 12:240.25 1,2-Dichloropropane ug/L <0.50 0.50 07/22/16 12:240.25 1,3,5-Trimethylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 1,3-Dichlorobenzene ug/L <0.50 0.50 07/22/16 12:240.25 1,3-Dichloropropane ug/L <0.50 0.50 07/22/16 12:240.25 1,4-Dichlorobenzene ug/L <0.50 0.50 07/22/16 12:240.25 2,2-Dichloropropane ug/L <0.50 0.50 07/22/16 12:240.25 2-Chlorotoluene ug/L <0.50 0.50 07/22/16 12:240.25 4-Chlorotoluene ug/L <0.50 0.50 07/22/16 12:240.25 Benzene ug/L <0.50 0.50 07/22/16 12:240.25 Bromobenzene ug/L <0.50 0.50 07/22/16 12:240.25 Bromochloromethane ug/L <0.50 0.50 07/22/16 12:240.25 Bromodichloromethane ug/L <0.50 0.50 07/22/16 12:240.25 Bromoform ug/L <0.50 0.50 07/22/16 12:240.25 Bromomethane ug/L <5.0 5.0 07/22/16 12:240.50 Carbon tetrachloride ug/L <0.50 0.50 07/22/16 12:240.25 Chlorobenzene ug/L <0.50 0.50 07/22/16 12:240.25 Chloroethane ug/L <1.0 1.0 07/22/16 12:240.50 Chloroform ug/L <0.50 0.50 07/22/16 12:240.25 Chloromethane ug/L <1.0 1.0 07/22/16 12:240.50 cis-1,2-Dichloroethene ug/L <0.50 0.50 07/22/16 12:240.25 cis-1,3-Dichloropropene ug/L <0.50 0.50 07/22/16 12:240.25 Dibromochloromethane ug/L <0.50 0.50 07/22/16 12:240.25 Dibromomethane ug/L <0.50 0.50 07/22/16 12:240.25 Dichlorodifluoromethane ug/L <0.50 0.50 07/22/16 12:240.25 Diisopropyl ether ug/L <0.50 0.50 07/22/16 12:240.25 Ethylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1785600 Associated Lab Samples:92305873006 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <2.0 2.0 07/22/16 12:241.0 Isopropylbenzene (Cumene)ug/L <0.50 0.50 07/22/16 12:240.25 m&p-Xylene ug/L <1.0 1.0 07/22/16 12:240.50 Methyl-tert-butyl ether ug/L <0.50 0.50 07/22/16 12:240.25 Methylene Chloride ug/L <2.0 2.0 07/22/16 12:241.0 n-Butylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 n-Propylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 Naphthalene ug/L <2.0 2.0 07/22/16 12:241.0 o-Xylene ug/L <0.50 0.50 07/22/16 12:240.25 sec-Butylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 Styrene ug/L <0.50 0.50 07/22/16 12:240.25 tert-Butylbenzene ug/L <0.50 0.50 07/22/16 12:240.25 Tetrachloroethene ug/L <0.50 0.50 07/22/16 12:240.25 Toluene ug/L <0.50 0.50 07/22/16 12:240.25 trans-1,2-Dichloroethene ug/L <0.50 0.50 07/22/16 12:240.25 trans-1,3-Dichloropropene ug/L <0.50 0.50 07/22/16 12:240.25 Trichloroethene ug/L <0.50 0.50 07/22/16 12:240.25 Trichlorofluoromethane ug/L <1.0 1.0 07/22/16 12:240.50 Vinyl chloride ug/L <1.0 1.0 07/22/16 12:240.25 1,2-Dichloroethane-d4 (S)%100 70-130 07/22/16 12:24 4-Bromofluorobenzene (S)%97 70-130 07/22/16 12:24 Toluene-d8 (S)%103 70-130 07/22/16 12:24 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785601LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 43.150 86 60-140 1,1,1-Trichloroethane ug/L 45.450 91 60-140 1,1,2,2-Tetrachloroethane ug/L 41.450 83 60-140 1,1,2-Trichloroethane ug/L 41.850 84 60-140 1,1-Dichloroethane ug/L 42.650 85 60-140 1,1-Dichloroethene ug/L 47.250 94 60-140 1,1-Dichloropropene ug/L 45.750 91 60-140 1,2,3-Trichlorobenzene ug/L 44.150 88 60-140 1,2,3-Trichloropropane ug/L 40.650 81 60-140 1,2,4-Trichlorobenzene ug/L 44.950 90 60-140 1,2,4-Trimethylbenzene ug/L 45.250 90 60-140 1,2-Dibromo-3-chloropropane ug/L 43.450 87 60-140 1,2-Dibromoethane (EDB)ug/L 43.950 88 60-140 1,2-Dichlorobenzene ug/L 43.950 88 60-140 1,2-Dichloroethane ug/L 38.750 77 60-140 1,2-Dichloropropane ug/L 42.150 84 60-140 1,3,5-Trimethylbenzene ug/L 44.650 89 60-140 1,3-Dichlorobenzene ug/L 44.950 90 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1785601LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 41.150 82 60-140 1,4-Dichlorobenzene ug/L 44.750 89 60-140 2,2-Dichloropropane ug/L 45.950 92 60-140 2-Chlorotoluene ug/L 43.750 87 60-140 4-Chlorotoluene ug/L 44.850 90 60-140 Benzene ug/L 43.650 87 60-140 Bromobenzene ug/L 48.050 96 60-140 Bromochloromethane ug/L 42.050 84 60-140 Bromodichloromethane ug/L 41.650 83 60-140 Bromoform ug/L 42.150 84 60-140 Bromomethane ug/L 47.850 96 60-140 Carbon tetrachloride ug/L 46.250 92 60-140 Chlorobenzene ug/L 44.350 89 60-140 Chloroethane ug/L 45.750 91 60-140 Chloroform ug/L 42.650 85 60-140 Chloromethane ug/L 43.450 87 60-140 cis-1,2-Dichloroethene ug/L 43.750 87 60-140 cis-1,3-Dichloropropene ug/L 44.950 90 60-140 Dibromochloromethane ug/L 42.650 85 60-140 Dibromomethane ug/L 41.850 84 60-140 Dichlorodifluoromethane ug/L 46.150 92 60-140 Diisopropyl ether ug/L 45.750 91 60-140 Ethylbenzene ug/L 43.950 88 60-140 Hexachloro-1,3-butadiene ug/L 47.450 95 60-140 Isopropylbenzene (Cumene)ug/L 44.450 89 60-140 m&p-Xylene ug/L 86.2100 86 60-140 Methyl-tert-butyl ether ug/L 45.250 90 60-140 Methylene Chloride ug/L 47.150 94 60-140 n-Butylbenzene ug/L 47.350 95 60-140 n-Propylbenzene ug/L 44.150 88 60-140 Naphthalene ug/L 43.250 86 60-140 o-Xylene ug/L 42.750 85 60-140 sec-Butylbenzene ug/L 44.750 89 60-140 Styrene ug/L 46.150 92 60-140 tert-Butylbenzene ug/L 37.050 74 60-140 Tetrachloroethene ug/L 43.850 88 60-140 Toluene ug/L 42.950 86 60-140 trans-1,2-Dichloroethene ug/L 45.050 90 60-140 trans-1,3-Dichloropropene ug/L 43.650 87 60-140 Trichloroethene ug/L 43.950 88 60-140 Trichlorofluoromethane ug/L 43.950 88 60-140 Vinyl chloride ug/L 47.150 94 60-140 1,2-Dichloroethane-d4 (S)%98 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1785602MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305959005 1785603 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 84 60-14091 8 3020ND16.8 18.1 1,1,1-Trichloroethane ug/L 20 95 60-140101 6 3020ND19.0 20.2 1,1,2,2-Tetrachloroethane ug/L 20 83 60-14088 6 3020ND16.7 17.7 1,1,2-Trichloroethane ug/L 20 85 60-14092 8 3020ND17.0 18.5 1,1-Dichloroethane ug/L 20 89 60-14094 5 3020ND17.8 18.8 1,1-Dichloroethene ug/L 20 100 60-140108 7 3020ND20.1 21.6 1,1-Dichloropropene ug/L 20 95 60-140101 7 3020ND19.0 20.3 1,2,3-Trichlorobenzene ug/L 20 84 60-14088 5 3020ND16.7 17.6 1,2,3-Trichloropropane ug/L 20 83 60-14092 11 3020ND16.5 18.4 1,2,4-Trichlorobenzene ug/L 20 85 60-14091 7 3020ND17.0 18.2 1,2,4-Trimethylbenzene ug/L 20 88 60-14095 7 3020ND17.6 19.0 1,2-Dibromo-3- chloropropane ug/L 20 81 60-14089 9 3020ND16.3 17.8 1,2-Dibromoethane (EDB)ug/L 20 87 60-14094 8 3020ND17.5 18.9 1,2-Dichlorobenzene ug/L 20 85 60-14092 8 3020ND17.0 18.3 1,2-Dichloroethane ug/L 20 78 60-14083 6 3020ND15.8 16.8 1,2-Dichloropropane ug/L 20 85 60-14092 9 3020ND16.9 18.5 1,3,5-Trimethylbenzene ug/L 20 88 60-14094 7 3020ND17.5 18.8 1,3-Dichlorobenzene ug/L 20 87 60-14094 8 3020ND17.3 18.7 1,3-Dichloropropane ug/L 20 82 60-14089 8 3020ND16.5 17.8 1,4-Dichlorobenzene ug/L 20 88 60-14094 7 3020ND17.6 18.8 2,2-Dichloropropane ug/L 20 87 60-14092 5 3020ND17.5 18.4 2-Chlorotoluene ug/L 20 86 60-14095 11 3020ND17.1 19.1 4-Chlorotoluene ug/L 20 88 60-14094 7 3020ND17.6 18.9 Benzene ug/L 20 90 60-14098 9 3020ND17.9 19.6 Bromobenzene ug/L 20 88 60-140101 13 3020ND17.6 20.2 Bromochloromethane ug/L 20 86 60-14092 7 3020ND17.2 18.4 Bromodichloromethane ug/L 20 84 60-14091 8 3020ND16.8 18.2 Bromoform ug/L 20 77 60-14084 9 3020ND15.4 16.9 Bromomethane ug/L 20 62 60-14078 24 3020ND12.4 15.7 Carbon tetrachloride ug/L 20 96 60-140103 7 3020ND19.1 20.6 Chlorobenzene ug/L 20 89 60-14097 8 3020ND17.9 19.4 Chloroethane ug/L 20 89 60-140104 16 3020ND17.8 20.8 Chloroform ug/L 20 87 60-14094 7 3020ND17.4 18.8 Chloromethane ug/L 20 88 60-14098 11 3020ND17.5 19.7 cis-1,2-Dichloroethene ug/L 20 90 60-14096 7 3020ND17.9 19.3 cis-1,3-Dichloropropene ug/L 20 85 60-14092 8 3020ND17.0 18.3 Dibromochloromethane ug/L 20 81 60-14089 9 3020ND16.2 17.7 Dibromomethane ug/L 20 85 60-14094 10 3020ND17.1 18.8 Dichlorodifluoromethane ug/L 20 94 60-140100 6 3020ND18.9 20.1 Diisopropyl ether ug/L 20 98 60-14096 2 3020ND19.5 19.2 Ethylbenzene ug/L 20 90 60-14096 7 3020ND18.0 19.2 Hexachloro-1,3-butadiene ug/L 20 85 60-14089 5 3020ND16.9 17.9 Isopropylbenzene (Cumene)ug/L 20 89 60-14095 7 3020ND17.7 19.1 m&p-Xylene ug/L 40 87 60-14094 8 3040ND34.7 37.7 Methyl-tert-butyl ether ug/L 20 96 60-14095 1 3020ND19.1 19.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 55 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1785602MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305959005 1785603 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 81 60-14089 9 3020ND16.2 17.8 n-Butylbenzene ug/L 20 89 60-14096 7 3020ND17.7 19.1 n-Propylbenzene ug/L 20 87 60-14093 7 3020ND17.3 18.6 Naphthalene ug/L 20 83 60-14090 9 3020ND16.5 18.1 o-Xylene ug/L 20 86 60-14092 7 3020ND17.1 18.4 sec-Butylbenzene ug/L 20 88 60-14094 8 3020ND17.5 18.9 Styrene ug/L 20 90 60-14097 7 3020ND18.1 19.4 tert-Butylbenzene ug/L 20 73 60-14077 6 3020ND14.5 15.5 Tetrachloroethene ug/L 20 88 60-14096 8 3020ND17.6 19.1 Toluene ug/L 20 90 60-14097 7 3020ND17.9 19.3 trans-1,2-Dichloroethene ug/L 20 93 60-140101 8 3020ND18.7 20.2 trans-1,3-Dichloropropene ug/L 20 82 60-14089 8 3020ND16.4 17.7 Trichloroethene ug/L 20 90 60-14096 6 3020ND18.0 19.1 Trichlorofluoromethane ug/L 20 98 60-140104 6 3020ND19.6 20.7 Vinyl chloride ug/L 20 96 60-140103 7 3020ND19.2 20.6 1,2-Dichloroethane-d4 (S)%99 70-13098 4-Bromofluorobenzene (S)%100 70-130100 Toluene-d8 (S)%100 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 55 #=QL# QUALIFIERS Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 55 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92305873 CAJAH'S MOUNTAIN SUPERETTE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92305873001 322121 322332MW-1 EPA 3010A EPA 6010 92305873002 322122 322333MW-2 EPA 3010A EPA 6010 92305873003 322122 322333MW-5 EPA 3010A EPA 6010 92305873004 322122 322333MW-7 EPA 3010A EPA 6010 92305873005 322122 322333MW-8 EPA 3010A EPA 6010 92305873006 322122 322333MW-11 EPA 3010A EPA 6010 92305873007 322122 322333MW-12 EPA 3010A EPA 6010 92305873008 322122 322333MW-14 EPA 3010A EPA 6010 92305873009 322122 322333MW-18 EPA 3010A EPA 6010 92305873010 322122 322333MW-22 EPA 3010A EPA 6010 92305873011 322122 322333IMW-1 EPA 3010A EPA 6010 92305873012 322122 322333IMW-2 EPA 3010A EPA 6010 92305873013 322122 322333DMW-1 EPA 3010A EPA 6010 92305873014 322122 322333DMW-2 EPA 3010A EPA 6010 92305873015 322122 322333DMW-3 EPA 3010A EPA 6010 92305873016 322122 322333DMW-4 EPA 3010A EPA 6010 92305873017 322122 322333DMW-5 EPA 3010A EPA 6010 92305873001 322096MW-1 SM 6200B 92305873002 322096MW-2 SM 6200B 92305873003 322096MW-5 SM 6200B 92305873004 322096MW-7 SM 6200B 92305873005 322096MW-8 SM 6200B 92305873006 322232MW-11 SM 6200B 92305873007 322096MW-12 SM 6200B 92305873008 322096MW-14 SM 6200B 92305873009 322096MW-18 SM 6200B 92305873010 322096MW-22 SM 6200B 92305873011 322096IMW-1 SM 6200B 92305873012 322096IMW-2 SM 6200B 92305873013 322096DMW-1 SM 6200B 92305873014 322096DMW-2 SM 6200B 92305873015 322096DMW-3 SM 6200B 92305873016 322096DMW-4 SM 6200B 92305873017 322096DMW-5 SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 03:45 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 55 Page 53 of 55 Page 54 of 55 Page 55 of 55 07/01/16 Technical Report for ATC Associates, Inc Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC 89.03451.1018 SGS Accutest Job Number: FA35057 Sampling Date: 06/27/16 Report to: ATC Associates, Inc Christine.schaefer@atcassociates.com ATTN: Christine Schaefer Total number of pages in report: Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001) DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177), AK, AR, GA, KY, MA, NV, OK, UT, WA This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest. Test results relate only to samples analyzed. Southeast 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407-425-6700 fax: 407-425-0707 http://www.accutest.com Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Southeast 07/01/16 e-Hardcopy 2.0 Automated Report 15 SGS Accutest is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. 1 of 15 FA35057 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................5 3.1: FA35057-1: ON-SITE ...................................................................................................6 3.2: FA35057-2: OFF-SITE .................................................................................................7 Section 4: Misc. Forms ............................................................................................................8 4.1: Chain of Custody ...........................................................................................................9 Section 5: GC Volatiles - QC Data Summaries .....................................................................12 5.1: Method Blank Summary ................................................................................................13 5.2: Blank Spike Summary ...................................................................................................14 5.3: Duplicate Summary .......................................................................................................15 1 2 3 4 5 2 of 15 FA35057 SGS Accutest Sample Summary ATC Associates, Inc Job No:FA35057 Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Project No: 89.03451.1018 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA35057-1 06/27/16 14:45 JV 06/28/16 AIR Air ON-SITE FA35057-2 06/27/16 15:00 JV 06/28/16 AIR Air OFF-SITE 3 of 15 FA35057 1 Summary of Hits Page 1 of 1 Job Number:FA35057 Account:ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Collected:06/27/16 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA35057-1 ON-SITE Benzene 1.3 0.50 0.10 ppmv EPA TO-3 Toluene 15.4 0.50 0.10 ppmv EPA TO-3 Ethylbenzene 4.1 0.50 0.10 ppmv EPA TO-3 Xylenes (total)19.0 1.5 0.30 ppmv EPA TO-3 TPH as Equiv Pentane 336 5.0 2.4 ppmv EPA TO-3 Benzene 4.2 1.6 0.32 mg/m3 EPA TO-3 Toluene 58.0 1.9 0.38 mg/m3 EPA TO-3 Ethylbenzene 18 2.2 0.43 mg/m3 EPA TO-3 Xylenes (total)82.5 6.5 1.3 mg/m3 EPA TO-3 TPH as Equiv Pentane 989 15 7.1 mg/m3 EPA TO-3 FA35057-2 OFF-SITE No hits reported in this sample. 4 of 15 FA35057 2 SGS Accutest Sample Results Report of Analysis Southeast Section 3 5 of 15 FA35057 3 SGS Accutest Report of Analysis Page 1 of 1 Client Sample ID:ON-SITE Lab Sample ID:FA35057-1 Date Sampled:06/27/16 Matrix:AIR - Air Date Received:06/28/16 Method:EPA TO-3 Percent Solids:n/a Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 HH054161.D 1 06/29/16 AJC n/a n/a GHH3036 Run #2 Initial Volume Run #1 0.50 ml Run #2 Purgeable Aromatics CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units 71-43-2 78.11 Benzene 1.3 0.50 0.10 ppmv 4.2 1.6 0.32 mg/m3 108-88-3 92.14 Toluene 15.4 0.50 0.10 ppmv 58.0 1.9 0.38 mg/m3 100-41-4 106.2 Ethylbenzene 4.1 0.50 0.10 ppmv 18 2.2 0.43 mg/m3 1330-20-7 106.2 Xylenes (total)19.0 1.5 0.30 ppmv 82.5 6.5 1.3 mg/m3 1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3 72 TPH as Equiv Pentane 336 5.0 2.4 ppmv 989 15 7.1 mg/m3 CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 97%54-142% 460-00-4 4-Bromofluorobenzene 85%54-142% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 15 FA35057 3 3. 1 SGS Accutest Report of Analysis Page 1 of 1 Client Sample ID:OFF-SITE Lab Sample ID:FA35057-2 Date Sampled:06/27/16 Matrix:AIR - Air Date Received:06/28/16 Method:EPA TO-3 Percent Solids:n/a Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 HH054162.D 1 06/29/16 AJC n/a n/a GHH3036 Run #2 Initial Volume Run #1 0.50 ml Run #2 Purgeable Aromatics CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units 71-43-2 78.11 Benzene ND 0.50 0.10 ppmv ND 1.6 0.32 mg/m3 108-88-3 92.14 Toluene ND 0.50 0.10 ppmv ND 1.9 0.38 mg/m3 100-41-4 106.2 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 0.43 mg/m3 1330-20-7 106.2 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 1.3 mg/m3 1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3 72 TPH as Equiv Pentane ND 5.0 2.4 ppmv ND 15 7.1 mg/m3 CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 93%54-142% 460-00-4 4-Bromofluorobenzene 83%54-142% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 15 FA35057 3 3. 2 SGS Accutest Misc. Forms Custody Documents and Other Forms Includes the following where applicable: Chain of Custody Southeast Section 4 8 of 15 FA35057 4 FA35057: Chain of Custody Page 1 of 3 9 of 15 FA35057 4 4. 1 FA35057: Chain of Custody Page 2 of 3 10 of 15 FA35057 4 4. 1 FA35057: Chain of Custody Page 3 of 3 11 of 15 FA35057 4 4. 1 SGS Accutest GC Volatiles QC Data Summaries Includes the following where applicable: Method Blank Summaries Blank Spike Summaries Matrix Spike and Duplicate Summaries Southeast Section 5 12 of 15 FA35057 5 Method Blank Summary Page 1 of 1 Job Number:FA35057 Account:ATCNCC ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GHH3036-MB HH054160.D 1 06/29/16 AJC n/a n/a GHH3036 The QC reported here applies to the following samples:Method: EPA TO-3 FA35057-1, FA35057-2 CAS No.Compound Result RL MDL Units Q Result RL Units 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 mg/m3 71-43-2 Benzene ND 0.50 0.10 ppmv ND 1.6 mg/m3 108-88-3 Toluene ND 0.50 0.10 ppmv ND 1.9 mg/m3 100-41-4 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 mg/m3 1330-20-7 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 mg/m3 TPH as Equiv Pentane ND 5.0 2.4 ppmv ND 15 mg/m3 CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 93%54-142% 460-00-4 4-Bromofluorobenzene 84%54-142% 13 of 15 FA35057 5 5. 1 . 1 Blank Spike Summary Page 1 of 1 Job Number:FA35057 Account:ATCNCC ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GHH3036-BS HH054159.D 1 06/29/16 AJC n/a n/a GHH3036 The QC reported here applies to the following samples:Method: EPA TO-3 FA35057-1, FA35057-2 Spike BSP BSP CAS No.Compound ppmv ppmv %Limits 1634-04-4 Methyl Tert Butyl Ether 10 7.5 75 60-111 71-43-2 Benzene 10 8.2 82 64-111 108-88-3 Toluene 10 8.5 85 60-112 100-41-4 Ethylbenzene 10 9.0 90 59-112 1330-20-7 Xylenes (total)30 27.4 91 58-110 TPH as Equiv Pentane 135 126 93 66-116 CAS No.Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 90%54-142% 460-00-4 4-Bromofluorobenzene 84%54-142% * = Outside of Control Limits. 14 of 15 FA35057 5 5. 2 . 1 Duplicate Summary Page 1 of 1 Job Number:FA35057 Account:ATCNCC ATC Associates, Inc Project:Cajah's Mountain; 1900 Connelly Springs Rd, Lenoir, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA35057-2DUP HH054163.D 1 06/29/16 AJC n/a n/a GHH3036 FA35057-2 HH054162.D 1 06/29/16 AJC n/a n/a GHH3036 The QC reported here applies to the following samples:Method: EPA TO-3 FA35057-1, FA35057-2 FA35057-2 DUP CAS No.Compound ppmv Q ppmv Q RPD Limits 1634-04-4 Methyl Tert Butyl Ether ND ND nc 10 71-43-2 Benzene ND ND nc 11 108-88-3 Toluene ND ND nc 14 100-41-4 Ethylbenzene ND ND nc 13 1330-20-7 Xylenes (total)ND ND nc 15 TPH as Equiv Pentane ND ND nc 28 CAS No.Surrogate Recoveries DUP FA35057-2 Limits 460-00-4 4-Bromofluorobenzene 94%93%54-142% 460-00-4 4-Bromofluorobenzene 83%83%54-142% * = Outside of Control Limits. 15 of 15 FA35057 5 5. 3 . 1