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7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Tel: 704-529-3200
Fax: 704-529-3272
www.atcassociates.com
N.C. Engineering License No. C-1598
1
March 5, 2014
Mr. Dan Murphy
North Carolina Department of Environment and Natural Resources
Asheville Regional Office
Division of Waste Management - UST Section
2090 US Highway 70
Swannanoa, North Carolina 28778
Re: AS/SVE O&M Summary
Former Tilley’s Superette
1710 Union Grove Road
Lenoir, North Carolina 28645
Facility ID No. 0-007680
NCDENR Incident No. 28466
Site Risk: H155D
ATC Project No. 89.03451.1033
Dear Mr. Murphy:
ATC Associates of North Carolina, P.C. (ATC), on behalf of Cary Oil Company (Cary Oil), is submitting the
enclosed summary of Air Sparge/Soil Vapor Extraction (AS/SVE) system operation and maintenance
(O&M) activities conducted from November 2013 through January 2014.
If you have any questions or comments, please contact us at (704) 529-3200.
Sincerely,
ATC Associates of North Carolina, P.C.
Christine E. Schaefer
Project Manager
cc: Mr. Glenn Petti – Cary Oil Company
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
Tel: 704-529-3200
Fax: 704-529-3272
www.atcassociates.com
N.C. Engineering License No. C-1598
1
March 5, 2014
Mr. Dan Murphy
North Carolina Department of Environment and Natural Resources
Asheville Regional Office
Division of Waste Management - UST Section
2090 US Highway 70
Swannanoa, North Carolina 28778
Re: AS/SVE O&M Summary
Former Tilley’s Superette
1710 Union Grove Road
Lenoir, North Carolina 28645
Facility ID No. 0-007680
NCDENR Incident No. 28466
Site Risk: H155D
ATC Project No. 89.03451.1033
Dear Mr. Murphy:
ATC Associates of North Carolina, P.C. (ATC), on behalf of Cary Oil Company (Cary Oil), is submitting a
summary of Air Sparge/Soil Vapor Extraction (AS/SVE) system operation and maintenance (O&M)
activities conducted from November 2013 through January 2014.
O&M site visits were conducted by ATC personnel on November 14, November 27, December 10 and
December 30, 2013, and January 16 and January 28, 2014. System run-time was 100% from November 2013
through January 2014. Soil vapor extraction wells SVE-6 through SVE-8 were turned off on April 8, 2013,
to increase system vacuum in areas of highest groundwater impact. During site visits in October and
November 2013, air sparge wells AS-4, AS-5, AS-7, AS-8, AS-9, and AS-10 were turned off and pressures at
the remaining operational sparge wells were adjusted to focus remedial efforts in areas of remaining
contaminant impact. Vacuum readings for each well point at the SVE manifold were set at approximately 56
inches of water. Pressure readings for each well point at the AS manifold were set at approximately 16 psi.
An SVE effluent air sample was collected on December 30, 2013. The air sample was submitted to Accutest
Laboratories for analysis by EPA Method 18. The laboratory analytical report is provided in Appendix A.
Table 2 shows SVE cumulative recovery calculations based on system effluent sampling data. Assuming
consistent recovery during each day of operation between sampling dates, approximately 3,036 lbs of total
BTEX have been recovered since system startup.
Measurements of depth to water and dissolved oxygen were recorded from 20 site monitoring wells on a
monthly basis during the first quarter of system operation and are now recorded on a semi-annual basis
during groundwater monitoring events, to determine the effectiveness of the air sparge system. Readings are
Former Tilley’s Superette – O&M Summary March 5, 2014
NCDENR Incident No. 28466 ATC Project No. 89.03451.1033
3
TABLES
Table 1
Depth to Water and Dissolved Oxygen Readings
Former Tilley's Superette
1710 Union Grove Road
Lenoir, North Carolina
Facility ID Number 0-007680
Incident Number 28466
DTW DO DTW DO DTW DO DTW DO DTW DO DTW DO
(ft below
TOC)(mg/L)(ft below
TOC)(mg/L)(ft below
TOC)(mg/L)(ft below
TOC)(mg/L)(ft below
TOC)(mg/L)(ft below
TOC)(mg/L)
MW-1 40.90 8.11 40.20 7.69 40.08 8.68 40.22 6.29 42.26 3.22 35.12 7.92
MW-2 41.05 NR 40.38 1.46 40.14 2.82 40.21 1.49 41.98 2.26 35.23 3.53
MW-3 40.51 NR 39.88 4.12 39.59 5.46 39.52 2.53 41.91 2.07 34.91 8.29
MW-4 34.51 7.42 33.69 7.99 33.60 10.48 33.90 8.51 35.75 8.06 28.06 7.03
MW-5D 41.38 8.58 40.64 1.33 40.50 1.68 40.76 2.46 42.58 2.08 35.23 2.47
MW-6 37.33 7.21 36.39 8.37 36.33 9.74 36.58 7.17 38.66 7.71 30.78 8.43
MW-7 31.83 9.24 31.23 8.66 30.23 11.11 31.55 8.99 33.43 9.42 25.26 8.28
MW-8 35.05 9.52 34.58 8.31 34.76 10.20 35.16 7.78 36.52 9.02 29.08 8.32
MW-9 39.23 2.81 38.78 5.05 38.75 7.83 39.06 2.35 40.61 2.67 33.27 8.26
MW-10 41.53 5.83 41.13 6.60 40.80 7.58 40.84 6.60 42.53 6.93 36.18 8.22
MW-11 40.80 9.14 40.11 4.11 39.82 4.22 39.81 2.89 41.85 2.06 35.32 6.96
MW-12 39.23 5.62 39.02 8.12 39.05 6.88 39.38 4.38 40.91 2.28 33.88 8.25
MW-13 27.74 9.46 27.43 8.05 27.59 9.53 28.03 8.10 29.27 8.98 22.13 8.64
MW-14 29.59 6.57 28.96 7.10 29.15 9.24 29.64 7.77 30.98 8.24 23.57 8.78
MW-15 31.16 9.28 30.86 10.02 30.90 11.15 31.37 8.88 32.62 10.40 25.24 8.76
MW-16D 39.74 5.99 39.40 1.70 41.00 2.90 39.86 1.64 41.20 1.65 34.06 5.98
MW-17 40.66 8.52 40.38 5.48 40.37 7.38 40.63 4.98 42.08 Dry 35.86 8.85
MW-18 37.21 7.49 36.92 6.26 37.02 6.95 37.38 5.24 38.75 6.47 31.77 7.68
MW-19 25.54 8.99 25.23 6.59 25.41 9.43 25.81 5.23 27.04 Dry 19.93 8.83
MW-20 16.11 5.67 15.89 5.62 16.04 8.96 16.42 5.40 17.54 8.01 10.53 8.90
TOC = top of casing
NR = not recorded (sheen observed)
8/14/2013
Well ID
5/7/2012 6/6/2012 7/9/2012 8/8/2012 2/13/2013
Date
Cross-Sectional
Area of Pipe
Conversion
Factor3 Days of
Operation
Cumulative
Recovery
(ft2) (lb-m3/mg-ft3)(lb/hr) (lb/day) (days) (lbs)
06/20/12 0.08700 2,982 259.4 835.9 0.00000006243 0.8123 19.50 57.00 1,111
09/19/12 0.08700 3,433 298.7 367.0 0.00000006243 0.4106 9.85 91.00 2,008
12/19/12 * 0.08700 3,433 298.7 305.0 0.00000006243 0.3412 8.189 91.00 2,753
03/20/13 0.08700 2,260 196.6 90.50 0.00000006243 0.06665 1.600 91.00 2,899
06/26/13 0.08700 828.0 72.04 101.9 0.00000006243 0.02750 0.6599 98.00 2,963
09/28/13 * 0.08700 828.0 72.04 25.10 0.00000006243 0.00677 0.1625 94.00 2,979
12/30/13 * 0.08700 564.0 49.07 140.10 0.00000006243 0.02575 0.6180 93.00 3,036
Notes:
* Effluent velocity inferred; reading not collected due to water in line
2. Total BTEX concentrations in effluent air are based on EPA Method 18 laboratory data
3. Conversion factor to convert units of concentration from mg/m3 to lb/ft3
4. Mass removal rate = (air flow rate) x (total BTEX) x (conversion factor) x (60 min/hr or 1,440 min/day)
Incident Number 28466
Effluent
Velocity
(ft/min)
Air Flow
Rate1
(ft3/min)
Total
BTEX2
(mg/m3)
Mass Removal Rate4
1. Air flow rate = (cross-sectional area) x (effluent velocity)
Table 2
SVE System Cumulative Recovery
Former Tilley's Superette
1710 Union Grove Road
Lenoir, North Carolina
Facility ID Number 0-007680
Former Tilley’s Superette – O&M Summary March 5, 2014
NCDENR Incident No. 28466 ATC Project No. 89.03451.1033
4
FIGURES
Former Tilley’s Superette – O&M Summary March 5, 2014
NCDENR Incident No. 28466 ATC Project No. 89.03451.1033
5
APPENDIX A
01/06/14
Technical Report for
Cardno ATC Associates, Inc
Tilleys; 1710 Union Grove Rd, Lenior, NC
089.03451.1037
Accutest Job Number: FA11242
Sampling Date: 12/30/13
Report to:
Cardno ATC Associates
4020 Old Pineville Rd
Charlotte, NC 28217
mike.shaw@atcassociates.com; christine.dupuis@atcassociates.com
ATTN: Mike Shaw
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407-425-6700 fax: 407-425-0707 http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
01/06/14
e-Hardcopy 2.0
Automated Report
13
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 13
FA11242
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA11242-1: SVE ...........................................................................................................6
Section 4: Misc. Forms ............................................................................................................7
4.1: Chain of Custody ...........................................................................................................8
Section 5: GC Volatiles - QC Data Summaries .....................................................................10
5.1: Method Blank Summary ................................................................................................11
5.2: Blank Spike Summary ...................................................................................................12
5.3: Duplicate Summary .......................................................................................................13
1
2
3
4
5
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FA11242
Accutest Laboratories
Sample Summary
Cardno ATC Associates, Inc
Job No:FA11242
Tilleys; 1710 Union Grove Rd, Lenior, NC
Project No: 089.03451.1037
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA11242-1 12/30/13 13:00 CL 12/31/13 AIR Air SVE
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FA11242
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Summary of Hits Page 1 of 1
Job Number:FA11242
Account:Cardno ATC Associates, Inc
Project:Tilleys; 1710 Union Grove Rd, Lenior, NC
Collected:12/30/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA11242-1 SVE
Benzene 0.55 0.50 0.10 ppmv EPA TO-3
Toluene 11.6 0.50 0.10 ppmv EPA TO-3
Ethylbenzene 3.6 0.50 0.10 ppmv EPA TO-3
Xylenes (total)18.1 1.5 0.30 ppmv EPA TO-3
TPH as Equiv Pentane 271 5.0 1.0 ppmv EPA TO-3
Benzene 1.8 1.6 0.32 mg/m3 EPA TO-3
Toluene 43.7 1.9 0.38 mg/m3 EPA TO-3
Ethylbenzene 16 2.2 0.43 mg/m3 EPA TO-3
Xylenes (total)78.6 6.5 1.3 mg/m3 EPA TO-3
TPH as Equiv Pentane 798 15 2.9 mg/m3 EPA TO-3
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FA11242
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Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:SVE
Lab Sample ID:FA11242-1 Date Sampled:12/30/13
Matrix:AIR - Air Date Received:12/31/13
Method:EPA TO-3 Percent Solids:n/a
Project:Tilleys; 1710 Union Grove Rd, Lenior, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 HH047742.D 1 12/31/13 SH n/a n/a GHH2542
Run #2
Initial Volume
Run #1 0.50 ml
Run #2
Purgeable Aromatics
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
71-43-2 78.11 Benzene 0.55 0.50 0.10 ppmv 1.8 1.6 0.32 mg/m3
108-88-3 92.14 Toluene 11.6 0.50 0.10 ppmv 43.7 1.9 0.38 mg/m3
100-41-4 106.2 Ethylbenzene 3.6 0.50 0.10 ppmv 16 2.2 0.43 mg/m3
1330-20-7 106.2 Xylenes (total)18.1 1.5 0.30 ppmv 78.6 6.5 1.3 mg/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3
72 TPH as Equiv Pentane 271 5.0 1.0 ppmv 798 15 2.9 mg/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 94%54-142%
460-00-4 4-Bromofluorobenzene 86%54-142%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA11242
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3.
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
Chain of Custody
Southeast
Section 4
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FA11242: Chain of Custody
Page 1 of 2
8 of 13
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4
4.
1
FA11242: Chain of Custody
Page 2 of 2
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4
4.
1
Accutest Laboratories
GC Volatiles
QC Data Summaries
Includes the following where applicable:
Method Blank Summaries
Blank Spike Summaries
Matrix Spike and Duplicate Summaries
Southeast
Section 5
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FA11242
5
Method Blank Summary Page 1 of 1
Job Number:FA11242
Account:ATCNCC Cardno ATC Associates, Inc
Project:Tilleys; 1710 Union Grove Rd, Lenior, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GHH2542-MB HH047736.D1 12/31/13 SH n/a n/a GHH2542
The QC reported here applies to the following samples:Method: EPA TO-3
FA11242-1
CAS No.Compound Result RL MDL Units Q Result RL Units
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 mg/m3
71-43-2 Benzene ND 0.50 0.10 ppmv ND 1.6 mg/m3
108-88-3 Toluene ND 0.50 0.10 ppmv ND 1.9 mg/m3
100-41-4 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 mg/m3
1330-20-7 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 mg/m3
TPH as Equiv Pentane ND 5.0 1.0 ppmv ND 15 mg/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 84%54-142%
460-00-4 4-Bromofluorobenzene 91%54-142%
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FA11242
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5.
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Blank Spike Summary Page 1 of 1
Job Number:FA11242
Account:ATCNCC Cardno ATC Associates, Inc
Project:Tilleys; 1710 Union Grove Rd, Lenior, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GHH2542-BS HH047735.D1 12/31/13 SH n/a n/a GHH2542
The QC reported here applies to the following samples:Method: EPA TO-3
FA11242-1
Spike BSP BSP
CAS No.Compound ppmv ppmv %Limits
1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 60-111
71-43-2 Benzene 10 9.0 90 64-111
108-88-3 Toluene 10 9.3 93 60-112
100-41-4 Ethylbenzene 10 9.7 97 59-112
1330-20-7 Xylenes (total)30 29.7 99 58-110
TPH as Equiv Pentane 135 116 86 66-116
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 85%54-142%
460-00-4 4-Bromofluorobenzene 94%54-142%
* = Outside of Control Limits.
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Duplicate Summary Page 1 of 1
Job Number:FA11242
Account:ATCNCC Cardno ATC Associates, Inc
Project:Tilleys; 1710 Union Grove Rd, Lenior, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA11238-2DUP HH047739.D1 12/31/13 SH n/a n/a GHH2542
FA11238-2 HH047738.D1 12/31/13 SH n/a n/a GHH2542
The QC reported here applies to the following samples:Method: EPA TO-3
FA11242-1
FA11238-2 DUP
CAS No.Compound ppmv Q ppmv Q RPD Limits
1634-04-4 Methyl Tert Butyl Ether 0.50 U ND nc 10
71-43-2 Benzene 0.50 U ND nc 11
108-88-3 Toluene 0.50 U ND nc 14
100-41-4 Ethylbenzene 0.50 U ND nc 13
1330-20-7 Xylenes (total)1.5 U ND nc 15
TPH as Equiv Pentane 5.0 U ND nc 28
CAS No.Surrogate Recoveries DUP FA11238-2 Limits
460-00-4 4-Bromofluorobenzene 82%86%54-142%
460-00-4 4-Bromofluorobenzene 86%87%54-142%
* = Outside of Control Limits.
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