AS-3132_28327_CA_MRP_20170208

Antea USA of North Carolina, Inc. 
3530 Toringdon Way, Suite 106 
Charlotte, North Carolina 28227 USA 
www.anteagroup.com 
Antea USA, Inc. 
February 8, 2017 
North Carolina Department of Environmental Quality 
Division of Waste Management 
Underground Storage Tank Section 
2090 US 70 Highway 
Swannanoa, North Carolina 28788 
Attention: 
Subject:  
Mr. Dan Murphy 
Incident Manager 
2016 Annual Groundwater Monitoring 
Report GPM 3089 (Former Scotchman #89) 
3045 Tynecastle  Highway 
Banner Elk, Avery County, North Carolina 
Incident No. 28327 
Antea USA of NC Project No. NC30891601 
Dear Mr. Murphy: 
Attached please find the 2016 Annual Groundwater Monitoring Report for the above referenced facility. If you have any 
questions please feel free to contact me at (704) 324‐7045.  
Sincerely, 
Antea USA of North Carolina, Inc, 
Kyle Sorensen 
Project Manager 
cc:  Mr. Rolfe Lann – Director of Environmental; GPM Southeast, LLC 
Antea USA, Inc. 
Prepared for: 
GPM Southeast, LLC 
8565 Magellan Parkway, Suite 400 
Richmond, VA 23227 
[phone]
2016 Annual Groundwater 
Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Incident # 28327 
Antea USA of N  Project No. NC30891601  
February 8, 2017 
Prepared by: 
Antea USA of North Carolina, Inc. 
3530 Toringdon Way, Suite 106 
Charlotte, NC 28227 
[phone]
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 
i www.anteagroup.com 
Table of Contents  
1.0 INTRODUCTION AND BACKGROUND INFORMATION .................................................................................................. 1 
1.1 Site History .............................................................................................................................................................. 1 
2.0 FIELD ACTIVITIES.......................................................................................................................................................... 2 
3.0 GROUNDWATER ELEVATIONS ..................................................................................................................................... 2 
4.0 GROUNDWATER SAMPLING ........................................................................................................................................ 2 
5.0 LABORATORY ANALYTICAL RESULTS ........................................................................................................................... 3 
6.0 RECOMMENDATIONS .................................................................................................................................................. 3 
7.0 REMARKS ..................................................................................................................................................................... 4 
Tables 
Table 1   Water Supply Well Information 
Table 2   Groundwater Elevation Data 
Table 3   Groundwater Analytical Data 
Figures 
Figure 1 Site Location Map 
Figure 2 Site Map 
Figure 3 Shallow Groundwater Contour Map 
Appendices 
Appendix A Groundwater Sampling Records 
Appendix B Laboratory Analytical Reports and Chain‐of‐Custody Records 
1 www.anteagroup.com 
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Incident Number 28327 
1.0 INTRODUCTION AND BACKGROUND INFORMATION 
Antea USA of North Carolina, Inc. (Antea USA of NC) is pleased to present the following Groundwater Monitoring 
Report for GPM Southeast, LLC. (GPM) site 3089 located at 3045 Tynecastle Highway, Banner Elk, Avery County, 
North Carolina (the site). This report was prepared on behalf of GPM and documents the results of the January 
2016 and June 2016 groundwater monitoring event. 
1.1 Site History  
The property is owned by the Norwood Family Limited Partnership and currently operates as a winter ski retail 
store and gem mining store (Figure 2). The site is approximately 18.02‐acres and is located at the intersection of 
Arnett Road and North Carolina Highway 184 (Tynecastle Highway) in Banner Elk, North Carolina. Historically the 
site was owned and operated by Worsley Companies, Inc. as a retail service station from 1983 until 2005. Worsley 
operated five underground storage tanks (UST) including: three 6,000‐gallon gasoline USTs, one 4,000‐gallon 
kerosene UST, and one 4,000‐gallon diesel UST. 
During UST closure assessment activities it was determined that a gasoline release had occurred. Consequently, 
the UST Section requested that a Phase I Limited Site Assessment (LSA) be performed for the site. LSA activities 
were initiated by Geological Resources, Inc. (GRI) of Charlotte, North Carolina, on July 11, 2007, with the 
installation of one source area monitoring well (MW‐1). The LSA indicated the presence of petroleum compounds 
above the North Carolina groundwater quality standards as defined in North Carolina Administrative Code Title 
15A Chapter 2L .0202 (2L Standards). On February 18, 2008, Best Geologic and Environmental Consulting, P.A. 
(Best) advanced five soil probes to define the extent of impacted soil. Best installed four new 2‐inch Type II 
monitoring wells (MW‐2, MW‐3, MW‐4, and MW‐5) on March 13 and 14, 2008, to complete the horizontal 
delineation of the petroleum compounds in groundwater. One Type III groundwater monitoring well (MW‐1D) was 
installed to determine the vertical extent of impacted groundwater. One additional monitoring well (MW‐6) was 
installed by Best on June 5, 2008 to further define the extent of impacted groundwater. Laboratory analyses of the 
groundwater sample collected from MW‐6 indicated that the horizontal delineation of groundwater impact had 
been completed. On June 16, 2010, Best installed a 2‐inch Type II monitoring well (MW‐3R) to replace MW‐3 which 
was damaged beyond repair during parking lot improvement activities. In addition to the installation of MW‐3R, 
the manways for monitoring wells MW‐1 and MW‐5 were replaced. A total of seven groundwater monitoring wells 
have been installed at the site to assess the release. 
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 
2 www.anteagroup.com 
2.0 FIELD ACTIVITIES 
The following tasks were completed during the January 26, 2016 and June 22, 2016 site visits: 
On January 26, 2016, depth‐to‐groundwater measurements and groundwater samples were obtained
from monitoring wells MW‐1, MW‐1D, MW‐2, MW‐3R, MW‐5, and MW‐6 and groundwater samples were
also obtained from water supply well WSW‐4.
On June 22, 2016, groundwater samples were collected from water supply wells WSW‐1 and WSW‐3.
Groundwater monitoring well MW‐4 was not located during the December 8, 2014 and January 26, 2016 sampling 
events and is believed to be buried beneath a sluice that was constructed for gem mining operations. In January 
2016 water supply wells WSW‐1 and WSW‐3 could not be located. A site visit was conducted in June 2016 and 
wells WSW‐1 and WSW‐3 were located and sampled. A water supply well table has been provided as Table 1. For 
reference purposes, a Site Location Map and a Site Map are included as Figures 1 and 2, respectively. 
3.0 GROUNDWATER ELEVATIONS 
On January 26, 2016, an Antea USA of NC representative conducted gauging activities at the subject site. Depth to 
groundwater measurements were collected from monitoring wells MW‐1, MW‐1D, MW‐2, MW‐3R, MW‐5, and 
MW‐6 using a decontaminated electronic oil/water interface meter with an accuracy of 0.01 feet. Free product 
was not detected in any of the wells gauged on January 26, 2016. Disposable nitrile gloves were worn and changed 
between measurements. Groundwater elevation data is summarized in Table 2 and groundwater sampling records 
are included in Appendix A. 
Groundwater flow direction in the shallow aquifer was estimated by developing a groundwater contour map based 
on water table elevation data obtained from the wells on January 26, 2016 (Figure 3). Interpretation of the water 
table contour map suggests that the shallow water table across the Site flows generally toward the west. 
4.0 GROUNDWATER SAMPLING 
On January 26, 2016, an Antea USA of NC representative collected groundwater samples from monitoring wells 
MW‐1, MW‐1D, MW‐2, MW‐3R, MW‐5, MW‐6, and from water supply well WSW‐4. The monitoring wells were 
purged of at least three volumes of water, or until dry, using new disposable bailers. Groundwater sampling 
records that document the sampling process are included in Appendix A. The water supply wells during the 
January 2016 and June 2016 sampling events were purged for 15 minutes each prior to collection of samples. 
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 
3 www.anteagroup.com 
Following purging of the wells, groundwater samples were collected in laboratory‐supplied containers, placed into 
an ice‐filled cooler, and transported under chain‐of‐custody to FTS Analytical Services (FTS) in Norcross, Georgia. 
Disposable nitrile gloves were worn during the sampling of each well to minimize the potential for cross‐
contamination during the sampling process. At the laboratory, the January 2016 samples were analyzed by EPA 
Method 6200B for volatile organic compounds (VOCs) Total lead samples were inadvertently not analyzed during 
the January 26, 2016 sampling event. Total lead will return to the list of analyses during the next sampling event. 
The June 2016 water supply well samples were analyzed for VOCs by SM 6200B and EPA Method 6010 for total 
lead. 
5.0 LABORATORY ANALYTICAL RESULTS 
The laboratory analytical reports and chain‐of‐custody record for the groundwater samples collected during the 
January 2016 and June 2016 sampling events are provided in Appendix B. Groundwater analytical data is 
summarized in Table 3.  
MTBE was detected in the groundwater samples collected from monitoring wells MW‐1 (44.1 micrograms per liter 
[µg/L]) and MW‐3R (30.1 µg/L) at concentrations exceeding the 2L Standard of 20 µg/L. Benzene was detected in 
the sample collected from monitoring well MW‐3R at an estimated concentration of 1.30 µg/L, exceeding the 
respective 2L Standard of 1 µg/L. Other VOCs were detected below 2L Standards in the groundwater samples 
collected from monitoring wells MW‐1, MW‐3R, and MW‐5. No additional VOCs were detected in any of the 
groundwater samples analyzed at concentrations exceeding laboratory method detection limits (MDLs). 
Total lead samples were inadvertently not collected during the January 26, 2016 sampling event. During the 
previous sampling event (December 8, 2014) total lead was detected at concentrations exceeding the 2L standard 
of 15 µg/L in monitoring wells MW‐1 (58.8 µg/L) and MW‐6 (42.1 µg/L). Total lead will return to the list of analyses 
during the next sampling event. 
The laboratory results of groundwater samples collected at water supply wells WSW‐1, WSW‐3, and WSW‐4 did 
not reveal target compounds above laboratory method detection limits. 
6.0 RECOMMENDATIONS 
Based on the data collected during groundwater monitoring activities, Antea USA of NC recommends continued 
annual groundwater monitoring with the next sampling event conducted in June 2017. Groundwater samples 
should be collected from monitoring wells MW‐1, MW‐1D, MW‐2, MW‐3R, MW‐4 (if accessible), MW‐5, MW‐6, 
and from water supply wells WSW‐1, WSW‐3, and WSW‐4 for analysis of EPA Method 602 compounds including 
benzene, toluene, ethylbenzene, total xylenes, methyl tert‐butyl ether, diisopropyl ether, and naphthalene. 
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7.0　　R各MARKS
The recommendations contained in this ｢epo直rep｢esent Antea USA of No直h Carolina, ~nc･′s p｢ofessionai opinions
based upon the currently available information and are arrived at in ac∞｢dance with currently accepted professional
standa｢ds･丁his ｢ep〇両s based upon a spec楯c scope of work requested by the client.The contract between Antea
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that contract o｢ out=ned in this ｢epo巾were pe血｢med･丁his ｢ep〇両s intended oniy for the use ofAntea USA of No忙h
Ca｢oiina′ Inc･′s client and anyone eise specific訓y identified in writing b∨ Antea USA of No直h Ca｢o=na, Inc. as a user of
this ｢epo巾Antea USA of No直h Ca｢oiina′ inc･ w川n｡t and cannot be =able for unautho｢ized ｢e=ance by any other
third pa叫･ Other than as contained in this pa｢ag｢aph′ Antea USA of No軸Carolina, Inc･ makes no express o｢ imp=ed
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www.anteag｢oup.com
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 
www.anteagroup.com 
Tables 
Table 1 Water Supply Well Information 
Table 2 Groundwater Elevation Data 
Table 3 Groundwater Analytical Data 
Map ID/ 
Well 
Number
Property Location Owner Address Property Owner Well Use
Connected To 
Municipal 
Water System
Well Depth
(ft. BGS)
Type of 
Well
Well Casing 
Depth
(ft. BGS)
Approximate 
Distance of Well 
from Source Area of 
Release (ft.)
WSW‐1 65 Arnett Road      
Banner Elk, NC 28604
55 Paupers Ridge Road
Banner Elk, NC 28604
Norwood Family 
Limited Partnership Potable No Unknown Unknown Unknown 250 East
WSW‐3 55 Paupers Ridge Road
Banner Elk, NC 28604
55 Paupers Ridge Road
Banner Elk, NC 28604 Bettie Norwood Potable No Unknown Drilled Unknown 420 Northwest
WSW‐4 3071 Tynecastle Hwy 
Banner Elk, NC 28604
PO Box 1175
Banner Elk, NC 28604
Banner Elk Sports 
Properties, LLC Potable No Unknown Drilled Unknown 250 Southeast
TABLE 1
Water Supply Well Information
GPM 3089 (Former Scotchman #89)
3045 Tynecastle Highway, Banner Elk, NC
Incident No. 28327
Page 1 of 1
Well ID Date Top‐of‐Casing Elevation
(Feet)
Depth to Water from TOC
(Feet)
Assumed Groundwater 
Elevation
(Feet)
Well Depth (Feet)Well Screen Interval
(Feet)
MW‐1 1/26/16 99.58 7.05 92.53 19 4‐19
MW‐1D 1/26/16 99.11 6.31 92.80 40 35‐40
MW‐2 1/26/16 97.99 13.45 84.54 20 5‐20
MW‐3R 1/26/16 96.31 6.60 89.71 14 4‐14
MW‐4 1/26/16 99.68 NG NG 20 5‐20
MW‐5 1/26/16 98.70 7.50 91.20 20 5‐20
MW‐6 1/26/16 100.88 6.43 94.45 15 5‐15
Notes
Top‐of‐casing (TOC) elevations are based on an arbitrary benchmark elevation of 100.00 feet above mean sea level.
NG ‐ Monitoring well could not be located and was not gauged
GPM 3089 (Former Scotchman #89)
Groundwater Elevation Data
TABLE 2
Incident No. 28327
3045 Tynecastle Highway, Banner Elk, NC
Page 1 of 1
Well ID Date Benzene 
(μg/L)
Ethylbenzene 
(μg/L)
Isopropyl Ether
(μg/L)
Lead 
(μg/L)
Methy Tert‐Butyl 
Ether 
(μg/L)
Toluene 
(μg/L)
Total Xylenes 
(μg/L)
1 600 70 15 20 600 500
5,000 84,500 25,000 15,000 20,000 260,000 85,500
MW‐1 1/26/2016 0.390 J < 0.0920 U 0.430 J NA 44.1 < 0.0570 U < 0.122 U
MW‐1D 1/26/2016 < 0.119 U < 0.0920 U < 0.0920 U NA < 0.169 U < 0.0570 U < 0.122 U
MW‐2 1/26/2016 < 0.119 U < 0.0920 U < 0.0920 U NA < 0.169 U < 0.0570 U < 0.122 U
MW‐3R 1/26/2016 1.30 2.18 8.91 NA 30.1 0.100 J 1.11
MW‐4 1/26/2016 NS NS NS NS NS NS NS
MW‐5 1/26/2016 < 0.119 U < 0.0920 U < 0.0920 U NA 1.59 < 0.0570 U < 0.122 U
MW‐6 1/26/2016 < 0.119 U < 0.0920 U < 0.0920 U NA < 0.169 U < 0.0570 U < 0.122 U
WSW‐1 6/22/2016 < 0.119 U < 0.0920 U < 0.0920 U <3.30 U < 0.169 U < 0.0570 U <0.180 U
WSW‐3 6/22/2016 < 0.119 U < 0.0920 U < 0.0920 U <3.30 U < 0.169 U < 0.0570 U <0.180 U
WSW‐4 1/26/2016 < 0.119 U < 0.0920 U < 0.0980 U NA < 0.169 U < 0.0570 U < 0.122 U
Notes
Bold/Highlighted ‐ Concentration exceeds applicable groundwater quality standard
2L Standard ‐ North Carolina Administrative Code 2L Groundwater Quality Standard
GCL ‐ Gross Contamination Levels for Groundwater (NCDEQ Guidelines for Assessment and Corrective Action for UST Releases)
NS ‐ Monitoring well could not be located and was not sampled
< ‐ Denotes analytical result below laboratory method detection limit
ug/L ‐ Micrograms per liter
J ‐ Indicates estimated concentration between laboratory report limit and method detection limit
U ‐ Concentration is below laboratory method detection limit
NA ‐ Sample not analyzed for specified analyte
TABLE 3
2L Standard
GCL
3045 Tynecastle Highway, Banner Elk, NC
Groundwater Analytical Data
GPM 3089
Incident No. 28327
Page 1 of 1
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 

   www.anteagroup.com 

Figures 

Figure 1 Site Location Map 
Figure 2 Site Map 
Figure 3 Shallow Groundwater Contour Map 
PROJECT NO: NC30891601 
DATE: 2/8/2017
SCALE: NTS
DRAWN BY: MHH
Source: Valle Crucis, NC;  Valle Crucis Quadrangle (7.5 Minute), USGS, 2013 CHECKED BY: KS
3530 Toringdon Way, Suite 106
Charlotte, North Carolina 28227
FIGURE 1 ‐ SITE LOCATION MAP
GPM 3089 (Former Scotchman #89)
3045 Tynecastle Highway
Banner Elk, North Carolina
N
SITE LOCATION
PROJECT NO: NC30891601 
DATE: 2/26/2016
SCALE: NTS
DRAWN BY: ME
CHECKED BY: KAS Charlotte, North Carolina 28227
3530 Toringdon Way, Suite 106
FIGURE 2 ‐ SITE MAP
GPM 3089 
3045 Tynecastle Highway
Banner Elk, Avery County, North Carolina
Legend
Approximate Monitoring Well  Location
(Type II & Type III)
Approximate Water Supply Well Location
MW‐6
MW‐3R
MW‐2
WSW‐3
WSW‐4
WSW‐1
MW‐5
MW‐1/1D
PROJECT NO: NC30891601 
DATE: 2/26/2016
SCALE: As Shown
DRAWN BY: ME
CHECKED BY: KAS
FIGURE 3 ‐ SHALLOW GROUNDWATER 
CONTOUR MAP
GPM 3089 
3045 Tynecastle Highway 3530 Toringdon Way, Suite 106
Banner Elk, Avery County, North Carolina Charlotte, North Carolina 28227
Legend
Approximate Deep Monitoring Well Location with 
Groundwater Elevation (not used in contouring)             
Approximate Shallow Monitoring Well Location with          
Groundwater Elevation                                                                    
Groundwater Contour Line (Feet)
MW‐6
94.45
84.54
MW‐2
84.54
MW‐5
91.20
MW‐1
92.53
MW‐3R
89.71
MW‐1D
92.80
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 

   www.anteagroup.com 

Appendix A 

Groundwater Sampling Records 
2016 Annual Groundwater Monitoring Report 
GPM 3089 (Former Scotchman #89) 
Banner Elk, Avery County, North Carolina 
Antea USA of NC Project No. NC30891601 

   www.anteagroup.com 

Appendix B 

Laboratory Analytical Reports and Chain‐of‐Custody Records 
Analytical Report
A6F0123
Project
GPM 3089
Project Number
[none]
June 30, 2016
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
Charlotte, North Carolina 28277
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
Page 1 of 20
6017 Financial Drive Phone #:[phone]
Website:www.ftsanalytical.comNorcross, GA 30071
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
June 30, 2016
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
Kyle Sorensen
RE: GPM 3089
We are reporting the results of the analyses performed on the samples recieved on 6/23/2016 under the
project name referenced above and identified as the lab Work Order A6F0123. All results being reported
under this Report apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontracted lab, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reporting using all other available quality control methods.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed
for at least 5 years in our archives after which time it will be destroyed without further notice, unless
otherwise agreed upon. The samples received, and described as recorded in Work Order A6F0123 will be
filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise
agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard
practices, controlled/regulated substances, etc.)
We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions
concerning this report, please do not hesitate to contact us at any time. We will be happy to help.
Charlotte, North Carolina 28277
Sincerely,
J. Derek Rounsley
Project Manager
Page 2 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Samples in this Report
Sample Lab ID Matrix Date Sampled Date Received
WSW-1 WaterA6F0123-01 23-Jun-2016 09:3822-Jun-2016 09:00
WSW-3 WaterA6F0123-02 23-Jun-2016 09:3822-Jun-2016 09:15
Page 3 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 3 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Analysis Case Narrative

SM6200B
B6F0618
The percent recovery of the Blank Spike, Blank Spike Duplicate was above QC limits for Tetrachloroethene. There were no
detectable concentrations reported in the associated samples.
Samples affected: A6F0123-01, -02.
Page 4 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 4 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Hits Summary
Sample:
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID:
Page 5 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 5 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Sample Results

ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6F0123-01 (Water)
Client Sample ID: WSW-1
RL Dil Date Prepared
Sampled: 6/22/16 9:00
CAS #
Total Metal Analysis by Method 6010C
10.0 ug/L3.30 13.30 U 6/27/16 13:416/27/16 8:41 7439-92-1Lead
VOCs by NC Method 6200B
1.00 ug/L0.180 10.180 U 6/24/16 12:296/24/16 7:53 630-20-61,1,1,2-Tetrachloroethane
0.500 ug/L0.0760 10.0760 U 6/24/16 12:296/24/16 7:53 71-55-61,1,1-Trichloroethane
0.500 ug/L0.0700 10.0700 U 6/24/16 12:296/24/16 7:53 79-34-51,1,2,2-Tetrachloroethane
0.500 ug/L0.113 10.113 U 6/24/16 12:296/24/16 7:53 79-00-51,1,2-Trichloroethane
0.500 ug/L0.121 10.121 U 6/24/16 12:296/24/16 7:53 75-34-31,1-Dichloroethane
0.500 ug/L0.104 10.104 U 6/24/16 12:296/24/16 7:53 75-35-41,1-Dichloroethene
0.500 ug/L0.0600 10.0600 U 6/24/16 12:296/24/16 7:53 563-58-61,1-Dichloropropene
2.00 ug/L0.118 10.118 U 6/24/16 12:296/24/16 7:53 87-61-61,2,3-Trichlorobenzene
1.00 ug/L0.138 10.138 U 6/24/16 12:296/24/16 7:53 96-18-41,2,3-Trichloropropane
1.00 ug/L0.0690 10.0690 U 6/24/16 12:296/24/16 7:53 120-82-11,2,4-Trichlorobenzene
0.500 ug/L0.103 10.103 U 6/24/16 12:296/24/16 7:53 95-63-61,2,4-Trimethylbenzene
1.00 ug/L0.180 10.180 U 6/24/16 12:296/24/16 7:53 106-93-41,2-Dibromoethane (EDB)
0.500 ug/L0.0940 10.0940 U 6/24/16 12:296/24/16 7:53 95-50-11,2-Dichlorobenzene
0.500 ug/L0.0900 10.0900 U 6/24/16 12:296/24/16 7:53 107-06-21,2-Dichloroethane
0.500 ug/L0.122 10.122 U 6/24/16 12:296/24/16 7:53 78-87-51,2-Dichloropropane
0.500 ug/L0.0870 10.0870 U 6/24/16 12:296/24/16 7:53 108-67-81,3,5-trimethylbenzene
0.500 ug/L0.0980 10.0980 U 6/24/16 12:296/24/16 7:53 541-73-11,3-Dichlorobenzene
0.500 ug/L0.133 10.133 U 6/24/16 12:296/24/16 7:53 142-28-91,3-Dichloropropane
0.500 ug/L0.0670 10.0670 U 6/24/16 12:296/24/16 7:53 106-46-71,4-Dichlorobenzene
0.200 ug/L0.0970 10.0970 U 6/24/16 12:296/24/16 7:53 590-20-72,2-Dichloropropane
20.0 ug/L0.378 10.378 U 6/24/16 12:296/24/16 7:53 78-93-32-Butanone (MEK)
0.200 ug/L0.0880 10.0880 U 6/24/16 12:296/24/16 7:53 95-49-82-Chlorotoluene
5.00 ug/L0.352 10.352 U 6/24/16 12:296/24/16 7:53 591-78-62-Hexanone
0.500 ug/L0.0900 10.0900 U 6/24/16 12:296/24/16 7:53 106-43-44-Chlorotoluene
0.500 ug/L0.0890 10.0890 U 6/24/16 12:296/24/16 7:53 99-87-64-Isopropyltoluene (p-Cymene)
5.00 ug/L0.253 10.253 U 6/24/16 12:296/24/16 7:53 108-10-14-Methyl-2-pentanone (MIBK)
5.00 ug/L0.352 10.352 U 6/24/16 12:296/24/16 7:53 67-64-1Acetone
0.500 ug/L0.119 10.119 U 6/24/16 12:296/24/16 7:53 71-43-2Benzene
0.500 ug/L0.132 10.132 U 6/24/16 12:296/24/16 7:53 108-86-1Bromobenzene
0.500 ug/L0.112 10.112 U 6/24/16 12:296/24/16 7:53 74-97-5Bromochloromethane
0.500 ug/L0.124 10.124 U 6/24/16 12:296/24/16 7:53 75-27-4Bromodichloromethane
2.00 ug/L0.159 10.159 U 6/24/16 12:296/24/16 7:53 75-25-2Bromoform
1.00 ug/L0.0970 10.0970 U 6/24/16 12:296/24/16 7:53 74-83-9Bromomethane (Methyl Bromide)
0.500 ug/L0.0990 10.0990 U 6/24/16 12:296/24/16 7:53 56-23-5Carbon Tetrachloride
0.500 ug/L0.105 10.105 U 6/24/16 12:296/24/16 7:53 108-90-7Chlorobenzene
0.500 ug/L0.0420 10.0420 U 6/24/16 12:296/24/16 7:53 75-00-3Chloroethane
0.500 ug/L0.172 10.172 U 6/24/16 12:296/24/16 7:53 67-66-3Chloroform
0.500 ug/L0.0850 10.0850 U 6/24/16 12:296/24/16 7:53 74-87-3Chloromethane (Methyl Chloride)
Page 6 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 6 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6F0123-01 (Water)
Client Sample ID: WSW-1 (Continued)
RL Dil Date Prepared
Sampled: 6/22/16 9:00
CAS #
VOCs by NC Method 6200B (Continued)
0.500 ug/L0.114 10.114 U 6/24/16 12:296/24/16 7:53 156-59-4cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 6/24/16 12:296/24/16 7:53 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.177 10.177 U 6/24/16 12:296/24/16 7:53 124-48-1Dibromochloromethane
0.500 ug/L0.0670 10.0670 U 6/24/16 12:296/24/16 7:53 75-71-8Dichlorodifluoromethane
50.0 ug/L3.00 13.00 U 6/24/16 12:296/24/16 7:53 64-17-5Ethanol
0.500 ug/L0.0920 10.0920 U 6/24/16 12:296/24/16 7:53 100-41-4Ethylbenzene
5.00 ug/L0.0920 10.0920 U 6/24/16 12:296/24/16 7:53 108-20-3Isopropyl Ether
0.500 ug/L0.0980 10.0980 U 6/24/16 12:296/24/16 7:53 98-82-8isopropylbenzene
1.00 ug/L0.169 10.169 U 6/24/16 12:296/24/16 7:53 1634-04-4Methyl tert-butyl ether (MTBE)
0.500 ug/L0.190 10.190 U 6/24/16 12:296/24/16 7:53 75-09-2Methylene Chloride
2.00 ug/L0.0940 10.0940 U 6/24/16 12:296/24/16 7:53 91-20-3Naphthalene
2.00 ug/L0.0600 10.0600 U 6/24/16 12:296/24/16 7:53 104-51-8n-Butylbenzene
1.00 ug/L0.0650 10.0650 U 6/24/16 12:296/24/16 7:53 103-65-1n-Propylbenzene
0.500 ug/L0.0920 10.0920 U 6/24/16 12:296/24/16 7:53 135-98-8Sec-Butylbenzene
0.500 ug/L0.0740 10.0740 U 6/24/16 12:296/24/16 7:53 100-42-5Styrene
0.500 ug/L0.0890 10.0890 U 6/24/16 12:296/24/16 7:53 98-06-6tert-Butylbenzene
0.500 ug/L0.0540 10.0540 U, H 6/24/16 12:296/24/16 7:53 127-18-4Tetrachloroethylene
0.500 ug/L0.0570 10.0570 U 6/24/16 12:296/24/16 7:53 108-88-3Toluene
0.500 ug/L0.188 10.188 U 6/24/16 12:296/24/16 7:53 156-60-5trans-1,2-dichloroethene
1.00 ug/L0.110 10.110 U 6/24/16 12:296/24/16 7:53 1006-10-26trans-1,3-dichloropropene
0.500 ug/L0.139 10.139 U 6/24/16 12:296/24/16 7:53 79-01-6Trichloroethylene
0.500 ug/L0.0540 10.0540 U 6/24/16 12:296/24/16 7:53 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 6/24/16 12:296/24/16 7:53 108-05-4Vinyl Acetate
0.500 ug/L0.0810 10.0810 U 6/24/16 12:296/24/16 7:53 75-01-4Vinyl Chloride
1.00 ug/L0.176 10.176 U 6/24/16 12:296/24/16 7:53 179601-23-1m,p-Xylenes
0.500 ug/L0.122 10.122 U 6/24/16 12:296/24/16 7:53 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 6/24/16 12:296/24/16 7:53 1330-20-7Total Xylenes
Surrogate: 1,2-Dichloroethane-D4 (SUR)65-12694%6/24/16 12:29 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)86-111101%6/24/16 12:29 460-00-4
Surrogate: Toluene-D8 (SUR)83-11696%6/24/16 12:29 2037-26-5
Page 7 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 7 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6F0123-02 (Water)
Client Sample ID: WSW-3
RL Dil Date Prepared
Sampled: 6/22/16 9:15
CAS #
Total Metal Analysis by Method 6010C
10.0 ug/L3.30 13.30 U 6/27/16 13:436/27/16 8:41 7439-92-1Lead
VOCs by NC Method 6200B
1.00 ug/L0.180 10.180 U 6/24/16 13:016/24/16 7:53 630-20-61,1,1,2-Tetrachloroethane
0.500 ug/L0.0760 10.0760 U 6/24/16 13:016/24/16 7:53 71-55-61,1,1-Trichloroethane
0.500 ug/L0.0700 10.0700 U 6/24/16 13:016/24/16 7:53 79-34-51,1,2,2-Tetrachloroethane
0.500 ug/L0.113 10.113 U 6/24/16 13:016/24/16 7:53 79-00-51,1,2-Trichloroethane
0.500 ug/L0.121 10.121 U 6/24/16 13:016/24/16 7:53 75-34-31,1-Dichloroethane
0.500 ug/L0.104 10.104 U 6/24/16 13:016/24/16 7:53 75-35-41,1-Dichloroethene
0.500 ug/L0.0600 10.0600 U 6/24/16 13:016/24/16 7:53 563-58-61,1-Dichloropropene
2.00 ug/L0.118 10.118 U 6/24/16 13:016/24/16 7:53 87-61-61,2,3-Trichlorobenzene
1.00 ug/L0.138 10.138 U 6/24/16 13:016/24/16 7:53 96-18-41,2,3-Trichloropropane
1.00 ug/L0.0690 10.0690 U 6/24/16 13:016/24/16 7:53 120-82-11,2,4-Trichlorobenzene
0.500 ug/L0.103 10.103 U 6/24/16 13:016/24/16 7:53 95-63-61,2,4-Trimethylbenzene
1.00 ug/L0.180 10.180 U 6/24/16 13:016/24/16 7:53 106-93-41,2-Dibromoethane (EDB)
0.500 ug/L0.0940 10.0940 U 6/24/16 13:016/24/16 7:53 95-50-11,2-Dichlorobenzene
0.500 ug/L0.0900 10.0900 U 6/24/16 13:016/24/16 7:53 107-06-21,2-Dichloroethane
0.500 ug/L0.122 10.122 U 6/24/16 13:016/24/16 7:53 78-87-51,2-Dichloropropane
0.500 ug/L0.0870 10.0870 U 6/24/16 13:016/24/16 7:53 108-67-81,3,5-trimethylbenzene
0.500 ug/L0.0980 10.0980 U 6/24/16 13:016/24/16 7:53 541-73-11,3-Dichlorobenzene
0.500 ug/L0.133 10.133 U 6/24/16 13:016/24/16 7:53 142-28-91,3-Dichloropropane
0.500 ug/L0.0670 10.0670 U 6/24/16 13:016/24/16 7:53 106-46-71,4-Dichlorobenzene
0.200 ug/L0.0970 10.0970 U 6/24/16 13:016/24/16 7:53 590-20-72,2-Dichloropropane
20.0 ug/L0.378 10.378 U 6/24/16 13:016/24/16 7:53 78-93-32-Butanone (MEK)
0.200 ug/L0.0880 10.0880 U 6/24/16 13:016/24/16 7:53 95-49-82-Chlorotoluene
5.00 ug/L0.352 10.352 U 6/24/16 13:016/24/16 7:53 591-78-62-Hexanone
0.500 ug/L0.0900 10.0900 U 6/24/16 13:016/24/16 7:53 106-43-44-Chlorotoluene
0.500 ug/L0.0890 10.0890 U 6/24/16 13:016/24/16 7:53 99-87-64-Isopropyltoluene (p-Cymene)
5.00 ug/L0.253 10.253 U 6/24/16 13:016/24/16 7:53 108-10-14-Methyl-2-pentanone (MIBK)
5.00 ug/L0.352 10.352 U 6/24/16 13:016/24/16 7:53 67-64-1Acetone
0.500 ug/L0.119 10.119 U 6/24/16 13:016/24/16 7:53 71-43-2Benzene
0.500 ug/L0.132 10.132 U 6/24/16 13:016/24/16 7:53 108-86-1Bromobenzene
0.500 ug/L0.112 10.112 U 6/24/16 13:016/24/16 7:53 74-97-5Bromochloromethane
0.500 ug/L0.124 10.124 U 6/24/16 13:016/24/16 7:53 75-27-4Bromodichloromethane
2.00 ug/L0.159 10.159 U 6/24/16 13:016/24/16 7:53 75-25-2Bromoform
1.00 ug/L0.0970 10.0970 U 6/24/16 13:016/24/16 7:53 74-83-9Bromomethane (Methyl Bromide)
0.500 ug/L0.0990 10.0990 U 6/24/16 13:016/24/16 7:53 56-23-5Carbon Tetrachloride
0.500 ug/L0.105 10.105 U 6/24/16 13:016/24/16 7:53 108-90-7Chlorobenzene
0.500 ug/L0.0420 10.0420 U 6/24/16 13:016/24/16 7:53 75-00-3Chloroethane
0.500 ug/L0.172 10.172 U 6/24/16 13:016/24/16 7:53 67-66-3Chloroform
0.500 ug/L0.0850 10.0850 U 6/24/16 13:016/24/16 7:53 74-87-3Chloromethane (Methyl Chloride)
0.500 ug/L0.114 10.114 U 6/24/16 13:016/24/16 7:53 156-59-4cis-1,2-Dichloroethene
Page 8 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 8 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: A6F0123-02 (Water)
Client Sample ID: WSW-3 (Continued)
RL Dil Date Prepared
Sampled: 6/22/16 9:15
CAS #
VOCs by NC Method 6200B (Continued)
1.00 ug/L0.100 10.100 U 6/24/16 13:016/24/16 7:53 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.177 10.177 U 6/24/16 13:016/24/16 7:53 124-48-1Dibromochloromethane
0.500 ug/L0.0670 10.0670 U 6/24/16 13:016/24/16 7:53 75-71-8Dichlorodifluoromethane
50.0 ug/L3.00 13.00 U 6/24/16 13:016/24/16 7:53 64-17-5Ethanol
0.500 ug/L0.0920 10.0920 U 6/24/16 13:016/24/16 7:53 100-41-4Ethylbenzene
5.00 ug/L0.0920 10.0920 U 6/24/16 13:016/24/16 7:53 108-20-3Isopropyl Ether
0.500 ug/L0.0980 10.0980 U 6/24/16 13:016/24/16 7:53 98-82-8isopropylbenzene
1.00 ug/L0.169 10.169 U 6/24/16 13:016/24/16 7:53 1634-04-4Methyl tert-butyl ether (MTBE)
0.500 ug/L0.190 10.190 U 6/24/16 13:016/24/16 7:53 75-09-2Methylene Chloride
2.00 ug/L0.0940 10.0940 U 6/24/16 13:016/24/16 7:53 91-20-3Naphthalene
2.00 ug/L0.0600 10.0600 U 6/24/16 13:016/24/16 7:53 104-51-8n-Butylbenzene
1.00 ug/L0.0650 10.0650 U 6/24/16 13:016/24/16 7:53 103-65-1n-Propylbenzene
0.500 ug/L0.0920 10.0920 U 6/24/16 13:016/24/16 7:53 135-98-8Sec-Butylbenzene
0.500 ug/L0.0740 10.0740 U 6/24/16 13:016/24/16 7:53 100-42-5Styrene
0.500 ug/L0.0890 10.0890 U 6/24/16 13:016/24/16 7:53 98-06-6tert-Butylbenzene
0.500 ug/L0.0540 10.0540 U, H 6/24/16 13:016/24/16 7:53 127-18-4Tetrachloroethylene
0.500 ug/L0.0570 10.0570 U 6/24/16 13:016/24/16 7:53 108-88-3Toluene
0.500 ug/L0.188 10.188 U 6/24/16 13:016/24/16 7:53 156-60-5trans-1,2-dichloroethene
1.00 ug/L0.110 10.110 U 6/24/16 13:016/24/16 7:53 1006-10-26trans-1,3-dichloropropene
0.500 ug/L0.139 10.139 U 6/24/16 13:016/24/16 7:53 79-01-6Trichloroethylene
0.500 ug/L0.0540 10.0540 U 6/24/16 13:016/24/16 7:53 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 6/24/16 13:016/24/16 7:53 108-05-4Vinyl Acetate
0.500 ug/L0.0810 10.0810 U 6/24/16 13:016/24/16 7:53 75-01-4Vinyl Chloride
1.00 ug/L0.176 10.176 U 6/24/16 13:016/24/16 7:53 179601-23-1m,p-Xylenes
0.500 ug/L0.122 10.122 U 6/24/16 13:016/24/16 7:53 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 6/24/16 13:016/24/16 7:53 1330-20-7Total Xylenes
Surrogate: 1,2-Dichloroethane-D4 (SUR)65-12693%6/24/16 13:01 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)86-111111%6/24/16 13:01 460-00-4
Surrogate: Toluene-D8 (SUR)83-11694%6/24/16 13:01 2037-26-5
Page 9 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 9 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
VOCs by NC Method 6200B
MDL
Batch: B6F0618
Prepared & Analyzed: 6/24/2016Blank (B6F0618-BLK1)
1.00 ug/L0.180 U 0.1801,1,1,2-Tetrachloroethane
0.500 ug/L0.0760 U 0.07601,1,1-Trichloroethane
0.500 ug/L0.0700 U 0.07001,1,2,2-Tetrachloroethane
0.500 ug/L0.113 U 0.1131,1,2-Trichloroethane
0.500 ug/L0.121 U 0.1211,1-Dichloroethane
0.500 ug/L0.104 U 0.1041,1-Dichloroethene
0.500 ug/L0.0600 U 0.06001,1-Dichloropropene
2.00 ug/L0.118 U 0.1181,2,3-Trichlorobenzene
1.00 ug/L0.138 U 0.1381,2,3-Trichloropropane
1.00 ug/L0.0690 U 0.06901,2,4-Trichlorobenzene
0.500 ug/L0.103 U 0.1031,2,4-Trimethylbenzene
1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB)
0.500 ug/L0.0940 U 0.09401,2-Dichlorobenzene
0.500 ug/L0.0900 U 0.09001,2-Dichloroethane
0.500 ug/L0.122 U 0.1221,2-Dichloropropane
0.500 ug/L0.0870 U 0.08701,3,5-trimethylbenzene
0.500 ug/L0.0980 U 0.09801,3-Dichlorobenzene
0.500 ug/L0.133 U 0.1331,3-Dichloropropane
0.500 ug/L0.0670 U 0.06701,4-Dichlorobenzene
0.200 ug/L0.0970 U 0.09702,2-Dichloropropane
20.0 ug/L0.378 U 0.3782-Butanone (MEK)
0.200 ug/L0.0880 U 0.08802-Chlorotoluene
5.00 ug/L0.352 U 0.3522-Hexanone
0.500 ug/L0.0900 U 0.09004-Chlorotoluene
0.500 ug/L0.0890 U 0.08904-Isopropyltoluene (p-Cymene)
5.00 ug/L0.253 U 0.2534-Methyl-2-pentanone (MIBK)
5.00 ug/L0.352 U 0.352Acetone
0.500 ug/L0.119 U 0.119Benzene
0.500 ug/L0.132 U 0.132Bromobenzene
0.500 ug/L0.112 U 0.112Bromochloromethane
0.500 ug/L0.124 U 0.124Bromodichloromethane
2.00 ug/L0.159 U 0.159Bromoform
1.00 ug/L0.0970 U 0.0970Bromomethane (Methyl Bromide)
0.500 ug/L0.0990 U 0.0990Carbon Tetrachloride
0.500 ug/L0.105 U 0.105Chlorobenzene
0.500 ug/L0.0420 U 0.0420Chloroethane
0.500 ug/L0.172 U 0.172Chloroform
0.500 ug/L0.0850 U 0.0850Chloromethane (Methyl Chloride)
0.500 ug/L0.114 U 0.114cis-1,2-Dichloroethene
1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene
1.00 ug/L0.177 U 0.177Dibromochloromethane
Page 10 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 10 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016Blank (B6F0618-BLK1)
0.500 ug/L0.0670 U 0.0670Dichlorodifluoromethane
50.0 ug/L3.00 U 3.00Ethanol
0.500 ug/L0.0920 U 0.0920Ethylbenzene
5.00 ug/L0.0920 U 0.0920Isopropyl Ether
0.500 ug/L0.0980 U 0.0980isopropylbenzene
1.00 ug/L0.169 U 0.169Methyl tert-butyl ether (MTBE)
0.500 ug/L0.190 U 0.190Methylene Chloride
2.00 ug/L0.0940 U 0.0940Naphthalene
2.00 ug/L0.0600 U 0.0600n-Butylbenzene
1.00 ug/L0.0650 U 0.0650n-Propylbenzene
0.500 ug/L0.0920 U 0.0920Sec-Butylbenzene
0.500 ug/L0.0740 U 0.0740Styrene
0.500 ug/L0.0890 U 0.0890tert-Butylbenzene
0.500 ug/L0.0540 U 0.0540Tetrachloroethylene
0.500 ug/L0.0570 U 0.0570Toluene
0.500 ug/L0.188 U 0.188trans-1,2-dichloroethene
1.00 ug/L0.110 U 0.110trans-1,3-dichloropropene
0.500 ug/L0.139 U 0.139Trichloroethylene
0.500 ug/L0.0540 U 0.0540Trichlorofluoromethane
1.00 ug/L0.720 U 0.720Vinyl Acetate
0.500 ug/L0.0810 U 0.0810Vinyl Chloride
1.00 ug/L0.176 U 0.176m,p-Xylenes
0.500 ug/L0.122 U 0.122o-Xylene
1.00 ug/L0.180 U 0.180Total Xylenes
25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)9323.2 ug/L
25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)10225.6 ug/L
25.0 83-116Surrogate: Toluene-D8 (SUR)9624.0 ug/L
Page 11 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 11 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016LCS (B6F0618-BS1)
1.00 25.0 70-130101ug/L25.3 0.1801,1,1,2-Tetrachloroethane
0.500 25.0 70-130106ug/L26.5 0.07601,1,1-Trichloroethane
0.500 25.0 70-13098ug/L24.4 0.07001,1,2,2-Tetrachloroethane
0.500 25.0 70-130109ug/L27.2 0.1131,1,2-Trichloroethane
0.500 25.0 70-130111ug/L27.7 0.1211,1-Dichloroethane
0.500 25.0 70-130107ug/L26.8 0.1041,1-Dichloroethene
0.500 25.0 70-130110ug/L27.4 0.06001,1-Dichloropropene
2.00 25.0 70-13097ug/L24.3 0.1181,2,3-Trichlorobenzene
1.00 25.0 70-13099ug/L24.7 0.1381,2,3-Trichloropropane
1.00 25.0 70-13096ug/L23.9 0.06901,2,4-Trichlorobenzene
0.500 25.0 70-13095ug/L23.7 0.1031,2,4-Trimethylbenzene
1.00 25.0 70-130107ug/L26.7 0.1801,2-Dibromoethane (EDB)
0.500 25.0 70-13096ug/L23.9 0.09401,2-Dichlorobenzene
0.500 25.0 70-13091ug/L22.8 0.09001,2-Dichloroethane
0.500 25.0 70-130106ug/L26.6 0.1221,2-Dichloropropane
0.500 25.0 70-13096ug/L24.0 0.08701,3,5-trimethylbenzene
0.500 25.0 70-13096ug/L23.9 0.09801,3-Dichlorobenzene
0.500 25.0 70-130104ug/L26.1 0.1331,3-Dichloropropane
0.500 25.0 70-13094ug/L23.4 0.06701,4-Dichlorobenzene
0.200 25.0 70-130108ug/L27.1 0.09702,2-Dichloropropane
20.0 50.0 70-130117ug/L58.7 0.3782-Butanone (MEK)
0.200 25.0 70-13095ug/L23.7 0.08802-Chlorotoluene
5.00 50.0 70-130108ug/L53.9 0.3522-Hexanone
0.500 25.0 70-13096ug/L23.9 0.09004-Chlorotoluene
0.500 25.0 70-13095ug/L23.6 0.08904-Isopropyltoluene (p-Cymene)
5.00 50.0 70-13094ug/L47.0 0.2534-Methyl-2-pentanone (MIBK)
5.00 50.0 70-130105ug/L52.4 0.352Acetone
0.500 25.0 70-130105ug/L26.3 0.119Benzene
0.500 25.0 70-13097ug/L24.2 0.132Bromobenzene
0.500 25.0 70-130117ug/L29.3 0.112Bromochloromethane
0.500 25.0 70-130107ug/L26.6 0.124Bromodichloromethane
2.00 25.0 70-130102ug/L25.4 0.159Bromoform
1.00 25.0 60-140109ug/L27.2 0.0970Bromomethane (Methyl Bromide)
0.500 25.0 70-130107ug/L26.7 0.0990Carbon Tetrachloride
0.500 25.0 70-13099ug/L24.8 0.105Chlorobenzene
0.500 25.0 60-140123ug/L30.6 0.0420Chloroethane
0.500 25.0 70-130113ug/L28.2 0.172Chloroform
0.500 25.0 60-140100ug/L25.1 0.0850Chloromethane (Methyl Chloride)
0.500 25.0 70-130114ug/L28.5 0.114cis-1,2-Dichloroethene
1.00 25.0 70-130110ug/L27.4 0.100cis-1,3-Dichloropropene
1.00 25.0 70-130106ug/L26.6 0.177Dibromochloromethane
Page 12 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 12 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016LCS (B6F0618-BS1)
0.500 25.0 60-140106ug/L26.4 0.0670Dichlorodifluoromethane
50.0 1000 70-130121ug/L12103.00Ethanol
0.500 25.0 70-13099ug/L24.8 0.0920Ethylbenzene
5.00 25.0 70-130117ug/L29.2 0.0920Isopropyl Ether
0.500 25.0 70-13097ug/L24.3 0.0980isopropylbenzene
1.00 50.0 70-130118ug/L59.0 0.169Methyl tert-butyl ether (MTBE)
0.500 25.0 70-130117ug/L29.3 0.190Methylene Chloride
2.00 25.0 70-130106ug/L26.5 0.0940Naphthalene
2.00 25.0 70-13095ug/L23.6 0.0600n-Butylbenzene
1.00 25.0 70-13097ug/L24.3 0.0650n-Propylbenzene
0.500 25.0 70-13094ug/L23.6 0.0920Sec-Butylbenzene
0.500 25.0 70-130102ug/L25.6 0.0740Styrene
0.500 25.0 70-13095ug/L23.8 0.0890tert-Butylbenzene
0.500 25.0 70-130163ug/L40.8 X 0.0540Tetrachloroethylene
0.500 25.0 70-13099ug/L24.6 0.0570Toluene
0.500 25.0 70-130113ug/L28.3 0.188trans-1,2-dichloroethene
1.00 25.0 70-130109ug/L27.1 0.110trans-1,3-dichloropropene
0.500 25.0 70-130109ug/L27.3 0.139Trichloroethylene
0.500 25.0 60-140100ug/L24.9 0.0540Trichlorofluoromethane
1.00 25.0 70-13093ug/L23.3 0.720Vinyl Acetate
0.500 25.0 60-140108ug/L27.1 0.0810Vinyl Chloride
1.00 50.0 70-13099ug/L49.6 0.176m,p-Xylenes
0.500 25.0 70-130101ug/L25.2 0.122o-Xylene
25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)9223.0 ug/L
25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9924.8 ug/L
25.0 83-116Surrogate: Toluene-D8 (SUR)9924.8 ug/L
Prepared & Analyzed: 6/24/2016LCS Dup (B6F0618-BSD1)
1.00 25.0 2070-13096 5ug/L24.0 0.1801,1,1,2-Tetrachloroethane
0.500 25.0 2070-130109 3ug/L27.3 0.07601,1,1-Trichloroethane
0.500 25.0 2070-13096 2ug/L23.9 0.07001,1,2,2-Tetrachloroethane
0.500 25.0 2070-130103 5ug/L25.8 0.1131,1,2-Trichloroethane
0.500 25.0 2070-130111 0.04ug/L27.8 0.1211,1-Dichloroethane
0.500 25.0 2070-130103 4ug/L25.8 0.1041,1-Dichloroethene
0.500 25.0 2070-130109 1ug/L27.1 0.06001,1-Dichloropropene
2.00 25.0 2070-130100 3ug/L25.1 0.1181,2,3-Trichlorobenzene
1.00 25.0 2070-13092 7ug/L23.1 0.1381,2,3-Trichloropropane
1.00 25.0 2070-13097 1ug/L24.2 0.06901,2,4-Trichlorobenzene
0.500 25.0 2070-13092 3ug/L23.1 0.1031,2,4-Trimethylbenzene
1.00 25.0 2070-130101 5ug/L25.3 0.1801,2-Dibromoethane (EDB)
Page 13 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 13 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016LCS Dup (B6F0618-BSD1)
0.500 25.0 2070-13094 2ug/L23.5 0.09401,2-Dichlorobenzene
0.500 25.0 2070-13092 0.5ug/L22.9 0.09001,2-Dichloroethane
0.500 25.0 2070-130105 0.9ug/L26.4 0.1221,2-Dichloropropane
0.500 25.0 2070-13093 3ug/L23.3 0.08701,3,5-trimethylbenzene
0.500 25.0 2070-13095 1ug/L23.6 0.09801,3-Dichlorobenzene
0.500 25.0 2070-130102 3ug/L25.4 0.1331,3-Dichloropropane
0.500 25.0 2070-13094 0.09ug/L23.4 0.06701,4-Dichlorobenzene
0.200 25.0 2070-130107 0.8ug/L26.9 0.09702,2-Dichloropropane
20.0 50.0 2070-130115 2ug/L57.5 0.3782-Butanone (MEK)
0.200 25.0 2070-13091 4ug/L22.8 0.08802-Chlorotoluene
5.00 50.0 2070-130110 2ug/L54.8 0.3522-Hexanone
0.500 25.0 2070-13092 3ug/L23.1 0.09004-Chlorotoluene
0.500 25.0 2070-13094 0.6ug/L23.5 0.08904-Isopropyltoluene (p-Cymene)
5.00 50.0 2070-13097 3ug/L48.4 0.2534-Methyl-2-pentanone (MIBK)
5.00 50.0 2070-130108 3ug/L53.9 0.352Acetone
0.500 25.0 2070-130105 0.3ug/L26.2 0.119Benzene
0.500 25.0 2070-13093 4ug/L23.3 0.132Bromobenzene
0.500 25.0 2070-130118 1ug/L29.6 0.112Bromochloromethane
0.500 25.0 2070-130107 0.08ug/L26.6 0.124Bromodichloromethane
2.00 25.0 2070-13095 6ug/L23.8 0.159Bromoform
1.00 25.0 2060-140111 2ug/L27.8 0.0970Bromomethane (Methyl Bromide)
0.500 25.0 2070-130101 5ug/L25.3 0.0990Carbon Tetrachloride
0.500 25.0 2070-13096 3ug/L24.1 0.105Chlorobenzene
0.500 25.0 2060-140126 3ug/L31.4 0.0420Chloroethane
0.500 25.0 2070-130111 2ug/L27.8 0.172Chloroform
0.500 25.0 2060-140107 6ug/L26.7 0.0850Chloromethane (Methyl Chloride)
0.500 25.0 2070-130114 0.2ug/L28.4 0.114cis-1,2-Dichloroethene
1.00 25.0 2070-130107 3ug/L26.7 0.100cis-1,3-Dichloropropene
1.00 25.0 2070-130102 4ug/L25.5 0.177Dibromochloromethane
0.500 25.0 2060-140103 3ug/L25.8 0.0670Dichlorodifluoromethane
50.0 1000 2070-130116 4ug/L11603.00Ethanol
0.500 25.0 2070-13095 4ug/L23.8 0.0920Ethylbenzene
5.00 25.0 2070-130116 0.9ug/L29.0 0.0920Isopropyl Ether
0.500 25.0 2070-13094 3ug/L23.5 0.0980isopropylbenzene
1.00 50.0 2070-130117 0.7ug/L58.6 0.169Methyl tert-butyl ether (MTBE)
0.500 25.0 2070-130116 1ug/L28.9 0.190Methylene Chloride
2.00 25.0 2070-130113 7ug/L28.3 0.0940Naphthalene
2.00 25.0 2070-13095 1ug/L23.9 0.0600n-Butylbenzene
1.00 25.0 2070-13093 4ug/L23.3 0.0650n-Propylbenzene
0.500 25.0 2070-13093 2ug/L23.2 0.0920Sec-Butylbenzene
0.500 25.0 2070-130101 2ug/L25.2 0.0740Styrene
Page 14 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 14 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016LCS Dup (B6F0618-BSD1)
0.500 25.0 2070-13093 3ug/L23.1 0.0890tert-Butylbenzene
0.500 25.0 2070-130135 19ug/L33.8 X 0.0540Tetrachloroethylene
0.500 25.0 2070-13093 5ug/L23.4 0.0570Toluene
0.500 25.0 2070-130112 0.9ug/L28.1 0.188trans-1,2-dichloroethene
1.00 25.0 2070-130102 7ug/L25.4 0.110trans-1,3-dichloropropene
0.500 25.0 2070-130104 4ug/L26.1 0.139Trichloroethylene
0.500 25.0 2060-14099 0.9ug/L24.7 0.0540Trichlorofluoromethane
1.00 25.0 2070-130108 14ug/L26.9 0.720Vinyl Acetate
0.500 25.0 2060-140113 4ug/L28.3 0.0810Vinyl Chloride
1.00 50.0 2070-13097 2ug/L48.6 0.176m,p-Xylenes
0.500 25.0 2070-13097 4ug/L24.2 0.122o-Xylene
25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)9223.1 ug/L
25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9924.8 ug/L
25.0 83-116Surrogate: Toluene-D8 (SUR)9724.2 ug/L
Prepared & Analyzed: 6/24/2016Source: A6F0123-02Matrix Spike (B6F0618-MS1)
1.00 25.0 ND 70-130103ug/L25.7 0.1801,1,1,2-Tetrachloroethane
0.500 25.0 ND 70-130122ug/L30.4 0.07601,1,1-Trichloroethane
0.500 25.0 ND 70-130101ug/L25.3 0.07001,1,2,2-Tetrachloroethane
0.500 25.0 ND 70-130106ug/L26.6 0.1131,1,2-Trichloroethane
0.500 25.0 ND 70-130117ug/L29.3 0.1211,1-Dichloroethane
0.500 25.0 ND 70-130126ug/L31.6 0.1041,1-Dichloroethene
0.500 25.0 ND 70-130116ug/L29.1 0.06001,1-Dichloropropene
2.00 25.0 ND 70-13085ug/L21.2 0.1181,2,3-Trichlorobenzene
1.00 25.0 ND 70-130100ug/L25.1 0.1381,2,3-Trichloropropane
1.00 25.0 ND 70-13089ug/L22.4 0.06901,2,4-Trichlorobenzene
0.500 25.0 ND 70-13097ug/L24.3 0.1031,2,4-Trimethylbenzene
1.00 25.0 ND 70-130105ug/L26.2 0.1801,2-Dibromoethane (EDB)
0.500 25.0 ND 70-13096ug/L24.0 0.09401,2-Dichlorobenzene
0.500 25.0 ND 70-130107ug/L26.6 0.09001,2-Dichloroethane
0.500 25.0 ND 70-130114ug/L28.4 0.1221,2-Dichloropropane
0.500 25.0 ND 70-13098ug/L24.6 0.08701,3,5-trimethylbenzene
0.500 25.0 ND 70-130100ug/L25.0 0.09801,3-Dichlorobenzene
0.500 25.0 ND 70-130105ug/L26.1 0.1331,3-Dichloropropane
0.500 25.0 ND 70-13098ug/L24.4 0.06701,4-Dichlorobenzene
0.200 25.0 ND 70-130123ug/L30.6 0.09702,2-Dichloropropane
20.0 50.0 ND 70-130108ug/L53.8 0.3782-Butanone (MEK)
0.200 25.0 ND 70-130100ug/L25.1 0.08802-Chlorotoluene
5.00 50.0 ND 70-13095ug/L47.5 0.3522-Hexanone
0.500 25.0 ND 70-130101ug/L25.3 0.09004-Chlorotoluene
Page 15 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 15 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016Source: A6F0123-02Matrix Spike (B6F0618-MS1)
0.500 25.0 ND 70-13099ug/L24.7 0.08904-Isopropyltoluene (p-Cymene)
5.00 50.0 ND 70-13089ug/L44.3 0.2534-Methyl-2-pentanone (MIBK)
5.00 50.0 ND 70-13088ug/L43.9 0.352Acetone
0.500 25.0 ND 70-130113ug/L28.2 0.119Benzene
0.500 25.0 ND 70-130101ug/L25.2 0.132Bromobenzene
0.500 25.0 ND 70-130122ug/L30.6 0.112Bromochloromethane
0.500 25.0 ND 70-130111ug/L27.8 0.124Bromodichloromethane
2.00 25.0 ND 70-13096ug/L24.0 0.159Bromoform
1.00 25.0 ND 60-140106ug/L26.5 0.0970Bromomethane (Methyl Bromide)
0.500 25.0 ND 70-130116ug/L29.0 0.0990Carbon Tetrachloride
0.500 25.0 ND 70-130103ug/L25.6 0.105Chlorobenzene
0.500 25.0 ND 60-140124ug/L31.0 0.0420Chloroethane
0.500 25.0 ND 70-130120ug/L30.0 0.172Chloroform
0.500 25.0 ND 60-140104ug/L25.9 0.0850Chloromethane (Methyl Chloride)
0.500 25.0 ND 70-130118ug/L29.6 0.114cis-1,2-Dichloroethene
1.00 25.0 ND 70-130111ug/L27.8 0.100cis-1,3-Dichloropropene
1.00 25.0 ND 70-130104ug/L26.0 0.177Dibromochloromethane
0.500 25.0 ND 60-14093ug/L23.2 0.0670Dichlorodifluoromethane
50.0 1000 ND 70-130117ug/L11703.00Ethanol
0.500 25.0 ND 70-130101ug/L25.2 0.0920Ethylbenzene
5.00 25.0 ND 70-130117ug/L29.3 0.0920Isopropyl Ether
0.500 25.0 ND 70-130102ug/L25.6 0.0980isopropylbenzene
1.00 50.0 ND 70-130113ug/L56.4 0.169Methyl tert-butyl ether (MTBE)
0.500 25.0 ND 70-130126ug/L31.4 0.190Methylene Chloride
2.00 25.0 ND 70-13088ug/L21.9 0.0940Naphthalene
2.00 25.0 ND 70-13098ug/L24.4 0.0600n-Butylbenzene
1.00 25.0 ND 70-130102ug/L25.6 0.0650n-Propylbenzene
0.500 25.0 ND 70-13098ug/L24.4 0.0920Sec-Butylbenzene
0.500 25.0 ND 70-130108ug/L26.9 0.0740Styrene
0.500 25.0 ND 70-13099ug/L24.6 0.0890tert-Butylbenzene
0.500 25.0 ND 70-130103ug/L25.8 0.0540Tetrachloroethylene
0.500 25.0 ND 70-130104ug/L26.0 0.0570Toluene
0.500 25.0 ND 70-130122ug/L30.4 0.188trans-1,2-dichloroethene
1.00 25.0 ND 70-130105ug/L26.4 0.110trans-1,3-dichloropropene
0.500 25.0 ND 70-130114ug/L28.5 0.139Trichloroethylene
0.500 25.0 ND 60-140102ug/L25.6 0.0540Trichlorofluoromethane
1.00 25.0 ND 70-130115ug/L28.7 0.720Vinyl Acetate
0.500 25.0 ND 60-140110ug/L27.6 0.0810Vinyl Chloride
1.00 50.0 ND 70-130103ug/L51.3 0.176m,p-Xylenes
0.500 25.0 ND 70-130104ug/L26.0 0.122o-Xylene
Page 16 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 16 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
VOCs by NC Method 6200B (Continued)
MDL
Batch: B6F0618 (Continued)
Prepared & Analyzed: 6/24/2016Source: A6F0123-02Matrix Spike (B6F0618-MS1)
25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)9022.5 ug/L
25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)10225.6 ug/L
25.0 83-116Surrogate: Toluene-D8 (SUR)9824.4 ug/L
Page 17 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 17 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Total Metal Analysis by Method 6010C
MDL
Batch: B6F0602
Prepared & Analyzed: 6/27/2016Blank (B6F0602-BLK1)
10.0 ug/L3.30 U 3.30Lead
Prepared & Analyzed: 6/27/2016LCS (B6F0602-BS1)
10.0 1000 80-12096ug/L9593.30Lead
Prepared & Analyzed: 6/27/2016LCS Dup (B6F0602-BSD1)
10.0 1000 2080-12089 7ug/L8913.30Lead
Prepared & Analyzed: 6/27/2016Source: A6F0120-01Duplicate (B6F0602-DUP1)
10.0 ND 20ug/L3.30 U 3.30Lead
Prepared & Analyzed: 6/27/2016Source: A6F0120-01Matrix Spike (B6F0602-MS1)
10.0 1000 ND 80-12096ug/L9613.30Lead
Prepared & Analyzed: 6/27/2016Source: A6F0120-01Matrix Spike Dup (B6F0602-MSD1)
10.0 1000 ND 2080-12091 6ug/L9083.30Lead
Page 18 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 18 of 20
Project:
Project Number:
Project Manager:
Reported:
Antea Group Charlotte-Charlotte
3530 Toringdon Way STE 106
GPM 3089
Kyle Sorensen 6/30/16 9:15
MWBE SDBE
NELAC DoD Accredited
Charlotte, North Carolina 28277
List of Certifications for FTS Analytical Services - Atlanta
CodeDescriptionNumber ExpiresFacility
LANELAC04176LA CERTIFICATE 06/30/2016FTSA
ANC483NC CERTIFICATE 12/31/2016FTSA
KENTUKY85KENTUKY CERTIFICATE FTSA
ASC98015SC CERTIFICATE 06/30/2016FTSA
LFLNELACE84098FL NELAC CERTIFICATE 06/30/2016FTSL
AFLNELACE87429FL NELAC CERTIFICATE 06/30/2016FTSA
DODLI0-135 DoD CERTIFICATE 06/30/2016FTSA
USDAP330-07-00105 USDA CERTIFICATE FTSA
Notes and Definitions
Item Definition
The LCS data for this analytical batch was reported above the laboratory control limits.H
Dry Sample results reported on a dry weight basis.
U Analyte NOT DETECTED at or above the reporting limit.
A Suspected adol-condensation product.
B Analyte detected in the method blank.
C Confirmed by GC/MS analysis.
E Concentration exceeds calibration range.
K Hold Time exceeded.
N Tentatively Identified Compound.
P >25% difference between primary and secondary columns.
S Quantitation based on single-point calibration.
X General QC Failure see Case Narrative.
J The target analyte was positively identified below the Reporting Limit and above the Method Detection Limit.
RPD Relative Percent Difference
%REC Percent Recovery
Source Sample that was matrix spiked or duplicated.
Page 19 of 20
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 19 of 20
Page 20 of 20
Analytical Report 523803
for
Antea Group - Charlotte
Project Manager: Kyle Sorensen
GPM 3089
02-FEB-16
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400)
Xenco-San Antonio: Texas (T104704534-15-1)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Collected By: Client
Page 1 of 29 Final 1.000
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Kyle Sorensen
Antea Group - Charlotte
8008 Corporate Center Dr, Ste 100
Charlotte, NC 28226

Reference: XENCO Report No(s): 523803
GPM 3089
Project Address: NC
Kyle Sorensen:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 523803. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 523803 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
02-FEB-16
Project Manager
J. Derek Rounsley
Page 2 of 29 Final 1.000
Sample Cross Reference 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
Sample Id
MW-1
MW-1D
MW-2
MW-3R
MW-5
MW-6
WSW-4
01-26-16 11:25
01-26-16 11:10
01-26-16 10:45
01-26-16 10:35
01-26-16 11:05
01-26-16 10:25
01-26-16 12:10
Date Collected Lab Sample Id
523803-001
523803-002
523803-003
523803-004
523803-005
523803-006
523803-007
16 ft
40 ft

Sample DepthMatrix
W
W
W
W
W
W
W
Page 3 of 29 Final 1.000
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4147 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
1211 W Florida Ave, Midland, TX 79701
2525 W. Huntington Dr. - Suite 102, Tempe AZ 85282
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 4 of 29 Final 1.000
Hits Summary 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00
01.28.16 10.00
Date Received :
Date Received :
% Moisture :
% Moisture :
01.26.16 11.25
01.26.16 10.35
Date Collected :
Date Collected :
523803-001
523803-004
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW-1
MW-3R
Sample Id :
Sample Id :
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
01.31.16 13.57
01.31.16 13.57
Date Prep:
Date Prep:
Benzene
cis-1,2-Dichloroethene
Diisopropyl ether
isopropylbenzene
Methyl tert-butyl ether (MTBE)
n-Butylbenzene
n-Propylbenzene
Sec-Butylbenzene
1,2,4-Trimethylbenzene
Benzene
Diisopropyl ether
Ethylbenzene
isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether (MTBE)
n-Butylbenzene
n-Propylbenzene
Sec-Butylbenzene
Toluene
Total Xylenes
Parameter
Parameter
Result
Result
J
J
J
J
J
J
J
J
J
J
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
95-63-6
71-43-2
156-59-2
108-20-3
98-82-8
1634-04-4
104-51-8
103-65-1
135-98-8
95-63-6
71-43-2
108-20-3
100-41-4
98-82-8
179601-23-1
1634-04-4
104-51-8
103-65-1
135-98-8
108-88-3
1330-20-7
0.360
0.390
0.280
0.430
0.350
44.1
0.500
0.210
0.920
1.60
1.30
8.91
2.18
2.29
1.11
30.1
0.380
4.50
0.480
0.100
1.11
986847
986847Seq Number
16 ftSample Depth :
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
Analysis Date
Analysis Date
Page 5 of 29 Final 1.000
Hits Summary 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received :
% Moisture :
01.26.16 11.05 Date Collected : 523803-005Lab Sample Id :
Ground WaterMatrix : MW-5Sample Id :
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method :SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
Methyl tert-butyl ether (MTBE)
Parameter Result Flag
ug/L
Units
1
DilCas Number
1634-04-4 1.59
986847
01.31.16 21.15
Analysis Date
Page 6 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 11.25 Date Collected:523803-001Lab Sample Id:
Ground WaterMatrix: MW-1Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
J
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
0.360
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.390
U
U
U
U
U
U
U
U
U
U
U
0.280
986847Seq Number:
16 ftSample Depth:
RL MDL
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
Analysis Date
% Moisture:
Page 7 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 11.25 Date Collected:523803-001Lab Sample Id:
Ground WaterMatrix: MW-1Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
J
U
U
J
U
U
U
J
J
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
0.430
U
U
0.350
U
U
44.1
U
0.500
0.210
U
U
0.920
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
16 ftSample Depth:
RL MDL
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
115
99
115
01.31.16 19.27
01.31.16 19.27
01.31.16 19.27
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 8 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 11.10 Date Collected:523803-002Lab Sample Id:
Ground WaterMatrix: MW-1DSample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
40 ftSample Depth:
RL MDL
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
Analysis Date
% Moisture:
Page 9 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 11.10 Date Collected:523803-002Lab Sample Id:
Ground WaterMatrix: MW-1DSample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
40 ftSample Depth:
RL MDL
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
113
103
116
01.31.16 19.54
01.31.16 19.54
01.31.16 19.54
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 10 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 10.45 Date Collected:523803-003Lab Sample Id:
Ground WaterMatrix: MW-2Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
Analysis Date
% Moisture:
Page 11 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 10.45 Date Collected:523803-003Lab Sample Id:
Ground WaterMatrix: MW-2Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
112
102
114
01.31.16 20.21
01.31.16 20.21
01.31.16 20.21
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 12 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 10.35 Date Collected:523803-004Lab Sample Id:
Ground WaterMatrix: MW-3RSample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
1.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.30
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
Analysis Date
% Moisture:
Page 13 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 10.35 Date Collected:523803-004Lab Sample Id:
Ground WaterMatrix: MW-3RSample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
J
U
U
J
U
U
U
J
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
8.91
2.18
U
2.29
1.11
U
30.1
U
0.380
4.50
U
U
0.480
U
U
U
0.100
1.11
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
114
102
113
01.31.16 20.48
01.31.16 20.48
01.31.16 20.48
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 14 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 11.05 Date Collected:523803-005Lab Sample Id:
Ground WaterMatrix: MW-5Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
Analysis Date
% Moisture:
Page 15 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 11.05 Date Collected:523803-005Lab Sample Id:
Ground WaterMatrix: MW-5Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
1.59
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
118
100
115
01.31.16 21.15
01.31.16 21.15
01.31.16 21.15
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 16 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 10.25 Date Collected:523803-006Lab Sample Id:
Ground WaterMatrix: MW-6Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
Analysis Date
% Moisture:
Page 17 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 10.25 Date Collected:523803-006Lab Sample Id:
Ground WaterMatrix: MW-6Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
116
107
113
01.31.16 21.42
01.31.16 21.42
01.31.16 21.42
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 18 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 12.10 Date Collected:523803-007Lab Sample Id:
Ground WaterMatrix: WSW-4Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
Analysis Date
% Moisture:
Page 19 of 29 Final 1.000
Certificate of Analytical Results 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
01.28.16 10.00 Date Received:
01.26.16 12.10 Date Collected:523803-007Lab Sample Id:
Ground WaterMatrix: WSW-4Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13.57 Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.100
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.122
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
1330-20-7
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
RL MDL
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
114
104
116
01.31.16 19.00
01.31.16 19.00
01.31.16 19.00
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 20 of 29 Final 1.000
QC Summary 523803
Antea Group - Charlotte
GPM 3089
704190-1-BLKMB Sample Id:
WaterMatrix:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200BAnalytical Method:SM6200B_PREPPrep Method:
01.31.16Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
Parameter %RPD
H
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
0
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
0
5
1
1
2
3
2
2
5
15
3
1
0
3
0
1
2
2
5
1
1
1
1
2
2
1
3
2
14
3
1
6
2
4
0
0
13
5
4
3
1
1
1
4
2
2
2
4
4
0
1
3
986847Seq Number:
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
Analysis
Date
Limits
75-127
62-128
77-129
32-67
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
56-133
86-118
90-126
85-121
88-121
76-126
80-128
70-130
82-130
74-129
51-143
-
-
81-123
84-114
89-127
79-129
73-140
53-143
70-130
66-136
88-118
70-123
72-118
65-125
85-125
92-126
73-139
-
48-143
77-125
87-123
-
82-115
90-125
75-119
53-149
52-116
83-130
LCSD
%Rec
107
96
104
46
103
90
87
87
129
90
124
114
104
90
110
116
102
114
100
110
110
113
88
104
116
90
86
109
94
91
120
81
111
90
104
97
83
84
95
95
112
92
74
95
103
116
111
103
90
96
113
116
LCSD
Result
26.7
24.0
26.0
22.8
25.7
22.6
21.7
21.7
32.3
22.4
31.0
28.4
25.9
22.6
27.5
28.9
25.6
28.6
25.0
27.4
54.8
28.2
43.8
52.1
58.1
44.8
21.5
27.3
23.6
22.7
30.1
20.3
27.8
22.5
26.1
24.3
20.8
21.0
23.8
23.8
27.9
23.1
18.6
23.8
25.8
28.9
27.8
51.6
22.4
48.0
28.3
28.9
LCS
%Rec
107
101
103
46
104
94
85
88
123
104
121
115
104
93
110
116
105
117
105
111
109
112
89
107
118
89
89
111
108
94
122
86
113
94
105
97
95
88
99
98
113
91
75
99
105
113
113
108
93
96
114
112
26.7
25.2
25.8
23.1
26.1
23.4
21.3
22.1
30.7
26.1
30.2
28.7
25.9
23.2
27.5
29.1
26.2
29.2
26.2
27.7
54.3
27.9
44.3
53.3
59.2
44.3
22.2
27.8
27.1
23.5
30.4
21.5
28.3
23.4
26.2
24.2
23.7
22.0
24.8
24.5
28.3
22.8
18.7
24.7
26.3
28.3
28.3
53.8
23.3
47.9
28.5
28.0
Spike
Amount
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
50.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<2.00
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0900
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.0880
<0.352
<0.0900
<0.253
<0.352
<0.240
<0.396
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<1.91
<0.0990
<0.105
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.177
<0.0970
<0.0670
<0.0920
<0.0920
<0.0980
<0.0980
<0.176
<0.190
<0.169
<0.0940
<0.0600
704190-1-BKSLCS Sample Id:704190-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 21 of 29 Final 1.000
QC Summary 523803
Antea Group - Charlotte
GPM 3089
704190-1-BLKMB Sample Id:
WaterMatrix:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200BAnalytical Method:SM6200B_PREPPrep Method:
01.31.16Date Prep:
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
1
2
3
2
3
1
6
2
2
1
4
2
4
2
986847Seq Number:
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
Analysis
Date
Limits
84-122
86-119
80-128
86-120
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
LCSD
%Rec
110
103
116
110
105
113
111
101
86
116
86
86
98
84
LCSD
Result
27.5
25.7
28.9
27.6
26.2
28.3
27.7
25.2
21.5
29.0
21.6
21.4
24.6
21.1
LCS
%Rec
112
105
112
108
108
112
105
103
88
118
90
84
103
86
27.9
26.3
28.1
27.0
27.1
28.0
26.2
25.8
22.0
29.4
22.5
21.0
25.7
21.6
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.0650
<0.122
<0.0890
<0.0920
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
704190-1-BKSLCS Sample Id:704190-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
01.31.16 14:55
01.31.16 14:55
01.31.16 14:55
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
112
102
115
LCS
%Rec
110
104
116
MB
%Rec
113
104
116
%
%
%
UnitsLCS
Flag
MB
Flag
Page 22 of 29 Final 1.000
QC Summary 523803
Antea Group - Charlotte
GPM 3089
523801-002Parent Sample Id:
Ground WaterMatrix:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200BAnalytical Method:SM6200B_PREPPrep Method:
01.31.16Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
Parameter %RPD
X
X
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
0
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
5
0
2
11
0
2
5
7
8
7
3
2
1
7
1
0
5
0
9
2
1
2
7
10
12
9
4
0
1
4
3
5
15
2
4
2
4
2
1
2
4
0
11
0
4
2
3
4
2
0
14
1
986847Seq Number:
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
Analysis
Date
Limits
76-126
63-128
79-133
66-123
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
59-134
69-125
83-126
85-124
82-121
56-122
73-129
63-140
76-129
71-140
47-138
52-140
72-133
70-135
76-120
83-132
66-132
63-143
60-134
36-139
59-139
83-120
67-125
72-120
59-128
80-125
74-122
68-140
81-126
48-138
77-125
70-140
56-129
75-117
65-151
75-119
51-155
34-135
73-128
MSD
%Rec
100
78
114
34
111
86
69
83
116
122
109
104
109
91
100
108
110
108
64
101
118
104
103
96
116
99
84
107
93
90
126
82
77
84
99
99
78
69
90
95
114
96
63
94
97
85
103
100
74
97
148
94
MSD
Result
24.9
19.6
28.5
17.0
27.7
21.5
17.3
20.8
29.0
30.4
27.2
26.0
27.2
22.7
25.0
27.0
27.6
27.0
15.9
25.3
59.1
25.9
51.7
47.8
57.9
49.5
21.0
26.8
23.2
22.6
31.5
20.5
19.2
21.0
24.7
24.8
19.6
17.2
22.4
23.8
28.5
24.1
15.7
23.5
24.3
21.3
25.7
49.8
18.6
48.5
36.9
23.6
MS
%Rec
105
78
112
38
111
88
72
89
107
113
106
106
110
97
101
108
116
108
70
103
119
102
96
87
103
91
88
108
94
94
123
86
90
86
103
102
82
70
91
97
118
97
70
94
101
87
106
104
76
97
128
95
26.2
19.6
27.9
18.9
27.8
22.0
18.1
22.2
26.7
28.3
26.4
26.4
27.4
24.3
25.3
27.0
28.9
27.1
17.4
25.8
59.4
25.4
48.1
43.3
51.5
45.4
21.9
26.9
23.5
23.6
30.7
21.6
22.4
21.4
25.7
25.4
20.4
17.5
22.7
24.2
29.6
24.2
17.5
23.5
25.3
21.7
26.4
52.0
18.9
48.5
32.0
23.8
Spike
Amount
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
50.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
Parent
Result
<0.180
<0.0760
<0.0700
<2.00
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0900
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.0880
<0.352
<0.0900
<0.253
<0.352
<0.240
<0.396
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<1.91
<0.0990
<0.105
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.177
<0.0970
<0.0670
<0.0920
<0.0920
<0.0980
<0.0980
<0.176
<0.190
<0.169
<0.0940
<0.0600
523801-002 SMS Sample Id:523801-002 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 23 of 29 Final 1.000
QC Summary 523803
Antea Group - Charlotte
GPM 3089
523801-002Parent Sample Id:
Ground WaterMatrix:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200BAnalytical Method:SM6200B_PREPPrep Method:
01.31.16Date Prep:
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
1
5
2
3
2
3
5
4
5
1
3
7
1
4
986847Seq Number:
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
Analysis
Date
Limits
75-125
58-148
73-126
77-122
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
MSD
%Rec
102
98
101
98
101
102
92
96
78
121
83
72
80
80
MSD
Result
25.4
24.6
25.2
24.4
25.2
25.5
23.1
24.0
19.6
30.2
20.7
17.9
19.9
20.0
MS
%Rec
103
104
102
101
103
105
97
100
83
122
86
77
80
84
25.7
25.9
25.6
25.2
25.7
26.2
24.2
24.9
20.7
30.4
21.4
19.2
20.0
20.9
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
Parent
Result
<0.0650
<0.122
<0.0890
<0.0920
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
523801-002 SMS Sample Id:523801-002 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
02.01.16 00:55
02.01.16 00:55
02.01.16 00:55
Analysis
Date
Limits
65-126
86-111
83-116
MSD
%Rec
120
105
111
MS
%Rec
116
102
111
%
%
%
UnitsMS
Flag
Page 24 of 29 Final 1.000
Blank Summary 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
704190-1-BLKLab Sample Id:
WATERMatrix: 704190-1-BLK Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13:57Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Parameter
0.180
0.0760
0.0700
2.00
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0900
0.0870
0.0980
0.133
0.0670
0.0970
0.0880
0.352
0.0900
0.253
0.352
0.240
0.396
0.119
0.132
0.112
0.124
0.159
0.0970
1.91
0.0990
0.105
0.0420
0.172
0.0850
0.114
0.100
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
8.00
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.200
0.200
0.400
0.500
0.400
2.00
2.00
2.00
0.500
0.500
0.500
0.500
2.00
1.00
8.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
107-06-2
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
95-49-8
591-78-6
106-43-4
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
MDLRL
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
Analysis
Date
Page 25 of 29 Final 1.000
Blank Summary 523803
Antea Group - Charlotte, Charlotte, NC
GPM 3089
704190-1-BLKLab Sample Id:
WATERMatrix: 704190-1-BLK Sample Id:
6200 + BTEX, MTBE,IPE by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
01.31.16 13:57Date Prep:
ZHOTech:
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachlorobutadiene
isopropylbenzene
m,p-Xylenes
Methylene Chloride
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Cymene (p-Isopropyltoluene)
Sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
trans-1,2-dichloroethene
trans-1,3-dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Parameter
0.177
0.0970
0.0670
0.0920
0.0920
0.0980
0.0980
0.176
0.190
0.169
0.0940
0.0600
0.0650
0.122
0.0890
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
0.500
1.00
0.500
0.500
2.00
0.500
1.00
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
124-48-1
74-95-3
75-71-8
108-20-3
100-41-4
87-68-3
98-82-8
179601-23-1
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
986847Seq Number:
MDLRL
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
01.31.16 16:42
Analysis
Date
Page 26 of 29 Final 1.000
Page 27 of 29 Final 1.000
Page 28 of 29 Final 1.000
Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
523803Work Order #:
01/28/2016 10:00:00 AMDate/ Time Received:
Antea Group - Charlotte Client:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
J. Derek Rounsley
01/28/2016
01/29/2016
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
N/A
N/A

Missing sample containers for
Metals analysis

#1 *Temperature of cooler(s)?1.3
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:
Comments
Dario Lagunas
Temperature Measuring device used : #61
Page 29 of 29 Final 1.000