MO-30356_0_CA_CLO_20240104

Via Email

January 4, 2024

North Carolina Department of Environmental Quality
UST Section – Corrective Action Branch
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, NC 28115

Attn: Mr. Dan Bowser, PG

Re: UST Closure Report
401 S. College Street
Charlotte, North Carolina
Facility ID No. 00-0-0000034670
H&H Job No. AGI-002

Dear Dan:

On behalf of 401 S College Street NC, LLC, Hart & Hickman, PC (H&H) is providing the
attached UST Closure Report in PDF format for the above referenced site as an electronic copy.
No hard copy will follow unless requested. If you have any questions, please let us know.

Sincerely,

Hart & Hickman, PC
Matt Bramblett, PE Robert Sorgel
Principal Sr. Project Geologist

Enclosures

cc: Mr. Seth Goad, DEQ Brownfields (Via Email)
Mr. Alex Hay, ANiMAL Group Holdings, LLC (Via Email)
Ms. Laura Truesdale, Moore & Van Allen (Via Email)

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B. Site History and Characterization
1. UST Owner and Operator Information:
UST ID Number A1 and A2 Facility ID Number 0000034670
Name of Owner Dates of Ownership
401 S. College Street NC, LLC 12/13/2022 – present
Street Address
2303 Wineleas Road
City State Zip Telephone Number
Decatur GA 30033 [phone]
Name of Operator Dates of Operation
Duke Energy Carolinas, LLC 11/12/1996 – 12/12/2022
Street Address
526 S. Church Street
City State Zip Telephone Number
Charlotte NC 28202 [phone]
3 https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Animal Group/AGI.002 College/UST/UST Removal/Report/UST Closure Report.doc 2. UST/AST Information: UST ID Number State Regulated? Current/Last Contents Previous Contents Capacity (gallons) Construction Details Approximate Tank Dimensions Description of Associated Piping and Pumps Date Tank Installed Status of UST Was release associated with the UST System? A1 YES Diesel None 6,000 Fiberglass 19’ x 7’ Product Line 11/12/96 Removed 9/25/2023 Yes A2 YES Diesel None 6,000 Fiberglass 19’ x 7’ Product Line 11/12/96 Removed 9/25/2023 Yes UST-1 NO Fuel Oil None 500 Steel 5’ x 2.5’ Product Line Unknown Removed 9/25/2023 No

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3. Non-UST spills at the site:
No non-UST spills are known to have occurred at the Site.

4. Description of release:
According to regulatory records and DEQ annual tank registration fees, no release
incidents are reported in available databases in connection with the UST system.

5. Site characteristics:
The Site consists of one parcel totaling approximately 2.3 acres of land located in
Uptown Charlotte. Most recently, the Site was developed with structures
associated with the Duke Energy Data Center. Above-ground demolition of the
Site buildings (i.e. down to slab) began in 2023 and is currently ongoing. As of
the present, the following building features remain: the building shell and
basement associated with the southeastern Site building and the basement
associated with a former generator building. A site location map is presented as
Figure 1, and a Site Map is presented as Figure 2.

According to the Geologic Map of North Carolina dated 1985, the subject
property is located in the Charlotte Belt of the Piedmont Physiographic Province
of North Carolina, which is characterized by a thick mantle of weathered
residuum over fractured crystalline and metamorphic rock. The Piedmont region
consists of low, rounded hills and long, rolling, northeast southwest trending
ridges. The site area is underlain by bedrock consisting primarily of biotite gneiss
and schist.

In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed
saprolite or residuum. The saprolite consists of unconsolidated clay, silt, and sand
with lesser amounts of rock fragments. Due to the range of parent rock types and
their variable susceptibility to weathering, the saprolite ranges widely in color,
texture, and thickness. Generally, the saprolite is thickest near interstream divides
and thins toward streambeds. In profile, the saprolite normally grades from
clayey soils near the land surface to highly weathered rock above competent
bedrock.

The occurrence and movement of groundwater in the Piedmont is within two
separate but interconnected water-bearing zones. A shallow water-bearing zone
occurs within the saprolite, and a deeper water-bearing zone occurs within the
underlying bedrock.

Groundwater in the shallow saprolite zone occurs in the interstitial pore spaces
between the grains comprising the saprolitic soils, and is typically under water
table or unconfined conditions. Groundwater movement is generally lateral from
recharge areas to small streams that serve as localized discharge points.

The occurrence and movement of groundwater in the underlying water-bearing
zone within the crystalline bedrock is controlled by secondary joints, fractures,

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and faults within the bedrock. On a regional scale, the direction of groundwater
flow is typically from uplands to major streams and groundwater sinks. The
saprolite has a higher porosity than the bedrock and serves as a reservoir that
supplies water to a network of fractures in the bedrock.

The Site is located at an approximate elevation of 725 to 740 ft above mean sea
level. Topography at the site generally slopes to the west (Figure 1). Visual
observations during the UST removal (maximum depth of approximately 10 ft
below ground surface) indicate that the soil in the area of the UST consists of
sandy silt. Groundwater was encountered during previous assessment activities at
approximately 40 ft below ground surface (bgs). Bedrock was not encountered in
the excavation.

C. UST Closure Report following UST-12 format and Site Investigation Report
for Permanent Closure or Change-in-Service of UST (UST-2 Form):

1. Preparations for closure including the steps taken to notify authorities,
permits obtained and the steps taken to clean and purge the tanks:
Following purchase of the property, the NC DEQ UST Section was notified that
the two (2) regulated 6,000-gallon diesel USTs were emptied and placed in
temporary closure. It should be noted that 401 S. College Street NC, LLC did not
operate the USTs located at the Site. Prior to UST closure activities, H&H
submitted a Notice of Intent for UST Closure or Change-in-Service (UST-3)
Form to DEQ. Following UST closure activities, a Site Investigation (UST-2A)
Form was also submitted to DEQ. The completed UST Forms are provided in
Appendix A.

2. Closure procedures:
On September 25, 2023, Trifecta removed two (2) regulated 6,000-gallon diesel
USTs and one (1) unregulated 500-gallon fuel oil UST and associated product
piping. Trifecta utilized a vacuum truck to remove approximately 1,400 gallons
of residual fuel, sludge, and wash water from the USTs. Prior to UST removal
activities, Trifecta confirmed that there was less than 1 inch of water/sludge
present in the tank.

Once the tanks had been adequately emptied, overburden was removed with an
excavator and stockpiled on plastic sheeting adjacent to the excavation.
Overburden material consisted of washed crushed gravel (approximately 0.5 in).
During removal, the overburden gravel was screened for the presence of impacts
using sensory methods (i.e., visual and olfactory evaluation) as well as for the
presence of organic vapors using a photoionization detector (PID).
Redevelopment activities on the property are currently being managed through the
DEQ Brownfields Redevelopment Section (Brownfields Project No. 27007-23-
060). The DEQ Brownfields Redevelopment Section also approved our scope of
work associated with UST removal activities. There were no obvious impacts in
the stockpile based on field screening. In accordance with typical DEQ

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Brownfields requirements, excavated material from the UST basin was backfilled
into the excavation area.

Following removal of residual material within the USTs and removal of
overburden material, a lower explosion level (LEL) meter was utilized to monitor
for explosive atmospheres in the tank during the vapor purging process. A Fire
Marshal for the City of Charlotte was present on the Site to confirm the tank was
purged of vapors prior to removal. Following confirmation of acceptable LEL,
the tanks were then removed from the UST basin using an excavator. The two
regulated fiberglass tank dimensions were 19 ft in length and 7 ft in diameter.
The unregulated steel tank dimensions were 5 ft in length and 3.5 feet in diameter.
Following removal, the tanks were inspected and there were no visible cracks,
dents, pits, rusting, or other damage observed on the tanks or associated fittings
and pipes. Subsurface product piping connected to the USTs was also removed
for proper disposal. Subsurface product piping consisted of flexible piping
encased in polyvinyl chloride (PVC) pipe. The USTs and associated product lines
were properly disposed off-site.

3. Note the amount of residual material pumped from the tank and describes
the storage, sampling and disposal of the residual material and the disposal
of the tank, pumps and piping:
Residual product from the 6,000-gallon USTs was previously pumped out by
others. Trifecta used a vacuum truck to remove approximately 1,400 gallons of
water and sludge from the USTs prior to removal of the tanks. On September 25,
2023, the three tanks were transported off-site for disposal. The fiberglass USTs
were transported to the Gaston County Landfill for disposal and the steel UST
was transported to the Southern Metals Company to be recycled. A Tank
Disposal Certificate and the non-hazardous materials waste manifest
documentation are provided in Appendix B.

D. Site Investigation activities:
After removal of the USTs and associated product piping, 15 closure soil samples
were collected in general accordance with the Underground Storage Tank Section
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for
UST Releases dated March 1, 2007, effective February 1, 2019.

The base of the USTs was approximately 10 feet below ground surface (ft bgs)
and the USTs were underlain with a concrete pad. The product piping was
approximately two (2) ft bgs and was underlain by approximately 1 ft of washed
crushed gravel. Eight base soil samples (UST-A through UST-H) were collected
along the outside edge of the concrete pad at depths of approximately 10 ft bgs.
The base soil samples were collected from native soil directly adjacent to the
concrete pad and beneath the washed crushed gravel observed in the tank basin.
Based on the approximate 45 ft length of product piping associated with the
regulated USTs, five (5) product line closure soil samples (Piping-1 through
Piping 5) were collected from a depth of approximately 3 ft bgs. To satisfy the

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Brownfields Redevelopment Section, H&H also collected a sample beneath the
product piping of the non-regulated UST from a depth of approximately 3 ft bgs
and a side wall sample from the UST basin at a depth of approximately 6 ft bgs.

The soil samples were analyzed by Waypoint Analytical Laboratory (Waypoint),
a North Carolina certified laboratory. A chain-of-custody record was completed
for samples collected and included sample description, date collected, time
collected, matrix, sample container information, and analyses required. The
chain-of-custody was signed by H&H prior to placement in an iced cooler for
shipment to the laboratory.

The soil samples associated with the two regulated USTs were analyzed for total
petroleum hydrocarbons gasoline range organics (TPH-GRO) and diesel range
organics (TPH-DRO) by EPA Method 8015C. In accordance with the DEQ
Brownfields Redevelopment Section request, select soil samples were also
analyzed for volatile organic compounds (VOCs) by EPA Method 8260D, semi-
volatile organic compounds (SVOCs) by EPA Method 8270E, Resource
Conservation and Recovery Act (RCRA) metals by EPA Methods 6020B/7471B
and hexavalent chromium by EPA Method 7199. Considering the 20:1 rule for
screening of the soil metal concentrations for hazardous waste, one of the soil
samples (UST-SW-NE) was also analyzed for toxicity characteristic leaching
procedure (TCLP) RCRA metals by EPA Method 6010D.

The laboratory analytical results for the soil samples collected from the UST base
and product line of the regulated USTs indicated that TPH-DRO was detected in
several soil samples above laboratory detection limits. TPH-DRO was detected in
the Piping-1 soil sample at a concentration of 123 milligrams per kilogram
(mg/kg), which exceeds the NC DEQ Action Level of 100 mg/kg. Several
petroleum related VOCs and SVOCs were also detected in select soil samples.
The polycyclic aromatic hydrocarbon (PAH) benzo(a)pyrene was detected in
UST-SW-NE (0.432 J mg/kg), Piping-4 (0.173 mg/kg), and Piping-6 (0.323 J
mg/kg) soil samples at concentrations above the Soil-to-Water MSCC of 0.058
mg/kg and Residential PSRG of 0.11 mg/kg. Benzo(a)anthracene was detected in
UST-SW-NE (0.345 J mg/kg) and Piping-6 (0.285 J mg/kg) soil samples at
concentrations above the Soil-to-Water MSCC of 0.17 mg/kg. No other VOCs or
SVOCs were detected in the soil samples collected above the DEQ UST Section
or DEQ Brownfields Redevelopment Section screening criteria. Several metals
were detected in the UST closure samples above the laboratory method detection
limits, but within ranges of naturally occurring metals in North Carolina and local
soil. Additionally, the results of TCLP RCRA metals analysis performed on the
UST-SW-NE soil sample indicated that the soil does not qualify as
characteristically hazardous.

The approximate locations of the closure samples are depicted in Figure 3, and
soil sample results are summarized in Table 1. The laboratory analytical report is
included in Appendix C.

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E. Conclusions and Recommendations

In September 2023, H&H oversaw the removal of two (2) regulated 6,000-gallon
diesel USTs, one unregulated approximately 500-gallon heating oil UST, and
associated product piping. Approximately 1,400 gallons of water and sludge were
removed from the USTs. Following the removal of overburden gravel and
confirmation of the inert tanks using an LEL meter, the tanks were then removed
from the UST basin using an excavator. No visible cracks, dents, pits, rusting, or
other damage was observed on the tanks or associated fittings and pipes. The
tanks were transported off-site for proper disposal.

After removal of the USTs and associated product piping, 15 closure soil samples
were collected from the perimeter of a concrete pad underlying the USTs, from
the excavation sidewall, and beneath sub-grade product piping. UST closure
samples associated with the regulated USTs were analyzed for TPH-DRO and
TPH-GRO. In addition, at the request of the NC DEQ Brownfields
Redevelopment Section, select soil samples were also analyzed for VOCs,
SVOCs, RCRA metals, and hexavalent chromium. TPH-DRO was detected in the
Piping-1 soil sample at a concentration above the Action Level. Additionally,
benzo(a)anthracene and/or benzo(a)pyrene were detected in the UST-SW-NE,
Piping-4, and/or Piping-6 soil samples at concentrations above the Soil-to-Water
MSCCs and/or Residential PSRGs.

The Site is in the NC DEQ Brownfields Redevelopment Section (Brownfields
Project No. 27007-23-060). Therefore, H&H recommends that soil impacts
associated with the UST system be managed through the NC DEQ Brownfields
Redevelopment Section.

Table 1Summary of UST System Soil Sample Analytical Data Standard Roll Coverings
Charlotte, North Carolina
H&H Job No. AGI-002
Sample ID UST-A UST-B UST-C UST-D UST-E UST-F UST-G UST-H UST-SW-NE
Sample Location Northeastern
SidewallDepth (ft bgs)10 10 10 10 10 10 10 10 6
Date 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/26/2023
Units
TPH (8015C)
DRO 20.3 13.4 <5.35 <6.06 <5.52 <6.34 <6.39 20.6 NA 100 ----------------
GRO <4.54 <2.64 <2.38 <2.70 <2.46 <2.82 <2.84 <2.72 NA 50 ----------------
VOCs (8260D)
Acetone NA 0.026 NA NA NA NA 0.028 NA 0.033 --24 14,000 210,000 14,000 210,000 ------
Benzene NA 0.001 J NA NA NA NA <0.0008 NA <0.0007 --0.0072 12 59.4 1.2 5 ------
Carbon Disulfide NA <0.0008 NA NA NA NA <0.0009 NA <0.0008 --3.7 1,560 23,300 160 740 ------
Ethanol NA 3.20 NA NA NA NA <0.019 NA <0.017 --16 5,160 77,000 510 6,600 ------
Methylene Chloride NA 0.003 J NA NA NA NA 0.004 J NA <0.001 --0.023 93.8 1,400 58 650 ------
SVOC (8270E)
Benzo(a)anthracene NA <0.177 NA NA NA NA <0.225 NA 0.345 J --0.17 6.6 32 1.1 21 ------
Benzo(a)pyrene NA <0.187 NA NA NA NA <0.239 NA 0.432 J --0.058 0.66 3.2 0.11 2.1 ------
Benzo(b)fluoranthene NA <0.185 NA NA NA NA <0.237 NA 0.484 J --0.6 6.6 32 1.1 21 ------
Benzo(g,h,i)perylene NA <0.173 NA NA NA NA <0.221 NA 0.297 J --7,600 469 7,000 NE NE ------
Benzo(k)fluoranthene NA <0.174 NA NA NA NA <0.222 NA 0.177 J --5.8 66 327 11 210 ------
Chrysene NA 0.185 J NA NA NA NA <0.230 NA 0.389 J --18 663 3,270 110 2,100 ------
Fluoranthene NA 0.173 J NA NA NA NA <0.199 NA 0.509 J --330 625 9,340 480 6,000 ------
Ideno(1,2,3-cd)pyrene NA <0.228 NA NA NA NA <0.291 NA 0.281 J --1.9 6.63 32.7 1.1 21 ------
2-Methylnaphthalene NA <0.127 NA NA NA NA <0.162 NA 0.142 J --1.5 62.5 934 48 600 ------
Phenanthrene NA 0.335 J NA NA NA NA <0.337 NA 0.308 J --64 469 7,000 NE NE ------
Pyrene NA 0.276 J NA NA NA NA <0.217 NA 0.582 J --210 469 7,000 360 4,500 ------
RCRA Metals (6020B/7471B/7199)
Arsenic NA 1.58 NA NA NA NA 3.23 NA 1.85 --NE NE NE 0.68 3.0 1.1 - 3.0 1.0 - 18 --
Barium NA 124 NA NA NA NA 66.6 NA 101 --620 3,100 46,000 3,100 47,000 38 - 110 50 - 1,000 --
Cadmium NA 0.0528 J NA NA NA NA 0.101 J NA 0.122 J --NE NE NE 1.4 20 ND - 0.36 J 1.0 - 10 --
Chromium (Total)NA 80.1 NA NA NA NA 45.3 NA 218 --3.8 1.32 6.54 NE NE 14 - 45 7.0 - 300 --
Chromium (III)NA 78.8 NA NA NA NA 44.6 NA 216.9 --360,000 23,400 350,000 23,000 350,000 13.7 - 44.0 NS --
Chromium (IV)NA 1.29 NA NA NA NA 0.695 NA 1.12 --3.8 1.32 6.54 0.31 6.5 0.34 J - 0.98 J NS --
Lead NA 46.5 NA NA NA NA 10.2 NA 36.1 --270 400 400 400 800 11 - 36 ND - 50 --
Mercury NA 0.648 NA NA NA NA 0.821 NA 0.811 --NE NE NE 2.3 9.7 0.024 - 0.097 0.03 - 0.52 --
Selenium NA 0.698 NA NA NA NA 0.653 NA 0.599 --NE NE NE 78 1,200 ND <0.1 - 0.8 --
Silver NA 0.122 J NA NA NA NA 0.0614 J NA 0.110 J --4.8 78.2 1,160 78 1,200 0.033 J - 0.60 ND - 5.0 --
TCLP RCRA Metals (6010D)
Arsenic NA NA NA NA NA NA NA NA <0.014 ----------------5.0
Barium NA NA NA NA NA NA NA NA 1.04 ----------------100.0
Cadmium NA NA NA NA NA NA NA NA <0.0065 ----------------1.0
Chromium (Total)NA NA NA NA NA NA NA NA 0.020 J ----------------5.0
Lead NA NA NA NA NA NA NA NA 0.041 ----------------5.0
Mercury NA NA NA NA NA NA NA NA 0.0010 ----------------0.2
Selenium NA NA NA NA NA NA NA NA <0.026 ----------------NE
Silver NA NA NA NA NA NA NA NA <0.003 ----------------5.0
Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Underground Storage Tank (UST) Section Action Level dated July 2016.2) DEQ UST Section Maximum Soil Contaminant Concentrations (MSCCs) revised March 2022.
5) Regional background metals data taken from Elements in North American Soils by Dragun and Chekiri, 2005.6) Obtained from Chapter Seven of the Environmental Protection Agency (EPA) SW-846 Compendium: Introductory and Regulatory Definitions Pertaining to Hazardous Waste Characteristics (2004).Compound concentrations are reported to the laboratory method detection limits.
With the exception of metals, only compounds detected in at least one sample are shown in the table above.
Bold values exceed the Action Level.
Underlined values exceed the Soil-to-Water MSCCs.Gray Shaded values exceed the Residential PSRGs. Metals concentrations appear to be naturally occuring and are not shaded gray.mg/kg = milligrams per kilogram; mg/L = milligrams per LiterTPH = total petroleum hydrocarbons; DRO = diesel range organics; GRO = gasoline range organics; VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; TCLP = toxicity characteristing leaching procedureRCRA = Resource Conservation and Recovery Act; ft bgs= feet below ground surface; NE = not established; -- = not applicable; NA = not analyzedJ = Compound was detected above the laboratory method detection limit but below the laboratory reporting limit, resulting in a laboratory estimated concentration.
4) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060).3) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023.
mg/kg (8015C, 8270E, 6020B/7471B/7199); mg/L (6010D)
DEQ UST Section Screening Criteria
Residential
MSCCs (2)
Soil-to-Water
MSCCs (2)
Industrial /
Commercial
MSCCs (2)
Industrial /
Commercial
PSRGs (3)
Residential
PSRGs (3)
Local
Background
Metals in Soil (4)
Regional
Background
Metals in Soil(5)
Maximum
Concentration of Contaminants for
Toxicity
Characteristic (6)
DEQ Brownfields Screening Criteria
Perimeter of Concrete Pad Underlying USTs
Action Level (1)
mg/kg (8015C, 8270E, 6020B/7471B/7199); mg/L (6010D)
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Table 1 (Page 1 of 2)Hart & Hickman, PC
Table 1Summary of UST System Soil Sample Analytical Data Standard Roll Coverings
Charlotte, North Carolina
H&H Job No. AGI-002
Sample ID Piping-1 Piping-2 Piping-3 Piping-4 Piping-5 Piping-6
Sample Location
Depth (ft bgs)3 3 3 3 3 3
Date 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/26/2023 9/6/2023
Units
TPH (8015C)
DRO 123 <5.09 10.0 J 55.2 90.8 NA 100 ----------------
GRO <2.43 <2.26 <2.54 <2.23 <2.57 NA 50 ----------------
VOCs (8260D)
Acetone NA NA NA 0.008 J NA 0.004 J --24 14,000 210,000 14,000 210,000 ------
Benzene NA NA NA <0.0006 NA <0.0007 --0.0072 12 59.4 1.2 5 ------
Carbon Disulfide NA NA NA 0.0008 J NA 0.0008 J --3.7 1,560 23,300 160 740 ------
Ethanol NA NA NA <0.015 NA <0.016 --16 5,160 77,000 510 6,600 ------
Methylene Chloride NA NA NA <0.001 NA 0.003 J --0.023 93.8 1,400 58 650 ------
SVOC (8270E)
Benzo(a)anthracene NA NA NA 0.154 J NA 0.285 J --0.17 6.6 32 1.1 21 ------
Benzo(a)pyrene NA NA NA 0.173 J NA 0.323 J --0.058 0.66 3.2 0.11 2.1 ------
Benzo(b)fluoranthene NA NA NA 0.207 J NA 0.389 J --0.6 6.6 32 1.1 21 ------
Benzo(g,h,i)perylene NA NA NA <0.146 NA 0.218 J --7,600 469 7,000 NE NE ------
Benzo(k)fluoranthene NA NA NA <0.147 NA <0.156 --5.8 66 327 11 210 ------
Chrysene NA NA NA 0.158 J NA 0.308 J --18 663 3,270 110 2,100 ------
Fluoranthene NA NA NA 0.287 J NA 0.564 J --330 625 9,340 480 6,000 ------
Ideno(1,2,3-cd)pyrene NA NA NA <0.193 NA 0.232 J --1.9 6.63 32.7 1.1 21 ------
2-Methylnaphthalene NA NA NA <0.107 NA <0.110 --1.5 62.5 934 48 600 ------
Phenanthrene NA NA NA <0.224 NA 0.298 J --64 469 7,000 NE NE ------
Pyrene NA NA NA 0.272 J NA 0.513 J --210 469 7,000 360 4,500 ------
RCRA Metals (6020B/7471B/7199)
Arsenic NA NA NA 2.14 NA 2.47 --NE NE NE 0.68 3.0 1.1 - 3.0 1.0 - 18 --
Barium NA NA NA 88.4 NA 117 --620 3,100 46,000 3,100 47,000 38 - 110 50 - 1,000 --
Cadmium NA NA NA 0.203 J NA 0.0745 J --NE NE NE 1.4 20 ND - 0.36 J 1.0 - 10 --
Chromium (Total)NA NA NA 33.4 NA 19.3 --3.8 1.32 6.54 NE NE 14 - 45 7.0 - 300 --
Chromium (III)NA NA NA 32.8 NA 18.3 --360,000 23,400 350,000 23,000 350,000 13.7 - 44.0 NS --
Chromium (IV)NA NA NA 0.591 NA 1.04 --3.8 1.32 6.54 0.31 6.5 0.34 J - 0.98 J NS --
Lead NA NA NA 10.5 NA 12.8 --270 400 400 400 800 11 - 36 ND - 50 --
Mercury NA NA NA 0.0398 NA 0.0832 --NE NE NE 2.3 9.7 0.024 - 0.097 0.03 - 0.52 --
Selenium NA NA NA 0.276 NA 0.643 --NE NE NE 78 1,200 ND <0.1 - 0.8 --
Silver NA NA NA 0.0481 J NA 0.0449 J --4.8 78.2 1,160 78 1,200 0.033 J - 0.60 ND - 5.0 --
TCLP RCRA Metals (6020B/7470A)
Arsenic NA NA NA NA NA NA ----------------5.0
Barium NA NA NA NA NA NA ----------------100.0
Cadmium NA NA NA NA NA NA ----------------1.0
Chromium (Total)NA NA NA NA NA NA ----------------5.0
Lead NA NA NA NA NA NA ----------------5.0
Mercury NA NA NA NA NA NA ----------------0.2
Selenium NA NA NA NA NA NA ----------------NE
Silver NA NA NA NA NA NA ----------------5.0
Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Underground Storage Tank (UST) Section Action Level dated July 2016.2) DEQ UST Section Maximum Soil Contaminant Concentrations (MSCCs) revised March 2022.
5) Regional background metals data taken from Elements in North American Soils by Dragun and Chekiri, 2005.6) Obtained from Chapter Seven of the Environmental Protection Agency (EPA) SW-846 Compendium: Introductory and Regulatory Definitions Pertaining to Hazardous Waste Characteristics (2004).Compound concentrations are reported to the laboratory method detection limits.
With the exception of metals, only compounds detected in at least one sample are shown in the table above.
Bold values exceed the Action Level.
Underlined values exceed the Soil-to-Water MSCCs.Gray Shaded values exceed the Residential PSRGs. Metals concentrations appear to be naturally occuring and are not shaded gray.mg/kg = milligrams per kilogram; mg/L = milligrams per LiterTPH = total petroleum hydrocarbons; DRO = diesel range organics; GRO = gasoline range organics; VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; TCLP = toxicity characteristing leaching procedureRCRA = Resource Conservation and Recovery Act; ft bgs= feet below ground surface; NE = not established; -- = not applicable; NA = not analyzedJ = Compound was detected above the laboratory method detection limit but below the laboratory reporting limit, resulting in a laboratory estimated concentration.
mg/kg (8015C, 8270E, 6020B/7471B/7199); mg/L (6010D)
Beneath UST Product Piping
3) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023.4) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060).
Maximum
Concentration of Contaminants for
Toxicity
Characteristic (6)
mg/kg (8015C, 8270E, 6020B/7471B/7199); mg/L (6010D)
Action Level (1)Soil-to-Water
MSCCs (2)
Regional
Background
Metals in Soil(5)
DEQ UST Section Screening Criteria DEQ Brownfields Screening Criteria
Residential
MSCCs (2)
Industrial /
Commercial
MSCCs (2)
Residential
PSRGs (3)
Industrial /
Commercial
PSRGs (3)
Local
Background
Metals in Soil (4)
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Animal Group/AGI.002 College/UST/UST Removal/Tables/Data Tables_Standard Roll Coverings
Table 1 (Page 2 of 2)Hart & Hickman, PC
REVISION NO. 0
JOB NO. AGI-002
DATE: 10-31-23
FIGURE NO. 2
STANDARD ROLL COVERINGS
401 S. COLLEGE STREET
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
NOTE:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2023.
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
E
.
M
A
R
T
IN

L
U
T
H
ER

K
I
NG

JR
BOU
L
E
V
A
R
D
S. C
O
L
L
E
G
E
S
T
R
E
E
T
CHARLOTTE CONVENTION CENTER
(501 S. COLLEGE STREET)
ONE WELLS FARGO
(301 S. COLLEGE STREET)
VARIOUS OCCUPANTS
(500 S. COLLEGE STREET)
VARIOUS OCCUPANTS
(413-437 S. COLLEGE STREET)
NORFOLK SOUTHERN
RAILWAY
S:\AAA-Master Projects\Animal Group\AGI.002 College\Figures\PH1ESA-AGI002.dwg, FIG 2(2), 10/31/2023 12:07:41 PM, tmarbuery
REVISION NO. 0
JOB NO. AGI-002
DATE: 10-11-23
FIGURE NO. 3
STANDARD ROLL COVERINGS
401 S. COLLEGE STREET
CHARLOTTE, NORTH CAROLINA
SOIL SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
SUBGRADE PRODUCT PIPING
SOIL SAMPLE LOCATION
UST BASIN
CONCRETE PAD BENEATH USTs
FORMER UNDERGROUND STORAGE
TANK (UST)
NOTE:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2023.
2. TWO REGULATED 6,000-GALLON FUEL OIL USTs AND ONE
UNREGLUATED 500 GALLON FUEL OIL UST REMOVED ON
SEPTEMBER 25, 2023.
3. SAMPLES UST-A THROUGH UST-H WERE COLLECTED
FROM APPROXIMATELY 10 FEET BELOW GROUND
SURFACE (FT BGS). SAMPLES PIPING-1 THROUGH
PIPING-6 WERE COLLECTED FROM APPROXIMATELY 3 FT
BGS.
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
E
.
M
A
R
T
I
N

L
U
T
H
ER

K
I
NG

JR

BOU
L
EV
A
R
D
S. C
O
L
L
E
G
E
S
T
R
E
E
T
CHARLOTTE CONVENTION CENTER
ONE WELLS FARGO
STRUCTURE WAS RAZED
IN SUMMER 2023
STRUCTURE WAS RAZED
IN SUMMER 2023;
BASEMENT REMAINS
WITH SLAB INTACT
UST-D
UST-E
PIPING-1
INSET: 1'=20"
PIPING-4
PIPING-5
PIPING-3
UST-BUST-A
UST-H
UST-G
UST-F
UST-SW-NE
PIPING-6
PIPING-2
UST-C
PIPING-4
PIPING-5PIPING-3
UST-B
UST-A
UST-H
UST-G
UST-F
PIPING-2
UST-E PIPING-1
UST-D
UST-SW-NE
UST-C
PIPING-6
BASEMENT
ASSOCIATED WITH
FORMER STRUCTURE
S:\AAA-Master Projects\Animal Group\AGI.002 College\UST\UST Removal\Figures\AGI.002_20230927.dwg, FIG 3, 10/11/2023 11:56:43 AM, tmarbuery

Appendix A

UST Closure Forms (UST-2A and UST-3)
DocuSign Envelope ID: 4FFA2898-6002-48B4-95E6-321581D8CAFF
September 5, 2023
UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST
Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
phone [phone] fax [phone] http://www.wastenotnc.org/
STATE USE ONLY: Facility ID #
Date Received
INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II, III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City County Street Address
State Zip Code City

County

Zip Code

Phone Number
Phone Number
III. CONTACT PERSONNEL
Contact for Facility: Job Title: Phone #:
Closure Contractor Name:

Closure Contractor Company:

Address:

Phone #
Primary Consultant Name:

Primary Consultant Company:

Address:

Phone #
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/ concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete.
Print name and official title of owner or owner’s authorized representative

Signature Date Signed
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016
401 S. College Street NC, LLC
2303 Wineleas Road
Decatur Dekalb County
GA 30033
323-447-4434
College Street Facility
#00-0-0000034670
401 S. College Street
Charlotte 28202Mecklenburg
Alex Hay 323-447-4434
Mac Lee Trifecta Service Company 1722 Toal Street
704-990-1977
Matt Bramblett, PE Hart & Hickman, PC 2923 S. Tryon Street
704-586-0007
A1 6,000 Diesel 12/22 9/25/23 REMOVED ■■■
A2 6,000 Diesel 12/22 9/25/23 ■■■REMOVED
Matt Bramblett, PE of Hart & Hickman, PC as representative for 401 S. College Street NC, LLC
11/9/2023

Appendix B

Non-Hazardous Waste Materials Manifest and Tank Disposal Certificate
TRIFECTA SERVICES COMPANY
1722 Toal Street
Charlotte, NC 28206
704-900-1977TrifectaInc.com
“Cleaning Up the Past, Making Way for the Future”
|Atlanta|Baton Rouge|Charlotte|Greenville-Spartanburg|Nashville|Raleigh|Tallahassee|Wilmington|
1
TANK DISPOSAL CERTIFICATE
Tank Owner:401 S. College Street NC LLC
Site Address:401 S.College Street, Charlotte, NC 28202
Description of Tanks:
Tank Number Size of Tank Contents
1 6,000 gallons Diesel
2 6,000 gallons Diesel
3 500 gallons Diesel
Certification:
Trifecta Services Company does hereby certify that Tanks 1 and 2 were transported by Carolina
Waste Group to Gaston County Landfill (3155 Philadelphia Church Road, Dallas, NC 28034)for
proper disposal in accordance with applicable regulations.Tank 3 was transported by Trifecta to
Southern Metals Co (2200 Donald Ross Road, Charllotte, NC 28208)for disposal/recycling in
accordance with applicable regulations.Excess tank residue from the above-described tanks
was disposed of in accordance with US EPA regulations.
______________________________Signature
Mark LeeVice PresidentTrifecta Services Company
Mark Lee

Hart & Hickman, PC
Appendix C

Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/17/2023
Hart & Hickman (Charlotte) Robert Sorgel
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-270-0022 Client Project Description: Standard Roll Coverings
Dear Robert Sorgel:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/27/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 114
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/23-270-0022
Page 2 of 114
Report Number:
Sample Summary Table
Client Project Description:
23-270-0022
Standard Roll Coverings
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
09/26/2023 10:30Solids 96395 UST-A 09/27/2023 12:49
09/26/2023 10:45Solids 96396 UST-B 09/27/2023 12:49
09/26/2023 10:45Solids 96396 UST-B 09/27/2023 12:49 6020B WP MTN -
09/26/2023 10:45Solids 96396 UST-B 09/27/2023 12:49 SW-7199 WP MTN -
09/26/2023 11:00Solids 96397 UST-C 09/27/2023 12:49
09/26/2023 11:10Solids 96398 UST-D 09/27/2023 12:49
09/26/2023 11:30Solids 96399 UST-E 09/27/2023 12:49
09/26/2023 11:35Solids 96400 UST-F 09/27/2023 12:49
09/26/2023 11:45Solids 96401 UST-G 09/27/2023 12:49
09/26/2023 11:45Solids 96401 UST-G 09/27/2023 12:49 SW-7199 WP MTN -
09/26/2023 11:45Solids 96401 UST-G 09/27/2023 12:49 6020B WP MTN -
09/26/2023 11:55Solids 96402 UST-H 09/27/2023 12:49
09/26/2023 12:10Solids 96403 UST-SW-NE 09/27/2023 12:49
09/26/2023 12:10Solids 96403 UST-SW-NE 09/27/2023 12:49 SW-7199 WP MTN -
09/26/2023 12:10Solids 96403 UST-SW-NE 09/27/2023 12:49 6020B WP MTN -
09/26/2023 16:30Solids 96404 Piping-1 09/27/2023 12:49
09/26/2023 16:45Solids 96405 Piping-2 09/27/2023 12:49
09/26/2023 16:55Solids 96406 Piping-3 09/27/2023 12:49
09/26/2023 17:05Solids 96407 Piping-4 09/27/2023 12:49
09/26/2023 17:05Solids 96407 Piping-4 09/27/2023 12:49 SW-7199 WP MTN -
09/26/2023 17:05Solids 96407 Piping-4 09/27/2023 12:49 6020B WP MTN -
09/26/2023 17:10Solids 96408 Piping-5 09/27/2023 12:49
09/26/2023 17:20Solids 96409 Piping-6 09/27/2023 12:49
09/26/2023 17:20Solids 96409 Piping-6 09/27/2023 12:49 SW-7199 WP MTN -
09/26/2023 17:20Solids 96409 Piping-6 09/27/2023 12:49 6020B WP MTN -
09/26/2023 12:10TCLP 97349 UST-SW-NE 09/27/2023 12:49
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-270-0022
Report Limit
Project:Standard Roll Coverings
V 96395UST-A
20.3 09/29/2023 14:258015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 7.28
36.1 09/28/2023 14:48SW-DRYWT Moisture %
V 96396UST-B
1.58 10/02/2023 18:366020BArsenicmg/Kg - dry 0.109
124 10/02/2023 18:366020BBariummg/Kg - dry 0.054
J0.0528 10/02/2023 18:366020BCadmiummg/Kg - dry 0.0331
80.1 10/02/2023 18:366020BChromiummg/Kg - dry 0.147
46.5 10/02/2023 18:366020BLeadmg/Kg - dry 0.0394
0.698 10/02/2023 18:366020BSeleniummg/Kg - dry 0.131
J0.122 10/02/2023 18:366020BSilvermg/Kg - dry 0.0085
0.648 10/02/2023 15:177471BMercury (Total)mg/Kg - dry 0.0153
13.4 09/29/2023 14:468015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.92
0.026 09/27/2023 19:028260DAcetonemg/Kg - dry 0.003
J0.001 09/27/2023 19:028260DBenzenemg/Kg - dry 0.0007
3.20 09/27/2023 19:028260DEthanolmg/Kg - dry 0.017
J0.003 09/27/2023 19:028260DMethylene Chloride mg/Kg - dry 0.001
J0.185 09/29/2023 17:248270EChrysenemg/Kg - dry 0.180
J0.173 09/29/2023 17:248270EFluoranthenemg/Kg - dry 0.156
J0.335 09/29/2023 17:248270EPhenanthrenemg/Kg - dry 0.264
J0.276 09/29/2023 17:248270EPyrenemg/Kg - dry 0.170
1.29 10/10/2023 17:22SW-7199 Chromium, Hexavalent mg/Kg - dry 0.179
21.5 09/28/2023 14:48SW-DRYWT Moisture %
V 96397UST-C
13.1 09/28/2023 14:48SW-DRYWT Moisture %
V 96398UST-D
23.3 09/28/2023 14:48SW-DRYWT Moisture %
V 96399UST-E
15.8 09/28/2023 14:48SW-DRYWT Moisture %
V 96400UST-F
26.7 09/28/2023 14:48SW-DRYWT Moisture %
V 96401UST-G
3.23 10/02/2023 18:406020BArsenicmg/Kg - dry 0.117
66.6 10/02/2023 18:406020BBariummg/Kg - dry 0.058
Page 4 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-270-0022
Report Limit
Project:Standard Roll Coverings
V 96401UST-G
J0.101 10/02/2023 18:406020BCadmiummg/Kg - dry 0.0357
45.3 10/02/2023 18:406020BChromiummg/Kg - dry 0.159
10.2 10/02/2023 18:406020BLeadmg/Kg - dry 0.0425
0.653 10/02/2023 18:406020BSeleniummg/Kg - dry 0.141
J0.0614 10/02/2023 18:406020BSilvermg/Kg - dry 0.0092
0.821 10/02/2023 15:217471BMercury (Total)mg/Kg - dry 0.0165
0.028 09/27/2023 19:298260DAcetonemg/Kg - dry 0.003
J0.004 09/27/2023 19:298260DMethylene Chloride mg/Kg - dry 0.002
0.695 10/10/2023 17:33SW-7199 Chromium, Hexavalent mg/Kg - dry 0.193
27.2 09/28/2023 14:48SW-DRYWT Moisture %
V 96402UST-H
20.6 09/29/2023 14:038015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 6.10
23.8 09/28/2023 14:48SW-DRYWT Moisture %
V 96403UST-SW-NE
1.85 10/02/2023 18:526020BArsenicmg/Kg - dry 0.104
101 10/02/2023 18:526020BBariummg/Kg - dry 0.052
J0.122 10/02/2023 18:526020BCadmiummg/Kg - dry 0.0316
218 10/02/2023 18:526020BChromiummg/Kg - dry 0.141
36.1 10/02/2023 18:526020BLeadmg/Kg - dry 0.0377
0.599 10/02/2023 18:526020BSeleniummg/Kg - dry 0.125
J0.110 10/02/2023 18:526020BSilvermg/Kg - dry 0.0082
0.811 10/02/2023 15:577471BMercury (Total)mg/Kg - dry 0.0731
0.033 09/28/2023 20:488260DAcetonemg/Kg - dry 0.002
J0.345 10/03/2023 15:128270EBenzo(a)anthracene mg/Kg - dry 0.169
J0.432 10/03/2023 15:128270EBenzo(a)pyrene mg/Kg - dry 0.179
J0.484 10/03/2023 15:128270EBenzo(b)fluoranthene mg/Kg - dry 0.177
J0.297 10/03/2023 15:128270EBenzo(g,h,i)perylene mg/Kg - dry 0.165
J0.177 10/03/2023 15:128270EBenzo(k)fluoranthene mg/Kg - dry 0.166
J0.389 10/03/2023 15:128270EChrysenemg/Kg - dry 0.172
J0.509 10/03/2023 15:128270EFluoranthenemg/Kg - dry 0.149
J0.281 10/03/2023 15:128270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.218
J0.142 10/03/2023 15:128270E2-Methylnaphthalene mg/Kg - dry 0.121
J0.308 10/03/2023 15:128270EPhenanthrenemg/Kg - dry 0.253
J0.582 10/03/2023 15:128270EPyrenemg/Kg - dry 0.163
1.12 10/10/2023 16:27SW-7199 Chromium, Hexavalent mg/Kg - dry 0.171
Page 5 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-270-0022
Report Limit
Project:Standard Roll Coverings
V 96403UST-SW-NE
17.9 09/28/2023 14:48SW-DRYWT Moisture %
V 96404Piping-1
123 09/29/2023 15:298015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.46
14.8 09/28/2023 14:48SW-DRYWT Moisture %
V 96405Piping-2
8.59 09/28/2023 14:48SW-DRYWT Moisture %
V 96406Piping-3
J10.0 10/03/2023 20:338015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.71
18.6 09/28/2023 14:48SW-DRYWT Moisture %
V 96407Piping-4
2.14 10/02/2023 18:566020BArsenicmg/Kg - dry 0.0921
88.4 10/02/2023 18:566020BBariummg/Kg - dry 0.046
J0.203 10/02/2023 18:566020BCadmiummg/Kg - dry 0.0280
33.4 10/02/2023 18:566020BChromiummg/Kg - dry 0.125
10.5 10/02/2023 18:566020BLeadmg/Kg - dry 0.0334
0.276 10/02/2023 18:566020BSeleniummg/Kg - dry 0.111
J0.0481 10/02/2023 18:566020BSilvermg/Kg - dry 0.0072
0.0398 10/02/2023 15:377471BMercury (Total)mg/Kg - dry 0.0129
55.2 10/03/2023 20:548015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.01
J0.008 09/27/2023 20:248260DAcetonemg/Kg - dry 0.002
J0.0008 09/27/2023 20:248260DCarbon Disulfide mg/Kg - dry 0.0007
J0.154 10/03/2023 18:588270EBenzo(a)anthracene mg/Kg - dry 0.149
J0.173 10/03/2023 18:588270EBenzo(a)pyrene mg/Kg - dry 0.158
J0.207 10/03/2023 18:588270EBenzo(b)fluoranthene mg/Kg - dry 0.157
J0.158 10/03/2023 18:588270EChrysenemg/Kg - dry 0.153
J0.287 10/03/2023 18:588270EFluoranthenemg/Kg - dry 0.132
J0.272 10/03/2023 18:588270EPyrenemg/Kg - dry 0.144
0.591 10/10/2023 17:44SW-7199 Chromium, Hexavalent mg/Kg - dry 0.153
7.26 09/28/2023 14:48SW-DRYWT Moisture %
V 96408Piping-5
90.8 10/03/2023 21:168015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.78
19.5 09/28/2023 14:48SW-DRYWT Moisture %
Page 6 of 114
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-270-0022
Report Limit
Project:Standard Roll Coverings
V 96409Piping-6
2.47 10/02/2023 19:006020BArsenicmg/Kg - dry 0.0977
117 10/02/2023 19:006020BBariummg/Kg - dry 0.048
J0.0745 10/02/2023 19:006020BCadmiummg/Kg - dry 0.0297
19.3 10/02/2023 19:006020BChromiummg/Kg - dry 0.132
12.8 10/02/2023 19:006020BLeadmg/Kg - dry 0.0354
0.643 10/02/2023 19:006020BSeleniummg/Kg - dry 0.117
J0.0449 10/02/2023 19:006020BSilvermg/Kg - dry 0.0077
0.0832 10/02/2023 15:407471BMercury (Total)mg/Kg - dry 0.0137
J0.004 09/27/2023 20:518260DAcetonemg/Kg - dry 0.002
J0.0008 09/27/2023 20:518260DCarbon Disulfide mg/Kg - dry 0.0007
J0.003 09/27/2023 20:518260DMethylene Chloride mg/Kg - dry 0.001
J0.285 10/03/2023 18:138270EBenzo(a)anthracene mg/Kg - dry 0.158
J0.323 10/03/2023 18:138270EBenzo(a)pyrene mg/Kg - dry 0.168
J0.389 10/03/2023 18:138270EBenzo(b)fluoranthene mg/Kg - dry 0.166
J0.218 10/03/2023 18:138270EBenzo(g,h,i)perylene mg/Kg - dry 0.155
J0.308 10/03/2023 18:138270EChrysenemg/Kg - dry 0.162
J0.564 10/03/2023 18:138270EFluoranthenemg/Kg - dry 0.140
J0.232 10/03/2023 18:138270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.204
J0.298 10/03/2023 18:138270EPhenanthrenemg/Kg - dry 0.237
J0.513 10/03/2023 18:138270EPyrenemg/Kg - dry 0.153
1.04 10/11/2023 09:05SW-7199 Chromium, Hexavalent mg/Kg - dry 0.162
12.5 09/28/2023 14:48SW-DRYWT Moisture %
V 97349UST-SW-NE
1.04 10/17/2023 03:246010DTCLP Barium mg/L 0.005
J0.020 10/12/2023 00:266010DTCLP Chromium mg/L 0.012
0.041 10/12/2023 00:266010DTCLP Lead mg/L 0.008
0.0010 10/11/2023 16:557470ATCLP Mercury mg/L 0.00003
Leachate 10/09/2023 15:40SW-1311 TCLP Metals Extraction
Page 7 of 114

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: Standard Roll Coverings Lab Report Number: 23-270-0022
Date: 10/17/2023
Metals Analyses Method 6020B Sample 96450 (FG-DUP) Analyte: Arsenic
QC Batch No: L708292/L707911 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96450 (FG-DUP)
Analyte: Barium QC Batch No: L708292/L707911
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 96450 (FG-DUP)
Analyte: Cadmium QC Batch No: L708292/L707911
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Sample 96450 (FG-DUP) Analyte: Chromium
QC Batch No: L708292/L707911 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 96450 (FG-DUP) Analyte: Lead QC Batch No: L708292/L707911 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 96450 (FG-DUP) Analyte: Selenium QC Batch No: L708292/L707911 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Hexavalent Chromium by Ion Chromatography Method SW-7199 Analyte: Hexavalent Chromium QC Batch No: L709932 Matrix spike recovery outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 8 of 114

Total Aqueous Mercury Analysis - CVAA (TCLP) Method 7470A Sample 97349 (UST-SW-NE)
Analyte: Mercury QC Batch No: V38928/V38903
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97349 (UST-SW-NE) Analyte: Mercury
QC Batch No: V38928/V38903 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acrolein QC Batch No: V38509/V38480
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Benzoic Acid QC Batch No: V38472/V38445 Analyte was flagged for 0% recovery in the LCS and LCSD due to the result being below the MQL. The actual
result was 13.986 and 16.106 respectively, which calculates to a recovery of 27.972% and 32.212% and is within the acceptable recovery range.
Sample 96596 Analyte: Benzoic Acid QC Batch No: V38621/V38566 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 9 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-A
96395 Matrix:
9/26/2023 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
36.1 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-A
96395 Matrix:
9/26/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
20.3 mg/Kg - dry 7.28 15.6Diesel Range Organics (C10-C28)1 09/29/23 14:25 V38475AMP
8015C DROSurrogate: OTP Surrogate 70.2 Limits: 31-123%09/29/23 14:251 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<4.54 mg/Kg - dry 4.54 11.0Gasoline Range Organics (C6-C10)50 09/28/23 20:54 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 113 Limits: 50-137%09/28/23 20:5450 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.5 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
1.29 mg/Kg - dry 0.179 0.254Chromium, Hexavalent 1 10/10/23 17:22 SW-7199SWB
1.58 mg/Kg - dry 0.109 0.318Arsenic 5 10/02/23 18:36 6020BCPW
124 mg/Kg - dry 0.054 0.318Barium 5 10/02/23 18:36 6020BCPW
0.0528 J mg/Kg - dry 0.0331 0.318Cadmium 5 10/02/23 18:36 6020BCPW
80.1 mg/Kg - dry 0.147 0.318
Chromium 5 10/02/23 18:36 6020BCPW
46.5 mg/Kg - dry 0.0394 0.318Lead 5 10/02/23 18:36 6020BCPW
0.648 mg/Kg - dry 0.0153 0.0382Mercury (Total)1 10/02/23 15:17 7471BJKC
0.698 mg/Kg - dry 0.131 0.318Selenium 5 10/02/23 18:36 6020BCPW
0.122 J mg/Kg - dry 0.0085 0.318Silver 5 10/02/23 18:36 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
13.4 mg/Kg - dry 5.92 12.7Diesel Range Organics (C10-C28)1 09/29/23 14:46 V38475AMP
8015C DROSurrogate: OTP Surrogate 72.6 Limits: 31-123%09/29/23 14:461 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.64 mg/Kg - dry 2.64 6.37Gasoline Range Organics (C6-C10)50 09/28/23 21:22 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 126 Limits: 50-137%09/28/23 21:2250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
0.026 mg/Kg - dry 0.003 0.025
Acetone 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/27/23 19:02 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/27/23 19:02 V38481TBL
0.001 J mg/Kg - dry 0.0007 0.006Benzene 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 09/27/23 19:02 V38481TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 09/27/23 19:02 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/27/23 19:02 V38481TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/27/23 19:02 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
Chloroform 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/27/23 19:02 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/27/23 19:02 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 09/27/23 19:02 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/27/23 19:02 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/27/23 19:02 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/27/23 19:02 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 09/27/23 19:02 V38481TBL
3.20 mg/Kg - dry 0.017 0.318Ethanol 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Isopropylbenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/27/23 19:02 V38481TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/27/23 19:02 V38481TBL
0.003 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/27/23 19:02 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/27/23 19:02 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/27/23 19:02 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1,1-Trichloroethane 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/27/23 19:02 V38481TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/27/23 19:02 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/27/23 19:02 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Acetate 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/27/23 19:02 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/27/23 19:02 V38481TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/27/23 19:02 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/27/23 19:02 V38481
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/27/23 19:021 TBL V38481
Surrogate: Dibromofluoromethane 103 Limits: 84-123%09/27/23 19:021 TBL V38481
Surrogate: Toluene-d8 97.7 Limits: 76-129%09/27/23 19:021 TBL V38481
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38445 09/28/23 09:30
<0.147 mg/Kg - dry 0.147 0.840Acenaphthene 1 09/29/23 17:24 V38472AMP
<0.133 mg/Kg - dry 0.133 0.840Acenaphthylene 1 09/29/23 17:24 V38472AMP
<0.193 mg/Kg - dry 0.193 0.840Aniline 1 09/29/23 17:24 V38472AMP
<0.182 mg/Kg - dry 0.182 0.840
Anthracene 1 09/29/23 17:24 V38472AMP
<0.177 mg/Kg - dry 0.177 0.840Benzo(a)anthracene 1 09/29/23 17:24 V38472AMP
<0.187 mg/Kg - dry 0.187 0.840Benzo(a)pyrene 1 09/29/23 17:24 V38472AMP
<0.185 mg/Kg - dry 0.185 0.840Benzo(b)fluoranthene 1 09/29/23 17:24 V38472AMP
<0.173 mg/Kg - dry 0.173 0.840Benzo(g,h,i)perylene 1 09/29/23 17:24 V38472AMP
<0.174 mg/Kg - dry 0.174 0.840Benzo(k)fluoranthene 1 09/29/23 17:24 V38472AMP
<0.738 mg/Kg - dry 0.738 2.55Benzoic Acid 1 09/29/23 17:24 V38472AMP
<0.133 mg/Kg - dry 0.133 0.840
Benzyl alcohol 1 09/29/23 17:24 V38472AMP
<0.150 mg/Kg - dry 0.150 0.840Bis(2-Chloroethoxy)methane 1 09/29/23 17:24 V38472AMP
<0.136 mg/Kg - dry 0.136 0.840Bis(2-Chloroethyl)ether 1 09/29/23 17:24 V38472AMP
<0.173 mg/Kg - dry 0.173 0.420Bis(2-Chloroisopropyl)ether 1 09/29/23 17:24 V38472AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38445 09/28/23 09:30
<0.152 mg/Kg - dry 0.152 0.840Bis(2-ethylhexyl)phthalate 1 09/29/23 17:24 V38472AMP
<0.138 mg/Kg - dry 0.138 0.8404-Bromophenyl phenyl ether 1 09/29/23 17:24 V38472AMP
<0.143 mg/Kg - dry 0.143 0.420Butyl benzyl phthalate 1 09/29/23 17:24 V38472AMP
<0.117 mg/Kg - dry 0.117 0.8404-Chloro-3-methylphenol 1 09/29/23 17:24 V38472AMP
<0.142 mg/Kg - dry 0.142 0.4204-Chloroaniline 1 09/29/23 17:24 V38472AMP
<0.147 mg/Kg - dry 0.147 0.8402-Chloronaphthalene 1 09/29/23 17:24 V38472AMP
<0.125 mg/Kg - dry 0.125 0.8402-Chlorophenol 1 09/29/23 17:24 V38472AMP
<0.160 mg/Kg - dry 0.160 1.274-Chlorophenyl phenyl ether 1 09/29/23 17:24 V38472AMP
0.185 J
mg/Kg - dry 0.180 0.840
Chrysene 1 09/29/23 17:24 V38472AMP
<0.292 mg/Kg - dry 0.292 0.840Dibenz(a,h)anthracene 1 09/29/23 17:24 V38472AMP
<0.151 mg/Kg - dry 0.151 0.840Dibenzofuran 1 09/29/23 17:24 V38472AMP
<0.120 mg/Kg - dry 0.120 0.8401,2-Dichlorobenzene 1 09/29/23 17:24 V38472AMP
<0.123 mg/Kg - dry 0.123 0.8401,3-Dichlorobenzene 1 09/29/23 17:24 V38472AMP
<0.124 mg/Kg - dry 0.124 0.4201,4-Dichlorobenzene 1 09/29/23 17:24 V38472AMP
<0.187 mg/Kg - dry 0.187 0.8403,3'-Dichlorobenzidine 1 09/29/23 17:24 V38472AMP
<0.122 mg/Kg - dry 0.122 0.840
2,4-Dichlorophenol 1 09/29/23 17:24 V38472AMP
<0.229 mg/Kg - dry 0.229 0.840Diethyl phthalate 1 09/29/23 17:24 V38472AMP
<0.221 mg/Kg - dry 0.221 0.840Dimethyl phthalate 1 09/29/23 17:24 V38472AMP
<0.137 mg/Kg - dry 0.137 0.4202,4-Dimethylphenol 1 09/29/23 17:24 V38472AMP
<0.136 mg/Kg - dry 0.136 0.840Di-n-butyl phthalate 1 09/29/23 17:24 V38472AMP
<0.305 mg/Kg - dry 0.305 1.914,6-Dinitro-2-methylphenol 1 09/29/23 17:24 V38472AMP
<0.662 mg/Kg - dry 0.662 1.912,4-Dinitrophenol 1 09/29/23 17:24 V38472AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38445 09/28/23 09:30
<0.123 mg/Kg - dry 0.123 0.8402,4-Dinitrotoluene 1 09/29/23 17:24 V38472AMP
<0.137 mg/Kg - dry 0.137 0.8402,6-Dinitrotoluene 1 09/29/23 17:24 V38472AMP
<0.182 mg/Kg - dry 0.182 0.420Di-n-Octyl Phthalate 1 09/29/23 17:24 V38472AMP
0.173 J mg/Kg - dry 0.156 0.840Fluoranthene 1 09/29/23 17:24 V38472AMP
<0.163 mg/Kg - dry 0.163 0.840Fluorene 1 09/29/23 17:24 V38472AMP
<0.135 mg/Kg - dry 0.135 0.840Hexachlorobenzene 1 09/29/23 17:24 V38472AMP
<0.124 mg/Kg - dry 0.124 0.840Hexachlorobutadiene 1 09/29/23 17:24 V38472AMP
<0.200 mg/Kg - dry 0.200 0.840Hexachlorocyclopentadiene 1 09/29/23 17:24 V38472AMP
<0.100 mg/Kg - dry 0.100 0.840
Hexachloroethane 1 09/29/23 17:24 V38472AMP
<0.228 mg/Kg - dry 0.228 0.840Indeno(1,2,3-cd)pyrene 1 09/29/23 17:24 V38472AMP
<0.243 mg/Kg - dry 0.243 0.840Isophorone 1 09/29/23 17:24 V38472AMP
<0.135 mg/Kg - dry 0.135 0.8401-Methylnaphthalene 1 09/29/23 17:24 V38472AMP
<0.127 mg/Kg - dry 0.127 0.8402-Methylnaphthalene 1 09/29/23 17:24 V38472AMP
<0.123 mg/Kg - dry 0.123 0.8402-Methylphenol 1 09/29/23 17:24 V38472AMP
<0.108 mg/Kg - dry 0.108 0.8403&4 Methylphenol 1 09/29/23 17:24 V38472AMP
<0.183 mg/Kg - dry 0.183 0.840
Naphthalene 1 09/29/23 17:24 V38472AMP
<0.123 mg/Kg - dry 0.123 0.8402-Nitroaniline 1 09/29/23 17:24 V38472AMP
<0.152 mg/Kg - dry 0.152 0.8403-Nitroaniline 1 09/29/23 17:24 V38472AMP
<0.118 mg/Kg - dry 0.118 0.4204-Nitroaniline 1 09/29/23 17:24 V38472AMP
<0.147 mg/Kg - dry 0.147 0.420Nitrobenzene 1 09/29/23 17:24 V38472AMP
<0.113 mg/Kg - dry 0.113 0.8402-Nitrophenol 1 09/29/23 17:24 V38472AMP
<0.149 mg/Kg - dry 0.149 0.8404-Nitrophenol 1 09/29/23 17:24 V38472AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-B
96396 Matrix:
9/26/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38445 09/28/23 09:30
<0.335 mg/Kg - dry 0.335 0.840N-Nitrosodimethylamine 1 09/29/23 17:24 V38472AMP
<0.230 mg/Kg - dry 0.230 0.840N-Nitrosodiphenylamine 1 09/29/23 17:24 V38472AMP
<0.150 mg/Kg - dry 0.150 0.840N-Nitroso-di-n-propylamine 1 09/29/23 17:24 V38472AMP
<0.442 mg/Kg - dry 0.442 1.27Pentachlorophenol 1 09/29/23 17:24 V38472AMP
0.335 J mg/Kg - dry 0.264 0.840Phenanthrene 1 09/29/23 17:24 V38472AMP
<0.142 mg/Kg - dry 0.142 0.840Phenol 1 09/29/23 17:24 V38472AMP
0.276 J mg/Kg - dry 0.170 0.840Pyrene 1 09/29/23 17:24 V38472AMP
<0.100 mg/Kg - dry 0.100 0.420Pyridine 1 09/29/23 17:24 V38472AMP
<0.136 mg/Kg - dry 0.136 0.840
1,2,4-Trichlorobenzene 1 09/29/23 17:24 V38472AMP
<0.122 mg/Kg - dry 0.122 0.8402,4,5-Trichlorophenol 1 09/29/23 17:24 V38472AMP
<0.123 mg/Kg - dry 0.123 0.8402,4,6-Trichlorophenol 1 09/29/23 17:24 V38472AMP
8270ESurrogate: Phenol-d5 82.0 Limits: 34-121%09/29/23 17:241 AMP
Surrogate: 2-Fluorobiphenyl 87.4 Limits: 44-115%09/29/23 17:241 AMP V38472
Surrogate: 2-Fluorophenol 85.3 Limits: 35-115%09/29/23 17:241 AMP V38472
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%09/29/23 17:241 AMP V38472
Surrogate: 4-Terphenyl-d14 85.6 Limits: 54-127%09/29/23 17:241 AMP V38472
Surrogate: 2,4,6-Tribromophenol 88.6 Limits: 39-132%09/29/23 17:241 AMP V38472
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-C
96397 Matrix:
9/26/2023 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.1 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-C
96397 Matrix:
9/26/2023 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
<5.35 mg/Kg - dry 5.35 11.5Diesel Range Organics (C10-C28)1 09/29/23 11:55 V38475AMP
8015C DROSurrogate: OTP Surrogate 72.5 Limits: 31-123%09/29/23 11:551 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.38 mg/Kg - dry 2.38 5.75Gasoline Range Organics (C6-C10)50 09/28/23 21:50 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 126 Limits: 50-137%09/28/23 21:5050 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-D
96398 Matrix:
9/26/2023 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.3 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-D
96398 Matrix:
9/26/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
<6.06 mg/Kg - dry 6.06 13.0Diesel Range Organics (C10-C28)1 09/29/23 12:16 V38475AMP
8015C DROSurrogate: OTP Surrogate 72.4 Limits: 31-123%09/29/23 12:161 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.70 mg/Kg - dry 2.70 6.52Gasoline Range Organics (C6-C10)50 09/28/23 22:18 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 114 Limits: 50-137%09/28/23 22:1850 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-E
96399 Matrix:
9/26/2023 11:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.8 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-E
96399 Matrix:
9/26/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
<5.52 mg/Kg - dry 5.52 11.9Diesel Range Organics (C10-C28)1 09/29/23 12:38 V38475AMP
8015C DROSurrogate: OTP Surrogate 71.7 Limits: 31-123%09/29/23 12:381 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.46 mg/Kg - dry 2.46 5.94Gasoline Range Organics (C6-C10)50 09/28/23 22:46 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 135 Limits: 50-137%09/28/23 22:4650 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-F
96400 Matrix:
9/26/2023 11:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.7 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-F
96400 Matrix:
9/26/2023 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
<6.34 mg/Kg - dry 6.34 13.6Diesel Range Organics (C10-C28)1 09/29/23 12:59 V38475AMP
8015C DROSurrogate: OTP Surrogate 75.2 Limits: 31-123%09/29/23 12:591 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.82 mg/Kg - dry 2.82 6.82Gasoline Range Organics (C6-C10)50 09/28/23 23:14 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 103 Limits: 50-137%09/28/23 23:1450 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.2 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
0.695 mg/Kg - dry 0.193 0.274Chromium, Hexavalent 1 10/10/23 17:33 SW-7199SWB
3.23 mg/Kg - dry 0.117 0.343Arsenic 5 10/02/23 18:40 6020BCPW
66.6 mg/Kg - dry 0.058 0.343Barium 5 10/02/23 18:40 6020BCPW
0.101 J mg/Kg - dry 0.0357 0.343Cadmium 5 10/02/23 18:40 6020BCPW
45.3 mg/Kg - dry 0.159 0.343
Chromium 5 10/02/23 18:40 6020BCPW
10.2 mg/Kg - dry 0.0425 0.343Lead 5 10/02/23 18:40 6020BCPW
0.821 mg/Kg - dry 0.0165 0.0412Mercury (Total)1 10/02/23 15:21 7471BJKC
0.653 mg/Kg - dry 0.141 0.343Selenium 5 10/02/23 18:40 6020BCPW
0.0614 J mg/Kg - dry 0.0092 0.343Silver 5 10/02/23 18:40 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
<6.39 mg/Kg - dry 6.39 13.7Diesel Range Organics (C10-C28)1 09/29/23 13:42 V38475AMP
8015C DROSurrogate: OTP Surrogate 72.2 Limits: 31-123%09/29/23 13:421 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.84 mg/Kg - dry 2.84 6.87Gasoline Range Organics (C6-C10)50 09/28/23 23:43 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 116 Limits: 50-137%09/28/23 23:4350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
0.028 mg/Kg - dry 0.003 0.027
Acetone 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 09/27/23 19:29 V38481TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 09/27/23 19:29 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 09/27/23 19:29 V38481TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
Chloroform 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/27/23 19:29 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 09/27/23 19:29 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 09/27/23 19:29 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/27/23 19:29 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/27/23 19:29 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/27/23 19:29 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 09/27/23 19:29 V38481TBL
<0.019 mg/Kg - dry 0.019 0.343Ethanol 1 09/27/23 19:29 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.068Ethyl Tertiary Butyl Ether (ETBE)1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 09/27/23 19:29 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Isopropylbenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 09/27/23 19:29 V38481TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 09/27/23 19:29 V38481TBL
0.004 J mg/Kg - dry 0.002 0.013Methylene Chloride 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 09/27/23 19:29 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/27/23 19:29 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 09/27/23 19:29 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1,1-Trichloroethane 1 09/27/23 19:29 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/27/23 19:29 V38481TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/27/23 19:29 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/27/23 19:29 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Acetate 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 09/27/23 19:29 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/27/23 19:29 V38481TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/27/23 19:29 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/27/23 19:29 V38481
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/27/23 19:291 TBL V38481
Surrogate: Dibromofluoromethane 103 Limits: 84-123%09/27/23 19:291 TBL V38481
Surrogate: Toluene-d8 97.4 Limits: 76-129%09/27/23 19:291 TBL V38481
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.188 mg/Kg - dry 0.188 1.07Acenaphthene 1 10/03/23 14:49 V38621AMP
<0.170 mg/Kg - dry 0.170 1.07Acenaphthylene 1 10/03/23 14:49 V38621AMP
<0.247 mg/Kg - dry 0.247 1.07Aniline 1 10/03/23 14:49 V38621AMP
<0.232 mg/Kg - dry 0.232 1.07
Anthracene 1 10/03/23 14:49 V38621AMP
<0.225 mg/Kg - dry 0.225 1.07Benzo(a)anthracene 1 10/03/23 14:49 V38621AMP
<0.239 mg/Kg - dry 0.239 1.07Benzo(a)pyrene 1 10/03/23 14:49 V38621AMP
<0.237 mg/Kg - dry 0.237 1.07Benzo(b)fluoranthene 1 10/03/23 14:49 V38621AMP
<0.221 mg/Kg - dry 0.221 1.07Benzo(g,h,i)perylene 1 10/03/23 14:49 V38621AMP
<0.222 mg/Kg - dry 0.222 1.07Benzo(k)fluoranthene 1 10/03/23 14:49 V38621AMP
<0.939 mg/Kg - dry 0.939 3.24Benzoic Acid 1 10/03/23 14:49 V38621AMP
<0.170 mg/Kg - dry 0.170 1.07
Benzyl alcohol 1 10/03/23 14:49 V38621AMP
<0.190 mg/Kg - dry 0.190 1.07Bis(2-Chloroethoxy)methane 1 10/03/23 14:49 V38621AMP
<0.173 mg/Kg - dry 0.173 1.07Bis(2-Chloroethyl)ether 1 10/03/23 14:49 V38621AMP
<0.221 mg/Kg - dry 0.221 0.535Bis(2-Chloroisopropyl)ether 1 10/03/23 14:49 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.195 mg/Kg - dry 0.195 1.07Bis(2-ethylhexyl)phthalate 1 10/03/23 14:49 V38621AMP
<0.177 mg/Kg - dry 0.177 1.074-Bromophenyl phenyl ether 1 10/03/23 14:49 V38621AMP
<0.184 mg/Kg - dry 0.184 0.535Butyl benzyl phthalate 1 10/03/23 14:49 V38621AMP
<0.149 mg/Kg - dry 0.149 1.074-Chloro-3-methylphenol 1 10/03/23 14:49 V38621AMP
<0.181 mg/Kg - dry 0.181 0.5354-Chloroaniline 1 10/03/23 14:49 V38621AMP
<0.188 mg/Kg - dry 0.188 1.072-Chloronaphthalene 1 10/03/23 14:49 V38621AMP
<0.159 mg/Kg - dry 0.159 1.072-Chlorophenol 1 10/03/23 14:49 V38621AMP
<0.204 mg/Kg - dry 0.204 1.624-Chlorophenyl phenyl ether 1 10/03/23 14:49 V38621AMP
<0.230 mg/Kg - dry 0.230 1.07
Chrysene 1 10/03/23 14:49 V38621AMP
<0.373 mg/Kg - dry 0.373 1.07Dibenz(a,h)anthracene 1 10/03/23 14:49 V38621AMP
<0.193 mg/Kg - dry 0.193 1.07Dibenzofuran 1 10/03/23 14:49 V38621AMP
<0.153 mg/Kg - dry 0.153 1.071,2-Dichlorobenzene 1 10/03/23 14:49 V38621AMP
<0.157 mg/Kg - dry 0.157 1.071,3-Dichlorobenzene 1 10/03/23 14:49 V38621AMP
<0.157 mg/Kg - dry 0.157 0.5351,4-Dichlorobenzene 1 10/03/23 14:49 V38621AMP
<0.239 mg/Kg - dry 0.239 1.073,3'-Dichlorobenzidine 1 10/03/23 14:49 V38621AMP
<0.155 mg/Kg - dry 0.155 1.07
2,4-Dichlorophenol 1 10/03/23 14:49 V38621AMP
<0.292 mg/Kg - dry 0.292 1.07Diethyl phthalate 1 10/03/23 14:49 V38621AMP
<0.282 mg/Kg - dry 0.282 1.07Dimethyl phthalate 1 10/03/23 14:49 V38621AMP
<0.175 mg/Kg - dry 0.175 0.5352,4-Dimethylphenol 1 10/03/23 14:49 V38621AMP
<0.173 mg/Kg - dry 0.173 1.07Di-n-butyl phthalate 1 10/03/23 14:49 V38621AMP
<0.388 mg/Kg - dry 0.388 2.434,6-Dinitro-2-methylphenol 1 10/03/23 14:49 V38621AMP
<0.843 mg/Kg - dry 0.843 2.432,4-Dinitrophenol 1 10/03/23 14:49 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.156 mg/Kg - dry 0.156 1.072,4-Dinitrotoluene 1 10/03/23 14:49 V38621AMP
<0.175 mg/Kg - dry 0.175 1.072,6-Dinitrotoluene 1 10/03/23 14:49 V38621AMP
<0.232 mg/Kg - dry 0.232 0.535Di-n-Octyl Phthalate 1 10/03/23 14:49 V38621AMP
<0.199 mg/Kg - dry 0.199 1.07Fluoranthene 1 10/03/23 14:49 V38621AMP
<0.207 mg/Kg - dry 0.207 1.07Fluorene 1 10/03/23 14:49 V38621AMP
<0.171 mg/Kg - dry 0.171 1.07Hexachlorobenzene 1 10/03/23 14:49 V38621AMP
<0.157 mg/Kg - dry 0.157 1.07Hexachlorobutadiene 1 10/03/23 14:49 V38621AMP
<0.255 mg/Kg - dry 0.255 1.07Hexachlorocyclopentadiene 1 10/03/23 14:49 V38621AMP
<0.128 mg/Kg - dry 0.128 1.07
Hexachloroethane 1 10/03/23 14:49 V38621AMP
<0.291 mg/Kg - dry 0.291 1.07Indeno(1,2,3-cd)pyrene 1 10/03/23 14:49 V38621AMP
<0.310 mg/Kg - dry 0.310 1.07Isophorone 1 10/03/23 14:49 V38621AMP
<0.171 mg/Kg - dry 0.171 1.071-Methylnaphthalene 1 10/03/23 14:49 V38621AMP
<0.162 mg/Kg - dry 0.162 1.072-Methylnaphthalene 1 10/03/23 14:49 V38621AMP
<0.157 mg/Kg - dry 0.157 1.072-Methylphenol 1 10/03/23 14:49 V38621AMP
<0.137 mg/Kg - dry 0.137 1.073&4 Methylphenol 1 10/03/23 14:49 V38621AMP
<0.233 mg/Kg - dry 0.233 1.07
Naphthalene 1 10/03/23 14:49 V38621AMP
<0.156 mg/Kg - dry 0.156 1.072-Nitroaniline 1 10/03/23 14:49 V38621AMP
<0.195 mg/Kg - dry 0.195 1.073-Nitroaniline 1 10/03/23 14:49 V38621AMP
<0.151 mg/Kg - dry 0.151 0.5354-Nitroaniline 1 10/03/23 14:49 V38621AMP
<0.188 mg/Kg - dry 0.188 0.535Nitrobenzene 1 10/03/23 14:49 V38621AMP
<0.144 mg/Kg - dry 0.144 1.072-Nitrophenol 1 10/03/23 14:49 V38621AMP
<0.189 mg/Kg - dry 0.189 1.074-Nitrophenol 1 10/03/23 14:49 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-G
96401 Matrix:
9/26/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.427 mg/Kg - dry 0.427 1.07N-Nitrosodimethylamine 1 10/03/23 14:49 V38621AMP
<0.293 mg/Kg - dry 0.293 1.07N-Nitrosodiphenylamine 1 10/03/23 14:49 V38621AMP
<0.190 mg/Kg - dry 0.190 1.07N-Nitroso-di-n-propylamine 1 10/03/23 14:49 V38621AMP
<0.561 mg/Kg - dry 0.561 1.62Pentachlorophenol 1 10/03/23 14:49 V38621AMP
<0.337 mg/Kg - dry 0.337 1.07Phenanthrene 1 10/03/23 14:49 V38621AMP
<0.181 mg/Kg - dry 0.181 1.07Phenol 1 10/03/23 14:49 V38621AMP
<0.217 mg/Kg - dry 0.217 1.07Pyrene 1 10/03/23 14:49 V38621AMP
<0.128 mg/Kg - dry 0.128 0.535Pyridine 1 10/03/23 14:49 V38621AMP
<0.173 mg/Kg - dry 0.173 1.07
1,2,4-Trichlorobenzene 1 10/03/23 14:49 V38621AMP
<0.156 mg/Kg - dry 0.156 1.072,4,5-Trichlorophenol 1 10/03/23 14:49 V38621AMP
<0.156 mg/Kg - dry 0.156 1.072,4,6-Trichlorophenol 1 10/03/23 14:49 V38621AMP
8270ESurrogate: Phenol-d5 77.9 Limits: 34-121%10/03/23 14:491 AMP
Surrogate: 2-Fluorobiphenyl 85.8 Limits: 44-115%10/03/23 14:491 AMP V38621
Surrogate: 2-Fluorophenol 82.2 Limits: 35-115%10/03/23 14:491 AMP V38621
Surrogate: Nitrobenzene-d5 77.7 Limits: 37-122%10/03/23 14:491 AMP V38621
Surrogate: 4-Terphenyl-d14 86.3 Limits: 54-127%10/03/23 14:491 AMP V38621
Surrogate: 2,4,6-Tribromophenol 90.9 Limits: 39-132%10/03/23 14:491 AMP V38621
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-H
96402 Matrix:
9/26/2023 11:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.8 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-H
96402 Matrix:
9/26/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
20.6 mg/Kg - dry 6.10 13.1Diesel Range Organics (C10-C28)1 09/29/23 14:03 V38475AMP
8015C DROSurrogate: OTP Surrogate 80.5 Limits: 31-123%09/29/23 14:031 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.72 mg/Kg - dry 2.72 6.56Gasoline Range Organics (C6-C10)50 09/29/23 00:11 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 105 Limits: 50-137%09/29/23 00:1150 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.9 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
1.12 mg/Kg - dry 0.171 0.243Chromium, Hexavalent 1 10/10/23 16:27 SW-7199SWB
1.85 mg/Kg - dry 0.104 0.305Arsenic 5 10/02/23 18:52 6020BCPW
101 mg/Kg - dry 0.052 0.304Barium 5 10/02/23 18:52 6020BCPW
0.122 J mg/Kg - dry 0.0316 0.305Cadmium 5 10/02/23 18:52 6020BCPW
218 mg/Kg - dry 0.141 0.304
Chromium 5 10/02/23 18:52 6020BCPW
36.1 mg/Kg - dry 0.0377 0.305Lead 5 10/02/23 18:52 6020BCPW
0.811 mg/Kg - dry 0.0731 0.183Mercury (Total)5 10/02/23 15:57 7471BJKC
0.599 mg/Kg - dry 0.125 0.304Selenium 5 10/02/23 18:52 6020BCPW
0.110 J mg/Kg - dry 0.0082 0.305Silver 5 10/02/23 18:52 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38508 09/28/23 08:00
0.033 mg/Kg - dry 0.002 0.024Acetone 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 09/28/23 20:48 V38509TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/28/23 20:48 V38509TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/28/23 20:48 V38509TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/28/23 20:48 V38509TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/28/23 20:48 V38509TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/28/23 20:48 V38509TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38508 09/28/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/28/23 20:48 V38509TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/28/23 20:48 V38509TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/28/23 20:48 V38509TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/28/23 20:48 V38509TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/28/23 20:48 V38509TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/28/23 20:48 V38509TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/28/23 20:48 V38509TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/28/23 20:48 V38509TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/28/23 20:48 V38509TBL
<0.017 mg/Kg - dry 0.017 0.304Ethanol 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 09/28/23 20:48 V38509TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/28/23 20:48 V38509TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38508 09/28/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/28/23 20:48 V38509TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/28/23 20:48 V38509TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/28/23 20:48 V38509TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/28/23 20:48 V38509TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/28/23 20:48 V38509TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/28/23 20:48 V38509TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38508 09/28/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/28/23 20:48 V38509TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/28/23 20:48 V38509TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/28/23 20:48 V38509TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/28/23 20:48 V38509
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/28/23 20:481 TBL V38509
Surrogate: Dibromofluoromethane 108 Limits: 84-123%09/28/23 20:481 TBL V38509
Surrogate: Toluene-d8 93.7 Limits: 76-129%09/28/23 20:481 TBL V38509
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.141 mg/Kg - dry 0.141 0.803Acenaphthene 1 10/03/23 15:12 V38621AMP
<0.127 mg/Kg - dry 0.127 0.803Acenaphthylene 1 10/03/23 15:12 V38621AMP
<0.185 mg/Kg - dry 0.185 0.803Aniline 1 10/03/23 15:12 V38621AMP
<0.174 mg/Kg - dry 0.174 0.803Anthracene 1 10/03/23 15:12 V38621AMP
0.345 J
mg/Kg - dry 0.169 0.803
Benzo(a)anthracene 1 10/03/23 15:12 V38621AMP
0.432 J mg/Kg - dry 0.179 0.803Benzo(a)pyrene 1 10/03/23 15:12 V38621AMP
0.484 J mg/Kg - dry 0.177 0.803Benzo(b)fluoranthene 1 10/03/23 15:12 V38621AMP
0.297 J mg/Kg - dry 0.165 0.803Benzo(g,h,i)perylene 1 10/03/23 15:12 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
0.177 J mg/Kg - dry 0.166 0.803Benzo(k)fluoranthene 1 10/03/23 15:12 V38621AMP
<0.706 mg/Kg - dry 0.706 2.44Benzoic Acid 1 10/03/23 15:12 V38621AMP
<0.127 mg/Kg - dry 0.127 0.803Benzyl alcohol 1 10/03/23 15:12 V38621AMP
<0.143 mg/Kg - dry 0.143 0.803Bis(2-Chloroethoxy)methane 1 10/03/23 15:12 V38621AMP
<0.130 mg/Kg - dry 0.130 0.803Bis(2-Chloroethyl)ether 1 10/03/23 15:12 V38621AMP
<0.165 mg/Kg - dry 0.165 0.401Bis(2-Chloroisopropyl)ether 1 10/03/23 15:12 V38621AMP
<0.146 mg/Kg - dry 0.146 0.803Bis(2-ethylhexyl)phthalate 1 10/03/23 15:12 V38621AMP
<0.132 mg/Kg - dry 0.132 0.8034-Bromophenyl phenyl ether 1 10/03/23 15:12 V38621AMP
<0.137 mg/Kg - dry 0.137 0.401
Butyl benzyl phthalate 1 10/03/23 15:12 V38621AMP
<0.112 mg/Kg - dry 0.112 0.8034-Chloro-3-methylphenol 1 10/03/23 15:12 V38621AMP
<0.136 mg/Kg - dry 0.136 0.4014-Chloroaniline 1 10/03/23 15:12 V38621AMP
<0.141 mg/Kg - dry 0.141 0.8032-Chloronaphthalene 1 10/03/23 15:12 V38621AMP
<0.119 mg/Kg - dry 0.119 0.8032-Chlorophenol 1 10/03/23 15:12 V38621AMP
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 10/03/23 15:12 V38621AMP
0.389 J mg/Kg - dry 0.172 0.803Chrysene 1 10/03/23 15:12 V38621AMP
<0.280 mg/Kg - dry 0.280 0.803
Dibenz(a,h)anthracene 1 10/03/23 15:12 V38621AMP
<0.144 mg/Kg - dry 0.144 0.803Dibenzofuran 1 10/03/23 15:12 V38621AMP
<0.114 mg/Kg - dry 0.114 0.8031,2-Dichlorobenzene 1 10/03/23 15:12 V38621AMP
<0.118 mg/Kg - dry 0.118 0.8031,3-Dichlorobenzene 1 10/03/23 15:12 V38621AMP
<0.118 mg/Kg - dry 0.118 0.4011,4-Dichlorobenzene 1 10/03/23 15:12 V38621AMP
<0.179 mg/Kg - dry 0.179 0.8033,3'-Dichlorobenzidine 1 10/03/23 15:12 V38621AMP
<0.116 mg/Kg - dry 0.116 0.8032,4-Dichlorophenol 1 10/03/23 15:12 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.219 mg/Kg - dry 0.219 0.803Diethyl phthalate 1 10/03/23 15:12 V38621AMP
<0.211 mg/Kg - dry 0.211 0.803Dimethyl phthalate 1 10/03/23 15:12 V38621AMP
<0.131 mg/Kg - dry 0.131 0.4012,4-Dimethylphenol 1 10/03/23 15:12 V38621AMP
<0.130 mg/Kg - dry 0.130 0.803Di-n-butyl phthalate 1 10/03/23 15:12 V38621AMP
<0.292 mg/Kg - dry 0.292 1.834,6-Dinitro-2-methylphenol 1 10/03/23 15:12 V38621AMP
<0.633 mg/Kg - dry 0.633 1.832,4-Dinitrophenol 1 10/03/23 15:12 V38621AMP
<0.117 mg/Kg - dry 0.117 0.8032,4-Dinitrotoluene 1 10/03/23 15:12 V38621AMP
<0.131 mg/Kg - dry 0.131 0.8032,6-Dinitrotoluene 1 10/03/23 15:12 V38621AMP
<0.174 mg/Kg - dry 0.174 0.401
Di-n-Octyl Phthalate 1 10/03/23 15:12 V38621AMP
0.509 J mg/Kg - dry 0.149 0.803Fluoranthene 1 10/03/23 15:12 V38621AMP
<0.155 mg/Kg - dry 0.155 0.803Fluorene 1 10/03/23 15:12 V38621AMP
<0.129 mg/Kg - dry 0.129 0.803Hexachlorobenzene 1 10/03/23 15:12 V38621AMP
<0.118 mg/Kg - dry 0.118 0.803Hexachlorobutadiene 1 10/03/23 15:12 V38621AMP
<0.191 mg/Kg - dry 0.191 0.803Hexachlorocyclopentadiene 1 10/03/23 15:12 V38621AMP
<0.096 mg/Kg - dry 0.096 0.803Hexachloroethane 1 10/03/23 15:12 V38621AMP
0.281 J
mg/Kg - dry 0.218 0.803
Indeno(1,2,3-cd)pyrene 1 10/03/23 15:12 V38621AMP
<0.232 mg/Kg - dry 0.232 0.803Isophorone 1 10/03/23 15:12 V38621AMP
<0.129 mg/Kg - dry 0.129 0.8031-Methylnaphthalene 1 10/03/23 15:12 V38621AMP
0.142 J mg/Kg - dry 0.121 0.8032-Methylnaphthalene 1 10/03/23 15:12 V38621AMP
<0.118 mg/Kg - dry 0.118 0.8032-Methylphenol 1 10/03/23 15:12 V38621AMP
<0.103 mg/Kg - dry 0.103 0.8033&4 Methylphenol 1 10/03/23 15:12 V38621AMP
<0.175 mg/Kg - dry 0.175 0.803Naphthalene 1 10/03/23 15:12 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
96403 Matrix:
9/26/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.117 mg/Kg - dry 0.117 0.8032-Nitroaniline 1 10/03/23 15:12 V38621AMP
<0.146 mg/Kg - dry 0.146 0.8033-Nitroaniline 1 10/03/23 15:12 V38621AMP
<0.113 mg/Kg - dry 0.113 0.4014-Nitroaniline 1 10/03/23 15:12 V38621AMP
<0.141 mg/Kg - dry 0.141 0.401Nitrobenzene 1 10/03/23 15:12 V38621AMP
<0.108 mg/Kg - dry 0.108 0.8032-Nitrophenol 1 10/03/23 15:12 V38621AMP
<0.142 mg/Kg - dry 0.142 0.8034-Nitrophenol 1 10/03/23 15:12 V38621AMP
<0.320 mg/Kg - dry 0.320 0.803N-Nitrosodimethylamine 1 10/03/23 15:12 V38621AMP
<0.220 mg/Kg - dry 0.220 0.803N-Nitrosodiphenylamine 1 10/03/23 15:12 V38621AMP
<0.143 mg/Kg - dry 0.143 0.803
N-Nitroso-di-n-propylamine 1 10/03/23 15:12 V38621AMP
<0.422 mg/Kg - dry 0.422 1.22Pentachlorophenol 1 10/03/23 15:12 V38621AMP
0.308 J mg/Kg - dry 0.253 0.803Phenanthrene 1 10/03/23 15:12 V38621AMP
<0.136 mg/Kg - dry 0.136 0.803Phenol 1 10/03/23 15:12 V38621AMP
0.582 J mg/Kg - dry 0.163 0.803Pyrene 1 10/03/23 15:12 V38621AMP
<0.096 mg/Kg - dry 0.096 0.401Pyridine 1 10/03/23 15:12 V38621AMP
<0.130 mg/Kg - dry 0.130 0.8031,2,4-Trichlorobenzene 1 10/03/23 15:12 V38621AMP
<0.117 mg/Kg - dry 0.117 0.803
2,4,5-Trichlorophenol 1 10/03/23 15:12 V38621AMP
<0.117 mg/Kg - dry 0.117 0.8032,4,6-Trichlorophenol 1 10/03/23 15:12 V38621AMP
8270ESurrogate: Phenol-d5 81.4 Limits: 34-121%10/03/23 15:121 AMP
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%10/03/23 15:121 AMP V38621
Surrogate: 2-Fluorophenol 84.4 Limits: 35-115%10/03/23 15:121 AMP V38621
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%10/03/23 15:121 AMP V38621
Surrogate: 4-Terphenyl-d14 91.6 Limits: 54-127%10/03/23 15:121 AMP V38621
Surrogate: 2,4,6-Tribromophenol 95.2 Limits: 39-132%10/03/23 15:121 AMP V38621
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-1
96404 Matrix:
9/26/2023 16:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.8 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-1
96404 Matrix:
9/26/2023 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
123 mg/Kg - dry 5.46 11.7Diesel Range Organics (C10-C28)1 09/29/23 15:29 V38475AMP
8015C DROSurrogate: OTP Surrogate 76.7 Limits: 31-123%09/29/23 15:291 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.43 mg/Kg - dry 2.43 5.87Gasoline Range Organics (C6-C10)50 09/29/23 00:39 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 136 Limits: 50-137%09/29/23 00:3950 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-2
96405 Matrix:
9/26/2023 16:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.59 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-2
96405 Matrix:
9/26/2023 16:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38444 09/28/23 09:30
<5.09 mg/Kg - dry 5.09 10.9Diesel Range Organics (C10-C28)1 09/29/23 13:21 V38475AMP
8015C DROSurrogate: OTP Surrogate 73.8 Limits: 31-123%09/29/23 13:211 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.26 mg/Kg - dry 2.26 5.47Gasoline Range Organics (C6-C10)50 09/29/23 01:08 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 134 Limits: 50-137%09/29/23 01:0850 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-3
96406 Matrix:
9/26/2023 16:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.6 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-3
96406 Matrix:
9/26/2023 16:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38557 10/02/23 09:20
10.0 J mg/Kg - dry 5.71 12.3Diesel Range Organics (C10-C28)1 10/03/23 20:33 V38643NDL
8015C DROSurrogate: OTP Surrogate 66.6 Limits: 31-123%10/03/23 20:331 NDL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.54 mg/Kg - dry 2.54 6.14Gasoline Range Organics (C6-C10)50 09/29/23 02:03 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 124 Limits: 50-137%09/29/23 02:0350 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
7.26 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
0.591 mg/Kg - dry 0.153 0.217Chromium, Hexavalent 1 10/10/23 17:44 SW-7199SWB
2.14 mg/Kg - dry 0.0921 0.270Arsenic 5 10/02/23 18:56 6020BCPW
88.4 mg/Kg - dry 0.046 0.269Barium 5 10/02/23 18:56 6020BCPW
0.203 J mg/Kg - dry 0.0280 0.270Cadmium 5 10/02/23 18:56 6020BCPW
33.4 mg/Kg - dry 0.125 0.269
Chromium 5 10/02/23 18:56 6020BCPW
10.5 mg/Kg - dry 0.0334 0.270Lead 5 10/02/23 18:56 6020BCPW
0.0398 mg/Kg - dry 0.0129 0.0323Mercury (Total)1 10/02/23 15:37 7471BJKC
0.276 mg/Kg - dry 0.111 0.269Selenium 5 10/02/23 18:56 6020BCPW
0.0481 J mg/Kg - dry 0.0072 0.270Silver 5 10/02/23 18:56 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38557 10/02/23 09:20
55.2 mg/Kg - dry 5.01 10.8Diesel Range Organics (C10-C28)1 10/03/23 20:54 V38643NDL
8015C DROSurrogate: OTP Surrogate 68.1 Limits: 31-123%10/03/23 20:541 NDL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.23 mg/Kg - dry 2.23 5.39Gasoline Range Organics (C6-C10)50 09/29/23 02:32 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 132 Limits: 50-137%09/29/23 02:3250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
0.008 J
mg/Kg - dry 0.002 0.021
Acetone 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 09/27/23 20:24 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 09/27/23 20:24 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 09/27/23 20:24 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 09/27/23 20:24 V38481TBL
0.0008 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 09/27/23 20:24 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 09/27/23 20:24 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 09/27/23 20:24 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/27/23 20:24 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 09/27/23 20:24 V38481TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 09/27/23 20:24 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 09/27/23 20:24 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 09/27/23 20:24 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/27/23 20:24 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/27/23 20:24 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/27/23 20:24 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 09/27/23 20:24 V38481TBL
<0.015 mg/Kg - dry 0.015 0.269Ethanol 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 09/27/23 20:24 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.053Ethyl Tertiary Butyl Ether (ETBE)1 09/27/23 20:24 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.005
Isopropylbenzene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/27/23 20:24 V38481TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 09/27/23 20:24 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/27/23 20:24 V38481TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 09/27/23 20:24 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 09/27/23 20:24 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005
1,1,1-Trichloroethane 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/27/23 20:24 V38481TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 09/27/23 20:24 V38481TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 09/27/23 20:24 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 09/27/23 20:24 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.010
Vinyl Acetate 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 09/27/23 20:24 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 09/27/23 20:24 V38481TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 09/27/23 20:24 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 09/27/23 20:24 V38481
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/27/23 20:241 TBL V38481
Surrogate: Dibromofluoromethane 104 Limits: 84-123%09/27/23 20:241 TBL V38481
Surrogate: Toluene-d8 95.7 Limits: 76-129%09/27/23 20:241 TBL V38481
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.125 mg/Kg - dry 0.125 0.711Acenaphthene 1 10/03/23 18:58 V38621AMP
<0.113 mg/Kg - dry 0.113 0.711Acenaphthylene 1 10/03/23 18:58 V38621AMP
<0.163 mg/Kg - dry 0.163 0.711Aniline 1 10/03/23 18:58 V38621AMP
<0.154 mg/Kg - dry 0.154 0.711
Anthracene 1 10/03/23 18:58 V38621AMP
0.154 J mg/Kg - dry 0.149 0.711Benzo(a)anthracene 1 10/03/23 18:58 V38621AMP
0.173 J mg/Kg - dry 0.158 0.711Benzo(a)pyrene 1 10/03/23 18:58 V38621AMP
0.207 J mg/Kg - dry 0.157 0.711Benzo(b)fluoranthene 1 10/03/23 18:58 V38621AMP
<0.146 mg/Kg - dry 0.146 0.711Benzo(g,h,i)perylene 1 10/03/23 18:58 V38621AMP
<0.147 mg/Kg - dry 0.147 0.711Benzo(k)fluoranthene 1 10/03/23 18:58 V38621AMP
<0.625 mg/Kg - dry 0.625 2.16Benzoic Acid 1 10/03/23 18:58 V38621AMP
<0.113 mg/Kg - dry 0.113 0.711
Benzyl alcohol 1 10/03/23 18:58 V38621AMP
<0.127 mg/Kg - dry 0.127 0.711Bis(2-Chloroethoxy)methane 1 10/03/23 18:58 V38621AMP
<0.115 mg/Kg - dry 0.115 0.711Bis(2-Chloroethyl)ether 1 10/03/23 18:58 V38621AMP
<0.146 mg/Kg - dry 0.146 0.355Bis(2-Chloroisopropyl)ether 1 10/03/23 18:58 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.129 mg/Kg - dry 0.129 0.711Bis(2-ethylhexyl)phthalate 1 10/03/23 18:58 V38621AMP
<0.117 mg/Kg - dry 0.117 0.7114-Bromophenyl phenyl ether 1 10/03/23 18:58 V38621AMP
<0.121 mg/Kg - dry 0.121 0.355Butyl benzyl phthalate 1 10/03/23 18:58 V38621AMP
<0.099 mg/Kg - dry 0.099 0.7114-Chloro-3-methylphenol 1 10/03/23 18:58 V38621AMP
<0.120 mg/Kg - dry 0.120 0.3554-Chloroaniline 1 10/03/23 18:58 V38621AMP
<0.125 mg/Kg - dry 0.125 0.7112-Chloronaphthalene 1 10/03/23 18:58 V38621AMP
<0.105 mg/Kg - dry 0.105 0.7112-Chlorophenol 1 10/03/23 18:58 V38621AMP
<0.135 mg/Kg - dry 0.135 1.084-Chlorophenyl phenyl ether 1 10/03/23 18:58 V38621AMP
0.158 J
mg/Kg - dry 0.153 0.711
Chrysene 1 10/03/23 18:58 V38621AMP
<0.248 mg/Kg - dry 0.248 0.711Dibenz(a,h)anthracene 1 10/03/23 18:58 V38621AMP
<0.128 mg/Kg - dry 0.128 0.711Dibenzofuran 1 10/03/23 18:58 V38621AMP
<0.101 mg/Kg - dry 0.101 0.7111,2-Dichlorobenzene 1 10/03/23 18:58 V38621AMP
<0.104 mg/Kg - dry 0.104 0.7111,3-Dichlorobenzene 1 10/03/23 18:58 V38621AMP
<0.105 mg/Kg - dry 0.105 0.3551,4-Dichlorobenzene 1 10/03/23 18:58 V38621AMP
<0.158 mg/Kg - dry 0.158 0.7113,3'-Dichlorobenzidine 1 10/03/23 18:58 V38621AMP
<0.103 mg/Kg - dry 0.103 0.711
2,4-Dichlorophenol 1 10/03/23 18:58 V38621AMP
<0.194 mg/Kg - dry 0.194 0.711Diethyl phthalate 1 10/03/23 18:58 V38621AMP
<0.187 mg/Kg - dry 0.187 0.711Dimethyl phthalate 1 10/03/23 18:58 V38621AMP
<0.116 mg/Kg - dry 0.116 0.3552,4-Dimethylphenol 1 10/03/23 18:58 V38621AMP
<0.115 mg/Kg - dry 0.115 0.711Di-n-butyl phthalate 1 10/03/23 18:58 V38621AMP
<0.258 mg/Kg - dry 0.258 1.624,6-Dinitro-2-methylphenol 1 10/03/23 18:58 V38621AMP
<0.560 mg/Kg - dry 0.560 1.622,4-Dinitrophenol 1 10/03/23 18:58 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.104 mg/Kg - dry 0.104 0.7112,4-Dinitrotoluene 1 10/03/23 18:58 V38621AMP
<0.116 mg/Kg - dry 0.116 0.7112,6-Dinitrotoluene 1 10/03/23 18:58 V38621AMP
<0.154 mg/Kg - dry 0.154 0.355Di-n-Octyl Phthalate 1 10/03/23 18:58 V38621AMP
0.287 J mg/Kg - dry 0.132 0.711Fluoranthene 1 10/03/23 18:58 V38621AMP
<0.138 mg/Kg - dry 0.138 0.711Fluorene 1 10/03/23 18:58 V38621AMP
<0.114 mg/Kg - dry 0.114 0.711Hexachlorobenzene 1 10/03/23 18:58 V38621AMP
<0.105 mg/Kg - dry 0.105 0.711Hexachlorobutadiene 1 10/03/23 18:58 V38621AMP
<0.169 mg/Kg - dry 0.169 0.711Hexachlorocyclopentadiene 1 10/03/23 18:58 V38621AMP
<0.085 mg/Kg - dry 0.085 0.711
Hexachloroethane 1 10/03/23 18:58 V38621AMP
<0.193 mg/Kg - dry 0.193 0.711Indeno(1,2,3-cd)pyrene 1 10/03/23 18:58 V38621AMP
<0.205 mg/Kg - dry 0.205 0.711Isophorone 1 10/03/23 18:58 V38621AMP
<0.114 mg/Kg - dry 0.114 0.7111-Methylnaphthalene 1 10/03/23 18:58 V38621AMP
<0.107 mg/Kg - dry 0.107 0.7112-Methylnaphthalene 1 10/03/23 18:58 V38621AMP
<0.104 mg/Kg - dry 0.104 0.7112-Methylphenol 1 10/03/23 18:58 V38621AMP
<0.091 mg/Kg - dry 0.091 0.7113&4 Methylphenol 1 10/03/23 18:58 V38621AMP
<0.155 mg/Kg - dry 0.155 0.711
Naphthalene 1 10/03/23 18:58 V38621AMP
<0.104 mg/Kg - dry 0.104 0.7112-Nitroaniline 1 10/03/23 18:58 V38621AMP
<0.129 mg/Kg - dry 0.129 0.7113-Nitroaniline 1 10/03/23 18:58 V38621AMP
<0.100 mg/Kg - dry 0.100 0.3554-Nitroaniline 1 10/03/23 18:58 V38621AMP
<0.125 mg/Kg - dry 0.125 0.355Nitrobenzene 1 10/03/23 18:58 V38621AMP
<0.095 mg/Kg - dry 0.095 0.7112-Nitrophenol 1 10/03/23 18:58 V38621AMP
<0.126 mg/Kg - dry 0.126 0.7114-Nitrophenol 1 10/03/23 18:58 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-4
96407 Matrix:
9/26/2023 17:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.283 mg/Kg - dry 0.283 0.711N-Nitrosodimethylamine 1 10/03/23 18:58 V38621AMP
<0.195 mg/Kg - dry 0.195 0.711N-Nitrosodiphenylamine 1 10/03/23 18:58 V38621AMP
<0.127 mg/Kg - dry 0.127 0.711N-Nitroso-di-n-propylamine 1 10/03/23 18:58 V38621AMP
<0.374 mg/Kg - dry 0.374 1.08Pentachlorophenol 1 10/03/23 18:58 V38621AMP
<0.224 mg/Kg - dry 0.224 0.711Phenanthrene 1 10/03/23 18:58 V38621AMP
<0.120 mg/Kg - dry 0.120 0.711Phenol 1 10/03/23 18:58 V38621AMP
0.272 J mg/Kg - dry 0.144 0.711Pyrene 1 10/03/23 18:58 V38621AMP
<0.085 mg/Kg - dry 0.085 0.355Pyridine 1 10/03/23 18:58 V38621AMP
<0.115 mg/Kg - dry 0.115 0.711
1,2,4-Trichlorobenzene 1 10/03/23 18:58 V38621AMP
<0.103 mg/Kg - dry 0.103 0.7112,4,5-Trichlorophenol 1 10/03/23 18:58 V38621AMP
<0.104 mg/Kg - dry 0.104 0.7112,4,6-Trichlorophenol 1 10/03/23 18:58 V38621AMP
8270ESurrogate: Phenol-d5 82.0 Limits: 34-121%10/03/23 18:581 AMP
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%10/03/23 18:581 AMP V38621
Surrogate: 2-Fluorophenol 86.8 Limits: 35-115%10/03/23 18:581 AMP V38621
Surrogate: Nitrobenzene-d5 84.4 Limits: 37-122%10/03/23 18:581 AMP V38621
Surrogate: 4-Terphenyl-d14 91.6 Limits: 54-127%10/03/23 18:581 AMP V38621
Surrogate: 2,4,6-Tribromophenol 98.5 Limits: 39-132%10/03/23 18:581 AMP V38621
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-5
96408 Matrix:
9/26/2023 17:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.5 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-5
96408 Matrix:
9/26/2023 17:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V38557 10/02/23 09:20
90.8 mg/Kg - dry 5.78 12.4Diesel Range Organics (C10-C28)1 10/03/23 21:16 V38643NDL
8015C DROSurrogate: OTP Surrogate 65.3 Limits: 31-123%10/03/23 21:161 NDL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V38484 09/28/23 08:00
<2.57 mg/Kg - dry 2.57 6.21Gasoline Range Organics (C6-C10)50 09/29/23 03:00 V38485TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 109 Limits: 50-137%09/29/23 03:0050 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.5 %Moisture 1 09/28/23 14:48 SW-DRYWTCNC
1.04 mg/Kg - dry 0.162 0.230Chromium, Hexavalent 1 10/11/23 09:05 SW-7199SWB
2.47 mg/Kg - dry 0.0977 0.286Arsenic 5 10/02/23 19:00 6020BCPW
117 mg/Kg - dry 0.048 0.285Barium 5 10/02/23 19:00 6020BCPW
0.0745 J mg/Kg - dry 0.0297 0.286Cadmium 5 10/02/23 19:00 6020BCPW
19.3 mg/Kg - dry 0.132 0.285
Chromium 5 10/02/23 19:00 6020BCPW
12.8 mg/Kg - dry 0.0354 0.286Lead 5 10/02/23 19:00 6020BCPW
0.0832 mg/Kg - dry 0.0137 0.0343Mercury (Total)1 10/02/23 15:40 7471BJKC
0.643 mg/Kg - dry 0.117 0.285Selenium 5 10/02/23 19:00 6020BCPW
0.0449 J mg/Kg - dry 0.0077 0.286Silver 5 10/02/23 19:00 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
0.004 J mg/Kg - dry 0.002 0.022Acetone 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/27/23 20:51 V38481TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 09/27/23 20:51 V38481TBL
0.0008 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/27/23 20:51 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/27/23 20:51 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/27/23 20:51 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/27/23 20:51 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/27/23 20:51 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 09/27/23 20:51 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/27/23 20:51 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/27/23 20:51 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/27/23 20:51 V38481TBL
<0.016 mg/Kg - dry 0.016 0.285Ethanol 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.057Ethyl Tertiary Butyl Ether (ETBE)1 09/27/23 20:51 V38481TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 09/27/23 20:51 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 09/27/23 20:51 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/27/23 20:51 V38481TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 09/27/23 20:51 V38481TBL
0.003 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/27/23 20:51 V38481TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 09/27/23 20:51 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 09/27/23 20:51 V38481TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/27/23 20:51 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 09/27/23 20:51 V38481TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 09/27/23 20:51 V38481TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/27/23 20:51 V38481TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38480 09/28/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 09/27/23 20:51 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 09/27/23 20:51 V38481TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 09/27/23 20:51 V38481TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 09/27/23 20:51 V38481TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 09/27/23 20:51 V38481
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/27/23 20:511 TBL V38481
Surrogate: Dibromofluoromethane 104 Limits: 84-123%09/27/23 20:511 TBL V38481
Surrogate: Toluene-d8 97.3 Limits: 76-129%09/27/23 20:511 TBL V38481
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.132 mg/Kg - dry 0.132 0.754Acenaphthene 1 10/03/23 18:13 V38621AMP
<0.120 mg/Kg - dry 0.120 0.754Acenaphthylene 1 10/03/23 18:13 V38621AMP
<0.173 mg/Kg - dry 0.173 0.754Aniline 1 10/03/23 18:13 V38621AMP
<0.163 mg/Kg - dry 0.163 0.754Anthracene 1 10/03/23 18:13 V38621AMP
0.285 J
mg/Kg - dry 0.158 0.754
Benzo(a)anthracene 1 10/03/23 18:13 V38621AMP
0.323 J mg/Kg - dry 0.168 0.754Benzo(a)pyrene 1 10/03/23 18:13 V38621AMP
0.389 J mg/Kg - dry 0.166 0.754Benzo(b)fluoranthene 1 10/03/23 18:13 V38621AMP
0.218 J mg/Kg - dry 0.155 0.754Benzo(g,h,i)perylene 1 10/03/23 18:13 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.156 mg/Kg - dry 0.156 0.754Benzo(k)fluoranthene 1 10/03/23 18:13 V38621AMP
<0.662 mg/Kg - dry 0.662 2.29Benzoic Acid 1 10/03/23 18:13 V38621AMP
<0.120 mg/Kg - dry 0.120 0.754Benzyl alcohol 1 10/03/23 18:13 V38621AMP
<0.134 mg/Kg - dry 0.134 0.754Bis(2-Chloroethoxy)methane 1 10/03/23 18:13 V38621AMP
<0.122 mg/Kg - dry 0.122 0.754Bis(2-Chloroethyl)ether 1 10/03/23 18:13 V38621AMP
<0.155 mg/Kg - dry 0.155 0.377Bis(2-Chloroisopropyl)ether 1 10/03/23 18:13 V38621AMP
<0.137 mg/Kg - dry 0.137 0.754Bis(2-ethylhexyl)phthalate 1 10/03/23 18:13 V38621AMP
<0.124 mg/Kg - dry 0.124 0.7544-Bromophenyl phenyl ether 1 10/03/23 18:13 V38621AMP
<0.129 mg/Kg - dry 0.129 0.377
Butyl benzyl phthalate 1 10/03/23 18:13 V38621AMP
<0.105 mg/Kg - dry 0.105 0.7544-Chloro-3-methylphenol 1 10/03/23 18:13 V38621AMP
<0.128 mg/Kg - dry 0.128 0.3774-Chloroaniline 1 10/03/23 18:13 V38621AMP
<0.132 mg/Kg - dry 0.132 0.7542-Chloronaphthalene 1 10/03/23 18:13 V38621AMP
<0.112 mg/Kg - dry 0.112 0.7542-Chlorophenol 1 10/03/23 18:13 V38621AMP
<0.144 mg/Kg - dry 0.144 1.144-Chlorophenyl phenyl ether 1 10/03/23 18:13 V38621AMP
0.308 J mg/Kg - dry 0.162 0.754Chrysene 1 10/03/23 18:13 V38621AMP
<0.262 mg/Kg - dry 0.262 0.754
Dibenz(a,h)anthracene 1 10/03/23 18:13 V38621AMP
<0.136 mg/Kg - dry 0.136 0.754Dibenzofuran 1 10/03/23 18:13 V38621AMP
<0.107 mg/Kg - dry 0.107 0.7541,2-Dichlorobenzene 1 10/03/23 18:13 V38621AMP
<0.111 mg/Kg - dry 0.111 0.7541,3-Dichlorobenzene 1 10/03/23 18:13 V38621AMP
<0.111 mg/Kg - dry 0.111 0.3771,4-Dichlorobenzene 1 10/03/23 18:13 V38621AMP
<0.168 mg/Kg - dry 0.168 0.7543,3'-Dichlorobenzidine 1 10/03/23 18:13 V38621AMP
<0.109 mg/Kg - dry 0.109 0.7542,4-Dichlorophenol 1 10/03/23 18:13 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.205 mg/Kg - dry 0.205 0.754Diethyl phthalate 1 10/03/23 18:13 V38621AMP
<0.198 mg/Kg - dry 0.198 0.754Dimethyl phthalate 1 10/03/23 18:13 V38621AMP
<0.123 mg/Kg - dry 0.123 0.3772,4-Dimethylphenol 1 10/03/23 18:13 V38621AMP
<0.122 mg/Kg - dry 0.122 0.754Di-n-butyl phthalate 1 10/03/23 18:13 V38621AMP
<0.274 mg/Kg - dry 0.274 1.714,6-Dinitro-2-methylphenol 1 10/03/23 18:13 V38621AMP
<0.594 mg/Kg - dry 0.594 1.712,4-Dinitrophenol 1 10/03/23 18:13 V38621AMP
<0.110 mg/Kg - dry 0.110 0.7542,4-Dinitrotoluene 1 10/03/23 18:13 V38621AMP
<0.123 mg/Kg - dry 0.123 0.7542,6-Dinitrotoluene 1 10/03/23 18:13 V38621AMP
<0.163 mg/Kg - dry 0.163 0.377
Di-n-Octyl Phthalate 1 10/03/23 18:13 V38621AMP
0.564 J mg/Kg - dry 0.140 0.754Fluoranthene 1 10/03/23 18:13 V38621AMP
<0.146 mg/Kg - dry 0.146 0.754Fluorene 1 10/03/23 18:13 V38621AMP
<0.121 mg/Kg - dry 0.121 0.754Hexachlorobenzene 1 10/03/23 18:13 V38621AMP
<0.111 mg/Kg - dry 0.111 0.754Hexachlorobutadiene 1 10/03/23 18:13 V38621AMP
<0.179 mg/Kg - dry 0.179 0.754Hexachlorocyclopentadiene 1 10/03/23 18:13 V38621AMP
<0.090 mg/Kg - dry 0.090 0.754Hexachloroethane 1 10/03/23 18:13 V38621AMP
0.232 J
mg/Kg - dry 0.204 0.754
Indeno(1,2,3-cd)pyrene 1 10/03/23 18:13 V38621AMP
<0.218 mg/Kg - dry 0.218 0.754Isophorone 1 10/03/23 18:13 V38621AMP
<0.121 mg/Kg - dry 0.121 0.7541-Methylnaphthalene 1 10/03/23 18:13 V38621AMP
<0.114 mg/Kg - dry 0.114 0.7542-Methylnaphthalene 1 10/03/23 18:13 V38621AMP
<0.110 mg/Kg - dry 0.110 0.7542-Methylphenol 1 10/03/23 18:13 V38621AMP
<0.097 mg/Kg - dry 0.097 0.7543&4 Methylphenol 1 10/03/23 18:13 V38621AMP
<0.164 mg/Kg - dry 0.164 0.754Naphthalene 1 10/03/23 18:13 V38621AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Piping-6
96409 Matrix:
9/26/2023 17:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V38566 10/02/23 12:00
<0.110 mg/Kg - dry 0.110 0.7542-Nitroaniline 1 10/03/23 18:13 V38621AMP
<0.137 mg/Kg - dry 0.137 0.7543-Nitroaniline 1 10/03/23 18:13 V38621AMP
<0.106 mg/Kg - dry 0.106 0.3774-Nitroaniline 1 10/03/23 18:13 V38621AMP
<0.132 mg/Kg - dry 0.132 0.377Nitrobenzene 1 10/03/23 18:13 V38621AMP
<0.101 mg/Kg - dry 0.101 0.7542-Nitrophenol 1 10/03/23 18:13 V38621AMP
<0.133 mg/Kg - dry 0.133 0.7544-Nitrophenol 1 10/03/23 18:13 V38621AMP
<0.300 mg/Kg - dry 0.300 0.754N-Nitrosodimethylamine 1 10/03/23 18:13 V38621AMP
<0.206 mg/Kg - dry 0.206 0.754N-Nitrosodiphenylamine 1 10/03/23 18:13 V38621AMP
<0.134 mg/Kg - dry 0.134 0.754
N-Nitroso-di-n-propylamine 1 10/03/23 18:13 V38621AMP
<0.396 mg/Kg - dry 0.396 1.14Pentachlorophenol 1 10/03/23 18:13 V38621AMP
0.298 J mg/Kg - dry 0.237 0.754Phenanthrene 1 10/03/23 18:13 V38621AMP
<0.128 mg/Kg - dry 0.128 0.754Phenol 1 10/03/23 18:13 V38621AMP
0.513 J mg/Kg - dry 0.153 0.754Pyrene 1 10/03/23 18:13 V38621AMP
<0.090 mg/Kg - dry 0.090 0.377Pyridine 1 10/03/23 18:13 V38621AMP
<0.122 mg/Kg - dry 0.122 0.7541,2,4-Trichlorobenzene 1 10/03/23 18:13 V38621AMP
<0.109 mg/Kg - dry 0.109 0.754
2,4,5-Trichlorophenol 1 10/03/23 18:13 V38621AMP
<0.110 mg/Kg - dry 0.110 0.7542,4,6-Trichlorophenol 1 10/03/23 18:13 V38621AMP
8270ESurrogate: Phenol-d5 79.0 Limits: 34-121%10/03/23 18:131 AMP
Surrogate: 2-Fluorobiphenyl 86.2 Limits: 44-115%10/03/23 18:131 AMP V38621
Surrogate: 2-Fluorophenol 84.1 Limits: 35-115%10/03/23 18:131 AMP V38621
Surrogate: Nitrobenzene-d5 79.0 Limits: 37-122%10/03/23 18:131 AMP V38621
Surrogate: 4-Terphenyl-d14 89.2 Limits: 54-127%10/03/23 18:131 AMP V38621
Surrogate: 2,4,6-Tribromophenol 91.3 Limits: 39-132%10/03/23 18:131 AMP V38621
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 114
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-270-0022
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Received : 09/27/2023
Standard Roll Coverings
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:UST-SW-NE
97349 Matrix:
9/26/2023 12:10
TCLP
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
LeachateTCLP Metals Extraction 1 10/09/23 15:40 SW-1311BMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
SW-3010A
6010D Prep Batch(es):V38917 10/11/23 14:10
<0.014 mg/L 0.014 0.050TCLP Arsenic 1 10/12/23 00:26 V38940BMP
1.04 mg/L 0.005 0.050TCLP Barium 1 10/17/23 03:24 V39132JKC
<0.0065 mg/L 0.0065 0.0150TCLP Cadmium 1 10/12/23 00:26 V38940BMP
0.020 J mg/L 0.012 0.025TCLP Chromium 1 10/12/23 00:26 V38940BMP
0.041 mg/L 0.008 0.030TCLP Lead 1 10/12/23 00:26 V38940BMP
<0.026 mg/L 0.026 0.100
TCLP Selenium 1 10/17/23 03:24 V39132JKC
<0.003 mg/L 0.003 0.025TCLP Silver 1 10/12/23 00:26 V38940BMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
7470A
7470A Prep Batch(es):V38903 10/11/23 13:40
0.0010 mg/L 0.00003 0.0002TCLP Mercury 1 10/11/23 16:55 V38928BMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Metals Analysis (TCLP)
6010D
V38940,V39132QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3010A
QC Prep:V38917
Associated Lab Samples: 97349
LRB-V38917 Matrix: TCLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/12/23 00:120.0500.014<0.014mg/LTCLP Arsenic
10/17/23 03:110.0500.005<0.005mg/LTCLP Barium
10/12/23 00:120.01500.0065<0.0065mg/LTCLP Cadmium
10/12/23 00:120.0250.012<0.012mg/LTCLP Chromium
10/12/23 00:120.0300.008<0.008mg/LTCLP Lead
10/17/23 03:110.1000.026<0.026mg/LTCLP Selenium
10/12/23 00:120.0250.003<0.003mg/LTCLP Silver
LCS-V38917Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.00.4770.500mg/LTCLP Arsenic 80-120
1105.485.00mg/LTCLP Barium 80-120
1090.5470.500mg/LTCLP Cadmium 80-120
1055.235.00mg/LTCLP Chromium 80-120
1080.5380.500mg/LTCLP Lead 80-120
99.00.4970.500mg/LTCLP Selenium 80-120
1060.5290.500mg/LTCLP Silver 80-120
V 97404-MS-V38917 V 97404-MSD-V38917Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.482 96.00.4680.5000.500<0.014mg/LTCLP Arsenic 94.0 75-125 2.9 20
6.27 1096.185.005.000.835mg/LTCLP Barium 107 75-125 1.4 20
0.558 1090.5550.5000.5000.0122mg/LTCLP Cadmium 109 75-125 0.5 20
5.25 1055.215.005.00<0.012mg/LTCLP Chromium 104 75-125 0.7 20
Page 1 of 38Date:10/17/2023 03:31 PM
Page 74 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Metals Analysis (TCLP)
6010D
V38940,V39132QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3010A
QC Prep:V38917
V 97404-MS-V38917 V 97404-MSD-V38917Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.769 1070.7620.5000.5000.232mg/LTCLP Lead 106 75-125 0.9 20
0.500 1000.4920.5000.500<0.026mg/LTCLP Selenium 98.0 75-125 1.6 20
0.535 1070.5280.5000.500<0.003mg/LTCLP Silver 106 75-125 1.3 20
V 97404-PDS-V38917Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/12/23 01:0295.01.19mg/LTCLP Arsenic
10/17/23 03:3310713.9mg/LTCLP Barium
10/12/23 01:021091.37mg/LTCLP Cadmium
10/12/23 01:0210513.1mg/LTCLP Chromium
10/12/23 01:021061.44mg/LTCLP Lead
10/17/23 03:3399.01.24mg/LTCLP Selenium
10/12/23 01:021061.33mg/LTCLP Silver
Page 2 of 38Date:10/17/2023 03:31 PM
Page 75 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Metals Analyses
6020B
L708292QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L707911
Associated Lab Samples: 96396, 96401, 96403, 96407, 96409
LRB-L707911 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/02/23 18:280.2500.0855<0.0855mg/KgArsenic
10/02/23 18:280.2500.042<0.042mg/KgBarium
10/02/23 18:280.2500.0260<0.0260mg/KgCadmium
10/02/23 18:280.2500.116<0.116mg/KgChromium
10/02/23 18:280.2500.0310<0.0310mg/KgLead
10/02/23 18:280.2500.103<0.103mg/KgSelenium
10/02/23 18:280.2500.0067<0.0067mg/KgSilver
LCS-L707911Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.02.142.50mg/KgArsenic 80-120
88.04.385.00mg/KgBarium 80-120
88.00.4420.500mg/KgCadmium 80-120
90.04.495.00mg/KgChromium 80-120
91.02.282.50mg/KgLead 80-120
86.04.295.00mg/KgSelenium 80-120
93.00.4640.500mg/KgSilver 80-120
V 96450-MS-L707911 V 96450-MSD-L707911Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
4.66 44.0*4.232.352.393.62mg/KgArsenic 26.0*75-125 9.6 80
82.7 0.0*1034.704.7797.1mg/KgBarium 126*75-125 21.8 80
0.839 83.00.7800.4700.4770.444mg/KgCadmium 72.0*75-125 7.2 80
46.1 82.037.94.704.7742.2mg/KgChromium 0.0*75-125 19.5 80
Page 3 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 76 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Metals Analyses
6020B
L708292QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L707911
V 96450-MS-L707911 V 96450-MSD-L707911Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
95.4 0.0*1012.352.39158mg/KgLead 0.0*75-125 5.7 80
4.05 72.0*3.854.704.770.625mg/KgSelenium 69.0*75-125 5.0 80
0.575 92.00.5290.4700.4770.135mg/KgSilver 84.0 75-125 8.3 80
V 96450-PDS-L707911Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/02/23 19:4192.01.45mg/KgArsenic
10/02/23 19:4187.010.6mg/KgBarium
10/02/23 19:4191.00.263mg/KgCadmium
10/02/23 19:4186.05.73mg/KgChromium
10/02/23 19:4191.015.5mg/KgLead
10/02/23 19:4191.02.29mg/KgSelenium
10/02/23 19:4193.00.241mg/KgSilver
Page 4 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 77 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA (TCLP)
7470A
V38928QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V38903
Associated Lab Samples: 97349
LRB-V38903 Matrix: TCLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/11/23 16:500.00020.00003<0.00003mg/LTCLP Mercury
LCS-V38903Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.00.00450.0046mg/LTCLP Mercury 80-120
V 97349-MS-V38903 V 97349-MSD-V38903Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.0071 130*0.00530.00460.00460.0010mg/LTCLP Mercury 92.0 80-120 29.0*20
V 97349-PDS-V38903Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/11/23 16:5792.00.0026mg/LTCLP Mercury
Page 5 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 78 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V38593QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V38536
Associated Lab Samples: 96396, 96401, 96403, 96407, 96409
LRB-V38536 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/02/23 14:210.03000.0120<0.0120mg/KgMercury (Total)
LCS-V38536Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1060.4400.417mg/KgMercury (Total)80-120
V 96332-MS-V38536 V 96332-MSD-V38536Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.465 92.00.4470.4170.4170.0832mg/KgMercury (Total)87.0 80-120 3.9 20
V 96332-PDS-V38536Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/02/23 14:541040.256mg/KgMercury (Total)
Page 6 of 38Date:10/17/2023 03:31 PM
Page 79 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V38475QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38444
Associated Lab Samples: 96395, 96396, 96397, 96398, 96399, 96400, 96401, 96402, 96404, 96405
LRB-V38444 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/29/23 10:5010.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
09/29/23 10:50OTP Surrogate (S)71.5 31-123
LCS-V38444 LCSD-V38444Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
68.2 10210167.166.7mg/KgDiesel Range Organics (C10-C28)46-126 1.6 20
78.974.7OTP Surrogate (S)31-123
Page 7 of 38Date:10/17/2023 03:31 PM
Page 80 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V38643QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38557
Associated Lab Samples: 96406, 96407, 96408
LRB-V38557 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/03/23 12:2110.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
10/03/23 12:21OTP Surrogate (S)76.6 31-123
LCS-V38557Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.464.366.7mg/KgDiesel Range Organics (C10-C28)46-126
67.2OTP Surrogate (S)31-123
V 96654-MS-V38557 V 96654-MSD-V38557Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
59.5 89.260.666.666.78.89mg/KgDiesel Range Organics (C10-C28)90.9 50-117 1.8 24
63.8OTP Surrogate (S)66.8 31-123
Page 8 of 38Date:10/17/2023 03:31 PM
Page 81 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V38485QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V38484
Associated Lab Samples: 96395, 96396, 96397, 96398, 96399, 96400, 96401, 96402, 96404, 96405, 96406, 96407, 96408
LRB-V38484 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 20:265.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
09/28/23 20:26a,a,a-Trifluorotoluene (S)120 50-137
LCS-V38484Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10552.550.0mg/KgGasoline Range Organics (C6-C10)41-138
121a,a,a-Trifluorotoluene (S)50-137
V 96395-MS-V38484 V 96395-MSD-V38484Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
55.5 11157.150.050.0<2.07mg/KgGasoline Range Organics (C6-C10)114 41-138 2.8 34
130a,a,a-Trifluorotoluene (S)137 50-137
Page 9 of 38Date:10/17/2023 03:31 PM
Page 82 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38480
Associated Lab Samples: 96396, 96401, 96407, 96409
LRB-V38480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/27/23 14:580.0200.002<0.002mg/KgAcetone
09/27/23 14:580.0200.001<0.001mg/KgAcrolein
09/27/23 14:580.0200.0008<0.0008mg/KgAcrylonitrile
09/27/23 14:580.0050.0006<0.0006mg/KgBenzene
09/27/23 14:580.0050.0005<0.0005mg/KgBromobenzene
09/27/23 14:580.0050.0008<0.0008mg/KgBromochloromethane
09/27/23 14:580.0050.001<0.001mg/KgBromodichloromethane
09/27/23 14:580.0050.001<0.001mg/KgBromoform
09/27/23 14:580.0100.001<0.001mg/KgBromomethane
09/27/23 14:580.0050.0005<0.0005mg/Kgn-Butylbenzene
09/27/23 14:580.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/27/23 14:580.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/27/23 14:580.0050.0006<0.0006mg/KgCarbon Disulfide
09/27/23 14:580.0050.001<0.001mg/KgCarbon Tetrachloride
09/27/23 14:580.0050.0007<0.0007mg/KgChlorobenzene
09/27/23 14:580.0050.0009<0.0009mg/KgChlorodibromomethane
09/27/23 14:580.0100.0009<0.0009mg/KgChloroethane
09/27/23 14:580.0050.001<0.001mg/KgChloroform
09/27/23 14:580.0100.0006<0.0006mg/KgChloromethane
09/27/23 14:580.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/27/23 14:580.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/27/23 14:580.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/27/23 14:580.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/27/23 14:580.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/27/23 14:580.0050.0006<0.0006mg/KgDibromomethane
09/27/23 14:580.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/27/23 14:580.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 38Date:10/17/2023 03:31 PM
Page 83 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38480
Associated Lab Samples: 96396, 96401, 96407, 96409
LRB-V38480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/27/23 14:580.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/27/23 14:580.0100.001<0.001mg/KgDichlorodifluoromethane
09/27/23 14:580.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/27/23 14:580.0050.001<0.001mg/Kg1,2-Dichloroethane
09/27/23 14:580.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/27/23 14:580.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/27/23 14:580.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/27/23 14:580.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/27/23 14:580.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/27/23 14:580.0050.001<0.001mg/Kg2,2-Dichloropropane
09/27/23 14:580.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/27/23 14:580.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/27/23 14:580.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/27/23 14:580.2500.014<0.014mg/KgEthanol
09/27/23 14:580.0050.0006<0.0006mg/KgEthylbenzene
09/27/23 14:580.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/27/23 14:580.0100.0008<0.0008mg/KgHexachlorobutadiene
09/27/23 14:580.0100.0007<0.0007mg/Kgn-Hexane
09/27/23 14:580.0200.0006<0.0006mg/Kg2-Hexanone
09/27/23 14:580.0050.0005<0.0005mg/KgIsopropylbenzene
09/27/23 14:580.0050.001<0.001mg/Kg4-Isopropyl toluene
09/27/23 14:580.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/27/23 14:580.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/27/23 14:580.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/27/23 14:580.0100.001<0.001mg/KgMethylene Chloride
09/27/23 14:580.0100.0010<0.0010mg/KgNaphthalene
09/27/23 14:580.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 11 of 38Date:10/17/2023 03:31 PM
Page 84 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38480
Associated Lab Samples: 96396, 96401, 96407, 96409
LRB-V38480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/27/23 14:580.0050.001<0.001mg/KgStyrene
09/27/23 14:580.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/27/23 14:580.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/27/23 14:580.0050.0009<0.0009mg/KgTetrachloroethene
09/27/23 14:580.0050.0007<0.0007mg/KgToluene
09/27/23 14:580.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/27/23 14:580.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/27/23 14:580.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/27/23 14:580.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/27/23 14:580.0050.0009<0.0009mg/KgTrichloroethene
09/27/23 14:580.0100.002<0.002mg/KgTrichlorofluoromethane
09/27/23 14:580.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/27/23 14:580.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/27/23 14:580.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/27/23 14:580.0100.0005<0.0005mg/KgVinyl Acetate
09/27/23 14:580.0100.0005<0.0005mg/KgVinyl Chloride
09/27/23 14:580.0050.0005<0.0005mg/Kgo-Xylene
09/27/23 14:580.0100.001<0.001mg/Kgm,p-Xylene
09/27/23 14:584-Bromofluorobenzene (S)97.4 70-130
09/27/23 14:58Dibromofluoromethane (S)102 84-123
09/27/23 14:58Toluene-d8 (S)99.2 76-129
LCS-V38480 LCSD-V38480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.125 1251170.1170.100mg/KgAcetone 29-198 6.6 20
Page 12 of 38Date:10/17/2023 03:31 PM
Page 85 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38480
LCS-V38480 LCSD-V38480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.115 1151100.1100.100mg/KgAcrolein 70-130 4.4 20
0.113 1131010.1010.100mg/KgAcrylonitrile 65-134 11.2 20
0.049 98.497.20.0480.050mg/KgBenzene 74-127 1.2 20
0.051 1021020.0500.050mg/KgBromobenzene 73-125 0.1 20
0.049 98.294.00.0470.050mg/KgBromochloromethane 72-134 4.3 20
0.051 10299.20.0490.050mg/KgBromodichloromethane 75-122 2.9 20
0.051 10399.20.0490.050mg/KgBromoform 66-135 3.7 20
0.047 95.092.40.0460.050mg/KgBromomethane 20-180 2.7 20
0.050 1011040.0520.050mg/Kgn-Butylbenzene 65-135 2.9 20
0.047 95.497.80.0480.050mg/Kgsec-Butyl benzene 66-131 2.4 20
0.047 95.497.20.0480.050mg/Kgtert-Butyl benzene 67-132 1.8 20
0.048 96.297.80.0480.050mg/KgCarbon Disulfide 61-129 1.6 20
0.041 83.095.20.0470.050mg/KgCarbon Tetrachloride 64-143 13.6 20
0.049 99.498.80.0490.050mg/KgChlorobenzene 74-118 0.6 20
0.050 10199.80.0490.050mg/KgChlorodibromomethane 73-122 0.9 20
0.046 93.296.20.0480.050mg/KgChloroethane 33-149 3.1 20
0.049 98.495.60.0470.050mg/KgChloroform 73-127 2.8 20
0.047 95.894.80.0470.050mg/KgChloromethane 45-143 1.0 20
0.048 97.499.00.0490.050mg/Kg2-Chlorotoluene 67-124 1.6 20
0.048 97.499.00.0490.050mg/Kg4-Chlorotoluene 71-126 1.6 20
0.051 1031000.0500.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.3 20
0.054 1081030.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.9 20
0.053 1061040.0510.050mg/Kg1,2-Dibromoethane 70-132 2.0 20
0.054 1081030.0510.050mg/KgDibromomethane 74-133 4.3 20
0.049 99.898.40.0490.050mg/Kg1,2-Dichlorobenzene 72-123 1.4 20
0.049 99.498.60.0490.050mg/Kg1,3-Dichlorobenzene 71-120 0.8 20
Page 13 of 38Date:10/17/2023 03:31 PM
Page 86 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38480
LCS-V38480 LCSD-V38480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 96.896.40.0480.050mg/Kg1,4-Dichlorobenzene 71-123 0.4 20
0.039 79.681.20.0400.050mg/KgDichlorodifluoromethane 26-146 1.9 20
0.050 10197.40.0480.050mg/Kg1,1-Dichloroethane 74-127 3.6 20
0.051 10497.20.0480.050mg/Kg1,2-Dichloroethane 68-128 6.3 20
0.048 96.698.00.0490.050mg/Kg1,1-Dichloroethene 67-149 1.4 20
0.051 1031000.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 2.7 20
0.051 1021000.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 2.1 20
0.052 1041020.0510.050mg/Kg1,2-Dichloropropane 73-130 1.9 20
0.052 1061020.0510.050mg/Kg1,3-Dichloropropane 75-124 3.6 20
0.048 96.897.20.0480.050mg/Kg2,2-Dichloropropane 50-142 0.4 20
0.048 96.899.80.0490.050mg/Kg1,1-Dichloropropene 71-130 3.0 20
0.053 1061050.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 1.3 20
0.055 1111050.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 5.1 20
1.24 99.21001.251.25mg/KgEthanol 70-130 0.8 20
0.048 96.096.40.0480.050mg/KgEthylbenzene 74-128 0.4 20
0.101 10196.80.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.2 20
0.049 98.099.40.0490.050mg/KgHexachlorobutadiene 64-125 1.4 20
0.048 96.61020.0500.050mg/Kgn-Hexane 70-130 5.0 20
0.054 1081070.0530.050mg/Kg2-Hexanone 61-157 1.1 20
0.047 95.897.80.0480.050mg/KgIsopropylbenzene 68-126 2.0 20
0.048 96.298.00.0490.050mg/Kg4-Isopropyl toluene 68-129 1.8 20
0.053 1061040.0510.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.4 20
0.049 99.693.80.0460.050mg/KgMethyl tert-butyl ether (MTBE)70-130 5.9 20
0.053 1061080.0540.050mg/Kg4-Methyl-2-Pentanone 57-162 2.0 20
0.048 97.095.20.0470.050mg/KgMethylene Chloride 74-129 1.8 20
0.054 1081010.0500.050mg/KgNaphthalene 57-157 7.2 20
Page 14 of 38Date:10/17/2023 03:31 PM
Page 87 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38480
LCS-V38480 LCSD-V38480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 98.21010.0500.050mg/Kgn-Propylbenzene 67-130 2.4 20
0.052 1051010.0500.050mg/KgStyrene 77-121 3.2 20
0.048 97.496.80.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.6 20
0.052 1041000.0500.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.5 20
0.046 92.693.00.0460.050mg/KgTetrachloroethene 68-130 0.4 20
0.048 97.498.00.0490.050mg/KgToluene 71-129 0.6 20
0.055 1121070.0530.050mg/Kg1,2,3-Trichlorobenzene 68-130 4.3 20
0.054 1081070.0530.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.1 20
0.046 93.692.00.0460.050mg/Kg1,1,1-Trichloroethane 67-131 1.7 20
0.051 1041030.0510.050mg/Kg1,1,2-Trichloroethane 70-133 0.7 20
0.047 95.697.60.0480.050mg/KgTrichloroethene 75-133 2.0 20
0.043 86.889.20.0440.050mg/KgTrichlorofluoromethane 44-146 2.7 20
0.049 99.896.00.0480.050mg/Kg1,2,3-Trichloropropane 60-137 3.8 20
0.049 98.899.40.0490.050mg/Kg1,2,4-Trimethylbenzene 69-129 0.6 20
0.049 98.899.80.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.0 20
0.051 10298.40.0490.050mg/KgVinyl Acetate 60-140 3.9 20
0.046 93.295.80.0470.050mg/KgVinyl Chloride 48-147 2.7 20
0.050 1001010.0500.050mg/Kgo-Xylene 74-126 0.5 20
0.098 98.41010.1010.100mg/Kgm,p-Xylene 75-124 2.6 20
98.898.04-Bromofluorobenzene (S)70-130
99.697.8Dibromofluoromethane (S)84-123
101101Toluene-d8 (S)76-129
Page 15 of 38Date:10/17/2023 03:31 PM
Page 88 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38509QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38508
Associated Lab Samples: 96403
LRB-V38508 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 18:590.0200.002<0.002mg/KgAcetone
09/28/23 18:590.0200.001<0.001mg/KgAcrolein
09/28/23 18:590.0200.0008<0.0008mg/KgAcrylonitrile
09/28/23 18:590.0050.0006<0.0006mg/KgBenzene
09/28/23 18:590.0050.0005<0.0005mg/KgBromobenzene
09/28/23 18:590.0050.0008<0.0008mg/KgBromochloromethane
09/28/23 18:590.0050.001<0.001mg/KgBromodichloromethane
09/28/23 18:590.0050.001<0.001mg/KgBromoform
09/28/23 18:590.0100.001<0.001mg/KgBromomethane
09/28/23 18:590.0050.0005<0.0005mg/Kgn-Butylbenzene
09/28/23 18:590.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/28/23 18:590.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/28/23 18:590.0050.0006<0.0006mg/KgCarbon Disulfide
09/28/23 18:590.0050.001<0.001mg/KgCarbon Tetrachloride
09/28/23 18:590.0050.0007<0.0007mg/KgChlorobenzene
09/28/23 18:590.0050.0009<0.0009mg/KgChlorodibromomethane
09/28/23 18:590.0100.0009<0.0009mg/KgChloroethane
09/28/23 18:590.0050.001<0.001mg/KgChloroform
09/28/23 18:590.0100.0006<0.0006mg/KgChloromethane
09/28/23 18:590.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/28/23 18:590.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/28/23 18:590.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/28/23 18:590.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/28/23 18:590.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/28/23 18:590.0050.0006<0.0006mg/KgDibromomethane
09/28/23 18:590.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/28/23 18:590.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 16 of 38Date:10/17/2023 03:31 PM
Page 89 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38509QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38508
Associated Lab Samples: 96403
LRB-V38508 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 18:590.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/28/23 18:590.0100.001<0.001mg/KgDichlorodifluoromethane
09/28/23 18:590.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/28/23 18:590.0050.001<0.001mg/Kg1,2-Dichloroethane
09/28/23 18:590.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/28/23 18:590.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/28/23 18:590.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/28/23 18:590.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/28/23 18:590.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/28/23 18:590.0050.001<0.001mg/Kg2,2-Dichloropropane
09/28/23 18:590.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/28/23 18:590.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/28/23 18:590.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/28/23 18:590.2500.014<0.014mg/KgEthanol
09/28/23 18:590.0050.0006<0.0006mg/KgEthylbenzene
09/28/23 18:590.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/28/23 18:590.0100.0008<0.0008mg/KgHexachlorobutadiene
09/28/23 18:590.0100.0007<0.0007mg/Kgn-Hexane
09/28/23 18:590.0200.0006<0.0006mg/Kg2-Hexanone
09/28/23 18:590.0050.0005<0.0005mg/KgIsopropylbenzene
09/28/23 18:590.0050.001<0.001mg/Kg4-Isopropyl toluene
09/28/23 18:590.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/28/23 18:590.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/28/23 18:590.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/28/23 18:590.0100.001<0.001mg/KgMethylene Chloride
09/28/23 18:590.0100.0010<0.0010mg/KgNaphthalene
09/28/23 18:590.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 17 of 38Date:10/17/2023 03:31 PM
Page 90 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38509QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38508
Associated Lab Samples: 96403
LRB-V38508 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 18:590.0050.001<0.001mg/KgStyrene
09/28/23 18:590.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/28/23 18:590.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/28/23 18:590.0050.0009<0.0009mg/KgTetrachloroethene
09/28/23 18:590.0050.0007<0.0007mg/KgToluene
09/28/23 18:590.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/28/23 18:590.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/28/23 18:590.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/28/23 18:590.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/28/23 18:590.0050.0009<0.0009mg/KgTrichloroethene
09/28/23 18:590.0100.002<0.002mg/KgTrichlorofluoromethane
09/28/23 18:590.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/28/23 18:590.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/28/23 18:590.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/28/23 18:590.0100.0005<0.0005mg/KgVinyl Acetate
09/28/23 18:590.0100.0005<0.0005mg/KgVinyl Chloride
09/28/23 18:590.0050.0005<0.0005mg/Kgo-Xylene
09/28/23 18:590.0100.001<0.001mg/Kgm,p-Xylene
09/28/23 18:594-Bromofluorobenzene (S)99.4 70-130
09/28/23 18:59Dibromofluoromethane (S)103 84-123
09/28/23 18:59Toluene-d8 (S)96.2 76-129
LCS-V38508 LCSD-V38508Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.126 1261210.1210.100mg/KgAcetone 29-198 4.0 20
Page 18 of 38Date:10/17/2023 03:31 PM
Page 91 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38509QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38508
LCS-V38508 LCSD-V38508Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.132 132*1160.1160.100mg/KgAcrolein 70-130 12.9 20
0.124 1241130.1130.100mg/KgAcrylonitrile 65-134 9.2 20
0.042 84.691.40.0450.050mg/KgBenzene 74-127 7.7 20
0.042 85.288.20.0440.050mg/KgBromobenzene 73-125 3.4 20
0.047 94.098.20.0490.050mg/KgBromochloromethane 72-134 4.3 20
0.047 94.61000.0500.050mg/KgBromodichloromethane 75-122 5.9 20
0.053 1071060.0520.050mg/KgBromoform 66-135 1.3 20
0.047 94.81000.0500.050mg/KgBromomethane 20-180 5.7 20
0.042 85.493.60.0460.050mg/Kgn-Butylbenzene 65-135 9.1 20
0.041 82.089.60.0440.050mg/Kgsec-Butyl benzene 66-131 8.8 20
0.041 82.692.40.0460.050mg/Kgtert-Butyl benzene 67-132 11.2 20
0.040 81.088.60.0440.050mg/KgCarbon Disulfide 61-129 8.9 20
0.044 88.886.60.0430.050mg/KgCarbon Tetrachloride 64-143 2.5 20
0.043 87.492.80.0460.050mg/KgChlorobenzene 74-118 5.9 20
0.051 10299.40.0490.050mg/KgChlorodibromomethane 73-122 2.7 20
0.045 90.498.40.0490.050mg/KgChloroethane 33-149 8.4 20
0.044 89.696.00.0480.050mg/KgChloroform 73-127 6.8 20
0.042 84.082.20.0410.050mg/KgChloromethane 45-143 2.1 20
0.041 83.086.80.0430.050mg/Kg2-Chlorotoluene 67-124 4.4 20
0.041 83.086.80.0430.050mg/Kg4-Chlorotoluene 71-126 4.4 20
0.045 90.289.80.0440.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.4 20
0.054 1091070.0530.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.6 20
0.052 1051030.0510.050mg/Kg1,2-Dibromoethane 70-132 2.4 20
0.050 1011030.0510.050mg/KgDibromomethane 74-133 1.9 20
0.044 89.894.20.0470.050mg/Kg1,2-Dichlorobenzene 72-123 4.7 20
0.044 89.896.40.0480.050mg/Kg1,3-Dichlorobenzene 71-120 7.0 20
Page 19 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 92 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38509QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38508
LCS-V38508 LCSD-V38508Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.092.80.0460.050mg/Kg1,4-Dichlorobenzene 71-123 6.4 20
0.034 69.878.40.0390.050mg/KgDichlorodifluoromethane 26-146 11.6 20
0.043 87.492.20.0460.050mg/Kg1,1-Dichloroethane 74-127 5.3 20
0.048 96.699.20.0490.050mg/Kg1,2-Dichloroethane 68-128 2.6 20
0.039 79.089.00.0440.050mg/Kg1,1-Dichloroethene 67-149 11.9 20
0.044 88.292.60.0460.050mg/Kgcis-1,2-Dichloroethene 76-134 4.8 20
0.046 92.690.60.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 2.1 20
0.043 87.090.80.0450.050mg/Kg1,2-Dichloropropane 73-130 4.2 20
0.050 10094.40.0470.050mg/Kg1,3-Dichloropropane 75-124 6.1 20
0.043 87.696.60.0480.050mg/Kg2,2-Dichloropropane 50-142 9.7 20
0.041 82.492.20.0460.050mg/Kg1,1-Dichloropropene 71-130 11.2 20
0.045 91.61000.0500.050mg/Kgcis-1,3-Dichloropropene 71-125 8.7 20
0.052 1051060.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.1 20
1.16 92.890.41.131.25mg/KgEthanol 70-130 2.6 20
0.043 86.491.40.0450.050mg/KgEthylbenzene 74-128 5.6 20
0.093 93.993.00.0930.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.045 90.898.60.0490.050mg/KgHexachlorobutadiene 64-125 8.2 20
0.044 88.892.40.0460.050mg/Kgn-Hexane 70-130 3.9 20
0.052 10496.80.0480.050mg/Kg2-Hexanone 61-157 7.1 20
0.041 82.288.20.0440.050mg/KgIsopropylbenzene 68-126 7.0 20
0.042 84.693.00.0460.050mg/Kg4-Isopropyl toluene 68-129 9.4 20
0.047 94.295.40.0470.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.2 20
0.051 10296.40.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 5.8 20
0.053 1061040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 2.2 20
0.048 96.287.60.0430.050mg/KgMethylene Chloride 74-129 9.3 20
0.050 1001010.0500.050mg/KgNaphthalene 57-157 0.7 20
Page 20 of 38Date:10/17/2023 03:31 PM
Page 93 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38509QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38508
LCS-V38508 LCSD-V38508Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.089.20.0440.050mg/Kgn-Propylbenzene 67-130 7.2 20
0.046 93.697.00.0480.050mg/KgStyrene 77-121 3.5 20
0.045 91.295.40.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.5 20
0.047 94.291.60.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.7 20
0.045 90.895.40.0470.050mg/KgTetrachloroethene 68-130 4.9 20
0.043 86.494.40.0470.050mg/KgToluene 71-129 8.8 20
0.050 1021060.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.8 20
0.050 1001050.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 4.8 20
0.044 88.695.40.0470.050mg/Kg1,1,1-Trichloroethane 67-131 7.3 20
0.050 10196.80.0480.050mg/Kg1,1,2-Trichloroethane 70-133 4.6 20
0.044 89.894.80.0470.050mg/KgTrichloroethene 75-133 5.4 20
0.042 85.494.60.0470.050mg/KgTrichlorofluoromethane 44-146 10.2 20
0.047 94.495.40.0470.050mg/Kg1,2,3-Trichloropropane 60-137 1.0 20
0.043 86.090.80.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 5.4 20
0.042 84.889.20.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.0 20
0.056 1131090.0540.050mg/KgVinyl Acetate 60-140 3.9 20
0.041 82.483.40.0410.050mg/KgVinyl Chloride 48-147 1.2 20
0.044 89.292.20.0460.050mg/Kgo-Xylene 74-126 3.3 20
0.085 85.392.30.0920.100mg/Kgm,p-Xylene 75-124 7.8 20
10099.44-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
94.497.4Toluene-d8 (S)76-129
Page 21 of 38Date:10/17/2023 03:31 PM
Page 94 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38472QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38445
Associated Lab Samples: 96396
LRB-V38445 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/29/23 15:530.6600.116<0.116mg/KgAcenaphthene
09/29/23 15:530.6600.105<0.105mg/KgAcenaphthylene
09/29/23 15:530.6600.152<0.152mg/KgAniline
09/29/23 15:530.6600.143<0.143mg/KgAnthracene
09/29/23 15:530.6600.139<0.139mg/KgBenzo(a)anthracene
09/29/23 15:530.6600.147<0.147mg/KgBenzo(a)pyrene
09/29/23 15:530.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/29/23 15:530.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/29/23 15:530.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/29/23 15:532.000.580<0.580mg/KgBenzoic Acid
09/29/23 15:530.6600.105<0.105mg/KgBenzyl alcohol
09/29/23 15:530.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/29/23 15:530.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/29/23 15:530.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/29/23 15:530.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/29/23 15:530.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/29/23 15:530.3300.113<0.113mg/KgButyl benzyl phthalate
09/29/23 15:530.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/29/23 15:530.3300.112<0.112mg/Kg4-Chloroaniline
09/29/23 15:530.6600.116<0.116mg/Kg2-Chloronaphthalene
09/29/23 15:530.6600.098<0.098mg/Kg2-Chlorophenol
09/29/23 15:531.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/29/23 15:530.6600.142<0.142mg/KgChrysene
09/29/23 15:530.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/29/23 15:530.6600.119<0.119mg/KgDibenzofuran
09/29/23 15:530.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/29/23 15:530.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 22 of 38Date:10/17/2023 03:31 PM
Page 95 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38472QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38445
Associated Lab Samples: 96396
LRB-V38445 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/29/23 15:530.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/29/23 15:530.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/29/23 15:530.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/29/23 15:530.6600.180<0.180mg/KgDiethyl phthalate
09/29/23 15:530.6600.174<0.174mg/KgDimethyl phthalate
09/29/23 15:530.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/29/23 15:530.6600.107<0.107mg/KgDi-n-butyl phthalate
09/29/23 15:531.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/29/23 15:531.500.520<0.520mg/Kg2,4-Dinitrophenol
09/29/23 15:530.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/29/23 15:530.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/29/23 15:530.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/29/23 15:530.6600.123<0.123mg/KgFluoranthene
09/29/23 15:530.6600.128<0.128mg/KgFluorene
09/29/23 15:530.6600.106<0.106mg/KgHexachlorobenzene
09/29/23 15:530.6600.097<0.097mg/KgHexachlorobutadiene
09/29/23 15:530.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/29/23 15:530.6600.079<0.079mg/KgHexachloroethane
09/29/23 15:530.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/29/23 15:530.6600.191<0.191mg/KgIsophorone
09/29/23 15:530.6600.106<0.106mg/Kg1-Methylnaphthalene
09/29/23 15:530.6600.100<0.100mg/Kg2-Methylnaphthalene
09/29/23 15:530.6600.097<0.097mg/Kg2-Methylphenol
09/29/23 15:530.6600.084<0.084mg/Kg3&4 Methylphenol
09/29/23 15:530.6600.144<0.144mg/KgNaphthalene
09/29/23 15:530.6600.096<0.096mg/Kg2-Nitroaniline
09/29/23 15:530.6600.120<0.120mg/Kg3-Nitroaniline
Page 23 of 38Date:10/17/2023 03:31 PM
Page 96 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38472QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38445
Associated Lab Samples: 96396
LRB-V38445 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/29/23 15:530.3300.093<0.093mg/Kg4-Nitroaniline
09/29/23 15:530.3300.116<0.116mg/KgNitrobenzene
09/29/23 15:530.6600.088<0.088mg/Kg2-Nitrophenol
09/29/23 15:530.6600.117<0.117mg/Kg4-Nitrophenol
09/29/23 15:530.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/29/23 15:530.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/29/23 15:530.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/29/23 15:531.000.347<0.347mg/KgPentachlorophenol
09/29/23 15:530.6600.208<0.208mg/KgPhenanthrene
09/29/23 15:530.6600.112<0.112mg/KgPhenol
09/29/23 15:530.6600.134<0.134mg/KgPyrene
09/29/23 15:530.3300.079<0.079mg/KgPyridine
09/29/23 15:530.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/29/23 15:530.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/29/23 15:530.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/29/23 15:532-Fluorobiphenyl (S)91.0 44-115
09/29/23 15:532-Fluorophenol (S)83.4 35-115
09/29/23 15:53Nitrobenzene-d5 (S)83.8 37-122
09/29/23 15:534-Terphenyl-d14 (S)94.0 54-127
09/29/23 15:532,4,6-Tribromophenol (S)81.3 39-132
09/29/23 15:53Phenol-d5 (S)83.4 34-121
LCS-V38445 LCSD-V38445Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.52 91.090.41.511.67mg/KgAcenaphthene 40-123 0.6 20
Page 24 of 38Date:10/17/2023 03:31 PM
Page 97 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38472QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38445
LCS-V38445 LCSD-V38445Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.50 89.891.01.521.67mg/KgAcenaphthylene 32-132 1.3 20
2.00 1201131.891.67mg/KgAniline 12-197 5.6 20
1.64 98.296.41.611.67mg/KgAnthracene 47-123 1.8 20
1.56 93.491.61.531.67mg/KgBenzo(a)anthracene 49-126 1.9 20
1.89 1131131.891.67mg/KgBenzo(a)pyrene 45-129 0.0 20
1.78 1071071.781.67mg/KgBenzo(b)fluoranthene 45-132 0.0 20
1.72 1031021.711.67mg/KgBenzo(g,h,i)perylene 43-134 0.5 20
1.70 1021031.721.67mg/KgBenzo(k)fluoranthene 47-132 1.1 20
<0.580 0.0*0.0*<0.5801.67mg/KgBenzoic Acid 10-83 0.0 20
1.60 95.890.41.511.67mg/KgBenzyl alcohol 29-122 5.7 20
1.30 77.876.01.271.67mg/KgBis(2-Chloroethoxy)methane 36-121 2.3 20
1.25 74.872.41.211.67mg/KgBis(2-Chloroethyl)ether 31-120 3.2 20
1.37 82.079.61.331.67mg/KgBis(2-Chloroisopropyl)ether 33-131 2.9 20
1.81 1081071.781.67mg/KgBis(2-ethylhexyl)phthalate 51-133 1.6 20
1.53 91.690.41.511.67mg/Kg4-Bromophenyl phenyl ether 46-124 1.3 20
1.71 1021021.701.67mg/KgButyl benzyl phthalate 48-132 0.5 20
1.36 81.481.41.361.67mg/Kg4-Chloro-3-methylphenol 45-122 0.0 20
1.30 77.876.61.281.67mg/Kg4-Chloroaniline 17-106 1.5 20
1.54 92.292.81.551.67mg/Kg2-Chloronaphthalene 41-114 0.6 20
1.45 86.883.81.401.67mg/Kg2-Chlorophenol 34-121 3.5 20
1.51 90.489.21.491.67mg/Kg4-Chlorophenyl phenyl ether 45-121 1.3 20
1.66 99.497.01.621.67mg/KgChrysene 50-124 2.4 20
1.45 86.886.21.441.67mg/KgDibenz(a,h)anthracene 45-134 0.6 20
1.57 94.092.81.551.67mg/KgDibenzofuran 44-120 1.2 20
1.37 82.079.01.321.67mg/Kg1,2-Dichlorobenzene 33-117 3.7 20
1.33 79.677.21.291.67mg/Kg1,3-Dichlorobenzene 30-115 3.0 20
Page 25 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 98 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38472QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38445
LCS-V38445 LCSD-V38445Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.28 76.674.21.241.67mg/Kg1,4-Dichlorobenzene 31-115 3.1 20
1.27 76.071.81.201.67mg/Kg3,3'-Dichlorobenzidine 22-121 5.6 20
1.38 82.682.01.371.67mg/Kg2,4-Dichlorophenol 40-122 0.7 20
1.62 97.097.61.631.67mg/KgDiethyl phthalate 50-124 0.6 20
1.62 97.097.61.631.67mg/KgDimethyl phthalate 48-124 0.6 20
1.66 99.492.81.551.67mg/Kg2,4-Dimethylphenol 30-127 6.8 20
1.76 1051031.721.67mg/KgDi-n-butyl phthalate 51-128 2.2 20
1.65 98.892.81.551.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 6.2 20
1.07 64.053.40.8921.67mg/Kg2,4-Dinitrophenol 27-129 18.1 20
1.72 1031041.741.67mg/Kg2,4-Dinitrotoluene 48-126 1.1 20
1.70 1021011.691.67mg/Kg2,6-Dinitrotoluene 46-124 0.5 20
1.86 1111111.861.67mg/KgDi-n-Octyl Phthalate 45-140 0.0 20
1.63 97.696.41.611.67mg/KgFluoranthene 50-127 1.2 20
1.58 94.695.21.591.67mg/KgFluorene 43-125 0.6 20
1.62 97.097.01.621.67mg/KgHexachlorobenzene 45-122 0.0 20
1.33 79.678.41.311.67mg/KgHexachlorobutadiene 32-123 1.5 20
1.17 70.070.61.181.67mg/KgHexachlorocyclopentadiene 32-117 0.8 20
1.33 79.676.01.271.67mg/KgHexachloroethane 28-117 4.6 20
1.69 1011031.721.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 1.7 20
1.20 71.871.21.191.67mg/KgIsophorone 30-122 0.8 20
1.29 77.275.41.261.67mg/Kg1-Methylnaphthalene 40-119 2.3 20
1.31 78.477.81.301.67mg/Kg2-Methylnaphthalene 38-122 0.7 20
1.52 91.087.41.461.67mg/Kg2-Methylphenol 32-122 4.0 20
1.35 80.878.41.311.67mg/Kg3&4 Methylphenol 34-119 3.0 20
1.23 73.674.21.241.67mg/KgNaphthalene 35-123 0.8 20
1.55 92.895.81.601.67mg/Kg2-Nitroaniline 44-127 3.1 20
Page 26 of 38Date:10/17/2023 03:31 PM
Page 99 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38472QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38445
LCS-V38445 LCSD-V38445Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.51 90.491.01.521.67mg/Kg3-Nitroaniline 33-119 0.6 20
1.63 97.695.81.601.67mg/Kg4-Nitroaniline 63-147 1.8 20
1.24 74.274.81.251.67mg/KgNitrobenzene 34-122 0.8 20
1.29 77.276.01.271.67mg/Kg2-Nitrophenol 36-123 1.5 20
1.73 1041041.741.67mg/Kg4-Nitrophenol 30-132 0.5 20
1.22 73.071.21.191.67mg/KgN-Nitrosodimethylamine 10-146 2.4 20
1.90 1141111.861.67mg/KgN-Nitrosodiphenylamine 38-127 2.1 20
1.49 89.286.21.441.67mg/KgN-Nitroso-di-n-propylamine 36-120 3.4 20
1.80 1081071.781.67mg/KgPentachlorophenol 25-133 1.1 20
1.66 99.497.01.621.67mg/KgPhenanthrene 50-121 2.4 20
1.42 85.081.41.361.67mg/KgPhenol 34-121 4.3 20
1.63 97.697.61.631.67mg/KgPyrene 47-127 0.0 20
0.915 54.751.80.8661.67mg/KgPyridine 10-80 5.5 20
1.26 75.474.21.241.67mg/Kg1,2,4-Trichlorobenzene 34-118 1.6 20
1.50 89.891.01.521.67mg/Kg2,4,5-Trichlorophenol 41-124 1.3 20
1.52 91.092.21.541.67mg/Kg2,4,6-Trichlorophenol 39-126 1.3 20
88.689.22-Fluorobiphenyl (S)44-115
88.287.02-Fluorophenol (S)35-115
72.473.6Nitrobenzene-d5 (S)37-122
92.292.24-Terphenyl-d14 (S)54-127
97.597.52,4,6-Tribromophenol (S)39-132
85.583.4Phenol-d5 (S)34-121
Page 27 of 38Date:10/17/2023 03:31 PM
Page 100 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
Associated Lab Samples: 96401, 96403, 96407, 96409
LRB-V38566 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/03/23 12:330.6600.116<0.116mg/KgAcenaphthene
10/03/23 12:330.6600.105<0.105mg/KgAcenaphthylene
10/03/23 12:330.6600.152<0.152mg/KgAniline
10/03/23 12:330.6600.143<0.143mg/KgAnthracene
10/03/23 12:330.6600.139<0.139mg/KgBenzo(a)anthracene
10/03/23 12:330.6600.147<0.147mg/KgBenzo(a)pyrene
10/03/23 12:330.6600.146<0.146mg/KgBenzo(b)fluoranthene
10/03/23 12:330.6600.136<0.136mg/KgBenzo(g,h,i)perylene
10/03/23 12:330.6600.137<0.137mg/KgBenzo(k)fluoranthene
10/03/23 12:332.000.580<0.580mg/KgBenzoic Acid
10/03/23 12:330.6600.105<0.105mg/KgBenzyl alcohol
10/03/23 12:330.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
10/03/23 12:330.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
10/03/23 12:330.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
10/03/23 12:330.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
10/03/23 12:330.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
10/03/23 12:330.3300.113<0.113mg/KgButyl benzyl phthalate
10/03/23 12:330.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
10/03/23 12:330.3300.112<0.112mg/Kg4-Chloroaniline
10/03/23 12:330.6600.116<0.116mg/Kg2-Chloronaphthalene
10/03/23 12:330.6600.098<0.098mg/Kg2-Chlorophenol
10/03/23 12:331.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
10/03/23 12:330.6600.142<0.142mg/KgChrysene
10/03/23 12:330.6600.230<0.230mg/KgDibenz(a,h)anthracene
10/03/23 12:330.6600.119<0.119mg/KgDibenzofuran
10/03/23 12:330.6600.094<0.094mg/Kg1,2-Dichlorobenzene
10/03/23 12:330.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 28 of 38Date:10/17/2023 03:31 PM
Page 101 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
Associated Lab Samples: 96401, 96403, 96407, 96409
LRB-V38566 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/03/23 12:330.3300.097<0.097mg/Kg1,4-Dichlorobenzene
10/03/23 12:330.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
10/03/23 12:330.6600.095<0.095mg/Kg2,4-Dichlorophenol
10/03/23 12:330.6600.180<0.180mg/KgDiethyl phthalate
10/03/23 12:330.6600.174<0.174mg/KgDimethyl phthalate
10/03/23 12:330.3300.108<0.108mg/Kg2,4-Dimethylphenol
10/03/23 12:330.6600.107<0.107mg/KgDi-n-butyl phthalate
10/03/23 12:331.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
10/03/23 12:331.500.520<0.520mg/Kg2,4-Dinitrophenol
10/03/23 12:330.6600.096<0.096mg/Kg2,4-Dinitrotoluene
10/03/23 12:330.6600.108<0.108mg/Kg2,6-Dinitrotoluene
10/03/23 12:330.3300.143<0.143mg/KgDi-n-Octyl Phthalate
10/03/23 12:330.6600.123<0.123mg/KgFluoranthene
10/03/23 12:330.6600.128<0.128mg/KgFluorene
10/03/23 12:330.6600.106<0.106mg/KgHexachlorobenzene
10/03/23 12:330.6600.097<0.097mg/KgHexachlorobutadiene
10/03/23 12:330.6600.157<0.157mg/KgHexachlorocyclopentadiene
10/03/23 12:330.6600.079<0.079mg/KgHexachloroethane
10/03/23 12:330.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
10/03/23 12:330.6600.191<0.191mg/KgIsophorone
10/03/23 12:330.6600.106<0.106mg/Kg1-Methylnaphthalene
10/03/23 12:330.6600.100<0.100mg/Kg2-Methylnaphthalene
10/03/23 12:330.6600.097<0.097mg/Kg2-Methylphenol
10/03/23 12:330.6600.084<0.084mg/Kg3&4 Methylphenol
10/03/23 12:330.6600.144<0.144mg/KgNaphthalene
10/03/23 12:330.6600.096<0.096mg/Kg2-Nitroaniline
10/03/23 12:330.6600.120<0.120mg/Kg3-Nitroaniline
Page 29 of 38Date:10/17/2023 03:31 PM
Page 102 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
Associated Lab Samples: 96401, 96403, 96407, 96409
LRB-V38566 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/03/23 12:330.3300.093<0.093mg/Kg4-Nitroaniline
10/03/23 12:330.3300.116<0.116mg/KgNitrobenzene
10/03/23 12:330.6600.088<0.088mg/Kg2-Nitrophenol
10/03/23 12:330.6600.117<0.117mg/Kg4-Nitrophenol
10/03/23 12:330.6600.263<0.263mg/KgN-Nitrosodimethylamine
10/03/23 12:330.6600.181<0.181mg/KgN-Nitrosodiphenylamine
10/03/23 12:330.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
10/03/23 12:331.000.347<0.347mg/KgPentachlorophenol
10/03/23 12:330.6600.208<0.208mg/KgPhenanthrene
10/03/23 12:330.6600.112<0.112mg/KgPhenol
10/03/23 12:330.6600.134<0.134mg/KgPyrene
10/03/23 12:330.3300.079<0.079mg/KgPyridine
10/03/23 12:330.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
10/03/23 12:330.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
10/03/23 12:330.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
10/03/23 12:332-Fluorobiphenyl (S)91.0 44-115
10/03/23 12:332-Fluorophenol (S)85.2 35-115
10/03/23 12:33Nitrobenzene-d5 (S)81.4 37-122
10/03/23 12:334-Terphenyl-d14 (S)96.4 54-127
10/03/23 12:332,4,6-Tribromophenol (S)93.0 39-132
10/03/23 12:33Phenol-d5 (S)83.7 34-121
LCS-V38566Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.81.551.67mg/KgAcenaphthene 40-123
92.21.541.67mg/KgAcenaphthylene 32-132
Page 30 of 38Date:10/17/2023 03:31 PM
Page 103 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
LCS-V38566Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1031.721.67mg/KgAniline 12-197
97.61.631.67mg/KgAnthracene 47-123
93.41.561.67mg/KgBenzo(a)anthracene 49-126
1131.891.67mg/KgBenzo(a)pyrene 45-129
1081.801.67mg/KgBenzo(b)fluoranthene 45-132
1041.741.67mg/KgBenzo(g,h,i)perylene 43-134
1051.751.67mg/KgBenzo(k)fluoranthene 47-132
41.90.7001.67mg/KgBenzoic Acid 10-83
92.81.551.67mg/KgBenzyl alcohol 29-122
76.61.281.67mg/KgBis(2-Chloroethoxy)methane 36-121
78.41.311.67mg/KgBis(2-Chloroethyl)ether 31-120
77.21.291.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1081.811.67mg/KgBis(2-ethylhexyl)phthalate 51-133
92.21.541.67mg/Kg4-Bromophenyl phenyl ether 46-124
1011.691.67mg/KgButyl benzyl phthalate 48-132
80.21.341.67mg/Kg4-Chloro-3-methylphenol 45-122
72.41.211.67mg/Kg4-Chloroaniline 17-106
94.61.581.67mg/Kg2-Chloronaphthalene 41-114
85.61.431.67mg/Kg2-Chlorophenol 34-121
93.41.561.67mg/Kg4-Chlorophenyl phenyl ether 45-121
99.41.661.67mg/KgChrysene 50-124
78.41.311.67mg/KgDibenz(a,h)anthracene 45-134
94.01.571.67mg/KgDibenzofuran 44-120
80.81.351.67mg/Kg1,2-Dichlorobenzene 33-117
78.41.311.67mg/Kg1,3-Dichlorobenzene 30-115
75.41.261.67mg/Kg1,4-Dichlorobenzene 31-115
66.41.111.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 31 of 38Date:10/17/2023 03:31 PM
Page 104 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
LCS-V38566Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/Kg2,4-Dichlorophenol 40-122
97.61.631.67mg/KgDiethyl phthalate 50-124
97.01.621.67mg/KgDimethyl phthalate 48-124
1011.691.67mg/Kg2,4-Dimethylphenol 30-127
1041.731.67mg/KgDi-n-butyl phthalate 51-128
83.21.391.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
54.40.9091.67mg/Kg2,4-Dinitrophenol 27-129
1021.711.67mg/Kg2,4-Dinitrotoluene 48-126
1021.701.67mg/Kg2,6-Dinitrotoluene 46-124
1131.891.67mg/KgDi-n-Octyl Phthalate 45-140
96.41.611.67mg/KgFluoranthene 50-127
95.21.591.67mg/KgFluorene 43-125
1011.681.67mg/KgHexachlorobenzene 45-122
82.01.371.67mg/KgHexachlorobutadiene 32-123
70.01.171.67mg/KgHexachlorocyclopentadiene 32-117
77.81.301.67mg/KgHexachloroethane 28-117
1051.751.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
70.01.171.67mg/KgIsophorone 30-122
76.01.271.67mg/Kg1-Methylnaphthalene 40-119
78.41.311.67mg/Kg2-Methylnaphthalene 38-122
88.01.471.67mg/Kg2-Methylphenol 32-122
79.61.331.67mg/Kg3&4 Methylphenol 34-119
73.01.221.67mg/KgNaphthalene 35-123
92.81.551.67mg/Kg2-Nitroaniline 44-127
85.01.421.67mg/Kg3-Nitroaniline 33-119
95.21.591.67mg/Kg4-Nitroaniline 63-147
73.61.231.67mg/KgNitrobenzene 34-122
Page 32 of 38Date:10/17/2023 03:31 PM
Page 105 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
LCS-V38566Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
76.61.281.67mg/Kg2-Nitrophenol 36-123
1011.681.67mg/Kg4-Nitrophenol 30-132
68.21.141.67mg/KgN-Nitrosodimethylamine 10-146
1131.881.67mg/KgN-Nitrosodiphenylamine 38-127
83.81.401.67mg/KgN-Nitroso-di-n-propylamine 36-120
1171.961.67mg/KgPentachlorophenol 25-133
97.61.631.67mg/KgPhenanthrene 50-121
81.41.361.67mg/KgPhenol 34-121
1011.691.67mg/KgPyrene 47-127
46.00.7691.67mg/KgPyridine 10-80
76.61.281.67mg/Kg1,2,4-Trichlorobenzene 34-118
92.21.541.67mg/Kg2,4,5-Trichlorophenol 41-124
94.61.581.67mg/Kg2,4,6-Trichlorophenol 39-126
93.42-Fluorobiphenyl (S)44-115
90.32-Fluorophenol (S)35-115
73.6Nitrobenzene-d5 (S)37-122
97.64-Terphenyl-d14 (S)54-127
1032,4,6-Tribromophenol (S)39-132
85.5Phenol-d5 (S)34-121
V 96596-MS-V38566 V 96596-MSD-V38566Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.48 88.61.551.671.67<0.116mg/KgAcenaphthene 92.8 40-123 4.6 20
1.48 88.61.541.671.67<0.105mg/KgAcenaphthylene 92.2 32-132 3.9 20
1.57 94.01.551.671.67<0.152mg/KgAniline 92.8 12-197 1.2 20
Page 33 of 38Date:10/17/2023 03:31 PM
Page 106 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
V 96596-MS-V38566 V 96596-MSD-V38566Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.58 94.61.651.671.67<0.143mg/KgAnthracene 98.8 47-123 4.3 20
1.51 90.41.591.671.67<0.139mg/KgBenzo(a)anthracene 95.2 49-126 5.1 20
1.85 1111.931.671.67<0.147mg/KgBenzo(a)pyrene 116 45-129 4.2 20
1.72 1031.811.671.67<0.146mg/KgBenzo(b)fluoranthene 108 45-132 5.0 20
1.67 1001.771.671.67<0.136mg/KgBenzo(g,h,i)perylene 106 43-134 5.8 20
1.66 99.41.741.671.67<0.137mg/KgBenzo(k)fluoranthene 104 47-132 4.7 20
0.992 59.41.241.671.67<0.580mg/KgBenzoic Acid 74.2 10-83 22.2*20
1.49 89.21.591.671.67<0.105mg/KgBenzyl alcohol 95.2 29-122 6.4 20
1.26 75.41.271.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 76.0 36-121 0.7 20
1.29 77.21.311.671.67<0.107mg/KgBis(2-Chloroethyl)ether 78.4 31-120 1.5 20
1.26 75.41.291.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 77.2 33-131 2.3 20
1.74 1041.851.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 111 51-133 6.1 20
1.48 88.61.561.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 93.4 46-124 5.2 20
1.63 97.61.711.671.67<0.113mg/KgButyl benzyl phthalate 102 48-132 4.7 20
1.26 75.41.361.671.67<0.092mg/Kg4-Chloro-3-methylphenol 81.4 45-122 7.6 20
1.17 70.01.251.671.67<0.112mg/Kg4-Chloroaniline 74.8 17-106 6.6 20
1.54 92.21.591.671.67<0.116mg/Kg2-Chloronaphthalene 95.2 41-114 3.1 20
1.39 83.21.421.671.67<0.098mg/Kg2-Chlorophenol 85.0 34-121 2.1 20
1.45 86.81.541.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 92.2 45-121 6.0 20
1.60 95.81.661.671.67<0.142mg/KgChrysene 99.4 50-124 3.6 20
1.37 82.01.431.671.67<0.230mg/KgDibenz(a,h)anthracene 85.6 45-134 4.2 20
1.53 91.61.601.671.67<0.119mg/KgDibenzofuran 95.8 44-120 4.4 20
1.31 78.41.351.671.67<0.094mg/Kg1,2-Dichlorobenzene 80.8 33-117 3.0 20
1.27 76.01.291.671.67<0.097mg/Kg1,3-Dichlorobenzene 77.2 30-115 1.5 20
1.22 73.01.241.671.67<0.097mg/Kg1,4-Dichlorobenzene 74.2 31-115 1.6 20
1.04 62.21.071.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 64.0 22-121 2.8 20
Page 34 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 107 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
V 96596-MS-V38566 V 96596-MSD-V38566Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.34 80.21.411.671.67<0.095mg/Kg2,4-Dichlorophenol 84.4 40-122 5.0 20
1.52 91.01.641.671.67<0.180mg/KgDiethyl phthalate 98.2 50-124 7.5 20
1.53 91.61.611.671.67<0.174mg/KgDimethyl phthalate 96.4 48-124 5.0 30
1.58 94.61.621.671.67<0.108mg/Kg2,4-Dimethylphenol 97.0 30-127 2.5 20
1.67 1001.741.671.67<0.107mg/KgDi-n-butyl phthalate 104 51-128 4.1 20
1.48 88.61.511.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 90.4 29-132 2.0 20
1.22 73.01.241.671.67<0.520mg/Kg2,4-Dinitrophenol 74.2 27-129 1.6 20
1.62 97.01.741.671.67<0.096mg/Kg2,4-Dinitrotoluene 104 48-126 7.1 20
1.60 95.81.731.671.67<0.108mg/Kg2,6-Dinitrotoluene 104 46-124 7.8 20
1.81 1081.881.671.67<0.143mg/KgDi-n-Octyl Phthalate 113 45-140 3.7 20
1.57 94.01.641.671.67<0.123mg/KgFluoranthene 98.2 50-127 4.3 20
1.54 92.21.621.671.67<0.128mg/KgFluorene 97.0 43-125 5.0 20
1.66 99.41.731.671.67<0.106mg/KgHexachlorobenzene 104 45-122 4.1 20
1.37 82.01.391.671.67<0.097mg/KgHexachlorobutadiene 83.2 32-123 1.4 20
1.21 72.41.231.671.67<0.157mg/KgHexachlorocyclopentadiene 73.6 32-117 1.6 20
1.24 74.21.251.671.67<0.079mg/KgHexachloroethane 74.8 28-117 0.8 20
1.68 1011.761.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 105 45-133 4.6 20
1.12 67.01.171.671.67<0.191mg/KgIsophorone 70.0 30-122 4.3 20
1.27 76.01.291.671.67<0.106mg/Kg1-Methylnaphthalene 77.2 40-119 1.5 20
1.30 77.81.311.671.67<0.100mg/Kg2-Methylnaphthalene 78.4 38-122 0.7 20
1.39 83.21.431.671.67<0.097mg/Kg2-Methylphenol 85.6 32-122 2.8 20
1.22 73.01.281.671.67<0.085mg/Kg3&4 Methylphenol 76.6 34-119 4.8 20
1.24 74.21.251.671.67<0.144mg/KgNaphthalene 74.8 35-123 0.8 20
1.51 90.41.571.671.67<0.096mg/Kg2-Nitroaniline 94.0 44-127 3.8 20
1.45 86.81.531.671.67<0.120mg/Kg3-Nitroaniline 91.6 33-119 5.3 20
1.47 88.01.611.671.67<0.093mg/Kg4-Nitroaniline 96.4 63-147 9.0 20
Page 35 of 38Date:10/17/2023 03:31 PM
Page 108 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V38621QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V38566
V 96596-MS-V38566 V 96596-MSD-V38566Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.23 73.61.261.671.67<0.116mg/KgNitrobenzene 75.4 34-122 2.4 20
1.26 75.41.311.671.67<0.088mg/Kg2-Nitrophenol 78.4 32-123 3.8 20
1.58 94.61.751.671.67<0.117mg/Kg4-Nitrophenol 105 30-132 10.2 20
1.11 66.41.121.671.67<0.263mg/KgN-Nitrosodimethylamine 67.0 10-146 0.8 30
1.79 1071.861.671.67<0.181mg/KgN-Nitrosodiphenylamine 111 38-127 3.8 20
1.37 82.01.421.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 85.0 36-120 3.5 20
1.93 1162.051.671.67<0.347mg/KgPentachlorophenol 123 25-133 6.0 20
1.59 95.21.661.671.67<0.208mg/KgPhenanthrene 99.4 50-121 4.3 20
1.29 77.21.341.671.67<0.112mg/KgPhenol 80.2 34-121 3.8 20
1.64 98.21.691.671.67<0.134mg/KgPyrene 101 47-127 3.0 20
0.843 50.40.8781.671.67<0.079mg/KgPyridine 52.5 10-80 4.0 20
1.28 76.61.291.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 77.2 34-118 0.7 20
1.50 89.81.591.671.67<0.096mg/Kg2,4,5-Trichlorophenol 95.2 41-124 5.8 20
1.48 88.61.541.671.67<0.096mg/Kg2,4,6-Trichlorophenol 92.2 39-126 3.9 20
89.22-Fluorobiphenyl (S)88.0 44-115
85.32-Fluorophenol (S)82.9 35-115
72.4Nitrobenzene-d5 (S)71.2 37-122
92.84-Terphenyl-d14 (S)93.4 54-127
93.12,4,6-Tribromophenol (S)98.2 39-132
79.9Phenol-d5 (S)79.3 34-121
Page 36 of 38Date:10/17/2023 03:31 PM
Page 109 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L709932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L709491
Associated Lab Samples: 96396, 96401, 96403, 96407, 96409
LRB-L709491 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/10/23 16:060.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L709491Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.03.274.00mg/KgChromium, Hexavalent 80-120
V 96403-DUP-L709491Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/10/23 16:3843.9*1.440.921mg/KgChromium, Hexavalent
V 96403-MS-L709491Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
26.5 65.0*39.4< 1.39mg/KgChromium, Hexavalent 75-125
Page 37 of 38* QC Fail Date:10/17/2023 03:31 PM
Page 110 of 114
Quality Control Data
23-270-0022Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
Standard Roll Coverings
Dry Weight Determination
SW-DRYWT
V38458QC Analytical Batch:
Analysis Method:
Analysis Description:
V 96388-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/28/23 14:480.824.424.6%Moisture
V 96440-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/28/23 14:481.118.218.0%Moisture
Page 38 of 38Date:10/17/2023 03:31 PM
Page 111 of 114
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-270-0022
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:09/27/2023 16:16:24
Special precautions or instructions included?
Comments:
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