MO-28645_47884_CA_LSA_20210602

PHASE I LIMITED SITE ASSESSMENT REPORT
3200 Freedom Drive
Charlotte, Mecklenburg County, NC
Groundwater Incident No. Unknown
Facility ID No. N/A
SUMMIT Project No. 4493.E0002

Prepared For:
MPV Properties
2400 South Blvd, Suite 300
Charlotte, NC 28203

Prepared By:
SUMMIT Engineering, Laboratory & Testing, Inc.
PO Box 7384
Charlotte, NC 28241
[phone]

June 2, 2021

I, Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE, a Professional
Engineer for SUMMIT, do certify that the information contained in this
report is correct and accurate to the best of my knowledge.
Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE
SUMMIT Engineering, Laboratory & Testing, Inc. SUMMIT Engineering, Laboratory & Testing, Inc. is licensed to practice engineering in the State of
North Carolina.

The certification number of SUMMIT Engineering, Laboratory & Testing, Inc. is F-1454.
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC i
TABLE OF CONTENTS
1.0 SITE INFORMATION ................................................................................................................... 1
2.0 SITE HISTORY .............................................................................................................................. 2
2.1 UST Information ............................................................................................................................... 2
2.2 Initial Abatement Activities .............................................................................................................. 2
3.0 RECEPTOR SURVEY ................................................................................................................... 3
4.0 SITE GEOLOGY AND HYDROGEOLOGY .............................................................................. 4
5.0 ASSESSMENT ACTIVITIES ........................................................................................................ 5
5.1 Soil .................................................................................................................................................... 5
5.2 Groundwater ..................................................................................................................................... 5
6.0 CONCLUSIONS AND RECOMMENDATIONS ........................................................................ 7
7.0 LIMITATIONS ............................................................................................................................... 8

FIGURES

Figure 1: USGS Topographic Map
Figure 2: Site Map
Figure 3: Soil and Groundwater Sampling Map
Figure 4: Land Use and Water Supply Well

TABLES

Table 1: Adjacent Property Owners
Table 2: Water Supply Well Information

APPENDICES

Appendix A: Limited Site Assessment Risk Classification and Land Use Form
Appendix B: Well Construction Log
Appendix C: Laboratory Analytical Reports – Soil and Groundwater
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 1
1.0 SITE INFORMATION
 Site Name: 3200 Freedom Drive
 Location: 3200 Freedom Drive
Charlotte, Mecklenburg County (Figure 1)
 Groundwater Incident No. Unknown
 Facility I.D. No. N/A
 UST Owner/Operator: Amerco Real Estate Company
2727 N Central Ave
Phoenix, AZ 85004
 Property Owner: Amerco Real Estate Company
2727 N Central Ave
Phoenix, AZ 85004
 Consultant/Contractor: SUMMIT Engineering, Laboratory & Testing, Inc.
PO Box 7384
Charlotte, North Carolina 28241
[phone]
 Release Information
Date Discovered: Unknown
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Former Gasoline Refueling Station
UST Size/Contents: Unknown
Latitude: 35°14’41.39” N
Longitude: -80°53’29.10” W

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 2
2.0 SITE HISTORY
2.1 UST Information

UST ID
Number
Current
/Last
Contents
Previous
Contents
Capacity
(in
gallons)
Construct
ion
Details
Tank
Dimensions
Description
of
Associated
Piping and
Pumps
Date Tank
Installed
Status of
UST
Was
release
associate
d
with the
UST
System?
Unknown Gasoline N/A Unknown Unknown Unknown Unknown Unknown Removed Yes

 Property Owner: Amerco Real Estate Company
2727 N Central Ave
Phoenix, AZ 85004
 Previous Owner(s): Unknown
2.2 Initial Abatement Activities
 Quantity of Regulated Substance Removed from UST: N/A
 Source Control Actions: On May 10, 2018, Partner collected soil and groundwater samples
of the site in the area of the former UST tank basin. Analytical laboratory results indicated a
petroleum release from the former UST tank basin. Partner recommended the completion of
a Phase I Limited Site Assessment (LSA) to determine the rick classification of the site. On
May 8, 2021, SUMMIT installed one (1) permanent monitoring well to collect soil and
groundwater samples.
 Contaminant Migration Control Measures: The release was to the subsurface. Therefore,
no contaminant migration control measures were necessary.
 Measures Taken to Mitigate Fire/Safety Hazards: There do not appear to be any
immediate fire or safety hazards present as a result of the release.
 Contaminated Soil Storage/Treatment and/or Disposal: SUMMIT did not observe the
removal of the USTs or the collection of soil and groundwater samples in May 2018.
 Status of Free Product Investigation/Removal: Free product has not been observed at the
site.
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 3
3.0 RECEPTOR SURVEY
 Water Supply Wells: Three (3) monitoring wells were identified within 1,500 feet of the
site. A list of the monitoring well information is presented in Table 2. The Well and
Groundwater Contamination locations are indicated on Figure 4.
 Public Water Supply: The area within a 1,500-foot radius of the source area has access to
the City of Charlotte municipal water system, which is derived from the Catawba River.
 Surface Water: an un-maned creek is approximately 1,000 feet to the east of the subject site.
 Wellhead Protection Areas: No wellhead protection areas were identified within a 1,500-
foot radius of the source area. Water supplies in the vicinity are derived from the Catawba
River.
 Subsurface Structures: No structures with basements were observed in the immediate
vicinity of the site. There is a subsurface stormwater drain located approximately 100 feet to
the north-northeast of the former tank basin.
 Land Use: The site formally contains a vacant commercial building.. The site is located in a
mixed residential and commercial area in Mecklenburg County. The site is surrounded by
commercial properties to the east, west and to the south, and residential properties to the
north. A Site Map has been included as Figure 2. A Limited Site Assessment Risk
Classification and Land Use Form has been included as Appendix A.
 Property Owners and Occupants: The names and addresses of the owners of properties
adjacent to the site is presented in Table 1.

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 4
4.0 SITE GEOLOGY AND HYDROGEOLOGY
The United States Geological Survey (USGS) “Charlotte, North Carolina, United States”
topographic quadrangle map was reviewed. According to the contour lines on the topographic
maps, the elevation of the subject property ranges from approximately 750 feet (along western
property boundaries) to approximately 740 feet (along eastern property boundaries) above Mean
Sea Level (MSL). The inferred groundwater flow direction based on topography appears to be to
the east towards an un-named creek. The un-named creek flows into Stewart Creek. Stewart
Creek flows into Irwin Creek. Irwin Creek flows into Sugar Creek. Sugar Creek flows into the
Catawba River, near Goat Island.

This property contains the soil types: Ur—Urban land. The surface cover of the UST basin was
asphalt.

Surficial soils observed during boring advancement activities were orange, red and tan clayey silt
to silt to depths of approximately 17.5 feet. The depth to groundwater in Type II temporary
monitoring well W-1 installed on My 8, 2021 and developed on May 12, 2021 was 9.5 feet Below
Ground Surface (BGS). A boring log for monitoring well W-1 has been included as Appendix B.
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 5
5.0 ASSESSMENT ACTIVITIES

Surficial soils observed during boring advancement activities were orange, red and tan clayey silt
to silt to depths of approximately 17.5 feet. The depth to groundwater in Type II temporary
monitoring well W-1 installed on My 8, 2021 and developed on May 12, 2021 was 9.5 feet Below
Ground Surface (BGS). A boring log for monitoring well W-1 has been included as Appendix B.

5.1 Soil

Soil samples “S-1 @ 5” and “S-1 @ 10” were collected during well installation on May 8, 2021.
Acetone (11.0 ug/kg) was detected by the laboratory analytical instruments in “S-1 @ 5.”

Acetone (11.0 ug/kg), Benzo(a)anthracene (10 ug/kg), Benzo(a)pyrene (27 ug/kg),
Benzo(b)fluoranthene (42 ug/kg) Benzo(g,h,i)perylene (16 ug/kg), Benzo(k)fluoranthene (15
ug/kg) Chrysene (14 ug/kg), Indeno(1,2,3-c,d)pyrene (13 ug/kg), and Pyrene (9.5 ug/kg) were
detected by the laboratory analytical instruments. These compounds are associated with
petroleum releases and are below the North Carolina Soil-to-Groundwater Maximums. A
complete report of laboratory analyses for the soil samples has been included as Appendix C.

5.2 Groundwater

On May 8, 2021, Type II monitoring well W-1 was installed north (and downgradient) of the
former tank basin using hollow stem augers. The monitoring well was installed for the purpose
of completing a Phase I Limited Site Assessment associated with the former UST basin. The
location of the monitoring well is shown on Figure 3. A well construction record is included as
Appendix B. Monitoring well W-1 was gauged, purged and sampled on May 12, 2021. The
groundwater sample collected from monitoring well W-1 was analyzed by EPA Method 8260 and
8270 and by MADEP VPH and EPH.

Acetone (8.0 ug/L), Methyl Tertiary Butyl Ether (MTBE) (2.6 ug/L), Acetophenone (0.61 ug/L),
Caprolactam (2.2 ug/L), Diethylphthalate (0.55 ug/L), bis(2-Ethylhexyl)phthalate (0.55 ug/L) and
C9-C12 Aliphatics (30 ug/L) were detected by the laboratory analytical instruments. These
compounds are associated with petroleum releases and are below the North Carolina
Groundwater Quality Standards. No additional concentrations of requested method constituents
were reported in the groundwater sample collected from monitoring well W-1. A complete report
of laboratory analyses for the groundwater sample has been included as Appendix C.

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 6
6.0 CONCLUSIONS AND RECOMMENDATIONS
 The 3200 Freedom Drive is currently vacant. The site formerly operated as a commercial
building. Property use in the immediate vicinity is mixed residential and commercial, but
mostly commercial. The down gradient direction for the site is commercial. Therefore, the
site should be assigned a commercial land use classification.
 Potable water in the area is provided by the City of Charlotte. The source of the potable
water is from the Catawba River. No supply wells were identified within 1,500 feet of the
site. No water supply wells being utilized as sources of potable water are located within
1,000 feet of the source area. No water supply wells being utilized for irrigation or other non-
potable uses are located within 250 feet of the source area. In addition, the site is not located
within a designated wellhead protection area.
 An un-named creek is approximately 1,000 feet to the east of the subject site.
 The soil sampled during the monitoring well construction do not exceed the soil to
groundwater maximums.
 No concentrations of requested analytical parameters were reported above the maximum
allowable concentrations in the groundwater sample (W-1) collected during the Phase I LSA
for the former UST basin.
 Based on this information, although a release has occurred, it does not appear to meet any of
the NCDEQ criteria for a high or intermediate risk classification. Therefore, the release
should be assigned a low risk classification. Additionally, based on LSA analytical results,
no further assessment or remediation of soil or groundwater in the former UST area is
warranted.
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\R-LSA- 3200 Freedom - UST.DOC 7
7.0 LIMITATIONS
This report has been prepared for the exclusive use of MPV Properties for specific application to
the referenced site in Charlotte, Mecklenburg County, North Carolina. The assessment was
conducted based on the scope of work and level of effort specified by the NCDEQ and with
resources adequate only for that scope of work. Our findings have been developed in accordance
with generally accepted standards of geology and hydrogeology practices in the State of North
Carolina, available information, and our professional judgment. No other warranty is expressed
or implied.

The data that are presented in this report are indicative of conditions that existed at the precise
location sampled and at the time the samples were collected. Additionally, the data obtained
from the samples would be interpreted as being meaningful with respect to parameters indicated
in the laboratory report. No additional information can logically be inferred from these data.

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

FIGURES

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\UST - Figure 1 Topo.doc SUMMIT ELT, PC Project: 4493.E0002 Figure 1 USGS Topographic Map 3200 Freedom Drive Charlotte, NC 1500’ Radius Site
D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\UST - Figure 2 Site Map.doc SUMMIT ELT, PC Project: 4493.E0002 Figure 2 Site Location Map 3200 Freedom Drive Charlotte, NC
D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\UST - Figure 3 Aerial Map.doc SUMMIT ELT, PC Project: 4493.E0002 Figure 3 Aerial Map 3200 Freedom Drive Charlotte, NC Monitoring Well Former Tank Basin
D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\UST - Figure 4 Well Map.doc SUMMIT ELT, PC Project: 4493.E0002 Figure 4 Land Use and Water Supply Well Map 3200 Freedom Drive Charlotte, NC
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx

TABLES

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
Table B-1: Site History – System Information

UST ID
Number
Current
/Last
Contents
Previous
Contents
Capacity
(in
gallons)
Construction
Details
Tank
Dimension
s
Description
of
Associated
Piping and
Pumps
Date Tank
Installed
Status of
UST
Was
release
associated
with the
UST
System?
UST
basin
Gasoline N/A Unknown Unknown Unknown Unknown Unknown Removed Yes

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
Table B-2: Site History - Owner and Operator Information

ID Number UST Facility ID Number N/A
Name of Owner

Dates of Operation
(mm/dd/yy to mm/dd/yy)
Amerco Real Estate Company Unknown to current
Street Address
2727 N Central Ave
City State Zip Telephone Number
Phoenix AZ 85004
Name of Operator Dates of Operation
(mm/dd/yy to mm/dd/yy)
N/A Unknown to current
Street Address

City State Zip Telephone Number

Page 1 of 1 

TABLE 1 
ADJACENT PROPERTY OWNERS 
3200 Freedom Drive 

Parcel ID Property Owner(s) Mailing Address 
06503620 (site) Amerco Real Estate Company 2727 N Central Ave, Phoenix, AZ 85004 
06503618 Sein Divine, LLC 3964 Grovesner St, Harrisburg, NC 28075 
06503614 CK Freedom, LLC 301 S College St, Suite 2800, Charlotte, 
NC 28202 
06503616 TSG 4001 LLC 4024‐B Triangle Dr, Charlotte, NC 28208 
06503617 Clean Clothes Enterprises, Inc. 10924 Sorrell Ridge Dr, Mint Hill, NC 
28227 
06503609 Carolina Urban Properties, LTD PO Box 668529, Charlotte, NC 28266 
06503608 Elijah & Jackie Hackett 3909 Tuckaseegee Rd, Charlotte, NC 
28208 
06503607 Bren Dasson, LLC 3833 Tuckaseegee Rd, Charlotte, NC 
28208 
06503606 David Davies & Sandra Dickinson 3819 Tuckaseegee Rd, Charlotte, NC 
28208 
06503605 Andrew Bennett & Tracie Mahoney 3809 Tuckaseegee Rd, Charlotte, NC 
28208 
06503604 Yaffa Investments, LLC 9716‐B Rea Rd, Unit 158, Charlotte, NC 
28277 
06503603 David Elmer & Lollie Griffith 1218 Hazel St, Charlotte, NC 28208 
06503602 Victoria McGarry 1224 Hazel St, Charlotte, NC 28208 
06503619 John Tsoulos 15000 Crooked Branch Ln, Charlotte, NC 
28278 
06503610 Freedom Opportunity Fund, LLC 121 W Trade St, Suite 2550, Charlotte, 
NC 28202 
06503621 C4 Freedom Op LLC 121 W Trade St, Suite 2550, Charlotte, 
NC 28202 
06503622 C4 Freedom Op LLC 121 W Trade St, Suite 2550, Charlotte, 
NC 28202 
06503611 Joan Ruth LCC 2730 Rozzelles Ferry Rd, Suite A, 
Charlotte, NC 28208 
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
06502361 Labrakis Investments LLC 1961 Stonewyck Ave, Kannapolis, NC 
28081 
06502362 Hemingway Joan LLC 2730 Rozzelles Ferry Rd, Suite A, 
Charlotte, NC 28208 
06502365 Ellison Kimborough Wood‐Charlotte 
Properties 
1445 Donlon St, suite 20, Ventura, CA 
93003 
06503601 Bill & Sharon Barros 602 Fountain Ave, Redlands, CA 92373 
06502357 SRMZ 2 LLC 5001 Plaza on the Lake, Suite 200, 
Austin, TX 78746 
06502356 Marilyn Janeczek 3723 Rogers St, Charlotte, NC 28208 
06502355 Anderson & Mattie Bennett 6712 Woodfield Dr, Charlotte, NC 28215 
06502354 Durbert O’Neal Brandon 3711 Rogers St, Charlotte, NC 28208 
06502367 Nicholas Nunziato 3709 Rogers St, Charlotte, NC 28208 
06502352 TPM Properties Limited Partnership 3816 Mooreland Farm Rd, Charlotte, NC 
28226 
06502351 Carolyn Helms 1533 Bear Mountain Rd, Charlotte, NC, 
28214 
06505410 Angela McIntyre 1226 Gaston St, Charlotte, NC 28208 
06505409 Weston Properties Ltd 16310 Barcica Ln, Cornelius, NC 28031 
06505408 Charles Cunning & Bryan Armstrong 1711 Clooney Ln, Charlotte, NC 28262 
06505407 Bright Future Funding, LLC 2301 W Morehead St., Suite C, Charlotte, 
NC 28208 
06505406 Christopher Wilson 1225 Hazel St, Charlotte, NC 28208 
06505405 John H IV Symons 12191 Hazel St, Charlotte, NC 28208 
06505411 Charlotte Skyline Properties, LLC 1911 Tyvola Rd, Charlotte, NC 28210 
06505401 Lisa & Wainright Samuel 207‐19 100th Ave, Queens Village, NY 
11429 
06505402 Teasa N Farmer 3711 Tuckaseegee Rd, Charlotte, NC 
28208 
06505403 Lynda & Joseph Alexander 3719 Tuckaseegee Rd, Charlotte, NC 
28208 
06505404 Nell Baldwin 209 Kemp Dr, West Jefferson, NC 28694 
06505312 La Buena Vista Properties, Inc 5626 Coulee place, Charlotte, NC 28217 
06505313 Michael & McCayley Pettus 3720 Tuckaseegee Rd, Charlotte, NC 
28208 
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
06505314 Jeffry Smith & Terry Davis PO Box 35214, Charlotte, NC 28235 
06505311 Naomi Brown 1107 Hazel St, Charlotte, NC 28208 
06505310 Mazfield Bowen 8220 Bella Vista Ct, Charlotte, NC 28216 
06505309 MTK Investment Fund 1, LLC PO Box 23725, Mint Hill, NC 28227 
06503111 Tommy Keith Johnson 1113 Rutledge Ave, Charlotte, NC 28211 
06503119 James Jackson 1114 Hazel St, Charlotte, NC 28208 
06503110 Alan Buch & Bill Mowry 3621 French Woods Rd, Charlotte, NC 
28269 
06503109 ABA614, LLC 4300 Bridgewood Ln, Charlotte, NC 
28226 
06503108 Tommy & Frances Johnson 1113 Rutledge Ave, Charlotte, NC 28211 
06503106 Catherine Hunter 7804 Fairview Rd, PMB 311, Charlotte, 
NC 28226 
06503105 Mitchell Wayne Francis 3906 Tuckaseegee Rd, Charlotte, NC 
28208 
06503104 DKMK LLC PO Box 77502, Charlotte, NC 28271 
06503103 Little Flower Realty LLC 15815 Foreleigh Rd, Huntersville, NC 
28078 
06503102 George Terrell Casey 1109 Tennyson Dr, Charlotte, NC 28208 
06503101 Scott Daileu 1101 Tennyson Dr, Charlotte, NC 28208 
06503118 Melvin Earl Jenkins 3845 Avalon Ave, Charlotte, NC 28208 
06503117 Rupp Holdings, Inc. 6420 Rea Rd, Suite A1‐160, Matthews, 
NC 28277 
06503116 Aimee Irene Aquino 429 State St, Charlotte, NC 28208 
06503115 Clarence Winslow Jr 3819 Avalon Ave, Charlotte, NC 28208 
06503114 Jonnie Burris 3815 Avalon Ave, Charlotte, NC 28208 
06503113 Tricon SFR 2020‐2 Borrower, LLC 1508 Brookhollow Dr, Santa ana, CA 
92705 
06503112 Cassandra Loftin 6029 Plaza Ln, Charlotte, NC 28215 
06506115 Gummybear Properties, LLC 3511 Tuckaseegee Rd, Charlotte, NC 
28208 
06506114 Colin Andrew Thomas 1031 Tennyson Dr, Charlotte, NC 28208 
06506116 Justin Poovey 1711 Merriman Ave, Charlotte, NC 28203 
06506117 Brendon Harris 3824 Avalon Ave, Charlotte, NC 28208 
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
06506118 Betty Joan Walker 3818 Avalon Ave, Charlotte, NC 28208 
06506149 Betty Joan Walker 3818 Avalon Ave, Charlotte, NC 28208 
06506221 Vincent Cruz Serrano & Alba A Galeno 
Lopez 1036 Tennyson Dr, Charlotte, NC 28208 
06506220 The North Carolina II LP 1717 Main St, Suite 2000 c/o Invitation 
Homes, Dallas, TX 75201 
06506219 Patrick & Amber Wloch 4073 Birkshire Heights, Fort Mill, SC 
29708 
06506228 Danille & Barry Buckins 4024 Avalon Ave, Charlotte, NC 28208 
06506227 Deandrae & Elizabeth Watson 4030 Avalon Ave, Charlotte, NC 28208 
06506230 Brian Rowe & Parks Kingery 4034 Avalon Ave, Charlotte, NC 28208 
06506229 Mary Allison Mitchell & Evan York 4038 Avalon Ave, Charlotte, NC 28208 
06506216 Christine Massey & Brian Bowden 4044 Avalon Ave, Charlotte, NC 28208 
06506215 Jason & Yamel Siesel 17214 Harcombe Dr, Charlotte, NC 
28277 
06503210 Berry Mountain Associates, LP 125 Old Home Place, Kings Mountain, NC 
28086 
06503211 Berry Mountain Associates, LP 125 Old Home Place, Kings Mountain, NC 
28086 
06503209 Star Mountain West LLC 4024 Triangle Dr, Charlotte, NC 28208 
06503207 B & E 27 LLC 402 E Sugar Creek Rd, Charlotte, NC 
28213 
06503206 Star Mountain West LLC 4016 Triangle Dr, Charlotte, NC 28208 
06503218 Jason Derek Elgin 4057 Avalon Ave, Charlotte, NC 28208 
06503217 Shane Michael Spencer & Laura Olivo 
Estrada 4053 Avalon Ave, Charlotte, NC 28208 
06503204 Geraldine & Marshall Kendrick 4047 Avalon Ave, Charlotte, NC 28208 
06503215 Jewell P Carr 4037 Avalon Ave, Charlotte, NC 28208 
06503216 Timothy & Cortney Young 4031 Avalon Ave, Charlotte, NC 28208 
06503219 Brittany Kemper Fritz & Richard 
Brandon Runde 4025 Avalon Ave, Charlotte, NC 28208 
06503220 Alessandro Pasut & Brittany Elise 
Philip 4021 Avalon Ave, Charlotte, NC 28208 
06503201 Trent Kendrick 4047 Avalon Ave, Charlotte, NC 28208 

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
06503212 Berry Mountain Associates, LP 125 Old Home Place, Kings Mountain, NC 
28086 
06503214 Stephanie Deone Clay 5927 Carriage Oaks Dr, Charlotte, NC 
28262 
06503306 Frances K Pepper 1100 Crestmere St, Charlotte, NC 28208 
06503305 AJA Family Properties, LLC 20028 Knox Rd, Cornelius, NC 28031 
06503307 Mehdi Farahmand & Azadeh Hosseini 11822 Southcrest Ln, Pineville, NC 28134 
06503308 Loren Tamara & Pedro Luis Sanchez 4119 Avalon Ave, Charlotte, NC 28208 
06503304 Robert & Lillie Scott 14212 Kirkan Way, Huntersville, NC 
28078 
06503303 Fred & Edna Moretti 374 Camino Rd, Mooresville, NC 28117 
06503302 Fred & Edna Moretti 374 Camino Rd, Mooresville, NC 28117 
06503301 Mehdi Farahmand & Azadeh Hosseini 11822 Southcrest Ln, Pineville, NC 28134 
06503502 Collias Family Limited Liability 
Company 
8040 Arrowridge Blvd, 
Charlotte, NC 28273 
06503501 St George Holdings, LLC PO Box 240682, Charlotte, NC 28224 
06503402 Clementi Riverview LLC PO Box 471904, Charlotte, NC 28247 
06714101 Perry Family Farms LLC 2778 W Riverwalk Cir, Unit B, Littleton, 
CO 81023 
06714107 JP Investment Partners LLC 101 East Matthews St, Suite 500, 
Matthews, NC 28105 
06714108 General Business Properties LLC 2063 Kaylee Dr, The Villages, FL 32162 
06714109 MLM & R Investments, LLC 3301 Freedom Dr, Charlotte, NC 28208 
06714102 JP Investment Partners LLC 101 East Matthews St, Suite 500, 
Matthews, NC 28105 
06714208 Minnetonka Capital Investments, LLC 300 Wilmot Rd, Deerfield, IL 60015 
06714222 Mone Bia Properties, LLC 1308 Camellia Blvd, Suite 200, Lafayette, 
LA 70508 
06714204 Mecklenburg County 600 E Fourth St, 11th Floor, Charlotte, NC 
28202 
06714203 Novant Health, Inc. 2085 Frontis Plaza Blvd, Winston Salem, 
NC 27103 
09714202 Charlotte‐Mecklenburg Board of 
Education PO Box 30035, Charlotte, NC 28230 
06714201 Kingott, LLC PO Box 17901, Richmond, VA 23226 
Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
06713106 Esther Elder 5621 Alanhurst Pl, Charlotte, NC 28217 
06713117 Branful, LLC 104 Mull St, Morganton, NC 28688 
06713115 Jamestown Bob, LLC 2730 Rozzelles Ferry Rd, Suite A, 
Charlotte, NC 28208 

Note: 
1. Properties in Table 2 are correlated with those shown on Figure 2. 

Phase I LSA, 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Charlotte, North Carolina June 2, 2021

D:\!Michael!\!SUMMIT!\4493 - MPV Properties\4493.E0002 - 3200 Freedom Drive\LSA\Report Files\TABLES.docx
TABLE 2 
WATER SUPPLY WELL INFORMATION 
3200 Freedom Drive 

Well ID Parcel ID Property Owner(s) Mailing Address Distance From 
Source Area (feet) Well Depth 
Active/ 
Inactive 
(Use) 
Unknown 06503502 
Collias Family 
Limited Liability 
Company 
8040 Arrowridge Blvd, 
Charlotte, NC 28273 700’ NNW Unknown Monitoring 
Unknown 06503610 
Freedom 
Opportunity Fund, 
LLC 
121 W Trade St, Suite 2550, 
Charlotte, NC 28202 500’ ESE Unknown Monitoring 
Unknown 06714204 Mecklenburg 
County 
600 E Fourth St, 11th Floor, 
Charlotte, NC 28202 500’ WSW Unknown Monitoring 

Phase I LSA - 3200 Freedom Drive SUMMIT Project No. 4493.E0002 Limited Site Assessment Risk Classification and Land Use Form
3200 Freedom Drive, Charlotte, NC
Part I - Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including any used for non-drinking
purposes?YES/NO
If yes, explain.
2. Is a water supply well used for drinking water located within 1000 feet of the source area the discharge or
release?YES/NO
If yes, explain. No supply wells utilized for potable water were identified within 1,500 feet of the site.
3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial cooling water, filling
swimming pools) located within 250 feet of the source area of the release or discharge?YES/NO
4. Does groundwater within 500 feet of the source area of the discharge or release have the potential for
future use in that there is no other source of water supply other than the groundwater?YES/NO
Explain. Municipal water is available to the site and vicinity.
5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of the vapors
in a confined space or pose any other serious threat to public health, safety or the environment?YES/NO
If yes, explain.
6. Are there any other factors that would cause the discharge or release to pose an imminent danger to public
health, safety or the environment?YES/NO
If yes, explain.
Page 1
Phase I LSA - 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Limited Site Assessment Report
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the discharge or release?YES/NO
The nearest surface water occurs as a an un-named creek, and is approximately 1,000
feet east-southeast of the source area.
If yes, does the maximum groundwater contaminant concentration exceed the surface water quality standards
and criteria found in 15A NCAC 2B .0200 by a factor of 10?YES/NO
8. Is the source area of the discharge or release located within a designated wellhead protection area as defined
in 42 USC 300h-7(e)?YES/NO
If yes, explain.
9. Is the discharge or release located in the Coastal Plain physiographic region as designated on a map entitled
"Geology of North Carolina" published by the department in 1985?YES/NO
If yes, is the source area of the discharge or release located in an area in which there is recharge to an unconfined
or semi-confined deeper aquifer that is being used or may be used as a source of drinking water? YES/NO
If yes, explain.
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels
established (see Table 7) by the Department?YES/NO
Page 2
Phase I LSA - 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Limited Site Assessment Report
Part II - Land Use
Property Containing Source Area of Discharge or Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)?YES/NO
Explain.
2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly?YES/NO
Explain.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage etc.)
enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped?YES/NO
Explain. The site contains a vacant residential garage, which is scheduled for demolition.
4. Do children visit the property?YES/NO
Explain.
5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)?
YES/NO
Explain. The site is vacant, and access is restricted via a temporary fence.
6. Do pavement, buildings, or other structures cap the contaminant soil?YES/NO
Explain. The site is prodominantly paved.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will
remain capped in the foreseeable future?
Unknown at this time.
Page 3
Phase I LSA - 3200 Freedom Drive SUMMIT Project No. 4493.E0002
Limited Site Assessment Report
7. What is the zoning status of the property?
The site is zoned COMMERCIAL CENTER B-1SCD
8. Is the use of the property likely to change in the next 20 years?YES/NO
Explain.
The subject site is likely to be commercial for the next 20 years.
Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area area within 1,000 feet of the source area of discharge or release.
(excludes property containing source area of the release):
9 What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)? The nearest primary residence is approximately 500 north-northeast of the
source area.
10 What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly?
Phillip O Berry Academy of Technology is approximately 900 feet south of the source area.
11 What is the zoning status of the properties in the surrounding area?
The zoning designations of surrounding areas include COMMERCIAL CENTER B-1SCD
12 Briefly characterize the use and activities of the land in the surrounding area.
Commercially utilized properties border the site to the east, south and west (commercial offices), to the north
is residential.
Page 4
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Michael Zavislak
Project Name:3200 Freedom Drive
Project Number:4493.E0002
Lot Number:WE14021
Date Completed:05/27/2021
05/27/2021 4:21 PM
Approved and released by:
Project Manager II:Lucas Odom
Page 1 of 73
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:WE14021
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")
Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or
discussed below.
Where applicable,all soil sample results (including LOQ and DL if requested)are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VOCs by GC/MS
The laboratory control sample (LCS)for analytical batch 92641 exceeded acceptance criteria for Acetone.
This analyte is biased highbut not detected in the samples affected.
VPH
Surrogate recovery for the following sampl was outside the upper control limit:WE14021-001.This
sample did not contain any target analytes;therefore,re-extraction and/or re-analysis was not performed.
SVOCs by GC/MS
Due to the large number of spiked analytes,there is a high probability that one or more analytes will
recover outside acceptance limits.The laboratory's SOP allows for 10%of analytes to recover marginally
outside criteria.The following analytes recovered marginally outside LCS/LCSD criteria:bis(2-Chloro-1-
methylethyl)ether.
The following sample was diluted due to appearance or color:WE14021-001.The LOQ has been
elevated to reflect the dilution.
Page 2 of 73
PACE ANALYTICAL SERVICES, LLC
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: WE14021

Sample Number Sample ID Matrix Date Sampled Date Received
001 05/08/2021 1700S-1/Soil Solid 05/13/2021
002 05/12/2021 1130W-1/Water Aqueous 05/14/2021
003 05/08/2021S-1 @10 Solid 05/14/2021
(3 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 73
PACE ANALYTICAL SERVICES, LLC
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: WE14021

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 S-1/Soil Solid Acetone 8260D 11 JL ug/kg 6
001 S-1/Soil Solid Lead 6010D 2.8 J mg/kg 10
002 W-1/Water Aqueous Acetone 8260D 8.0 JL ug/L 11
002 W-1/Water Aqueous Methyl tertiary butyl ether 8260D 2.6 ug/L 11
002 W-1/Water Aqueous Acetophenone 8270E 0.61 J ug/L 12
002 W-1/Water Aqueous Caprolactam 8270E 2.2 J ug/L 12
002 W-1/Water Aqueous Diethylphthalate 8270E 0.55 J ug/L 13
002 W-1/Water Aqueous bis(2-Ethylhexyl)phthalate 8270E 0.55 J ug/L 13
002 W-1/Water Aqueous C9 - C12 Aliphatics MADEP-VPH-30 J ug/L 15
002 W-1/Water Aqueous Lead 6010D 0.20 mg/L 15
003 S-1 @10 Solid Acetone 8260D 10 JL ug/kg 16
003 S-1 @10 Solid Benzo(a)anthracene 8270E 10 J ug/kg 17
003 S-1 @10 Solid Benzo(a)pyrene 8270E 27 ug/kg 17
003 S-1 @10 Solid Benzo(b)fluoranthene 8270E 42 ug/kg 17
003 S-1 @10 Solid Benzo(g,h,i)perylene 8270E 16 J ug/kg 17
003 S-1 @10 Solid Benzo(k)fluoranthene 8270E 15 J ug/kg 17
003 S-1 @10 Solid Chrysene 8270E 14 J ug/kg 18
003 S-1 @10 Solid Di-n-butyl phthalate 8270E 55 BJ ug/kg 18
003 S-1 @10 Solid Fluoranthene 8270E 11 J ug/kg 18
003 S-1 @10 Solid Indeno(1,2,3-c,d)pyrene 8270E 13 J ug/kg 18
003 S-1 @10 Solid Pyrene 8270E 9.5 J ug/kg 19
003 S-1 @10 Solid Lead 6010D 3.9 mg/kg 20
(22 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1/Soil
WE14021-001
05/08/2021 1700
05/13/2021
Solid
% Solids:78.5 05/14/2021 2218
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 05/14/2021 1504 JM1 92316 5.30
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D 11 JL 1ug/kg9.624
Benzene 71-43-2 8260D ND 1ug/kg2.46.0
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.46.0
Bromoform 75-25-2 8260D ND 1ug/kg2.46.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.66.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.824
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.46.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.46.0
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.46.0
Chloroethane 75-00-3 8260D ND 1ug/kg2.46.0
Chloroform 67-66-3 8260D ND 1ug/kg2.46.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.66.0
Cyclohexane 110-82-7 8260D ND 1ug/kg2.46.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.46.0
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.46.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.46.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.46.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.46.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.46.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.66.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.46.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.46.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.46.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.46.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.46.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.46.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.46.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.46.0
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.46.0
2-Hexanone 591-78-6 8260D ND 1ug/kg4.812
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.46.0
Methyl acetate 79-20-9 8260D ND 1ug/kg2.46.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.46.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.812
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.46.0
Methylene chloride 75-09-2 8260D ND 1ug/kg2.46.0
Styrene 100-42-5 8260D ND 1ug/kg2.46.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.46.0
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.46.0
Toluene 108-88-3 8260D ND 1ug/kg2.46.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1/Soil
WE14021-001
05/08/2021 1700
05/13/2021
Solid
% Solids:78.5 05/14/2021 2218
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 05/14/2021 1504 JM1 92316 5.30
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.46.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.46.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.46.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.46.0
Trichloroethene 79-01-6 8260D ND 1ug/kg2.46.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.46.0
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.66.0
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.812
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 47-138
1,2-Dichloroethane-d4 90 53-142
Toluene-d8 114 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 05/21/2021 2007 STM 05/14/2021 2010 92387
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg5.016
Acenaphthylene 208-96-8 8270E ND 1ug/kg5.716
Acetophenone 98-86-2 8270E ND 1ug/kg3079
Anthracene 120-12-7 8270E ND 1ug/kg3.116
Atrazine 1912-24-9 8270E ND 1ug/kg3079
Benzaldehyde 100-52-7 8270E ND 1ug/kg3079
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg3.616
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg4.016
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg3.016
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg3.916
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg2.916
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg3079
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg3079
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg3079
Caprolactam 105-60-2 8270E ND 1ug/kg3079
Carbazole 86-74-8 8270E ND 1ug/kg3079
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND L 1ug/kg3079
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg3079
4-Chloroaniline 106-47-8 8270E ND 1ug/kg3079
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg3079
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1/Soil
WE14021-001
05/08/2021 1700
05/13/2021
Solid
% Solids:78.5 05/14/2021 2218
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 05/21/2021 2007 STM 05/14/2021 2010 92387
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg3079
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg3079
2-Chlorophenol 95-57-8 8270E ND 1ug/kg3079
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg3079
Chrysene 218-01-9 8270E ND 1ug/kg2.716
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg3.116
Dibenzofuran 132-64-9 8270E ND 1ug/kg3079
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg3079
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg3079
Diethylphthalate 84-66-2 8270E ND 1ug/kg3079
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg4579
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg3079
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg3079
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg150410
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg150410
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg61160
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg61160
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg3079
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg150410
Fluoranthene 206-44-0 8270E ND 1ug/kg2.516
Fluorene 86-73-7 8270E ND 1ug/kg3.416
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg3079
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg3079
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg150410
Hexachloroethane 67-72-1 8270E ND 1ug/kg3079
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg6.116
Isophorone 78-59-1 8270E ND 1ug/kg3079
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg6.016
2-Methylphenol 95-48-7 8270E ND 1ug/kg3079
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg61160
Naphthalene 91-20-3 8270E ND 1ug/kg5.916
2-Nitroaniline 88-74-4 8270E ND 1ug/kg61160
3-Nitroaniline 99-09-2 8270E ND 1ug/kg61160
4-Nitroaniline 100-01-6 8270E ND 1ug/kg61160
Nitrobenzene 98-95-3 8270E ND 1ug/kg3079
2-Nitrophenol 88-75-5 8270E ND 1ug/kg61160
4-Nitrophenol 100-02-7 8270E ND 1ug/kg150410
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg3079
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg3079
Pentachlorophenol 87-86-5 8270E ND 1ug/kg150410
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1/Soil
WE14021-001
05/08/2021 1700
05/13/2021
Solid
% Solids:78.5 05/14/2021 2218
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 05/21/2021 2007 STM 05/14/2021 2010 92387
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Phenanthrene 85-01-8 8270E ND 1ug/kg4.416
Phenol 108-95-2 8270E ND 1ug/kg3079
Pyrene 129-00-0 8270E ND 1ug/kg3.016
Pyridine 110-86-1 8270E ND 1ug/kg3079
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg3079
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg3079
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 90 33-102
2-Fluorophenol 85 35-115
Nitrobenzene-d5 90 22-109
Phenol-d5 87 33-122
Terphenyl-d14 103 41-120
2,4,6-Tribromophenol 96 30-117
MA EPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 1 05/20/2021 0509 NCM 05/17/2021 1107 92473
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)91 40-140
2-Fluorobiphenyl (fractionation 1)98 40-140
o - Terphenyl (aromatic)79 40-140
MA EPH (aliphatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 1 05/20/2021 0923 NCM 05/17/2021 1107 92472
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212
C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212
AcceptanceRun 1
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)98 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1/Soil
WE14021-001
05/08/2021 1700
05/13/2021
Solid
% Solids:78.5 05/14/2021 2218
MADEP VPH (aliphatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 05/19/2021 1716 ECB 92778
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C5 - C8 Aliphatics MADEP-VPH-18-ND Q 1mg/kg1.15.4
C9 - C12 Aliphatics MADEP-VPH-18-ND Q 1mg/kg1.15.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)N 154 70-130
MADEP VPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 05/19/2021 1716 ECB 92779
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C10 Aromatics MADEP-VPH-18-ND 1mg/kg0.721.8
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)124 70-130
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 5 05/17/2021 0914 JMH 05/16/2021 0521 92327
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Lead 7439-92-1 6010D 2.8 J 1mg/kg1.32.9
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
W-1/Water
WE14021-002
05/12/2021 1130
05/14/2021
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/18/2021 1621 BWS 92641
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D 8.0 JL 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
Carbon disulfide 75-15-0 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
Cyclohexane 110-82-7 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 2.6 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260D ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
W-1/Water
WE14021-002
05/12/2021 1130
05/14/2021
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/18/2021 1621 BWS 92641
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 106 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 05/25/2021 1326 STM 05/14/2021 1705 92374
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/L0.0400.16
Acenaphthylene 208-96-8 8270E ND 1ug/L0.0400.16
Acetophenone 98-86-2 8270E 0.61 J 1ug/L0.230.80
Anthracene 120-12-7 8270E ND 1ug/L0.0400.16
Atrazine 1912-24-9 8270E ND 1ug/L0.200.80
Benzaldehyde 100-52-7 8270E ND 1ug/L0.274.0
Benzo(a)anthracene 56-55-3 8270E ND 1ug/L0.0400.16
Benzo(a)pyrene 50-32-8 8270E ND 1ug/L0.0400.16
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/L0.0400.16
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/L0.0400.16
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/L0.0400.16
1,1'-Biphenyl 92-52-4 8270E ND 1ug/L0.210.80
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/L0.150.80
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/L0.214.0
Caprolactam 105-60-2 8270E 2.2 J 1ug/L0.714.0
Carbazole 86-74-8 8270E ND 1ug/L0.0400.80
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/L0.170.80
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/L0.260.80
4-Chloroaniline 106-47-8 8270E ND 1ug/L0.130.80
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/L0.0600.80
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
W-1/Water
WE14021-002
05/12/2021 1130
05/14/2021
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 05/25/2021 1326 STM 05/14/2021 1705 92374
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/L0.160.80
2-Chloronaphthalene 91-58-7 8270E ND 1ug/L0.150.80
2-Chlorophenol 95-57-8 8270E ND 1ug/L0.150.80
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/L0.160.80
Chrysene 218-01-9 8270E ND 1ug/L0.0400.16
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/L0.0400.16
Dibenzofuran 132-64-9 8270E ND 1ug/L0.160.80
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/L0.814.0
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/L0.190.80
Diethylphthalate 84-66-2 8270E 0.55 J 1ug/L0.194.0
Dimethyl phthalate 131-11-3 8270E ND 1ug/L0.184.0
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/L0.150.80
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/L0.424.0
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/L0.894.0
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/L1.34.0
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/L0.361.6
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/L0.341.6
Di-n-octylphthalate 117-84-0 8270E ND 1ug/L0.484.0
bis(2-Ethylhexyl)phthalate 117-81-7 8270E 0.55 J 1ug/L0.384.0
Fluoranthene 206-44-0 8270E ND 1ug/L0.0400.16
Fluorene 86-73-7 8270E ND 1ug/L0.0400.16
Hexachlorobenzene 118-74-1 8270E ND 1ug/L0.150.80
Hexachlorobutadiene 87-68-3 8270E ND 1ug/L0.170.80
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/L1.14.0
Hexachloroethane 67-72-1 8270E ND 1ug/L0.170.80
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/L0.0400.16
Isophorone 78-59-1 8270E ND 1ug/L0.220.80
2-Methylnaphthalene 91-57-6 8270E ND 1ug/L0.0400.16
2-Methylphenol 95-48-7 8270E ND 1ug/L0.210.80
3+4-Methylphenol 106-44-5 8270E ND 1ug/L0.461.6
Naphthalene 91-20-3 8270E ND 1ug/L0.0400.16
2-Nitroaniline 88-74-4 8270E ND 1ug/L0.661.6
3-Nitroaniline 99-09-2 8270E ND 1ug/L0.151.6
4-Nitroaniline 100-01-6 8270E ND 1ug/L1.31.6
Nitrobenzene 98-95-3 8270E ND 1ug/L0.170.80
2-Nitrophenol 88-75-5 8270E ND 1ug/L0.441.6
4-Nitrophenol 100-02-7 8270E ND 1ug/L2.14.0
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/L0.280.80
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/L0.500.80
Pentachlorophenol 87-86-5 8270E ND 1ug/L1.34.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
W-1/Water
WE14021-002
05/12/2021 1130
05/14/2021
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 05/25/2021 1326 STM 05/14/2021 1705 92374
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Phenanthrene 85-01-8 8270E ND 1ug/L0.0400.16
Phenol 108-95-2 8270E ND 1ug/L0.190.80
Pyrene 129-00-0 8270E ND 1ug/L0.0400.16
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/L0.190.80
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/L0.220.80
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 72 37-129
2-Fluorophenol 47 24-127
Nitrobenzene-d5 82 38-127
Phenol-d5 60 28-128
Terphenyl-d14 64 10-148
2,4,6-Tribromophenol 77 35-144
MADEP EPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH-MADEP-EPH-04 1 05/26/2021 2135 NCM 05/26/2021 0850 93401
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C11 - C22 Aromatics MADEP-EPH-04 ND 2ug/L130130
AcceptanceRun 2
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)80 40-140
2-Fluorobiphenyl (fractionation 1)93 40-140
2-Bromonaphthalene (fractionation 2)94 40-140
MADEP EPH (aliphatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH-MADEP-EPH-04 1 05/26/2021 1807 NCM 05/26/2021 0850 93400
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C18 Aliphatics MADEP-EPH-04 ND 2ug/L130130
C19 - C36 Aliphatics MADEP-EPH-04 ND 2ug/L130130
AcceptanceRun 2
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)64 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
W-1/Water
WE14021-002
05/12/2021 1130
05/14/2021
Aqueous
MADEP VPH (aliphatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 05/19/2021 1522 ECB 92780
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C5 - C8 Aliphatics MADEP-VPH-18-ND 1ug/L1575
C9 - C12 Aliphatics MADEP-VPH-18-30 J 1ug/L1575
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)104 70-130
MADEP VPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 05/19/2021 1522 ECB 92782
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C10 Aromatics MADEP-VPH-18-ND 1ug/L5.025
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)86 70-130
ICP-AES Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6010D 5 05/17/2021 0757 JMH 05/16/2021 0645 92433
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Lead 7439-92-1 6010D 0.20 1mg/L0.0240.050
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1 @10
WE14021-003
05/08/2021
05/14/2021
Solid
% Solids:81.2 05/14/2021 2218
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 05/14/2021 1527 JM1 92316 5.14
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D 10 JL 1ug/kg9.624
Benzene 71-43-2 8260D ND 1ug/kg2.46.0
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.46.0
Bromoform 75-25-2 8260D ND 1ug/kg2.46.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.66.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.824
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.46.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.46.0
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.46.0
Chloroethane 75-00-3 8260D ND 1ug/kg2.46.0
Chloroform 67-66-3 8260D ND 1ug/kg2.46.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.66.0
Cyclohexane 110-82-7 8260D ND 1ug/kg2.46.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.46.0
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.46.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.46.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.46.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.46.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.46.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.66.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.46.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.46.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.46.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.46.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.46.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.46.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.46.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.46.0
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.46.0
2-Hexanone 591-78-6 8260D ND 1ug/kg4.812
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.46.0
Methyl acetate 79-20-9 8260D ND 1ug/kg2.46.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.46.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.812
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.46.0
Methylene chloride 75-09-2 8260D ND 1ug/kg2.46.0
Styrene 100-42-5 8260D ND 1ug/kg2.46.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.46.0
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.46.0
Toluene 108-88-3 8260D ND 1ug/kg2.46.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1 @10
WE14021-003
05/08/2021
05/14/2021
Solid
% Solids:81.2 05/14/2021 2218
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 05/14/2021 1527 JM1 92316 5.14
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.46.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.46.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.46.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.46.0
Trichloroethene 79-01-6 8260D ND 1ug/kg2.46.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.46.0
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.66.0
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.812
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 107 47-138
1,2-Dichloroethane-d4 97 53-142
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 05/21/2021 2032 STM 05/14/2021 2010 92387
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg5.117
Acenaphthylene 208-96-8 8270E ND 1ug/kg5.817
Acetophenone 98-86-2 8270E ND 1ug/kg3180
Anthracene 120-12-7 8270E ND 1ug/kg3.117
Atrazine 1912-24-9 8270E ND 1ug/kg3180
Benzaldehyde 100-52-7 8270E ND 1ug/kg3180
Benzo(a)anthracene 56-55-3 8270E 10 J 1ug/kg3.617
Benzo(a)pyrene 50-32-8 8270E 27 1ug/kg4.017
Benzo(b)fluoranthene 205-99-2 8270E 42 1ug/kg3.117
Benzo(g,h,i)perylene 191-24-2 8270E 16 J 1ug/kg4.017
Benzo(k)fluoranthene 207-08-9 8270E 15 J 1ug/kg2.917
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg3180
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg3180
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg3180
Caprolactam 105-60-2 8270E ND 1ug/kg3180
Carbazole 86-74-8 8270E ND 1ug/kg3180
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND L 1ug/kg3180
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg3180
4-Chloroaniline 106-47-8 8270E ND 1ug/kg3180
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg3180
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1 @10
WE14021-003
05/08/2021
05/14/2021
Solid
% Solids:81.2 05/14/2021 2218
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 05/21/2021 2032 STM 05/14/2021 2010 92387
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg3180
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg3180
2-Chlorophenol 95-57-8 8270E ND 1ug/kg3180
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg3180
Chrysene 218-01-9 8270E 14 J 1ug/kg2.817
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg3.117
Dibenzofuran 132-64-9 8270E ND 1ug/kg3180
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg3180
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg3180
Diethylphthalate 84-66-2 8270E ND 1ug/kg3180
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg4580
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg3180
Di-n-butyl phthalate 84-74-2 8270E 55 BJ 1ug/kg3180
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg150410
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg150410
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg61170
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg61170
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg3180
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg150410
Fluoranthene 206-44-0 8270E 11 J 1ug/kg2.617
Fluorene 86-73-7 8270E ND 1ug/kg3.517
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg3180
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg3180
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg150410
Hexachloroethane 67-72-1 8270E ND 1ug/kg3180
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 13 J 1ug/kg6.117
Isophorone 78-59-1 8270E ND 1ug/kg3180
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg6.117
2-Methylphenol 95-48-7 8270E ND 1ug/kg3180
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg61170
Naphthalene 91-20-3 8270E ND 1ug/kg5.917
2-Nitroaniline 88-74-4 8270E ND 1ug/kg61170
3-Nitroaniline 99-09-2 8270E ND 1ug/kg61170
4-Nitroaniline 100-01-6 8270E ND 1ug/kg61170
Nitrobenzene 98-95-3 8270E ND 1ug/kg3180
2-Nitrophenol 88-75-5 8270E ND 1ug/kg61170
4-Nitrophenol 100-02-7 8270E ND 1ug/kg150410
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg3180
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg3180
Pentachlorophenol 87-86-5 8270E ND 1ug/kg150410
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1 @10
WE14021-003
05/08/2021
05/14/2021
Solid
% Solids:81.2 05/14/2021 2218
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 05/21/2021 2032 STM 05/14/2021 2010 92387
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Phenanthrene 85-01-8 8270E ND 1ug/kg4.417
Phenol 108-95-2 8270E ND 1ug/kg3180
Pyrene 129-00-0 8270E 9.5 J 1ug/kg3.117
Pyridine 110-86-1 8270E ND 1ug/kg3180
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg3180
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg3180
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 83 33-102
2-Fluorophenol 93 35-115
Nitrobenzene-d5 72 22-109
Phenol-d5 103 33-122
Terphenyl-d14 84 41-120
2,4,6-Tribromophenol 92 30-117
MA EPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 1 05/20/2021 0540 NCM 05/17/2021 1107 92473
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)88 40-140
2-Fluorobiphenyl (fractionation 1)98 40-140
o - Terphenyl (aromatic)81 40-140
MA EPH (aliphatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 1 05/20/2021 0954 NCM 05/17/2021 1107 92472
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212
C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212
AcceptanceRun 1
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)99 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
S-1 @10
WE14021-003
05/08/2021
05/14/2021
Solid
% Solids:81.2 05/14/2021 2218
MADEP VPH (aliphatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 05/19/2021 1745 ECB 92778
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.1
C9 - C12 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.1
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)116 70-130
MADEP VPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 05/19/2021 1745 ECB 92779
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C10 Aromatics MADEP-VPH-18-ND 1mg/kg0.681.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)93 70-130
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 5 05/17/2021 0933 JMH 05/16/2021 0521 92327
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Lead 7439-92-1 6010D 3.9 1mg/kg1.32.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 73
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:WQ92316-001
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 05/14/2021 1007208.0 ug/kg1
Benzene ND 05/14/2021 10075.0 2.0 ug/kg1
Bromodichloromethane ND 05/14/2021 10075.0 2.0 ug/kg1
Bromoform ND 05/14/2021 10075.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 05/14/2021 10075.0 3.0 ug/kg1
2-Butanone (MEK)ND 05/14/2021 1007204.0 ug/kg1
Carbon disulfide ND 05/14/2021 10075.0 2.0 ug/kg1
Carbon tetrachloride ND 05/14/2021 10075.0 2.0 ug/kg1
Chlorobenzene ND 05/14/2021 10075.0 2.0 ug/kg1
Chloroethane ND 05/14/2021 10075.0 2.0 ug/kg1
Chloroform ND 05/14/2021 10075.0 2.0 ug/kg1
Chloromethane (Methyl chloride)ND 05/14/2021 10075.0 3.0 ug/kg1
Cyclohexane ND 05/14/2021 10075.0 2.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 05/14/2021 10075.0 2.0 ug/kg1
Dibromochloromethane ND 05/14/2021 10075.0 2.0 ug/kg1
1,2-Dibromoethane (EDB)ND 05/14/2021 10075.0 2.0 ug/kg1
1,2-Dichlorobenzene ND 05/14/2021 10075.0 2.0 ug/kg1
1,3-Dichlorobenzene ND 05/14/2021 10075.0 2.0 ug/kg1
1,4-Dichlorobenzene ND 05/14/2021 10075.0 2.0 ug/kg1
Dichlorodifluoromethane ND 05/14/2021 10075.0 3.0 ug/kg1
1,1-Dichloroethane ND 05/14/2021 10075.0 2.0 ug/kg1
1,2-Dichloroethane ND 05/14/2021 10075.0 2.0 ug/kg1
1,1-Dichloroethene ND 05/14/2021 10075.0 2.0 ug/kg1
cis-1,2-Dichloroethene ND 05/14/2021 10075.0 2.0 ug/kg1
trans-1,2-Dichloroethene ND 05/14/2021 10075.0 2.0 ug/kg1
1,2-Dichloropropane ND 05/14/2021 10075.0 2.0 ug/kg1
cis-1,3-Dichloropropene ND 05/14/2021 10075.0 2.0 ug/kg1
trans-1,3-Dichloropropene ND 05/14/2021 10075.0 2.0 ug/kg1
Ethylbenzene ND 05/14/2021 10075.0 2.0 ug/kg1
2-Hexanone ND 05/14/2021 1007104.0 ug/kg1
Isopropylbenzene ND 05/14/2021 10075.0 2.0 ug/kg1
Methyl acetate ND 05/14/2021 10075.0 2.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 05/14/2021 10075.0 2.0 ug/kg1
4-Methyl-2-pentanone ND 05/14/2021 1007104.0 ug/kg1
Methylcyclohexane ND 05/14/2021 10075.0 2.0 ug/kg1
Methylene chloride ND 05/14/2021 10075.0 2.0 ug/kg1
Styrene ND 05/14/2021 10075.0 2.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 05/14/2021 10075.0 2.0 ug/kg1
Tetrachloroethene ND 05/14/2021 10075.0 2.0 ug/kg1
Toluene ND 05/14/2021 10075.0 2.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 05/14/2021 10075.0 2.0 ug/kg1
1,2,4-Trichlorobenzene ND 05/14/2021 10075.0 2.0 ug/kg1
1,1,1-Trichloroethane ND 05/14/2021 10075.0 2.0 ug/kg1
1,1,2-Trichloroethane ND 05/14/2021 10075.0 2.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 21 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:WQ92316-001
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 05/14/2021 10075.0 2.0 ug/kg1
Trichlorofluoromethane ND 05/14/2021 10075.0 2.0 ug/kg1
Vinyl chloride ND 05/14/2021 10075.0 3.0 ug/kg1
Xylenes (total)ND 05/14/2021 1007104.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 104 47-138
1,2-Dichloroethane-d4 93 53-142
Toluene-d8 102 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 22 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:WQ92316-002
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/kg)(ug/kg)
Acetone 140 05/14/2021 0921N14210060-1401
Benzene 50 05/14/2021 09211005070-1301
Bromodichloromethane 53 05/14/2021 09211075070-1301
Bromoform 57 05/14/2021 09211135070-1301
Bromomethane (Methyl bromide)51 05/14/2021 09211035070-1301
2-Butanone (MEK)130 05/14/2021 092112810060-1401
Carbon disulfide 52 05/14/2021 09211045070-1301
Carbon tetrachloride 51 05/14/2021 09211035070-1301
Chlorobenzene 52 05/14/2021 09211055070-1301
Chloroethane 50 05/14/2021 09211005070-1301
Chloroform 51 05/14/2021 09211015070-1301
Chloromethane (Methyl chloride)46 05/14/2021 0921935060-1401
Cyclohexane 47 05/14/2021 0921935070-1301
1,2-Dibromo-3-chloropropane (DBCP)52 05/14/2021 09211055070-1301
Dibromochloromethane 50 05/14/2021 09211005070-1301
1,2-Dibromoethane (EDB)55 05/14/2021 09211105070-1301
1,2-Dichlorobenzene 50 05/14/2021 09211015070-1301
1,3-Dichlorobenzene 51 05/14/2021 09211015070-1301
1,4-Dichlorobenzene 51 05/14/2021 09211025070-1301
Dichlorodifluoromethane 47 05/14/2021 0921955060-1401
1,1-Dichloroethane 50 05/14/2021 09211005070-1301
1,2-Dichloroethane 49 05/14/2021 0921985070-1301
1,1-Dichloroethene 50 05/14/2021 09211005070-1301
cis-1,2-Dichloroethene 51 05/14/2021 09211025070-1301
trans-1,2-Dichloroethene 51 05/14/2021 09211035070-1301
1,2-Dichloropropane 48 05/14/2021 0921975070-1301
cis-1,3-Dichloropropene 53 05/14/2021 09211055070-1301
trans-1,3-Dichloropropene 53 05/14/2021 09211065070-1301
Ethylbenzene 54 05/14/2021 09211095070-1301
2-Hexanone 110 05/14/2021 092111210070-1301
Isopropylbenzene 54 05/14/2021 09211085070-1301
Methyl acetate 45 05/14/2021 0921895070-1301
Methyl tertiary butyl ether (MTBE)50 05/14/2021 09211005070-1301
4-Methyl-2-pentanone 100 05/14/2021 092110010070-1301
Methylcyclohexane 52 05/14/2021 09211035070-1301
Methylene chloride 48 05/14/2021 0921975070-1301
Styrene 54 05/14/2021 09211085070-1301
1,1,2,2-Tetrachloroethane 53 05/14/2021 09211055070-1301
Tetrachloroethene 55 05/14/2021 09211115070-1301
Toluene 53 05/14/2021 09211065070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 05/14/2021 09211015070-1301
1,2,4-Trichlorobenzene 58 05/14/2021 09211165070-1301
1,1,1-Trichloroethane 52 05/14/2021 09211045070-1301
1,1,2-Trichloroethane 53 05/14/2021 09211065070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 23 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:WQ92316-002
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 52 05/14/2021 09211045070-1301
Trichlorofluoromethane 50 05/14/2021 09211005070-1301
Vinyl chloride 43 05/14/2021 0921865070-1301
Xylenes (total)110 05/14/2021 092111010070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 106 47-138
1,2-Dichloroethane-d4 98 53-142
Toluene-d8 103 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 24 of 73
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:WE14021-001DU
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
%RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Acetone ND 05/14/2021 19430.00 20111
Benzene ND 05/14/2021 19430.00 20ND1
Bromodichloromethane ND 05/14/2021 19430.00 20ND1
Bromoform ND 05/14/2021 19430.00 20ND1
Bromomethane (Methyl bromide)ND 05/14/2021 19430.00 20ND1
2-Butanone (MEK)ND 05/14/2021 19430.00 20ND1
Carbon disulfide ND 05/14/2021 19430.00 20ND1
Carbon tetrachloride ND 05/14/2021 19430.00 20ND1
Chlorobenzene ND 05/14/2021 19430.00 20ND1
Chloroethane ND 05/14/2021 19430.00 20ND1
Chloroform ND 05/14/2021 19430.00 20ND1
Chloromethane (Methyl chloride)ND 05/14/2021 19430.00 20ND1
Cyclohexane ND 05/14/2021 19430.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 05/14/2021 19430.00 20ND1
Dibromochloromethane ND 05/14/2021 19430.00 20ND1
1,2-Dibromoethane (EDB)ND 05/14/2021 19430.00 20ND1
1,2-Dichlorobenzene ND 05/14/2021 19430.00 20ND1
1,3-Dichlorobenzene ND 05/14/2021 19430.00 20ND1
1,4-Dichlorobenzene ND 05/14/2021 19430.00 20ND1
Dichlorodifluoromethane ND 05/14/2021 19430.00 20ND1
1,1-Dichloroethane ND 05/14/2021 19430.00 20ND1
1,2-Dichloroethane ND 05/14/2021 19430.00 20ND1
1,1-Dichloroethene ND 05/14/2021 19430.00 20ND1
cis-1,2-Dichloroethene ND 05/14/2021 19430.00 20ND1
trans-1,2-Dichloroethene ND 05/14/2021 19430.00 20ND1
1,2-Dichloropropane ND 05/14/2021 19430.00 20ND1
cis-1,3-Dichloropropene ND 05/14/2021 19430.00 20ND1
trans-1,3-Dichloropropene ND 05/14/2021 19430.00 20ND1
Ethylbenzene ND 05/14/2021 19430.00 20ND1
2-Hexanone ND 05/14/2021 19430.00 20ND1
Isopropylbenzene ND 05/14/2021 19430.00 20ND1
Methyl acetate ND 05/14/2021 19430.00 20ND1
Methyl tertiary butyl ether (MTBE)ND 05/14/2021 19430.00 20ND1
4-Methyl-2-pentanone ND 05/14/2021 19430.00 20ND1
Methylcyclohexane ND 05/14/2021 19430.00 20ND1
Methylene chloride ND 05/14/2021 19430.00 20ND1
Styrene ND 05/14/2021 19430.00 20ND1
1,1,2,2-Tetrachloroethane ND 05/14/2021 19430.00 20ND1
Tetrachloroethene ND 05/14/2021 19430.00 20ND1
Toluene ND 05/14/2021 19430.00 20ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 05/14/2021 19430.00 20ND1
1,2,4-Trichlorobenzene ND 05/14/2021 19430.00 20ND1
1,1,1-Trichloroethane ND 05/14/2021 19430.00 20ND1
1,1,2-Trichloroethane ND 05/14/2021 19430.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 25 of 73
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:WE14021-001DU
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
%RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Trichloroethene ND 05/14/2021 19430.00 20ND1
Trichlorofluoromethane ND 05/14/2021 19430.00 20ND1
Vinyl chloride ND 05/14/2021 19430.00 20ND1
Xylenes (total)ND 05/14/2021 19430.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 107 47-138
1,2-Dichloroethane-d4 106 53-142
Toluene-d8 102 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 26 of 73
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:WE14021-003MS
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 140 05/14/2021 200611211070-130101
Benzene 54 05/14/2021 2006945770-130ND1
Bromodichloromethane 58 05/14/2021 20061015770-130ND1
Bromoform 60 05/14/2021 20061045770-130ND1
Bromomethane (Methyl bromide)56 05/14/2021 2006975770-130ND1
2-Butanone (MEK)130 05/14/2021 200611011070-130ND1
Carbon disulfide 55 05/14/2021 2006965770-130ND1
Carbon tetrachloride 56 05/14/2021 2006985770-130ND1
Chlorobenzene 56 05/14/2021 2006975770-130ND1
Chloroethane 53 05/14/2021 2006925770-130ND1
Chloroform 54 05/14/2021 2006945770-130ND1
Chloromethane (Methyl chloride)50 05/14/2021 2006875760-140ND1
Cyclohexane 55 05/14/2021 2006955770-130ND1
1,2-Dibromo-3-chloropropane (DBCP)54 05/14/2021 2006955770-130ND1
Dibromochloromethane 54 05/14/2021 2006945770-130ND1
1,2-Dibromoethane (EDB)59 05/14/2021 20061035770-130ND1
1,2-Dichlorobenzene 54 05/14/2021 2006935770-130ND1
1,3-Dichlorobenzene 54 05/14/2021 2006945770-130ND1
1,4-Dichlorobenzene 55 05/14/2021 2006955770-130ND1
Dichlorodifluoromethane 59 05/14/2021 20061035760-140ND1
1,1-Dichloroethane 53 05/14/2021 2006925770-130ND1
1,2-Dichloroethane 53 05/14/2021 2006935770-130ND1
1,1-Dichloroethene 54 05/14/2021 2006935770-130ND1
cis-1,2-Dichloroethene 54 05/14/2021 2006945770-130ND1
trans-1,2-Dichloroethene 55 05/14/2021 2006965770-130ND1
1,2-Dichloropropane 53 05/14/2021 2006925770-130ND1
cis-1,3-Dichloropropene 57 05/14/2021 2006995770-130ND1
trans-1,3-Dichloropropene 56 05/14/2021 2006975770-130ND1
Ethylbenzene 58 05/14/2021 20061005770-130ND1
2-Hexanone 120 05/14/2021 200610211070-130ND1
Isopropylbenzene 56 05/14/2021 2006985770-130ND1
Methyl acetate 52 05/14/2021 2006915770-130ND1
Methyl tertiary butyl ether (MTBE)54 05/14/2021 2006955770-130ND1
4-Methyl-2-pentanone 110 05/14/2021 20069511070-130ND1
Methylcyclohexane 65 05/14/2021 20061125770-130ND1
Methylene chloride 52 05/14/2021 2006905770-130ND1
Styrene 58 05/14/2021 20061005770-130ND1
1,1,2,2-Tetrachloroethane 57 05/14/2021 2006995770-130ND1
Tetrachloroethene 61 05/14/2021 20061065770-130ND1
Toluene 57 05/14/2021 20061005770-130ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane 62 05/14/2021 20061085770-130ND1
1,2,4-Trichlorobenzene 60 05/14/2021 20061045770-130ND1
1,1,1-Trichloroethane 56 05/14/2021 2006975770-130ND1
1,1,2-Trichloroethane 58 05/14/2021 20061015770-130ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 27 of 73
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:WE14021-003MS
92316 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Trichloroethene 56 05/14/2021 2006985770-130ND1
Trichlorofluoromethane 60 05/14/2021 20061045770-130ND1
Vinyl chloride 48 05/14/2021 2006845770-130ND1
Xylenes (total)120 05/14/2021 200610211070-130ND1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 106 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 104 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 28 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:WQ92641-001
92641 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 05/18/2021 1021205.0 ug/L1
Benzene ND 05/18/2021 10211.0 0.40 ug/L1
Bromodichloromethane ND 05/18/2021 10211.0 0.40 ug/L1
Bromoform ND 05/18/2021 10211.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 05/18/2021 10212.0 0.40 ug/L1
2-Butanone (MEK)ND 05/18/2021 1021102.0 ug/L1
Carbon disulfide ND 05/18/2021 10211.0 0.40 ug/L1
Carbon tetrachloride ND 05/18/2021 10211.0 0.40 ug/L1
Chlorobenzene ND 05/18/2021 10211.0 0.40 ug/L1
Chloroethane ND 05/18/2021 10212.0 0.40 ug/L1
Chloroform ND 05/18/2021 10211.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 05/18/2021 10211.0 0.50 ug/L1
Cyclohexane ND 05/18/2021 10211.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 05/18/2021 10211.0 0.40 ug/L1
Dibromochloromethane ND 05/18/2021 10211.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 05/18/2021 10211.0 0.40 ug/L1
1,2-Dichlorobenzene ND 05/18/2021 10211.0 0.40 ug/L1
1,3-Dichlorobenzene ND 05/18/2021 10211.0 0.40 ug/L1
1,4-Dichlorobenzene ND 05/18/2021 10211.0 0.40 ug/L1
Dichlorodifluoromethane ND 05/18/2021 10212.0 0.60 ug/L1
1,1-Dichloroethane ND 05/18/2021 10211.0 0.40 ug/L1
1,2-Dichloroethane ND 05/18/2021 10211.0 0.40 ug/L1
1,1-Dichloroethene ND 05/18/2021 10211.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 05/18/2021 10211.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 05/18/2021 10211.0 0.40 ug/L1
1,2-Dichloropropane ND 05/18/2021 10211.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 05/18/2021 10211.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 05/18/2021 10211.0 0.40 ug/L1
Ethylbenzene ND 05/18/2021 10211.0 0.40 ug/L1
2-Hexanone ND 05/18/2021 1021102.0 ug/L1
Isopropylbenzene ND 05/18/2021 10211.0 0.40 ug/L1
Methyl acetate ND 05/18/2021 10211.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 05/18/2021 10211.0 0.40 ug/L1
4-Methyl-2-pentanone ND 05/18/2021 1021102.0 ug/L1
Methylcyclohexane ND 05/18/2021 10215.0 0.40 ug/L1
Methylene chloride ND 05/18/2021 10211.0 0.40 ug/L1
Styrene ND 05/18/2021 10211.0 0.41 ug/L1
1,1,2,2-Tetrachloroethane ND 05/18/2021 10211.0 0.40 ug/L1
Tetrachloroethene ND 05/18/2021 10211.0 0.40 ug/L1
Toluene ND 05/18/2021 10211.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 05/18/2021 10211.0 0.42 ug/L1
1,2,4-Trichlorobenzene ND 05/18/2021 10211.0 0.40 ug/L1
1,1,1-Trichloroethane ND 05/18/2021 10211.0 0.40 ug/L1
1,1,2-Trichloroethane ND 05/18/2021 10211.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 29 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:WQ92641-001
92641 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 05/18/2021 10211.0 0.40 ug/L1
Trichlorofluoromethane ND 05/18/2021 10211.0 0.40 ug/L1
Vinyl chloride ND 05/18/2021 10211.0 0.40 ug/L1
Xylenes (total)ND 05/18/2021 10211.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 110 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 30 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:WQ92641-002
92641 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 140 05/18/2021 0920N14410060-1401
Benzene 49 05/18/2021 0920985070-1301
Bromodichloromethane 49 05/18/2021 0920995070-1301
Bromoform 46 05/18/2021 0920935070-1301
Bromomethane (Methyl bromide)50 05/18/2021 0920995070-1301
2-Butanone (MEK)120 05/18/2021 092012410070-1301
Carbon disulfide 50 05/18/2021 09201005070-1301
Carbon tetrachloride 48 05/18/2021 0920975070-1301
Chlorobenzene 49 05/18/2021 0920985070-1301
Chloroethane 49 05/18/2021 0920985070-1301
Chloroform 47 05/18/2021 0920935070-1301
Chloromethane (Methyl chloride)53 05/18/2021 09201055060-1401
Cyclohexane 47 05/18/2021 0920945070-1301
1,2-Dibromo-3-chloropropane (DBCP)43 05/18/2021 0920865070-1301
Dibromochloromethane 49 05/18/2021 0920985070-1301
1,2-Dibromoethane (EDB)51 05/18/2021 09201015070-1301
1,2-Dichlorobenzene 50 05/18/2021 0920995070-1301
1,3-Dichlorobenzene 51 05/18/2021 09201015070-1301
1,4-Dichlorobenzene 48 05/18/2021 0920975070-1301
Dichlorodifluoromethane 46 05/18/2021 0920925060-1401
1,1-Dichloroethane 47 05/18/2021 0920945070-1301
1,2-Dichloroethane 43 05/18/2021 0920875070-1301
1,1-Dichloroethene 50 05/18/2021 0920995070-1301
cis-1,2-Dichloroethene 47 05/18/2021 0920945070-1301
trans-1,2-Dichloroethene 51 05/18/2021 09201025070-1301
1,2-Dichloropropane 47 05/18/2021 0920945070-1301
cis-1,3-Dichloropropene 53 05/18/2021 09201055070-1301
trans-1,3-Dichloropropene 46 05/18/2021 0920925070-1301
Ethylbenzene 50 05/18/2021 09201015070-1301
2-Hexanone 100 05/18/2021 092010210070-1301
Isopropylbenzene 52 05/18/2021 09201045070-1301
Methyl acetate 47 05/18/2021 0920945070-1301
Methyl tertiary butyl ether (MTBE)53 05/18/2021 09201065070-1301
4-Methyl-2-pentanone 100 05/18/2021 092010310070-1301
Methylcyclohexane 51 05/18/2021 09201025070-1301
Methylene chloride 46 05/18/2021 0920915070-1301
Styrene 55 05/18/2021 09201095070-1301
1,1,2,2-Tetrachloroethane 52 05/18/2021 09201035070-1301
Tetrachloroethene 50 05/18/2021 09201005070-1301
Toluene 50 05/18/2021 0920995070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 51 05/18/2021 09201025070-1301
1,2,4-Trichlorobenzene 48 05/18/2021 0920965070-1301
1,1,1-Trichloroethane 50 05/18/2021 09201005070-1301
1,1,2-Trichloroethane 51 05/18/2021 09201035070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 31 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:WQ92641-002
92641 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 46 05/18/2021 0920925070-1301
Trichlorofluoromethane 49 05/18/2021 0920985070-1301
Vinyl chloride 53 05/18/2021 09201065070-1301
Xylenes (total)100 05/18/2021 092010310070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 32 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92374-001
92374 3520C
05/14/2021 1705Analytical Method:8270E
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 05/25/2021 10060.16 0.040 ug/L1
Acenaphthylene ND 05/25/2021 10060.16 0.040 ug/L1
Acetophenone ND 05/25/2021 10060.80 0.23 ug/L1
Anthracene ND 05/25/2021 10060.16 0.040 ug/L1
Atrazine ND 05/25/2021 10060.80 0.20 ug/L1
Benzaldehyde ND 05/25/2021 10064.0 0.27 ug/L1
Benzo(a)anthracene ND 05/25/2021 10060.16 0.040 ug/L1
Benzo(a)pyrene ND 05/25/2021 10060.16 0.040 ug/L1
Benzo(b)fluoranthene ND 05/25/2021 10060.16 0.040 ug/L1
Benzo(g,h,i)perylene ND 05/25/2021 10060.16 0.040 ug/L1
Benzo(k)fluoranthene ND 05/25/2021 10060.16 0.040 ug/L1
1,1'-Biphenyl ND 05/25/2021 10060.80 0.21 ug/L1
4-Bromophenyl phenyl ether ND 05/25/2021 10060.80 0.15 ug/L1
Butyl benzyl phthalate ND 05/25/2021 10064.0 0.21 ug/L1
Caprolactam ND 05/25/2021 10064.0 0.71 ug/L1
Carbazole ND 05/25/2021 10060.80 0.040 ug/L1
bis (2-Chloro-1-methylethyl) ether ND 05/25/2021 10060.80 0.17 ug/L1
4-Chloro-3-methyl phenol ND 05/25/2021 10060.80 0.26 ug/L1
4-Chloroaniline ND 05/25/2021 10060.80 0.13 ug/L1
bis(2-Chloroethoxy)methane ND 05/25/2021 10060.80 0.060 ug/L1
bis(2-Chloroethyl)ether ND 05/25/2021 10060.80 0.16 ug/L1
2-Chloronaphthalene ND 05/25/2021 10060.80 0.15 ug/L1
2-Chlorophenol ND 05/25/2021 10060.80 0.15 ug/L1
4-Chlorophenyl phenyl ether ND 05/25/2021 10060.80 0.16 ug/L1
Chrysene ND 05/25/2021 10060.16 0.040 ug/L1
Dibenzo(a,h)anthracene ND 05/25/2021 10060.16 0.040 ug/L1
Dibenzofuran ND 05/25/2021 10060.80 0.16 ug/L1
3,3'-Dichlorobenzidine ND 05/25/2021 10064.0 0.81 ug/L1
2,4-Dichlorophenol ND 05/25/2021 10060.80 0.19 ug/L1
Diethylphthalate ND 05/25/2021 10064.0 0.19 ug/L1
Dimethyl phthalate ND 05/25/2021 10064.0 0.18 ug/L1
2,4-Dimethylphenol ND 05/25/2021 10060.80 0.15 ug/L1
Di-n-butyl phthalate ND 05/25/2021 10064.0 0.42 ug/L1
4,6-Dinitro-2-methylphenol ND 05/25/2021 10064.0 0.89 ug/L1
2,4-Dinitrophenol ND 05/25/2021 10064.0 1.3 ug/L1
2,4-Dinitrotoluene ND 05/25/2021 10061.6 0.36 ug/L1
2,6-Dinitrotoluene ND 05/25/2021 10061.6 0.34 ug/L1
Di-n-octylphthalate ND 05/25/2021 10064.0 0.48 ug/L1
bis(2-Ethylhexyl)phthalate ND 05/25/2021 10064.0 0.38 ug/L1
Fluoranthene ND 05/25/2021 10060.16 0.040 ug/L1
Fluorene ND 05/25/2021 10060.16 0.040 ug/L1
Hexachlorobenzene ND 05/25/2021 10060.80 0.15 ug/L1
Hexachlorobutadiene ND 05/25/2021 10060.80 0.17 ug/L1
Hexachlorocyclopentadiene ND 05/25/2021 10064.0 1.1 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 33 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92374-001
92374 3520C
05/14/2021 1705Analytical Method:8270E
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 05/25/2021 10060.80 0.17 ug/L1
Indeno(1,2,3-c,d)pyrene ND 05/25/2021 10060.16 0.040 ug/L1
Isophorone ND 05/25/2021 10060.80 0.22 ug/L1
2-Methylnaphthalene ND 05/25/2021 10060.16 0.040 ug/L1
2-Methylphenol ND 05/25/2021 10060.80 0.21 ug/L1
3+4-Methylphenol ND 05/25/2021 10061.6 0.46 ug/L1
Naphthalene ND 05/25/2021 10060.16 0.040 ug/L1
2-Nitroaniline ND 05/25/2021 10061.6 0.66 ug/L1
3-Nitroaniline ND 05/25/2021 10061.6 0.15 ug/L1
4-Nitroaniline ND 05/25/2021 10061.6 1.3 ug/L1
Nitrobenzene ND 05/25/2021 10060.80 0.17 ug/L1
2-Nitrophenol ND 05/25/2021 10061.6 0.44 ug/L1
4-Nitrophenol ND 05/25/2021 10064.0 2.1 ug/L1
N-Nitrosodi-n-propylamine ND 05/25/2021 10060.80 0.28 ug/L1
N-Nitrosodiphenylamine (Diphenylamine)ND 05/25/2021 10060.80 0.50 ug/L1
Pentachlorophenol ND 05/25/2021 10064.0 1.3 ug/L1
Phenanthrene ND 05/25/2021 10060.16 0.040 ug/L1
Phenol ND 05/25/2021 10060.80 0.19 ug/L1
Pyrene ND 05/25/2021 10060.16 0.040 ug/L1
2,4,5-Trichlorophenol ND 05/25/2021 10060.80 0.19 ug/L1
2,4,6-Trichlorophenol ND 05/25/2021 10060.80 0.22 ug/L1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 69 37-129
2-Fluorophenol 47 24-127
Nitrobenzene-d5 67 38-127
Phenol-d5 58 28-128
Terphenyl-d14 91 10-148
2,4,6-Tribromophenol 76 35-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 34 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92374-002
92374 3520C
05/14/2021 1705Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acenaphthene 6.1 05/25/2021 1031768.0 30-1221
Acenaphthylene 6.4 05/25/2021 1031798.0 30-1301
Acetophenone 6.5 05/25/2021 1031818.0 52-1251
Anthracene 6.4 05/25/2021 1031808.0 30-1231
Atrazine 6.1 05/25/2021 1031778.0 25-1211
Benzaldehyde 3.8 05/25/2021 1031478.0 20-1151
Benzo(a)anthracene 6.3 05/25/2021 1031798.0 40-1251
Benzo(a)pyrene 7.3 05/25/2021 1031918.0 40-1281
Benzo(b)fluoranthene 7.1 05/25/2021 1031888.0 30-1301
Benzo(g,h,i)perylene 6.5 05/25/2021 1031818.0 30-1301
Benzo(k)fluoranthene 6.6 05/25/2021 1031838.0 30-1301
1,1'-Biphenyl 6.3 05/25/2021 1031788.0 42-1201
4-Bromophenyl phenyl ether 7.0 05/25/2021 1031888.0 30-1241
Butyl benzyl phthalate 7.9 05/25/2021 1031998.0 54-1351
Caprolactam 7.0 05/25/2021 1031878.0 44-1521
Carbazole 6.6 05/25/2021 1031838.0 45-1011
bis (2-Chloro-1-methylethyl) ether 7.3 05/25/2021 1031918.0 42-1241
4-Chloro-3-methyl phenol 6.0 05/25/2021 1031758.0 30-1231
4-Chloroaniline 5.4 05/25/2021 1031678.0 12-1571
bis(2-Chloroethoxy)methane 6.5 05/25/2021 1031818.0 44-1271
bis(2-Chloroethyl)ether 7.1 05/25/2021 1031898.0 46-1201
2-Chloronaphthalene 6.1 05/25/2021 1031778.0 46-1001
2-Chlorophenol 5.5 05/25/2021 1031698.0 50-1171
4-Chlorophenyl phenyl ether 6.5 05/25/2021 1031818.0 30-1211
Chrysene 6.5 05/25/2021 1031818.0 30-1301
Dibenzo(a,h)anthracene 6.5 05/25/2021 1031828.0 30-1301
Dibenzofuran 6.1 05/25/2021 1031768.0 30-1181
3,3'-Dichlorobenzidine 4.0 05/25/2021 1031508.0 10-1261
2,4-Dichlorophenol 5.5 05/25/2021 1031698.0 30-1211
Diethylphthalate 6.6 05/25/2021 1031838.0 40-1251
Dimethyl phthalate 6.7 05/25/2021 1031838.0 40-1271
2,4-Dimethylphenol 5.3 05/25/2021 1031668.0 20-1251
Di-n-butyl phthalate 7.2 05/25/2021 1031908.0 40-1271
4,6-Dinitro-2-methylphenol 4.8 05/25/2021 1031608.0 56-1281
2,4-Dinitrophenol 5.4 05/25/2021 1031331611-1261
2,4-Dinitrotoluene 6.7 05/25/2021 1031848.0 59-1271
2,6-Dinitrotoluene 6.8 05/25/2021 1031858.0 59-1261
Di-n-octylphthalate 6.3 05/25/2021 1031798.0 50-1361
bis(2-Ethylhexyl)phthalate 6.7 05/25/2021 1031848.0 56-1281
Fluoranthene 6.5 05/25/2021 1031818.0 40-1281
Fluorene 5.8 05/25/2021 1031738.0 30-1241
Hexachlorobenzene 6.8 05/25/2021 1031858.0 30-1251
Hexachlorobutadiene 5.9 05/25/2021 1031748.0 24-1101
Hexachlorocyclopentadiene 23 05/25/2021 1031584016-961
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 35 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92374-002
92374 3520C
05/14/2021 1705Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Hexachloroethane 5.3 05/25/2021 1031668.0 31-1101
Indeno(1,2,3-c,d)pyrene 5.9 05/25/2021 1031738.0 30-1301
Isophorone 7.6 05/25/2021 1031958.0 57-1231
2-Methylnaphthalene 6.4 05/25/2021 1031808.0 40-1321
2-Methylphenol 5.2 05/25/2021 1031668.0 56-1191
3+4-Methylphenol 5.0 05/25/2021 1031628.0 53-1191
Naphthalene 6.4 05/25/2021 1031808.0 30-1301
2-Nitroaniline 5.8 05/25/2021 1031728.0 60-1241
3-Nitroaniline 4.5 05/25/2021 1031568.0 43-1231
4-Nitroaniline 5.4 05/25/2021 1031678.0 30-1351
Nitrobenzene 5.8 05/25/2021 1031738.0 51-1221
2-Nitrophenol 5.9 05/25/2021 1031738.0 51-1181
4-Nitrophenol 10 05/25/2021 1031621653-1301
N-Nitrosodi-n-propylamine 6.9 05/25/2021 1031868.0 54-1271
N-Nitrosodiphenylamine (Diphenylamine)6.1 05/25/2021 1031768.0 30-1231
Pentachlorophenol 8.6 05/25/2021 1031541642-1311
Phenanthrene 6.1 05/25/2021 1031778.0 40-1231
Phenol 5.8 05/25/2021 1031728.0 49-1171
Pyrene 6.8 05/25/2021 1031858.0 40-1261
2,4,5-Trichlorophenol 5.3 05/25/2021 1031668.0 30-1231
2,4,6-Trichlorophenol 5.2 05/25/2021 1031658.0 30-1251
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 73 37-129
2-Fluorophenol 64 24-127
Nitrobenzene-d5 81 38-127
Phenol-d5 74 28-128
Terphenyl-d14 83 10-148
2,4,6-Tribromophenol 79 35-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 36 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92387-001
92387 3546
05/14/2021 2010Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 05/20/2021 12332.7 0.83 ug/kg1
Acenaphthylene ND 05/20/2021 12332.7 0.95 ug/kg1
Acetophenone ND 05/20/2021 1233135.0 ug/kg1
Anthracene ND 05/20/2021 12332.7 0.51 ug/kg1
Atrazine ND 05/20/2021 1233135.0 ug/kg1
Benzaldehyde ND 05/20/2021 1233135.0 ug/kg1
Benzo(a)anthracene ND 05/20/2021 12332.7 0.59 ug/kg1
Benzo(a)pyrene ND 05/20/2021 12332.7 0.66 ug/kg1
Benzo(b)fluoranthene ND 05/20/2021 12332.7 0.50 ug/kg1
Benzo(g,h,i)perylene ND 05/20/2021 12332.7 0.65 ug/kg1
Benzo(k)fluoranthene ND 05/20/2021 12332.7 0.48 ug/kg1
1,1'-Biphenyl ND 05/20/2021 1233135.0 ug/kg1
4-Bromophenyl phenyl ether ND 05/20/2021 1233135.0 ug/kg1
Butyl benzyl phthalate ND 05/20/2021 1233135.0 ug/kg1
Caprolactam ND 05/20/2021 1233135.0 ug/kg1
Carbazole ND 05/20/2021 1233135.0 ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 05/20/2021 1233135.0 ug/kg1
4-Chloro-3-methyl phenol ND 05/20/2021 1233135.0 ug/kg1
4-Chloroaniline ND 05/20/2021 1233135.0 ug/kg1
bis(2-Chloroethoxy)methane ND 05/20/2021 1233135.0 ug/kg1
bis(2-Chloroethyl)ether ND 05/20/2021 1233135.0 ug/kg1
2-Chloronaphthalene ND 05/20/2021 1233135.0 ug/kg1
2-Chlorophenol ND 05/20/2021 1233135.0 ug/kg1
4-Chlorophenyl phenyl ether ND 05/20/2021 1233135.0 ug/kg1
Chrysene ND 05/20/2021 12332.7 0.45 ug/kg1
Dibenzo(a,h)anthracene ND 05/20/2021 12332.7 0.51 ug/kg1
Dibenzofuran ND 05/20/2021 1233135.0 ug/kg1
3,3'-Dichlorobenzidine ND 05/20/2021 1233135.0 ug/kg1
2,4-Dichlorophenol ND 05/20/2021 1233135.0 ug/kg1
Diethylphthalate ND 05/20/2021 1233135.0 ug/kg1
Dimethyl phthalate ND 05/20/2021 1233137.4 ug/kg1
2,4-Dimethylphenol ND 05/20/2021 1233135.0 ug/kg1
Di-n-butyl phthalate 12 05/20/2021 1233J135.0 ug/kg1
4,6-Dinitro-2-methylphenol ND 05/20/2021 12336725ug/kg1
2,4-Dinitrophenol ND 05/20/2021 12336725ug/kg1
2,4-Dinitrotoluene ND 05/20/2021 12332710ug/kg1
2,6-Dinitrotoluene ND 05/20/2021 12332710ug/kg1
Di-n-octylphthalate ND 05/20/2021 1233135.0 ug/kg1
bis(2-Ethylhexyl)phthalate ND 05/20/2021 12336725ug/kg1
Fluoranthene ND 05/20/2021 12332.7 0.42 ug/kg1
Fluorene ND 05/20/2021 12332.7 0.57 ug/kg1
Hexachlorobenzene ND 05/20/2021 1233135.0 ug/kg1
Hexachlorobutadiene ND 05/20/2021 1233135.0 ug/kg1
Hexachlorocyclopentadiene ND 05/20/2021 12336725ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 37 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92387-001
92387 3546
05/14/2021 2010Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 05/20/2021 1233135.0 ug/kg1
Indeno(1,2,3-c,d)pyrene ND 05/20/2021 12332.7 1.0 ug/kg1
Isophorone ND 05/20/2021 1233135.0 ug/kg1
2-Methylnaphthalene ND 05/20/2021 12332.7 0.99 ug/kg1
2-Methylphenol ND 05/20/2021 1233135.0 ug/kg1
3+4-Methylphenol ND 05/20/2021 12332710ug/kg1
Naphthalene ND 05/20/2021 12332.7 0.97 ug/kg1
2-Nitroaniline ND 05/20/2021 12332710ug/kg1
3-Nitroaniline ND 05/20/2021 12332710ug/kg1
4-Nitroaniline ND 05/20/2021 12332710ug/kg1
Nitrobenzene ND 05/20/2021 1233135.0 ug/kg1
2-Nitrophenol ND 05/20/2021 12332710ug/kg1
4-Nitrophenol ND 05/20/2021 12336725ug/kg1
N-Nitrosodi-n-propylamine ND 05/20/2021 1233135.0 ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 05/20/2021 1233135.0 ug/kg1
Pentachlorophenol ND 05/20/2021 12336725ug/kg1
Phenanthrene ND 05/20/2021 12332.7 0.72 ug/kg1
Phenol ND 05/20/2021 1233135.0 ug/kg1
Pyrene ND 05/20/2021 12332.7 0.50 ug/kg1
Pyridine ND 05/20/2021 1233135.0 ug/kg1
2,4,5-Trichlorophenol ND 05/20/2021 1233135.0 ug/kg1
2,4,6-Trichlorophenol ND 05/20/2021 1233135.0 ug/kg1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 45 35-115
Nitrobenzene-d5 45 22-109
Phenol-d5 48 33-122
Terphenyl-d14 65 41-120
2,4,6-Tribromophenol 64 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 38 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92387-002
92387 3546
05/14/2021 2010Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/kg)(ug/kg)
Acenaphthene 82 05/20/2021 12586213012-1111
Acenaphthylene 84 05/20/2021 12586313044-1221
Acetophenone 77 05/20/2021 12585813048-1111
Anthracene 90 05/20/2021 12586813016-1221
Atrazine 87 05/20/2021 12586613048-1161
Benzaldehyde 63 05/20/2021 12584713010-1101
Benzo(a)anthracene 99 05/20/2021 12587513040-1211
Benzo(a)pyrene 110 05/20/2021 12588313036-1141
Benzo(b)fluoranthene 100 05/20/2021 12587913038-1231
Benzo(g,h,i)perylene 100 05/20/2021 12587613043-1201
Benzo(k)fluoranthene 93 05/20/2021 12587013040-1261
1,1'-Biphenyl 83 05/20/2021 12586213049-1101
4-Bromophenyl phenyl ether 98 05/20/2021 12587413046-1181
Butyl benzyl phthalate 120 05/20/2021 12589213046-1281
Caprolactam 81 05/20/2021 12586113043-1211
Carbazole 95 05/20/2021 12587213047-1281
bis (2-Chloro-1-methylethyl) ether 38 05/20/2021 1258N2913031-1021
4-Chloro-3-methyl phenol 89 05/20/2021 12586713049-1181
4-Chloroaniline 41 05/20/2021 12583113017-1061
bis(2-Chloroethoxy)methane 71 05/20/2021 12585413039-1081
bis(2-Chloroethyl)ether 57 05/20/2021 12584313032-1051
2-Chloronaphthalene 83 05/20/2021 12586313031-1271
2-Chlorophenol 74 05/20/2021 12585613037-1061
4-Chlorophenyl phenyl ether 96 05/20/2021 12587213047-1161
Chrysene 95 05/20/2021 12587113041-1241
Dibenzo(a,h)anthracene 100 05/20/2021 12587613038-1251
Dibenzofuran 90 05/20/2021 12586813045-1121
3,3'-Dichlorobenzidine 64 05/20/2021 12584813010-1191
2,4-Dichlorophenol 95 05/20/2021 12587113041-1131
Diethylphthalate 90 05/20/2021 12586713049-1231
Dimethyl phthalate 92 05/20/2021 12586913048-1201
2,4-Dimethylphenol 84 05/20/2021 12586313033-1231
Di-n-butyl phthalate 110 05/20/2021 12588013051-1291
4,6-Dinitro-2-methylphenol 65 05/20/2021 12584913040-1301
2,4-Dinitrophenol 100 05/20/2021 12583927032-1151
2,4-Dinitrotoluene 96 05/20/2021 12587213048-1241
2,6-Dinitrotoluene 98 05/20/2021 12587413047-1251
Di-n-octylphthalate 96 05/20/2021 12587213049-1421
bis(2-Ethylhexyl)phthalate 95 05/20/2021 12587113045-1281
Fluoranthene 92 05/20/2021 12586913026-1331
Fluorene 89 05/20/2021 12586713019-1081
Hexachlorobenzene 100 05/20/2021 12587513044-1221
Hexachlorobutadiene 100 05/20/2021 12587613033-1031
Hexachlorocyclopentadiene 610 05/20/2021 12589167018-1211
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 39 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92387-002
92387 3546
05/14/2021 2010Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/kg)(ug/kg)
Hexachloroethane 80 05/20/2021 12586013030-961
Indeno(1,2,3-c,d)pyrene 97 05/20/2021 12587313042-1231
Isophorone 95 05/20/2021 12587113041-1131
2-Methylnaphthalene 83 05/20/2021 12586313010-1071
2-Methylphenol 80 05/20/2021 12586013032-1071
3+4-Methylphenol 78 05/20/2021 12585813039-1081
Naphthalene 83 05/20/2021 12586213010-1121
2-Nitroaniline 77 05/20/2021 12585813045-1231
3-Nitroaniline 66 05/20/2021 12584913024-1271
4-Nitroaniline 90 05/20/2021 12586813048-1271
Nitrobenzene 68 05/20/2021 12585113033-1141
2-Nitrophenol 79 05/20/2021 12585913035-1081
4-Nitrophenol 180 05/20/2021 12586827018-1541
N-Nitrosodi-n-propylamine 79 05/20/2021 12585913032-1151
N-Nitrosodiphenylamine (Diphenylamine)94 05/20/2021 12587113053-1501
Pentachlorophenol 180 05/20/2021 12586927027-1381
Phenanthrene 90 05/20/2021 12586813016-1231
Phenol 79 05/20/2021 12585913036-1081
Pyrene 89 05/20/2021 12586713034-1211
Pyridine 71 05/20/2021 12585313030-1301
2,4,5-Trichlorophenol 94 05/20/2021 12587113046-1221
2,4,6-Trichlorophenol 92 05/20/2021 12587013038-1151
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 62 33-102
2-Fluorophenol 54 35-115
Nitrobenzene-d5 55 22-109
Phenol-d5 59 33-122
Terphenyl-d14 71 41-120
2,4,6-Tribromophenol 73 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 40 of 73
MA EPH (aliphatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92472-001
92472 MADEP-EPH-04
05/17/2021 1107Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
C9 - C18 Aliphatics ND 05/20/2021 06101010mg/kg1
C19 - C36 Aliphatics ND 05/20/2021 06101010mg/kg1
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)90 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 41 of 73
MA EPH (aliphatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92472-002
92472 MADEP-EPH-04
05/17/2021 1107Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg)(mg/kg)
C9 - C18 Aliphatics 18 05/20/2021 0640593040-1401
C19 - C36 Aliphatics 39 05/20/2021 0640984040-1401
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)97 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 42 of 73
MA EPH (aliphatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:WQ92472-003
92472 MADEP-EPH-04
05/17/2021 1107Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C9 - C18 Aliphatics 17 05/20/2021 0710563040-1404.5 251
C19 - C36 Aliphatics 38 05/20/2021 0710954040-1403.1 251
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)92 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 43 of 73
MA EPH (aromatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92473-001
92473 MADEP-EPH-04
05/17/2021 1107Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
C11 - C22 Aromatics ND 05/20/2021 01071010mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)84 40-140
2-Fluorobiphenyl (fractionation 1)94 40-140
o - Terphenyl (aromatic)71 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 44 of 73
MA EPH (aromatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92473-002
92473 MADEP-EPH-04
05/17/2021 1107Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg)(mg/kg)
C11 - C22 Aromatics 69 05/20/2021 0137818540-1401
Surrogate Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)84 40-140
2-Fluorobiphenyl (fractionation 1)98 40-140
o - Terphenyl (aromatic)77 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 45 of 73
MA EPH (aromatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:WQ92473-003
92473 MADEP-EPH-04
05/17/2021 1107Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C11 - C22 Aromatics 67 05/20/2021 0207798540-1403.0 251
Surrogate Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)84 40-140
2-Fluorobiphenyl (fractionation 1)98 40-140
o - Terphenyl (aromatic)75 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 46 of 73
MADEP EPH (aliphatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ93400-001
93400 MADEP-EPH-04
05/26/2021 0850Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C9 - C18 Aliphatics ND 05/26/2021 1551100100ug/L1
C19 - C36 Aliphatics ND 05/26/2021 1551100100ug/L1
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)90 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 47 of 73
MADEP EPH (aliphatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ93400-002
93400 MADEP-EPH-04
05/26/2021 0850Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
C9 - C18 Aliphatics 130 05/26/2021 16254330040-1401
C19 - C36 Aliphatics 380 05/26/2021 16259540040-1401
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)87 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 48 of 73
MADEP EPH (aliphatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:WQ93400-003
93400 MADEP-EPH-04
05/26/2021 0850Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C9 - C18 Aliphatics 120 05/26/2021 16594130040-1404.8 251
C19 - C36 Aliphatics 380 05/26/2021 16599640040-1401.3 251
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)86 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 49 of 73
MADEP EPH (aromatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ93401-001
93401 MADEP-EPH-04
05/26/2021 0850Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C11 - C22 Aromatics ND 05/26/2021 1917100100ug/L1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic)70 40-140
2-Fluorobiphenyl (fractionation 1)81 40-140
2-Bromonaphthalene (fractionation 2)81 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 50 of 73
MADEP EPH (aromatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ93401-002
93401 MADEP-EPH-04
05/26/2021 0850Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
C11 - C22 Aromatics 680 05/26/2021 19528085040-1401
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic)75 40-140
2-Fluorobiphenyl (fractionation 1)85 40-140
2-Bromonaphthalene (fractionation 2)86 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 51 of 73
MADEP EPH (aromatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:WQ93401-003
93401 MADEP-EPH-04
05/26/2021 0850Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C11 - C22 Aromatics 690 05/26/2021 20268185040-1401.9 251
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic)73 40-140
2-Fluorobiphenyl (fractionation 1)88 40-140
2-Bromonaphthalene (fractionation 2)88 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 52 of 73
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:WQ92778-001
92778 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
C5 - C8 Aliphatics ND 05/19/2021 14473.8 0.75 mg/kg1
C9 - C12 Aliphatics ND 05/19/2021 14473.8 0.75 mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)93 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 53 of 73
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:WQ92778-002
92778 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg)(mg/kg)
C5 - C8 Aliphatics 7.9 05/19/2021 13501067.5 70-1301
C9 - C12 Aliphatics 9.8 05/19/2021 13501128.8 70-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 54 of 73
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:WQ92778-003
92778 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C5 - C8 Aliphatics 8.0 05/19/2021 14191067.5 70-1300.48 251
C9 - C12 Aliphatics 9.4 05/19/2021 14191078.8 70-1304.2 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)107 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 55 of 73
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:WQ92779-001
92779 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
C9 - C10 Aromatics ND 05/19/2021 14471.3 0.50 mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)74 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 56 of 73
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:WQ92779-002
92779 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg)(mg/kg)
C9 - C10 Aromatics 1.1 05/19/2021 1350881.3 70-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)88 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 57 of 73
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:WQ92779-003
92779 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C9 - C10 Aromatics 1.1 05/19/2021 1419881.3 70-1300.00 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)88 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 58 of 73
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:WQ92780-001
92780 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C5 - C8 Aliphatics ND 05/19/2021 12547515ug/L1
C9 - C12 Aliphatics ND 05/19/2021 12547515ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)107 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 59 of 73
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:WQ92780-002
92780 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 170 05/19/2021 115711515070-1301
C9 - C12 Aliphatics 180 05/19/2021 115710518070-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 60 of 73
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:WQ92780-003
92780 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 170 05/19/2021 122511115070-1303.5 251
C9 - C12 Aliphatics 180 05/19/2021 122510318070-1301.9 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)106 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 61 of 73
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:WQ92782-001
92782 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C9 - C10 Aromatics ND 05/19/2021 1254255.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)90 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 62 of 73
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:WQ92782-002
92782 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 22 05/19/2021 1157862570-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)84 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 63 of 73
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:WQ92782-003
92782 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 21 05/19/2021 1225842570-1302.3 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)85 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 64 of 73
ICP-AES - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92327-001
92327 3050B
05/16/2021 0521Analytical Method:6010D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Lead ND 05/17/2021 06320.50 0.23 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 65 of 73
ICP-AES - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92327-002
92327 3050B
05/16/2021 0521Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg)(mg/kg)
Lead 260 05/17/2021 063510525080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 66 of 73
ICP-AES - MS
Batch:Prep Method:
Prep Date:
Sample ID:WE14021-001MS
92327 3050B
05/16/2021 0521Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Lead 240 05/17/2021 08398228075-1252.8 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 67 of 73
ICP-AES - MSD
Batch:Prep Method:
Prep Date:
Sample ID:WE14021-001MD
92327 3050B
05/16/2021 0521Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Lead 260 05/17/2021 08438530075-1259.2 202.8 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 68 of 73
ICP-AES Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ92433-001
92433 3005A
05/16/2021 0645Analytical Method:6010D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Lead ND 05/17/2021 08310.010 0.0047 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 69 of 73
ICP-AES Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ92433-002
92433 3005A
05/16/2021 0645Analytical Method:6010D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/L)(mg/L)
Lead 0.41 05/17/2021 07531030.40 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 70 of 73
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 71 of 73
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 72 of 73
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 73 of 73