25027_Pharr Yarns Lowell Phase II ESA__2021322

Phase II ESA
Former Pharr Yarn Mills

700 West 1st Street
Lowell, North Carolina

H&H Job No. HNY-001
February 18, 2021
Revised March 22, 2021

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Phase II ESA Former Pharr Yarn Mills
700 West 1st Street Lowell, North Carolina H&H Job No. HNY-001
Table of Contents
1.0 Introduction .............................................................................................................................1
2.0 Phase II ESA Sampling Activities .........................................................................................4
2.1 Utility Locating/Geophysical Survey ....................................................................................4
2.2 Soil Sampling Methodology ..................................................................................................4
2.3 Groundwater Sampling Methodology ...................................................................................6
2.4 Asbestos Sampling Activities ................................................................................................7
3.0 Assessment Results..................................................................................................................8
3.1 Soil Analytical Results ..........................................................................................................8
3.2 Groundwater Analytical Results ............................................................................................9
3.3 Asbestos Sampling Results ..................................................................................................10
4.0 Summary, Conclusions, and Recommendations ................................................................11

List of Tables
Table 1 Summary of Temporary Monitoring Well Construction and Water Level Data
Table 2 Summary of Soil Analytical Results
Table 3 Summary of Groundwater Analytical Results
List of Figures

Figure 1 Site Location Map
Figure 2 Site and Sample Location Map
List of Appendices

Appendix A Soil Boring Logs
Appendix B Low Flow Groundwater Sampling Logs
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Appendix C Laboratory Analytical Reports
Appendix D DEQ Risk Calculator Input/Output Forms
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Phase II ESA Former Pharr Yarn Mills
700 West 1st Street Lowell, North Carolina H&H Job No. HNY-001
1.0 Introduction

In accordance with our authorized scope of work, Hart & Hickman, PC (H&H) has performed a
Phase II Environmental Site Assessment (ESA) of the former Pharr Yarn Mills property located at
700 West 1st Street in Lowell, Gaston County, North Carolina (Site or subject Site). A Site
location map is provided as Figure 1.

The Site is comprised of approximately 13.83 acres of primarily vacant land (Parcel Identification
Number 127730). A Duke Energy overhead electrical right-of-way crosses the western and
northern portions of the Site. Birch Street crosses the eastern portion of the Site, and West 1st
Street bisects the northern and southern portions of the subject Site. A brick garage is located in
the southeastern corner of the Site.

H&H recently conducted Phase I ESA activities at the Site and identified the following Recognized
Environmental Conditions (RECs):

• The Site was occupied by two cotton milling and yarn spinning mills from the early 1900s
until approximately 2001/2002. The mill buildings were razed in 2004/2005. According
to the Site contacts, representatives of Pharr Yarns, mill operations consisted of carding,
spinning, and winding of cotton yarns. The mill is listed as a former generator of ignitable
hazardous waste in the Resources Conservation and Recovery Act (RCRA) database.
Textile spinning mills commonly used chlorinated solvents and petroleum products as part
of the milling equipment maintenance. As indicated in a United Spinners Corporation
memorandum dated October 31, 1986, 29 drums of unspecified chemicals/oil and 30 empty
drums were observed adjacent to the eastern mill building during a compliance review.
Details regarding the types of chemicals used during milling operations, chemical storage,
waste disposal practices, and early industrial process water disposal are unknown. Areas
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of potential environmental concern identified on Sanborn Fire Insurance Maps include a
machine shop, a coal trestle and nearby chimney (presumably used to burn coal), and an
electrical substation. H&H identified the potential for impact from nearly a century of on-
Site milling operations (multiple decades of which were prior to the implementation of
hazardous waste regulations and other applicable environmental protection regulations) as
an REC.

• Representatives of Pharr Yarns reported that two 1,000-gallon fuel oil underground storage
tanks (USTs) and two 5,000-gallon fuel oil USTs were removed near the former mill
buildings. A survey also depicts a UST (presumably fuel oil) adjacent to a former office
building in the eastern portion of the Site. The environmental database report indicates
that five fuel oil USTs were installed at the Site between 1964 and 1991 and removed in
2004. According to Site contacts, soil samples were collected for laboratory analysis
during UST closure activities, but the Site contacts were unable to provide
documentation/closure reports associated with removal of the USTs. Based on the
extended period of UST operation and the lack of reports documenting UST closure
activities, the potential for impact to the subject Site from the former fuel oil UST systems
was identified as an REC.

• During the Site reconnaissance, H&H observed a vent pipe associated with a UST located
adjacent to the garage structure located in the southeastern corner of the subject Site.
Additional information pertaining to the UST, including its size, contents, and date of
installation, is unknown. H&H identified the potential for a release from the UST as an
REC.

H&H also identified the following potential environmental concern which, based upon our
evaluation, was not identified as a REC:

• During Site reconnaissance, two open trash bags of cementitious building materials that
are considered suspect asbestos-containing materials (ACMs) were observed in the
northeastern portion of the Site. The asbestos content of building materials cannot be
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confirmed without laboratory testing. The suspect ACMs appear to have been broken into
pieces prior to placing them in plastic bags. However, the materials did not appear
obviously degraded. Based on the relatively small quantity of material observed, the lack
of data to confirm the presence of asbestos, and the lack of obvious evidence of degraded
materials on the ground surface, H&H did not identify the suspect ACM debris as an REC.

On January 11 and 12, 2021, H&H performed soil and groundwater sampling activities at the Site
to evaluate potential environmental impacts from the RECs noted above. In addition, samples of
the suspect asbestos-containing debris were collected for laboratory analysis. The methods and
results of the assessment activities are detailed in the following sections.

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2.0 Phase II ESA Sampling Activities

2.1 Utility Locating/Geophysical Survey
Prior to conducting the assessment activities, H&H contacted North Carolina 811, the public utility
locator, to mark subsurface utilities on the Site. H&H also contracted with Probe Utility Locating
(PUL), a private utility locator, to screen proposed sample locations for subgrade utilities and to
confirm public utility locator markings using electromagnetic and ground-penetrating radar (GPR)
methods. Soil boring locations were hand cleared using a decontaminated stainless-steel hand auger
to approximately 5 ft below ground surface (bgs) prior to use of mechanical drilling equipment to
further screen the boring locations for the presence of subsurface utilities.

In addition to screening for subsurface utilities, PUL utilized GPR to survey areas of
current/former USTs at the Site. The results of the GPR survey indicated the presence of one UST
in the vicinity of the former office building in the eastern portion of the Site. Evidence of former
USTs was observed during the GPR survey of UST basins located north of Mill Building No. 1,
north of Mill Building No. 2, and adjacent to the vent pipe in the southern portion of the Site near
Phillips Street. Current and former UST basins are depicted on Figure 2.

2.2 Soil Sampling Methodology
H&H contracted Innovative Environmental Technologies (IET), a North Carolina-licensed drilling
contractor, to advance 13 soil borings (SB-1 through SB-13) using a track-mounted direct push
technology (DPT) drill rig and a hand auger. Soil boring locations are described below and are
depicted on Figure 2.

• Two soil borings (SB-1 and SB-2) were advanced adjacent to two former fuel oil USTs
located north of Mill Building No. 2.
• One soil boring (SB-3) was advanced within the former electrical substation in the central
portion of the Site.
• One soil boring (SB-4) was advanced adjacent to a former coal trestle in the northeastern
portion of the Site.
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• Two soil borings (SB-5 and SB-6) were advanced within a former machine shop in the
northwestern portion of Mill Building No. 1.
• Two soil borings (SB-7 and SB-8) were advanced adjacent to two former fuel oil USTs
located north of Mill Building No. 1.
• Two soil borings (SB-9 and SB-10) were advanced adjacent to an existing fuel oil UST
near a former office building in the eastern portion of the Site.
• Two soil borings (SB-11 and SB-12) were advanced adjacent to a former UST in the
southern portion of the Site.
• One soil boring (SB-13/TMW-6) was advanced within a former carpentry shop in the
southern portion of the Site.

Continuous soil samples were collected from each boring, logged for lithological description, and
field screened for the presence of staining, odors, and volatile organic vapors using a calibrated
photoionization detector (PID). Based on field screening results, one soil sample was collected
from each boring for laboratory analysis from the estimated depth below the current/former USTs
or to evaluate a shallow release in non-UST areas. In addition, a deeper (11-13 ft) soil sample was
collected from boring SB-4 based on apparent elevated PID readings observed during field
screening. Soil boring logs including PID screening results are included in Appendix A.

Soil samples were placed directly into laboratory-supplied glassware, labeled, and placed on ice
in a laboratory-supplied cooler. The cooler was delivered under standard chain of custody
protocols to Waypoint Analytical in Charlotte, North Carolina. Soil sample analyses are
summarized as follows:

• Samples SB-1, SB-2, SB-7, SB-8, SB-9, SB-10, SB-11, and SB-12 were analyzed for
diesel-range total petroleum hydrocarbons (TPH-DRO) and gasoline-range TPH (TPH-
GRO) by EPA Method 8015C.
• Sample SB-3 was analyzed for polychlorinated biphenyls (PCBs) by EPA Method 8082A.
• Sample SB-4 (1-3 ft) was analyzed for polynuclear aromatic hydrocarbons (PAHs) by EPA
Method 8270E, and sample SB-4 (11-13 ft) was analyzed for volatile organic compounds
(VOCs) by EPA Method 8260D.
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• Samples SB-5, SB-6, and SB-13 were analyzed for VOCs by EPA Method 8260D and
PAHs by EPA Method 8270E.

Upon completion of soil sampling, the soil borings were properly abandoned with hydrated
bentonite, and the surfaces were restored to approximately match pre-drilling conditions. Because
H&H did not identify evidence of significant soil impacts (i.e., free product) during field activities,
soil cuttings were thin-spread on-Site.

2.3 Groundwater Sampling Methodology

To evaluate groundwater conditions, six of the soil borings (SB-1, SB-4, SB-8, SB-10, SB-12, and
SB-13) were converted to temporary monitoring wells for collection of groundwater samples as
described below. Temporary monitoring well locations are depicted on Figure 2 and are described
below.

• Temporary monitoring well TMW-1 was installed adjacent to two former fuel oil USTs
located north of Mill Building No. 2.
• Temporary monitoring well TMW-2 was installed adjacent to a former coal trestle and
downgradient of the former machine shop in the northeastern portion of the Site.
• Temporary monitoring well TMW-3 was installed adjacent to two former fuel oil USTs
located north of Mill Building No. 1.
• Temporary monitoring well TMW-4 was installed adjacent to an existing fuel oil UST near a
former office building in the southeastern portion of the Site.
• Temporary monitoring well TMW-5 was installed adjacent to a former UST in the southern
portion of the Site.
• Temporary monitoring well TMW-6 was installed within a former carpentry shop in the
southern portion of the Site.

The temporary monitoring wells were advanced beyond the water table to depths of approximately
25 to 30 ft bgs using DPT methods. The temporary monitoring wells were constructed of 1-inch
diameter PVC with 10 to 15 ft of well screen set to bracket the water table. Filter sand was placed in
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the well annulus from the base of the borehole to approximately 2 ft above the well screen. At least
2 ft of hydrated bentonite was placed above the sand pack of each well. Temporary monitoring well
construction details are provided in Table 1.

Prior to purging and sampling, H&H measured the depth to water in the temporary wells using an
electronic water level indicator. Groundwater was measured at depths ranging from approximately
17.19 ft bgs in TMW-1 to 27.80 ft bgs in TMW-3 (see Table 1). Based on topography, groundwater
at the Site is expected to flow primarily to the north in the northern portion of the Site and to the south
in the southern portion of the Site.

Following installation, H&H developed the temporary monitoring wells by removing at least three
well volumes using a peristaltic pump. Once three well volumes had been removed and the
development water was visibly clear of suspended sediment, the temporary wells were purged using
a peristaltic pump and low flow techniques until field parameters of temperature, pH, specific
conductivity, and oxidation reduction potential (ORP) stabilized. Groundwater sampling field forms
completed by H&H sampling personnel are provided in Appendix B.

The groundwater samples were placed in dedicated laboratory-supplied sample containers and then
delivered to Waypoint Analytical, a North Carolina-certified laboratory, under standard chain of
custody protocols. Groundwater samples were analyzed for VOCs by EPA Method 8260D and PAHs
by EPA Method 8270E.

2.4 Asbestos Sampling Activities
During field activities, Mr. Sean Horgan of H&H collected four samples of suspect asbestos-
containing cementitious building materials and an unidentified black building material that were
observed in the eastern portion of the Site. Mr. Horgan is an Asbestos Hazards Emergency Response
Act (AHERA)-trained asbestos inspector. The suspect shingle material was placed in dedicated
sample containers and shipped to a National Voluntary Laboratory Accreditation Program (NVLAP)
certified laboratory for analysis of asbestos by Polarized Light Microscopy (PLM) by EPA Method
600/R-93/116.
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3.0 Assessment Results

3.1 Soil Analytical Results
A tabular summary of soil analytical results is presented in Table 2. The laboratory analytical report
and chain of custody record are provided in Appendix C. The VOC, PAH, and PCB analytical
results were compared to the North Carolina Department of Environmental Quality (DEQ)
protection of groundwater, residential, and industrial/commercial Preliminary Soil Remediation
Goals (PSRGs) dated July 2020. TPH-DRO and TPH-GRO data were compared to the DEQ UST
Section Action Levels.

Soil analytical data indicate the presence of TPH-DRO in samples SB-1 (10-12 ft) and SB-10
(10-12 ft) at concentrations of 4.4 mg/kg and 3.9 mg/kg, respectively. These concentrations are
below the Action Level of 100 mg/kg. No TPH-GRO was detected in soil samples collected
adjacent to current/former USTs at concentrations above the laboratory method detection limits
(MDLs).

The VOC tetrachloroethene (PCE) was detected in samples SB-4 (11-13 ft) and SB-5 (3-5 ft) at
concentrations of 0.0085 mg/kg and 0.018 mg/kg, respectively. These detections exceed the
protection of groundwater PSRG of 0.0063 mg/kg but are below the respective residential and
industrial/commercial PSRGs of 17 mg/kg and 82 mg/kg. Sample SB-4 (11-13 ft) was collected
adjacent to the former coal trestle/machine shop, and sample SB-5 (3-5 ft) was collected within
the former machine shop. Acetone was detected in sample SB-13 (1-3 ft) and PCE was detected
in sample SB-6 (3-5 ft) at concentrations below the protection of groundwater, residential, and
industrial/commercial PSRGs. Acetone is a common laboratory contaminant; therefore, the
detection is not likely representative of Site soil conditions.

Multiple PAHs were detected in samples SB-5 (3-5 ft) and SB-13 (1-3 ft), which were collected
within the former machine shop and the former carpentry shop, respectively. The detected
benzo(a)anthracene concentration of 0.67 mg/kg in sample SB-5 (3-5 ft) exceeds the protection of
groundwater PSRG of 0.35 mg/kg. The detected benzo(a)pyrene concentrations of 0.68 mg/kg
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(sample SB-5) and 0.25 mg/kg (sample SB-13) exceed the protection of groundwater PSRG of
0.12 mg/kg and the residential PSRG of 0.11 mg/kg.

No PCBs were detected above the MDLs in sample SB-3 (1-3 ft).

3.2 Groundwater Analytical Results
A tabular summary of groundwater analytical results is presented in Table 3. Groundwater data were
compared to the North Carolina 2L Groundwater Standards (2L Standards) dated April 2013.
Groundwater data were also compared to the DEQ Division of Waste Management (DWM) Vapor
Intrusion Groundwater Screening Levels (GWSLs) dated July 2020 as a preliminary evaluation of
vapor intrusion into future Site buildings. The laboratory analytical report and chain of custody record
are provided in Appendix C.

Laboratory analytical data indicate that several VOCs were detected in groundwater samples collected
at the Site. PCE (2,100 µg/L) and trichloroethene (TCE; 7.9 µg/L) were detected in temporary well
sample TMW-2 at concentrations above the 2L Standards of 0.7 µg/L and 3.0 µg/L, respectively. The
detected PCE and TCE concentrations also exceed the respective non-residential GWSLs of 48 µg/L
and 4.4 µg/L. Sample TMW-2 was collected downgradient of the former machine shop. PCE was
also detected in samples TMW-3 (6.6 µg/L), TMW-4 (5.6 µg/L), and TMW-6 (0.7 µg/L) at
concentrations greater than or equal to the 2L Standard of 0.7 µg/L. Additional petroleum-related
VOCs were detected in sample TMW-1, and 1,2-dichlorobenzene was detected in sample TMW-3.
However, the detected concentrations are below the 2L Standards and the GWSLs.

Results of PAH analysis indicate the presence of naphthalene in sample TMW-1 at a concentration
of 1.6 µg/L, which is below the 2L Standard of 6.0 µg/L. No PAHs were detected in samples
TMW-2 through TMW-6 at concentrations above the MDLs.

Risk Calculations
DEQ GWSLs are conservative and based upon a lifetime incremental cancer risk (LICR) for
potential carcinogenic risks of 1 x 10-6 and a non-carcinogenic hazard index (HI) of 0.2 for
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potential non-carcinogenic risks. The DEQ acceptable LICR is typically 1 x 10-4 or less, and the
acceptable cumulative risk level for non-carcinogenic risks is an HI equal to or less than 1.0. To
further evaluate vapor intrusion using groundwater VOC data for sample TMW-2, H&H utilized
the DEQ Risk Calculator (July 2020 version) to calculate potential cumulative risks. Calculations
were completed for residential and non-residential hypothetical exposure scenarios. The results
of risk calculations are summarized below and are included in Appendix D.

Land Use Scenario Calculated Cumulative LICR Calculated Cumulative HI Calculated LICR or HI Exceeds Acceptable Risk Levels?
Residential 1.5 x 10-4 38 Yes
Non-Residential Worker 3.3 x 10-5 9.0 Yes

Cumulative risk calculations show that the non-carcinogenic and carcinogenic risk levels are above
acceptable risk levels for both residential and non-residential exposure scenarios. Therefore, based
on groundwater data, vapor intrusion is a potential concern for future buildings in the vicinity of
sample TMW-2.

3.3 Asbestos Sampling Results
Results of asbestos analysis did not indicate the presence of asbestos in the debris samples
collected from the Site. The asbestos analytical report is included in Appendix C.
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4.0 Summary, Conclusions, and Recommendations

In January 2021, H&H performed Phase II ESA soil and groundwater sampling activities at the
former Pharr Yarn Mills property located at 700 West 1st Street in Lowell, Gaston County, North
Carolina. A summary of the results of the Phase II ESA is provided below.

GPR Survey
• Results of the GPR survey indicated evidence of two former UST basins (reportedly
containing two fuel oil USTs in each basin) in the northern portion of the Site and one
former UST (contents unknown) in the southern portion of the Site.
• An existing UST (reportedly containing fuel oil) was identified in the eastern portion of
the Site during the GPR survey.

Soil
• Soil analytical data do not indicate the presence of TPH-DRO or TPH-GRO at
concentrations above the UST Section Action Levels in samples collected adjacent to
current/former USTs.
• PCE was detected in samples SB-4 (11-13 ft) and SB-5 (3-5 ft) at concentrations above the
protection of groundwater PSRG but below the residential and industrial/commercial
PSRGs. Sample SB-4 (11-13 ft) was collected adjacent to the former coal trestle/machine
shop, and sample SB-5 (3-5 ft) was collected within the former machine shop.
• Multiple PAHs were detected in samples SB-5 (3-5 ft) and SB-13 (1-3 ft), which were
collected within the former machine shop and the former carpentry shop, respectively. The
detected benzo(a)anthracene concentration in sample SB-5 (3-5 ft) exceeds the protection
of groundwater PSRG. The detected benzo(a)pyrene concentrations in samples SB-5 (3-5
ft) and SB-13 (1-3 ft) exceed the protection of groundwater and residential PSRGs.
• No PCBs were detected above the MDLs in sample SB-3 (1-3 ft), which was collected at
the former electrical substation.

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Groundwater
•Groundwater analytical data indicate that PCE and TCE were detected in temporary well
sample TMW-2 at concentrations above the respective 2L Standards. The detected PCE and
TCE concentrations in TMW-2 also exceed the respective non-residential GWSLs. Sample
TMW-2 was collected downgradient of the former machine shop.
•PCE was also detected in samples TMW-3, TMW-4, and TMW-6 at concentrations greater
than or equal to the 2L Standard. These samples were collected in the northeastern, eastern,
and southern portions of the Site, respectively.
•Cumulative risk calculations using VOC groundwater data for sample TMW-2 show that
the non-carcinogenic and carcinogenic risk levels are above acceptable risk levels for both
residential and non-residential exposure scenarios. Therefore, based on groundwater data,
vapor intrusion is a potential concern for future buildings in the vicinity of sample
TMW-2.
Suspect Asbestos Debris
•Results of asbestos analysis did not indicate the presence of asbestos in the debris samples
collected from the Site.
Recommendations
Based on the results of the Phase II ESA, H&H recommends that the prospective owner/developer
pursue a Brownfields Agreement with DEQ to address and manage environmental impacts at the Site.
In addition, H&H recommends that the UST in the southeastern portion of the Site be removed in
accordance with DEQ UST Section Guidelines or in accordance with a DEQ Brownfields Program
approved Environmental Management Plan during Site redevelopment.
Table 1
Summary of Temporary Monitoring Well Construction and Water Level Data
Former Pharr Yarn Mills
700 West 1st Street
Lowell, North Carolina
H&H Job No. HNY-001
Well ID Well Diameter
(inches)
Approximate Well
Depth
(ft bgs)
Screen Interval
(ft bgs)
Depth to
Groundwater
(ft bgs)
TMW-1 1 25 15-25 17.19
TMW-2 1 30 20-30 25.13
TMW-3 1 30 20-30 27.80
TMW-4 1 30 20-30 26.09
TMW-5 1 30 15-30 19.65
TMW-6 1 30 15-30 19.11
Notes:
ft bgs = feet below ground surface
Depth to groundwater measurements collected on January 12, 2021.
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2/17/2021
Table 1
Hart & Hickman, PC
Table 2 (Page 1 of 2)Summary of Soil Analytical ResultsFormer Pharr Yarn Mills700 West 1st StreetLowell, North CarolinaH&H Job No. HNY-001Sample ID SB-1 (10-12) SB-2 (10-12) SB-3 (1-3) SB-4 (1-3) SB-4 (11-13) SB-5 (3-5) SB-6 (3-5)Date 01/11/21 01/11/21 01/12/21 01/11/21 01/11/21 01/11/21 01/11/21DescriptionFormer Electrical SubstationDepth (ft bgs)10-12 10-12 1-3 1-3 11-13 3-5 3-5UnitsTPH (EPA Method 8015C)Diesel Range Organics 4.4 J<3.5 NA NA NA NA NA100 -- -- --Gasoline Range Organics<1.8 <1.8 NA NA NA NA NA50 -- -- --VOCs (EPA Method 8260D)AcetoneNA NA NA NA <0.0018 <0.0013 <0.0012-- 25 12,000 140,000TetrachloroethyleneNA NA NA NA0.0085 0.0180.0015 J -- 0.0063 17 82PAHs (EPA Method 8270E)AcenaphtheneNANANA<0.020 NA0.064 J<0.020-- 16 720 9,000AnthraceneNANANA<0.0097 NA0.18 J<0.0094-- 1,300 3,600 45,000Benzo(a)anthraceneNANANA<0.011 NA0.67 J<0.010-- 0.35 1.1 21Benzo(a)pyreneNANANA<0.0079 NA0.68 J<0.0076--0.12 0.11 2.1Benzo(b)fluorantheneNANANA<0.0081 NA0.79 J<0.0079--1.2 1.1 21Benzo(g,h,i)peryleneNANANA<0.0087 NA0.37 J<0.0084--NS NS NSBenzo(k)fluorantheneNANANA<0.0093 NA0.25 J<0.0090--12 11 210ChryseneNANANA<0.010 NA0.62 J<0.010--36 110 2,100Dibenzo(a,h)anthraceneNANANA<0.025 NA0.11 J<0.025--0.38 0.11 2.1FluorantheneNANANA<0.01 NA1.3<0.0097--670 480 6,000FluoreneNANANA<0.015 NA0.062 J<0.015--110 480 6,000Indeno(1,2,3-cd)pyreneNANANA<0.025 NA0.42 J<0.024--3.9 1.1 211-MethylnaphthaleneNANANA<0.013 NA0.092 J<0.013--0.11 18 732-MethylnaphthaleneNANANA<0.017 NA0.13 J<0.017--3.1 48 600NaphthaleneNANANA<0.019 NA0.099 J<0.018--0.39 2.1 8.8PhenanthreneNANANA<0.0096 NA0.80 J<0.0093--NS NS NSPyreneNA NA NA <0.013 NA1.1<0.012-- 440 360 4,500PCBs (EPA Method 8082A)Aroclor 1016NANA<0.0073 NANANANA-- 0.94 0.82 10Aroclor 1221NANA<0.053 NANANANA-- 0.0059 0.20 0.84Aroclor 1232NANA<0.017 NANANANA-- 0.0059 0.18 0.73Aroclor 1242NANA<0.018 NANANANA-- 0.055 0.23 0.95Aroclor 1248NANA<0.013 NANANANA-- 0.054 0.23 0.94Aroclor 1254NANA<0.016 NANANANA-- 0.091 0.23 0.97Aroclor 1260NANA<0.0084 NANANANA-- 0.24 0.24 0.99Notes:1) Action Levels obtained from the North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Underground Storage Tank (UST) Section Guidance forSite Checks, Tank Closure, and Initial Response and Abatement (February 2019).2) DEQ Preliminary Soil Remediation Goals (PSRGs) (July 2020).Bold indicates concentration exceeds the Protection of Groundwater PSRG.Underline indicates concentration exceeds the Residential PSRG.With the exception of Gasoline Range Organics, Diesel Range Organics, and polychlorinated bihenyls (PCBs), only those compounds detected in at least one sample are shown above.J = estimated value between the laboratory method detection limit and the laboratory reporting limitTPH = Total Petroleum Hydrocarbons; VOCs = Volatile Organic Compounds; PAHs = Polynuclear Aromatic HydrocarbonsNA = Not Analyzed; ft bgs = feet below ground surface; UST = Underground Storage TankNS = Not Specified; -- = Not Applicable; mg/kg = milligrams per kilogrammg/kgResidential PSRGs(2)Protection of Groundwater PSRGs(2)DEQ UST Section Action Levels(1)Industrial/ Commercial PSRGs(2)Mill Building No. 2 Former Fuel Oil USTsMill Building No. 1 Former Coal TrestleMill Building No. 1 Machine ShopS:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Phase II ESA\Tables\Data Table (2-18-21).xlsm2/18/2021Table 2 (Page 1 of 2) Hart & Hickman, PC
Table 2 (Page 2 of 2)Summary of Soil Analytical ResultsFormer Pharr Yarn Mills700 West 1st StreetLowell, North CarolinaH&H Job No. HNY-001Sample ID SB-7 (10-12) SB-8 (10-12) SB-9 (10-12) SB-10 (10-12) SB-11 (10-12) SB-12 (10-12) SB-13 (1-3)Date 01/11/21 01/11/21 01/11/21 01/11/21 01/11/21 01/11/21 01/11/21DescriptionFormer Carpentry ShopDepth (ft bgs)10-12 10-12 10-12 10-12 10-12 10-12 1-3UnitsTPH (EPA Method 8015C)Diesel Range Organics<3.0 <3.1 <3.23.9 J<2.8 <2.7 NA100 -- -- --Gasoline Range Organics<1.4 <1.8 <1.8 <2.1 <1.4 <1.0 NA50 -- -- --VOCs (EPA Method 8260D)AcetoneNA NA NA NA NA NA0.021 -- 25 12,000 140,000TetrachloroethyleneNA NA NA NA NA NA <0.00092-- 0.0063 17 82PAHs (EPA Method 8270E)AcenaphtheneNANANANANANA0.027 J -- 16 720 9,000AnthraceneNANANANANANA0.097 J -- 1,300 3,600 45,000Benzo(a)anthraceneNANANANANANA0.29 J -- 0.35 1.1 21Benzo(a)pyreneNANANANANANA0.25 J--0.12 0.11 2.1Benzo(b)fluorantheneNANANANANANA0.31 J--1.2 1.1 21Benzo(g,h,i)peryleneNANANANANANA0.14 J--NS NS NSBenzo(k)fluorantheneNANANANANANA0.10 J--12 11 210ChryseneNANANANANANA0.26 J--36 110 2,100Dibenzo(a,h)anthraceneNANANANANANA0.038 J--0.38 0.11 2.1FluorantheneNANANANANANA0.59 J--670 480 6,000FluoreneNANANANANANA0.029 J--110 480 6,000Indeno(1,2,3-cd)pyreneNANANANANANA0.15 J--3.9 1.1 211-MethylnaphthaleneNANANANANANA<0.013--0.11 18 732-MethylnaphthaleneNANANANANANA<0.016--3.1 48 600NaphthaleneNANANANANANA<0.018--0.39 2.1 8.8PhenanthreneNANANANANANA0.43 J--NS NS NSPyreneNA NA NA NA NA NA0.48 J -- 440 360 4,500PCBs (EPA Method 8082A)Aroclor 1016NANANANANANANA-- 0.94 0.82 10Aroclor 1221NANANANANANANA-- 0.0059 0.20 0.84Aroclor 1232NANANANANANANA-- 0.0059 0.18 0.73Aroclor 1242NANANANANANANA-- 0.055 0.23 0.95Aroclor 1248NANANANANANANA-- 0.054 0.23 0.94Aroclor 1254NANANANANANANA-- 0.091 0.23 0.97Aroclor 1260NANANANANANANA-- 0.24 0.24 0.99Notes:1) Action Levels obtained from the North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Underground Storage Tank (UST) Section Guidance forSite Checks, Tank Closure, and Initial Response and Abatement (February 2019).2) DEQ Preliminary Soil Remediation Goals (PSRGs) (July 2020).Bold indicates concentration exceeds the Protection of Groundwater PSRG.Underline indicates concentration exceeds the Residential PSRG.With the exception of Gasoline Range Organics, Diesel Range Organics, and polychlorinated bihenyls (PCBs), only those compounds detected in at least one sample are shown above.J = estimated value between the laboratory method detection limit and the laboratory reporting limitTPH = Total Petroleum Hydrocarbons; VOCs = Volatile Organic Compounds; PAHs = Polynuclear Aromatic HydrocarbonsNA = Not Analyzed; ft bgs = feet below ground surface; UST = Underground Storage TankNS = Not Specified; -- = Not Applicable; mg/kg = milligrams per kilogramIndustrial/ Commercial PSRGs(2)Residential PSRGs(2)Protection of Groundwater PSRGs(2)NC DEQ UST Section Action Levels(1)mg/kgMill Building No. 1 Former Fuel Oil USTsFormer Office Building UST LocationFormer USTS:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Phase II ESA\Tables\Data Table (2-18-21).xlsm2/18/2021Table 2 (Page 2 of 2) Hart & Hickman, PC
Table 3Summary of Groundwater Analytical ResultsFormer Pharr Yarn Mills700 West 1st StreetLowell, North CarolinaH&H Job No. HNY-001Sample ID TMW-1 TMW-2 TMW-3 TMW-4 TMW-5 TMW-6Date 01/12/21 01/12/21 01/12/21 01/12/21 01/12/21 01/12/21DescriptionMill Building No. 2 Former Fuel Oil USTsMill Building No. 1 Former Coal Trestle/Downgradient of former Machine ShopMill Building No. 1 Former Fuel Oil USTsFormer Office Building UST Location Former UST Former Carpentry ShopUnitsVOCs (EPA Method 8260D)1,2-Dichlorobenzene<0.076 <0.760.51<0.076 <0.076 <0.07620 530 2,200Naphthalene 3.0<3.0 <0.30 <0.30 <0.30 <0.306.0 4.6 20Tetrachloroethylene<0.0982,1006.6 5.6<0.0980.70 0.70 12 48Trichloroethylene<0.0787.9<0.078 <0.078 <0.078 <0.0783.0 1.0 4.41,2,4-Trimethylbenzene 0.84<0.54 <0.054 <0.054 <0.054 <0.054400 50 2101,3,5-Trimethylbenzene 0.22 J<0.76 <0.076 <0.076 <0.076 <0.076400 35 150m,p-Xylenes 0.30 J<1.2 <0.12 <0.12 <0.12 <0.12500 NS NSXylenes, total 0.30 J<1.5 <0.15 <0.15 <0.15 <0.15500 77 320PAHs (EPA Method 8270E)Naphthalene 1.6 J<1.3 <2.7 <1.3 <1.3 <1.46.0 4.6 20Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) (April 2013).2) DEQ Vapor Intrusion Groundwater Screening Levels (July 2020).Bold concentrations exceed the 2L Standard.Bold and Underlined concentrations exceed the 2L Standard and Residential GWSL.Bold and Highlighted values exceed the 2L Standard and Non-Residential GWSL.Only those compounds detected in at least one sample are shown above.J = estimated value between the laboratory method detection limit and the laboratory reporting limitVOCs = Volatile Organic Compounds; PAHs = Polynuclear Aromatic Hydrocarbons; µg/L = micrograms per literug/L2L Standards(1)Residential GWSLs(2)Non-Residential GWSLs(2)S:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Phase II ESA\Tables\Data Table (1-29-21).xlsm2/17/2021Table 3 Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed May, 2020.
SITE LOCATION MAP
FORMER PHARR YARN MILLS700 WEST 1ST STREETLOWELL, NORTH CAROLINA
DATE: 11-23-20
JOB NO: HNY-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\HNY-001\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
MOUNT HOLLY, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
SB-11SB-12/TMW-5
SB-9
SB-10/TMW-4
SB-8/TMW-3
SB-6
SB-5
SB-4/TMW-2
SB-2
SB-3
SB-13/TMW-6
SB-1/TMW-1
SB-7
REVISION NO. 0
JOB NO. HNY-001
DATE: 2-17-21
FIGURE NO. 3
FORMER PHARR YARN MILLS
700 WEST 1ST STREET
LOWELL, NORTH CAROLINA
SITE AND SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
RAILROAD
HISTORICAL BUILDING
FOOTPRINT
UNDERGROUND STORAGE TANK
LOCATION
FORMER UNDERGROUND
STORAGE TANK LOCATION
VENT PIPE
POLE-MOUNTED TRANSFORMER
SOIL BORING LOCATION
TEMPORARY MONITORING WELL/
SOIL BORING LOCATION
SUSPECTED ASBESTOS-
CONTAINING-MATERIAL DEBRIS
PILE (ASBESTOS NOT DETECTED)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
W
E
S
T

1
S
T

S
T
R
E
E
T
NO
RTH CL
A
Y STREETBIRCH STREETPOTTS
STREET
NOTES:
1.PARCEL DATA OBTAINED FROM GASTON COUNTY GIS
DEPARTMENT, 2020.
2.AERIAL IMAGERY OBTAINED FORM NC ONEMAP, 2019.
RESIDENTIAL
RESIDENTIAL
FORMER TOWN
OF LOWELL
WATER TOWER
FORMER OFFICE
BUILDING
NON-POTABLE
WATER SUPPLY WELL
FORMER DUKE
POWER SUB-STATION
FORMER
WASTE
HOUSE
MILL BUILDING
NO. 2
MILL BUILDING
NO. 1
FORMER
COTTON
WAREHOUSE
COTTON
WAREHOUSE
HIGHWAY 7 COOL JUNK
(607 WEST 1ST STREET)
PLASTIC MATERIALS, INC./
PELICANS TRAINING FACILITY
(210 ASH STREET/
510 WEST 1ST STREET)
LOWELL CHURCH OF GOD
(800 WEST 1ST STREET)
FORMER
WATER
RESERVOIR
R
A
I
L
R
O
A
D

S
T
R
E
E
T ASH STREETPHILLIPS STREETFORMER
CARPENTER
SHOP
FORMER STORES
FORMER
MACHINE
SHOP
FORMER
COAL
TRESTLE
S:\AAA-Master Projects\Henley Capital LLC (HNY)\HNY-001 - Lowell, NC ESA\Phase I ESA\Figures\Site Map.dwg, Figure 3, 2/17/2021 1:11:36 PM, sperry

Appendix A Boring Logs
NOTES: Hole precleared to 5' by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
WELL LOG
Well No.
Page:
SB-1/TMW-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 9:25
1/11/21 10:05
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
2.5
Grab
17.19
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
25
1
0.120
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') SILT (ML); little clay, stiff, moist, dark reddish-brown, few black
(1.5') Lean CLAY (CL); few coarse gravel, some silt, medium plasticity, stiff, moist,
reddish
(4') SILT (ML); some clay, medium stiff, moist, reddish
(7.5') SILT (ML); medium stiff, moist, red with few black mottling
(13') SILT (ML); medium stiff, wet, yellowish-red with black mottling
(22') As Above: Saturated
(25') Boring terminated
4.4
3.7
2.0
1.9
1.8
1.4
1.8
1.8
SB-1(10-12)
0
5
10
15
20
25
30
35
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 10:10
1/11/21 10:40
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Lean CLAY (CL); little fine sand, some silt, medium plasticity, medium stiff, moist,
dark reddish-brown
(1.5') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, reddish
(7') SILT (ML); medium stiff, moist, red with black mottling
(11') As Above: yellowish-red
(15') Boring terminated
1.4
1.1
1.7
1.4
1.8
1.8
1.9
SB-2(10-12)
0
5
10
15
20
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/12/21 17:30
1/12/21
Hart & Hickman
Other
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Silty GRAVEL with sand (GM); some medium-coarse sand, dense, moist,
brownish-gray
(1.5') Lean CLAY (CL); few fine-medium sand, some silt, medium plasticity, stiff, moist,
reddish
(3.5') Lean CLAY (CL); few silt, medium plasticity, stiff, moist, reddish
(5') Boring terminated
0.9
1.2
0.8
SB-3(1-3)
0
5
10
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
WELL LOG
Well No.
Page:
SB-4/TMW-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 13:05
1/11/21 13:35
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
2.50
25.13
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
30.0
1.0
0.120
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') Sandy lean CLAY (CL); medium plasticity, medium stiff, wet, yellowish-brown
(0.5') SILT (ML); some clay, stiff, moist, reddish
(4') SILT (ML); trace fine sand, trace clay, stiff, moist, reddish
(9') As Above: dark yellowish-red
(12') As Above: red with black mottling
(17') SILT (ML); few clay, stiff, wet, reddish, with black mottling
(19') As Above: yellowish red with black mottling
(26') As Above: wet, medium stiff
(30') Boring terminated
2.0
6.0
6.6
14.4
15.4
18.9
27.9
15.8
SB-4(11-13)
SB-4(1-3)
0
5
10
15
20
25
30
35
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 16:00
1/11/21
IET
Other
Hand Auger
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Silty SAND (SM); few fine gravel, few clay, dense, moist, reddish-brown
(1') Poorly graded GRAVEL (GP); concrete debris
(2') SILT (ML); few medium sand, some clay, stiff, moist, reddish
(5') Boring terminated
1.6
1.8
SB-5(3-5)
0
5
10
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 15:50
1/11/21
IET
Other
Hand Auger
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Silty SAND (SM); few clay, dense, moist, reddish-brown
(1') Poorly graded GRAVEL (GP); concrete debris
(3') SILT (ML); few fine-medium sand, stiff, moist, reddish
(5') Boring terminated
1.7
1.2 SB-6(3-5)
0
5
10
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 10:45
1/11/21 11:05
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Sandy SILT (ML); few coarse gravel, stiff, moist, reddish
(1') Poorly graded GRAVEL (GP); and brick fragments
(2') Lean CLAY (CL); few fine sand, some silt, medium plasticity, stiff, moist, dark
reddish
(5') SILT (ML); few fine-medium sand, stiff, moist, yellowish-red
(13') SILT (ML); stiff, moist, red with black mottling
(15') Boring terminated
2.0
1.5
2.3
2.3
2.5
2.4
2.9
SB-7(10-12)
0
5
10
15
20
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
WELL LOG
Well No.
Page:
SB-8/TMW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 11:10
1/11/21 11:40
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
2.50
27.80
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
30.0
1.0
0.120
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') Silty SAND (SM); dense, moist, reddish-black, with few gravel and brick
fragments
(1') Poorly graded GRAVEL (GP); and brick fragments
(2') Lean CLAY (CL); medium plasticity, stiff, moist, reddish
(5') SILT (ML); few clay, stiff, moist, reddish
(9') SILT (ML); medium stiff, moist, reddish, no clay
(14') As Above: red with some black mottling
(16') SILT (ML); trace fine sand, medium stiff, moist, yellowish-red with black mottling
(26') As Above: wet
(30') Boring terminated
3.4
1.5
0.9
0.9
1.3
1.8
2.1
SB-8(10-12)
0
5
10
15
20
25
30
35
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-9
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 11:45
1/11/21 11:45
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, reddish
(4') SILT (ML); few clay, stiff, moist, reddish
(8') Sandy SILT (ML); few fine gravel, medium stiff, moist, yellowish-red
(9') As Above: no gravel
(12') SILT (ML); trace fine sand, trace clay, stiff, moist, red with black mottling
(15') Boring terminated
1.4
1.2
1.6
1.2
1.4
1.3
1.7
SB-9(10-12)
0
5
10
15
20
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
WELL LOG
Well No.
Page:
SB-10/TMW-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 12:00
1/11/21 12:55
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
2.50
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
30.0
1.0
0.120
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, reddish
(3.5') As Above: some medium gravel
(4.5') SILT (ML); stiff, moist, reddish
(7') As Above: red with few white
(11') SILT (ML); medium stiff, moist, dark red with white mottling
(14.5') Sandy SILT (ML); medium stiff, moist, red with black and white mottling
(19.5') Poorly graded SAND with gravel (SP); some fine gravel
(20') SILT (ML); some clay, stiff, wet, brown with black mottling
(25') As Above: very wet to saturated
(30') Boring terminated
1.5
1.8
1.9
2.0
1.9
2.0
1.8
SB-10(10-12)
0
5
10
15
20
25
30
35
26.09
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
BORING LOG
Boring No.
Page:
SB-11
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 15:25
1/11/21 15:45
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Sandy SILT (ML); little clay, soft, wet, dark brown, with organics
(0.5') Lean CLAY (CL); few fine sand, some silt, medium plasticity, medium stiff, moist,
dark reddish
(2.5') SILT (ML); few fine sand, some clay, stiff, moist, dark reddish
(4') SILT (ML); trace fine sand, trace clay, stiff, moist, reddish
(5.5') Sandy SILT (ML); medium stiff, moist, yellowish-red with white
(7') As Above: yellowish-red with black and white mottling
(13') Sandy SILT (ML); few fine gravel, medium stiff, moist, white yellowish-brown with
black and white mottling
(15') Boring terminated
1.7
1.8
1.5
2.2
1.9
3.1
1.9
1.7
SB-11(10-12)
0
5
10
15
20
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
WELL LOG
Well No.
Page:
SB-12/TMW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 14:55
1/11/21 15:20
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
2.50
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
30.0
1.0
0.120
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') SILT (ML); little fine-medium sand, some clay, soft, moist, dark brown, with
organics
(0.5') Lean CLAY (CL); few fine-medium sand, some silt, medium plasticity, medium
stiff, moist, dark reddish
(3') SILT (ML); few fine-medium sand, stiff, moist, reddish
(6') Sandy SILT (ML); medium stiff, moist, yellowish-brown
(9') As Above: with few black
(10.5') As Above: very stiff
(12.5') Sandy SILT (ML); medium stiff, moist, light yellowish-brown
(19') As Above: with red
(22') Sandy SILT (ML); stiff, wet, reddish-yellow, with partially weathered rock
(27') Sandy SILT (ML); soft, wet, reddish-brown
(30') Boring terminated
1.5
1.4
1.7
1.9
1.8
2.2
2.1
2.2
SB-12(10-12)
0
5
10
15
20
25
30
35
19.65
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Henley Capital LLC
HNY-001
700 West 1st Street, Lowell, NC
WELL LOG
Well No.
Page:
SB-13/TMW-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
1/11/21 14:00
1/11/21 14:35
IET
Direct Push
Geoprobe VMS
Mike Tynan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
2.50
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
30.0
1.0
0.120
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') Sandy SILT (ML); soft, wet, brown, with organics
(0.5') Lean CLAY (CL); trace fine gravel, few fine-medium sand, some silt, medium
plasticity, medium stiff, moist, reddish
(1') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, reddish
(2.5') SILT (ML); some clay, stiff, moist, reddish
(6') Sandy SILT (ML); stiff, moist, yellowish-red
(8') SILT (ML); stiff, moist, yellowish-red with white
(12') As Above: yellowish-red with black and white mottling
(20.5') SILT (ML); stiff, wet, pale red with black and white mottling
(30') Boring terminated
3.8
2.5
8.0
2.3
2.4
5.6
2.1
SB-13(1-3)
0
5
10
15
20
25
30
35
19.11
NOTES:
BORING AND WELL LOG LEGEND
LITHOLOGYWATER LEVELWELL/BORINGCOMPLETIONSample TypeDESCRIPTION
GR
EN
SS
SH
CO
DP
ID
ASPHALT
CONCRETE
BEDROCK
IGNEOUS Rock
METAMORPHIC Rock
SEDIMENTARY Rock
Well-graded GRAVEL (GW)
Poorly graded GRAVEL (GP)
Silty GRAVEL (GM)
Clayey GRAVEL (GC)
Well-graded GRAVEL with silt (GW-GM)
Poorly graded GRAVEL with silt (GP-GM)
Well-graded GRAVEL with clay (GW-GC)
Poorly graded GRAVEL with clay (GP-GC)
Well-graded SAND (SW)
Poorly graded SAND (SP)
Silty SAND (SM)
Clayey SAND (SC)
Well-graded SAND with silt (SW-SM)
Poorly graded SAND with silt (SP-SM)
Well-graded SAND with clay (SW-SC)
Poorly graded SAND with clay (SP-SC)
SILT (ML)
Lean CLAY (CL)
Organic SOIL (OL)
Elastic SILT (MH)
Fat CLAY (CH)
Organic SOIL (OH)
Organic SOIL (OL/OH)
PEAT (PT)
Volume Descriptors:
Trace = <5%
Few = 5-10%
Little = 15-25%
Some = 30-45%
Mostly = >=50%
Water Level During Drilling
Water Level at End of Drilling/in Completed Well
Cap
Riser
Screen
End Plug
Annular Seal (Bentonite-Cement Grout, Bentonite Slurry/Chips/Pellets/Powder, Other)
Sanitary Seal (Bentonite Slurry/Chips/Pellets/Powder, Other)
Filter Pack (Sand, Gravel, Other)
Backfill
Grab
Encore
Split Spoon
Shelby Tube
Core Barrel
Direct Push
Lab Sample and ID

Appendix B Low Flow Groundwater Sampling Forms

Appendix C Laboratory Analytical Reports
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
1/20/21 9:36
Hart & Hickman (Charlotte)
Bo Cappleman
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: HNY-001
Lab Submittal Date: 01/13/2021
Work Order: 1010203
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Senior Project Manager
Angela D. Overcash
Data Qualifiers Key Reference:
A Parameter reported with possible high bias. LCS recovery QC limit.
CCVH CCV result is above control limits but within method parameters. Result is considered estimated.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
M Matrix spike outside of the control limits.
SR Surrogate recovery outside of the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 69
Sample Receipt Summary
01/20/2021
Work Order: 1010203
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
1010203-01 01/11/21 16:45SB-1 (10-12)01/13/21 9:40Solid
1010203-02 01/11/21 16:55SB-2 (10-12)01/13/21 9:40Solid
1010203-03 01/12/21 18:10SB-3 (1-3)01/13/21 9:40Solid
1010203-04 01/11/21 17:10SB-4 (1-3)01/13/21 9:40Solid
1010203-05 01/11/21 18:45SB-4 (11-13)01/13/21 9:40Solid
1010203-06 01/11/21 18:30SB-5 (3-5)01/13/21 9:40Solid
1010203-07 01/11/21 18:40SB-6 (3-5)01/13/21 9:40Solid
1010203-08 01/11/21 17:15SB-7 (10-12)01/13/21 9:40Solid
1010203-09 01/11/21 17:25SB-8 (10-12)01/13/21 9:40Solid
1010203-10 01/11/21 17:35SB-9 (10-12)01/13/21 9:40Solid
1010203-11 01/11/21 17:45SB-10 (10-12)01/13/21 9:40Solid
1010203-12 01/11/21 17:55SB-11 (10-12)01/13/21 9:40Solid
1010203-13 01/11/21 18:10SB-12 (10-12)01/13/21 9:40Solid
1010203-14 01/11/21 18:20SB-13 (1-3)01/13/21 9:40Solid
1010203-15 01/12/21 14:25TMW-1 01/13/21 9:40Water
1010203-16 01/12/21 15:50TMW-2 01/13/21 9:40Water
1010203-17 01/12/21 17:05TMW-3 01/13/21 9:40Water
1010203-18 01/12/21 16:30TMW-4 01/13/21 9:40Water
1010203-19 01/12/21 11:35TMW-5 01/13/21 9:40Water
1010203-20 01/12/21 13:20TMW-6 01/13/21 9:40Water
1010203-21 01/12/21 0:00Trip Blank 01/13/21 9:40Water
Samples were received in good condition at 0.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 69
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 1010203
01/20/2021
Summary of Detections
4.4 J mg/kg dry1010203-01 SB-1 (10-12)Diesel Range Organics 8015C
0.0085 mg/kg dry1010203-05 SB-4 (11-13)Tetrachloroethylene 8260D
0.092 J mg/kg dry1010203-06 SB-5 (3-5)1-Methylnaphthalene 8270E
0.13 J mg/kg dry1010203-06 SB-5 (3-5)2-Methylnaphthalene 8270E
0.064 J mg/kg dry1010203-06 SB-5 (3-5)Acenaphthene 8270E
0.18 J mg/kg dry1010203-06 SB-5 (3-5)Anthracene 8270E
0.67 J mg/kg dry1010203-06 SB-5 (3-5)Benzo(a)anthracene 8270E
0.68 J mg/kg dry1010203-06 SB-5 (3-5)Benzo(a)pyrene 8270E
0.79 J mg/kg dry1010203-06 SB-5 (3-5)Benzo(b)fluoranthene 8270E
0.37 J mg/kg dry1010203-06 SB-5 (3-5)Benzo(g,h,i)perylene 8270E
0.25 J mg/kg dry1010203-06 SB-5 (3-5)Benzo(k)fluoranthene 8270E
0.62 J mg/kg dry1010203-06 SB-5 (3-5)Chrysene 8270E
0.11 J mg/kg dry1010203-06 SB-5 (3-5)Dibenzo(a,h)anthracene 8270E
1.3 mg/kg dry1010203-06 SB-5 (3-5)Fluoranthene 8270E
0.062 J mg/kg dry1010203-06 SB-5 (3-5)Fluorene 8270E
0.42 J mg/kg dry1010203-06 SB-5 (3-5)Indeno(1,2,3-cd)pyrene 8270E
0.099 J mg/kg dry1010203-06 SB-5 (3-5)Naphthalene 8270E
0.80 J mg/kg dry1010203-06 SB-5 (3-5)Phenanthrene 8270E
1.1 mg/kg dry1010203-06 SB-5 (3-5)Pyrene 8270E
0.018 mg/kg dry1010203-06 SB-5 (3-5)Tetrachloroethylene 8260D
0.0015 J mg/kg dry1010203-07 SB-6 (3-5)Tetrachloroethylene 8260D
3.9 J mg/kg dry1010203-11 SB-10 (10-12)Diesel Range Organics 8015C
0.027 J mg/kg dry1010203-14 SB-13 (1-3)Acenaphthene 8270E
0.097 J mg/kg dry1010203-14 SB-13 (1-3)Anthracene 8270E
0.29 J mg/kg dry1010203-14 SB-13 (1-3)Benzo(a)anthracene 8270E
0.25 J mg/kg dry1010203-14 SB-13 (1-3)Benzo(a)pyrene 8270E
0.31 J mg/kg dry1010203-14 SB-13 (1-3)Benzo(b)fluoranthene 8270E
0.14 J mg/kg dry1010203-14 SB-13 (1-3)Benzo(g,h,i)perylene 8270E
0.10 J mg/kg dry1010203-14 SB-13 (1-3)Benzo(k)fluoranthene 8270E
0.26 J mg/kg dry1010203-14 SB-13 (1-3)Chrysene 8270E
0.038 J mg/kg dry1010203-14 SB-13 (1-3)Dibenzo(a,h)anthracene 8270E
0.59 J mg/kg dry1010203-14 SB-13 (1-3)Fluoranthene 8270E
0.029 J mg/kg dry1010203-14 SB-13 (1-3)Fluorene 8270E
0.15 J mg/kg dry1010203-14 SB-13 (1-3)Indeno(1,2,3-cd)pyrene 8270E
0.43 J mg/kg dry1010203-14 SB-13 (1-3)Phenanthrene 8270E
0.48 J mg/kg dry1010203-14 SB-13 (1-3)Pyrene 8270E
0.021 CCVH mg/kg dry1010203-14 SB-13 (1-3)Acetone 8260D
1.6 J ug/L1010203-15 TMW-1 Naphthalene 8270E
0.84 ug/L1010203-15 TMW-1 1,2,4-Trimethylbenzene 8260D
0.22 J ug/L1010203-15 TMW-1 1,3,5-Trimethylbenzene 8260D
0.30 J ug/L1010203-15 TMW-1 m,p-Xylenes 8260D
3.0 ug/L1010203-15 TMW-1 Naphthalene 8260D
0.30 J ug/L1010203-15 TMW-1 Xylenes, total 8260D
2100 ug/L1010203-16 TMW-2 Tetrachloroethylene 8260D
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 69
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 1010203
01/20/2021
Summary of Detections
7.9 ug/L1010203-16 TMW-2 Trichloroethylene 8260D
0.51 ug/L1010203-17 TMW-3 1,2-Dichlorobenzene 8260D
6.6 ug/L1010203-17 TMW-3 Tetrachloroethylene 8260D
5.6 ug/L1010203-18 TMW-4 Tetrachloroethylene 8260D
0.70 ug/L1010203-20 TMW-6 Tetrachloroethylene 8260D
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-1 (10-12)
Sample ID: 1010203-01
Work Order: 1010203
Time Collected: 01/11/21 16:45
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A06521111/15/21 14:13 ZRCJmg/kg dry 3.5Diesel Range Organics 4.4
Surrogate Recovery Control Limits
31-12373 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632506.7 1/15/21 11:36 TBLmg/kg dry 1.8Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137111 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 67.2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-2 (10-12)
Sample ID: 1010203-02
Work Order: 1010203
Time Collected: 01/11/21 16:55
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A06521101/15/21 14:50 ZRCmg/kg dry 3.5Diesel Range Organics BDL
Surrogate Recovery Control Limits
31-12377 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632506.6 1/15/21 12:04 TBLmg/kg dry 1.8Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137106 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 68.7
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-3 (1-3)
Sample ID: 1010203-03
Work Order: 1010203
Time Collected: 01/12/21 18:10
Time Submitted: 01/13/21 09:40
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 76.0
Polychlorinated Biphenyls (PCBs) by GC/ECD
8082A P1A071810.066 1/19/21 10:55 NMBmg/kg dry 0.0073Aroclor 1016 BDL
8082A P1A071810.13 1/19/21 10:55 NMBmg/kg dry 0.053Aroclor 1221 BDL
8082A P1A071810.13 1/19/21 10:55 NMBmg/kg dry 0.017Aroclor 1232 BDL
8082A P1A071810.066 1/19/21 10:55 NMBmg/kg dry 0.018Aroclor 1242 BDL
8082A P1A071810.066 1/19/21 10:55 NMBmg/kg dry 0.013Aroclor 1248 BDL
8082A P1A071810.066 1/19/21 10:55 NMBmg/kg dry 0.016Aroclor 1254 BDL
8082A P1A071810.066 1/19/21 10:55 NMBmg/kg dry 0.0084Aroclor 1260 BDL
Surrogate Recovery Control Limits
36-182106 %Tetrachloro-m-xylene
34-18278 %Decachlorobiphenyl
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-4 (1-3)
Sample ID: 1010203-04
Work Order: 1010203
Time Collected: 01/11/21 17:10
Time Submitted: 01/13/21 09:40
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 75.4
Semivolatile Organic Compounds by GC/MS
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0131-Methylnaphthalene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0172-Methylnaphthalene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.020AcenaphtheneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.017AcenaphthyleneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0097AnthraceneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.011Benzo(a)anthracene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0079Benzo(a)pyrene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0081Benzo(b)fluoranthene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0087Benzo(g,h,i)perylene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0093Benzo(k)fluoranthene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.010ChryseneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.025Dibenzo(a,h)anthracene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.010FluorantheneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.015FluoreneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.025Indeno(1,2,3-cd)pyrene BDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.019NaphthaleneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.0096PhenanthreneBDL
8270E P1A065110.88 1/15/21 15:37 JMVmg/kg dry 0.013PyreneBDL
Surrogate Recovery Control Limits
44-115102 %2-Fluorobiphenyl
37-12296 %Nitrobenzene-d5
54-127104 %Terphenyl-d14
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-4 (11-13)
Sample ID: 1010203-05
Work Order: 1010203
Time Collected: 01/11/21 18:45
Time Submitted: 01/13/21 09:40
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 75.4
Volatile Organic Compounds by GC/MS
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000841,1,1,2-Tetrachloroethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00101,1,1-Trichloroethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000501,1,2,2-Tetrachloroethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000741,1,2-Trichloroethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00121,1-Dichloroethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00131,1-Dichloroethylene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00111,1-Dichloropropylene BDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.000991,2,3-Trichlorobenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000781,2,3-Trichloropropane BDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.000661,2,4-Trichlorobenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000731,2,4-Trimethylbenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000621,2-Dibromoethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000771,2-Dichlorobenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000821,2-Dichloroethane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00101,2-Dichloropropane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000871,3,5-Trimethylbenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000861,3-Dichlorobenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000581,3-Dichloropropane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000871,4-Dichlorobenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000862,2-Dichloropropane BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000922-Chlorotoluene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.000784-Chlorotoluene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00174-Isopropyltoluene BDL
8260D P1A063310.028 1/14/21 16:52 TBLCCVHmg/kg dry 0.0018AcetoneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0011BenzeneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00096BromobenzeneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0011BromochloromethaneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00065BromodichloromethaneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00053BromoformBDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0034BromomethaneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0014Carbon Tetrachloride BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0011ChlorobenzeneBDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0013ChloroethaneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00084ChloroformBDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0021ChloromethaneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0011cis-1,2-Dichloroethylene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00068cis-1,3-Dichloropropylene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00046DibromochloromethaneBDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0019DichlorodifluoromethaneBDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-4 (11-13)
Sample ID: 1010203-05
Work Order: 1010203
Time Collected: 01/11/21 18:45
Time Submitted: 01/13/21 09:40
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0010EthylbenzeneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0010Isopropyl Ether BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00080Isopropylbenzene (Cumene)BDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0018m,p-Xylenes BDL
8260D P1A063310.028 1/14/21 16:52 TBLmg/kg dry 0.00048Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A063310.028 1/14/21 16:52 TBLmg/kg dry 0.0016Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A063310.028 1/14/21 16:52 TBLmg/kg dry 0.00056Methyl Isobutyl Ketone BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0011Methylene Chloride BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00097Methyl-tert-Butyl Ether BDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.00070NaphthaleneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00065n-Butylbenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0010n-Propylbenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00073o-Xylene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00074sec-Butylbenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00067StyreneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00082tert-Butylbenzene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0012Tetrachloroethylene0.0085
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0011TolueneBDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0013trans-1,2-Dichloroethylene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.00059trans-1,3-Dichloropropylene BDL
8260D P1A063310.0069 1/14/21 16:52 TBLmg/kg dry 0.0013TrichloroethyleneBDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0019TrichlorofluoromethaneBDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.00075Vinyl acetate BDL
8260D P1A063310.014 1/14/21 16:52 TBLmg/kg dry 0.0014Vinyl chloride BDL
8260D P1A063310.021 1/14/21 16:52 TBLmg/kg dry 0.0025Xylenes, total BDL
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-12398 %Dibromofluoromethane
76-129108 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-5 (3-5)
Sample ID: 1010203-06
Work Order: 1010203
Time Collected: 01/11/21 18:30
Time Submitted: 01/13/21 09:40
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 76.5
Semivolatile Organic Compounds by GC/MS
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0131-Methylnaphthalene 0.092
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0172-Methylnaphthalene 0.13
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.020Acenaphthene0.064
8270E P1A065110.87 1/15/21 16:00 JMVmg/kg dry 0.017AcenaphthyleneBDL
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0096Anthracene0.18
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.010Benzo(a)anthracene 0.67
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0078Benzo(a)pyrene 0.68
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0081Benzo(b)fluoranthene 0.79
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0086Benzo(g,h,i)perylene 0.37
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0093Benzo(k)fluoranthene 0.25
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.010Chrysene0.62
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.025Dibenzo(a,h)anthracene 0.11
8270E P1A065110.87 1/15/21 16:00 JMVmg/kg dry 0.0099Fluoranthene1.3
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.015Fluorene0.062
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.025Indeno(1,2,3-cd)pyrene 0.42
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.019Naphthalene0.099
8270E P1A065110.87 1/15/21 16:00 JMVJmg/kg dry 0.0095Phenanthrene0.80
8270E P1A065110.87 1/15/21 16:00 JMVmg/kg dry 0.013Pyrene1.1
Surrogate Recovery Control Limits
44-11585 %2-Fluorobiphenyl
37-12277 %Nitrobenzene-d5
54-12790 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000611,1,1,2-Tetrachloroethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000731,1,1-Trichloroethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000361,1,2,2-Tetrachloroethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000541,1,2-Trichloroethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000901,1-Dichloroethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000921,1-Dichloroethylene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000771,1-Dichloropropylene BDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.000711,2,3-Trichlorobenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000571,2,3-Trichloropropane BDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.000481,2,4-Trichlorobenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000531,2,4-Trimethylbenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000451,2-Dibromoethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000561,2-Dichlorobenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000591,2-Dichloroethane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000751,2-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-5 (3-5)
Sample ID: 1010203-06
Work Order: 1010203
Time Collected: 01/11/21 18:30
Time Submitted: 01/13/21 09:40
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000631,3,5-Trimethylbenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000621,3-Dichlorobenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000421,3-Dichloropropane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000631,4-Dichlorobenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000622,2-Dichloropropane BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000672-Chlorotoluene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.000574-Chlorotoluene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00134-Isopropyltoluene BDL
8260D P1A063310.020 1/14/21 15:21 TBLCCVHmg/kg dry 0.0013AcetoneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00078BenzeneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00069BromobenzeneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00082BromochloromethaneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00047BromodichloromethaneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00039BromoformBDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.0024BromomethaneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00098Carbon Tetrachloride BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00078ChlorobenzeneBDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.00095ChloroethaneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00061ChloroformBDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.0015ChloromethaneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00078cis-1,2-Dichloroethylene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00049cis-1,3-Dichloropropylene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00033DibromochloromethaneBDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.0014DichlorodifluoromethaneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00075EthylbenzeneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00073Isopropyl Ether BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00058Isopropylbenzene (Cumene)BDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.0013m,p-Xylenes BDL
8260D P1A063310.020 1/14/21 15:21 TBLmg/kg dry 0.00035Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A063310.020 1/14/21 15:21 TBLmg/kg dry 0.0012Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A063310.020 1/14/21 15:21 TBLmg/kg dry 0.00041Methyl Isobutyl Ketone BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00081Methylene Chloride BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00070Methyl-tert-Butyl Ether BDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.00050NaphthaleneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00047n-Butylbenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00072n-Propylbenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00053o-Xylene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00054sec-Butylbenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00048StyreneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00059tert-Butylbenzene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00090Tetrachloroethylene0.018
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00079TolueneBDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00096trans-1,2-Dichloroethylene BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-5 (3-5)
Sample ID: 1010203-06
Work Order: 1010203
Time Collected: 01/11/21 18:30
Time Submitted: 01/13/21 09:40
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00043trans-1,3-Dichloropropylene BDL
8260D P1A063310.0050 1/14/21 15:21 TBLmg/kg dry 0.00097TrichloroethyleneBDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.0013TrichlorofluoromethaneBDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.00054Vinyl acetate BDL
8260D P1A063310.010 1/14/21 15:21 TBLmg/kg dry 0.00099Vinyl chloride BDL
8260D P1A063310.015 1/14/21 15:21 TBLmg/kg dry 0.0018Xylenes, total BDL
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-12393 %Dibromofluoromethane
76-129109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-6 (3-5)
Sample ID: 1010203-07
Work Order: 1010203
Time Collected: 01/11/21 18:40
Time Submitted: 01/13/21 09:40
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 77.0
Semivolatile Organic Compounds by GC/MS
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0131-Methylnaphthalene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0172-Methylnaphthalene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.020AcenaphtheneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.017AcenaphthyleneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0094AnthraceneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.010Benzo(a)anthracene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0076Benzo(a)pyrene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0079Benzo(b)fluoranthene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0084Benzo(g,h,i)perylene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0090Benzo(k)fluoranthene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.010ChryseneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.025Dibenzo(a,h)anthracene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0097FluorantheneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.015FluoreneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.024Indeno(1,2,3-cd)pyrene BDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.018NaphthaleneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.0093PhenanthreneBDL
8270E P1A065110.85 1/15/21 16:22 JMVmg/kg dry 0.012PyreneBDL
Surrogate Recovery Control Limits
44-11587 %2-Fluorobiphenyl
37-12275 %Nitrobenzene-d5
54-12785 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000591,1,1,2-Tetrachloroethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000721,1,1-Trichloroethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000351,1,2,2-Tetrachloroethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000531,1,2-Trichloroethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000881,1-Dichloroethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000891,1-Dichloroethylene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000751,1-Dichloropropylene BDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.000701,2,3-Trichlorobenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000551,2,3-Trichloropropane BDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.000461,2,4-Trichlorobenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000521,2,4-Trimethylbenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000441,2-Dibromoethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000541,2-Dichlorobenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000581,2-Dichloroethane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000731,2-Dichloropropane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000611,3,5-Trimethylbenzene BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-6 (3-5)
Sample ID: 1010203-07
Work Order: 1010203
Time Collected: 01/11/21 18:40
Time Submitted: 01/13/21 09:40
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000611,3-Dichlorobenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000411,3-Dichloropropane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000621,4-Dichlorobenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000612,2-Dichloropropane BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000652-Chlorotoluene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.000554-Chlorotoluene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00124-Isopropyltoluene BDL
8260D P1A063310.019 1/14/21 15:51 TBLCCVHmg/kg dry 0.0012AcetoneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00076BenzeneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00068BromobenzeneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00080BromochloromethaneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00046BromodichloromethaneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00038BromoformBDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.0024BromomethaneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00096Carbon Tetrachloride BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00076ChlorobenzeneBDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.00093ChloroethaneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00060ChloroformBDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.0015ChloromethaneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00077cis-1,2-Dichloroethylene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00048cis-1,3-Dichloropropylene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00033DibromochloromethaneBDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.0014DichlorodifluoromethaneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00073EthylbenzeneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00071Isopropyl Ether BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00057Isopropylbenzene (Cumene)BDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.0012m,p-Xylenes BDL
8260D P1A063310.019 1/14/21 15:51 TBLmg/kg dry 0.00034Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A063310.019 1/14/21 15:51 TBLmg/kg dry 0.0011Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A063310.019 1/14/21 15:51 TBLmg/kg dry 0.00040Methyl Isobutyl Ketone BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00079Methylene Chloride BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00068Methyl-tert-Butyl Ether BDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.00049NaphthaleneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00046n-Butylbenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00071n-Propylbenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00052o-Xylene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00053sec-Butylbenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00047StyreneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00058tert-Butylbenzene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLJmg/kg dry 0.00088Tetrachloroethylene0.0015
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00077TolueneBDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00093trans-1,2-Dichloroethylene BDL
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00042trans-1,3-Dichloropropylene BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-6 (3-5)
Sample ID: 1010203-07
Work Order: 1010203
Time Collected: 01/11/21 18:40
Time Submitted: 01/13/21 09:40
8260D P1A063310.0049 1/14/21 15:51 TBLmg/kg dry 0.00094TrichloroethyleneBDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.0013TrichlorofluoromethaneBDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.00053Vinyl acetate BDL
8260D P1A063310.0097 1/14/21 15:51 TBLmg/kg dry 0.00096Vinyl chloride BDL
8260D P1A063310.015 1/14/21 15:51 TBLmg/kg dry 0.0018Xylenes, total BDL
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-129112 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-7 (10-12)
Sample ID: 1010203-08
Work Order: 1010203
Time Collected: 01/11/21 17:15
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A065218.9 1/15/21 15:27 ZRCmg/kg dry 3.0Diesel Range Organics BDL
Surrogate Recovery Control Limits
31-12369 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632505.1 1/15/21 12:33 TBLmg/kg dry 1.4Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137118 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 79.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-8 (10-12)
Sample ID: 1010203-09
Work Order: 1010203
Time Collected: 01/11/21 17:25
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A065219.3 1/15/21 16:03 ZRCmg/kg dry 3.1Diesel Range Organics BDL
Surrogate Recovery Control Limits
31-12381 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632506.5 1/15/21 13:01 TBLmg/kg dry 1.8Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137113 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 76.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-9 (10-12)
Sample ID: 1010203-10
Work Order: 1010203
Time Collected: 01/11/21 17:35
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A065219.5 1/15/21 16:40 ZRCmg/kg dry 3.2Diesel Range Organics BDL
Surrogate Recovery Control Limits
31-12389 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632506.7 1/15/21 13:29 TBLmg/kg dry 1.8Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137110 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 73.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-10 (10-12)
Sample ID: 1010203-11
Work Order: 1010203
Time Collected: 01/11/21 17:45
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A06521111/15/21 17:17 ZRCJmg/kg dry 3.6Diesel Range Organics 3.9
Surrogate Recovery Control Limits
31-12391 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632507.9 1/15/21 13:57 TBLmg/kg dry 2.1Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137110 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 64.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-11 (10-12)
Sample ID: 1010203-12
Work Order: 1010203
Time Collected: 01/11/21 17:55
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A065218.3 1/15/21 17:54 ZRCmg/kg dry 2.8Diesel Range Organics BDL
Surrogate Recovery Control Limits
31-12381 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632505.3 1/15/21 14:25 TBLmg/kg dry 1.4Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137116 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 84.4
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-12 (10-12)
Sample ID: 1010203-13
Work Order: 1010203
Time Collected: 01/11/21 18:10
Time Submitted: 01/13/21 09:40
Diesel Range Organics by GC/FID
8015C P1A065218.0 1/15/21 18:31 ZRCmg/kg dry 2.7Diesel Range Organics BDL
Surrogate Recovery Control Limits
31-12370 %o-Terphenyl
Gasoline Range Organics by GC/FID
8015C P1A0632503.8 1/15/21 14:53 TBLmg/kg dry 1.0Gasoline Range Organics BDL
Surrogate Recovery Control Limits
50-137113 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 88.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-13 (1-3)
Sample ID: 1010203-14
Work Order: 1010203
Time Collected: 01/11/21 18:20
Time Submitted: 01/13/21 09:40
General Chemistry Parameters
SM2540 G P1A067110.100 1/18/21 8:20 EDV% by
Weight
0.100% Solids 79.9
Semivolatile Organic Compounds by GC/MS
8270E P1A065110.83 1/15/21 16:45 JMVmg/kg dry 0.0131-Methylnaphthalene BDL
8270E P1A065110.83 1/15/21 16:45 JMVmg/kg dry 0.0162-Methylnaphthalene BDL
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.019Acenaphthene0.027
8270E P1A065110.83 1/15/21 16:45 JMVmg/kg dry 0.016AcenaphthyleneBDL
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0092Anthracene0.097
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.010Benzo(a)anthracene 0.29
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0074Benzo(a)pyrene 0.25
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0077Benzo(b)fluoranthene 0.31
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0082Benzo(g,h,i)perylene 0.14
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0088Benzo(k)fluoranthene 0.10
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0098Chrysene0.26
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.024Dibenzo(a,h)anthracene 0.038
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0095Fluoranthene0.59
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.014Fluorene0.029
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.023Indeno(1,2,3-cd)pyrene 0.15
8270E P1A065110.83 1/15/21 16:45 JMVmg/kg dry 0.018NaphthaleneBDL
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.0091Phenanthrene0.43
8270E P1A065110.83 1/15/21 16:45 JMVJmg/kg dry 0.012Pyrene0.48
Surrogate Recovery Control Limits
44-11583 %2-Fluorobiphenyl
37-12273 %Nitrobenzene-d5
54-12785 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000621,1,1,2-Tetrachloroethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000751,1,1-Trichloroethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000371,1,2,2-Tetrachloroethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000551,1,2-Trichloroethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000921,1-Dichloroethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000931,1-Dichloroethylene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000781,1-Dichloropropylene BDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.000731,2,3-Trichlorobenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000581,2,3-Trichloropropane BDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.000481,2,4-Trichlorobenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000541,2,4-Trimethylbenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000451,2-Dibromoethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000571,2-Dichlorobenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000601,2-Dichloroethane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000761,2-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-13 (1-3)
Sample ID: 1010203-14
Work Order: 1010203
Time Collected: 01/11/21 18:20
Time Submitted: 01/13/21 09:40
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000641,3,5-Trimethylbenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000631,3-Dichlorobenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000421,3-Dichloropropane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000641,4-Dichlorobenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000632,2-Dichloropropane BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000682-Chlorotoluene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.000584-Chlorotoluene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00134-Isopropyltoluene BDL
8260D P1A063310.020 1/14/21 16:21 TBLCCVHmg/kg dry 0.0013Acetone0.021
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00079BenzeneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00070BromobenzeneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00083BromochloromethaneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00048BromodichloromethaneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00039BromoformBDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.0025BromomethaneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.0010Carbon Tetrachloride BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00079ChlorobenzeneBDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.00097ChloroethaneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00062ChloroformBDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.0015ChloromethaneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00080cis-1,2-Dichloroethylene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00050cis-1,3-Dichloropropylene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00034DibromochloromethaneBDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.0014DichlorodifluoromethaneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00076EthylbenzeneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00074Isopropyl Ether BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00059Isopropylbenzene (Cumene)BDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.0013m,p-Xylenes BDL
8260D P1A063310.020 1/14/21 16:21 TBLmg/kg dry 0.00035Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A063310.020 1/14/21 16:21 TBLCCVHmg/kg dry 0.0012Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A063310.020 1/14/21 16:21 TBLmg/kg dry 0.00041Methyl Isobutyl Ketone BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00082Methylene Chloride BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00071Methyl-tert-Butyl Ether BDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.00051NaphthaleneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00047n-Butylbenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00074n-Propylbenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00054o-Xylene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00055sec-Butylbenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00049StyreneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00060tert-Butylbenzene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00092TetrachloroethyleneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00081TolueneBDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00097trans-1,2-Dichloroethylene BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Solid
Client Sample ID: SB-13 (1-3)
Sample ID: 1010203-14
Work Order: 1010203
Time Collected: 01/11/21 18:20
Time Submitted: 01/13/21 09:40
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00043trans-1,3-Dichloropropylene BDL
8260D P1A063310.0051 1/14/21 16:21 TBLmg/kg dry 0.00098TrichloroethyleneBDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.0014TrichlorofluoromethaneBDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.00055Vinyl acetate BDL
8260D P1A063310.010 1/14/21 16:21 TBLmg/kg dry 0.0010Vinyl chloride BDL
8260D P1A063310.015 1/14/21 16:21 TBLmg/kg dry 0.0018Xylenes, total BDL
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-129113 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-1
Sample ID: 1010203-15
Work Order: 1010203
Time Collected: 01/12/21 14:25
Time Submitted: 01/13/21 09:40
Semivolatile Organic Compounds by GC/MS
8270E P1A06311101/14/21 16:36 JMVug/L 1.11-Methylnaphthalene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 1.22-Methylnaphthalene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.80AcenaphtheneBDL
8270E P1A06311211/14/21 16:36 JMVug/L 0.62AcenaphthyleneBDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.49AnthraceneBDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.78Benzo(a)anthracene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.46Benzo(a)pyrene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.91Benzo(b)fluoranthene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 1.0Benzo(g,h,i)perylene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.85Benzo(k)fluoranthene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 1.0ChryseneBDL
8270E P1A06311211/14/21 16:36 JMVug/L 1.6Dibenzo(a,h)anthracene BDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.59FluorantheneBDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.48FluoreneBDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.78Indeno(1,2,3-cd)pyrene BDL
8270E P1A06311101/14/21 16:36 JMVJug/L 1.3Naphthalene1.6
8270E P1A06311101/14/21 16:36 JMVug/L 0.42PhenanthreneBDL
8270E P1A06311101/14/21 16:36 JMVug/L 0.70PyreneBDL
Surrogate Recovery Control Limits
44-11981 %2-Fluorobiphenyl
44-12073 %Nitrobenzene-d5
50-13477 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.111,1,1,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0611,1,1-Trichloroethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0361,1,2,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0661,1,2-Trichloroethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0831,1-Dichloroethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0831,1-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0511,1-Dichloropropylene BDL
8260D P1A072812.0 1/18/21 23:26 JLBug/L 0.401,2,3-Trichlorobenzene BDL
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.141,2,3-Trichloropropane BDL
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.131,2,4-Trichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0541,2,4-Trimethylbenzene 0.84
8260D P1A072812.0 1/18/21 23:26 JLBug/L 0.171,2-Dibromo-3-chloropropane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0511,2-Dibromoethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0761,2-Dichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0661,2-Dichloroethane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.111,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:26 JLBJug/L 0.0761,3,5-Trimethylbenzene 0.22
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0541,3-Dichlorobenzene BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-1
Sample ID: 1010203-15
Work Order: 1010203
Time Collected: 01/12/21 14:25
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0431,3-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0501,4-Dichlorobenzene BDL
8260D P1A072812.0 1/18/21 23:26 JLBug/L 0.112,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0662-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0504-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.0894-Isopropyltoluene BDL
8260D P1A072815.0 1/18/21 23:26 JLBug/L 0.31AcetoneBDL
8260D P1A07281201/18/21 23:26 JLBug/L 0.20AcroleinBDL
8260D P1A07281201/18/21 23:26 JLBug/L 0.20AcrylonitrileBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.048BenzeneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.057BromobenzeneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.14BromochloromethaneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.062BromodichloromethaneBDL
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.040BromoformBDL
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.18BromomethaneBDL
8260D P1A072815.0 1/18/21 23:26 JLBug/L 0.075Carbon disulfide BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.11Carbon Tetrachloride BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.062ChlorobenzeneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.22ChloroethaneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.076ChloroformBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.079ChloromethaneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.056cis-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.079cis-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.081DibromochloromethaneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.065DibromomethaneBDL
8260D P1A072815.0 1/18/21 23:26 JLBug/L 0.11DichlorodifluoromethaneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.061EthylbenzeneBDL
8260D P1A072812.0 1/18/21 23:26 JLBug/L 0.16HexachlorobutadieneBDL
8260D P1A072815.0 1/18/21 23:26 JLBug/L 0.96Isopropyl Ether BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.054Isopropylbenzene (Cumene)BDL
8260D P1A072811.0 1/18/21 23:26 JLBJug/L 0.12m,p-Xylenes 0.30
8260D P1A072815.0 1/18/21 23:26 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072815.0 1/18/21 23:26 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072815.0 1/18/21 23:26 JLBug/L 1.0Methyl Isobutyl Ketone BDL
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.083Methylene Chloride BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.042Methyl-tert-Butyl Ether BDL
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.30Naphthalene3.0
8260D P1A072811.0 1/18/21 23:26 JLBug/L 0.076n-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.087n-Propylbenzene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.044o-Xylene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.076sec-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.047StyreneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.088tert-Butylbenzene BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-1
Sample ID: 1010203-15
Work Order: 1010203
Time Collected: 01/12/21 14:25
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.098TetrachloroethyleneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.044TolueneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.094trans-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.070trans-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.078TrichloroethyleneBDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.062TrichlorofluoromethaneBDL
8260D P1A072812.0 1/18/21 23:26 JLBug/L 0.060Vinyl acetate BDL
8260D P1A072810.50 1/18/21 23:26 JLBug/L 0.097Vinyl chloride BDL
8260D P1A072811.5 1/18/21 23:26 JLBJug/L 0.15Xylenes, total 0.30
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-2
Sample ID: 1010203-16
Work Order: 1010203
Time Collected: 01/12/21 15:50
Time Submitted: 01/13/21 09:40
Semivolatile Organic Compounds by GC/MS
8270E P1A06311101/14/21 16:59 JMVug/L 1.11-Methylnaphthalene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 1.22-Methylnaphthalene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.80AcenaphtheneBDL
8270E P1A06311211/14/21 16:59 JMVug/L 0.62AcenaphthyleneBDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.49AnthraceneBDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.78Benzo(a)anthracene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.46Benzo(a)pyrene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.91Benzo(b)fluoranthene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 1.0Benzo(g,h,i)perylene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.85Benzo(k)fluoranthene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 1.0ChryseneBDL
8270E P1A06311211/14/21 16:59 JMVug/L 1.6Dibenzo(a,h)anthracene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.59FluorantheneBDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.48FluoreneBDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.78Indeno(1,2,3-cd)pyrene BDL
8270E P1A06311101/14/21 16:59 JMVug/L 1.3NaphthaleneBDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.42PhenanthreneBDL
8270E P1A06311101/14/21 16:59 JMVug/L 0.70PyreneBDL
Surrogate Recovery Control Limits
44-11987 %2-Fluorobiphenyl
44-12080 %Nitrobenzene-d5
50-13472 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 1.11,1,1,2-Tetrachloroethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.611,1,1-Trichloroethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.361,1,2,2-Tetrachloroethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.661,1,2-Trichloroethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.831,1-Dichloroethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.831,1-Dichloroethylene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.511,1-Dichloropropylene BDL
8260D P1A072810201/19/21 1:01 JLBug/L 4.01,2,3-Trichlorobenzene BDL
8260D P1A072810101/19/21 1:01 JLBug/L 1.41,2,3-Trichloropropane BDL
8260D P1A072810101/19/21 1:01 JLBug/L 1.31,2,4-Trichlorobenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.541,2,4-Trimethylbenzene BDL
8260D P1A072810201/19/21 1:01 JLBug/L 1.71,2-Dibromo-3-chloropropane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.511,2-Dibromoethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.761,2-Dichlorobenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.661,2-Dichloroethane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 1.11,2-Dichloropropane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.761,3,5-Trimethylbenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.541,3-Dichlorobenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.431,3-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-2
Sample ID: 1010203-16
Work Order: 1010203
Time Collected: 01/12/21 15:50
Time Submitted: 01/13/21 09:40
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.501,4-Dichlorobenzene BDL
8260D P1A072810201/19/21 1:01 JLBug/L 1.12,2-Dichloropropane BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.662-Chlorotoluene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.504-Chlorotoluene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.894-Isopropyltoluene BDL
8260D P1A072810501/19/21 1:01 JLBug/L 3.1AcetoneBDL
8260D P1A0728102001/19/21 1:01 JLBug/L 2.0AcroleinBDL
8260D P1A0728102001/19/21 1:01 JLBug/L 2.0AcrylonitrileBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.48BenzeneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.57BromobenzeneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 1.4BromochloromethaneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.62BromodichloromethaneBDL
8260D P1A072810101/19/21 1:01 JLBug/L 0.40BromoformBDL
8260D P1A072810101/19/21 1:01 JLBug/L 1.8BromomethaneBDL
8260D P1A072810501/19/21 1:01 JLBug/L 0.75Carbon disulfide BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 1.1Carbon Tetrachloride BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.62ChlorobenzeneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 2.2ChloroethaneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.76ChloroformBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.79ChloromethaneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.56cis-1,2-Dichloroethylene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.79cis-1,3-Dichloropropylene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.81DibromochloromethaneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.65DibromomethaneBDL
8260D P1A072810501/19/21 1:01 JLBug/L 1.1DichlorodifluoromethaneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.61EthylbenzeneBDL
8260D P1A072810201/19/21 1:01 JLBug/L 1.6HexachlorobutadieneBDL
8260D P1A072810501/19/21 1:01 JLBug/L 9.6Isopropyl Ether BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.54Isopropylbenzene (Cumene)BDL
8260D P1A072810101/19/21 1:01 JLBug/L 1.2m,p-Xylenes BDL
8260D P1A072810501/19/21 1:01 JLBug/L 0.65Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072810501/19/21 1:01 JLBug/L 2.4Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072810501/19/21 1:01 JLBug/L 10Methyl Isobutyl Ketone BDL
8260D P1A072810101/19/21 1:01 JLBug/L 0.83Methylene Chloride BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.42Methyl-tert-Butyl Ether BDL
8260D P1A072810101/19/21 1:01 JLBug/L 3.0NaphthaleneBDL
8260D P1A072810101/19/21 1:01 JLBug/L 0.76n-Butylbenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.87n-Propylbenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.44o-Xylene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.76sec-Butylbenzene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.47StyreneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.88tert-Butylbenzene BDL
8260D P1A0728100501/19/21 1:25 JLBug/L 9.8Tetrachloroethylene2100
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-2
Sample ID: 1010203-16
Work Order: 1010203
Time Collected: 01/12/21 15:50
Time Submitted: 01/13/21 09:40
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.44TolueneBDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.94trans-1,2-Dichloroethylene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.70trans-1,3-Dichloropropylene BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.78Trichloroethylene7.9
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.62TrichlorofluoromethaneBDL
8260D P1A072810201/19/21 1:01 JLBug/L 0.60Vinyl acetate BDL
8260D P1A0728105.0 1/19/21 1:01 JLBug/L 0.97Vinyl chloride BDL
8260D P1A072810151/19/21 1:01 JLBug/L 1.5Xylenes, total BDL
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-3
Sample ID: 1010203-17
Work Order: 1010203
Time Collected: 01/12/21 17:05
Time Submitted: 01/13/21 09:40
Semivolatile Organic Compounds by GC/MS
8270E P1A06311211/14/21 17:21 JMVug/L 2.31-Methylnaphthalene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 2.62-Methylnaphthalene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.6AcenaphtheneBDL
8270E P1A06311431/14/21 17:21 JMVug/L 1.3AcenaphthyleneBDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.0AnthraceneBDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.6Benzo(a)anthracene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 0.95Benzo(a)pyrene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.9Benzo(b)fluoranthene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 2.1Benzo(g,h,i)perylene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.7Benzo(k)fluoranthene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 2.1ChryseneBDL
8270E P1A06311431/14/21 17:21 JMVug/L 3.3Dibenzo(a,h)anthracene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.2FluorantheneBDL
8270E P1A06311211/14/21 17:21 JMVug/L 0.98FluoreneBDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.6Indeno(1,2,3-cd)pyrene BDL
8270E P1A06311211/14/21 17:21 JMVug/L 2.7NaphthaleneBDL
8270E P1A06311211/14/21 17:21 JMVug/L 0.86PhenanthreneBDL
8270E P1A06311211/14/21 17:21 JMVug/L 1.4PyreneBDL
Surrogate Recovery Control Limits
44-11989 %2-Fluorobiphenyl
44-12080 %Nitrobenzene-d5
50-13484 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.111,1,1,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0611,1,1-Trichloroethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0361,1,2,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0661,1,2-Trichloroethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0831,1-Dichloroethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0831,1-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0511,1-Dichloropropylene BDL
8260D P1A072812.0 1/18/21 23:50 JLBug/L 0.401,2,3-Trichlorobenzene BDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.141,2,3-Trichloropropane BDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.131,2,4-Trichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0541,2,4-Trimethylbenzene BDL
8260D P1A072812.0 1/18/21 23:50 JLBug/L 0.171,2-Dibromo-3-chloropropane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0511,2-Dibromoethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0761,2-Dichlorobenzene 0.51
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0661,2-Dichloroethane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.111,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0761,3,5-Trimethylbenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0541,3-Dichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0431,3-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-3
Sample ID: 1010203-17
Work Order: 1010203
Time Collected: 01/12/21 17:05
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0501,4-Dichlorobenzene BDL
8260D P1A072812.0 1/18/21 23:50 JLBug/L 0.112,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0662-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0504-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.0894-Isopropyltoluene BDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 0.31AcetoneBDL
8260D P1A07281201/18/21 23:50 JLBug/L 0.20AcroleinBDL
8260D P1A07281201/18/21 23:50 JLBug/L 0.20AcrylonitrileBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.048BenzeneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.057BromobenzeneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.14BromochloromethaneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.062BromodichloromethaneBDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.040BromoformBDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.18BromomethaneBDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 0.075Carbon disulfide BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.11Carbon Tetrachloride BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.062ChlorobenzeneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.22ChloroethaneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.076ChloroformBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.079ChloromethaneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.056cis-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.079cis-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.081DibromochloromethaneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.065DibromomethaneBDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 0.11DichlorodifluoromethaneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.061EthylbenzeneBDL
8260D P1A072812.0 1/18/21 23:50 JLBug/L 0.16HexachlorobutadieneBDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 0.96Isopropyl Ether BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.054Isopropylbenzene (Cumene)BDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.12m,p-Xylenes BDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072815.0 1/18/21 23:50 JLBug/L 1.0Methyl Isobutyl Ketone BDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.083Methylene Chloride BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.042Methyl-tert-Butyl Ether BDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.30NaphthaleneBDL
8260D P1A072811.0 1/18/21 23:50 JLBug/L 0.076n-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.087n-Propylbenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.044o-Xylene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.076sec-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.047StyreneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.088tert-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.098Tetrachloroethylene6.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-3
Sample ID: 1010203-17
Work Order: 1010203
Time Collected: 01/12/21 17:05
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.044TolueneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.094trans-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.070trans-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.078TrichloroethyleneBDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.062TrichlorofluoromethaneBDL
8260D P1A072812.0 1/18/21 23:50 JLBug/L 0.060Vinyl acetate BDL
8260D P1A072810.50 1/18/21 23:50 JLBug/L 0.097Vinyl chloride BDL
8260D P1A072811.5 1/18/21 23:50 JLBug/L 0.15Xylenes, total BDL
Surrogate Recovery Control Limits
80-124100 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-123109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-4
Sample ID: 1010203-18
Work Order: 1010203
Time Collected: 01/12/21 16:30
Time Submitted: 01/13/21 09:40
Semivolatile Organic Compounds by GC/MS
8270E P1A06311101/14/21 17:43 JMVug/L 1.11-Methylnaphthalene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 1.22-Methylnaphthalene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.79AcenaphtheneBDL
8270E P1A06311211/14/21 17:43 JMVug/L 0.61AcenaphthyleneBDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.49AnthraceneBDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.77Benzo(a)anthracene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.46Benzo(a)pyrene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.90Benzo(b)fluoranthene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 1.0Benzo(g,h,i)perylene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.84Benzo(k)fluoranthene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 1.0ChryseneBDL
8270E P1A06311211/14/21 17:43 JMVug/L 1.6Dibenzo(a,h)anthracene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.59FluorantheneBDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.47FluoreneBDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.77Indeno(1,2,3-cd)pyrene BDL
8270E P1A06311101/14/21 17:43 JMVug/L 1.3NaphthaleneBDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.42PhenanthreneBDL
8270E P1A06311101/14/21 17:43 JMVug/L 0.69PyreneBDL
Surrogate Recovery Control Limits
44-11989 %2-Fluorobiphenyl
44-12082 %Nitrobenzene-d5
50-13470 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.111,1,1,2-Tetrachloroethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0611,1,1-Trichloroethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0361,1,2,2-Tetrachloroethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0661,1,2-Trichloroethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0831,1-Dichloroethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0831,1-Dichloroethylene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0511,1-Dichloropropylene BDL
8260D P1A072812.0 1/19/21 0:13 JLBug/L 0.401,2,3-Trichlorobenzene BDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.141,2,3-Trichloropropane BDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.131,2,4-Trichlorobenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0541,2,4-Trimethylbenzene BDL
8260D P1A072812.0 1/19/21 0:13 JLBug/L 0.171,2-Dibromo-3-chloropropane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0511,2-Dibromoethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0761,2-Dichlorobenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0661,2-Dichloroethane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.111,2-Dichloropropane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0761,3,5-Trimethylbenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0541,3-Dichlorobenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0431,3-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-4
Sample ID: 1010203-18
Work Order: 1010203
Time Collected: 01/12/21 16:30
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0501,4-Dichlorobenzene BDL
8260D P1A072812.0 1/19/21 0:13 JLBug/L 0.112,2-Dichloropropane BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0662-Chlorotoluene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0504-Chlorotoluene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.0894-Isopropyltoluene BDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 0.31AcetoneBDL
8260D P1A07281201/19/21 0:13 JLBug/L 0.20AcroleinBDL
8260D P1A07281201/19/21 0:13 JLBug/L 0.20AcrylonitrileBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.048BenzeneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.057BromobenzeneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.14BromochloromethaneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.062BromodichloromethaneBDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.040BromoformBDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.18BromomethaneBDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 0.075Carbon disulfide BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.11Carbon Tetrachloride BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.062ChlorobenzeneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.22ChloroethaneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.076ChloroformBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.079ChloromethaneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.056cis-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.079cis-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.081DibromochloromethaneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.065DibromomethaneBDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 0.11DichlorodifluoromethaneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.061EthylbenzeneBDL
8260D P1A072812.0 1/19/21 0:13 JLBug/L 0.16HexachlorobutadieneBDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 0.96Isopropyl Ether BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.054Isopropylbenzene (Cumene)BDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.12m,p-Xylenes BDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072815.0 1/19/21 0:13 JLBug/L 1.0Methyl Isobutyl Ketone BDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.083Methylene Chloride BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.042Methyl-tert-Butyl Ether BDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.30NaphthaleneBDL
8260D P1A072811.0 1/19/21 0:13 JLBug/L 0.076n-Butylbenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.087n-Propylbenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.044o-Xylene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.076sec-Butylbenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.047StyreneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.088tert-Butylbenzene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.098Tetrachloroethylene5.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-4
Sample ID: 1010203-18
Work Order: 1010203
Time Collected: 01/12/21 16:30
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.044TolueneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.094trans-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.070trans-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.078TrichloroethyleneBDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.062TrichlorofluoromethaneBDL
8260D P1A072812.0 1/19/21 0:13 JLBug/L 0.060Vinyl acetate BDL
8260D P1A072810.50 1/19/21 0:13 JLBug/L 0.097Vinyl chloride BDL
8260D P1A072811.5 1/19/21 0:13 JLBug/L 0.15Xylenes, total BDL
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-5
Sample ID: 1010203-19
Work Order: 1010203
Time Collected: 01/12/21 11:35
Time Submitted: 01/13/21 09:40
Semivolatile Organic Compounds by GC/MS
8270E P1A06311101/14/21 18:06 JMVug/L 1.11-Methylnaphthalene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 1.22-Methylnaphthalene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.76AcenaphtheneBDL
8270E P1A06311201/14/21 18:06 JMVug/L 0.60AcenaphthyleneBDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.47AnthraceneBDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.74Benzo(a)anthracene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.44Benzo(a)pyrene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.87Benzo(b)fluoranthene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.98Benzo(g,h,i)perylene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.81Benzo(k)fluoranthene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.98ChryseneBDL
8270E P1A06311201/14/21 18:06 JMVug/L 1.6Dibenzo(a,h)anthracene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.57FluorantheneBDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.46FluoreneBDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.75Indeno(1,2,3-cd)pyrene BDL
8270E P1A06311101/14/21 18:06 JMVug/L 1.3NaphthaleneBDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.40PhenanthreneBDL
8270E P1A06311101/14/21 18:06 JMVug/L 0.67PyreneBDL
Surrogate Recovery Control Limits
44-11969 %2-Fluorobiphenyl
44-12065 %Nitrobenzene-d5
50-13473 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.111,1,1,2-Tetrachloroethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0611,1,1-Trichloroethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0361,1,2,2-Tetrachloroethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0661,1,2-Trichloroethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0831,1-Dichloroethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0831,1-Dichloroethylene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0511,1-Dichloropropylene BDL
8260D P1A072812.0 1/19/21 0:37 JLBug/L 0.401,2,3-Trichlorobenzene BDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.141,2,3-Trichloropropane BDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.131,2,4-Trichlorobenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0541,2,4-Trimethylbenzene BDL
8260D P1A072812.0 1/19/21 0:37 JLBug/L 0.171,2-Dibromo-3-chloropropane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0511,2-Dibromoethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0761,2-Dichlorobenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0661,2-Dichloroethane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.111,2-Dichloropropane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0761,3,5-Trimethylbenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0541,3-Dichlorobenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0431,3-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-5
Sample ID: 1010203-19
Work Order: 1010203
Time Collected: 01/12/21 11:35
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0501,4-Dichlorobenzene BDL
8260D P1A072812.0 1/19/21 0:37 JLBug/L 0.112,2-Dichloropropane BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0662-Chlorotoluene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0504-Chlorotoluene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.0894-Isopropyltoluene BDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 0.31AcetoneBDL
8260D P1A07281201/19/21 0:37 JLBug/L 0.20AcroleinBDL
8260D P1A07281201/19/21 0:37 JLBug/L 0.20AcrylonitrileBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.048BenzeneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.057BromobenzeneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.14BromochloromethaneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.062BromodichloromethaneBDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.040BromoformBDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.18BromomethaneBDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 0.075Carbon disulfide BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.11Carbon Tetrachloride BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.062ChlorobenzeneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.22ChloroethaneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.076ChloroformBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.079ChloromethaneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.056cis-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.079cis-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.081DibromochloromethaneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.065DibromomethaneBDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 0.11DichlorodifluoromethaneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.061EthylbenzeneBDL
8260D P1A072812.0 1/19/21 0:37 JLBug/L 0.16HexachlorobutadieneBDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 0.96Isopropyl Ether BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.054Isopropylbenzene (Cumene)BDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.12m,p-Xylenes BDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072815.0 1/19/21 0:37 JLBug/L 1.0Methyl Isobutyl Ketone BDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.083Methylene Chloride BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.042Methyl-tert-Butyl Ether BDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.30NaphthaleneBDL
8260D P1A072811.0 1/19/21 0:37 JLBug/L 0.076n-Butylbenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.087n-Propylbenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.044o-Xylene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.076sec-Butylbenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.047StyreneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.088tert-Butylbenzene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.098TetrachloroethyleneBDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-5
Sample ID: 1010203-19
Work Order: 1010203
Time Collected: 01/12/21 11:35
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.044TolueneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.094trans-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.070trans-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.078TrichloroethyleneBDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.062TrichlorofluoromethaneBDL
8260D P1A072812.0 1/19/21 0:37 JLBug/L 0.060Vinyl acetate BDL
8260D P1A072810.50 1/19/21 0:37 JLBug/L 0.097Vinyl chloride BDL
8260D P1A072811.5 1/19/21 0:37 JLBug/L 0.15Xylenes, total BDL
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-6
Sample ID: 1010203-20
Work Order: 1010203
Time Collected: 01/12/21 13:20
Time Submitted: 01/13/21 09:40
Semivolatile Organic Compounds by GC/MS
8270E P1A06311111/14/21 18:28 JMVug/L 1.21-Methylnaphthalene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 1.32-Methylnaphthalene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.81AcenaphtheneBDL
8270E P1A06311211/14/21 18:28 JMVug/L 0.63AcenaphthyleneBDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.50AnthraceneBDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.79Benzo(a)anthracene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.47Benzo(a)pyrene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.93Benzo(b)fluoranthene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 1.0Benzo(g,h,i)perylene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.86Benzo(k)fluoranthene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 1.0ChryseneBDL
8270E P1A06311211/14/21 18:28 JMVug/L 1.7Dibenzo(a,h)anthracene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.60FluorantheneBDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.49FluoreneBDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.80Indeno(1,2,3-cd)pyrene BDL
8270E P1A06311111/14/21 18:28 JMVug/L 1.4NaphthaleneBDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.43PhenanthreneBDL
8270E P1A06311111/14/21 18:28 JMVug/L 0.71PyreneBDL
Surrogate Recovery Control Limits
44-11983 %2-Fluorobiphenyl
44-12074 %Nitrobenzene-d5
50-13475 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.111,1,1,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0611,1,1-Trichloroethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0361,1,2,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0661,1,2-Trichloroethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0831,1-Dichloroethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0831,1-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0511,1-Dichloropropylene BDL
8260D P1A072812.0 1/18/21 23:02 JLBug/L 0.401,2,3-Trichlorobenzene BDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.141,2,3-Trichloropropane BDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.131,2,4-Trichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0541,2,4-Trimethylbenzene BDL
8260D P1A072812.0 1/18/21 23:02 JLBug/L 0.171,2-Dibromo-3-chloropropane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0511,2-Dibromoethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0761,2-Dichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0661,2-Dichloroethane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.111,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0761,3,5-Trimethylbenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0541,3-Dichlorobenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0431,3-Dichloropropane BDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-6
Sample ID: 1010203-20
Work Order: 1010203
Time Collected: 01/12/21 13:20
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0501,4-Dichlorobenzene BDL
8260D P1A072812.0 1/18/21 23:02 JLBug/L 0.112,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0662-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0504-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.0894-Isopropyltoluene BDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 0.31AcetoneBDL
8260D P1A07281201/18/21 23:02 JLBug/L 0.20AcroleinBDL
8260D P1A07281201/18/21 23:02 JLBug/L 0.20AcrylonitrileBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.048BenzeneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.057BromobenzeneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.14BromochloromethaneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.062BromodichloromethaneBDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.040BromoformBDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.18BromomethaneBDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 0.075Carbon disulfide BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.11Carbon Tetrachloride BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.062ChlorobenzeneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.22ChloroethaneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.076ChloroformBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.079ChloromethaneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.056cis-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.079cis-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.081DibromochloromethaneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.065DibromomethaneBDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 0.11DichlorodifluoromethaneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.061EthylbenzeneBDL
8260D P1A072812.0 1/18/21 23:02 JLBug/L 0.16HexachlorobutadieneBDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 0.96Isopropyl Ether BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.054Isopropylbenzene (Cumene)BDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.12m,p-Xylenes BDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072815.0 1/18/21 23:02 JLBug/L 1.0Methyl Isobutyl Ketone BDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.083Methylene Chloride BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.042Methyl-tert-Butyl Ether BDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.30NaphthaleneBDL
8260D P1A072811.0 1/18/21 23:02 JLBug/L 0.076n-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.087n-Propylbenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.044o-Xylene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.076sec-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.047StyreneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.088tert-Butylbenzene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.098Tetrachloroethylene0.70
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: TMW-6
Sample ID: 1010203-20
Work Order: 1010203
Time Collected: 01/12/21 13:20
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.044TolueneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.094trans-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.070trans-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.078TrichloroethyleneBDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.062TrichlorofluoromethaneBDL
8260D P1A072812.0 1/18/21 23:02 JLBug/L 0.060Vinyl acetate BDL
8260D P1A072810.50 1/18/21 23:02 JLBug/L 0.097Vinyl chloride BDL
8260D P1A072811.5 1/18/21 23:02 JLBug/L 0.15Xylenes, total BDL
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: Trip Blank
Sample ID: 1010203-21
Work Order: 1010203
Time Collected: 01/12/21 00:00
Time Submitted: 01/13/21 09:40
Volatile Organic Compounds by GC/MS
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.111,1,1,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0611,1,1-Trichloroethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0361,1,2,2-Tetrachloroethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0661,1,2-Trichloroethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0831,1-Dichloroethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0831,1-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0511,1-Dichloropropylene BDL
8260D P1A072812.0 1/18/21 22:38 JLBug/L 0.401,2,3-Trichlorobenzene BDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.141,2,3-Trichloropropane BDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.131,2,4-Trichlorobenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0541,2,4-Trimethylbenzene BDL
8260D P1A072812.0 1/18/21 22:38 JLBug/L 0.171,2-Dibromo-3-chloropropane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0511,2-Dibromoethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0761,2-Dichlorobenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0661,2-Dichloroethane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.111,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0761,3,5-Trimethylbenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0541,3-Dichlorobenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0431,3-Dichloropropane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0501,4-Dichlorobenzene BDL
8260D P1A072812.0 1/18/21 22:38 JLBug/L 0.112,2-Dichloropropane BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0662-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0504-Chlorotoluene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.0894-Isopropyltoluene BDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 0.31AcetoneBDL
8260D P1A07281201/18/21 22:38 JLBug/L 0.20AcroleinBDL
8260D P1A07281201/18/21 22:38 JLBug/L 0.20AcrylonitrileBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.048BenzeneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.057BromobenzeneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.14BromochloromethaneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.062BromodichloromethaneBDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.040BromoformBDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.18BromomethaneBDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 0.075Carbon disulfide BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.11Carbon Tetrachloride BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.062ChlorobenzeneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.22ChloroethaneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.076ChloroformBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.079ChloromethaneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.056cis-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.079cis-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.081DibromochloromethaneBDL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 69
Laboratory Report
01/20/2021
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Sample Matrix: Water
Client Sample ID: Trip Blank
Sample ID: 1010203-21
Work Order: 1010203
Time Collected: 01/12/21 00:00
Time Submitted: 01/13/21 09:40
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.065DibromomethaneBDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 0.11DichlorodifluoromethaneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.061EthylbenzeneBDL
8260D P1A072812.0 1/18/21 22:38 JLBug/L 0.16HexachlorobutadieneBDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 0.96Isopropyl Ether BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.054Isopropylbenzene (Cumene)BDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.12m,p-Xylenes BDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)BDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)BDL
8260D P1A072815.0 1/18/21 22:38 JLBug/L 1.0Methyl Isobutyl Ketone BDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.083Methylene Chloride BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.042Methyl-tert-Butyl Ether BDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.30NaphthaleneBDL
8260D P1A072811.0 1/18/21 22:38 JLBug/L 0.076n-Butylbenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.087n-Propylbenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.044o-Xylene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.076sec-Butylbenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.047StyreneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.088tert-Butylbenzene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.098TetrachloroethyleneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.044TolueneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.094trans-1,2-Dichloroethylene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.070trans-1,3-Dichloropropylene BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.078TrichloroethyleneBDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.062TrichlorofluoromethaneBDL
8260D P1A072812.0 1/18/21 22:38 JLBug/L 0.060Vinyl acetate BDL
8260D P1A072810.50 1/18/21 22:38 JLBug/L 0.097Vinyl chloride BDL
8260D P1A072811.5 1/18/21 22:38 JLBug/L 0.15Xylenes, total BDL
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123108 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0633 - 5035
Blank (P1A0633-BLK1)Prepared & Analyzed: 01/14/21
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wet0.00149 0.020 J
Benzene mg/kg wetBRL0.0050
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.020
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0633 - 5035
Blank (P1A0633-BLK1)Prepared & Analyzed: 01/14/21
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.010
Vinyl acetate mg/kg wetBRL0.010
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9346.5
ug/L 50.00 76-129Surrogate: Toluene-d8 11456.8
LCS (P1A0633-BS1)Prepared & Analyzed: 01/14/21
1,1,1,2-Tetrachloroethane mg/kg wet0.0481 0.0050 0.05000 72-11596
1,1,1-Trichloroethane mg/kg wet0.0458 0.0050 0.05000 67-13192
1,1,2,2-Tetrachloroethane mg/kg wet0.0501 0.0050 0.05000 56-126100
1,1,2-Trichloroethane mg/kg wet0.0494 0.0050 0.05000 70-13399
1,1-Dichloroethane mg/kg wet0.0507 0.0050 0.05000 74-127101
1,1-Dichloroethylene mg/kg wet0.0437 0.0050 0.05000 67-14987
1,1-Dichloropropylene mg/kg wet0.0451 0.0050 0.05000 71-13090
1,2,3-Trichlorobenzene mg/kg wet0.0471 0.010 0.05000 68-13094
1,2,3-Trichloropropane mg/kg wet0.0510 0.0050 0.05000 60-137102
1,2,4-Trichlorobenzene mg/kg wet0.0470 0.010 0.05000 66-12594
1,2,4-Trimethylbenzene mg/kg wet0.0478 0.0050 0.05000 69-12996
1,2-Dibromoethane mg/kg wet0.0482 0.0050 0.05000 70-13296
1,2-Dichlorobenzene mg/kg wet0.0492 0.0050 0.05000 72-12398
1,2-Dichloroethane mg/kg wet0.0543 0.0050 0.05000 68-128109
1,2-Dichloropropane mg/kg wet0.0513 0.0050 0.05000 73-130103
1,3,5-Trimethylbenzene mg/kg wet0.0457 0.0050 0.05000 69-12891
1,3-Dichlorobenzene mg/kg wet0.0485 0.0050 0.05000 71-12097
1,3-Dichloropropane mg/kg wet0.0526 0.0050 0.05000 75-124105
1,4-Dichlorobenzene mg/kg wet0.0488 0.0050 0.05000 71-12398
2,2-Dichloropropane mg/kg wet0.0467 0.0050 0.05000 50-14293
2-Chlorotoluene mg/kg wet0.0479 0.0050 0.05000 67-12496
4-Chlorotoluene mg/kg wet0.0474 0.0050 0.05000 71-12695
4-Isopropyltoluene mg/kg wet0.0464 0.0050 0.05000 68-12993
Acetone mg/kg wet0.125 0.020 0.1000 29-198125
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0633 - 5035
LCS (P1A0633-BS1)Prepared & Analyzed: 01/14/21
Benzene mg/kg wet0.0503 0.0050 0.05000 74-127101
Bromobenzene mg/kg wet0.0493 0.0050 0.05000 73-12599
Bromochloromethane mg/kg wet0.0493 0.0050 0.05000 72-13499
Bromodichloromethane mg/kg wet0.0525 0.0050 0.05000 75-122105
Bromoform mg/kg wet0.0488 0.0050 0.05000 66-13598
Bromomethane mg/kg wet0.0747 0.010 0.05000 20-180149
Carbon Tetrachloride mg/kg wet0.0444 0.0050 0.05000 64-14389
Chlorobenzene mg/kg wet0.0503 0.0050 0.05000 74-118101
Chloroethane mg/kg wet0.0444 0.010 0.05000 33-14989
Chloroform mg/kg wet0.0500 0.0050 0.05000 73-127100
Chloromethane mg/kg wet0.0719 0.010 0.05000 LH45-143144
cis-1,2-Dichloroethylene mg/kg wet0.0516 0.0050 0.05000 76-134103
cis-1,3-Dichloropropylene mg/kg wet0.0533 0.0050 0.05000 71-125107
Dibromochloromethane mg/kg wet0.0490 0.0050 0.05000 73-12298
Dichlorodifluoromethane mg/kg wet0.0430 0.010 0.05000 26-14686
Ethylbenzene mg/kg wet0.0480 0.0050 0.05000 74-12896
Isopropyl Ether mg/kg wet0.0547 0.0050 0.05000 59-159109
Isopropylbenzene (Cumene)mg/kg wet0.0457 0.0050 0.05000 68-12691
m,p-Xylenes mg/kg wet0.0879 0.010 0.1000 75-12488
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0579 0.020 0.05000 61-157116
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0645 0.020 0.05000 63-149129
Methyl Isobutyl Ketone mg/kg wet0.0572 0.020 0.05000 57-162114
Methylene Chloride mg/kg wet0.0498 0.0050 0.05000 74-129100
Methyl-tert-Butyl Ether mg/kg wet0.0578 0.0050 0.05000 70-130116
Naphthalene mg/kg wet0.0505 0.010 0.05000 57-157101
n-Butylbenzene mg/kg wet0.0470 0.0050 0.05000 65-13594
n-Propylbenzene mg/kg wet0.0446 0.0050 0.05000 67-13089
o-Xylene mg/kg wet0.0487 0.0050 0.05000 74-12697
sec-Butylbenzene mg/kg wet0.0458 0.0050 0.05000 66-13192
Styrene mg/kg wet0.0523 0.0050 0.05000 77-121105
tert-Butylbenzene mg/kg wet0.0473 0.0050 0.05000 67-13295
Tetrachloroethylene mg/kg wet0.0442 0.0050 0.05000 68-13088
Toluene mg/kg wet0.0499 0.0050 0.05000 71-129100
trans-1,2-Dichloroethylene mg/kg wet0.0477 0.0050 0.05000 73-13295
trans-1,3-Dichloropropylene mg/kg wet0.0540 0.0050 0.05000 68-123108
Trichloroethylene mg/kg wet0.0475 0.0050 0.05000 75-13395
Trichlorofluoromethane mg/kg wet0.0392 0.010 0.05000 44-14678
Vinyl acetate mg/kg wet0.0577 0.010 0.05000 85-161115
Vinyl chloride mg/kg wet0.0481 0.010 0.05000 48-14796
Xylenes, total mg/kg wet0.137 0.015 0.1500 74-12691
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 76-129Surrogate: Toluene-d8 10954.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0633 - 5035
Matrix Spike (P1A0633-MS1)Prepared & Analyzed: 01/14/21 Source: 1010203-06
1,1,1,2-Tetrachloroethane mg/kg dry0.0605 0.0065 0.06538 BRL 60-12092
1,1,1-Trichloroethane mg/kg dry0.0720 0.0065 0.06538 BRL 52-139110
1,1,2,2-Tetrachloroethane mg/kg dry0.0610 0.0065 0.06538 BRL 39-13593
1,1,2-Trichloroethane mg/kg dry0.0605 0.0065 0.06538 BRL 44-14092
1,1-Dichloroethane mg/kg dry0.0739 0.0065 0.06538 BRL 59-137113
1,1-Dichloroethylene mg/kg dry0.0703 0.0065 0.06538 BRL 54-162108
1,1-Dichloropropylene mg/kg dry0.0642 0.0065 0.06538 BRL 55-13798
1,2,3-Trichlorobenzene mg/kg dry0.0349 0.013 0.06538 BRL 34-12053
1,2,3-Trichloropropane mg/kg dry0.0599 0.0065 0.06538 BRL 45-13992
1,2,4-Trichlorobenzene mg/kg dry0.0357 0.013 0.06538 BRL 35-11655
1,2,4-Trimethylbenzene mg/kg dry0.0557 0.0065 0.06538 BRL 38-14285
1,2-Dibromoethane mg/kg dry0.0545 0.0065 0.06538 BRL 49-13283
1,2-Dichlorobenzene mg/kg dry0.0497 0.0065 0.06538 BRL 42-13076
1,2-Dichloroethane mg/kg dry0.0683 0.0065 0.06538 BRL 51-131104
1,2-Dichloropropane mg/kg dry0.0697 0.0065 0.06538 BRL 55-138107
1,3,5-Trimethylbenzene mg/kg dry0.0604 0.0065 0.06538 BRL 44-14092
1,3-Dichlorobenzene mg/kg dry0.0492 0.0065 0.06538 BRL 41-12975
1,3-Dichloropropane mg/kg dry0.0617 0.0065 0.06538 BRL 53-12994
1,4-Dichlorobenzene mg/kg dry0.0475 0.0065 0.06538 BRL 44-13473
2,2-Dichloropropane mg/kg dry0.0682 0.0065 0.06538 BRL 30-147104
2-Chlorotoluene mg/kg dry0.0527 0.0065 0.06538 BRL 46-13281
4-Chlorotoluene mg/kg dry0.0523 0.0065 0.06538 BRL 44-13580
4-Isopropyltoluene mg/kg dry0.0532 0.0065 0.06538 BRL 32-14481
Acetone mg/kg dry0.0852 0.026 0.1308 BRL 34-14365
Benzene mg/kg dry0.0695 0.0065 0.06538 BRL 60-135106
Bromobenzene mg/kg dry0.0552 0.0065 0.06538 BRL 45-13584
Bromochloromethane mg/kg dry0.0630 0.0065 0.06538 BRL 55-13696
Bromodichloromethane mg/kg dry0.0708 0.0065 0.06538 BRL 55-127108
Bromoform mg/kg dry0.0556 0.0065 0.06538 BRL 40-13685
Bromomethane mg/kg dry0.0716 0.013 0.06538 BRL 30-137110
Carbon Tetrachloride mg/kg dry0.0671 0.0065 0.06538 BRL 48-153103
Chlorobenzene mg/kg dry0.0590 0.0065 0.06538 BRL 57-12590
Chloroethane mg/kg dry0.0657 0.013 0.06538 BRL 16-177100
Chloroform mg/kg dry0.0705 0.0065 0.06538 BRL 56-137108
Chloromethane mg/kg dry0.0941 0.013 0.06538 BRL 40-145144
cis-1,2-Dichloroethylene mg/kg dry0.0657 0.0065 0.06538 BRL 58-140100
cis-1,3-Dichloropropylene mg/kg dry0.0615 0.0065 0.06538 BRL 42-13594
Dibromochloromethane mg/kg dry0.0587 0.0065 0.06538 BRL 49-12790
Dichlorodifluoromethane mg/kg dry0.0546 0.013 0.06538 BRL 25-15184
Ethylbenzene mg/kg dry0.0599 0.0065 0.06538 BRL 44-14492
Isopropyl Ether mg/kg dry0.0731 0.0065 0.06538 BRL 51-155112
Isopropylbenzene (Cumene)mg/kg dry0.0604 0.0065 0.06538 BRL 41-14092
m,p-Xylenes mg/kg dry0.110 0.013 0.1308 BRL 36-14884
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0535 0.026 0.06538 BRL 30-14782
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0532 0.026 0.06538 BRL 24-16081
Methyl Isobutyl Ketone mg/kg dry0.0687 0.026 0.06538 BRL 25-163105
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0633 - 5035
Matrix Spike (P1A0633-MS1)Prepared & Analyzed: 01/14/21 Source: 1010203-06
Methylene Chloride mg/kg dry0.0690 0.0065 0.06538 BRL 53-144106
Methyl-tert-Butyl Ether mg/kg dry0.0741 0.0065 0.06538 BRL 49-135113
Naphthalene mg/kg dry0.0444 0.013 0.06538 BRL 32-12768
n-Butylbenzene mg/kg dry0.0500 0.0065 0.06538 BRL 23-14876
n-Propylbenzene mg/kg dry0.0553 0.0065 0.06538 BRL 35-14485
o-Xylene mg/kg dry0.0606 0.0065 0.06538 BRL 43-14393
sec-Butylbenzene mg/kg dry0.0560 0.0065 0.06538 BRL 34-14486
Styrene mg/kg dry0.0563 0.0065 0.06538 BRL 42-13286
tert-Butylbenzene mg/kg dry0.0597 0.0065 0.06538 BRL 36-15091
Tetrachloroethylene mg/kg dry0.0930 0.0065 0.06538 0.0177 47-142115
Toluene mg/kg dry0.0664 0.0065 0.06538 BRL 57-135102
trans-1,2-Dichloroethylene mg/kg dry0.0644 0.0065 0.06538 BRL 58-14199
trans-1,3-Dichloropropylene mg/kg dry0.0562 0.0065 0.06538 BRL 41-12486
Trichloroethylene mg/kg dry0.0645 0.0065 0.06538 BRL 38-16499
Trichlorofluoromethane mg/kg dry0.0600 0.013 0.06538 BRL 30-15792
Vinyl acetate mg/kg dry0.0109 0.013 0.06538 BRL M, J61-15417
Vinyl chloride mg/kg dry0.0609 0.013 0.06538 BRL 40-15693
Xylenes, total mg/kg dry0.171 0.020 0.1961 BRL 36-14887
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10753.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9849.1
ug/L 50.00 76-129Surrogate: Toluene-d8 11356.5
Matrix Spike Dup (P1A0633-MSD1)Prepared & Analyzed: 01/14/21 Source: 1010203-06
1,1,1,2-Tetrachloroethane mg/kg dry0.0604 0.0065 0.06538 BRL 1560-12092 0.09
1,1,1-Trichloroethane mg/kg dry0.0678 0.0065 0.06538 BRL 2152-139104 6
1,1,2,2-Tetrachloroethane mg/kg dry0.0531 0.0065 0.06538 BRL 2239-13581 14
1,1,2-Trichloroethane mg/kg dry0.0579 0.0065 0.06538 BRL 2144-14089 4
1,1-Dichloroethane mg/kg dry0.0675 0.0065 0.06538 BRL 2159-137103 9
1,1-Dichloroethylene mg/kg dry0.0641 0.0065 0.06538 BRL 2254-16298 9
1,1-Dichloropropylene mg/kg dry0.0597 0.0065 0.06538 BRL 1955-13791 7
1,2,3-Trichlorobenzene mg/kg dry0.0337 0.013 0.06538 BRL 4134-12052 3
1,2,3-Trichloropropane mg/kg dry0.0529 0.0065 0.06538 BRL 2545-13981 12
1,2,4-Trichlorobenzene mg/kg dry0.0343 0.013 0.06538 BRL 6235-11652 4
1,2,4-Trimethylbenzene mg/kg dry0.0516 0.0065 0.06538 BRL 2438-14279 8
1,2-Dibromoethane mg/kg dry0.0518 0.0065 0.06538 BRL 1549-13279 5
1,2-Dichlorobenzene mg/kg dry0.0468 0.0065 0.06538 BRL 2142-13072 6
1,2-Dichloroethane mg/kg dry0.0615 0.0065 0.06538 BRL 1351-13194 10
1,2-Dichloropropane mg/kg dry0.0642 0.0065 0.06538 BRL 1655-13898 8
1,3,5-Trimethylbenzene mg/kg dry0.0552 0.0065 0.06538 BRL 2944-14084 9
1,3-Dichlorobenzene mg/kg dry0.0459 0.0065 0.06538 BRL 2441-12970 7
1,3-Dichloropropane mg/kg dry0.0601 0.0065 0.06538 BRL 1553-12992 3
1,4-Dichlorobenzene mg/kg dry0.0450 0.0065 0.06538 BRL 2144-13469 5
2,2-Dichloropropane mg/kg dry0.0622 0.0065 0.06538 BRL 2030-14795 9
2-Chlorotoluene mg/kg dry0.0485 0.0065 0.06538 BRL 2946-13274 8
4-Chlorotoluene mg/kg dry0.0480 0.0065 0.06538 BRL 2344-13573 9
4-Isopropyltoluene mg/kg dry0.0501 0.0065 0.06538 BRL 2232-14477 6
Acetone mg/kg dry0.0746 0.026 0.1308 BRL 4934-14357 13
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0633 - 5035
Matrix Spike Dup (P1A0633-MSD1)Prepared & Analyzed: 01/14/21 Source: 1010203-06
Benzene mg/kg dry0.0652 0.0065 0.06538 BRL 2060-135100 6
Bromobenzene mg/kg dry0.0503 0.0065 0.06538 BRL 2545-13577 9
Bromochloromethane mg/kg dry0.0565 0.0065 0.06538 BRL 1855-13686 11
Bromodichloromethane mg/kg dry0.0658 0.0065 0.06538 BRL 1755-127101 7
Bromoform mg/kg dry0.0537 0.0065 0.06538 BRL 3540-13682 4
Bromomethane mg/kg dry0.0856 0.013 0.06538 BRL 3030-137131 18
Carbon Tetrachloride mg/kg dry0.0643 0.0065 0.06538 BRL 2348-15398 4
Chlorobenzene mg/kg dry0.0586 0.0065 0.06538 BRL 1457-12590 0.6
Chloroethane mg/kg dry0.0603 0.013 0.06538 BRL 4716-17792 9
Chloroform mg/kg dry0.0652 0.0065 0.06538 BRL 1856-137100 8
Chloromethane mg/kg dry0.0946 0.013 0.06538 BRL 2640-145145 0.5
cis-1,2-Dichloroethylene mg/kg dry0.0603 0.0065 0.06538 BRL 2858-14092 8
cis-1,3-Dichloropropylene mg/kg dry0.0556 0.0065 0.06538 BRL 3242-13585 10
Dibromochloromethane mg/kg dry0.0573 0.0065 0.06538 BRL 2449-12788 2
Dichlorodifluoromethane mg/kg dry0.0514 0.013 0.06538 BRL 3725-15179 6
Ethylbenzene mg/kg dry0.0608 0.0065 0.06538 BRL 1944-14493 1
Isopropyl Ether mg/kg dry0.0684 0.0065 0.06538 BRL 1351-155105 7
Isopropylbenzene (Cumene)mg/kg dry0.0552 0.0065 0.06538 BRL 2741-14084 9
m,p-Xylenes mg/kg dry0.110 0.013 0.1308 BRL 2036-14884 0.2
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0505 0.026 0.06538 BRL 4230-14777 6
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0466 0.026 0.06538 BRL 4224-16071 13
Methyl Isobutyl Ketone mg/kg dry0.0613 0.026 0.06538 BRL 4425-16394 11
Methylene Chloride mg/kg dry0.0631 0.0065 0.06538 BRL 1453-14497 9
Methyl-tert-Butyl Ether mg/kg dry0.0666 0.0065 0.06538 BRL 2249-135102 11
Naphthalene mg/kg dry0.0420 0.013 0.06538 BRL 4432-12764 6
n-Butylbenzene mg/kg dry0.0470 0.0065 0.06538 BRL 3923-14872 6
n-Propylbenzene mg/kg dry0.0503 0.0065 0.06538 BRL 2735-14477 9
o-Xylene mg/kg dry0.0613 0.0065 0.06538 BRL 1743-14394 1
sec-Butylbenzene mg/kg dry0.0511 0.0065 0.06538 BRL 2834-14478 9
Styrene mg/kg dry0.0556 0.0065 0.06538 BRL 2842-13285 1
tert-Butylbenzene mg/kg dry0.0546 0.0065 0.06538 BRL 2936-15084 9
Tetrachloroethylene mg/kg dry0.0981 0.0065 0.06538 0.0177 2647-142123 5
Toluene mg/kg dry0.0629 0.0065 0.06538 BRL 2257-13596 6
trans-1,2-Dichloroethylene mg/kg dry0.0571 0.0065 0.06538 BRL 1858-14187 12
trans-1,3-Dichloropropylene mg/kg dry0.0517 0.0065 0.06538 BRL 2041-12479 8
Trichloroethylene mg/kg dry0.0603 0.0065 0.06538 BRL 1838-16492 7
Trichlorofluoromethane mg/kg dry0.0628 0.013 0.06538 BRL 2730-15796 5
Vinyl acetate mg/kg dry0.00881 0.013 0.06538 BRL 35 M, J61-15413 21
Vinyl chloride mg/kg dry0.0576 0.013 0.06538 BRL 3540-15688 5
Xylenes, total mg/kg dry0.172 0.020 0.1961 BRL 2036-14888 0.6
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9447.2
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9145.7
ug/L 50.00 76-129Surrogate: Toluene-d8 11255.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0728 - 5030B
Blank (P1A0728-BLK1)Prepared & Analyzed: 01/18/21
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/L1.68 5.0 J
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL5.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0728 - 5030B
Blank (P1A0728-BLK1)Prepared & Analyzed: 01/18/21
Isopropyl Ether ug/LBRL5.0
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.4
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.3
ug/L 50.00 77-123Surrogate: Toluene-d8 10854.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0728 - 5030B
LCS (P1A0728-BS1)Prepared & Analyzed: 01/18/21
1,1,1,2-Tetrachloroethane ug/L20.6 0.50 20.00 79-134103
1,1,1-Trichloroethane ug/L19.5 0.50 20.00 75-13698
1,1,2,2-Tetrachloroethane ug/L21.5 0.50 20.00 62-127108
1,1,2-Trichloroethane ug/L19.3 0.50 20.00 70-14096
1,1-Dichloroethane ug/L19.4 0.50 20.00 78-13097
1,1-Dichloroethylene ug/L19.6 0.50 20.00 70-15498
1,1-Dichloropropylene ug/L19.4 0.50 20.00 71-13697
1,2,3-Trichlorobenzene ug/L22.2 2.0 20.00 58-144111
1,2,3-Trichloropropane ug/L22.1 1.0 20.00 71-127111
1,2,4-Trichlorobenzene ug/L22.2 1.0 20.00 66-139111
1,2,4-Trimethylbenzene ug/L21.6 0.50 20.00 75-133108
1,2-Dibromo-3-chloropropane ug/L22.5 2.0 20.00 63-134113
1,2-Dibromoethane ug/L21.0 0.50 20.00 77-135105
1,2-Dichlorobenzene ug/L21.7 0.50 20.00 78-128109
1,2-Dichloroethane ug/L19.6 0.50 20.00 68-13198
1,2-Dichloropropane ug/L19.2 0.50 20.00 77-13096
1,3,5-Trimethylbenzene ug/L21.5 0.50 20.00 75-131108
1,3-Dichlorobenzene ug/L21.3 0.50 20.00 77-125107
1,3-Dichloropropane ug/L20.8 0.50 20.00 76-132104
1,4-Dichlorobenzene ug/L21.5 0.50 20.00 75-126107
2,2-Dichloropropane ug/L19.1 2.0 20.00 29-14996
2-Chlorotoluene ug/L21.8 0.50 20.00 74-126109
4-Chlorotoluene ug/L21.3 0.50 20.00 78-129107
4-Isopropyltoluene ug/L21.5 0.50 20.00 69-132108
Acetone ug/L35.2 5.0 40.00 40-16688
Acrolein ug/L38.0 20 40.00 70-13095
Acrylonitrile ug/L39.9 20 40.00 81-127100
Benzene ug/L19.5 0.50 20.00 77-12898
Bromobenzene ug/L21.9 0.50 20.00 78-129110
Bromochloromethane ug/L19.6 0.50 20.00 78-13598
Bromodichloromethane ug/L19.6 0.50 20.00 76-13898
Bromoform ug/L20.8 1.0 20.00 71-135104
Bromomethane ug/L20.1 1.0 20.00 41-168100
Carbon disulfide ug/L19.1 5.0 20.00 59-13595
Carbon Tetrachloride ug/L19.4 0.50 20.00 72-14297
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L18.4 0.50 20.00 57-14292
Chloroform ug/L19.1 0.50 20.00 77-13096
Chloromethane ug/L18.5 0.50 20.00 47-14593
cis-1,2-Dichloroethylene ug/L19.5 0.50 20.00 76-14197
cis-1,3-Dichloropropylene ug/L19.6 0.50 20.00 65-14098
Dibromochloromethane ug/L21.3 0.50 20.00 75-134106
Dibromomethane ug/L19.2 0.50 20.00 76-13896
Dichlorodifluoromethane ug/L18.6 5.0 20.00 28-16393
Ethylbenzene ug/L20.1 0.50 20.00 80-127100
Hexachlorobutadiene ug/L22.1 2.0 20.00 61-134110
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0728 - 5030B
LCS (P1A0728-BS1)Prepared & Analyzed: 01/18/21
Isopropyl Ether ug/L19.9 5.0 20.00 60-15499
Isopropylbenzene (Cumene)ug/L22.2 0.50 20.00 70-130111
m,p-Xylenes ug/L41.9 1.0 40.00 77-133105
Methyl Butyl Ketone (2-Hexanone)ug/L19.2 5.0 20.00 64-13796
Methyl Ethyl Ketone (2-Butanone)ug/L19.5 5.0 20.00 71-13498
Methyl Isobutyl Ketone ug/L18.9 5.0 20.00 69-13495
Methylene Chloride ug/L19.4 1.0 20.00 73-13197
Methyl-tert-Butyl Ether ug/L19.5 0.50 20.00 68-13598
Naphthalene ug/L21.3 1.0 20.00 64-136107
n-Butylbenzene ug/L21.7 1.0 20.00 68-134109
n-Propylbenzene ug/L21.6 0.50 20.00 72-132108
o-Xylene ug/L20.4 0.50 20.00 78-128102
sec-Butylbenzene ug/L21.7 0.50 20.00 71-131109
Styrene ug/L20.5 0.50 20.00 78-129103
tert-Butylbenzene ug/L21.6 0.50 20.00 70-132108
Tetrachloroethylene ug/L21.0 0.50 20.00 80-129105
Toluene ug/L19.1 0.50 20.00 76-13195
trans-1,2-Dichloroethylene ug/L19.8 0.50 20.00 76-13599
trans-1,3-Dichloropropylene ug/L19.5 0.50 20.00 67-14098
Trichloroethylene ug/L19.7 0.50 20.00 77-13398
Trichlorofluoromethane ug/L20.1 0.50 20.00 62-148100
Vinyl acetate ug/L19.4 2.0 20.00 34-16797
Vinyl chloride ug/L18.7 0.50 20.00 57-14193
Xylenes, total ug/L62.3 1.5 60.00 77-133104
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10250.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.7
ug/L 50.00 77-123Surrogate: Toluene-d8 10552.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0728 - 5030B
LCS Dup (P1A0728-BSD1)Prepared & Analyzed: 01/18/21
1,1,1,2-Tetrachloroethane ug/L20.0 0.50 20.00 2079-134100 3
1,1,1-Trichloroethane ug/L18.6 0.50 20.00 2075-13693 5
1,1,2,2-Tetrachloroethane ug/L20.2 0.50 20.00 2062-127101 6
1,1,2-Trichloroethane ug/L18.2 0.50 20.00 2070-14091 6
1,1-Dichloroethane ug/L18.8 0.50 20.00 2078-13094 3
1,1-Dichloroethylene ug/L18.8 0.50 20.00 2070-15494 5
1,1-Dichloropropylene ug/L18.5 0.50 20.00 2071-13693 5
1,2,3-Trichlorobenzene ug/L21.2 2.0 20.00 2058-144106 4
1,2,3-Trichloropropane ug/L21.2 1.0 20.00 2071-127106 4
1,2,4-Trichlorobenzene ug/L21.2 1.0 20.00 2066-139106 5
1,2,4-Trimethylbenzene ug/L20.8 0.50 20.00 2075-133104 4
1,2-Dibromo-3-chloropropane ug/L21.0 2.0 20.00 2063-134105 7
1,2-Dibromoethane ug/L20.4 0.50 20.00 2077-135102 3
1,2-Dichlorobenzene ug/L21.1 0.50 20.00 2078-128105 3
1,2-Dichloroethane ug/L18.9 0.50 20.00 2068-13194 4
1,2-Dichloropropane ug/L18.5 0.50 20.00 2077-13092 4
1,3,5-Trimethylbenzene ug/L21.2 0.50 20.00 2075-131106 1
1,3-Dichlorobenzene ug/L20.8 0.50 20.00 2077-125104 2
1,3-Dichloropropane ug/L20.2 0.50 20.00 2076-132101 3
1,4-Dichlorobenzene ug/L21.2 0.50 20.00 2075-126106 1
2,2-Dichloropropane ug/L18.6 2.0 20.00 2029-14993 3
2-Chlorotoluene ug/L21.2 0.50 20.00 2074-126106 3
4-Chlorotoluene ug/L21.0 0.50 20.00 2078-129105 2
4-Isopropyltoluene ug/L21.1 0.50 20.00 2069-132105 2
Acetone ug/L33.8 5.0 40.00 2040-16685 4
Acrolein ug/L35.8 20 40.00 2070-13089 6
Acrylonitrile ug/L37.2 20 40.00 2081-12793 7
Benzene ug/L18.8 0.50 20.00 2077-12894 4
Bromobenzene ug/L21.4 0.50 20.00 2078-129107 2
Bromochloromethane ug/L18.8 0.50 20.00 2078-13594 4
Bromodichloromethane ug/L18.9 0.50 20.00 2076-13894 4
Bromoform ug/L20.1 1.0 20.00 2071-135100 3
Bromomethane ug/L19.0 1.0 20.00 2041-16895 5
Carbon disulfide ug/L18.3 5.0 20.00 2059-13592 4
Carbon Tetrachloride ug/L18.7 0.50 20.00 2072-14294 4
Chlorobenzene ug/L20.2 0.50 20.00 2078-119101 2
Chloroethane ug/L18.3 0.50 20.00 2057-14292 0.6
Chloroform ug/L18.8 0.50 20.00 2077-13094 2
Chloromethane ug/L18.5 0.50 20.00 2047-14592 0.2
cis-1,2-Dichloroethylene ug/L18.8 0.50 20.00 2076-14194 4
cis-1,3-Dichloropropylene ug/L18.9 0.50 20.00 2065-14095 4
Dibromochloromethane ug/L20.4 0.50 20.00 2075-134102 4
Dibromomethane ug/L18.7 0.50 20.00 2076-13893 3
Dichlorodifluoromethane ug/L17.4 5.0 20.00 2028-16387 6
Ethylbenzene ug/L19.5 0.50 20.00 2080-12798 3
Hexachlorobutadiene ug/L21.4 2.0 20.00 2061-134107 3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P1A0728 - 5030B
LCS Dup (P1A0728-BSD1)Prepared & Analyzed: 01/18/21
Isopropyl Ether ug/L19.2 5.0 20.00 2060-15496 4
Isopropylbenzene (Cumene)ug/L21.3 0.50 20.00 2070-130107 4
m,p-Xylenes ug/L41.2 1.0 40.00 2077-133103 2
Methyl Butyl Ketone (2-Hexanone)ug/L18.6 5.0 20.00 2064-13793 3
Methyl Ethyl Ketone (2-Butanone)ug/L19.3 5.0 20.00 2071-13497 1
Methyl Isobutyl Ketone ug/L17.0 5.0 20.00 2069-13485 11
Methylene Chloride ug/L18.8 1.0 20.00 2073-13194 3
Methyl-tert-Butyl Ether ug/L18.8 0.50 20.00 2068-13594 4
Naphthalene ug/L19.4 1.0 20.00 2064-13697 9
n-Butylbenzene ug/L21.1 1.0 20.00 2068-134106 3
n-Propylbenzene ug/L21.0 0.50 20.00 2072-132105 3
o-Xylene ug/L20.0 0.50 20.00 2078-128100 2
sec-Butylbenzene ug/L21.2 0.50 20.00 2071-131106 2
Styrene ug/L20.1 0.50 20.00 2078-129101 2
tert-Butylbenzene ug/L21.1 0.50 20.00 2070-132106 2
Tetrachloroethylene ug/L20.6 0.50 20.00 2080-129103 2
Toluene ug/L18.3 0.50 20.00 2076-13192 4
trans-1,2-Dichloroethylene ug/L19.0 0.50 20.00 2076-13595 4
trans-1,3-Dichloropropylene ug/L18.8 0.50 20.00 2067-14094 4
Trichloroethylene ug/L19.0 0.50 20.00 2077-13395 3
Trichlorofluoromethane ug/L19.8 0.50 20.00 2062-14899 1
Vinyl acetate ug/L18.8 2.0 20.00 2034-16794 3
Vinyl chloride ug/L18.3 0.50 20.00 2057-14191 2
Xylenes, total ug/L61.1 1.5 60.00 2077-133102 2
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10049.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10652.8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P1A0631 - 3510C MS
Blank (P1A0631-BLK1)Prepared & Analyzed: 01/14/21
1-Methylnaphthalene ug/LBRL10
2-Methylnaphthalene ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL20
Anthracene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Chrysene ug/LBRL10
Dibenzo(a,h)anthracene ug/LBRL20
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Naphthalene ug/LBRL10
Phenanthrene ug/LBRL10
Pyrene ug/LBRL10
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8039.8
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7437.0
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8944.5
LCS (P1A0631-BS1)Prepared & Analyzed: 01/14/21
1-Methylnaphthalene ug/L36.0 10 50.00 41-11972
2-Methylnaphthalene ug/L35.8 10 50.00 40-12172
Acenaphthene ug/L39.5 10 50.00 47-12279
Acenaphthylene ug/L41.7 20 50.00 41-13083
Anthracene ug/L48.5 10 50.00 57-12397
Benzo(a)anthracene ug/L49.2 10 50.00 58-12598
Benzo(a)pyrene ug/L60.6 10 50.00 54-128121
Benzo(b)fluoranthene ug/L51.0 10 50.00 53-131102
Benzo(g,h,i)perylene ug/L51.4 10 50.00 50-134103
Benzo(k)fluoranthene ug/L49.5 10 50.00 57-12999
Chrysene ug/L46.1 10 50.00 59-12392
Dibenzo(a,h)anthracene ug/L34.0 20 50.00 51-13468
Fluoranthene ug/L49.1 10 50.00 57-12898
Fluorene ug/L44.1 10 50.00 52-12488
Indeno(1,2,3-cd)pyrene ug/L51.3 10 50.00 52-134103
Naphthalene ug/L32.8 10 50.00 40-12166
Phenanthrene ug/L45.8 10 50.00 59-12092
Pyrene ug/L50.4 10 50.00 57-126101
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7336.4
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6432.1
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8743.4
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P1A0631 - 3510C MS
LCS Dup (P1A0631-BSD1)Prepared & Analyzed: 01/14/21
1-Methylnaphthalene ug/L24.9 10 50.00 20 D41-11950 36
2-Methylnaphthalene ug/L23.6 10 50.00 20 D40-12147 41
Acenaphthene ug/L28.7 10 50.00 20 D47-12257 32
Acenaphthylene ug/L30.0 20 50.00 20 D41-13060 33
Anthracene ug/L39.0 10 50.00 20 D57-12378 22
Benzo(a)anthracene ug/L41.4 10 50.00 2058-12583 17
Benzo(a)pyrene ug/L50.3 10 50.00 2054-128101 19
Benzo(b)fluoranthene ug/L42.3 10 50.00 2053-13185 19
Benzo(g,h,i)perylene ug/L42.5 10 50.00 2050-13485 19
Benzo(k)fluoranthene ug/L39.2 10 50.00 20 D57-12978 23
Chrysene ug/L39.3 10 50.00 2059-12379 16
Dibenzo(a,h)anthracene ug/L55.0 20 50.00 20 D51-134110 47
Fluoranthene ug/L40.8 10 50.00 2057-12882 18
Fluorene ug/L32.8 10 50.00 20 D52-12466 29
Indeno(1,2,3-cd)pyrene ug/L40.2 10 50.00 20 D52-13480 24
Naphthalene ug/L22.0 10 50.00 20 D40-12144 39
Phenanthrene ug/L36.8 10 50.00 20 D59-12074 22
Pyrene ug/L41.5 10 50.00 2057-12683 19
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 4824.2
ug/L 50.00 SR44-120Surrogate: Nitrobenzene-d5 3919.6
ug/L 50.00 50-134Surrogate: Terphenyl-d14 6934.4
Batch P1A0651 - 3546
Blank (P1A0651-BLK1)Prepared & Analyzed: 01/15/21
1-Methylnaphthalene mg/kg wetBRL0.66
2-Methylnaphthalene mg/kg wetBRL0.66
Acenaphthene mg/kg wetBRL0.66
Acenaphthylene mg/kg wetBRL0.66
Anthracene mg/kg wetBRL0.66
Benzo(a)anthracene mg/kg wetBRL0.66
Benzo(a)pyrene mg/kg wetBRL0.66
Benzo(b)fluoranthene mg/kg wetBRL0.66
Benzo(g,h,i)perylene mg/kg wetBRL0.66
Benzo(k)fluoranthene mg/kg wetBRL0.66
Chrysene mg/kg wetBRL0.66
Dibenzo(a,h)anthracene mg/kg wetBRL0.66
Fluoranthene mg/kg wetBRL0.66
Fluorene mg/kg wetBRL0.66
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.66
Naphthalene mg/kg wetBRL0.66
Phenanthrene mg/kg wetBRL0.66
Pyrene mg/kg wetBRL0.66
mg/kg wet 1.672 44-115Surrogate: 2-Fluorobiphenyl 1061.77
mg/kg wet 1.672 37-122Surrogate: Nitrobenzene-d5 981.63
mg/kg wet 1.672 54-127Surrogate: Terphenyl-d14 1031.72
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P1A0651 - 3546
LCS (P1A0651-BS1)Prepared & Analyzed: 01/15/21
1-Methylnaphthalene mg/kg wet1.65 0.66 1.674 40-11999
2-Methylnaphthalene mg/kg wet1.63 0.66 1.674 38-12298
Acenaphthene mg/kg wet1.68 0.66 1.674 40-123100
Acenaphthylene mg/kg wet1.78 0.66 1.674 32-132106
Anthracene mg/kg wet1.85 0.66 1.674 47-123111
Benzo(a)anthracene mg/kg wet1.80 0.66 1.674 49-126108
Benzo(a)pyrene mg/kg wet2.27 0.66 1.674 A45-129135
Benzo(b)fluoranthene mg/kg wet1.94 0.66 1.674 45-132116
Benzo(g,h,i)perylene mg/kg wet1.91 0.66 1.674 43-134114
Benzo(k)fluoranthene mg/kg wet1.79 0.66 1.674 47-132107
Chrysene mg/kg wet1.76 0.66 1.674 50-124105
Dibenzo(a,h)anthracene mg/kg wet1.25 0.66 1.674 45-13475
Fluoranthene mg/kg wet1.84 0.66 1.674 50-127110
Fluorene mg/kg wet1.77 0.66 1.674 43-125106
Indeno(1,2,3-cd)pyrene mg/kg wet1.94 0.66 1.674 45-133116
Naphthalene mg/kg wet1.60 0.66 1.674 35-12396
Phenanthrene mg/kg wet1.77 0.66 1.674 50-121106
Pyrene mg/kg wet1.88 0.66 1.674 47-127112
mg/kg wet 1.674 44-115Surrogate: 2-Fluorobiphenyl 991.65
mg/kg wet 1.674 37-122Surrogate: Nitrobenzene-d5 891.50
mg/kg wet 1.674 54-127Surrogate: Terphenyl-d14 961.61
Matrix Spike (P1A0651-MS1)Prepared & Analyzed: 01/15/21 Source: 1010203-14
1-Methylnaphthalene mg/kg dry1.63 0.83 2.100 BRL 40-11978
2-Methylnaphthalene mg/kg dry1.63 0.83 2.100 BRL 38-12277
Acenaphthene mg/kg dry1.68 0.83 2.100 0.0273 40-12379
Acenaphthylene mg/kg dry1.74 0.83 2.100 BRL 32-13283
Anthracene mg/kg dry1.87 0.83 2.100 0.0971 47-12384
Benzo(a)anthracene mg/kg dry1.96 0.83 2.100 0.286 49-12680
Benzo(a)pyrene mg/kg dry2.46 0.83 2.100 0.249 45-129105
Benzo(b)fluoranthene mg/kg dry2.15 0.83 2.100 0.305 45-13288
Benzo(g,h,i)perylene mg/kg dry1.95 0.83 2.100 0.137 43-13486
Benzo(k)fluoranthene mg/kg dry1.89 0.83 2.100 0.103 47-13285
Chrysene mg/kg dry1.99 0.83 2.100 0.262 50-12482
Dibenzo(a,h)anthracene mg/kg dry1.06 0.83 2.100 0.0383 45-13449
Fluoranthene mg/kg dry2.32 0.83 2.100 0.587 50-12782
Fluorene mg/kg dry1.75 0.83 2.100 0.0290 43-12582
Indeno(1,2,3-cd)pyrene mg/kg dry1.94 0.83 2.100 0.154 45-13385
Naphthalene mg/kg dry1.55 0.83 2.100 BRL 35-12374
Phenanthrene mg/kg dry2.04 0.83 2.100 0.426 50-12177
Pyrene mg/kg dry2.29 0.83 2.100 0.484 47-12786
mg/kg dry 2.100 44-115Surrogate: 2-Fluorobiphenyl 751.58
mg/kg dry 2.100 37-122Surrogate: Nitrobenzene-d5 661.38
mg/kg dry 2.100 54-127Surrogate: Terphenyl-d14 751.57
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P1A0651 - 3546
Matrix Spike Dup (P1A0651-MSD1)Prepared & Analyzed: 01/15/21 Source: 1010203-14
1-Methylnaphthalene mg/kg dry1.92 0.83 2.107 BRL 2040-11991 16
2-Methylnaphthalene mg/kg dry1.92 0.83 2.107 BRL 2038-12291 16
Acenaphthene mg/kg dry1.89 0.83 2.107 0.0273 2040-12388 12
Acenaphthylene mg/kg dry2.10 0.83 2.107 BRL 2032-132100 19
Anthracene mg/kg dry2.17 0.83 2.107 0.0971 2047-12398 15
Benzo(a)anthracene mg/kg dry2.88 0.83 2.107 0.286 20 D49-126123 38
Benzo(a)pyrene mg/kg dry3.68 0.83 2.107 0.249 20 D, M45-129163 40
Benzo(b)fluoranthene mg/kg dry3.95 0.83 2.107 0.305 20 D, M45-132173 59
Benzo(g,h,i)perylene mg/kg dry2.79 0.83 2.107 0.137 20 D43-134126 36
Benzo(k)fluoranthene mg/kg dry2.38 0.83 2.107 0.103 20 D47-132108 23
Chrysene mg/kg dry3.53 0.83 2.107 0.262 20 D, M50-124155 56
Dibenzo(a,h)anthracene mg/kg dry1.32 0.83 2.107 0.0383 20 D45-13461 22
Fluoranthene mg/kg dry5.89 0.83 2.107 0.587 20 D, M50-127251 87
Fluorene mg/kg dry2.07 0.83 2.107 0.0290 2043-12597 17
Indeno(1,2,3-cd)pyrene mg/kg dry2.78 0.83 2.107 0.154 20 D45-133125 36
Naphthalene mg/kg dry1.83 0.83 2.107 BRL 2035-12387 17
Phenanthrene mg/kg dry5.92 0.83 2.107 0.426 20 D, M50-121261 97
Pyrene mg/kg dry5.26 0.83 2.107 0.484 20 D, M47-127227 79
mg/kg dry 2.107 44-115Surrogate: 2-Fluorobiphenyl 811.70
mg/kg dry 2.107 37-122Surrogate: Nitrobenzene-d5 731.53
mg/kg dry 2.107 54-127Surrogate: Terphenyl-d14 791.67
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Batch P1A0718 - 3550C GC
Blank (P1A0718-BLK1)Prepared & Analyzed: 01/19/21
Aroclor 1016 mg/kg wetBRL0.051
Aroclor 1221 mg/kg wetBRL0.10
Aroclor 1232 mg/kg wetBRL0.10
Aroclor 1242 mg/kg wetBRL0.051
Aroclor 1248 mg/kg wetBRL0.051
Aroclor 1254 mg/kg wetBRL0.051
Aroclor 1260 mg/kg wetBRL0.051
mg/kg wet 0.03376 36-182Surrogate: Tetrachloro-m-xylene 1040.0351
mg/kg wet 0.03376 34-182Surrogate: Decachlorobiphenyl 840.0284
LCS (P1A0718-BS1)Prepared & Analyzed: 01/19/21
Aroclor 1016 mg/kg wet0.299 0.051 0.3372 64-15189
Aroclor 1221 mg/kg wetBRL0.10 50-150
Aroclor 1232 mg/kg wetBRL0.10 50-150
Aroclor 1242 mg/kg wetBRL0.051 50-150
Aroclor 1248 mg/kg wetBRL0.051 50-150
Aroclor 1254 mg/kg wetBRL0.051 50-150
Aroclor 1260 mg/kg wet0.259 0.051 0.3372 45-16677
mg/kg wet 0.03372 36-182Surrogate: Tetrachloro-m-xylene 970.0327
mg/kg wet 0.03372 34-182Surrogate: Decachlorobiphenyl 840.0283
LCS Dup (P1A0718-BSD1)Prepared & Analyzed: 01/19/21
Aroclor 1016 mg/kg wet0.272 0.050 0.3357 5064-15181 10
Aroclor 1221 mg/kg wetBRL0.10 5050-150
Aroclor 1232 mg/kg wetBRL0.10 5050-150
Aroclor 1242 mg/kg wetBRL0.050 5050-150
Aroclor 1248 mg/kg wetBRL0.050 5050-150
Aroclor 1254 mg/kg wetBRL0.050 5050-150
Aroclor 1260 mg/kg wet0.267 0.050 0.3357 5045-16680 3
mg/kg wet 0.03357 36-182Surrogate: Tetrachloro-m-xylene 1020.0342
mg/kg wet 0.03357 34-182Surrogate: Decachlorobiphenyl 830.0279
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Gasoline Range Organics by GC/FID - Quality Control
Batch P1A0632 - 5030B
Blank (P1A0632-BLK1)Prepared: 01/14/21 Analyzed: 01/15/21
Gasoline Range Organics mg/kg wetBRL5.0
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1185.90
LCS (P1A0632-BS1)Prepared: 01/14/21 Analyzed: 01/15/21
Gasoline Range Organics mg/kg wet66.2 5.0 50.00 41-138132
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1236.15
Matrix Spike (P1A0632-MS1)Prepared: 01/14/21 Analyzed: 01/15/21 Source: 1010203-01
Gasoline Range Organics mg/kg dry87.9 7.4 74.45 BRL 41-138118
mg/kg dry 7.445 50-137Surrogate: a,a,a-Trifluorotoluene 1108.19
Matrix Spike Dup (P1A0632-MSD1)Prepared: 01/14/21 Analyzed: 01/15/21 Source: 1010203-01
Gasoline Range Organics mg/kg dry87.9 7.4 74.45 BRL 3441-138118 0
mg/kg dry 7.445 50-137Surrogate: a,a,a-Trifluorotoluene 1138.41
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Diesel Range Organics by GC/FID - Quality Control
Batch P1A0652 - 3546
Blank (P1A0652-BLK1)Prepared & Analyzed: 01/15/21
Diesel Range Organics mg/kg wetBRL7.1
mg/kg wet 1.350 31-123Surrogate: o-Terphenyl 941.26
LCS (P1A0652-BS1)Prepared & Analyzed: 01/15/21
Diesel Range Organics mg/kg wet60.3 7.1 67.73 46-12689
mg/kg wet 1.355 31-123Surrogate: o-Terphenyl 851.15
Matrix Spike (P1A0652-MS1)Prepared & Analyzed: 01/15/21 Source: 1010203-10
Diesel Range Organics mg/kg dry83.1 9.6 91.29 BRL 50-11791
mg/kg dry 1.826 31-123Surrogate: o-Terphenyl 851.56
Matrix Spike Dup (P1A0652-MSD1)Prepared & Analyzed: 01/15/21 Source: 1010203-10
Diesel Range Organics mg/kg dry75.7 9.5 90.60 BRL 2450-11784 9
mg/kg dry 1.812 31-123Surrogate: o-Terphenyl 741.35
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 69
1/20/21
Level II QC Report
2923 South Tryon St. Ste 100
Project: HNY-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Bo Cappleman
Work Order: 1010203
Time Submitted: 1/13/2021 9:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P1A0671 - Solids, Dry Weight
Duplicate (P1A0671-DUP1)Prepared: 01/15/21 Analyzed: 01/18/21 Source: 1010203-09
% Solids % by Weight77.1 0.100 76.9 200.3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 69
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P1A06521010203-01 01/15/21 8:4029.57 1g mL
P1A06521010203-02 01/15/21 8:4029.5 1g mL
P1A06521010203-08 01/15/21 8:4029.76 1g mL
P1A06521010203-09 01/15/21 8:4029.52 1g mL
P1A06521010203-10 01/15/21 8:4030.22 1g mL
P1A06521010203-11 01/15/21 8:4029.99 1g mL
P1A06521010203-12 01/15/21 8:4030.02 1g mL
P1A06521010203-13 01/15/21 8:4029.56 1g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P1A06321010203-01 01/14/21 9:545.54 5mL mL
P1A06321010203-02 01/14/21 9:545.47 5mL mL
P1A06321010203-08 01/14/21 9:546.15 5mL mL
P1A06321010203-09 01/14/21 9:544.97 5mL mL
P1A06321010203-10 01/14/21 9:545.08 5mL mL
P1A06321010203-11 01/14/21 9:544.89 5mL mL
P1A06321010203-12 01/14/21 9:545.63 5mL mL
P1A06321010203-13 01/14/21 9:547.34 5mL mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P1A06711010203-01 01/15/21 15:3530 30g g
P1A06711010203-02 01/15/21 15:3530 30g g
P1A06711010203-03 01/15/21 15:3530 30g g
P1A06711010203-04 01/15/21 15:3530 30g g
P1A06711010203-05 01/15/21 15:3530 30g g
P1A06711010203-06 01/15/21 15:3530 30g g
P1A06711010203-07 01/15/21 15:3530 30g g
P1A06711010203-08 01/15/21 15:3530 30g g
P1A06711010203-09 01/15/21 15:3530 30g g
P1A06711010203-10 01/15/21 15:3530 30g g
P1A06711010203-11 01/15/21 15:3530 30g g
P1A06711010203-12 01/15/21 15:3530 30g g
P1A06711010203-13 01/15/21 15:3530 30g g
P1A06711010203-14 01/15/21 15:3530 30g g
Prep Method: 3550C GC
Lab Number Batch Date/TimeInitialFinal
P1A07181010203-03 01/19/21 7:4529.71 10g mL
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P1A06311010203-15 01/14/21 9:359601mL mL
P1A06311010203-16 01/14/21 9:359601mL mL
P1A06311010203-17 01/14/21 9:354701mL mL
P1A06311010203-18 01/14/21 9:359701mL mL
P1A06311010203-19 01/14/21 9:351000 1mL mL
P1A06311010203-20 01/14/21 9:359401mL mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 69
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P1A06511010203-04 01/15/21 8:1529.8 1g mL
P1A06511010203-06 01/15/21 8:1529.68 1g mL
P1A06511010203-07 01/15/21 8:1530.14 1g mL
P1A06511010203-14 01/15/21 8:1529.78 1g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P1A07281010203-15 01/18/21 10:2410 10mL mL
P1A07281010203-16 01/18/21 10:2410 10mL mL
P1A07281010203-16 01/18/21 10:2410 10mL mL
P1A07281010203-17 01/18/21 10:2410 10mL mL
P1A07281010203-18 01/18/21 10:2410 10mL mL
P1A07281010203-19 01/18/21 10:2410 10mL mL
P1A07281010203-20 01/18/21 10:2410 10mL mL
P1A07281010203-21 01/18/21 10:2410 10mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P1A06331010203-05 01/14/21 9:554.81 5g mL
P1A06331010203-06 01/14/21 9:556.55 5g mL
P1A06331010203-07 01/14/21 9:556.67 5g mL
P1A06331010203-14 01/14/21 9:556.17 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 67 of 69
Page 68 of 69
Page 69 of 69
SanAir ID#: 21002277
Project #: HNY-001
Project Name:
Report Date: 1/19/2021
Analysis Report
prepared for
Hart & Hickman
Page 1 of 5
Dear Sean Horgan,
We at SanAir would like to thank you for the work you recently submitted. The 4 sample(s) were received on Monday,
January 18, 2021 via FedEx. The final report(s) is enclosed for the following sample(s): 001A, 001B, 002A, 002B.
These results only pertain to this job and should not be used in the interpretation of any other job. This report is only
complete in its entirety. Refer to the listing below of the pages included in a complete final report.
Sincerely,
Sandra Sobrino
Asbestos & Materials Laboratory Manager
SanAir Technologies Laboratory
Final Report Includes:
- Cover Letter
- Analysis Pages
- Disclaimers and Additional Information
Sample conditions:
- 4 samples in Good condition.
1551 Oakbridge Dr. Suite B, Powhatan, VA 23139 | 804.897.1177 | Fax: [phone] | www.SanAir.com | [e-mail]
HNY-001Project Number:
P.O. Number:
Project Name:
1/12/2021Collected Date:
1/18/2021 9:30:00 AMReceived Date:
1/19/2021 5:33:50 PM
21002277
SanAir ID Number
FINAL REPORT
Hart & HickmanName:
Address:2923 South Tryon Street
Suite 100
Charlotte, NC 28203
704-586-0007Phone:
Page 2 of 5
Analyst: Vaughan, Nathaniel
Asbestos Bulk PLM EPA 600/R-93/116
Stereoscopic Components
SanAir ID / Description Appearance % Fibrous % Non-fibrous Asbestos Fibers
001A / 21002277-001
Cementitious Building Material
Debris Pile
Gray
Non-Fibrous
Heterogeneous
45% Cellulose 55% Other None Detected
001B / 21002277-002
Cementitious Building Material
Debris Pile
Gray
Non-Fibrous
Heterogeneous
45% Cellulose 55% Other None Detected
002A / 21002277-003
Building Material Debris Pile
Black
Fibrous
Heterogeneous
85% Cellulose 15% Other None Detected
002B / 21002277-004
Building Material Debris Piles
Black
Fibrous
Heterogeneous
85% Cellulose 15% Other None Detected
Analyst:
Analysis Date:1/19/2021 Date:1/19/2021
Approved Signatory:
HNY-001Project Number:
P.O. Number:
Project Name:
1/12/2021Collected Date:
1/18/2021 9:30:00 AMReceived Date:
1/19/2021 5:33:50 PM
21002277
SanAir ID Number
FINAL REPORT
Hart & HickmanName:
Address:2923 South Tryon Street
Suite 100
Charlotte, NC 28203
704-586-0007Phone:
Page 3 of 5
Disclaimer
This report is the sole property of the client named on the SanAir Technologies Laboratory chain-
of-custody (COC). Results in the report are confidential information intended only for the use by the customer listed on the COC. Neither results nor reports will be discussed with or released to
any third party without our client's written permission. The final report shall not be reproduced except in full without written approval of the laboratory to assure that parts of the report are not
taken out of context. The information provided in this report applies only to the samples submitted and is relevant only for the date, time, and location of sampling. The accuracy of the
results is dependent upon the client’s sampling procedure and information provided to the
laboratory by the client. SanAir assumes no responsibility for the sampling procedure and will
provide evaluation reports based solely on the sample(s) in the condition in which they arrived at the laboratory and information provided by the client on the COC, such as: project number,
project name, collection dates, po number, special instructions, samples collected by, sample numbers, sample identifications, sample type, selected analysis type, flow rate, total volume or
area, and start stop times that may affect the validity of the results in this report. Samples were received in good condition unless otherwise noted on the report. SanAir assumes no
responsibility or liability for the manner in which the results are used or interpreted. This report does not constitute and shall not be used to claim product certification, approval, or endorsement
by NVLAP, NIST, or any other U.S. governmental agencies and may not be certified by every local, state, and federal regulatory agencies.
Samples are held for a period of 60 days. Fibers smaller than 5 microns cannot be seen with this
method due to scope limitations.
For NY state samples, method EPA 600/M4-82-020 is performed.
NYELAP Disclaimer:
Polarized- light microscopy is not consistently reliable in detecting asbestos in floor covering and
similar non-friable organically bound materials. Quantitative transmission electron microscopy is
currently the only method that can be used to determine if this material can be considered or
treated as non-asbestos containing.
Asbestos Certifications
NVLAP lab code 200870-0
City of Philadelphia: ALL-460
PA Department of Environmental Protection Number: 68-05397
California License Number: 2915
Colorado License Number: AL-23143
Connecticut License Number: PH-0105
Massachusetts License Number: AA000222
Maine License Number: LB-0075, LA-0084
New York ELAP lab ID: 11983
Rhode Island License Number: PCM00126, PLM00126, TEM00126
Texas Department of State Health Services License Number: 300440
Commonwealth of Virginia 3333000323
Washington State License Number: C989
West Virginia License Number: LT000616
Vermont License: AL166318 Louisiana Department of Environmental Quality: 212253, Cert 05088
Revision Date: 8/14/2020
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Appendix D DEQ Risk Calculator Input/Output Forms
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
TMW-2
North Carolina Department of Environmental Quality
Risk Calculator
Former Pharr Yarn Mills
700 West 1st Street, Lowell, NC
July 2020
May 2020 EPA RSL Table
Prepared By:Bo Cappleman
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID:
Exposure Unit ID: TMW-2
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2020Basis: May 2020 EPA RSL TableSite ID: Exposure Unit ID: TMW-2Description of Exposure Point Concentration Selection:Exposure Point Concentration (ug/L)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion2100 127-18-4 Tetrachloroethylene ug/L7.9 79-01-6 Trichloroethylene ug/LInput Form 2BGroundwater Exposure Point Concentration TableNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID:
Exposure Unit ID: TMW-2
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 1.5E-04 3.8E+01 YES
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 3.3E-05 9.0E+00 YES
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Groundwater to Indoor Air
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID:
Exposure Unit ID: TMW-2
CAS # Chemical Name:
Groundwater Concentration
(ug/L)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air Conc. for
Non-Carcinogens
@ THQ = 0.2
Calculated Carcinogenic
Risk
Calculated
Non-Carcinogenic
Hazard
Quotient
127-18-4 Tetrachloroethylene 2100 1519.623876 1.1E+01 8.3E+00 1.4E-04 3.6E+01
79-01-6 Trichloroethylene 7.9 3.181316435 4.8E-01 4.2E-01 6.7E-06 1.5E+00
Cumulative:1.5E-04 3.8E+01
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3A
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Groundwater to Indoor Air
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID:
Exposure Unit ID: TMW-2
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
127-18-4 Tetrachloroethylene 2100 1519.623876 4.7E+01 3.5E+01 3.2E-05 8.7E+00
79-01-6 Trichloroethylene 7.9 3.181316435 3.0E+00 1.8E+00 1.1E-06 3.6E-01
Cumulative: 3.3E-05 9.0E+00
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3D
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator