25094_Mock Judson Mill_Supplimental Sampling_20221003

SUPPLEMENTAL SOIL AND GROUNDWATER
SAMPLING REPORT

Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
Brownfields Project Number: 25094-21-041

Submitted By
Atlantic Shores Environmental Services, Ltd.
ASE License No. C-4767
September 30, 2022
Cheryl J. Moody, PE, REM
Principal Engineer

Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

i
TABLE OF CONTENTS

1.0 BACKGROUND ........................................................................................................................... 1
2.0 SAMPLING METHODOLOGY ................................................................................................. 3
2.1 Soil Samples ............................................................................................................................... 3
2.2 Groundwater Samples .............................................................................................................. 3
3.0 RESULTS ...................................................................................................................................... 4
3.1 Soil Sampling ........................................................................................................................... 4
3.2 Groundwater Sampling .......................................................................................................... 4
4.0 CONCLUSIONS ........................................................................................................................... 4
4.1 Soil Sampling ........................................................................................................................... 4
4.3 Groundwater Sampling .......................................................................................................... 4

Attachments:
Figures:
Figure 1 – Site Location Map
Figure 2A – Soil Sampling Locations
Figure 2B – Soil Sampling Locations
Figure 2C – Soil Sampling Locations
Figure 2D – Soil Sampling Locations
Figure 2E – Soil Sampling Locations
Figure 3 – Groundwater Sampling Locations
Figure 4 – Soil Pile Location Map
Tables:
Table 1: Soil Sample Analytical Results
Table 2: Groundwater Well Purge Data
Table 3: Groundwater Analytical Results

Appendices:
Appendix A – Photographs
Appendix B – Laboratory Data
Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

1

1.0 BACKGROUND

Atlantic Shores Environmental Services, Ltd. (ASE) is pleased to provide this Supplemental Soil and
Groundwater Sampling Report for the 2610 Oakland Avenue Brownfield site (Refer to Figure 1).

The site consists of approximately 8.67 acres and encompasses all of the property in the block between
Oakland Avenue, South Lindell Street, Hiatt Street and Harold Street in Greensboro, North Carolina. The
site is developed with a vacant two story mill building, its associated boiler room building, and a smoke
stack. The south half of the property is currently undeveloped. The site buildings are being redeveloped
into a 173 unit apartment complex, which will ultimately encompass the northern two thirds of the property.
The existing main mill building is constructed primarily on a slab. However, a small basement is located in
the northwest corner of the c.1928 portion of the building. The boiler room is also constructed on a slab
foundation. However, this structure is partially sub grade and is currently flooded with approximately 4 feet
of water. This water was sampled in two locations prior to the site being admitted into the Brownfield
Program. Target constituents above unrestricted use were not identified in the standing water.

The planned amenities include a swimming pool, outdoor lawn and grilling area and a dog park. The dog
park will be covered with turf to prevent digging. Paved parking will be located both north and south of the
buildings.

Assessment of the site, prior to inclusion of the site into the Brownfields program include:
Environmental Reports
Report Prepared by Date
Closure Report for Kayser-Roth
Corporation
Four Seasons
Industrial Service, Inc. September 30, 1991
Phase I Environmental Site Assessment Swift Creek
Environmental, Inc. March 23, 2017
Subsurface Investigation Report Swift Creek
Environmental, Inc. May 19, 2017
Phase I Environmental Site Assessment Swift Creek
Environmental, Inc.
April 2, 2020
Boiler Room Water Sampling
(November 3, 2021)
Atlantic Shores Environmental
Services Ltd. September 20, 2022
Phase I Environmental Site Assessment
Report
Atlantic Shores Environmental
Services Ltd. December 2, 2021
Phase II Environmental
Assessment/Remediation Investigation
Report
Swift Creek
Environmental, Inc. December 6, 2021

These assessments occurred prior to receiving eligibility into the Brownfield Program.
September 1991 (UST Removal) - Three fuel oil USTs and one Varsol UST have been removed from the
site. Approximately 1,200 tons of fuel oil impacted soil was excavated from the fuel oil tank pits. However,
elevated oil & grease remain on the site in this area at a depth of 16-17 feet. Testing from beneath the Varsol
tank did not identify impacts.
Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

2
May 2017 – Six soil borings, four of which were completed as temporary monitoring wells were advanced
at the site. Chromium was identified in one of the three analyzed samples and lead, silver and TPH- ORO
were identified in one of the three soil samples above residential PSRGs. Benzo(a)anthracene and 1-
Methylnaphthalene were also identified in two of the collected soil samples above residential PSRGs.
Barium, chromium and lead were identified in one of the two groundwater samples that were analyzed for
metals above 2L standards.
Two sub slab soil vapor samples were collected within the main building. Results of the analyses did not
identify VOCs above NCDEQ Residential Sub Slab SCLs (Soil Gas Screening Levels).
November 2021: Two samples were collected from the four foot of water located within the boiler room. These
samples were analyzed for VOCs, SVOCs and RCRA 8 metals. Two volatile organic compounds (VOCs) and
one metal were identified in the samples. However, each identified constituent was below their respective
NCDEQ Groundwater Quality Standards (2L).

December 2021: A total of 32 soil borings were advanced on the property at locations of concern identified
during previous assessment activities. Volatile Organic Compounds (VOCs) were detected in soil samples.
Several PAHs, metals, and PCB congeners were detected at concentrations above Residential PSRGs. A
risk assessment was performed by Swift Creek, which indicated that soil concentrations identified at the
site do not pose an unacceptable risk to a residential receptor under the direct contact soil pathway.

Groundwater investigation activities consisted of installation and sampling of 11 groundwater
monitoring wells at the site. The results of the sampling and analyses did not identify exceedances of the 2L
Standards. Swift Creek preformed a NCDEQ risk evaluation of detected constituents which did not indicate
unacceptable risk for direct contact for a residential receptor.

Sub-slab soil vapor samples were collected from eight locations within the main mill building. Swift Creek
reported naphthalene was detected at a concentration above its Residential SGSL in five of the sub-slab soil
gas samples. A risk assessment was completed by Swift Creek using the sub-slab soil gas data. The
results showed that neither the target carcinogenic risk nor the target hazard index were exceeded. Based on
these results, vapor intrusion into the main building is not anticipated to pose an unacceptable risk to
receptors under a residential use scenario. To evaluate vapor intrusion risk in the boiler room, and as an additional
line of evidence for vapor intrusion risk in the main building, VOC groundwater data was used to evaluate
the potential for vapor intrusion risk. The results indicated that the potential for vapor intrusion in the
main building and boiler room is not anticipated to pose an unacceptable risk to residential receptors.

Cumulative site-wide risk was calculated by summing the risks associated with the soil direct use,
groundwater direct use, and vapor intrusion pathways. The results indicate that site-wide risks are within
allowable risk limits under a residential use scenario.

Data gaps identified in the historic sampling included the lack of soil and groundwater samples analyzed
for hexavalent chromium, and a lack of SVOC and VOC analysis from three of the on-site wells.

Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

3
2.0 SAMPLING METHODOLOGY

Sampling was conducted in accordance with the Draft Work Plan for the site dated September 27, 2022. This
report discusses the assessment of a portion of the work outlined in the Draft Work Plan. The remaining
assessment is pending the Work Plan approval.

2.1 Soil Samples

The redevelopment is utilizing the existing site structures which is slab on grade with the exception of a
small basement in the main mill portion of the site. Due to schedule constraints, the interior of the
redevelopment project has been started. The concrete cutting required for the utility trenching for the
redevelopment within the ground floor of the main mill was conducted between July 11, 2022 and July 22,
2022. The concrete was saw cut, then removed with a bobcat. ASE collected soil samples SS-1 through
SS-11 on July 15, 2022 and collected soil sampled SS-12 through SS-14 on July 22, 2022.

Samples for laboratory analysis were collected from the soil just beneath the removed concrete slab in the
sampling locations identified on Figure 2A through 2E. Their GPS coordinates have been listed in Table 1.
The samples were collected using a decontaminated stainless steel spoon.

The samples were analyzed for volatile organic compounds (VOCs) and semi volatile compounds (SVOCs)
by EPA Methods 8260 and 8270, respectively. The samples were also analyzed for the presence of
hexavalent chromium by EPA Method 7199. The soil samples were submitted to Pace Analytical
Laboratory located at 9800 Kincey Avenue, Suite 100 in Huntersville, North Carolina under the chain of
custody protocol.

Sample collection was conducted in accordance with the NCDEQ Inactive Hazardous Sites
Program Guidelines for Assessment and Cleanup (July 2021). The samples will be compared to the North
Carolina DEQ Preliminary Soil Remediation Goals (PSRG, dated July 2022).

2.2 Groundwater Samples

The existing permanent groundwater wells are constructed with 1 inch PVC. However, the Swift Creek
reports identify them as 2 inch wells. Four (4) to five (5) well volumes (approximately 0.042 gallons per
foot of 1-inch well is one well volume) were purged prior to sampling. Purge water was placed in a labelled
55-gallon drum. The purging was completed with low flow peristaltic pump and dedicated tubing. The
Turbidity (NTUs) was recorded after each well volume. In addition to turbidity, conductivity and pH
readings were monitored at each well volume during purging to document stabilization readings. Turbidity
readings did not go down to 10 NTU or less after five well volumes. Therefore, the development stopped
based on the stabilization of the parameters. The samples were collected using a low flow peristaltic pump
and dedicated tubing. The location of these wells are illustrated on Figure 3.

The samples from MW-2 and MW-3 were analyzed the presence of hexavalent chromium by EPA Method
7199. The samples from MW-6, MW-7 and MW-8 were analyzed for volatile organic compounds (VOCs)
and semi volatile compounds (SVOCs) by EPA Methods 8260 and 8270, respectively. The samples were
also analyzed for the presence of hexavalent chromium by EPA Method 7199. The groundwater samples
were submitted to Pace Analytical Laboratory located at 9800 Kincey Avenue, Suite 100 in Huntersville,
North Carolina under the chain of custody protocol.

Due to a sampling oversight, neither a duplicate, nor a trip blank was submitted to the laboratory. This was
Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

4
documented in the Draft Work Plan.
3.0 RESULTS

3.1 Soil Sampling

A photoionization detector was used to field screen soils from the sampling. Since borings were not
advanced, boring logs have not been included in this report. Soils beneath the slab were uniform and
consists of red clay with trace fine sand and silt. A positive response (<1 ppm) was not recorded by the PID
from the collected samples. Soil sampling results have been included in Table 1. Copies of the lab data
sheets have been included in Appendix B.

Several VOCs and metals were identified in the soil samples. However, the only target VOC and metal that
were identified above PSRGs include methylene chloride (in seven (7) of the 14 samples), and hexavalent
chromium (in three (3) of the 14 samples). The soils were below residential PSRGs, but above protection
of groundwater PSRGs.

3.2 Groundwater Sampling

ASE collected groundwater samples from MW-2, MW-3, MW-6, MW-7, and MW-8 on July 22, 2022.
Baseline water levels were recorded prior to purging. Baseline water levels and parameter values are listed
in Table 2.

Groundwater impacts above established NCAC 2L Groundwater Standards were not identified in the
collected samples. Refer to Table 3 for a summary of the groundwater data. Copies of the lab data sheets
have been included in Appendix B.

4.0 CONCLUSIONS

4.1 Soil Sampling

Methylene chloride was identified in seven (7) of the 14 samples above the protection of groundwater
PSRGs. The methylene chloride has been tagged by the lab a potential lab contaminant.

Hexavalent chromium was identified in three (3) of the 14 samples above the protection of groundwater
PSRGs.

As of the date of this report, the excess soil from the interior trenching is being staged on-site as illustrated
on Figure 4. The piles are covered and secured with plastic. ASE requests permission to spread the excess
soils under the proposed impervious areas of the site or be placed on the southern area of the site.

4.3 Groundwater Sampling

Target analytes were not identified in the collected groundwater samples above 2L Standards. Since the
purge water was placed in drums used for the Swift Creeks groundwater and soil sampling, the drums will
Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

5
be disposed of under manifest.

ASE requests permission to abandon the on-site monitoring wells. The wells will be abandoned by a North
Carolina Certified well driller in accordance with State requirements.
Supplemental Soil and Groundwater Sampling Report September 20, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1487

FIGURES

Figure 1 – Site Location Map
Figure 2A – Soil Sampling Locations
Figure 2B – Soil Sampling Locations
Figure 2C – Soil Sampling Locations
Figure 2D – Soil Sampling Locations
Figure 2E – Soil Sampling Locations
Figure 3 – Groundwater Sampling Locations
Figure 4 – Soil Pile Location Map

FIGURE 1: SITE LOCATION MAP
Source: USGS Greensboro, North Carolina Quadrangle, 2013.N
Brownfield No.25094-21-041
September 2022
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
FIGURE 2A: SAMPLE LOCATIONS -C. 1938, 1927 and 1928
Brownfield No.25094-21-041
September 2022
N
SS-11 SS-10
SS-9
SS-8
SS-7
Approximate scale (ft)
0 37
Source: Belk Architecture Site and Utility Plan
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
FIGURE 2B: SAMPLE LOCATIONS -C. 1928 and 1929 N
SS-6
SS-5
SS-2
Approximate scale (ft)
300
Brownfield No.25094-21-041
September 2022
Source: Belk Architecture Site and Utility Plan
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
FIGURE 2C: SAMPLE LOCATIONS -C. 1929 N
SS-4
SS-3
SS-1
Approximate scale (ft)
0 15
Brownfield No.25094-21-041
September 2022
Source: Belk Architecture Site and Utility Plan
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
FIGURE 2D: SAMPLE LOCATIONS -C. 1936 N
SS-14
SS-13
SS-12
Approximate scale (ft)
0 28
Brownfield No.25094-21-041
September 2022
Source: Belk Architecture Site and Utility Plan
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
NSource: Belk Architecture Site and Utility Plan
FIGURE 3: MONITORING WELL LOCATIONS
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
Brownfield No.25094-21-041
September 2022
MW6 MW7 MW8
MW3
MW2
Approximate Scale (Ft)0 110
NSource: Belk Architecture Stormwater Plan
FIGURE 4: SOIL PILE LOCATIONS
Soil and Groundwater Sampling
Former Mock Judson Mill
2610 Oakland Avenue
Greensboro, North Carolina
Brownfield No.25094-21-041
September 2022
SS-15
SS-16
SS-17
SS-18
MW6 MW7 MW8
MW2
Approximate Scale (Ft)0 110
PCB Soil
Impact Area
TW2
TW1
TW3
T4
SS1(Swift)
SS2(Swift)
Supplemental Soil and Groundwater Sampling Report September 20, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1487

TABLES

Table 1: Soil Sample Analytical Results
Table 2: Groundwater Well Purge Data
Table 3: Groundwater Analytical Results

Sample ID SS-1 SS-2 SS-3 SS-4 SS-5 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 SS-13 SS-14
Depth (Feet)Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab Just below slab
Lattitude 36.062085 N 36.062246 N 36.062325 N 36.062219 N36.062195 N 36.062069 N 36.062288 N 36.062133 N36.062241 N 36.062045 N 36.062178 N 36.062013 N36.062032 N 36.062181 N
Longitude -79.836069 W -79.835220 W -79.835720 W -79.835922 W-79.834633 W-79.835036 W-79.834172 W-79.834534 W-79.834289 W-79.834239 W-79.834532 W-79.836375 W-79.836231 W -79.836541 W
Date 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/15/22 7/22/22 7/22/22 7/22/22
2-Butanone (MEK)*<0.0357 0.0514J 0.059J 0.0626J 0.0567J 0.0403J 0.043J 0.0438J 0.0511J 0.049J 0.0567J 0.0469J 0.0494J 0.0571J 17 5,500
Ethylbenzene <0.0035 <0.0034 <0.0035 <0.0042 <0.0039 <0.0033 <0.0031 <0.0032 <0.0034 <0.0034 <0.0039 0.004J 0.0036J <0.0034 6.1 13
Methylene Chloride**0.0813 <0.02 <0.0203 <0.0247 0.037 <0.0196 0.0222J <0.0189 0.0313 <0.0199 0.0564 0.0653 0.0566 0.0738 0.025 58
1,2,4-Trimethylbenzene <0.002 <0.002 <0.002 <0.0025 <0.0023 <0.002 <0.0033 <0.0019 <0.002 <0.002 <0.0023 0.004J <0.0018 <0.002 12 63
Xylene (total)<0.0042 <0.0042 <0.0042 <0.0051 <0.0048 <0.0041 <0.0038 <0.0039 <0.0041 <0.0041 <0.0048 0.0104J 0.0053J <0.0042 9.9 120
m&p Xylene <0.0051 <0.005 <0.0051 <0.0062 <0.0058 <0.0049 <0.0045 <0.0047 <0.0049 <0.005 <0.0058 0.0066J 0.0053J <0.005 9.8 120
o-Xylene <0.0033 <0.0032 <0.0033 <0.004 <0.0037 <0.0032 <0.0029 <0.0031 <0.0032 <0.00312 <0.0037 0.0038J <0.0029 <0.0032 9.8 140
Barium 15.1 140 87.3 89.5 177 40.8 52.8 13.9 33.9 346 90.8 NA NA NA 580 3,100
Chromium 3.0 4.2 4.9 25.9 6.6 25.5 25.8 13.0 18.5 13.9 15.9 NA NA NA NE NE
Chromium VI (Method 7199)<0.366 <0.311 <0.313 <0.361 <0.353 <0.335 <0.358 <0.348 <0.340 <0.369 <0.367 1.3 1.4 0.71 0.31 3.8
Lead 4.5 9.3 9.4 6.1 6.5 9.9 8.7 10.5 13.1 80.2 52.8 NA NA NA NE 400
Mercury <0.013 <0.012 0.014J 0.026J 0.030J 0.054J 0.063J 0.034J 0.038J 0.071J 0.12J NA NA NA NE 4.7
* MEK is suspected of being a lab contaminant
** Methylen Choride is a common laboratory contaminant
Red items are exceedances of residential and/or protectection of groundwater PSRGs
NE - Not Established
NA = Not Analyzed
Data compared to NCDEQ PSRGs July 2022
VOCs - 8260 (mg/kg)
SVOCs - 8270 (mg/kg) - Not Detected
Metals (mg/kg)
TABLE 1 - Soil Sampling Analytical Results
Mock Judson Mill, 2610 Oakland Avenue
Greensboro, North Carolina
Brownfield No. 25094-21-041
Soil toWater
PSRG
Residential
PSRG
Sample Date Well Depth
(ft)
Depth to
Water (ft)
Purge Volume
(Gallons)Purge No.pH Conductivity
(Ms/cm)
Turbidity
(NTU)
1 4.57 0.043 283
2 4.37 0.042 276
3 4.47 0.047 280
4 4.52 0.043 278
5 4.60 0.041 275
1 4.57 0.038 281
2 3.89 0.045 277
3 4.43 0.042 279
4 4.44 0.044 272
5 4.42 0.042 275
1 3.82 0.061 98.4
2 4.50 0.052 131
3 4.30 0.060 145
4 4.60 0.058 135
5 4.60 0.059 132
1 4.72 0.043 137
2 5.20 0.053 134
3 5.33 0.051 135
4 5.26 0.054 136
1 5.07 0.052 286
2 5.12 0.049 289
3 4.89 0.045 290
4 5.10 0.047 292
5 5.12 0.046 289
7/22/22
Table 2 - Baseline water Level and Groundwater Well Purge Data
Greensboro, North Carolina
7/22/22MW7
Mock Judson Mill
MW2
MW3
MW6
7/22/22
7/22/22
7/22/22
14.8
0.07
0.06
2610 Oakland Avenue
0.17
0.46
0.18
20.0 18.5
20.00 18.12
19.8
10.8
9.0720
15.6
MW8
Sample ID MW-2 MW-3 MW-6 MW-7 MW-8
Date 7/22/22 7/22/22 7/22/22 7/22/22 7/22/22
Acetone*NA NA <5.1 78.4 <5.1 6,000
Phenol**NA NA 20.5 25.1J 1.9J 30
Chromium VI <0.0400 <0.0400 1.57 0.0764J 0.437J NE
* Acetone is believe to be a laboratory contaminant
**Phenol was detected in the method blanks and appears to be lab contaminant
VOCs - 8260 (ug/L)
RCRA 8 Metals (ug/L)
NA - Not Analized, NE - Not Established
Bold values exceed the NCAC 2L Groundwater Quality Standards set by the North Carolina Department of Environmental Quality (April 1 2022)
SVOC - 8270 (ug/L)
TABLE 3 - Groundwater Analytical Results
Mock Judson Mill, 2610 Oakland Avenue
Greensboro, North Carolina
Brownfield No. 25094-21-041
NCDEQ
Groundwater Quality
Standards (2L)
Supplemental Soil and Groundwater Sampling Report September 20, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1487

APPENDIX A

PHOTOGRAPHS

Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

1
Photograph 1 – Interior saw cuts in foundation

Photograph 2 – Interior saw cuts in foundation – removal of concrete
Supplemental Soil and Groundwater Sampling Report September 30, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1533

2
Photograph 3 – Typical soils under slab

Photograph 4 – Interior utility lines
Supplemental Soil and Groundwater Sampling Report September 20, 2022
2610 Oakland Avenue
Brownfield Project Number: 25094-21-041
ASE Project No: 1487

APPENDIX B
LABORATORY DATA

#=CL#
August 21, 2022
LIMS USE: FR - CHERYL MOODY
LIMS OBJECT ID: 92615483
92615483
Project:
Pace Project No.:
RE:
Cheryl Moody
Atlantic Shore Environmental
175-1 Venture Drive
Belville, NC 28451
Mock Judson 1533
Dear Cheryl Moody:
Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Daniel J. Schiwinger, Atlantic Shores Environmental
Services, Ltd.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 98
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Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 98
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92615483
Mock Judson 1533
Lab ID Sample ID Matrix Date Collected Date Received
92615483001 SS-1 Solid 07/15/22 13:45 07/18/22 10:20
92615483002 SS-2 Solid 07/15/22 14:13 07/18/22 10:20
92615483003 SS-3 Solid 07/15/22 14:25 07/18/22 10:20
92615483004 SS-4 Solid 07/15/22 14:38 07/18/22 10:20
92615483005 SS-5 Solid 07/15/22 15:00 07/18/22 10:20
92615483006 SS-6 Solid 07/15/22 15:15 07/18/22 10:20
92615483007 SS-7 Solid 07/15/22 15:30 07/18/22 10:20
92615483008 SS-8 Solid 07/15/22 15:43 07/18/22 10:20
92615483009 SS-9 Solid 07/15/22 15:50 07/18/22 10:20
92615483010 SS-10 Solid 07/15/22 16:00 07/18/22 10:20
92615483011 SS-11 Solid 07/15/22 16:10 07/18/22 10:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 98
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92615483
Mock Judson 1533
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92615483001 SS-1 EPA 6010D 7 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANARD
92615483002 SS-2 EPA 6010D 7 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANARD
92615483003 SS-3 EPA 6010D 7 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANARD
92615483004 SS-4 EPA 6010D 7 PASI-GADRB, KH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANARD
92615483005 SS-5 EPA 6010D 7 PASI-GADRB, KH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMAS
EPA 7199 1 PANARD
92615483006 SS-6 EPA 6010D 7 PASI-GADRB, KH
EPA 7471B 1 PASI-GAVB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 98
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92615483
Mock Judson 1533
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMAS
EPA 7199 1 PANARD
92615483007 SS-7 EPA 6010D 7 PASI-GADRB, KH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMAS
EPA 7199 1 PANARD
92615483008 SS-8 EPA 6010D 7 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMAS
EPA 7199 1 PANARD
92615483009 SS-9 EPA 6010D 7 PASI-GADRB, KH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
92615483010 SS-10 EPA 6010D 7 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
92615483011 SS-11 EPA 6010D 7 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 98
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92615483
Mock Judson 1533
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANARD
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-1 Lab ID:92615483001 Collected:07/15/22 13:45 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 15:50 7440-38-207/20/22 11:373.6 2.6 1
Barium 15.1 mg/kg 07/20/22 15:50 7440-39-307/20/22 11:371.2 0.50 1
Cadmium ND mg/kg 07/20/22 15:50 7440-43-907/20/22 11:371.2 0.36 1
Chromium 3.0 mg/kg 07/20/22 15:50 7440-47-307/20/22 11:371.2 1.1 1
Lead 4.5 mg/kg 07/20/22 15:50 7439-92-107/20/22 11:373.0 1.9 1
Selenium ND mg/kg 07/20/22 15:50 7782-49-207/20/22 11:376.0 5.2 1
Silver ND mg/kg 07/20/22 15:50 7440-22-407/20/22 11:371.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 07/25/22 13:31 7439-97-607/25/22 08:300.32 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/25/22 09:20 83-32-907/22/22 11:504191471
Acenaphthylene ND ug/kg 07/25/22 09:20 208-96-807/22/22 11:504191471
Aniline ND ug/kg 07/25/22 09:20 62-53-307/22/22 11:504191641
Anthracene ND ug/kg 07/25/22 09:20 120-12-707/22/22 11:504191371
Benzo(a)anthracene ND ug/kg 07/25/22 09:20 56-55-307/22/22 11:504191401
Benzo(a)pyrene ND ug/kg 07/25/22 09:20 50-32-807/22/22 11:504191451
Benzo(b)fluoranthene ND ug/kg 07/25/22 09:20 205-99-207/22/22 11:504191401
Benzo(g,h,i)perylene ND ug/kg 07/25/22 09:20 191-24-207/22/22 11:504191631
Benzo(k)fluoranthene ND ug/kg 07/25/22 09:20 207-08-907/22/22 11:504191471
Benzoic Acid ND ug/kg 07/25/22 09:20 65-85-007/22/22 11:5021009001
Benzyl alcohol ND ug/kg 07/25/22 09:20 100-51-607/22/22 11:508383171
4-Bromophenylphenyl ether ND ug/kg 07/25/22 09:20 101-55-307/22/22 11:504191611
Butylbenzylphthalate ND ug/kg 07/25/22 09:20 85-68-707/22/22 11:504191761
4-Chloro-3-methylphenol ND ug/kg 07/25/22 09:20 59-50-707/22/22 11:508382951
4-Chloroaniline ND ug/kg 07/25/22 09:20 106-47-807/22/22 11:508383291
bis(2-Chloroethoxy)methane ND ug/kg 07/25/22 09:20 111-91-107/22/22 11:504191741
bis(2-Chloroethyl) ether ND ug/kg 07/25/22 09:20 111-44-407/22/22 11:504191571
2-Chloronaphthalene ND ug/kg 07/25/22 09:20 91-58-707/22/22 11:504191661
2-Chlorophenol ND ug/kg 07/25/22 09:20 95-57-807/22/22 11:504191571
4-Chlorophenylphenyl ether ND ug/kg 07/25/22 09:20 7005-72-307/22/22 11:504191561
Chrysene ND ug/kg 07/25/22 09:20 218-01-907/22/22 11:504191521
Dibenz(a,h)anthracene ND ug/kg 07/25/22 09:20 53-70-307/22/22 11:504191611
Dibenzofuran ND ug/kg 07/25/22 09:20 132-64-907/22/22 11:504191511
1,2-Dichlorobenzene ND ug/kg 07/25/22 09:20 95-50-107/22/22 11:504191511
1,3-Dichlorobenzene ND ug/kg 07/25/22 09:20 541-73-107/22/22 11:504191491
1,4-Dichlorobenzene ND ug/kg 07/25/22 09:20 106-46-707/22/22 11:504191601
3,3'-Dichlorobenzidine ND ug/kg 07/25/22 09:20 91-94-107/22/22 11:508382831
2,4-Dichlorophenol ND ug/kg 07/25/22 09:20 120-83-207/22/22 11:504191641
Diethylphthalate ND ug/kg 07/25/22 09:20 84-66-207/22/22 11:504191541
2,4-Dimethylphenol ND ug/kg 07/25/22 09:20 105-67-907/22/22 11:504191741
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-1 Lab ID:92615483001 Collected:07/15/22 13:45 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/25/22 09:20 131-11-307/22/22 11:504191521
Di-n-butylphthalate ND ug/kg 07/25/22 09:20 84-74-207/22/22 11:504191411
4,6-Dinitro-2-methylphenol ND ug/kg 07/25/22 09:20 534-52-107/22/22 11:508383911
2,4-Dinitrophenol ND ug/kg 07/25/22 09:20 51-28-507/22/22 11:50210013001
2,4-Dinitrotoluene ND ug/kg 07/25/22 09:20 121-14-207/22/22 11:504191611
2,6-Dinitrotoluene ND ug/kg 07/25/22 09:20 606-20-207/22/22 11:504191541
Di-n-octylphthalate ND ug/kg 07/25/22 09:20 117-84-007/22/22 11:504191651
bis(2-Ethylhexyl)phthalate ND ug/kg 07/25/22 09:20 117-81-707/22/22 11:504191631
Fluoranthene ND ug/kg 07/25/22 09:20 206-44-007/22/22 11:504191431
Fluorene ND ug/kg 07/25/22 09:20 86-73-707/22/22 11:504191471
Hexachloro-1,3-butadiene ND ug/kg 07/25/22 09:20 87-68-307/22/22 11:504191821
Hexachlorobenzene ND ug/kg 07/25/22 09:20 118-74-107/22/22 11:504191641
Hexachlorocyclopentadiene ND ug/kg 07/25/22 09:20 77-47-407/22/22 11:504192401
Hexachloroethane ND ug/kg 07/25/22 09:20 67-72-107/22/22 11:504191601
Indeno(1,2,3-cd)pyrene ND ug/kg 07/25/22 09:20 193-39-507/22/22 11:504191651
Isophorone ND ug/kg 07/25/22 09:20 78-59-107/22/22 11:504191871
1-Methylnaphthalene ND ug/kg 07/25/22 09:20 90-12-007/22/22 11:504191471
2-Methylnaphthalene ND ug/kg 07/25/22 09:20 91-57-607/22/22 11:504191681
2-Methylphenol(o-Cresol)ND ug/kg 07/25/22 09:20 95-48-707/22/22 11:504191711
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/25/22 09:20 15831-10-407/22/22 11:504191691
Naphthalene ND ug/kg 07/25/22 09:20 91-20-307/22/22 11:504191421
2-Nitroaniline ND ug/kg 07/25/22 09:20 88-74-407/22/22 11:5021003431
3-Nitroaniline ND ug/kg 07/25/22 09:20 99-09-207/22/22 11:5021003291
4-Nitroaniline ND ug/kg 07/25/22 09:20 100-01-607/22/22 11:508383191
Nitrobenzene ND ug/kg 07/25/22 09:20 98-95-307/22/22 11:504191941
2-Nitrophenol ND ug/kg 07/25/22 09:20 88-75-507/22/22 11:504191821
4-Nitrophenol ND ug/kg 07/25/22 09:20 100-02-707/22/22 11:5021008101
N-Nitrosodimethylamine ND ug/kg 07/25/22 09:20 62-75-907/22/22 11:504191411
N-Nitroso-di-n-propylamine ND ug/kg 07/25/22 09:20 621-64-707/22/22 11:504191571
N-Nitrosodiphenylamine ND ug/kg 07/25/22 09:20 86-30-607/22/22 11:504191491
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/25/22 09:20 108-60-107/22/22 11:504191991
Pentachlorophenol ND ug/kg 07/25/22 09:20 87-86-507/22/22 11:508384101
Phenanthrene ND ug/kg 07/25/22 09:20 85-01-807/22/22 11:504191371
Phenol ND ug/kg 07/25/22 09:20 108-95-207/22/22 11:504191871
Pyrene ND ug/kg 07/25/22 09:20 129-00-007/22/22 11:504191701
Pyridine ND ug/kg 07/25/22 09:20 110-86-107/22/22 11:504191321
1,2,4-Trichlorobenzene ND ug/kg 07/25/22 09:20 120-82-107/22/22 11:504191651
2,4,5-Trichlorophenol ND ug/kg 07/25/22 09:20 95-95-407/22/22 11:504191921
2,4,6-Trichlorophenol ND ug/kg 07/25/22 09:20 88-06-207/22/22 11:504191731
Surrogates
Nitrobenzene-d5 (S)68 %07/25/22 09:20 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)65 %07/25/22 09:20 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)77 %07/25/22 09:20 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)68 %07/25/22 09:20 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-1 Lab ID:92615483001 Collected:07/15/22 13:45 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)67 %07/25/22 09:20 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)68 %07/25/22 09:20 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 08:13 67-64-107/19/22 15:2914947.8 1
Benzene ND ug/kg 07/20/22 08:13 71-43-207/19/22 15:297.4 3.0 1
Bromobenzene ND ug/kg 07/20/22 08:13 108-86-107/19/22 15:297.4 2.4 1
Bromochloromethane ND ug/kg 07/20/22 08:13 74-97-507/19/22 15:297.4 2.2 1
Bromodichloromethane ND ug/kg 07/20/22 08:13 75-27-407/19/22 15:297.4 2.9 1
Bromoform ND ug/kg 07/20/22 08:13 75-25-207/19/22 15:297.4 2.6 1
Bromomethane ND ug/kg 07/20/22 08:13 74-83-9 L107/19/22 15:2914.9 11.8 1
2-Butanone (MEK)ND ug/kg 07/20/22 08:13 78-93-307/19/22 15:2914935.7 1
n-Butylbenzene ND ug/kg 07/20/22 08:13 104-51-807/19/22 15:297.4 3.5 1
sec-Butylbenzene ND ug/kg 07/20/22 08:13 135-98-807/19/22 15:297.4 3.3 1
tert-Butylbenzene ND ug/kg 07/20/22 08:13 98-06-607/19/22 15:297.4 2.7 1
Carbon tetrachloride ND ug/kg 07/20/22 08:13 56-23-507/19/22 15:297.4 2.8 1
Chlorobenzene ND ug/kg 07/20/22 08:13 108-90-707/19/22 15:297.4 1.4 1
Chloroethane ND ug/kg 07/20/22 08:13 75-00-3 IH07/19/22 15:2914.9 5.7 1
Chloroform ND ug/kg 07/20/22 08:13 67-66-307/19/22 15:297.4 4.5 1
Chloromethane ND ug/kg 07/20/22 08:13 74-87-3 IH,L107/19/22 15:2914.9 6.3 1
2-Chlorotoluene ND ug/kg 07/20/22 08:13 95-49-807/19/22 15:297.4 2.6 1
4-Chlorotoluene ND ug/kg 07/20/22 08:13 106-43-407/19/22 15:297.4 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 08:13 96-12-8 v207/19/22 15:297.4 2.9 1
Dibromochloromethane ND ug/kg 07/20/22 08:13 124-48-107/19/22 15:297.4 4.2 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 08:13 106-93-407/19/22 15:297.4 3.3 1
Dibromomethane ND ug/kg 07/20/22 08:13 74-95-307/19/22 15:297.4 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 08:13 95-50-107/19/22 15:297.4 2.7 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 08:13 541-73-107/19/22 15:297.4 2.3 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 08:13 106-46-707/19/22 15:297.4 1.9 1
Dichlorodifluoromethane ND ug/kg 07/20/22 08:13 75-71-8 IH07/19/22 15:2914.9 3.2 1
1,1-Dichloroethane ND ug/kg 07/20/22 08:13 75-34-307/19/22 15:297.4 3.1 1
1,2-Dichloroethane ND ug/kg 07/20/22 08:13 107-06-207/19/22 15:297.4 4.9 1
1,1-Dichloroethene ND ug/kg 07/20/22 08:13 75-35-407/19/22 15:297.4 3.1 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 08:13 156-59-207/19/22 15:297.4 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 08:13 156-60-507/19/22 15:297.4 2.6 1
1,2-Dichloropropane ND ug/kg 07/20/22 08:13 78-87-507/19/22 15:297.4 2.2 1
1,3-Dichloropropane ND ug/kg 07/20/22 08:13 142-28-907/19/22 15:297.4 2.3 1
2,2-Dichloropropane ND ug/kg 07/20/22 08:13 594-20-707/19/22 15:297.4 2.4 1
1,1-Dichloropropene ND ug/kg 07/20/22 08:13 563-58-607/19/22 15:297.4 3.6 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 08:13 10061-01-507/19/22 15:297.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 08:13 10061-02-607/19/22 15:297.4 2.6 1
Diisopropyl ether ND ug/kg 07/20/22 08:13 108-20-307/19/22 15:297.4 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-1 Lab ID:92615483001 Collected:07/15/22 13:45 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 08:13 100-41-407/19/22 15:297.4 3.5 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 08:13 87-68-307/19/22 15:2914.9 12.2 1
2-Hexanone ND ug/kg 07/20/22 08:13 591-78-607/19/22 15:2974.4 7.2 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 08:13 98-82-807/19/22 15:297.4 2.5 1
p-Isopropyltoluene ND ug/kg 07/20/22 08:13 99-87-607/19/22 15:297.4 3.7 1
Methylene Chloride 81.3 ug/kg 07/20/22 08:13 75-09-2 C907/19/22 15:2929.8 20.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 08:13 108-10-107/19/22 15:2974.4 7.2 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 08:13 1634-04-407/19/22 15:297.4 2.8 1
Naphthalene ND ug/kg 07/20/22 08:13 91-20-3 v207/19/22 15:297.4 3.9 1
n-Propylbenzene ND ug/kg 07/20/22 08:13 103-65-107/19/22 15:297.4 2.7 1
Styrene ND ug/kg 07/20/22 08:13 100-42-507/19/22 15:297.4 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 08:13 630-20-607/19/22 15:297.4 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 08:13 79-34-507/19/22 15:297.4 2.0 1
Tetrachloroethene ND ug/kg 07/20/22 08:13 127-18-407/19/22 15:297.4 2.4 1
Toluene ND ug/kg 07/20/22 08:13 108-88-307/19/22 15:297.4 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 08:13 87-61-6 v207/19/22 15:297.4 6.0 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 08:13 120-82-107/19/22 15:297.4 6.3 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 08:13 71-55-607/19/22 15:297.4 3.9 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 08:13 79-00-507/19/22 15:297.4 2.5 1
Trichloroethene ND ug/kg 07/20/22 08:13 79-01-607/19/22 15:297.4 1.9 1
Trichlorofluoromethane ND ug/kg 07/20/22 08:13 75-69-407/19/22 15:297.4 4.1 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 08:13 96-18-407/19/22 15:297.4 3.8 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 08:13 95-63-607/19/22 15:297.4 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 08:13 108-67-807/19/22 15:297.4 2.5 1
Vinyl acetate ND ug/kg 07/20/22 08:13 108-05-407/19/22 15:2974.4 5.4 1
Vinyl chloride ND ug/kg 07/20/22 08:13 75-01-4 IH07/19/22 15:2914.9 3.8 1
Xylene (Total)ND ug/kg 07/20/22 08:13 1330-20-707/19/22 15:2914.9 4.2 1
m&p-Xylene ND ug/kg 07/20/22 08:13 179601-23-107/19/22 15:2914.9 5.1 1
o-Xylene ND ug/kg 07/20/22 08:13 95-47-607/19/22 15:297.4 3.3 1
Surrogates
Toluene-d8 (S)102 %07/20/22 08:13 2037-26-507/19/22 15:2970-130 1
4-Bromofluorobenzene (S)101 %07/20/22 08:13 460-00-407/19/22 15:2969-134 1
1,2-Dichloroethane-d4 (S)109 %07/20/22 08:13 17060-07-007/19/22 15:2970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.0 %07/19/22 17:55 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 69.7 %07/22/22 19:0507/22/22 18:521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-1 Lab ID:92615483001 Collected:07/15/22 13:45 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 13:45 18540-29-908/11/22 10:211.43 0.366 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-2 Lab ID:92615483002 Collected:07/15/22 14:13 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:09 7440-38-207/20/22 11:373.6 2.5 1
Barium 140 mg/kg 07/20/22 16:09 7440-39-307/20/22 11:371.2 0.49 1
Cadmium ND mg/kg 07/20/22 16:09 7440-43-907/20/22 11:371.2 0.35 1
Chromium 4.2 mg/kg 07/20/22 16:09 7440-47-307/20/22 11:371.2 1.1 1
Lead 9.3 mg/kg 07/20/22 16:09 7439-92-107/20/22 11:373.0 1.8 1
Selenium ND mg/kg 07/20/22 16:09 7782-49-207/20/22 11:375.9 5.1 1
Silver ND mg/kg 07/20/22 16:09 7440-22-407/20/22 11:371.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 07/25/22 13:34 7439-97-607/25/22 08:300.30 0.012 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/25/22 09:47 83-32-907/22/22 11:504041421
Acenaphthylene ND ug/kg 07/25/22 09:47 208-96-807/22/22 11:504041421
Aniline ND ug/kg 07/25/22 09:47 62-53-307/22/22 11:504041581
Anthracene ND ug/kg 07/25/22 09:47 120-12-707/22/22 11:504041321
Benzo(a)anthracene ND ug/kg 07/25/22 09:47 56-55-307/22/22 11:504041351
Benzo(a)pyrene ND ug/kg 07/25/22 09:47 50-32-807/22/22 11:504041401
Benzo(b)fluoranthene ND ug/kg 07/25/22 09:47 205-99-207/22/22 11:504041351
Benzo(g,h,i)perylene ND ug/kg 07/25/22 09:47 191-24-207/22/22 11:504041571
Benzo(k)fluoranthene ND ug/kg 07/25/22 09:47 207-08-907/22/22 11:504041421
Benzoic Acid ND ug/kg 07/25/22 09:47 65-85-007/22/22 11:5020208691
Benzyl alcohol ND ug/kg 07/25/22 09:47 100-51-607/22/22 11:508093061
4-Bromophenylphenyl ether ND ug/kg 07/25/22 09:47 101-55-307/22/22 11:504041561
Butylbenzylphthalate ND ug/kg 07/25/22 09:47 85-68-707/22/22 11:504041701
4-Chloro-3-methylphenol ND ug/kg 07/25/22 09:47 59-50-707/22/22 11:508092841
4-Chloroaniline ND ug/kg 07/25/22 09:47 106-47-807/22/22 11:508093171
bis(2-Chloroethoxy)methane ND ug/kg 07/25/22 09:47 111-91-107/22/22 11:504041681
bis(2-Chloroethyl) ether ND ug/kg 07/25/22 09:47 111-44-407/22/22 11:504041521
2-Chloronaphthalene ND ug/kg 07/25/22 09:47 91-58-707/22/22 11:504041611
2-Chlorophenol ND ug/kg 07/25/22 09:47 95-57-807/22/22 11:504041521
4-Chlorophenylphenyl ether ND ug/kg 07/25/22 09:47 7005-72-307/22/22 11:504041511
Chrysene ND ug/kg 07/25/22 09:47 218-01-907/22/22 11:504041471
Dibenz(a,h)anthracene ND ug/kg 07/25/22 09:47 53-70-307/22/22 11:504041561
Dibenzofuran ND ug/kg 07/25/22 09:47 132-64-907/22/22 11:504041461
1,2-Dichlorobenzene ND ug/kg 07/25/22 09:47 95-50-107/22/22 11:504041461
1,3-Dichlorobenzene ND ug/kg 07/25/22 09:47 541-73-107/22/22 11:504041431
1,4-Dichlorobenzene ND ug/kg 07/25/22 09:47 106-46-707/22/22 11:504041541
3,3'-Dichlorobenzidine ND ug/kg 07/25/22 09:47 91-94-107/22/22 11:508092731
2,4-Dichlorophenol ND ug/kg 07/25/22 09:47 120-83-207/22/22 11:504041581
Diethylphthalate ND ug/kg 07/25/22 09:47 84-66-207/22/22 11:504041481
2,4-Dimethylphenol ND ug/kg 07/25/22 09:47 105-67-907/22/22 11:504041681
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-2 Lab ID:92615483002 Collected:07/15/22 14:13 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/25/22 09:47 131-11-307/22/22 11:504041471
Di-n-butylphthalate ND ug/kg 07/25/22 09:47 84-74-207/22/22 11:504041361
4,6-Dinitro-2-methylphenol ND ug/kg 07/25/22 09:47 534-52-107/22/22 11:508093771
2,4-Dinitrophenol ND ug/kg 07/25/22 09:47 51-28-507/22/22 11:50202012501
2,4-Dinitrotoluene ND ug/kg 07/25/22 09:47 121-14-207/22/22 11:504041561
2,6-Dinitrotoluene ND ug/kg 07/25/22 09:47 606-20-207/22/22 11:504041481
Di-n-octylphthalate ND ug/kg 07/25/22 09:47 117-84-007/22/22 11:504041591
bis(2-Ethylhexyl)phthalate ND ug/kg 07/25/22 09:47 117-81-707/22/22 11:504041571
Fluoranthene ND ug/kg 07/25/22 09:47 206-44-007/22/22 11:504041381
Fluorene ND ug/kg 07/25/22 09:47 86-73-707/22/22 11:504041421
Hexachloro-1,3-butadiene ND ug/kg 07/25/22 09:47 87-68-307/22/22 11:504041751
Hexachlorobenzene ND ug/kg 07/25/22 09:47 118-74-107/22/22 11:504041581
Hexachlorocyclopentadiene ND ug/kg 07/25/22 09:47 77-47-407/22/22 11:504042321
Hexachloroethane ND ug/kg 07/25/22 09:47 67-72-107/22/22 11:504041541
Indeno(1,2,3-cd)pyrene ND ug/kg 07/25/22 09:47 193-39-507/22/22 11:504041591
Isophorone ND ug/kg 07/25/22 09:47 78-59-107/22/22 11:504041801
1-Methylnaphthalene ND ug/kg 07/25/22 09:47 90-12-007/22/22 11:504041421
2-Methylnaphthalene ND ug/kg 07/25/22 09:47 91-57-607/22/22 11:504041621
2-Methylphenol(o-Cresol)ND ug/kg 07/25/22 09:47 95-48-707/22/22 11:504041651
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/25/22 09:47 15831-10-407/22/22 11:504041631
Naphthalene ND ug/kg 07/25/22 09:47 91-20-307/22/22 11:504041371
2-Nitroaniline ND ug/kg 07/25/22 09:47 88-74-407/22/22 11:5020203311
3-Nitroaniline ND ug/kg 07/25/22 09:47 99-09-207/22/22 11:5020203171
4-Nitroaniline ND ug/kg 07/25/22 09:47 100-01-607/22/22 11:508093081
Nitrobenzene ND ug/kg 07/25/22 09:47 98-95-307/22/22 11:504041871
2-Nitrophenol ND ug/kg 07/25/22 09:47 88-75-507/22/22 11:504041751
4-Nitrophenol ND ug/kg 07/25/22 09:47 100-02-707/22/22 11:5020207821
N-Nitrosodimethylamine ND ug/kg 07/25/22 09:47 62-75-907/22/22 11:504041361
N-Nitroso-di-n-propylamine ND ug/kg 07/25/22 09:47 621-64-707/22/22 11:504041521
N-Nitrosodiphenylamine ND ug/kg 07/25/22 09:47 86-30-607/22/22 11:504041431
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/25/22 09:47 108-60-107/22/22 11:504041921
Pentachlorophenol ND ug/kg 07/25/22 09:47 87-86-507/22/22 11:508093961
Phenanthrene ND ug/kg 07/25/22 09:47 85-01-807/22/22 11:504041321
Phenol ND ug/kg 07/25/22 09:47 108-95-207/22/22 11:504041801
Pyrene ND ug/kg 07/25/22 09:47 129-00-007/22/22 11:504041641
Pyridine ND ug/kg 07/25/22 09:47 110-86-107/22/22 11:504041271
1,2,4-Trichlorobenzene ND ug/kg 07/25/22 09:47 120-82-107/22/22 11:504041591
2,4,5-Trichlorophenol ND ug/kg 07/25/22 09:47 95-95-407/22/22 11:504041851
2,4,6-Trichlorophenol ND ug/kg 07/25/22 09:47 88-06-207/22/22 11:504041671
Surrogates
Nitrobenzene-d5 (S)56 %07/25/22 09:47 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)56 %07/25/22 09:47 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)66 %07/25/22 09:47 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)57 %07/25/22 09:47 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-2 Lab ID:92615483002 Collected:07/15/22 14:13 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)56 %07/25/22 09:47 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)52 %07/25/22 09:47 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 01:07 67-64-107/19/22 17:0714646.8 1
Benzene ND ug/kg 07/20/22 01:07 71-43-207/19/22 17:077.3 2.9 1
Bromobenzene ND ug/kg 07/20/22 01:07 108-86-107/19/22 17:077.3 2.4 1
Bromochloromethane ND ug/kg 07/20/22 01:07 74-97-507/19/22 17:077.3 2.2 1
Bromodichloromethane ND ug/kg 07/20/22 01:07 75-27-407/19/22 17:077.3 2.8 1
Bromoform ND ug/kg 07/20/22 01:07 75-25-207/19/22 17:077.3 2.6 1
Bromomethane ND ug/kg 07/20/22 01:07 74-83-9 L107/19/22 17:0714.6 11.5 1
2-Butanone (MEK)51.4J ug/kg 07/20/22 01:07 78-93-3 C707/19/22 17:0714635.0 1
n-Butylbenzene ND ug/kg 07/20/22 01:07 104-51-807/19/22 17:077.3 3.4 1
sec-Butylbenzene ND ug/kg 07/20/22 01:07 135-98-807/19/22 17:077.3 3.2 1
tert-Butylbenzene ND ug/kg 07/20/22 01:07 98-06-607/19/22 17:077.3 2.6 1
Carbon tetrachloride ND ug/kg 07/20/22 01:07 56-23-507/19/22 17:077.3 2.7 1
Chlorobenzene ND ug/kg 07/20/22 01:07 108-90-707/19/22 17:077.3 1.4 1
Chloroethane ND ug/kg 07/20/22 01:07 75-00-3 IH07/19/22 17:0714.6 5.6 1
Chloroform ND ug/kg 07/20/22 01:07 67-66-307/19/22 17:077.3 4.4 1
Chloromethane ND ug/kg 07/20/22 01:07 74-87-3 IH07/19/22 17:0714.6 6.1 1
2-Chlorotoluene ND ug/kg 07/20/22 01:07 95-49-807/19/22 17:077.3 2.6 1
4-Chlorotoluene ND ug/kg 07/20/22 01:07 106-43-407/19/22 17:077.3 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 01:07 96-12-8 v207/19/22 17:077.3 2.8 1
Dibromochloromethane ND ug/kg 07/20/22 01:07 124-48-107/19/22 17:077.3 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 01:07 106-93-407/19/22 17:077.3 3.2 1
Dibromomethane ND ug/kg 07/20/22 01:07 74-95-307/19/22 17:077.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 01:07 95-50-107/19/22 17:077.3 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 01:07 541-73-107/19/22 17:077.3 2.3 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 01:07 106-46-707/19/22 17:077.3 1.9 1
Dichlorodifluoromethane ND ug/kg 07/20/22 01:07 75-71-8 IH,L107/19/22 17:0714.6 3.2 1
1,1-Dichloroethane ND ug/kg 07/20/22 01:07 75-34-307/19/22 17:077.3 3.0 1
1,2-Dichloroethane ND ug/kg 07/20/22 01:07 107-06-207/19/22 17:077.3 4.8 1
1,1-Dichloroethene ND ug/kg 07/20/22 01:07 75-35-407/19/22 17:077.3 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 01:07 156-59-207/19/22 17:077.3 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 01:07 156-60-507/19/22 17:077.3 2.6 1
1,2-Dichloropropane ND ug/kg 07/20/22 01:07 78-87-507/19/22 17:077.3 2.2 1
1,3-Dichloropropane ND ug/kg 07/20/22 01:07 142-28-907/19/22 17:077.3 2.3 1
2,2-Dichloropropane ND ug/kg 07/20/22 01:07 594-20-707/19/22 17:077.3 2.4 1
1,1-Dichloropropene ND ug/kg 07/20/22 01:07 563-58-607/19/22 17:077.3 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 01:07 10061-01-507/19/22 17:077.3 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 01:07 10061-02-607/19/22 17:077.3 2.5 1
Diisopropyl ether ND ug/kg 07/20/22 01:07 108-20-307/19/22 17:077.3 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-2 Lab ID:92615483002 Collected:07/15/22 14:13 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 01:07 100-41-407/19/22 17:077.3 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 01:07 87-68-3 M107/19/22 17:0714.6 11.9 1
2-Hexanone ND ug/kg 07/20/22 01:07 591-78-607/19/22 17:0772.9 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 01:07 98-82-807/19/22 17:077.3 2.5 1
p-Isopropyltoluene ND ug/kg 07/20/22 01:07 99-87-607/19/22 17:077.3 3.6 1
Methylene Chloride ND ug/kg 07/20/22 01:07 75-09-207/19/22 17:0729.2 20.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 01:07 108-10-107/19/22 17:0772.9 7.0 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 01:07 1634-04-407/19/22 17:077.3 2.7 1
Naphthalene ND ug/kg 07/20/22 01:07 91-20-3 v207/19/22 17:077.3 3.8 1
n-Propylbenzene ND ug/kg 07/20/22 01:07 103-65-107/19/22 17:077.3 2.6 1
Styrene ND ug/kg 07/20/22 01:07 100-42-507/19/22 17:077.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 01:07 630-20-607/19/22 17:077.3 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 01:07 79-34-507/19/22 17:077.3 1.9 1
Tetrachloroethene ND ug/kg 07/20/22 01:07 127-18-407/19/22 17:077.3 2.3 1
Toluene ND ug/kg 07/20/22 01:07 108-88-307/19/22 17:077.3 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 01:07 87-61-6 M1,v207/19/22 17:077.3 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 01:07 120-82-1 M107/19/22 17:077.3 6.1 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 01:07 71-55-607/19/22 17:077.3 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 01:07 79-00-507/19/22 17:077.3 2.4 1
Trichloroethene ND ug/kg 07/20/22 01:07 79-01-607/19/22 17:077.3 1.9 1
Trichlorofluoromethane ND ug/kg 07/20/22 01:07 75-69-407/19/22 17:077.3 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 01:07 96-18-407/19/22 17:077.3 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 01:07 95-63-607/19/22 17:077.3 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 01:07 108-67-807/19/22 17:077.3 2.4 1
Vinyl acetate ND ug/kg 07/20/22 01:07 108-05-407/19/22 17:0772.9 5.3 1
Vinyl chloride ND ug/kg 07/20/22 01:07 75-01-4 IH07/19/22 17:0714.6 3.7 1
Xylene (Total)ND ug/kg 07/20/22 01:07 1330-20-707/19/22 17:0714.6 4.2 1
m&p-Xylene ND ug/kg 07/20/22 01:07 179601-23-107/19/22 17:0714.6 5.0 1
o-Xylene ND ug/kg 07/20/22 01:07 95-47-607/19/22 17:077.3 3.2 1
Surrogates
Toluene-d8 (S)100 %07/20/22 01:07 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)100 %07/20/22 01:07 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)103 %07/20/22 01:07 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.9 %07/19/22 17:55 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.0 %07/22/22 19:0507/22/22 18:521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-2 Lab ID:92615483002 Collected:07/15/22 14:13 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 13:50 18540-29-908/11/22 10:211.22 0.311 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-3 Lab ID:92615483003 Collected:07/15/22 14:25 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:15 7440-38-207/20/22 11:373.5 2.5 1
Barium 87.3 mg/kg 07/20/22 16:15 7440-39-307/20/22 11:371.2 0.49 1
Cadmium ND mg/kg 07/20/22 16:15 7440-43-907/20/22 11:371.2 0.35 1
Chromium 4.9 mg/kg 07/20/22 16:15 7440-47-307/20/22 11:371.2 1.1 1
Lead 9.4 mg/kg 07/20/22 16:15 7439-92-107/20/22 11:372.9 1.8 1
Selenium ND mg/kg 07/20/22 16:15 7782-49-207/20/22 11:375.9 5.1 1
Silver ND mg/kg 07/20/22 16:15 7440-22-407/20/22 11:371.2 0.48 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.014J mg/kg 07/25/22 13:36 7439-97-607/25/22 08:300.29 0.012 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/22/22 17:18 83-32-907/22/22 11:504051421
Acenaphthylene ND ug/kg 07/22/22 17:18 208-96-807/22/22 11:504051421
Aniline ND ug/kg 07/22/22 17:18 62-53-307/22/22 11:504051581
Anthracene ND ug/kg 07/22/22 17:18 120-12-707/22/22 11:504051331
Benzo(a)anthracene ND ug/kg 07/22/22 17:18 56-55-307/22/22 11:504051351
Benzo(a)pyrene ND ug/kg 07/22/22 17:18 50-32-807/22/22 11:504051401
Benzo(b)fluoranthene ND ug/kg 07/22/22 17:18 205-99-207/22/22 11:504051351
Benzo(g,h,i)perylene ND ug/kg 07/22/22 17:18 191-24-207/22/22 11:504051571
Benzo(k)fluoranthene ND ug/kg 07/22/22 17:18 207-08-907/22/22 11:504051421
Benzoic Acid ND ug/kg 07/22/22 17:18 65-85-0 v207/22/22 11:5020208701
Benzyl alcohol ND ug/kg 07/22/22 17:18 100-51-607/22/22 11:508103071
4-Bromophenylphenyl ether ND ug/kg 07/22/22 17:18 101-55-307/22/22 11:504051561
Butylbenzylphthalate ND ug/kg 07/22/22 17:18 85-68-707/22/22 11:504051711
4-Chloro-3-methylphenol ND ug/kg 07/22/22 17:18 59-50-707/22/22 11:508102851
4-Chloroaniline ND ug/kg 07/22/22 17:18 106-47-807/22/22 11:508103181
bis(2-Chloroethoxy)methane ND ug/kg 07/22/22 17:18 111-91-107/22/22 11:504051681
bis(2-Chloroethyl) ether ND ug/kg 07/22/22 17:18 111-44-407/22/22 11:504051521
2-Chloronaphthalene ND ug/kg 07/22/22 17:18 91-58-707/22/22 11:504051611
2-Chlorophenol ND ug/kg 07/22/22 17:18 95-57-807/22/22 11:504051521
4-Chlorophenylphenyl ether ND ug/kg 07/22/22 17:18 7005-72-307/22/22 11:504051511
Chrysene ND ug/kg 07/22/22 17:18 218-01-907/22/22 11:504051471
Dibenz(a,h)anthracene ND ug/kg 07/22/22 17:18 53-70-307/22/22 11:504051561
Dibenzofuran ND ug/kg 07/22/22 17:18 132-64-907/22/22 11:504051461
1,2-Dichlorobenzene ND ug/kg 07/22/22 17:18 95-50-107/22/22 11:504051461
1,3-Dichlorobenzene ND ug/kg 07/22/22 17:18 541-73-107/22/22 11:504051441
1,4-Dichlorobenzene ND ug/kg 07/22/22 17:18 106-46-707/22/22 11:504051551
3,3'-Dichlorobenzidine ND ug/kg 07/22/22 17:18 91-94-107/22/22 11:508102741
2,4-Dichlorophenol ND ug/kg 07/22/22 17:18 120-83-207/22/22 11:504051581
Diethylphthalate ND ug/kg 07/22/22 17:18 84-66-207/22/22 11:504051481
2,4-Dimethylphenol ND ug/kg 07/22/22 17:18 105-67-907/22/22 11:504051681
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-3 Lab ID:92615483003 Collected:07/15/22 14:25 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/22/22 17:18 131-11-307/22/22 11:504051471
Di-n-butylphthalate ND ug/kg 07/22/22 17:18 84-74-207/22/22 11:504051361
4,6-Dinitro-2-methylphenol ND ug/kg 07/22/22 17:18 534-52-107/22/22 11:508103781
2,4-Dinitrophenol ND ug/kg 07/22/22 17:18 51-28-5 v207/22/22 11:50202012501
2,4-Dinitrotoluene ND ug/kg 07/22/22 17:18 121-14-207/22/22 11:504051561
2,6-Dinitrotoluene ND ug/kg 07/22/22 17:18 606-20-207/22/22 11:504051481
Di-n-octylphthalate ND ug/kg 07/22/22 17:18 117-84-007/22/22 11:504051601
bis(2-Ethylhexyl)phthalate ND ug/kg 07/22/22 17:18 117-81-707/22/22 11:504051571
Fluoranthene ND ug/kg 07/22/22 17:18 206-44-007/22/22 11:504051391
Fluorene ND ug/kg 07/22/22 17:18 86-73-707/22/22 11:504051421
Hexachloro-1,3-butadiene ND ug/kg 07/22/22 17:18 87-68-307/22/22 11:504051751
Hexachlorobenzene ND ug/kg 07/22/22 17:18 118-74-107/22/22 11:504051581
Hexachlorocyclopentadiene ND ug/kg 07/22/22 17:18 77-47-407/22/22 11:504052321
Hexachloroethane ND ug/kg 07/22/22 17:18 67-72-107/22/22 11:504051551
Indeno(1,2,3-cd)pyrene ND ug/kg 07/22/22 17:18 193-39-507/22/22 11:504051601
Isophorone ND ug/kg 07/22/22 17:18 78-59-107/22/22 11:504051801
1-Methylnaphthalene ND ug/kg 07/22/22 17:18 90-12-007/22/22 11:504051421
2-Methylnaphthalene ND ug/kg 07/22/22 17:18 91-57-607/22/22 11:504051621
2-Methylphenol(o-Cresol)ND ug/kg 07/22/22 17:18 95-48-707/22/22 11:504051661
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/22/22 17:18 15831-10-407/22/22 11:504051631
Naphthalene ND ug/kg 07/22/22 17:18 91-20-307/22/22 11:504051371
2-Nitroaniline ND ug/kg 07/22/22 17:18 88-74-407/22/22 11:5020203311
3-Nitroaniline ND ug/kg 07/22/22 17:18 99-09-207/22/22 11:5020203181
4-Nitroaniline ND ug/kg 07/22/22 17:18 100-01-607/22/22 11:508103081
Nitrobenzene ND ug/kg 07/22/22 17:18 98-95-307/22/22 11:504051881
2-Nitrophenol ND ug/kg 07/22/22 17:18 88-75-507/22/22 11:504051751
4-Nitrophenol ND ug/kg 07/22/22 17:18 100-02-707/22/22 11:5020207831
N-Nitrosodimethylamine ND ug/kg 07/22/22 17:18 62-75-907/22/22 11:504051361
N-Nitroso-di-n-propylamine ND ug/kg 07/22/22 17:18 621-64-707/22/22 11:504051521
N-Nitrosodiphenylamine ND ug/kg 07/22/22 17:18 86-30-607/22/22 11:504051441
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/22/22 17:18 108-60-107/22/22 11:504051931
Pentachlorophenol ND ug/kg 07/22/22 17:18 87-86-507/22/22 11:508103961
Phenanthrene ND ug/kg 07/22/22 17:18 85-01-807/22/22 11:504051331
Phenol ND ug/kg 07/22/22 17:18 108-95-207/22/22 11:504051801
Pyrene ND ug/kg 07/22/22 17:18 129-00-007/22/22 11:504051641
Pyridine ND ug/kg 07/22/22 17:18 110-86-107/22/22 11:504051281
1,2,4-Trichlorobenzene ND ug/kg 07/22/22 17:18 120-82-107/22/22 11:504051601
2,4,5-Trichlorophenol ND ug/kg 07/22/22 17:18 95-95-407/22/22 11:504051851
2,4,6-Trichlorophenol ND ug/kg 07/22/22 17:18 88-06-207/22/22 11:504051671
Surrogates
Nitrobenzene-d5 (S)69 %07/22/22 17:18 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)68 %07/22/22 17:18 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)82 %07/22/22 17:18 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)68 %07/22/22 17:18 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-3 Lab ID:92615483003 Collected:07/15/22 14:25 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)75 %07/22/22 17:18 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)75 %07/22/22 17:18 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 01:25 67-64-107/19/22 17:0714847.7 1
Benzene ND ug/kg 07/20/22 01:25 71-43-207/19/22 17:077.4 3.0 1
Bromobenzene ND ug/kg 07/20/22 01:25 108-86-107/19/22 17:077.4 2.4 1
Bromochloromethane ND ug/kg 07/20/22 01:25 74-97-507/19/22 17:077.4 2.2 1
Bromodichloromethane ND ug/kg 07/20/22 01:25 75-27-407/19/22 17:077.4 2.9 1
Bromoform ND ug/kg 07/20/22 01:25 75-25-207/19/22 17:077.4 2.6 1
Bromomethane ND ug/kg 07/20/22 01:25 74-83-9 L107/19/22 17:0714.8 11.7 1
2-Butanone (MEK)59.0J ug/kg 07/20/22 01:25 78-93-3 C707/19/22 17:0714835.6 1
n-Butylbenzene ND ug/kg 07/20/22 01:25 104-51-807/19/22 17:077.4 3.5 1
sec-Butylbenzene ND ug/kg 07/20/22 01:25 135-98-807/19/22 17:077.4 3.3 1
tert-Butylbenzene ND ug/kg 07/20/22 01:25 98-06-607/19/22 17:077.4 2.6 1
Carbon tetrachloride ND ug/kg 07/20/22 01:25 56-23-507/19/22 17:077.4 2.8 1
Chlorobenzene ND ug/kg 07/20/22 01:25 108-90-707/19/22 17:077.4 1.4 1
Chloroethane ND ug/kg 07/20/22 01:25 75-00-3 IH07/19/22 17:0714.8 5.7 1
Chloroform ND ug/kg 07/20/22 01:25 67-66-307/19/22 17:077.4 4.5 1
Chloromethane ND ug/kg 07/20/22 01:25 74-87-3 IH07/19/22 17:0714.8 6.2 1
2-Chlorotoluene ND ug/kg 07/20/22 01:25 95-49-807/19/22 17:077.4 2.6 1
4-Chlorotoluene ND ug/kg 07/20/22 01:25 106-43-407/19/22 17:077.4 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 01:25 96-12-8 v207/19/22 17:077.4 2.9 1
Dibromochloromethane ND ug/kg 07/20/22 01:25 124-48-107/19/22 17:077.4 4.2 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 01:25 106-93-407/19/22 17:077.4 3.3 1
Dibromomethane ND ug/kg 07/20/22 01:25 74-95-307/19/22 17:077.4 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 01:25 95-50-107/19/22 17:077.4 2.7 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 01:25 541-73-107/19/22 17:077.4 2.3 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 01:25 106-46-707/19/22 17:077.4 1.9 1
Dichlorodifluoromethane ND ug/kg 07/20/22 01:25 75-71-8 IH,L107/19/22 17:0714.8 3.2 1
1,1-Dichloroethane ND ug/kg 07/20/22 01:25 75-34-307/19/22 17:077.4 3.1 1
1,2-Dichloroethane ND ug/kg 07/20/22 01:25 107-06-207/19/22 17:077.4 4.9 1
1,1-Dichloroethene ND ug/kg 07/20/22 01:25 75-35-407/19/22 17:077.4 3.1 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 01:25 156-59-207/19/22 17:077.4 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 01:25 156-60-507/19/22 17:077.4 2.6 1
1,2-Dichloropropane ND ug/kg 07/20/22 01:25 78-87-507/19/22 17:077.4 2.2 1
1,3-Dichloropropane ND ug/kg 07/20/22 01:25 142-28-907/19/22 17:077.4 2.3 1
2,2-Dichloropropane ND ug/kg 07/20/22 01:25 594-20-707/19/22 17:077.4 2.4 1
1,1-Dichloropropene ND ug/kg 07/20/22 01:25 563-58-607/19/22 17:077.4 3.6 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 01:25 10061-01-507/19/22 17:077.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 01:25 10061-02-607/19/22 17:077.4 2.6 1
Diisopropyl ether ND ug/kg 07/20/22 01:25 108-20-307/19/22 17:077.4 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-3 Lab ID:92615483003 Collected:07/15/22 14:25 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 01:25 100-41-407/19/22 17:077.4 3.5 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 01:25 87-68-307/19/22 17:0714.8 12.1 1
2-Hexanone ND ug/kg 07/20/22 01:25 591-78-607/19/22 17:0774.2 7.2 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 01:25 98-82-807/19/22 17:077.4 2.5 1
p-Isopropyltoluene ND ug/kg 07/20/22 01:25 99-87-607/19/22 17:077.4 3.7 1
Methylene Chloride ND ug/kg 07/20/22 01:25 75-09-207/19/22 17:0729.7 20.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 01:25 108-10-107/19/22 17:0774.2 7.2 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 01:25 1634-04-407/19/22 17:077.4 2.8 1
Naphthalene ND ug/kg 07/20/22 01:25 91-20-3 v207/19/22 17:077.4 3.9 1
n-Propylbenzene ND ug/kg 07/20/22 01:25 103-65-107/19/22 17:077.4 2.6 1
Styrene ND ug/kg 07/20/22 01:25 100-42-507/19/22 17:077.4 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 01:25 630-20-607/19/22 17:077.4 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 01:25 79-34-507/19/22 17:077.4 2.0 1
Tetrachloroethene ND ug/kg 07/20/22 01:25 127-18-407/19/22 17:077.4 2.3 1
Toluene ND ug/kg 07/20/22 01:25 108-88-307/19/22 17:077.4 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 01:25 87-61-6 v207/19/22 17:077.4 6.0 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 01:25 120-82-107/19/22 17:077.4 6.2 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 01:25 71-55-607/19/22 17:077.4 3.9 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 01:25 79-00-507/19/22 17:077.4 2.5 1
Trichloroethene ND ug/kg 07/20/22 01:25 79-01-607/19/22 17:077.4 1.9 1
Trichlorofluoromethane ND ug/kg 07/20/22 01:25 75-69-407/19/22 17:077.4 4.1 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 01:25 96-18-407/19/22 17:077.4 3.8 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 01:25 95-63-607/19/22 17:077.4 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 01:25 108-67-807/19/22 17:077.4 2.5 1
Vinyl acetate ND ug/kg 07/20/22 01:25 108-05-407/19/22 17:0774.2 5.4 1
Vinyl chloride ND ug/kg 07/20/22 01:25 75-01-4 IH07/19/22 17:0714.8 3.8 1
Xylene (Total)ND ug/kg 07/20/22 01:25 1330-20-707/19/22 17:0714.8 4.2 1
m&p-Xylene ND ug/kg 07/20/22 01:25 179601-23-107/19/22 17:0714.8 5.1 1
o-Xylene ND ug/kg 07/20/22 01:25 95-47-607/19/22 17:077.4 3.3 1
Surrogates
Toluene-d8 (S)100 %07/20/22 01:25 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)101 %07/20/22 01:25 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)105 %07/20/22 01:25 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.0 %07/19/22 17:56 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 81.4 %07/22/22 19:0507/22/22 18:521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-3 Lab ID:92615483003 Collected:07/15/22 14:25 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 14:11 18540-29-908/11/22 10:211.23 0.313 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-4 Lab ID:92615483004 Collected:07/15/22 14:38 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:19 7440-38-207/20/22 11:374.3 3.0 1
Barium 89.5 mg/kg 07/20/22 16:19 7440-39-307/20/22 11:371.4 0.59 1
Cadmium ND mg/kg 07/20/22 16:19 7440-43-907/20/22 11:371.4 0.42 1
Chromium 25.9 mg/kg 07/20/22 16:19 7440-47-307/20/22 11:371.4 1.3 1
Lead 6.1 mg/kg 07/20/22 16:19 7439-92-107/20/22 11:373.6 2.2 1
Selenium ND mg/kg 07/21/22 13:29 7782-49-2 D307/20/22 11:3735.6 30.8 5
Silver ND mg/kg 07/20/22 16:19 7440-22-407/20/22 11:371.4 0.58 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.026J mg/kg 07/25/22 13:44 7439-97-607/25/22 08:300.32 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/22/22 17:45 83-32-907/22/22 11:504731661
Acenaphthylene ND ug/kg 07/22/22 17:45 208-96-807/22/22 11:504731661
Aniline ND ug/kg 07/22/22 17:45 62-53-307/22/22 11:504731851
Anthracene ND ug/kg 07/22/22 17:45 120-12-707/22/22 11:504731551
Benzo(a)anthracene ND ug/kg 07/22/22 17:45 56-55-307/22/22 11:504731581
Benzo(a)pyrene ND ug/kg 07/22/22 17:45 50-32-807/22/22 11:504731631
Benzo(b)fluoranthene ND ug/kg 07/22/22 17:45 205-99-207/22/22 11:504731581
Benzo(g,h,i)perylene ND ug/kg 07/22/22 17:45 191-24-207/22/22 11:504731841
Benzo(k)fluoranthene ND ug/kg 07/22/22 17:45 207-08-907/22/22 11:504731661
Benzoic Acid ND ug/kg 07/22/22 17:45 65-85-0 v207/22/22 11:50237010201
Benzyl alcohol ND ug/kg 07/22/22 17:45 100-51-607/22/22 11:509463581
4-Bromophenylphenyl ether ND ug/kg 07/22/22 17:45 101-55-307/22/22 11:504731821
Butylbenzylphthalate ND ug/kg 07/22/22 17:45 85-68-707/22/22 11:504731991
4-Chloro-3-methylphenol ND ug/kg 07/22/22 17:45 59-50-707/22/22 11:509463331
4-Chloroaniline ND ug/kg 07/22/22 17:45 106-47-807/22/22 11:509463711
bis(2-Chloroethoxy)methane ND ug/kg 07/22/22 17:45 111-91-107/22/22 11:504731961
bis(2-Chloroethyl) ether ND ug/kg 07/22/22 17:45 111-44-407/22/22 11:504731781
2-Chloronaphthalene ND ug/kg 07/22/22 17:45 91-58-707/22/22 11:504731881
2-Chlorophenol ND ug/kg 07/22/22 17:45 95-57-807/22/22 11:504731781
4-Chlorophenylphenyl ether ND ug/kg 07/22/22 17:45 7005-72-307/22/22 11:504731761
Chrysene ND ug/kg 07/22/22 17:45 218-01-907/22/22 11:504731721
Dibenz(a,h)anthracene ND ug/kg 07/22/22 17:45 53-70-307/22/22 11:504731821
Dibenzofuran ND ug/kg 07/22/22 17:45 132-64-907/22/22 11:504731711
1,2-Dichlorobenzene ND ug/kg 07/22/22 17:45 95-50-107/22/22 11:504731711
1,3-Dichlorobenzene ND ug/kg 07/22/22 17:45 541-73-107/22/22 11:504731681
1,4-Dichlorobenzene ND ug/kg 07/22/22 17:45 106-46-707/22/22 11:504731811
3,3'-Dichlorobenzidine ND ug/kg 07/22/22 17:45 91-94-107/22/22 11:509463201
2,4-Dichlorophenol ND ug/kg 07/22/22 17:45 120-83-207/22/22 11:504731851
Diethylphthalate ND ug/kg 07/22/22 17:45 84-66-207/22/22 11:504731731
2,4-Dimethylphenol ND ug/kg 07/22/22 17:45 105-67-907/22/22 11:504731961
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-4 Lab ID:92615483004 Collected:07/15/22 14:38 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/22/22 17:45 131-11-307/22/22 11:504731721
Di-n-butylphthalate ND ug/kg 07/22/22 17:45 84-74-207/22/22 11:504731591
4,6-Dinitro-2-methylphenol ND ug/kg 07/22/22 17:45 534-52-107/22/22 11:509464421
2,4-Dinitrophenol ND ug/kg 07/22/22 17:45 51-28-5 v207/22/22 11:50237014601
2,4-Dinitrotoluene ND ug/kg 07/22/22 17:45 121-14-207/22/22 11:504731821
2,6-Dinitrotoluene ND ug/kg 07/22/22 17:45 606-20-207/22/22 11:504731731
Di-n-octylphthalate ND ug/kg 07/22/22 17:45 117-84-007/22/22 11:504731861
bis(2-Ethylhexyl)phthalate ND ug/kg 07/22/22 17:45 117-81-707/22/22 11:504731841
Fluoranthene ND ug/kg 07/22/22 17:45 206-44-007/22/22 11:504731621
Fluorene ND ug/kg 07/22/22 17:45 86-73-707/22/22 11:504731661
Hexachloro-1,3-butadiene ND ug/kg 07/22/22 17:45 87-68-307/22/22 11:504732051
Hexachlorobenzene ND ug/kg 07/22/22 17:45 118-74-107/22/22 11:504731851
Hexachlorocyclopentadiene ND ug/kg 07/22/22 17:45 77-47-407/22/22 11:504732711
Hexachloroethane ND ug/kg 07/22/22 17:45 67-72-107/22/22 11:504731811
Indeno(1,2,3-cd)pyrene ND ug/kg 07/22/22 17:45 193-39-507/22/22 11:504731861
Isophorone ND ug/kg 07/22/22 17:45 78-59-107/22/22 11:504732111
1-Methylnaphthalene ND ug/kg 07/22/22 17:45 90-12-007/22/22 11:504731661
2-Methylnaphthalene ND ug/kg 07/22/22 17:45 91-57-607/22/22 11:504731891
2-Methylphenol(o-Cresol)ND ug/kg 07/22/22 17:45 95-48-707/22/22 11:504731941
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/22/22 17:45 15831-10-407/22/22 11:504731911
Naphthalene ND ug/kg 07/22/22 17:45 91-20-307/22/22 11:504731611
2-Nitroaniline ND ug/kg 07/22/22 17:45 88-74-407/22/22 11:5023703871
3-Nitroaniline ND ug/kg 07/22/22 17:45 99-09-207/22/22 11:5023703711
4-Nitroaniline ND ug/kg 07/22/22 17:45 100-01-607/22/22 11:509463601
Nitrobenzene ND ug/kg 07/22/22 17:45 98-95-307/22/22 11:504732191
2-Nitrophenol ND ug/kg 07/22/22 17:45 88-75-507/22/22 11:504732051
4-Nitrophenol ND ug/kg 07/22/22 17:45 100-02-707/22/22 11:5023709151
N-Nitrosodimethylamine ND ug/kg 07/22/22 17:45 62-75-907/22/22 11:504731591
N-Nitroso-di-n-propylamine ND ug/kg 07/22/22 17:45 621-64-707/22/22 11:504731781
N-Nitrosodiphenylamine ND ug/kg 07/22/22 17:45 86-30-607/22/22 11:504731681
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/22/22 17:45 108-60-107/22/22 11:504732251
Pentachlorophenol ND ug/kg 07/22/22 17:45 87-86-507/22/22 11:509464631
Phenanthrene ND ug/kg 07/22/22 17:45 85-01-807/22/22 11:504731551
Phenol ND ug/kg 07/22/22 17:45 108-95-207/22/22 11:504732111
Pyrene ND ug/kg 07/22/22 17:45 129-00-007/22/22 11:504731921
Pyridine ND ug/kg 07/22/22 17:45 110-86-107/22/22 11:504731491
1,2,4-Trichlorobenzene ND ug/kg 07/22/22 17:45 120-82-107/22/22 11:504731861
2,4,5-Trichlorophenol ND ug/kg 07/22/22 17:45 95-95-407/22/22 11:504732171
2,4,6-Trichlorophenol ND ug/kg 07/22/22 17:45 88-06-207/22/22 11:504731951
Surrogates
Nitrobenzene-d5 (S)69 %07/22/22 17:45 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)66 %07/22/22 17:45 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)79 %07/22/22 17:45 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)70 %07/22/22 17:45 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-4 Lab ID:92615483004 Collected:07/15/22 14:38 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)70 %07/22/22 17:45 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)74 %07/22/22 17:45 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 02:00 67-64-107/19/22 17:0718057.9 1
Benzene ND ug/kg 07/20/22 02:00 71-43-207/19/22 17:079.0 3.6 1
Bromobenzene ND ug/kg 07/20/22 02:00 108-86-107/19/22 17:079.0 2.9 1
Bromochloromethane ND ug/kg 07/20/22 02:00 74-97-507/19/22 17:079.0 2.7 1
Bromodichloromethane ND ug/kg 07/20/22 02:00 75-27-407/19/22 17:079.0 3.5 1
Bromoform ND ug/kg 07/20/22 02:00 75-25-207/19/22 17:079.0 3.2 1
Bromomethane ND ug/kg 07/20/22 02:00 74-83-9 L107/19/22 17:0718.0 14.2 1
2-Butanone (MEK)62.6J ug/kg 07/20/22 02:00 78-93-3 C707/19/22 17:0718043.3 1
n-Butylbenzene ND ug/kg 07/20/22 02:00 104-51-807/19/22 17:079.0 4.3 1
sec-Butylbenzene ND ug/kg 07/20/22 02:00 135-98-807/19/22 17:079.0 4.0 1
tert-Butylbenzene ND ug/kg 07/20/22 02:00 98-06-607/19/22 17:079.0 3.2 1
Carbon tetrachloride ND ug/kg 07/20/22 02:00 56-23-507/19/22 17:079.0 3.4 1
Chlorobenzene ND ug/kg 07/20/22 02:00 108-90-707/19/22 17:079.0 1.7 1
Chloroethane ND ug/kg 07/20/22 02:00 75-00-3 IH07/19/22 17:0718.0 7.0 1
Chloroform ND ug/kg 07/20/22 02:00 67-66-307/19/22 17:079.0 5.5 1
Chloromethane ND ug/kg 07/20/22 02:00 74-87-3 IH07/19/22 17:0718.0 7.6 1
2-Chlorotoluene ND ug/kg 07/20/22 02:00 95-49-807/19/22 17:079.0 3.2 1
4-Chlorotoluene ND ug/kg 07/20/22 02:00 106-43-407/19/22 17:079.0 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 02:00 96-12-8 v207/19/22 17:079.0 3.5 1
Dibromochloromethane ND ug/kg 07/20/22 02:00 124-48-107/19/22 17:079.0 5.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 02:00 106-93-407/19/22 17:079.0 4.0 1
Dibromomethane ND ug/kg 07/20/22 02:00 74-95-307/19/22 17:079.0 1.9 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 02:00 95-50-107/19/22 17:079.0 3.2 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 02:00 541-73-107/19/22 17:079.0 2.8 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 02:00 106-46-707/19/22 17:079.0 2.3 1
Dichlorodifluoromethane ND ug/kg 07/20/22 02:00 75-71-8 IH,L107/19/22 17:0718.0 3.9 1
1,1-Dichloroethane ND ug/kg 07/20/22 02:00 75-34-307/19/22 17:079.0 3.7 1
1,2-Dichloroethane ND ug/kg 07/20/22 02:00 107-06-207/19/22 17:079.0 6.0 1
1,1-Dichloroethene ND ug/kg 07/20/22 02:00 75-35-407/19/22 17:079.0 3.7 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 02:00 156-59-207/19/22 17:079.0 3.1 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 02:00 156-60-507/19/22 17:079.0 3.2 1
1,2-Dichloropropane ND ug/kg 07/20/22 02:00 78-87-507/19/22 17:079.0 2.7 1
1,3-Dichloropropane ND ug/kg 07/20/22 02:00 142-28-907/19/22 17:079.0 2.8 1
2,2-Dichloropropane ND ug/kg 07/20/22 02:00 594-20-707/19/22 17:079.0 2.9 1
1,1-Dichloropropene ND ug/kg 07/20/22 02:00 563-58-607/19/22 17:079.0 4.3 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 02:00 10061-01-507/19/22 17:079.0 2.5 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 02:00 10061-02-607/19/22 17:079.0 3.1 1
Diisopropyl ether ND ug/kg 07/20/22 02:00 108-20-307/19/22 17:079.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-4 Lab ID:92615483004 Collected:07/15/22 14:38 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 02:00 100-41-407/19/22 17:079.0 4.2 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 02:00 87-68-307/19/22 17:0718.0 14.7 1
2-Hexanone ND ug/kg 07/20/22 02:00 591-78-607/19/22 17:0790.2 8.7 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 02:00 98-82-807/19/22 17:079.0 3.1 1
p-Isopropyltoluene ND ug/kg 07/20/22 02:00 99-87-607/19/22 17:079.0 4.4 1
Methylene Chloride ND ug/kg 07/20/22 02:00 75-09-207/19/22 17:0736.1 24.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 02:00 108-10-107/19/22 17:0790.2 8.7 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 02:00 1634-04-407/19/22 17:079.0 3.4 1
Naphthalene ND ug/kg 07/20/22 02:00 91-20-3 v207/19/22 17:079.0 4.7 1
n-Propylbenzene ND ug/kg 07/20/22 02:00 103-65-107/19/22 17:079.0 3.2 1
Styrene ND ug/kg 07/20/22 02:00 100-42-507/19/22 17:079.0 2.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 02:00 630-20-607/19/22 17:079.0 3.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 02:00 79-34-507/19/22 17:079.0 2.4 1
Tetrachloroethene ND ug/kg 07/20/22 02:00 127-18-407/19/22 17:079.0 2.8 1
Toluene ND ug/kg 07/20/22 02:00 108-88-307/19/22 17:079.0 2.6 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 02:00 87-61-6 v207/19/22 17:079.0 7.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 02:00 120-82-107/19/22 17:079.0 7.6 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 02:00 71-55-607/19/22 17:079.0 4.7 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 02:00 79-00-507/19/22 17:079.0 3.0 1
Trichloroethene ND ug/kg 07/20/22 02:00 79-01-607/19/22 17:079.0 2.3 1
Trichlorofluoromethane ND ug/kg 07/20/22 02:00 75-69-407/19/22 17:079.0 5.0 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 02:00 96-18-407/19/22 17:079.0 4.6 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 02:00 95-63-607/19/22 17:079.0 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 02:00 108-67-807/19/22 17:079.0 3.0 1
Vinyl acetate ND ug/kg 07/20/22 02:00 108-05-407/19/22 17:0790.2 6.6 1
Vinyl chloride ND ug/kg 07/20/22 02:00 75-01-4 IH07/19/22 17:0718.0 4.6 1
Xylene (Total)ND ug/kg 07/20/22 02:00 1330-20-707/19/22 17:0718.0 5.1 1
m&p-Xylene ND ug/kg 07/20/22 02:00 179601-23-107/19/22 17:0718.0 6.2 1
o-Xylene ND ug/kg 07/20/22 02:00 95-47-607/19/22 17:079.0 4.0 1
Surrogates
Toluene-d8 (S)100 %07/20/22 02:00 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)101 %07/20/22 02:00 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)104 %07/20/22 02:00 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.8 %07/19/22 17:56 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.5 %07/22/22 19:0507/22/22 18:521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-4 Lab ID:92615483004 Collected:07/15/22 14:38 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 14:16 18540-29-908/11/22 10:211.42 0.361 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-5 Lab ID:92615483005 Collected:07/15/22 15:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:24 7440-38-207/20/22 11:374.0 2.8 1
Barium 177 mg/kg 07/20/22 16:24 7440-39-307/20/22 11:371.3 0.55 1
Cadmium ND mg/kg 07/20/22 16:24 7440-43-907/20/22 11:371.3 0.39 1
Chromium 6.6 mg/kg 07/20/22 16:24 7440-47-307/20/22 11:371.3 1.2 1
Lead 6.5 mg/kg 07/20/22 16:24 7439-92-107/20/22 11:373.3 2.1 1
Selenium ND mg/kg 07/21/22 13:33 7782-49-2 D307/20/22 11:3733.0 28.6 5
Silver ND mg/kg 07/20/22 16:24 7440-22-407/20/22 11:371.3 0.54 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.030J mg/kg 07/25/22 13:47 7439-97-607/25/22 08:300.33 0.014 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/22/22 18:13 83-32-907/22/22 11:504401551
Acenaphthylene ND ug/kg 07/22/22 18:13 208-96-807/22/22 11:504401551
Aniline ND ug/kg 07/22/22 18:13 62-53-307/22/22 11:504401721
Anthracene ND ug/kg 07/22/22 18:13 120-12-707/22/22 11:504401441
Benzo(a)anthracene ND ug/kg 07/22/22 18:13 56-55-307/22/22 11:504401471
Benzo(a)pyrene ND ug/kg 07/22/22 18:13 50-32-807/22/22 11:504401521
Benzo(b)fluoranthene ND ug/kg 07/22/22 18:13 205-99-207/22/22 11:504401471
Benzo(g,h,i)perylene ND ug/kg 07/22/22 18:13 191-24-207/22/22 11:504401711
Benzo(k)fluoranthene ND ug/kg 07/22/22 18:13 207-08-907/22/22 11:504401551
Benzoic Acid ND ug/kg 07/22/22 18:13 65-85-0 v207/22/22 11:5022009461
Benzyl alcohol ND ug/kg 07/22/22 18:13 100-51-607/22/22 11:508813341
4-Bromophenylphenyl ether ND ug/kg 07/22/22 18:13 101-55-307/22/22 11:504401691
Butylbenzylphthalate ND ug/kg 07/22/22 18:13 85-68-707/22/22 11:504401861
4-Chloro-3-methylphenol ND ug/kg 07/22/22 18:13 59-50-707/22/22 11:508813101
4-Chloroaniline ND ug/kg 07/22/22 18:13 106-47-807/22/22 11:508813461
bis(2-Chloroethoxy)methane ND ug/kg 07/22/22 18:13 111-91-107/22/22 11:504401831
bis(2-Chloroethyl) ether ND ug/kg 07/22/22 18:13 111-44-407/22/22 11:504401651
2-Chloronaphthalene ND ug/kg 07/22/22 18:13 91-58-707/22/22 11:504401751
2-Chlorophenol ND ug/kg 07/22/22 18:13 95-57-807/22/22 11:504401651
4-Chlorophenylphenyl ether ND ug/kg 07/22/22 18:13 7005-72-307/22/22 11:504401641
Chrysene ND ug/kg 07/22/22 18:13 218-01-907/22/22 11:504401601
Dibenz(a,h)anthracene ND ug/kg 07/22/22 18:13 53-70-307/22/22 11:504401691
Dibenzofuran ND ug/kg 07/22/22 18:13 132-64-907/22/22 11:504401591
1,2-Dichlorobenzene ND ug/kg 07/22/22 18:13 95-50-107/22/22 11:504401591
1,3-Dichlorobenzene ND ug/kg 07/22/22 18:13 541-73-107/22/22 11:504401561
1,4-Dichlorobenzene ND ug/kg 07/22/22 18:13 106-46-707/22/22 11:504401681
3,3'-Dichlorobenzidine ND ug/kg 07/22/22 18:13 91-94-107/22/22 11:508812981
2,4-Dichlorophenol ND ug/kg 07/22/22 18:13 120-83-207/22/22 11:504401721
Diethylphthalate ND ug/kg 07/22/22 18:13 84-66-207/22/22 11:504401611
2,4-Dimethylphenol ND ug/kg 07/22/22 18:13 105-67-907/22/22 11:504401831
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-5 Lab ID:92615483005 Collected:07/15/22 15:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/22/22 18:13 131-11-307/22/22 11:504401601
Di-n-butylphthalate ND ug/kg 07/22/22 18:13 84-74-207/22/22 11:504401481
4,6-Dinitro-2-methylphenol ND ug/kg 07/22/22 18:13 534-52-107/22/22 11:508814111
2,4-Dinitrophenol ND ug/kg 07/22/22 18:13 51-28-5 v207/22/22 11:50220013601
2,4-Dinitrotoluene ND ug/kg 07/22/22 18:13 121-14-207/22/22 11:504401691
2,6-Dinitrotoluene ND ug/kg 07/22/22 18:13 606-20-207/22/22 11:504401611
Di-n-octylphthalate ND ug/kg 07/22/22 18:13 117-84-007/22/22 11:504401741
bis(2-Ethylhexyl)phthalate ND ug/kg 07/22/22 18:13 117-81-707/22/22 11:504401711
Fluoranthene ND ug/kg 07/22/22 18:13 206-44-007/22/22 11:504401511
Fluorene ND ug/kg 07/22/22 18:13 86-73-707/22/22 11:504401551
Hexachloro-1,3-butadiene ND ug/kg 07/22/22 18:13 87-68-307/22/22 11:504401911
Hexachlorobenzene ND ug/kg 07/22/22 18:13 118-74-107/22/22 11:504401721
Hexachlorocyclopentadiene ND ug/kg 07/22/22 18:13 77-47-407/22/22 11:504402521
Hexachloroethane ND ug/kg 07/22/22 18:13 67-72-107/22/22 11:504401681
Indeno(1,2,3-cd)pyrene ND ug/kg 07/22/22 18:13 193-39-507/22/22 11:504401741
Isophorone ND ug/kg 07/22/22 18:13 78-59-107/22/22 11:504401961
1-Methylnaphthalene ND ug/kg 07/22/22 18:13 90-12-007/22/22 11:504401551
2-Methylnaphthalene ND ug/kg 07/22/22 18:13 91-57-607/22/22 11:504401761
2-Methylphenol(o-Cresol)ND ug/kg 07/22/22 18:13 95-48-707/22/22 11:504401801
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/22/22 18:13 15831-10-407/22/22 11:504401781
Naphthalene ND ug/kg 07/22/22 18:13 91-20-307/22/22 11:504401491
2-Nitroaniline ND ug/kg 07/22/22 18:13 88-74-407/22/22 11:5022003601
3-Nitroaniline ND ug/kg 07/22/22 18:13 99-09-207/22/22 11:5022003461
4-Nitroaniline ND ug/kg 07/22/22 18:13 100-01-607/22/22 11:508813351
Nitrobenzene ND ug/kg 07/22/22 18:13 98-95-307/22/22 11:504402041
2-Nitrophenol ND ug/kg 07/22/22 18:13 88-75-507/22/22 11:504401911
4-Nitrophenol ND ug/kg 07/22/22 18:13 100-02-707/22/22 11:5022008521
N-Nitrosodimethylamine ND ug/kg 07/22/22 18:13 62-75-907/22/22 11:504401481
N-Nitroso-di-n-propylamine ND ug/kg 07/22/22 18:13 621-64-707/22/22 11:504401651
N-Nitrosodiphenylamine ND ug/kg 07/22/22 18:13 86-30-607/22/22 11:504401561
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/22/22 18:13 108-60-107/22/22 11:504402101
Pentachlorophenol ND ug/kg 07/22/22 18:13 87-86-507/22/22 11:508814311
Phenanthrene ND ug/kg 07/22/22 18:13 85-01-807/22/22 11:504401441
Phenol ND ug/kg 07/22/22 18:13 108-95-207/22/22 11:504401961
Pyrene ND ug/kg 07/22/22 18:13 129-00-007/22/22 11:504401791
Pyridine ND ug/kg 07/22/22 18:13 110-86-107/22/22 11:504401391
1,2,4-Trichlorobenzene ND ug/kg 07/22/22 18:13 120-82-107/22/22 11:504401741
2,4,5-Trichlorophenol ND ug/kg 07/22/22 18:13 95-95-407/22/22 11:504402021
2,4,6-Trichlorophenol ND ug/kg 07/22/22 18:13 88-06-207/22/22 11:504401821
Surrogates
Nitrobenzene-d5 (S)72 %07/22/22 18:13 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)64 %07/22/22 18:13 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)79 %07/22/22 18:13 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)67 %07/22/22 18:13 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-5 Lab ID:92615483005 Collected:07/15/22 15:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)63 %07/22/22 18:13 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)75 %07/22/22 18:13 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 02:18 67-64-107/19/22 17:0716954.3 1
Benzene ND ug/kg 07/20/22 02:18 71-43-207/19/22 17:078.5 3.4 1
Bromobenzene ND ug/kg 07/20/22 02:18 108-86-107/19/22 17:078.5 2.8 1
Bromochloromethane ND ug/kg 07/20/22 02:18 74-97-507/19/22 17:078.5 2.5 1
Bromodichloromethane ND ug/kg 07/20/22 02:18 75-27-407/19/22 17:078.5 3.3 1
Bromoform ND ug/kg 07/20/22 02:18 75-25-207/19/22 17:078.5 3.0 1
Bromomethane ND ug/kg 07/20/22 02:18 74-83-9 L107/19/22 17:0716.9 13.4 1
2-Butanone (MEK)56.7J ug/kg 07/20/22 02:18 78-93-3 C707/19/22 17:0716940.6 1
n-Butylbenzene ND ug/kg 07/20/22 02:18 104-51-807/19/22 17:078.5 4.0 1
sec-Butylbenzene ND ug/kg 07/20/22 02:18 135-98-807/19/22 17:078.5 3.7 1
tert-Butylbenzene ND ug/kg 07/20/22 02:18 98-06-607/19/22 17:078.5 3.0 1
Carbon tetrachloride ND ug/kg 07/20/22 02:18 56-23-507/19/22 17:078.5 3.2 1
Chlorobenzene ND ug/kg 07/20/22 02:18 108-90-707/19/22 17:078.5 1.6 1
Chloroethane ND ug/kg 07/20/22 02:18 75-00-3 IH07/19/22 17:0716.9 6.5 1
Chloroform ND ug/kg 07/20/22 02:18 67-66-307/19/22 17:078.5 5.1 1
Chloromethane ND ug/kg 07/20/22 02:18 74-87-3 IH07/19/22 17:0716.9 7.1 1
2-Chlorotoluene ND ug/kg 07/20/22 02:18 95-49-807/19/22 17:078.5 3.0 1
4-Chlorotoluene ND ug/kg 07/20/22 02:18 106-43-407/19/22 17:078.5 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 02:18 96-12-8 v207/19/22 17:078.5 3.3 1
Dibromochloromethane ND ug/kg 07/20/22 02:18 124-48-107/19/22 17:078.5 4.8 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 02:18 106-93-407/19/22 17:078.5 3.7 1
Dibromomethane ND ug/kg 07/20/22 02:18 74-95-307/19/22 17:078.5 1.8 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 02:18 95-50-107/19/22 17:078.5 3.0 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 02:18 541-73-107/19/22 17:078.5 2.6 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 02:18 106-46-707/19/22 17:078.5 2.2 1
Dichlorodifluoromethane ND ug/kg 07/20/22 02:18 75-71-8 IH,L107/19/22 17:0716.9 3.7 1
1,1-Dichloroethane ND ug/kg 07/20/22 02:18 75-34-307/19/22 17:078.5 3.5 1
1,2-Dichloroethane ND ug/kg 07/20/22 02:18 107-06-207/19/22 17:078.5 5.6 1
1,1-Dichloroethene ND ug/kg 07/20/22 02:18 75-35-407/19/22 17:078.5 3.5 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 02:18 156-59-207/19/22 17:078.5 2.9 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 02:18 156-60-507/19/22 17:078.5 3.0 1
1,2-Dichloropropane ND ug/kg 07/20/22 02:18 78-87-507/19/22 17:078.5 2.5 1
1,3-Dichloropropane ND ug/kg 07/20/22 02:18 142-28-907/19/22 17:078.5 2.6 1
2,2-Dichloropropane ND ug/kg 07/20/22 02:18 594-20-707/19/22 17:078.5 2.8 1
1,1-Dichloropropene ND ug/kg 07/20/22 02:18 563-58-607/19/22 17:078.5 4.1 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 02:18 10061-01-507/19/22 17:078.5 2.3 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 02:18 10061-02-607/19/22 17:078.5 2.9 1
Diisopropyl ether ND ug/kg 07/20/22 02:18 108-20-307/19/22 17:078.5 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-5 Lab ID:92615483005 Collected:07/15/22 15:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 02:18 100-41-407/19/22 17:078.5 3.9 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 02:18 87-68-307/19/22 17:0716.9 13.8 1
2-Hexanone ND ug/kg 07/20/22 02:18 591-78-607/19/22 17:0784.5 8.1 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 02:18 98-82-807/19/22 17:078.5 2.9 1
p-Isopropyltoluene ND ug/kg 07/20/22 02:18 99-87-607/19/22 17:078.5 4.2 1
Methylene Chloride 37.0 ug/kg 07/20/22 02:18 75-09-2 C707/19/22 17:0733.8 23.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 02:18 108-10-107/19/22 17:0784.5 8.1 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 02:18 1634-04-407/19/22 17:078.5 3.2 1
Naphthalene ND ug/kg 07/20/22 02:18 91-20-3 v207/19/22 17:078.5 4.4 1
n-Propylbenzene ND ug/kg 07/20/22 02:18 103-65-107/19/22 17:078.5 3.0 1
Styrene ND ug/kg 07/20/22 02:18 100-42-507/19/22 17:078.5 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 02:18 630-20-607/19/22 17:078.5 3.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 02:18 79-34-507/19/22 17:078.5 2.2 1
Tetrachloroethene ND ug/kg 07/20/22 02:18 127-18-407/19/22 17:078.5 2.7 1
Toluene ND ug/kg 07/20/22 02:18 108-88-307/19/22 17:078.5 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 02:18 87-61-6 v207/19/22 17:078.5 6.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 02:18 120-82-107/19/22 17:078.5 7.1 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 02:18 71-55-607/19/22 17:078.5 4.4 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 02:18 79-00-507/19/22 17:078.5 2.8 1
Trichloroethene ND ug/kg 07/20/22 02:18 79-01-607/19/22 17:078.5 2.2 1
Trichlorofluoromethane ND ug/kg 07/20/22 02:18 75-69-407/19/22 17:078.5 4.6 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 02:18 96-18-407/19/22 17:078.5 4.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 02:18 95-63-607/19/22 17:078.5 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 02:18 108-67-807/19/22 17:078.5 2.8 1
Vinyl acetate ND ug/kg 07/20/22 02:18 108-05-407/19/22 17:0784.5 6.2 1
Vinyl chloride ND ug/kg 07/20/22 02:18 75-01-4 IH07/19/22 17:0716.9 4.3 1
Xylene (Total)ND ug/kg 07/20/22 02:18 1330-20-707/19/22 17:0716.9 4.8 1
m&p-Xylene ND ug/kg 07/20/22 02:18 179601-23-107/19/22 17:0716.9 5.8 1
o-Xylene ND ug/kg 07/20/22 02:18 95-47-607/19/22 17:078.5 3.7 1
Surrogates
Toluene-d8 (S)101 %07/20/22 02:18 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)98 %07/20/22 02:18 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)106 %07/20/22 02:18 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.8 %07/19/22 17:56 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.3 %07/23/22 11:2507/23/22 10:481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-5 Lab ID:92615483005 Collected:07/15/22 15:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 14:42 18540-29-908/11/22 10:211.38 0.353 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-6 Lab ID:92615483006 Collected:07/15/22 15:15 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:29 7440-38-207/20/22 11:373.6 2.6 1
Barium 40.8 mg/kg 07/20/22 16:29 7440-39-307/20/22 11:371.2 0.50 1
Cadmium ND mg/kg 07/20/22 16:29 7440-43-907/20/22 11:371.2 0.36 1
Chromium 25.5 mg/kg 07/20/22 16:29 7440-47-307/20/22 11:371.2 1.1 1
Lead 9.9 mg/kg 07/20/22 16:29 7439-92-107/20/22 11:373.0 1.9 1
Selenium ND mg/kg 07/21/22 13:38 7782-49-2 D307/20/22 11:3730.2 26.1 5
Silver ND mg/kg 07/20/22 16:29 7440-22-407/20/22 11:371.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.054J mg/kg 07/25/22 13:49 7439-97-607/25/22 08:300.31 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/22/22 18:40 83-32-907/22/22 11:504231491
Acenaphthylene ND ug/kg 07/22/22 18:40 208-96-807/22/22 11:504231491
Aniline ND ug/kg 07/22/22 18:40 62-53-307/22/22 11:504231651
Anthracene ND ug/kg 07/22/22 18:40 120-12-707/22/22 11:504231381
Benzo(a)anthracene ND ug/kg 07/22/22 18:40 56-55-307/22/22 11:504231411
Benzo(a)pyrene ND ug/kg 07/22/22 18:40 50-32-807/22/22 11:504231461
Benzo(b)fluoranthene ND ug/kg 07/22/22 18:40 205-99-207/22/22 11:504231411
Benzo(g,h,i)perylene ND ug/kg 07/22/22 18:40 191-24-207/22/22 11:504231641
Benzo(k)fluoranthene ND ug/kg 07/22/22 18:40 207-08-907/22/22 11:504231491
Benzoic Acid ND ug/kg 07/22/22 18:40 65-85-0 v207/22/22 11:5021209091
Benzyl alcohol ND ug/kg 07/22/22 18:40 100-51-607/22/22 11:508463211
4-Bromophenylphenyl ether ND ug/kg 07/22/22 18:40 101-55-307/22/22 11:504231631
Butylbenzylphthalate ND ug/kg 07/22/22 18:40 85-68-707/22/22 11:504231781
4-Chloro-3-methylphenol ND ug/kg 07/22/22 18:40 59-50-707/22/22 11:508462971
4-Chloroaniline ND ug/kg 07/22/22 18:40 106-47-807/22/22 11:508463321
bis(2-Chloroethoxy)methane ND ug/kg 07/22/22 18:40 111-91-107/22/22 11:504231761
bis(2-Chloroethyl) ether ND ug/kg 07/22/22 18:40 111-44-407/22/22 11:504231591
2-Chloronaphthalene ND ug/kg 07/22/22 18:40 91-58-707/22/22 11:504231681
2-Chlorophenol ND ug/kg 07/22/22 18:40 95-57-807/22/22 11:504231591
4-Chlorophenylphenyl ether ND ug/kg 07/22/22 18:40 7005-72-307/22/22 11:504231581
Chrysene ND ug/kg 07/22/22 18:40 218-01-907/22/22 11:504231541
Dibenz(a,h)anthracene ND ug/kg 07/22/22 18:40 53-70-307/22/22 11:504231631
Dibenzofuran ND ug/kg 07/22/22 18:40 132-64-907/22/22 11:504231531
1,2-Dichlorobenzene ND ug/kg 07/22/22 18:40 95-50-107/22/22 11:504231531
1,3-Dichlorobenzene ND ug/kg 07/22/22 18:40 541-73-107/22/22 11:504231501
1,4-Dichlorobenzene ND ug/kg 07/22/22 18:40 106-46-707/22/22 11:504231621
3,3'-Dichlorobenzidine ND ug/kg 07/22/22 18:40 91-94-107/22/22 11:508462861
2,4-Dichlorophenol ND ug/kg 07/22/22 18:40 120-83-207/22/22 11:504231651
Diethylphthalate ND ug/kg 07/22/22 18:40 84-66-207/22/22 11:504231551
2,4-Dimethylphenol ND ug/kg 07/22/22 18:40 105-67-907/22/22 11:504231761
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-6 Lab ID:92615483006 Collected:07/15/22 15:15 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/22/22 18:40 131-11-307/22/22 11:504231541
Di-n-butylphthalate ND ug/kg 07/22/22 18:40 84-74-207/22/22 11:504231421
4,6-Dinitro-2-methylphenol ND ug/kg 07/22/22 18:40 534-52-107/22/22 11:508463951
2,4-Dinitrophenol ND ug/kg 07/22/22 18:40 51-28-5 v207/22/22 11:50212013101
2,4-Dinitrotoluene ND ug/kg 07/22/22 18:40 121-14-207/22/22 11:504231631
2,6-Dinitrotoluene ND ug/kg 07/22/22 18:40 606-20-207/22/22 11:504231551
Di-n-octylphthalate ND ug/kg 07/22/22 18:40 117-84-007/22/22 11:504231671
bis(2-Ethylhexyl)phthalate ND ug/kg 07/22/22 18:40 117-81-707/22/22 11:504231641
Fluoranthene ND ug/kg 07/22/22 18:40 206-44-007/22/22 11:504231451
Fluorene ND ug/kg 07/22/22 18:40 86-73-707/22/22 11:504231491
Hexachloro-1,3-butadiene ND ug/kg 07/22/22 18:40 87-68-307/22/22 11:504231831
Hexachlorobenzene ND ug/kg 07/22/22 18:40 118-74-107/22/22 11:504231651
Hexachlorocyclopentadiene ND ug/kg 07/22/22 18:40 77-47-407/22/22 11:504232421
Hexachloroethane ND ug/kg 07/22/22 18:40 67-72-107/22/22 11:504231621
Indeno(1,2,3-cd)pyrene ND ug/kg 07/22/22 18:40 193-39-507/22/22 11:504231671
Isophorone ND ug/kg 07/22/22 18:40 78-59-107/22/22 11:504231881
1-Methylnaphthalene ND ug/kg 07/22/22 18:40 90-12-007/22/22 11:504231491
2-Methylnaphthalene ND ug/kg 07/22/22 18:40 91-57-607/22/22 11:504231691
2-Methylphenol(o-Cresol)ND ug/kg 07/22/22 18:40 95-48-707/22/22 11:504231731
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/22/22 18:40 15831-10-407/22/22 11:504231711
Naphthalene ND ug/kg 07/22/22 18:40 91-20-307/22/22 11:504231441
2-Nitroaniline ND ug/kg 07/22/22 18:40 88-74-407/22/22 11:5021203461
3-Nitroaniline ND ug/kg 07/22/22 18:40 99-09-207/22/22 11:5021203321
4-Nitroaniline ND ug/kg 07/22/22 18:40 100-01-607/22/22 11:508463221
Nitrobenzene ND ug/kg 07/22/22 18:40 98-95-307/22/22 11:504231961
2-Nitrophenol ND ug/kg 07/22/22 18:40 88-75-507/22/22 11:504231831
4-Nitrophenol ND ug/kg 07/22/22 18:40 100-02-707/22/22 11:5021208181
N-Nitrosodimethylamine ND ug/kg 07/22/22 18:40 62-75-907/22/22 11:504231421
N-Nitroso-di-n-propylamine ND ug/kg 07/22/22 18:40 621-64-707/22/22 11:504231591
N-Nitrosodiphenylamine ND ug/kg 07/22/22 18:40 86-30-607/22/22 11:504231501
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/22/22 18:40 108-60-107/22/22 11:504232011
Pentachlorophenol ND ug/kg 07/22/22 18:40 87-86-507/22/22 11:508464141
Phenanthrene ND ug/kg 07/22/22 18:40 85-01-807/22/22 11:504231381
Phenol ND ug/kg 07/22/22 18:40 108-95-207/22/22 11:504231881
Pyrene ND ug/kg 07/22/22 18:40 129-00-007/22/22 11:504231721
Pyridine ND ug/kg 07/22/22 18:40 110-86-107/22/22 11:504231331
1,2,4-Trichlorobenzene ND ug/kg 07/22/22 18:40 120-82-107/22/22 11:504231671
2,4,5-Trichlorophenol ND ug/kg 07/22/22 18:40 95-95-407/22/22 11:504231941
2,4,6-Trichlorophenol ND ug/kg 07/22/22 18:40 88-06-207/22/22 11:504231741
Surrogates
Nitrobenzene-d5 (S)68 %07/22/22 18:40 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)62 %07/22/22 18:40 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)79 %07/22/22 18:40 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)67 %07/22/22 18:40 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-6 Lab ID:92615483006 Collected:07/15/22 15:15 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)65 %07/22/22 18:40 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)75 %07/22/22 18:40 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 02:36 67-64-107/19/22 17:0714345.8 1
Benzene ND ug/kg 07/20/22 02:36 71-43-207/19/22 17:077.1 2.8 1
Bromobenzene ND ug/kg 07/20/22 02:36 108-86-107/19/22 17:077.1 2.3 1
Bromochloromethane ND ug/kg 07/20/22 02:36 74-97-507/19/22 17:077.1 2.1 1
Bromodichloromethane ND ug/kg 07/20/22 02:36 75-27-407/19/22 17:077.1 2.8 1
Bromoform ND ug/kg 07/20/22 02:36 75-25-207/19/22 17:077.1 2.5 1
Bromomethane ND ug/kg 07/20/22 02:36 74-83-9 L107/19/22 17:0714.3 11.3 1
2-Butanone (MEK)40.3J ug/kg 07/20/22 02:36 78-93-3 C707/19/22 17:0714334.3 1
n-Butylbenzene ND ug/kg 07/20/22 02:36 104-51-807/19/22 17:077.1 3.4 1
sec-Butylbenzene ND ug/kg 07/20/22 02:36 135-98-807/19/22 17:077.1 3.1 1
tert-Butylbenzene ND ug/kg 07/20/22 02:36 98-06-607/19/22 17:077.1 2.5 1
Carbon tetrachloride ND ug/kg 07/20/22 02:36 56-23-507/19/22 17:077.1 2.7 1
Chlorobenzene ND ug/kg 07/20/22 02:36 108-90-707/19/22 17:077.1 1.4 1
Chloroethane ND ug/kg 07/20/22 02:36 75-00-3 IH07/19/22 17:0714.3 5.5 1
Chloroform ND ug/kg 07/20/22 02:36 67-66-307/19/22 17:077.1 4.3 1
Chloromethane ND ug/kg 07/20/22 02:36 74-87-3 IH07/19/22 17:0714.3 6.0 1
2-Chlorotoluene ND ug/kg 07/20/22 02:36 95-49-807/19/22 17:077.1 2.5 1
4-Chlorotoluene ND ug/kg 07/20/22 02:36 106-43-407/19/22 17:077.1 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 02:36 96-12-8 v207/19/22 17:077.1 2.8 1
Dibromochloromethane ND ug/kg 07/20/22 02:36 124-48-107/19/22 17:077.1 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 02:36 106-93-407/19/22 17:077.1 3.1 1
Dibromomethane ND ug/kg 07/20/22 02:36 74-95-307/19/22 17:077.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 02:36 95-50-107/19/22 17:077.1 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 02:36 541-73-107/19/22 17:077.1 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 02:36 106-46-707/19/22 17:077.1 1.9 1
Dichlorodifluoromethane ND ug/kg 07/20/22 02:36 75-71-8 IH,L107/19/22 17:0714.3 3.1 1
1,1-Dichloroethane ND ug/kg 07/20/22 02:36 75-34-307/19/22 17:077.1 2.9 1
1,2-Dichloroethane ND ug/kg 07/20/22 02:36 107-06-207/19/22 17:077.1 4.7 1
1,1-Dichloroethene ND ug/kg 07/20/22 02:36 75-35-407/19/22 17:077.1 2.9 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 02:36 156-59-207/19/22 17:077.1 2.4 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 02:36 156-60-507/19/22 17:077.1 2.5 1
1,2-Dichloropropane ND ug/kg 07/20/22 02:36 78-87-507/19/22 17:077.1 2.1 1
1,3-Dichloropropane ND ug/kg 07/20/22 02:36 142-28-907/19/22 17:077.1 2.2 1
2,2-Dichloropropane ND ug/kg 07/20/22 02:36 594-20-707/19/22 17:077.1 2.3 1
1,1-Dichloropropene ND ug/kg 07/20/22 02:36 563-58-607/19/22 17:077.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 02:36 10061-01-507/19/22 17:077.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 02:36 10061-02-607/19/22 17:077.1 2.5 1
Diisopropyl ether ND ug/kg 07/20/22 02:36 108-20-307/19/22 17:077.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-6 Lab ID:92615483006 Collected:07/15/22 15:15 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 02:36 100-41-407/19/22 17:077.1 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 02:36 87-68-307/19/22 17:0714.3 11.7 1
2-Hexanone ND ug/kg 07/20/22 02:36 591-78-607/19/22 17:0771.4 6.9 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 02:36 98-82-807/19/22 17:077.1 2.4 1
p-Isopropyltoluene ND ug/kg 07/20/22 02:36 99-87-607/19/22 17:077.1 3.5 1
Methylene Chloride ND ug/kg 07/20/22 02:36 75-09-207/19/22 17:0728.6 19.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 02:36 108-10-107/19/22 17:0771.4 6.9 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 02:36 1634-04-407/19/22 17:077.1 2.7 1
Naphthalene ND ug/kg 07/20/22 02:36 91-20-3 v207/19/22 17:077.1 3.8 1
n-Propylbenzene ND ug/kg 07/20/22 02:36 103-65-107/19/22 17:077.1 2.5 1
Styrene ND ug/kg 07/20/22 02:36 100-42-507/19/22 17:077.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 02:36 630-20-607/19/22 17:077.1 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 02:36 79-34-507/19/22 17:077.1 1.9 1
Tetrachloroethene ND ug/kg 07/20/22 02:36 127-18-407/19/22 17:077.1 2.3 1
Toluene ND ug/kg 07/20/22 02:36 108-88-307/19/22 17:077.1 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 02:36 87-61-6 v207/19/22 17:077.1 5.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 02:36 120-82-107/19/22 17:077.1 6.0 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 02:36 71-55-607/19/22 17:077.1 3.7 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 02:36 79-00-507/19/22 17:077.1 2.4 1
Trichloroethene ND ug/kg 07/20/22 02:36 79-01-607/19/22 17:077.1 1.8 1
Trichlorofluoromethane ND ug/kg 07/20/22 02:36 75-69-407/19/22 17:077.1 3.9 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 02:36 96-18-407/19/22 17:077.1 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 02:36 95-63-607/19/22 17:077.1 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 02:36 108-67-807/19/22 17:077.1 2.4 1
Vinyl acetate ND ug/kg 07/20/22 02:36 108-05-407/19/22 17:0771.4 5.2 1
Vinyl chloride ND ug/kg 07/20/22 02:36 75-01-4 IH07/19/22 17:0714.3 3.6 1
Xylene (Total)ND ug/kg 07/20/22 02:36 1330-20-707/19/22 17:0714.3 4.1 1
m&p-Xylene ND ug/kg 07/20/22 02:36 179601-23-107/19/22 17:0714.3 4.9 1
o-Xylene ND ug/kg 07/20/22 02:36 95-47-607/19/22 17:077.1 3.2 1
Surrogates
Toluene-d8 (S)101 %07/20/22 02:36 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)101 %07/20/22 02:36 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)105 %07/20/22 02:36 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.3 %07/19/22 17:56 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.1 %07/23/22 11:2507/23/22 10:481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-6 Lab ID:92615483006 Collected:07/15/22 15:15 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 14:48 18540-29-908/11/22 10:211.31 0.335 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-7 Lab ID:92615483007 Collected:07/15/22 15:30 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:43 7440-38-207/20/22 11:373.8 2.7 1
Barium 52.8 mg/kg 07/20/22 16:43 7440-39-307/20/22 11:371.3 0.53 1
Cadmium ND mg/kg 07/20/22 16:43 7440-43-907/20/22 11:371.3 0.38 1
Chromium 25.8 mg/kg 07/20/22 16:43 7440-47-307/20/22 11:371.3 1.2 1
Lead 8.7 mg/kg 07/20/22 16:43 7439-92-107/20/22 11:373.2 2.0 1
Selenium ND mg/kg 07/21/22 13:43 7782-49-2 D307/20/22 11:3731.8 27.5 5
Silver ND mg/kg 07/20/22 16:43 7440-22-407/20/22 11:371.3 0.52 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.063J mg/kg 07/25/22 13:52 7439-97-607/25/22 08:300.31 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/22/22 19:08 83-32-907/22/22 11:504301511
Acenaphthylene ND ug/kg 07/22/22 19:08 208-96-807/22/22 11:504301511
Aniline ND ug/kg 07/22/22 19:08 62-53-307/22/22 11:504301681
Anthracene ND ug/kg 07/22/22 19:08 120-12-707/22/22 11:504301411
Benzo(a)anthracene ND ug/kg 07/22/22 19:08 56-55-307/22/22 11:504301431
Benzo(a)pyrene ND ug/kg 07/22/22 19:08 50-32-807/22/22 11:504301491
Benzo(b)fluoranthene ND ug/kg 07/22/22 19:08 205-99-207/22/22 11:504301431
Benzo(g,h,i)perylene ND ug/kg 07/22/22 19:08 191-24-207/22/22 11:504301671
Benzo(k)fluoranthene ND ug/kg 07/22/22 19:08 207-08-907/22/22 11:504301511
Benzoic Acid ND ug/kg 07/22/22 19:08 65-85-0 v207/22/22 11:5021509251
Benzyl alcohol ND ug/kg 07/22/22 19:08 100-51-607/22/22 11:508613261
4-Bromophenylphenyl ether ND ug/kg 07/22/22 19:08 101-55-307/22/22 11:504301661
Butylbenzylphthalate ND ug/kg 07/22/22 19:08 85-68-707/22/22 11:504301811
4-Chloro-3-methylphenol ND ug/kg 07/22/22 19:08 59-50-707/22/22 11:508613031
4-Chloroaniline ND ug/kg 07/22/22 19:08 106-47-807/22/22 11:508613381
bis(2-Chloroethoxy)methane ND ug/kg 07/22/22 19:08 111-91-107/22/22 11:504301791
bis(2-Chloroethyl) ether ND ug/kg 07/22/22 19:08 111-44-407/22/22 11:504301621
2-Chloronaphthalene ND ug/kg 07/22/22 19:08 91-58-707/22/22 11:504301711
2-Chlorophenol ND ug/kg 07/22/22 19:08 95-57-807/22/22 11:504301621
4-Chlorophenylphenyl ether ND ug/kg 07/22/22 19:08 7005-72-307/22/22 11:504301601
Chrysene ND ug/kg 07/22/22 19:08 218-01-907/22/22 11:504301571
Dibenz(a,h)anthracene ND ug/kg 07/22/22 19:08 53-70-307/22/22 11:504301661
Dibenzofuran ND ug/kg 07/22/22 19:08 132-64-907/22/22 11:504301551
1,2-Dichlorobenzene ND ug/kg 07/22/22 19:08 95-50-107/22/22 11:504301551
1,3-Dichlorobenzene ND ug/kg 07/22/22 19:08 541-73-107/22/22 11:504301531
1,4-Dichlorobenzene ND ug/kg 07/22/22 19:08 106-46-707/22/22 11:504301641
3,3'-Dichlorobenzidine ND ug/kg 07/22/22 19:08 91-94-107/22/22 11:508612911
2,4-Dichlorophenol ND ug/kg 07/22/22 19:08 120-83-207/22/22 11:504301681
Diethylphthalate ND ug/kg 07/22/22 19:08 84-66-207/22/22 11:504301581
2,4-Dimethylphenol ND ug/kg 07/22/22 19:08 105-67-907/22/22 11:504301791
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-7 Lab ID:92615483007 Collected:07/15/22 15:30 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/22/22 19:08 131-11-307/22/22 11:504301571
Di-n-butylphthalate ND ug/kg 07/22/22 19:08 84-74-207/22/22 11:504301451
4,6-Dinitro-2-methylphenol ND ug/kg 07/22/22 19:08 534-52-107/22/22 11:508614021
2,4-Dinitrophenol ND ug/kg 07/22/22 19:08 51-28-5 v207/22/22 11:50215013301
2,4-Dinitrotoluene ND ug/kg 07/22/22 19:08 121-14-207/22/22 11:504301661
2,6-Dinitrotoluene ND ug/kg 07/22/22 19:08 606-20-207/22/22 11:504301581
Di-n-octylphthalate ND ug/kg 07/22/22 19:08 117-84-007/22/22 11:504301701
bis(2-Ethylhexyl)phthalate ND ug/kg 07/22/22 19:08 117-81-707/22/22 11:504301671
Fluoranthene ND ug/kg 07/22/22 19:08 206-44-007/22/22 11:504301471
Fluorene ND ug/kg 07/22/22 19:08 86-73-707/22/22 11:504301511
Hexachloro-1,3-butadiene ND ug/kg 07/22/22 19:08 87-68-307/22/22 11:504301871
Hexachlorobenzene ND ug/kg 07/22/22 19:08 118-74-107/22/22 11:504301681
Hexachlorocyclopentadiene ND ug/kg 07/22/22 19:08 77-47-407/22/22 11:504302471
Hexachloroethane ND ug/kg 07/22/22 19:08 67-72-107/22/22 11:504301641
Indeno(1,2,3-cd)pyrene ND ug/kg 07/22/22 19:08 193-39-507/22/22 11:504301701
Isophorone ND ug/kg 07/22/22 19:08 78-59-107/22/22 11:504301921
1-Methylnaphthalene ND ug/kg 07/22/22 19:08 90-12-007/22/22 11:504301511
2-Methylnaphthalene ND ug/kg 07/22/22 19:08 91-57-607/22/22 11:504301721
2-Methylphenol(o-Cresol)ND ug/kg 07/22/22 19:08 95-48-707/22/22 11:504301761
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/22/22 19:08 15831-10-407/22/22 11:504301731
Naphthalene ND ug/kg 07/22/22 19:08 91-20-307/22/22 11:504301461
2-Nitroaniline ND ug/kg 07/22/22 19:08 88-74-407/22/22 11:5021503521
3-Nitroaniline ND ug/kg 07/22/22 19:08 99-09-207/22/22 11:5021503381
4-Nitroaniline ND ug/kg 07/22/22 19:08 100-01-607/22/22 11:508613271
Nitrobenzene ND ug/kg 07/22/22 19:08 98-95-307/22/22 11:504302001
2-Nitrophenol ND ug/kg 07/22/22 19:08 88-75-507/22/22 11:504301871
4-Nitrophenol ND ug/kg 07/22/22 19:08 100-02-707/22/22 11:5021508321
N-Nitrosodimethylamine ND ug/kg 07/22/22 19:08 62-75-907/22/22 11:504301451
N-Nitroso-di-n-propylamine ND ug/kg 07/22/22 19:08 621-64-707/22/22 11:504301621
N-Nitrosodiphenylamine ND ug/kg 07/22/22 19:08 86-30-607/22/22 11:504301531
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/22/22 19:08 108-60-107/22/22 11:504302051
Pentachlorophenol ND ug/kg 07/22/22 19:08 87-86-507/22/22 11:508614211
Phenanthrene ND ug/kg 07/22/22 19:08 85-01-807/22/22 11:504301411
Phenol ND ug/kg 07/22/22 19:08 108-95-207/22/22 11:504301921
Pyrene ND ug/kg 07/22/22 19:08 129-00-007/22/22 11:504301751
Pyridine ND ug/kg 07/22/22 19:08 110-86-107/22/22 11:504301361
1,2,4-Trichlorobenzene ND ug/kg 07/22/22 19:08 120-82-107/22/22 11:504301701
2,4,5-Trichlorophenol ND ug/kg 07/22/22 19:08 95-95-407/22/22 11:504301971
2,4,6-Trichlorophenol ND ug/kg 07/22/22 19:08 88-06-207/22/22 11:504301771
Surrogates
Nitrobenzene-d5 (S)74 %07/22/22 19:08 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)66 %07/22/22 19:08 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)74 %07/22/22 19:08 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)70 %07/22/22 19:08 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-7 Lab ID:92615483007 Collected:07/15/22 15:30 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)71 %07/22/22 19:08 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)77 %07/22/22 19:08 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 02:53 67-64-107/19/22 17:0713242.2 1
Benzene ND ug/kg 07/20/22 02:53 71-43-207/19/22 17:076.6 2.6 1
Bromobenzene ND ug/kg 07/20/22 02:53 108-86-107/19/22 17:076.6 2.1 1
Bromochloromethane ND ug/kg 07/20/22 02:53 74-97-507/19/22 17:076.6 1.9 1
Bromodichloromethane ND ug/kg 07/20/22 02:53 75-27-407/19/22 17:076.6 2.5 1
Bromoform ND ug/kg 07/20/22 02:53 75-25-207/19/22 17:076.6 2.3 1
Bromomethane ND ug/kg 07/20/22 02:53 74-83-9 L107/19/22 17:0713.2 10.4 1
2-Butanone (MEK)43.0J ug/kg 07/20/22 02:53 78-93-3 C707/19/22 17:0713231.6 1
n-Butylbenzene ND ug/kg 07/20/22 02:53 104-51-807/19/22 17:076.6 3.1 1
sec-Butylbenzene ND ug/kg 07/20/22 02:53 135-98-807/19/22 17:076.6 2.9 1
tert-Butylbenzene ND ug/kg 07/20/22 02:53 98-06-607/19/22 17:076.6 2.3 1
Carbon tetrachloride ND ug/kg 07/20/22 02:53 56-23-507/19/22 17:076.6 2.5 1
Chlorobenzene ND ug/kg 07/20/22 02:53 108-90-707/19/22 17:076.6 1.3 1
Chloroethane ND ug/kg 07/20/22 02:53 75-00-3 IH07/19/22 17:0713.2 5.1 1
Chloroform ND ug/kg 07/20/22 02:53 67-66-307/19/22 17:076.6 4.0 1
Chloromethane ND ug/kg 07/20/22 02:53 74-87-3 IH07/19/22 17:0713.2 5.5 1
2-Chlorotoluene ND ug/kg 07/20/22 02:53 95-49-807/19/22 17:076.6 2.3 1
4-Chlorotoluene ND ug/kg 07/20/22 02:53 106-43-407/19/22 17:076.6 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 02:53 96-12-8 v207/19/22 17:076.6 2.6 1
Dibromochloromethane ND ug/kg 07/20/22 02:53 124-48-107/19/22 17:076.6 3.7 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 02:53 106-93-407/19/22 17:076.6 2.9 1
Dibromomethane ND ug/kg 07/20/22 02:53 74-95-307/19/22 17:076.6 1.4 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 02:53 95-50-107/19/22 17:076.6 2.4 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 02:53 541-73-107/19/22 17:076.6 2.0 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 02:53 106-46-707/19/22 17:076.6 1.7 1
Dichlorodifluoromethane ND ug/kg 07/20/22 02:53 75-71-8 IH,L107/19/22 17:0713.2 2.9 1
1,1-Dichloroethane ND ug/kg 07/20/22 02:53 75-34-307/19/22 17:076.6 2.7 1
1,2-Dichloroethane ND ug/kg 07/20/22 02:53 107-06-207/19/22 17:076.6 4.4 1
1,1-Dichloroethene ND ug/kg 07/20/22 02:53 75-35-407/19/22 17:076.6 2.7 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 02:53 156-59-207/19/22 17:076.6 2.3 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 02:53 156-60-507/19/22 17:076.6 2.3 1
1,2-Dichloropropane ND ug/kg 07/20/22 02:53 78-87-507/19/22 17:076.6 2.0 1
1,3-Dichloropropane ND ug/kg 07/20/22 02:53 142-28-907/19/22 17:076.6 2.1 1
2,2-Dichloropropane ND ug/kg 07/20/22 02:53 594-20-707/19/22 17:076.6 2.1 1
1,1-Dichloropropene ND ug/kg 07/20/22 02:53 563-58-607/19/22 17:076.6 3.2 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 02:53 10061-01-507/19/22 17:076.6 1.8 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 02:53 10061-02-607/19/22 17:076.6 2.3 1
Diisopropyl ether ND ug/kg 07/20/22 02:53 108-20-307/19/22 17:076.6 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-7 Lab ID:92615483007 Collected:07/15/22 15:30 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 02:53 100-41-407/19/22 17:076.6 3.1 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 02:53 87-68-307/19/22 17:0713.2 10.8 1
2-Hexanone ND ug/kg 07/20/22 02:53 591-78-607/19/22 17:0765.8 6.3 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 02:53 98-82-807/19/22 17:076.6 2.2 1
p-Isopropyltoluene ND ug/kg 07/20/22 02:53 99-87-607/19/22 17:076.6 3.2 1
Methylene Chloride 22.2J ug/kg 07/20/22 02:53 75-09-2 C707/19/22 17:0726.3 18.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 02:53 108-10-107/19/22 17:0765.8 6.3 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 02:53 1634-04-407/19/22 17:076.6 2.5 1
Naphthalene ND ug/kg 07/20/22 02:53 91-20-3 v207/19/22 17:076.6 3.5 1
n-Propylbenzene ND ug/kg 07/20/22 02:53 103-65-107/19/22 17:076.6 2.3 1
Styrene ND ug/kg 07/20/22 02:53 100-42-507/19/22 17:076.6 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 02:53 630-20-607/19/22 17:076.6 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 02:53 79-34-507/19/22 17:076.6 1.7 1
Tetrachloroethene ND ug/kg 07/20/22 02:53 127-18-407/19/22 17:076.6 2.1 1
Toluene ND ug/kg 07/20/22 02:53 108-88-307/19/22 17:076.6 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 02:53 87-61-6 v207/19/22 17:076.6 5.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 02:53 120-82-107/19/22 17:076.6 5.5 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 02:53 71-55-607/19/22 17:076.6 3.4 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 02:53 79-00-507/19/22 17:076.6 2.2 1
Trichloroethene ND ug/kg 07/20/22 02:53 79-01-607/19/22 17:076.6 1.7 1
Trichlorofluoromethane ND ug/kg 07/20/22 02:53 75-69-407/19/22 17:076.6 3.6 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 02:53 96-18-407/19/22 17:076.6 3.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 02:53 95-63-607/19/22 17:076.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 02:53 108-67-807/19/22 17:076.6 2.2 1
Vinyl acetate ND ug/kg 07/20/22 02:53 108-05-407/19/22 17:0765.8 4.8 1
Vinyl chloride ND ug/kg 07/20/22 02:53 75-01-4 IH07/19/22 17:0713.2 3.3 1
Xylene (Total)ND ug/kg 07/20/22 02:53 1330-20-707/19/22 17:0713.2 3.8 1
m&p-Xylene ND ug/kg 07/20/22 02:53 179601-23-107/19/22 17:0713.2 4.5 1
o-Xylene ND ug/kg 07/20/22 02:53 95-47-607/19/22 17:076.6 2.9 1
Surrogates
Toluene-d8 (S)101 %07/20/22 02:53 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)100 %07/20/22 02:53 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)104 %07/20/22 02:53 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.8 %07/19/22 17:56 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.3 %07/23/22 11:2507/23/22 10:481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-7 Lab ID:92615483007 Collected:07/15/22 15:30 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 14:53 18540-29-908/11/22 10:211.40 0.358 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-8 Lab ID:92615483008 Collected:07/15/22 15:43 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:48 7440-38-207/20/22 11:373.6 2.6 1
Barium 13.9 mg/kg 07/20/22 16:48 7440-39-307/20/22 11:371.2 0.50 1
Cadmium ND mg/kg 07/20/22 16:48 7440-43-907/20/22 11:371.2 0.36 1
Chromium 13.0 mg/kg 07/20/22 16:48 7440-47-307/20/22 11:371.2 1.1 1
Lead 10.5 mg/kg 07/20/22 16:48 7439-92-107/20/22 11:373.0 1.9 1
Selenium ND mg/kg 07/20/22 16:48 7782-49-207/20/22 11:376.0 5.2 1
Silver ND mg/kg 07/20/22 16:48 7440-22-407/20/22 11:371.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.034J mg/kg 07/25/22 13:55 7439-97-607/25/22 08:300.32 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/25/22 10:14 83-32-907/22/22 11:504221481
Acenaphthylene ND ug/kg 07/25/22 10:14 208-96-807/22/22 11:504221481
Aniline ND ug/kg 07/25/22 10:14 62-53-307/22/22 11:504221651
Anthracene ND ug/kg 07/25/22 10:14 120-12-707/22/22 11:504221381
Benzo(a)anthracene ND ug/kg 07/25/22 10:14 56-55-307/22/22 11:504221411
Benzo(a)pyrene ND ug/kg 07/25/22 10:14 50-32-807/22/22 11:504221461
Benzo(b)fluoranthene ND ug/kg 07/25/22 10:14 205-99-207/22/22 11:504221411
Benzo(g,h,i)perylene ND ug/kg 07/25/22 10:14 191-24-207/22/22 11:504221641
Benzo(k)fluoranthene ND ug/kg 07/25/22 10:14 207-08-907/22/22 11:504221481
Benzoic Acid ND ug/kg 07/25/22 10:14 65-85-007/22/22 11:5021109071
Benzyl alcohol ND ug/kg 07/25/22 10:14 100-51-607/22/22 11:508453201
4-Bromophenylphenyl ether ND ug/kg 07/25/22 10:14 101-55-307/22/22 11:504221631
Butylbenzylphthalate ND ug/kg 07/25/22 10:14 85-68-707/22/22 11:504221781
4-Chloro-3-methylphenol ND ug/kg 07/25/22 10:14 59-50-707/22/22 11:508452971
4-Chloroaniline ND ug/kg 07/25/22 10:14 106-47-807/22/22 11:508453311
bis(2-Chloroethoxy)methane ND ug/kg 07/25/22 10:14 111-91-107/22/22 11:504221751
bis(2-Chloroethyl) ether ND ug/kg 07/25/22 10:14 111-44-407/22/22 11:504221591
2-Chloronaphthalene ND ug/kg 07/25/22 10:14 91-58-707/22/22 11:504221681
2-Chlorophenol ND ug/kg 07/25/22 10:14 95-57-807/22/22 11:504221591
4-Chlorophenylphenyl ether ND ug/kg 07/25/22 10:14 7005-72-307/22/22 11:504221571
Chrysene ND ug/kg 07/25/22 10:14 218-01-907/22/22 11:504221541
Dibenz(a,h)anthracene ND ug/kg 07/25/22 10:14 53-70-307/22/22 11:504221631
Dibenzofuran ND ug/kg 07/25/22 10:14 132-64-907/22/22 11:504221521
1,2-Dichlorobenzene ND ug/kg 07/25/22 10:14 95-50-107/22/22 11:504221521
1,3-Dichlorobenzene ND ug/kg 07/25/22 10:14 541-73-107/22/22 11:504221501
1,4-Dichlorobenzene ND ug/kg 07/25/22 10:14 106-46-707/22/22 11:504221611
3,3'-Dichlorobenzidine ND ug/kg 07/25/22 10:14 91-94-107/22/22 11:508452851
2,4-Dichlorophenol ND ug/kg 07/25/22 10:14 120-83-207/22/22 11:504221651
Diethylphthalate ND ug/kg 07/25/22 10:14 84-66-207/22/22 11:504221551
2,4-Dimethylphenol ND ug/kg 07/25/22 10:14 105-67-907/22/22 11:504221751
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-8 Lab ID:92615483008 Collected:07/15/22 15:43 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/25/22 10:14 131-11-307/22/22 11:504221541
Di-n-butylphthalate ND ug/kg 07/25/22 10:14 84-74-207/22/22 11:504221421
4,6-Dinitro-2-methylphenol ND ug/kg 07/25/22 10:14 534-52-107/22/22 11:508453941
2,4-Dinitrophenol ND ug/kg 07/25/22 10:14 51-28-507/22/22 11:50211013101
2,4-Dinitrotoluene ND ug/kg 07/25/22 10:14 121-14-207/22/22 11:504221631
2,6-Dinitrotoluene ND ug/kg 07/25/22 10:14 606-20-207/22/22 11:504221551
Di-n-octylphthalate ND ug/kg 07/25/22 10:14 117-84-007/22/22 11:504221661
bis(2-Ethylhexyl)phthalate ND ug/kg 07/25/22 10:14 117-81-707/22/22 11:504221641
Fluoranthene ND ug/kg 07/25/22 10:14 206-44-007/22/22 11:504221451
Fluorene ND ug/kg 07/25/22 10:14 86-73-707/22/22 11:504221481
Hexachloro-1,3-butadiene ND ug/kg 07/25/22 10:14 87-68-307/22/22 11:504221831
Hexachlorobenzene ND ug/kg 07/25/22 10:14 118-74-107/22/22 11:504221651
Hexachlorocyclopentadiene ND ug/kg 07/25/22 10:14 77-47-407/22/22 11:504222421
Hexachloroethane ND ug/kg 07/25/22 10:14 67-72-107/22/22 11:504221611
Indeno(1,2,3-cd)pyrene ND ug/kg 07/25/22 10:14 193-39-507/22/22 11:504221661
Isophorone ND ug/kg 07/25/22 10:14 78-59-107/22/22 11:504221881
1-Methylnaphthalene ND ug/kg 07/25/22 10:14 90-12-007/22/22 11:504221481
2-Methylnaphthalene ND ug/kg 07/25/22 10:14 91-57-607/22/22 11:504221691
2-Methylphenol(o-Cresol)ND ug/kg 07/25/22 10:14 95-48-707/22/22 11:504221731
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/25/22 10:14 15831-10-407/22/22 11:504221701
Naphthalene ND ug/kg 07/25/22 10:14 91-20-307/22/22 11:504221431
2-Nitroaniline ND ug/kg 07/25/22 10:14 88-74-407/22/22 11:5021103451
3-Nitroaniline ND ug/kg 07/25/22 10:14 99-09-207/22/22 11:5021103311
4-Nitroaniline ND ug/kg 07/25/22 10:14 100-01-607/22/22 11:508453211
Nitrobenzene ND ug/kg 07/25/22 10:14 98-95-307/22/22 11:504221961
2-Nitrophenol ND ug/kg 07/25/22 10:14 88-75-507/22/22 11:504221831
4-Nitrophenol ND ug/kg 07/25/22 10:14 100-02-707/22/22 11:5021108161
N-Nitrosodimethylamine ND ug/kg 07/25/22 10:14 62-75-907/22/22 11:504221421
N-Nitroso-di-n-propylamine ND ug/kg 07/25/22 10:14 621-64-707/22/22 11:504221591
N-Nitrosodiphenylamine ND ug/kg 07/25/22 10:14 86-30-607/22/22 11:504221501
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/25/22 10:14 108-60-107/22/22 11:504222011
Pentachlorophenol ND ug/kg 07/25/22 10:14 87-86-507/22/22 11:508454131
Phenanthrene ND ug/kg 07/25/22 10:14 85-01-807/22/22 11:504221381
Phenol ND ug/kg 07/25/22 10:14 108-95-207/22/22 11:504221881
Pyrene ND ug/kg 07/25/22 10:14 129-00-007/22/22 11:504221711
Pyridine ND ug/kg 07/25/22 10:14 110-86-107/22/22 11:504221331
1,2,4-Trichlorobenzene ND ug/kg 07/25/22 10:14 120-82-107/22/22 11:504221661
2,4,5-Trichlorophenol ND ug/kg 07/25/22 10:14 95-95-407/22/22 11:504221931
2,4,6-Trichlorophenol ND ug/kg 07/25/22 10:14 88-06-207/22/22 11:504221741
Surrogates
Nitrobenzene-d5 (S)75 %07/25/22 10:14 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)66 %07/25/22 10:14 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)76 %07/25/22 10:14 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)74 %07/25/22 10:14 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-8 Lab ID:92615483008 Collected:07/15/22 15:43 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)74 %07/25/22 10:14 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)72 %07/25/22 10:14 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 03:11 67-64-107/19/22 17:0713844.4 1
Benzene ND ug/kg 07/20/22 03:11 71-43-207/19/22 17:076.9 2.8 1
Bromobenzene ND ug/kg 07/20/22 03:11 108-86-107/19/22 17:076.9 2.3 1
Bromochloromethane ND ug/kg 07/20/22 03:11 74-97-507/19/22 17:076.9 2.0 1
Bromodichloromethane ND ug/kg 07/20/22 03:11 75-27-407/19/22 17:076.9 2.7 1
Bromoform ND ug/kg 07/20/22 03:11 75-25-207/19/22 17:076.9 2.4 1
Bromomethane ND ug/kg 07/20/22 03:11 74-83-9 L107/19/22 17:0713.8 10.9 1
2-Butanone (MEK)43.8J ug/kg 07/20/22 03:11 78-93-3 C707/19/22 17:0713833.2 1
n-Butylbenzene ND ug/kg 07/20/22 03:11 104-51-807/19/22 17:076.9 3.3 1
sec-Butylbenzene ND ug/kg 07/20/22 03:11 135-98-807/19/22 17:076.9 3.0 1
tert-Butylbenzene ND ug/kg 07/20/22 03:11 98-06-607/19/22 17:076.9 2.5 1
Carbon tetrachloride ND ug/kg 07/20/22 03:11 56-23-507/19/22 17:076.9 2.6 1
Chlorobenzene ND ug/kg 07/20/22 03:11 108-90-707/19/22 17:076.9 1.3 1
Chloroethane ND ug/kg 07/20/22 03:11 75-00-3 IH07/19/22 17:0713.8 5.3 1
Chloroform ND ug/kg 07/20/22 03:11 67-66-307/19/22 17:076.9 4.2 1
Chloromethane ND ug/kg 07/20/22 03:11 74-87-3 IH07/19/22 17:0713.8 5.8 1
2-Chlorotoluene ND ug/kg 07/20/22 03:11 95-49-807/19/22 17:076.9 2.4 1
4-Chlorotoluene ND ug/kg 07/20/22 03:11 106-43-407/19/22 17:076.9 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 03:11 96-12-8 v207/19/22 17:076.9 2.7 1
Dibromochloromethane ND ug/kg 07/20/22 03:11 124-48-107/19/22 17:076.9 3.9 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 03:11 106-93-407/19/22 17:076.9 3.0 1
Dibromomethane ND ug/kg 07/20/22 03:11 74-95-307/19/22 17:076.9 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 03:11 95-50-107/19/22 17:076.9 2.5 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 03:11 541-73-107/19/22 17:076.9 2.1 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 03:11 106-46-707/19/22 17:076.9 1.8 1
Dichlorodifluoromethane ND ug/kg 07/20/22 03:11 75-71-8 IH,L107/19/22 17:0713.8 3.0 1
1,1-Dichloroethane ND ug/kg 07/20/22 03:11 75-34-307/19/22 17:076.9 2.8 1
1,2-Dichloroethane ND ug/kg 07/20/22 03:11 107-06-207/19/22 17:076.9 4.6 1
1,1-Dichloroethene ND ug/kg 07/20/22 03:11 75-35-407/19/22 17:076.9 2.8 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 03:11 156-59-207/19/22 17:076.9 2.4 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 03:11 156-60-507/19/22 17:076.9 2.4 1
1,2-Dichloropropane ND ug/kg 07/20/22 03:11 78-87-507/19/22 17:076.9 2.1 1
1,3-Dichloropropane ND ug/kg 07/20/22 03:11 142-28-907/19/22 17:076.9 2.2 1
2,2-Dichloropropane ND ug/kg 07/20/22 03:11 594-20-707/19/22 17:076.9 2.3 1
1,1-Dichloropropene ND ug/kg 07/20/22 03:11 563-58-607/19/22 17:076.9 3.3 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 03:11 10061-01-507/19/22 17:076.9 1.9 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 03:11 10061-02-607/19/22 17:076.9 2.4 1
Diisopropyl ether ND ug/kg 07/20/22 03:11 108-20-307/19/22 17:076.9 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-8 Lab ID:92615483008 Collected:07/15/22 15:43 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 03:11 100-41-407/19/22 17:076.9 3.2 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 03:11 87-68-307/19/22 17:0713.8 11.3 1
2-Hexanone ND ug/kg 07/20/22 03:11 591-78-607/19/22 17:0769.1 6.7 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 03:11 98-82-807/19/22 17:076.9 2.3 1
p-Isopropyltoluene ND ug/kg 07/20/22 03:11 99-87-607/19/22 17:076.9 3.4 1
Methylene Chloride ND ug/kg 07/20/22 03:11 75-09-207/19/22 17:0727.6 18.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 03:11 108-10-107/19/22 17:0769.1 6.7 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 03:11 1634-04-407/19/22 17:076.9 2.6 1
Naphthalene ND ug/kg 07/20/22 03:11 91-20-3 v207/19/22 17:076.9 3.6 1
n-Propylbenzene ND ug/kg 07/20/22 03:11 103-65-107/19/22 17:076.9 2.5 1
Styrene ND ug/kg 07/20/22 03:11 100-42-507/19/22 17:076.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 03:11 630-20-607/19/22 17:076.9 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 03:11 79-34-507/19/22 17:076.9 1.8 1
Tetrachloroethene ND ug/kg 07/20/22 03:11 127-18-407/19/22 17:076.9 2.2 1
Toluene ND ug/kg 07/20/22 03:11 108-88-307/19/22 17:076.9 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 03:11 87-61-6 v207/19/22 17:076.9 5.6 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 03:11 120-82-107/19/22 17:076.9 5.8 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 03:11 71-55-607/19/22 17:076.9 3.6 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 03:11 79-00-507/19/22 17:076.9 2.3 1
Trichloroethene ND ug/kg 07/20/22 03:11 79-01-607/19/22 17:076.9 1.8 1
Trichlorofluoromethane ND ug/kg 07/20/22 03:11 75-69-407/19/22 17:076.9 3.8 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 03:11 96-18-407/19/22 17:076.9 3.5 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 03:11 95-63-607/19/22 17:076.9 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 03:11 108-67-807/19/22 17:076.9 2.3 1
Vinyl acetate ND ug/kg 07/20/22 03:11 108-05-407/19/22 17:0769.1 5.0 1
Vinyl chloride ND ug/kg 07/20/22 03:11 75-01-4 IH07/19/22 17:0713.8 3.5 1
Xylene (Total)ND ug/kg 07/20/22 03:11 1330-20-707/19/22 17:0713.8 3.9 1
m&p-Xylene ND ug/kg 07/20/22 03:11 179601-23-107/19/22 17:0713.8 4.7 1
o-Xylene ND ug/kg 07/20/22 03:11 95-47-607/19/22 17:076.9 3.1 1
Surrogates
Toluene-d8 (S)101 %07/20/22 03:11 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)102 %07/20/22 03:11 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)107 %07/20/22 03:11 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.1 %07/20/22 17:12 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 73.3 %07/23/22 11:2507/23/22 10:481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-8 Lab ID:92615483008 Collected:07/15/22 15:43 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/12/22 14:58 18540-29-908/11/22 10:211.37 0.348 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-9 Lab ID:92615483009 Collected:07/15/22 15:50 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:52 7440-38-207/20/22 11:373.9 2.7 1
Barium 33.9 mg/kg 07/20/22 16:52 7440-39-307/20/22 11:371.3 0.53 1
Cadmium ND mg/kg 07/20/22 16:52 7440-43-907/20/22 11:371.3 0.38 1
Chromium 18.5 mg/kg 07/20/22 16:52 7440-47-307/20/22 11:371.3 1.2 1
Lead 13.1 mg/kg 07/20/22 16:52 7439-92-107/20/22 11:373.2 2.0 1
Selenium ND mg/kg 07/21/22 13:47 7782-49-2 D307/20/22 11:3732.1 27.8 5
Silver ND mg/kg 07/20/22 16:52 7440-22-407/20/22 11:371.3 0.53 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.038J mg/kg 07/25/22 13:57 7439-97-607/25/22 08:300.32 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/25/22 10:41 83-32-907/22/22 11:504411551
Acenaphthylene ND ug/kg 07/25/22 10:41 208-96-807/22/22 11:504411551
Aniline ND ug/kg 07/25/22 10:41 62-53-307/22/22 11:504411721
Anthracene ND ug/kg 07/25/22 10:41 120-12-707/22/22 11:504411441
Benzo(a)anthracene ND ug/kg 07/25/22 10:41 56-55-307/22/22 11:504411471
Benzo(a)pyrene ND ug/kg 07/25/22 10:41 50-32-807/22/22 11:504411521
Benzo(b)fluoranthene ND ug/kg 07/25/22 10:41 205-99-207/22/22 11:504411471
Benzo(g,h,i)perylene ND ug/kg 07/25/22 10:41 191-24-207/22/22 11:504411711
Benzo(k)fluoranthene ND ug/kg 07/25/22 10:41 207-08-907/22/22 11:504411551
Benzoic Acid ND ug/kg 07/25/22 10:41 65-85-007/22/22 11:5022109481
Benzyl alcohol ND ug/kg 07/25/22 10:41 100-51-607/22/22 11:508833341
4-Bromophenylphenyl ether ND ug/kg 07/25/22 10:41 101-55-307/22/22 11:504411701
Butylbenzylphthalate ND ug/kg 07/25/22 10:41 85-68-707/22/22 11:504411861
4-Chloro-3-methylphenol ND ug/kg 07/25/22 10:41 59-50-707/22/22 11:508833101
4-Chloroaniline ND ug/kg 07/25/22 10:41 106-47-807/22/22 11:508833461
bis(2-Chloroethoxy)methane ND ug/kg 07/25/22 10:41 111-91-107/22/22 11:504411831
bis(2-Chloroethyl) ether ND ug/kg 07/25/22 10:41 111-44-407/22/22 11:504411661
2-Chloronaphthalene ND ug/kg 07/25/22 10:41 91-58-707/22/22 11:504411751
2-Chlorophenol ND ug/kg 07/25/22 10:41 95-57-807/22/22 11:504411661
4-Chlorophenylphenyl ether ND ug/kg 07/25/22 10:41 7005-72-307/22/22 11:504411641
Chrysene ND ug/kg 07/25/22 10:41 218-01-907/22/22 11:504411601
Dibenz(a,h)anthracene ND ug/kg 07/25/22 10:41 53-70-307/22/22 11:504411701
Dibenzofuran ND ug/kg 07/25/22 10:41 132-64-907/22/22 11:504411591
1,2-Dichlorobenzene ND ug/kg 07/25/22 10:41 95-50-107/22/22 11:504411591
1,3-Dichlorobenzene ND ug/kg 07/25/22 10:41 541-73-107/22/22 11:504411561
1,4-Dichlorobenzene ND ug/kg 07/25/22 10:41 106-46-707/22/22 11:504411681
3,3'-Dichlorobenzidine ND ug/kg 07/25/22 10:41 91-94-107/22/22 11:508832981
2,4-Dichlorophenol ND ug/kg 07/25/22 10:41 120-83-207/22/22 11:504411721
Diethylphthalate ND ug/kg 07/25/22 10:41 84-66-207/22/22 11:504411621
2,4-Dimethylphenol ND ug/kg 07/25/22 10:41 105-67-907/22/22 11:504411831
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-9 Lab ID:92615483009 Collected:07/15/22 15:50 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/25/22 10:41 131-11-307/22/22 11:504411601
Di-n-butylphthalate ND ug/kg 07/25/22 10:41 84-74-207/22/22 11:504411481
4,6-Dinitro-2-methylphenol ND ug/kg 07/25/22 10:41 534-52-107/22/22 11:508834121
2,4-Dinitrophenol ND ug/kg 07/25/22 10:41 51-28-507/22/22 11:50221013601
2,4-Dinitrotoluene ND ug/kg 07/25/22 10:41 121-14-207/22/22 11:504411701
2,6-Dinitrotoluene ND ug/kg 07/25/22 10:41 606-20-207/22/22 11:504411621
Di-n-octylphthalate ND ug/kg 07/25/22 10:41 117-84-007/22/22 11:504411741
bis(2-Ethylhexyl)phthalate ND ug/kg 07/25/22 10:41 117-81-707/22/22 11:504411711
Fluoranthene ND ug/kg 07/25/22 10:41 206-44-007/22/22 11:504411511
Fluorene ND ug/kg 07/25/22 10:41 86-73-707/22/22 11:504411551
Hexachloro-1,3-butadiene ND ug/kg 07/25/22 10:41 87-68-307/22/22 11:504411911
Hexachlorobenzene ND ug/kg 07/25/22 10:41 118-74-107/22/22 11:504411721
Hexachlorocyclopentadiene ND ug/kg 07/25/22 10:41 77-47-407/22/22 11:504412531
Hexachloroethane ND ug/kg 07/25/22 10:41 67-72-107/22/22 11:504411681
Indeno(1,2,3-cd)pyrene ND ug/kg 07/25/22 10:41 193-39-507/22/22 11:504411741
Isophorone ND ug/kg 07/25/22 10:41 78-59-107/22/22 11:504411971
1-Methylnaphthalene ND ug/kg 07/25/22 10:41 90-12-007/22/22 11:504411551
2-Methylnaphthalene ND ug/kg 07/25/22 10:41 91-57-607/22/22 11:504411771
2-Methylphenol(o-Cresol)ND ug/kg 07/25/22 10:41 95-48-707/22/22 11:504411811
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/25/22 10:41 15831-10-407/22/22 11:504411781
Naphthalene ND ug/kg 07/25/22 10:41 91-20-307/22/22 11:504411501
2-Nitroaniline ND ug/kg 07/25/22 10:41 88-74-407/22/22 11:5022103611
3-Nitroaniline ND ug/kg 07/25/22 10:41 99-09-207/22/22 11:5022103461
4-Nitroaniline ND ug/kg 07/25/22 10:41 100-01-607/22/22 11:508833361
Nitrobenzene ND ug/kg 07/25/22 10:41 98-95-307/22/22 11:504412051
2-Nitrophenol ND ug/kg 07/25/22 10:41 88-75-507/22/22 11:504411911
4-Nitrophenol ND ug/kg 07/25/22 10:41 100-02-707/22/22 11:5022108531
N-Nitrosodimethylamine ND ug/kg 07/25/22 10:41 62-75-907/22/22 11:504411481
N-Nitroso-di-n-propylamine ND ug/kg 07/25/22 10:41 621-64-707/22/22 11:504411661
N-Nitrosodiphenylamine ND ug/kg 07/25/22 10:41 86-30-607/22/22 11:504411561
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/25/22 10:41 108-60-107/22/22 11:504412101
Pentachlorophenol ND ug/kg 07/25/22 10:41 87-86-507/22/22 11:508834321
Phenanthrene ND ug/kg 07/25/22 10:41 85-01-807/22/22 11:504411441
Phenol ND ug/kg 07/25/22 10:41 108-95-207/22/22 11:504411971
Pyrene ND ug/kg 07/25/22 10:41 129-00-007/22/22 11:504411791
Pyridine ND ug/kg 07/25/22 10:41 110-86-107/22/22 11:504411391
1,2,4-Trichlorobenzene ND ug/kg 07/25/22 10:41 120-82-107/22/22 11:504411741
2,4,5-Trichlorophenol ND ug/kg 07/25/22 10:41 95-95-407/22/22 11:504412021
2,4,6-Trichlorophenol ND ug/kg 07/25/22 10:41 88-06-207/22/22 11:504411821
Surrogates
Nitrobenzene-d5 (S)72 %07/25/22 10:41 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)64 %07/25/22 10:41 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)77 %07/25/22 10:41 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)71 %07/25/22 10:41 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-9 Lab ID:92615483009 Collected:07/15/22 15:50 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)70 %07/25/22 10:41 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)72 %07/25/22 10:41 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 03:29 67-64-107/19/22 17:0714546.4 1
Benzene ND ug/kg 07/20/22 03:29 71-43-207/19/22 17:077.2 2.9 1
Bromobenzene ND ug/kg 07/20/22 03:29 108-86-107/19/22 17:077.2 2.4 1
Bromochloromethane ND ug/kg 07/20/22 03:29 74-97-507/19/22 17:077.2 2.1 1
Bromodichloromethane ND ug/kg 07/20/22 03:29 75-27-407/19/22 17:077.2 2.8 1
Bromoform ND ug/kg 07/20/22 03:29 75-25-207/19/22 17:077.2 2.5 1
Bromomethane ND ug/kg 07/20/22 03:29 74-83-9 L107/19/22 17:0714.5 11.4 1
2-Butanone (MEK)51.1J ug/kg 07/20/22 03:29 78-93-3 C707/19/22 17:0714534.7 1
n-Butylbenzene ND ug/kg 07/20/22 03:29 104-51-807/19/22 17:077.2 3.4 1
sec-Butylbenzene ND ug/kg 07/20/22 03:29 135-98-807/19/22 17:077.2 3.2 1
tert-Butylbenzene ND ug/kg 07/20/22 03:29 98-06-607/19/22 17:077.2 2.6 1
Carbon tetrachloride ND ug/kg 07/20/22 03:29 56-23-507/19/22 17:077.2 2.7 1
Chlorobenzene ND ug/kg 07/20/22 03:29 108-90-707/19/22 17:077.2 1.4 1
Chloroethane ND ug/kg 07/20/22 03:29 75-00-3 IH07/19/22 17:0714.5 5.6 1
Chloroform ND ug/kg 07/20/22 03:29 67-66-307/19/22 17:077.2 4.4 1
Chloromethane ND ug/kg 07/20/22 03:29 74-87-3 IH07/19/22 17:0714.5 6.1 1
2-Chlorotoluene ND ug/kg 07/20/22 03:29 95-49-807/19/22 17:077.2 2.6 1
4-Chlorotoluene ND ug/kg 07/20/22 03:29 106-43-407/19/22 17:077.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 03:29 96-12-8 v207/19/22 17:077.2 2.8 1
Dibromochloromethane ND ug/kg 07/20/22 03:29 124-48-107/19/22 17:077.2 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 03:29 106-93-407/19/22 17:077.2 3.2 1
Dibromomethane ND ug/kg 07/20/22 03:29 74-95-307/19/22 17:077.2 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 03:29 95-50-107/19/22 17:077.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 03:29 541-73-107/19/22 17:077.2 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 03:29 106-46-707/19/22 17:077.2 1.9 1
Dichlorodifluoromethane ND ug/kg 07/20/22 03:29 75-71-8 IH,L107/19/22 17:0714.5 3.1 1
1,1-Dichloroethane ND ug/kg 07/20/22 03:29 75-34-307/19/22 17:077.2 3.0 1
1,2-Dichloroethane ND ug/kg 07/20/22 03:29 107-06-207/19/22 17:077.2 4.8 1
1,1-Dichloroethene ND ug/kg 07/20/22 03:29 75-35-407/19/22 17:077.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 03:29 156-59-207/19/22 17:077.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 03:29 156-60-507/19/22 17:077.2 2.5 1
1,2-Dichloropropane ND ug/kg 07/20/22 03:29 78-87-507/19/22 17:077.2 2.2 1
1,3-Dichloropropane ND ug/kg 07/20/22 03:29 142-28-907/19/22 17:077.2 2.3 1
2,2-Dichloropropane ND ug/kg 07/20/22 03:29 594-20-707/19/22 17:077.2 2.4 1
1,1-Dichloropropene ND ug/kg 07/20/22 03:29 563-58-607/19/22 17:077.2 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 03:29 10061-01-507/19/22 17:077.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 03:29 10061-02-607/19/22 17:077.2 2.5 1
Diisopropyl ether ND ug/kg 07/20/22 03:29 108-20-307/19/22 17:077.2 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-9 Lab ID:92615483009 Collected:07/15/22 15:50 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 03:29 100-41-407/19/22 17:077.2 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 03:29 87-68-307/19/22 17:0714.5 11.8 1
2-Hexanone ND ug/kg 07/20/22 03:29 591-78-607/19/22 17:0772.3 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 03:29 98-82-807/19/22 17:077.2 2.5 1
p-Isopropyltoluene ND ug/kg 07/20/22 03:29 99-87-607/19/22 17:077.2 3.6 1
Methylene Chloride 31.3 ug/kg 07/20/22 03:29 75-09-2 C707/19/22 17:0728.9 19.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 03:29 108-10-107/19/22 17:0772.3 7.0 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 03:29 1634-04-407/19/22 17:077.2 2.7 1
Naphthalene ND ug/kg 07/20/22 03:29 91-20-3 v207/19/22 17:077.2 3.8 1
n-Propylbenzene ND ug/kg 07/20/22 03:29 103-65-107/19/22 17:077.2 2.6 1
Styrene ND ug/kg 07/20/22 03:29 100-42-507/19/22 17:077.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 03:29 630-20-607/19/22 17:077.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 03:29 79-34-507/19/22 17:077.2 1.9 1
Tetrachloroethene ND ug/kg 07/20/22 03:29 127-18-407/19/22 17:077.2 2.3 1
Toluene ND ug/kg 07/20/22 03:29 108-88-307/19/22 17:077.2 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 03:29 87-61-6 v207/19/22 17:077.2 5.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 03:29 120-82-107/19/22 17:077.2 6.1 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 03:29 71-55-607/19/22 17:077.2 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 03:29 79-00-507/19/22 17:077.2 2.4 1
Trichloroethene ND ug/kg 07/20/22 03:29 79-01-607/19/22 17:077.2 1.9 1
Trichlorofluoromethane ND ug/kg 07/20/22 03:29 75-69-407/19/22 17:077.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 03:29 96-18-407/19/22 17:077.2 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 03:29 95-63-607/19/22 17:077.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 03:29 108-67-807/19/22 17:077.2 2.4 1
Vinyl acetate ND ug/kg 07/20/22 03:29 108-05-407/19/22 17:0772.3 5.3 1
Vinyl chloride ND ug/kg 07/20/22 03:29 75-01-4 IH07/19/22 17:0714.5 3.7 1
Xylene (Total)ND ug/kg 07/20/22 03:29 1330-20-707/19/22 17:0714.5 4.1 1
m&p-Xylene ND ug/kg 07/20/22 03:29 179601-23-107/19/22 17:0714.5 4.9 1
o-Xylene ND ug/kg 07/20/22 03:29 95-47-607/19/22 17:077.2 3.2 1
Surrogates
Toluene-d8 (S)101 %07/20/22 03:29 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)100 %07/20/22 03:29 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)107 %07/20/22 03:29 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.2 %07/20/22 17:12 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 74.9 %07/25/22 13:2907/25/22 13:231
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-9 Lab ID:92615483009 Collected:07/15/22 15:50 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/18/22 12:10 18540-29-908/15/22 11:461.33 0.340 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-10 Lab ID:92615483010 Collected:07/15/22 16:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 16:57 7440-38-207/20/22 11:373.7 2.6 1
Barium 346 mg/kg 07/20/22 16:57 7440-39-307/20/22 11:371.2 0.51 1
Cadmium ND mg/kg 07/20/22 16:57 7440-43-907/20/22 11:371.2 0.36 1
Chromium 13.9 mg/kg 07/20/22 16:57 7440-47-307/20/22 11:371.2 1.1 1
Lead 80.2 mg/kg 07/20/22 16:57 7439-92-107/20/22 11:373.1 1.9 1
Selenium ND mg/kg 07/20/22 16:57 7782-49-207/20/22 11:376.1 5.3 1
Silver ND mg/kg 07/20/22 16:57 7440-22-407/20/22 11:371.2 0.50 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.071J mg/kg 07/25/22 14:00 7439-97-607/25/22 08:300.31 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/22/22 18:19 83-32-907/22/22 11:504321521
Acenaphthylene ND ug/kg 07/22/22 18:19 208-96-807/22/22 11:504321521
Aniline ND ug/kg 07/22/22 18:19 62-53-307/22/22 11:504321691
Anthracene ND ug/kg 07/22/22 18:19 120-12-707/22/22 11:504321411
Benzo(a)anthracene ND ug/kg 07/22/22 18:19 56-55-307/22/22 11:504321441
Benzo(a)pyrene ND ug/kg 07/22/22 18:19 50-32-807/22/22 11:504321491
Benzo(b)fluoranthene ND ug/kg 07/22/22 18:19 205-99-207/22/22 11:504321441
Benzo(g,h,i)perylene ND ug/kg 07/22/22 18:19 191-24-207/22/22 11:504321671
Benzo(k)fluoranthene ND ug/kg 07/22/22 18:19 207-08-907/22/22 11:504321521
Benzoic Acid ND ug/kg 07/22/22 18:19 65-85-007/22/22 11:5021609271
Benzyl alcohol ND ug/kg 07/22/22 18:19 100-51-607/22/22 11:508633271
4-Bromophenylphenyl ether ND ug/kg 07/22/22 18:19 101-55-307/22/22 11:504321661
Butylbenzylphthalate ND ug/kg 07/22/22 18:19 85-68-707/22/22 11:504321821
4-Chloro-3-methylphenol ND ug/kg 07/22/22 18:19 59-50-707/22/22 11:508633031
4-Chloroaniline ND ug/kg 07/22/22 18:19 106-47-807/22/22 11:508633391
bis(2-Chloroethoxy)methane ND ug/kg 07/22/22 18:19 111-91-107/22/22 11:504321791
bis(2-Chloroethyl) ether ND ug/kg 07/22/22 18:19 111-44-407/22/22 11:504321621
2-Chloronaphthalene ND ug/kg 07/22/22 18:19 91-58-707/22/22 11:504321711
2-Chlorophenol ND ug/kg 07/22/22 18:19 95-57-807/22/22 11:504321621
4-Chlorophenylphenyl ether ND ug/kg 07/22/22 18:19 7005-72-307/22/22 11:504321611
Chrysene ND ug/kg 07/22/22 18:19 218-01-907/22/22 11:504321571
Dibenz(a,h)anthracene ND ug/kg 07/22/22 18:19 53-70-307/22/22 11:504321661
Dibenzofuran ND ug/kg 07/22/22 18:19 132-64-907/22/22 11:504321561
1,2-Dichlorobenzene ND ug/kg 07/22/22 18:19 95-50-107/22/22 11:504321561
1,3-Dichlorobenzene ND ug/kg 07/22/22 18:19 541-73-107/22/22 11:504321531
1,4-Dichlorobenzene ND ug/kg 07/22/22 18:19 106-46-707/22/22 11:504321651
3,3'-Dichlorobenzidine ND ug/kg 07/22/22 18:19 91-94-107/22/22 11:508632921
2,4-Dichlorophenol ND ug/kg 07/22/22 18:19 120-83-207/22/22 11:504321691
Diethylphthalate ND ug/kg 07/22/22 18:19 84-66-207/22/22 11:504321581
2,4-Dimethylphenol ND ug/kg 07/22/22 18:19 105-67-907/22/22 11:504321791
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-10 Lab ID:92615483010 Collected:07/15/22 16:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/22/22 18:19 131-11-307/22/22 11:504321571
Di-n-butylphthalate ND ug/kg 07/22/22 18:19 84-74-207/22/22 11:504321451
4,6-Dinitro-2-methylphenol ND ug/kg 07/22/22 18:19 534-52-1 v207/22/22 11:508634031
2,4-Dinitrophenol ND ug/kg 07/22/22 18:19 51-28-5 v207/22/22 11:50216013301
2,4-Dinitrotoluene ND ug/kg 07/22/22 18:19 121-14-207/22/22 11:504321661
2,6-Dinitrotoluene ND ug/kg 07/22/22 18:19 606-20-207/22/22 11:504321581
Di-n-octylphthalate ND ug/kg 07/22/22 18:19 117-84-007/22/22 11:504321701
bis(2-Ethylhexyl)phthalate ND ug/kg 07/22/22 18:19 117-81-707/22/22 11:504321671
Fluoranthene ND ug/kg 07/22/22 18:19 206-44-007/22/22 11:504321481
Fluorene ND ug/kg 07/22/22 18:19 86-73-707/22/22 11:504321521
Hexachloro-1,3-butadiene ND ug/kg 07/22/22 18:19 87-68-307/22/22 11:504321871
Hexachlorobenzene ND ug/kg 07/22/22 18:19 118-74-107/22/22 11:504321691
Hexachlorocyclopentadiene ND ug/kg 07/22/22 18:19 77-47-4 v207/22/22 11:504322471
Hexachloroethane ND ug/kg 07/22/22 18:19 67-72-107/22/22 11:504321651
Indeno(1,2,3-cd)pyrene ND ug/kg 07/22/22 18:19 193-39-507/22/22 11:504321701
Isophorone ND ug/kg 07/22/22 18:19 78-59-107/22/22 11:504321921
1-Methylnaphthalene ND ug/kg 07/22/22 18:19 90-12-007/22/22 11:504321521
2-Methylnaphthalene ND ug/kg 07/22/22 18:19 91-57-607/22/22 11:504321731
2-Methylphenol(o-Cresol)ND ug/kg 07/22/22 18:19 95-48-707/22/22 11:504321771
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/22/22 18:19 15831-10-407/22/22 11:504321741
Naphthalene ND ug/kg 07/22/22 18:19 91-20-307/22/22 11:504321461
2-Nitroaniline ND ug/kg 07/22/22 18:19 88-74-407/22/22 11:5021603531
3-Nitroaniline ND ug/kg 07/22/22 18:19 99-09-207/22/22 11:5021603391
4-Nitroaniline ND ug/kg 07/22/22 18:19 100-01-6 v107/22/22 11:508633281
Nitrobenzene ND ug/kg 07/22/22 18:19 98-95-307/22/22 11:504322001
2-Nitrophenol ND ug/kg 07/22/22 18:19 88-75-507/22/22 11:504321871
4-Nitrophenol ND ug/kg 07/22/22 18:19 100-02-7 v107/22/22 11:5021608341
N-Nitrosodimethylamine ND ug/kg 07/22/22 18:19 62-75-9 v107/22/22 11:504321451
N-Nitroso-di-n-propylamine ND ug/kg 07/22/22 18:19 621-64-707/22/22 11:504321621
N-Nitrosodiphenylamine ND ug/kg 07/22/22 18:19 86-30-607/22/22 11:504321531
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/22/22 18:19 108-60-107/22/22 11:504322051
Pentachlorophenol ND ug/kg 07/22/22 18:19 87-86-507/22/22 11:508634221
Phenanthrene ND ug/kg 07/22/22 18:19 85-01-807/22/22 11:504321411
Phenol ND ug/kg 07/22/22 18:19 108-95-207/22/22 11:504321921
Pyrene ND ug/kg 07/22/22 18:19 129-00-007/22/22 11:504321751
Pyridine ND ug/kg 07/22/22 18:19 110-86-1 v107/22/22 11:504321361
1,2,4-Trichlorobenzene ND ug/kg 07/22/22 18:19 120-82-107/22/22 11:504321701
2,4,5-Trichlorophenol ND ug/kg 07/22/22 18:19 95-95-407/22/22 11:504321971
2,4,6-Trichlorophenol ND ug/kg 07/22/22 18:19 88-06-207/22/22 11:504321781
Surrogates
Nitrobenzene-d5 (S)79 %07/22/22 18:19 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)64 %07/22/22 18:19 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)66 %07/22/22 18:19 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)82 %07/22/22 18:19 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-10 Lab ID:92615483010 Collected:07/15/22 16:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)74 %07/22/22 18:19 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)88 %07/22/22 18:19 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 03:47 67-64-107/19/22 17:0714546.5 1
Benzene ND ug/kg 07/20/22 03:47 71-43-207/19/22 17:077.2 2.9 1
Bromobenzene ND ug/kg 07/20/22 03:47 108-86-107/19/22 17:077.2 2.4 1
Bromochloromethane ND ug/kg 07/20/22 03:47 74-97-507/19/22 17:077.2 2.1 1
Bromodichloromethane ND ug/kg 07/20/22 03:47 75-27-407/19/22 17:077.2 2.8 1
Bromoform ND ug/kg 07/20/22 03:47 75-25-207/19/22 17:077.2 2.6 1
Bromomethane ND ug/kg 07/20/22 03:47 74-83-9 L107/19/22 17:0714.5 11.5 1
2-Butanone (MEK)49.0J ug/kg 07/20/22 03:47 78-93-3 C707/19/22 17:0714534.8 1
n-Butylbenzene ND ug/kg 07/20/22 03:47 104-51-807/19/22 17:077.2 3.4 1
sec-Butylbenzene ND ug/kg 07/20/22 03:47 135-98-807/19/22 17:077.2 3.2 1
tert-Butylbenzene ND ug/kg 07/20/22 03:47 98-06-607/19/22 17:077.2 2.6 1
Carbon tetrachloride ND ug/kg 07/20/22 03:47 56-23-507/19/22 17:077.2 2.7 1
Chlorobenzene ND ug/kg 07/20/22 03:47 108-90-707/19/22 17:077.2 1.4 1
Chloroethane ND ug/kg 07/20/22 03:47 75-00-3 IH07/19/22 17:0714.5 5.6 1
Chloroform ND ug/kg 07/20/22 03:47 67-66-307/19/22 17:077.2 4.4 1
Chloromethane ND ug/kg 07/20/22 03:47 74-87-3 IH07/19/22 17:0714.5 6.1 1
2-Chlorotoluene ND ug/kg 07/20/22 03:47 95-49-807/19/22 17:077.2 2.6 1
4-Chlorotoluene ND ug/kg 07/20/22 03:47 106-43-407/19/22 17:077.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 03:47 96-12-8 v207/19/22 17:077.2 2.8 1
Dibromochloromethane ND ug/kg 07/20/22 03:47 124-48-107/19/22 17:077.2 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 03:47 106-93-407/19/22 17:077.2 3.2 1
Dibromomethane ND ug/kg 07/20/22 03:47 74-95-307/19/22 17:077.2 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 03:47 95-50-107/19/22 17:077.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 03:47 541-73-107/19/22 17:077.2 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 03:47 106-46-707/19/22 17:077.2 1.9 1
Dichlorodifluoromethane ND ug/kg 07/20/22 03:47 75-71-8 IH,L107/19/22 17:0714.5 3.1 1
1,1-Dichloroethane ND ug/kg 07/20/22 03:47 75-34-307/19/22 17:077.2 3.0 1
1,2-Dichloroethane ND ug/kg 07/20/22 03:47 107-06-207/19/22 17:077.2 4.8 1
1,1-Dichloroethene ND ug/kg 07/20/22 03:47 75-35-407/19/22 17:077.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 03:47 156-59-207/19/22 17:077.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 03:47 156-60-507/19/22 17:077.2 2.5 1
1,2-Dichloropropane ND ug/kg 07/20/22 03:47 78-87-507/19/22 17:077.2 2.2 1
1,3-Dichloropropane ND ug/kg 07/20/22 03:47 142-28-907/19/22 17:077.2 2.3 1
2,2-Dichloropropane ND ug/kg 07/20/22 03:47 594-20-707/19/22 17:077.2 2.4 1
1,1-Dichloropropene ND ug/kg 07/20/22 03:47 563-58-607/19/22 17:077.2 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 03:47 10061-01-507/19/22 17:077.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 03:47 10061-02-607/19/22 17:077.2 2.5 1
Diisopropyl ether ND ug/kg 07/20/22 03:47 108-20-307/19/22 17:077.2 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-10 Lab ID:92615483010 Collected:07/15/22 16:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 03:47 100-41-407/19/22 17:077.2 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 03:47 87-68-307/19/22 17:0714.5 11.9 1
2-Hexanone ND ug/kg 07/20/22 03:47 591-78-607/19/22 17:0772.5 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 03:47 98-82-807/19/22 17:077.2 2.5 1
p-Isopropyltoluene ND ug/kg 07/20/22 03:47 99-87-607/19/22 17:077.2 3.6 1
Methylene Chloride ND ug/kg 07/20/22 03:47 75-09-207/19/22 17:0729.0 19.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 03:47 108-10-107/19/22 17:0772.5 7.0 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 03:47 1634-04-407/19/22 17:077.2 2.7 1
Naphthalene ND ug/kg 07/20/22 03:47 91-20-3 v207/19/22 17:077.2 3.8 1
n-Propylbenzene ND ug/kg 07/20/22 03:47 103-65-107/19/22 17:077.2 2.6 1
Styrene ND ug/kg 07/20/22 03:47 100-42-507/19/22 17:077.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 03:47 630-20-607/19/22 17:077.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 03:47 79-34-507/19/22 17:077.2 1.9 1
Tetrachloroethene ND ug/kg 07/20/22 03:47 127-18-407/19/22 17:077.2 2.3 1
Toluene ND ug/kg 07/20/22 03:47 108-88-307/19/22 17:077.2 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 03:47 87-61-6 v207/19/22 17:077.2 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 03:47 120-82-107/19/22 17:077.2 6.1 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 03:47 71-55-607/19/22 17:077.2 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 03:47 79-00-507/19/22 17:077.2 2.4 1
Trichloroethene ND ug/kg 07/20/22 03:47 79-01-607/19/22 17:077.2 1.9 1
Trichlorofluoromethane ND ug/kg 07/20/22 03:47 75-69-407/19/22 17:077.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 03:47 96-18-407/19/22 17:077.2 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 03:47 95-63-607/19/22 17:077.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 03:47 108-67-807/19/22 17:077.2 2.4 1
Vinyl acetate ND ug/kg 07/20/22 03:47 108-05-407/19/22 17:0772.5 5.3 1
Vinyl chloride ND ug/kg 07/20/22 03:47 75-01-4 IH07/19/22 17:0714.5 3.7 1
Xylene (Total)ND ug/kg 07/20/22 03:47 1330-20-707/19/22 17:0714.5 4.1 1
m&p-Xylene ND ug/kg 07/20/22 03:47 179601-23-107/19/22 17:0714.5 5.0 1
o-Xylene ND ug/kg 07/20/22 03:47 95-47-607/19/22 17:077.2 3.2 1
Surrogates
Toluene-d8 (S)102 %07/20/22 03:47 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)101 %07/20/22 03:47 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)105 %07/20/22 03:47 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.3 %07/20/22 17:12 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 69.0 %07/25/22 13:2907/25/22 13:231
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-10 Lab ID:92615483010 Collected:07/15/22 16:00 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/18/22 12:15 18540-29-908/15/22 11:461.45 0.369 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-11 Lab ID:92615483011 Collected:07/15/22 16:10 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 07/20/22 17:02 7440-38-207/20/22 11:374.1 2.9 1
Barium 90.8 mg/kg 07/20/22 17:02 7440-39-307/20/22 11:371.4 0.57 1
Cadmium ND mg/kg 07/20/22 17:02 7440-43-907/20/22 11:371.4 0.41 1
Chromium 15.9 mg/kg 07/20/22 17:02 7440-47-307/20/22 11:371.4 1.2 1
Lead 52.8 mg/kg 07/20/22 17:02 7439-92-107/20/22 11:373.4 2.1 1
Selenium ND mg/kg 07/20/22 17:06 7782-49-2 D307/20/22 11:3734.3 29.7 5
Silver ND mg/kg 07/20/22 17:02 7440-22-407/20/22 11:371.4 0.56 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.12J mg/kg 07/25/22 14:03 7439-97-607/25/22 08:300.35 0.015 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/25/22 11:08 83-32-907/22/22 11:504631631
Acenaphthylene ND ug/kg 07/25/22 11:08 208-96-807/22/22 11:504631631
Aniline ND ug/kg 07/25/22 11:08 62-53-307/22/22 11:504631811
Anthracene ND ug/kg 07/25/22 11:08 120-12-707/22/22 11:504631521
Benzo(a)anthracene ND ug/kg 07/25/22 11:08 56-55-307/22/22 11:504631541
Benzo(a)pyrene ND ug/kg 07/25/22 11:08 50-32-807/22/22 11:504631601
Benzo(b)fluoranthene ND ug/kg 07/25/22 11:08 205-99-207/22/22 11:504631541
Benzo(g,h,i)perylene ND ug/kg 07/25/22 11:08 191-24-207/22/22 11:504631801
Benzo(k)fluoranthene ND ug/kg 07/25/22 11:08 207-08-907/22/22 11:504631631
Benzoic Acid ND ug/kg 07/25/22 11:08 65-85-007/22/22 11:5023209951
Benzyl alcohol ND ug/kg 07/25/22 11:08 100-51-607/22/22 11:509263511
4-Bromophenylphenyl ether ND ug/kg 07/25/22 11:08 101-55-307/22/22 11:504631781
Butylbenzylphthalate ND ug/kg 07/25/22 11:08 85-68-707/22/22 11:504631951
4-Chloro-3-methylphenol ND ug/kg 07/25/22 11:08 59-50-707/22/22 11:509263261
4-Chloroaniline ND ug/kg 07/25/22 11:08 106-47-807/22/22 11:509263631
bis(2-Chloroethoxy)methane ND ug/kg 07/25/22 11:08 111-91-107/22/22 11:504631921
bis(2-Chloroethyl) ether ND ug/kg 07/25/22 11:08 111-44-407/22/22 11:504631741
2-Chloronaphthalene ND ug/kg 07/25/22 11:08 91-58-707/22/22 11:504631841
2-Chlorophenol ND ug/kg 07/25/22 11:08 95-57-807/22/22 11:504631741
4-Chlorophenylphenyl ether ND ug/kg 07/25/22 11:08 7005-72-307/22/22 11:504631731
Chrysene ND ug/kg 07/25/22 11:08 218-01-907/22/22 11:504631681
Dibenz(a,h)anthracene ND ug/kg 07/25/22 11:08 53-70-307/22/22 11:504631781
Dibenzofuran ND ug/kg 07/25/22 11:08 132-64-907/22/22 11:504631671
1,2-Dichlorobenzene ND ug/kg 07/25/22 11:08 95-50-107/22/22 11:504631671
1,3-Dichlorobenzene ND ug/kg 07/25/22 11:08 541-73-107/22/22 11:504631641
1,4-Dichlorobenzene ND ug/kg 07/25/22 11:08 106-46-707/22/22 11:504631771
3,3'-Dichlorobenzidine ND ug/kg 07/25/22 11:08 91-94-107/22/22 11:509263131
2,4-Dichlorophenol ND ug/kg 07/25/22 11:08 120-83-207/22/22 11:504631811
Diethylphthalate ND ug/kg 07/25/22 11:08 84-66-207/22/22 11:504631701
2,4-Dimethylphenol ND ug/kg 07/25/22 11:08 105-67-907/22/22 11:504631921
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-11 Lab ID:92615483011 Collected:07/15/22 16:10 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 07/25/22 11:08 131-11-307/22/22 11:504631681
Di-n-butylphthalate ND ug/kg 07/25/22 11:08 84-74-207/22/22 11:504631561
4,6-Dinitro-2-methylphenol ND ug/kg 07/25/22 11:08 534-52-107/22/22 11:509264321
2,4-Dinitrophenol ND ug/kg 07/25/22 11:08 51-28-507/22/22 11:50232014301
2,4-Dinitrotoluene ND ug/kg 07/25/22 11:08 121-14-207/22/22 11:504631781
2,6-Dinitrotoluene ND ug/kg 07/25/22 11:08 606-20-207/22/22 11:504631701
Di-n-octylphthalate ND ug/kg 07/25/22 11:08 117-84-007/22/22 11:504631821
bis(2-Ethylhexyl)phthalate ND ug/kg 07/25/22 11:08 117-81-707/22/22 11:504631801
Fluoranthene ND ug/kg 07/25/22 11:08 206-44-007/22/22 11:504631591
Fluorene ND ug/kg 07/25/22 11:08 86-73-707/22/22 11:504631631
Hexachloro-1,3-butadiene ND ug/kg 07/25/22 11:08 87-68-307/22/22 11:504632011
Hexachlorobenzene ND ug/kg 07/25/22 11:08 118-74-107/22/22 11:504631811
Hexachlorocyclopentadiene ND ug/kg 07/25/22 11:08 77-47-407/22/22 11:504632651
Hexachloroethane ND ug/kg 07/25/22 11:08 67-72-107/22/22 11:504631771
Indeno(1,2,3-cd)pyrene ND ug/kg 07/25/22 11:08 193-39-507/22/22 11:504631821
Isophorone ND ug/kg 07/25/22 11:08 78-59-107/22/22 11:504632061
1-Methylnaphthalene ND ug/kg 07/25/22 11:08 90-12-007/22/22 11:504631631
2-Methylnaphthalene ND ug/kg 07/25/22 11:08 91-57-607/22/22 11:504631851
2-Methylphenol(o-Cresol)ND ug/kg 07/25/22 11:08 95-48-707/22/22 11:504631891
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/25/22 11:08 15831-10-407/22/22 11:504631871
Naphthalene ND ug/kg 07/25/22 11:08 91-20-307/22/22 11:504631571
2-Nitroaniline ND ug/kg 07/25/22 11:08 88-74-407/22/22 11:5023203791
3-Nitroaniline ND ug/kg 07/25/22 11:08 99-09-207/22/22 11:5023203631
4-Nitroaniline ND ug/kg 07/25/22 11:08 100-01-607/22/22 11:509263521
Nitrobenzene ND ug/kg 07/25/22 11:08 98-95-307/22/22 11:504632151
2-Nitrophenol ND ug/kg 07/25/22 11:08 88-75-507/22/22 11:504632011
4-Nitrophenol ND ug/kg 07/25/22 11:08 100-02-707/22/22 11:5023208951
N-Nitrosodimethylamine ND ug/kg 07/25/22 11:08 62-75-907/22/22 11:504631561
N-Nitroso-di-n-propylamine ND ug/kg 07/25/22 11:08 621-64-707/22/22 11:504631741
N-Nitrosodiphenylamine ND ug/kg 07/25/22 11:08 86-30-607/22/22 11:504631641
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/25/22 11:08 108-60-107/22/22 11:504632201
Pentachlorophenol ND ug/kg 07/25/22 11:08 87-86-507/22/22 11:509264531
Phenanthrene ND ug/kg 07/25/22 11:08 85-01-807/22/22 11:504631521
Phenol ND ug/kg 07/25/22 11:08 108-95-207/22/22 11:504632061
Pyrene ND ug/kg 07/25/22 11:08 129-00-007/22/22 11:504631881
Pyridine ND ug/kg 07/25/22 11:08 110-86-107/22/22 11:504631461
1,2,4-Trichlorobenzene ND ug/kg 07/25/22 11:08 120-82-107/22/22 11:504631821
2,4,5-Trichlorophenol ND ug/kg 07/25/22 11:08 95-95-407/22/22 11:504632121
2,4,6-Trichlorophenol ND ug/kg 07/25/22 11:08 88-06-207/22/22 11:504631911
Surrogates
Nitrobenzene-d5 (S)68 %07/25/22 11:08 4165-60-007/22/22 11:5021-130 1
2-Fluorobiphenyl (S)56 %07/25/22 11:08 321-60-807/22/22 11:5019-130 1
Terphenyl-d14 (S)71 %07/25/22 11:08 1718-51-007/22/22 11:5015-130 1
Phenol-d6 (S)65 %07/25/22 11:08 13127-88-307/22/22 11:5018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-11 Lab ID:92615483011 Collected:07/15/22 16:10 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)65 %07/25/22 11:08 367-12-407/22/22 11:5018-130 1
2,4,6-Tribromophenol (S)68 %07/25/22 11:08 118-79-607/22/22 11:5018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/20/22 04:04 67-64-107/19/22 17:0716954.2 1
Benzene ND ug/kg 07/20/22 04:04 71-43-207/19/22 17:078.4 3.4 1
Bromobenzene ND ug/kg 07/20/22 04:04 108-86-107/19/22 17:078.4 2.8 1
Bromochloromethane ND ug/kg 07/20/22 04:04 74-97-507/19/22 17:078.4 2.5 1
Bromodichloromethane ND ug/kg 07/20/22 04:04 75-27-407/19/22 17:078.4 3.3 1
Bromoform ND ug/kg 07/20/22 04:04 75-25-207/19/22 17:078.4 3.0 1
Bromomethane ND ug/kg 07/20/22 04:04 74-83-9 L107/19/22 17:0716.9 13.3 1
2-Butanone (MEK)56.7J ug/kg 07/20/22 04:04 78-93-3 C707/19/22 17:0716940.5 1
n-Butylbenzene ND ug/kg 07/20/22 04:04 104-51-807/19/22 17:078.4 4.0 1
sec-Butylbenzene ND ug/kg 07/20/22 04:04 135-98-807/19/22 17:078.4 3.7 1
tert-Butylbenzene ND ug/kg 07/20/22 04:04 98-06-607/19/22 17:078.4 3.0 1
Carbon tetrachloride ND ug/kg 07/20/22 04:04 56-23-507/19/22 17:078.4 3.2 1
Chlorobenzene ND ug/kg 07/20/22 04:04 108-90-707/19/22 17:078.4 1.6 1
Chloroethane ND ug/kg 07/20/22 04:04 75-00-3 IH07/19/22 17:0716.9 6.5 1
Chloroform ND ug/kg 07/20/22 04:04 67-66-307/19/22 17:078.4 5.1 1
Chloromethane ND ug/kg 07/20/22 04:04 74-87-3 IH07/19/22 17:0716.9 7.1 1
2-Chlorotoluene ND ug/kg 07/20/22 04:04 95-49-807/19/22 17:078.4 3.0 1
4-Chlorotoluene ND ug/kg 07/20/22 04:04 106-43-407/19/22 17:078.4 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/20/22 04:04 96-12-8 v207/19/22 17:078.4 3.3 1
Dibromochloromethane ND ug/kg 07/20/22 04:04 124-48-107/19/22 17:078.4 4.7 1
1,2-Dibromoethane (EDB)ND ug/kg 07/20/22 04:04 106-93-407/19/22 17:078.4 3.7 1
Dibromomethane ND ug/kg 07/20/22 04:04 74-95-307/19/22 17:078.4 1.8 1
1,2-Dichlorobenzene ND ug/kg 07/20/22 04:04 95-50-107/19/22 17:078.4 3.0 1
1,3-Dichlorobenzene ND ug/kg 07/20/22 04:04 541-73-107/19/22 17:078.4 2.6 1
1,4-Dichlorobenzene ND ug/kg 07/20/22 04:04 106-46-707/19/22 17:078.4 2.2 1
Dichlorodifluoromethane ND ug/kg 07/20/22 04:04 75-71-8 IH,L107/19/22 17:0716.9 3.7 1
1,1-Dichloroethane ND ug/kg 07/20/22 04:04 75-34-307/19/22 17:078.4 3.5 1
1,2-Dichloroethane ND ug/kg 07/20/22 04:04 107-06-207/19/22 17:078.4 5.6 1
1,1-Dichloroethene ND ug/kg 07/20/22 04:04 75-35-407/19/22 17:078.4 3.5 1
cis-1,2-Dichloroethene ND ug/kg 07/20/22 04:04 156-59-207/19/22 17:078.4 2.9 1
trans-1,2-Dichloroethene ND ug/kg 07/20/22 04:04 156-60-507/19/22 17:078.4 3.0 1
1,2-Dichloropropane ND ug/kg 07/20/22 04:04 78-87-507/19/22 17:078.4 2.5 1
1,3-Dichloropropane ND ug/kg 07/20/22 04:04 142-28-907/19/22 17:078.4 2.6 1
2,2-Dichloropropane ND ug/kg 07/20/22 04:04 594-20-707/19/22 17:078.4 2.8 1
1,1-Dichloropropene ND ug/kg 07/20/22 04:04 563-58-607/19/22 17:078.4 4.1 1
cis-1,3-Dichloropropene ND ug/kg 07/20/22 04:04 10061-01-507/19/22 17:078.4 2.3 1
trans-1,3-Dichloropropene ND ug/kg 07/20/22 04:04 10061-02-607/19/22 17:078.4 2.9 1
Diisopropyl ether ND ug/kg 07/20/22 04:04 108-20-307/19/22 17:078.4 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-11 Lab ID:92615483011 Collected:07/15/22 16:10 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 07/20/22 04:04 100-41-407/19/22 17:078.4 3.9 1
Hexachloro-1,3-butadiene ND ug/kg 07/20/22 04:04 87-68-307/19/22 17:0716.9 13.8 1
2-Hexanone ND ug/kg 07/20/22 04:04 591-78-607/19/22 17:0784.4 8.1 1
Isopropylbenzene (Cumene)ND ug/kg 07/20/22 04:04 98-82-807/19/22 17:078.4 2.9 1
p-Isopropyltoluene ND ug/kg 07/20/22 04:04 99-87-607/19/22 17:078.4 4.2 1
Methylene Chloride 56.4 ug/kg 07/20/22 04:04 75-09-2 C707/19/22 17:0733.8 23.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/20/22 04:04 108-10-107/19/22 17:0784.4 8.1 1
Methyl-tert-butyl ether ND ug/kg 07/20/22 04:04 1634-04-407/19/22 17:078.4 3.2 1
Naphthalene ND ug/kg 07/20/22 04:04 91-20-3 v207/19/22 17:078.4 4.4 1
n-Propylbenzene ND ug/kg 07/20/22 04:04 103-65-107/19/22 17:078.4 3.0 1
Styrene ND ug/kg 07/20/22 04:04 100-42-507/19/22 17:078.4 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/20/22 04:04 630-20-607/19/22 17:078.4 3.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/20/22 04:04 79-34-507/19/22 17:078.4 2.2 1
Tetrachloroethene ND ug/kg 07/20/22 04:04 127-18-407/19/22 17:078.4 2.7 1
Toluene ND ug/kg 07/20/22 04:04 108-88-307/19/22 17:078.4 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 07/20/22 04:04 87-61-6 v207/19/22 17:078.4 6.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/20/22 04:04 120-82-107/19/22 17:078.4 7.1 1
1,1,1-Trichloroethane ND ug/kg 07/20/22 04:04 71-55-607/19/22 17:078.4 4.4 1
1,1,2-Trichloroethane ND ug/kg 07/20/22 04:04 79-00-507/19/22 17:078.4 2.8 1
Trichloroethene ND ug/kg 07/20/22 04:04 79-01-607/19/22 17:078.4 2.2 1
Trichlorofluoromethane ND ug/kg 07/20/22 04:04 75-69-407/19/22 17:078.4 4.6 1
1,2,3-Trichloropropane ND ug/kg 07/20/22 04:04 96-18-407/19/22 17:078.4 4.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/20/22 04:04 95-63-607/19/22 17:078.4 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 07/20/22 04:04 108-67-807/19/22 17:078.4 2.8 1
Vinyl acetate ND ug/kg 07/20/22 04:04 108-05-407/19/22 17:0784.4 6.1 1
Vinyl chloride ND ug/kg 07/20/22 04:04 75-01-4 IH07/19/22 17:0716.9 4.3 1
Xylene (Total)ND ug/kg 07/20/22 04:04 1330-20-707/19/22 17:0716.9 4.8 1
m&p-Xylene ND ug/kg 07/20/22 04:04 179601-23-107/19/22 17:0716.9 5.8 1
o-Xylene ND ug/kg 07/20/22 04:04 95-47-607/19/22 17:078.4 3.7 1
Surrogates
Toluene-d8 (S)102 %07/20/22 04:04 2037-26-507/19/22 17:0770-130 1
4-Bromofluorobenzene (S)101 %07/20/22 04:04 460-00-407/19/22 17:0769-134 1
1,2-Dichloroethane-d4 (S)108 %07/20/22 04:04 17060-07-007/19/22 17:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.9 %07/20/22 17:12 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 69.5 %07/25/22 13:2907/25/22 13:231
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92615483
Mock Judson 1533
Sample:SS-11 Lab ID:92615483011 Collected:07/15/22 16:10 Received:07/18/22 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/18/22 12:31 18540-29-908/15/22 11:461.44 0.367 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
711699
EPA 3050B
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3711132
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.9 07/20/22 15:162.1
Barium mg/kg ND 0.96 07/20/22 15:160.40
Cadmium mg/kg ND 0.96 07/20/22 15:160.28
Chromium mg/kg ND 0.96 07/20/22 15:160.87
Lead mg/kg ND 2.4 07/20/22 15:161.5
Selenium mg/kg ND 4.8 07/20/22 15:164.2
Silver mg/kg ND 0.96 07/20/22 15:160.39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3711133LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 92.998 95 80-120
Barium mg/kg 94.798 97 80-120
Cadmium mg/kg 97.398 99 80-120
Chromium mg/kg 97.998 100 80-120
Lead mg/kg 97.198 99 80-120
Selenium mg/kg 87.398 89 80-120
Silver mg/kg 94.198 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3711134MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92615483001
3711135
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 121 93 75-12595 2 20121ND112115
Barium mg/kg 121 99 75-12595 3 2012115.1 134 130
Cadmium mg/kg 121 99 75-125102 2 20121ND120123
Chromium mg/kg 121 98 75-125100 1 201213.0 122 124
Lead mg/kg 121 99 75-125102 3 201214.5 124 128
Selenium mg/kg 121 85 75-12585 0 20121ND103103
Silver mg/kg 121 95 75-12597 2 20121ND115118
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712335
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3714213
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.24 07/25/22 12:580.010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3714214LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.290.33 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3714215MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92615328006
3714216
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.36 88 75-12579 6 200.380.013J 0.33 0.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
711539
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92615483001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3710363
Associated Lab Samples:92615483001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/20/22 00:491.9
1,1,1-Trichloroethane ug/kg ND 5.0 07/20/22 00:492.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/20/22 00:491.3
1,1,2-Trichloroethane ug/kg ND 5.0 07/20/22 00:491.7
1,1-Dichloroethane ug/kg ND 5.0 07/20/22 00:492.1
1,1-Dichloroethene ug/kg ND 5.0 07/20/22 00:492.1
1,1-Dichloropropene ug/kg ND 5.0 07/20/22 00:492.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 v207/20/22 00:494.0
1,2,3-Trichloropropane ug/kg ND 5.0 07/20/22 00:492.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/20/22 00:494.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/20/22 00:491.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 v207/20/22 00:491.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/20/22 00:492.2
1,2-Dichlorobenzene ug/kg ND 5.0 07/20/22 00:491.8
1,2-Dichloroethane ug/kg ND 5.0 07/20/22 00:493.3
1,2-Dichloropropane ug/kg ND 5.0 07/20/22 00:491.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/20/22 00:491.7
1,3-Dichlorobenzene ug/kg ND 5.0 07/20/22 00:491.6
1,3-Dichloropropane ug/kg ND 5.0 07/20/22 00:491.6
1,4-Dichlorobenzene ug/kg ND 5.0 07/20/22 00:491.3
2,2-Dichloropropane ug/kg ND 5.0 07/20/22 00:491.6
2-Butanone (MEK)ug/kg ND 100 07/20/22 00:4924.0
2-Chlorotoluene ug/kg ND 5.0 07/20/22 00:491.8
2-Hexanone ug/kg ND 50.0 07/20/22 00:494.8
4-Chlorotoluene ug/kg ND 5.0 07/20/22 00:490.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/20/22 00:494.8
Acetone ug/kg ND 100 07/20/22 00:4932.1
Benzene ug/kg ND 5.0 07/20/22 00:492.0
Bromobenzene ug/kg ND 5.0 07/20/22 00:491.6
Bromochloromethane ug/kg ND 5.0 07/20/22 00:491.5
Bromodichloromethane ug/kg ND 5.0 07/20/22 00:491.9
Bromoform ug/kg ND 5.0 07/20/22 00:491.8
Bromomethane ug/kg ND 10.0 07/20/22 00:497.9
Carbon tetrachloride ug/kg ND 5.0 07/20/22 00:491.9
Chlorobenzene ug/kg ND 5.0 07/20/22 00:490.96
Chloroethane ug/kg ND 10.0 IH07/20/22 00:493.9
Chloroform ug/kg 4.2J 5.0 07/20/22 00:493.0
Chloromethane ug/kg ND 10.0 IH07/20/22 00:494.2
cis-1,2-Dichloroethene ug/kg ND 5.0 07/20/22 00:491.7
cis-1,3-Dichloropropene ug/kg ND 5.0 07/20/22 00:491.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3710363
Associated Lab Samples:92615483001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 07/20/22 00:492.8
Dibromomethane ug/kg ND 5.0 07/20/22 00:491.1
Dichlorodifluoromethane ug/kg ND 10.0 IH07/20/22 00:492.2
Diisopropyl ether ug/kg ND 5.0 07/20/22 00:491.4
Ethylbenzene ug/kg ND 5.0 07/20/22 00:492.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/20/22 00:498.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/20/22 00:491.7
m&p-Xylene ug/kg ND 10.0 07/20/22 00:493.4
Methyl-tert-butyl ether ug/kg ND 5.0 07/20/22 00:491.9
Methylene Chloride ug/kg ND 20.0 07/20/22 00:4913.7
n-Butylbenzene ug/kg ND 5.0 07/20/22 00:492.4
n-Propylbenzene ug/kg ND 5.0 07/20/22 00:491.8
Naphthalene ug/kg ND 5.0 v207/20/22 00:492.6
o-Xylene ug/kg ND 5.0 07/20/22 00:492.2
p-Isopropyltoluene ug/kg ND 5.0 07/20/22 00:492.5
sec-Butylbenzene ug/kg ND 5.0 07/20/22 00:492.2
Styrene ug/kg ND 5.0 07/20/22 00:491.3
tert-Butylbenzene ug/kg ND 5.0 07/20/22 00:491.8
Tetrachloroethene ug/kg ND 5.0 07/20/22 00:491.6
Toluene ug/kg ND 5.0 07/20/22 00:491.4
trans-1,2-Dichloroethene ug/kg ND 5.0 07/20/22 00:491.8
trans-1,3-Dichloropropene ug/kg ND 5.0 07/20/22 00:491.7
Trichloroethene ug/kg ND 5.0 07/20/22 00:491.3
Trichlorofluoromethane ug/kg ND 5.0 07/20/22 00:492.8
Vinyl acetate ug/kg ND 50.0 07/20/22 00:493.6
Vinyl chloride ug/kg ND 10.0 IH07/20/22 00:492.5
Xylene (Total)ug/kg ND 10.0 07/20/22 00:492.8
1,2-Dichloroethane-d4 (S)%107 70-130 07/20/22 00:49
4-Bromofluorobenzene (S)%101 69-134 07/20/22 00:49
Toluene-d8 (S)%99 70-130 07/20/22 00:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3710364LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 14701250 118 70-130
1,1,1-Trichloroethane ug/kg 13401250 107 70-130
1,1,2,2-Tetrachloroethane ug/kg 13501250 108 70-130
1,1,2-Trichloroethane ug/kg 14701250 117 70-130
1,1-Dichloroethane ug/kg 12801250 103 70-130
1,1-Dichloroethene ug/kg 13601250 109 70-130
1,1-Dichloropropene ug/kg 13801250 110 70-130
1,2,3-Trichlorobenzene ug/kg 1010 v312508165-130
1,2,3-Trichloropropane ug/kg 13301250 106 70-130
1,2,4-Trichlorobenzene ug/kg 11901250 95 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3710364LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 14301250 115 70-130
1,2-Dibromo-3-chloropropane ug/kg 1030 v312508370-130
1,2-Dibromoethane (EDB)ug/kg 14601250 117 70-130
1,2-Dichlorobenzene ug/kg 14101250 113 70-130
1,2-Dichloroethane ug/kg 14801250 119 63-130
1,2-Dichloropropane ug/kg 14201250 114 70-130
1,3,5-Trimethylbenzene ug/kg 14701250 118 70-130
1,3-Dichlorobenzene ug/kg 14401250 115 70-130
1,3-Dichloropropane ug/kg 14101250 113 70-130
1,4-Dichlorobenzene ug/kg 13801250 110 70-130
2,2-Dichloropropane ug/kg 13901250 111 66-130
2-Butanone (MEK)ug/kg 24302500 97 70-130
2-Chlorotoluene ug/kg 14601250 117 70-130
2-Hexanone ug/kg 29602500 118 70-130
4-Chlorotoluene ug/kg 14601250 116 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 28702500 115 70-130
Acetone ug/kg 24002500 96 69-130
Benzene ug/kg 13501250 108 70-130
Bromobenzene ug/kg 15101250 121 70-130
Bromochloromethane ug/kg 13601250 109 70-130
Bromodichloromethane ug/kg 15001250 120 69-130
Bromoform ug/kg 14401250 116 70-130
Bromomethane ug/kg 1910 L1125015352-130
Carbon tetrachloride ug/kg 15301250 123 70-130
Chlorobenzene ug/kg 14101250 113 70-130
Chloroethane ug/kg 1540 IH125012365-130
Chloroform ug/kg 12201250 98 70-130
Chloromethane ug/kg 1630 IH,L1125013155-130
cis-1,2-Dichloroethene ug/kg 13201250 105 70-130
cis-1,3-Dichloropropene ug/kg 14801250 119 70-130
Dibromochloromethane ug/kg 14401250 116 70-130
Dibromomethane ug/kg 14801250 118 70-130
Dichlorodifluoromethane ug/kg 1920 IH125015445-156
Diisopropyl ether ug/kg 13101250 105 70-130
Ethylbenzene ug/kg 13401250 107 70-130
Hexachloro-1,3-butadiene ug/kg 12001250 96 66-130
Isopropylbenzene (Cumene)ug/kg 14001250 112 70-130
m&p-Xylene ug/kg 28702500 115 70-130
Methyl-tert-butyl ether ug/kg 13601250 109 70-130
Methylene Chloride ug/kg 12501250 100 65-130
n-Butylbenzene ug/kg 14101250 113 67-130
n-Propylbenzene ug/kg 14301250 114 70-130
Naphthalene ug/kg 1060 v312508570-130
o-Xylene ug/kg 14701250 118 70-130
p-Isopropyltoluene ug/kg 14801250 118 67-130
sec-Butylbenzene ug/kg 14101250 113 69-130
Styrene ug/kg 15101250 120 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3710364LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 14201250 114 67-130
Tetrachloroethene ug/kg 13601250 109 70-130
Toluene ug/kg 13901250 111 70-130
trans-1,2-Dichloroethene ug/kg 13001250 104 70-130
trans-1,3-Dichloropropene ug/kg 15301250 122 68-130
Trichloroethene ug/kg 14501250 116 70-130
Trichlorofluoromethane ug/kg 13801250 110 70-130
Vinyl acetate ug/kg 28902500 116 70-130
Vinyl chloride ug/kg 1620 IH125013061-130
Xylene (Total)ug/kg 43503750 116 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3710365MATRIX SPIKE SAMPLE:
MSSpike
Result
92615303001
1,1,1,2-Tetrachloroethane ug/kg 670771 87 70-131ND
1,1,1-Trichloroethane ug/kg 723771 94 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 622771 81 66-130ND
1,1,2-Trichloroethane ug/kg 659771 85 66-133ND
1,1-Dichloroethane ug/kg 689771 89 65-130ND
1,1-Dichloroethene ug/kg 789771 102 10-158ND
1,1-Dichloropropene ug/kg 720771 93 68-133ND
1,2,3-Trichlorobenzene ug/kg 252 v37713327-138ND
1,2,3-Trichloropropane ug/kg 584771 76 67-130ND
1,2,4-Trichlorobenzene ug/kg 427771 55 51-134ND
1,2,4-Trimethylbenzene ug/kg 680771 88 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 380 v37714932-130ND
1,2-Dibromoethane (EDB)ug/kg 683771 89 70-130ND
1,2-Dichlorobenzene ug/kg 661771 86 69-130ND
1,2-Dichloroethane ug/kg 761771 99 59-130ND
1,2-Dichloropropane ug/kg 702771 91 70-130ND
1,3,5-Trimethylbenzene ug/kg 711771 92 65-137ND
1,3-Dichlorobenzene ug/kg 674771 87 70-130ND
1,3-Dichloropropane ug/kg 686771 89 70-130ND
1,4-Dichlorobenzene ug/kg 622771 81 68-130ND
2,2-Dichloropropane ug/kg 663771 86 32-130ND
2-Butanone (MEK)ug/kg 11301550 69 10-136ND
2-Chlorotoluene ug/kg 694771 90 69-141ND
2-Hexanone ug/kg 12601550 81 10-144ND
4-Chlorotoluene ug/kg 671771 87 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 12601550 81 25-143ND
Acetone ug/kg 11101550 72 10-130ND
Benzene ug/kg 679771 88 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3710365MATRIX SPIKE SAMPLE:
MSSpike
Result
92615303001
Bromobenzene ug/kg 669771 87 70-130ND
Bromochloromethane ug/kg 672771 87 69-134ND
Bromodichloromethane ug/kg 663771 86 64-130ND
Bromoform ug/kg 558771 72 62-130ND
Bromomethane ug/kg 1020771 133 20-176ND
Carbon tetrachloride ug/kg 738771 96 65-140ND
Chlorobenzene ug/kg 682771 88 70-130ND
Chloroethane ug/kg 870 IH77111310-130ND
Chloroform ug/kg 648771 84 63-130ND
Chloromethane ug/kg 949 IH77112358-130ND
cis-1,2-Dichloroethene ug/kg 695771 90 66-130ND
cis-1,3-Dichloropropene ug/kg 649771 84 67-130ND
Dibromochloromethane ug/kg 606771 79 67-130ND
Dibromomethane ug/kg 641771 83 63-131ND
Dichlorodifluoromethane ug/kg 1310 IH77117044-180ND
Diisopropyl ether ug/kg 685771 89 63-130ND
Ethylbenzene ug/kg 659771 86 66-130ND
Hexachloro-1,3-butadiene ug/kg 518771 67 64-150ND
Isopropylbenzene (Cumene)ug/kg 703771 91 69-135ND
m&p-Xylene ug/kg 13901550 90 60-133ND
Methyl-tert-butyl ether ug/kg 693771 90 65-130ND
Methylene Chloride ug/kg 759771 98 61-130ND
n-Butylbenzene ug/kg 644771 84 65-140ND
n-Propylbenzene ug/kg 674771 87 67-140ND
Naphthalene ug/kg 308 v37714015-145ND
o-Xylene ug/kg 709771 92 66-133ND
p-Isopropyltoluene ug/kg 701771 91 56-147ND
sec-Butylbenzene ug/kg 713771 93 65-139ND
Styrene ug/kg 722771 90 70-1320.026 mg/kg
tert-Butylbenzene ug/kg 738771 96 62-135ND
Tetrachloroethene ug/kg 636771 82 70-135ND
Toluene ug/kg 675771 88 67-130ND
trans-1,2-Dichloroethene ug/kg 714771 93 69-130ND
trans-1,3-Dichloropropene ug/kg 660771 86 62-130ND
Trichloroethene ug/kg 722771 94 70-135ND
Trichlorofluoromethane ug/kg 873771 113 10-130ND
Vinyl acetate ug/kg 13201550 86 53-130ND
Vinyl chloride ug/kg 862 IH77111261-148ND
Xylene (Total)ug/kg 21002320 91 63-132ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615302009
3710366SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND v230ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND v230ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 101J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND IH30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND IH30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615302009
3710366SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND v230ND
o-Xylene ug/kg 5.7J 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND IH30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%107106
4-Bromofluorobenzene (S)%101100
Toluene-d8 (S)%101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
711569
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007, 92615483008,
92615483009, 92615483010, 92615483011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3710604
Associated Lab Samples:92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007, 92615483008,
92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/20/22 00:321.9
1,1,1-Trichloroethane ug/kg ND 5.0 07/20/22 00:322.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/20/22 00:321.3
1,1,2-Trichloroethane ug/kg ND 5.0 07/20/22 00:321.7
1,1-Dichloroethane ug/kg ND 5.0 07/20/22 00:322.1
1,1-Dichloroethene ug/kg ND 5.0 07/20/22 00:322.1
1,1-Dichloropropene ug/kg ND 5.0 07/20/22 00:322.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 v207/20/22 00:324.0
1,2,3-Trichloropropane ug/kg ND 5.0 07/20/22 00:322.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/20/22 00:324.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/20/22 00:321.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 v207/20/22 00:321.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/20/22 00:322.2
1,2-Dichlorobenzene ug/kg ND 5.0 07/20/22 00:321.8
1,2-Dichloroethane ug/kg ND 5.0 07/20/22 00:323.3
1,2-Dichloropropane ug/kg ND 5.0 07/20/22 00:321.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/20/22 00:321.7
1,3-Dichlorobenzene ug/kg ND 5.0 07/20/22 00:321.6
1,3-Dichloropropane ug/kg ND 5.0 07/20/22 00:321.6
1,4-Dichlorobenzene ug/kg ND 5.0 07/20/22 00:321.3
2,2-Dichloropropane ug/kg ND 5.0 07/20/22 00:321.6
2-Butanone (MEK)ug/kg ND 100 07/20/22 00:3224.0
2-Chlorotoluene ug/kg ND 5.0 07/20/22 00:321.8
2-Hexanone ug/kg ND 50.0 07/20/22 00:324.8
4-Chlorotoluene ug/kg ND 5.0 07/20/22 00:320.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/20/22 00:324.8
Acetone ug/kg ND 100 07/20/22 00:3232.1
Benzene ug/kg ND 5.0 07/20/22 00:322.0
Bromobenzene ug/kg ND 5.0 07/20/22 00:321.6
Bromochloromethane ug/kg ND 5.0 07/20/22 00:321.5
Bromodichloromethane ug/kg ND 5.0 07/20/22 00:321.9
Bromoform ug/kg ND 5.0 07/20/22 00:321.8
Bromomethane ug/kg ND 10.0 07/20/22 00:327.9
Carbon tetrachloride ug/kg ND 5.0 07/20/22 00:321.9
Chlorobenzene ug/kg ND 5.0 07/20/22 00:320.96
Chloroethane ug/kg ND 10.0 IH07/20/22 00:323.9
Chloroform ug/kg 4.2J 5.0 07/20/22 00:323.0
Chloromethane ug/kg ND 10.0 IH07/20/22 00:324.2
cis-1,2-Dichloroethene ug/kg ND 5.0 07/20/22 00:321.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3710604
Associated Lab Samples:92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007, 92615483008,
92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
cis-1,3-Dichloropropene ug/kg ND 5.0 07/20/22 00:321.4
Dibromochloromethane ug/kg ND 5.0 07/20/22 00:322.8
Dibromomethane ug/kg ND 5.0 07/20/22 00:321.1
Dichlorodifluoromethane ug/kg ND 10.0 IH07/20/22 00:322.2
Diisopropyl ether ug/kg ND 5.0 07/20/22 00:321.4
Ethylbenzene ug/kg ND 5.0 07/20/22 00:322.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/20/22 00:328.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/20/22 00:321.7
m&p-Xylene ug/kg ND 10.0 07/20/22 00:323.4
Methyl-tert-butyl ether ug/kg ND 5.0 07/20/22 00:321.9
Methylene Chloride ug/kg ND 20.0 07/20/22 00:3213.7
n-Butylbenzene ug/kg ND 5.0 07/20/22 00:322.4
n-Propylbenzene ug/kg ND 5.0 07/20/22 00:321.8
Naphthalene ug/kg ND 5.0 v207/20/22 00:322.6
o-Xylene ug/kg ND 5.0 07/20/22 00:322.2
p-Isopropyltoluene ug/kg ND 5.0 07/20/22 00:322.5
sec-Butylbenzene ug/kg ND 5.0 07/20/22 00:322.2
Styrene ug/kg ND 5.0 07/20/22 00:321.3
tert-Butylbenzene ug/kg ND 5.0 07/20/22 00:321.8
Tetrachloroethene ug/kg ND 5.0 07/20/22 00:321.6
Toluene ug/kg ND 5.0 07/20/22 00:321.4
trans-1,2-Dichloroethene ug/kg ND 5.0 07/20/22 00:321.8
trans-1,3-Dichloropropene ug/kg ND 5.0 07/20/22 00:321.7
Trichloroethene ug/kg ND 5.0 07/20/22 00:321.3
Trichlorofluoromethane ug/kg ND 5.0 07/20/22 00:322.8
Vinyl acetate ug/kg ND 50.0 07/20/22 00:323.6
Vinyl chloride ug/kg ND 10.0 IH07/20/22 00:322.5
Xylene (Total)ug/kg ND 10.0 07/20/22 00:322.8
1,2-Dichloroethane-d4 (S)%107 70-130 07/20/22 00:32
4-Bromofluorobenzene (S)%100 69-134 07/20/22 00:32
Toluene-d8 (S)%100 70-130 07/20/22 00:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3710605LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 14001250 112 70-130
1,1,1-Trichloroethane ug/kg 12801250 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 13401250 107 70-130
1,1,2-Trichloroethane ug/kg 13701250 110 70-130
1,1-Dichloroethane ug/kg 12301250 98 70-130
1,1-Dichloroethene ug/kg 13001250 104 70-130
1,1-Dichloropropene ug/kg 13001250 104 70-130
1,2,3-Trichlorobenzene ug/kg 939 v312507565-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3710605LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane ug/kg 12801250 102 70-130
1,2,4-Trichlorobenzene ug/kg 10801250 86 68-130
1,2,4-Trimethylbenzene ug/kg 13001250 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 967 v312507770-130
1,2-Dibromoethane (EDB)ug/kg 14101250 113 70-130
1,2-Dichlorobenzene ug/kg 12701250 101 70-130
1,2-Dichloroethane ug/kg 14201250 114 63-130
1,2-Dichloropropane ug/kg 13501250 108 70-130
1,3,5-Trimethylbenzene ug/kg 13301250 106 70-130
1,3-Dichlorobenzene ug/kg 13101250 105 70-130
1,3-Dichloropropane ug/kg 13701250 110 70-130
1,4-Dichlorobenzene ug/kg 12501250 100 70-130
2,2-Dichloropropane ug/kg 13401250 107 66-130
2-Butanone (MEK)ug/kg 23602500 94 70-130
2-Chlorotoluene ug/kg 13301250 107 70-130
2-Hexanone ug/kg 29702500 119 70-130
4-Chlorotoluene ug/kg 13201250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 27602500 111 70-130
Acetone ug/kg 23102500 92 69-130
Benzene ug/kg 12901250 103 70-130
Bromobenzene ug/kg 13701250 110 70-130
Bromochloromethane ug/kg 12701250 102 70-130
Bromodichloromethane ug/kg 14001250 112 69-130
Bromoform ug/kg 13701250 110 70-130
Bromomethane ug/kg 1700 L1125013652-130
Carbon tetrachloride ug/kg 14401250 116 70-130
Chlorobenzene ug/kg 13701250 109 70-130
Chloroethane ug/kg 1510 IH125012065-130
Chloroform ug/kg 11601250 93 70-130
Chloromethane ug/kg 1560 IH125012555-130
cis-1,2-Dichloroethene ug/kg 12701250 102 70-130
cis-1,3-Dichloropropene ug/kg 13801250 111 70-130
Dibromochloromethane ug/kg 13901250 111 70-130
Dibromomethane ug/kg 13901250 112 70-130
Dichlorodifluoromethane ug/kg 2100 IH,L1125016845-156
Diisopropyl ether ug/kg 12501250 100 70-130
Ethylbenzene ug/kg 12901250 103 70-130
Hexachloro-1,3-butadiene ug/kg 10601250 85 66-130
Isopropylbenzene (Cumene)ug/kg 13401250 107 70-130
m&p-Xylene ug/kg 27602500 110 70-130
Methyl-tert-butyl ether ug/kg 12801250 103 70-130
Methylene Chloride ug/kg 11901250 95 65-130
n-Butylbenzene ug/kg 12801250 102 67-130
n-Propylbenzene ug/kg 13001250 104 70-130
Naphthalene ug/kg 973 v312507870-130
o-Xylene ug/kg 14001250 112 70-130
p-Isopropyltoluene ug/kg 13401250 107 67-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3710605LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/kg 12801250 103 69-130
Styrene ug/kg 14601250 116 70-130
tert-Butylbenzene ug/kg 12801250 102 67-130
Tetrachloroethene ug/kg 13201250 105 70-130
Toluene ug/kg 13001250 104 70-130
trans-1,2-Dichloroethene ug/kg 12501250 100 70-130
trans-1,3-Dichloropropene ug/kg 14401250 116 68-130
Trichloroethene ug/kg 13801250 110 70-130
Trichlorofluoromethane ug/kg 13601250 109 70-130
Vinyl acetate ug/kg 27602500 110 70-130
Vinyl chloride ug/kg 1560 IH125012461-130
Xylene (Total)ug/kg 41603750 111 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%106 69-134
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3710606MATRIX SPIKE SAMPLE:
MSSpike
Result
92615483002
1,1,1,2-Tetrachloroethane ug/kg 624729 86 70-131ND
1,1,1-Trichloroethane ug/kg 665729 91 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 597729 82 66-130ND
1,1,2-Trichloroethane ug/kg 618729 85 66-133ND
1,1-Dichloroethane ug/kg 632729 87 65-130ND
1,1-Dichloroethene ug/kg 755729 104 10-158ND
1,1-Dichloropropene ug/kg 699729 96 68-133ND
1,2,3-Trichlorobenzene ug/kg 168 M1,v37292327-138ND
1,2,3-Trichloropropane ug/kg 575729 79 67-130ND
1,2,4-Trichlorobenzene ug/kg 344 M17294751-134ND
1,2,4-Trimethylbenzene ug/kg 631729 87 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 309 v37294232-130ND
1,2-Dibromoethane (EDB)ug/kg 657729 90 70-130ND
1,2-Dichlorobenzene ug/kg 617729 85 69-130ND
1,2-Dichloroethane ug/kg 704729 96 59-130ND
1,2-Dichloropropane ug/kg 653729 90 70-130ND
1,3,5-Trimethylbenzene ug/kg 667729 91 65-137ND
1,3-Dichlorobenzene ug/kg 622729 85 70-130ND
1,3-Dichloropropane ug/kg 660729 90 70-130ND
1,4-Dichlorobenzene ug/kg 583729 80 68-130ND
2,2-Dichloropropane ug/kg 633729 87 32-130ND
2-Butanone (MEK)ug/kg 11301460 74 10-13651.4J
2-Chlorotoluene ug/kg 642729 88 69-141ND
2-Hexanone ug/kg 12301460 84 10-144ND
4-Chlorotoluene ug/kg 637729 87 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 12501460 86 25-143ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3710606MATRIX SPIKE SAMPLE:
MSSpike
Result
92615483002
Acetone ug/kg 11101460 76 10-130ND
Benzene ug/kg 648729 89 67-130ND
Bromobenzene ug/kg 639729 88 70-130ND
Bromochloromethane ug/kg 637729 87 69-134ND
Bromodichloromethane ug/kg 612729 84 64-130ND
Bromoform ug/kg 540729 74 62-130ND
Bromomethane ug/kg 1120729 153 20-176ND
Carbon tetrachloride ug/kg 683729 94 65-140ND
Chlorobenzene ug/kg 656729 90 70-130ND
Chloroethane ug/kg 826 IH72911310-130ND
Chloroform ug/kg 595729 82 63-130ND
Chloromethane ug/kg 889 IH72912258-130ND
cis-1,2-Dichloroethene ug/kg 657729 90 66-130ND
cis-1,3-Dichloropropene ug/kg 605729 83 67-130ND
Dibromochloromethane ug/kg 576729 79 67-130ND
Dibromomethane ug/kg 600729 82 63-131ND
Dichlorodifluoromethane ug/kg 1270 IH72917444-180ND
Diisopropyl ether ug/kg 624729 86 63-130ND
Ethylbenzene ug/kg 619729 85 66-130ND
Hexachloro-1,3-butadiene ug/kg 443 M17296164-150ND
Isopropylbenzene (Cumene)ug/kg 650729 89 69-135ND
m&p-Xylene ug/kg 13301460 91 60-133ND
Methyl-tert-butyl ether ug/kg 653729 90 65-130ND
Methylene Chloride ug/kg 672729 92 61-130ND
n-Butylbenzene ug/kg 623729 85 65-140ND
n-Propylbenzene ug/kg 633729 87 67-140ND
Naphthalene ug/kg 189 v37292615-145ND
o-Xylene ug/kg 668729 92 66-133ND
p-Isopropyltoluene ug/kg 665729 91 56-147ND
sec-Butylbenzene ug/kg 670729 92 65-139ND
Styrene ug/kg 653729 90 70-132ND
tert-Butylbenzene ug/kg 682729 94 62-135ND
Tetrachloroethene ug/kg 619729 85 70-135ND
Toluene ug/kg 642729 88 67-130ND
trans-1,2-Dichloroethene ug/kg 665729 91 69-130ND
trans-1,3-Dichloropropene ug/kg 618729 85 62-130ND
Trichloroethene ug/kg 686729 94 70-135ND
Trichlorofluoromethane ug/kg 826729 113 10-130ND
Vinyl acetate ug/kg 12601460 87 53-130ND
Vinyl chloride ug/kg 790 IH72910861-148ND
Xylene (Total)ug/kg 20002180 92 63-132ND
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615483003
3710607SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND v230ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND v230ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 3059.0J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND IH30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND IH30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615483003
3710607SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND v230ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND IH30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%104105
4-Bromofluorobenzene (S)%102101
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712293
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3714080
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 328 07/22/22 14:36129
1,2-Dichlorobenzene ug/kg ND 328 07/22/22 14:36118
1,3-Dichlorobenzene ug/kg ND 328 07/22/22 14:36116
1,4-Dichlorobenzene ug/kg ND 328 07/22/22 14:36125
1-Methylnaphthalene ug/kg ND 328 07/22/22 14:36115
2,2'-Oxybis(1-chloropropane)ug/kg ND 328 07/22/22 14:36156
2,4,5-Trichlorophenol ug/kg ND 328 07/22/22 14:36150
2,4,6-Trichlorophenol ug/kg ND 328 07/22/22 14:36135
2,4-Dichlorophenol ug/kg ND 328 07/22/22 14:36128
2,4-Dimethylphenol ug/kg ND 328 07/22/22 14:36136
2,4-Dinitrophenol ug/kg ND 1640 v207/22/22 14:361010
2,4-Dinitrotoluene ug/kg ND 328 07/22/22 14:36126
2,6-Dinitrotoluene ug/kg ND 328 07/22/22 14:36120
2-Chloronaphthalene ug/kg ND 328 07/22/22 14:36130
2-Chlorophenol ug/kg ND 328 07/22/22 14:36123
2-Methylnaphthalene ug/kg ND 328 07/22/22 14:36131
2-Methylphenol(o-Cresol)ug/kg ND 328 07/22/22 14:36134
2-Nitroaniline ug/kg ND 1640 07/22/22 14:36268
2-Nitrophenol ug/kg ND 328 07/22/22 14:36142
3&4-Methylphenol(m&p Cresol)ug/kg ND 328 07/22/22 14:36132
3,3'-Dichlorobenzidine ug/kg ND 656 07/22/22 14:36222
3-Nitroaniline ug/kg ND 1640 07/22/22 14:36257
4,6-Dinitro-2-methylphenol ug/kg ND 656 07/22/22 14:36306
4-Bromophenylphenyl ether ug/kg ND 328 07/22/22 14:36126
4-Chloro-3-methylphenol ug/kg ND 656 07/22/22 14:36230
4-Chloroaniline ug/kg ND 656 07/22/22 14:36257
4-Chlorophenylphenyl ether ug/kg ND 328 07/22/22 14:36122
4-Nitroaniline ug/kg ND 656 07/22/22 14:36249
4-Nitrophenol ug/kg ND 1640 07/22/22 14:36634
Acenaphthene ug/kg ND 328 07/22/22 14:36115
Acenaphthylene ug/kg ND 328 07/22/22 14:36115
Aniline ug/kg ND 328 07/22/22 14:36128
Anthracene ug/kg ND 328 07/22/22 14:36107
Benzo(a)anthracene ug/kg ND 328 07/22/22 14:36109
Benzo(a)pyrene ug/kg ND 328 07/22/22 14:36113
Benzo(b)fluoranthene ug/kg ND 328 07/22/22 14:36109
Benzo(g,h,i)perylene ug/kg ND 328 07/22/22 14:36127
Benzo(k)fluoranthene ug/kg ND 328 07/22/22 14:36115
Benzoic Acid ug/kg ND 1640 v207/22/22 14:36704
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3714080
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008, 92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
Benzyl alcohol ug/kg ND 656 07/22/22 14:36248
bis(2-Chloroethoxy)methane ug/kg ND 328 07/22/22 14:36136
bis(2-Chloroethyl) ether ug/kg ND 328 07/22/22 14:36123
bis(2-Ethylhexyl)phthalate ug/kg ND 328 07/22/22 14:36127
Butylbenzylphthalate ug/kg ND 328 07/22/22 14:36138
Chrysene ug/kg ND 328 07/22/22 14:36119
Di-n-butylphthalate ug/kg ND 328 07/22/22 14:36110
Di-n-octylphthalate ug/kg ND 328 07/22/22 14:36129
Dibenz(a,h)anthracene ug/kg ND 328 07/22/22 14:36126
Dibenzofuran ug/kg ND 328 07/22/22 14:36118
Diethylphthalate ug/kg ND 328 07/22/22 14:36120
Dimethylphthalate ug/kg ND 328 07/22/22 14:36119
Fluoranthene ug/kg ND 328 07/22/22 14:36112
Fluorene ug/kg ND 328 07/22/22 14:36115
Hexachloro-1,3-butadiene ug/kg ND 328 07/22/22 14:36142
Hexachlorobenzene ug/kg ND 328 07/22/22 14:36128
Hexachlorocyclopentadiene ug/kg ND 328 07/22/22 14:36188
Hexachloroethane ug/kg ND 328 07/22/22 14:36125
Indeno(1,2,3-cd)pyrene ug/kg ND 328 07/22/22 14:36129
Isophorone ug/kg ND 328 07/22/22 14:36146
N-Nitroso-di-n-propylamine ug/kg ND 328 07/22/22 14:36123
N-Nitrosodimethylamine ug/kg ND 328 07/22/22 14:36110
N-Nitrosodiphenylamine ug/kg ND 328 07/22/22 14:36116
Naphthalene ug/kg ND 328 07/22/22 14:36111
Nitrobenzene ug/kg ND 328 07/22/22 14:36152
Pentachlorophenol ug/kg ND 656 07/22/22 14:36321
Phenanthrene ug/kg ND 328 07/22/22 14:36107
Phenol ug/kg ND 328 07/22/22 14:36146
Pyrene ug/kg ND 328 07/22/22 14:36133
Pyridine ug/kg ND 328 07/22/22 14:36103
2,4,6-Tribromophenol (S)%78 18-130 07/22/22 14:36
2-Fluorobiphenyl (S)%74 19-130 07/22/22 14:36
2-Fluorophenol (S)%72 18-130 07/22/22 14:36
Nitrobenzene-d5 (S)%68 21-130 07/22/22 14:36
Phenol-d6 (S)%89 18-130 07/22/22 14:36
Terphenyl-d14 (S)%73 15-130 07/22/22 14:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3714081LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11101660 67 47-130
1,2-Dichlorobenzene ug/kg 11301660 68 49-130
1,3-Dichlorobenzene ug/kg 11001660 66 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3714081LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/kg 11001660 66 49-130
1-Methylnaphthalene ug/kg 12401660 75 54-130
2,2'-Oxybis(1-chloropropane)ug/kg 10501660 63 38-130
2,4,5-Trichlorophenol ug/kg 13201660 80 49-130
2,4,6-Trichlorophenol ug/kg 14201660 86 50-130
2,4-Dichlorophenol ug/kg 12601660 76 51-130
2,4-Dimethylphenol ug/kg 13601660 82 53-130
2,4-Dinitrophenol ug/kg 6930 v383108339-130
2,4-Dinitrotoluene ug/kg 14801660 89 53-130
2,6-Dinitrotoluene ug/kg 14501660 87 55-130
2-Chloronaphthalene ug/kg 12901660 78 48-130
2-Chlorophenol ug/kg 12401660 75 54-130
2-Methylnaphthalene ug/kg 12101660 73 57-130
2-Methylphenol(o-Cresol)ug/kg 12401660 74 50-130
2-Nitroaniline ug/kg 28003320 84 49-130
2-Nitrophenol ug/kg 12501660 75 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 12701660 77 50-130
3,3'-Dichlorobenzidine ug/kg 27303320 82 47-130
3-Nitroaniline ug/kg 28803320 87 45-130
4,6-Dinitro-2-methylphenol ug/kg 29703320 89 50-142
4-Bromophenylphenyl ether ug/kg 13801660 83 55-130
4-Chloro-3-methylphenol ug/kg 28803320 87 52-130
4-Chloroaniline ug/kg 25703320 77 49-130
4-Chlorophenylphenyl ether ug/kg 13301660 80 53-130
4-Nitroaniline ug/kg 29903320 90 51-130
4-Nitrophenol ug/kg 76408310 92 40-130
Acenaphthene ug/kg 13601660 82 56-130
Acenaphthylene ug/kg 14701660 88 58-130
Aniline ug/kg 10301660 62 44-130
Anthracene ug/kg 13401660 80 60-130
Benzo(a)anthracene ug/kg 14601660 88 59-130
Benzo(a)pyrene ug/kg 17901660 108 57-130
Benzo(b)fluoranthene ug/kg 16901660 102 54-130
Benzo(g,h,i)perylene ug/kg 13701660 83 59-130
Benzo(k)fluoranthene ug/kg 16501660 100 54-130
Benzoic Acid ug/kg 5180 v383106219-130
Benzyl alcohol ug/kg 26003320 78 50-130
bis(2-Chloroethoxy)methane ug/kg 12201660 73 55-130
bis(2-Chloroethyl) ether ug/kg 11501660 69 53-130
bis(2-Ethylhexyl)phthalate ug/kg 15901660 96 58-130
Butylbenzylphthalate ug/kg 15301660 92 46-138
Chrysene ug/kg 14201660 85 57-130
Di-n-butylphthalate ug/kg 15401660 93 57-130
Di-n-octylphthalate ug/kg 16801660 101 57-130
Dibenz(a,h)anthracene ug/kg 14301660 86 60-130
Dibenzofuran ug/kg 13901660 84 54-130
Diethylphthalate ug/kg 14001660 84 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3714081LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethylphthalate ug/kg 13701660 82 57-130
Fluoranthene ug/kg 15001660 90 57-130
Fluorene ug/kg 14001660 84 56-130
Hexachloro-1,3-butadiene ug/kg 9741660 59 41-130
Hexachlorobenzene ug/kg 12801660 77 53-130
Hexachlorocyclopentadiene ug/kg 9511660 57 23-130
Hexachloroethane ug/kg 10601660 64 48-130
Indeno(1,2,3-cd)pyrene ug/kg 14001660 84 61-130
Isophorone ug/kg 12201660 74 49-130
N-Nitroso-di-n-propylamine ug/kg 12701660 76 52-130
N-Nitrosodimethylamine ug/kg 11601660 70 45-130
N-Nitrosodiphenylamine ug/kg 13901660 84 56-130
Naphthalene ug/kg 11601660 70 56-130
Nitrobenzene ug/kg 11501660 70 50-130
Pentachlorophenol ug/kg 30803320 93 33-130
Phenanthrene ug/kg 14401660 86 60-130
Phenol ug/kg 13801660 83 54-130
Pyrene ug/kg 14301660 86 61-130
Pyridine ug/kg 10101660 61 35-130
2,4,6-Tribromophenol (S)%80 18-130
2-Fluorobiphenyl (S)%69 19-130
2-Fluorophenol (S)%70 18-130
Nitrobenzene-d5 (S)%66 21-130
Phenol-d6 (S)%75 18-130
Terphenyl-d14 (S)%81 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3714082MATRIX SPIKE SAMPLE:
MSSpike
Result
92615319001
1,2,4-Trichlorobenzene ug/kg 15902040 78 22-130ND
1,2-Dichlorobenzene ug/kg 16502040 81 23-130ND
1,3-Dichlorobenzene ug/kg 16202040 79 26-130ND
1,4-Dichlorobenzene ug/kg 15802040 77 27-130ND
1-Methylnaphthalene ug/kg 16402040 80 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 15502040 76 30-130ND
2,4,5-Trichlorophenol ug/kg 18402040 90 26-130ND
2,4,6-Trichlorophenol ug/kg 19302040 94 23-130ND
2,4-Dichlorophenol ug/kg 16502040 81 29-130ND
2,4-Dimethylphenol ug/kg 17502040 86 13-130ND
2,4-Dinitrophenol ug/kg 9210 v3102009010-131ND
2,4-Dinitrotoluene ug/kg 18202040 89 28-130ND
2,6-Dinitrotoluene ug/kg 18602040 91 36-130ND
2-Chloronaphthalene ug/kg 17102040 83 27-130ND
2-Chlorophenol ug/kg 17802040 87 29-130ND
2-Methylnaphthalene ug/kg 15702040 77 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3714082MATRIX SPIKE SAMPLE:
MSSpike
Result
92615319001
2-Methylphenol(o-Cresol)ug/kg 16802040 82 20-130ND
2-Nitroaniline ug/kg 32704090 80 29-130ND
2-Nitrophenol ug/kg 18302040 90 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 16002040 78 10-176ND
3,3'-Dichlorobenzidine ug/kg 34404090 84 15-130ND
3-Nitroaniline ug/kg 34104090 83 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 41504090 101 15-132ND
4-Bromophenylphenyl ether ug/kg 19102040 93 35-130ND
4-Chloro-3-methylphenol ug/kg 34604090 85 30-130ND
4-Chloroaniline ug/kg 32204090 79 28-130ND
4-Chlorophenylphenyl ether ug/kg 17602040 86 32-130ND
4-Nitroaniline ug/kg 37204090 91 30-130ND
4-Nitrophenol ug/kg 836010200 82 17-130ND
Acenaphthene ug/kg 16802040 82 29-130ND
Acenaphthylene ug/kg 18502040 91 31-130ND
Aniline ug/kg 12202040 59 10-130ND
Anthracene ug/kg 16302040 80 33-130ND
Benzo(a)anthracene ug/kg 18302040 89 32-130ND
Benzo(a)pyrene ug/kg 22102040 108 32-130ND
Benzo(b)fluoranthene ug/kg 21602040 106 33-130ND
Benzo(g,h,i)perylene ug/kg 18402040 90 28-130ND
Benzo(k)fluoranthene ug/kg 20702040 101 31-130ND
Benzoic Acid ug/kg 5710 v3102005610-130ND
Benzyl alcohol ug/kg 34404090 84 31-130ND
bis(2-Chloroethoxy)methane ug/kg 17002040 83 30-130ND
bis(2-Chloroethyl) ether ug/kg 16502040 81 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 20902040 102 40-130ND
Butylbenzylphthalate ug/kg 22802040 112 40-130ND
Chrysene ug/kg 17702040 87 30-130ND
Di-n-butylphthalate ug/kg 18702040 91 41-130ND
Di-n-octylphthalate ug/kg 22102040 108 42-130ND
Dibenz(a,h)anthracene ug/kg 17902040 88 27-130ND
Dibenzofuran ug/kg 17402040 85 32-130ND
Diethylphthalate ug/kg 18502040 90 40-130ND
Dimethylphthalate ug/kg 17202040 84 37-130ND
Fluoranthene ug/kg 17602040 86 26-130ND
Fluorene ug/kg 18402040 90 31-130ND
Hexachloro-1,3-butadiene ug/kg 14202040 70 20-130ND
Hexachlorobenzene ug/kg 17802040 87 29-130ND
Hexachlorocyclopentadiene ug/kg 15302040 75 10-130ND
Hexachloroethane ug/kg 15902040 78 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 17702040 87 28-130ND
Isophorone ug/kg 16102040 78 32-130ND
N-Nitroso-di-n-propylamine ug/kg 16102040 78 31-130ND
N-Nitrosodimethylamine ug/kg 16302040 80 20-130ND
N-Nitrosodiphenylamine ug/kg 19002040 93 32-130ND
Naphthalene ug/kg 16002040 78 30-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
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Huntersville, NC 28078
[phone]
Page 82 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3714082MATRIX SPIKE SAMPLE:
MSSpike
Result
92615319001
Nitrobenzene ug/kg 16502040 81 25-130ND
Pentachlorophenol ug/kg 40304090 99 10-130ND
Phenanthrene ug/kg 17402040 85 34-130ND
Phenol ug/kg 18002040 88 14-130ND
Pyrene ug/kg 18802040 92 31-130ND
Pyridine ug/kg 7882040 39 10-130ND
2,4,6-Tribromophenol (S)%88 18-130
2-Fluorobiphenyl (S)%69 19-130
2-Fluorophenol (S)%80 18-130
Nitrobenzene-d5 (S)%76 21-130
Phenol-d6 (S)%80 18-130
Terphenyl-d14 (S)%84 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615385001
3714083SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND v230ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND v230ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND v130ND
4-Nitrophenol ug/kg ND v130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
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[phone]
Page 83 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615385001
3714083SAMPLE DUPLICATE:
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND v230ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND v130ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND v130ND
2,4,6-Tribromophenol (S)%8277
2-Fluorobiphenyl (S)%5855
2-Fluorophenol (S)%7072
Nitrobenzene-d5 (S)%7877
Phenol-d6 (S)%8077
Terphenyl-d14 (S)%6055
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 84 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
711584
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615302012
3710737SAMPLE DUPLICATE:
Percent Moisture %12.8 N2122514.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615332011
3710738SAMPLE DUPLICATE:
Percent Moisture %15.1 N2182512.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
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9800 Kincey Ave. Suite 100
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Page 85 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
711866
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92615483008, 92615483009, 92615483010, 92615483011
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615248001
3712182SAMPLE DUPLICATE:
Percent Moisture %14.5 N202514.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615657004
3712183SAMPLE DUPLICATE:
Percent Moisture %10.9 N222511.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1899429
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3818412-1
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004
Matrix:Solid
AnalyzedMDL
Total Solids %ND 07/22/22 19:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3818412-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615483002
R3818412-3SAMPLE DUPLICATE:
Total Solids %82.2 0.235 1082.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1899431
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92615483005, 92615483006, 92615483007, 92615483008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3818731-1
Associated Lab Samples:92615483005, 92615483006, 92615483007, 92615483008
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 07/23/22 11:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3818731-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615483005
R3818731-3SAMPLE DUPLICATE:
Total Solids %70.5 2.57 1072.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1899491
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92615483009, 92615483010, 92615483011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3819208-1
Associated Lab Samples:92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 07/25/22 13:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3819208-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1517522-02
R3819208-3SAMPLE DUPLICATE:
Total Solids %81.5 5.18 1085.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1908869
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3826254-1
Associated Lab Samples:92615483001, 92615483002, 92615483003, 92615483004, 92615483005, 92615483006, 92615483007,
92615483008
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/12/22 13:070.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3826254-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 11.910.0 119 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3826254-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92615483004
R3826254-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 28.4 93.5 75.0-12594.3 0.825 2028.4ND 18.7 18.9
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3826254-7MATRIX SPIKE SAMPLE:
MSSpike
Result
92615483004
Chromium, Hexavalent mg/kg 792894 126 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615483002
R3826254-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1519058-06
R3826254-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92615483
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1911016
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92615483009, 92615483010, 92615483011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3828358-1
Associated Lab Samples:92615483009, 92615483010, 92615483011
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/18/22 11:260.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3828358-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.9010.0 99.0 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3828358-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1515856-03
R3828358-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 20.0 37.8 75.0-12521.1 56.6 2020.0ND 7.55 4.22
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3828358-8MATRIX SPIKE SAMPLE:
MSSpike
Result
L1515856-03
Chromium, Hexavalent mg/kg 349631 55.3 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1519092-01
R3828358-9SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.706J 1.02 200.713
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1519092-03
R3828358-10SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.530J 1.07 200.524
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 91 of 98
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92615483
Mock Judson 1533
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: L1515856-03
Wet Chemistry by Method 7199 - Sample is a reducer.[1]
ANALYTE QUALIFIERS
Analyte is a possible laboratory contaminant (not present in method blank).C7
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 98
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92615483
Mock Judson 1533
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
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[phone]
Page 93 of 98
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92615483
Mock Judson 1533
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92615483001 711699 711783SS-1 EPA 3050B EPA 6010D
92615483002 711699 711783SS-2 EPA 3050B EPA 6010D
92615483003 711699 711783SS-3 EPA 3050B EPA 6010D
92615483004 711699 711783SS-4 EPA 3050B EPA 6010D
92615483005 711699 711783SS-5 EPA 3050B EPA 6010D
92615483006 711699 711783SS-6 EPA 3050B EPA 6010D
92615483007 711699 711783SS-7 EPA 3050B EPA 6010D
92615483008 711699 711783SS-8 EPA 3050B EPA 6010D
92615483009 711699 711783SS-9 EPA 3050B EPA 6010D
92615483010 711699 711783SS-10 EPA 3050B EPA 6010D
92615483011 711699 711783SS-11 EPA 3050B EPA 6010D
92615483001 712335 712581SS-1 EPA 7471B EPA 7471B
92615483002 712335 712581SS-2 EPA 7471B EPA 7471B
92615483003 712335 712581SS-3 EPA 7471B EPA 7471B
92615483004 712335 712581SS-4 EPA 7471B EPA 7471B
92615483005 712335 712581SS-5 EPA 7471B EPA 7471B
92615483006 712335 712581SS-6 EPA 7471B EPA 7471B
92615483007 712335 712581SS-7 EPA 7471B EPA 7471B
92615483008 712335 712581SS-8 EPA 7471B EPA 7471B
92615483009 712335 712581SS-9 EPA 7471B EPA 7471B
92615483010 712335 712581SS-10 EPA 7471B EPA 7471B
92615483011 712335 712581SS-11 EPA 7471B EPA 7471B
92615483001 712293 712409SS-1 EPA 3546 EPA 8270E
92615483002 712293 712409SS-2 EPA 3546 EPA 8270E
92615483003 712293 712409SS-3 EPA 3546 EPA 8270E
92615483004 712293 712409SS-4 EPA 3546 EPA 8270E
92615483005 712293 712409SS-5 EPA 3546 EPA 8270E
92615483006 712293 712409SS-6 EPA 3546 EPA 8270E
92615483007 712293 712409SS-7 EPA 3546 EPA 8270E
92615483008 712293 712409SS-8 EPA 3546 EPA 8270E
92615483009 712293 712409SS-9 EPA 3546 EPA 8270E
92615483010 712293 712409SS-10 EPA 3546 EPA 8270E
92615483011 712293 712409SS-11 EPA 3546 EPA 8270E
92615483001 711539 711694SS-1 EPA 5035A/5030B EPA 8260D
92615483002 711569 711692SS-2 EPA 5035A/5030B EPA 8260D
92615483003 711569 711692SS-3 EPA 5035A/5030B EPA 8260D
92615483004 711569 711692SS-4 EPA 5035A/5030B EPA 8260D
92615483005 711569 711692SS-5 EPA 5035A/5030B EPA 8260D
92615483006 711569 711692SS-6 EPA 5035A/5030B EPA 8260D
92615483007 711569 711692SS-7 EPA 5035A/5030B EPA 8260D
92615483008 711569 711692SS-8 EPA 5035A/5030B EPA 8260D
92615483009 711569 711692SS-9 EPA 5035A/5030B EPA 8260D
92615483010 711569 711692SS-10 EPA 5035A/5030B EPA 8260D
92615483011 711569 711692SS-11 EPA 5035A/5030B EPA 8260D
92615483001 711584SS-1 SW-846
92615483002 711584SS-2 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
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Page 94 of 98
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92615483
Mock Judson 1533
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92615483003 711584SS-3 SW-846
92615483004 711584SS-4 SW-846
92615483005 711584SS-5 SW-846
92615483006 711584SS-6 SW-846
92615483007 711584SS-7 SW-846
92615483008 711866SS-8 SW-846
92615483009 711866SS-9 SW-846
92615483010 711866SS-10 SW-846
92615483011 711866SS-11 SW-846
92615483001 1899429 1899429SS-1 SM 2540 G SM 2540G
92615483002 1899429 1899429SS-2 SM 2540 G SM 2540G
92615483003 1899429 1899429SS-3 SM 2540 G SM 2540G
92615483004 1899429 1899429SS-4 SM 2540 G SM 2540G
92615483005 1899431 1899431SS-5 SM 2540 G SM 2540G
92615483006 1899431 1899431SS-6 SM 2540 G SM 2540G
92615483007 1899431 1899431SS-7 SM 2540 G SM 2540G
92615483008 1899431 1899431SS-8 SM 2540 G SM 2540G
92615483009 1899491 1899491SS-9 SM 2540 G SM 2540G
92615483010 1899491 1899491SS-10 SM 2540 G SM 2540G
92615483011 1899491 1899491SS-11 SM 2540 G SM 2540G
92615483001 1908869 1908869SS-1 3060A EPA 7199
92615483002 1908869 1908869SS-2 3060A EPA 7199
92615483003 1908869 1908869SS-3 3060A EPA 7199
92615483004 1908869 1908869SS-4 3060A EPA 7199
92615483005 1908869 1908869SS-5 3060A EPA 7199
92615483006 1908869 1908869SS-6 3060A EPA 7199
92615483007 1908869 1908869SS-7 3060A EPA 7199
92615483008 1908869 1908869SS-8 3060A EPA 7199
92615483009 1911016 1911016SS-9 3060A EPA 7199
92615483010 1911016 1911016SS-10 3060A EPA 7199
92615483011 1911016 1911016SS-11 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2022 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 98
#=CL#
September 07, 2022
LIMS USE: FR - CHERYL MOODY
LIMS OBJECT ID: 92616845
92616845
Project:
Pace Project No.:
RE:
Cheryl Moody
Atlantic Shore Environmental
175-1 Venture Drive
Belville, NC 28451
Mock Judson 1533
Dear Cheryl Moody:
Enclosed are the analytical results for sample(s) received by the laboratory on July 26, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
A revised laboratory report is being submitted on 9/7/22 to include results from an interregional laboratory that did not
initially merge.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Daniel J. Schiwinger, Atlantic Shores Environmental
Services, Ltd.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 91
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 91
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92616845
Mock Judson 1533
Lab ID Sample ID Matrix Date Collected Date Received
92616845001 MW-6 Water 07/22/22 12:10 07/26/22 09:40
92616845002 MW-7 Water 07/22/22 13:10 07/26/22 09:40
92616845003 MW-8 Water 07/22/22 14:20 07/26/22 09:40
92616845004 MW-2 Water 07/22/22 16:10 07/26/22 09:40
92616845005 MW-3 Water 07/22/22 16:55 07/26/22 09:40
92616845006 SS-12 Solid 07/22/22 12:15 07/26/22 09:40
92616845007 SS-13 Solid 07/22/22 13:10 07/26/22 09:40
92616845008 SS-14 Solid 07/22/22 13:30 07/26/22 09:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 91
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92616845
Mock Judson 1533
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92616845001 MW-6 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92616845002 MW-7 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92616845003 MW-8 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92616845006 SS-12 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92616845007 SS-13 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92616845008 SS-14 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-6 Lab ID:92616845001 Collected:07/22/22 12:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/30/22 12:40 83-32-907/29/22 11:359.1 1.8 1
Acenaphthylene ND ug/L 07/30/22 12:40 208-96-807/29/22 11:359.1 1.8 1
Aniline ND ug/L 07/30/22 12:40 62-53-307/29/22 11:359.1 1.5 1
Anthracene ND ug/L 07/30/22 12:40 120-12-707/29/22 11:359.1 2.1 1
Benzo(a)anthracene ND ug/L 07/30/22 12:40 56-55-307/29/22 11:359.1 2.4 1
Benzo(a)pyrene ND ug/L 07/30/22 12:40 50-32-807/29/22 11:359.1 2.5 1
Benzo(b)fluoranthene ND ug/L 07/30/22 12:40 205-99-2 L107/29/22 11:359.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 07/30/22 12:40 191-24-207/29/22 11:359.1 2.6 1
Benzo(k)fluoranthene ND ug/L 07/30/22 12:40 207-08-9 L107/29/22 11:359.1 2.5 1
Benzoic Acid ND ug/L 07/30/22 12:40 65-85-007/29/22 11:3545.5 20.0 1
Benzyl alcohol ND ug/L 07/30/22 12:40 100-51-607/29/22 11:3518.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 07/30/22 12:40 101-55-307/29/22 11:359.1 1.6 1
Butylbenzylphthalate ND ug/L 07/30/22 12:40 85-68-707/29/22 11:359.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 07/30/22 12:40 59-50-707/29/22 11:359.1 3.0 1
4-Chloroaniline ND ug/L 07/30/22 12:40 106-47-807/29/22 11:3518.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 07/30/22 12:40 111-91-107/29/22 11:359.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/30/22 12:40 111-44-407/29/22 11:359.1 1.7 1
2-Chloronaphthalene ND ug/L 07/30/22 12:40 91-58-707/29/22 11:359.1 1.6 1
2-Chlorophenol ND ug/L 07/30/22 12:40 95-57-807/29/22 11:359.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 07/30/22 12:40 7005-72-307/29/22 11:359.1 1.8 1
Chrysene ND ug/L 07/30/22 12:40 218-01-907/29/22 11:359.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 07/30/22 12:40 53-70-307/29/22 11:359.1 2.7 1
Dibenzofuran ND ug/L 07/30/22 12:40 132-64-907/29/22 11:359.1 1.9 1
1,2-Dichlorobenzene ND ug/L 07/30/22 12:40 95-50-107/29/22 11:359.1 1.6 1
1,3-Dichlorobenzene ND ug/L 07/30/22 12:40 541-73-107/29/22 11:359.1 1.5 1
1,4-Dichlorobenzene ND ug/L 07/30/22 12:40 106-46-707/29/22 11:359.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 07/30/22 12:40 91-94-107/29/22 11:3518.2 7.4 1
2,4-Dichlorophenol ND ug/L 07/30/22 12:40 120-83-207/29/22 11:359.1 1.3 1
Diethylphthalate ND ug/L 07/30/22 12:40 84-66-207/29/22 11:359.1 1.9 1
2,4-Dimethylphenol ND ug/L 07/30/22 12:40 105-67-907/29/22 11:359.1 1.5 1
Dimethylphthalate ND ug/L 07/30/22 12:40 131-11-307/29/22 11:359.1 1.9 1
Di-n-butylphthalate ND ug/L 07/30/22 12:40 84-74-207/29/22 11:359.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/30/22 12:40 534-52-107/29/22 11:3518.2 7.1 1
2,4-Dinitrophenol ND ug/L 07/30/22 12:40 51-28-507/29/22 11:3545.5 23.6 1
2,4-Dinitrotoluene ND ug/L 07/30/22 12:40 121-14-207/29/22 11:359.1 1.5 1
2,6-Dinitrotoluene ND ug/L 07/30/22 12:40 606-20-207/29/22 11:359.1 1.6 1
Di-n-octylphthalate ND ug/L 07/30/22 12:40 117-84-007/29/22 11:359.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/30/22 12:40 117-81-707/29/22 11:355.5 3.4 1
Fluoranthene ND ug/L 07/30/22 12:40 206-44-007/29/22 11:359.1 2.0 1
Fluorene ND ug/L 07/30/22 12:40 86-73-707/29/22 11:359.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 07/30/22 12:40 87-68-307/29/22 11:359.1 1.6 1
Hexachlorobenzene ND ug/L 07/30/22 12:40 118-74-107/29/22 11:359.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 07/30/22 12:40 77-47-407/29/22 11:359.1 1.4 1
Hexachloroethane ND ug/L 07/30/22 12:40 67-72-107/29/22 11:359.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/30/22 12:40 193-39-507/29/22 11:359.1 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-6 Lab ID:92616845001 Collected:07/22/22 12:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 07/30/22 12:40 78-59-107/29/22 11:359.1 1.5 1
1-Methylnaphthalene ND ug/L 07/30/22 12:40 90-12-007/29/22 11:359.1 1.8 1
2-Methylnaphthalene ND ug/L 07/30/22 12:40 91-57-607/29/22 11:359.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 07/30/22 12:40 95-48-707/29/22 11:359.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/30/22 12:40 15831-10-407/29/22 11:359.1 1.1 1
Naphthalene ND ug/L 07/30/22 12:40 91-20-307/29/22 11:359.1 1.9 1
2-Nitroaniline ND ug/L 07/30/22 12:40 88-74-407/29/22 11:3518.2 2.7 1
3-Nitroaniline ND ug/L 07/30/22 12:40 99-09-207/29/22 11:3518.2 3.4 1
4-Nitroaniline ND ug/L 07/30/22 12:40 100-01-6 v207/29/22 11:3518.2 4.6 1
Nitrobenzene ND ug/L 07/30/22 12:40 98-95-307/29/22 11:359.1 1.7 1
2-Nitrophenol ND ug/L 07/30/22 12:40 88-75-507/29/22 11:359.1 1.3 1
4-Nitrophenol ND ug/L 07/30/22 12:40 100-02-707/29/22 11:3545.5 6.0 1
N-Nitrosodimethylamine ND ug/L 07/30/22 12:40 62-75-907/29/22 11:359.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 07/30/22 12:40 621-64-707/29/22 11:359.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 07/30/22 12:40 86-30-607/29/22 11:359.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/30/22 12:40 108-60-107/29/22 11:359.1 1.0 1
Pentachlorophenol ND ug/L 07/30/22 12:40 87-86-507/29/22 11:3518.2 3.4 1
Phenanthrene ND ug/L 07/30/22 12:40 85-01-807/29/22 11:359.1 1.8 1
Phenol 20.5 ug/L 07/30/22 12:40 108-95-2 B,C907/29/22 11:359.1 1.2 1
Phenol ND ug/L 08/02/22 00:00 108-95-2 H208/01/22 11:1810.0 1.4 1
Pyrene ND ug/L 07/30/22 12:40 129-00-007/29/22 11:359.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 07/30/22 12:40 120-82-107/29/22 11:359.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/30/22 12:40 95-95-407/29/22 11:359.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 07/30/22 12:40 88-06-207/29/22 11:359.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)71 %07/30/22 12:40 4165-60-007/29/22 11:3510-144 1
2-Fluorobiphenyl (S)65 %07/30/22 12:40 321-60-807/29/22 11:3510-130 1
Terphenyl-d14 (S)133 %07/30/22 12:40 1718-51-007/29/22 11:3534-163 1
Phenol-d6 (S)19 %08/02/22 00:00 13127-88-308/01/22 11:1810-130 1
Phenol-d6 (S)40 %07/30/22 12:40 13127-88-307/29/22 11:3510-130 1
2-Fluorophenol (S)7 %08/02/22 00:00 367-12-4 S008/01/22 11:1810-130 1
2-Fluorophenol (S)52 %07/30/22 12:40 367-12-407/29/22 11:3510-130 1
2,4,6-Tribromophenol (S)24 %08/02/22 00:00 118-79-608/01/22 11:1810-144 1
2,4,6-Tribromophenol (S)93 %07/30/22 12:40 118-79-607/29/22 11:3510-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/28/22 14:41 67-64-125.0 5.1 1
Benzene ND ug/L 07/28/22 14:41 71-43-21.0 0.34 1
Bromobenzene ND ug/L 07/28/22 14:41 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 07/28/22 14:41 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 07/28/22 14:41 75-27-41.0 0.31 1
Bromoform ND ug/L 07/28/22 14:41 75-25-21.0 0.34 1
Bromomethane ND ug/L 07/28/22 14:41 74-83-9 v32.0 1.7 1
2-Butanone (MEK)ND ug/L 07/28/22 14:41 78-93-35.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-6 Lab ID:92616845001 Collected:07/22/22 12:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Carbon tetrachloride ND ug/L 07/28/22 14:41 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 07/28/22 14:41 108-90-71.0 0.28 1
Chloroethane ND ug/L 07/28/22 14:41 75-00-31.0 0.65 1
Chloroform ND ug/L 07/28/22 14:41 67-66-31.0 0.43 1
Chloromethane ND ug/L 07/28/22 14:41 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 07/28/22 14:41 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 07/28/22 14:41 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/22 14:41 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 07/28/22 14:41 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/22 14:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/22 14:41 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 07/28/22 14:41 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 07/28/22 14:41 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 07/28/22 14:41 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 07/28/22 14:41 75-71-8 M11.0 0.35 1
1,1-Dichloroethane ND ug/L 07/28/22 14:41 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 07/28/22 14:41 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 07/28/22 14:41 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/28/22 14:41 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/28/22 14:41 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 07/28/22 14:41 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 07/28/22 14:41 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/28/22 14:41 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 07/28/22 14:41 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 07/28/22 14:41 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/28/22 14:41 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 07/28/22 14:41 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 07/28/22 14:41 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 07/28/22 14:41 87-68-32.0 1.5 1
2-Hexanone ND ug/L 07/28/22 14:41 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 07/28/22 14:41 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 07/28/22 14:41 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/22 14:41 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 07/28/22 14:41 1634-04-41.0 0.42 1
Naphthalene ND ug/L 07/28/22 14:41 91-20-31.0 0.64 1
Styrene ND ug/L 07/28/22 14:41 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/22 14:41 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/22 14:41 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 07/28/22 14:41 127-18-41.0 0.29 1
Toluene ND ug/L 07/28/22 14:41 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 07/28/22 14:41 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 07/28/22 14:41 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/28/22 14:41 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 07/28/22 14:41 79-00-51.0 0.32 1
Trichloroethene ND ug/L 07/28/22 14:41 79-01-61.0 0.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-6 Lab ID:92616845001 Collected:07/22/22 12:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Trichlorofluoromethane ND ug/L 07/28/22 14:41 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 07/28/22 14:41 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 07/28/22 14:41 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 07/28/22 14:41 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 07/28/22 14:41 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 07/28/22 14:41 179601-23-12.0 0.71 1
o-Xylene ND ug/L 07/28/22 14:41 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/22 14:41 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/22 14:41 17060-07-070-130 1
Toluene-d8 (S)98 %07/28/22 14:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-7 Lab ID:92616845002 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/30/22 13:05 83-32-907/29/22 11:3510020.1 1
Acenaphthylene ND ug/L 07/30/22 13:05 208-96-807/29/22 11:3510019.5 1
Aniline ND ug/L 07/30/22 13:05 62-53-307/29/22 11:3510016.4 1
Anthracene ND ug/L 07/30/22 13:05 120-12-707/29/22 11:3510023.1 1
Benzo(a)anthracene ND ug/L 07/30/22 13:05 56-55-307/29/22 11:3510026.9 1
Benzo(a)pyrene ND ug/L 07/30/22 13:05 50-32-807/29/22 11:3510027.8 1
Benzo(b)fluoranthene ND ug/L 07/30/22 13:05 205-99-2 L107/29/22 11:3510026.0 1
Benzo(g,h,i)perylene ND ug/L 07/30/22 13:05 191-24-207/29/22 11:3510028.4 1
Benzo(k)fluoranthene ND ug/L 07/30/22 13:05 207-08-9 L107/29/22 11:3510027.1 1
Benzoic Acid ND ug/L 07/30/22 13:05 65-85-007/29/22 11:355002201
Benzyl alcohol ND ug/L 07/30/22 13:05 100-51-607/29/22 11:3520029.0 1
4-Bromophenylphenyl ether ND ug/L 07/30/22 13:05 101-55-307/29/22 11:3510017.7 1
Butylbenzylphthalate ND ug/L 07/30/22 13:05 85-68-707/29/22 11:3510031.4 1
4-Chloro-3-methylphenol ND ug/L 07/30/22 13:05 59-50-707/29/22 11:3510033.4 1
4-Chloroaniline ND ug/L 07/30/22 13:05 106-47-807/29/22 11:3520036.3 1
bis(2-Chloroethoxy)methane ND ug/L 07/30/22 13:05 111-91-107/29/22 11:3510018.2 1
bis(2-Chloroethyl) ether ND ug/L 07/30/22 13:05 111-44-407/29/22 11:3510019.1 1
2-Chloronaphthalene ND ug/L 07/30/22 13:05 91-58-707/29/22 11:3510017.2 1
2-Chlorophenol ND ug/L 07/30/22 13:05 95-57-807/29/22 11:3510012.0 1
4-Chlorophenylphenyl ether ND ug/L 07/30/22 13:05 7005-72-307/29/22 11:3510020.0 1
Chrysene ND ug/L 07/30/22 13:05 218-01-907/29/22 11:3510027.7 1
Dibenz(a,h)anthracene ND ug/L 07/30/22 13:05 53-70-307/29/22 11:3510029.5 1
Dibenzofuran ND ug/L 07/30/22 13:05 132-64-907/29/22 11:3510021.0 1
1,2-Dichlorobenzene ND ug/L 07/30/22 13:05 95-50-107/29/22 11:3510018.0 1
1,3-Dichlorobenzene ND ug/L 07/30/22 13:05 541-73-107/29/22 11:3510016.0 1
1,4-Dichlorobenzene ND ug/L 07/30/22 13:05 106-46-707/29/22 11:3510016.7 1
3,3'-Dichlorobenzidine ND ug/L 07/30/22 13:05 91-94-107/29/22 11:3520081.2 1
2,4-Dichlorophenol ND ug/L 07/30/22 13:05 120-83-207/29/22 11:3510014.0 1
Diethylphthalate ND ug/L 07/30/22 13:05 84-66-207/29/22 11:3510020.5 1
2,4-Dimethylphenol ND ug/L 07/30/22 13:05 105-67-907/29/22 11:3510017.0 1
Dimethylphthalate ND ug/L 07/30/22 13:05 131-11-307/29/22 11:3510021.3 1
Di-n-butylphthalate ND ug/L 07/30/22 13:05 84-74-207/29/22 11:3510022.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/30/22 13:05 534-52-107/29/22 11:3520077.8 1
2,4-Dinitrophenol ND ug/L 07/30/22 13:05 51-28-507/29/22 11:355002601
2,4-Dinitrotoluene ND ug/L 07/30/22 13:05 121-14-207/29/22 11:3510016.2 1
2,6-Dinitrotoluene ND ug/L 07/30/22 13:05 606-20-207/29/22 11:3510017.2 1
Di-n-octylphthalate ND ug/L 07/30/22 13:05 117-84-007/29/22 11:3510039.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/30/22 13:05 117-81-707/29/22 11:3560.0 37.3 1
Fluoranthene ND ug/L 07/30/22 13:05 206-44-007/29/22 11:3510021.9 1
Fluorene ND ug/L 07/30/22 13:05 86-73-707/29/22 11:3510020.9 1
Hexachloro-1,3-butadiene ND ug/L 07/30/22 13:05 87-68-307/29/22 11:3510017.7 1
Hexachlorobenzene ND ug/L 07/30/22 13:05 118-74-107/29/22 11:3510021.6 1
Hexachlorocyclopentadiene ND ug/L 07/30/22 13:05 77-47-407/29/22 11:3510015.9 1
Hexachloroethane ND ug/L 07/30/22 13:05 67-72-107/29/22 11:3510013.8 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/30/22 13:05 193-39-507/29/22 11:3510028.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-7 Lab ID:92616845002 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 07/30/22 13:05 78-59-107/29/22 11:3510016.6 1
1-Methylnaphthalene ND ug/L 07/30/22 13:05 90-12-007/29/22 11:3510020.3 1
2-Methylnaphthalene ND ug/L 07/30/22 13:05 91-57-607/29/22 11:3510018.7 1
2-Methylphenol(o-Cresol)ND ug/L 07/30/22 13:05 95-48-707/29/22 11:3510018.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/30/22 13:05 15831-10-407/29/22 11:3510012.2 1
Naphthalene ND ug/L 07/30/22 13:05 91-20-307/29/22 11:3510020.9 1
2-Nitroaniline ND ug/L 07/30/22 13:05 88-74-407/29/22 11:3520029.8 1
3-Nitroaniline ND ug/L 07/30/22 13:05 99-09-207/29/22 11:3520037.5 1
4-Nitroaniline ND ug/L 07/30/22 13:05 100-01-6 v207/29/22 11:3520051.0 1
Nitrobenzene ND ug/L 07/30/22 13:05 98-95-307/29/22 11:3510018.7 1
2-Nitrophenol ND ug/L 07/30/22 13:05 88-75-507/29/22 11:3510014.0 1
4-Nitrophenol ND ug/L 07/30/22 13:05 100-02-707/29/22 11:3550065.9 1
N-Nitrosodimethylamine ND ug/L 07/30/22 13:05 62-75-907/29/22 11:3510018.9 1
N-Nitroso-di-n-propylamine ND ug/L 07/30/22 13:05 621-64-707/29/22 11:3510013.3 1
N-Nitrosodiphenylamine ND ug/L 07/30/22 13:05 86-30-607/29/22 11:3510030.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/30/22 13:05 108-60-107/29/22 11:3510011.5 1
Pentachlorophenol ND ug/L 07/30/22 13:05 87-86-507/29/22 11:3520037.6 1
Phenanthrene ND ug/L 07/30/22 13:05 85-01-807/29/22 11:3510020.0 1
Phenol 25.1J ug/L 07/30/22 13:05 108-95-2 B,C907/29/22 11:3510013.5 1
Pyrene ND ug/L 07/30/22 13:05 129-00-007/29/22 11:3510022.0 1
1,2,4-Trichlorobenzene ND ug/L 07/30/22 13:05 120-82-107/29/22 11:3510017.3 1
2,4,5-Trichlorophenol ND ug/L 07/30/22 13:05 95-95-407/29/22 11:3510014.2 1
2,4,6-Trichlorophenol ND ug/L 07/30/22 13:05 88-06-207/29/22 11:3510015.5 1
Surrogates
Nitrobenzene-d5 (S)83 %07/30/22 13:05 4165-60-007/29/22 11:3510-144 1
2-Fluorobiphenyl (S)62 %07/30/22 13:05 321-60-807/29/22 11:3510-130 1
Terphenyl-d14 (S)140 %07/30/22 13:05 1718-51-007/29/22 11:3534-163 1
Phenol-d6 (S)39 %07/30/22 13:05 13127-88-307/29/22 11:3510-130 1
2-Fluorophenol (S)52 %07/30/22 13:05 367-12-407/29/22 11:3510-130 1
2,4,6-Tribromophenol (S)103 %07/30/22 13:05 118-79-607/29/22 11:3510-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 78.4 ug/L 07/28/22 14:59 67-64-1 D625.0 5.1 1
Benzene ND ug/L 07/28/22 14:59 71-43-21.0 0.34 1
Bromobenzene ND ug/L 07/28/22 14:59 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 07/28/22 14:59 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 07/28/22 14:59 75-27-41.0 0.31 1
Bromoform ND ug/L 07/28/22 14:59 75-25-21.0 0.34 1
Bromomethane ND ug/L 07/28/22 14:59 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 07/28/22 14:59 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 07/28/22 14:59 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 07/28/22 14:59 108-90-71.0 0.28 1
Chloroethane ND ug/L 07/28/22 14:59 75-00-31.0 0.65 1
Chloroform ND ug/L 07/28/22 14:59 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-7 Lab ID:92616845002 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 07/28/22 14:59 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 07/28/22 14:59 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 07/28/22 14:59 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/22 14:59 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 07/28/22 14:59 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/22 14:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/22 14:59 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 07/28/22 14:59 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 07/28/22 14:59 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 07/28/22 14:59 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 07/28/22 14:59 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 07/28/22 14:59 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 07/28/22 14:59 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 07/28/22 14:59 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/28/22 14:59 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/28/22 14:59 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 07/28/22 14:59 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 07/28/22 14:59 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/28/22 14:59 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 07/28/22 14:59 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 07/28/22 14:59 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/28/22 14:59 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 07/28/22 14:59 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 07/28/22 14:59 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 07/28/22 14:59 87-68-32.0 1.5 1
2-Hexanone ND ug/L 07/28/22 14:59 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 07/28/22 14:59 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 07/28/22 14:59 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/22 14:59 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 07/28/22 14:59 1634-04-41.0 0.42 1
Naphthalene ND ug/L 07/28/22 14:59 91-20-31.0 0.64 1
Styrene ND ug/L 07/28/22 14:59 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/22 14:59 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/22 14:59 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 07/28/22 14:59 127-18-41.0 0.29 1
Toluene ND ug/L 07/28/22 14:59 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 07/28/22 14:59 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 07/28/22 14:59 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/28/22 14:59 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 07/28/22 14:59 79-00-51.0 0.32 1
Trichloroethene ND ug/L 07/28/22 14:59 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 07/28/22 14:59 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 07/28/22 14:59 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 07/28/22 14:59 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 07/28/22 14:59 75-01-41.0 0.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-7 Lab ID:92616845002 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 07/28/22 14:59 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 07/28/22 14:59 179601-23-12.0 0.71 1
o-Xylene ND ug/L 07/28/22 14:59 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %07/28/22 14:59 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)104 %07/28/22 14:59 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/22 14:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-8 Lab ID:92616845003 Collected:07/22/22 14:20 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/30/22 13:31 83-32-907/29/22 11:359.1 1.8 1
Acenaphthylene ND ug/L 07/30/22 13:31 208-96-807/29/22 11:359.1 1.8 1
Aniline ND ug/L 07/30/22 13:31 62-53-307/29/22 11:359.1 1.5 1
Anthracene ND ug/L 07/30/22 13:31 120-12-707/29/22 11:359.1 2.1 1
Benzo(a)anthracene ND ug/L 07/30/22 13:31 56-55-307/29/22 11:359.1 2.4 1
Benzo(a)pyrene ND ug/L 07/30/22 13:31 50-32-807/29/22 11:359.1 2.5 1
Benzo(b)fluoranthene ND ug/L 07/30/22 13:31 205-99-2 L107/29/22 11:359.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 07/30/22 13:31 191-24-207/29/22 11:359.1 2.6 1
Benzo(k)fluoranthene ND ug/L 07/30/22 13:31 207-08-9 L107/29/22 11:359.1 2.5 1
Benzoic Acid ND ug/L 07/30/22 13:31 65-85-007/29/22 11:3545.5 20.0 1
Benzyl alcohol ND ug/L 07/30/22 13:31 100-51-607/29/22 11:3518.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 07/30/22 13:31 101-55-307/29/22 11:359.1 1.6 1
Butylbenzylphthalate ND ug/L 07/30/22 13:31 85-68-707/29/22 11:359.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 07/30/22 13:31 59-50-707/29/22 11:359.1 3.0 1
4-Chloroaniline ND ug/L 07/30/22 13:31 106-47-807/29/22 11:3518.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 07/30/22 13:31 111-91-107/29/22 11:359.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/30/22 13:31 111-44-407/29/22 11:359.1 1.7 1
2-Chloronaphthalene ND ug/L 07/30/22 13:31 91-58-707/29/22 11:359.1 1.6 1
2-Chlorophenol ND ug/L 07/30/22 13:31 95-57-807/29/22 11:359.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 07/30/22 13:31 7005-72-307/29/22 11:359.1 1.8 1
Chrysene ND ug/L 07/30/22 13:31 218-01-907/29/22 11:359.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 07/30/22 13:31 53-70-307/29/22 11:359.1 2.7 1
Dibenzofuran ND ug/L 07/30/22 13:31 132-64-907/29/22 11:359.1 1.9 1
1,2-Dichlorobenzene ND ug/L 07/30/22 13:31 95-50-107/29/22 11:359.1 1.6 1
1,3-Dichlorobenzene ND ug/L 07/30/22 13:31 541-73-107/29/22 11:359.1 1.5 1
1,4-Dichlorobenzene ND ug/L 07/30/22 13:31 106-46-707/29/22 11:359.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 07/30/22 13:31 91-94-107/29/22 11:3518.2 7.4 1
2,4-Dichlorophenol ND ug/L 07/30/22 13:31 120-83-207/29/22 11:359.1 1.3 1
Diethylphthalate ND ug/L 07/30/22 13:31 84-66-207/29/22 11:359.1 1.9 1
2,4-Dimethylphenol ND ug/L 07/30/22 13:31 105-67-907/29/22 11:359.1 1.5 1
Dimethylphthalate ND ug/L 07/30/22 13:31 131-11-307/29/22 11:359.1 1.9 1
Di-n-butylphthalate ND ug/L 07/30/22 13:31 84-74-207/29/22 11:359.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/30/22 13:31 534-52-107/29/22 11:3518.2 7.1 1
2,4-Dinitrophenol ND ug/L 07/30/22 13:31 51-28-507/29/22 11:3545.5 23.6 1
2,4-Dinitrotoluene ND ug/L 07/30/22 13:31 121-14-207/29/22 11:359.1 1.5 1
2,6-Dinitrotoluene ND ug/L 07/30/22 13:31 606-20-207/29/22 11:359.1 1.6 1
Di-n-octylphthalate ND ug/L 07/30/22 13:31 117-84-007/29/22 11:359.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/30/22 13:31 117-81-707/29/22 11:355.5 3.4 1
Fluoranthene ND ug/L 07/30/22 13:31 206-44-007/29/22 11:359.1 2.0 1
Fluorene ND ug/L 07/30/22 13:31 86-73-707/29/22 11:359.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 07/30/22 13:31 87-68-307/29/22 11:359.1 1.6 1
Hexachlorobenzene ND ug/L 07/30/22 13:31 118-74-107/29/22 11:359.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 07/30/22 13:31 77-47-407/29/22 11:359.1 1.4 1
Hexachloroethane ND ug/L 07/30/22 13:31 67-72-107/29/22 11:359.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/30/22 13:31 193-39-507/29/22 11:359.1 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-8 Lab ID:92616845003 Collected:07/22/22 14:20 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 07/30/22 13:31 78-59-107/29/22 11:359.1 1.5 1
1-Methylnaphthalene ND ug/L 07/30/22 13:31 90-12-007/29/22 11:359.1 1.8 1
2-Methylnaphthalene ND ug/L 07/30/22 13:31 91-57-607/29/22 11:359.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 07/30/22 13:31 95-48-707/29/22 11:359.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/30/22 13:31 15831-10-407/29/22 11:359.1 1.1 1
Naphthalene ND ug/L 07/30/22 13:31 91-20-307/29/22 11:359.1 1.9 1
2-Nitroaniline ND ug/L 07/30/22 13:31 88-74-407/29/22 11:3518.2 2.7 1
3-Nitroaniline ND ug/L 07/30/22 13:31 99-09-207/29/22 11:3518.2 3.4 1
4-Nitroaniline ND ug/L 07/30/22 13:31 100-01-6 v207/29/22 11:3518.2 4.6 1
Nitrobenzene ND ug/L 07/30/22 13:31 98-95-307/29/22 11:359.1 1.7 1
2-Nitrophenol ND ug/L 07/30/22 13:31 88-75-507/29/22 11:359.1 1.3 1
4-Nitrophenol ND ug/L 07/30/22 13:31 100-02-707/29/22 11:3545.5 6.0 1
N-Nitrosodimethylamine ND ug/L 07/30/22 13:31 62-75-907/29/22 11:359.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 07/30/22 13:31 621-64-707/29/22 11:359.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 07/30/22 13:31 86-30-607/29/22 11:359.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/30/22 13:31 108-60-107/29/22 11:359.1 1.0 1
Pentachlorophenol ND ug/L 07/30/22 13:31 87-86-507/29/22 11:3518.2 3.4 1
Phenanthrene ND ug/L 07/30/22 13:31 85-01-807/29/22 11:359.1 1.8 1
Phenol 1.9J ug/L 07/30/22 13:31 108-95-2 B,C907/29/22 11:359.1 1.2 1
Pyrene ND ug/L 07/30/22 13:31 129-00-007/29/22 11:359.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 07/30/22 13:31 120-82-107/29/22 11:359.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/30/22 13:31 95-95-407/29/22 11:359.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 07/30/22 13:31 88-06-207/29/22 11:359.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)44 %07/30/22 13:31 4165-60-007/29/22 11:3510-144 1
2-Fluorobiphenyl (S)38 %07/30/22 13:31 321-60-807/29/22 11:3510-130 1
Terphenyl-d14 (S)125 %07/30/22 13:31 1718-51-007/29/22 11:3534-163 1
Phenol-d6 (S)23 %07/30/22 13:31 13127-88-307/29/22 11:3510-130 1
2-Fluorophenol (S)28 %07/30/22 13:31 367-12-407/29/22 11:3510-130 1
2,4,6-Tribromophenol (S)78 %07/30/22 13:31 118-79-607/29/22 11:3510-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/28/22 15:18 67-64-125.0 5.1 1
Benzene ND ug/L 07/28/22 15:18 71-43-21.0 0.34 1
Bromobenzene ND ug/L 07/28/22 15:18 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 07/28/22 15:18 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 07/28/22 15:18 75-27-41.0 0.31 1
Bromoform ND ug/L 07/28/22 15:18 75-25-21.0 0.34 1
Bromomethane ND ug/L 07/28/22 15:18 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 07/28/22 15:18 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 07/28/22 15:18 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 07/28/22 15:18 108-90-71.0 0.28 1
Chloroethane ND ug/L 07/28/22 15:18 75-00-31.0 0.65 1
Chloroform ND ug/L 07/28/22 15:18 67-66-31.0 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-8 Lab ID:92616845003 Collected:07/22/22 14:20 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 07/28/22 15:18 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 07/28/22 15:18 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 07/28/22 15:18 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/22 15:18 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 07/28/22 15:18 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/22 15:18 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/22 15:18 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 07/28/22 15:18 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 07/28/22 15:18 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 07/28/22 15:18 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 07/28/22 15:18 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 07/28/22 15:18 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 07/28/22 15:18 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 07/28/22 15:18 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/28/22 15:18 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/28/22 15:18 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 07/28/22 15:18 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 07/28/22 15:18 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 07/28/22 15:18 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 07/28/22 15:18 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 07/28/22 15:18 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/28/22 15:18 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 07/28/22 15:18 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 07/28/22 15:18 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 07/28/22 15:18 87-68-32.0 1.5 1
2-Hexanone ND ug/L 07/28/22 15:18 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 07/28/22 15:18 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 07/28/22 15:18 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/22 15:18 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 07/28/22 15:18 1634-04-41.0 0.42 1
Naphthalene ND ug/L 07/28/22 15:18 91-20-31.0 0.64 1
Styrene ND ug/L 07/28/22 15:18 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/22 15:18 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/22 15:18 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 07/28/22 15:18 127-18-41.0 0.29 1
Toluene ND ug/L 07/28/22 15:18 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 07/28/22 15:18 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 07/28/22 15:18 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/28/22 15:18 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 07/28/22 15:18 79-00-51.0 0.32 1
Trichloroethene ND ug/L 07/28/22 15:18 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 07/28/22 15:18 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 07/28/22 15:18 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 07/28/22 15:18 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 07/28/22 15:18 75-01-41.0 0.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:MW-8 Lab ID:92616845003 Collected:07/22/22 14:20 Received:07/26/22 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 07/28/22 15:18 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 07/28/22 15:18 179601-23-12.0 0.71 1
o-Xylene ND ug/L 07/28/22 15:18 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/22 15:18 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/22 15:18 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/22 15:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-12 Lab ID:92616845006 Collected:07/22/22 12:15 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 08/01/22 11:32 83-32-907/28/22 18:024171461
Acenaphthylene ND ug/kg 08/01/22 11:32 208-96-807/28/22 18:024171461
Aniline ND ug/kg 08/01/22 11:32 62-53-307/28/22 18:024171631
Anthracene ND ug/kg 08/01/22 11:32 120-12-707/28/22 18:024171361
Benzo(a)anthracene ND ug/kg 08/01/22 11:32 56-55-307/28/22 18:024171391
Benzo(a)pyrene ND ug/kg 08/01/22 11:32 50-32-807/28/22 18:024171441
Benzo(b)fluoranthene ND ug/kg 08/01/22 11:32 205-99-207/28/22 18:024171391
Benzo(g,h,i)perylene ND ug/kg 08/01/22 11:32 191-24-207/28/22 18:024171621
Benzo(k)fluoranthene ND ug/kg 08/01/22 11:32 207-08-907/28/22 18:024171461
Benzoic Acid ND ug/kg 08/01/22 11:32 65-85-007/28/22 18:0220808951
Benzyl alcohol ND ug/kg 08/01/22 11:32 100-51-607/28/22 18:028333161
4-Bromophenylphenyl ether ND ug/kg 08/01/22 11:32 101-55-307/28/22 18:024171601
Butylbenzylphthalate ND ug/kg 08/01/22 11:32 85-68-707/28/22 18:024171761
4-Chloro-3-methylphenol ND ug/kg 08/01/22 11:32 59-50-707/28/22 18:028332931
4-Chloroaniline ND ug/kg 08/01/22 11:32 106-47-807/28/22 18:028333271
bis(2-Chloroethoxy)methane ND ug/kg 08/01/22 11:32 111-91-107/28/22 18:024171731
bis(2-Chloroethyl) ether ND ug/kg 08/01/22 11:32 111-44-407/28/22 18:024171571
2-Chloronaphthalene ND ug/kg 08/01/22 11:32 91-58-707/28/22 18:024171651
2-Chlorophenol ND ug/kg 08/01/22 11:32 95-57-807/28/22 18:024171571
4-Chlorophenylphenyl ether ND ug/kg 08/01/22 11:32 7005-72-307/28/22 18:024171551
Chrysene ND ug/kg 08/01/22 11:32 218-01-907/28/22 18:024171521
Dibenz(a,h)anthracene ND ug/kg 08/01/22 11:32 53-70-307/28/22 18:024171601
Dibenzofuran ND ug/kg 08/01/22 11:32 132-64-907/28/22 18:024171501
1,2-Dichlorobenzene ND ug/kg 08/01/22 11:32 95-50-107/28/22 18:024171501
1,3-Dichlorobenzene ND ug/kg 08/01/22 11:32 541-73-107/28/22 18:024171481
1,4-Dichlorobenzene ND ug/kg 08/01/22 11:32 106-46-707/28/22 18:024171591
3,3'-Dichlorobenzidine ND ug/kg 08/01/22 11:32 91-94-107/28/22 18:028332821
2,4-Dichlorophenol ND ug/kg 08/01/22 11:32 120-83-207/28/22 18:024171631
Diethylphthalate ND ug/kg 08/01/22 11:32 84-66-207/28/22 18:024171531
2,4-Dimethylphenol ND ug/kg 08/01/22 11:32 105-67-907/28/22 18:024171731
Dimethylphthalate ND ug/kg 08/01/22 11:32 131-11-307/28/22 18:024171521
Di-n-butylphthalate ND ug/kg 08/01/22 11:32 84-74-207/28/22 18:024171401
4,6-Dinitro-2-methylphenol ND ug/kg 08/01/22 11:32 534-52-107/28/22 18:028333891
2,4-Dinitrophenol ND ug/kg 08/01/22 11:32 51-28-507/28/22 18:02208012901
2,4-Dinitrotoluene ND ug/kg 08/01/22 11:32 121-14-207/28/22 18:024171601
2,6-Dinitrotoluene ND ug/kg 08/01/22 11:32 606-20-207/28/22 18:024171531
Di-n-octylphthalate ND ug/kg 08/01/22 11:32 117-84-007/28/22 18:024171641
bis(2-Ethylhexyl)phthalate ND ug/kg 08/01/22 11:32 117-81-707/28/22 18:024171621
Fluoranthene ND ug/kg 08/01/22 11:32 206-44-007/28/22 18:024171431
Fluorene ND ug/kg 08/01/22 11:32 86-73-707/28/22 18:024171461
Hexachloro-1,3-butadiene ND ug/kg 08/01/22 11:32 87-68-307/28/22 18:024171811
Hexachlorobenzene ND ug/kg 08/01/22 11:32 118-74-107/28/22 18:024171631
Hexachlorocyclopentadiene ND ug/kg 08/01/22 11:32 77-47-407/28/22 18:024172391
Hexachloroethane ND ug/kg 08/01/22 11:32 67-72-107/28/22 18:024171591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-12 Lab ID:92616845006 Collected:07/22/22 12:15 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 08/01/22 11:32 193-39-507/28/22 18:024171641
Isophorone ND ug/kg 08/01/22 11:32 78-59-107/28/22 18:024171861
1-Methylnaphthalene ND ug/kg 08/01/22 11:32 90-12-007/28/22 18:024171461
2-Methylnaphthalene ND ug/kg 08/01/22 11:32 91-57-607/28/22 18:024171671
2-Methylphenol(o-Cresol)ND ug/kg 08/01/22 11:32 95-48-707/28/22 18:024171701
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/01/22 11:32 15831-10-407/28/22 18:024171681
Naphthalene ND ug/kg 08/01/22 11:32 91-20-307/28/22 18:024171411
2-Nitroaniline ND ug/kg 08/01/22 11:32 88-74-407/28/22 18:0220803411
3-Nitroaniline ND ug/kg 08/01/22 11:32 99-09-207/28/22 18:0220803271
4-Nitroaniline ND ug/kg 08/01/22 11:32 100-01-607/28/22 18:028333171
Nitrobenzene ND ug/kg 08/01/22 11:32 98-95-307/28/22 18:024171931
2-Nitrophenol ND ug/kg 08/01/22 11:32 88-75-507/28/22 18:024171811
4-Nitrophenol ND ug/kg 08/01/22 11:32 100-02-707/28/22 18:0220808061
N-Nitrosodimethylamine ND ug/kg 08/01/22 11:32 62-75-907/28/22 18:024171401
N-Nitroso-di-n-propylamine ND ug/kg 08/01/22 11:32 621-64-707/28/22 18:024171571
N-Nitrosodiphenylamine ND ug/kg 08/01/22 11:32 86-30-607/28/22 18:024171481
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/01/22 11:32 108-60-107/28/22 18:024171981
Pentachlorophenol ND ug/kg 08/01/22 11:32 87-86-507/28/22 18:028334081
Phenanthrene ND ug/kg 08/01/22 11:32 85-01-807/28/22 18:024171361
Phenol ND ug/kg 08/01/22 11:32 108-95-207/28/22 18:024171861
Pyrene ND ug/kg 08/01/22 11:32 129-00-007/28/22 18:024171691
Pyridine ND ug/kg 08/01/22 11:32 110-86-107/28/22 18:024171311
1,2,4-Trichlorobenzene ND ug/kg 08/01/22 11:32 120-82-107/28/22 18:024171641
2,4,5-Trichlorophenol ND ug/kg 08/01/22 11:32 95-95-407/28/22 18:024171911
2,4,6-Trichlorophenol ND ug/kg 08/01/22 11:32 88-06-207/28/22 18:024171721
Surrogates
Nitrobenzene-d5 (S)46 %08/01/22 11:32 4165-60-007/28/22 18:0221-130 1
2-Fluorobiphenyl (S)44 %08/01/22 11:32 321-60-807/28/22 18:0219-130 1
Terphenyl-d14 (S)51 %08/01/22 11:32 1718-51-007/28/22 18:0215-130 1
Phenol-d6 (S)49 %08/01/22 11:32 13127-88-307/28/22 18:0218-130 1
2-Fluorophenol (S)46 %08/01/22 11:32 367-12-407/28/22 18:0218-130 1
2,4,6-Tribromophenol (S)50 %08/01/22 11:32 118-79-607/28/22 18:0218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/28/22 02:37 67-64-107/27/22 18:0513944.5 1
Benzene ND ug/kg 07/28/22 02:37 71-43-207/27/22 18:056.9 2.8 1
Bromobenzene ND ug/kg 07/28/22 02:37 108-86-107/27/22 18:056.9 2.3 1
Bromochloromethane ND ug/kg 07/28/22 02:37 74-97-507/27/22 18:056.9 2.1 1
Bromodichloromethane ND ug/kg 07/28/22 02:37 75-27-407/27/22 18:056.9 2.7 1
Bromoform ND ug/kg 07/28/22 02:37 75-25-207/27/22 18:056.9 2.4 1
Bromomethane ND ug/kg 07/28/22 02:37 74-83-9 IK,L107/27/22 18:0513.9 10.9 1
2-Butanone (MEK)46.9J ug/kg 07/28/22 02:37 78-93-3 C707/27/22 18:0513933.3 1
n-Butylbenzene ND ug/kg 07/28/22 02:37 104-51-807/27/22 18:056.9 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-12 Lab ID:92616845006 Collected:07/22/22 12:15 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene ND ug/kg 07/28/22 02:37 135-98-807/27/22 18:056.9 3.0 1
tert-Butylbenzene ND ug/kg 07/28/22 02:37 98-06-607/27/22 18:056.9 2.5 1
Carbon tetrachloride ND ug/kg 07/28/22 02:37 56-23-507/27/22 18:056.9 2.6 1
Chlorobenzene ND ug/kg 07/28/22 02:37 108-90-707/27/22 18:056.9 1.3 1
Chloroethane ND ug/kg 07/28/22 02:37 75-00-307/27/22 18:0513.9 5.3 1
Chloroform ND ug/kg 07/28/22 02:37 67-66-307/27/22 18:056.9 4.2 1
Chloromethane ND ug/kg 07/28/22 02:37 74-87-307/27/22 18:0513.9 5.8 1
2-Chlorotoluene ND ug/kg 07/28/22 02:37 95-49-807/27/22 18:056.9 2.5 1
4-Chlorotoluene ND ug/kg 07/28/22 02:37 106-43-407/27/22 18:056.9 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/28/22 02:37 96-12-8 IK,v207/27/22 18:056.9 2.7 1
Dibromochloromethane ND ug/kg 07/28/22 02:37 124-48-107/27/22 18:056.9 3.9 1
1,2-Dibromoethane (EDB)ND ug/kg 07/28/22 02:37 106-93-407/27/22 18:056.9 3.0 1
Dibromomethane ND ug/kg 07/28/22 02:37 74-95-307/27/22 18:056.9 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/28/22 02:37 95-50-107/27/22 18:056.9 2.5 1
1,3-Dichlorobenzene ND ug/kg 07/28/22 02:37 541-73-107/27/22 18:056.9 2.1 1
1,4-Dichlorobenzene ND ug/kg 07/28/22 02:37 106-46-707/27/22 18:056.9 1.8 1
Dichlorodifluoromethane ND ug/kg 07/28/22 02:37 75-71-8 IH,v107/27/22 18:0513.9 3.0 1
1,1-Dichloroethane ND ug/kg 07/28/22 02:37 75-34-307/27/22 18:056.9 2.9 1
1,2-Dichloroethane ND ug/kg 07/28/22 02:37 107-06-207/27/22 18:056.9 4.6 1
1,1-Dichloroethene ND ug/kg 07/28/22 02:37 75-35-407/27/22 18:056.9 2.9 1
cis-1,2-Dichloroethene ND ug/kg 07/28/22 02:37 156-59-207/27/22 18:056.9 2.4 1
trans-1,2-Dichloroethene ND ug/kg 07/28/22 02:37 156-60-507/27/22 18:056.9 2.4 1
1,2-Dichloropropane ND ug/kg 07/28/22 02:37 78-87-507/27/22 18:056.9 2.1 1
1,3-Dichloropropane ND ug/kg 07/28/22 02:37 142-28-907/27/22 18:056.9 2.2 1
2,2-Dichloropropane ND ug/kg 07/28/22 02:37 594-20-707/27/22 18:056.9 2.3 1
1,1-Dichloropropene ND ug/kg 07/28/22 02:37 563-58-607/27/22 18:056.9 3.3 1
cis-1,3-Dichloropropene ND ug/kg 07/28/22 02:37 10061-01-507/27/22 18:056.9 1.9 1
trans-1,3-Dichloropropene ND ug/kg 07/28/22 02:37 10061-02-607/27/22 18:056.9 2.4 1
Diisopropyl ether ND ug/kg 07/28/22 02:37 108-20-307/27/22 18:056.9 1.9 1
Ethylbenzene 4.0J ug/kg 07/28/22 02:37 100-41-407/27/22 18:056.9 3.2 1
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 02:37 87-68-307/27/22 18:0513.9 11.3 1
2-Hexanone ND ug/kg 07/28/22 02:37 591-78-607/27/22 18:0569.3 6.7 1
Isopropylbenzene (Cumene)ND ug/kg 07/28/22 02:37 98-82-807/27/22 18:056.9 2.4 1
p-Isopropyltoluene ND ug/kg 07/28/22 02:37 99-87-607/27/22 18:056.9 3.4 1
Methylene Chloride 65.3 ug/kg 07/28/22 02:37 75-09-2 C907/27/22 18:0527.7 19.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/28/22 02:37 108-10-107/27/22 18:0569.3 6.7 1
Methyl-tert-butyl ether ND ug/kg 07/28/22 02:37 1634-04-407/27/22 18:056.9 2.6 1
Naphthalene ND ug/kg 07/28/22 02:37 91-20-3 v207/27/22 18:056.9 3.6 1
n-Propylbenzene ND ug/kg 07/28/22 02:37 103-65-107/27/22 18:056.9 2.5 1
Styrene ND ug/kg 07/28/22 02:37 100-42-507/27/22 18:056.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/28/22 02:37 630-20-607/27/22 18:056.9 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/28/22 02:37 79-34-507/27/22 18:056.9 1.8 1
Tetrachloroethene ND ug/kg 07/28/22 02:37 127-18-407/27/22 18:056.9 2.2 1
Toluene ND ug/kg 07/28/22 02:37 108-88-307/27/22 18:056.9 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-12 Lab ID:92616845006 Collected:07/22/22 12:15 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 07/28/22 02:37 87-61-6 IK,L2,v207/27/22 18:056.9 5.6 1
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 02:37 120-82-107/27/22 18:056.9 5.8 1
1,1,1-Trichloroethane ND ug/kg 07/28/22 02:37 71-55-607/27/22 18:056.9 3.6 1
1,1,2-Trichloroethane ND ug/kg 07/28/22 02:37 79-00-507/27/22 18:056.9 2.3 1
Trichloroethene ND ug/kg 07/28/22 02:37 79-01-607/27/22 18:056.9 1.8 1
Trichlorofluoromethane ND ug/kg 07/28/22 02:37 75-69-407/27/22 18:056.9 3.8 1
1,2,3-Trichloropropane ND ug/kg 07/28/22 02:37 96-18-407/27/22 18:056.9 3.5 1
1,2,4-Trimethylbenzene 4.0J ug/kg 07/28/22 02:37 95-63-607/27/22 18:056.9 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 07/28/22 02:37 108-67-807/27/22 18:056.9 2.3 1
Vinyl acetate ND ug/kg 07/28/22 02:37 108-05-407/27/22 18:0569.3 5.0 1
Vinyl chloride ND ug/kg 07/28/22 02:37 75-01-407/27/22 18:0513.9 3.5 1
Xylene (Total)10.4J ug/kg 07/28/22 02:37 1330-20-707/27/22 18:0513.9 3.9 1
m&p-Xylene 6.6J ug/kg 07/28/22 02:37 179601-23-107/27/22 18:0513.9 4.7 1
o-Xylene 3.8J ug/kg 07/28/22 02:37 95-47-607/27/22 18:056.9 3.1 1
Surrogates
Toluene-d8 (S)101 %07/28/22 02:37 2037-26-507/27/22 18:0570-130 1
4-Bromofluorobenzene (S)98 %07/28/22 02:37 460-00-407/27/22 18:0569-134 1
1,2-Dichloroethane-d4 (S)109 %07/28/22 02:37 17060-07-007/27/22 18:0570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.1 %07/27/22 18:55 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-13 Lab ID:92616845007 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 08/01/22 11:59 83-32-907/28/22 18:024091441
Acenaphthylene ND ug/kg 08/01/22 11:59 208-96-807/28/22 18:024091441
Aniline ND ug/kg 08/01/22 11:59 62-53-307/28/22 18:024091601
Anthracene ND ug/kg 08/01/22 11:59 120-12-707/28/22 18:024091341
Benzo(a)anthracene ND ug/kg 08/01/22 11:59 56-55-307/28/22 18:024091361
Benzo(a)pyrene ND ug/kg 08/01/22 11:59 50-32-807/28/22 18:024091411
Benzo(b)fluoranthene ND ug/kg 08/01/22 11:59 205-99-207/28/22 18:024091361
Benzo(g,h,i)perylene ND ug/kg 08/01/22 11:59 191-24-207/28/22 18:024091581
Benzo(k)fluoranthene ND ug/kg 08/01/22 11:59 207-08-907/28/22 18:024091441
Benzoic Acid ND ug/kg 08/01/22 11:59 65-85-007/28/22 18:0220408781
Benzyl alcohol ND ug/kg 08/01/22 11:59 100-51-607/28/22 18:028173101
4-Bromophenylphenyl ether ND ug/kg 08/01/22 11:59 101-55-307/28/22 18:024091571
Butylbenzylphthalate ND ug/kg 08/01/22 11:59 85-68-707/28/22 18:024091721
4-Chloro-3-methylphenol ND ug/kg 08/01/22 11:59 59-50-707/28/22 18:028172871
4-Chloroaniline ND ug/kg 08/01/22 11:59 106-47-807/28/22 18:028173211
bis(2-Chloroethoxy)methane ND ug/kg 08/01/22 11:59 111-91-107/28/22 18:024091701
bis(2-Chloroethyl) ether ND ug/kg 08/01/22 11:59 111-44-407/28/22 18:024091541
2-Chloronaphthalene ND ug/kg 08/01/22 11:59 91-58-707/28/22 18:024091621
2-Chlorophenol ND ug/kg 08/01/22 11:59 95-57-807/28/22 18:024091541
4-Chlorophenylphenyl ether ND ug/kg 08/01/22 11:59 7005-72-307/28/22 18:024091521
Chrysene ND ug/kg 08/01/22 11:59 218-01-907/28/22 18:024091491
Dibenz(a,h)anthracene ND ug/kg 08/01/22 11:59 53-70-307/28/22 18:024091571
Dibenzofuran ND ug/kg 08/01/22 11:59 132-64-907/28/22 18:024091471
1,2-Dichlorobenzene ND ug/kg 08/01/22 11:59 95-50-107/28/22 18:024091471
1,3-Dichlorobenzene ND ug/kg 08/01/22 11:59 541-73-107/28/22 18:024091451
1,4-Dichlorobenzene ND ug/kg 08/01/22 11:59 106-46-707/28/22 18:024091561
3,3'-Dichlorobenzidine ND ug/kg 08/01/22 11:59 91-94-107/28/22 18:028172761
2,4-Dichlorophenol ND ug/kg 08/01/22 11:59 120-83-207/28/22 18:024091601
Diethylphthalate ND ug/kg 08/01/22 11:59 84-66-207/28/22 18:024091501
2,4-Dimethylphenol ND ug/kg 08/01/22 11:59 105-67-907/28/22 18:024091701
Dimethylphthalate ND ug/kg 08/01/22 11:59 131-11-307/28/22 18:024091491
Di-n-butylphthalate ND ug/kg 08/01/22 11:59 84-74-207/28/22 18:024091371
4,6-Dinitro-2-methylphenol ND ug/kg 08/01/22 11:59 534-52-107/28/22 18:028173811
2,4-Dinitrophenol ND ug/kg 08/01/22 11:59 51-28-507/28/22 18:02204012601
2,4-Dinitrotoluene ND ug/kg 08/01/22 11:59 121-14-207/28/22 18:024091571
2,6-Dinitrotoluene ND ug/kg 08/01/22 11:59 606-20-207/28/22 18:024091501
Di-n-octylphthalate ND ug/kg 08/01/22 11:59 117-84-007/28/22 18:024091611
bis(2-Ethylhexyl)phthalate ND ug/kg 08/01/22 11:59 117-81-707/28/22 18:024091581
Fluoranthene ND ug/kg 08/01/22 11:59 206-44-007/28/22 18:024091401
Fluorene ND ug/kg 08/01/22 11:59 86-73-707/28/22 18:024091441
Hexachloro-1,3-butadiene ND ug/kg 08/01/22 11:59 87-68-307/28/22 18:024091771
Hexachlorobenzene ND ug/kg 08/01/22 11:59 118-74-107/28/22 18:024091601
Hexachlorocyclopentadiene ND ug/kg 08/01/22 11:59 77-47-407/28/22 18:024092341
Hexachloroethane ND ug/kg 08/01/22 11:59 67-72-107/28/22 18:024091561
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-13 Lab ID:92616845007 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 08/01/22 11:59 193-39-507/28/22 18:024091611
Isophorone ND ug/kg 08/01/22 11:59 78-59-107/28/22 18:024091821
1-Methylnaphthalene ND ug/kg 08/01/22 11:59 90-12-007/28/22 18:024091441
2-Methylnaphthalene ND ug/kg 08/01/22 11:59 91-57-607/28/22 18:024091631
2-Methylphenol(o-Cresol)ND ug/kg 08/01/22 11:59 95-48-707/28/22 18:024091671
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/01/22 11:59 15831-10-407/28/22 18:024091651
Naphthalene ND ug/kg 08/01/22 11:59 91-20-307/28/22 18:024091391
2-Nitroaniline ND ug/kg 08/01/22 11:59 88-74-407/28/22 18:0220403341
3-Nitroaniline ND ug/kg 08/01/22 11:59 99-09-207/28/22 18:0220403211
4-Nitroaniline ND ug/kg 08/01/22 11:59 100-01-607/28/22 18:028173111
Nitrobenzene ND ug/kg 08/01/22 11:59 98-95-307/28/22 18:024091891
2-Nitrophenol ND ug/kg 08/01/22 11:59 88-75-507/28/22 18:024091771
4-Nitrophenol ND ug/kg 08/01/22 11:59 100-02-707/28/22 18:0220407901
N-Nitrosodimethylamine ND ug/kg 08/01/22 11:59 62-75-907/28/22 18:024091371
N-Nitroso-di-n-propylamine ND ug/kg 08/01/22 11:59 621-64-707/28/22 18:024091541
N-Nitrosodiphenylamine ND ug/kg 08/01/22 11:59 86-30-607/28/22 18:024091451
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/01/22 11:59 108-60-107/28/22 18:024091941
Pentachlorophenol ND ug/kg 08/01/22 11:59 87-86-507/28/22 18:028174001
Phenanthrene ND ug/kg 08/01/22 11:59 85-01-807/28/22 18:024091341
Phenol ND ug/kg 08/01/22 11:59 108-95-207/28/22 18:024091821
Pyrene ND ug/kg 08/01/22 11:59 129-00-007/28/22 18:024091661
Pyridine ND ug/kg 08/01/22 11:59 110-86-107/28/22 18:024091291
1,2,4-Trichlorobenzene ND ug/kg 08/01/22 11:59 120-82-107/28/22 18:024091611
2,4,5-Trichlorophenol ND ug/kg 08/01/22 11:59 95-95-407/28/22 18:024091871
2,4,6-Trichlorophenol ND ug/kg 08/01/22 11:59 88-06-207/28/22 18:024091681
Surrogates
Nitrobenzene-d5 (S)68 %08/01/22 11:59 4165-60-007/28/22 18:0221-130 1
2-Fluorobiphenyl (S)61 %08/01/22 11:59 321-60-807/28/22 18:0219-130 1
Terphenyl-d14 (S)73 %08/01/22 11:59 1718-51-007/28/22 18:0215-130 1
Phenol-d6 (S)71 %08/01/22 11:59 13127-88-307/28/22 18:0218-130 1
2-Fluorophenol (S)65 %08/01/22 11:59 367-12-407/28/22 18:0218-130 1
2,4,6-Tribromophenol (S)73 %08/01/22 11:59 118-79-607/28/22 18:0218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/28/22 02:55 67-64-107/27/22 18:0513141.9 1
Benzene ND ug/kg 07/28/22 02:55 71-43-207/27/22 18:056.5 2.6 1
Bromobenzene ND ug/kg 07/28/22 02:55 108-86-107/27/22 18:056.5 2.1 1
Bromochloromethane ND ug/kg 07/28/22 02:55 74-97-507/27/22 18:056.5 1.9 1
Bromodichloromethane ND ug/kg 07/28/22 02:55 75-27-407/27/22 18:056.5 2.5 1
Bromoform ND ug/kg 07/28/22 02:55 75-25-207/27/22 18:056.5 2.3 1
Bromomethane ND ug/kg 07/28/22 02:55 74-83-9 IK,L107/27/22 18:0513.1 10.3 1
2-Butanone (MEK)49.4J ug/kg 07/28/22 02:55 78-93-3 C707/27/22 18:0513131.3 1
n-Butylbenzene ND ug/kg 07/28/22 02:55 104-51-807/27/22 18:056.5 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-13 Lab ID:92616845007 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene ND ug/kg 07/28/22 02:55 135-98-807/27/22 18:056.5 2.9 1
tert-Butylbenzene ND ug/kg 07/28/22 02:55 98-06-607/27/22 18:056.5 2.3 1
Carbon tetrachloride ND ug/kg 07/28/22 02:55 56-23-507/27/22 18:056.5 2.4 1
Chlorobenzene ND ug/kg 07/28/22 02:55 108-90-707/27/22 18:056.5 1.3 1
Chloroethane ND ug/kg 07/28/22 02:55 75-00-307/27/22 18:0513.1 5.0 1
Chloroform ND ug/kg 07/28/22 02:55 67-66-307/27/22 18:056.5 4.0 1
Chloromethane ND ug/kg 07/28/22 02:55 74-87-307/27/22 18:0513.1 5.5 1
2-Chlorotoluene ND ug/kg 07/28/22 02:55 95-49-807/27/22 18:056.5 2.3 1
4-Chlorotoluene ND ug/kg 07/28/22 02:55 106-43-407/27/22 18:056.5 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/28/22 02:55 96-12-8 IK,v207/27/22 18:056.5 2.5 1
Dibromochloromethane ND ug/kg 07/28/22 02:55 124-48-107/27/22 18:056.5 3.7 1
1,2-Dibromoethane (EDB)ND ug/kg 07/28/22 02:55 106-93-407/27/22 18:056.5 2.9 1
Dibromomethane ND ug/kg 07/28/22 02:55 74-95-307/27/22 18:056.5 1.4 1
1,2-Dichlorobenzene ND ug/kg 07/28/22 02:55 95-50-107/27/22 18:056.5 2.3 1
1,3-Dichlorobenzene ND ug/kg 07/28/22 02:55 541-73-107/27/22 18:056.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 07/28/22 02:55 106-46-707/27/22 18:056.5 1.7 1
Dichlorodifluoromethane ND ug/kg 07/28/22 02:55 75-71-8 IH,v107/27/22 18:0513.1 2.8 1
1,1-Dichloroethane ND ug/kg 07/28/22 02:55 75-34-307/27/22 18:056.5 2.7 1
1,2-Dichloroethane ND ug/kg 07/28/22 02:55 107-06-207/27/22 18:056.5 4.3 1
1,1-Dichloroethene ND ug/kg 07/28/22 02:55 75-35-407/27/22 18:056.5 2.7 1
cis-1,2-Dichloroethene ND ug/kg 07/28/22 02:55 156-59-207/27/22 18:056.5 2.2 1
trans-1,2-Dichloroethene ND ug/kg 07/28/22 02:55 156-60-507/27/22 18:056.5 2.3 1
1,2-Dichloropropane ND ug/kg 07/28/22 02:55 78-87-507/27/22 18:056.5 2.0 1
1,3-Dichloropropane ND ug/kg 07/28/22 02:55 142-28-907/27/22 18:056.5 2.0 1
2,2-Dichloropropane ND ug/kg 07/28/22 02:55 594-20-707/27/22 18:056.5 2.1 1
1,1-Dichloropropene ND ug/kg 07/28/22 02:55 563-58-607/27/22 18:056.5 3.1 1
cis-1,3-Dichloropropene ND ug/kg 07/28/22 02:55 10061-01-507/27/22 18:056.5 1.8 1
trans-1,3-Dichloropropene ND ug/kg 07/28/22 02:55 10061-02-607/27/22 18:056.5 2.2 1
Diisopropyl ether ND ug/kg 07/28/22 02:55 108-20-307/27/22 18:056.5 1.8 1
Ethylbenzene 3.6J ug/kg 07/28/22 02:55 100-41-407/27/22 18:056.5 3.0 1
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 02:55 87-68-307/27/22 18:0513.1 10.7 1
2-Hexanone ND ug/kg 07/28/22 02:55 591-78-607/27/22 18:0565.3 6.3 1
Isopropylbenzene (Cumene)ND ug/kg 07/28/22 02:55 98-82-807/27/22 18:056.5 2.2 1
p-Isopropyltoluene ND ug/kg 07/28/22 02:55 99-87-607/27/22 18:056.5 3.2 1
Methylene Chloride 56.6 ug/kg 07/28/22 02:55 75-09-2 C907/27/22 18:0526.1 17.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/28/22 02:55 108-10-107/27/22 18:0565.3 6.3 1
Methyl-tert-butyl ether ND ug/kg 07/28/22 02:55 1634-04-407/27/22 18:056.5 2.4 1
Naphthalene ND ug/kg 07/28/22 02:55 91-20-3 v207/27/22 18:056.5 3.4 1
n-Propylbenzene ND ug/kg 07/28/22 02:55 103-65-107/27/22 18:056.5 2.3 1
Styrene ND ug/kg 07/28/22 02:55 100-42-507/27/22 18:056.5 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/28/22 02:55 630-20-607/27/22 18:056.5 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/28/22 02:55 79-34-507/27/22 18:056.5 1.7 1
Tetrachloroethene ND ug/kg 07/28/22 02:55 127-18-407/27/22 18:056.5 2.1 1
Toluene ND ug/kg 07/28/22 02:55 108-88-307/27/22 18:056.5 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-13 Lab ID:92616845007 Collected:07/22/22 13:10 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 07/28/22 02:55 87-61-6 IK,L2,v207/27/22 18:056.5 5.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 02:55 120-82-107/27/22 18:056.5 5.5 1
1,1,1-Trichloroethane ND ug/kg 07/28/22 02:55 71-55-607/27/22 18:056.5 3.4 1
1,1,2-Trichloroethane ND ug/kg 07/28/22 02:55 79-00-507/27/22 18:056.5 2.2 1
Trichloroethene ND ug/kg 07/28/22 02:55 79-01-607/27/22 18:056.5 1.7 1
Trichlorofluoromethane ND ug/kg 07/28/22 02:55 75-69-407/27/22 18:056.5 3.6 1
1,2,3-Trichloropropane ND ug/kg 07/28/22 02:55 96-18-407/27/22 18:056.5 3.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/28/22 02:55 95-63-607/27/22 18:056.5 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 07/28/22 02:55 108-67-807/27/22 18:056.5 2.2 1
Vinyl acetate ND ug/kg 07/28/22 02:55 108-05-407/27/22 18:0565.3 4.8 1
Vinyl chloride ND ug/kg 07/28/22 02:55 75-01-407/27/22 18:0513.1 3.3 1
Xylene (Total)5.3J ug/kg 07/28/22 02:55 1330-20-707/27/22 18:0513.1 3.7 1
m&p-Xylene 5.3J ug/kg 07/28/22 02:55 179601-23-107/27/22 18:0513.1 4.5 1
o-Xylene ND ug/kg 07/28/22 02:55 95-47-607/27/22 18:056.5 2.9 1
Surrogates
Toluene-d8 (S)100 %07/28/22 02:55 2037-26-507/27/22 18:0570-130 1
4-Bromofluorobenzene (S)99 %07/28/22 02:55 460-00-407/27/22 18:0569-134 1
1,2-Dichloroethane-d4 (S)106 %07/28/22 02:55 17060-07-007/27/22 18:0570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.3 %07/27/22 18:55 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-14 Lab ID:92616845008 Collected:07/22/22 13:30 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 08/01/22 12:26 83-32-907/28/22 18:024311521
Acenaphthylene ND ug/kg 08/01/22 12:26 208-96-807/28/22 18:024311521
Aniline ND ug/kg 08/01/22 12:26 62-53-307/28/22 18:024311691
Anthracene ND ug/kg 08/01/22 12:26 120-12-707/28/22 18:024311411
Benzo(a)anthracene ND ug/kg 08/01/22 12:26 56-55-307/28/22 18:024311441
Benzo(a)pyrene ND ug/kg 08/01/22 12:26 50-32-807/28/22 18:024311491
Benzo(b)fluoranthene ND ug/kg 08/01/22 12:26 205-99-207/28/22 18:024311441
Benzo(g,h,i)perylene ND ug/kg 08/01/22 12:26 191-24-207/28/22 18:024311671
Benzo(k)fluoranthene ND ug/kg 08/01/22 12:26 207-08-907/28/22 18:024311521
Benzoic Acid ND ug/kg 08/01/22 12:26 65-85-007/28/22 18:0221609271
Benzyl alcohol ND ug/kg 08/01/22 12:26 100-51-607/28/22 18:028633271
4-Bromophenylphenyl ether ND ug/kg 08/01/22 12:26 101-55-307/28/22 18:024311661
Butylbenzylphthalate ND ug/kg 08/01/22 12:26 85-68-707/28/22 18:024311821
4-Chloro-3-methylphenol ND ug/kg 08/01/22 12:26 59-50-707/28/22 18:028633031
4-Chloroaniline ND ug/kg 08/01/22 12:26 106-47-807/28/22 18:028633391
bis(2-Chloroethoxy)methane ND ug/kg 08/01/22 12:26 111-91-107/28/22 18:024311791
bis(2-Chloroethyl) ether ND ug/kg 08/01/22 12:26 111-44-407/28/22 18:024311621
2-Chloronaphthalene ND ug/kg 08/01/22 12:26 91-58-707/28/22 18:024311711
2-Chlorophenol ND ug/kg 08/01/22 12:26 95-57-807/28/22 18:024311621
4-Chlorophenylphenyl ether ND ug/kg 08/01/22 12:26 7005-72-307/28/22 18:024311611
Chrysene ND ug/kg 08/01/22 12:26 218-01-907/28/22 18:024311571
Dibenz(a,h)anthracene ND ug/kg 08/01/22 12:26 53-70-307/28/22 18:024311661
Dibenzofuran ND ug/kg 08/01/22 12:26 132-64-907/28/22 18:024311561
1,2-Dichlorobenzene ND ug/kg 08/01/22 12:26 95-50-107/28/22 18:024311561
1,3-Dichlorobenzene ND ug/kg 08/01/22 12:26 541-73-107/28/22 18:024311531
1,4-Dichlorobenzene ND ug/kg 08/01/22 12:26 106-46-707/28/22 18:024311651
3,3'-Dichlorobenzidine ND ug/kg 08/01/22 12:26 91-94-107/28/22 18:028632921
2,4-Dichlorophenol ND ug/kg 08/01/22 12:26 120-83-207/28/22 18:024311691
Diethylphthalate ND ug/kg 08/01/22 12:26 84-66-207/28/22 18:024311581
2,4-Dimethylphenol ND ug/kg 08/01/22 12:26 105-67-907/28/22 18:024311791
Dimethylphthalate ND ug/kg 08/01/22 12:26 131-11-307/28/22 18:024311571
Di-n-butylphthalate ND ug/kg 08/01/22 12:26 84-74-207/28/22 18:024311451
4,6-Dinitro-2-methylphenol ND ug/kg 08/01/22 12:26 534-52-107/28/22 18:028634031
2,4-Dinitrophenol ND ug/kg 08/01/22 12:26 51-28-507/28/22 18:02216013301
2,4-Dinitrotoluene ND ug/kg 08/01/22 12:26 121-14-207/28/22 18:024311661
2,6-Dinitrotoluene ND ug/kg 08/01/22 12:26 606-20-207/28/22 18:024311581
Di-n-octylphthalate ND ug/kg 08/01/22 12:26 117-84-007/28/22 18:024311701
bis(2-Ethylhexyl)phthalate ND ug/kg 08/01/22 12:26 117-81-707/28/22 18:024311671
Fluoranthene ND ug/kg 08/01/22 12:26 206-44-007/28/22 18:024311481
Fluorene ND ug/kg 08/01/22 12:26 86-73-707/28/22 18:024311521
Hexachloro-1,3-butadiene ND ug/kg 08/01/22 12:26 87-68-307/28/22 18:024311871
Hexachlorobenzene ND ug/kg 08/01/22 12:26 118-74-107/28/22 18:024311691
Hexachlorocyclopentadiene ND ug/kg 08/01/22 12:26 77-47-407/28/22 18:024312471
Hexachloroethane ND ug/kg 08/01/22 12:26 67-72-107/28/22 18:024311651
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-14 Lab ID:92616845008 Collected:07/22/22 13:30 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 08/01/22 12:26 193-39-507/28/22 18:024311701
Isophorone ND ug/kg 08/01/22 12:26 78-59-107/28/22 18:024311921
1-Methylnaphthalene ND ug/kg 08/01/22 12:26 90-12-007/28/22 18:024311521
2-Methylnaphthalene ND ug/kg 08/01/22 12:26 91-57-607/28/22 18:024311731
2-Methylphenol(o-Cresol)ND ug/kg 08/01/22 12:26 95-48-707/28/22 18:024311771
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/01/22 12:26 15831-10-407/28/22 18:024311741
Naphthalene ND ug/kg 08/01/22 12:26 91-20-307/28/22 18:024311461
2-Nitroaniline ND ug/kg 08/01/22 12:26 88-74-407/28/22 18:0221603531
3-Nitroaniline ND ug/kg 08/01/22 12:26 99-09-207/28/22 18:0221603391
4-Nitroaniline ND ug/kg 08/01/22 12:26 100-01-607/28/22 18:028633281
Nitrobenzene ND ug/kg 08/01/22 12:26 98-95-307/28/22 18:024312001
2-Nitrophenol ND ug/kg 08/01/22 12:26 88-75-507/28/22 18:024311871
4-Nitrophenol ND ug/kg 08/01/22 12:26 100-02-707/28/22 18:0221608341
N-Nitrosodimethylamine ND ug/kg 08/01/22 12:26 62-75-907/28/22 18:024311451
N-Nitroso-di-n-propylamine ND ug/kg 08/01/22 12:26 621-64-707/28/22 18:024311621
N-Nitrosodiphenylamine ND ug/kg 08/01/22 12:26 86-30-607/28/22 18:024311531
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/01/22 12:26 108-60-107/28/22 18:024312051
Pentachlorophenol ND ug/kg 08/01/22 12:26 87-86-507/28/22 18:028634221
Phenanthrene ND ug/kg 08/01/22 12:26 85-01-807/28/22 18:024311411
Phenol ND ug/kg 08/01/22 12:26 108-95-207/28/22 18:024311921
Pyrene ND ug/kg 08/01/22 12:26 129-00-007/28/22 18:024311751
Pyridine ND ug/kg 08/01/22 12:26 110-86-107/28/22 18:024311361
1,2,4-Trichlorobenzene ND ug/kg 08/01/22 12:26 120-82-107/28/22 18:024311701
2,4,5-Trichlorophenol ND ug/kg 08/01/22 12:26 95-95-407/28/22 18:024311971
2,4,6-Trichlorophenol ND ug/kg 08/01/22 12:26 88-06-207/28/22 18:024311781
Surrogates
Nitrobenzene-d5 (S)57 %08/01/22 12:26 4165-60-007/28/22 18:0221-130 1
2-Fluorobiphenyl (S)38 %08/01/22 12:26 321-60-807/28/22 18:0219-130 1
Terphenyl-d14 (S)41 %08/01/22 12:26 1718-51-007/28/22 18:0215-130 1
Phenol-d6 (S)60 %08/01/22 12:26 13127-88-307/28/22 18:0218-130 1
2-Fluorophenol (S)58 %08/01/22 12:26 367-12-407/28/22 18:0218-130 1
2,4,6-Tribromophenol (S)62 %08/01/22 12:26 118-79-607/28/22 18:0218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/28/22 03:14 67-64-107/27/22 18:0514747.0 1
Benzene ND ug/kg 07/28/22 03:14 71-43-207/27/22 18:057.3 2.9 1
Bromobenzene ND ug/kg 07/28/22 03:14 108-86-107/27/22 18:057.3 2.4 1
Bromochloromethane ND ug/kg 07/28/22 03:14 74-97-507/27/22 18:057.3 2.2 1
Bromodichloromethane ND ug/kg 07/28/22 03:14 75-27-407/27/22 18:057.3 2.8 1
Bromoform ND ug/kg 07/28/22 03:14 75-25-207/27/22 18:057.3 2.6 1
Bromomethane ND ug/kg 07/28/22 03:14 74-83-9 IK,L107/27/22 18:0514.7 11.6 1
2-Butanone (MEK)57.1J ug/kg 07/28/22 03:14 78-93-3 C707/27/22 18:0514735.2 1
n-Butylbenzene ND ug/kg 07/28/22 03:14 104-51-807/27/22 18:057.3 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-14 Lab ID:92616845008 Collected:07/22/22 13:30 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
sec-Butylbenzene ND ug/kg 07/28/22 03:14 135-98-807/27/22 18:057.3 3.2 1
tert-Butylbenzene ND ug/kg 07/28/22 03:14 98-06-607/27/22 18:057.3 2.6 1
Carbon tetrachloride ND ug/kg 07/28/22 03:14 56-23-507/27/22 18:057.3 2.7 1
Chlorobenzene ND ug/kg 07/28/22 03:14 108-90-707/27/22 18:057.3 1.4 1
Chloroethane ND ug/kg 07/28/22 03:14 75-00-307/27/22 18:0514.7 5.7 1
Chloroform ND ug/kg 07/28/22 03:14 67-66-307/27/22 18:057.3 4.5 1
Chloromethane ND ug/kg 07/28/22 03:14 74-87-307/27/22 18:0514.7 6.2 1
2-Chlorotoluene ND ug/kg 07/28/22 03:14 95-49-807/27/22 18:057.3 2.6 1
4-Chlorotoluene ND ug/kg 07/28/22 03:14 106-43-407/27/22 18:057.3 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/28/22 03:14 96-12-8 IK,v207/27/22 18:057.3 2.8 1
Dibromochloromethane ND ug/kg 07/28/22 03:14 124-48-107/27/22 18:057.3 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/28/22 03:14 106-93-407/27/22 18:057.3 3.2 1
Dibromomethane ND ug/kg 07/28/22 03:14 74-95-307/27/22 18:057.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/28/22 03:14 95-50-107/27/22 18:057.3 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/28/22 03:14 541-73-107/27/22 18:057.3 2.3 1
1,4-Dichlorobenzene ND ug/kg 07/28/22 03:14 106-46-707/27/22 18:057.3 1.9 1
Dichlorodifluoromethane ND ug/kg 07/28/22 03:14 75-71-8 IH,v107/27/22 18:0514.7 3.2 1
1,1-Dichloroethane ND ug/kg 07/28/22 03:14 75-34-307/27/22 18:057.3 3.0 1
1,2-Dichloroethane ND ug/kg 07/28/22 03:14 107-06-207/27/22 18:057.3 4.9 1
1,1-Dichloroethene ND ug/kg 07/28/22 03:14 75-35-407/27/22 18:057.3 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/28/22 03:14 156-59-207/27/22 18:057.3 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/28/22 03:14 156-60-507/27/22 18:057.3 2.6 1
1,2-Dichloropropane ND ug/kg 07/28/22 03:14 78-87-507/27/22 18:057.3 2.2 1
1,3-Dichloropropane ND ug/kg 07/28/22 03:14 142-28-907/27/22 18:057.3 2.3 1
2,2-Dichloropropane ND ug/kg 07/28/22 03:14 594-20-707/27/22 18:057.3 2.4 1
1,1-Dichloropropene ND ug/kg 07/28/22 03:14 563-58-607/27/22 18:057.3 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/28/22 03:14 10061-01-507/27/22 18:057.3 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/28/22 03:14 10061-02-607/27/22 18:057.3 2.5 1
Diisopropyl ether ND ug/kg 07/28/22 03:14 108-20-307/27/22 18:057.3 2.0 1
Ethylbenzene ND ug/kg 07/28/22 03:14 100-41-407/27/22 18:057.3 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 03:14 87-68-307/27/22 18:0514.7 12.0 1
2-Hexanone ND ug/kg 07/28/22 03:14 591-78-607/27/22 18:0573.3 7.1 1
Isopropylbenzene (Cumene)ND ug/kg 07/28/22 03:14 98-82-807/27/22 18:057.3 2.5 1
p-Isopropyltoluene ND ug/kg 07/28/22 03:14 99-87-607/27/22 18:057.3 3.6 1
Methylene Chloride 73.8 ug/kg 07/28/22 03:14 75-09-2 C907/27/22 18:0529.3 20.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/28/22 03:14 108-10-107/27/22 18:0573.3 7.1 1
Methyl-tert-butyl ether ND ug/kg 07/28/22 03:14 1634-04-407/27/22 18:057.3 2.7 1
Naphthalene ND ug/kg 07/28/22 03:14 91-20-3 v207/27/22 18:057.3 3.9 1
n-Propylbenzene ND ug/kg 07/28/22 03:14 103-65-107/27/22 18:057.3 2.6 1
Styrene ND ug/kg 07/28/22 03:14 100-42-507/27/22 18:057.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/28/22 03:14 630-20-607/27/22 18:057.3 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/28/22 03:14 79-34-507/27/22 18:057.3 1.9 1
Tetrachloroethene ND ug/kg 07/28/22 03:14 127-18-407/27/22 18:057.3 2.3 1
Toluene ND ug/kg 07/28/22 03:14 108-88-307/27/22 18:057.3 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616845
Mock Judson 1533
Sample:SS-14 Lab ID:92616845008 Collected:07/22/22 13:30 Received:07/26/22 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichlorobenzene ND ug/kg 07/28/22 03:14 87-61-6 IK,L2,v207/27/22 18:057.3 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 03:14 120-82-107/27/22 18:057.3 6.2 1
1,1,1-Trichloroethane ND ug/kg 07/28/22 03:14 71-55-607/27/22 18:057.3 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/28/22 03:14 79-00-507/27/22 18:057.3 2.4 1
Trichloroethene ND ug/kg 07/28/22 03:14 79-01-607/27/22 18:057.3 1.9 1
Trichlorofluoromethane ND ug/kg 07/28/22 03:14 75-69-407/27/22 18:057.3 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/28/22 03:14 96-18-407/27/22 18:057.3 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/28/22 03:14 95-63-607/27/22 18:057.3 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/28/22 03:14 108-67-807/27/22 18:057.3 2.5 1
Vinyl acetate ND ug/kg 07/28/22 03:14 108-05-407/27/22 18:0573.3 5.3 1
Vinyl chloride ND ug/kg 07/28/22 03:14 75-01-407/27/22 18:0514.7 3.7 1
Xylene (Total)ND ug/kg 07/28/22 03:14 1330-20-707/27/22 18:0514.7 4.2 1
m&p-Xylene ND ug/kg 07/28/22 03:14 179601-23-107/27/22 18:0514.7 5.0 1
o-Xylene ND ug/kg 07/28/22 03:14 95-47-607/27/22 18:057.3 3.2 1
Surrogates
Toluene-d8 (S)100 %07/28/22 03:14 2037-26-507/27/22 18:0570-130 1
4-Bromofluorobenzene (S)98 %07/28/22 03:14 460-00-407/27/22 18:0569-134 1
1,2-Dichloroethane-d4 (S)110 %07/28/22 03:14 17060-07-007/27/22 18:0570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.8 %07/27/22 18:56 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713314
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616845006, 92616845007, 92616845008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3719271
Associated Lab Samples:92616845006, 92616845007, 92616845008
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/28/22 00:451.9
1,1,1-Trichloroethane ug/kg ND 5.0 07/28/22 00:452.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/28/22 00:451.3
1,1,2-Trichloroethane ug/kg ND 5.0 07/28/22 00:451.7
1,1-Dichloroethane ug/kg ND 5.0 07/28/22 00:452.1
1,1-Dichloroethene ug/kg ND 5.0 07/28/22 00:452.1
1,1-Dichloropropene ug/kg ND 5.0 07/28/22 00:452.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 IK,v207/28/22 00:454.0
1,2,3-Trichloropropane ug/kg ND 5.0 07/28/22 00:452.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/28/22 00:454.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/28/22 00:451.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 IK,v207/28/22 00:451.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/28/22 00:452.2
1,2-Dichlorobenzene ug/kg ND 5.0 07/28/22 00:451.8
1,2-Dichloroethane ug/kg ND 5.0 07/28/22 00:453.3
1,2-Dichloropropane ug/kg ND 5.0 07/28/22 00:451.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/28/22 00:451.7
1,3-Dichlorobenzene ug/kg ND 5.0 07/28/22 00:451.6
1,3-Dichloropropane ug/kg ND 5.0 07/28/22 00:451.6
1,4-Dichlorobenzene ug/kg ND 5.0 07/28/22 00:451.3
2,2-Dichloropropane ug/kg ND 5.0 07/28/22 00:451.6
2-Butanone (MEK)ug/kg ND 100 07/28/22 00:4524.0
2-Chlorotoluene ug/kg ND 5.0 07/28/22 00:451.8
2-Hexanone ug/kg ND 50.0 07/28/22 00:454.8
4-Chlorotoluene ug/kg ND 5.0 07/28/22 00:450.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/28/22 00:454.8
Acetone ug/kg ND 100 07/28/22 00:4532.1
Benzene ug/kg ND 5.0 07/28/22 00:452.0
Bromobenzene ug/kg ND 5.0 07/28/22 00:451.6
Bromochloromethane ug/kg ND 5.0 07/28/22 00:451.5
Bromodichloromethane ug/kg ND 5.0 07/28/22 00:451.9
Bromoform ug/kg ND 5.0 07/28/22 00:451.8
Bromomethane ug/kg ND 10.0 IK07/28/22 00:457.9
Carbon tetrachloride ug/kg ND 5.0 07/28/22 00:451.9
Chlorobenzene ug/kg ND 5.0 07/28/22 00:450.96
Chloroethane ug/kg ND 10.0 07/28/22 00:453.9
Chloroform ug/kg 8.1 5.0 07/28/22 00:453.0
Chloromethane ug/kg ND 10.0 07/28/22 00:454.2
cis-1,2-Dichloroethene ug/kg ND 5.0 07/28/22 00:451.7
cis-1,3-Dichloropropene ug/kg ND 5.0 07/28/22 00:451.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3719271
Associated Lab Samples:92616845006, 92616845007, 92616845008
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 07/28/22 00:452.8
Dibromomethane ug/kg ND 5.0 07/28/22 00:451.1
Dichlorodifluoromethane ug/kg ND 10.0 IH,v107/28/22 00:452.2
Diisopropyl ether ug/kg ND 5.0 07/28/22 00:451.4
Ethylbenzene ug/kg ND 5.0 07/28/22 00:452.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/28/22 00:458.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/28/22 00:451.7
m&p-Xylene ug/kg ND 10.0 07/28/22 00:453.4
Methyl-tert-butyl ether ug/kg ND 5.0 07/28/22 00:451.9
Methylene Chloride ug/kg ND 20.0 07/28/22 00:4513.7
n-Butylbenzene ug/kg ND 5.0 07/28/22 00:452.4
n-Propylbenzene ug/kg ND 5.0 07/28/22 00:451.8
Naphthalene ug/kg ND 5.0 v207/28/22 00:452.6
o-Xylene ug/kg ND 5.0 07/28/22 00:452.2
p-Isopropyltoluene ug/kg ND 5.0 07/28/22 00:452.5
sec-Butylbenzene ug/kg ND 5.0 07/28/22 00:452.2
Styrene ug/kg ND 5.0 07/28/22 00:451.3
tert-Butylbenzene ug/kg ND 5.0 07/28/22 00:451.8
Tetrachloroethene ug/kg ND 5.0 07/28/22 00:451.6
Toluene ug/kg ND 5.0 07/28/22 00:451.4
trans-1,2-Dichloroethene ug/kg ND 5.0 07/28/22 00:451.8
trans-1,3-Dichloropropene ug/kg ND 5.0 07/28/22 00:451.7
Trichloroethene ug/kg ND 5.0 07/28/22 00:451.3
Trichlorofluoromethane ug/kg ND 5.0 07/28/22 00:452.8
Vinyl acetate ug/kg ND 50.0 07/28/22 00:453.6
Vinyl chloride ug/kg ND 10.0 07/28/22 00:452.5
Xylene (Total)ug/kg ND 10.0 07/28/22 00:452.8
1,2-Dichloroethane-d4 (S)%108 70-130 07/28/22 00:45
4-Bromofluorobenzene (S)%95 69-134 07/28/22 00:45
Toluene-d8 (S)%98 70-130 07/28/22 00:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3719272LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12701250 102 70-130
1,1,1-Trichloroethane ug/kg 11901250 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 11801250 94 70-130
1,1,2-Trichloroethane ug/kg 12101250 97 70-130
1,1-Dichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethene ug/kg 13001250 104 70-130
1,1-Dichloropropene ug/kg 12501250 100 70-130
1,2,3-Trichlorobenzene ug/kg 805 IK,L2,v312506465-130
1,2,3-Trichloropropane ug/kg 12101250 96 70-130
1,2,4-Trichlorobenzene ug/kg 10901250 87 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3719272LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13001250 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 1060 IK,v312508570-130
1,2-Dibromoethane (EDB)ug/kg 13101250 105 70-130
1,2-Dichlorobenzene ug/kg 12701250 101 70-130
1,2-Dichloroethane ug/kg 12501250 100 63-130
1,2-Dichloropropane ug/kg 12701250 102 70-130
1,3,5-Trimethylbenzene ug/kg 13501250 108 70-130
1,3-Dichlorobenzene ug/kg 12801250 102 70-130
1,3-Dichloropropane ug/kg 12901250 103 70-130
1,4-Dichlorobenzene ug/kg 12601250 101 70-130
2,2-Dichloropropane ug/kg 10501250 84 66-130
2-Butanone (MEK)ug/kg 21102500 84 70-130
2-Chlorotoluene ug/kg 13301250 107 70-130
2-Hexanone ug/kg 24402500 98 70-130
4-Chlorotoluene ug/kg 13301250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23902500 96 70-130
Acetone ug/kg 23602500 94 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 13101250 105 70-130
Bromochloromethane ug/kg 12001250 96 70-130
Bromodichloromethane ug/kg 12501250 100 69-130
Bromoform ug/kg 12401250 99 70-130
Bromomethane ug/kg 1750 IK,L1125014052-130
Carbon tetrachloride ug/kg 11601250 93 70-130
Chlorobenzene ug/kg 13001250 104 70-130
Chloroethane ug/kg 14501250 116 65-130
Chloroform ug/kg 12201250 98 70-130
Chloromethane ug/kg 15101250 121 55-130
cis-1,2-Dichloroethene ug/kg 12801250 103 70-130
cis-1,3-Dichloropropene ug/kg 12601250 101 70-130
Dibromochloromethane ug/kg 12801250 102 70-130
Dibromomethane ug/kg 12101250 97 70-130
Dichlorodifluoromethane ug/kg 1720 IH,v1125013845-156
Diisopropyl ether ug/kg 13001250 104 70-130
Ethylbenzene ug/kg 11801250 94 70-130
Hexachloro-1,3-butadiene ug/kg 11401250 92 66-130
Isopropylbenzene (Cumene)ug/kg 12001250 96 70-130
m&p-Xylene ug/kg 25102500 100 70-130
Methyl-tert-butyl ether ug/kg 11901250 95 70-130
Methylene Chloride ug/kg 13501250 108 65-130
n-Butylbenzene ug/kg 13201250 106 67-130
n-Propylbenzene ug/kg 13201250 106 70-130
Naphthalene ug/kg 913 v312507370-130
o-Xylene ug/kg 12101250 97 70-130
p-Isopropyltoluene ug/kg 13601250 109 67-130
sec-Butylbenzene ug/kg 13001250 104 69-130
Styrene ug/kg 12701250 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3719272LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13701250 109 67-130
Tetrachloroethene ug/kg 12601250 101 70-130
Toluene ug/kg 11301250 90 70-130
trans-1,2-Dichloroethene ug/kg 12801250 103 70-130
trans-1,3-Dichloropropene ug/kg 12501250 100 68-130
Trichloroethene ug/kg 12101250 97 70-130
Trichlorofluoromethane ug/kg 13301250 107 70-130
Vinyl acetate ug/kg 28002500 112 70-130
Vinyl chloride ug/kg 15101250 121 61-130
Xylene (Total)ug/kg 37203750 99 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3719273MATRIX SPIKE SAMPLE:
MSSpike
Result
92616346001
1,1,1,2-Tetrachloroethane ug/kg 661622 106 70-131ND
1,1,1-Trichloroethane ug/kg 701622 112 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 591622 95 66-130ND
1,1,2-Trichloroethane ug/kg 592622 95 66-133ND
1,1-Dichloroethane ug/kg 689622 111 65-130ND
1,1-Dichloroethene ug/kg 779622 125 10-158ND
1,1-Dichloropropene ug/kg 749622 120 68-133ND
1,2,3-Trichlorobenzene ug/kg 143 IK,M0,v36222327-138ND
1,2,3-Trichloropropane ug/kg 593622 95 67-130ND
1,2,4-Trichlorobenzene ug/kg 430622 69 51-134ND
1,2,4-Trimethylbenzene ug/kg 725622 116 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 426 IK,v36226832-130ND
1,2-Dibromoethane (EDB)ug/kg 630622 101 70-130ND
1,2-Dichlorobenzene ug/kg 675622 108 69-130ND
1,2-Dichloroethane ug/kg 644622 103 59-130ND
1,2-Dichloropropane ug/kg 685622 110 70-130ND
1,3,5-Trimethylbenzene ug/kg 730622 117 65-137ND
1,3-Dichlorobenzene ug/kg 687622 110 70-130ND
1,3-Dichloropropane ug/kg 655622 105 70-130ND
1,4-Dichlorobenzene ug/kg 690622 111 68-130ND
2,2-Dichloropropane ug/kg 579622 93 32-130ND
2-Butanone (MEK)ug/kg 10001240 77 10-136ND
2-Chlorotoluene ug/kg 712622 114 69-141ND
2-Hexanone ug/kg 11001240 88 10-144ND
4-Chlorotoluene ug/kg 716622 115 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 10701240 86 25-143ND
Acetone ug/kg 9841240 79 10-130ND
Benzene ug/kg 657622 105 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3719273MATRIX SPIKE SAMPLE:
MSSpike
Result
92616346001
Bromobenzene ug/kg 662622 106 70-130ND
Bromochloromethane ug/kg 609622 98 69-134ND
Bromodichloromethane ug/kg 626622 101 64-130ND
Bromoform ug/kg 571622 92 62-130ND
Bromomethane ug/kg 269 IK6224320-176ND
Carbon tetrachloride ug/kg 660622 106 65-140ND
Chlorobenzene ug/kg 707622 114 70-130ND
Chloroethane ug/kg 157622 25 10-130ND
Chloroform ug/kg 641622 102 63-130ND
Chloromethane ug/kg 930 M162214958-130ND
cis-1,2-Dichloroethene ug/kg 705622 113 66-130ND
cis-1,3-Dichloropropene ug/kg 644622 103 67-130ND
Dibromochloromethane ug/kg 614622 99 67-130ND
Dibromomethane ug/kg 571622 92 63-131ND
Dichlorodifluoromethane ug/kg 1130 IH,M1,v162218144-180ND
Diisopropyl ether ug/kg 711622 114 63-130ND
Ethylbenzene ug/kg 662622 105 66-130ND
Hexachloro-1,3-butadiene ug/kg 986 M162215864-150ND
Isopropylbenzene (Cumene)ug/kg 700622 112 69-135ND
m&p-Xylene ug/kg 14201240 113 60-133ND
Methyl-tert-butyl ether ug/kg 612622 98 65-130ND
Methylene Chloride ug/kg 773622 110 61-13086.1
n-Butylbenzene ug/kg 817622 131 65-140ND
n-Propylbenzene ug/kg 734622 118 67-140ND
Naphthalene ug/kg 141 v36222315-145ND
o-Xylene ug/kg 658622 104 66-1338.2
p-Isopropyltoluene ug/kg 795622 128 56-147ND
sec-Butylbenzene ug/kg 783622 126 65-139ND
Styrene ug/kg 669622 107 70-132ND
tert-Butylbenzene ug/kg 755622 121 62-135ND
Tetrachloroethene ug/kg 693622 111 70-135ND
Toluene ug/kg 626622 100 67-130ND
trans-1,2-Dichloroethene ug/kg 745622 120 69-130ND
trans-1,3-Dichloropropene ug/kg 615622 99 62-130ND
Trichloroethene ug/kg 666622 107 70-135ND
Trichlorofluoromethane ug/kg 173622 28 10-130ND
Vinyl acetate ug/kg 13601240 109 53-130ND
Vinyl chloride ug/kg 875622 140 61-148ND
Xylene (Total)ug/kg 20701860 111 63-132ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616796001
3719274SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND IK,v230ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND IK,v230ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 3052.6J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH,v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 4.8J 305.6J
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616796001
3719274SAMPLE DUPLICATE:
m&p-Xylene ug/kg 8.8J 309.4J
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 95.5 4 3091.6
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND v230ND
o-Xylene ug/kg 9.0 11 308.1
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 3.5J 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 9.0J 3017.5
1,2-Dichloroethane-d4 (S)%106107
4-Bromofluorobenzene (S)%9899
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713443
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616845001, 92616845002, 92616845003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3719631
Associated Lab Samples:92616845001, 92616845002, 92616845003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/28/22 13:450.31
1,1,1-Trichloroethane ug/L ND 1.0 07/28/22 13:450.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/28/22 13:450.22
1,1,2-Trichloroethane ug/L ND 1.0 07/28/22 13:450.32
1,1-Dichloroethane ug/L ND 1.0 07/28/22 13:450.37
1,1-Dichloroethene ug/L ND 1.0 07/28/22 13:450.35
1,1-Dichloropropene ug/L ND 1.0 07/28/22 13:450.43
1,2,3-Trichlorobenzene ug/L ND 1.0 07/28/22 13:450.81
1,2,3-Trichloropropane ug/L ND 1.0 07/28/22 13:450.26
1,2,4-Trichlorobenzene ug/L ND 1.0 07/28/22 13:450.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/28/22 13:450.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/22 13:450.27
1,2-Dichlorobenzene ug/L ND 1.0 07/28/22 13:450.34
1,2-Dichloroethane ug/L ND 1.0 07/28/22 13:450.32
1,2-Dichloropropane ug/L ND 1.0 07/28/22 13:450.36
1,3-Dichlorobenzene ug/L ND 1.0 07/28/22 13:450.34
1,3-Dichloropropane ug/L ND 1.0 07/28/22 13:450.28
1,4-Dichlorobenzene ug/L ND 1.0 07/28/22 13:450.33
2,2-Dichloropropane ug/L ND 1.0 07/28/22 13:450.39
2-Butanone (MEK)ug/L ND 5.0 07/28/22 13:454.0
2-Chlorotoluene ug/L ND 1.0 07/28/22 13:450.32
2-Hexanone ug/L ND 5.0 07/28/22 13:450.48
4-Chlorotoluene ug/L ND 1.0 07/28/22 13:450.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/28/22 13:452.7
Acetone ug/L ND 25.0 07/28/22 13:455.1
Benzene ug/L ND 1.0 07/28/22 13:450.34
Bromobenzene ug/L ND 1.0 07/28/22 13:450.29
Bromochloromethane ug/L ND 1.0 07/28/22 13:450.47
Bromodichloromethane ug/L ND 1.0 07/28/22 13:450.31
Bromoform ug/L ND 1.0 07/28/22 13:450.34
Bromomethane ug/L ND 2.0 07/28/22 13:451.7
Carbon tetrachloride ug/L ND 1.0 07/28/22 13:450.33
Chlorobenzene ug/L ND 1.0 07/28/22 13:450.28
Chloroethane ug/L ND 1.0 07/28/22 13:450.65
Chloroform ug/L ND 1.0 07/28/22 13:450.43
Chloromethane ug/L ND 1.0 07/28/22 13:450.54
cis-1,2-Dichloroethene ug/L ND 1.0 07/28/22 13:450.38
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/22 13:450.36
Dibromochloromethane ug/L ND 1.0 07/28/22 13:450.36
Dibromomethane ug/L ND 1.0 07/28/22 13:450.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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Page 36 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3719631
Associated Lab Samples:92616845001, 92616845002, 92616845003
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 07/28/22 13:450.35
Diisopropyl ether ug/L ND 1.0 07/28/22 13:450.31
Ethylbenzene ug/L ND 1.0 07/28/22 13:450.30
Hexachloro-1,3-butadiene ug/L ND 2.0 07/28/22 13:451.5
m&p-Xylene ug/L ND 2.0 07/28/22 13:450.71
Methyl-tert-butyl ether ug/L ND 1.0 07/28/22 13:450.42
Methylene Chloride ug/L ND 5.0 07/28/22 13:452.0
Naphthalene ug/L ND 1.0 07/28/22 13:450.64
o-Xylene ug/L ND 1.0 07/28/22 13:450.34
p-Isopropyltoluene ug/L ND 1.0 07/28/22 13:450.41
Styrene ug/L ND 1.0 07/28/22 13:450.29
Tetrachloroethene ug/L ND 1.0 07/28/22 13:450.29
Toluene ug/L ND 1.0 07/28/22 13:450.48
trans-1,2-Dichloroethene ug/L ND 1.0 07/28/22 13:450.40
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/22 13:450.36
Trichloroethene ug/L ND 1.0 07/28/22 13:450.38
Trichlorofluoromethane ug/L ND 1.0 07/28/22 13:450.30
Vinyl acetate ug/L ND 2.0 07/28/22 13:451.3
Vinyl chloride ug/L ND 1.0 07/28/22 13:450.39
Xylene (Total)ug/L ND 1.0 07/28/22 13:450.34
1,2-Dichloroethane-d4 (S)%106 70-130 07/28/22 13:45
4-Bromofluorobenzene (S)%100 70-130 07/28/22 13:45
Toluene-d8 (S)%99 70-130 07/28/22 13:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3719632LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 70-130
1,1,1-Trichloroethane ug/L 46.750 93 70-130
1,1,2,2-Tetrachloroethane ug/L 48.050 96 70-130
1,1,2-Trichloroethane ug/L 47.150 94 70-130
1,1-Dichloroethane ug/L 45.150 90 70-130
1,1-Dichloroethene ug/L 44.650 89 70-132
1,1-Dichloropropene ug/L 49.250 98 70-131
1,2,3-Trichlorobenzene ug/L 44.550 89 70-134
1,2,3-Trichloropropane ug/L 46.150 92 70-130
1,2,4-Trichlorobenzene ug/L 46.350 93 70-130
1,2-Dibromo-3-chloropropane ug/L 46.650 93 70-132
1,2-Dibromoethane (EDB)ug/L 49.150 98 70-130
1,2-Dichlorobenzene ug/L 48.750 97 70-130
1,2-Dichloroethane ug/L 47.050 94 70-130
1,2-Dichloropropane ug/L 45.050 90 70-130
1,3-Dichlorobenzene ug/L 47.450 95 70-130
1,3-Dichloropropane ug/L 48.850 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3719632LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 47.950 96 70-130
2,2-Dichloropropane ug/L 48.450 97 70-130
2-Butanone (MEK)ug/L 94.2100 94 70-133
2-Chlorotoluene ug/L 48.250 96 70-130
2-Hexanone ug/L 99.2100 99 70-130
4-Chlorotoluene ug/L 47.650 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 91.1100 91 70-130
Acetone ug/L 86.9100 87 70-144
Benzene ug/L 43.550 87 70-130
Bromobenzene ug/L 46.050 92 70-130
Bromochloromethane ug/L 49.050 98 70-130
Bromodichloromethane ug/L 46.150 92 70-130
Bromoform ug/L 50.650 101 70-131
Bromomethane ug/L 44.150 88 30-177
Carbon tetrachloride ug/L 48.650 97 70-130
Chlorobenzene ug/L 47.650 95 70-130
Chloroethane ug/L 51.150 102 46-131
Chloroform ug/L 43.950 88 70-130
Chloromethane ug/L 47.250 94 49-130
cis-1,2-Dichloroethene ug/L 45.650 91 70-130
cis-1,3-Dichloropropene ug/L 47.650 95 70-130
Dibromochloromethane ug/L 48.850 98 70-130
Dibromomethane ug/L 45.950 92 70-130
Dichlorodifluoromethane ug/L 54.750 109 52-134
Diisopropyl ether ug/L 46.850 94 70-131
Ethylbenzene ug/L 47.750 95 70-130
Hexachloro-1,3-butadiene ug/L 49.250 98 70-131
m&p-Xylene ug/L 97.3100 97 70-130
Methyl-tert-butyl ether ug/L 46.450 93 70-130
Methylene Chloride ug/L 43.150 86 68-130
Naphthalene ug/L 46.950 94 70-133
o-Xylene ug/L 49.450 99 70-130
p-Isopropyltoluene ug/L 50.950 102 70-130
Styrene ug/L 49.950 100 70-130
Tetrachloroethene ug/L 47.050 94 70-130
Toluene ug/L 44.250 88 70-130
trans-1,2-Dichloroethene ug/L 46.350 93 70-130
trans-1,3-Dichloropropene ug/L 47.550 95 70-130
Trichloroethene ug/L 47.650 95 70-130
Trichlorofluoromethane ug/L 45.050 90 61-130
Vinyl acetate ug/L 95.0100 95 70-140
Vinyl chloride ug/L 52.550 105 59-142
Xylene (Total)ug/L 147150 98 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3719633MATRIX SPIKE SAMPLE:
MSSpike
Result
92616845001
1,1,1,2-Tetrachloroethane ug/L 25.720 128 70-135ND
1,1,1-Trichloroethane ug/L 26.020 130 70-148ND
1,1,2,2-Tetrachloroethane ug/L 24.820 124 70-131ND
1,1,2-Trichloroethane ug/L 24.320 121 70-136ND
1,1-Dichloroethane ug/L 24.920 124 70-147ND
1,1-Dichloroethene ug/L 25.720 128 70-158ND
1,1-Dichloropropene ug/L 27.620 138 70-149ND
1,2,3-Trichlorobenzene ug/L 22.720 113 68-140ND
1,2,3-Trichloropropane ug/L 23.020 115 67-137ND
1,2,4-Trichlorobenzene ug/L 23.620 118 70-139ND
1,2-Dibromo-3-chloropropane ug/L 20.820 104 69-136ND
1,2-Dibromoethane (EDB)ug/L 25.220 126 70-137ND
1,2-Dichlorobenzene ug/L 24.920 125 70-133ND
1,2-Dichloroethane ug/L 26.420 132 67-138ND
1,2-Dichloropropane ug/L 24.920 124 70-138ND
1,3-Dichlorobenzene ug/L 24.120 121 70-133ND
1,3-Dichloropropane ug/L 24.920 125 70-136ND
1,4-Dichlorobenzene ug/L 24.420 122 70-133ND
2,2-Dichloropropane ug/L 27.120 135 52-155ND
2-Butanone (MEK)ug/L 55.740 139 61-147ND
2-Chlorotoluene ug/L 24.720 124 70-141ND
2-Hexanone ug/L 54.940 137 67-139ND
4-Chlorotoluene ug/L 24.720 123 70-135ND
4-Methyl-2-pentanone (MIBK)ug/L 50.440 126 67-136ND
Acetone ug/L 55.740 139 55-159ND
Benzene ug/L 23.520 117 67-150ND
Bromobenzene ug/L 23.620 118 70-134ND
Bromochloromethane ug/L 27.020 135 70-146ND
Bromodichloromethane ug/L 24.220 121 70-138ND
Bromoform ug/L 19.620 98 57-138ND
Bromomethane ug/L 23.2 v32011610-200ND
Carbon tetrachloride ug/L 25.120 126 70-147ND
Chlorobenzene ug/L 24.520 123 70-137ND
Chloroethane ug/L 31.920 160 51-166ND
Chloroform ug/L 24.620 123 70-144ND
Chloromethane ug/L 27.820 139 24-161ND
cis-1,2-Dichloroethene ug/L 25.120 125 67-148ND
cis-1,3-Dichloropropene ug/L 23.820 119 70-142ND
Dibromochloromethane ug/L 22.420 112 68-138ND
Dibromomethane ug/L 23.320 117 70-134ND
Dichlorodifluoromethane ug/L 33.0 M12016543-155ND
Diisopropyl ether ug/L 26.720 133 65-146ND
Ethylbenzene ug/L 25.320 127 68-143ND
Hexachloro-1,3-butadiene ug/L 24.320 121 62-151ND
m&p-Xylene ug/L 50.140 125 53-157ND
Methyl-tert-butyl ether ug/L 25.120 126 59-156ND
Methylene Chloride ug/L 22.420 112 64-148ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3719633MATRIX SPIKE SAMPLE:
MSSpike
Result
92616845001
Naphthalene ug/L 22.920 115 57-150ND
o-Xylene ug/L 25.220 126 68-143ND
p-Isopropyltoluene ug/L 26.020 130 70-141ND
Styrene ug/L 25.420 127 70-136ND
Tetrachloroethene ug/L 23.720 119 70-139ND
Toluene ug/L 23.520 118 47-157ND
trans-1,2-Dichloroethene ug/L 27.020 135 70-149ND
trans-1,3-Dichloropropene ug/L 24.120 120 70-138ND
Trichloroethene ug/L 24.020 120 70-149ND
Trichlorofluoromethane ug/L 27.320 137 61-154ND
Vinyl acetate ug/L 53.640 134 48-156ND
Vinyl chloride ug/L 30.320 152 55-172ND
Xylene (Total)ug/L 75.360 126 66-145ND
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616845002
3719634SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L 0.57J 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 27.9 D6953078.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616845002
3719634SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108104
4-Bromofluorobenzene (S)%101100
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713767
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616845001, 92616845002, 92616845003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3721298
Associated Lab Samples:92616845001, 92616845002, 92616845003
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 07/30/22 09:441.7
1,2-Dichlorobenzene ug/L ND 10.0 07/30/22 09:441.8
1,3-Dichlorobenzene ug/L ND 10.0 07/30/22 09:441.6
1,4-Dichlorobenzene ug/L ND 10.0 07/30/22 09:441.7
1-Methylnaphthalene ug/L ND 10.0 07/30/22 09:442.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/30/22 09:441.2
2,4,5-Trichlorophenol ug/L ND 10.0 07/30/22 09:441.4
2,4,6-Trichlorophenol ug/L ND 10.0 07/30/22 09:441.6
2,4-Dichlorophenol ug/L ND 10.0 07/30/22 09:441.4
2,4-Dimethylphenol ug/L ND 10.0 07/30/22 09:441.7
2,4-Dinitrophenol ug/L ND 50.0 07/30/22 09:4426.0
2,4-Dinitrotoluene ug/L ND 10.0 07/30/22 09:441.6
2,6-Dinitrotoluene ug/L ND 10.0 07/30/22 09:441.7
2-Chloronaphthalene ug/L ND 10.0 07/30/22 09:441.7
2-Chlorophenol ug/L ND 10.0 07/30/22 09:441.2
2-Methylnaphthalene ug/L ND 10.0 07/30/22 09:441.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/30/22 09:441.9
2-Nitroaniline ug/L ND 20.0 07/30/22 09:443.0
2-Nitrophenol ug/L ND 10.0 07/30/22 09:441.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/30/22 09:441.2
3,3'-Dichlorobenzidine ug/L ND 20.0 07/30/22 09:448.1
3-Nitroaniline ug/L ND 20.0 07/30/22 09:443.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/30/22 09:447.8
4-Bromophenylphenyl ether ug/L ND 10.0 07/30/22 09:441.8
4-Chloro-3-methylphenol ug/L ND 10.0 07/30/22 09:443.3
4-Chloroaniline ug/L ND 20.0 07/30/22 09:443.6
4-Chlorophenylphenyl ether ug/L ND 10.0 07/30/22 09:442.0
4-Nitroaniline ug/L ND 20.0 v207/30/22 09:445.1
4-Nitrophenol ug/L ND 50.0 07/30/22 09:446.6
Acenaphthene ug/L ND 10.0 07/30/22 09:442.0
Acenaphthylene ug/L ND 10.0 07/30/22 09:442.0
Aniline ug/L ND 10.0 07/30/22 09:441.6
Anthracene ug/L ND 10.0 07/30/22 09:442.3
Benzo(a)anthracene ug/L ND 10.0 07/30/22 09:442.7
Benzo(a)pyrene ug/L ND 10.0 07/30/22 09:442.8
Benzo(b)fluoranthene ug/L ND 10.0 07/30/22 09:442.6
Benzo(g,h,i)perylene ug/L ND 10.0 07/30/22 09:442.8
Benzo(k)fluoranthene ug/L ND 10.0 07/30/22 09:442.7
Benzoic Acid ug/L ND 50.0 07/30/22 09:4422.0
Benzyl alcohol ug/L ND 20.0 07/30/22 09:442.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3721298
Associated Lab Samples:92616845001, 92616845002, 92616845003
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/30/22 09:441.8
bis(2-Chloroethyl) ether ug/L ND 10.0 07/30/22 09:441.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/30/22 09:443.7
Butylbenzylphthalate ug/L ND 10.0 07/30/22 09:443.1
Chrysene ug/L ND 10.0 07/30/22 09:442.8
Di-n-butylphthalate ug/L ND 10.0 07/30/22 09:442.2
Di-n-octylphthalate ug/L ND 10.0 07/30/22 09:443.9
Dibenz(a,h)anthracene ug/L ND 10.0 07/30/22 09:443.0
Dibenzofuran ug/L ND 10.0 07/30/22 09:442.1
Diethylphthalate ug/L ND 10.0 07/30/22 09:442.0
Dimethylphthalate ug/L ND 10.0 07/30/22 09:442.1
Fluoranthene ug/L ND 10.0 07/30/22 09:442.2
Fluorene ug/L ND 10.0 07/30/22 09:442.1
Hexachloro-1,3-butadiene ug/L ND 10.0 07/30/22 09:441.8
Hexachlorobenzene ug/L ND 10.0 07/30/22 09:442.2
Hexachlorocyclopentadiene ug/L ND 10.0 07/30/22 09:441.6
Hexachloroethane ug/L ND 10.0 07/30/22 09:441.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/30/22 09:442.9
Isophorone ug/L ND 10.0 07/30/22 09:441.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/30/22 09:441.3
N-Nitrosodimethylamine ug/L ND 10.0 07/30/22 09:441.9
N-Nitrosodiphenylamine ug/L ND 10.0 07/30/22 09:443.0
Naphthalene ug/L ND 10.0 07/30/22 09:442.1
Nitrobenzene ug/L ND 10.0 07/30/22 09:441.9
Pentachlorophenol ug/L ND 20.0 07/30/22 09:443.8
Phenanthrene ug/L ND 10.0 07/30/22 09:442.0
Phenol ug/L 25.8 10.0 C907/30/22 09:441.4
Pyrene ug/L ND 10.0 07/30/22 09:442.2
2,4,6-Tribromophenol (S)%106 10-144 07/30/22 09:44
2-Fluorobiphenyl (S)%92 10-130 07/30/22 09:44
2-Fluorophenol (S)%76 10-130 07/30/22 09:44
Nitrobenzene-d5 (S)%122 10-144 07/30/22 09:44
Phenol-d6 (S)%60 10-130 07/30/22 09:44
Terphenyl-d14 (S)%147 34-163 07/30/22 09:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3721299LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 39.850 80 18-130
1,2-Dichlorobenzene ug/L 28.750 57 20-130
1,3-Dichlorobenzene ug/L 25.350 51 18-130
1,4-Dichlorobenzene ug/L 26.750 53 18-130
1-Methylnaphthalene ug/L 46.150 92 29-130
2,2'-Oxybis(1-chloropropane)ug/L 31.250 62 28-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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Page 43 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3721299LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 54.550 109 35-130
2,4,6-Trichlorophenol ug/L 53.450 107 31-130
2,4-Dichlorophenol ug/L 51.950 104 35-130
2,4-Dimethylphenol ug/L 62.350 125 34-130
2,4-Dinitrophenol ug/L 198250 79 10-153
2,4-Dinitrotoluene ug/L 51.050 102 37-136
2,6-Dinitrotoluene ug/L 56.550 113 33-136
2-Chloronaphthalene ug/L 48.550 97 26-130
2-Chlorophenol ug/L 41.850 84 37-130
2-Methylnaphthalene ug/L 45.650 91 29-130
2-Methylphenol(o-Cresol)ug/L 44.150 88 35-130
2-Nitroaniline ug/L 115100 115 37-130
2-Nitrophenol ug/L 47.250 94 32-130
3&4-Methylphenol(m&p Cresol)ug/L 47.550 95 34-130
3,3'-Dichlorobenzidine ug/L 105100 105 34-136
3-Nitroaniline ug/L 106100 106 37-138
4,6-Dinitro-2-methylphenol ug/L 112100 112 21-157
4-Bromophenylphenyl ether ug/L 57.150 114 38-130
4-Chloro-3-methylphenol ug/L 112100 112 37-130
4-Chloroaniline ug/L 96.0100 96 38-130
4-Chlorophenylphenyl ether ug/L 51.350 103 33-130
4-Nitroaniline ug/L 93.5 v31009442-137
4-Nitrophenol ug/L 160250 64 10-130
Acenaphthene ug/L 47.750 95 33-130
Acenaphthylene ug/L 48.950 98 35-130
Aniline ug/L 39.150 78 22-130
Anthracene ug/L 47.150 94 48-130
Benzo(a)anthracene ug/L 54.450 109 48-137
Benzo(a)pyrene ug/L 67.150 134 49-138
Benzo(b)fluoranthene ug/L 73.1 L15014652-138
Benzo(g,h,i)perylene ug/L 60.050 120 48-140
Benzo(k)fluoranthene ug/L 72.5 L15014548-139
Benzoic Acid ug/L 39.6J250 16 10-130
Benzyl alcohol ug/L 93.3100 93 35-130
bis(2-Chloroethoxy)methane ug/L 52.250 104 34-130
bis(2-Chloroethyl) ether ug/L 48.650 97 36-130
bis(2-Ethylhexyl)phthalate ug/L 61.350 123 32-165
Butylbenzylphthalate ug/L 67.450 135 34-161
Chrysene ug/L 52.250 104 47-131
Di-n-butylphthalate ug/L 56.850 114 39-144
Di-n-octylphthalate ug/L 57.150 114 30-170
Dibenz(a,h)anthracene ug/L 58.650 117 49-138
Dibenzofuran ug/L 50.750 101 33-130
Diethylphthalate ug/L 53.450 107 38-131
Dimethylphthalate ug/L 52.950 106 37-130
Fluoranthene ug/L 53.350 107 46-137
Fluorene ug/L 49.350 99 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3721299LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 36.550 73 11-130
Hexachlorobenzene ug/L 53.650 107 38-130
Hexachlorocyclopentadiene ug/L 44.550 89 10-130
Hexachloroethane ug/L 23.850 48 14-130
Indeno(1,2,3-cd)pyrene ug/L 62.350 125 41-130
Isophorone ug/L 55.850 112 33-130
N-Nitroso-di-n-propylamine ug/L 54.050 108 36-130
N-Nitrosodimethylamine ug/L 41.450 83 34-130
N-Nitrosodiphenylamine ug/L 54.150 108 37-130
Naphthalene ug/L 39.350 79 30-130
Nitrobenzene ug/L 52.150 104 36-130
Pentachlorophenol ug/L 113100 113 23-149
Phenanthrene ug/L 51.550 103 44-130
Phenol ug/L 52.350 105 18-130
Pyrene ug/L 62.550 125 47-134
2,4,6-Tribromophenol (S)%126 10-144
2-Fluorobiphenyl (S)%92 10-130
2-Fluorophenol (S)%74 10-130
Nitrobenzene-d5 (S)%110 10-144
Phenol-d6 (S)%65 10-130
Terphenyl-d14 (S)%147 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3721300MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441008
3721301
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 25 10-13019 30100ND24.7 18.9J
1,2-Dichlorobenzene ug/L 100 21 10-13015 30100ND20.5 14.6J
1,3-Dichlorobenzene ug/L 100 17 10-13011 30100ND16.8J 11.4J
1,4-Dichlorobenzene ug/L 100 18 10-13013 30100ND18.1J 12.8J
1-Methylnaphthalene ug/L R11004410-13030 38 30100ND43.9 29.8
2,2'-Oxybis(1-chloropropane)ug/L R11003312-14222 41 30100ND32.9 21.8
2,4,5-Trichlorophenol ug/L R11008610-14361 35 30100ND86.1 60.7
2,4,6-Trichlorophenol ug/L R11008110-14746 55 30100ND80.8 46.1
2,4-Dichlorophenol ug/L R11005710-13832 55 30100ND57.1 32.3
2,4-Dimethylphenol ug/L R11007525-13043 54 30100ND75.4 43.4
2,4-Dinitrophenol ug/L 500 50 10-16540 24 30500ND252198
2,4-Dinitrotoluene ug/L R11007329-14852 34 30100ND72.7 51.8
2,6-Dinitrotoluene ug/L 100 85 26-14670 19 30100ND85.4 70.2
2-Chloronaphthalene ug/L R11005711-13034 51 30100ND56.7 33.6
2-Chlorophenol ug/L R11004410-13329 40 30100ND43.9 29.1
2-Methylnaphthalene ug/L R11004013-13029 34 30100ND40.5 28.7
2-Methylphenol(o-Cresol)ug/L R11004620-13029 44 30100ND45.7 29.3
2-Nitroaniline ug/L 200 85 24-13667 24 30200ND171133
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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Page 45 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3721300MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441008
3721301
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L R11005110-15332 46 30100ND50.6 31.6
3&4-Methylphenol(m&p
Cresol)ug/L R11005016-13029 52 30100ND49.8 29.1
3,3'-Dichlorobenzidine ug/L 200 94 10-15398 4 30200ND188195
3-Nitroaniline ug/L 200 80 22-15179 1 30200ND159158
4,6-Dinitro-2-methylphenol ug/L 200 86 10-18084 2 30200ND172168
4-Bromophenylphenyl ether ug/L 100 89 25-13067 28 30100ND89.0 67.3
4-Chloro-3-methylphenol ug/L R12007525-13349 42 30200ND14997.0
4-Chloroaniline ug/L R12005614-13233 52 30200ND11365.9
4-Chlorophenylphenyl ether ug/L R11007419-13050 39 30100ND73.7 49.7
4-Nitroaniline ug/L v32007729-15085 10 30200ND155171
4-Nitrophenol ug/L 500 42 10-13048 13 30500ND208238
Acenaphthene ug/L R11006316-13036 54 30100ND62.9 36.2
Acenaphthylene ug/L R11006515-13736 56 30100ND65.1 36.5
Aniline ug/L R11004110-13027 42 30100ND40.8 26.6
Anthracene ug/L 100 76 37-13670 9 30100ND76.4 69.9
Benzo(a)anthracene ug/L 100 94 40-14592 2 30100ND94.3 92.4
Benzo(a)pyrene ug/L 100 113 41-146111 1 30100ND113111
Benzo(b)fluoranthene ug/L 100 116 39-151112 4 30100ND116112
Benzo(g,h,i)perylene ug/L 100 107 40-147120 11 30100ND107120
Benzo(k)fluoranthene ug/L 100 113 40-146121 7 30100ND113121
Benzoic Acid ug/L M1500510-1300 30500NDNDND
Benzyl alcohol ug/L R12004825-13031 42 30200ND96.4 62.7
bis(2-Chloroethoxy)methane ug/L R11005523-13036 43 30100ND55.1 35.7
bis(2-Chloroethyl) ether ug/L R11005125-13034 39 30100ND50.8 34.3
bis(2-Ethylhexyl)phthalate ug/L 100 110 28-166105 5 30100ND110105
Butylbenzylphthalate ug/L 100 115 33-165110 4 30100ND115110
Chrysene ug/L 100 92 38-14190 2 30100ND91.8 90.4
Di-n-butylphthalate ug/L 100 94 32-15396 2 30100ND94.1 96.0
Di-n-octylphthalate ug/L 100 108 30-175108 0 30100ND108108
Dibenz(a,h)anthracene ug/L 100 100 39-148109 9 30100ND100109
Dibenzofuran ug/L R11007120-13043 50 30100ND71.2 42.8
Diethylphthalate ug/L 100 80 28-14281 0 30100ND80.5 80.9
Dimethylphthalate ug/L 100 81 26-13668 17 30100ND80.6 67.9
Fluoranthene ug/L 100 86 39-14390 5 30100ND85.8 90.5
Fluorene ug/L R11007124-13250 34 30100ND71.2 50.4
Hexachloro-1,3-butadiene ug/L 100 13 10-13012 30100ND13.4J 12.1J
Hexachlorobenzene ug/L 100 88 29-13071 22 30100ND88.3 71.1
Hexachlorocyclopentadiene ug/L R11003110-13020 41 30100ND31.0 20.4
Hexachloroethane ug/L M11001110-1308 30100ND11.4J 7.7J
Indeno(1,2,3-cd)pyrene ug/L 100 107 39-148118 9 30100ND107118
Isophorone ug/L R11006523-13037 54 30100ND64.6 37.3
N-Nitroso-di-n-propylamine ug/L R11005825-13037 44 30100ND57.9 37.0
N-Nitrosodimethylamine ug/L R11004322-13030 34 30100ND42.8 30.5
N-Nitrosodiphenylamine ug/L 100 88 26-13474 17 30100ND87.8 74.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3721300MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441008
3721301
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L R11003414-13024 34 30100ND33.5 23.8
Nitrobenzene ug/L R11005725-13036 45 30100ND57.3 36.1
Pentachlorophenol ug/L 200 86 10-17588 2 30200ND172175
Phenanthrene ug/L 100 82 36-13376 7 30100ND82.2 76.3
Phenol ug/L 100 27 10-13017 30100ND29.8 19.5J
Pyrene ug/L 100 102 40-14394 9 30100ND10293.8
2,4,6-Tribromophenol (S)%91 10-14481
2-Fluorobiphenyl (S)%51 10-13029
2-Fluorophenol (S)%36 10-13025
Nitrobenzene-d5 (S)%56 10-14435
Phenol-d6 (S)%30 10-13019
Terphenyl-d14 (S)%110 34-163102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
714075
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616845001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3722782
Associated Lab Samples:92616845001
Matrix:Water
AnalyzedMDL
Phenol ug/L ND 10.0 08/01/22 15:521.4
2,4,6-Tribromophenol (S)%11 10-144 08/01/22 15:52
2-Fluorobiphenyl (S)%74 10-130 08/01/22 15:52
2-Fluorophenol (S)%6 10-130 S008/01/22 15:52
Nitrobenzene-d5 (S)%79 10-144 08/01/22 15:52
Phenol-d6 (S)%22 10-130 08/01/22 15:52
Terphenyl-d14 (S)%86 34-163 08/01/22 15:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3722783LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol ug/L 33.450 67 18-130
2,4,6-Tribromophenol (S)%114 10-144
2-Fluorobiphenyl (S)%105 10-130
2-Fluorophenol (S)%78 10-130
Nitrobenzene-d5 (S)%107 10-144
Phenol-d6 (S)%65 10-130
Terphenyl-d14 (S)%128 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3722784MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441009
3722785
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol ug/L 41.7 32 10-13028 15 3041.7ND 13.5 11.6
2,4,6-Tribromophenol (S)%73 10-14484
2-Fluorobiphenyl (S)%46 10-13070
2-Fluorophenol (S)%29 10-13053
Nitrobenzene-d5 (S)%39 10-14467
Phenol-d6 (S)%26 10-13047
Terphenyl-d14 (S)%75 34-16389
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713605
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616845006, 92616845007, 92616845008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3720611
Associated Lab Samples:92616845006, 92616845007, 92616845008
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 328 07/29/22 14:27129
1,2-Dichlorobenzene ug/kg ND 328 07/29/22 14:27118
1,3-Dichlorobenzene ug/kg ND 328 07/29/22 14:27116
1,4-Dichlorobenzene ug/kg ND 328 07/29/22 14:27125
1-Methylnaphthalene ug/kg ND 328 07/29/22 14:27115
2,2'-Oxybis(1-chloropropane)ug/kg ND 328 07/29/22 14:27156
2,4,5-Trichlorophenol ug/kg ND 328 07/29/22 14:27150
2,4,6-Trichlorophenol ug/kg ND 328 07/29/22 14:27135
2,4-Dichlorophenol ug/kg ND 328 07/29/22 14:27128
2,4-Dimethylphenol ug/kg ND 328 07/29/22 14:27136
2,4-Dinitrophenol ug/kg ND 1640 07/29/22 14:271010
2,4-Dinitrotoluene ug/kg ND 328 07/29/22 14:27126
2,6-Dinitrotoluene ug/kg ND 328 07/29/22 14:27120
2-Chloronaphthalene ug/kg ND 328 07/29/22 14:27130
2-Chlorophenol ug/kg ND 328 07/29/22 14:27123
2-Methylnaphthalene ug/kg ND 328 07/29/22 14:27131
2-Methylphenol(o-Cresol)ug/kg ND 328 07/29/22 14:27134
2-Nitroaniline ug/kg ND 1640 07/29/22 14:27268
2-Nitrophenol ug/kg ND 328 07/29/22 14:27142
3&4-Methylphenol(m&p Cresol)ug/kg ND 328 07/29/22 14:27132
3,3'-Dichlorobenzidine ug/kg ND 656 07/29/22 14:27222
3-Nitroaniline ug/kg ND 1640 07/29/22 14:27257
4,6-Dinitro-2-methylphenol ug/kg ND 656 07/29/22 14:27306
4-Bromophenylphenyl ether ug/kg ND 328 07/29/22 14:27126
4-Chloro-3-methylphenol ug/kg ND 656 07/29/22 14:27230
4-Chloroaniline ug/kg ND 656 07/29/22 14:27257
4-Chlorophenylphenyl ether ug/kg ND 328 07/29/22 14:27122
4-Nitroaniline ug/kg ND 656 07/29/22 14:27249
4-Nitrophenol ug/kg ND 1640 07/29/22 14:27634
Acenaphthene ug/kg ND 328 07/29/22 14:27115
Acenaphthylene ug/kg ND 328 07/29/22 14:27115
Aniline ug/kg ND 328 07/29/22 14:27128
Anthracene ug/kg ND 328 07/29/22 14:27107
Benzo(a)anthracene ug/kg ND 328 07/29/22 14:27109
Benzo(a)pyrene ug/kg ND 328 07/29/22 14:27113
Benzo(b)fluoranthene ug/kg ND 328 07/29/22 14:27109
Benzo(g,h,i)perylene ug/kg ND 328 07/29/22 14:27127
Benzo(k)fluoranthene ug/kg ND 328 07/29/22 14:27115
Benzoic Acid ug/kg ND 1640 07/29/22 14:27704
Benzyl alcohol ug/kg ND 656 07/29/22 14:27248
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3720611
Associated Lab Samples:92616845006, 92616845007, 92616845008
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 328 07/29/22 14:27136
bis(2-Chloroethyl) ether ug/kg ND 328 07/29/22 14:27123
bis(2-Ethylhexyl)phthalate ug/kg ND 328 v107/29/22 14:27127
Butylbenzylphthalate ug/kg ND 328 07/29/22 14:27138
Chrysene ug/kg ND 328 07/29/22 14:27119
Di-n-butylphthalate ug/kg ND 328 07/29/22 14:27110
Di-n-octylphthalate ug/kg ND 328 v107/29/22 14:27129
Dibenz(a,h)anthracene ug/kg ND 328 07/29/22 14:27126
Dibenzofuran ug/kg ND 328 07/29/22 14:27118
Diethylphthalate ug/kg ND 328 07/29/22 14:27120
Dimethylphthalate ug/kg ND 328 07/29/22 14:27119
Fluoranthene ug/kg ND 328 07/29/22 14:27112
Fluorene ug/kg ND 328 07/29/22 14:27115
Hexachloro-1,3-butadiene ug/kg ND 328 07/29/22 14:27142
Hexachlorobenzene ug/kg ND 328 07/29/22 14:27128
Hexachlorocyclopentadiene ug/kg ND 328 07/29/22 14:27188
Hexachloroethane ug/kg ND 328 07/29/22 14:27125
Indeno(1,2,3-cd)pyrene ug/kg ND 328 07/29/22 14:27129
Isophorone ug/kg ND 328 07/29/22 14:27146
N-Nitroso-di-n-propylamine ug/kg ND 328 07/29/22 14:27123
N-Nitrosodimethylamine ug/kg ND 328 07/29/22 14:27110
N-Nitrosodiphenylamine ug/kg ND 328 07/29/22 14:27116
Naphthalene ug/kg ND 328 07/29/22 14:27111
Nitrobenzene ug/kg ND 328 07/29/22 14:27152
Pentachlorophenol ug/kg ND 656 07/29/22 14:27321
Phenanthrene ug/kg ND 328 07/29/22 14:27107
Phenol ug/kg ND 328 07/29/22 14:27146
Pyrene ug/kg ND 328 07/29/22 14:27133
Pyridine ug/kg ND 328 07/29/22 14:27103
2,4,6-Tribromophenol (S)%58 18-130 07/29/22 14:27
2-Fluorobiphenyl (S)%52 19-130 07/29/22 14:27
2-Fluorophenol (S)%54 18-130 07/29/22 14:27
Nitrobenzene-d5 (S)%52 21-130 07/29/22 14:27
Phenol-d6 (S)%55 18-130 07/29/22 14:27
Terphenyl-d14 (S)%62 15-130 07/29/22 14:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3720612LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 9981660 60 47-130
1,2-Dichlorobenzene ug/kg 10201660 61 49-130
1,3-Dichlorobenzene ug/kg 10101660 61 48-130
1,4-Dichlorobenzene ug/kg 9931660 60 49-130
1-Methylnaphthalene ug/kg 10501660 64 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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9800 Kincey Ave. Suite 100
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3720612LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 9251660 56 38-130
2,4,5-Trichlorophenol ug/kg 10401660 63 49-130
2,4,6-Trichlorophenol ug/kg 11501660 69 50-130
2,4-Dichlorophenol ug/kg 10701660 64 51-130
2,4-Dimethylphenol ug/kg 11401660 69 53-130
2,4-Dinitrophenol ug/kg 55708310 67 39-130
2,4-Dinitrotoluene ug/kg 11201660 67 53-130
2,6-Dinitrotoluene ug/kg 11601660 70 55-130
2-Chloronaphthalene ug/kg 10801660 65 48-130
2-Chlorophenol ug/kg 10901660 66 54-130
2-Methylnaphthalene ug/kg 10301660 62 57-130
2-Methylphenol(o-Cresol)ug/kg 10201660 62 50-130
2-Nitroaniline ug/kg 21003320 63 49-130
2-Nitrophenol ug/kg 11901660 72 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 10301660 62 50-130
3,3'-Dichlorobenzidine ug/kg 21103320 63 47-130
3-Nitroaniline ug/kg 22003320 66 45-130
4,6-Dinitro-2-methylphenol ug/kg 24903320 75 50-142
4-Bromophenylphenyl ether ug/kg 11601660 70 55-130
4-Chloro-3-methylphenol ug/kg 22003320 66 52-130
4-Chloroaniline ug/kg 21003320 63 49-130
4-Chlorophenylphenyl ether ug/kg 10501660 63 53-130
4-Nitroaniline ug/kg 21203320 64 51-130
4-Nitrophenol ug/kg 53208310 64 40-130
Acenaphthene ug/kg 11001660 66 56-130
Acenaphthylene ug/kg 11801660 71 58-130
Aniline ug/kg 8581660 52 44-130
Anthracene ug/kg 10401660 63 60-130
Benzo(a)anthracene ug/kg 11701660 71 59-130
Benzo(a)pyrene ug/kg 14101660 85 57-130
Benzo(b)fluoranthene ug/kg 13501660 81 54-130
Benzo(g,h,i)perylene ug/kg 10901660 66 59-130
Benzo(k)fluoranthene ug/kg 13301660 80 54-130
Benzoic Acid ug/kg 32408310 39 19-130
Benzyl alcohol ug/kg 20903320 63 50-130
bis(2-Chloroethoxy)methane ug/kg 10601660 64 55-130
bis(2-Chloroethyl) ether ug/kg 10201660 62 53-130
bis(2-Ethylhexyl)phthalate ug/kg 1360 v116608258-130
Butylbenzylphthalate ug/kg 13201660 80 46-138
Chrysene ug/kg 11301660 68 57-130
Di-n-butylphthalate ug/kg 11901660 72 57-130
Di-n-octylphthalate ug/kg 1340 v116608157-130
Dibenz(a,h)anthracene ug/kg 11301660 68 60-130
Dibenzofuran ug/kg 11001660 66 54-130
Diethylphthalate ug/kg 10801660 65 55-130
Dimethylphthalate ug/kg 10601660 64 57-130
Fluoranthene ug/kg 10801660 65 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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Huntersville, NC 28078
[phone]
Page 51 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3720612LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 10701660 64 56-130
Hexachloro-1,3-butadiene ug/kg 9061660 55 41-130
Hexachlorobenzene ug/kg 10701660 64 53-130
Hexachlorocyclopentadiene ug/kg 10901660 66 23-130
Hexachloroethane ug/kg 9801660 59 48-130
Indeno(1,2,3-cd)pyrene ug/kg 11001660 66 61-130
Isophorone ug/kg 9801660 59 49-130
N-Nitroso-di-n-propylamine ug/kg 10101660 61 52-130
N-Nitrosodimethylamine ug/kg 9521660 57 45-130
N-Nitrosodiphenylamine ug/kg 11601660 70 56-130
Naphthalene ug/kg 10401660 62 56-130
Nitrobenzene ug/kg 10401660 63 50-130
Pentachlorophenol ug/kg 23903320 72 33-130
Phenanthrene ug/kg 11301660 68 60-130
Phenol ug/kg 11401660 69 54-130
Pyrene ug/kg 12401660 75 61-130
Pyridine ug/kg 8251660 50 35-130
2,4,6-Tribromophenol (S)%64 18-130
2-Fluorobiphenyl (S)%56 19-130
2-Fluorophenol (S)%58 18-130
Nitrobenzene-d5 (S)%56 21-130
Phenol-d6 (S)%60 18-130
Terphenyl-d14 (S)%68 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3720613MATRIX SPIKE SAMPLE:
MSSpike
Result
92615607001
1,2,4-Trichlorobenzene ug/kg 8381770 47 22-130ND
1,2-Dichlorobenzene ug/kg 8561770 48 23-130ND
1,3-Dichlorobenzene ug/kg 8411770 47 26-130ND
1,4-Dichlorobenzene ug/kg 8321770 47 27-130ND
1-Methylnaphthalene ug/kg 9291770 52 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 7821770 44 30-130ND
2,4,5-Trichlorophenol ug/kg 10101770 57 26-130ND
2,4,6-Trichlorophenol ug/kg 10801770 61 23-130ND
2,4-Dichlorophenol ug/kg 9371770 53 29-130ND
2,4-Dimethylphenol ug/kg 9881770 56 13-130ND
2,4-Dinitrophenol ug/kg 61408850 69 10-131ND
2,4-Dinitrotoluene ug/kg 11301770 64 28-130ND
2,6-Dinitrotoluene ug/kg 11401770 65 36-130ND
2-Chloronaphthalene ug/kg 9461770 53 27-130ND
2-Chlorophenol ug/kg 9271770 52 29-130ND
2-Methylnaphthalene ug/kg 9021770 51 29-130ND
2-Methylphenol(o-Cresol)ug/kg 8861770 50 20-130ND
2-Nitroaniline ug/kg 20703540 58 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3720613MATRIX SPIKE SAMPLE:
MSSpike
Result
92615607001
2-Nitrophenol ug/kg 10201770 58 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 9091770 51 10-176ND
3,3'-Dichlorobenzidine ug/kg 20003540 56 15-130ND
3-Nitroaniline ug/kg 22003540 62 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 25203540 71 15-132ND
4-Bromophenylphenyl ether ug/kg 11001770 62 35-130ND
4-Chloro-3-methylphenol ug/kg 21703540 61 30-130ND
4-Chloroaniline ug/kg 18003540 51 28-130ND
4-Chlorophenylphenyl ether ug/kg 10101770 57 32-130ND
4-Nitroaniline ug/kg 21203540 60 30-130ND
4-Nitrophenol ug/kg 56008850 63 17-130ND
Acenaphthene ug/kg 10201770 58 29-130ND
Acenaphthylene ug/kg 11001770 62 31-130ND
Aniline ug/kg 6011770 34 10-130ND
Anthracene ug/kg 10401770 58 33-130ND
Benzo(a)anthracene ug/kg 11701770 66 32-130ND
Benzo(a)pyrene ug/kg 13701770 77 32-130ND
Benzo(b)fluoranthene ug/kg 13001770 73 33-130ND
Benzo(g,h,i)perylene ug/kg 11301770 64 28-130ND
Benzo(k)fluoranthene ug/kg 12501770 71 31-130ND
Benzoic Acid ug/kg 53308850 60 10-130ND
Benzyl alcohol ug/kg 18703540 53 31-130ND
bis(2-Chloroethoxy)methane ug/kg 8841770 50 30-130ND
bis(2-Chloroethyl) ether ug/kg 861 M117704968-130ND
bis(2-Ethylhexyl)phthalate ug/kg 1320 v117707440-130ND
Butylbenzylphthalate ug/kg 12901770 73 40-130ND
Chrysene ug/kg 11301770 64 30-130ND
Di-n-butylphthalate ug/kg 12001770 68 41-130ND
Di-n-octylphthalate ug/kg 1370 v117707742-130ND
Dibenz(a,h)anthracene ug/kg 11201770 63 27-130ND
Dibenzofuran ug/kg 10601770 60 32-130ND
Diethylphthalate ug/kg 11001770 62 40-130ND
Dimethylphthalate ug/kg 10501770 59 37-130ND
Fluoranthene ug/kg 11101770 63 26-130ND
Fluorene ug/kg 10501770 59 31-130ND
Hexachloro-1,3-butadiene ug/kg 7581770 43 20-130ND
Hexachlorobenzene ug/kg 10401770 59 29-130ND
Hexachlorocyclopentadiene ug/kg 8841770 50 10-130ND
Hexachloroethane ug/kg 8221770 46 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 11401770 64 28-130ND
Isophorone ug/kg 9021770 51 32-130ND
N-Nitroso-di-n-propylamine ug/kg 8991770 51 31-130ND
N-Nitrosodimethylamine ug/kg 8001770 45 20-130ND
N-Nitrosodiphenylamine ug/kg 11101770 63 32-130ND
Naphthalene ug/kg 8721770 49 30-130ND
Nitrobenzene ug/kg 8691770 49 25-130ND
Pentachlorophenol ug/kg 24503540 69 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3720613MATRIX SPIKE SAMPLE:
MSSpike
Result
92615607001
Phenanthrene ug/kg 11101770 63 34-130ND
Phenol ug/kg 9731770 55 14-130ND
Pyrene ug/kg 11701770 66 31-130ND
Pyridine ug/kg 4631770 26 10-130ND
2,4,6-Tribromophenol (S)%62 18-130
2-Fluorobiphenyl (S)%47 19-130
2-Fluorophenol (S)%46 18-130
Nitrobenzene-d5 (S)%45 21-130
Phenol-d6 (S)%49 18-130
Terphenyl-d14 (S)%61 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615607002
3720614SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615607002
3720614SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND v130ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND v130ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%7272
2-Fluorobiphenyl (S)%6363
2-Fluorophenol (S)%6665
Nitrobenzene-d5 (S)%6566
Phenol-d6 (S)%7068
Terphenyl-d14 (S)%7067
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616845
Mock Judson 1533
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713328
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616845006, 92616845007, 92616845008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616328002
3719304SAMPLE DUPLICATE:
Percent Moisture %19.9 N282518.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616845008
3719305SAMPLE DUPLICATE:
Percent Moisture %25.9 N252524.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 91
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92616845
Mock Judson 1533
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte is a possible laboratory contaminant (not present in method blank).C7
Common Laboratory Contaminant.C9
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Extraction or preparation conducted outside EPA method holding time.H2
Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result shouldbe considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 91
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92616845
Mock Judson 1533
ANALYTE QUALIFIERS
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 91
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92616845
Mock Judson 1533
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92616845001 713767 713977MW-6 EPA 3510C EPA 8270E
92616845001 714075 714221MW-6 EPA 3510C EPA 8270E
92616845002 713767 713977MW-7 EPA 3510C EPA 8270E
92616845003 713767 713977MW-8 EPA 3510C EPA 8270E
92616845006 713605 713716SS-12 EPA 3546 EPA 8270E
92616845007 713605 713716SS-13 EPA 3546 EPA 8270E
92616845008 713605 713716SS-14 EPA 3546 EPA 8270E
92616845006 713314 713410SS-12 EPA 5035A/5030B EPA 8260D
92616845007 713314 713410SS-13 EPA 5035A/5030B EPA 8260D
92616845008 713314 713410SS-14 EPA 5035A/5030B EPA 8260D
92616845001 713443MW-6 EPA 8260D
92616845002 713443MW-7 EPA 8260D
92616845003 713443MW-8 EPA 8260D
92616845006 713328SS-12 SW-846
92616845007 713328SS-13 SW-846
92616845008 713328SS-14 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/07/2022 08:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 91
Page 60 of 91
Page 61 of 91
Page 62 of 91
08/05/22
Technical Report for
Pace Analytical
92616845, Mock Judson 1533, NC
Workorder: 92616845 PO# AMB 92616845
SGS Job Number: JD49021
Sampling Date: 07/22/22
Report to:
Pace Analytical
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
[e-mail]
ATTN: Angela Baioni
Total number of pages in report:
Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC,
OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA(68-00408), RI, SC, TX, UT, VA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Victoria Pushkova 732-329-0200
David Chastain
General Manager
Dayton, NJ 08/05/22
e-Hardcopy 2.0
Automated Report
15
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 15
JD49021
Page 63 of 91
Table of Contents
-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3
Section 2: Summary of Hits .................................................................................................... 4
Section 3: Sample Results ........................................................................................................5
3.1: JD49021-1: SS-12 ......................................................................................................... 6
3.2: JD49021-2: SS-13 ......................................................................................................... 7
3.3: JD49021-3: SS-14 ......................................................................................................... 8
Section 4: Misc. Forms ............................................................................................................9
4.1: Chain of Custody ........................................................................................................... 10
Section 5: General Chemistry - QC Data Summaries .......................................................... 12
5.1: Method Blank and Spike Results Summary .................................................................. 13
5.2: Duplicate Results Summary .......................................................................................... 14
5.3: Matrix Spike Results Summary ..................................................................................... 15 123452 of 15
JD49021
Page 64 of 91
SGS North America Inc.
Sample Summary
Pace Analytical
Job No:JD49021
92616845, Mock Judson 1533, NC
Project No: Workorder: 92616845 PO# AMB 92616845
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
JD49021-1 07/22/22 12:15 07/28/22 SO Solid SS-12
JD49021-2 07/22/22 13:10 07/28/22 SO Solid SS-13
JD49021-3 07/22/22 13:30 07/28/22 SO Solid SS-14
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 15
JD490211Page 65 of 91
Summary of Hits Page 1 of 1
Job Number:JD49021
Account:Pace Analytical
Project:92616845, Mock Judson 1533, NC
Collected:07/22/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD49021-1 SS-12
Chromium, Hexavalent 1.3 0.61 mg/kg SW846 3060A/7199
JD49021-2 SS-13
Chromium, Hexavalent 1.4 0.61 mg/kg SW846 3060A/7199
JD49021-3 SS-14
Chromium, Hexavalent 0.71 0.59 mg/kg SW846 3060A/7199
4 of 15
JD490212Page 66 of 91
SGS North America Inc.
Sample Results
Report of Analysis
Dayton, NJ
Section 3
5 of 15
JD490213Page 67 of 91
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SS-12
Lab Sample ID:JD49021-1 Date Sampled:07/22/22
Matrix:SO - Solid Date Received:07/28/22
Percent Solids:67.2
Project:92616845, Mock Judson 1533, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent 1.3 0.61 mg/kg 1 08/02/22 11:59 RI SW846 3060A/7199
Solids, Percent 67.2 % 1 08/01/22 16:20 BG SM2540 G 18TH ED MOD
RL = Reporting Limit
6 of 15
JD4902133.1Page 68 of 91
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SS-13
Lab Sample ID:JD49021-2 Date Sampled:07/22/22
Matrix:SO - Solid Date Received:07/28/22
Percent Solids:65.4
Project:92616845, Mock Judson 1533, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent 1.4 0.61 mg/kg 1 08/02/22 12:15 RI SW846 3060A/7199
Solids, Percent 65.4 % 1 08/01/22 16:20 BG SM2540 G 18TH ED MOD
RL = Reporting Limit
7 of 15
JD4902133.2Page 69 of 91
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SS-14
Lab Sample ID:JD49021-3 Date Sampled:07/22/22
Matrix:SO - Solid Date Received:07/28/22
Percent Solids:68.7
Project:92616845, Mock Judson 1533, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent 0.71 0.59 mg/kg 1 08/02/22 12:54 RI SW846 3060A/7199
Solids, Percent 68.7 % 1 08/01/22 16:20 BG SM2540 G 18TH ED MOD
RL = Reporting Limit
8 of 15
JD4902133.3Page 70 of 91
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Dayton, NJ
Section 4
9 of 15
JD490214Page 71 of 91
)utotGhain of Custody
PASI Charlotte Laboratory €ct"*:5]6l -?sn- [ttV
I [llt illl illI lllil ill[ilnxffiillflt
Workorder:926'16845 Workorder Name:Mock Judson 1533 Rssults Rcqsssted By:
R.porl r lnvolc. To ffint.ctTo d AialY!it
Angela Baioni
Pace Analytical Charlotte
9800 KinceyAve. Suite'100
Huntersville, NC 28078
Phone [phone]
Email: angela.baioni@pac€labs.com
State ot Sample Origin: NC
<G3
ACcu-+est'y1-35 \ls-\3DT:ag+on,N: ot.q
1Vl--b2 q-o?-,oO
I o__
f.ffi.vtdJ--;6in.n-
c5
t
LAB USE ONLYItams.lnpl.lD L.b lO .iilx
g
E
5
1 SSI2 7 l2Z2O22 12:15 92616845006 Solid x D5
2 SS.13 7 l2Z2O22 13:10 926'16845007 Solid x
3 SS-14 7 12212022 13.30 92616845008 Solid X
4
5
Taanafg16 Released By D.teITlme Rocoivod By n OrtolTlme
ut1K?,t?A(r,- tur-)hthr z€Ja.o')unl? 4.
2 r,l,e./\t,
3 \
Cooler TemDerature on Receipt Y"c I Custodv Seal Y or N I Recsived on lce tt or N Samples lntact Y or N
t
1
3
ffilry)
Wedresday. Jlly 27 20221:31).O5 PM
2-t-zz-
PO.
2-Q\le
JD49021: Chain of Custody
Page 1 of 2
10 of 15
JD4902144.1Page 72 of 91
Job Number:JD49021 Client:PACE ANALYTICAL
Date / Time Received:7/28/2022 9:48:00 AM Delivery Method:
Project:92616845
4. No. Coolers:1
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (Bag)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.8);
Cooler 1: (2.4);
SM089-03Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:231619 pH 12+:203117A Other: (Specify)
JD49021: Chain of Custody
Page 2 of 2
11 of 15
JD4902144.1Page 73 of 91
SGS North America Inc.
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Method Blank and Blank Spike Summaries
• Duplicate Summaries
• Matrix Spike Summaries
Dayton, NJ
Section 5
12 of 15
JD490215Page 74 of 91
METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: JD49021
Account: PACENC - Pace Analytical
Project: 92616845, Mock Judson 1533, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chromium, Hexavalent GP41499/GN31914 0.40 0.0 mg/kg 40 39.9 99.8 80-120%
Chromium, Hexavalent GP41499/GN31914 mg/kg 940 891 94.8 80-120%
Chromium, Hexavalent GP41499/GN31914 mg/kg 154 89.5 58.1 46-95%
Associated Samples:
Batch GP41499: JD49021-1, JD49021-2, JD49021-3
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
13 of 15
JD4902155.1Page 75 of 91
DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: JD49021
Account: PACENC - Pace Analytical
Project: 92616845, Mock Judson 1533, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Chromium, Hexavalent GP41499/GN31914 JD49022-1 mg/kg 0.85 0.79 7.3 0-20%
Solids, Percent GN31849 JD48964-21 % 93.6 93.2 0.4 0-5%
Associated Samples:
Batch GN31849: JD49021-1, JD49021-2, JD49021-3
Batch GP41499: JD49021-1, JD49021-2, JD49021-3
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
14 of 15
JD4902155.2Page 76 of 91
MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: JD49021
Account: PACENC - Pace Analytical
Project: 92616845, Mock Judson 1533, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chromium, Hexavalent GP41499/GN31914 JD49022-1 mg/kg 0.85 938 897 95.5(a) 75-125%
Chromium, Hexavalent GP41499/GN31914 JD49022-1 mg/kg 0.85 49.3 51.0 101.6(b) 75-125%
Associated Samples:
Batch GP41499: JD49021-1, JD49021-2, JD49021-3
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(a) Good recovery on insoluble XCR matrix spike. See additional comments on soluble matrix spike recovery.
(b) Good recovery on soluble XCR matrix spike. Good recovery (103.2%) on the post-spike.
__________________________________________________________________________________________________________________________
Page 1
15 of 15
JD4902155.3Page 77 of 91
ANALYTICAL REPORT
August 17, 2022
Pace Analytical - Huntersville, NC
Sample Delivery Group:L1519482
Samples Received:07/28/2022
Project Number:92616845
Description:Mock Johnson 1533
Site:001
Report To:Angela Baioni
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
August 17, 2022
[Preliminary Report]
Christl M Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Huntersville, NC 92616845 L1519482 08/17/22 17:19 1 of 14
August 18, 2022
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Huntersville, NC 92616845 L1519482 08/18/22 11:01 1 of 14
Page 78 of 91
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-6 L1519482-01 5
MW-7 L1519482-02 6
MW-8 L1519482-03 7
MW-2 L1519482-04 8
MW-3 L1519482-05 9
Qc: Quality Control Summary 10
Wet Chemistry by Method 7199 10
Gl: Glossary of Terms 12
Al: Accreditations & Locations 13
Sc: Sample Chain of Custody 14
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 79 of 91
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-6 L1519482-01 GW 07/22/22 12:10 07/28/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 7199 WG1911276 1 08/16/22 10:56 08/16/22 10:56 ARD Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-7 L1519482-02 GW 07/22/22 13:10 07/28/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 7199 WG1911276 1 08/16/22 11:04 08/16/22 11:04 ARD Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-8 L1519482-03 GW 07/22/22 14:20 07/28/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 7199 WG1911276 5 08/16/22 11:11 08/16/22 11:11 ARD Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1519482-04 GW 07/22/22 16:10 07/28/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 7199 WG1911276 1 08/16/22 11:19 08/16/22 11:19 ARD Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1519482-05 GW 07/22/22 16:55 07/28/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 7199 WG1911276 1 08/16/22 11:27 08/16/22 11:27 ARD Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 80 of 91
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Christl M Wagner
Project Manager
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1519482-05 MW-3 7199
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 81 of 91
SAMPLE RESULTS - 01
L1519482
MW-6
Collected date/time: 07/22/22 12:10
Wet Chemistry by Method 7199
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexavalent Chromium-Low
Level 1.57 0.0400 0.100 1 08/16/2022 10:56 WG1911276
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 82 of 91
SAMPLE RESULTS - 02
L1519482
MW-7
Collected date/time: 07/22/22 13:10
Wet Chemistry by Method 7199
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexavalent Chromium-Low
Level 0.0764 J 0.0400 0.100 1 08/16/2022 11:04 WG1911276
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 83 of 91
SAMPLE RESULTS - 03
L1519482
MW-8
Collected date/time: 07/22/22 14:20
Wet Chemistry by Method 7199
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexavalent Chromium-Low
Level 0.437 J 0.200 0.500 5 08/16/2022 11:11 WG1911276
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 84 of 91
SAMPLE RESULTS - 04
L1519482
MW-2
Collected date/time: 07/22/22 16:10
Wet Chemistry by Method 7199
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexavalent Chromium-Low
Level U 0.0400 0.100 1 08/16/2022 11:19 WG1911276
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 85 of 91
SAMPLE RESULTS - 05
L1519482
MW-3
Collected date/time: 07/22/22 16:55
Wet Chemistry by Method 7199
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexavalent Chromium-Low
Level U Q 0.0400 0.100 1 08/16/2022 11:27 WG1911276
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 86 of 91
QUALITY CONTROL SUMMARYWG1911276
Wet Chemistry by Method 7199 L1519482-01,02,03,04,05
Method Blank (MB)
(MB) R3827358-1 08/16/22 07:26
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Hexavalent Chromium-Low
Level U 0.0400 0.100
L1519079-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1519079-01 08/16/22 09:31 • (DUP) R3827358-5 08/16/22 09:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Hexavalent Chromium-Low
Level U U 1 0.000 20
L1523143-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1523143-01 08/16/22 12:36 • (DUP) R3827358-7 08/16/22 12:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Hexavalent Chromium-Low
Level U U 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3827358-2 08/16/22 07:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Hexavalent Chromium-Low
Level 0.500 0.492 98.3 90.0-110
L1519071-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1519071-01 08/16/22 09:06 • (MS) R3827358-3 08/16/22 09:16 • (MSD) R3827358-4 08/16/22 09:24
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Hexavalent Chromium-Low Level 1.00 U 1.02 1.02 102 102 1 90.0-110 0.00163 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 87 of 91
QUALITY CONTROL SUMMARYWG1911276
Wet Chemistry by Method 7199 L1519482-01,02,03,04,05
L1523140-06 Original Sample (OS) • Matrix Spike (MS)
(OS) L1523140-06 08/16/22 12:13 • (MS) R3827358-6 08/16/22 12:21
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Hexavalent Chromium-Low
Level 1.00 U 1.03 103 1 90.0-110
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 88 of 91
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical - Huntersville, NC 92616845 L1519482 08/17/22 17:19 13 of 14
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Pace Analytical - Huntersville, NC 92616845 L1519482 08/18/22 11:01 13 of 14
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