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HomeMy WebLinkAbout25094_Mock Judson Mill_SoilTransferRequest_20231024175-1 Venture Drive, Belville NC 28451 P:(910)371-5980 -A Woman Owned Business - License No. C-4762 October 24, 2023 Claire Sorrell Brownfields Project Manager 217 West Jones Street Raleigh, North Carolina 27603 Reference: Import Soil Sampling – Martin Marietta Salem Stone Quarry R1 Mock Judson Mill 2610 Oakland Avenue in Greensboro, North Carolina Brownfields Project Number 25094-21-041 Ms. Sorrell, Soil sampling has been conducted of the proposed imported fill to be used at the Former Mock Judson Mill site, located at 2610 Oakland Avenue in Greensboro, North Carolina. Mr. Kevin Dillon of Atlantic Shores Environmental Services, Ltd. (ASE) collected soil samples from virgin soil at the Martin Marietta Salem Stone Quarry (Permit Number 34-09) on September 19, 2023, in accordance with the Environmental Management Plan (EMP) for the site, dated September 29, 2022, and revised on December 13, 2022. The Martin Marietta Salem Stone Quarry (Salem Quarry) is located at 4572 High Point Road, in Kernersville, Forsyth County, North Carolina. The Salem Quarry is situated south of Interstate 74 and west of Highpoint Road, in the southeast corner of Forsyth County (see attached Figure 1). Operations at the Salem Quarry consist of excavation and removal of the upper-most layers of soil (cover), allowing access to the rock stata below. The rock is mined and resulting aggregates processed using a crusher to produce the final products. The removed cover, which does not have any significant value to the Salem Quarry, is sold for to various commercial and industrial entities. On September 19, 2023, ASE collected soil samples from the cover material, which is scheduled to be utilized as imported fill at the Former Mock Judson Mill site to bring the site up to final grade. Five (5) soil samples, including one (1) duplicate sample, were collected from four (4) locations (sample areas) at the Salem Quarry site (refer to Figure 2). Martin Marietta Salem Stone Quarry Sampling RI October 24, 2023 Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina Brownfields Project Number 25094-21-041 2 Samples were collected from ground surface to 1-foot below ground surface. The random sample locations were determined based on Salem Quarry estimates of where the cover excavation would be occurring the last two (2) weeks of October 2023. The soil samples were analyzed for the following analytes: • Volatile organic compounds (VOCs) by EPA method 8260D • Semi-volatile organic compounds (SVOCs) by EPA Method 8270E • Resource, Conservation and Recovery Act (RCRA) 8 Metals by EPA Method 6010/74711 • Hexavalent Chromium by EPA Method 7199 Each sample for SVOCs, and metals analyses was composited from aliquots taken from four (4) locations within each sample area, using a decontaminated stainless-steel spoon and bowl. The VOCs sample from each sample-area was collected as a discrete sample from the location of the fourth aliquot in each sample area. Samples for laboratory analysis were placed in laboratory prepared containers using new, disposable, nitrile gloves for each sample. After being filled, the sample containers were labeled with the project name and number, the time and date of sample collection, the analyses to be performed, and the absence or presence of preservative. The filled sample containers were placed into an ice filled cooler to maintain the samples at approximately 4° Celsius. A chain-of-custody was filled out and the samples were transported to ASE’s office where they were picked up by a Pace Analytical employee and delivered to Pace Analytical in Raleigh, North Carolina Sample collection was conducted in accordance with the North Carolina Department of Environmental Quality (NCDEQ) Inactive Hazardous Sites Program Guidelines for Assessment and Cleanup (September 2022). The samples were compared to the NCDEQ Preliminary Soil Remediation Goals (PSRGs), Residential Health Based PSRGs (July 2023). The results of laboratory analysis of the soil samples submitted is summarized in the attached Table 1. The Report of Laboratory Analysis and chain-of-custody record are attached. RCRA 8 Analysis Summary When submitting the soil samples for analysis, ASE personnel listed EPA Method 6020/7471 on the chain of custody. This request was forwarded from the Pace Analytical Raleigh, North Carolina Office’s project manager to the Pace Analytical satellite testing laboratory in Florida. However, the satellite testing laboratory analyzed the samples using EPA Method 6010 due to an apparent internal communication error within the satellite laboratory. The Pace Analytical Raleigh, North Carolina Office’s project manager indicated that Methods 6010 and 6020 are nearly identical, with Method 6020 having slightly lower method detection limits (MDLs), depending on the dry weight of the samples. Laboratory analysis indicated the presence of barium, cadmium, chromium, and lead in the soil samples below the Residential PSRGs for those analytes. 1 Varies from EMP – Reasoning discussed below Martin Marietta Salem Stone Quarry Sampling R1 October 24, 2023 Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina Brownfields Project Number 25094-21-041 Arsenic was not identified above the MDLs for the soil samples. However, the MDLs for arsenic were slightly above the Residential PSRG for that analyte in samples QS-1, QS-2, QS-4, and QS-4D. The alteration from EPA Method 7470A to 7471 occurred because EPA Method 7470A is an aqueous method, while EPA Method 7471 is a soil method. When preparing the Environmental Management Plan (EMP), ASE inadvertently indicated the aqueous method. During preparations for the imported soil sampling effort, ASE identified the error and requested the soil method (Method 7471) when submitting the soil samples for laboratory analysis. Mercury was not identified above the MDL in soil sample QS-1. Mercury was identified in soil samples QS-2, QS-3, QS-4, and QS-4D at concentrations well below the Residential PSRG for that analyte. SVOCs Analysis Summary SVOCs were not detected in any of the soil samples submitted to the laboratory for analysis. VOCs Analysis Summary Ethylbenzene was identified in soil samples QS-1 and QS-2 at concentrations well below Residential PSRGs. Methylene chloride was identified in soil sample QS-2 at a very low concentration. It should be noted that methylene chloride is a common laboratory contaminant. Toluene was identified in soil samples QS-1 and QS-2 at concentrations less than Residential PSRGs. Xylenes were identified in soil samples QS-1 and QS-2 at concentrations less than Residential PSRGs. Hexavalent Chromium Analysis Summary Hexavalent chromium was not detected in the soil samples submitted to the laboratory for analysis. Based on the analytical results of the soil samples, , ASE requests approval to utilize the Salem Quarry soil as imported fill for final grade at the Former Mock Judson Mill site. If there are questions regarding this report, or a need for further information, please contact us at 910-371- 5980. Sincerely, ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. Cheryl J. Moody, PE, REM Kevin Dillon, REP Principal Engineer Senior Project Manager Attachments: Table 1 Figure 1 Figure 2 Report of Laboratory Analysis and Chain-of-Custody Field Notes Martin Marietta Salem Stone Quarry Sampling RI October 24, 2023 Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina Brownfields Project Number 25094-21-041 FIGURES FIGURE 1: QUARRY LOCATION MAP Source: Google Maps 2020. Import Soil Sampling – Martin Marietta Salem Stone Quarry Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina N Brownfield No. 25094-21-041 October 2023 QS-1 QS-2 QS-3 QS-4 QS-4DSample Locations FIGURE 2: SAMPLE LOCATION MAP Source: Google Maps 2020. Import Soil Sampling – Martin Marietta Salem Stone Quarry Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina N Brownfield No. 25094-21-041 October 2023 QS-1 QS-2 QS-3 QS-4 QS-4D Martin Marietta Salem Stone Quarry Sampling R1 October 24, 2023 Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina Brownfields Project Number 25094-21-041 TABLES Sample ID QS-1 QS-2 QS-3 QS-4 QS-4D Depth (Feet)0-1 0-1 0-1 0-1 0-1 Lattitude 36.025813 36.025703 36.025767 36.025561 36.025561 Longitude -80.109612 -80.109937 -80.109314 -80.109796 -80.109796 Date 9/19/23 9/19/23 9/19/23 9/19/23 9/19/23 Ethylbenzene 0.008 0.0054J < 0.0030 < 0.0028 < 0.0035 6.1 Methylene Chloride*< 0.0196 0.0188J < 0.0178 < 0.0165 < 0.0208 58 Toluene 0.0169 0.0101 < 0.0045 < 0.0041 < 0.0052 990 Xylene (total)0.0234 0.0149 < 0.0037 < 0.0034 < 0.0043 120 m&p Xylene 0.0174 0.0111J < 0.0044 < 0.0041 < 0.0052 120 o-Xylene 0.006J 0.0038J < 0.0029 < 0.0027 < 0.0033 140 Arsenic < 1.4 < 1.3 < 0.32 < 1.5 < 1.5 0.68 Barium 137 131 99.1 197 214 3,100 Cadmium 0.19 0.15 0.13 0.21 0.24 1.4 Chromium 16.8 20.4 13.1 20.9 24.3 NE Chromium VI (Method 7199)< 0.0575 < 0.0578 < 0.0617 < 0.0581 < 0.0690 0.31 Lead 9.4 6.1 4.8 6.8 5.9 250 Selenium < 0.42 < 0.38 < 0.49 < 0.45 < 0.44 78 Silver < 0.31 < 0.28 < 0.14 < 0.33 < 0.32 78 Mercury < 0.0042 0.0051J 0.0080J 0.010J 0.0057J 4.7 * Methylene Chloride is a common laboratory contaminant Red items are exceedances of residential PSRGs and/or the method detection limit is above the PSRG NE - Not Established NA = Not Analyzed Data compared to NCDEQ PSRGs July 2023 SVOCs - 8270 (mg/kg) - Not Detected Metals (mg/kg) TABLE 1 - Imported Soil Sampling Analytical Results Mock Judson Mill, 2610 Oakland Avenue Greensboro, North Carolina Brownfield No. 25094-21-041 Residential PSRG (mg/kg) VOCs - 8260 (mg/kg) Martin Marietta Salem Stone Quarry Sampling R1 October 24, 2023 Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina Brownfields Project Number 25094-21-041 REPORT OF LABORATORY ANALYSIS CHAIN-OF-CUSTODY #=CL# October 09, 2023 LIMS USE: FR - CHERYL MOODY LIMS OBJECT ID: 92689576 92689576 Project: Pace Project No.: RE: Cheryl Moody Atlantic Shore Environmental 175-1 Venture Drive Belville, NC 28451 Mock Judson Mill PN: 1533-Revised Report Dear Cheryl Moody: Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte • Pace Analytical Services - Ormond Beach This revision was issued on 10/09/23 to report all finalized results. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com Project Manager 704-977-0942 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 93 #=CP# CERTIFICATIONS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Pace Analytical Services Ormond Beach 8 East Tower Circle, Ormond Beach, FL 32174 Alaska DEC- CS/UST/LUST Alabama Certification #: 41320 Colorado Certification: FL NELAC Reciprocity Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity DoD-ANAB #:ADE-3199 Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maine Certification #: FL01264 Maryland Certification: #346 Massachusetts Certification #: M-FL1264 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS-28-14 New Hampshire Certification #: 2958 New Jersey Certification #: FL022 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 North Dakota Certification #: R-216 Ohio DEP 87780 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FL01264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity Pace Analytical Services National 12065 Lebanon Road, Mt. 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Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 93 #=CP# CERTIFICATIONS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Pace Analytical Services National Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A2LA 2926.01 A2LA-ISO 17025 Certification #: 1461.01 A2LA-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 93 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Lab ID Sample ID Matrix Date Collected Date Received 92689576001 QS-1 Solid 09/19/23 13:44 09/20/23 15:35 92689576002 QS-2 Solid 09/19/23 13:52 09/20/23 15:35 92689576003 QS-3 Solid 09/19/23 14:02 09/20/23 15:35 92689576004 QS-4 Solid 09/19/23 14:15 09/20/23 15:35 92689576005 QS-4d Solid 09/19/23 14:15 09/20/23 15:35 92689576006 AS-1 Solid 09/19/23 16:55 09/20/23 15:35 92689576007 AS-1d Solid 09/19/23 16:55 09/20/23 15:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 93 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92689576001 QS-1 EPA 6010 7 PASI-OKC2, TMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92689576002 QS-2 EPA 6010 7 PASI-OKC2, TMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92689576003 QS-3 EPA 6010 7 PASI-OAAM1, TMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92689576004 QS-4 EPA 6010 7 PASI-OKC2, TMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92689576005 QS-4d EPA 6010 7 PASI-OKC2, TMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92689576006 AS-1 EPA 8141B 27 PANMEW EPA 8151A 11 PANHMH REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 93 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts EPA 8082A 8 PASI-CBAJ EPA 6010 7 PASI-OTMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92689576007 AS-1d EPA 8141B 27 PANMEW, RDH EPA 8151A 11 PANHMH EPA 8082A 8 PASI-CBAJ EPA 6010 7 PASI-OTMA EPA 7471 1 PASI-OJNK EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CLMB SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte PASI-O = Pace Analytical Services - Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-1 Lab ID:92689576001 Collected:09/19/23 13:44 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3050 Pace Analytical Services - Ormond Beach 6010 MET ICP Arsenic ND mg/kg 09/29/23 10:56 7440-38-2 D309/28/23 07:462.8 1.4 5 Barium 137 mg/kg 09/29/23 10:56 7440-39-309/28/23 07:462.8 0.47 5 Cadmium 0.19 mg/kg 09/28/23 19:42 7440-43-909/28/23 07:460.056 0.028 1 Chromium 16.8 mg/kg 09/28/23 19:42 7440-47-309/28/23 07:460.28 0.14 1 Lead 9.4 mg/kg 09/28/23 19:42 7439-92-109/28/23 07:460.56 0.28 1 Selenium ND mg/kg 09/28/23 19:42 7782-49-209/28/23 07:460.84 0.42 1 Silver ND mg/kg 09/29/23 10:56 7440-22-4 D309/28/23 07:461.4 0.31 5 Analytical Method: EPA 7471 Preparation Method: EPA 7471 Pace Analytical Services - Ormond Beach 7471 Mercury Mercury ND mg/kg 10/02/23 14:15 7439-97-610/02/23 10:470.0083 0.0042 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 09/25/23 14:14 83-32-909/23/23 12:583531241 Acenaphthylene ND ug/kg 09/25/23 14:14 208-96-809/23/23 12:583531241 Aniline ND ug/kg 09/25/23 14:14 62-53-309/23/23 12:583531381 Anthracene ND ug/kg 09/25/23 14:14 120-12-709/23/23 12:583531161 Benzo(a)anthracene ND ug/kg 09/25/23 14:14 56-55-309/23/23 12:583531181 Benzo(a)pyrene ND ug/kg 09/25/23 14:14 50-32-809/23/23 12:583531221 Benzo(b)fluoranthene ND ug/kg 09/25/23 14:14 205-99-209/23/23 12:583531181 Benzo(g,h,i)perylene ND ug/kg 09/25/23 14:14 191-24-209/23/23 12:583531371 Benzo(k)fluoranthene ND ug/kg 09/25/23 14:14 207-08-909/23/23 12:583531241 Benzoic Acid ND ug/kg 09/25/23 14:14 65-85-009/23/23 12:5817707591 Benzyl alcohol ND ug/kg 09/25/23 14:14 100-51-609/23/23 12:587062671 4-Bromophenylphenyl ether ND ug/kg 09/25/23 14:14 101-55-309/23/23 12:583531361 Butylbenzylphthalate ND ug/kg 09/25/23 14:14 85-68-709/23/23 12:583531491 4-Chloro-3-methylphenol ND ug/kg 09/25/23 14:14 59-50-709/23/23 12:587062481 4-Chloroaniline ND ug/kg 09/25/23 14:14 106-47-809/23/23 12:587062771 bis(2-Chloroethoxy)methane ND ug/kg 09/25/23 14:14 111-91-109/23/23 12:583531471 bis(2-Chloroethyl) ether ND ug/kg 09/25/23 14:14 111-44-409/23/23 12:583531331 2-Chloronaphthalene ND ug/kg 09/25/23 14:14 91-58-709/23/23 12:583531401 2-Chlorophenol ND ug/kg 09/25/23 14:14 95-57-809/23/23 12:583531331 4-Chlorophenylphenyl ether ND ug/kg 09/25/23 14:14 7005-72-309/23/23 12:583531321 Chrysene ND ug/kg 09/25/23 14:14 218-01-909/23/23 12:583531281 Dibenz(a,h)anthracene ND ug/kg 09/25/23 14:14 53-70-309/23/23 12:583531361 Dibenzofuran ND ug/kg 09/25/23 14:14 132-64-909/23/23 12:583531271 1,2-Dichlorobenzene ND ug/kg 09/25/23 14:14 95-50-109/23/23 12:583531271 1,3-Dichlorobenzene ND ug/kg 09/25/23 14:14 541-73-109/23/23 12:583531251 1,4-Dichlorobenzene ND ug/kg 09/25/23 14:14 106-46-709/23/23 12:583531351 3,3'-Dichlorobenzidine ND ug/kg 09/25/23 14:14 91-94-109/23/23 12:587062391 2,4-Dichlorophenol ND ug/kg 09/25/23 14:14 120-83-209/23/23 12:583531381 Diethylphthalate ND ug/kg 09/25/23 14:14 84-66-209/23/23 12:583531291 2,4-Dimethylphenol ND ug/kg 09/25/23 14:14 105-67-909/23/23 12:583531471 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-1 Lab ID:92689576001 Collected:09/19/23 13:44 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 09/25/23 14:14 131-11-309/23/23 12:583531281 Di-n-butylphthalate ND ug/kg 09/25/23 14:14 84-74-209/23/23 12:583531191 4,6-Dinitro-2-methylphenol ND ug/kg 09/25/23 14:14 534-52-109/23/23 12:587063301 2,4-Dinitrophenol ND ug/kg 09/25/23 14:14 51-28-509/23/23 12:58177010901 2,4-Dinitrotoluene ND ug/kg 09/25/23 14:14 121-14-209/23/23 12:583531361 2,6-Dinitrotoluene ND ug/kg 09/25/23 14:14 606-20-209/23/23 12:583531291 Di-n-octylphthalate ND ug/kg 09/25/23 14:14 117-84-009/23/23 12:583531391 bis(2-Ethylhexyl)phthalate ND ug/kg 09/25/23 14:14 117-81-709/23/23 12:583531371 Fluoranthene ND ug/kg 09/25/23 14:14 206-44-009/23/23 12:583531211 Fluorene ND ug/kg 09/25/23 14:14 86-73-709/23/23 12:583531241 Hexachloro-1,3-butadiene ND ug/kg 09/25/23 14:14 87-68-309/23/23 12:583531531 Hexachlorobenzene ND ug/kg 09/25/23 14:14 118-74-109/23/23 12:583531381 Hexachlorocyclopentadiene ND ug/kg 09/25/23 14:14 77-47-409/23/23 12:583532021 Hexachloroethane ND ug/kg 09/25/23 14:14 67-72-109/23/23 12:583531351 Indeno(1,2,3-cd)pyrene ND ug/kg 09/25/23 14:14 193-39-509/23/23 12:583531391 Isophorone ND ug/kg 09/25/23 14:14 78-59-109/23/23 12:583531571 1-Methylnaphthalene ND ug/kg 09/25/23 14:14 90-12-009/23/23 12:583531241 2-Methylnaphthalene ND ug/kg 09/25/23 14:14 91-57-609/23/23 12:583531411 2-Methylphenol(o-Cresol)ND ug/kg 09/25/23 14:14 95-48-709/23/23 12:583531441 3&4-Methylphenol(m&p Cresol)ND ug/kg 09/25/23 14:14 15831-10-409/23/23 12:583531421 Naphthalene ND ug/kg 09/25/23 14:14 91-20-309/23/23 12:583531201 2-Nitroaniline ND ug/kg 09/25/23 14:14 88-74-409/23/23 12:5817702891 3-Nitroaniline ND ug/kg 09/25/23 14:14 99-09-209/23/23 12:5817702771 4-Nitroaniline ND ug/kg 09/25/23 14:14 100-01-609/23/23 12:587062691 Nitrobenzene ND ug/kg 09/25/23 14:14 98-95-309/23/23 12:583531641 2-Nitrophenol ND ug/kg 09/25/23 14:14 88-75-509/23/23 12:583531531 4-Nitrophenol ND ug/kg 09/25/23 14:14 100-02-709/23/23 12:5817706831 N-Nitrosodimethylamine ND ug/kg 09/25/23 14:14 62-75-909/23/23 12:583531191 N-Nitroso-di-n-propylamine ND ug/kg 09/25/23 14:14 621-64-709/23/23 12:583531331 N-Nitrosodiphenylamine ND ug/kg 09/25/23 14:14 86-30-609/23/23 12:583531251 2,2'-Oxybis(1-chloropropane)ND ug/kg 09/25/23 14:14 108-60-109/23/23 12:583531681 Pentachlorophenol ND ug/kg 09/25/23 14:14 87-86-509/23/23 12:587063461 Phenanthrene ND ug/kg 09/25/23 14:14 85-01-809/23/23 12:583531161 Phenol ND ug/kg 09/25/23 14:14 108-95-209/23/23 12:583531571 Pyrene ND ug/kg 09/25/23 14:14 129-00-009/23/23 12:583531431 Pyridine ND ug/kg 09/25/23 14:14 110-86-109/23/23 12:583531111 1,2,4-Trichlorobenzene ND ug/kg 09/25/23 14:14 120-82-109/23/23 12:583531391 2,4,5-Trichlorophenol ND ug/kg 09/25/23 14:14 95-95-409/23/23 12:583531621 2,4,6-Trichlorophenol ND ug/kg 09/25/23 14:14 88-06-209/23/23 12:583531461 Surrogates Nitrobenzene-d5 (S)39 %09/25/23 14:14 4165-60-009/23/23 12:5810-130 1 2-Fluorobiphenyl (S)48 %09/25/23 14:14 321-60-809/23/23 12:5810-130 1 Terphenyl-d14 (S)62 %09/25/23 14:14 1718-51-009/23/23 12:5810-130 1 Phenol-d6 (S)38 %09/25/23 14:14 13127-88-309/23/23 12:5810-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-1 Lab ID:92689576001 Collected:09/19/23 13:44 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)32 %09/25/23 14:14 367-12-409/23/23 12:5810-130 1 2,4,6-Tribromophenol (S)66 %09/25/23 14:14 118-79-609/23/23 12:5810-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 09/26/23 04:41 67-64-109/25/23 20:2614345.8 1 Benzene ND ug/kg 09/26/23 04:41 71-43-209/25/23 20:267.1 2.8 1 Bromobenzene ND ug/kg 09/26/23 04:41 108-86-109/25/23 20:267.1 2.3 1 Bromochloromethane ND ug/kg 09/26/23 04:41 74-97-509/25/23 20:267.1 2.1 1 Bromodichloromethane ND ug/kg 09/26/23 04:41 75-27-409/25/23 20:267.1 2.8 1 Bromoform ND ug/kg 09/26/23 04:41 75-25-209/25/23 20:267.1 2.5 1 Bromomethane ND ug/kg 09/26/23 04:41 74-83-909/25/23 20:2628.6 22.1 1 2-Butanone (MEK)ND ug/kg 09/26/23 04:41 78-93-309/25/23 20:2614334.3 1 n-Butylbenzene ND ug/kg 09/26/23 04:41 104-51-809/25/23 20:267.1 4.5 1 sec-Butylbenzene ND ug/kg 09/26/23 04:41 135-98-809/25/23 20:267.1 3.1 1 tert-Butylbenzene ND ug/kg 09/26/23 04:41 98-06-609/25/23 20:267.1 2.5 1 Carbon tetrachloride ND ug/kg 09/26/23 04:41 56-23-509/25/23 20:267.1 2.7 1 Chlorobenzene ND ug/kg 09/26/23 04:41 108-90-709/25/23 20:267.1 4.1 1 Chloroethane ND ug/kg 09/26/23 04:41 75-00-309/25/23 20:2614.3 5.5 1 Chloroform ND ug/kg 09/26/23 04:41 67-66-309/25/23 20:267.1 6.0 1 Chloromethane ND ug/kg 09/26/23 04:41 74-87-309/25/23 20:2614.3 6.0 1 2-Chlorotoluene ND ug/kg 09/26/23 04:41 95-49-809/25/23 20:267.1 2.5 1 4-Chlorotoluene ND ug/kg 09/26/23 04:41 106-43-409/25/23 20:267.1 4.0 1 1,2-Dibromo-3-chloropropane ND ug/kg 09/26/23 04:41 96-12-809/25/23 20:267.1 2.8 1 Dibromochloromethane ND ug/kg 09/26/23 04:41 124-48-109/25/23 20:267.1 4.0 1 1,2-Dibromoethane (EDB)ND ug/kg 09/26/23 04:41 106-93-409/25/23 20:267.1 3.1 1 Dibromomethane ND ug/kg 09/26/23 04:41 74-95-309/25/23 20:267.1 1.5 1 1,2-Dichlorobenzene ND ug/kg 09/26/23 04:41 95-50-109/25/23 20:267.1 2.6 1 1,3-Dichlorobenzene ND ug/kg 09/26/23 04:41 541-73-109/25/23 20:267.1 2.2 1 1,4-Dichlorobenzene ND ug/kg 09/26/23 04:41 106-46-709/25/23 20:267.1 1.9 1 Dichlorodifluoromethane ND ug/kg 09/26/23 04:41 75-71-8 v109/25/23 20:2614.3 7.3 1 1,1-Dichloroethane ND ug/kg 09/26/23 04:41 75-34-309/25/23 20:267.1 2.9 1 1,2-Dichloroethane ND ug/kg 09/26/23 04:41 107-06-209/25/23 20:267.1 4.7 1 1,1-Dichloroethene ND ug/kg 09/26/23 04:41 75-35-4 v109/25/23 20:267.1 2.9 1 cis-1,2-Dichloroethene ND ug/kg 09/26/23 04:41 156-59-209/25/23 20:267.1 2.4 1 trans-1,2-Dichloroethene ND ug/kg 09/26/23 04:41 156-60-509/25/23 20:267.1 6.1 1 1,2-Dichloropropane ND ug/kg 09/26/23 04:41 78-87-509/25/23 20:267.1 2.1 1 1,3-Dichloropropane ND ug/kg 09/26/23 04:41 142-28-909/25/23 20:267.1 2.2 1 2,2-Dichloropropane ND ug/kg 09/26/23 04:41 594-20-709/25/23 20:267.1 5.4 1 1,1-Dichloropropene ND ug/kg 09/26/23 04:41 563-58-609/25/23 20:267.1 3.4 1 cis-1,3-Dichloropropene ND ug/kg 09/26/23 04:41 10061-01-509/25/23 20:267.1 1.9 1 trans-1,3-Dichloropropene ND ug/kg 09/26/23 04:41 10061-02-609/25/23 20:267.1 2.5 1 Diisopropyl ether ND ug/kg 09/26/23 04:41 108-20-309/25/23 20:267.1 1.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-1 Lab ID:92689576001 Collected:09/19/23 13:44 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene 8.0 ug/kg 09/26/23 04:41 100-41-409/25/23 20:267.1 3.3 1 Hexachloro-1,3-butadiene ND ug/kg 09/26/23 04:41 87-68-309/25/23 20:2614.3 11.7 1 2-Hexanone ND ug/kg 09/26/23 04:41 591-78-609/25/23 20:2671.4 6.9 1 Isopropylbenzene (Cumene)ND ug/kg 09/26/23 04:41 98-82-809/25/23 20:267.1 2.4 1 p-Isopropyltoluene ND ug/kg 09/26/23 04:41 99-87-609/25/23 20:267.1 3.5 1 Methylene Chloride ND ug/kg 09/26/23 04:41 75-09-209/25/23 20:2628.6 19.6 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/23 04:41 108-10-109/25/23 20:2671.4 6.9 1 Methyl-tert-butyl ether ND ug/kg 09/26/23 04:41 1634-04-409/25/23 20:267.1 2.7 1 Naphthalene ND ug/kg 09/26/23 04:41 91-20-309/25/23 20:267.1 3.8 1 n-Propylbenzene ND ug/kg 09/26/23 04:41 103-65-109/25/23 20:267.1 2.5 1 Styrene ND ug/kg 09/26/23 04:41 100-42-509/25/23 20:267.1 1.9 1 1,1,1,2-Tetrachloroethane ND ug/kg 09/26/23 04:41 630-20-609/25/23 20:267.1 2.7 1 1,1,2,2-Tetrachloroethane ND ug/kg 09/26/23 04:41 79-34-509/25/23 20:267.1 1.9 1 Tetrachloroethene ND ug/kg 09/26/23 04:41 127-18-409/25/23 20:267.1 2.3 1 Toluene 16.9 ug/kg 09/26/23 04:41 108-88-309/25/23 20:267.1 4.9 1 1,2,3-Trichlorobenzene ND ug/kg 09/26/23 04:41 87-61-609/25/23 20:267.1 5.8 1 1,2,4-Trichlorobenzene ND ug/kg 09/26/23 04:41 120-82-109/25/23 20:267.1 6.0 1 1,1,1-Trichloroethane ND ug/kg 09/26/23 04:41 71-55-609/25/23 20:267.1 3.7 1 1,1,2-Trichloroethane ND ug/kg 09/26/23 04:41 79-00-509/25/23 20:267.1 2.4 1 Trichloroethene ND ug/kg 09/26/23 04:41 79-01-609/25/23 20:267.1 5.8 1 Trichlorofluoromethane ND ug/kg 09/26/23 04:41 75-69-409/25/23 20:267.1 3.9 1 1,2,3-Trichloropropane ND ug/kg 09/26/23 04:41 96-18-409/25/23 20:267.1 3.6 1 1,2,4-Trimethylbenzene ND ug/kg 09/26/23 04:41 95-63-609/25/23 20:267.1 4.2 1 1,3,5-Trimethylbenzene ND ug/kg 09/26/23 04:41 108-67-809/25/23 20:267.1 2.4 1 Vinyl acetate ND ug/kg 09/26/23 04:41 108-05-409/25/23 20:2671.4 14.7 1 Vinyl chloride ND ug/kg 09/26/23 04:41 75-01-409/25/23 20:2614.3 3.6 1 Xylene (Total)23.4 ug/kg 09/26/23 04:41 1330-20-709/25/23 20:2614.3 4.1 1 m&p-Xylene 17.4 ug/kg 09/26/23 04:41 179601-23-109/25/23 20:2614.3 4.9 1 o-Xylene 6.0J ug/kg 09/26/23 04:41 95-47-609/25/23 20:267.1 3.2 1 Surrogates Toluene-d8 (S)102 %09/26/23 04:41 2037-26-509/25/23 20:2670-130 1 4-Bromofluorobenzene (S)102 %09/26/23 04:41 460-00-409/25/23 20:2670-130 1 1,2-Dichloroethane-d4 (S)107 %09/26/23 04:41 17060-07-009/25/23 20:2670-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 6.2 %09/25/23 13:21 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 88.6 %09/29/23 13:1309/29/23 13:021 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-1 Lab ID:92689576001 Collected:09/19/23 13:44 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 10/03/23 03:19 18540-29-909/29/23 12:220.226 0.0575 0.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-2 Lab ID:92689576002 Collected:09/19/23 13:52 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3050 Pace Analytical Services - Ormond Beach 6010 MET ICP Arsenic ND mg/kg 09/29/23 11:03 7440-38-2 D309/28/23 07:462.6 1.3 5 Barium 131 mg/kg 09/29/23 11:03 7440-39-309/28/23 07:462.6 0.43 5 Cadmium 0.15 mg/kg 09/28/23 19:46 7440-43-909/28/23 07:460.051 0.026 1 Chromium 20.4 mg/kg 09/28/23 19:46 7440-47-309/28/23 07:460.26 0.13 1 Lead 6.1 mg/kg 09/28/23 19:46 7439-92-109/28/23 07:460.51 0.26 1 Selenium ND mg/kg 09/28/23 19:46 7782-49-209/28/23 07:460.77 0.38 1 Silver ND mg/kg 09/29/23 11:03 7440-22-4 D309/28/23 07:461.3 0.28 5 Analytical Method: EPA 7471 Preparation Method: EPA 7471 Pace Analytical Services - Ormond Beach 7471 Mercury Mercury 0.0051J mg/kg 10/02/23 14:47 7439-97-610/02/23 10:470.010 0.0051 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 09/25/23 14:42 83-32-909/23/23 12:583631271 Acenaphthylene ND ug/kg 09/25/23 14:42 208-96-809/23/23 12:583631271 Aniline ND ug/kg 09/25/23 14:42 62-53-309/23/23 12:583631421 Anthracene ND ug/kg 09/25/23 14:42 120-12-709/23/23 12:583631191 Benzo(a)anthracene ND ug/kg 09/25/23 14:42 56-55-309/23/23 12:583631211 Benzo(a)pyrene ND ug/kg 09/25/23 14:42 50-32-809/23/23 12:583631251 Benzo(b)fluoranthene ND ug/kg 09/25/23 14:42 205-99-209/23/23 12:583631211 Benzo(g,h,i)perylene ND ug/kg 09/25/23 14:42 191-24-209/23/23 12:583631411 Benzo(k)fluoranthene ND ug/kg 09/25/23 14:42 207-08-909/23/23 12:583631271 Benzoic Acid ND ug/kg 09/25/23 14:42 65-85-009/23/23 12:5818107791 Benzyl alcohol ND ug/kg 09/25/23 14:42 100-51-609/23/23 12:587252751 4-Bromophenylphenyl ether ND ug/kg 09/25/23 14:42 101-55-309/23/23 12:583631401 Butylbenzylphthalate ND ug/kg 09/25/23 14:42 85-68-709/23/23 12:583631531 4-Chloro-3-methylphenol ND ug/kg 09/25/23 14:42 59-50-709/23/23 12:587252551 4-Chloroaniline ND ug/kg 09/25/23 14:42 106-47-809/23/23 12:587252851 bis(2-Chloroethoxy)methane ND ug/kg 09/25/23 14:42 111-91-109/23/23 12:583631511 bis(2-Chloroethyl) ether ND ug/kg 09/25/23 14:42 111-44-409/23/23 12:583631361 2-Chloronaphthalene ND ug/kg 09/25/23 14:42 91-58-709/23/23 12:583631441 2-Chlorophenol ND ug/kg 09/25/23 14:42 95-57-809/23/23 12:583631361 4-Chlorophenylphenyl ether ND ug/kg 09/25/23 14:42 7005-72-309/23/23 12:583631351 Chrysene ND ug/kg 09/25/23 14:42 218-01-909/23/23 12:583631321 Dibenz(a,h)anthracene ND ug/kg 09/25/23 14:42 53-70-309/23/23 12:583631401 Dibenzofuran ND ug/kg 09/25/23 14:42 132-64-909/23/23 12:583631311 1,2-Dichlorobenzene ND ug/kg 09/25/23 14:42 95-50-109/23/23 12:583631311 1,3-Dichlorobenzene ND ug/kg 09/25/23 14:42 541-73-109/23/23 12:583631291 1,4-Dichlorobenzene ND ug/kg 09/25/23 14:42 106-46-709/23/23 12:583631381 3,3'-Dichlorobenzidine ND ug/kg 09/25/23 14:42 91-94-109/23/23 12:587252451 2,4-Dichlorophenol ND ug/kg 09/25/23 14:42 120-83-209/23/23 12:583631421 Diethylphthalate ND ug/kg 09/25/23 14:42 84-66-209/23/23 12:583631331 2,4-Dimethylphenol ND ug/kg 09/25/23 14:42 105-67-909/23/23 12:583631511 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-2 Lab ID:92689576002 Collected:09/19/23 13:52 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 09/25/23 14:42 131-11-309/23/23 12:583631321 Di-n-butylphthalate ND ug/kg 09/25/23 14:42 84-74-209/23/23 12:583631221 4,6-Dinitro-2-methylphenol ND ug/kg 09/25/23 14:42 534-52-109/23/23 12:587253381 2,4-Dinitrophenol ND ug/kg 09/25/23 14:42 51-28-509/23/23 12:58181011201 2,4-Dinitrotoluene ND ug/kg 09/25/23 14:42 121-14-209/23/23 12:583631401 2,6-Dinitrotoluene ND ug/kg 09/25/23 14:42 606-20-209/23/23 12:583631331 Di-n-octylphthalate ND ug/kg 09/25/23 14:42 117-84-009/23/23 12:583631431 bis(2-Ethylhexyl)phthalate ND ug/kg 09/25/23 14:42 117-81-709/23/23 12:583631411 Fluoranthene ND ug/kg 09/25/23 14:42 206-44-009/23/23 12:583631241 Fluorene ND ug/kg 09/25/23 14:42 86-73-709/23/23 12:583631271 Hexachloro-1,3-butadiene ND ug/kg 09/25/23 14:42 87-68-309/23/23 12:583631571 Hexachlorobenzene ND ug/kg 09/25/23 14:42 118-74-109/23/23 12:583631421 Hexachlorocyclopentadiene ND ug/kg 09/25/23 14:42 77-47-409/23/23 12:583632081 Hexachloroethane ND ug/kg 09/25/23 14:42 67-72-109/23/23 12:583631381 Indeno(1,2,3-cd)pyrene ND ug/kg 09/25/23 14:42 193-39-509/23/23 12:583631431 Isophorone ND ug/kg 09/25/23 14:42 78-59-109/23/23 12:583631611 1-Methylnaphthalene ND ug/kg 09/25/23 14:42 90-12-009/23/23 12:583631271 2-Methylnaphthalene ND ug/kg 09/25/23 14:42 91-57-609/23/23 12:583631451 2-Methylphenol(o-Cresol)ND ug/kg 09/25/23 14:42 95-48-709/23/23 12:583631481 3&4-Methylphenol(m&p Cresol)ND ug/kg 09/25/23 14:42 15831-10-409/23/23 12:583631461 Naphthalene ND ug/kg 09/25/23 14:42 91-20-309/23/23 12:583631231 2-Nitroaniline ND ug/kg 09/25/23 14:42 88-74-409/23/23 12:5818102971 3-Nitroaniline ND ug/kg 09/25/23 14:42 99-09-209/23/23 12:5818102851 4-Nitroaniline ND ug/kg 09/25/23 14:42 100-01-609/23/23 12:587252761 Nitrobenzene ND ug/kg 09/25/23 14:42 98-95-309/23/23 12:583631681 2-Nitrophenol ND ug/kg 09/25/23 14:42 88-75-509/23/23 12:583631571 4-Nitrophenol ND ug/kg 09/25/23 14:42 100-02-709/23/23 12:5818107011 N-Nitrosodimethylamine ND ug/kg 09/25/23 14:42 62-75-909/23/23 12:583631221 N-Nitroso-di-n-propylamine ND ug/kg 09/25/23 14:42 621-64-709/23/23 12:583631361 N-Nitrosodiphenylamine ND ug/kg 09/25/23 14:42 86-30-609/23/23 12:583631291 2,2'-Oxybis(1-chloropropane)ND ug/kg 09/25/23 14:42 108-60-109/23/23 12:583631721 Pentachlorophenol ND ug/kg 09/25/23 14:42 87-86-509/23/23 12:587253551 Phenanthrene ND ug/kg 09/25/23 14:42 85-01-809/23/23 12:583631191 Phenol ND ug/kg 09/25/23 14:42 108-95-209/23/23 12:583631611 Pyrene ND ug/kg 09/25/23 14:42 129-00-009/23/23 12:583631471 Pyridine ND ug/kg 09/25/23 14:42 110-86-109/23/23 12:583631141 1,2,4-Trichlorobenzene ND ug/kg 09/25/23 14:42 120-82-109/23/23 12:583631431 2,4,5-Trichlorophenol ND ug/kg 09/25/23 14:42 95-95-409/23/23 12:583631661 2,4,6-Trichlorophenol ND ug/kg 09/25/23 14:42 88-06-209/23/23 12:583631491 Surrogates Nitrobenzene-d5 (S)12 %09/25/23 14:42 4165-60-009/23/23 12:5810-130 1 2-Fluorobiphenyl (S)15 %09/25/23 14:42 321-60-809/23/23 12:5810-130 1 Terphenyl-d14 (S)24 %09/25/23 14:42 1718-51-009/23/23 12:5810-130 1 Phenol-d6 (S)12 %09/25/23 14:42 13127-88-309/23/23 12:5810-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-2 Lab ID:92689576002 Collected:09/19/23 13:52 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)11 %09/25/23 14:42 367-12-409/23/23 12:5810-130 1 2,4,6-Tribromophenol (S)21 %09/25/23 14:42 118-79-609/23/23 12:5810-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 09/26/23 04:58 67-64-109/25/23 20:2612038.4 1 Benzene ND ug/kg 09/26/23 04:58 71-43-209/25/23 20:266.0 2.4 1 Bromobenzene ND ug/kg 09/26/23 04:58 108-86-109/25/23 20:266.0 2.0 1 Bromochloromethane ND ug/kg 09/26/23 04:58 74-97-509/25/23 20:266.0 1.8 1 Bromodichloromethane ND ug/kg 09/26/23 04:58 75-27-409/25/23 20:266.0 2.3 1 Bromoform ND ug/kg 09/26/23 04:58 75-25-209/25/23 20:266.0 2.1 1 Bromomethane ND ug/kg 09/26/23 04:58 74-83-909/25/23 20:2624.0 18.6 1 2-Butanone (MEK)ND ug/kg 09/26/23 04:58 78-93-309/25/23 20:2612028.7 1 n-Butylbenzene ND ug/kg 09/26/23 04:58 104-51-809/25/23 20:266.0 3.8 1 sec-Butylbenzene ND ug/kg 09/26/23 04:58 135-98-809/25/23 20:266.0 2.6 1 tert-Butylbenzene ND ug/kg 09/26/23 04:58 98-06-609/25/23 20:266.0 2.1 1 Carbon tetrachloride ND ug/kg 09/26/23 04:58 56-23-509/25/23 20:266.0 2.2 1 Chlorobenzene ND ug/kg 09/26/23 04:58 108-90-709/25/23 20:266.0 3.4 1 Chloroethane ND ug/kg 09/26/23 04:58 75-00-309/25/23 20:2612.0 4.6 1 Chloroform ND ug/kg 09/26/23 04:58 67-66-309/25/23 20:266.0 5.0 1 Chloromethane ND ug/kg 09/26/23 04:58 74-87-309/25/23 20:2612.0 5.0 1 2-Chlorotoluene ND ug/kg 09/26/23 04:58 95-49-809/25/23 20:266.0 2.1 1 4-Chlorotoluene ND ug/kg 09/26/23 04:58 106-43-409/25/23 20:266.0 3.3 1 1,2-Dibromo-3-chloropropane ND ug/kg 09/26/23 04:58 96-12-809/25/23 20:266.0 2.3 1 Dibromochloromethane ND ug/kg 09/26/23 04:58 124-48-109/25/23 20:266.0 3.4 1 1,2-Dibromoethane (EDB)ND ug/kg 09/26/23 04:58 106-93-409/25/23 20:266.0 2.6 1 Dibromomethane ND ug/kg 09/26/23 04:58 74-95-309/25/23 20:266.0 1.3 1 1,2-Dichlorobenzene ND ug/kg 09/26/23 04:58 95-50-109/25/23 20:266.0 2.2 1 1,3-Dichlorobenzene ND ug/kg 09/26/23 04:58 541-73-109/25/23 20:266.0 1.9 1 1,4-Dichlorobenzene ND ug/kg 09/26/23 04:58 106-46-709/25/23 20:266.0 1.6 1 Dichlorodifluoromethane ND ug/kg 09/26/23 04:58 75-71-8 v109/25/23 20:2612.0 6.1 1 1,1-Dichloroethane ND ug/kg 09/26/23 04:58 75-34-309/25/23 20:266.0 2.5 1 1,2-Dichloroethane ND ug/kg 09/26/23 04:58 107-06-209/25/23 20:266.0 4.0 1 1,1-Dichloroethene ND ug/kg 09/26/23 04:58 75-35-4 v109/25/23 20:266.0 2.5 1 cis-1,2-Dichloroethene ND ug/kg 09/26/23 04:58 156-59-209/25/23 20:266.0 2.0 1 trans-1,2-Dichloroethene ND ug/kg 09/26/23 04:58 156-60-509/25/23 20:266.0 5.1 1 1,2-Dichloropropane ND ug/kg 09/26/23 04:58 78-87-509/25/23 20:266.0 1.8 1 1,3-Dichloropropane ND ug/kg 09/26/23 04:58 142-28-909/25/23 20:266.0 1.9 1 2,2-Dichloropropane ND ug/kg 09/26/23 04:58 594-20-709/25/23 20:266.0 4.5 1 1,1-Dichloropropene ND ug/kg 09/26/23 04:58 563-58-609/25/23 20:266.0 2.9 1 cis-1,3-Dichloropropene ND ug/kg 09/26/23 04:58 10061-01-509/25/23 20:266.0 1.6 1 trans-1,3-Dichloropropene ND ug/kg 09/26/23 04:58 10061-02-609/25/23 20:266.0 2.1 1 Diisopropyl ether ND ug/kg 09/26/23 04:58 108-20-309/25/23 20:266.0 1.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-2 Lab ID:92689576002 Collected:09/19/23 13:52 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene 5.4J ug/kg 09/26/23 04:58 100-41-409/25/23 20:266.0 2.8 1 Hexachloro-1,3-butadiene ND ug/kg 09/26/23 04:58 87-68-309/25/23 20:2612.0 9.8 1 2-Hexanone ND ug/kg 09/26/23 04:58 591-78-609/25/23 20:2659.9 5.8 1 Isopropylbenzene (Cumene)ND ug/kg 09/26/23 04:58 98-82-809/25/23 20:266.0 2.0 1 p-Isopropyltoluene ND ug/kg 09/26/23 04:58 99-87-609/25/23 20:266.0 2.9 1 Methylene Chloride 18.8J ug/kg 09/26/23 04:58 75-09-2 C909/25/23 20:2624.0 16.4 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/23 04:58 108-10-109/25/23 20:2659.9 5.8 1 Methyl-tert-butyl ether ND ug/kg 09/26/23 04:58 1634-04-409/25/23 20:266.0 2.2 1 Naphthalene ND ug/kg 09/26/23 04:58 91-20-309/25/23 20:266.0 3.1 1 n-Propylbenzene ND ug/kg 09/26/23 04:58 103-65-109/25/23 20:266.0 2.1 1 Styrene ND ug/kg 09/26/23 04:58 100-42-509/25/23 20:266.0 1.6 1 1,1,1,2-Tetrachloroethane ND ug/kg 09/26/23 04:58 630-20-609/25/23 20:266.0 2.3 1 1,1,2,2-Tetrachloroethane ND ug/kg 09/26/23 04:58 79-34-509/25/23 20:266.0 1.6 1 Tetrachloroethene ND ug/kg 09/26/23 04:58 127-18-409/25/23 20:266.0 1.9 1 Toluene 10.1 ug/kg 09/26/23 04:58 108-88-309/25/23 20:266.0 4.1 1 1,2,3-Trichlorobenzene ND ug/kg 09/26/23 04:58 87-61-609/25/23 20:266.0 4.8 1 1,2,4-Trichlorobenzene ND ug/kg 09/26/23 04:58 120-82-109/25/23 20:266.0 5.0 1 1,1,1-Trichloroethane ND ug/kg 09/26/23 04:58 71-55-609/25/23 20:266.0 3.1 1 1,1,2-Trichloroethane ND ug/kg 09/26/23 04:58 79-00-509/25/23 20:266.0 2.0 1 Trichloroethene ND ug/kg 09/26/23 04:58 79-01-609/25/23 20:266.0 4.8 1 Trichlorofluoromethane ND ug/kg 09/26/23 04:58 75-69-409/25/23 20:266.0 3.3 1 1,2,3-Trichloropropane ND ug/kg 09/26/23 04:58 96-18-409/25/23 20:266.0 3.0 1 1,2,4-Trimethylbenzene ND ug/kg 09/26/23 04:58 95-63-609/25/23 20:266.0 3.6 1 1,3,5-Trimethylbenzene ND ug/kg 09/26/23 04:58 108-67-809/25/23 20:266.0 2.0 1 Vinyl acetate ND ug/kg 09/26/23 04:58 108-05-409/25/23 20:2659.9 12.3 1 Vinyl chloride ND ug/kg 09/26/23 04:58 75-01-409/25/23 20:2612.0 3.0 1 Xylene (Total)14.9 ug/kg 09/26/23 04:58 1330-20-709/25/23 20:2612.0 3.4 1 m&p-Xylene 11.1J ug/kg 09/26/23 04:58 179601-23-109/25/23 20:2612.0 4.1 1 o-Xylene 3.8J ug/kg 09/26/23 04:58 95-47-609/25/23 20:266.0 2.6 1 Surrogates Toluene-d8 (S)101 %09/26/23 04:58 2037-26-509/25/23 20:2670-130 1 4-Bromofluorobenzene (S)100 %09/26/23 04:58 460-00-409/25/23 20:2670-130 1 1,2-Dichloroethane-d4 (S)107 %09/26/23 04:58 17060-07-009/25/23 20:2670-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 8.7 %09/25/23 13:21 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 90.8 %09/29/23 13:1309/29/23 13:021 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-2 Lab ID:92689576002 Collected:09/19/23 13:52 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 10/03/23 03:24 18540-29-909/29/23 12:220.227 0.0578 0.206 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-3 Lab ID:92689576003 Collected:09/19/23 14:02 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3050 Pace Analytical Services - Ormond Beach 6010 MET ICP Arsenic ND mg/kg 10/02/23 20:38 7440-38-210/02/23 10:520.65 0.32 1 Barium 99.1 mg/kg 10/02/23 20:38 7440-39-310/02/23 10:520.65 0.11 1 Cadmium 0.13 mg/kg 10/02/23 20:38 7440-43-910/02/23 10:520.065 0.032 1 Chromium 13.1 mg/kg 10/02/23 20:38 7440-47-310/02/23 10:520.32 0.16 1 Lead 4.8 mg/kg 10/02/23 20:38 7439-92-110/02/23 10:520.65 0.32 1 Selenium ND mg/kg 10/02/23 20:38 7782-49-210/02/23 10:520.97 0.49 1 Silver ND mg/kg 10/03/23 15:41 7440-22-4 D310/02/23 10:520.65 0.14 2 Analytical Method: EPA 7471 Preparation Method: EPA 7471 Pace Analytical Services - Ormond Beach 7471 Mercury Mercury 0.0080J mg/kg 10/03/23 13:29 7439-97-610/03/23 08:470.011 0.0053 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 09/25/23 15:10 83-32-909/23/23 12:583541241 Acenaphthylene ND ug/kg 09/25/23 15:10 208-96-809/23/23 12:583541241 Aniline ND ug/kg 09/25/23 15:10 62-53-309/23/23 12:583541381 Anthracene ND ug/kg 09/25/23 15:10 120-12-709/23/23 12:583541161 Benzo(a)anthracene ND ug/kg 09/25/23 15:10 56-55-309/23/23 12:583541181 Benzo(a)pyrene ND ug/kg 09/25/23 15:10 50-32-809/23/23 12:583541221 Benzo(b)fluoranthene ND ug/kg 09/25/23 15:10 205-99-209/23/23 12:583541181 Benzo(g,h,i)perylene ND ug/kg 09/25/23 15:10 191-24-209/23/23 12:583541371 Benzo(k)fluoranthene ND ug/kg 09/25/23 15:10 207-08-909/23/23 12:583541241 Benzoic Acid ND ug/kg 09/25/23 15:10 65-85-009/23/23 12:5817707601 Benzyl alcohol ND ug/kg 09/25/23 15:10 100-51-609/23/23 12:587072681 4-Bromophenylphenyl ether ND ug/kg 09/25/23 15:10 101-55-309/23/23 12:583541361 Butylbenzylphthalate ND ug/kg 09/25/23 15:10 85-68-709/23/23 12:583541491 4-Chloro-3-methylphenol ND ug/kg 09/25/23 15:10 59-50-709/23/23 12:587072491 4-Chloroaniline ND ug/kg 09/25/23 15:10 106-47-809/23/23 12:587072771 bis(2-Chloroethoxy)methane ND ug/kg 09/25/23 15:10 111-91-109/23/23 12:583541471 bis(2-Chloroethyl) ether ND ug/kg 09/25/23 15:10 111-44-409/23/23 12:583541331 2-Chloronaphthalene ND ug/kg 09/25/23 15:10 91-58-709/23/23 12:583541401 2-Chlorophenol ND ug/kg 09/25/23 15:10 95-57-809/23/23 12:583541331 4-Chlorophenylphenyl ether ND ug/kg 09/25/23 15:10 7005-72-309/23/23 12:583541321 Chrysene ND ug/kg 09/25/23 15:10 218-01-909/23/23 12:583541291 Dibenz(a,h)anthracene ND ug/kg 09/25/23 15:10 53-70-309/23/23 12:583541361 Dibenzofuran ND ug/kg 09/25/23 15:10 132-64-909/23/23 12:583541271 1,2-Dichlorobenzene ND ug/kg 09/25/23 15:10 95-50-109/23/23 12:583541271 1,3-Dichlorobenzene ND ug/kg 09/25/23 15:10 541-73-109/23/23 12:583541251 1,4-Dichlorobenzene ND ug/kg 09/25/23 15:10 106-46-709/23/23 12:583541351 3,3'-Dichlorobenzidine ND ug/kg 09/25/23 15:10 91-94-109/23/23 12:587072391 2,4-Dichlorophenol ND ug/kg 09/25/23 15:10 120-83-209/23/23 12:583541381 Diethylphthalate ND ug/kg 09/25/23 15:10 84-66-209/23/23 12:583541301 2,4-Dimethylphenol ND ug/kg 09/25/23 15:10 105-67-909/23/23 12:583541471 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-3 Lab ID:92689576003 Collected:09/19/23 14:02 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 09/25/23 15:10 131-11-309/23/23 12:583541291 Di-n-butylphthalate ND ug/kg 09/25/23 15:10 84-74-209/23/23 12:583541191 4,6-Dinitro-2-methylphenol ND ug/kg 09/25/23 15:10 534-52-109/23/23 12:587073301 2,4-Dinitrophenol ND ug/kg 09/25/23 15:10 51-28-509/23/23 12:58177010901 2,4-Dinitrotoluene ND ug/kg 09/25/23 15:10 121-14-209/23/23 12:583541361 2,6-Dinitrotoluene ND ug/kg 09/25/23 15:10 606-20-209/23/23 12:583541301 Di-n-octylphthalate ND ug/kg 09/25/23 15:10 117-84-009/23/23 12:583541391 bis(2-Ethylhexyl)phthalate ND ug/kg 09/25/23 15:10 117-81-709/23/23 12:583541371 Fluoranthene ND ug/kg 09/25/23 15:10 206-44-009/23/23 12:583541211 Fluorene ND ug/kg 09/25/23 15:10 86-73-709/23/23 12:583541241 Hexachloro-1,3-butadiene ND ug/kg 09/25/23 15:10 87-68-309/23/23 12:583541531 Hexachlorobenzene ND ug/kg 09/25/23 15:10 118-74-109/23/23 12:583541381 Hexachlorocyclopentadiene ND ug/kg 09/25/23 15:10 77-47-409/23/23 12:583542021 Hexachloroethane ND ug/kg 09/25/23 15:10 67-72-109/23/23 12:583541351 Indeno(1,2,3-cd)pyrene ND ug/kg 09/25/23 15:10 193-39-509/23/23 12:583541391 Isophorone ND ug/kg 09/25/23 15:10 78-59-109/23/23 12:583541571 1-Methylnaphthalene ND ug/kg 09/25/23 15:10 90-12-009/23/23 12:583541241 2-Methylnaphthalene ND ug/kg 09/25/23 15:10 91-57-609/23/23 12:583541411 2-Methylphenol(o-Cresol)ND ug/kg 09/25/23 15:10 95-48-709/23/23 12:583541451 3&4-Methylphenol(m&p Cresol)ND ug/kg 09/25/23 15:10 15831-10-409/23/23 12:583541421 Naphthalene ND ug/kg 09/25/23 15:10 91-20-309/23/23 12:583541201 2-Nitroaniline ND ug/kg 09/25/23 15:10 88-74-409/23/23 12:5817702891 3-Nitroaniline ND ug/kg 09/25/23 15:10 99-09-209/23/23 12:5817702771 4-Nitroaniline ND ug/kg 09/25/23 15:10 100-01-609/23/23 12:587072691 Nitrobenzene ND ug/kg 09/25/23 15:10 98-95-309/23/23 12:583541641 2-Nitrophenol ND ug/kg 09/25/23 15:10 88-75-509/23/23 12:583541531 4-Nitrophenol ND ug/kg 09/25/23 15:10 100-02-709/23/23 12:5817706841 N-Nitrosodimethylamine ND ug/kg 09/25/23 15:10 62-75-909/23/23 12:583541191 N-Nitroso-di-n-propylamine ND ug/kg 09/25/23 15:10 621-64-709/23/23 12:583541331 N-Nitrosodiphenylamine ND ug/kg 09/25/23 15:10 86-30-609/23/23 12:583541251 2,2'-Oxybis(1-chloropropane)ND ug/kg 09/25/23 15:10 108-60-109/23/23 12:583541681 Pentachlorophenol ND ug/kg 09/25/23 15:10 87-86-509/23/23 12:587073461 Phenanthrene ND ug/kg 09/25/23 15:10 85-01-809/23/23 12:583541161 Phenol ND ug/kg 09/25/23 15:10 108-95-209/23/23 12:583541571 Pyrene ND ug/kg 09/25/23 15:10 129-00-009/23/23 12:583541441 Pyridine ND ug/kg 09/25/23 15:10 110-86-109/23/23 12:583541111 1,2,4-Trichlorobenzene ND ug/kg 09/25/23 15:10 120-82-109/23/23 12:583541391 2,4,5-Trichlorophenol ND ug/kg 09/25/23 15:10 95-95-409/23/23 12:583541621 2,4,6-Trichlorophenol ND ug/kg 09/25/23 15:10 88-06-209/23/23 12:583541461 Surrogates Nitrobenzene-d5 (S)32 %09/25/23 15:10 4165-60-009/23/23 12:5810-130 1 2-Fluorobiphenyl (S)42 %09/25/23 15:10 321-60-809/23/23 12:5810-130 1 Terphenyl-d14 (S)72 %09/25/23 15:10 1718-51-009/23/23 12:5810-130 1 Phenol-d6 (S)28 %09/25/23 15:10 13127-88-309/23/23 12:5810-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-3 Lab ID:92689576003 Collected:09/19/23 14:02 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)24 %09/25/23 15:10 367-12-409/23/23 12:5810-130 1 2,4,6-Tribromophenol (S)63 %09/25/23 15:10 118-79-609/23/23 12:5810-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 09/26/23 10:04 67-64-109/25/23 22:4513041.6 1 Benzene ND ug/kg 09/26/23 10:04 71-43-209/25/23 22:456.5 2.6 1 Bromobenzene ND ug/kg 09/26/23 10:04 108-86-109/25/23 22:456.5 2.1 1 Bromochloromethane ND ug/kg 09/26/23 10:04 74-97-509/25/23 22:456.5 1.9 1 Bromodichloromethane ND ug/kg 09/26/23 10:04 75-27-409/25/23 22:456.5 2.5 1 Bromoform ND ug/kg 09/26/23 10:04 75-25-209/25/23 22:456.5 2.3 1 Bromomethane ND ug/kg 09/26/23 10:04 74-83-9 IK09/25/23 22:4525.9 20.1 1 2-Butanone (MEK)ND ug/kg 09/26/23 10:04 78-93-309/25/23 22:4513031.1 1 n-Butylbenzene ND ug/kg 09/26/23 10:04 104-51-809/25/23 22:456.5 4.1 1 sec-Butylbenzene ND ug/kg 09/26/23 10:04 135-98-809/25/23 22:456.5 2.9 1 tert-Butylbenzene ND ug/kg 09/26/23 10:04 98-06-609/25/23 22:456.5 2.3 1 Carbon tetrachloride ND ug/kg 09/26/23 10:04 56-23-509/25/23 22:456.5 2.4 1 Chlorobenzene ND ug/kg 09/26/23 10:04 108-90-709/25/23 22:456.5 3.7 1 Chloroethane ND ug/kg 09/26/23 10:04 75-00-309/25/23 22:4513.0 5.0 1 Chloroform ND ug/kg 09/26/23 10:04 67-66-309/25/23 22:456.5 5.4 1 Chloromethane ND ug/kg 09/26/23 10:04 74-87-309/25/23 22:4513.0 5.4 1 2-Chlorotoluene ND ug/kg 09/26/23 10:04 95-49-809/25/23 22:456.5 2.3 1 4-Chlorotoluene ND ug/kg 09/26/23 10:04 106-43-409/25/23 22:456.5 3.6 1 1,2-Dibromo-3-chloropropane ND ug/kg 09/26/23 10:04 96-12-809/25/23 22:456.5 2.5 1 Dibromochloromethane ND ug/kg 09/26/23 10:04 124-48-109/25/23 22:456.5 3.6 1 1,2-Dibromoethane (EDB)ND ug/kg 09/26/23 10:04 106-93-409/25/23 22:456.5 2.9 1 Dibromomethane ND ug/kg 09/26/23 10:04 74-95-309/25/23 22:456.5 1.4 1 1,2-Dichlorobenzene ND ug/kg 09/26/23 10:04 95-50-109/25/23 22:456.5 2.3 1 1,3-Dichlorobenzene ND ug/kg 09/26/23 10:04 541-73-109/25/23 22:456.5 2.0 1 1,4-Dichlorobenzene ND ug/kg 09/26/23 10:04 106-46-709/25/23 22:456.5 1.7 1 Dichlorodifluoromethane ND ug/kg 09/26/23 10:04 75-71-809/25/23 22:4513.0 6.6 1 1,1-Dichloroethane ND ug/kg 09/26/23 10:04 75-34-309/25/23 22:456.5 2.7 1 1,2-Dichloroethane ND ug/kg 09/26/23 10:04 107-06-209/25/23 22:456.5 4.3 1 1,1-Dichloroethene ND ug/kg 09/26/23 10:04 75-35-409/25/23 22:456.5 2.7 1 cis-1,2-Dichloroethene ND ug/kg 09/26/23 10:04 156-59-209/25/23 22:456.5 2.2 1 trans-1,2-Dichloroethene ND ug/kg 09/26/23 10:04 156-60-509/25/23 22:456.5 5.5 1 1,2-Dichloropropane ND ug/kg 09/26/23 10:04 78-87-509/25/23 22:456.5 1.9 1 1,3-Dichloropropane ND ug/kg 09/26/23 10:04 142-28-909/25/23 22:456.5 2.0 1 2,2-Dichloropropane ND ug/kg 09/26/23 10:04 594-20-709/25/23 22:456.5 4.9 1 1,1-Dichloropropene ND ug/kg 09/26/23 10:04 563-58-609/25/23 22:456.5 3.1 1 cis-1,3-Dichloropropene ND ug/kg 09/26/23 10:04 10061-01-509/25/23 22:456.5 1.8 1 trans-1,3-Dichloropropene ND ug/kg 09/26/23 10:04 10061-02-609/25/23 22:456.5 2.2 1 Diisopropyl ether ND ug/kg 09/26/23 10:04 108-20-309/25/23 22:456.5 1.8 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-3 Lab ID:92689576003 Collected:09/19/23 14:02 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 09/26/23 10:04 100-41-409/25/23 22:456.5 3.0 1 Hexachloro-1,3-butadiene ND ug/kg 09/26/23 10:04 87-68-3 v209/25/23 22:4513.0 10.6 1 2-Hexanone ND ug/kg 09/26/23 10:04 591-78-609/25/23 22:4564.9 6.3 1 Isopropylbenzene (Cumene)ND ug/kg 09/26/23 10:04 98-82-809/25/23 22:456.5 2.2 1 p-Isopropyltoluene ND ug/kg 09/26/23 10:04 99-87-609/25/23 22:456.5 3.2 1 Methylene Chloride ND ug/kg 09/26/23 10:04 75-09-209/25/23 22:4525.9 17.8 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/23 10:04 108-10-109/25/23 22:4564.9 6.3 1 Methyl-tert-butyl ether ND ug/kg 09/26/23 10:04 1634-04-409/25/23 22:456.5 2.4 1 Naphthalene ND ug/kg 09/26/23 10:04 91-20-309/25/23 22:456.5 3.4 1 n-Propylbenzene ND ug/kg 09/26/23 10:04 103-65-109/25/23 22:456.5 2.3 1 Styrene ND ug/kg 09/26/23 10:04 100-42-509/25/23 22:456.5 1.7 1 1,1,1,2-Tetrachloroethane ND ug/kg 09/26/23 10:04 630-20-609/25/23 22:456.5 2.5 1 1,1,2,2-Tetrachloroethane ND ug/kg 09/26/23 10:04 79-34-509/25/23 22:456.5 1.7 1 Tetrachloroethene ND ug/kg 09/26/23 10:04 127-18-409/25/23 22:456.5 2.0 1 Toluene ND ug/kg 09/26/23 10:04 108-88-309/25/23 22:456.5 4.5 1 1,2,3-Trichlorobenzene ND ug/kg 09/26/23 10:04 87-61-609/25/23 22:456.5 5.2 1 1,2,4-Trichlorobenzene ND ug/kg 09/26/23 10:04 120-82-109/25/23 22:456.5 5.4 1 1,1,1-Trichloroethane ND ug/kg 09/26/23 10:04 71-55-609/25/23 22:456.5 3.4 1 1,1,2-Trichloroethane ND ug/kg 09/26/23 10:04 79-00-509/25/23 22:456.5 2.2 1 Trichloroethene ND ug/kg 09/26/23 10:04 79-01-609/25/23 22:456.5 5.2 1 Trichlorofluoromethane ND ug/kg 09/26/23 10:04 75-69-409/25/23 22:456.5 3.6 1 1,2,3-Trichloropropane ND ug/kg 09/26/23 10:04 96-18-409/25/23 22:456.5 3.3 1 1,2,4-Trimethylbenzene ND ug/kg 09/26/23 10:04 95-63-609/25/23 22:456.5 3.9 1 1,3,5-Trimethylbenzene ND ug/kg 09/26/23 10:04 108-67-809/25/23 22:456.5 2.2 1 Vinyl acetate ND ug/kg 09/26/23 10:04 108-05-409/25/23 22:4564.9 13.3 1 Vinyl chloride ND ug/kg 09/26/23 10:04 75-01-409/25/23 22:4513.0 3.3 1 Xylene (Total)ND ug/kg 09/26/23 10:04 1330-20-709/25/23 22:4513.0 3.7 1 m&p-Xylene ND ug/kg 09/26/23 10:04 179601-23-109/25/23 22:4513.0 4.4 1 o-Xylene ND ug/kg 09/26/23 10:04 95-47-609/25/23 22:456.5 2.9 1 Surrogates Toluene-d8 (S)102 %09/26/23 10:04 2037-26-509/25/23 22:4570-130 1 4-Bromofluorobenzene (S)100 %09/26/23 10:04 460-00-409/25/23 22:4570-130 1 1,2-Dichloroethane-d4 (S)100 %09/26/23 10:04 17060-07-009/25/23 22:4570-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 7.3 %09/25/23 13:21 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 84.7 %09/29/23 13:0009/29/23 12:491 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-3 Lab ID:92689576003 Collected:09/19/23 14:02 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 10/03/23 03:29 18540-29-909/29/23 12:220.242 0.0617 0.205 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4 Lab ID:92689576004 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3050 Pace Analytical Services - Ormond Beach 6010 MET ICP Arsenic ND mg/kg 09/29/23 11:10 7440-38-2 D309/28/23 07:463.0 1.5 5 Barium 197 mg/kg 09/29/23 11:10 7440-39-309/28/23 07:463.0 0.50 5 Cadmium 0.21 mg/kg 09/28/23 19:49 7440-43-909/28/23 07:460.060 0.030 1 Chromium 20.9 mg/kg 09/28/23 19:49 7440-47-309/28/23 07:460.30 0.15 1 Lead 6.8 mg/kg 09/28/23 19:49 7439-92-109/28/23 07:460.60 0.30 1 Selenium ND mg/kg 09/28/23 19:49 7782-49-209/28/23 07:460.90 0.45 1 Silver ND mg/kg 09/29/23 11:10 7440-22-4 D309/28/23 07:461.5 0.33 5 Analytical Method: EPA 7471 Preparation Method: EPA 7471 Pace Analytical Services - Ormond Beach 7471 Mercury Mercury 0.010J mg/kg 10/03/23 13:31 7439-97-610/03/23 08:470.011 0.0055 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 09/25/23 15:38 83-32-909/23/23 12:583651281 Acenaphthylene ND ug/kg 09/25/23 15:38 208-96-809/23/23 12:583651281 Aniline ND ug/kg 09/25/23 15:38 62-53-309/23/23 12:583651431 Anthracene ND ug/kg 09/25/23 15:38 120-12-709/23/23 12:583651201 Benzo(a)anthracene ND ug/kg 09/25/23 15:38 56-55-309/23/23 12:583651221 Benzo(a)pyrene ND ug/kg 09/25/23 15:38 50-32-809/23/23 12:583651261 Benzo(b)fluoranthene ND ug/kg 09/25/23 15:38 205-99-209/23/23 12:583651221 Benzo(g,h,i)perylene ND ug/kg 09/25/23 15:38 191-24-209/23/23 12:583651421 Benzo(k)fluoranthene ND ug/kg 09/25/23 15:38 207-08-909/23/23 12:583651281 Benzoic Acid ND ug/kg 09/25/23 15:38 65-85-009/23/23 12:5818307851 Benzyl alcohol ND ug/kg 09/25/23 15:38 100-51-609/23/23 12:587312771 4-Bromophenylphenyl ether ND ug/kg 09/25/23 15:38 101-55-309/23/23 12:583651411 Butylbenzylphthalate ND ug/kg 09/25/23 15:38 85-68-709/23/23 12:583651541 4-Chloro-3-methylphenol ND ug/kg 09/25/23 15:38 59-50-709/23/23 12:587312571 4-Chloroaniline ND ug/kg 09/25/23 15:38 106-47-809/23/23 12:587312871 bis(2-Chloroethoxy)methane ND ug/kg 09/25/23 15:38 111-91-109/23/23 12:583651521 bis(2-Chloroethyl) ether ND ug/kg 09/25/23 15:38 111-44-409/23/23 12:583651371 2-Chloronaphthalene ND ug/kg 09/25/23 15:38 91-58-709/23/23 12:583651451 2-Chlorophenol ND ug/kg 09/25/23 15:38 95-57-809/23/23 12:583651371 4-Chlorophenylphenyl ether ND ug/kg 09/25/23 15:38 7005-72-309/23/23 12:583651361 Chrysene ND ug/kg 09/25/23 15:38 218-01-909/23/23 12:583651331 Dibenz(a,h)anthracene ND ug/kg 09/25/23 15:38 53-70-309/23/23 12:583651411 Dibenzofuran ND ug/kg 09/25/23 15:38 132-64-909/23/23 12:583651321 1,2-Dichlorobenzene ND ug/kg 09/25/23 15:38 95-50-109/23/23 12:583651321 1,3-Dichlorobenzene ND ug/kg 09/25/23 15:38 541-73-109/23/23 12:583651301 1,4-Dichlorobenzene ND ug/kg 09/25/23 15:38 106-46-709/23/23 12:583651401 3,3'-Dichlorobenzidine ND ug/kg 09/25/23 15:38 91-94-109/23/23 12:587312471 2,4-Dichlorophenol ND ug/kg 09/25/23 15:38 120-83-209/23/23 12:583651431 Diethylphthalate ND ug/kg 09/25/23 15:38 84-66-209/23/23 12:583651341 2,4-Dimethylphenol ND ug/kg 09/25/23 15:38 105-67-909/23/23 12:583651521 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4 Lab ID:92689576004 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 09/25/23 15:38 131-11-309/23/23 12:583651331 Di-n-butylphthalate ND ug/kg 09/25/23 15:38 84-74-209/23/23 12:583651231 4,6-Dinitro-2-methylphenol ND ug/kg 09/25/23 15:38 534-52-109/23/23 12:587313411 2,4-Dinitrophenol ND ug/kg 09/25/23 15:38 51-28-509/23/23 12:58183011301 2,4-Dinitrotoluene ND ug/kg 09/25/23 15:38 121-14-209/23/23 12:583651411 2,6-Dinitrotoluene ND ug/kg 09/25/23 15:38 606-20-209/23/23 12:583651341 Di-n-octylphthalate ND ug/kg 09/25/23 15:38 117-84-009/23/23 12:583651441 bis(2-Ethylhexyl)phthalate ND ug/kg 09/25/23 15:38 117-81-709/23/23 12:583651421 Fluoranthene ND ug/kg 09/25/23 15:38 206-44-009/23/23 12:583651251 Fluorene ND ug/kg 09/25/23 15:38 86-73-709/23/23 12:583651281 Hexachloro-1,3-butadiene ND ug/kg 09/25/23 15:38 87-68-309/23/23 12:583651581 Hexachlorobenzene ND ug/kg 09/25/23 15:38 118-74-109/23/23 12:583651431 Hexachlorocyclopentadiene ND ug/kg 09/25/23 15:38 77-47-409/23/23 12:583652091 Hexachloroethane ND ug/kg 09/25/23 15:38 67-72-109/23/23 12:583651401 Indeno(1,2,3-cd)pyrene ND ug/kg 09/25/23 15:38 193-39-509/23/23 12:583651441 Isophorone ND ug/kg 09/25/23 15:38 78-59-109/23/23 12:583651631 1-Methylnaphthalene ND ug/kg 09/25/23 15:38 90-12-009/23/23 12:583651281 2-Methylnaphthalene ND ug/kg 09/25/23 15:38 91-57-609/23/23 12:583651461 2-Methylphenol(o-Cresol)ND ug/kg 09/25/23 15:38 95-48-709/23/23 12:583651491 3&4-Methylphenol(m&p Cresol)ND ug/kg 09/25/23 15:38 15831-10-409/23/23 12:583651471 Naphthalene ND ug/kg 09/25/23 15:38 91-20-309/23/23 12:583651241 2-Nitroaniline ND ug/kg 09/25/23 15:38 88-74-409/23/23 12:5818302991 3-Nitroaniline ND ug/kg 09/25/23 15:38 99-09-209/23/23 12:5818302871 4-Nitroaniline ND ug/kg 09/25/23 15:38 100-01-609/23/23 12:587312781 Nitrobenzene ND ug/kg 09/25/23 15:38 98-95-309/23/23 12:583651691 2-Nitrophenol ND ug/kg 09/25/23 15:38 88-75-509/23/23 12:583651581 4-Nitrophenol ND ug/kg 09/25/23 15:38 100-02-709/23/23 12:5818307071 N-Nitrosodimethylamine ND ug/kg 09/25/23 15:38 62-75-909/23/23 12:583651231 N-Nitroso-di-n-propylamine ND ug/kg 09/25/23 15:38 621-64-709/23/23 12:583651371 N-Nitrosodiphenylamine ND ug/kg 09/25/23 15:38 86-30-609/23/23 12:583651301 2,2'-Oxybis(1-chloropropane)ND ug/kg 09/25/23 15:38 108-60-109/23/23 12:583651741 Pentachlorophenol ND ug/kg 09/25/23 15:38 87-86-509/23/23 12:587313581 Phenanthrene ND ug/kg 09/25/23 15:38 85-01-809/23/23 12:583651201 Phenol ND ug/kg 09/25/23 15:38 108-95-209/23/23 12:583651631 Pyrene ND ug/kg 09/25/23 15:38 129-00-009/23/23 12:583651481 Pyridine ND ug/kg 09/25/23 15:38 110-86-109/23/23 12:583651151 1,2,4-Trichlorobenzene ND ug/kg 09/25/23 15:38 120-82-109/23/23 12:583651441 2,4,5-Trichlorophenol ND ug/kg 09/25/23 15:38 95-95-409/23/23 12:583651671 2,4,6-Trichlorophenol ND ug/kg 09/25/23 15:38 88-06-209/23/23 12:583651511 Surrogates Nitrobenzene-d5 (S)25 %09/25/23 15:38 4165-60-009/23/23 12:5810-130 1 2-Fluorobiphenyl (S)37 %09/25/23 15:38 321-60-809/23/23 12:5810-130 1 Terphenyl-d14 (S)61 %09/25/23 15:38 1718-51-009/23/23 12:5810-130 1 Phenol-d6 (S)23 %09/25/23 15:38 13127-88-309/23/23 12:5810-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4 Lab ID:92689576004 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)16 %09/25/23 15:38 367-12-409/23/23 12:5810-130 1 2,4,6-Tribromophenol (S)52 %09/25/23 15:38 118-79-609/23/23 12:5810-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 09/26/23 10:22 67-64-109/25/23 22:4512038.6 1 Benzene ND ug/kg 09/26/23 10:22 71-43-209/25/23 22:456.0 2.4 1 Bromobenzene ND ug/kg 09/26/23 10:22 108-86-109/25/23 22:456.0 2.0 1 Bromochloromethane ND ug/kg 09/26/23 10:22 74-97-509/25/23 22:456.0 1.8 1 Bromodichloromethane ND ug/kg 09/26/23 10:22 75-27-409/25/23 22:456.0 2.3 1 Bromoform ND ug/kg 09/26/23 10:22 75-25-209/25/23 22:456.0 2.1 1 Bromomethane ND ug/kg 09/26/23 10:22 74-83-9 IK09/25/23 22:4524.0 18.6 1 2-Butanone (MEK)ND ug/kg 09/26/23 10:22 78-93-309/25/23 22:4512028.8 1 n-Butylbenzene ND ug/kg 09/26/23 10:22 104-51-809/25/23 22:456.0 3.8 1 sec-Butylbenzene ND ug/kg 09/26/23 10:22 135-98-809/25/23 22:456.0 2.6 1 tert-Butylbenzene ND ug/kg 09/26/23 10:22 98-06-609/25/23 22:456.0 2.1 1 Carbon tetrachloride ND ug/kg 09/26/23 10:22 56-23-509/25/23 22:456.0 2.2 1 Chlorobenzene ND ug/kg 09/26/23 10:22 108-90-709/25/23 22:456.0 3.4 1 Chloroethane ND ug/kg 09/26/23 10:22 75-00-309/25/23 22:4512.0 4.6 1 Chloroform ND ug/kg 09/26/23 10:22 67-66-309/25/23 22:456.0 5.0 1 Chloromethane ND ug/kg 09/26/23 10:22 74-87-309/25/23 22:4512.0 5.0 1 2-Chlorotoluene ND ug/kg 09/26/23 10:22 95-49-809/25/23 22:456.0 2.1 1 4-Chlorotoluene ND ug/kg 09/26/23 10:22 106-43-409/25/23 22:456.0 3.3 1 1,2-Dibromo-3-chloropropane ND ug/kg 09/26/23 10:22 96-12-809/25/23 22:456.0 2.3 1 Dibromochloromethane ND ug/kg 09/26/23 10:22 124-48-109/25/23 22:456.0 3.4 1 1,2-Dibromoethane (EDB)ND ug/kg 09/26/23 10:22 106-93-409/25/23 22:456.0 2.6 1 Dibromomethane ND ug/kg 09/26/23 10:22 74-95-309/25/23 22:456.0 1.3 1 1,2-Dichlorobenzene ND ug/kg 09/26/23 10:22 95-50-109/25/23 22:456.0 2.2 1 1,3-Dichlorobenzene ND ug/kg 09/26/23 10:22 541-73-109/25/23 22:456.0 1.9 1 1,4-Dichlorobenzene ND ug/kg 09/26/23 10:22 106-46-709/25/23 22:456.0 1.6 1 Dichlorodifluoromethane ND ug/kg 09/26/23 10:22 75-71-809/25/23 22:4512.0 6.1 1 1,1-Dichloroethane ND ug/kg 09/26/23 10:22 75-34-309/25/23 22:456.0 2.5 1 1,2-Dichloroethane ND ug/kg 09/26/23 10:22 107-06-209/25/23 22:456.0 4.0 1 1,1-Dichloroethene ND ug/kg 09/26/23 10:22 75-35-409/25/23 22:456.0 2.5 1 cis-1,2-Dichloroethene ND ug/kg 09/26/23 10:22 156-59-209/25/23 22:456.0 2.1 1 trans-1,2-Dichloroethene ND ug/kg 09/26/23 10:22 156-60-509/25/23 22:456.0 5.1 1 1,2-Dichloropropane ND ug/kg 09/26/23 10:22 78-87-509/25/23 22:456.0 1.8 1 1,3-Dichloropropane ND ug/kg 09/26/23 10:22 142-28-909/25/23 22:456.0 1.9 1 2,2-Dichloropropane ND ug/kg 09/26/23 10:22 594-20-709/25/23 22:456.0 4.6 1 1,1-Dichloropropene ND ug/kg 09/26/23 10:22 563-58-609/25/23 22:456.0 2.9 1 cis-1,3-Dichloropropene ND ug/kg 09/26/23 10:22 10061-01-509/25/23 22:456.0 1.6 1 trans-1,3-Dichloropropene ND ug/kg 09/26/23 10:22 10061-02-609/25/23 22:456.0 2.1 1 Diisopropyl ether ND ug/kg 09/26/23 10:22 108-20-309/25/23 22:456.0 1.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4 Lab ID:92689576004 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 09/26/23 10:22 100-41-409/25/23 22:456.0 2.8 1 Hexachloro-1,3-butadiene ND ug/kg 09/26/23 10:22 87-68-3 v209/25/23 22:4512.0 9.8 1 2-Hexanone ND ug/kg 09/26/23 10:22 591-78-609/25/23 22:4560.1 5.8 1 Isopropylbenzene (Cumene)ND ug/kg 09/26/23 10:22 98-82-809/25/23 22:456.0 2.0 1 p-Isopropyltoluene ND ug/kg 09/26/23 10:22 99-87-609/25/23 22:456.0 3.0 1 Methylene Chloride ND ug/kg 09/26/23 10:22 75-09-209/25/23 22:4524.0 16.5 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/23 10:22 108-10-109/25/23 22:4560.1 5.8 1 Methyl-tert-butyl ether ND ug/kg 09/26/23 10:22 1634-04-409/25/23 22:456.0 2.2 1 Naphthalene ND ug/kg 09/26/23 10:22 91-20-309/25/23 22:456.0 3.2 1 n-Propylbenzene ND ug/kg 09/26/23 10:22 103-65-109/25/23 22:456.0 2.1 1 Styrene ND ug/kg 09/26/23 10:22 100-42-509/25/23 22:456.0 1.6 1 1,1,1,2-Tetrachloroethane ND ug/kg 09/26/23 10:22 630-20-609/25/23 22:456.0 2.3 1 1,1,2,2-Tetrachloroethane ND ug/kg 09/26/23 10:22 79-34-509/25/23 22:456.0 1.6 1 Tetrachloroethene ND ug/kg 09/26/23 10:22 127-18-409/25/23 22:456.0 1.9 1 Toluene ND ug/kg 09/26/23 10:22 108-88-309/25/23 22:456.0 4.1 1 1,2,3-Trichlorobenzene ND ug/kg 09/26/23 10:22 87-61-609/25/23 22:456.0 4.9 1 1,2,4-Trichlorobenzene ND ug/kg 09/26/23 10:22 120-82-109/25/23 22:456.0 5.0 1 1,1,1-Trichloroethane ND ug/kg 09/26/23 10:22 71-55-609/25/23 22:456.0 3.1 1 1,1,2-Trichloroethane ND ug/kg 09/26/23 10:22 79-00-509/25/23 22:456.0 2.0 1 Trichloroethene ND ug/kg 09/26/23 10:22 79-01-609/25/23 22:456.0 4.8 1 Trichlorofluoromethane ND ug/kg 09/26/23 10:22 75-69-409/25/23 22:456.0 3.3 1 1,2,3-Trichloropropane ND ug/kg 09/26/23 10:22 96-18-409/25/23 22:456.0 3.0 1 1,2,4-Trimethylbenzene ND ug/kg 09/26/23 10:22 95-63-609/25/23 22:456.0 3.6 1 1,3,5-Trimethylbenzene ND ug/kg 09/26/23 10:22 108-67-809/25/23 22:456.0 2.0 1 Vinyl acetate ND ug/kg 09/26/23 10:22 108-05-409/25/23 22:4560.1 12.4 1 Vinyl chloride ND ug/kg 09/26/23 10:22 75-01-409/25/23 22:4512.0 3.1 1 Xylene (Total)ND ug/kg 09/26/23 10:22 1330-20-709/25/23 22:4512.0 3.4 1 m&p-Xylene ND ug/kg 09/26/23 10:22 179601-23-109/25/23 22:4512.0 4.1 1 o-Xylene ND ug/kg 09/26/23 10:22 95-47-609/25/23 22:456.0 2.7 1 Surrogates Toluene-d8 (S)100 %09/26/23 10:22 2037-26-509/25/23 22:4570-130 1 4-Bromofluorobenzene (S)101 %09/26/23 10:22 460-00-409/25/23 22:4570-130 1 1,2-Dichloroethane-d4 (S)101 %09/26/23 10:22 17060-07-009/25/23 22:4570-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 10 %09/25/23 14:03 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 87.8 %09/29/23 13:0009/29/23 12:491 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4 Lab ID:92689576004 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 10/03/23 03:34 18540-29-909/29/23 12:220.228 0.0581 0.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4d Lab ID:92689576005 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3050 Pace Analytical Services - Ormond Beach 6010 MET ICP Arsenic ND mg/kg 09/29/23 11:17 7440-38-2 D309/28/23 07:462.9 1.5 5 Barium 214 mg/kg 09/29/23 11:17 7440-39-309/28/23 07:462.9 0.49 5 Cadmium 0.24 mg/kg 09/28/23 19:53 7440-43-909/28/23 07:460.059 0.029 1 Chromium 24.3 mg/kg 09/28/23 19:53 7440-47-309/28/23 07:460.29 0.15 1 Lead 5.9 mg/kg 09/28/23 19:53 7439-92-109/28/23 07:460.59 0.29 1 Selenium ND mg/kg 09/28/23 19:53 7782-49-209/28/23 07:460.88 0.44 1 Silver ND mg/kg 09/29/23 11:17 7440-22-4 D309/28/23 07:461.5 0.32 5 Analytical Method: EPA 7471 Preparation Method: EPA 7471 Pace Analytical Services - Ormond Beach 7471 Mercury Mercury 0.0057J mg/kg 10/04/23 11:31 7439-97-610/04/23 07:300.0095 0.0048 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 09/25/23 16:06 83-32-909/23/23 12:583781331 Acenaphthylene ND ug/kg 09/25/23 16:06 208-96-809/23/23 12:583781331 Aniline ND ug/kg 09/25/23 16:06 62-53-309/23/23 12:583781481 Anthracene ND ug/kg 09/25/23 16:06 120-12-709/23/23 12:583781241 Benzo(a)anthracene ND ug/kg 09/25/23 16:06 56-55-309/23/23 12:583781261 Benzo(a)pyrene ND ug/kg 09/25/23 16:06 50-32-809/23/23 12:583781311 Benzo(b)fluoranthene ND ug/kg 09/25/23 16:06 205-99-209/23/23 12:583781261 Benzo(g,h,i)perylene ND ug/kg 09/25/23 16:06 191-24-209/23/23 12:583781471 Benzo(k)fluoranthene ND ug/kg 09/25/23 16:06 207-08-909/23/23 12:583781331 Benzoic Acid ND ug/kg 09/25/23 16:06 65-85-009/23/23 12:5818908121 Benzyl alcohol ND ug/kg 09/25/23 16:06 100-51-609/23/23 12:587562861 4-Bromophenylphenyl ether ND ug/kg 09/25/23 16:06 101-55-309/23/23 12:583781451 Butylbenzylphthalate ND ug/kg 09/25/23 16:06 85-68-709/23/23 12:583781591 4-Chloro-3-methylphenol ND ug/kg 09/25/23 16:06 59-50-709/23/23 12:587562661 4-Chloroaniline ND ug/kg 09/25/23 16:06 106-47-809/23/23 12:587562971 bis(2-Chloroethoxy)methane ND ug/kg 09/25/23 16:06 111-91-109/23/23 12:583781571 bis(2-Chloroethyl) ether ND ug/kg 09/25/23 16:06 111-44-409/23/23 12:583781421 2-Chloronaphthalene ND ug/kg 09/25/23 16:06 91-58-709/23/23 12:583781501 2-Chlorophenol ND ug/kg 09/25/23 16:06 95-57-809/23/23 12:583781421 4-Chlorophenylphenyl ether ND ug/kg 09/25/23 16:06 7005-72-309/23/23 12:583781411 Chrysene ND ug/kg 09/25/23 16:06 218-01-909/23/23 12:583781371 Dibenz(a,h)anthracene ND ug/kg 09/25/23 16:06 53-70-309/23/23 12:583781451 Dibenzofuran ND ug/kg 09/25/23 16:06 132-64-909/23/23 12:583781361 1,2-Dichlorobenzene ND ug/kg 09/25/23 16:06 95-50-109/23/23 12:583781361 1,3-Dichlorobenzene ND ug/kg 09/25/23 16:06 541-73-109/23/23 12:583781341 1,4-Dichlorobenzene ND ug/kg 09/25/23 16:06 106-46-709/23/23 12:583781441 3,3'-Dichlorobenzidine ND ug/kg 09/25/23 16:06 91-94-109/23/23 12:587562551 2,4-Dichlorophenol ND ug/kg 09/25/23 16:06 120-83-209/23/23 12:583781481 Diethylphthalate ND ug/kg 09/25/23 16:06 84-66-209/23/23 12:583781391 2,4-Dimethylphenol ND ug/kg 09/25/23 16:06 105-67-909/23/23 12:583781571 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4d Lab ID:92689576005 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 09/25/23 16:06 131-11-309/23/23 12:583781371 Di-n-butylphthalate ND ug/kg 09/25/23 16:06 84-74-209/23/23 12:583781271 4,6-Dinitro-2-methylphenol ND ug/kg 09/25/23 16:06 534-52-109/23/23 12:587563531 2,4-Dinitrophenol ND ug/kg 09/25/23 16:06 51-28-509/23/23 12:58189011701 2,4-Dinitrotoluene ND ug/kg 09/25/23 16:06 121-14-209/23/23 12:583781451 2,6-Dinitrotoluene ND ug/kg 09/25/23 16:06 606-20-209/23/23 12:583781391 Di-n-octylphthalate ND ug/kg 09/25/23 16:06 117-84-009/23/23 12:583781491 bis(2-Ethylhexyl)phthalate ND ug/kg 09/25/23 16:06 117-81-709/23/23 12:583781471 Fluoranthene ND ug/kg 09/25/23 16:06 206-44-009/23/23 12:583781291 Fluorene ND ug/kg 09/25/23 16:06 86-73-709/23/23 12:583781331 Hexachloro-1,3-butadiene ND ug/kg 09/25/23 16:06 87-68-309/23/23 12:583781641 Hexachlorobenzene ND ug/kg 09/25/23 16:06 118-74-109/23/23 12:583781481 Hexachlorocyclopentadiene ND ug/kg 09/25/23 16:06 77-47-409/23/23 12:583782161 Hexachloroethane ND ug/kg 09/25/23 16:06 67-72-109/23/23 12:583781441 Indeno(1,2,3-cd)pyrene ND ug/kg 09/25/23 16:06 193-39-509/23/23 12:583781491 Isophorone ND ug/kg 09/25/23 16:06 78-59-109/23/23 12:583781681 1-Methylnaphthalene ND ug/kg 09/25/23 16:06 90-12-009/23/23 12:583781331 2-Methylnaphthalene ND ug/kg 09/25/23 16:06 91-57-609/23/23 12:583781511 2-Methylphenol(o-Cresol)ND ug/kg 09/25/23 16:06 95-48-709/23/23 12:583781551 3&4-Methylphenol(m&p Cresol)ND ug/kg 09/25/23 16:06 15831-10-409/23/23 12:583781521 Naphthalene ND ug/kg 09/25/23 16:06 91-20-309/23/23 12:583781281 2-Nitroaniline ND ug/kg 09/25/23 16:06 88-74-409/23/23 12:5818903091 3-Nitroaniline ND ug/kg 09/25/23 16:06 99-09-209/23/23 12:5818902971 4-Nitroaniline ND ug/kg 09/25/23 16:06 100-01-609/23/23 12:587562871 Nitrobenzene ND ug/kg 09/25/23 16:06 98-95-309/23/23 12:583781751 2-Nitrophenol ND ug/kg 09/25/23 16:06 88-75-509/23/23 12:583781641 4-Nitrophenol ND ug/kg 09/25/23 16:06 100-02-709/23/23 12:5818907311 N-Nitrosodimethylamine ND ug/kg 09/25/23 16:06 62-75-909/23/23 12:583781271 N-Nitroso-di-n-propylamine ND ug/kg 09/25/23 16:06 621-64-709/23/23 12:583781421 N-Nitrosodiphenylamine ND ug/kg 09/25/23 16:06 86-30-609/23/23 12:583781341 2,2'-Oxybis(1-chloropropane)ND ug/kg 09/25/23 16:06 108-60-109/23/23 12:583781801 Pentachlorophenol ND ug/kg 09/25/23 16:06 87-86-509/23/23 12:587563701 Phenanthrene ND ug/kg 09/25/23 16:06 85-01-809/23/23 12:583781241 Phenol ND ug/kg 09/25/23 16:06 108-95-209/23/23 12:583781681 Pyrene ND ug/kg 09/25/23 16:06 129-00-009/23/23 12:583781531 Pyridine ND ug/kg 09/25/23 16:06 110-86-109/23/23 12:583781191 1,2,4-Trichlorobenzene ND ug/kg 09/25/23 16:06 120-82-109/23/23 12:583781491 2,4,5-Trichlorophenol ND ug/kg 09/25/23 16:06 95-95-409/23/23 12:583781731 2,4,6-Trichlorophenol ND ug/kg 09/25/23 16:06 88-06-209/23/23 12:583781561 Surrogates Nitrobenzene-d5 (S)33 %09/25/23 16:06 4165-60-009/23/23 12:5810-130 1 2-Fluorobiphenyl (S)26 %09/25/23 16:06 321-60-809/23/23 12:5810-130 1 Terphenyl-d14 (S)34 %09/25/23 16:06 1718-51-009/23/23 12:5810-130 1 Phenol-d6 (S)32 %09/25/23 16:06 13127-88-309/23/23 12:5810-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4d Lab ID:92689576005 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)32 %09/25/23 16:06 367-12-409/23/23 12:5810-130 1 2,4,6-Tribromophenol (S)45 %09/25/23 16:06 118-79-609/23/23 12:5810-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 09/26/23 10:41 67-64-109/25/23 22:4515148.6 1 Benzene ND ug/kg 09/26/23 10:41 71-43-209/25/23 22:457.6 3.0 1 Bromobenzene ND ug/kg 09/26/23 10:41 108-86-109/25/23 22:457.6 2.5 1 Bromochloromethane ND ug/kg 09/26/23 10:41 74-97-509/25/23 22:457.6 2.2 1 Bromodichloromethane ND ug/kg 09/26/23 10:41 75-27-409/25/23 22:457.6 2.9 1 Bromoform ND ug/kg 09/26/23 10:41 75-25-209/25/23 22:457.6 2.7 1 Bromomethane ND ug/kg 09/26/23 10:41 74-83-9 IK09/25/23 22:4530.3 23.5 1 2-Butanone (MEK)ND ug/kg 09/26/23 10:41 78-93-309/25/23 22:4515136.4 1 n-Butylbenzene ND ug/kg 09/26/23 10:41 104-51-809/25/23 22:457.6 4.8 1 sec-Butylbenzene ND ug/kg 09/26/23 10:41 135-98-809/25/23 22:457.6 3.3 1 tert-Butylbenzene ND ug/kg 09/26/23 10:41 98-06-609/25/23 22:457.6 2.7 1 Carbon tetrachloride ND ug/kg 09/26/23 10:41 56-23-509/25/23 22:457.6 2.8 1 Chlorobenzene ND ug/kg 09/26/23 10:41 108-90-709/25/23 22:457.6 4.3 1 Chloroethane ND ug/kg 09/26/23 10:41 75-00-309/25/23 22:4515.1 5.8 1 Chloroform ND ug/kg 09/26/23 10:41 67-66-309/25/23 22:457.6 6.3 1 Chloromethane ND ug/kg 09/26/23 10:41 74-87-309/25/23 22:4515.1 6.4 1 2-Chlorotoluene ND ug/kg 09/26/23 10:41 95-49-809/25/23 22:457.6 2.7 1 4-Chlorotoluene ND ug/kg 09/26/23 10:41 106-43-409/25/23 22:457.6 4.2 1 1,2-Dibromo-3-chloropropane ND ug/kg 09/26/23 10:41 96-12-809/25/23 22:457.6 2.9 1 Dibromochloromethane ND ug/kg 09/26/23 10:41 124-48-109/25/23 22:457.6 4.3 1 1,2-Dibromoethane (EDB)ND ug/kg 09/26/23 10:41 106-93-409/25/23 22:457.6 3.3 1 Dibromomethane ND ug/kg 09/26/23 10:41 74-95-309/25/23 22:457.6 1.6 1 1,2-Dichlorobenzene ND ug/kg 09/26/23 10:41 95-50-109/25/23 22:457.6 2.7 1 1,3-Dichlorobenzene ND ug/kg 09/26/23 10:41 541-73-109/25/23 22:457.6 2.3 1 1,4-Dichlorobenzene ND ug/kg 09/26/23 10:41 106-46-709/25/23 22:457.6 2.0 1 Dichlorodifluoromethane ND ug/kg 09/26/23 10:41 75-71-809/25/23 22:4515.1 7.7 1 1,1-Dichloroethane ND ug/kg 09/26/23 10:41 75-34-309/25/23 22:457.6 3.1 1 1,2-Dichloroethane ND ug/kg 09/26/23 10:41 107-06-209/25/23 22:457.6 5.0 1 1,1-Dichloroethene ND ug/kg 09/26/23 10:41 75-35-409/25/23 22:457.6 3.1 1 cis-1,2-Dichloroethene ND ug/kg 09/26/23 10:41 156-59-209/25/23 22:457.6 2.6 1 trans-1,2-Dichloroethene ND ug/kg 09/26/23 10:41 156-60-509/25/23 22:457.6 6.4 1 1,2-Dichloropropane ND ug/kg 09/26/23 10:41 78-87-509/25/23 22:457.6 2.3 1 1,3-Dichloropropane ND ug/kg 09/26/23 10:41 142-28-909/25/23 22:457.6 2.4 1 2,2-Dichloropropane ND ug/kg 09/26/23 10:41 594-20-709/25/23 22:457.6 5.7 1 1,1-Dichloropropene ND ug/kg 09/26/23 10:41 563-58-609/25/23 22:457.6 3.6 1 cis-1,3-Dichloropropene ND ug/kg 09/26/23 10:41 10061-01-509/25/23 22:457.6 2.1 1 trans-1,3-Dichloropropene ND ug/kg 09/26/23 10:41 10061-02-609/25/23 22:457.6 2.6 1 Diisopropyl ether ND ug/kg 09/26/23 10:41 108-20-309/25/23 22:457.6 2.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4d Lab ID:92689576005 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Ethylbenzene ND ug/kg 09/26/23 10:41 100-41-409/25/23 22:457.6 3.5 1 Hexachloro-1,3-butadiene ND ug/kg 09/26/23 10:41 87-68-3 v209/25/23 22:4515.1 12.4 1 2-Hexanone ND ug/kg 09/26/23 10:41 591-78-609/25/23 22:4575.7 7.3 1 Isopropylbenzene (Cumene)ND ug/kg 09/26/23 10:41 98-82-809/25/23 22:457.6 2.6 1 p-Isopropyltoluene ND ug/kg 09/26/23 10:41 99-87-609/25/23 22:457.6 3.7 1 Methylene Chloride ND ug/kg 09/26/23 10:41 75-09-209/25/23 22:4530.3 20.8 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/23 10:41 108-10-109/25/23 22:4575.7 7.3 1 Methyl-tert-butyl ether ND ug/kg 09/26/23 10:41 1634-04-409/25/23 22:457.6 2.8 1 Naphthalene ND ug/kg 09/26/23 10:41 91-20-309/25/23 22:457.6 4.0 1 n-Propylbenzene ND ug/kg 09/26/23 10:41 103-65-109/25/23 22:457.6 2.7 1 Styrene ND ug/kg 09/26/23 10:41 100-42-509/25/23 22:457.6 2.0 1 1,1,1,2-Tetrachloroethane ND ug/kg 09/26/23 10:41 630-20-609/25/23 22:457.6 2.9 1 1,1,2,2-Tetrachloroethane ND ug/kg 09/26/23 10:41 79-34-509/25/23 22:457.6 2.0 1 Tetrachloroethene ND ug/kg 09/26/23 10:41 127-18-409/25/23 22:457.6 2.4 1 Toluene ND ug/kg 09/26/23 10:41 108-88-309/25/23 22:457.6 5.2 1 1,2,3-Trichlorobenzene ND ug/kg 09/26/23 10:41 87-61-609/25/23 22:457.6 6.1 1 1,2,4-Trichlorobenzene ND ug/kg 09/26/23 10:41 120-82-109/25/23 22:457.6 6.4 1 1,1,1-Trichloroethane ND ug/kg 09/26/23 10:41 71-55-609/25/23 22:457.6 3.9 1 1,1,2-Trichloroethane ND ug/kg 09/26/23 10:41 79-00-509/25/23 22:457.6 2.5 1 Trichloroethene ND ug/kg 09/26/23 10:41 79-01-609/25/23 22:457.6 6.1 1 Trichlorofluoromethane ND ug/kg 09/26/23 10:41 75-69-409/25/23 22:457.6 4.2 1 1,2,3-Trichloropropane ND ug/kg 09/26/23 10:41 96-18-409/25/23 22:457.6 3.8 1 1,2,4-Trimethylbenzene ND ug/kg 09/26/23 10:41 95-63-609/25/23 22:457.6 4.5 1 1,3,5-Trimethylbenzene ND ug/kg 09/26/23 10:41 108-67-809/25/23 22:457.6 2.5 1 Vinyl acetate ND ug/kg 09/26/23 10:41 108-05-409/25/23 22:4575.7 15.6 1 Vinyl chloride ND ug/kg 09/26/23 10:41 75-01-409/25/23 22:4515.1 3.8 1 Xylene (Total)ND ug/kg 09/26/23 10:41 1330-20-709/25/23 22:4515.1 4.3 1 m&p-Xylene ND ug/kg 09/26/23 10:41 179601-23-109/25/23 22:4515.1 5.2 1 o-Xylene ND ug/kg 09/26/23 10:41 95-47-609/25/23 22:457.6 3.3 1 Surrogates Toluene-d8 (S)101 %09/26/23 10:41 2037-26-509/25/23 22:4570-130 1 4-Bromofluorobenzene (S)100 %09/26/23 10:41 460-00-409/25/23 22:4570-130 1 1,2-Dichloroethane-d4 (S)101 %09/26/23 10:41 17060-07-009/25/23 22:4570-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 11.5 %09/25/23 14:03 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 73.9 %09/29/23 13:0009/29/23 12:491 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 93 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Sample:QS-4d Lab ID:92689576005 Collected:09/19/23 14:15 Received:09/20/23 15:35 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 10/03/23 03:39 18540-29-909/29/23 12:220.271 0.0690 0.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2142684 3546 EPA 8141B OP Pesticides 8141B Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:R3981515-1 Associated Lab Samples:92689576006, 92689576007 Matrix:Solid AnalyzedMDL Azinphos, methyl (Guthion)mg/kg ND 0.100 10/02/23 15:030.0318 Bolstar mg/kg ND 0.100 10/02/23 15:030.0149 Chlorpyrifos mg/kg ND 0.100 10/02/23 15:030.0157 Coumaphos mg/kg ND 0.100 10/02/23 15:030.0243 Total Demeton mg/kg ND 0.0700 10/02/23 15:030.00584 Diazinon mg/kg ND 0.100 10/02/23 15:030.0225 Dichlorvos mg/kg ND 0.100 10/02/23 15:030.0300 Dimethoate mg/kg ND 0.100 10/02/23 15:030.0334 Disulfoton mg/kg ND 0.100 10/02/23 15:030.0254 EPN (ENT)mg/kg ND 0.100 10/02/23 15:030.0276 Ethoprop mg/kg ND 0.100 10/02/23 15:030.0118 Parathion (Ethyl parathion)mg/kg ND 0.100 10/02/23 15:030.0164 Fensulfothion mg/kg ND 0.100 10/02/23 15:030.0353 Fenthion mg/kg ND 0.100 10/02/23 15:030.0133 Malathion mg/kg ND 0.100 10/02/23 15:030.0179 Merphos mg/kg ND 0.100 10/02/23 15:030.0232 Methyl parathion mg/kg ND 0.100 10/02/23 15:030.0203 Mevinphos mg/kg ND 0.100 10/02/23 15:030.0230 Naled mg/kg ND 0.100 10/02/23 15:030.0480 Phorate mg/kg ND 0.100 10/02/23 15:030.0210 Ronnel mg/kg ND 0.100 10/02/23 15:030.0149 Stirophos (Tetrachlorvinphos)mg/kg ND 0.100 10/02/23 15:030.0178 Sulfotepp (Thiodiphosphoric Ac mg/kg ND 0.100 10/02/23 15:030.00986 TEPP mg/kg ND 1.00 10/02/23 15:030.157 Tokuthion (Prothiofos)mg/kg ND 0.100 10/02/23 15:030.0150 Trichloronate mg/kg ND 0.100 10/02/23 15:030.0201 Triphenylphosphate (S)%85.6 36.0-121 10/02/23 15:03 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3981515-2LABORATORY CONTROL SAMPLE: LCSSpike Azinphos, methyl (Guthion)mg/kg 0.2900.333 87.1 58.0-125 Bolstar mg/kg 0.2990.333 89.8 64.0-120 Chlorpyrifos mg/kg 0.2890.333 86.8 62.0-120 Coumaphos mg/kg 0.2850.333 85.6 60.0-120 Total Demeton mg/kg 0.1500.167 89.8 59.0-120 Diazinon mg/kg 0.2780.333 83.5 49.0-120 Dichlorvos mg/kg 0.1990.333 59.8 37.0-120 Dimethoate mg/kg 0.2640.333 79.3 46.0-127 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3981515-2LABORATORY CONTROL SAMPLE: LCSSpike Disulfoton mg/kg 0.3010.333 90.4 60.0-121 EPN (ENT)mg/kg 0.2750.333 82.6 60.0-121 Ethoprop mg/kg 0.3180.333 95.5 59.0-120 Parathion (Ethyl parathion)mg/kg 0.2850.333 85.6 62.0-120 Fensulfothion mg/kg 0.2860.333 85.9 58.0-123 Fenthion mg/kg 0.3010.333 90.4 61.0-121 Malathion mg/kg 0.2880.333 86.5 59.0-120 Merphos mg/kg 0.2880.333 86.5 59.0-120 Methyl parathion mg/kg 0.2810.333 84.4 63.0-120 Mevinphos mg/kg 0.2610.333 78.4 50.0-120 Naled mg/kg 0.1630.333 48.9 10.0-125 Phorate mg/kg 0.2930.333 88.0 60.0-120 Ronnel mg/kg 0.2980.333 89.5 62.0-120 Stirophos (Tetrachlorvinphos)mg/kg 0.2810.333 84.4 62.0-120 Sulfotepp (Thiodiphosphoric Ac mg/kg 0.2920.333 87.7 62.0-122 TEPP mg/kg 0.5123.33 15.4 10.0-135 Tokuthion (Prothiofos)mg/kg 0.3020.333 90.7 63.0-120 Trichloronate mg/kg 0.2930.333 88.0 62.0-120 Triphenylphosphate (S)%88.3 36.0-121 Parameter Units MS Result % Rec Limits Qual% RecConc. R3981515-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1659891-08 R3981515-4 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Azinphos, methyl (Guthion)mg/kg 0.320 82.5 10.0-16085.3 5.17 220.326ND 0.264 0.278 Bolstar mg/kg 0.320 83.4 10.0-15186.2 5.11 200.326ND 0.267 0.281 Chlorpyrifos mg/kg 0.320 80.0 12.0-14983.1 5.69 200.326ND 0.256 0.271 Coumaphos mg/kg 0.320 79.1 10.0-16081.6 5.01 220.326ND 0.253 0.266 Total Demeton mg/kg 0.160 86.3 10.0-16090.2 6.32 230.163ND 0.138 0.147 Diazinon mg/kg 0.320 82.8 11.0-15785.9 5.50 200.326ND 0.265 0.280 Dichlorvos mg/kg 0.320 80.0 10.0-16090.5 14.2 240.326ND 0.256 0.295 Dimethoate mg/kg 0.320 84.7 10.0-15086.5 3.98 270.326ND 0.271 0.282 Disulfoton mg/kg 0.320 83.1 12.0-15586.5 5.84 200.326ND 0.266 0.282 EPN (ENT)mg/kg 0.320 86.9 10.0-15987.4 2.49 200.326ND 0.278 0.285 Ethoprop mg/kg 0.320 88.4 11.0-15695.4 9.43 200.326ND 0.283 0.311 Parathion (Ethyl parathion)mg/kg 0.320 85.9 10.0-14788.7 4.96 200.326ND 0.275 0.289 Fensulfothion mg/kg 0.320 86.9 10.0-15789.3 4.57 270.326ND 0.278 0.291 Fenthion mg/kg 0.320 84.1 13.0-15587.1 5.42 200.326ND 0.269 0.284 Malathion mg/kg 0.320 85.3 13.0-13788.3 5.35 210.326ND 0.273 0.288 Merphos mg/kg 0.320 75.9 10.0-14780.4 7.52 260.326ND 0.243 0.262 Methyl parathion mg/kg 0.320 80.0 10.0-15083.1 5.69 210.326ND 0.256 0.271 Mevinphos mg/kg 0.320 77.2 10.0-15881.3 7.03 240.326ND 0.247 0.265 Naled mg/kg 0.320 35.6 10.0-13725.6 30.8 400.326ND 0.114 0.0836 Phorate mg/kg 0.320 80.6 13.0-15484.7 6.74 200.326ND 0.258 0.276 Ronnel mg/kg 0.320 82.5 14.0-14985.9 5.88 200.326ND 0.264 0.280 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. R3981515-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1659891-08 R3981515-4 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Stirophos (Tetrachlorvinphos)mg/kg 0.320 78.4 10.0-15081.3 5.43 200.326ND 0.251 0.265 Sulfotepp (Thiodiphosphoric Ac mg/kg 0.320 85.3 10.0-16089.0 6.04 200.326ND 0.273 0.290 TEPP mg/kg 3.20 46.9 10.0-14254.9 17.6 283.26ND 1.50 1.79 Tokuthion (Prothiofos)mg/kg 0.320 83.8 12.0-15386.5 5.09 200.326ND 0.268 0.282 Trichloronate mg/kg 0.320 81.3 12.0-15284.0 5.24 200.326ND 0.260 0.274 Triphenylphosphate (S)%82.5 36.0-12182.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2140051 8151A EPA 8151A Chlorinated Herb. (GC) 8151A Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:R3980478-1 Associated Lab Samples:92689576006, 92689576007 Matrix:Solid AnalyzedMDL 2,4-D mg/kg ND 0.0700 10/02/23 04:430.00702 Dalapon mg/kg ND 0.0700 10/02/23 04:430.0113 2,4-DB mg/kg ND 0.0700 10/02/23 04:430.0297 Dicamba mg/kg ND 0.0700 10/02/23 04:430.0157 Dichlorprop mg/kg ND 0.0700 10/02/23 04:430.0245 Dinoseb mg/kg ND 0.0700 10/02/23 04:430.00697 MCPA mg/kg ND 6.50 10/02/23 04:430.443 2-(2-methyl-4-chlorophenoxy)pa mg/kg ND 6.50 10/02/23 04:430.367 2,4,5-T mg/kg ND 0.0700 10/02/23 04:430.00852 2,4,5-TP (Silvex)mg/kg ND 0.0700 10/02/23 04:430.0107 2,4-DCAA (S)%83.2 22.0-132 10/02/23 04:43 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3980478-2LABORATORY CONTROL SAMPLE: LCSSpike 2,4-D mg/kg 0.1640.167 98.2 40.0-120 Dalapon mg/kg 0.1120.167 67.1 15.0-120 2,4-DB mg/kg 0.1550.167 92.8 25.0-143 Dicamba mg/kg 0.1360.167 81.4 43.0-120 Dichlorprop mg/kg 0.1480.167 88.6 32.0-129 Dinoseb mg/kg 0.1330.167 79.6 10.0-120 MCPA mg/kg 12.316.7 73.7 31.0-121 2-(2-methyl-4-chlorophenoxy)pa mg/kg 9.5416.7 57.1 28.0-133 2,4,5-T mg/kg 0.1640.167 98.2 41.0-120 2,4,5-TP (Silvex)mg/kg 0.1520.167 91.0 42.0-120 2,4-DCAA (S)%82.0 22.0-132 Parameter Units MS Result % Rec Limits Qual% RecConc. R3980478-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1659170-03 R3980478-4 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2,4-D mg/kg E0.206 115 10.0-160110 3.75 240.207ND 0.237 0.228 Dalapon mg/kg 0.206 72.1 10.0-12171.1 0.844 270.207ND 0.148 0.147 2,4-DB mg/kg 0.206 75.8 10.0-16078.3 3.92 220.207ND 0.156 0.162 Dicamba mg/kg 0.206 73.9 10.0-15477.7 5.58 210.207ND 0.152 0.161 Dichlorprop mg/kg 0.206 81.2 10.0-15886.7 7.19 200.207ND 0.167 0.180 Dinoseb mg/kg 0.206 61.2 10.0-12069.3 13.0 400.207ND 0.126 0.143 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. R3980478-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1659170-03 R3980478-4 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. MCPA mg/kg 20.6 78.8 10.0-16090.4 14.3 4020.7ND 16.2 18.7 2-(2-methyl-4- chlorophenoxy)pa mg/kg P920.6 55.4 10.0-16057.1 3.65 4020.7ND 11.4 11.8 2,4,5-T mg/kg 0.206 78.8 10.0-15784.3 7.41 200.207ND 0.162 0.175 2,4,5-TP (Silvex)mg/kg 0.206 72.1 10.0-15677.7 8.06 200.207ND 0.148 0.161 2,4-DCAA (S)%81.2 22.0-13278.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 954341 EPA 7471 EPA 7471 7471 Mercury Laboratory:Pace Analytical Services - Ormond Beach Associated Lab Samples:92689576001, 92689576002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:5247764 Associated Lab Samples:92689576001, 92689576002 Matrix:Solid AnalyzedMDL Mercury mg/kg ND 0.0086 10/02/23 13:080.0043 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 5247765LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.0820.085 97 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 5247766MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92689624010 5247767 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg 0.117 95 80-12096 8 200.127ND 0.12 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 954620 EPA 7471 EPA 7471 7471 Mercury Laboratory:Pace Analytical Services - Ormond Beach Associated Lab Samples:92689576003, 92689576004, 92689576006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:5249501 Associated Lab Samples:92689576003, 92689576004, 92689576006 Matrix:Solid AnalyzedMDL Mercury mg/kg 0.0050J 0.0083 10/03/23 13:060.0042 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 5249502LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.0810.081 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 5249503MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 35829666001 5249504 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg 0.089 81 80-12081 6 200.0970.038 0.12 0.13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 954842 EPA 7471 EPA 7471 7471 Mercury Laboratory:Pace Analytical Services - Ormond Beach Associated Lab Samples:92689576005, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:5250360 Associated Lab Samples:92689576005, 92689576007 Matrix:Solid AnalyzedMDL Mercury mg/kg ND 0.0088 10/04/23 10:590.0044 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 5250361LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.0770.085 90 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 5250362MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 35829666002 5250363 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg 0.069 86 80-12099 12 200.0690.0096 0.069 0.078 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 953507 EPA 3050 EPA 6010 6010 MET Solid Laboratory:Pace Analytical Services - Ormond Beach Associated Lab Samples:92689576001, 92689576002, 92689576004, 92689576005, 92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:5242681 Associated Lab Samples:92689576001, 92689576002, 92689576004, 92689576005, 92689576006, 92689576007 Matrix:Solid AnalyzedMDL Arsenic mg/kg ND 0.60 09/29/23 12:460.30 Barium mg/kg ND 0.60 09/29/23 12:460.10 Cadmium mg/kg ND 0.060 09/29/23 12:460.030 Chromium mg/kg ND 0.30 09/29/23 12:460.15 Lead mg/kg ND 0.60 09/29/23 12:460.30 Selenium mg/kg ND 0.90 09/29/23 12:460.45 Silver mg/kg ND 0.30 09/29/23 12:460.066 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 5242682LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/kg 13.014.2 91 80-120 Barium mg/kg 14.614.2 102 80-120 Cadmium mg/kg 1.41.4 97 80-120 Chromium mg/kg 14.214.2 100 80-120 Lead mg/kg 14.314.2 101 80-120 Selenium mg/kg 13.014.2 91 80-120 Silver mg/kg 1.41.4 98 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 5242683MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 35829388002 5242684 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/kg M1,R118.5 81 75-125636 143 2018.55.4 20.4 124 Barium mg/kg M1,R118.5 343 75-125235 22 2018.535.8 99.5 79.5 Cadmium mg/kg R11.84 80 75-125113 29 201.840.36 1.8 2.5 Chromium mg/kg M1,R118.5 19 75-125243 83 2018.525.6 29.2 70.8 Lead mg/kg 18.5 101 75-125115 9 2018.59.1 27.9 30.5 Selenium mg/kg 18.5 81 75-12592 13 2018.50.57U 15.4 17.5 Silver mg/kg 1.84 104 75-12598 5 201.840.11J 2.0 1.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 954343 EPA 3050 EPA 6010 6010 MET Solid Laboratory:Pace Analytical Services - Ormond Beach Associated Lab Samples:92689576003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:5247777 Associated Lab Samples:92689576003 Matrix:Solid AnalyzedMDL Arsenic mg/kg ND 0.57 10/02/23 19:040.29 Barium mg/kg ND 0.57 10/02/23 19:040.096 Cadmium mg/kg ND 0.057 10/02/23 19:040.029 Chromium mg/kg ND 0.29 10/02/23 19:040.14 Lead mg/kg ND 0.57 10/02/23 19:040.29 Selenium mg/kg ND 0.86 10/02/23 19:040.43 Silver mg/kg ND 0.29 10/02/23 19:040.063 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 5247778LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/kg 12.413.8 90 80-120 Barium mg/kg 14.413.8 105 80-120 Cadmium mg/kg 1.41.4 98 80-120 Chromium mg/kg 14.013.8 102 80-120 Lead mg/kg 14.013.8 102 80-120 Selenium mg/kg 12.513.8 91 80-120 Silver mg/kg 1.31.4 95 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 5247779MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 35830353001 5247780 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/kg 520 88 75-12588 2 2051210.6U 460 451 Barium mg/kg 520 119 75-12592 20 20512194810665 Cadmium mg/kg 51.6 96 75-12595 3 2051.61.1U 50.5 48.9 Chromium mg/kg 520 99 75-12599 1 2051228.4 541 534 Lead mg/kg 520 98 75-125100 0 2051218.3J 526 527 Selenium mg/kg 520 88 75-12588 2 2051215.8U 461 451 Silver mg/kg 51.6 99 75-12595 6 2051.62.3U 51.7 48.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 53 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 801920 EPA 5035A/5030B EPA 8260D 8260D 5035A 5030B Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576001, 92689576002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4154094 Associated Lab Samples:92689576001, 92689576002 Matrix:Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/25/23 21:081.9 1,1,1-Trichloroethane ug/kg ND 5.0 09/25/23 21:082.6 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/25/23 21:081.3 1,1,2-Trichloroethane ug/kg ND 5.0 09/25/23 21:081.7 1,1-Dichloroethane ug/kg ND 5.0 09/25/23 21:082.1 1,1-Dichloroethene ug/kg ND 5.0 v109/25/23 21:082.1 1,1-Dichloropropene ug/kg ND 5.0 09/25/23 21:082.4 1,2,3-Trichlorobenzene ug/kg ND 5.0 09/25/23 21:084.0 1,2,3-Trichloropropane ug/kg ND 5.0 09/25/23 21:082.5 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/25/23 21:084.2 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/25/23 21:083.0 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/25/23 21:081.9 1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/25/23 21:082.2 1,2-Dichlorobenzene ug/kg ND 5.0 09/25/23 21:081.8 1,2-Dichloroethane ug/kg ND 5.0 09/25/23 21:083.3 1,2-Dichloropropane ug/kg ND 5.0 09/25/23 21:081.5 1,3,5-Trimethylbenzene ug/kg ND 5.0 09/25/23 21:081.7 1,3-Dichlorobenzene ug/kg ND 5.0 09/25/23 21:081.6 1,3-Dichloropropane ug/kg ND 5.0 09/25/23 21:081.6 1,4-Dichlorobenzene ug/kg ND 5.0 09/25/23 21:081.3 2,2-Dichloropropane ug/kg ND 5.0 09/25/23 21:083.8 2-Butanone (MEK)ug/kg ND 100 09/25/23 21:0824.0 2-Chlorotoluene ug/kg ND 5.0 09/25/23 21:081.8 2-Hexanone ug/kg ND 50.0 09/25/23 21:084.8 4-Chlorotoluene ug/kg ND 5.0 09/25/23 21:082.8 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/25/23 21:084.8 Acetone ug/kg ND 100 09/25/23 21:0832.1 Benzene ug/kg ND 5.0 09/25/23 21:082.0 Bromobenzene ug/kg ND 5.0 09/25/23 21:081.6 Bromochloromethane ug/kg ND 5.0 09/25/23 21:081.5 Bromodichloromethane ug/kg ND 5.0 09/25/23 21:081.9 Bromoform ug/kg ND 5.0 09/25/23 21:081.8 Bromomethane ug/kg ND 20.0 09/25/23 21:0815.5 Carbon tetrachloride ug/kg ND 5.0 09/25/23 21:081.9 Chlorobenzene ug/kg ND 5.0 09/25/23 21:082.9 Chloroethane ug/kg ND 10.0 09/25/23 21:083.9 Chloroform ug/kg ND 5.0 09/25/23 21:084.2 Chloromethane ug/kg ND 10.0 09/25/23 21:084.2 cis-1,2-Dichloroethene ug/kg ND 5.0 09/25/23 21:081.7 cis-1,3-Dichloropropene ug/kg ND 5.0 09/25/23 21:081.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 54 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4154094 Associated Lab Samples:92689576001, 92689576002 Matrix:Solid AnalyzedMDL Dibromochloromethane ug/kg ND 5.0 09/25/23 21:082.8 Dibromomethane ug/kg ND 5.0 09/25/23 21:081.1 Dichlorodifluoromethane ug/kg ND 10.0 v109/25/23 21:085.1 Diisopropyl ether ug/kg ND 5.0 09/25/23 21:081.4 Ethylbenzene ug/kg ND 5.0 09/25/23 21:082.3 Hexachloro-1,3-butadiene ug/kg ND 10.0 09/25/23 21:088.2 Isopropylbenzene (Cumene)ug/kg ND 5.0 09/25/23 21:081.7 m&p-Xylene ug/kg ND 10.0 09/25/23 21:083.4 Methyl-tert-butyl ether ug/kg ND 5.0 09/25/23 21:081.9 Methylene Chloride ug/kg ND 20.0 09/25/23 21:0813.7 n-Butylbenzene ug/kg ND 5.0 09/25/23 21:083.2 n-Propylbenzene ug/kg ND 5.0 09/25/23 21:081.8 Naphthalene ug/kg ND 5.0 09/25/23 21:082.6 o-Xylene ug/kg ND 5.0 09/25/23 21:082.2 p-Isopropyltoluene ug/kg ND 5.0 09/25/23 21:082.5 sec-Butylbenzene ug/kg ND 5.0 09/25/23 21:082.2 Styrene ug/kg ND 5.0 09/25/23 21:081.3 tert-Butylbenzene ug/kg ND 5.0 09/25/23 21:081.8 Tetrachloroethene ug/kg ND 5.0 09/25/23 21:081.6 Toluene ug/kg ND 5.0 09/25/23 21:083.4 trans-1,2-Dichloroethene ug/kg ND 5.0 09/25/23 21:084.2 trans-1,3-Dichloropropene ug/kg ND 5.0 09/25/23 21:081.7 Trichloroethene ug/kg ND 5.0 09/25/23 21:084.0 Trichlorofluoromethane ug/kg ND 5.0 09/25/23 21:082.8 Vinyl acetate ug/kg ND 50.0 09/25/23 21:0810.3 Vinyl chloride ug/kg ND 10.0 09/25/23 21:082.5 Xylene (Total)ug/kg ND 10.0 09/25/23 21:082.8 1,2-Dichloroethane-d4 (S)%104 70-130 09/25/23 21:08 4-Bromofluorobenzene (S)%100 70-130 09/25/23 21:08 Toluene-d8 (S)%100 70-130 09/25/23 21:08 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4154095LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 575500 115 70-130 1,1,1-Trichloroethane ug/kg 548500 110 70-130 1,1,2,2-Tetrachloroethane ug/kg 571500 114 70-130 1,1,2-Trichloroethane ug/kg 552500 110 70-130 1,1-Dichloroethane ug/kg 546500 109 70-130 1,1-Dichloroethene ug/kg 613 v150012370-132 1,1-Dichloropropene ug/kg 573500 115 70-130 1,2,3-Trichlorobenzene ug/kg 526500 105 62-136 1,2,3-Trichloropropane ug/kg 573500 115 70-130 1,2,4-Trichlorobenzene ug/kg 520500 104 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 55 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4154095LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 575500 115 70-130 1,2-Dibromo-3-chloropropane ug/kg 542500 108 65-130 1,2-Dibromoethane (EDB)ug/kg 566500 113 70-130 1,2-Dichlorobenzene ug/kg 533500 107 70-130 1,2-Dichloroethane ug/kg 558500 112 70-130 1,2-Dichloropropane ug/kg 567500 113 70-130 1,3,5-Trimethylbenzene ug/kg 554500 111 70-130 1,3-Dichlorobenzene ug/kg 551500 110 70-130 1,3-Dichloropropane ug/kg 575500 115 70-130 1,4-Dichlorobenzene ug/kg 546500 109 70-130 2,2-Dichloropropane ug/kg 522500 104 60-130 2-Butanone (MEK)ug/kg 10501000 105 66-130 2-Chlorotoluene ug/kg 564500 113 70-130 2-Hexanone ug/kg 11301000 113 68-130 4-Chlorotoluene ug/kg 563500 113 70-130 4-Methyl-2-pentanone (MIBK)ug/kg 11001000 110 70-130 Acetone ug/kg 9781000 98 60-130 Benzene ug/kg 539500 108 70-130 Bromobenzene ug/kg 577500 115 70-130 Bromochloromethane ug/kg 507500 101 70-130 Bromodichloromethane ug/kg 547500 109 70-130 Bromoform ug/kg 587500 117 70-130 Bromomethane ug/kg 521500 104 43-175 Carbon tetrachloride ug/kg 569500 114 70-130 Chlorobenzene ug/kg 556500 111 70-130 Chloroethane ug/kg 568500 114 70-145 Chloroform ug/kg 553500 111 70-130 Chloromethane ug/kg 556500 111 66-146 cis-1,2-Dichloroethene ug/kg 545500 109 70-130 cis-1,3-Dichloropropene ug/kg 542500 108 70-130 Dibromochloromethane ug/kg 561500 112 70-130 Dibromomethane ug/kg 568500 114 70-130 Dichlorodifluoromethane ug/kg 770 v150015442-197 Diisopropyl ether ug/kg 545500 109 68-130 Ethylbenzene ug/kg 508500 102 70-130 Hexachloro-1,3-butadiene ug/kg 529500 106 70-130 Isopropylbenzene (Cumene)ug/kg 565500 113 70-130 m&p-Xylene ug/kg 11201000 112 70-130 Methyl-tert-butyl ether ug/kg 509500 102 70-130 Methylene Chloride ug/kg 517500 103 65-130 n-Butylbenzene ug/kg 568500 114 70-130 n-Propylbenzene ug/kg 564500 113 70-130 Naphthalene ug/kg 582500 116 65-135 o-Xylene ug/kg 566500 113 70-130 p-Isopropyltoluene ug/kg 560500 112 70-130 sec-Butylbenzene ug/kg 569500 114 70-130 Styrene ug/kg 566500 113 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 56 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4154095LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 529500 106 70-130 Tetrachloroethene ug/kg 567500 113 70-130 Toluene ug/kg 537500 107 70-130 trans-1,2-Dichloroethene ug/kg 572500 114 70-130 trans-1,3-Dichloropropene ug/kg 529500 106 70-130 Trichloroethene ug/kg 550500 110 70-130 Trichlorofluoromethane ug/kg 530500 106 62-140 Vinyl acetate ug/kg 10701000 107 70-140 Vinyl chloride ug/kg 526500 105 70-152 Xylene (Total)ug/kg 16901500 113 70-130 1,2-Dichloroethane-d4 (S)%98 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%98 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4154096MATRIX SPIKE SAMPLE: MSSpike Result 92689696003 1,1,1,2-Tetrachloroethane ug/kg 506775 65 22-166ND 1,1,1-Trichloroethane ug/kg 553775 71 23-172ND 1,1,2,2-Tetrachloroethane ug/kg 444775 57 21-158ND 1,1,2-Trichloroethane ug/kg 483775 62 25-160ND 1,1-Dichloroethane ug/kg 547775 71 22-166ND 1,1-Dichloroethene ug/kg 629 v17758118-183ND 1,1-Dichloropropene ug/kg 553775 71 20-181ND 1,2,3-Trichlorobenzene ug/kg 377775 49 10-161ND 1,2,3-Trichloropropane ug/kg 442775 57 21-147ND 1,2,4-Trichlorobenzene ug/kg 378775 49 10-159ND 1,2,4-Trimethylbenzene ug/kg 465775 60 17-170ND 1,2-Dibromo-3-chloropropane ug/kg 385775 50 10-135ND 1,2-Dibromoethane (EDB)ug/kg 452775 58 30-154ND 1,2-Dichlorobenzene ug/kg 443775 57 26-162ND 1,2-Dichloroethane ug/kg 523775 68 23-161ND 1,2-Dichloropropane ug/kg 511775 66 29-165ND 1,3,5-Trimethylbenzene ug/kg 470775 61 20-172ND 1,3-Dichlorobenzene ug/kg 452775 58 22-164ND 1,3-Dichloropropane ug/kg 480775 62 27-156ND 1,4-Dichlorobenzene ug/kg 447775 58 20-161ND 2,2-Dichloropropane ug/kg 490775 63 10-159ND 2-Butanone (MEK)ug/kg 8671550 56 13-143ND 2-Chlorotoluene ug/kg 480775 62 21-166ND 2-Hexanone ug/kg 7711550 50 19-145ND 4-Chlorotoluene ug/kg 462775 60 19-163ND 4-Methyl-2-pentanone (MIBK)ug/kg 8071550 52 21-151ND Acetone ug/kg 7321550 47 10-133ND Benzene ug/kg 507775 65 29-156ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 57 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4154096MATRIX SPIKE SAMPLE: MSSpike Result 92689696003 Bromobenzene ug/kg 495775 64 25-161ND Bromochloromethane ug/kg 493775 64 27-158ND Bromodichloromethane ug/kg 471775 61 23-158ND Bromoform ug/kg 419775 54 19-152ND Bromomethane ug/kg 227775 29 10-152ND Carbon tetrachloride ug/kg 531775 69 18-172ND Chlorobenzene ug/kg 488775 63 26-166ND Chloroethane ug/kg 94.6775 12 10-130ND Chloroform ug/kg 536775 69 25-161ND Chloromethane ug/kg 600775 77 27-197ND cis-1,2-Dichloroethene ug/kg 550775 71 28-165ND cis-1,3-Dichloropropene ug/kg 470775 61 23-159ND Dibromochloromethane ug/kg 442775 57 21-151ND Dibromomethane ug/kg 475775 61 38-158ND Dichlorodifluoromethane ug/kg 926 v177512010-200ND Diisopropyl ether ug/kg 507775 65 23-160ND Ethylbenzene ug/kg 450775 58 22-163ND Hexachloro-1,3-butadiene ug/kg 391775 50 10-192ND Isopropylbenzene (Cumene)ug/kg 500775 65 24-173ND m&p-Xylene ug/kg 9741550 63 22-171ND Methyl-tert-butyl ether ug/kg 462775 60 25-153ND Methylene Chloride ug/kg 534775 69 10-165ND n-Butylbenzene ug/kg 421775 54 10-186ND n-Propylbenzene ug/kg 469775 61 16-171ND Naphthalene ug/kg 431775 56 10-159ND o-Xylene ug/kg 484775 63 23-171ND p-Isopropyltoluene ug/kg 440775 57 13-184ND sec-Butylbenzene ug/kg 477775 62 16-182ND Styrene ug/kg 486775 63 25-169ND tert-Butylbenzene ug/kg 427775 55 20-174ND Tetrachloroethene ug/kg 433775 56 14-171ND Toluene ug/kg 491775 63 24-166ND trans-1,2-Dichloroethene ug/kg 548775 71 24-170ND trans-1,3-Dichloropropene ug/kg 443775 57 22-157ND Trichloroethene ug/kg 488775 63 23-176ND Trichlorofluoromethane ug/kg 362775 47 10-138ND Vinyl acetate ug/kg 8901550 57 11-166ND Vinyl chloride ug/kg 491775 63 21-200ND Xylene (Total)ug/kg 14602330 63 23-170ND 1,2-Dichloroethane-d4 (S)%106 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 58 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92689696004 4154097SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 30ND 1,1,1-Trichloroethane ug/kg ND 30ND 1,1,2,2-Tetrachloroethane ug/kg ND 30ND 1,1,2-Trichloroethane ug/kg ND 30ND 1,1-Dichloroethane ug/kg ND 30ND 1,1-Dichloroethene ug/kg ND v130ND 1,1-Dichloropropene ug/kg ND 30ND 1,2,3-Trichlorobenzene ug/kg ND 30ND 1,2,3-Trichloropropane ug/kg ND 30ND 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2,4-Trimethylbenzene ug/kg 9.7J 309.0J 1,2-Dibromo-3-chloropropane ug/kg ND 30ND 1,2-Dibromoethane (EDB)ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,2-Dichloroethane ug/kg ND 30ND 1,2-Dichloropropane ug/kg ND 30ND 1,3,5-Trimethylbenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,3-Dichloropropane ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 2,2-Dichloropropane ug/kg ND 30ND 2-Butanone (MEK)ug/kg ND 30ND 2-Chlorotoluene ug/kg ND 30ND 2-Hexanone ug/kg ND 30ND 4-Chlorotoluene ug/kg ND 30ND 4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND Acetone ug/kg ND 30ND Benzene ug/kg ND 30ND Bromobenzene ug/kg ND 30ND Bromochloromethane ug/kg ND 30ND Bromodichloromethane ug/kg ND 30ND Bromoform ug/kg ND 30ND Bromomethane ug/kg ND 30ND Carbon tetrachloride ug/kg ND 30ND Chlorobenzene ug/kg ND 30ND Chloroethane ug/kg ND 30ND Chloroform ug/kg ND 30ND Chloromethane ug/kg ND 30ND cis-1,2-Dichloroethene ug/kg ND 30ND cis-1,3-Dichloropropene ug/kg ND 30ND Dibromochloromethane ug/kg ND 30ND Dibromomethane ug/kg ND 30ND Dichlorodifluoromethane ug/kg ND v130ND Diisopropyl ether ug/kg ND 30ND Ethylbenzene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Isopropylbenzene (Cumene)ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 59 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92689696004 4154097SAMPLE DUPLICATE: m&p-Xylene ug/kg 7.3J 30ND Methyl-tert-butyl ether ug/kg ND 30ND Methylene Chloride ug/kg ND 30ND n-Butylbenzene ug/kg ND 30ND n-Propylbenzene ug/kg ND 30ND Naphthalene ug/kg ND 30ND o-Xylene ug/kg ND 30ND p-Isopropyltoluene ug/kg ND 30ND sec-Butylbenzene ug/kg ND 30ND Styrene ug/kg ND 30ND tert-Butylbenzene ug/kg ND 30ND Tetrachloroethene ug/kg ND 30ND Toluene ug/kg ND 30ND trans-1,2-Dichloroethene ug/kg ND 30ND trans-1,3-Dichloropropene ug/kg ND 30ND Trichloroethene ug/kg ND 30ND Trichlorofluoromethane ug/kg ND 30ND Vinyl acetate ug/kg ND 30ND Vinyl chloride ug/kg ND 30ND Xylene (Total)ug/kg ND 30ND 1,2-Dichloroethane-d4 (S)%111110 4-Bromofluorobenzene (S)%100101 Toluene-d8 (S)%101102 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 60 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 801923 EPA 5035A/5030B EPA 8260D 8260D 5035A 5030B Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576003, 92689576004, 92689576005, 92689576006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4154099 Associated Lab Samples:92689576003, 92689576004, 92689576005, 92689576006 Matrix:Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/26/23 09:451.9 1,1,1-Trichloroethane ug/kg ND 5.0 09/26/23 09:452.6 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/26/23 09:451.3 1,1,2-Trichloroethane ug/kg ND 5.0 09/26/23 09:451.7 1,1-Dichloroethane ug/kg ND 5.0 09/26/23 09:452.1 1,1-Dichloroethene ug/kg ND 5.0 09/26/23 09:452.1 1,1-Dichloropropene ug/kg ND 5.0 09/26/23 09:452.4 1,2,3-Trichlorobenzene ug/kg ND 5.0 09/26/23 09:454.0 1,2,3-Trichloropropane ug/kg ND 5.0 09/26/23 09:452.5 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/26/23 09:454.2 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/26/23 09:453.0 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/26/23 09:451.9 1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/26/23 09:452.2 1,2-Dichlorobenzene ug/kg ND 5.0 09/26/23 09:451.8 1,2-Dichloroethane ug/kg ND 5.0 09/26/23 09:453.3 1,2-Dichloropropane ug/kg ND 5.0 09/26/23 09:451.5 1,3,5-Trimethylbenzene ug/kg ND 5.0 09/26/23 09:451.7 1,3-Dichlorobenzene ug/kg ND 5.0 09/26/23 09:451.6 1,3-Dichloropropane ug/kg ND 5.0 09/26/23 09:451.6 1,4-Dichlorobenzene ug/kg ND 5.0 09/26/23 09:451.3 2,2-Dichloropropane ug/kg ND 5.0 09/26/23 09:453.8 2-Butanone (MEK)ug/kg ND 100 09/26/23 09:4524.0 2-Chlorotoluene ug/kg ND 5.0 09/26/23 09:451.8 2-Hexanone ug/kg ND 50.0 09/26/23 09:454.8 4-Chlorotoluene ug/kg ND 5.0 09/26/23 09:452.8 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/26/23 09:454.8 Acetone ug/kg ND 100 09/26/23 09:4532.1 Benzene ug/kg ND 5.0 09/26/23 09:452.0 Bromobenzene ug/kg ND 5.0 09/26/23 09:451.6 Bromochloromethane ug/kg ND 5.0 09/26/23 09:451.5 Bromodichloromethane ug/kg ND 5.0 09/26/23 09:451.9 Bromoform ug/kg ND 5.0 09/26/23 09:451.8 Bromomethane ug/kg ND 20.0 IK09/26/23 09:4515.5 Carbon tetrachloride ug/kg ND 5.0 09/26/23 09:451.9 Chlorobenzene ug/kg ND 5.0 09/26/23 09:452.9 Chloroethane ug/kg ND 10.0 09/26/23 09:453.9 Chloroform ug/kg ND 5.0 09/26/23 09:454.2 Chloromethane ug/kg ND 10.0 09/26/23 09:454.2 cis-1,2-Dichloroethene ug/kg ND 5.0 09/26/23 09:451.7 cis-1,3-Dichloropropene ug/kg ND 5.0 09/26/23 09:451.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 61 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4154099 Associated Lab Samples:92689576003, 92689576004, 92689576005, 92689576006 Matrix:Solid AnalyzedMDL Dibromochloromethane ug/kg ND 5.0 09/26/23 09:452.8 Dibromomethane ug/kg ND 5.0 09/26/23 09:451.1 Dichlorodifluoromethane ug/kg ND 10.0 09/26/23 09:455.1 Diisopropyl ether ug/kg ND 5.0 09/26/23 09:451.4 Ethylbenzene ug/kg ND 5.0 09/26/23 09:452.3 Hexachloro-1,3-butadiene ug/kg ND 10.0 v209/26/23 09:458.2 Isopropylbenzene (Cumene)ug/kg ND 5.0 09/26/23 09:451.7 m&p-Xylene ug/kg ND 10.0 09/26/23 09:453.4 Methyl-tert-butyl ether ug/kg ND 5.0 09/26/23 09:451.9 Methylene Chloride ug/kg ND 20.0 09/26/23 09:4513.7 n-Butylbenzene ug/kg ND 5.0 09/26/23 09:453.2 n-Propylbenzene ug/kg ND 5.0 09/26/23 09:451.8 Naphthalene ug/kg ND 5.0 09/26/23 09:452.6 o-Xylene ug/kg ND 5.0 09/26/23 09:452.2 p-Isopropyltoluene ug/kg ND 5.0 09/26/23 09:452.5 sec-Butylbenzene ug/kg ND 5.0 09/26/23 09:452.2 Styrene ug/kg ND 5.0 09/26/23 09:451.3 tert-Butylbenzene ug/kg ND 5.0 09/26/23 09:451.8 Tetrachloroethene ug/kg ND 5.0 09/26/23 09:451.6 Toluene ug/kg ND 5.0 09/26/23 09:453.4 trans-1,2-Dichloroethene ug/kg ND 5.0 09/26/23 09:454.2 trans-1,3-Dichloropropene ug/kg ND 5.0 09/26/23 09:451.7 Trichloroethene ug/kg ND 5.0 09/26/23 09:454.0 Trichlorofluoromethane ug/kg ND 5.0 09/26/23 09:452.8 Vinyl acetate ug/kg ND 50.0 09/26/23 09:4510.3 Vinyl chloride ug/kg ND 10.0 09/26/23 09:452.5 Xylene (Total)ug/kg ND 10.0 09/26/23 09:452.8 1,2-Dichloroethane-d4 (S)%102 70-130 09/26/23 09:45 4-Bromofluorobenzene (S)%101 70-130 09/26/23 09:45 Toluene-d8 (S)%101 70-130 09/26/23 09:45 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4154100LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 471500 94 70-130 1,1,1-Trichloroethane ug/kg 431500 86 70-130 1,1,2,2-Tetrachloroethane ug/kg 478500 96 70-130 1,1,2-Trichloroethane ug/kg 468500 94 70-130 1,1-Dichloroethane ug/kg 434500 87 70-130 1,1-Dichloroethene ug/kg 436500 87 70-132 1,1-Dichloropropene ug/kg 444500 89 70-130 1,2,3-Trichlorobenzene ug/kg 463500 93 62-136 1,2,3-Trichloropropane ug/kg 450500 90 70-130 1,2,4-Trichlorobenzene ug/kg 451500 90 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 62 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4154100LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 440500 88 70-130 1,2-Dibromo-3-chloropropane ug/kg 457500 91 65-130 1,2-Dibromoethane (EDB)ug/kg 469500 94 70-130 1,2-Dichlorobenzene ug/kg 477500 95 70-130 1,2-Dichloroethane ug/kg 446500 89 70-130 1,2-Dichloropropane ug/kg 452500 90 70-130 1,3,5-Trimethylbenzene ug/kg 433500 87 70-130 1,3-Dichlorobenzene ug/kg 473500 95 70-130 1,3-Dichloropropane ug/kg 451500 90 70-130 1,4-Dichlorobenzene ug/kg 479500 96 70-130 2,2-Dichloropropane ug/kg 411500 82 60-130 2-Butanone (MEK)ug/kg 8821000 88 66-130 2-Chlorotoluene ug/kg 431500 86 70-130 2-Hexanone ug/kg 9851000 99 68-130 4-Chlorotoluene ug/kg 436500 87 70-130 4-Methyl-2-pentanone (MIBK)ug/kg 9331000 93 70-130 Acetone ug/kg 8581000 86 60-130 Benzene ug/kg 441500 88 70-130 Bromobenzene ug/kg 463500 93 70-130 Bromochloromethane ug/kg 463500 93 70-130 Bromodichloromethane ug/kg 448500 90 70-130 Bromoform ug/kg 483500 97 70-130 Bromomethane ug/kg 463 IK5009343-175 Carbon tetrachloride ug/kg 446500 89 70-130 Chlorobenzene ug/kg 451500 90 70-130 Chloroethane ug/kg 469500 94 70-145 Chloroform ug/kg 431500 86 70-130 Chloromethane ug/kg 453500 91 66-146 cis-1,2-Dichloroethene ug/kg 439500 88 70-130 cis-1,3-Dichloropropene ug/kg 446500 89 70-130 Dibromochloromethane ug/kg 461500 92 70-130 Dibromomethane ug/kg 472500 94 70-130 Dichlorodifluoromethane ug/kg 454500 91 42-197 Diisopropyl ether ug/kg 415500 83 68-130 Ethylbenzene ug/kg 482500 96 70-130 Hexachloro-1,3-butadiene ug/kg 382 v35007670-130 Isopropylbenzene (Cumene)ug/kg 447500 89 70-130 m&p-Xylene ug/kg 8871000 89 70-130 Methyl-tert-butyl ether ug/kg 409500 82 70-130 Methylene Chloride ug/kg 447500 89 65-130 n-Butylbenzene ug/kg 444500 89 70-130 n-Propylbenzene ug/kg 417500 83 70-130 Naphthalene ug/kg 464500 93 65-135 o-Xylene ug/kg 445500 89 70-130 p-Isopropyltoluene ug/kg 437500 87 70-130 sec-Butylbenzene ug/kg 412500 82 70-130 Styrene ug/kg 471500 94 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 63 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4154100LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 435500 87 70-130 Tetrachloroethene ug/kg 445500 89 70-130 Toluene ug/kg 437500 87 70-130 trans-1,2-Dichloroethene ug/kg 440500 88 70-130 trans-1,3-Dichloropropene ug/kg 459500 92 70-130 Trichloroethene ug/kg 451500 90 70-130 Trichlorofluoromethane ug/kg 407500 81 62-140 Vinyl acetate ug/kg 8971000 90 70-140 Vinyl chloride ug/kg 415500 83 70-152 Xylene (Total)ug/kg 13301500 89 70-130 1,2-Dichloroethane-d4 (S)%94 70-130 4-Bromofluorobenzene (S)%104 70-130 Toluene-d8 (S)%99 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 4154101MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92689624010 4154102 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 964 88 22-16687 1 30964ND849839 1,1,1-Trichloroethane ug/kg 964 88 23-17285 4 30964ND851818 1,1,2,2-Tetrachloroethane ug/kg 964 90 21-15889 1 30964ND869858 1,1,2-Trichloroethane ug/kg 964 90 25-16087 3 30964ND866842 1,1-Dichloroethane ug/kg 964 84 22-16687 4 30964ND810840 1,1-Dichloroethene ug/kg 964 89 18-18387 2 30964ND858841 1,1-Dichloropropene ug/kg 964 89 20-18181 9 30964ND863785 1,2,3-Trichlorobenzene ug/kg 964 79 10-16174 6 30964ND760717 1,2,3-Trichloropropane ug/kg 964 82 21-14780 3 30964ND787768 1,2,4-Trichlorobenzene ug/kg 964 82 10-15972 12 30964ND787699 1,2,4-Trimethylbenzene ug/kg 964 79 17-17073 9 30964ND764701 1,2-Dibromo-3- chloropropane ug/kg 964 76 10-13575 2 30964ND738724 1,2-Dibromoethane (EDB)ug/kg 964 87 30-15487 1 30964ND835839 1,2-Dichlorobenzene ug/kg 964 89 26-16285 4 30964ND858822 1,2-Dichloroethane ug/kg 964 86 23-16188 3 30964ND828849 1,2-Dichloropropane ug/kg 964 90 29-16588 3 30964ND868845 1,3,5-Trimethylbenzene ug/kg 964 79 20-17272 9 30964ND765697 1,3-Dichlorobenzene ug/kg 964 87 22-16478 10 30964ND838755 1,3-Dichloropropane ug/kg 964 84 27-15685 1 30964ND812823 1,4-Dichlorobenzene ug/kg 964 87 20-16181 7 30964ND841786 2,2-Dichloropropane ug/kg 964 79 10-15979 0 30964ND759762 2-Butanone (MEK)ug/kg 1930 85 13-14380 6 301930ND16401550 2-Chlorotoluene ug/kg 964 79 21-16675 6 30964ND766724 2-Hexanone ug/kg 1930 87 19-14581 7 301930ND16701560 4-Chlorotoluene ug/kg 964 79 19-16373 7 30964ND759707 4-Methyl-2-pentanone (MIBK)ug/kg 1930 88 21-15183 6 301930ND16901600 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 64 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4154101MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92689624010 4154102 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Acetone ug/kg 1930 71 10-13369 3 301930ND13701330 Benzene ug/kg 964 85 29-15685 1 30964ND817823 Bromobenzene ug/kg 964 85 25-16181 4 30964ND821785 Bromochloromethane ug/kg 964 88 27-15891 2 30964ND853875 Bromodichloromethane ug/kg 964 83 23-15884 1 30964ND805814 Bromoform ug/kg 964 85 19-15287 2 30964ND822841 Bromomethane ug/kg IK9641510-15217 11 30964ND146162 Carbon tetrachloride ug/kg 964 87 18-17282 6 30964ND842789 Chlorobenzene ug/kg 964 84 26-16682 3 30964ND813788 Chloroethane ug/kg 964 22 10-13022 3 30964ND210216 Chloroform ug/kg 964 85 25-16186 1 30964ND821831 Chloromethane ug/kg 964 117 27-197115 2 30964ND11301110 cis-1,2-Dichloroethene ug/kg 964 85 28-16586 1 30964ND824831 cis-1,3-Dichloropropene ug/kg 964 85 23-15985 1 30964ND822817 Dibromochloromethane ug/kg 964 84 21-15186 2 30964ND810825 Dibromomethane ug/kg 964 88 38-15889 0 30964ND853854 Dichlorodifluoromethane ug/kg 964 121 10-200108 12 30964ND11701040 Diisopropyl ether ug/kg 964 84 23-16083 1 30964ND807797 Ethylbenzene ug/kg 964 91 22-16386 6 30964ND879829 Hexachloro-1,3-butadiene ug/kg v39647510-19265 13 30964ND720631 Isopropylbenzene (Cumene)ug/kg 964 86 24-17379 8 30964ND831764 m&p-Xylene ug/kg 1930 83 22-17176 8 301930ND15901470 Methyl-tert-butyl ether ug/kg 964 78 25-15379 2 30964ND749763 Methylene Chloride ug/kg 964 91 10-16594 3 30964ND880904 n-Butylbenzene ug/kg 964 82 10-18672 13 30964ND790693 n-Propylbenzene ug/kg 964 77 16-17170 9 30964ND742677 Naphthalene ug/kg 964 77 10-15975 3 30964ND743724 o-Xylene ug/kg 964 85 23-17182 4 30964ND824787 p-Isopropyltoluene ug/kg 964 79 13-18471 11 30964ND767688 sec-Butylbenzene ug/kg 964 78 16-18271 9 30964ND749688 Styrene ug/kg 964 87 25-16983 4 30964ND841806 tert-Butylbenzene ug/kg 964 61 20-17459 4 30964ND588567 Tetrachloroethene ug/kg 964 78 14-17169 13 30964ND756666 Toluene ug/kg 964 86 24-16682 5 30964ND829789 trans-1,2-Dichloroethene ug/kg 964 85 24-17081 5 30964ND817780 trans-1,3-Dichloropropene ug/kg 964 85 22-15784 2 30964ND823807 Trichloroethene ug/kg 964 87 23-17681 7 30964ND839782 Trichlorofluoromethane ug/kg 964 20 10-13818 11 30964ND190170 Vinyl acetate ug/kg 1930 83 11-16682 1 301930ND16001590 Vinyl chloride ug/kg 964 88 21-20088 1 30964ND851846 Xylene (Total)ug/kg 2900 84 23-17078 7 302900ND24202260 1,2-Dichloroethane-d4 (S)%100 70-13098 4-Bromofluorobenzene (S)%102 70-130103 Toluene-d8 (S)%101 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 65 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 802240 EPA 5035A/5030B EPA 8260D 8260D 5035A 5030B Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4155661 Associated Lab Samples:92689576007 Matrix:Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/26/23 23:171.9 1,1,1-Trichloroethane ug/kg ND 5.0 09/26/23 23:172.6 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/26/23 23:171.3 1,1,2-Trichloroethane ug/kg ND 5.0 09/26/23 23:171.7 1,1-Dichloroethane ug/kg ND 5.0 09/26/23 23:172.1 1,1-Dichloroethene ug/kg ND 5.0 09/26/23 23:172.1 1,1-Dichloropropene ug/kg ND 5.0 09/26/23 23:172.4 1,2,3-Trichlorobenzene ug/kg ND 5.0 09/26/23 23:174.0 1,2,3-Trichloropropane ug/kg ND 5.0 09/26/23 23:172.5 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/26/23 23:174.2 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/26/23 23:173.0 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/26/23 23:171.9 1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/26/23 23:172.2 1,2-Dichlorobenzene ug/kg ND 5.0 09/26/23 23:171.8 1,2-Dichloroethane ug/kg ND 5.0 09/26/23 23:173.3 1,2-Dichloropropane ug/kg ND 5.0 09/26/23 23:171.5 1,3,5-Trimethylbenzene ug/kg ND 5.0 09/26/23 23:171.7 1,3-Dichlorobenzene ug/kg ND 5.0 09/26/23 23:171.6 1,3-Dichloropropane ug/kg ND 5.0 09/26/23 23:171.6 1,4-Dichlorobenzene ug/kg ND 5.0 09/26/23 23:171.3 2,2-Dichloropropane ug/kg ND 5.0 09/26/23 23:173.8 2-Butanone (MEK)ug/kg ND 100 09/26/23 23:1724.0 2-Chlorotoluene ug/kg ND 5.0 09/26/23 23:171.8 2-Hexanone ug/kg ND 50.0 09/26/23 23:174.8 4-Chlorotoluene ug/kg ND 5.0 09/26/23 23:172.8 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/26/23 23:174.8 Acetone ug/kg ND 100 09/26/23 23:1732.1 Benzene ug/kg ND 5.0 09/26/23 23:172.0 Bromobenzene ug/kg ND 5.0 09/26/23 23:171.6 Bromochloromethane ug/kg ND 5.0 09/26/23 23:171.5 Bromodichloromethane ug/kg ND 5.0 09/26/23 23:171.9 Bromoform ug/kg ND 5.0 09/26/23 23:171.8 Bromomethane ug/kg ND 20.0 IK09/26/23 23:1715.5 Carbon tetrachloride ug/kg ND 5.0 09/26/23 23:171.9 Chlorobenzene ug/kg ND 5.0 09/26/23 23:172.9 Chloroethane ug/kg ND 10.0 09/26/23 23:173.9 Chloroform ug/kg ND 5.0 09/26/23 23:174.2 Chloromethane ug/kg ND 10.0 09/26/23 23:174.2 cis-1,2-Dichloroethene ug/kg ND 5.0 09/26/23 23:171.7 cis-1,3-Dichloropropene ug/kg ND 5.0 09/26/23 23:171.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 66 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4155661 Associated Lab Samples:92689576007 Matrix:Solid AnalyzedMDL Dibromochloromethane ug/kg ND 5.0 09/26/23 23:172.8 Dibromomethane ug/kg ND 5.0 09/26/23 23:171.1 Dichlorodifluoromethane ug/kg ND 10.0 09/26/23 23:175.1 Diisopropyl ether ug/kg ND 5.0 09/26/23 23:171.4 Ethylbenzene ug/kg ND 5.0 09/26/23 23:172.3 Hexachloro-1,3-butadiene ug/kg ND 10.0 09/26/23 23:178.2 Isopropylbenzene (Cumene)ug/kg ND 5.0 09/26/23 23:171.7 m&p-Xylene ug/kg ND 10.0 09/26/23 23:173.4 Methyl-tert-butyl ether ug/kg ND 5.0 09/26/23 23:171.9 Methylene Chloride ug/kg ND 20.0 09/26/23 23:1713.7 n-Butylbenzene ug/kg ND 5.0 09/26/23 23:173.2 n-Propylbenzene ug/kg ND 5.0 09/26/23 23:171.8 Naphthalene ug/kg ND 5.0 09/26/23 23:172.6 o-Xylene ug/kg ND 5.0 09/26/23 23:172.2 p-Isopropyltoluene ug/kg ND 5.0 09/26/23 23:172.5 sec-Butylbenzene ug/kg ND 5.0 09/26/23 23:172.2 Styrene ug/kg ND 5.0 09/26/23 23:171.3 tert-Butylbenzene ug/kg ND 5.0 09/26/23 23:171.8 Tetrachloroethene ug/kg ND 5.0 09/26/23 23:171.6 Toluene ug/kg ND 5.0 09/26/23 23:173.4 trans-1,2-Dichloroethene ug/kg ND 5.0 09/26/23 23:174.2 trans-1,3-Dichloropropene ug/kg ND 5.0 09/26/23 23:171.7 Trichloroethene ug/kg ND 5.0 09/26/23 23:174.0 Trichlorofluoromethane ug/kg ND 5.0 09/26/23 23:172.8 Vinyl acetate ug/kg ND 50.0 09/26/23 23:1710.3 Vinyl chloride ug/kg ND 10.0 09/26/23 23:172.5 Xylene (Total)ug/kg ND 10.0 09/26/23 23:172.8 1,2-Dichloroethane-d4 (S)%103 70-130 09/26/23 23:17 4-Bromofluorobenzene (S)%98 70-130 09/26/23 23:17 Toluene-d8 (S)%102 70-130 09/26/23 23:17 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4155662LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 474500 95 70-130 1,1,1-Trichloroethane ug/kg 445500 89 70-130 1,1,2,2-Tetrachloroethane ug/kg 485500 97 70-130 1,1,2-Trichloroethane ug/kg 461500 92 70-130 1,1-Dichloroethane ug/kg 444500 89 70-130 1,1-Dichloroethene ug/kg 459500 92 70-132 1,1-Dichloropropene ug/kg 457500 91 70-130 1,2,3-Trichlorobenzene ug/kg 471500 94 62-136 1,2,3-Trichloropropane ug/kg 449500 90 70-130 1,2,4-Trichlorobenzene ug/kg 466500 93 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 67 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4155662LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 451500 90 70-130 1,2-Dibromo-3-chloropropane ug/kg 464500 93 65-130 1,2-Dibromoethane (EDB)ug/kg 466500 93 70-130 1,2-Dichlorobenzene ug/kg 482500 96 70-130 1,2-Dichloroethane ug/kg 450500 90 70-130 1,2-Dichloropropane ug/kg 448500 90 70-130 1,3,5-Trimethylbenzene ug/kg 436500 87 70-130 1,3-Dichlorobenzene ug/kg 474500 95 70-130 1,3-Dichloropropane ug/kg 450500 90 70-130 1,4-Dichlorobenzene ug/kg 489500 98 70-130 2,2-Dichloropropane ug/kg 455500 91 60-130 2-Butanone (MEK)ug/kg 9311000 93 66-130 2-Chlorotoluene ug/kg 440500 88 70-130 2-Hexanone ug/kg 9931000 99 68-130 4-Chlorotoluene ug/kg 449500 90 70-130 4-Methyl-2-pentanone (MIBK)ug/kg 9371000 94 70-130 Acetone ug/kg 8941000 89 60-130 Benzene ug/kg 444500 89 70-130 Bromobenzene ug/kg 455500 91 70-130 Bromochloromethane ug/kg 467500 93 70-130 Bromodichloromethane ug/kg 449500 90 70-130 Bromoform ug/kg 484500 97 70-130 Bromomethane ug/kg 489 IK5009843-175 Carbon tetrachloride ug/kg 449500 90 70-130 Chlorobenzene ug/kg 455500 91 70-130 Chloroethane ug/kg 491500 98 70-145 Chloroform ug/kg 445500 89 70-130 Chloromethane ug/kg 496500 99 66-146 cis-1,2-Dichloroethene ug/kg 451500 90 70-130 cis-1,3-Dichloropropene ug/kg 453500 91 70-130 Dibromochloromethane ug/kg 462500 92 70-130 Dibromomethane ug/kg 466500 93 70-130 Dichlorodifluoromethane ug/kg 504500 101 42-197 Diisopropyl ether ug/kg 427500 85 68-130 Ethylbenzene ug/kg 485500 97 70-130 Hexachloro-1,3-butadiene ug/kg 395500 79 70-130 Isopropylbenzene (Cumene)ug/kg 459500 92 70-130 m&p-Xylene ug/kg 8881000 89 70-130 Methyl-tert-butyl ether ug/kg 414500 83 70-130 Methylene Chloride ug/kg 466500 93 65-130 n-Butylbenzene ug/kg 473500 95 70-130 n-Propylbenzene ug/kg 427500 85 70-130 Naphthalene ug/kg 461500 92 65-135 o-Xylene ug/kg 457500 91 70-130 p-Isopropyltoluene ug/kg 446500 89 70-130 sec-Butylbenzene ug/kg 427500 85 70-130 Styrene ug/kg 474500 95 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 68 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4155662LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 444500 89 70-130 Tetrachloroethene ug/kg 459500 92 70-130 Toluene ug/kg 438500 88 70-130 trans-1,2-Dichloroethene ug/kg 454500 91 70-130 trans-1,3-Dichloropropene ug/kg 460500 92 70-130 Trichloroethene ug/kg 455500 91 70-130 Trichlorofluoromethane ug/kg 428500 86 62-140 Vinyl acetate ug/kg 9251000 92 70-140 Vinyl chloride ug/kg 440500 88 70-152 Xylene (Total)ug/kg 13501500 90 70-130 1,2-Dichloroethane-d4 (S)%95 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4155663MATRIX SPIKE SAMPLE: MSSpike Result 92689754002 1,1,1,2-Tetrachloroethane ug/kg 781715 109 22-166ND 1,1,1-Trichloroethane ug/kg 785715 110 23-172ND 1,1,2,2-Tetrachloroethane ug/kg 796715 111 21-158ND 1,1,2-Trichloroethane ug/kg 810715 113 25-160ND 1,1-Dichloroethane ug/kg 777715 109 22-166ND 1,1-Dichloroethene ug/kg 760715 106 18-183ND 1,1-Dichloropropene ug/kg 730715 102 20-181ND 1,2,3-Trichlorobenzene ug/kg 593715 83 10-161ND 1,2,3-Trichloropropane ug/kg 743715 104 21-147ND 1,2,4-Trichlorobenzene ug/kg 581715 81 10-159ND 1,2,4-Trimethylbenzene ug/kg 656715 92 17-170ND 1,2-Dibromo-3-chloropropane ug/kg 673715 94 10-135ND 1,2-Dibromoethane (EDB)ug/kg 781715 109 30-154ND 1,2-Dichlorobenzene ug/kg 760715 106 26-162ND 1,2-Dichloroethane ug/kg 788715 110 23-161ND 1,2-Dichloropropane ug/kg 779715 109 29-165ND 1,3,5-Trimethylbenzene ug/kg 650715 91 20-172ND 1,3-Dichlorobenzene ug/kg 688715 96 22-164ND 1,3-Dichloropropane ug/kg 750715 105 27-156ND 1,4-Dichlorobenzene ug/kg 712715 100 20-161ND 2,2-Dichloropropane ug/kg 746715 104 10-159ND 2-Butanone (MEK)ug/kg 15701420 110 13-143ND 2-Chlorotoluene ug/kg 653715 91 21-166ND 2-Hexanone ug/kg 15501420 109 19-145ND 4-Chlorotoluene ug/kg 650715 91 19-163ND 4-Methyl-2-pentanone (MIBK)ug/kg 16001420 112 21-151ND Acetone ug/kg 12501420 88 10-133ND Benzene ug/kg 755715 106 29-156ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 69 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4155663MATRIX SPIKE SAMPLE: MSSpike Result 92689754002 Bromobenzene ug/kg 737715 103 25-161ND Bromochloromethane ug/kg 825715 115 27-158ND Bromodichloromethane ug/kg 758715 106 23-158ND Bromoform ug/kg 792715 111 19-152ND Bromomethane ug/kg 116 IK7151610-152ND Carbon tetrachloride ug/kg 756715 106 18-172ND Chlorobenzene ug/kg 719715 101 26-166ND Chloroethane ug/kg 172715 24 10-130ND Chloroform ug/kg 771715 108 25-161ND Chloromethane ug/kg 887715 124 27-197ND cis-1,2-Dichloroethene ug/kg 779715 109 28-165ND cis-1,3-Dichloropropene ug/kg 784715 110 23-159ND Dibromochloromethane ug/kg 771715 108 21-151ND Dibromomethane ug/kg 823715 115 38-158ND Dichlorodifluoromethane ug/kg 923715 129 10-200ND Diisopropyl ether ug/kg 756715 106 23-160ND Ethylbenzene ug/kg 749715 105 22-163ND Hexachloro-1,3-butadiene ug/kg 516715 72 10-192ND Isopropylbenzene (Cumene)ug/kg 715715 100 24-173ND m&p-Xylene ug/kg 13401420 94 22-171ND Methyl-tert-butyl ether ug/kg 732715 102 25-153ND Methylene Chloride ug/kg 789715 110 10-165ND n-Butylbenzene ug/kg 616715 86 10-186ND n-Propylbenzene ug/kg 610715 85 16-171ND Naphthalene ug/kg 662715 93 10-159ND o-Xylene ug/kg 722715 101 23-171ND p-Isopropyltoluene ug/kg 632715 88 13-184ND sec-Butylbenzene ug/kg 622715 87 16-182ND Styrene ug/kg 740715 104 25-169ND tert-Butylbenzene ug/kg 538715 75 20-174ND Tetrachloroethene ug/kg 590715 83 14-171ND Toluene ug/kg 724715 101 24-166ND trans-1,2-Dichloroethene ug/kg 713715 100 24-170ND trans-1,3-Dichloropropene ug/kg 777715 109 22-157ND Trichloroethene ug/kg 732715 102 23-176ND Trichlorofluoromethane ug/kg 112715 16 10-138ND Vinyl acetate ug/kg 14901420 104 11-166ND Vinyl chloride ug/kg 755715 106 21-200ND Xylene (Total)ug/kg 20702150 96 23-170ND 1,2-Dichloroethane-d4 (S)%100 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 70 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92689754003 4155664SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 30ND 1,1,1-Trichloroethane ug/kg ND 30ND 1,1,2,2-Tetrachloroethane ug/kg ND 30ND 1,1,2-Trichloroethane ug/kg ND 30ND 1,1-Dichloroethane ug/kg ND 30ND 1,1-Dichloroethene ug/kg ND 30ND 1,1-Dichloropropene ug/kg ND 30ND 1,2,3-Trichlorobenzene ug/kg ND 30ND 1,2,3-Trichloropropane ug/kg ND 30ND 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2,4-Trimethylbenzene ug/kg ND 30ND 1,2-Dibromo-3-chloropropane ug/kg ND 30ND 1,2-Dibromoethane (EDB)ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,2-Dichloroethane ug/kg ND 30ND 1,2-Dichloropropane ug/kg ND 30ND 1,3,5-Trimethylbenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,3-Dichloropropane ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 2,2-Dichloropropane ug/kg ND 30ND 2-Butanone (MEK)ug/kg ND 30ND 2-Chlorotoluene ug/kg ND 30ND 2-Hexanone ug/kg ND 30ND 4-Chlorotoluene ug/kg ND 30ND 4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND Acetone ug/kg ND 30ND Benzene ug/kg ND 30ND Bromobenzene ug/kg ND 30ND Bromochloromethane ug/kg ND 30ND Bromodichloromethane ug/kg ND 30ND Bromoform ug/kg ND 30ND Bromomethane ug/kg ND IK30ND Carbon tetrachloride ug/kg ND 30ND Chlorobenzene ug/kg ND 30ND Chloroethane ug/kg ND 30ND Chloroform ug/kg ND 30ND Chloromethane ug/kg ND 30ND cis-1,2-Dichloroethene ug/kg ND 30ND cis-1,3-Dichloropropene ug/kg ND 30ND Dibromochloromethane ug/kg ND 30ND Dibromomethane ug/kg ND 30ND Dichlorodifluoromethane ug/kg ND 30ND Diisopropyl ether ug/kg ND 30ND Ethylbenzene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Isopropylbenzene (Cumene)ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 71 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92689754003 4155664SAMPLE DUPLICATE: m&p-Xylene ug/kg ND 30ND Methyl-tert-butyl ether ug/kg ND 30ND Methylene Chloride ug/kg ND 30ND n-Butylbenzene ug/kg ND 30ND n-Propylbenzene ug/kg ND 30ND Naphthalene ug/kg ND 30ND o-Xylene ug/kg ND 30ND p-Isopropyltoluene ug/kg ND 30ND sec-Butylbenzene ug/kg ND 30ND Styrene ug/kg ND 30ND tert-Butylbenzene ug/kg ND 30ND Tetrachloroethene ug/kg ND 30ND Toluene ug/kg ND 30ND trans-1,2-Dichloroethene ug/kg ND 30ND trans-1,3-Dichloropropene ug/kg ND 30ND Trichloroethene ug/kg ND 30ND Trichlorofluoromethane ug/kg ND 30ND Vinyl acetate ug/kg ND 30ND Vinyl chloride ug/kg ND 30ND Xylene (Total)ug/kg ND 30ND 1,2-Dichloroethane-d4 (S)%101100 4-Bromofluorobenzene (S)%100100 Toluene-d8 (S)%101101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 72 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 802129 EPA 3546 EPA 8082A 8082 GCS PCB Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4155030 Associated Lab Samples:92689576006, 92689576007 Matrix:Solid AnalyzedMDL PCB-1016 (Aroclor 1016)ug/kg ND 33.0 09/27/23 21:1313.1 PCB-1221 (Aroclor 1221)ug/kg ND 33.0 09/27/23 21:1322.2 PCB-1232 (Aroclor 1232)ug/kg ND 33.0 09/27/23 21:1314.7 PCB-1242 (Aroclor 1242)ug/kg ND 33.0 09/27/23 21:138.0 PCB-1248 (Aroclor 1248)ug/kg ND 33.0 09/27/23 21:138.9 PCB-1254 (Aroclor 1254)ug/kg ND 33.0 09/27/23 21:1314.5 PCB-1260 (Aroclor 1260)ug/kg ND 33.0 09/27/23 21:1314.6 Decachlorobiphenyl (S)%60 10-174 09/27/23 21:13 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4155031LABORATORY CONTROL SAMPLE: LCSSpike PCB-1016 (Aroclor 1016)ug/kg 103164 63 36-130 PCB-1260 (Aroclor 1260)ug/kg 115164 70 38-133 Decachlorobiphenyl (S)%67 10-174 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4155032MATRIX SPIKE SAMPLE: MSSpike Result 92689619001 PCB-1016 (Aroclor 1016)ug/kg 572940 61 10-144ND PCB-1260 (Aroclor 1260)ug/kg 1620 M194017210-141ND Decachlorobiphenyl (S)%S245410-174 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 73 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 801590 EPA 3546 EPA 8270E 8270E Solid MSSV Microwave Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576001, 92689576002, 92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4152309 Associated Lab Samples:92689576001, 92689576002, 92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Matrix:Solid AnalyzedMDL 1,2,4-Trichlorobenzene ug/kg ND 325 09/25/23 08:04128 1,2-Dichlorobenzene ug/kg ND 325 09/25/23 08:04117 1,3-Dichlorobenzene ug/kg ND 325 09/25/23 08:04115 1,4-Dichlorobenzene ug/kg ND 325 09/25/23 08:04124 1-Methylnaphthalene ug/kg ND 325 09/25/23 08:04114 2,2'-Oxybis(1-chloropropane)ug/kg ND 325 09/25/23 08:04154 2,4,5-Trichlorophenol ug/kg ND 325 09/25/23 08:04149 2,4,6-Trichlorophenol ug/kg ND 325 09/25/23 08:04134 2,4-Dichlorophenol ug/kg ND 325 09/25/23 08:04127 2,4-Dimethylphenol ug/kg ND 325 09/25/23 08:04135 2,4-Dinitrophenol ug/kg ND 1620 09/25/23 08:041000 2,4-Dinitrotoluene ug/kg ND 325 09/25/23 08:04125 2,6-Dinitrotoluene ug/kg ND 325 09/25/23 08:04119 2-Chloronaphthalene ug/kg ND 325 09/25/23 08:04129 2-Chlorophenol ug/kg ND 325 09/25/23 08:04122 2-Methylnaphthalene ug/kg ND 325 09/25/23 08:04130 2-Methylphenol(o-Cresol)ug/kg ND 325 09/25/23 08:04133 2-Nitroaniline ug/kg ND 1620 09/25/23 08:04266 2-Nitrophenol ug/kg ND 325 09/25/23 08:04141 3&4-Methylphenol(m&p Cresol)ug/kg ND 325 09/25/23 08:04131 3,3'-Dichlorobenzidine ug/kg ND 649 09/25/23 08:04219 3-Nitroaniline ug/kg ND 1620 09/25/23 08:04255 4,6-Dinitro-2-methylphenol ug/kg ND 649 09/25/23 08:04303 4-Bromophenylphenyl ether ug/kg ND 325 09/25/23 08:04125 4-Chloro-3-methylphenol ug/kg ND 649 09/25/23 08:04228 4-Chloroaniline ug/kg ND 649 09/25/23 08:04255 4-Chlorophenylphenyl ether ug/kg ND 325 09/25/23 08:04121 4-Nitroaniline ug/kg ND 649 09/25/23 08:04247 4-Nitrophenol ug/kg ND 1620 09/25/23 08:04628 Acenaphthene ug/kg ND 325 09/25/23 08:04114 Acenaphthylene ug/kg ND 325 09/25/23 08:04114 Aniline ug/kg ND 325 09/25/23 08:04127 Anthracene ug/kg ND 325 09/25/23 08:04106 Benzo(a)anthracene ug/kg ND 325 09/25/23 08:04108 Benzo(a)pyrene ug/kg ND 325 09/25/23 08:04112 Benzo(b)fluoranthene ug/kg ND 325 09/25/23 08:04108 Benzo(g,h,i)perylene ug/kg ND 325 09/25/23 08:04126 Benzo(k)fluoranthene ug/kg ND 325 09/25/23 08:04114 Benzoic Acid ug/kg ND 1620 09/25/23 08:04697 Benzyl alcohol ug/kg ND 649 09/25/23 08:04246 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 74 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4152309 Associated Lab Samples:92689576001, 92689576002, 92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Matrix:Solid AnalyzedMDL bis(2-Chloroethoxy)methane ug/kg ND 325 09/25/23 08:04135 bis(2-Chloroethyl) ether ug/kg ND 325 09/25/23 08:04122 bis(2-Ethylhexyl)phthalate ug/kg ND 325 09/25/23 08:04126 Butylbenzylphthalate ug/kg ND 325 09/25/23 08:04137 Chrysene ug/kg ND 325 09/25/23 08:04118 Di-n-butylphthalate ug/kg ND 325 09/25/23 08:04109 Di-n-octylphthalate ug/kg ND 325 09/25/23 08:04128 Dibenz(a,h)anthracene ug/kg ND 325 09/25/23 08:04125 Dibenzofuran ug/kg ND 325 09/25/23 08:04117 Diethylphthalate ug/kg ND 325 09/25/23 08:04119 Dimethylphthalate ug/kg ND 325 09/25/23 08:04118 Fluoranthene ug/kg ND 325 09/25/23 08:04111 Fluorene ug/kg ND 325 09/25/23 08:04114 Hexachloro-1,3-butadiene ug/kg ND 325 09/25/23 08:04141 Hexachlorobenzene ug/kg ND 325 09/25/23 08:04127 Hexachlorocyclopentadiene ug/kg ND 325 09/25/23 08:04186 Hexachloroethane ug/kg ND 325 09/25/23 08:04124 Indeno(1,2,3-cd)pyrene ug/kg ND 325 09/25/23 08:04128 Isophorone ug/kg ND 325 09/25/23 08:04145 N-Nitroso-di-n-propylamine ug/kg ND 325 09/25/23 08:04122 N-Nitrosodimethylamine ug/kg ND 325 09/25/23 08:04109 N-Nitrosodiphenylamine ug/kg ND 325 09/25/23 08:04115 Naphthalene ug/kg ND 325 09/25/23 08:04110 Nitrobenzene ug/kg ND 325 09/25/23 08:04150 Pentachlorophenol ug/kg ND 649 09/25/23 08:04318 Phenanthrene ug/kg ND 325 09/25/23 08:04106 Phenol ug/kg ND 325 09/25/23 08:04145 Pyrene ug/kg ND 325 09/25/23 08:04132 Pyridine ug/kg ND 325 09/25/23 08:04102 2,4,6-Tribromophenol (S)%55 10-131 09/25/23 08:04 2-Fluorobiphenyl (S)%51 10-130 09/25/23 08:04 2-Fluorophenol (S)%55 10-130 09/25/23 08:04 Nitrobenzene-d5 (S)%54 10-130 09/25/23 08:04 Phenol-d6 (S)%57 10-130 09/25/23 08:04 Terphenyl-d14 (S)%63 10-130 09/25/23 08:04 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4152310LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/kg 7891660 48 43-130 1,2-Dichlorobenzene ug/kg 8141660 49 43-130 1,3-Dichlorobenzene ug/kg 8021660 48 43-130 1,4-Dichlorobenzene ug/kg 8121660 49 44-130 1-Methylnaphthalene ug/kg 8721660 52 47-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 75 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4152310LABORATORY CONTROL SAMPLE: LCSSpike 2,2'-Oxybis(1-chloropropane)ug/kg 8541660 51 29-130 2,4,5-Trichlorophenol ug/kg 8481660 51 47-130 2,4,6-Trichlorophenol ug/kg 8521660 51 47-130 2,4-Dichlorophenol ug/kg 8741660 53 45-130 2,4-Dimethylphenol ug/kg 8881660 53 45-130 2,4-Dinitrophenol ug/kg 46308310 56 27-140 2,4-Dinitrotoluene ug/kg 9561660 58 46-130 2,6-Dinitrotoluene ug/kg 8941660 54 48-130 2-Chloronaphthalene ug/kg 8041660 48 46-130 2-Chlorophenol ug/kg 9361660 56 43-130 2-Methylnaphthalene ug/kg 8731660 53 47-130 2-Methylphenol(o-Cresol)ug/kg 9201660 55 42-130 2-Nitroaniline ug/kg 18803320 57 41-130 2-Nitrophenol ug/kg 8831660 53 48-130 3&4-Methylphenol(m&p Cresol)ug/kg 9411660 57 39-130 3,3'-Dichlorobenzidine ug/kg 17903320 54 41-130 3-Nitroaniline ug/kg 18803320 57 37-130 4,6-Dinitro-2-methylphenol ug/kg 18803320 56 38-141 4-Bromophenylphenyl ether ug/kg 8831660 53 47-130 4-Chloro-3-methylphenol ug/kg 18203320 55 44-130 4-Chloroaniline ug/kg 19003320 57 41-130 4-Chlorophenylphenyl ether ug/kg 9151660 55 45-130 4-Nitroaniline ug/kg 20003320 60 42-130 4-Nitrophenol ug/kg 48608310 59 39-131 Acenaphthene ug/kg 8611660 52 49-130 Acenaphthylene ug/kg 8801660 53 50-130 Aniline ug/kg 8831660 53 38-130 Anthracene ug/kg 8961660 54 49-130 Benzo(a)anthracene ug/kg 9251660 56 51-130 Benzo(a)pyrene ug/kg 9751660 59 51-130 Benzo(b)fluoranthene ug/kg 9601660 58 49-130 Benzo(g,h,i)perylene ug/kg 9601660 58 48-140 Benzo(k)fluoranthene ug/kg 9621660 58 51-130 Benzoic Acid ug/kg 26908310 32 22-130 Benzyl alcohol ug/kg 19003320 57 43-130 bis(2-Chloroethoxy)methane ug/kg 8981660 54 43-130 bis(2-Chloroethyl) ether ug/kg 9001660 54 42-130 bis(2-Ethylhexyl)phthalate ug/kg 10101660 61 43-130 Butylbenzylphthalate ug/kg 9291660 56 44-131 Chrysene ug/kg 9541660 57 51-130 Di-n-butylphthalate ug/kg 9671660 58 46-130 Di-n-octylphthalate ug/kg 9971660 60 45-130 Dibenz(a,h)anthracene ug/kg 9771660 59 48-130 Dibenzofuran ug/kg 8771660 53 10-130 Diethylphthalate ug/kg 9591660 58 48-130 Dimethylphthalate ug/kg 9251660 56 48-130 Fluoranthene ug/kg 9341660 56 48-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 76 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4152310LABORATORY CONTROL SAMPLE: LCSSpike Fluorene ug/kg 9251660 56 48-130 Hexachloro-1,3-butadiene ug/kg 7891660 47 39-130 Hexachlorobenzene ug/kg 8621660 52 47-130 Hexachlorocyclopentadiene ug/kg 7481660 45 17-130 Hexachloroethane ug/kg 7971660 48 40-130 Indeno(1,2,3-cd)pyrene ug/kg 9501660 57 50-130 Isophorone ug/kg 9061660 55 41-130 N-Nitroso-di-n-propylamine ug/kg 9581660 58 36-130 N-Nitrosodimethylamine ug/kg 8531660 51 34-130 N-Nitrosodiphenylamine ug/kg 8811660 53 48-130 Naphthalene ug/kg 8541660 51 46-130 Nitrobenzene ug/kg 8101660 49 39-130 Pentachlorophenol ug/kg 18303320 55 42-130 Phenanthrene ug/kg 9101660 55 50-130 Phenol ug/kg 9461660 57 42-130 Pyrene ug/kg 8941660 54 50-130 Pyridine ug/kg 5941660 36 26-130 2,4,6-Tribromophenol (S)%56 10-131 2-Fluorobiphenyl (S)%50 10-130 2-Fluorophenol (S)%55 10-130 Nitrobenzene-d5 (S)%52 10-130 Phenol-d6 (S)%57 10-130 Terphenyl-d14 (S)%55 10-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 4152311MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92689564004 4152729 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/kg R118203516-13026 33 301800ND642462 1,2-Dichlorobenzene ug/kg 1820 36 19-13028 29 301800ND665498 1,3-Dichlorobenzene ug/kg 1820 37 19-13028 30 301800ND671496 1,4-Dichlorobenzene ug/kg 1820 36 20-13028 27 301800ND656499 1-Methylnaphthalene ug/kg R118204319-13030 37 301800ND787541 2,2'-Oxybis(1- chloropropane)ug/kg 1820 38 10-13029 30 301800ND696513 2,4,5-Trichlorophenol ug/kg R118204419-13032 35 301800ND812570 2,4,6-Trichlorophenol ug/kg R118204318-13031 34 301800ND784554 2,4-Dichlorophenol ug/kg R118204116-13029 35 301800ND741520 2,4-Dimethylphenol ug/kg 1820 20 10-13027 301800ND357J484 2,4-Dinitrophenol ug/kg 9140 18 10-14321 308990ND1620J1900 2,4-Dinitrotoluene ug/kg R118205019-13036 33 301800ND907651 2,6-Dinitrotoluene ug/kg R118204622-13034 32 301800ND843613 2-Chloronaphthalene ug/kg R118204018-13028 36 301800ND734510 2-Chlorophenol ug/kg 1820 41 20-13031 30 301800ND745550 2-Methylnaphthalene ug/kg R118204318-13030 38 301800ND793539 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 77 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4152311MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92689564004 4152729 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2-Methylphenol(o-Cresol)ug/kg 1820 34 13-13030 15 301800ND618534 2-Nitroaniline ug/kg 3660 49 18-13035 303590ND1790J1270J 2-Nitrophenol ug/kg R118203919-13029 33 301800ND721516 3&4-Methylphenol(m&p Cresol)ug/kg 1820 37 13-13032 19 301800ND685567 3,3'-Dichlorobenzidine ug/kg 3660 36 10-13033 10 303590ND13001180 3-Nitroaniline ug/kg 3660 50 22-13039 303590ND18201390J 4,6-Dinitro-2-methylphenol ug/kg 3660 39 10-14430 27 303590ND14201090 4-Bromophenylphenyl ether ug/kg R118204518-13033 34 301800ND828587 4-Chloro-3-methylphenol ug/kg R136604716-13034 32 303590ND17001230 4-Chloroaniline ug/kg 3660 40 17-13031 25 303590ND14501130 4-Chlorophenylphenyl ether ug/kg R118204817-13034 35 301800ND886620 4-Nitroaniline ug/kg 3660 50 21-13039 27 303590ND18301390 4-Nitrophenol ug/kg R191404813-13136 32 308990ND44303190 Acenaphthene ug/kg R118204520-13033 34 301800ND827589 Acenaphthylene ug/kg R118204621-13033 33 301800ND837599 Aniline ug/kg 1820 29 10-13028 5 301800ND522498 Anthracene ug/kg R118204819-13034 36 301800ND885618 Benzo(a)anthracene ug/kg R118204917-13035 36 301800ND904630 Benzo(a)pyrene ug/kg R118205514-13039 34 301800ND1000709 Benzo(b)fluoranthene ug/kg R118205711-13440 36 301800ND1040722 Benzo(g,h,i)perylene ug/kg 1820 49 12-13037 30 301800ND893661 Benzo(k)fluoranthene ug/kg R118205415-13040 32 301800ND990716 Benzoic Acid ug/kg M19140510-1306 308990NDNDND Benzyl alcohol ug/kg 3660 42 20-13032 30 303590ND15301130 bis(2- Chloroethoxy)methane ug/kg R118204116-13030 32 301800ND749540 bis(2-Chloroethyl) ether ug/kg R118204418-13030 38 301800ND802545 bis(2-Ethylhexyl)phthalate ug/kg R118205311-13037 36 301800ND1010708 Butylbenzylphthalate ug/kg R118205110-13035 37 301800ND924636 Chrysene ug/kg R118205217-13036 38 301800ND942643 Di-n-butylphthalate ug/kg R118205516-13036 41 301800ND999656 Di-n-octylphthalate ug/kg R118205316-13038 36 301800ND978679 Dibenz(a,h)anthracene ug/kg R118204713-13035 31 301800ND854622 Dibenzofuran ug/kg R118204619-13033 34 301800ND842598 Diethylphthalate ug/kg R118205122-13037 34 301800ND934659 Dimethylphthalate ug/kg R118204923-13035 33 301800ND889637 Fluoranthene ug/kg R118205514-13037 41 301800ND999660 Fluorene ug/kg R118205019-13036 35 301800ND915642 Hexachloro-1,3-butadiene ug/kg R118203612-13025 35 301800ND649454 Hexachlorobenzene ug/kg R118204417-13032 34 301800ND806571 Hexachlorocyclopentadiene ug/kg 1820 26 10-13017 301800ND475314J Hexachloroethane ug/kg 1820 35 14-13026 30 301800ND640474 Indeno(1,2,3-cd)pyrene ug/kg 1820 49 13-13037 29 301800ND901673 Isophorone ug/kg R118204317-13031 33 301800ND787561 N-Nitroso-di-n-propylamine ug/kg R118204510-13033 32 301800ND814587 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 78 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4152311MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92689564004 4152729 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. N-Nitrosodimethylamine ug/kg R118203816-13028 31 301800ND696510 N-Nitrosodiphenylamine ug/kg R118204419-13033 31 301800ND807589 Naphthalene ug/kg R118204118-13029 35 301800ND747524 Nitrobenzene ug/kg R118203815-13027 36 301800ND693483 Pentachlorophenol ug/kg 3660 36 10-13029 22 303590ND13101060 Phenanthrene ug/kg R118205117-13035 38 301800ND933636 Phenol ug/kg 1820 40 15-13030 29 301800ND730548 Pyrene ug/kg R118205031-13035 37 301800ND919633 Pyridine ug/kg R118203310-13021 45 301800ND597376 2,4,6-Tribromophenol (S)%47 10-13127 2-Fluorobiphenyl (S)%39 10-13023 2-Fluorophenol (S)%39 10-13023 Nitrobenzene-d5 (S)%39 10-13022 Phenol-d6 (S)%40 10-13024 Terphenyl-d14 (S)%47 10-13022 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4152730MATRIX SPIKE SAMPLE: MSSpike Result 92689564005 1,2,4-Trichlorobenzene ug/kg 11501940 59 16-130ND 1,2-Dichlorobenzene ug/kg 12001940 62 19-130ND 1,3-Dichlorobenzene ug/kg 11901940 61 19-130ND 1,4-Dichlorobenzene ug/kg 12001940 62 20-130ND 1-Methylnaphthalene ug/kg 13101940 68 19-130ND 2,2'-Oxybis(1-chloropropane)ug/kg 12601940 65 10-130ND 2,4,5-Trichlorophenol ug/kg 13801940 71 19-130ND 2,4,6-Trichlorophenol ug/kg 13501940 70 18-130ND 2,4-Dichlorophenol ug/kg 13701940 71 16-130ND 2,4-Dimethylphenol ug/kg 13901940 72 10-130ND 2,4-Dinitrophenol ug/kg 57909680 60 10-143ND 2,4-Dinitrotoluene ug/kg 15001940 77 19-130ND 2,6-Dinitrotoluene ug/kg 14301940 74 22-130ND 2-Chloronaphthalene ug/kg 12301940 63 18-130ND 2-Chlorophenol ug/kg 14101940 73 20-130ND 2-Methylnaphthalene ug/kg 13201940 68 18-130ND 2-Methylphenol(o-Cresol)ug/kg 13701940 71 13-130ND 2-Nitroaniline ug/kg 30003870 77 18-130ND 2-Nitrophenol ug/kg 13401940 69 19-130ND 3&4-Methylphenol(m&p Cresol)ug/kg 14501940 75 13-130ND 3,3'-Dichlorobenzidine ug/kg 30703870 79 10-130ND 3-Nitroaniline ug/kg 32703870 84 22-130ND 4,6-Dinitro-2-methylphenol ug/kg 29303870 76 10-144ND 4-Bromophenylphenyl ether ug/kg 12701940 66 18-130ND 4-Chloro-3-methylphenol ug/kg 29403870 76 16-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 79 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4152730MATRIX SPIKE SAMPLE: MSSpike Result 92689564005 4-Chloroaniline ug/kg 29903870 77 17-130ND 4-Chlorophenylphenyl ether ug/kg 13301940 69 17-130ND 4-Nitroaniline ug/kg 32903870 85 21-130ND 4-Nitrophenol ug/kg 78209680 81 13-131ND Acenaphthene ug/kg 13201940 68 20-130ND Acenaphthylene ug/kg 13701940 71 21-130ND Aniline ug/kg 13401940 69 10-130ND Anthracene ug/kg 13501940 70 19-130ND Benzo(a)anthracene ug/kg 13701940 71 17-130ND Benzo(a)pyrene ug/kg 16101940 83 14-130ND Benzo(b)fluoranthene ug/kg 16001940 83 11-134ND Benzo(g,h,i)perylene ug/kg 14201940 73 12-130ND Benzo(k)fluoranthene ug/kg 16301940 84 15-130ND Benzoic Acid ug/kg ND M19680110-130ND Benzyl alcohol ug/kg 28503870 74 20-130ND bis(2-Chloroethoxy)methane ug/kg 13901940 72 16-130ND bis(2-Chloroethyl) ether ug/kg 13501940 70 18-130ND bis(2-Ethylhexyl)phthalate ug/kg 15401940 80 11-130ND Butylbenzylphthalate ug/kg 14101940 73 10-130ND Chrysene ug/kg 13801940 71 17-130ND Di-n-butylphthalate ug/kg 14301940 74 16-130ND Di-n-octylphthalate ug/kg 15301940 79 16-130ND Dibenz(a,h)anthracene ug/kg 14301940 74 13-130ND Dibenzofuran ug/kg 13401940 69 19-130ND Diethylphthalate ug/kg 15101940 78 22-130ND Dimethylphthalate ug/kg 15201940 78 23-130ND Fluoranthene ug/kg 14101940 73 14-130ND Fluorene ug/kg 14001940 72 19-130ND Hexachloro-1,3-butadiene ug/kg 11301940 58 12-130ND Hexachlorobenzene ug/kg 12101940 62 17-130ND Hexachlorocyclopentadiene ug/kg 9201940 48 10-130ND Hexachloroethane ug/kg 11501940 60 14-130ND Indeno(1,2,3-cd)pyrene ug/kg 14601940 75 13-130ND Isophorone ug/kg 14101940 73 17-130ND N-Nitroso-di-n-propylamine ug/kg 14901940 77 10-130ND N-Nitrosodimethylamine ug/kg 12901940 66 16-130ND N-Nitrosodiphenylamine ug/kg 13501940 70 19-130ND Naphthalene ug/kg 13201940 68 18-130ND Nitrobenzene ug/kg 12601940 65 15-130ND Pentachlorophenol ug/kg 30003870 77 10-130ND Phenanthrene ug/kg 13701940 71 17-130ND Phenol ug/kg 14901940 77 15-130ND Pyrene ug/kg 13901940 72 31-130ND Pyridine ug/kg 12001940 62 10-130ND 2,4,6-Tribromophenol (S)%73 10-131 2-Fluorobiphenyl (S)%60 10-130 2-Fluorophenol (S)%67 10-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 80 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 4152730MATRIX SPIKE SAMPLE: MSSpike Result 92689564005 Nitrobenzene-d5 (S)%65 10-130 Phenol-d6 (S)%67 10-130 Terphenyl-d14 (S)%53 10-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 81 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 801800 SW-846 SW-846 Dry Weight/Percent Moisture Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576001, 92689576002, 92689576003 Parameter Units Dup Result Max RPD QualifiersRPDResult 92689563004 4153293SAMPLE DUPLICATE: Percent Moisture %13.5 N222513.8 Parameter Units Dup Result Max RPD QualifiersRPDResult 92689576003 4153294SAMPLE DUPLICATE: Percent Moisture %6.6 N29257.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 82 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 801811 SW-846 SW-846 Dry Weight/Percent Moisture Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92689576004, 92689576005, 92689576006, 92689576007 Parameter Units Dup Result Max RPD QualifiersRPDResult 92689567001 4153369SAMPLE DUPLICATE: Percent Moisture %15.3 N2152517.9 Parameter Units Dup Result Max RPD QualifiersRPDResult 92689584002 4153370SAMPLE DUPLICATE: Percent Moisture %15.9 N212516.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 83 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2141737 SM 2540 G SM 2540G Total Solids 2540 G-2011 Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92689576001, 92689576002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:R3979874-1 Associated Lab Samples:92689576001, 92689576002 Matrix:Solid AnalyzedMDL Total Solids %0.00100 09/29/23 13:13 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3979874-2LABORATORY CONTROL SAMPLE: LCSSpike Total Solids %50.050.0 100 85.0-115 Parameter Units Dup Result Max RPD QualifiersRPDResult L1660102-13 R3979874-3SAMPLE DUPLICATE: Total Solids %78.9 2.41 1077.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 84 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2141738 SM 2540 G SM 2540G Total Solids 2540 G-2011 Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:R3979870-1 Associated Lab Samples:92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Matrix:Solid AnalyzedMDL Total Solids %ND 09/29/23 13:00 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3979870-2LABORATORY CONTROL SAMPLE: LCSSpike Total Solids %50.050.0 100 85.0-115 Parameter Units Dup Result Max RPD QualifiersRPDResult L1660220-01 R3979870-3SAMPLE DUPLICATE: Total Solids %83.2 2.27 1085.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 85 of 93 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2141931 3060A EPA 7199 Wet Chemistry 7199 Laboratory:Pace National - Mt. Juliet Associated Lab Samples:92689576001, 92689576002, 92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:R3980775-1 Associated Lab Samples:92689576001, 92689576002, 92689576003, 92689576004, 92689576005, 92689576006, 92689576007 Matrix:Solid AnalyzedMDL Chromium, Hexavalent mg/kg ND 1.00 10/03/23 01:070.255 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3980775-2LABORATORY CONTROL SAMPLE: LCSSpike Chromium, Hexavalent mg/kg 10.010.0 100 80.0-120 Parameter Units MS Result % Rec Limits Qual% RecConc. R3980775-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1659701-02 R3980775-5 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Chromium, Hexavalent mg/kg 20.0 93.5 75.0-125101 7.58 2020.0ND 18.7 20.2 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. R3980775-6MATRIX SPIKE SAMPLE: MSSpike Result L1659701-02 Chromium, Hexavalent mg/kg 381 ML64359.2 75.0-125ND Parameter Units Dup Result Max RPD QualifiersRPDResult L1659735-01 R3980775-7SAMPLE DUPLICATE: Chromium, Hexavalent mg/kg ND 0.00 20ND Parameter Units Dup Result Max RPD QualifiersRPDResult L1659745-03 R3980775-8SAMPLE DUPLICATE: Chromium, Hexavalent mg/kg ND 0.00 20ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 86 of 93 #=QL# QUALIFIERS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Common Laboratory Contaminant.C9 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 Analyte concentration exceeded the calibration range. The reported result is estimated.E Sample was received or analysis requested beyond the recognized method holding time.H3 The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value.IK Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low.ML The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request.N2 RPD between the primary and confirmatory analysis exceeded 40%.P9 RPD value was outside control limits.R1 Surrogate recovery outside laboratory control limits.S0 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-analysis).S2 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias.v1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 87 of 93 #=QL# QUALIFIERS Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report ANALYTE QUALIFIERS The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias.v3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 88 of 93 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92689576006 2142684 2142684AS-1 3546 EPA 8141B 92689576007 2142684 2142684AS-1d 3546 EPA 8141B 92689576006 2140051 2140051AS-1 8151A EPA 8151A 92689576007 2140051 2140051AS-1d 8151A EPA 8151A 92689576006 802129 802342AS-1 EPA 3546 EPA 8082A 92689576007 802129 802342AS-1d EPA 3546 EPA 8082A 92689576001 953507 953649QS-1 EPA 3050 EPA 6010 92689576002 953507 953649QS-2 EPA 3050 EPA 6010 92689576003 954343 954484QS-3 EPA 3050 EPA 6010 92689576004 953507 953649QS-4 EPA 3050 EPA 6010 92689576005 953507 953649QS-4d EPA 3050 EPA 6010 92689576006 953507 953649AS-1 EPA 3050 EPA 6010 92689576007 953507 953649AS-1d EPA 3050 EPA 6010 92689576001 954341 954385QS-1 EPA 7471 EPA 7471 92689576002 954341 954385QS-2 EPA 7471 EPA 7471 92689576003 954620 954695QS-3 EPA 7471 EPA 7471 92689576004 954620 954695QS-4 EPA 7471 EPA 7471 92689576005 954842 955044QS-4d EPA 7471 EPA 7471 92689576006 954620 954695AS-1 EPA 7471 EPA 7471 92689576007 954842 955044AS-1d EPA 7471 EPA 7471 92689576001 801590 801679QS-1 EPA 3546 EPA 8270E 92689576002 801590 801679QS-2 EPA 3546 EPA 8270E 92689576003 801590 801679QS-3 EPA 3546 EPA 8270E 92689576004 801590 801679QS-4 EPA 3546 EPA 8270E 92689576005 801590 801679QS-4d EPA 3546 EPA 8270E 92689576006 801590 801679AS-1 EPA 3546 EPA 8270E 92689576007 801590 801679AS-1d EPA 3546 EPA 8270E 92689576001 801920 802031QS-1 EPA 5035A/5030B EPA 8260D 92689576002 801920 802031QS-2 EPA 5035A/5030B EPA 8260D 92689576003 801923 802032QS-3 EPA 5035A/5030B EPA 8260D 92689576004 801923 802032QS-4 EPA 5035A/5030B EPA 8260D 92689576005 801923 802032QS-4d EPA 5035A/5030B EPA 8260D 92689576006 801923 802032AS-1 EPA 5035A/5030B EPA 8260D 92689576007 802240 802261AS-1d EPA 5035A/5030B EPA 8260D 92689576001 801800QS-1 SW-846 92689576002 801800QS-2 SW-846 92689576003 801800QS-3 SW-846 92689576004 801811QS-4 SW-846 92689576005 801811QS-4d SW-846 92689576006 801811AS-1 SW-846 92689576007 801811AS-1d SW-846 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 89 of 93 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92689576 Mock Judson Mill PN: 1533-Revised Report Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92689576001 2141737 2141737QS-1 SM 2540 G SM 2540G 92689576002 2141737 2141737QS-2 SM 2540 G SM 2540G 92689576003 2141738 2141738QS-3 SM 2540 G SM 2540G 92689576004 2141738 2141738QS-4 SM 2540 G SM 2540G 92689576005 2141738 2141738QS-4d SM 2540 G SM 2540G 92689576006 2141738 2141738AS-1 SM 2540 G SM 2540G 92689576007 2141738 2141738AS-1d SM 2540 G SM 2540G 92689576001 2141931 2141931QS-1 3060A EPA 7199 92689576002 2141931 2141931QS-2 3060A EPA 7199 92689576003 2141931 2141931QS-3 3060A EPA 7199 92689576004 2141931 2141931QS-4 3060A EPA 7199 92689576005 2141931 2141931QS-4d 3060A EPA 7199 92689576006 2141931 2141931AS-1 3060A EPA 7199 92689576007 2141931 2141931AS-1d 3060A EPA 7199 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 10/09/2023 01:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 90 of 93 Page 91 of 93 Page 92 of 93 Page 93 of 93 Martin Marietta Salem Stone Quarry Sampling R1 October 24, 2023 Mock Judson Mill 2610 Oakland Avenue Greensboro, North Carolina Brownfields Project Number 25094-21-041 FIELD NOTES