WS-3254_9547_CA_MRP_20221027

ANNUAL MONITORING REPORT
Jerry’s Place (Incident # 9547)
983 US Highway 21
State Road, Surry County, North Carolina
October 27, 2022
Terracon Project No. 75207118
Prepared for:
North Carolina Department of Environmental Quality
Division of Waste Management
Raleigh, North Carolina

Prepared by:
Terracon Consultants, Inc.
Greensboro, North Carolina

Terracon Consultants, Inc. 7327-G West Friendly Avenue Greensboro, NC 27410
P 336-854-8135 F 336-365-7020 terracon.com
October 27, 2022

Mr. Herbert Berger, P.G.
North Carolina Department of Environmental Quality
Division of Waste Management
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Email: [e-mail]

Re: Annual Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
UST Incident Number: 9547
Terracon Project No. 75207118

Dear Mr. Berger:

Terracon Consultants, Inc. (Terracon) is pleased to submit this Annual Monitoring Report for the
above referenced property. This report has been prepared in general accordance with North
Carolina Department of Environmental Quality (NCDEQ), UST Section Corrective Action
Guidelines, dated January 19, 2021 and Task Authorization No. TA-03, approved on August 24,
2022.

If you have any questions regarding this report or the assessment activities, please contact us at
336-854-8135.

Sincerely,
Terracon Consultants, Inc.

Laura R. Elliott, P.G. Edmund Woloszyn, Jr. R.E.M.
Senior Geologist Department Manager II
Environmental Services

Jared Rose, P.G.
Senior Staff Geologist

Enclosures

Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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Table of Contents
A. SITE INFORMATION ............................................................................................ 2
B. EXECUTIVE SUMMARY ...................................................................................... 3
C. SITE HISTORY AND CHARACTERIZATION ....................................................... 4
C.1 Site Setting ................................................................................................................................ 4
C.2 Release Summary ..................................................................................................................... 4
C.3 Previous Investigations ........................................................................................................... 4
C.4 Water Supply Wells .................................................................................................................. 5
C.5 Surface Water ........................................................................................................................... 5
D. ASSESSMENT INFORMATION ........................................................................... 5
D.1 Site Geology and Hydrology ................................................................................................... 5
D.2 Sampling Activities .................................................................................................................. 6
D.3 LNAPL Evaluation .................................................................................................................... 7
D.4 Groundwater Sampling Activities ........................................................................................... 7
D.5 Analytical Results ..................................................................................................................... 7
E. CONCLUSIONS AND RECOMMENDATIONS ..................................................... 8
H. REFERENCES ...................................................................................................... 9

EXHIBITS Exhibit 1: Topographic Map
Exhibit 2: Site Diagram
Exhibit 3: Water Supply Well Location Map
Exhibit 4: Groundwater Contour Map (August 2022)
Exhibit 5: Groundwater Analytical Results (August 2022)

TABLES
Table 1: Water Supply Well Information
Table 2: Monitoring Well Construction Details and Groundwater
Elevation Data
Table 3: Summary of Groundwater Analytical Results

APPENDICES
Appendix A: Field Notes and Photographs
Appendix B: Laboratory Analytical Results and Chain of Custody Form

Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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ANNUAL MONITORING REPORT
A. SITE INFORMATION
Date of Report: October 27, 2022
NCDEQ Incident No: 9547 UST #: WS-3254 Site Name: Jerry’s Place Site Location: 983 US Highway 21 State Road, Surry County, North Carolina Latitude: N: 36°18’52” Longitude: W: 80°51’38”
UST Owner/Operator: Jerry’s Place
Current Property Owner: Matthew Kennedy and Michael Maher 983 US Highway 21 State Road, Surry County, North Carolina Consultant: Terracon Consultants, Inc. (Contact: Laura Elliott) 7327-G West Friendly Avenue
Greensboro, North Carolina 27410 [phone] Laboratory: Pace Analytical National (NCDEQ No. 375) 12065 Lebanon Road Mt. Juliet, Tennessee 37122 [phone] Release Information: Release Date: 1992
Estimated Quantity: Unknown
Cause of Release: Underground Storage Tank (UST) System,
Former USTs: four 4,000-gallon gasoline USTs
Currently Active Tanks: None

Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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I, Laura R. Elliott, P.G., a Licensed Geologist for Terracon Consultants, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.

Laura R. Elliott, P.G.
NC License No. 2271

Terracon Consultants, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-367 and F-0869, respectively.
B. EXECUTIVE SUMMARY
Jerry’s Place, the subject property located at 983 US Highway 21, is situated on a 1.58-acre parcel
(Surry County Parcel No. 495301186476) in State Road, North Carolina. The facility reportedly
operated four 4,000-gallon gasoline underground storage tanks (USTs) which were removed from
the site in 1992.

At the direction of the NCDEQ, Terracon mobilized to the site on August 25, 2022, to collect
groundwater samples from eight monitoring wells (MW-2/RW-2, MW-3/RW-3, MW-4/RW-4, MW-5,
RW-5, MW-6, MW-7, and MW-8) for analysis by EPA Method 6200.

Based on information obtained during the completion of these assessment activities, Terracon
provides the following findings and conclusions:

 Several petroleum constituents were detected at concentrations exceeding the 2L
Standards but below the GCLs in groundwater samples from wells MW-2/RW-2 and
MW-3/RW-3 and RW-5.
 No target compounds were detected above laboratory detection limits in samples
collected from monitoring wells MW-4/RW-4, MW-5, or MW-6.
 There was insufficient groundwater present in monitoring wells MW-7 or MW-8 to
collect groundwater samples during this event.
 Measurable thicknesses of LNAPL were not observed in the monitoring wells
gauged.
 Groundwater flow was estimated, based on groundwater elevation data, to be
toward the northeast, east, and southeast.

Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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Based on the data presented in this Annual Monitoring Report, Terracon recommends the following
activities be completed at the site:

 Based on the results of this sampling event and the previous report’s biodegradation
model, the incident may be closed with a Notice of Residual Petroleum (NORP) and
a groundwater use restriction.
C. SITE HISTORY AND CHARACTERIZATION
This Monitoring Report was prepared in response to a request by Mr. Herbert Berger, P.G., Incident
Manager with the NCDEQ Division of Waste Management, Trust Fund Branch. The report was
prepared in general accordance with 15A NCAC 2L .0115 regulations and the NCDEQ UST Section
Corrective Action Guidelines dated January 19, 2021, under the supervision of Ms. Laura Elliott, a
North Carolina licensed geologist (North Carolina License No. 2271).

The purpose of this Monitoring Report is to present the current status of the groundwater quality at
the Jerry’s Place site located at 983 US Highway 21 in State Road, Surry County, North Carolina
(Exhibit 1). Terracon completed this report to summarize the findings of groundwater sampling
activities performed on August 25, 2022.

C.1 Site Setting
Jerry’s Place, the subject property located at 983 US Highway 21, is situated on a 1.58-acre parcel
(Surry County Parcel No. 495301186476) in State Road, North Carolina (Exhibit 1). The facility
reportedly operated four 4,000-gallon gasoline USTs which were removed from the site in 1992.
The site is currently occupied by commercial businesses (Exhibit 2).

C.2 Release Summary
According to prior reports, four 4,000-gallon gasoline USTs were removed from the site in 1992.
During closure activities, LNAPL was observed flowing into a test pit that was excavated to a depth
of approximately 19 feet below ground surface (bgs). Approximately 1,029 tons of petroleum
contaminated soil was subsequently excavated during the UST closure activities.

C.3 Previous Investigations
According to information included in the incident folder, four 4,000-gallon gasoline USTs were
removed from the site in 1992. Eight monitoring wells (MW-1 through MW-8) and two recovery wells
(RW-5 and RW-6) were installed between 1993 and 1994. On-site monitoring wells were sampled
in 1993, 2009, 2010, 2011, 2014, 2015, 2018, and 2019. The contaminant concentrations appear
to have been decreasing since 1993. A previous consultant conducted a free product/vapor
recovery event on July 29, 1996. A mobile multiphase extraction (MMPE) event was later conducted
in 2001. According to a Groundwater Monitoring Report completed by a previous consultant and
Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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dated January 7, 2020, methyl tert-butyl ether (MTBE) has been detected in the on-site water
supply well (WSW-5) since 2009 at a concentration below its 2L Standard.

In June 2022, Terracon conducted slug testing and groundwater modeling along with groundwater
sampling to assess the likelihood of downgradient water supply wells being affected by the
migration of petroleum compounds from the subject site. The model determined that the wells were
unlikely to be affected by petroleum-contaminated groundwater on the subject site.

C.4 Water Supply Wells
According to a Groundwater Monitoring Report prepared by Engineering Consulting Services (ECS)
and dated September 16, 2014, sixteen water supply wells were identified within 1,000 feet of the
site. A copy of the ECS water supply well location map is presented as Exhibit 3, and Table 1
presents information on the water supply wells located within approximately 500 feet of the site.
Water supply well WSW-5 is located on the site, approximately 90 feet southwest and cross-
gradient from the source area. Groundwater samples from well WSW-5 have not contained
detected concentrations of petroleum constituents since 2018. Well WSW-6 is located
approximately 350 feet north and upgradient of the source area of the release and has not
contained concentrations of petroleum constituents above the analytical method reporting limits
since at least 2009. Wells WSW-3 and WSW-4 are located approximately 550 to 600 feet
southwest and cross-gradient relative to the source area of the release. The wells previously
contained detected concentrations of petroleum products including MTBE; however, petroleum
constituents have not been reported in water samples collected from the water supply wells since at
least 2009. Municipal water is not available to the site and surrounding properties.

C.5 Surface Water
Based on review of the USGS Topographic Map, the closest body of water is intermittent Camp
Creek (Grass Creek, Stream Index 12-62-14, in the Yadkin Pee-Dee River Basin) located
approximately 225 feet east of the site. Surface water intakes are not known to be located within
1,500 feet of the source area of the release. Nearby surface water bodies are shown on Exhibit 1.
D. ASSESSMENT INFORMATION
D.1 Site Geology and Hydrology
The following resources were reviewed to evaluate site-specific geological and hydrogeological
characteristics.

Elkin N Quadrangle, North Carolina, USGS 7.5-minute series topographic map, dated 2000
(Exhibit 1).
Geologic Map of North Carolina, dated 1985.
Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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Soil Survey of Surry County, North Carolina, US Department of Agriculture, Natural
Resources Conservation Service, Web Soil Survey via the Internet,
http://websoilsurvey.nrcs.usda.gov/app/.

The site is located within the Alligator Back Formation of the Blue Ridge Belt in the Piedmont
Physiographic Province. The Piedmont Physiographic Province generally consists of low to medium
elevation, rounded hills and long rolling northeast to southwest trending ridges with incised creeks
and river channels. Rocks in the site vicinity consist of mica schist and phyllite.

In-place chemical and physical weathering of parent rocks typically forms residual soils in the
Piedmont region. Weathering is facilitated by the presence of fractures, joints, and less resistant
minerals in the rock. In areas not altered by erosion, alluvial deposition or the activities of man, the
typical residual soil profile consists of clay-rich unconsolidated materials at the surface, transitioning
to sandy silts and silty sands at depth. Typically, the boundary between soil and bedrock is not
sharply defined. This transitional zone is termed “partially weathered rock”. Information obtained
from the Surry County Soil Survey depicts soils on the site as Fairview sandy clay loam (FeC2). The
FeC2 is found on 8 to 15 percent slopes and consists of sandy clay loams that originated from
weathered schists and other micaceous metamorphic rock.

In the Piedmont, groundwater generally occurs in pore spaces within soils and in the structural
features present in the underlying rock (i.e. joints, fractures, and faults). Recharge to the water table
is primarily by precipitation infiltrating the surficial soils and percolating downward under the
influence of gravity to the water table. Typically, the water table is not a level surface, but a subdued
reflection of the land surface. The depth to the water table is not consistent and is dependent upon
several factors that include the amount of rainfall, permeability of the soil, the extent of fracturing in
the underlying rock and the influences of groundwater pumping. Groundwater typically flows in
directions sub-parallel to the ground surface and under the influence of gravity to discharge points
such as surface water features and the toes of slopes or natural springs.

Fluctuations in the depth of the water table can be expected depending on variations in
precipitation, surface water run-off and other factors not evident at the time of our subsurface
exploration. Normally, the highest levels of the water table occur in late winter and spring and the
lowest levels occur in the late summer and fall. Based on groundwater elevation measurements
taken in June 2022, groundwater is estimated to flow radially from the site toward the northeast,
east, and southeast on site.

D.2 Sampling Activities
Terracon mobilized to the site on August 25, 2022, to collect groundwater samples from the site
monitoring wells, which included MW-2/RW-2, MW-3/RW-3, MW-4/RW-4, MW-5, RW-5, MW-6,
MW-7, and MW-8. However, there was an insufficient volume of groundwater present in monitoring
wells MW-7 or MW-8 from which to collect a sample. The approximate locations of the wells are
depicted on Exhibit 2 and copies of Terracon’s field notes are included in Appendix A.
Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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D.3 LNAPL Evaluation
Measurable thicknesses of LNAPL were not encountered in the monitoring wells during this
assessment.

D.4 Groundwater Sampling Activities
Prior to sample collection, Terracon gauged the groundwater elevations in the monitoring wells
using a decontaminated electronic water level meter. The approximate locations of the wells are
shown on Exhibit 2, and monitoring well construction details and groundwater elevation
measurements are provided in Table 2. Groundwater flow was estimated, based on groundwater
elevation data, to be directed radially from the site to the northeast, east, and southeast. This is
consistent with recent data. Groundwater elevations and groundwater elevation contours are
depicted on Exhibit 4.

The monitoring wells were purged with a submersible pump using low flow sampling techniques
(i.e., <200 milliliters per minute) prior to sampling. The following parameters were periodically
measured during purging: pH, temperature, oxidation reduction potential (ORP), dissolved oxygen
(DO), and conductivity. Purging was considered complete once the field parameters stabilized.
Monitoring wells MW-7 and MW-8 did not have adequate volume present to purge the wells. The
groundwater samples were then collected into laboratory-supplied glassware, labeled, and stored in
an ice-packed cooler. The samples, along with chain-of-custody documentation, were delivered to
Pace National in Mt. Juliet, Tennessee under a standard turnaround time for analysis of volatile
organic compounds (VOCs) by EPA Method 6200B including xylenes, MTBE, EDB, and di-isopropyl
ether (IPE). Copies of field notes including groundwater parameters are provided in Appendix B.

D.5 Analytical Results
Based on the laboratory analytical report, several petroleum constituents were identified at
concentrations exceeding the established 2L Standards in groundwater samples collected from
monitoring wells MW-2/RW-2, MW-3/RW-3 and RW-5 during this sampling event.

 Benzene [1,740 µg/L], ethylbenzene [2,130 µg/L], isopropylbenzene [98.7 µg/L],
naphthalene [429 µg/L], n-propylbenzene [163 µg/L], toluene [1,700 µg/L], 1,2,4-
trimethylbenzene [1,940 µg/L], and total xylenes [7,330 µg/L] were reported by the
laboratory in the groundwater sample collected from monitoring well MW-2/RW-2 at
concentrations exceeding the 2L Standards but below the GCLs.
 Benzene [14.8 µg/L], naphthalene [191 µg/L], n-propylbenzene [187 µg/L], and
1,2,4-trimethylbenzene [285 µg/L] were reported by the laboratory in the
groundwater sample collected from monitoring well MW-3/RW-3 at concentrations
exceeding the 2L Standards but below the GCLs.
Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

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 Naphthalene [36.8 µg/L] was reported in the groundwater sample collected from
monitoring well RW-5 at concentrations exceeding the 2L Standard but below the
GCL.
 Multiple petroleum constituents were also reported in groundwater samples
collected from wells MW-2/RW-2, MW-3/RW-3, and RW-5 at concentrations
exceeding the laboratory detection limits but below the 2L Standards.
 No petroleum constituents were reported above laboratory method’s detection limits
in groundwater samples collected from monitoring wells MW-4/RW-4, MW-5, or MW-
6.

Summaries of the groundwater analytical results are included on Table 2 and Exhibit 5. The
historical groundwater analytical results summaries are in Table 4. A copy of the laboratory
analytical report is provided in Appendix B.
E. CONCLUSIONS AND RECOMMENDATIONS
Based on information obtained during the completion of these assessment activities, Terracon
provides the following findings and conclusions:

 Petroleum constituents were detected at concentrations exceeding the 2L Standards
but below the GCLs in groundwater samples from wells MW-2/RW-2, MW-3/RW-3,
and RW-5.
 Multiple petroleum constituents were also detected in groundwater samples from
wells MW-2/RW-2, MW-3/RW-3, and RW-5 at concentrations exceeding the
laboratory detection limits but below the 2L Standards.
 No target compounds were detected above laboratory detection limits in samples
collected from monitoring wells MW-4/RW-4, MW-5, or MW-6.
 Monitoring wells MW-7 and MW-8 were not able to be sampled, as there was not
enough groundwater volume in the wells at the time of sampling.
 Measurable thicknesses of LNAPL were not observed in the monitoring wells
gauged.
 Groundwater flow was estimated, based on groundwater elevation data, to be
toward the northeast, east, and southeast.

Based on the data presented in this Annual Monitoring Report, Terracon recommends the following
activities be completed at the site:

 Based on the results of this sampling event and the previous report’s biodegradation
model, the incident may be closed with a Notice of Residual Petroleum (NORP) and
a groundwater use restriction.

Annual Monitoring Report Jerry’s Place - Incident No. 9547 ■ State Road, NC October 27, 2022 ■ Terracon Project No. 75207118

Responsive ■ Resourceful ■ Reliable 9

H. REFERENCES
The following sources were utilized in developing this report:

Terracon, Inc., 2022. Annual Monitoring Report, Terracon, dated July 29, 2022.

ECS, Ltd., 2020. Groundwater Monitoring Report, ECS, dated January 7, 2020.

ECS, Ltd., 2015. Groundwater Monitoring Report, ECS, dated October 14, 2015.

ECS, Ltd., 2014. Groundwater Monitoring Report, ECS, dated September 16, 2014.

S&ME, Inc., 2011. Water Supply Well Sampling Report, S&ME, Inc., dated June 13, 2011.

Terraine, Inc., 2005. Groundwater Monitoring Report, Terraine, Inc., dated November 28, 2005.

Aggressive Fluid/Vapor Recovery Evaluation, November 22, 1996.

Bain, Palmer & Associates, Inc., 1993. Site Assessment Jerry’s Convenience Store, Bain, Palmer & Associates, Inc., dated June 30, 1993.

EXHIBITS

TOPOGRAPHIC MAP
Jerry’s Place (Incident No. 9547)
983 US Highway 21
State Road, Surry County, NC
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY QUADRANGLES INCLUDE: THURMOND, NC (1/1/1971) and ELKIN NORTH, NC (1/1/2000).
7327 W Friendly Ave Ste G
Greensboro, NC 27410-6253
75207118 Project Manager:
Drawn by:
Checked by:
Approved by:
JWR
EW
EW
1”=2,000’
May 2021
Project No.
Scale:
File Name:
Date: 1
Exhibit MIM
APPROXIMATE
SITE BOUNDARY
Jerrys Place
@A
@A
@A @A
@A
@A
@A@A
ED
"ÑÎ
"ÑÎ
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
0 30 60Feet
Legend
"ÑÎ Former Monitoring Well
ED Water Supply Well
@A Monitoring Well
Site Boundary
Parcel Boundary
File Path:
Date:
Project No.
Scale:
LRE
JWR
EW
EW
2
PM:
Drawn By:
Checked By:
Approved By:7327-G West Friendly Avenue Greensboro, NC 27410
Phone: [phone] Fax: [phone]
75207118 EXHIBITNO.SITE DIAGRAM
10/5/2022
Jerry's Place (Incident No. 9547)983 US Highway 21State Road, Surry County, NC
WSW-5
MW-7
MW-3/RW-3(PAVED OVER)RW-6
RW-5 U.S.
HI
GHWAY 21MW-2/RW-2
MW-6
MW-1(DESTROYED)
MW-8
MW-4/RW-4
MW-5
1 inch = 60 ft.
WATER SUPPLY WELL LOCATION MAP
Jerry’s Place (Incident No. 9547)
983 US Highway 21
State Road, Surry County, NC
MIM
EW
EW
Scale:
3
ExhibitProject Manager:
Drawn by:
Checked by:
Approved by:
Project No.
File Name:
Date:
MIM
Site boundary
7327-G West Friendly Avenue
Greensboro, NC
75207118
Jerry’s Place
May 2021
1” = 500’
Water Supply Well
Source: Groundwater Monitoring Report, ECS, 2014
@A
@A
@A @A
@A
@A
@A
@A
ED
"ÑÎ
"ÑÎ
0 30 60Feet
Legend
"ÑÎ Former Monitoring Well
ED Water Supply Well
@A Monitoring Well
Groundwater Elevation Contour
Groundwater Flow Direction
Site Boundary
Parcel Boundary
File Path:
Date:
Project No.
Scale:
LRE
JWR
EW
EW
4
PM:
Drawn By:
Checked By:
Approved By:7327-G West Friendly Avenue Greensboro, NC 27410
Phone: [phone] Fax: [phone]
75207118 EXHIBITNO.GROUNDWATER CONTOUR MAP (AUGUST 2022)
10/25/2022
Jerry's Place (Incident No. 9547)983 US Highway 21State Road, Surry County, NC
WSW-5
MW-7
MW-3/RW-3
RW-6(PAVED OVER)
RW-5
U.S
.
H
IGHWAY
21
MW-2/RW-2
MW-6
MW-1(DESTROYED)
MW-8
MW-4/RW-4
MW-5
1 inch = 60 ft.
(74.67)
(78.60)
(81.35)
(74.45)
(73.61)
(72.25)
(79.13)
(77.06)
74.00 76.0075.0073.00
7
8
.
0
0
7
7
.
0
0
79.
0
0
80.00
81.00
@A
@A
@A @A
@A
@A
@A@A
ED
"ÑÎ
"ÑÎ
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
0 30 60Feet
Legend
"ÑÎ Former Monitoring Well
ED Water Supply Well
@A Monitoring Well
Site Boundary
Parcel Boundary
File Path:
Date:
Project No.
Scale:
LRE
JWR
EW
EW
5
PM:
Drawn By:
Checked By:
Approved By:7327-G West Friendly Avenue Greensboro, NC 27410
Phone: [phone] Fax: [phone]
75207118 EXHIBITNO.GROUNDWATER ANALYTICAL RESULTS (AUGUST 2022)
10/25/2022
Jerry's Place (Incident No. 9547)983 US Highway 21State Road, Surry County, NC
WSW-5Not Sampled
MW-7
MW-3/RW-3
(PAVED OVER)RW-6
RW-5 U.S.
HI
GHWAY 21MW-2/RW-2
MW-6
MW-1(DESTROYED)
MW-8
MW-4/RW-4
MW-5
1 inch = 60 ft.
MW-2VOCs by 6200Benzene = 1,740 µg/LEthylbenzene = 2,130 µg/LIsopropylbenzene = 98.7 µg/LNaphthalene = 429 µg/Ln-Propylbenzene = 163 µg/LToluene = 1,700 µg/L1,2,4-Trimethylbenzene = 1,940 µg/L1,3,5-Trimethylbenzene = 382 µg/LXylenes (Total) = 7,330 µg/L
MW-3/RW-3VOCs by 6200Benzene = 14.8 µg/Lsec-Butylbenzene = 13.8 µg/LEthylbenzene = 106 µg/LIsopropylbenzene = 60.6 µg/Lp-Isopropyltoluene = 15.7 µg/LNaphthalene = 191 µg/Ln-Propylbenzene = 187 µg/LToluene = 1.60 µg/L1,2,4-Trimethylbenzene = 285 µg/L1,3,5-Trimethylbenzene = 108 µg/LXylenes (Total) = 86.5 µg/L
RW-5VOCs by 6200sec-Butylbenzene = 2.10 µg/LEthylbenzene = 15.7 µg/LIsopropylbenzene = 14.1 µg/Lp-Isopropylbenzene = 2.77 µg/LNaphthalene = 36.8 µg/Ln-Propylbenzene = 19.0 µg/L1,2,4-Trimethylbenzene = 43.1 µg/L1.3.5-Trimethylbenzene = 3.56 µg/LTotal Xylenes = 24.9 µg/L
MW-4/RW-4VOCs by 6200All Analytes Below Detection Limits
MW-5VOCs by 6200All Analytes Below Detection Limits
MW-7Not Sampled (Dry)
MW-8Not Sampled (Dry)
MW-6VOCs by 6200All Analytes Below Detection Limits

TABLES
TABLE 1
Water Supply Well Information
Jerry’s Place
State Road, Surry County, North Carolina
Terracon Project No. 75207118
NCDEQ Incident No. 9547
May 17, 2021

Note: Table generated from Groundwater Monitoring Report, ECS, dated September 16, 2014
TABLE 2Monitoring Well Construction Details and Groundwater Elevation DataJerry's PlaceState Road, Surry County, North CarolinaTerracon Project No. 75207118NCDEQ Incident No. 9547Well IDScreened Interval (ft. TOC)Total Well Depth (ft. BTOC)Top of Casing ElevationDate Water Level MeasuredDepth to Water (ft. BTOC)Groundwater ElevationComments6/16/2022 19.20 82.258/25/2022 20.10 81.356/16/2022 18.35 79.648/25/2022 19.39 78.606/16/2022 20.44 75.508/25/2022 21.27 74.676/16/2022 5.47 75.108/25/2022 6.12 74.456/16/2022 20.04 77.958/25/2022 20.93 77.066/16/2022 20.35 79.288/25/2022 20.50 79.136/16/2022 24.40 72.808/25/2022 24.95 72.256/16/2022 24.50 74.018/25/2022 24.90 73.61Notes:ft = feet TOC = Top of CasingbTOC = below TOC2-inch diameter Type II well 2-inch diameter Type II well 2-inch diameter Type II well MW-8MW-7MW-6RW-5MW-54-inch diameter Type II well 4-inch diameter Type II well 4-inch diameter Type II well 2-inch diameter Type II well; Stick-up completion4-inch diameter Type II well 2525271515-2515-2515-25Unknown15-25101.453012-32MW-2/RW-298.5197.2099.6397.9980.5725MW-4/RW-4 2-12 30 95.9497.993010-30MW-3/RW-3
TABLE 3
Summary of Groundwater Analytical Results
Jerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No. 9547
Terracon Project No. 75207118
Monitoring
Well
I.D. Date Collected
4/29/2021 510 <20.0 <20.0 4.21 590 47.3 <20.0 10.6 2.09 194 97.8 23.3 455 639 206 1716
6/16/2022 234 <20.0 <20.0 <20.0 379 49.8 <20.0 <200 <20.0 184 144 <20.0 42.7 650 295 752
8/25/2022 1740 <50.0 <50.0 <50.0 2130 98.7 <50.0 <500 <50.0 429 163 <50.0 1700 1940 382 7330
4/29/2021 <10.0 12.6 12.2 <10.0 99.4 59.4 <10.0 <10.0 <10.0 207 130 <10.0 <10.0 478 134 233
6/16/2022 14.8 13.4 15.9 <10.0 86.4 59.1 <10.0 <100 <10.0 179 157 <10.0 <10.0 384 130 143.5
8/25/2022 14.8 <1.00 13.8 <1.00 106 60.6 15.7 <10.0 <1.00 191 187 <1.00 1.60 285 108 86.5
4/29/2021 <1.0 <1.0 <1.0 <1.0 <1.0 1.41 <1.0 <10.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0
6/16/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
8/25/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <10.0 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
4/29/2021 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0
6/16/2022 <1.00 <1.00 <1.00 <1.00 1.26 1.27 <1.00 <1.00 <1.00 <5.00 3.03 <1.00 <1.00 1.89 <1.00 <2.00
8/25/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <10.0 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
4/29/2021 <5.0 <5.0 <5.0 <5.0 42 13.30 <5.0 <50.0 <5.0 58.5 21.30 <5.0 <5.0 131 17.4 108.2
6/16/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
8/25/2022 <1.00 <1.00 2.10 <1.00 15.7 14.1 2.77 <10.0 <1.00 36.8 19.0 <1.00 <1.00 43.1 3.56 24.9
6/16/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
8/25/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <10.0 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
MW-7 6/16/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
MW-8 6/16/2022 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <2.00
WSW-5 4/29/2021 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0
FB-1 4/29/2021 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0
1 70 70 70 600 70 25 100 20 6 70 70 600 400 400 500
5000 6900 8500 70000 84500 25000 11700 100000 20000 6000 30000 70000 260000 28500 25000 85500
Notes:All measurements in micrograms per liter (μ/L)Bold indicated detection above Laboratory Reported Detection Limit
NE = Not Established indicates concentrations exceeding 2L
J = Detected below laboratory reporting limit indicates concentrations exceeding GCL
NR = Not Reported Groundwater standards pursuant to NCDEQ, UST Section [Guidelines for Assessment and Corrective Action]
FB= Field Blank dated January 19, 2021
Gross Contamination Levels for
Groundwater (GCL)NaphthaleneNorth Carolina Groundwater Quality
Standards (2L Standards)4-Methyl-2-PentanoneMethyl Tert-Butyl etherMW-6
MW-5
MW-3/RW-3
MW-4/RW-4
RW-5
MW-2/RW-2
Analytical Method
Contaminant of Concern →Di-isopropyl etherEthylbenzeneIsopropylbenzeneN-ButylbenzeneSec-ButylbenzeneBenzeneVOCs by Method 6200B
1,2,4-TrimethylbenzeneTolueneStyrenen-PropylbenzeneXylenes (Total)1,3,5-Trimethylbenzenep-Isopropyltoluene1 of 1

APPENDIX A
FIELD NOTES AND PHOTOGRAPHS

NCDEQ 2020-2023-Jerrys Place ■ Incident # 9547 State Road, NC Date Pictures Taken: June 16, 2022 ■ Terracon Project No. 75207118
Responsive ■ Resourceful ■ Reliable

Photo 1 Overview of site, facing WNW. Photo 2 Monitoring well MW-5 stick up well in background. Storm drain access in foreground.

Photo 3 Monitoring well MW-5 stick up well. Photo 4 Monitoring well MW-4/RW-4.

Photo 5 Monitoring well MW-3/RW-3. Photo 6 Monitoring well MW-2/RW-2.
NCDEQ 2020-2023-Jerrys Place ■ Incident # 9547 State Road, NC Date Pictures Taken: June 16, 2022 ■ Terracon Project No. 75207118
Responsive ■ Resourceful ■ Reliable

Photo 7 Monitoring well MW-6. Photo 8 Recovery well RW-5.

Photo 9 Monitoring well MW-8. Photo 10 Monitoring well MW-7.

Photo 11 View from site toward cemetery to the east. Photo 12 View from site toward cemetery to the east.
NCDEQ 2020-2023-Jerrys Place ■ Incident # 9547 State Road, NC Date Pictures Taken: June 16, 2022 ■ Terracon Project No. 75207118
Responsive ■ Resourceful ■ Reliable

Photo 13 View from site toward the north. Photo 14 View from site toward the south.

Photo 15 View from site toward the west.

APPENDIX B
LABORATORY ANALYTICAL RESULTS AND
CHAIN-OF-CUSTODY FORMS
ANALYTICAL REPORT
September 07, 2022
Terracon - Greensboro, NC
Sample Delivery Group:L1530266
Samples Received:08/27/2022
Project Number:7520711B
Description:Jerry's Place
Report To:Jared Rose
7327-G, West Friendly Ave
Greensboro, NC 27410
Entire Report Reviewed By:
September 07, 2022
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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September 08, 2022
Heather J Wagner
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-2/RW-2 L1530266-01 5
RW-5 L1530266-02 7
MW4/RW-4 L1530266-03 9
MW3/RW-3 L1530266-04 11
MW-6 L1530266-05 13
MW-5 L1530266-06 15
Qc: Quality Control Summary 17
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 17
Gl: Glossary of Terms 25
Al: Accreditations & Locations 26
Sc: Sample Chain of Custody 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-2/RW-2 L1530266-01 GW Jared Rose 08/25/22 12:05 08/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1921999 50 09/06/22 18:31 09/06/22 18:31 JAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
RW-5 L1530266-02 GW Jared Rose 08/25/22 12:40 08/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1919995 1 09/01/22 16:26 09/01/22 16:26 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1921999 1 09/06/22 17:31 09/06/22 17:31 JAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW4/RW-4 L1530266-03 GW Jared Rose 08/25/22 13:45 08/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1919995 1 09/01/22 16:47 09/01/22 16:47 JAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW3/RW-3 L1530266-04 GW Jared Rose 08/25/22 15:00 08/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1919995 1 09/01/22 17:07 09/01/22 17:07 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1921999 10 09/06/22 18:51 09/06/22 18:51 JAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1530266-05 GW Jared Rose 08/25/22 15:20 08/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1919995 1 09/01/22 17:27 09/01/22 17:27 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1921999 1 09/06/22 17:51 09/06/22 17:51 JAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1530266-06 GW Jared Rose 08/25/22 16:15 08/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1919995 1 09/01/22 17:47 09/01/22 17:47 JAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Heather J Wagner
Project Manager
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SAMPLE RESULTS - 01
L1530266
MW-2/RW-2
Collected date/time: 08/25/22 12:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 2500 50 09/06/2022 18:31 WG1921999
Acrolein ND 2500 50 09/06/2022 18:31 WG1921999
Acrylonitrile ND 500 50 09/06/2022 18:31 WG1921999
Benzene 1740 50.0 50 09/06/2022 18:31 WG1921999
Bromobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
Bromodichloromethane ND 50.0 50 09/06/2022 18:31 WG1921999
Bromoform ND 50.0 50 09/06/2022 18:31 WG1921999
Bromomethane ND 250 50 09/06/2022 18:31 WG1921999
n-Butylbenzene ND 50.0 50 09/06/2022 18:31 WG1921999
sec-Butylbenzene ND 50.0 50 09/06/2022 18:31 WG1921999
tert-Butylbenzene ND 50.0 50 09/06/2022 18:31 WG1921999
Carbon tetrachloride ND 50.0 50 09/06/2022 18:31 WG1921999
Chlorobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
Chlorodibromomethane ND 50.0 50 09/06/2022 18:31 WG1921999
Chloroethane ND 250 50 09/06/2022 18:31 WG1921999
Chloroform ND 250 50 09/06/2022 18:31 WG1921999
Chloromethane ND 125 50 09/06/2022 18:31 WG1921999
2-Chlorotoluene ND 50.0 50 09/06/2022 18:31 WG1921999
4-Chlorotoluene ND 50.0 50 09/06/2022 18:31 WG1921999
1,2-Dibromo-3-Chloropropane ND 250 50 09/06/2022 18:31 WG1921999
1,2-Dibromoethane ND 50.0 50 09/06/2022 18:31 WG1921999
Dibromomethane ND 50.0 50 09/06/2022 18:31 WG1921999
1,2-Dichlorobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
1,3-Dichlorobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
1,4-Dichlorobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
Dichlorodifluoromethane ND 250 50 09/06/2022 18:31 WG1921999
1,1-Dichloroethane ND 50.0 50 09/06/2022 18:31 WG1921999
1,2-Dichloroethane ND 50.0 50 09/06/2022 18:31 WG1921999
1,1-Dichloroethene ND 50.0 50 09/06/2022 18:31 WG1921999
cis-1,2-Dichloroethene ND 50.0 50 09/06/2022 18:31 WG1921999
trans-1,2-Dichloroethene ND 50.0 50 09/06/2022 18:31 WG1921999
1,2-Dichloropropane ND 50.0 50 09/06/2022 18:31 WG1921999
1,1-Dichloropropene ND 50.0 50 09/06/2022 18:31 WG1921999
1,3-Dichloropropane ND 50.0 50 09/06/2022 18:31 WG1921999
2,2-Dichloropropane ND 50.0 50 09/06/2022 18:31 WG1921999
Di-isopropyl ether ND 50.0 50 09/06/2022 18:31 WG1921999
Ethylbenzene 2130 50.0 50 09/06/2022 18:31 WG1921999
Hexachloro-1,3-butadiene ND 50.0 50 09/06/2022 18:31 WG1921999
Isopropylbenzene 98.7 50.0 50 09/06/2022 18:31 WG1921999
p-Isopropyltoluene ND 50.0 50 09/06/2022 18:31 WG1921999
2-Butanone (MEK)ND 500 50 09/06/2022 18:31 WG1921999
Methylene Chloride ND 250 50 09/06/2022 18:31 WG1921999
4-Methyl-2-pentanone (MIBK)ND 500 50 09/06/2022 18:31 WG1921999
Methyl tert-butyl ether ND 50.0 50 09/06/2022 18:31 WG1921999
Naphthalene 429 250 50 09/06/2022 18:31 WG1921999
n-Propylbenzene 163 50.0 50 09/06/2022 18:31 WG1921999
Styrene ND 50.0 50 09/06/2022 18:31 WG1921999
1,1,1,2-Tetrachloroethane ND 50.0 50 09/06/2022 18:31 WG1921999
1,1,2,2-Tetrachloroethane ND 50.0 50 09/06/2022 18:31 WG1921999
Tetrachloroethene ND 50.0 50 09/06/2022 18:31 WG1921999
Toluene 1700 50.0 50 09/06/2022 18:31 WG1921999
1,2,3-Trichlorobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
1,2,4-Trichlorobenzene ND 50.0 50 09/06/2022 18:31 WG1921999
1,1,1-Trichloroethane ND 50.0 50 09/06/2022 18:31 WG1921999
1,1,2-Trichloroethane ND 50.0 50 09/06/2022 18:31 WG1921999
Trichloroethene ND 50.0 50 09/06/2022 18:31 WG1921999
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1530266
MW-2/RW-2
Collected date/time: 08/25/22 12:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Trichlorofluoromethane ND 250 50 09/06/2022 18:31 WG1921999
1,2,3-Trichloropropane ND 125 50 09/06/2022 18:31 WG1921999
1,2,4-Trimethylbenzene 1940 50.0 50 09/06/2022 18:31 WG1921999
1,3,5-Trimethylbenzene 382 50.0 50 09/06/2022 18:31 WG1921999
Vinyl chloride ND 50.0 50 09/06/2022 18:31 WG1921999
o-Xylene 2810 50.0 50 09/06/2022 18:31 WG1921999
m&p-Xylenes 4520 100 50 09/06/2022 18:31 WG1921999
(S) Toluene-d8 104 80.0-120 09/06/2022 18:31 WG1921999
(S) 4-Bromofluorobenzene 96.8 77.0-126 09/06/2022 18:31 WG1921999
(S) 1,2-Dichloroethane-d4 99.6 70.0-130 09/06/2022 18:31 WG1921999
Sample Narrative:
L1530266-01 WG1921999: Target compounds too high to run at a lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1530266
RW-5
Collected date/time: 08/25/22 12:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 09/01/2022 16:26 WG1919995
Acrolein ND 50.0 1 09/01/2022 16:26 WG1919995
Acrylonitrile ND 10.0 1 09/01/2022 16:26 WG1919995
Benzene ND 1.00 1 09/01/2022 16:26 WG1919995
Bromobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
Bromodichloromethane ND 1.00 1 09/01/2022 16:26 WG1919995
Bromoform ND 1.00 1 09/01/2022 16:26 WG1919995
Bromomethane ND 5.00 1 09/01/2022 16:26 WG1919995
n-Butylbenzene ND 1.00 1 09/01/2022 16:26 WG1919995
sec-Butylbenzene 2.10 1.00 1 09/06/2022 17:31 WG1921999
tert-Butylbenzene ND 1.00 1 09/01/2022 16:26 WG1919995
Carbon tetrachloride ND 1.00 1 09/01/2022 16:26 WG1919995
Chlorobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
Chlorodibromomethane ND 1.00 1 09/01/2022 16:26 WG1919995
Chloroethane ND 5.00 1 09/01/2022 16:26 WG1919995
Chloroform ND 5.00 1 09/01/2022 16:26 WG1919995
Chloromethane ND 2.50 1 09/01/2022 16:26 WG1919995
2-Chlorotoluene ND 1.00 1 09/01/2022 16:26 WG1919995
4-Chlorotoluene ND 1.00 1 09/01/2022 16:26 WG1919995
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/01/2022 16:26 WG1919995
1,2-Dibromoethane ND 1.00 1 09/01/2022 16:26 WG1919995
Dibromomethane ND 1.00 1 09/01/2022 16:26 WG1919995
1,2-Dichlorobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
1,3-Dichlorobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
1,4-Dichlorobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
Dichlorodifluoromethane ND 5.00 1 09/01/2022 16:26 WG1919995
1,1-Dichloroethane ND 1.00 1 09/01/2022 16:26 WG1919995
1,2-Dichloroethane ND 1.00 1 09/01/2022 16:26 WG1919995
1,1-Dichloroethene ND 1.00 1 09/01/2022 16:26 WG1919995
cis-1,2-Dichloroethene ND 1.00 1 09/01/2022 16:26 WG1919995
trans-1,2-Dichloroethene ND 1.00 1 09/01/2022 16:26 WG1919995
1,2-Dichloropropane ND J4 1.00 1 09/01/2022 16:26 WG1919995
1,1-Dichloropropene ND 1.00 1 09/01/2022 16:26 WG1919995
1,3-Dichloropropane ND 1.00 1 09/01/2022 16:26 WG1919995
2,2-Dichloropropane ND 1.00 1 09/01/2022 16:26 WG1919995
Di-isopropyl ether ND 1.00 1 09/01/2022 16:26 WG1919995
Ethylbenzene 15.7 1.00 1 09/06/2022 17:31 WG1921999
Hexachloro-1,3-butadiene ND 1.00 1 09/01/2022 16:26 WG1919995
Isopropylbenzene 14.1 1.00 1 09/06/2022 17:31 WG1921999
p-Isopropyltoluene 2.77 1.00 1 09/06/2022 17:31 WG1921999
2-Butanone (MEK)ND 10.0 1 09/01/2022 16:26 WG1919995
Methylene Chloride ND 5.00 1 09/01/2022 16:26 WG1919995
4-Methyl-2-pentanone (MIBK)ND 10.0 1 09/01/2022 16:26 WG1919995
Methyl tert-butyl ether ND 1.00 1 09/01/2022 16:26 WG1919995
Naphthalene 36.8 5.00 1 09/06/2022 17:31 WG1921999
n-Propylbenzene 19.0 1.00 1 09/06/2022 17:31 WG1921999
Styrene ND 1.00 1 09/01/2022 16:26 WG1919995
1,1,1,2-Tetrachloroethane ND 1.00 1 09/01/2022 16:26 WG1919995
1,1,2,2-Tetrachloroethane ND 1.00 1 09/01/2022 16:26 WG1919995
Tetrachloroethene ND 1.00 1 09/01/2022 16:26 WG1919995
Toluene ND 1.00 1 09/06/2022 17:31 WG1921999
1,2,3-Trichlorobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
1,2,4-Trichlorobenzene ND 1.00 1 09/01/2022 16:26 WG1919995
1,1,1-Trichloroethane ND 1.00 1 09/01/2022 16:26 WG1919995
1,1,2-Trichloroethane ND 1.00 1 09/01/2022 16:26 WG1919995
Trichloroethene ND 1.00 1 09/01/2022 16:26 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 7 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 7 of 27
SAMPLE RESULTS - 02
L1530266
RW-5
Collected date/time: 08/25/22 12:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Trichlorofluoromethane ND 5.00 1 09/01/2022 16:26 WG1919995
1,2,3-Trichloropropane ND 2.50 1 09/01/2022 16:26 WG1919995
1,2,4-Trimethylbenzene 43.1 1.00 1 09/06/2022 17:31 WG1921999
1,3,5-Trimethylbenzene 3.56 1.00 1 09/06/2022 17:31 WG1921999
Vinyl chloride ND 1.00 1 09/01/2022 16:26 WG1919995
o-Xylene 8.00 1.00 1 09/06/2022 17:31 WG1921999
m&p-Xylenes 16.9 2.00 1 09/06/2022 17:31 WG1921999
(S) Toluene-d8 99.9 80.0-120 09/01/2022 16:26 WG1919995
(S) Toluene-d8 102 80.0-120 09/06/2022 17:31 WG1921999
(S) 4-Bromofluorobenzene 101 77.0-126 09/01/2022 16:26 WG1919995
(S) 4-Bromofluorobenzene 106 77.0-126 09/06/2022 17:31 WG1921999
(S) 1,2-Dichloroethane-d4 101 70.0-130 09/01/2022 16:26 WG1919995
(S) 1,2-Dichloroethane-d4 116 70.0-130 09/06/2022 17:31 WG1921999
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 8 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 8 of 27
SAMPLE RESULTS - 03
L1530266
MW4/RW-4
Collected date/time: 08/25/22 13:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 09/01/2022 16:47 WG1919995
Acrolein ND 50.0 1 09/01/2022 16:47 WG1919995
Acrylonitrile ND 10.0 1 09/01/2022 16:47 WG1919995
Benzene ND 1.00 1 09/01/2022 16:47 WG1919995
Bromobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Bromodichloromethane ND 1.00 1 09/01/2022 16:47 WG1919995
Bromoform ND 1.00 1 09/01/2022 16:47 WG1919995
Bromomethane ND 5.00 1 09/01/2022 16:47 WG1919995
n-Butylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
sec-Butylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
tert-Butylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Carbon tetrachloride ND 1.00 1 09/01/2022 16:47 WG1919995
Chlorobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Chlorodibromomethane ND 1.00 1 09/01/2022 16:47 WG1919995
Chloroethane ND 5.00 1 09/01/2022 16:47 WG1919995
Chloroform ND 5.00 1 09/01/2022 16:47 WG1919995
Chloromethane ND 2.50 1 09/01/2022 16:47 WG1919995
2-Chlorotoluene ND 1.00 1 09/01/2022 16:47 WG1919995
4-Chlorotoluene ND 1.00 1 09/01/2022 16:47 WG1919995
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/01/2022 16:47 WG1919995
1,2-Dibromoethane ND 1.00 1 09/01/2022 16:47 WG1919995
Dibromomethane ND 1.00 1 09/01/2022 16:47 WG1919995
1,2-Dichlorobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
1,3-Dichlorobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
1,4-Dichlorobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Dichlorodifluoromethane ND 5.00 1 09/01/2022 16:47 WG1919995
1,1-Dichloroethane ND 1.00 1 09/01/2022 16:47 WG1919995
1,2-Dichloroethane ND 1.00 1 09/01/2022 16:47 WG1919995
1,1-Dichloroethene ND 1.00 1 09/01/2022 16:47 WG1919995
cis-1,2-Dichloroethene ND 1.00 1 09/01/2022 16:47 WG1919995
trans-1,2-Dichloroethene ND 1.00 1 09/01/2022 16:47 WG1919995
1,2-Dichloropropane ND J4 1.00 1 09/01/2022 16:47 WG1919995
1,1-Dichloropropene ND 1.00 1 09/01/2022 16:47 WG1919995
1,3-Dichloropropane ND 1.00 1 09/01/2022 16:47 WG1919995
2,2-Dichloropropane ND 1.00 1 09/01/2022 16:47 WG1919995
Di-isopropyl ether ND 1.00 1 09/01/2022 16:47 WG1919995
Ethylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Hexachloro-1,3-butadiene ND 1.00 1 09/01/2022 16:47 WG1919995
Isopropylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
p-Isopropyltoluene ND 1.00 1 09/01/2022 16:47 WG1919995
2-Butanone (MEK)ND 10.0 1 09/01/2022 16:47 WG1919995
Methylene Chloride ND 5.00 1 09/01/2022 16:47 WG1919995
4-Methyl-2-pentanone (MIBK)ND 10.0 1 09/01/2022 16:47 WG1919995
Methyl tert-butyl ether ND 1.00 1 09/01/2022 16:47 WG1919995
Naphthalene ND 5.00 1 09/01/2022 16:47 WG1919995
n-Propylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Styrene ND 1.00 1 09/01/2022 16:47 WG1919995
1,1,1,2-Tetrachloroethane ND 1.00 1 09/01/2022 16:47 WG1919995
1,1,2,2-Tetrachloroethane ND 1.00 1 09/01/2022 16:47 WG1919995
Tetrachloroethene ND 1.00 1 09/01/2022 16:47 WG1919995
Toluene ND 1.00 1 09/01/2022 16:47 WG1919995
1,2,3-Trichlorobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
1,2,4-Trichlorobenzene ND 1.00 1 09/01/2022 16:47 WG1919995
1,1,1-Trichloroethane ND 1.00 1 09/01/2022 16:47 WG1919995
1,1,2-Trichloroethane ND 1.00 1 09/01/2022 16:47 WG1919995
Trichloroethene ND 1.00 1 09/01/2022 16:47 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 9 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 9 of 27
SAMPLE RESULTS - 03
L1530266
MW4/RW-4
Collected date/time: 08/25/22 13:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Trichlorofluoromethane ND 5.00 1 09/01/2022 16:47 WG1919995
1,2,3-Trichloropropane ND 2.50 1 09/01/2022 16:47 WG1919995
1,2,4-Trimethylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
1,3,5-Trimethylbenzene ND 1.00 1 09/01/2022 16:47 WG1919995
Vinyl chloride ND 1.00 1 09/01/2022 16:47 WG1919995
o-Xylene ND 1.00 1 09/01/2022 16:47 WG1919995
m&p-Xylenes ND 2.00 1 09/01/2022 16:47 WG1919995
(S) Toluene-d8 108 80.0-120 09/01/2022 16:47 WG1919995
(S) 4-Bromofluorobenzene 104 77.0-126 09/01/2022 16:47 WG1919995
(S) 1,2-Dichloroethane-d4 95.4 70.0-130 09/01/2022 16:47 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 10 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 10 of 27
SAMPLE RESULTS - 04
L1530266
MW3/RW-3
Collected date/time: 08/25/22 15:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 09/01/2022 17:07 WG1919995
Acrolein ND 50.0 1 09/01/2022 17:07 WG1919995
Acrylonitrile ND 10.0 1 09/01/2022 17:07 WG1919995
Benzene 14.8 1.00 1 09/01/2022 17:07 WG1919995
Bromobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
Bromodichloromethane ND 1.00 1 09/01/2022 17:07 WG1919995
Bromoform ND 1.00 1 09/01/2022 17:07 WG1919995
Bromomethane ND 5.00 1 09/01/2022 17:07 WG1919995
n-Butylbenzene ND 1.00 1 09/01/2022 17:07 WG1919995
sec-Butylbenzene 13.8 1.00 1 09/01/2022 17:07 WG1919995
tert-Butylbenzene ND 1.00 1 09/01/2022 17:07 WG1919995
Carbon tetrachloride ND 1.00 1 09/01/2022 17:07 WG1919995
Chlorobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
Chlorodibromomethane ND 1.00 1 09/01/2022 17:07 WG1919995
Chloroethane ND 5.00 1 09/01/2022 17:07 WG1919995
Chloroform ND 5.00 1 09/01/2022 17:07 WG1919995
Chloromethane ND 2.50 1 09/01/2022 17:07 WG1919995
2-Chlorotoluene ND 1.00 1 09/01/2022 17:07 WG1919995
4-Chlorotoluene ND 1.00 1 09/01/2022 17:07 WG1919995
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/01/2022 17:07 WG1919995
1,2-Dibromoethane ND 1.00 1 09/01/2022 17:07 WG1919995
Dibromomethane ND 1.00 1 09/01/2022 17:07 WG1919995
1,2-Dichlorobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
1,3-Dichlorobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
1,4-Dichlorobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
Dichlorodifluoromethane ND 5.00 1 09/01/2022 17:07 WG1919995
1,1-Dichloroethane ND 1.00 1 09/01/2022 17:07 WG1919995
1,2-Dichloroethane ND 1.00 1 09/01/2022 17:07 WG1919995
1,1-Dichloroethene ND 1.00 1 09/01/2022 17:07 WG1919995
cis-1,2-Dichloroethene ND 1.00 1 09/01/2022 17:07 WG1919995
trans-1,2-Dichloroethene ND 1.00 1 09/01/2022 17:07 WG1919995
1,2-Dichloropropane ND J4 1.00 1 09/01/2022 17:07 WG1919995
1,1-Dichloropropene ND 1.00 1 09/01/2022 17:07 WG1919995
1,3-Dichloropropane ND 1.00 1 09/01/2022 17:07 WG1919995
2,2-Dichloropropane ND 1.00 1 09/01/2022 17:07 WG1919995
Di-isopropyl ether ND 1.00 1 09/01/2022 17:07 WG1919995
Ethylbenzene 106 1.00 1 09/01/2022 17:07 WG1919995
Hexachloro-1,3-butadiene ND 1.00 1 09/01/2022 17:07 WG1919995
Isopropylbenzene 60.6 1.00 1 09/01/2022 17:07 WG1919995
p-Isopropyltoluene 15.7 1.00 1 09/01/2022 17:07 WG1919995
2-Butanone (MEK)ND 10.0 1 09/01/2022 17:07 WG1919995
Methylene Chloride ND 5.00 1 09/01/2022 17:07 WG1919995
4-Methyl-2-pentanone (MIBK)ND 10.0 1 09/01/2022 17:07 WG1919995
Methyl tert-butyl ether ND 1.00 1 09/01/2022 17:07 WG1919995
Naphthalene 191 5.00 1 09/01/2022 17:07 WG1919995
n-Propylbenzene 187 1.00 1 09/01/2022 17:07 WG1919995
Styrene ND 1.00 1 09/01/2022 17:07 WG1919995
1,1,1,2-Tetrachloroethane ND 1.00 1 09/01/2022 17:07 WG1919995
1,1,2,2-Tetrachloroethane ND 1.00 1 09/01/2022 17:07 WG1919995
Tetrachloroethene ND 1.00 1 09/01/2022 17:07 WG1919995
Toluene 1.60 1.00 1 09/01/2022 17:07 WG1919995
1,2,3-Trichlorobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
1,2,4-Trichlorobenzene ND 1.00 1 09/01/2022 17:07 WG1919995
1,1,1-Trichloroethane ND 1.00 1 09/01/2022 17:07 WG1919995
1,1,2-Trichloroethane ND 1.00 1 09/01/2022 17:07 WG1919995
Trichloroethene ND 1.00 1 09/01/2022 17:07 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 11 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 11 of 27
SAMPLE RESULTS - 04
L1530266
MW3/RW-3
Collected date/time: 08/25/22 15:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Trichlorofluoromethane ND 5.00 1 09/01/2022 17:07 WG1919995
1,2,3-Trichloropropane ND 2.50 1 09/01/2022 17:07 WG1919995
1,2,4-Trimethylbenzene 285 10.0 10 09/06/2022 18:51 WG1921999
1,3,5-Trimethylbenzene 108 1.00 1 09/01/2022 17:07 WG1919995
Vinyl chloride ND 1.00 1 09/01/2022 17:07 WG1919995
o-Xylene 23.8 1.00 1 09/01/2022 17:07 WG1919995
m&p-Xylenes 62.7 2.00 1 09/01/2022 17:07 WG1919995
(S) Toluene-d8 97.2 80.0-120 09/01/2022 17:07 WG1919995
(S) Toluene-d8 105 80.0-120 09/06/2022 18:51 WG1921999
(S) 4-Bromofluorobenzene 98.8 77.0-126 09/01/2022 17:07 WG1919995
(S) 4-Bromofluorobenzene 102 77.0-126 09/06/2022 18:51 WG1921999
(S) 1,2-Dichloroethane-d4 106 70.0-130 09/01/2022 17:07 WG1919995
(S) 1,2-Dichloroethane-d4 100 70.0-130 09/06/2022 18:51 WG1921999
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 12 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 12 of 27
SAMPLE RESULTS - 05
L1530266
MW-6
Collected date/time: 08/25/22 15:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 09/01/2022 17:27 WG1919995
Acrolein ND 50.0 1 09/01/2022 17:27 WG1919995
Acrylonitrile ND 10.0 1 09/01/2022 17:27 WG1919995
Benzene ND 1.00 1 09/01/2022 17:27 WG1919995
Bromobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Bromodichloromethane ND 1.00 1 09/01/2022 17:27 WG1919995
Bromoform ND 1.00 1 09/01/2022 17:27 WG1919995
Bromomethane ND 5.00 1 09/01/2022 17:27 WG1919995
n-Butylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
sec-Butylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
tert-Butylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Carbon tetrachloride ND 1.00 1 09/01/2022 17:27 WG1919995
Chlorobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Chlorodibromomethane ND 1.00 1 09/01/2022 17:27 WG1919995
Chloroethane ND 5.00 1 09/01/2022 17:27 WG1919995
Chloroform ND 5.00 1 09/01/2022 17:27 WG1919995
Chloromethane ND 2.50 1 09/01/2022 17:27 WG1919995
2-Chlorotoluene ND 1.00 1 09/01/2022 17:27 WG1919995
4-Chlorotoluene ND 1.00 1 09/01/2022 17:27 WG1919995
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/01/2022 17:27 WG1919995
1,2-Dibromoethane ND 1.00 1 09/01/2022 17:27 WG1919995
Dibromomethane ND 1.00 1 09/01/2022 17:27 WG1919995
1,2-Dichlorobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
1,3-Dichlorobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
1,4-Dichlorobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Dichlorodifluoromethane ND 5.00 1 09/01/2022 17:27 WG1919995
1,1-Dichloroethane ND 1.00 1 09/01/2022 17:27 WG1919995
1,2-Dichloroethane ND 1.00 1 09/01/2022 17:27 WG1919995
1,1-Dichloroethene ND 1.00 1 09/01/2022 17:27 WG1919995
cis-1,2-Dichloroethene ND 1.00 1 09/01/2022 17:27 WG1919995
trans-1,2-Dichloroethene ND 1.00 1 09/01/2022 17:27 WG1919995
1,2-Dichloropropane ND J4 1.00 1 09/01/2022 17:27 WG1919995
1,1-Dichloropropene ND 1.00 1 09/01/2022 17:27 WG1919995
1,3-Dichloropropane ND 1.00 1 09/01/2022 17:27 WG1919995
2,2-Dichloropropane ND 1.00 1 09/01/2022 17:27 WG1919995
Di-isopropyl ether ND 1.00 1 09/01/2022 17:27 WG1919995
Ethylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Hexachloro-1,3-butadiene ND 1.00 1 09/01/2022 17:27 WG1919995
Isopropylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
p-Isopropyltoluene ND 1.00 1 09/01/2022 17:27 WG1919995
2-Butanone (MEK)ND 10.0 1 09/01/2022 17:27 WG1919995
Methylene Chloride ND 5.00 1 09/01/2022 17:27 WG1919995
4-Methyl-2-pentanone (MIBK)ND 10.0 1 09/01/2022 17:27 WG1919995
Methyl tert-butyl ether ND 1.00 1 09/01/2022 17:27 WG1919995
Naphthalene ND 5.00 1 09/06/2022 17:51 WG1921999
n-Propylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Styrene ND 1.00 1 09/01/2022 17:27 WG1919995
1,1,1,2-Tetrachloroethane ND 1.00 1 09/01/2022 17:27 WG1919995
1,1,2,2-Tetrachloroethane ND 1.00 1 09/01/2022 17:27 WG1919995
Tetrachloroethene ND 1.00 1 09/01/2022 17:27 WG1919995
Toluene ND 1.00 1 09/01/2022 17:27 WG1919995
1,2,3-Trichlorobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
1,2,4-Trichlorobenzene ND 1.00 1 09/01/2022 17:27 WG1919995
1,1,1-Trichloroethane ND 1.00 1 09/01/2022 17:27 WG1919995
1,1,2-Trichloroethane ND 1.00 1 09/01/2022 17:27 WG1919995
Trichloroethene ND 1.00 1 09/01/2022 17:27 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 13 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 13 of 27
SAMPLE RESULTS - 05
L1530266
MW-6
Collected date/time: 08/25/22 15:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Trichlorofluoromethane ND 5.00 1 09/01/2022 17:27 WG1919995
1,2,3-Trichloropropane ND 2.50 1 09/01/2022 17:27 WG1919995
1,2,4-Trimethylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
1,3,5-Trimethylbenzene ND 1.00 1 09/01/2022 17:27 WG1919995
Vinyl chloride ND 1.00 1 09/01/2022 17:27 WG1919995
o-Xylene ND 1.00 1 09/01/2022 17:27 WG1919995
m&p-Xylenes ND 2.00 1 09/01/2022 17:27 WG1919995
(S) Toluene-d8 106 80.0-120 09/01/2022 17:27 WG1919995
(S) Toluene-d8 110 80.0-120 09/06/2022 17:51 WG1921999
(S) 4-Bromofluorobenzene 104 77.0-126 09/01/2022 17:27 WG1919995
(S) 4-Bromofluorobenzene 107 77.0-126 09/06/2022 17:51 WG1921999
(S) 1,2-Dichloroethane-d4 98.6 70.0-130 09/01/2022 17:27 WG1919995
(S) 1,2-Dichloroethane-d4 104 70.0-130 09/06/2022 17:51 WG1921999
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/07/22 15:31 14 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 7520711B L1530266 09/08/22 09:12 14 of 27
SAMPLE RESULTS - 06
L1530266
MW-5
Collected date/time: 08/25/22 16:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 09/01/2022 17:47 WG1919995
Acrolein ND 50.0 1 09/01/2022 17:47 WG1919995
Acrylonitrile ND 10.0 1 09/01/2022 17:47 WG1919995
Benzene ND 1.00 1 09/01/2022 17:47 WG1919995
Bromobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Bromodichloromethane ND 1.00 1 09/01/2022 17:47 WG1919995
Bromoform ND 1.00 1 09/01/2022 17:47 WG1919995
Bromomethane ND 5.00 1 09/01/2022 17:47 WG1919995
n-Butylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
sec-Butylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
tert-Butylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Carbon tetrachloride ND 1.00 1 09/01/2022 17:47 WG1919995
Chlorobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Chlorodibromomethane ND 1.00 1 09/01/2022 17:47 WG1919995
Chloroethane ND 5.00 1 09/01/2022 17:47 WG1919995
Chloroform ND 5.00 1 09/01/2022 17:47 WG1919995
Chloromethane ND 2.50 1 09/01/2022 17:47 WG1919995
2-Chlorotoluene ND 1.00 1 09/01/2022 17:47 WG1919995
4-Chlorotoluene ND 1.00 1 09/01/2022 17:47 WG1919995
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/01/2022 17:47 WG1919995
1,2-Dibromoethane ND 1.00 1 09/01/2022 17:47 WG1919995
Dibromomethane ND 1.00 1 09/01/2022 17:47 WG1919995
1,2-Dichlorobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
1,3-Dichlorobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
1,4-Dichlorobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Dichlorodifluoromethane ND 5.00 1 09/01/2022 17:47 WG1919995
1,1-Dichloroethane ND 1.00 1 09/01/2022 17:47 WG1919995
1,2-Dichloroethane ND 1.00 1 09/01/2022 17:47 WG1919995
1,1-Dichloroethene ND 1.00 1 09/01/2022 17:47 WG1919995
cis-1,2-Dichloroethene ND 1.00 1 09/01/2022 17:47 WG1919995
trans-1,2-Dichloroethene ND 1.00 1 09/01/2022 17:47 WG1919995
1,2-Dichloropropane ND J4 1.00 1 09/01/2022 17:47 WG1919995
1,1-Dichloropropene ND 1.00 1 09/01/2022 17:47 WG1919995
1,3-Dichloropropane ND 1.00 1 09/01/2022 17:47 WG1919995
2,2-Dichloropropane ND 1.00 1 09/01/2022 17:47 WG1919995
Di-isopropyl ether ND 1.00 1 09/01/2022 17:47 WG1919995
Ethylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Hexachloro-1,3-butadiene ND 1.00 1 09/01/2022 17:47 WG1919995
Isopropylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
p-Isopropyltoluene ND 1.00 1 09/01/2022 17:47 WG1919995
2-Butanone (MEK)ND 10.0 1 09/01/2022 17:47 WG1919995
Methylene Chloride ND 5.00 1 09/01/2022 17:47 WG1919995
4-Methyl-2-pentanone (MIBK)ND 10.0 1 09/01/2022 17:47 WG1919995
Methyl tert-butyl ether ND 1.00 1 09/01/2022 17:47 WG1919995
Naphthalene ND 5.00 1 09/01/2022 17:47 WG1919995
n-Propylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Styrene ND 1.00 1 09/01/2022 17:47 WG1919995
1,1,1,2-Tetrachloroethane ND 1.00 1 09/01/2022 17:47 WG1919995
1,1,2,2-Tetrachloroethane ND 1.00 1 09/01/2022 17:47 WG1919995
Tetrachloroethene ND 1.00 1 09/01/2022 17:47 WG1919995
Toluene ND 1.00 1 09/01/2022 17:47 WG1919995
1,2,3-Trichlorobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
1,2,4-Trichlorobenzene ND 1.00 1 09/01/2022 17:47 WG1919995
1,1,1-Trichloroethane ND 1.00 1 09/01/2022 17:47 WG1919995
1,1,2-Trichloroethane ND 1.00 1 09/01/2022 17:47 WG1919995
Trichloroethene ND 1.00 1 09/01/2022 17:47 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 06
L1530266
MW-5
Collected date/time: 08/25/22 16:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Trichlorofluoromethane ND 5.00 1 09/01/2022 17:47 WG1919995
1,2,3-Trichloropropane ND 2.50 1 09/01/2022 17:47 WG1919995
1,2,4-Trimethylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
1,3,5-Trimethylbenzene ND 1.00 1 09/01/2022 17:47 WG1919995
Vinyl chloride ND 1.00 1 09/01/2022 17:47 WG1919995
o-Xylene ND 1.00 1 09/01/2022 17:47 WG1919995
m&p-Xylenes ND 2.00 1 09/01/2022 17:47 WG1919995
(S) Toluene-d8 108 80.0-120 09/01/2022 17:47 WG1919995
(S) 4-Bromofluorobenzene 103 77.0-126 09/01/2022 17:47 WG1919995
(S) 1,2-Dichloroethane-d4 95.9 70.0-130 09/01/2022 17:47 WG1919995
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1919995
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-02,03,04,05,06
Method Blank (MB)
(MB) R3834051-2 09/01/22 09:05
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1919995
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-02,03,04,05,06
Method Blank (MB)
(MB) R3834051-2 09/01/22 09:05
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 104 77.0-126
(S) 1,2-Dichloroethane-d4 98.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3834051-1 09/01/22 08:23
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acetone 25.0 24.6 98.4 19.0-160
Acrolein 25.0 20.9 83.6 10.0-160
Acrylonitrile 25.0 22.4 89.6 55.0-149
Benzene 5.00 4.25 85.0 70.0-123
Bromobenzene 5.00 4.50 90.0 73.0-121
Bromodichloromethane 5.00 4.40 88.0 75.0-120
Bromoform 5.00 4.43 88.6 68.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1919995
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3834051-1 09/01/22 08:23
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromomethane 5.00 4.54 90.8 10.0-160
n-Butylbenzene 5.00 3.99 79.8 73.0-125
sec-Butylbenzene 5.00 4.08 81.6 75.0-125
tert-Butylbenzene 5.00 4.27 85.4 76.0-124
Carbon tetrachloride 5.00 4.58 91.6 68.0-126
Chlorobenzene 5.00 4.68 93.6 80.0-121
Chlorodibromomethane 5.00 4.56 91.2 77.0-125
Chloroethane 5.00 3.75 75.0 47.0-150
Chloroform 5.00 4.66 93.2 73.0-120
Chloromethane 5.00 4.67 93.4 41.0-142
2-Chlorotoluene 5.00 4.29 85.8 76.0-123
4-Chlorotoluene 5.00 4.42 88.4 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.01 80.2 58.0-134
1,2-Dibromoethane 5.00 4.26 85.2 80.0-122
Dibromomethane 5.00 4.73 94.6 80.0-120
1,2-Dichlorobenzene 5.00 4.38 87.6 79.0-121
1,3-Dichlorobenzene 5.00 4.35 87.0 79.0-120
1,4-Dichlorobenzene 5.00 4.50 90.0 79.0-120
Dichlorodifluoromethane 5.00 4.05 81.0 51.0-149
1,1-Dichloroethane 5.00 4.46 89.2 70.0-126
1,2-Dichloroethane 5.00 4.05 81.0 70.0-128
1,1-Dichloroethene 5.00 4.42 88.4 71.0-124
cis-1,2-Dichloroethene 5.00 4.61 92.2 73.0-120
trans-1,2-Dichloroethene 5.00 4.53 90.6 73.0-120
1,2-Dichloropropane 5.00 3.80 76.0 77.0-125 J4
1,1-Dichloropropene 5.00 4.60 92.0 74.0-126
1,3-Dichloropropane 5.00 4.61 92.2 80.0-120
2,2-Dichloropropane 5.00 4.36 87.2 58.0-130
Di-isopropyl ether 5.00 4.67 93.4 58.0-138
Ethylbenzene 5.00 4.52 90.4 79.0-123
Hexachloro-1,3-butadiene 5.00 4.05 81.0 54.0-138
Isopropylbenzene 5.00 4.44 88.8 76.0-127
p-Isopropyltoluene 5.00 4.35 87.0 76.0-125
2-Butanone (MEK)25.0 22.6 90.4 44.0-160
Methylene Chloride 5.00 4.30 86.0 67.0-120
4-Methyl-2-pentanone (MIBK)25.0 24.2 96.8 68.0-142
Methyl tert-butyl ether 5.00 4.52 90.4 68.0-125
Naphthalene 5.00 3.87 77.4 54.0-135
n-Propylbenzene 5.00 4.30 86.0 77.0-124
Styrene 5.00 4.23 84.6 73.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1919995
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3834051-1 09/01/22 08:23
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,1,1,2-Tetrachloroethane 5.00 4.62 92.4 75.0-125
1,1,2,2-Tetrachloroethane 5.00 4.10 82.0 65.0-130
Tetrachloroethene 5.00 5.33 107 72.0-132
Toluene 5.00 4.54 90.8 79.0-120
1,2,3-Trichlorobenzene 5.00 4.26 85.2 50.0-138
1,2,4-Trichlorobenzene 5.00 4.08 81.6 57.0-137
1,1,1-Trichloroethane 5.00 4.75 95.0 73.0-124
1,1,2-Trichloroethane 5.00 4.64 92.8 80.0-120
Trichloroethene 5.00 4.58 91.6 78.0-124
Trichlorofluoromethane 5.00 4.63 92.6 59.0-147
1,2,3-Trichloropropane 5.00 4.40 88.0 73.0-130
1,2,4-Trimethylbenzene 5.00 4.31 86.2 76.0-121
1,3,5-Trimethylbenzene 5.00 4.24 84.8 76.0-122
Vinyl chloride 5.00 3.83 76.6 67.0-131
o-Xylene 5.00 4.38 87.6 80.0-122
m&p-Xylenes 10.0 8.90 89.0 80.0-122
(S) Toluene-d8 107 80.0-120
(S) 4-Bromofluorobenzene 103 77.0-126
(S) 1,2-Dichloroethane-d4 98.2 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1921999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-01,02,04,05
Method Blank (MB)
(MB) R3834617-3 09/06/22 12:02
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1921999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-01,02,04,05
Method Blank (MB)
(MB) R3834617-3 09/06/22 12:02
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 101 77.0-126
(S) 1,2-Dichloroethane-d4 109 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3834617-1 09/06/22 11:02 • (LCSD) R3834617-2 09/06/22 11:22
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 28.3 28.4 113 114 19.0-160 0.353 27
Acrolein 25.0 27.6 23.5 110 94.0 10.0-160 16.0 26
Acrylonitrile 25.0 22.5 23.9 90.0 95.6 55.0-149 6.03 20
Benzene 5.00 4.70 4.72 94.0 94.4 70.0-123 0.425 20
Bromobenzene 5.00 4.37 3.95 87.4 79.0 73.0-121 10.1 20
Bromodichloromethane 5.00 5.31 5.65 106 113 75.0-120 6.20 20
Bromoform 5.00 5.18 5.03 104 101 68.0-132 2.94 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1921999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-01,02,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3834617-1 09/06/22 11:02 • (LCSD) R3834617-2 09/06/22 11:22
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 5.68 6.31 114 126 10.0-160 10.5 25
n-Butylbenzene 5.00 4.65 4.89 93.0 97.8 73.0-125 5.03 20
sec-Butylbenzene 5.00 4.48 4.51 89.6 90.2 75.0-125 0.667 20
tert-Butylbenzene 5.00 4.46 4.48 89.2 89.6 76.0-124 0.447 20
Carbon tetrachloride 5.00 5.65 5.95 113 119 68.0-126 5.17 20
Chlorobenzene 5.00 4.92 5.10 98.4 102 80.0-121 3.59 20
Chlorodibromomethane 5.00 5.26 5.18 105 104 77.0-125 1.53 20
Chloroethane 5.00 4.84 5.74 96.8 115 47.0-150 17.0 20
Chloroform 5.00 5.03 5.36 101 107 73.0-120 6.35 20
Chloromethane 5.00 5.21 5.35 104 107 41.0-142 2.65 20
2-Chlorotoluene 5.00 4.43 4.25 88.6 85.0 76.0-123 4.15 20
4-Chlorotoluene 5.00 4.64 4.59 92.8 91.8 75.0-122 1.08 20
1,2-Dibromo-3-Chloropropane 5.00 4.49 4.53 89.8 90.6 58.0-134 0.887 20
1,2-Dibromoethane 5.00 4.65 4.63 93.0 92.6 80.0-122 0.431 20
Dibromomethane 5.00 5.30 5.54 106 111 80.0-120 4.43 20
1,2-Dichlorobenzene 5.00 4.53 4.89 90.6 97.8 79.0-121 7.64 20
1,3-Dichlorobenzene 5.00 4.74 4.70 94.8 94.0 79.0-120 0.847 20
1,4-Dichlorobenzene 5.00 4.47 5.14 89.4 103 79.0-120 13.9 20
Dichlorodifluoromethane 5.00 5.20 5.46 104 109 51.0-149 4.88 20
1,1-Dichloroethane 5.00 4.85 5.19 97.0 104 70.0-126 6.77 20
1,2-Dichloroethane 5.00 4.89 5.15 97.8 103 70.0-128 5.18 20
1,1-Dichloroethene 5.00 4.81 5.15 96.2 103 71.0-124 6.83 20
cis-1,2-Dichloroethene 5.00 4.94 5.02 98.8 100 73.0-120 1.61 20
trans-1,2-Dichloroethene 5.00 5.12 5.42 102 108 73.0-120 5.69 20
1,2-Dichloropropane 5.00 4.60 4.69 92.0 93.8 77.0-125 1.94 20
1,1-Dichloropropene 5.00 5.06 5.24 101 105 74.0-126 3.50 20
1,3-Dichloropropane 5.00 5.01 4.97 100 99.4 80.0-120 0.802 20
2,2-Dichloropropane 5.00 5.54 5.79 111 116 58.0-130 4.41 20
Di-isopropyl ether 5.00 5.18 5.15 104 103 58.0-138 0.581 20
Ethylbenzene 5.00 4.72 4.80 94.4 96.0 79.0-123 1.68 20
Hexachloro-1,3-butadiene 5.00 4.61 4.48 92.2 89.6 54.0-138 2.86 20
Isopropylbenzene 5.00 4.64 4.60 92.8 92.0 76.0-127 0.866 20
p-Isopropyltoluene 5.00 4.60 4.47 92.0 89.4 76.0-125 2.87 20
2-Butanone (MEK)25.0 26.2 27.4 105 110 44.0-160 4.48 20
Methylene Chloride 5.00 4.78 4.95 95.6 99.0 67.0-120 3.49 20
4-Methyl-2-pentanone (MIBK)25.0 28.0 27.1 112 108 68.0-142 3.27 20
Methyl tert-butyl ether 5.00 5.15 5.38 103 108 68.0-125 4.37 20
Naphthalene 5.00 4.01 4.22 80.2 84.4 54.0-135 5.10 20
n-Propylbenzene 5.00 4.37 3.99 87.4 79.8 77.0-124 9.09 20
Styrene 5.00 4.16 4.27 83.2 85.4 73.0-130 2.61 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1921999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1530266-01,02,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3834617-1 09/06/22 11:02 • (LCSD) R3834617-2 09/06/22 11:22
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,1,1,2-Tetrachloroethane 5.00 5.03 5.21 101 104 75.0-125 3.52 20
1,1,2,2-Tetrachloroethane 5.00 4.62 4.33 92.4 86.6 65.0-130 6.48 20
Tetrachloroethene 5.00 5.39 5.51 108 110 72.0-132 2.20 20
Toluene 5.00 4.82 5.05 96.4 101 79.0-120 4.66 20
1,2,3-Trichlorobenzene 5.00 4.58 4.78 91.6 95.6 50.0-138 4.27 20
1,2,4-Trichlorobenzene 5.00 4.75 4.60 95.0 92.0 57.0-137 3.21 20
1,1,1-Trichloroethane 5.00 5.57 5.67 111 113 73.0-124 1.78 20
1,1,2-Trichloroethane 5.00 4.94 4.63 98.8 92.6 80.0-120 6.48 20
Trichloroethene 5.00 4.88 5.10 97.6 102 78.0-124 4.41 20
Trichlorofluoromethane 5.00 5.70 6.17 114 123 59.0-147 7.92 20
1,2,3-Trichloropropane 5.00 4.15 4.20 83.0 84.0 73.0-130 1.20 20
1,2,4-Trimethylbenzene 5.00 4.16 4.48 83.2 89.6 76.0-121 7.41 20
1,3,5-Trimethylbenzene 5.00 4.31 4.23 86.2 84.6 76.0-122 1.87 20
Vinyl chloride 5.00 4.97 5.86 99.4 117 67.0-131 16.4 20
o-Xylene 5.00 4.61 4.59 92.2 91.8 80.0-122 0.435 20
m&p-Xylenes 10.0 9.45 9.23 94.5 92.3 80.0-122 2.36 20
(S) Toluene-d8 104 101 80.0-120
(S) 4-Bromofluorobenzene 107 101 77.0-126
(S) 1,2-Dichloroethane-d4 108 112 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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