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HomeMy WebLinkAboutRA-4406_26183_CA_MRP_20231006 ENVIRONMENTAL | CIVIL | GEOTECHNICAL MONITORING REPORT HARRINGTON PROPERTY 1200 BROAD STREET FUQUAY-VARINA, WAKE COUNTY, NC NCDEQ INCIDENT NO. 26183 RISK CLASSIFICATION: L060D OCTOBER 6, 2023 NCDEQ CONTRACT NO. N70522-A TASK AUTHORIZATION NO. 01 CATLIN PROJECT NO. 221196 PREPARED FOR: MS. LINDA BLALOCK NCDEQ, DWM, UST SECTION 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646 PREPARED BY: CATLIN ENGINEERS AND SCIENTISTS 220 OLD DAIRY ROAD WILMINGTON, NC 28405 (910) 452-5861 CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585 CORPORATE LICENSURE NO. FOR GEOLOGY SERVICES C-118 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 TABLE OF CONTENTS PAGE 1.0 SITE INFORMATION 1 2.0 EXECUTIVE SUMMARY 2 3.0 SCOPE OF SERVICES 2 4.0 SITE HISTORY AND CHARACTERIZATION 3 4.1 UST OWNER AND OPERATOR INFORMATION 3 4.2 UST INFORMATION 3 4.3 CONTAMINANT SOURCE INVENTORY 4 4.4 SITE CHARACTERISTICS 4 4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE 4 4.6 RECEPTOR INFORMATION 4 4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES 5 5.0 REGIONAL AND SITE GEOLOGY AND HYDROGEOLOGY 6 5.1 SOIL AND BEDROCK 6 5.2 HYDROGEOLOGY 7 6.0 SITE ASSESSMENT INFORMATION 7 6.1 GAUGING DATA 7 6.2 SAMPLING DATA 8 6.3 SUMMARY OF GROUNDWATER INFORMATION 8 6.4 EVALUATION OF ASSESSMENT INFORMATION 9 7.0 CONCLUSIONS AND RECOMMENDATIONS 10 8.0 STATEMENTS AND CERTIFICATION 11 9.0 LIMITATIONS 11 10.0 REFERENCES 12 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 TABLES TABLE 1 SITE HISTORY – UST SYSTEM AND OTHER RELEASE INFORMATION TABLE 2 PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION TABLE 3 WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA TABLE 4 SUMMARY OF GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B TABLE 5 SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B FIGURES FIGURE 1 SITE VICINITY MAP FIGURE 2 POTENTIAL RECEPTOR MAP FIGURE 3 SITE MAP FIGURE 4 GROUNDWATER ELEVATION – AUGUST 24, 2023 FIGURE 5 MONITORING WELL GROUNDWATER SAMPLE ANALYTICAL RESULTS – AUGUST 24, 2023 APPENDICES APPENDIX A HISTORICAL DATA APPENDIX B SITE PHOTOGRAPHS APPENDIX C DAILY ACTIVITIES LOG AND FIELD DATA SHEETS APPENDIX D LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 1 October 2023 1.0 SITE INFORMATION Site Identification Date: 10/06/2023 Site Risk/Priority Rank: L060D UST Number: RA-4406 Incident Number: 26183 Site Name: Harrington Property Facility ID: Not Applicable Site Location: 1200 Broad Street Nearest City/Town: Fuquay-Varina County: Wake Description of Geographical Data Point: Former UST basin Location Method: Google Earth Latitude (decimal degrees): 35.599777 Longitude (decimal degrees): -78.801167 Contacts Information Former UST Owner: Unknown Address: Unknown Phone: Unknown Former UST Operator: Unknown Address: Unknown Phone: Unknown Property Owner: Bobby and Anne B. Harrington Address: 302 Church Street, Fuquay-Varina, NC 27526 Phone: (919) 552-4645 Property Occupant: Tilley Brothers Body Shop Address: 1200 Broad Street, Fuquay-Varina, NC 27526 Phone: (919) 552-4338 Consultant: CATLIN Engineers and Scientists Address: 220 Old Dairy Rd., Wilmington, NC 28405 Phone: (910) 452-5861 Corporate Licensure No. For Engineering Services: C-0585 Corporate Geology License No.: C-118 Analytical Laboratory: Con-Test Analytical Laboratory State Certification: NC 652, NC-DW 25703 Address: 39 Spruce St., E. Longmeadow, MA 01028 Phone: (413) 525-2332 Release Information Date Discovered: 01/27/2003 Estimated Quantity of Release: Unknown Cause of Release: Leak in the UST system Source of Release: UST system or associated fitting(s) Sizes and contents of UST system(s) from which the release occurred: • One 1,000-suspected kerosene UST • One 575-gallon gasoline UST • One 610-gallon heating oil UST NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 2 October 2023 2.0 EXECUTIVE SUMMARY The Harrington Property site is located at 1200 Broad Street, Fuquay-Varina, Wake County, North Carolina. Three underground storage tanks (USTs) were previously operated at the site. One 1,000-gallon suspected kerosene UST was removed from the site in January 2003. One 575-gallon gasoline UST and one 610-gallon heating oil UST were removed from the site in May 2011. Petroleum releases were discovered during both the 2003 and 2011 tank closure activities. The purpose of this report is to document the latest site assessment and monitoring activities. On August 24, 2023, CATLIN Engineers and Scientists (CATLIN) personnel conducted groundwater monitoring activities. Depth-to-water was measured at approximately 12.7 feet deep across the site. Groundwater samples from four monitoring wells (MW-1, MW-02, MW-03, and MW-04) were collected. The samples were submitted for laboratory analysis of VOCs per Standard Method (SM) 6200B [plus ethylene dibromide (EDB), methyl tert-butyl ether (MTBE), and diisopropyl ether (DIPE)]. Laboratory results indicated the presence of multiple VOCs above their respective limits as established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section .0202 Groundwater Quality Standards (2L GWQS), but below their Gross Contaminant Levels (GCLs), in the samples from MW-1, MW-02, and MW-03. The concentrations of the detected VOCs in MW-1, MW-02, and MW-03 have increased since the March 2022 sampling event conducted by CATLIN. During the site visit, CATLIN was unable to locate water supply well WSW-1. It was noted there is no evidence of the well and that the is potential the well was destroyed when the house was previously demolished somewhere around 2013. In addition, the Harrington Property owner said indicated the parcel which previously housed WSW-1 has potential of being re-developed for town homes. Based on the lack of evidence of WSW-1 and groundwater contaminant concentrations below GCLs, CATLIN recommends the site be a candidate for No Further Action (NFA) status with a Notice of Residual Petroleum (NRP) for both soil and groundwater. In addition, the remaining tetrachloroethylene should be investigated under the Inactive Hazardous Sites Branch (IHSB) program. 3.0 SCOPE OF SERVICES The scope of services for this report was performed in general accordance with CATLIN proposal number 221196.01P, dated July 26, 2023. Services were authorized by the North Carolina Department of Environmental Quality’s (NCDEQ’s) Task Authorization (TA) #01, accepted on July 27, 2023, and Contract Number N70522-A. The approved scope of services for this Task Authorization included to: • Send out an agreement to the WSW-1 owner for abandonment; NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 3 October 2023 • Collect well dimensions for WSW-1 while on-site for sampling (if access is granted); • Collect groundwater samples from four monitoring wells (MW-1, MW-02, MW-03, and MW-04); • Analyze six water samples (four monitoring well samples, one equipment rinsate blank, and one trip blank) according to SM 6200B (including EDB, MTBE, and DIPE); and • Prepare and submit a monitoring report summarizing the findings. During the site visit, CATLIN was unable to locate water supply well WSW-1. It was noted there is no evidence of the well and that the is potential the well was destroyed when the house was previously demolished somewhere around 2013. Therefore, this well was not sampled. The remainder of the scope of services was conducted in general accordance with the approved TA. 4.0 SITE HISTORY AND CHARACTERIZATION The Harrington Property site is located at 1200 Broad Street, Fuquay-Varina, Wake County, North Carolina (Figures 1 and 2). Summarized historical sampling and gauging data are provided in Appendix A and site photographs are presented in Appendix B. 4.1 UST OWNER AND OPERATOR INFORMATION Three orphan USTs were historically operated on-site. Tank information (previous owners and operators, installation dates, etc.) is not available. Due to the possibility of impacted groundwater above regulatory limits, the site was recommended for acceptance into the North Carolina UST Section Trust Fund Branch State Lead Program (NCDENR, 2005). Available information regarding UST owners and operators is presented in Table 1. 4.2 UST INFORMATION Three USTs were previously operated at the site. One 1,000-gallon suspected kerosene UST was removed from the site in January 2003. According to the UST Tank Closure Report submitted by S&ME, Inc. (S&ME) in June 2011, two additional USTs (one 575-gallon gasoline and one 610-gallon heating oil UST) were removed from the site in May 2011. The UST Tank Closure Report included conflicting information about the tank capacities. Therefore, it is unclear what their exact sizes were (Weston, 2003; S&ME, 2011). Available UST system information is presented in Table 1 and the approximate former UST basin and dispenser locations are illustrated on Figure 3. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 4 October 2023 4.3 CONTAMINANT SOURCE INVENTORY An on-site release was discovered in 2003 during the initial 1000-gallon UST removal activities, and another release was discovered during the 2011 575-gallon and 610-gallon UST removals. Analytical results of soil samples obtained during the 2003 site activities revealed total petroleum hydrocarbons (TPH) gasoline range organics (GRO) and diesel range organics (DRO) above the State Action Levels at the time. Analytical results of soil samples obtained during the 2011 site activities detected TPH DRO above the State Action Levels (GMA, 2007; S&ME, 2011). 4.4 SITE CHARACTERISTICS The property is currently owned by Bobby and Anne Harrington and the store structure is now used as an active automobile repair and restoration shop (Tilley Brothers Body Shop). The site is no longer used for petroleum retail. The parcel is comprised of the main shop building, two additional garage buildings, a residence, two covered parking structures, a paved/gravel parking lot, and some grassy areas. Site photographs are presented in Appendix B. 4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE Properties in the site vicinity are commercial businesses and agricultural land. Commercial businesses are present to the north, east, and southeast of the subject site. Across Broad Street and to the southwest, west, and northwest of the site are agricultural lands. A retirement community lies further to the northwest, across Broad Street. 4.6 RECEPTOR INFORMATION Conducting a receptor survey was outside the scope of this monitoring event. A review of historical files available on the NCDEQ Waste Management Online Database (aka Laserfiche) indicates that the last receptor survey for the Harrington Property site was conducted in 2007 by Groundwater Management Associates (GMA). According to previous reports, municipal water is available to the site vicinity and the associated 1,500-foot radius. One inactive water supply well was identified approximately 400 feet southwest of the subject site (GMA, 2007). According to site reconnaissance conducted during this reporting period, it appears that WSW-1 no longer exists. GMA also identified a pond, reportedly located 550 feet northeast of the site (GMA, 2007). This pond is not currently evident. At the present time, CATLIN NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 5 October 2023 noted the presence of a pond on Google Earth (March 9, 2021 image) located approximately 935 feet southwest of the site. The subject site is not within a designated wellhead protection area as shown on the North Carolina Department of Environment and Natural Resources (NCDENR now NCDEQ) Public Water Supply section website. Additionally, underground utilities are present in the area. Basements were not identified in the immediate or surrounding area (GMA, 2007). Potential receptors are illustrated on Figure 2 and receptor information is shown in Table 2. 4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES As discussed in the UST Tank Closure Report prepared by Weston Solutions, Inc. (Weston) in 2003, the initial release was discovered in 2003 during the closure activities associated with the 1,000-gallon UST. Following UST removal, approximately 199 tons of petroleum impacted soil were also removed from the site. Confirmation soil sample laboratory analytical results reported concentrations of TPH DRO and GRO above their respective State Action Levels (Weston, 2003). A Phase I Limited Site Assessment (LSA) was prepared by GMA in 2007. The LSA documented the installation of one groundwater monitoring well (MW-1) near the former 1,000-gallon UST. The laboratory analytical results of the groundwater sample collected from MW-1 reported several VOC concentrations in excess of their respective 2L GWQS (GMA, 2007). On February 25, 2010, a geophysical survey was conducted at the site. The survey identified two USTs on the western portion of the property. A possible third UST was tentatively identified on the southwest corner of the building on-site, however due to subsurface utilities in the area, the presence of a UST could not be confirmed (S&ME, 2011). As discussed in the UST Tank Closure Report prepared by S&ME in 2011, two additional USTs (one gasoline and one heating oil) were removed from the site in May 2011. The third possible UST was determined to not be a tank, but rather the pedestal for an old dispensing pump (previously removed at an unknown date). The concrete pad for the pedestal was removed during the 2011 UST removal activities. Analytical results of soil samples obtained in 2011 revealed DRO above Stave Action Levels (S&ME, 2011). Records available on Laserfiche indicate that site visits and activities were conducted periodically 2007 and 2013. On January 2013, light non-aqueous phase liquid (LNAPL, aka free product) (1.58 feet thick) was observed in MW-1. An Aggressive Fluid Vapor Recovery (AFVR) event was subsequently conducted on March 12, 2013. Prior to the event, LNAPL was measured in MW-1 at a thickness of 0.46 feet. Reportedly, approximately five gallons of NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 6 October 2023 hydrocarbons (gasoline equivalent) were collected as LNAPL and 3.8 gallons were recovered in the vapor phase. LNAPL was not observed in MW-1 after the AFVR event (S&ME, 2013). CATLIN sampled monitoring well MW-1 in July 2021. Multiple VOCs were detected in the groundwater sample from MW-1 at concentrations above 2L GWQS but below GCL (CATLIN, 2021). In March 2022, CATLIN installed three shallow, Type II monitoring wells (MW-02, MW-03, and MW-04). Two soil samples were collected [MW-03 (10-12’) and MW-04 (10-12’)] from the monitoring well borings and analyzed for VOCs, semi-VOCs, volatile petroleum hydrocarbons (VPH), and extractable petroleum hydrocarbons (EPH). Laboratory analysis detected multiple VOCs in the MW-03 (10-12’) sample at concentrations greater than the soil-to- groundwater (STGW) maximum soil contaminant concentrations (MSCCs) with several concentrations above the Residential MSCCs. Later in March 2022, CATLIN collected groundwater samples from the four on-site monitoring wells. Several petroleum constituents were reported above their respective 2L GWQS in the samples from MW-1, MW-02, and MW-03. No targeted analytes were above GCL (CATLIN, 2022). Summarized available historical sampling and gauging data are presented in Appendix A. 5.0 REGIONAL AND SITE GEOLOGY AND HYDROGEOLOGY 5.1 SOIL AND BEDROCK As defined in the Geologic Map of North Carolina, published by the North Carolina Department of Natural Resources and Community Development (1985), the site lies within the Piedmont physiographic province. The site is underlain by the Middendorf Formation, within the Coastal Plain Belt. According to the 1985 Geologic Map of North Carolina, the rocks in this area consist of Cretaceous age sand and sandstones that are gray to pale-gray with an orange cast. According to GMA (2007), the site is immediately underlain by fine-to- medium grained tan sand up to 4.5 feet below land surface (BLS). From 4.5 feet to eight feet BLS, mottled red and tan, fine, sandy, silty clay was predominately observed. From approximately 8-14 feet BLS, mottled red, tan, and gray clayey fine-to-medium sand was observed. From 14-25 feet BLS, red and tan, fine-to-coarse sand was present (GMA, 2007). The boring logs generated from the March 2022 drilling activities, generally show all three borings as a combination of red-orange-brown clayey sands and sandy clays from 5-20 feet BLS with white-gray fine to coarse sands near 16 feet BLS (CATLIN, 2022). NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 7 October 2023 5.2 HYDROGEOLOGY Groundwater - The 2020 Visual Hydrogeologic Framework – North Carolina Hydrogeological Database did not identify boreholes within 10 miles of the site. Surface Water – A former receptor survey identified a pond, reportedly located 550 feet northeast of the site (GMA, 2007). This pond is not currently evident. At the present time, CATLIN noted the presence of a pond on Google Earth (March 9, 2021 image) located approximately 935 feet southwest of the site. 6.0 SITE ASSESSMENT INFORMATION CATLIN conducted field activities on August 24, 2023 in general accordance with the approved TA. Upon arrival at the site, potential hazards were evaluated before beginning field work and are documented on the Daily Activities Log. The Daily Activities Log is included in Appendix C. Photographs from the site visit are included in Appendix B. Field activities for this assessment included sampling four groundwater monitoring wells (MW-1, MW-02, MW-03, and MW-04) and searching for WSW-1, which was not able to be located. Well locations and site features are shown on Figure 3 and well construction details are presented in Table 3. 6.1 GAUGING DATA Monitoring well MW-1 was installed in 2007, and limited gauging information is available. Based on the available data, the depth to groundwater in MW-1 has varied from 11.57 feet below top of casing (BTOC) (2007) to 18.2 feet BTOC (2013). Depth to groundwater varied from 13.14 feet BTOC (MW-04) to 14.13 feet BTOC (MW-02) during the March 2022 sampling event conducted by CATLIN. Groundwater elevations and the current groundwater flow direction is depicted on Figure 4. Previously, groundwater flow direction has been calculated to be flowing to the south. During the August 2023 event, CATLIN personnel measured depth to water using an electronic water indicator probe. To prevent cross contamination, the probe and cabling were decontaminated according to manufacturer’s instructions after use in the well. Gauging data were recorded on electronic field data sheets using a tablet device. Gauging procedures were performed in general accordance with North Carolina Department of Environment and Natural Resources (NCDENR) and NCDEQ Guidelines, and Environmental Protection Agency (EPA) Region 4 Operating Procedures. Depth to water ranged from 11.95 feet BTOC (MW-04) to 13.11 feet BTOC (MW-02). LNAPL was not encountered during this event. Based on the NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 8 October 2023 gauging results, the groundwater flow direction was calculated to be toward the south. The monitoring well gauging results for the August 2023 event are presented in Table 3. The groundwater elevations and contours are presented on Figure 5 and the field data sheets are provided in Appendix C. 6.2 SAMPLING DATA Following gauging, the monitoring wells were sampled in general accordance with NCDENR and NCDEQ Guidelines, and EPA Region 4 Operating Procedures. Prior to obtaining representative groundwater samples, the monitoring wells were purged by removing a minimum of three well volumes using a new, disposable bailer. Monitoring well groundwater field parameter data were measured at one-minute intervals using an In-Situ Aqua TROLL 600 Multiparameter Sonde (Aqua TROLL). Conductivity, pH, oxidation reduction potential (ORP), dissolved oxygen, and temperature measurements were recorded utilizing the VuSitu mobile application (version 1.17.12). Groundwater parameter data were transferred from the VuSitu mobile application to the electronic field data sheets. Copies of the field data sheets are available in Appendix C. After a minimum of three well volumes were removed (or the well was bailed dry), a groundwater sample was collected from each well and poured into appropriate, laboratory-provided, pre-preserved glassware, labeled, and placed on ice in an insulated cooler. To verify that sampling equipment was decontaminated sufficiently between wells, an equipment blank sample was collected from the electronic probe. Clean distilled water was allowed to cascade down the electronic probe and into appropriate, laboratory-provided, pre-preserved glassware. The glassware was labeled and placed on ice in an insulated cooler. Additionally, a laboratory-provided trip blank was also maintained in the cooler for the duration of the sampling event. The monitoring well samples, equipment rinsate blank, and the laboratory-provided trip blank were submitted to Con-Test Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow, Massachusetts, under proper chain of custody (COC) protocol. 6.3 SUMMARY OF GROUNDWATER INFORMATION Historically, the sample from monitoring well MW-1 has contained petroleum constituent concentrations above their 2L GWQS. LNAPL has not been measured in MW-1 during multiple gauging events (S&ME, 2013; CATLIN, 2021, 2022). Available historical sampling and gauging information prepared by other consultants is included in Appendix A. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 9 October 2023 The latest groundwater sampling laboratory results for SM 6200B analysis are summarized in Table 4 and a summary of historical groundwater sampling laboratory results for events conducted by CATLIN is provided in Table 5. Monitoring well sample analytical results are illustrated on Figure 5. A copy of the complete laboratory report and COC documentation are included in Appendix D. Monitoring Wells During the August 2023 monitoring event, four monitoring well groundwater samples (MW-1, MW-02, MW-03, and MW-04) were collected and submitted for analysis via SM 6200B (including EDB, MTBE, and DIPE). No analyte concentrations were detected above their respective GCLs in the samples. Tetrachloroethylene was reported above the method detection limit in the MW-03 sample, but below the 2L GWQS. Analytical results reported the following constituents at concentrations above their 2L GWQS in the following samples: • MW-1: benzene, n-butylbenzene, sec-butylbenzene, ethylbenzene, isopropylbenzene, p-isopropyltoluene, naphthalene, n-propylbenzene, toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and total xylenes; • MW-02: tetrachloroethylene; and • MW-03: benzene, n-butylbenzene, ethylbenzene, isopropylbenzene, naphthalene, n-propylbenzene, toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and total xylenes. Tetrachloroethylene is a chlorinated solvent and is not petroleum constituent and therefore, not related to the former UST system release. Equipment Rinsate Blank and Trip Blank The equipment rinsate blank sample (EQ Rinse) and the laboratory-provided trip blank sample were submitted for analysis per SM 6200B (including EDB, MTBE, and IPE). A small concentration of toluene was detected in the EQ Rinse sample; it was significantly below the 2L GWQS. No additional target analytes were detected in either the EQ Rinse sample or the trip blank sample. 6.4 EVALUATION OF ASSESSMENT INFORMATION Extent of Contamination Multiple petroleum constituents were detected above their respective 2L GWQS in the sample from MW-1 and MW-03. A summary of monitoring well groundwater sample analytical results from the August 2023 sampling event is illustrated on Figure 5. No LNAPL was detected during the August 2023 groundwater monitoring event. The dissolved-phase contaminant plume has not been vertically or horizontally delineated. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 10 October 2023 Measurable LNAPL thickness has not been reported at this site. Dissolved-phase petroleum constituent concentrations above 2L GWQS persist in the groundwater sample obtained from MW-1 and MW-03; additionally, the concentrations detected during the August 2023 sampling event in the sample from MW-1 have generally increased since the previous sampling event (CATLIN, 2022). Cleanup Levels Achieved Soil – During the March 2022 soil boring and sampling activities associated with the monitoring well installations, soil samples were collected from the MW-03 and MW-04 borings [MW-03 (10-12’) and MW-04 (10-12’)]. The laboratory analytical results from the MW-03 (10-12’) sample indicated the presence of multiple analyte concentrations in excess of their respective STGW MSCCs; additionally, ethylbenzene, naphthalene, 1,2,4-trimethylbenzene, C5-C8 aliphatics, and C9-C22 aromatics exceeded their respective Residential MSCCs. Groundwater – Groundwater contaminant concentrations are above 2L GWQS, but below GCL at the site. LNAPL – LNAPL has not been measured at the site. 7.0 CONCLUSIONS AND RECOMMENDATIONS Conclusions Groundwater monitoring findings for this period are summarized below: • Four monitoring wells (MW-1, MW-02, MW-03, and MW-04) were sampled. • Groundwater sample analytical results from MW-1, MW-02, and MW-03 per SM 6200B plus EDB, MTBE, and DIPE revealed multiple VOCs detected above their respective 2L GWQS, but less than their respective GCL. • LNAPL was not measured at the site. • The dissolved phase contamination of petroleum constituents in the sample from MW-1 and MW-3 have generally increased since the previous sampling event. • Based on the receptor survey conducted in 2007, an inactive well was identified approximately 400 feet southwest (downgradient of the site). The parcel that contains this WSW is currently an open field with no structures and WSW-1 was not located during the recent site visit. In addition, the Harrington property owner indicated there is potential that the parcel which previously housed WSW-1 may be re-developed into Townhouses. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 11 October 2023 Recommendations Based on the lack of evidence of WSW-1 and groundwater contaminant concentrations below GCLs, CATLIN recommends the site be a candidate for NFA status with a NRP for both soil and groundwater. In addition, the remaining tetrachloroethylene should be investigated under the IHSB program. 8.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. October 6, 2023 Will this report be submitted after the established due date? NO 2 Was any required information from the above template missing from this report? YES No cross sections are provided; adequate subsurface information is not available. 3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? NA No CAP has been submitted for this site. 4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? NO 5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? NO 6 Certification: I, Sean J. O’Neil, a Licensed Engineering for CATLIN Engineers and Scientists, do certify that the information contained in this report is correct and accurate to the best of my knowledge. CATLIN Engineers and Scientists is licensed to practice engineering in North Carolina. The certification number of the company or corporation is C-0585. 9.0 LIMITATIONS The groundwater samples analyzed as part of this investigation only provide isolated data points and may not represent conditions at every location in the project area. Analyses and conclusions of this report, being based on interpolation between data points at the project area, may not be completely representative of all site conditions. Conclusions and recommendations of this investigation and report are based on the best available data in an effort to comply with current regulatory requirements. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 12 October 2023 10.0 REFERENCES CATLIN Engineers and Scientists, Monitoring Report, Harrington Property, 1200 Broad Street, Fuquay-Varina, Wake County, NC, NCDEQ Incident No. 26183, Risk Classification: L60D, August 31, 2021. CATLIN Engineers and Scientists, Monitoring Report, Harrington Property, 1200 Broad Street, Fuquay-Varina, Wake County, NC, NCDEQ Incident No. 26183, Risk Classification: L60D, April 14, 2022. Groundwater Management Associates, Inc. (GMA), Phase I Limited Site Assessment, Harrington Property, 1200 Broad Street, Fuquay-Varina, Wake County, FTF Incident #: TF-26183, May 22, 2007. Horton, J. Wright, Jr. and Victor A. Zullo, An Introduction to the Geology of the Carolinas: The Geology of the Carolinas, pp 1-11. Matthis, Jr., George C., NCDENR Letter, March 6, 2006. Narkunas, J., Groundwater Evaluation in the Central Coastal Plain of North Carolina, North Carolina Department of Natural Resources and Community Development, 1980, pp 119. NCDEQ, Division of Water Resources, 2020 Visual Hydrogeologic Framework, North Carolina Hydrogeological Database, ncwater.org/?page=350. NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Corrective Action Guidelines, January 19, 2021. NCDENR, UST Section, North Carolina Department of Environment and Natural Resources, Division of Waste Management, Guidelines for Sampling, December 1, 2013. NCDENR, DWM, UST Section, Recommendation for State Lead Cleanup, Harrington Property (Bobby), 1200 Broad Street, Fuquay-Varina, Wake County, Incident #26183, Low Risk Classification, From Bob Davies and Mickey Roberts to George Matthis, June 30, 2005. NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement, January 19, 2021. North Carolina Department of Natural Resources and Community Development, Geological Map of North Carolina, 1985. S&ME, Inc., Underground Storage Tank Closure Report, Harrington Property, 1200 Broad Street, Fuquay-Varina, Wake County, NC, NCDENR Incident No. 26183, June 9, 2011. S&ME, Inc., AFVR Event Report, TF-26183, Harrington Property, 1200 Broad Street, Fuquay-Varina, NC, May 7, 2013. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 13 October 2023 U.S. Department of Agriculture, Natural Resources Conservation Service, Web Soil Survey, https://websoilsurvey.sc.egov.usda.gov/App/WebSoilSurvey.aspx. U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Field Equipment Cleaning and Decontamination at the FEC, Striggow, B., U.S. EPA Report No. SESDPROC-206-R3, Effective Date December 18, 2015. U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Groundwater Level and Well Depth Measurement, Striggow, B., U.S. EPA Report No. SESDPROC-105-R3, Effective Date November 3, 2016. U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Groundwater Sampling, Striggow, B., U.S. EPA Report No. SESDPROC- 301-R4, Effective Date April 26, 2017. U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – In Situ Water Quality Monitoring, Chief, Field Services Branch, U.S. EPA Report No. SESDPROC-111-R4, Effective Date March 14, 2018. Weston Solutions, Inc., Underground Storage Tank Closure Report, Parcel #12, Bobby Harrington Property, 1200 Broad Street, Fuquay-Varina, Wake County, NC, February 21, 2003. Winner, M.D, Jr., and Coble, R.W., Hydrogeologic Framework of the North Carolina Coastal Plain Aquifer System: U.S. Geological Survey Open File Report 87- 690, 1989, pp 155. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 TABLES Page 1 of 1 TABLE 1 SITE HISTORY — UST SYSTEM AND OTHER RELEASE INFORMATION Incident Name and No.: Harrington Property - 26183 UST ID Number Name of Owner/ Operator Dates of Ownership Dates of Operation Last Contents Previous Contents Capacity (gal) Construction Details Tank Dimensions (inches) Installation Date Date Removed (mm/dd/yy) 1 Unknown Unknown Unknown Suspected Kerosene Suspected Kerosene 1,000 Steel 48 x 216 Unknown 01/15/03 2 Unknown Unknown Unknown Gasoline Gasoline 575*Unknown 48 x 78 Unknown 05/04/11 3 Unknown Unknown Unknown Heating Oil Heating Oil 610*Unknown 42 x 96 Unknown 05/04/11 Incident Number Material Released Date Release Discovered (mm/dd/yy) 26183 Gasoline 01/27/03 and 02/25/10 UST 1 information obtained from GMA (2007). UST 2 and UST 3 information obtained from S&ME (2011). gal = gallons Description of the Release TPH concentrations exceeding State Action Levels were discovered in soil samples in January 2003 when the 1,000- gallon UST was removed and also when the additional USTs were removed in May 2011. * - These tank sizes were quoted in the S&ME Tank Closure Report (2011) text, but differing sizes are presented on the disposal manifest and UST-3 Form in the attachments. NCDEQ; 26183_Harrington Property; T1_Site History CATLIN Project No. 221196 CATLIN Engineers and Scientists October 2023 Page 1 of 1 TABLE 2 Incident Name and No.: Harrington Property - 26183 Well ID Property Address Wake County PIN Number Owner Name (Last, First, MI) Owner Mailing Address Well Use Distance/ Direction from Source Area (ft.) Comment WSW-1 1115 Wake Chapel Rd Fuquay-Varina, NC 27526 27509 Ransdell, W.G.; Sr. Heirs; Ransdell, Philip 111 E Lakeside Dr Fuquay-Varina, NC 27526 Destroyed 400 / SW House was demolished in 2013. Receptor ID Location Contact Distance/ Direction from Source Area (ft.) Pond Southwest of Site —935 / SW Historic water supply well information obtained from GMA (2007). Surface receptor information obtained from Google Earth, 3/9/2021 image. ft. = feet Small pond Description PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION NCDEQ; 26183_Harrington Property; T2_Receptor Info CATLIN Project No. 221196 CATLIN Engineers and Scientists October 2023 Page 1 of 1 TABLE 3 WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA Incident Name and No.: Harrington Property - 26183 Well ID Date Installed (mm/dd/yy)* Date Water Level Measured (mm/dd/yy) Well Diameter (inches) Well Casing Depth (ft. BLS)* Screened Interval (x to y ft. BLS)* Bottom of Well (ft. BLS)* Top of Casing Elevation (ft.) Free-Phase Product Thickness Depth to Groundwater from Top of Casing (ft.) Groundwater Elevation (ft.)Comments 07/27/21 NMT 12.49 87.83 03/29/22 NMT 14.08 86.24 08/24/23 NMT 12.74 87.58 03/29/22 NMT 14.13 85.87 08/24/23 NMT 13.11 86.89 03/29/22 NMT 14.11 86.40 08/24/23 NMT 12.86 87.65 03/29/22 NMT 13.14 87.30 08/24/23 NMT 11.95 88.49 NMT = No Measurable Thickness 100.32 20 20 * = Data obtained from GMA (2007). ft. BLS = feet Below Land Surface 100.44 100.51 100.0020 25 10-20 10-20 10-20 5-25 10 10 10 5 2.0 2.0 2.0 2.0 03/11/22 03/11/22 03/11/22 04/12/07 MW-04 MW-03 MW-02 MW-1 NCDEQ; 26183_Harrington Property; T3_Well Construction & Gauging CATLIN Project No. 221196 CATLIN Engineers and Scientists October 2023 Page 1 of 1 TABLE 4 Incident Name and No.: Harrington Property - 26183 Date Collected (mm/dd/yy) 08/24/23 570 410 110 1,000 210 47 290 690 <1.7 ƚ 5,700 2,200 1,400 5,800 BMDL 08/24/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.38 <0.12 2.2 <0.22 <0.20 <0.15 <0.73 BMDL 08/24/23 1,100 84 28 2,000 180 12 490 560 <0.84 ƚ 1,500 3,200 990 9,400 BMDL 08/24/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.38 <0.12 0.67 <0.22 <0.20 <0.15 <0.73 BMDL 08/24/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.38 <0.12 <0.17 <0.22 <0.20 <0.15 <0.73 BMDL 08/24/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.38 <0.12 <0.17 0.50 <0.20 <0.15 <0.73 BMDL All results in micrograms per liter (µg/L). BMDL = Below Method Detection Limit (refer to analytical report for a complete list of analytes and detection limits) GCL = Gross Contaminant Level 2L GWQS = NCAC T15A:02L Groundwater Quality Standards Bold results indicate concentrations above 2L GWQS. Eq. = Equipment ƚ = The Method Detection Limit is above the 2L GWQS. SUMMARY OF GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B Contaminant of Concern Benzenen-Butylbenzene28,500 400 All Other SM 6200B AnalytesWell/ Sample ID MW-1 MW-04 MW-03 Eq. Rinse Trip Blank Ethylbenzenesec-Butylbenzene MW-02 GCL (µg/L) 2L GWQS (µg/L) 24,100 400 50,000 500 Varies Varies 8,800 70 80,000 600 260,000 600 5,000 1 5,900 70 1,3,5-TrimethylbenzeneTotal Xylenes26,100 70Isopropylbenzene (Cumene)p-Isopropyltoluene (p-Cymene)Naphthalene n-Propylbenzene30,500 70 11,700 25 6,000 6 700 0.7Tetrachloroethylene Toluene1,2,4-TrimethylbenzeneNCDEQ; 26183_Harrington Property; T4_GW Results (SM 6200B) CATLIN Project No. 221196 CATLIN Engineers and Scientists October 2023 Page 1 of 1 TABLE 5 Incident Name and No.: Harrington Property - 26183 Date Collected (mm/dd/yy) 07/27/21 63 J 68 <38 210 61 15 290 83 29 110 220 <4.0 ƚ 1,100 1,800 500 2,830 BMDL 03/29/22 98 J 59 120 260 64 <3.4 210 73 25 65 190 <3.7 ƚ 340 1,300 410 1,690 BMDL 08/24/23 <20 570 <17 410 110 <1.4 1,000 210 47 290 690 <1.7 ƚ 5,700 2,200 1,400 5,800 BMDL 03/29/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.17 <0.21 <0.11 <0.097 <0.24 <0.086 1.4 <0.22 <0.20 <0.11 <0.69 BMDL 08/24/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.22 <0.15 <0.13 <0.38 <0.12 2.2 <0.22 <0.20 <0.15 <0.73 BMDL 03/29/22 27 J 57 50 11 4.1 <0.84 130 17 0.85 J 21 32 <0.94 ƚ 140 260 63 750 BMDL 08/24/23 <10 1,100 <8.4 84 28 <0.70 2,000 180 12 490 560 <0.84 ƚ 1,500 3,200 990 9,400 BMDL 03/29/22 <2.0 <0.20 <1.6 0.96 0.97 <0.50 <0.21 0.60 1.1 2.4 <0.086 0.47 J <0.22 5.9 <0.11 0.90 J*BMDL 08/24/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.22 <0.15 <0.13 <0.38 <0.12 0.67 <0.22 <0.20 <0.15 <0.73 BMDL All results in micrograms per liter (µg/L). BMDL = Below Method Detection Limit (refer to analytical report for a complete list of analytes and detection limits) GCL = Gross Contaminant Level 2L GWQS = NCAC T15A:02L Groundwater Quality Standards Bold results indicate concentrations above 2L GWQS. ƚ = The Method Detection Limit is above the 2L GWQS. * = The value represents the sum of the reported practical quantitation limit of one analyte and the detected concentration of the other analyte. J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).TolueneMW-1 p-Isopropyltoluene (p-Cymene)Naphthalene n-PropylbenzeneSUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B Contaminant of Concern AcetoneBenzene2-Butanone (MEK)n-Butylbenzenesec-Butylbenzene ChloroformEthylbenzeneIsopropylbenzene (Cumene)1,3,5-TrimethylbenzeneTotal Xylenes1,2,4-TrimethylbenzeneAll Other SM 6200B AnalytesWell/ Sample ID Tetrachloroethylene8,800 70 70,000 70 80,000 600 GCL (µg/L) 2L GWQS (µg/L) 6,000,000 6,000 28,500 400 MW-02 24,100 400 50,000 500 Varies Varies MW-04 700 0.7 260,000 600 MW-03 30,500 70 11,700 25 6,000 6 26,100 70 5,000 1 4,000,000 4,000 5,900 70 NCDEQ; 26183_Harrington Property; T5_Historical GW CATLIN Project No. 221196 CATLIN Engineers and Scientists October 2023 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 FIGURES SITE LOCATION BROAD ST JUDD PKWYUS HWY 40Copyright:© 2013 National Geographic Society, i-cubed FIGUREPROJECTTITLE 1HARRINGTON PROPERTY1200 BROAD STREETFUQUAY-VARINA, NC SITE VICINITY MAP 2,000 0 2,000 4,0001,000 Feet INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY26183221196OCT 2023 AS SHOWN KMC/SJO ³ !(P SITE LOCATION B R O A D S T JUDD PKWY WSW-1 1 ,0 0 0 F EET RADIUS 250F E ET RADIU S POND Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community FIGUREPROJECTTITLE 2HARRINGTON PROPERTY1200 BROAD STREETFUQUAY-VARINA, NC POTENTIAL RECEPTOR MAP 500 0 500 1,000250 Feet INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY26183221196OCT 2023 AS SHOWN KMC/SJO ³ NOTE: Well locations were obtained from previous reports prepared by other consultants and are approximate. Inactive PotableWater Supply Well!(P LEGEND !(P !> !> !> !> B R O A D S T MW-1 FORMER FUEL OIL UST FORMERGASOLINEUSTFORMERDISPENSER FORMER 1,000-GAL.UST MW-02 MW-03 MW-04 Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community FIGUREPROJECTTITLE 3HARRINGTON PROPERTY1200 BROAD STREETFUQUAY-VARINA, NC SITE MAP 20 0 20 4010 Feet INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY26183221196OCT 2023 AS SHOWN KMC/SJO ³ NOTE: Well and tank locations were obtained from previous reports prepared by other consultants and are approximate. Monitoring Well (Type II)!> LEGEND Approximate Location of Former UST System Parcel Boundary !(P !> !> !> !><<B R O A D S T MW-1(87.58) MW-02(86.89) MW-03(87.65) MW-04(88.49)87.7587.508 8 .0 0 87.258 8 .2 5 87.00Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community FIGUREPROJECTTITLE 4HARRINGTON PROPERTY1200 BROAD STREETFUQUAY-VARINA, NC GROUNDWATER ELEVATION –AUGUST 24, 2023 20 0 20 4010 Feet INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY26183221196OCT 2023 AS SHOWN KMC/SJO ³ NOTES: 1. Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.2. The groundwater elevation contour interval is 0.25 feet. Gauged Monitoring Well (Type II)!> LEGEND Approximate Location of Former UST System Parcel Boundary Groundwater Elevation(Feet)(##) Groundwater Contour Groundwater Flow Direction< !(P !> !> !> !> B R O A D S T MW-1 MW-02** MW-03 MW-04 ESTIMATED HORIZONTAL EXTENT OF 2L GWQS EXCEEDANCES ?????Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community FIGUREPROJECTTITLE 5HARRINGTON PROPERTY1200 BROAD STREETFUQUAY-VARINA, NC MONITORING WELLGROUNDWATER SAMPLEANALYTICAL RESULTS –AUGUST 24, 2023 20 0 20 4010 Feet INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY26183221196OCT 2023 AS SHOWN KMC/SJO ³ NOTES: 1. Well and tank locations were obtained from previous reportsprepared by other consultants and are approximate.2. ** = Tetrachloroethylene not related to former UST system; source unknown. Sampled Monitoring Well (Type II)!> LEGEND Approximate Location of Former UST System Parcel Boundary Incident Name and No.: Harrington Property - 26183 DateCollected 08/24/23 570 410 110 1,000 210 47 290 690 <1.7 ƚ 5,700 2,200 1,400 5,80008/24/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.38 <0.12 2.2 <0.22 <0.20 <0.15 <0.7308/24/23 1,100 84 28 2,000 180 12 490 560 <0.84 ƚ 1,500 3,200 990 9,40008/24/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.38 <0.12 0.67 <0.22 <0.20 <0.15 <0.73 All results in micrograms per liter (µg/L).B old results are above 2L GWQS.Refer to Table 4 for all results and notes. MW-02 8,80070 p-Isopropyltoluene (p-Cymene)Toluene7000.7 50,000500 Well/ Sample IDMW-1 6,0006 26,10070 28,500400 24,100400GCL (µg/L)2L GWQS (µg/L) 5,0001 5,90070 30,50070 MW-04MW-03 80,000600 11,70025 260,000600 SUMMARY OF GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B Contaminant of Concern Benzenen-ButylbenzeneIsopropylbenzene (Cumene)Naphthalene n-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesTetrachloroethylenesec-Butylbenzene Ethylbenzene NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 APPENDICES NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 APPENDIX A HISTORICAL DATA APPENDIX A HISTORICAL DATA (GMA; 2007)NCDEQ; 26183_Harrington Property CATLIN Project No. 221196CATLIN Engineers and Scientists October 2023Table 4. Summary of Groundwater Sampling Analytical Results Bobby Harrington Property Fuquay-Varina, Wake County TF-26183 EPA Methods 6210D & 625 Well ID Date Collected benzene toluene ethyl benzene total xyleoes naphthalene MWl 4/13/2007 540 9000 2210 13,010 295 2L Standard (ug/L) 1 1000 550 530 21 GCL (ug/L) 5000 257,500 84,500 87,500 15,500 Surface Water Standard (ug/L) 71.4 11 524 670 102 lOX Surface Water Standard (ug/L) 714 110 5240 6700 1020 EPA Methods 6210D & 625 Well ID Date Collected 1,3,5-tri-metbyl-p-isopropyl-sec-n-propyl chloroform benzene toluene butylbenzene benzene MWl 4/13/2007 805 42 25 458 8.1 2L Standard (ug/L) 350 NSE 70 70 70 GCL (ug/L) 25,000 NSE 8500 30,000 70,000 Surface Water Standard (ug/L) 620 320 41 77.5 470 lOX Surface Water Standard (ug/L) 6200 3200 410 775 4,700 MADEP Method EPHIVP/1 Well ID Date Collected C5-C8 C9-C18 C19-C36 C9-C22 aliphatks aliphatics aliphatics aromatics MWl 4/13/2007 16.000 33.590 < 100 9590 2L Standard (ug/L) 420 4200 42,000 210 GCL (ug/L) NSE NSE NSE NSE Surface Water Standard (ug/L) NSE NSE NSE NSE lOX Surface Water Standard (ug/L) NSE NSE NSE NSE ] j isopropyl-t ,2,4-tri-methyl-benzene benzene 143 2610 70 350 25,000 28,500 310 380 3100 3800 504.1 303() C EDB lead 8.3 113 0.0004 15 50 15,000 0.8 25 8 250 Groundwater water sample MWl was collected on April 13, 2007, with the exception of the sample to be analyzed for lead, which was collected on May 3, 2007. All concentrations shown are expressed in micrograms per liter (ug/L), which is equivalent to parts per billion (ppb). GCL = gross contaminant levels NSE = no standard established EDB = ethylene dibromide 2L = groundwater standards as established under 15A NCAC 2L Bold = Concentrations above Detectable Limits Shaded = Concentrations exceed 2L groundwater standards J Monitoring Well gauging Data, AFVR Event Report, S&ME, May 7, 2013APPENDIX A HISTORICAL DATA (GMA; 2007)NCDEQ; 26183_Harrington Property CATLIN Project No. 221196CATLIN Engineers and Scientists October 2023WeHID Date Installed I ~ MW-1 4/12/2007 Notes: Table 1 Well Construction Details and Depth to Water and Product Harrington Property Well Casing Depth ;•,', (ft. bgs.) . -0.0-5.0 1200 North Broad Street Fuquay Varina, Wake County, North Carolina NCDENR Incident No. 26183 S&ME Project No. 1054-11-3054A Screen Total Depth Date Interval (ft. bgs.) Measured •. ' :(~. bgs.) 4/12/2007 5.0-25.0 25 1/11/2013 3/12/2012* 3/12/2013** Deptb.t() Product· (ft. BTOC) --16.62 15.52 --. -~ ··ncwth to Free Product Water Thickness . . . {ft._BTOe, (ft.) 11.57 --18.2 1.58 15.98 0.46 16.64 --Monitor well construction details obtained from the Phase I Limited Site Assessment performed by Groundwater Management Associates, Inc. on May 22, 2007. ft. bgs.: feet below ground surface ft. BTOC: feet below top of casing *: measured prior to the AFVR **: measured post AFVR ·. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 APPENDIX B SITE PHOTOGRAPHS APPENDIX B SITE PHOTOGRAPHS – AUGUST 24, 2023 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 View of the site, facing north. View of MW-1, facing northeast. APPENDIX B SITE PHOTOGRAPHS – AUGUST 24, 2023 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 View of MW-02, facing North. View of MW-03, facing east. APPENDIX B SITE PHOTOGRAPHS – AUGUST 24, 2023 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 View of MW-04, facing southeast. View of Assumed previous location of WSW-1. APPENDIX B SITE PHOTOGRAPHS – AUGUST 24, 2023 NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 View of property from the front facing west. NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 APPENDIX C DAILY ACTIVITIES LOG AND FIELD DATA SHEETS Page_of _ _d;~CATLIN DAILY ACTIVITIES LOG Engineers and Scientists CATLIN DAY: r'4,v'fe/!,tc.u DATE: r/z,1/./ -'2.. J' PROJECT: Harrington Property WEATHER: ;r'o,(' S/• IA •-v V . CATLIN PROJECT#: 221196 REPORT BY: CLIENT'S NAME: NCDEQ-SLP CATLIN A/~ ---- SUBCONTRACTORS: CREW: TIME ACTIVITY START END START STOP VEHICLE#: ODOMETER: ODOMETER: >< a:, "~ /,; U>,',11/;d-V ,_ ,,,_ tl6 ~· tJ. ~ C.'u "w#' UJIC,,.A,_J.., ,;>· ~ • ~« -.l---,/'~( '-'tl-t; ~(JO C&3, ().,.,. f1r /IA4Q V • ., l~t,C) 'Z-tf5 :XU,,, oiodl --n,A / < 1-lf, etJ.lts/aJJ5 Z.lrS 1-t,J~ IAt>k~J w 1. ,i,,, , J ~ ..fi,».; k LJ,-cf;.,.,.,~~ t' -.t ~ --IS IAJt;tj-f ~ IIP-r ~~~~+--f6.L--,.J-.<cdl ~-t-fo v.J t,,,/J-.-It,~~ - ~'i iP~l:i<'k.J tA ,.,., Zol~. L/i 111/ I~ ~e..( M i/te> -/ )An ,-J/ ,.,,d) ~ l\.a. J. 4.i-l(l \\,, \1. ~,,.._ +o , ·-1A·-.vl o st Oef /J~~ nJ.-~j?,,G (,41 ,. \~\J, 1£/t Jo F,'11,t:lt cal:.1 J.foo s.,,,,41,s 111 /o/,. b/"1K-+o " l+1ce,,. ~ 1-..!--L ~ -. . , 0 START END VEHICLE#: ODOMETER: ODOMETER: EQUIPMENT USED EQUIPMENT USED EQUIPMENT USED OTHER EQUIP. USED D.O. Meter YSI GPS Unit Generator Redi-Flo Pump Bailers Slug Test Equipment Geopump Sampling Supplies pH/Temp. Meter Conductivity Pen Tubing PID/FID Meter Water Level Indicator PPE Level C or D Approval of data for final report can only be made by CATLIN Engineers and Scientists and cannot be conveyed on this form. This is a field copy and is subject to review and revision. CATLIN PROJECT:SAMPLED BY: CATLIN PROJECT # :DATE SAMPLED: CLIENT'S NAME: MW-1 12.26 12.74 2.001 NMT 6.002 25 10.004 2 Method:Bailer Purge Start Time:11:13 Required Bails for 3 Well Volumes:26 Purge Stop Time:11:23 Required Bails for 5 Well Volumes:42 Was Well Purged Dry?No Number of Bails Removed:21 Sample Time:11:23 Groundwater Removed (gal):5.0 Equipment Used: Time pH (Standard Units) ORP (mV) Specific Cond. (µS/cm) Dissolved Oxygen (mg/L) Temperature (Co) 11:13 55.51 3.11 6.04 247.02 53.53 11:14 78.95 1.90 5.69 232.44 53.67 11:15 78.26 1.78 5.69 201.55 53.70 11:16 77.32 1.61 5.73 174.90 53.66 11:17 76.88 1.58 5.73 157.80 53.63 11:18 76.79 1.43 5.74 147.32 53.71 11:19 75.97 1.38 5.72 142.40 53.57 11:20 76.14 1.36 5.72 140.48 53.50 11:21 76.15 1.35 5.72 140.20 53.52 11:22 76.40 1.39 5.70 141.00 53.57 Laboratory:Con-Test Analysis: Well Data Well ID Depth to Product (ft below TOC) Total Well Depth (ft) Purging Information Information Volume of Groundwater in Well Well Diameter (inches) GROUNDWATER SAMPLING FORM Water Column (ft below TOC) One Well Volume (gal) Three Well Volumes (gal) Five Well Volumes (gal) 6200B Laboratory Analysis Information Geochemical Parameters Depth to Water (ft below TOC) Moderate turbidity; light brown. Sheen present. Aqua Troll 600 Turbidity and Additional Sampling Notes NCDEQ-SLP, Linda Blalock Monitoring Well Information Nate Newman 8/24/2023 Harrington Property 221196.01 CATLIN PROJECT:SAMPLED BY: CATLIN PROJECT # :DATE SAMPLED: CLIENT'S NAME: MW-02 6.89 13.11 1.124 NMT 3.373 20 5.622 2 Method:Bailer Purge Start Time:11:49 Required Bails for 3 Well Volumes:15 Purge Stop Time:11:57 Required Bails for 5 Well Volumes:24 Was Well Purged Dry?No Number of Bails Removed:21 Sample Time:11:57 Groundwater Removed (gal):5.0 Equipment Used: Time pH (Standard Units) ORP (mV) Specific Cond. (µS/cm) Dissolved Oxygen (mg/L) Temperature (Co) 11:49 58.19 2.85 4.94 173.50 55.05 11:50 59.23 2.33 4.83 197.95 54.99 11:51 61.59 2.40 4.81 211.89 55.03 11:52 64.08 2.48 4.78 220.74 55.05 11:53 67.03 2.53 4.74 230.74 55.03 11:54 66.84 2.53 4.76 232.90 55.15 11:55 67.50 2.52 4.75 238.29 55.12 Laboratory:Con-Test Analysis:6200B Depth to Product (ft below TOC)Three Well Volumes (gal) Total Well Depth (ft)Five Well Volumes (gal) Well Diameter (inches) Purging Information Information Geochemical Parameters Aqua Troll 600 Turbidity and Additional Sampling Notes Moderate turbidity; light brown. Laboratory Analysis Information Depth to Water (ft below TOC)One Well Volume (gal) GROUNDWATER SAMPLING FORM Harrington Property Nate Newman 221196.01 8/24/2023 NCDEQ-SLP, Linda Blalock Monitoring Well Information Well Data Volume of Groundwater in Well Well ID Water Column (ft below TOC) CATLIN PROJECT:SAMPLED BY: CATLIN PROJECT # :DATE SAMPLED: CLIENT'S NAME: MW-03 7.14 12.86 1.165 NMT 3.496 20 5.826 2 Method:Bailer Purge Start Time:11:33 Required Bails for 3 Well Volumes:15 Purge Stop Time:11:40 Required Bails for 5 Well Volumes:25 Was Well Purged Dry?No Number of Bails Removed:21 Sample Time:11:40 Groundwater Removed (gal):5.0 Equipment Used: Time pH (Standard Units) ORP (mV) Specific Cond. (µS/cm) Dissolved Oxygen (mg/L) Temperature (Co) 11:34 231.34 1.45 6.38 170.91 54.42 11:35 225.98 1.43 6.40 152.36 54.42 11:36 220.16 1.54 6.41 130.17 54.39 11:37 210.26 1.62 6.40 109.75 54.36 11:38 205.59 1.66 6.40 94.48 54.39 Laboratory:Con-Test Analysis:6200B Depth to Product (ft below TOC)Three Well Volumes (gal) Total Well Depth (ft)Five Well Volumes (gal) Well Diameter (inches) Purging Information Information Geochemical Parameters Aqua Troll 600 Turbidity and Additional Sampling Notes Moderate turbidity; light brown. Laboratory Analysis Information Depth to Water (ft below TOC)One Well Volume (gal) GROUNDWATER SAMPLING FORM Harrington Property Nate Newman 221196.01 8/24/2023 NCDEQ-SLP, Linda Blalock Monitoring Well Information Well Data Volume of Groundwater in Well Well ID Water Column (ft below TOC) CATLIN PROJECT:SAMPLED BY: CATLIN PROJECT # :DATE SAMPLED: CLIENT'S NAME: MW-4 8.05 11.95 1.314 NMT 3.941 20 6.569 2 Method:Bailer Purge Start Time:10:59 Required Bails for 3 Well Volumes:17 Purge Stop Time:11:06 Required Bails for 5 Well Volumes:28 Was Well Purged Dry?No Number of Bails Removed:21 Sample Time:11:06 Groundwater Removed (gal):5.0 Equipment Used: Time pH (Standard Units) ORP (mV) Specific Cond. (µS/cm) Dissolved Oxygen (mg/L) Temperature (Co) 11:00 60.75 1.94 4.61 297.96 53.26 11:01 70.20 2.00 4.59 301.72 52.98 11:02 71.73 2.06 4.57 305.57 52.95 11:03 70.47 2.05 4.56 307.15 53.06 11:04 65.20 2.06 4.56 309.08 53.13 11:05 64.88 2.04 4.56 310.19 53.29 Laboratory:Con-Test Analysis:6200B Depth to Product (ft below TOC)Three Well Volumes (gal) Total Well Depth (ft)Five Well Volumes (gal) Well Diameter (inches) Purging Information Information Geochemical Parameters Aqua Troll 600 Turbidity and Additional Sampling Notes Moderate turbidity; light brown. Laboratory Analysis Information Depth to Water (ft below TOC)One Well Volume (gal) GROUNDWATER SAMPLING FORM Harrington Property Nate Newman 221196.01 8/24/2023 NCDEQ-SLP, Linda Blalock Monitoring Well Information Well Data Volume of Groundwater in Well Well ID Water Column (ft below TOC) NCDEQ; 26183_Harrington Property CATLIN Engineers and Scientists CATLIN Project No. 221196 October 2023 APPENDIX D LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 October 3, 2023 Sean O’Neil CATLIN Engineers & Scientists 1044 Washington Street Raleigh, NC 27605 Project Location: Fuquay- Varina, NC Client Job Number: Project Number: 221196 Laboratory Work Order Number: 23H3799 Enclosed are results of analyses for samples as received by the laboratory on August 25, 2023. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kaitlyn A. Feliciano Project Manager Table of Contents Sample Summary 3 Hits Only Report 4 Case Narrative 6 Sample Results 7 23H3799-01 7 23H3799-02 9 23H3799-03 11 23H3799-04 13 23H3799-05 15 23H3799-06 17 Sample Preparation Information 19 QC Data 20 Volatile Organic Compounds by GC/MS 20 B350423 20 B350532 24 Flag/Qualifier Summary 25 Certifications 26 Chain of Custody/Sample Receipt 28 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL SUMMARY 10/3/2023 CATLIN Engineers & Scientists 1044 Washington Street Raleigh, NC 27605 ATTN: Sean O’Neil 221196 23H3799 The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. PROJECT LOCATION: PURCHASE ORDER NUMBER: PROJECT NUMBER: REPORT DATE: WORK ORDER NUMBER: FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB Fuquay- Varina, NC 230824-2 Eq. Rinse 23H3799-01 Water - SM21-23 6200B MW-1 23H3799-02 Ground Water SM21-23 6200B MW-02 23H3799-03 Ground Water SM21-23 6200B MW-03 23H3799-04 Ground Water SM21-23 6200B MW-04 23H3799-05 Ground Water SM21-23 6200B Trip Blank 23H3799-06 Trip Blank Water SM21-23 6200B [TOC_1]Sample Summary[TOC] 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 [TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY Client ID:Lab ID:23H3799-06Trip Blank No Results Detected Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary section of this report. Users must review this report in its entirety to determine data usability and assessment. 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 EXECUTIVE SUMMARY Client ID:Lab ID: Analyte Results/Qual RL Units Method 23H3799-01Eq. Rinse DL Toluene 0.50 0.50 g/L SM21-23 6200B0.22 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23H3799-02MW-1 DL 1,2,4-Trimethylbenzene 2200 250 g/L SM21-23 6200B99 1,3,5-Trimethylbenzene 1400 5.0 g/L SM21-23 6200B1.5 Benzene 570 5.0 g/L SM21-23 6200B1.8 Ethylbenzene 1000 5.0 g/L SM21-23 6200B2.2 Isopropylbenzene (Cumene)210 5.0 g/L SM21-23 6200B1.5 m+p Xylene 4100 500 g/L SM21-23 6200B250 Naphthalene 290 5.0 g/L SM21-23 6200B3.8 n-Butylbenzene 410 5.0 g/L SM21-23 6200B1.5 n-Propylbenzene 690 5.0 g/L SM21-23 6200B1.2 o-Xylene 1700 250 g/L SM21-23 6200B120 p-Isopropyltoluene (p-Cymene)47 5.0 g/L SM21-23 6200B1.3 sec-Butylbenzene 110 5.0 g/L SM21-23 6200B1.3 Toluene 5700 250 g/L SM21-23 6200B110 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23H3799-03MW-02 DL Tetrachloroethylene 2.2 0.50 g/L SM21-23 6200B0.17 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23H3799-04MW-03 DL 1,2,4-Trimethylbenzene 3200 120 g/L SM21-23 6200B50 1,3,5-Trimethylbenzene 990 2.5 g/L SM21-23 6200B0.75 Benzene 1100 120 g/L SM21-23 6200B46 Ethylbenzene 2000 120 g/L SM21-23 6200B55 Isopropylbenzene (Cumene)180 2.5 g/L SM21-23 6200B0.76 m+p Xylene 7400 250 g/L SM21-23 6200B120 Naphthalene 490 2.5 g/L SM21-23 6200B1.9 n-Butylbenzene 84 2.5 g/L SM21-23 6200B0.75 n-Propylbenzene 560 2.5 g/L SM21-23 6200B0.62 o-Xylene 2000 120 g/L SM21-23 6200B61 p-Isopropyltoluene (p-Cymene)12 2.5 g/L SM21-23 6200B0.63 sec-Butylbenzene 28 2.5 g/L SM21-23 6200B0.63 Toluene 1500 120 g/L SM21-23 6200B56 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23H3799-05MW-04 DL Tetrachloroethylene 0.67 0.50 g/L SM21-23 6200B0.17 Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary section of this report. Users must review this report in its entirety to determine data usability and assessment. 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method 6200B, elevated reporting limits for sample(s) 23H3799-02,-04 due to a high concentration of target compounds. REVISED 10-03-23: The results for ethylbenzene have been updated with the correct value. [TOC_1]Case Narrative[TOC] SM21-23 6200B Qualifications: Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: RL-11 23H3799-02[MW-1], 23H3799-04[MW-03] The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Technical Representative 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-01 Field Sample #: Eq. Rinse Sample Matrix: Water Sampled: 8/24/2023 10:45 [TOC_2]23H3799-01[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 8/29/23 11:29 MFFg/L2.0 8/29/23SM21-23 6200B1Acetone ND 0.50 8/29/23 11:29 MFFg/L0.18 8/29/23SM21-23 6200B1Benzene ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B1Bromobenzene ND 1.0 8/29/23 11:29 MFFg/L0.28 8/29/23SM21-23 6200B1Bromochloromethane ND 0.50 8/29/23 11:29 MFFg/L0.16 8/29/23SM21-23 6200B1Bromodichloromethane ND 1.0 8/29/23 11:29 MFFg/L0.41 8/29/23SM21-23 6200B1Bromoform ND 2.0 8/29/23 11:29 MFFg/L1.3 8/29/23SM21-23 6200B1Bromomethane ND 5.0 8/29/23 11:29 MFFg/L1.7 8/29/23SM21-23 6200B12-Butanone (MEK) ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B1n-Butylbenzene ND 0.50 8/29/23 11:29 MFFg/L0.13 8/29/23SM21-23 6200B1sec-Butylbenzene ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B1tert-Butylbenzene ND 0.50 8/29/23 11:29 MFFg/L0.16 8/29/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 8/29/23 11:29 MFFg/L0.12 8/29/23SM21-23 6200B1Chlorobenzene ND 50 8/29/23 11:29 MFFg/L20 8/29/23SM21-23 6200B1Ethanol ND 0.50 8/29/23 11:29 MFFg/L0.20 8/29/23SM21-23 6200B1Chlorodibromomethane ND 0.50 8/29/23 11:29 MFFg/L0.34 8/29/23SM21-23 6200B1Chloroethane ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B1Chloroform ND 0.60 8/29/23 11:29 MFFg/L0.50 8/29/23SM21-23 6200B1Chloromethane ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B12-Chlorotoluene ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B14-Chlorotoluene ND 0.50 8/29/23 11:29 MFFg/L0.16 8/29/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 8/29/23 11:29 MFFg/L0.13 8/29/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 8/29/23 11:29 MFFg/L0.13 8/29/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 8/29/23 11:29 MFFg/L0.16 8/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethane ND 0.50 8/29/23 11:29 MFFg/L0.30 8/29/23SM21-23 6200B11,2-Dichloroethane ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 8/29/23 11:29 MFFg/L0.17 8/29/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 8/29/23 11:29 MFFg/L0.19 8/29/23SM21-23 6200B11,2-Dichloropropane ND 0.50 8/29/23 11:29 MFFg/L0.12 8/29/23SM21-23 6200B11,3-Dichloropropane ND 0.50 8/29/23 11:29 MFFg/L0.35 8/29/23SM21-23 6200B12,2-Dichloropropane ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B11,1-Dichloropropene ND 0.50 8/29/23 11:29 MFFg/L0.16 8/29/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 8/29/23 11:29 MFFg/L0.20 8/29/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 8/29/23 11:29 MFFg/L0.22 8/29/23SM21-23 6200B1Ethylbenzene ND 5.0 8/29/23 11:29 MFFg/L1.2 8/29/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 8/29/23 11:29 MFFg/L0.13 8/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 8/29/23 11:29 MFFg/L0.17 8/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 8/29/23 11:29 MFFg/L0.18 8/29/23SM21-23 6200B1Methylene Chloride ND 5.0 8/29/23 11:29 MFFg/L1.3 8/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) [TOC_1]Sample Results[TOC] 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-01 Field Sample #: Eq. Rinse Sample Matrix: Water Sampled: 8/24/2023 10:45 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 8/29/23 11:29 MFFg/L0.38 8/29/23SM21-23 6200B1Naphthalene ND 0.50 8/29/23 11:29 MFFg/L0.12 8/29/23SM21-23 6200B1n-Propylbenzene ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B1Styrene ND 0.50 8/29/23 11:29 MFFg/L0.14 8/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 8/29/23 11:29 MFFg/L0.17 8/29/23SM21-23 6200B1Tetrachloroethylene 0.50 0.50 8/29/23 11:29 MFFg/L0.22 8/29/23SM21-23 6200B1Toluene ND 1.0 8/29/23 11:29 MFFg/L0.34 8/29/23SM21-23 6200B11,2,3-Trichlorobenzene ND 0.50 8/29/23 11:29 MFFg/L0.30 8/29/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 8/29/23 11:29 MFFg/L0.19 8/29/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 8/29/23 11:29 MFFg/L0.17 8/29/23SM21-23 6200B1Trichloroethylene ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 1.0 8/29/23 11:29 MFFg/L0.28 8/29/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 8/29/23 11:29 MFFg/L0.20 8/29/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 8/29/23 11:29 MFFg/L0.15 8/29/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 8/29/23 11:29 MFFg/L1.7 8/29/23SM21-23 6200B1Vinyl Acetate ND 0.50 8/29/23 11:29 MFFg/L0.24 8/29/23SM21-23 6200B1Vinyl Chloride ND 1.0 8/29/23 11:29 MFFg/L0.49 8/29/23SM21-23 6200B1m+p Xylene ND 0.50 8/29/23 11:29 MFFg/L0.24 8/29/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 92.0 8/29/23 11:2970-130 Toluene-d8 99.5 8/29/23 11:2970-130 4-Bromofluorobenzene 102 8/29/23 11:2970-130 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-02 Field Sample #: MW-1 Sample Matrix: Ground Water Sampled: 8/24/2023 11:23 [TOC_2]23H3799-02[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS ND 500 8/29/23 19:18 MFFg/L20 8/29/23SM21-23 6200B10Acetone 570 5.0 8/29/23 19:18 MFFg/L1.8 8/29/23SM21-23 6200B10Benzene ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B10Bromobenzene ND 10 8/29/23 19:18 MFFg/L2.8 8/29/23SM21-23 6200B10Bromochloromethane ND 5.0 8/29/23 19:18 MFFg/L1.6 8/29/23SM21-23 6200B10Bromodichloromethane ND 10 8/29/23 19:18 MFFg/L4.1 8/29/23SM21-23 6200B10Bromoform ND 20 8/29/23 19:18 MFFg/L13 8/29/23SM21-23 6200B10Bromomethane ND 50 8/29/23 19:18 MFFg/L17 8/29/23SM21-23 6200B102-Butanone (MEK) 410 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B10n-Butylbenzene 110 5.0 8/29/23 19:18 MFFg/L1.3 8/29/23SM21-23 6200B10sec-Butylbenzene ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B10tert-Butylbenzene ND 5.0 8/29/23 19:18 MFFg/L1.6 8/29/23SM21-23 6200B10Carbon Tetrachloride ND 5.0 8/29/23 19:18 MFFg/L1.2 8/29/23SM21-23 6200B10Chlorobenzene ND 500 8/29/23 19:18 MFFg/L200 8/29/23SM21-23 6200B10Ethanol ND 5.0 8/29/23 19:18 MFFg/L2.0 8/29/23SM21-23 6200B10Chlorodibromomethane ND 5.0 8/29/23 19:18 MFFg/L3.4 8/29/23SM21-23 6200B10Chloroethane ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B10Chloroform ND 6.0 8/29/23 19:18 MFFg/L5.0 8/29/23SM21-23 6200B10Chloromethane ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B102-Chlorotoluene ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B104-Chlorotoluene ND 5.0 8/29/23 19:18 MFFg/L1.6 8/29/23SM21-23 6200B101,2-Dibromoethane (EDB) ND 5.0 8/29/23 19:18 MFFg/L1.3 8/29/23SM21-23 6200B101,2-Dichlorobenzene ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B101,3-Dichlorobenzene ND 5.0 8/29/23 19:18 MFFg/L1.3 8/29/23SM21-23 6200B101,4-Dichlorobenzene ND 5.0 8/29/23 19:18 MFFg/L1.6 8/29/23SM21-23 6200B10Dichlorodifluoromethane (Freon 12) ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B101,1-Dichloroethane ND 5.0 8/29/23 19:18 MFFg/L3.0 8/29/23SM21-23 6200B101,2-Dichloroethane ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B101,1-Dichloroethylene ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B10cis-1,2-Dichloroethylene ND 5.0 8/29/23 19:18 MFFg/L1.7 8/29/23SM21-23 6200B10trans-1,2-Dichloroethylene ND 5.0 8/29/23 19:18 MFFg/L1.9 8/29/23SM21-23 6200B101,2-Dichloropropane ND 5.0 8/29/23 19:18 MFFg/L1.2 8/29/23SM21-23 6200B101,3-Dichloropropane ND 5.0 8/29/23 19:18 MFFg/L3.5 8/29/23SM21-23 6200B102,2-Dichloropropane ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B101,1-Dichloropropene ND 5.0 8/29/23 19:18 MFFg/L1.6 8/29/23SM21-23 6200B10cis-1,3-Dichloropropene ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B10trans-1,3-Dichloropropene ND 5.0 8/29/23 19:18 MFFg/L2.0 8/29/23SM21-23 6200B10Diisopropyl Ether (DIPE) 1000 5.0 8/29/23 19:18 MFFg/L2.2 8/29/23SM21-23 6200B10Ethylbenzene ND 50 8/29/23 19:18 MFFg/L12 8/29/23SM21-23 6200B102-Hexanone (MBK) 210 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B10Isopropylbenzene (Cumene) 47 5.0 8/29/23 19:18 MFFg/L1.3 8/29/23SM21-23 6200B10p-Isopropyltoluene (p-Cymene) ND 5.0 8/29/23 19:18 MFFg/L1.7 8/29/23SM21-23 6200B10Methyl tert-Butyl Ether (MTBE) ND 50 8/29/23 19:18 MFFg/L1.8 8/29/23SM21-23 6200B10Methylene Chloride ND 50 8/29/23 19:18 MFFg/L13 8/29/23SM21-23 6200B104-Methyl-2-pentanone (MIBK) 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-02 Field Sample #: MW-1 Sample Matrix: Ground Water Sampled: 8/24/2023 11:23 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 290 5.0 8/29/23 19:18 MFFg/L3.8 8/29/23SM21-23 6200B10Naphthalene 690 5.0 8/29/23 19:18 MFFg/L1.2 8/29/23SM21-23 6200B10n-Propylbenzene ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B10Styrene ND 5.0 8/29/23 19:18 MFFg/L1.4 8/29/23SM21-23 6200B101,1,2,2-Tetrachloroethane ND 5.0 8/29/23 19:18 MFFg/L1.7 8/29/23SM21-23 6200B10Tetrachloroethylene 5700 250 8/31/23 18:33 LBDg/L110 8/30/23SM21-23 6200B500Toluene ND 10 8/29/23 19:18 MFFg/L3.4 8/29/23SM21-23 6200B101,2,3-Trichlorobenzene ND 5.0 8/29/23 19:18 MFFg/L3.0 8/29/23SM21-23 6200B101,2,4-Trichlorobenzene ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B101,1,1-Trichloroethane ND 5.0 8/29/23 19:18 MFFg/L1.9 8/29/23SM21-23 6200B101,1,2-Trichloroethane ND 5.0 8/29/23 19:18 MFFg/L1.7 8/29/23SM21-23 6200B10Trichloroethylene ND 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B10Trichlorofluoromethane (Freon 11) ND 10 8/29/23 19:18 MFFg/L2.8 8/29/23SM21-23 6200B101,2,3-Trichloropropane 2200 250 8/31/23 18:33 LBDg/L99 8/30/23SM21-23 6200B5001,2,4-Trimethylbenzene 1400 5.0 8/29/23 19:18 MFFg/L1.5 8/29/23SM21-23 6200B101,3,5-Trimethylbenzene ND 200 8/29/23 19:18 MFFg/L17 8/29/23SM21-23 6200B10Vinyl Acetate ND 5.0 8/29/23 19:18 MFFg/L2.4 8/29/23SM21-23 6200B10Vinyl Chloride 4100 500 8/31/23 18:33 LBDg/L250 8/30/23SM21-23 6200B500m+p Xylene 1700 250 8/31/23 18:33 LBDg/L120 8/30/23SM21-23 6200B500o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 90.9 8/29/23 19:1870-130 1,2-Dichloroethane-d4 92.3 8/31/23 18:3370-130 Toluene-d8 97.4 8/29/23 19:1870-130 Toluene-d8 100 8/31/23 18:3370-130 4-Bromofluorobenzene 106 8/29/23 19:1870-130 4-Bromofluorobenzene 101 8/31/23 18:3370-130 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-03 Field Sample #: MW-02 Sample Matrix: Ground Water Sampled: 8/24/2023 11:57 [TOC_2]23H3799-03[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 8/29/23 18:25 MFFg/L2.0 8/29/23SM21-23 6200B1Acetone ND 0.50 8/29/23 18:25 MFFg/L0.18 8/29/23SM21-23 6200B1Benzene ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B1Bromobenzene ND 1.0 8/29/23 18:25 MFFg/L0.28 8/29/23SM21-23 6200B1Bromochloromethane ND 0.50 8/29/23 18:25 MFFg/L0.16 8/29/23SM21-23 6200B1Bromodichloromethane ND 1.0 8/29/23 18:25 MFFg/L0.41 8/29/23SM21-23 6200B1Bromoform ND 2.0 8/29/23 18:25 MFFg/L1.3 8/29/23SM21-23 6200B1Bromomethane ND 5.0 8/29/23 18:25 MFFg/L1.7 8/29/23SM21-23 6200B12-Butanone (MEK) ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B1n-Butylbenzene ND 0.50 8/29/23 18:25 MFFg/L0.13 8/29/23SM21-23 6200B1sec-Butylbenzene ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B1tert-Butylbenzene ND 0.50 8/29/23 18:25 MFFg/L0.16 8/29/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 8/29/23 18:25 MFFg/L0.12 8/29/23SM21-23 6200B1Chlorobenzene ND 50 8/29/23 18:25 MFFg/L20 8/29/23SM21-23 6200B1Ethanol ND 0.50 8/29/23 18:25 MFFg/L0.20 8/29/23SM21-23 6200B1Chlorodibromomethane ND 0.50 8/29/23 18:25 MFFg/L0.34 8/29/23SM21-23 6200B1Chloroethane ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B1Chloroform ND 0.60 8/29/23 18:25 MFFg/L0.50 8/29/23SM21-23 6200B1Chloromethane ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B12-Chlorotoluene ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B14-Chlorotoluene ND 0.50 8/29/23 18:25 MFFg/L0.16 8/29/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 8/29/23 18:25 MFFg/L0.13 8/29/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 8/29/23 18:25 MFFg/L0.13 8/29/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 8/29/23 18:25 MFFg/L0.16 8/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethane ND 0.50 8/29/23 18:25 MFFg/L0.30 8/29/23SM21-23 6200B11,2-Dichloroethane ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 8/29/23 18:25 MFFg/L0.17 8/29/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 8/29/23 18:25 MFFg/L0.19 8/29/23SM21-23 6200B11,2-Dichloropropane ND 0.50 8/29/23 18:25 MFFg/L0.12 8/29/23SM21-23 6200B11,3-Dichloropropane ND 0.50 8/29/23 18:25 MFFg/L0.35 8/29/23SM21-23 6200B12,2-Dichloropropane ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B11,1-Dichloropropene ND 0.50 8/29/23 18:25 MFFg/L0.16 8/29/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 8/29/23 18:25 MFFg/L0.20 8/29/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 8/29/23 18:25 MFFg/L0.22 8/29/23SM21-23 6200B1Ethylbenzene ND 5.0 8/29/23 18:25 MFFg/L1.2 8/29/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 8/29/23 18:25 MFFg/L0.13 8/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 8/29/23 18:25 MFFg/L0.17 8/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 8/29/23 18:25 MFFg/L0.18 8/29/23SM21-23 6200B1Methylene Chloride ND 5.0 8/29/23 18:25 MFFg/L1.3 8/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-03 Field Sample #: MW-02 Sample Matrix: Ground Water Sampled: 8/24/2023 11:57 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 8/29/23 18:25 MFFg/L0.38 8/29/23SM21-23 6200B1Naphthalene ND 0.50 8/29/23 18:25 MFFg/L0.12 8/29/23SM21-23 6200B1n-Propylbenzene ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B1Styrene ND 0.50 8/29/23 18:25 MFFg/L0.14 8/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane 2.2 0.50 8/29/23 18:25 MFFg/L0.17 8/29/23SM21-23 6200B1Tetrachloroethylene ND 0.50 8/29/23 18:25 MFFg/L0.22 8/29/23SM21-23 6200B1Toluene ND 1.0 8/29/23 18:25 MFFg/L0.34 8/29/23SM21-23 6200B11,2,3-Trichlorobenzene ND 0.50 8/29/23 18:25 MFFg/L0.30 8/29/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 8/29/23 18:25 MFFg/L0.19 8/29/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 8/29/23 18:25 MFFg/L0.17 8/29/23SM21-23 6200B1Trichloroethylene ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 1.0 8/29/23 18:25 MFFg/L0.28 8/29/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 8/29/23 18:25 MFFg/L0.20 8/29/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 8/29/23 18:25 MFFg/L0.15 8/29/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 8/29/23 18:25 MFFg/L1.7 8/29/23SM21-23 6200B1Vinyl Acetate ND 0.50 8/29/23 18:25 MFFg/L0.24 8/29/23SM21-23 6200B1Vinyl Chloride ND 1.0 8/29/23 18:25 MFFg/L0.49 8/29/23SM21-23 6200B1m+p Xylene ND 0.50 8/29/23 18:25 MFFg/L0.24 8/29/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 93.4 8/29/23 18:2570-130 Toluene-d8 100 8/29/23 18:2570-130 4-Bromofluorobenzene 100 8/29/23 18:2570-130 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-04 Field Sample #: MW-03 Sample Matrix: Ground Water Sampled: 8/24/2023 11:40 [TOC_2]23H3799-04[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS ND 250 8/29/23 19:44 MFFg/L10 8/29/23SM21-23 6200B5Acetone 1100 120 8/31/23 19:25 LBDg/L46 8/30/23SM21-23 6200B250Benzene ND 2.5 8/29/23 19:44 MFFg/L0.74 8/29/23SM21-23 6200B5Bromobenzene ND 5.0 8/29/23 19:44 MFFg/L1.4 8/29/23SM21-23 6200B5Bromochloromethane ND 2.5 8/29/23 19:44 MFFg/L0.79 8/29/23SM21-23 6200B5Bromodichloromethane ND 5.0 8/29/23 19:44 MFFg/L2.0 8/29/23SM21-23 6200B5Bromoform ND 10 8/29/23 19:44 MFFg/L6.6 8/29/23SM21-23 6200B5Bromomethane ND 25 8/29/23 19:44 MFFg/L8.4 8/29/23SM21-23 6200B52-Butanone (MEK) 84 2.5 8/29/23 19:44 MFFg/L0.75 8/29/23SM21-23 6200B5n-Butylbenzene 28 2.5 8/29/23 19:44 MFFg/L0.63 8/29/23SM21-23 6200B5sec-Butylbenzene ND 2.5 8/29/23 19:44 MFFg/L0.71 8/29/23SM21-23 6200B5tert-Butylbenzene ND 2.5 8/29/23 19:44 MFFg/L0.82 8/29/23SM21-23 6200B5Carbon Tetrachloride ND 2.5 8/29/23 19:44 MFFg/L0.59 8/29/23SM21-23 6200B5Chlorobenzene ND 250 8/29/23 19:44 MFFg/L100 8/29/23SM21-23 6200B5Ethanol ND 2.5 8/29/23 19:44 MFFg/L1.0 8/29/23SM21-23 6200B5Chlorodibromomethane ND 2.5 8/29/23 19:44 MFFg/L1.7 8/29/23SM21-23 6200B5Chloroethane ND 2.5 8/29/23 19:44 MFFg/L0.70 8/29/23SM21-23 6200B5Chloroform ND 3.0 8/29/23 19:44 MFFg/L2.5 8/29/23SM21-23 6200B5Chloromethane ND 2.5 8/29/23 19:44 MFFg/L0.77 8/29/23SM21-23 6200B52-Chlorotoluene ND 2.5 8/29/23 19:44 MFFg/L0.77 8/29/23SM21-23 6200B54-Chlorotoluene ND 2.5 8/29/23 19:44 MFFg/L0.80 8/29/23SM21-23 6200B51,2-Dibromoethane (EDB) ND 2.5 8/29/23 19:44 MFFg/L0.65 8/29/23SM21-23 6200B51,2-Dichlorobenzene ND 2.5 8/29/23 19:44 MFFg/L0.68 8/29/23SM21-23 6200B51,3-Dichlorobenzene ND 2.5 8/29/23 19:44 MFFg/L0.64 8/29/23SM21-23 6200B51,4-Dichlorobenzene ND 2.5 8/29/23 19:44 MFFg/L0.80 8/29/23SM21-23 6200B5Dichlorodifluoromethane (Freon 12) ND 2.5 8/29/23 19:44 MFFg/L0.68 8/29/23SM21-23 6200B51,1-Dichloroethane ND 2.5 8/29/23 19:44 MFFg/L1.5 8/29/23SM21-23 6200B51,2-Dichloroethane ND 2.5 8/29/23 19:44 MFFg/L0.70 8/29/23SM21-23 6200B51,1-Dichloroethylene ND 2.5 8/29/23 19:44 MFFg/L0.70 8/29/23SM21-23 6200B5cis-1,2-Dichloroethylene ND 2.5 8/29/23 19:44 MFFg/L0.86 8/29/23SM21-23 6200B5trans-1,2-Dichloroethylene ND 2.5 8/29/23 19:44 MFFg/L0.97 8/29/23SM21-23 6200B51,2-Dichloropropane ND 2.5 8/29/23 19:44 MFFg/L0.58 8/29/23SM21-23 6200B51,3-Dichloropropane ND 2.5 8/29/23 19:44 MFFg/L1.7 8/29/23SM21-23 6200B52,2-Dichloropropane ND 2.5 8/29/23 19:44 MFFg/L0.75 8/29/23SM21-23 6200B51,1-Dichloropropene ND 2.5 8/29/23 19:44 MFFg/L0.82 8/29/23SM21-23 6200B5cis-1,3-Dichloropropene ND 2.5 8/29/23 19:44 MFFg/L0.71 8/29/23SM21-23 6200B5trans-1,3-Dichloropropene ND 2.5 8/29/23 19:44 MFFg/L1.0 8/29/23SM21-23 6200B5Diisopropyl Ether (DIPE) 2000 120 8/31/23 19:25 LBDg/L55 8/30/23SM21-23 6200B250Ethylbenzene ND 25 8/29/23 19:44 MFFg/L6.0 8/29/23SM21-23 6200B52-Hexanone (MBK) 180 2.5 8/29/23 19:44 MFFg/L0.76 8/29/23SM21-23 6200B5Isopropylbenzene (Cumene) 12 2.5 8/29/23 19:44 MFFg/L0.63 8/29/23SM21-23 6200B5p-Isopropyltoluene (p-Cymene) ND 2.5 8/29/23 19:44 MFFg/L0.85 8/29/23SM21-23 6200B5Methyl tert-Butyl Ether (MTBE) ND 25 8/29/23 19:44 MFFg/L0.88 8/29/23SM21-23 6200B5Methylene Chloride ND 25 8/29/23 19:44 MFFg/L6.6 8/29/23SM21-23 6200B54-Methyl-2-pentanone (MIBK) 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-04 Field Sample #: MW-03 Sample Matrix: Ground Water Sampled: 8/24/2023 11:40 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 490 2.5 8/29/23 19:44 MFFg/L1.9 8/29/23SM21-23 6200B5Naphthalene 560 2.5 8/29/23 19:44 MFFg/L0.62 8/29/23SM21-23 6200B5n-Propylbenzene ND 2.5 8/29/23 19:44 MFFg/L0.75 8/29/23SM21-23 6200B5Styrene ND 2.5 8/29/23 19:44 MFFg/L0.68 8/29/23SM21-23 6200B51,1,2,2-Tetrachloroethane ND 2.5 8/29/23 19:44 MFFg/L0.84 8/29/23SM21-23 6200B5Tetrachloroethylene 1500 120 8/31/23 19:25 LBDg/L56 8/30/23SM21-23 6200B250Toluene ND 5.0 8/29/23 19:44 MFFg/L1.7 8/29/23SM21-23 6200B51,2,3-Trichlorobenzene ND 2.5 8/29/23 19:44 MFFg/L1.5 8/29/23SM21-23 6200B51,2,4-Trichlorobenzene ND 2.5 8/29/23 19:44 MFFg/L0.75 8/29/23SM21-23 6200B51,1,1-Trichloroethane ND 2.5 8/29/23 19:44 MFFg/L0.96 8/29/23SM21-23 6200B51,1,2-Trichloroethane ND 2.5 8/29/23 19:44 MFFg/L0.87 8/29/23SM21-23 6200B5Trichloroethylene ND 2.5 8/29/23 19:44 MFFg/L0.77 8/29/23SM21-23 6200B5Trichlorofluoromethane (Freon 11) ND 5.0 8/29/23 19:44 MFFg/L1.4 8/29/23SM21-23 6200B51,2,3-Trichloropropane 3200 120 8/31/23 19:25 LBDg/L50 8/30/23SM21-23 6200B2501,2,4-Trimethylbenzene 990 2.5 8/29/23 19:44 MFFg/L0.75 8/29/23SM21-23 6200B51,3,5-Trimethylbenzene ND 100 8/29/23 19:44 MFFg/L8.3 8/29/23SM21-23 6200B5Vinyl Acetate ND 2.5 8/29/23 19:44 MFFg/L1.2 8/29/23SM21-23 6200B5Vinyl Chloride 7400 250 8/31/23 19:25 LBDg/L120 8/30/23SM21-23 6200B250m+p Xylene 2000 120 8/31/23 19:25 LBDg/L61 8/30/23SM21-23 6200B250o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 89.4 8/29/23 19:4470-130 1,2-Dichloroethane-d4 94.4 8/31/23 19:2570-130 Toluene-d8 99.5 8/29/23 19:4470-130 Toluene-d8 100 8/31/23 19:2570-130 4-Bromofluorobenzene 102 8/29/23 19:4470-130 4-Bromofluorobenzene 101 8/31/23 19:2570-130 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-05 Field Sample #: MW-04 Sample Matrix: Ground Water Sampled: 8/24/2023 11:06 [TOC_2]23H3799-05[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 8/29/23 18:51 MFFg/L2.0 8/29/23SM21-23 6200B1Acetone ND 0.50 8/29/23 18:51 MFFg/L0.18 8/29/23SM21-23 6200B1Benzene ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B1Bromobenzene ND 1.0 8/29/23 18:51 MFFg/L0.28 8/29/23SM21-23 6200B1Bromochloromethane ND 0.50 8/29/23 18:51 MFFg/L0.16 8/29/23SM21-23 6200B1Bromodichloromethane ND 1.0 8/29/23 18:51 MFFg/L0.41 8/29/23SM21-23 6200B1Bromoform ND 2.0 8/29/23 18:51 MFFg/L1.3 8/29/23SM21-23 6200B1Bromomethane ND 5.0 8/29/23 18:51 MFFg/L1.7 8/29/23SM21-23 6200B12-Butanone (MEK) ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B1n-Butylbenzene ND 0.50 8/29/23 18:51 MFFg/L0.13 8/29/23SM21-23 6200B1sec-Butylbenzene ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B1tert-Butylbenzene ND 0.50 8/29/23 18:51 MFFg/L0.16 8/29/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 8/29/23 18:51 MFFg/L0.12 8/29/23SM21-23 6200B1Chlorobenzene ND 50 8/29/23 18:51 MFFg/L20 8/29/23SM21-23 6200B1Ethanol ND 0.50 8/29/23 18:51 MFFg/L0.20 8/29/23SM21-23 6200B1Chlorodibromomethane ND 0.50 8/29/23 18:51 MFFg/L0.34 8/29/23SM21-23 6200B1Chloroethane ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B1Chloroform ND 0.60 8/29/23 18:51 MFFg/L0.50 8/29/23SM21-23 6200B1Chloromethane ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B12-Chlorotoluene ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B14-Chlorotoluene ND 0.50 8/29/23 18:51 MFFg/L0.16 8/29/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 8/29/23 18:51 MFFg/L0.13 8/29/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 8/29/23 18:51 MFFg/L0.13 8/29/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 8/29/23 18:51 MFFg/L0.16 8/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethane ND 0.50 8/29/23 18:51 MFFg/L0.30 8/29/23SM21-23 6200B11,2-Dichloroethane ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 8/29/23 18:51 MFFg/L0.17 8/29/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 8/29/23 18:51 MFFg/L0.19 8/29/23SM21-23 6200B11,2-Dichloropropane ND 0.50 8/29/23 18:51 MFFg/L0.12 8/29/23SM21-23 6200B11,3-Dichloropropane ND 0.50 8/29/23 18:51 MFFg/L0.35 8/29/23SM21-23 6200B12,2-Dichloropropane ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B11,1-Dichloropropene ND 0.50 8/29/23 18:51 MFFg/L0.16 8/29/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 8/29/23 18:51 MFFg/L0.20 8/29/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 8/29/23 18:51 MFFg/L0.22 8/29/23SM21-23 6200B1Ethylbenzene ND 5.0 8/29/23 18:51 MFFg/L1.2 8/29/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 8/29/23 18:51 MFFg/L0.13 8/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 8/29/23 18:51 MFFg/L0.17 8/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 8/29/23 18:51 MFFg/L0.18 8/29/23SM21-23 6200B1Methylene Chloride ND 5.0 8/29/23 18:51 MFFg/L1.3 8/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-05 Field Sample #: MW-04 Sample Matrix: Ground Water Sampled: 8/24/2023 11:06 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 8/29/23 18:51 MFFg/L0.38 8/29/23SM21-23 6200B1Naphthalene ND 0.50 8/29/23 18:51 MFFg/L0.12 8/29/23SM21-23 6200B1n-Propylbenzene ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B1Styrene ND 0.50 8/29/23 18:51 MFFg/L0.14 8/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane 0.67 0.50 8/29/23 18:51 MFFg/L0.17 8/29/23SM21-23 6200B1Tetrachloroethylene ND 0.50 8/29/23 18:51 MFFg/L0.22 8/29/23SM21-23 6200B1Toluene ND 1.0 8/29/23 18:51 MFFg/L0.34 8/29/23SM21-23 6200B11,2,3-Trichlorobenzene ND 0.50 8/29/23 18:51 MFFg/L0.30 8/29/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 8/29/23 18:51 MFFg/L0.19 8/29/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 8/29/23 18:51 MFFg/L0.17 8/29/23SM21-23 6200B1Trichloroethylene ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 1.0 8/29/23 18:51 MFFg/L0.28 8/29/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 8/29/23 18:51 MFFg/L0.20 8/29/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 8/29/23 18:51 MFFg/L0.15 8/29/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 8/29/23 18:51 MFFg/L1.7 8/29/23SM21-23 6200B1Vinyl Acetate ND 0.50 8/29/23 18:51 MFFg/L0.24 8/29/23SM21-23 6200B1Vinyl Chloride ND 1.0 8/29/23 18:51 MFFg/L0.49 8/29/23SM21-23 6200B1m+p Xylene ND 0.50 8/29/23 18:51 MFFg/L0.24 8/29/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 92.0 8/29/23 18:5170-130 Toluene-d8 98.1 8/29/23 18:5170-130 4-Bromofluorobenzene 102 8/29/23 18:5170-130 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-06 Field Sample #: Trip Blank Sample Matrix: Trip Blank Water Sampled: 8/24/2023 00:00 [TOC_2]23H3799-06[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 8/29/23 11:02 MFFg/L2.0 8/29/23SM21-23 6200B1Acetone ND 0.50 8/29/23 11:02 MFFg/L0.18 8/29/23SM21-23 6200B1Benzene ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B1Bromobenzene ND 1.0 8/29/23 11:02 MFFg/L0.28 8/29/23SM21-23 6200B1Bromochloromethane ND 0.50 8/29/23 11:02 MFFg/L0.16 8/29/23SM21-23 6200B1Bromodichloromethane ND 1.0 8/29/23 11:02 MFFg/L0.41 8/29/23SM21-23 6200B1Bromoform ND 2.0 8/29/23 11:02 MFFg/L1.3 8/29/23SM21-23 6200B1Bromomethane ND 5.0 8/29/23 11:02 MFFg/L1.7 8/29/23SM21-23 6200B12-Butanone (MEK) ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B1n-Butylbenzene ND 0.50 8/29/23 11:02 MFFg/L0.13 8/29/23SM21-23 6200B1sec-Butylbenzene ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B1tert-Butylbenzene ND 0.50 8/29/23 11:02 MFFg/L0.16 8/29/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 8/29/23 11:02 MFFg/L0.12 8/29/23SM21-23 6200B1Chlorobenzene ND 50 8/29/23 11:02 MFFg/L20 8/29/23SM21-23 6200B1Ethanol ND 0.50 8/29/23 11:02 MFFg/L0.20 8/29/23SM21-23 6200B1Chlorodibromomethane ND 0.50 8/29/23 11:02 MFFg/L0.34 8/29/23SM21-23 6200B1Chloroethane ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B1Chloroform ND 0.60 8/29/23 11:02 MFFg/L0.50 8/29/23SM21-23 6200B1Chloromethane ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B12-Chlorotoluene ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B14-Chlorotoluene ND 0.50 8/29/23 11:02 MFFg/L0.16 8/29/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 8/29/23 11:02 MFFg/L0.13 8/29/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 8/29/23 11:02 MFFg/L0.13 8/29/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 8/29/23 11:02 MFFg/L0.16 8/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethane ND 0.50 8/29/23 11:02 MFFg/L0.30 8/29/23SM21-23 6200B11,2-Dichloroethane ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 8/29/23 11:02 MFFg/L0.17 8/29/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 8/29/23 11:02 MFFg/L0.19 8/29/23SM21-23 6200B11,2-Dichloropropane ND 0.50 8/29/23 11:02 MFFg/L0.12 8/29/23SM21-23 6200B11,3-Dichloropropane ND 0.50 8/29/23 11:02 MFFg/L0.35 8/29/23SM21-23 6200B12,2-Dichloropropane ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B11,1-Dichloropropene ND 0.50 8/29/23 11:02 MFFg/L0.16 8/29/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 8/29/23 11:02 MFFg/L0.20 8/29/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 8/29/23 11:02 MFFg/L0.22 8/29/23SM21-23 6200B1Ethylbenzene ND 5.0 8/29/23 11:02 MFFg/L1.2 8/29/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 8/29/23 11:02 MFFg/L0.13 8/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 8/29/23 11:02 MFFg/L0.17 8/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 8/29/23 11:02 MFFg/L0.18 8/29/23SM21-23 6200B1Methylene Chloride ND 5.0 8/29/23 11:02 MFFg/L1.3 8/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 8/25/2023 Work Order: 23H3799Sample Description:Project Location: Fuquay- Varina, NC Sample ID: 23H3799-06 Field Sample #: Trip Blank Sample Matrix: Trip Blank Water Sampled: 8/24/2023 00:00 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 8/29/23 11:02 MFFg/L0.38 8/29/23SM21-23 6200B1Naphthalene ND 0.50 8/29/23 11:02 MFFg/L0.12 8/29/23SM21-23 6200B1n-Propylbenzene ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B1Styrene ND 0.50 8/29/23 11:02 MFFg/L0.14 8/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 8/29/23 11:02 MFFg/L0.17 8/29/23SM21-23 6200B1Tetrachloroethylene ND 0.50 8/29/23 11:02 MFFg/L0.22 8/29/23SM21-23 6200B1Toluene ND 1.0 8/29/23 11:02 MFFg/L0.34 8/29/23SM21-23 6200B11,2,3-Trichlorobenzene ND 0.50 8/29/23 11:02 MFFg/L0.30 8/29/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 8/29/23 11:02 MFFg/L0.19 8/29/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 8/29/23 11:02 MFFg/L0.17 8/29/23SM21-23 6200B1Trichloroethylene ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 1.0 8/29/23 11:02 MFFg/L0.28 8/29/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 8/29/23 11:02 MFFg/L0.20 8/29/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 8/29/23 11:02 MFFg/L0.15 8/29/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 8/29/23 11:02 MFFg/L1.7 8/29/23SM21-23 6200B1Vinyl Acetate ND 0.50 8/29/23 11:02 MFFg/L0.24 8/29/23SM21-23 6200B1Vinyl Chloride ND 1.0 8/29/23 11:02 MFFg/L0.49 8/29/23SM21-23 6200B1m+p Xylene ND 0.50 8/29/23 11:02 MFFg/L0.24 8/29/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 96.4 8/29/23 11:0270-130 Toluene-d8 99.6 8/29/23 11:0270-130 4-Bromofluorobenzene 101 8/29/23 11:0270-130 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 5030B-SM21-23 6200B Lab Number [Field ID]Batch DateInitial [mL]Final [mL] B350423 08/29/235 5.0023H3799-01 [Eq. Rinse] B350423 08/29/230.5 5.0023H3799-02 [MW-1] B350423 08/29/235 5.0023H3799-03 [MW-02] B350423 08/29/231 5.0023H3799-04 [MW-03] B350423 08/29/235 5.0023H3799-05 [MW-04] B350423 08/29/235 5.0023H3799-06 [Trip Blank] Prep Method: SW-846 5030B-SM21-23 6200B Lab Number [Field ID]Batch DateInitial [mL]Final [mL] B350532 08/30/230.01 5.0023H3799-02RE1 [MW-1] B350532 08/30/230.02 5.0023H3799-04RE1 [MW-03] [TOC_1]Sample Preparation Information[TOC] 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Batch B350423 - SW-846 5030B [TOC_3]B350423[TOC] Blank (B350423-BLK1) Prepared & Analyzed: 08/29/23 Acetone g/L50ND Benzene g/L0.50ND Bromobenzene g/L0.50ND Bromochloromethane g/L0.50ND Bromodichloromethane g/L0.50ND Bromoform g/L0.50ND Bromomethane g/L2.0ND 2-Butanone (MEK)g/L5.0ND n-Butylbenzene g/L0.50ND sec-Butylbenzene g/L0.50ND tert-Butylbenzene g/L0.50ND Carbon Tetrachloride g/L0.50ND Chlorobenzene g/L0.50ND Ethanol g/L50ND Chlorodibromomethane g/L0.50ND Chloroethane g/L0.50ND Chloroform g/L0.50ND Chloromethane g/L0.60ND 2-Chlorotoluene g/L0.50ND 4-Chlorotoluene g/L0.50ND 1,2-Dibromoethane (EDB)g/L0.50ND 1,2-Dichlorobenzene g/L0.50ND 1,3-Dichlorobenzene g/L0.50ND 1,4-Dichlorobenzene g/L0.50ND Dichlorodifluoromethane (Freon 12)g/L0.50ND 1,1-Dichloroethane g/L0.50ND 1,2-Dichloroethane g/L0.50ND 1,1-Dichloroethylene g/L0.50ND cis-1,2-Dichloroethylene g/L0.50ND trans-1,2-Dichloroethylene g/L0.50ND 1,2-Dichloropropane g/L0.50ND 1,3-Dichloropropane g/L0.50ND 2,2-Dichloropropane g/L0.50ND 1,1-Dichloropropene g/L0.50ND cis-1,3-Dichloropropene g/L0.50ND trans-1,3-Dichloropropene g/L0.50ND Diisopropyl Ether (DIPE)g/L0.50ND Ethylbenzene g/L0.50ND 2-Hexanone (MBK)g/L5.0ND Isopropylbenzene (Cumene)g/L0.50ND p-Isopropyltoluene (p-Cymene)g/L0.50ND Methyl tert-Butyl Ether (MTBE)g/L0.50ND Methylene Chloride g/L5.0ND 4-Methyl-2-pentanone (MIBK)g/L5.0ND Naphthalene g/L0.50ND n-Propylbenzene g/L0.50ND Styrene g/L0.50ND 1,1,2,2-Tetrachloroethane g/L0.50ND Tetrachloroethylene g/L0.50ND Toluene g/L0.50ND 1,2,3-Trichlorobenzene g/L1.0ND 1,2,4-Trichlorobenzene g/L0.50ND [TOC_1]QC Data[TOC] 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B350423 - SW-846 5030B Blank (B350423-BLK1) Prepared & Analyzed: 08/29/23 1,1,1-Trichloroethane g/L0.50ND 1,1,2-Trichloroethane g/L0.50ND Trichloroethylene g/L0.50ND Trichlorofluoromethane (Freon 11)g/L0.50ND 1,2,3-Trichloropropane g/L0.50ND 1,2,4-Trimethylbenzene g/L0.50ND 1,3,5-Trimethylbenzene g/L0.50ND Vinyl Acetate g/L20ND Vinyl Chloride g/L0.50ND m+p Xylene g/L1.0ND o-Xylene g/L0.50ND g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 95.523.9 g/L 25.0 70-130Surrogate: Toluene-d8 98.924.7 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.324.8 LCS (B350423-BS1) Prepared & Analyzed: 08/29/23 Acetone g/L50 100 70-13090.890.8 Benzene g/L0.50 10.0 70-13010610.6 Bromobenzene g/L0.50 10.0 70-13011011.0 Bromochloromethane g/L0.50 10.0 70-13010710.7 Bromodichloromethane g/L0.50 10.0 70-13011011.0 Bromoform g/L0.50 10.0 70-13010710.7 Bromomethane g/L2.0 10.0 60-14010310.3 2-Butanone (MEK)g/L5.0 100 70-13099.899.8 n-Butylbenzene g/L0.50 10.0 70-13011011.0 sec-Butylbenzene g/L0.50 10.0 70-13010710.7 tert-Butylbenzene g/L0.50 10.0 70-13010710.7 Carbon Tetrachloride g/L0.50 10.0 70-13099.99.99 Chlorobenzene g/L0.50 10.0 70-13011211.2 Ethanol g/L50 100 70-13090.690.6 Chlorodibromomethane g/L0.50 10.0 70-13011011.0 Chloroethane g/L0.50 10.0 60-14095.49.54 Chloroform g/L0.50 10.0 70-13010710.7 Chloromethane g/L0.60 10.0 60-14010310.3 2-Chlorotoluene g/L0.50 10.0 70-13011111.1 4-Chlorotoluene g/L0.50 10.0 70-13011211.2 1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13011411.4 1,2-Dichlorobenzene g/L0.50 10.0 70-13010910.9 1,3-Dichlorobenzene g/L0.50 10.0 70-13010810.8 1,4-Dichlorobenzene g/L0.50 10.0 70-13010610.6 Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14010010.0 1,1-Dichloroethane g/L0.50 10.0 70-13010710.7 1,2-Dichloroethane g/L0.50 10.0 70-13011011.0 1,1-Dichloroethylene g/L0.50 10.0 70-13010110.1 cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010710.7 trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010910.9 1,2-Dichloropropane g/L0.50 10.0 70-13011211.2 1,3-Dichloropropane g/L0.50 10.0 70-13011211.2 2,2-Dichloropropane g/L0.50 10.0 70-13010510.5 1,1-Dichloropropene g/L0.50 10.0 70-13010810.8 cis-1,3-Dichloropropene g/L0.50 10.0 70-13011211.2 trans-1,3-Dichloropropene g/L0.50 10.0 70-13011011.0 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B350423 - SW-846 5030B LCS (B350423-BS1) Prepared & Analyzed: 08/29/23 Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010410.4 Ethylbenzene g/L0.50 10.0 70-13011111.1 2-Hexanone (MBK)g/L5.0 100 70-130107107 Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011011.0 p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010810.8 Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13010410.4 Methylene Chloride g/L5.0 10.0 70-13010210.2 4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130109109 Naphthalene g/L0.50 10.0 70-13011011.0 n-Propylbenzene g/L0.50 10.0 70-13011211.2 Styrene g/L0.50 10.0 70-13011411.4 1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13011311.3 Tetrachloroethylene g/L0.50 10.0 70-13011411.4 Toluene g/L0.50 10.0 70-13010910.9 1,2,3-Trichlorobenzene g/L1.0 10.0 70-13011611.6 1,2,4-Trichlorobenzene g/L0.50 10.0 70-13011311.3 1,1,1-Trichloroethane g/L0.50 10.0 70-13010710.7 1,1,2-Trichloroethane g/L0.50 10.0 70-13011111.1 Trichloroethylene g/L0.50 10.0 70-13011211.2 Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13010710.7 1,2,3-Trichloropropane g/L0.50 10.0 70-13010910.9 1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010610.6 1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011311.3 Vinyl Acetate g/L20 100 70-130108108 Vinyl Chloride g/L0.50 10.0 60-14010510.5 m+p Xylene g/L1.0 20.0 70-13011022.0 o-Xylene g/L0.50 10.0 70-13011011.0 g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.324.3 g/L 25.0 70-130Surrogate: Toluene-d8 10125.2 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.9 LCS Dup (B350423-BSD1) Prepared & Analyzed: 08/29/23 Acetone g/L50 100 2570-13095.2 4.7495.2 Benzene g/L0.50 10.0 2570-130109 2.2310.9 Bromobenzene g/L0.50 10.0 2570-130109 1.0910.9 Bromochloromethane g/L0.50 10.0 2570-130111 3.4811.1 Bromodichloromethane g/L0.50 10.0 2570-130109 0.18310.9 Bromoform g/L0.50 10.0 2570-130103 3.7110.3 Bromomethane g/L2.0 10.0 2560-140108 4.2710.8 2-Butanone (MEK)g/L5.0 100 2570-130104 3.71104 n-Butylbenzene g/L0.50 10.0 2570-130112 1.8111.2 sec-Butylbenzene g/L0.50 10.0 2570-130108 1.1210.8 tert-Butylbenzene g/L0.50 10.0 2570-130107 0.65410.7 Carbon Tetrachloride g/L0.50 10.0 2570-130106 6.4010.6 Chlorobenzene g/L0.50 10.0 2570-130111 0.71711.1 Ethanol g/L50 100 2570-13095.0 4.8095.0 Chlorodibromomethane g/L0.50 10.0 2570-130110 0.81911.0 Chloroethane g/L0.50 10.0 2560-140106 10.110.6 Chloroform g/L0.50 10.0 2570-130109 1.8510.9 Chloromethane g/L0.60 10.0 2560-140105 1.6310.5 2-Chlorotoluene g/L0.50 10.0 2570-130109 1.5510.9 4-Chlorotoluene g/L0.50 10.0 2570-130108 2.8210.8 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B350423 - SW-846 5030B LCS Dup (B350423-BSD1) Prepared & Analyzed: 08/29/23 1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130114 0.17511.4 1,2-Dichlorobenzene g/L0.50 10.0 2570-130109 0.091910.9 1,3-Dichlorobenzene g/L0.50 10.0 2570-130111 2.2811.1 1,4-Dichlorobenzene g/L0.50 10.0 2570-130107 0.65610.7 Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-140104 4.0010.4 1,1-Dichloroethane g/L0.50 10.0 2570-130110 2.2111.0 1,2-Dichloroethane g/L0.50 10.0 2570-130114 2.9511.4 1,1-Dichloroethylene g/L0.50 10.0 2570-130105 4.6610.5 cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130111 3.3111.1 trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130108 0.27710.8 1,2-Dichloropropane g/L0.50 10.0 2570-130114 1.4111.4 1,3-Dichloropropane g/L0.50 10.0 2570-130112 0.44611.2 2,2-Dichloropropane g/L0.50 10.0 2570-130107 1.7010.7 1,1-Dichloropropene g/L0.50 10.0 2570-130108 0.092910.8 cis-1,3-Dichloropropene g/L0.50 10.0 2570-130112 0.35811.2 trans-1,3-Dichloropropene g/L0.50 10.0 2570-130113 2.4211.3 Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130108 3.1110.8 Ethylbenzene g/L0.50 10.0 2570-130111 0.18011.1 2-Hexanone (MBK)g/L5.0 100 2570-130110 2.82110 Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130110 0.63711.0 p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130109 0.92510.9 Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130106 1.9110.6 Methylene Chloride g/L5.0 10.0 2570-130108 5.8310.8 4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130110 1.38110 Naphthalene g/L0.50 10.0 2570-130112 1.7211.2 n-Propylbenzene g/L0.50 10.0 2570-130112 0.26711.2 Styrene g/L0.50 10.0 2570-130113 0.53011.3 1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130112 1.1611.2 Tetrachloroethylene g/L0.50 10.0 2570-130117 2.3411.7 Toluene g/L0.50 10.0 2570-130110 0.91411.0 1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130114 1.8311.4 1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130112 1.4211.2 1,1,1-Trichloroethane g/L0.50 10.0 2570-130108 0.74310.8 1,1,2-Trichloroethane g/L0.50 10.0 2570-130113 1.9611.3 Trichloroethylene g/L0.50 10.0 2570-130110 1.7911.0 Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13098.7 7.799.87 1,2,3-Trichloropropane g/L0.50 10.0 2570-130110 0.73211.0 1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130107 0.84210.7 1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130112 0.62211.2 Vinyl Acetate g/L20 100 2570-130111 2.24111 Vinyl Chloride g/L0.50 10.0 2560-140108 2.7310.8 m+p Xylene g/L1.0 20.0 2570-130109 1.2821.8 o-Xylene g/L0.50 10.0 2570-130110 0.091111.0 g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.123.3 g/L 25.0 70-130Surrogate: Toluene-d8 10125.1 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.4 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B350532 - SW-846 5030B [TOC_3]B350532[TOC] Blank (B350532-BLK1) Prepared: 08/30/23 Analyzed: 08/31/23 Benzene g/L0.50ND Ethylbenzene g/L0.50ND Toluene g/L0.50ND 1,2,4-Trimethylbenzene g/L0.50ND m+p Xylene g/L1.0ND o-Xylene g/L0.50ND g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.824.4 g/L 25.0 70-130Surrogate: Toluene-d8 10125.3 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.4 LCS (B350532-BS1) Prepared: 08/30/23 Analyzed: 08/31/23 Benzene g/L0.50 10.0 70-13010110.1 Ethylbenzene g/L0.50 10.0 70-13010610.6 Toluene g/L0.50 10.0 70-13010910.9 1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010210.2 m+p Xylene g/L1.0 20.0 70-13010521.0 o-Xylene g/L0.50 10.0 70-13010610.6 g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.522.1 g/L 25.0 70-130Surrogate: Toluene-d8 10025.0 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10426.1 LCS Dup (B350532-BSD1) Prepared: 08/30/23 Analyzed: 08/31/23 Benzene g/L0.50 10.0 2570-130104 3.1110.4 Ethylbenzene g/L0.50 10.0 2570-130110 3.4211.0 Toluene g/L0.50 10.0 2570-130108 0.55210.8 1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130102 0.68710.2 m+p Xylene g/L1.0 20.0 2570-130108 2.2121.5 o-Xylene g/L0.50 10.0 2570-130107 1.3210.7 g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 91.522.9 g/L 25.0 70-130Surrogate: Toluene-d8 10125.2 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.3 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 *QC result is outside of established limits. Wide recovery limits established for difficult compound. Wide RPD limits established for difficult compound. #Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. FLAG/QUALIFIER SUMMARY Elevated reporting limit due to high concentration of target compounds.RL-11 [TOC_1]Flag/Qualifier Summary[TOC] 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report SM21-23 6200B in Water NCAcetone NCBenzene NCBromobenzene NCBromochloromethane NCBromodichloromethane NCBromoform NCBromomethane NC2-Butanone (MEK) NCn-Butylbenzene NCsec-Butylbenzene NCtert-Butylbenzene NCCarbon Tetrachloride NCChlorobenzene NCEthanol NCChlorodibromomethane NCChloroethane NCChloroform NCChloromethane NC2-Chlorotoluene NC4-Chlorotoluene NC1,2-Dibromoethane (EDB) NC1,2-Dichlorobenzene NC1,3-Dichlorobenzene NC1,4-Dichlorobenzene NCDichlorodifluoromethane (Freon 12) NC1,1-Dichloroethane NC1,2-Dichloroethane NC1,1-Dichloroethylene NCcis-1,2-Dichloroethylene NCtrans-1,2-Dichloroethylene NC1,2-Dichloropropane NC1,3-Dichloropropane NC2,2-Dichloropropane NC1,1-Dichloropropene NCcis-1,3-Dichloropropene NCtrans-1,3-Dichloropropene NCDiisopropyl Ether (DIPE) NCEthylbenzene NC2-Hexanone (MBK) NCIsopropylbenzene (Cumene) NCp-Isopropyltoluene (p-Cymene) NCMethyl tert-Butyl Ether (MTBE) NCMethylene Chloride NC4-Methyl-2-pentanone (MIBK) NCNaphthalene NCn-Propylbenzene NCStyrene [TOC_1]Certifications[TOC] 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report SM21-23 6200B in Water NC1,1,2,2-Tetrachloroethane NCTetrachloroethylene NCToluene NC1,2,3-Trichlorobenzene NC1,2,4-Trichlorobenzene NC1,1,1-Trichloroethane NC1,1,2-Trichloroethane NCTrichloroethylene NCTrichlorofluoromethane (Freon 11) NC1,2,3-Trichloropropane NC1,2,4-Trimethylbenzene NC1,3,5-Trimethylbenzene NCVinyl Acetate NCVinyl Chloride NCm+p Xylene NCo-Xylene The CON-TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires 652North Carolina Div. of Water QualityNC 12/31/2023 fed Sign Up or Log In FedEx" Tracking DELIVERED Friday 8/25/23 at 9:26 AM Signed for by: C.LUIS ~ Obtain proof of deli ry How was your de live ***** DELIVERY STATUS Delivered . TRACKING ID 773159095363 /' * FROM RALEIGH, NC US Label Created 8/24/23 12:42 P WEHAVEYOUR ACKAGE RALEIGH, NC 8/24/23 4:40 P IN TRANSIT 8/25/23 8:00 AM OUT FOR DELI VE Y WINDSOR LOCK , CT 8/25/23 8:09 AM DELIVERED EAST LONGMEA OW, MA US Delivered 8/25/23 at 9:26 M -1, View travel 1istory Want updates on this ship ent? Enter your email and we will do the rest! YOUR EMAIL ContesUab39 MORE OPTIONS SUBMIT DC#_Title: ENV-FRM-ELON-0001 v07 _Sample Receiving Checklist Effective Date: 07/13/2023 Log I n Back-Sheet Client t_~\1 " \:..f",C.\\<"\R...~, S 1 '::>c,~(""\\ ,':f..-~ J Project \\o.,, ,C"'\C\.\cr-. 'i?,c-.v~, \-,, .) MCP/RCP Required_"-)~\.i,.;A~l----------- Deliverable Package Requlrem rnt_\.)...::e...:\:..:.~---=------- Location "\= l , u \J c..,1 -\J G ,;;-·, r-<.., ~ (_ V 1 PWSID# (When Applicable) -+")<--.!.\_A...:__ _____ _ Arrival Method: Courier D Fed Ex d Walk In D OtherD ___ _ Received By/ Date / Time A. ~ M / ~-7 5-21 / o c., 7 v Back-Sheet By/ Date/ Time P A.I"\ l 1:> -'2.S -z... '\ / ,1 l\O T Temperature Method 1 '<--('('\ ::> G-v ("\ # _ _.S-'---- / o C-:. i:. o(_ Temp ✓ < 6 C Actual Tem , erature __ ..,=---·=-.J___;;;c __ _ Rush Samples: Yes /~ Notif~ Short Hold: Yes ,@ Notif-1 _________ _ Notes reeardine Samele s/COC outside of SOP: Qualtrax ID: 1208 16 Login Sample Receipt Checklist -(Relectlon Criteria Listing -Using Acceptance Policy! Any False statement wlll be brought to the attention of the Client -True or False Received on Ice Received in Cooler Custody Seal: DATE TIME COC Relinquished CCC/Samples Labels Agree All Samples in Good Condition Samples Received within Holding Time Is there enough Volume Proper Media/Container Used Splitting Samples Required MS/MSD Trip Blanks Lab to Filters COC Legible True □ tf.c i3; □ tv □✓ COC Included: (Check all included) Client ~ Analysis ~ Sampler Name Project l.::'.l IDs ~ Collection Date All Samples Proper pH: @ D Additional Container Notes ime False □ □ [T □ □ □ □ □ ~AM ~ ff □ ~ □ ~ ~ □ Note: West Virginia requires all samples to hove their temperature taken. Note any outliers. L;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;;-_ ---------- Page 1 of 2 ~! DC#_Tltle: ENV-FRM-ELON-0001 v07 _Sample Receiving Cn eckllst Effective Date: 07/13/2023 ~ -----~ ----Sample \D 00 ....., O'\ u, 1-M "' -0 \D 00 ...., O'\ u, .s:. ~ "' -16Cl z Amb/Clear 15 ;:; Q. 8oz Amb/Clear ii"" ~ .;.- 4oz Amb/Clear er --A> Cl ~ ,,, 2oz [Amb/Clear .... ~ Un,: reserved .... HCL ,-;::..· t'D .... Sulf JJric )> Sulf uric 3 ~ er V, 11> Pho l!;phorlc C, ~ 3 HCI ,- Unp eserved --8 3 r- Unp reserved .... ,-;:::.: Sulf ~rlc t'D ... Unp reserved V, C, C, Sul fµrlc 3 ,- Unpreserved -0 ii, Triz1 ina .,. ..... Sulf l,Jric ~- ~ V, Nitr C C, 3 ,- NaC H Amm c,nlum Acetate NaO H/Zinc Unp reserved N N N I'-> N ('l HCI c::: 0 Me< l>H )> ~ D.I. 'Water ~ .,.. Bi Sulfate Col/ ~act 0 ,-+ ;;:r n> .... -::!:? :::, Qualtrax ID: 120836 Page 2 of 2