RA-613_3831_CA_MRP_20171212

December 12, 2017
Mr. Mark Petermann
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Reference: Letter Report of Groundwater Sampling
Mt. Harmony Grocery
1818 Mt. Harmony Church Road
Rougemont, Person County, North Carolina
NCDEQ Incident No: 3831
ECS Project: 49:3051-B

Dear Mr. Petermann:

As authorized by your acceptance of ECS Southeast, LLP (ECS) Task Authorization Request
Number (TAR No. 2) dated November 17, 2017, ECS has completed the Letter Report of
groundwater sampling for the above referenced site.

On November 21, 2017, ECS collected a field blank and a groundwater sample from water
supply well WSW-2 (Bradsher Well) (Figures 1 and 2). Prior to collecting the groundwater
sample from WSW-2, ECS met with Mr. Clifton Bradsher and obtained a signed water supply
well permission letter. The signed letter is attached. ECS collected the groundwater sample
from water supply well WSW-2 by opening the spigot attached to the water supply well for three
to five minutes, thus allowing the groundwater to purge from the water supply well. After, ECS
collected the groundwater samples from the spigot into sample containers provided by the
laboratory.

Prior to beginning groundwater sampling activities, ECS collected the field blank by pouring DI
water (analyte-free water prepared at the laboratory and included in the sampling kit), at the
sampling site into the appropriate laboratory prepared sample containers.

The sample containers were labeled with ECS project number, sample identification, sample date
and time, and requested analytical analysis. The containers were placed into protective packaging
material and placed into a cooler with ice to maintain the samples at approximately 4 Celsius (C).
The samples were submitted to Pace Laboratories, Inc. located in Huntersville, North Carolina for
chemical analysis for Volatile Organic Compounds (VOCs) using Standard Method 6200B. ECS
maintained proper chain of custody (COC) procedures throughout the sample collection and
transportation process.

The laboratory did not report targeted analytes at concentrations above the laboratory reporting
limits in the groundwater sample collected from water supply well WSW-2 or the field blank.
The laboratory analytical data sheets and COC are attached.

SOURCE:

USGS TOPOGRAPHIC MAP
MORIAH & TIMBERLAKE
NORTH CAROLINA QUADRANGLE
DATED 2016

SCALE: 1 : 24,000

FIGURE 1
SITE LOCATION MAP

MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 3831
ECS PROJECT: 49:3051-B
SITE
SOURCE:

GOOGLE EARTH
DATED 2013

SCALE AS SHOWN

FIGURE 2
WATER SUPPLY WELL LOCATION MAP

MT. HARMONY GROCERY
1818 MT. HARMONY CHURCH ROAD
ROUGEMONT, PERSON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 3831
ECS PROJECT: 49:3051-B
LEGEND

Approximate Location of Active
Water Supply Well
Approximate Location of Inactive
Water Supply Well
1,000 ft.
Radius
WSW-3
PW-1
Scale: 1 inch = 290 feet
WSW-1
WSW-2
WSW-5
WSW-6
WSW-7
WSW-8
WSW-3
(WSW-4)
PW-4A
500 ft.
Radius
PW-2
(PW-3)
PW-4B
SITE
PW-2
#=CL#
December 04, 2017
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92364508
92364508
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
NCDEQ MT. HARMONY
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on November 22, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc: Sarah Kordon, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92364508001 WSW-2 SM 6200B 64 PASI-CSWB
92364508002 FIELD BLANK SM 6200B 64 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Sample: WSW-2 Lab ID: 92364508001 Collected: 11/21/17 09:30 Received: 11/22/17 15:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/01/17 20:17 71-43-20.50 1
Bromobenzene ND ug/L 12/01/17 20:17 108-86-10.50 1
Bromochloromethane ND ug/L 12/01/17 20:17 74-97-50.50 1
Bromodichloromethane ND ug/L 12/01/17 20:17 75-27-40.50 1
Bromoform ND ug/L 12/01/17 20:17 75-25-20.50 1
Bromomethane ND ug/L 12/01/17 20:17 74-83-95.0 1
n-Butylbenzene ND ug/L 12/01/17 20:17 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/01/17 20:17 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/01/17 20:17 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/01/17 20:17 56-23-50.50 1
Chlorobenzene ND ug/L 12/01/17 20:17 108-90-70.50 1
Chloroethane ND ug/L 12/01/17 20:17 75-00-3 M11.0 1
Chloroform ND ug/L 12/01/17 20:17 67-66-30.50 1
Chloromethane ND ug/L 12/01/17 20:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/01/17 20:17 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/01/17 20:17 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/17 20:17 96-12-81.0 1
Dibromochloromethane ND ug/L 12/01/17 20:17 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/17 20:17 106-93-40.50 1
Dibromomethane ND ug/L 12/01/17 20:17 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/01/17 20:17 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/01/17 20:17 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/01/17 20:17 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/01/17 20:17 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/01/17 20:17 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/01/17 20:17 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/01/17 20:17 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/01/17 20:17 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/01/17 20:17 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/01/17 20:17 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/01/17 20:17 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/01/17 20:17 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/01/17 20:17 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/01/17 20:17 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/01/17 20:17 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/01/17 20:17 108-20-30.50 1
Ethanol ND ug/L 12/01/17 20:17 64-17-5 M1200 1
Ethylbenzene ND ug/L 12/01/17 20:17 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/01/17 20:17 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/01/17 20:17 98-82-80.50 1
Methylene Chloride ND ug/L 12/01/17 20:17 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/01/17 20:17 1634-04-40.50 1
Naphthalene ND ug/L 12/01/17 20:17 91-20-32.0 1
n-Propylbenzene ND ug/L 12/01/17 20:17 103-65-10.50 1
Styrene ND ug/L 12/01/17 20:17 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/17 20:17 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/17 20:17 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Sample: WSW-2 Lab ID: 92364508001 Collected: 11/21/17 09:30 Received: 11/22/17 15:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/01/17 20:17 127-18-40.50 1
Toluene ND ug/L 12/01/17 20:17 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/01/17 20:17 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/01/17 20:17 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/01/17 20:17 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/01/17 20:17 79-00-50.50 1
Trichloroethene ND ug/L 12/01/17 20:17 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/01/17 20:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/01/17 20:17 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/01/17 20:17 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/01/17 20:17 108-67-80.50 1
Vinyl chloride ND ug/L 12/01/17 20:17 75-01-41.0 1
m&p-Xylene ND ug/L 12/01/17 20:17 179601-23-11.0 1
o-Xylene ND ug/L 12/01/17 20:17 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %12/01/17 20:17 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %12/01/17 20:17 460-00-470-130 1
Toluene-d8 (S)102 %12/01/17 20:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Sample: FIELD BLANK Lab ID: 92364508002 Collected: 11/21/17 09:00 Received: 11/22/17 15:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 11/30/17 10:23 71-43-20.50 1
Bromobenzene ND ug/L 11/30/17 10:23 108-86-10.50 1
Bromochloromethane ND ug/L 11/30/17 10:23 74-97-50.50 1
Bromodichloromethane ND ug/L 11/30/17 10:23 75-27-40.50 1
Bromoform ND ug/L 11/30/17 10:23 75-25-20.50 1
Bromomethane ND ug/L 11/30/17 10:23 74-83-95.0 1
n-Butylbenzene ND ug/L 11/30/17 10:23 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/30/17 10:23 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/30/17 10:23 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/30/17 10:23 56-23-50.50 1
Chlorobenzene ND ug/L 11/30/17 10:23 108-90-70.50 1
Chloroethane ND ug/L 11/30/17 10:23 75-00-31.0 1
Chloroform ND ug/L 11/30/17 10:23 67-66-30.50 1
Chloromethane ND ug/L 11/30/17 10:23 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/30/17 10:23 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/30/17 10:23 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/30/17 10:23 96-12-81.0 1
Dibromochloromethane ND ug/L 11/30/17 10:23 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/30/17 10:23 106-93-40.50 1
Dibromomethane ND ug/L 11/30/17 10:23 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/30/17 10:23 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/30/17 10:23 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/30/17 10:23 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/30/17 10:23 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/30/17 10:23 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/30/17 10:23 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/30/17 10:23 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/30/17 10:23 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/30/17 10:23 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/30/17 10:23 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/30/17 10:23 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/30/17 10:23 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/30/17 10:23 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/30/17 10:23 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/30/17 10:23 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/30/17 10:23 108-20-30.50 1
Ethanol ND ug/L 11/30/17 10:23 64-17-5200 1
Ethylbenzene ND ug/L 11/30/17 10:23 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/30/17 10:23 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/30/17 10:23 98-82-80.50 1
Methylene Chloride ND ug/L 11/30/17 10:23 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/30/17 10:23 1634-04-40.50 1
Naphthalene ND ug/L 11/30/17 10:23 91-20-32.0 1
n-Propylbenzene ND ug/L 11/30/17 10:23 103-65-10.50 1
Styrene ND ug/L 11/30/17 10:23 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/30/17 10:23 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/30/17 10:23 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Sample: FIELD BLANK Lab ID: 92364508002 Collected: 11/21/17 09:00 Received: 11/22/17 15:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 11/30/17 10:23 127-18-40.50 1
Toluene ND ug/L 11/30/17 10:23 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/30/17 10:23 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/30/17 10:23 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/30/17 10:23 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/30/17 10:23 79-00-50.50 1
Trichloroethene ND ug/L 11/30/17 10:23 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/30/17 10:23 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/30/17 10:23 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/30/17 10:23 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/30/17 10:23 108-67-80.50 1
Vinyl chloride ND ug/L 11/30/17 10:23 75-01-41.0 1
m&p-Xylene ND ug/L 11/30/17 10:23 179601-23-11.0 1
o-Xylene ND ug/L 11/30/17 10:23 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/30/17 10:23 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %11/30/17 10:23 460-00-470-130 1
Toluene-d8 (S)102 %11/30/17 10:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388822
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92364508002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2156824
Associated Lab Samples:92364508002
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/30/17 09:49
1,1,1-Trichloroethane ug/L ND 0.50 11/30/17 09:49
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/30/17 09:49
1,1,2-Trichloroethane ug/L ND 0.50 11/30/17 09:49
1,1-Dichloroethane ug/L ND 0.50 11/30/17 09:49
1,1-Dichloroethene ug/L ND 0.50 11/30/17 09:49
1,1-Dichloropropene ug/L ND 0.50 11/30/17 09:49
1,2,3-Trichlorobenzene ug/L ND 2.0 11/30/17 09:49
1,2,3-Trichloropropane ug/L ND 0.50 11/30/17 09:49
1,2,4-Trichlorobenzene ug/L ND 2.0 11/30/17 09:49
1,2,4-Trimethylbenzene ug/L ND 0.50 11/30/17 09:49
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/30/17 09:49
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/30/17 09:49
1,2-Dichlorobenzene ug/L ND 0.50 11/30/17 09:49
1,2-Dichloroethane ug/L ND 0.50 11/30/17 09:49
1,2-Dichloropropane ug/L ND 0.50 11/30/17 09:49
1,3,5-Trimethylbenzene ug/L ND 0.50 11/30/17 09:49
1,3-Dichlorobenzene ug/L ND 0.50 11/30/17 09:49
1,3-Dichloropropane ug/L ND 0.50 11/30/17 09:49
1,4-Dichlorobenzene ug/L ND 0.50 11/30/17 09:49
2,2-Dichloropropane ug/L ND 0.50 11/30/17 09:49
2-Chlorotoluene ug/L ND 0.50 11/30/17 09:49
4-Chlorotoluene ug/L ND 0.50 11/30/17 09:49
Benzene ug/L ND 0.50 11/30/17 09:49
Bromobenzene ug/L ND 0.50 11/30/17 09:49
Bromochloromethane ug/L ND 0.50 11/30/17 09:49
Bromodichloromethane ug/L ND 0.50 11/30/17 09:49
Bromoform ug/L ND 0.50 11/30/17 09:49
Bromomethane ug/L ND 5.0 11/30/17 09:49
Carbon tetrachloride ug/L ND 0.50 11/30/17 09:49
Chlorobenzene ug/L ND 0.50 11/30/17 09:49
Chloroethane ug/L ND 1.0 11/30/17 09:49
Chloroform ug/L ND 0.50 11/30/17 09:49
Chloromethane ug/L ND 1.0 11/30/17 09:49
cis-1,2-Dichloroethene ug/L ND 0.50 11/30/17 09:49
cis-1,3-Dichloropropene ug/L ND 0.50 11/30/17 09:49
Dibromochloromethane ug/L ND 0.50 11/30/17 09:49
Dibromomethane ug/L ND 0.50 11/30/17 09:49
Dichlorodifluoromethane ug/L ND 0.50 11/30/17 09:49
Diisopropyl ether ug/L ND 0.50 11/30/17 09:49
Ethanol ug/L ND 200 11/30/17 09:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2156824
Associated Lab Samples:92364508002
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 11/30/17 09:49
Hexachloro-1,3-butadiene ug/L ND 2.0 11/30/17 09:49
Isopropylbenzene (Cumene)ug/L ND 0.50 11/30/17 09:49
m&p-Xylene ug/L ND 1.0 11/30/17 09:49
Methyl-tert-butyl ether ug/L ND 0.50 11/30/17 09:49
Methylene Chloride ug/L ND 2.0 11/30/17 09:49
n-Butylbenzene ug/L ND 0.50 11/30/17 09:49
n-Propylbenzene ug/L ND 0.50 11/30/17 09:49
Naphthalene ug/L ND 2.0 11/30/17 09:49
o-Xylene ug/L ND 0.50 11/30/17 09:49
sec-Butylbenzene ug/L ND 0.50 11/30/17 09:49
Styrene ug/L ND 0.50 11/30/17 09:49
tert-Butylbenzene ug/L ND 0.50 11/30/17 09:49
Tetrachloroethene ug/L ND 0.50 11/30/17 09:49
Toluene ug/L ND 0.50 11/30/17 09:49
trans-1,2-Dichloroethene ug/L ND 0.50 11/30/17 09:49
trans-1,3-Dichloropropene ug/L ND 0.50 11/30/17 09:49
Trichloroethene ug/L ND 0.50 11/30/17 09:49
Trichlorofluoromethane ug/L ND 1.0 11/30/17 09:49
Vinyl chloride ug/L ND 1.0 11/30/17 09:49
1,2-Dichloroethane-d4 (S)%85 70-130 11/30/17 09:49
4-Bromofluorobenzene (S)%98 70-130 11/30/17 09:49
Toluene-d8 (S)%90 70-130 11/30/17 09:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2156825LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.350 101 60-140
1,1,1-Trichloroethane ug/L 43.950 88 60-140
1,1,2,2-Tetrachloroethane ug/L 49.350 99 60-140
1,1,2-Trichloroethane ug/L 57.550 115 60-140
1,1-Dichloroethane ug/L 48.450 97 60-140
1,1-Dichloroethene ug/L 54.850 110 60-140
1,1-Dichloropropene ug/L 48.450 97 60-140
1,2,3-Trichlorobenzene ug/L 49.550 99 60-140
1,2,3-Trichloropropane ug/L 47.150 94 60-140
1,2,4-Trichlorobenzene ug/L 52.350 105 60-140
1,2,4-Trimethylbenzene ug/L 51.450 103 60-140
1,2-Dibromo-3-chloropropane ug/L 50.150 100 60-140
1,2-Dibromoethane (EDB)ug/L 51.750 103 60-140
1,2-Dichlorobenzene ug/L 50.450 101 60-140
1,2-Dichloroethane ug/L 50.350 101 60-140
1,2-Dichloropropane ug/L 52.150 104 60-140
1,3,5-Trimethylbenzene ug/L 51.350 103 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
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Page 9 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2156825LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 50.050 100 60-140
1,3-Dichloropropane ug/L 52.650 105 60-140
1,4-Dichlorobenzene ug/L 49.550 99 60-140
2,2-Dichloropropane ug/L 46.150 92 60-140
2-Chlorotoluene ug/L 50.150 100 60-140
4-Chlorotoluene ug/L 50.550 101 60-140
Benzene ug/L 49.850 100 60-140
Bromobenzene ug/L 52.250 104 60-140
Bromochloromethane ug/L 50.550 101 60-140
Bromodichloromethane ug/L 46.950 94 60-140
Bromoform ug/L 50.250 100 60-140
Bromomethane ug/L 44.950 90 60-140
Carbon tetrachloride ug/L 42.550 85 60-140
Chlorobenzene ug/L 51.250 102 60-140
Chloroethane ug/L 54.450 109 60-140
Chloroform ug/L 45.750 91 60-140
Chloromethane ug/L 53.350 107 60-140
cis-1,2-Dichloroethene ug/L 50.050 100 60-140
cis-1,3-Dichloropropene ug/L 51.850 104 60-140
Dibromochloromethane ug/L 51.150 102 60-140
Dibromomethane ug/L 54.950 110 60-140
Dichlorodifluoromethane ug/L 40.350 81 60-140
Diisopropyl ether ug/L 47.150 94 60-140
Ethanol ug/L 22902000 115 60-140
Ethylbenzene ug/L 50.850 102 60-140
Hexachloro-1,3-butadiene ug/L 51.850 104 60-140
Isopropylbenzene (Cumene)ug/L 50.750 101 60-140
m&p-Xylene ug/L 101100 101 60-140
Methyl-tert-butyl ether ug/L 45.350 91 60-140
Methylene Chloride ug/L 52.850 106 60-140
n-Butylbenzene ug/L 51.350 103 60-140
n-Propylbenzene ug/L 51.250 102 60-140
Naphthalene ug/L 48.950 98 60-140
o-Xylene ug/L 50.850 102 60-140
sec-Butylbenzene ug/L 50.750 101 60-140
Styrene ug/L 52.250 104 60-140
tert-Butylbenzene ug/L 41.750 83 60-140
Tetrachloroethene ug/L 46.450 93 60-140
Toluene ug/L 51.850 104 60-140
trans-1,2-Dichloroethene ug/L 48.450 97 60-140
trans-1,3-Dichloropropene ug/L 53.650 107 60-140
Trichloroethene ug/L 49.650 99 60-140
Trichlorofluoromethane ug/L 48.250 96 60-140
Vinyl chloride ug/L 55.550 111 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2156826MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364039006
2156827
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 400 109 60-140113 4400ND435 452
1,1,1-Trichloroethane ug/L 400 113 60-140114 1400ND451 454
1,1,2,2-Tetrachloroethane ug/L 400 104 60-140108 4400ND418 433
1,1,2-Trichloroethane ug/L 400 114 60-140117 2400ND457 468
1,1-Dichloroethane ug/L 400 121 60-140123 1400ND486 491
1,1-Dichloroethene ug/L 400 129 60-140128 1400ND517 511
1,1-Dichloropropene ug/L 400 118 60-140117 0400ND471 469
1,2,3-Trichlorobenzene ug/L 400 102 60-140110 7400ND408 440
1,2,3-Trichloropropane ug/L 400 103 60-140109 6400ND411 435
1,2,4-Trichlorobenzene ug/L 400 110 60-140117 6400ND440 467
1,2,4-Trimethylbenzene ug/L 400 110 60-140114 2400353793 809
1,2-Dibromo-3-chloropropane ug/L 400 98 60-140104 7400ND390 417
1,2-Dibromoethane (EDB)ug/L 400 110 60-140113 3400ND438 453
1,2-Dichlorobenzene ug/L 400 110 60-140116 5400ND440 464
1,2-Dichloroethane ug/L 400 115 60-140111 2400321781 763
1,2-Dichloropropane ug/L 400 119 60-140120 1400ND483 486
1,3,5-Trimethylbenzene ug/L 400 126 60-140131 4400ND505 524
1,3-Dichlorobenzene ug/L 400 110 60-140115 4400ND441 459
1,3-Dichloropropane ug/L 400 112 60-140114 1400ND450 455
1,4-Dichlorobenzene ug/L 400 110 60-140115 4400ND439 458
2,2-Dichloropropane ug/L 400 114 60-140115 1400ND456 461
2-Chlorotoluene ug/L 400 99 60-140108 8400ND397 430
4-Chlorotoluene ug/L 400 112 60-140118 5400ND449 472
Benzene ug/L 400 112 60-14067 540031203570 3390
Bromobenzene ug/L 400 115 60-140117 2400ND459 468
Bromochloromethane ug/L 400 122 60-140119 2400ND487 476
Bromodichloromethane ug/L 400 109 60-140109 1400ND437 434
Bromoform ug/L 400 103 60-140104 2400ND411 418
Bromomethane ug/L 400 84 60-14090 8400ND334 361
Carbon tetrachloride ug/L 400 101 60-140105 3400ND406 420
Chlorobenzene ug/L 400 112 60-140115 2400ND450 459
Chloroethane ug/L 400 129 60-140129 0400ND516 517
Chloroform ug/L 400 109 60-140108 1400ND440 437
Chloromethane ug/L 400 125 60-140124 0400ND498 497
cis-1,2-Dichloroethene ug/L 400 124 60-140121 2400ND495 484
cis-1,3-Dichloropropene ug/L 400 114 60-140115 1400ND454 459
Dibromochloromethane ug/L 400 105 60-140110 5400ND419 440
Dibromomethane ug/L 400 113 60-140113 0400ND450 452
Dichlorodifluoromethane ug/L 400 96 60-14096 0400ND384 385
Diisopropyl ether ug/L 400 125 60-140123 140025.7 524 517
Ethanol ug/L 16000 83 60-14099 1716000ND13300 15800
Ethylbenzene ug/L 400 108 60-140105 14005851020 1000
Hexachloro-1,3-butadiene ug/L 400 111 60-140120 7400ND444 479
Isopropylbenzene (Cumene) ug/L 400 114 60-140115 140029.2 484 491
m&p-Xylene ug/L 800 107 60-140105 180010001860 1840
Methyl-tert-butyl ether ug/L 400 109 60-140108 1400ND436 434
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2156826MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364039006
2156827
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 400 134 60-140136 2400ND537 546
n-Butylbenzene ug/L 400 115 60-140122 6400ND459 488
n-Propylbenzene ug/L 400 125 60-140132 5400ND499 527
Naphthalene ug/L 400 93 60-140100 4400253625 652
o-Xylene ug/L 400 109 60-140107 1400423859 851
sec-Butylbenzene ug/L 400 115 60-140121 6400ND459 486
Styrene ug/L 400 114 60-140116 2400ND454 465
tert-Butylbenzene ug/L 400 94 60-140100 6400ND376 399
Tetrachloroethene ug/L 400 113 60-140114 1400ND451 457
Toluene ug/L 400 117 60-140117 040013.1 481 479
trans-1,2-Dichloroethene ug/L 400 125 60-140124 0400ND499 497
trans-1,3-Dichloropropene ug/L 400 107 60-140106 0400ND427 426
Trichloroethene ug/L 400 115 60-140114 1400ND458 454
Trichlorofluoromethane ug/L 400 115 60-140116 1400ND459 465
Vinyl chloride ug/L 400 130 60-140130 0400ND520 521
1,2-Dichloroethane-d4 (S)%98 70-13092
4-Bromofluorobenzene (S)%97 70-13094
Toluene-d8 (S)%103 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389120
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92364508001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2158521
Associated Lab Samples:92364508001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/01/17 19:59
1,1,1-Trichloroethane ug/L ND 0.50 12/01/17 19:59
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/01/17 19:59
1,1,2-Trichloroethane ug/L ND 0.50 12/01/17 19:59
1,1-Dichloroethane ug/L ND 0.50 12/01/17 19:59
1,1-Dichloroethene ug/L ND 0.50 12/01/17 19:59
1,1-Dichloropropene ug/L ND 0.50 12/01/17 19:59
1,2,3-Trichlorobenzene ug/L ND 2.0 12/01/17 19:59
1,2,3-Trichloropropane ug/L ND 0.50 12/01/17 19:59
1,2,4-Trichlorobenzene ug/L ND 2.0 12/01/17 19:59
1,2,4-Trimethylbenzene ug/L ND 0.50 12/01/17 19:59
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/01/17 19:59
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/01/17 19:59
1,2-Dichlorobenzene ug/L ND 0.50 12/01/17 19:59
1,2-Dichloroethane ug/L ND 0.50 12/01/17 19:59
1,2-Dichloropropane ug/L ND 0.50 12/01/17 19:59
1,3,5-Trimethylbenzene ug/L ND 0.50 12/01/17 19:59
1,3-Dichlorobenzene ug/L ND 0.50 12/01/17 19:59
1,3-Dichloropropane ug/L ND 0.50 12/01/17 19:59
1,4-Dichlorobenzene ug/L ND 0.50 12/01/17 19:59
2,2-Dichloropropane ug/L ND 0.50 12/01/17 19:59
2-Chlorotoluene ug/L ND 0.50 12/01/17 19:59
4-Chlorotoluene ug/L ND 0.50 12/01/17 19:59
Benzene ug/L ND 0.50 12/01/17 19:59
Bromobenzene ug/L ND 0.50 12/01/17 19:59
Bromochloromethane ug/L ND 0.50 12/01/17 19:59
Bromodichloromethane ug/L ND 0.50 12/01/17 19:59
Bromoform ug/L ND 0.50 12/01/17 19:59
Bromomethane ug/L ND 5.0 12/01/17 19:59
Carbon tetrachloride ug/L ND 0.50 12/01/17 19:59
Chlorobenzene ug/L ND 0.50 12/01/17 19:59
Chloroethane ug/L ND 1.0 12/01/17 19:59
Chloroform ug/L ND 0.50 12/01/17 19:59
Chloromethane ug/L ND 1.0 12/01/17 19:59
cis-1,2-Dichloroethene ug/L ND 0.50 12/01/17 19:59
cis-1,3-Dichloropropene ug/L ND 0.50 12/01/17 19:59
Dibromochloromethane ug/L ND 0.50 12/01/17 19:59
Dibromomethane ug/L ND 0.50 12/01/17 19:59
Dichlorodifluoromethane ug/L ND 0.50 12/01/17 19:59
Diisopropyl ether ug/L ND 0.50 12/01/17 19:59
Ethanol ug/L ND 200 12/01/17 19:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2158521
Associated Lab Samples:92364508001
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 12/01/17 19:59
Hexachloro-1,3-butadiene ug/L ND 2.0 12/01/17 19:59
Isopropylbenzene (Cumene)ug/L ND 0.50 12/01/17 19:59
m&p-Xylene ug/L ND 1.0 12/01/17 19:59
Methyl-tert-butyl ether ug/L ND 0.50 12/01/17 19:59
Methylene Chloride ug/L ND 2.0 12/01/17 19:59
n-Butylbenzene ug/L ND 0.50 12/01/17 19:59
n-Propylbenzene ug/L ND 0.50 12/01/17 19:59
Naphthalene ug/L ND 2.0 12/01/17 19:59
o-Xylene ug/L ND 0.50 12/01/17 19:59
sec-Butylbenzene ug/L ND 0.50 12/01/17 19:59
Styrene ug/L ND 0.50 12/01/17 19:59
tert-Butylbenzene ug/L ND 0.50 12/01/17 19:59
Tetrachloroethene ug/L ND 0.50 12/01/17 19:59
Toluene ug/L ND 0.50 12/01/17 19:59
trans-1,2-Dichloroethene ug/L ND 0.50 12/01/17 19:59
trans-1,3-Dichloropropene ug/L ND 0.50 12/01/17 19:59
Trichloroethene ug/L ND 0.50 12/01/17 19:59
Trichlorofluoromethane ug/L ND 1.0 12/01/17 19:59
Vinyl chloride ug/L ND 1.0 12/01/17 19:59
1,2-Dichloroethane-d4 (S)%102 70-130 12/01/17 19:59
4-Bromofluorobenzene (S)%95 70-130 12/01/17 19:59
Toluene-d8 (S)%104 70-130 12/01/17 19:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2158522LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.050 106 60-140
1,1,1-Trichloroethane ug/L 52.350 105 60-140
1,1,2,2-Tetrachloroethane ug/L 49.050 98 60-140
1,1,2-Trichloroethane ug/L 52.250 104 60-140
1,1-Dichloroethane ug/L 54.750 109 60-140
1,1-Dichloroethene ug/L 56.250 112 60-140
1,1-Dichloropropene ug/L 51.750 103 60-140
1,2,3-Trichlorobenzene ug/L 47.050 94 60-140
1,2,3-Trichloropropane ug/L 49.150 98 60-140
1,2,4-Trichlorobenzene ug/L 51.150 102 60-140
1,2,4-Trimethylbenzene ug/L 51.750 103 60-140
1,2-Dibromo-3-chloropropane ug/L 50.850 102 60-140
1,2-Dibromoethane (EDB)ug/L 52.750 105 60-140
1,2-Dichlorobenzene ug/L 50.550 101 60-140
1,2-Dichloroethane ug/L 56.650 113 60-140
1,2-Dichloropropane ug/L 52.750 105 60-140
1,3,5-Trimethylbenzene ug/L 51.850 104 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2158522LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 50.150 100 60-140
1,3-Dichloropropane ug/L 52.050 104 60-140
1,4-Dichlorobenzene ug/L 49.950 100 60-140
2,2-Dichloropropane ug/L 50.450 101 60-140
2-Chlorotoluene ug/L 49.150 98 60-140
4-Chlorotoluene ug/L 50.450 101 60-140
Benzene ug/L 50.050 100 60-140
Bromobenzene ug/L 51.950 104 60-140
Bromochloromethane ug/L 54.950 110 60-140
Bromodichloromethane ug/L 51.950 104 60-140
Bromoform ug/L 55.550 111 60-140
Bromomethane ug/L 37.350 75 60-140
Carbon tetrachloride ug/L 49.650 99 60-140
Chlorobenzene ug/L 51.850 104 60-140
Chloroethane ug/L 60.950 122 60-140
Chloroform ug/L 50.050 100 60-140
Chloromethane ug/L 37.550 75 60-140
cis-1,2-Dichloroethene ug/L 55.650 111 60-140
cis-1,3-Dichloropropene ug/L 52.450 105 60-140
Dibromochloromethane ug/L 54.850 110 60-140
Dibromomethane ug/L 51.850 104 60-140
Dichlorodifluoromethane ug/L 40.650 81 60-140
Diisopropyl ether ug/L 57.650 115 60-140
Ethanol ug/L 23002000 115 60-140
Ethylbenzene ug/L 51.350 103 60-140
Hexachloro-1,3-butadiene ug/L 51.750 103 60-140
Isopropylbenzene (Cumene)ug/L 51.450 103 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 50.750 101 60-140
Methylene Chloride ug/L 58.650 117 60-140
n-Butylbenzene ug/L 52.450 105 60-140
n-Propylbenzene ug/L 51.050 102 60-140
Naphthalene ug/L 47.450 95 60-140
o-Xylene ug/L 51.450 103 60-140
sec-Butylbenzene ug/L 51.950 104 60-140
Styrene ug/L 52.050 104 60-140
tert-Butylbenzene ug/L 42.050 84 60-140
Tetrachloroethene ug/L 51.150 102 60-140
Toluene ug/L 50.950 102 60-140
trans-1,2-Dichloroethene ug/L 54.650 109 60-140
trans-1,3-Dichloropropene ug/L 50.250 100 60-140
Trichloroethene ug/L 51.050 102 60-140
Trichlorofluoromethane ug/L 51.150 102 60-140
Vinyl chloride ug/L 52.650 105 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2158523MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364508001
2158524
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 116 60-140118 120ND23.2 23.6
1,1,1-Trichloroethane ug/L 20 118 60-140118 020ND23.7 23.7
1,1,2,2-Tetrachloroethane ug/L 20 112 60-140113 120ND22.4 22.5
1,1,2-Trichloroethane ug/L 20 117 60-140118 120ND23.4 23.6
1,1-Dichloroethane ug/L 20 118 60-140118 020ND23.7 23.7
1,1-Dichloroethene ug/L 20 129 60-140125 420ND25.9 24.9
1,1-Dichloropropene ug/L 20 117 60-140119 220ND23.3 23.8
1,2,3-Trichlorobenzene ug/L 20 115 60-140111 320ND23.0 22.3
1,2,3-Trichloropropane ug/L 20 113 60-140114 120ND22.6 22.7
1,2,4-Trichlorobenzene ug/L 20 119 60-140119 020ND23.9 23.8
1,2,4-Trimethylbenzene ug/L 20 120 60-140120 020ND24.0 23.9
1,2-Dibromo-3-chloropropane ug/L 20 117 60-140115 220ND23.5 23.0
1,2-Dibromoethane (EDB)ug/L 20 117 60-140117 120ND23.3 23.5
1,2-Dichlorobenzene ug/L 20 117 60-140114 320ND23.4 22.8
1,2-Dichloroethane ug/L 20 118 60-140119 120ND23.6 23.8
1,2-Dichloropropane ug/L 20 117 60-140118 120ND23.4 23.6
1,3,5-Trimethylbenzene ug/L 20 122 60-140120 120ND24.3 24.1
1,3-Dichlorobenzene ug/L 20 116 60-140116 020ND23.2 23.1
1,3-Dichloropropane ug/L 20 118 60-140116 220ND23.6 23.1
1,4-Dichlorobenzene ug/L 20 115 60-140115 120ND23.0 22.9
2,2-Dichloropropane ug/L 20 117 60-140114 220ND23.3 22.7
2-Chlorotoluene ug/L 20 119 60-140116 220ND23.7 23.1
4-Chlorotoluene ug/L 20 119 60-140119 120ND23.9 23.7
Benzene ug/L 20 113 60-140112 120ND22.5 22.4
Bromobenzene ug/L 20 120 60-140120 020ND24.0 24.0
Bromochloromethane ug/L 20 122 60-140120 220ND24.3 24.0
Bromodichloromethane ug/L 20 112 60-140115 220ND22.4 22.9
Bromoform ug/L 20 121 60-140114 520ND24.1 22.9
Bromomethane ug/L 20 84 60-14083 120ND16.7 16.6
Carbon tetrachloride ug/L 20 115 60-140113 220ND23.1 22.5
Chlorobenzene ug/L 20 118 60-140117 120ND23.6 23.5
Chloroethane ug/L M12015860-140148 720ND31.7 29.5
Chloroform ug/L 20 109 60-140111 220ND21.8 22.2
Chloromethane ug/L 20 104 60-14079 2720ND20.8 15.8
cis-1,2-Dichloroethene ug/L 20 121 60-140123 220ND24.2 24.7
cis-1,3-Dichloropropene ug/L 20 114 60-140113 120ND22.8 22.7
Dibromochloromethane ug/L 20 119 60-140119 020ND23.8 23.8
Dibromomethane ug/L 20 115 60-140115 020ND23.0 23.0
Dichlorodifluoromethane ug/L 20 94 60-14092 120ND18.7 18.5
Diisopropyl ether ug/L 20 124 60-140124 020ND24.7 24.8
Ethanol ug/L M180015160-140156 3800ND1210 1240
Ethylbenzene ug/L 20 118 60-140117 220ND23.7 23.3
Hexachloro-1,3-butadiene ug/L 20 132 60-140126 520ND26.4 25.3
Isopropylbenzene (Cumene) ug/L 20 119 60-140117 120ND23.8 23.5
m&p-Xylene ug/L 40 118 60-140117 140ND47.3 46.7
Methyl-tert-butyl ether ug/L 20 111 60-140110 120ND22.2 22.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2158523MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364508001
2158524
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 120 60-140117 320ND24.1 23.4
n-Butylbenzene ug/L 20 123 60-140119 320ND24.6 23.8
n-Propylbenzene ug/L 20 121 60-140121 020ND24.3 24.2
Naphthalene ug/L 20 117 60-140114 220ND23.4 22.9
o-Xylene ug/L 20 117 60-140115 220ND23.4 23.0
sec-Butylbenzene ug/L 20 124 60-140122 220ND24.8 24.3
Styrene ug/L 20 115 60-140113 220ND23.0 22.6
tert-Butylbenzene ug/L 20 100 60-140100 020ND20.0 19.9
Tetrachloroethene ug/L 20 120 60-140117 220ND24.0 23.5
Toluene ug/L 20 116 60-140116 020ND23.3 23.2
trans-1,2-Dichloroethene ug/L 20 125 60-140120 420ND24.9 24.0
trans-1,3-Dichloropropene ug/L 20 110 60-140109 120ND22.0 21.8
Trichloroethene ug/L 20 118 60-140116 220ND23.6 23.2
Trichlorofluoromethane ug/L 20 117 60-140114 220ND23.4 22.9
Vinyl chloride ug/L 20 120 60-140119 120ND24.0 23.9
1,2-Dichloroethane-d4 (S)%97 70-13097
4-Bromofluorobenzene (S)%97 70-13096
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92364508
NCDEQ MT. HARMONY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92364508001 389120WSW-2 SM 6200B
92364508002 388822FIELD BLANK SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2017 04:02 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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