RA-613_3831_CA_LAB_20200831_POE Testing Eurofins J192418 Final Report

ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-192418-1
Laboratory Sample Delivery Group: NC0256 TF#3831
Client Project/Site: Billy Barber
For:
North Carolina Dept of Env Quality
NCDEQ-DWM-UST SECTION
1646 Mail Service Center
Raleigh, North Carolina 27699
Attn: Linda Blalock
Authorized for release by:
8/31/2020 4:00:10 PM
Isabel Enfinger, Project Mgmt. Assistant
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: North Carolina Dept of Env Quality
Project/Site: Billy Barber
Laboratory Job ID: 400-192418-1
SDG: NC0256 TF#3831
Page 2 of 20 Eurofins TestAmerica, Pensacola8/31/2020
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
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Case Narrative
Client: North Carolina Dept of Env Quality Job ID: 400-192418-1
Project/Site: Billy Barber SDG: NC0256 TF#3831
Job ID: 400-192418-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-192418-1
Comments
No additional comments.
Receipt
The samples were received on 8/21/2020 10:04 AM; the samples arrived in good condition, and where required, properly preserved and
on ice. The temperature of the cooler at receipt was 4.5º C.
GC/MS VOA
Method SM6200-B: The following sample was diluted to bring the concentration of target analytes within the calibration range: D1
(400-192418-1). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, PensacolaPage 3 of 20 8/31/2020
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Detection Summary
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Client Sample ID: D1 Lab Sample ID: 400-192418-1
Methyl tert-butyl ether
RL
2.0 ug/L
MDLAnalyteResultQualifier Unit Dil Fac D Method Prep Type
Total/NA2540SM6200-B
Isopropyl ether 2.0 ug/L Total/NA211SM6200-B
Client Sample ID: D3 Lab Sample ID: 400-192418-2
No Detections.
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Method Summary
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Method Method Description LaboratoryProtocol
SMSM6200-B Volatile Organic Compounds TAL PEN
SW8465030BPurge and Trap TAL PEN
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Sample Summary
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID
400-192418-1 D1 Water 08/18/20 13:20 08/21/20 10:04
400-192418-2 D3 Water 08/18/20 13:22 08/21/20 10:04
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Lab Sample ID: 400-192418-1Client Sample ID: D1
Matrix: WaterDate Collected: 08/18/20 13:20
Date Received: 08/21/20 10:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1,1,1-Trichloroethane <2.0 2.0 ug/L 08/28/20 18:08 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 ug/L 08/28/20 18:08 21,1,2,2-Tetrachloroethane <2.0
2.0 ug/L 08/28/20 18:08 21,1,2-Trichloro-1,2,2-trifluoroethane <2.0
10 ug/L 08/28/20 18:08 21,1,2-Trichloroethane <10
2.0 ug/L 08/28/20 18:08 21,1-Dichloroethane <2.0
2.0 ug/L 08/28/20 18:08 21,1-Dichloroethene <2.0
2.0 ug/L 08/28/20 18:08 21,2,3-Trichlorobenzene <2.0
2.0 ug/L 08/28/20 18:08 21,2,4-Trichlorobenzene <2.0
2.0 ug/L 08/28/20 18:08 21,2,4-Trimethylbenzene <2.0
10 ug/L 08/28/20 18:08 21,2-Dibromo-3-Chloropropane <10
2.0 ug/L 08/28/20 18:08 21,2-Dichlorobenzene <2.0
2.0 ug/L 08/28/20 18:08 21,2-Dichloroethane <2.0
2.0 ug/L 08/28/20 18:08 21,2-Dichloropropane <2.0
2.0 ug/L 08/28/20 18:08 21,3,5-Trimethylbenzene <2.0
2.0 ug/L 08/28/20 18:08 21,3-Dichlorobenzene <2.0
2.0 ug/L 08/28/20 18:08 21,4-Dichlorobenzene <2.0
50 ug/L 08/28/20 18:08 22-Butanone (MEK)<50
50 ug/L 08/28/20 18:08 22-Hexanone <50
50 ug/L 08/28/20 18:08 24-Methyl-2-pentanone (MIBK)<50
50 ug/L 08/28/20 18:08 2Acetone<50
2.0 ug/L 08/28/20 18:08 2Benzene<2.0
10 ug/L 08/28/20 18:08 2Bromoform<10
2.0 ug/L 08/28/20 18:08 2Bromomethane<2.0
2.0 ug/L 08/28/20 18:08 2Carbon disulfide <2.0
2.0 ug/L 08/28/20 18:08 2Carbon tetrachloride <2.0
2.0 ug/L 08/28/20 18:08 2Chlorobenzene<2.0
2.0 ug/L 08/28/20 18:08 2Chlorobromomethane<2.0
2.0 ug/L 08/28/20 18:08 2Chlorodibromomethane<2.0
2.0 ug/L 08/28/20 18:08 2Chloroethane<2.0
2.0 ug/L 08/28/20 18:08 2Chloroform<2.0
2.0 ug/L 08/28/20 18:08 2Chloromethane<2.0
2.0 ug/L 08/28/20 18:08 2cis-1,2-Dichloroethene <2.0
10 ug/L 08/28/20 18:08 2cis-1,3-Dichloropropene <10
10 ug/L 08/28/20 18:08 2Dibromomethane<10
2.0 ug/L 08/28/20 18:08 2Dichlorobromomethane<2.0
2.0 ug/L 08/28/20 18:08 2Dichlorodifluoromethane<2.0
2.0 ug/L 08/28/20 18:08 2Ethylbenzene<2.0
2.0 ug/L 08/28/20 18:08 2Ethylene Dibromide <2.0
2.0 ug/L 08/28/20 18:08 2Methyl tert-butyl ether 540
10 ug/L 08/28/20 18:08 2Methylene Chloride <10
10 ug/L 08/28/20 18:08 2m-Xylene & p-Xylene <10
2.0 ug/L 08/28/20 18:08 2Naphthalene<2.0
10 ug/L 08/28/20 18:08 2o-Xylene <10
2.0 ug/L 08/28/20 18:08 2Styrene<2.0
2.0 ug/L 08/28/20 18:08 2Tetrachloroethene<2.0
2.0 ug/L 08/28/20 18:08 2Toluene<2.0
2.0 ug/L 08/28/20 18:08 2Trichloroethene<2.0
2.0 ug/L 08/28/20 18:08 2Trichlorofluoromethane<2.0
2.0 ug/L 08/28/20 18:08 2Vinyl chloride <2.0
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Lab Sample ID: 400-192418-1Client Sample ID: D1
Matrix: WaterDate Collected: 08/18/20 13:20
Date Received: 08/21/20 10:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Xylenes, Total <20 20 ug/L 08/28/20 18:08 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 ug/L 08/28/20 18:08 2Isopropyl ether 11
4-Bromofluorobenzene 94 78-118 08/28/20 18:08 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 105 08/28/20 18:08 281-121
Toluene-d8 (Surr)96 08/28/20 18:08 280-120
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Lab Sample ID: 400-192418-2Client Sample ID: D3
Matrix: WaterDate Collected: 08/18/20 13:22
Date Received: 08/21/20 10:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1,1,1-Trichloroethane <1.0 1.0 ug/L 08/28/20 16:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 ug/L 08/28/20 16:49 11,1,2,2-Tetrachloroethane <1.0
1.0 ug/L 08/28/20 16:49 11,1,2-Trichloro-1,2,2-trifluoroethane <1.0
5.0 ug/L 08/28/20 16:49 11,1,2-Trichloroethane <5.0
1.0 ug/L 08/28/20 16:49 11,1-Dichloroethane <1.0
1.0 ug/L 08/28/20 16:49 11,1-Dichloroethene <1.0
1.0 ug/L 08/28/20 16:49 11,2,3-Trichlorobenzene <1.0
1.0 ug/L 08/28/20 16:49 11,2,4-Trichlorobenzene <1.0
1.0 ug/L 08/28/20 16:49 11,2,4-Trimethylbenzene <1.0
5.0 ug/L 08/28/20 16:49 11,2-Dibromo-3-Chloropropane <5.0
1.0 ug/L 08/28/20 16:49 11,2-Dichlorobenzene <1.0
1.0 ug/L 08/28/20 16:49 11,2-Dichloroethane <1.0
1.0 ug/L 08/28/20 16:49 11,2-Dichloropropane <1.0
1.0 ug/L 08/28/20 16:49 11,3,5-Trimethylbenzene <1.0
1.0 ug/L 08/28/20 16:49 11,3-Dichlorobenzene <1.0
1.0 ug/L 08/28/20 16:49 11,4-Dichlorobenzene <1.0
25 ug/L 08/28/20 16:49 12-Butanone (MEK)<25
25 ug/L 08/28/20 16:49 12-Hexanone <25
25 ug/L 08/28/20 16:49 14-Methyl-2-pentanone (MIBK)<25
25 ug/L 08/28/20 16:49 1Acetone<25
1.0 ug/L 08/28/20 16:49 1Benzene<1.0
5.0 ug/L 08/28/20 16:49 1Bromoform<5.0
1.0 ug/L 08/28/20 16:49 1Bromomethane<1.0
1.0 ug/L 08/28/20 16:49 1Carbon disulfide <1.0
1.0 ug/L 08/28/20 16:49 1Carbon tetrachloride <1.0
1.0 ug/L 08/28/20 16:49 1Chlorobenzene<1.0
1.0 ug/L 08/28/20 16:49 1Chlorobromomethane<1.0
1.0 ug/L 08/28/20 16:49 1Chlorodibromomethane<1.0
1.0 ug/L 08/28/20 16:49 1Chloroethane<1.0
1.0 ug/L 08/28/20 16:49 1Chloroform<1.0
1.0 ug/L 08/28/20 16:49 1Chloromethane<1.0
1.0 ug/L 08/28/20 16:49 1cis-1,2-Dichloroethene <1.0
5.0 ug/L 08/28/20 16:49 1cis-1,3-Dichloropropene <5.0
5.0 ug/L 08/28/20 16:49 1Dibromomethane<5.0
1.0 ug/L 08/28/20 16:49 1Dichlorobromomethane<1.0
1.0 ug/L 08/28/20 16:49 1Dichlorodifluoromethane<1.0
1.0 ug/L 08/28/20 16:49 1Ethylbenzene<1.0
1.0 ug/L 08/28/20 16:49 1Ethylene Dibromide <1.0
1.0 ug/L 08/28/20 16:49 1Methyl tert-butyl ether <1.0
5.0 ug/L 08/28/20 16:49 1Methylene Chloride <5.0
5.0 ug/L 08/28/20 16:49 1m-Xylene & p-Xylene <5.0
1.0 ug/L 08/28/20 16:49 1Naphthalene<1.0
5.0 ug/L 08/28/20 16:49 1o-Xylene <5.0
1.0 ug/L 08/28/20 16:49 1Styrene<1.0
1.0 ug/L 08/28/20 16:49 1Tetrachloroethene<1.0
1.0 ug/L 08/28/20 16:49 1Toluene<1.0
1.0 ug/L 08/28/20 16:49 1Trichloroethene<1.0
1.0 ug/L 08/28/20 16:49 1Trichlorofluoromethane<1.0
1.0 ug/L 08/28/20 16:49 1Vinyl chloride <1.0
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Lab Sample ID: 400-192418-2Client Sample ID: D3
Matrix: WaterDate Collected: 08/18/20 13:22
Date Received: 08/21/20 10:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Xylenes, Total <10 10 ug/L 08/28/20 16:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 ug/L 08/28/20 16:49 1Isopropyl ether <1.0
4-Bromofluorobenzene 94 78-118 08/28/20 16:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 105 08/28/20 16:49 181-121
Toluene-d8 (Surr)97 08/28/20 16:49 180-120
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Method: SM6200-B - Volatile Organic Compounds
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (78-118)(81-121)(80-120)
BFB DBFM TOL
95 104 96400-192416-A-2 MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
94 103 95400-192416-A-2 MSD Matrix Spike Duplicate
94 105 96400-192418-1 D1
94 105 97400-192418-2 D3
94 106 95LCS 400-501750/1002 Lab Control Sample
92 105 96MB 400-501750/4 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Eurofins TestAmerica, Pensacola
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Definitions/Glossary
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
GC/MS VOA
Analysis Batch: 501750
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-192418-1 D1 Total/NA
Water SM6200-B400-192418-2 D3 Total/NA
Water SM6200-BMB 400-501750/4 Method Blank Total/NA
Water SM6200-BLCS 400-501750/1002 Lab Control Sample Total/NA
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 400-501750/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501750
RL MDL
1,1,1-Trichloroethane <1.0 1.0 ug/L 08/28/20 08:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 1.0 ug/L 08/28/20 08:34 11,1,2,2-Tetrachloroethane
<1.0 1.0 ug/L 08/28/20 08:34 11,1,2-Trichloro-1,2,2-trifluoroethane
<5.0 5.0 ug/L 08/28/20 08:34 11,1,2-Trichloroethane
<1.0 1.0 ug/L 08/28/20 08:34 11,1-Dichloroethane
<1.0 1.0 ug/L 08/28/20 08:34 11,1-Dichloroethene
<1.0 1.0 ug/L 08/28/20 08:34 11,2,3-Trichlorobenzene
<1.0 1.0 ug/L 08/28/20 08:34 11,2,4-Trichlorobenzene
<1.0 1.0 ug/L 08/28/20 08:34 11,2,4-Trimethylbenzene
<5.0 5.0 ug/L 08/28/20 08:34 11,2-Dibromo-3-Chloropropane
<1.0 1.0 ug/L 08/28/20 08:34 11,2-Dichlorobenzene
<1.0 1.0 ug/L 08/28/20 08:34 11,2-Dichloroethane
<1.0 1.0 ug/L 08/28/20 08:34 11,2-Dichloropropane
<1.0 1.0 ug/L 08/28/20 08:34 11,3,5-Trimethylbenzene
<1.0 1.0 ug/L 08/28/20 08:34 11,3-Dichlorobenzene
<1.0 1.0 ug/L 08/28/20 08:34 11,4-Dichlorobenzene
<25 25 ug/L 08/28/20 08:34 12-Butanone (MEK)
<25 25 ug/L 08/28/20 08:34 12-Hexanone
<25 25 ug/L 08/28/20 08:34 14-Methyl-2-pentanone (MIBK)
<25 25 ug/L 08/28/20 08:34 1Acetone
<1.0 1.0 ug/L 08/28/20 08:34 1Benzene
<5.0 5.0 ug/L 08/28/20 08:34 1Bromoform
<1.0 1.0 ug/L 08/28/20 08:34 1Bromomethane
<1.0 1.0 ug/L 08/28/20 08:34 1Carbon disulfide
<1.0 1.0 ug/L 08/28/20 08:34 1Carbon tetrachloride
<1.0 1.0 ug/L 08/28/20 08:34 1Chlorobenzene
<1.0 1.0 ug/L 08/28/20 08:34 1Chlorobromomethane
<1.0 1.0 ug/L 08/28/20 08:34 1Chlorodibromomethane
<1.0 1.0 ug/L 08/28/20 08:34 1Chloroethane
<1.0 1.0 ug/L 08/28/20 08:34 1Chloroform
<1.0 1.0 ug/L 08/28/20 08:34 1Chloromethane
<1.0 1.0 ug/L 08/28/20 08:34 1cis-1,2-Dichloroethene
<5.0 5.0 ug/L 08/28/20 08:34 1cis-1,3-Dichloropropene
<5.0 5.0 ug/L 08/28/20 08:34 1Dibromomethane
<1.0 1.0 ug/L 08/28/20 08:34 1Dichlorobromomethane
<1.0 1.0 ug/L 08/28/20 08:34 1Dichlorodifluoromethane
<1.0 1.0 ug/L 08/28/20 08:34 1Ethylbenzene
<1.0 1.0 ug/L 08/28/20 08:34 1Ethylene Dibromide
<1.0 1.0 ug/L 08/28/20 08:34 1Methyl tert-butyl ether
<5.0 5.0 ug/L 08/28/20 08:34 1Methylene Chloride
<5.0 5.0 ug/L 08/28/20 08:34 1m-Xylene & p-Xylene
<1.0 1.0 ug/L 08/28/20 08:34 1Naphthalene
<5.0 5.0 ug/L 08/28/20 08:34 1o-Xylene
<1.0 1.0 ug/L 08/28/20 08:34 1Styrene
<1.0 1.0 ug/L 08/28/20 08:34 1Tetrachloroethene
<1.0 1.0 ug/L 08/28/20 08:34 1Toluene
<1.0 1.0 ug/L 08/28/20 08:34 1Trichloroethene
<1.0 1.0 ug/L 08/28/20 08:34 1Trichlorofluoromethane
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-501750/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501750
RL MDL
Vinyl chloride <1.0 1.0 ug/L 08/28/20 08:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<10 10 ug/L 08/28/20 08:34 1Xylenes, Total
<1.0 1.0 ug/L 08/28/20 08:34 1Isopropyl ether
4-Bromofluorobenzene 92 78-118 08/28/20 08:34 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
105 08/28/20 08:34 1Dibromofluoromethane81-121
96 08/28/20 08:34 1Toluene-d8 (Surr)80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-501750/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501750
1,1,1-Trichloroethane 50.0 46.7 ug/L 93 68-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2,2-Tetrachloroethane 50.0 52.7 ug/L 105 70-131
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 51.8 ug/L 104 60-139
1,1,2-Trichloroethane 50.0 54.0 ug/L 108 70-130
1,1-Dichloroethane 50.0 50.3 ug/L 101 70-130
1,1-Dichloroethene 50.0 48.7 ug/L 97 63-134
1,2,3-Trichlorobenzene 50.0 59.6 ug/L 119 60-138
1,2,4-Trichlorobenzene 50.0 59.3 ug/L 119 60-140
1,2,4-Trimethylbenzene 50.0 53.8 ug/L 108 70-130
1,2-Dibromo-3-Chloropropane 50.0 46.8 ug/L 94 54-135
1,2-Dichlorobenzene 50.0 55.8 ug/L 112 67-130
1,2-Dichloroethane 50.0 53.8 ug/L 108 69-130
1,2-Dichloropropane 50.0 50.5 ug/L 101 70-130
1,3,5-Trimethylbenzene 50.0 53.8 ug/L 108 69-130
1,3-Dichlorobenzene 50.0 56.1 ug/L 112 70-130
1,4-Dichlorobenzene 50.0 56.4 ug/L 113 70-130
2-Butanone (MEK)200 224 ug/L 112 61-145
2-Hexanone 200 205 ug/L 103 65-137
4-Methyl-2-pentanone (MIBK)200 214 ug/L 107 69-138
Acetone 200 220 ug/L 110 43-160
Benzene 50.0 51.4 ug/L 103 70-130
Bromoform 50.0 47.1 ug/L 94 57-140
Bromomethane 100 99.8 ug/L 100 10-160
Carbon disulfide 50.0 45.6 ug/L 91 61-137
Carbon tetrachloride 50.0 40.8 ug/L 82 61-137
Chlorobenzene 50.0 53.8 ug/L 108 70-130
Chlorobromomethane 50.0 57.5 ug/L 115 70-130
Chlorodibromomethane 50.0 51.9 ug/L 104 67-135
Chloroethane 100 94.3 ug/L 94 55-141
Chloroform 50.0 53.1 ug/L 106 69-130
Chloromethane 100 80.2 ug/L 80 58-137
cis-1,2-Dichloroethene 50.0 49.1 ug/L 98 68-130
cis-1,3-Dichloropropene 50.0 47.8 ug/L 96 69-132
Dibromomethane 50.0 56.6 ug/L 113 70-130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-192418-1Client: North Carolina Dept of Env Quality
SDG: NC0256 TF#3831Project/Site: Billy Barber
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-501750/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501750
Dichlorobromomethane 50.0 52.3 ug/L 105 67-133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dichlorodifluoromethane 100 65.5 ug/L 65 41-146
Ethylbenzene 50.0 52.8 ug/L 106 70-130
Ethylene Dibromide 50.0 54.6 ug/L 109 70-130
Methyl tert-butyl ether 50.0 49.5 ug/L 99 66-130
Methylene Chloride 50.0 52.0 ug/L 104 66-135
m-Xylene & p-Xylene 50.0 52.7 ug/L 105 70-130
Naphthalene 50.0 58.5 ug/L 117 47-149
o-Xylene 50.0 53.3 ug/L 107 70-130
Styrene 50.0 54.3 ug/L 109 70-130
Tetrachloroethene 50.0 54.1 ug/L 108 65-130
Toluene 50.0 50.0 ug/L 100 70-130
Trichloroethene 50.0 56.5 ug/L 113 70-130
Trichlorofluoromethane 100 107 ug/L 107 65-138
Vinyl chloride 100 88.1 ug/L 88 59-136
Xylenes, Total 100 106 ug/L 106 70-130
Isopropyl ether 50.0 42.3 ug/L 85 64-132
4-Bromofluorobenzene 78 -118
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
106Dibromofluoromethane 81 -121
95Toluene-d8 (Surr)80 -120
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: North Carolina Dept of Env Quality Job ID: 400-192418-1
Project/Site: Billy Barber SDG: NC0256 TF#3831
Client Sample ID: D1 Lab Sample ID: 400-192418-1
Matrix: WaterDate Collected: 08/18/20 13:20
Date Received: 08/21/20 10:04
Analysis SM6200-B WPD08/28/20 18:082 TAL PEN501750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: D3 Lab Sample ID: 400-192418-2
Matrix: WaterDate Collected: 08/18/20 13:22
Date Received: 08/21/20 10:04
Analysis SM6200-B WPD08/28/20 16:491 TAL PEN501750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-501750/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD08/28/20 08:341 TAL PEN501750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-501750/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD08/28/20 07:461 TAL PEN501750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Accreditation/Certification Summary
Client: North Carolina Dept of Env Quality Job ID: 400-192418-1
Project/Site: Billy Barber SDG: NC0256 TF#3831
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)314State 12-31-20
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
SM6200-B Water 1,1,2-Trichloro-1,2,2-trifluoroethane
SM6200-B Water 2-Butanone (MEK)
SM6200-B Water 2-Hexanone
SM6200-B Water 4-Methyl-2-pentanone (MIBK)
SM6200-B Water Acetone
SM6200-B Water Carbon disulfide
SM6200-B Water Isopropyl ether
SM6200-B Water Xylenes, Total
Eurofins TestAmerica, Pensacola
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Login Sample Receipt Checklist
Client: North Carolina Dept of Env Quality Job Number: 400-192418-1
SDG Number: NC0256 TF#3831
Login Number: 192418
Question Answer Comment
Creator: Conrady, Hank W
List Source: Eurofins TestAmerica, Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.4.5°C IR-8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Pensacola
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