RA-613_3831_CA_LAB_20180831_Shealy Labs ProAct MaintReport

SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
NCDEQ-DWM-UST Section
1646 Mail Service Ctr.
Raleigh,NC 27699
Attention:Linda Blalock
Project Name:Billy Barber
Project Number:NC0256 TF#3831
Lot Number:TH16018
Date Completed:08/28/2018
08/31/2018 6:27 PM
Approved and released by:
Project Manager:Nisreen Saikaly
Page 1 of 18
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
NCDEQ-DWM-UST Section
Lot Number:TH16018
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Volatile Organic Compounds
Reanalysis of the following sample was performed outside of the analytical holding time:TH16018-001.
The sample was initially analyzed within hold time.Methyl-tert-butyl ether (MTBE)was over calibration
range.The sample was reanalyzed (approximately 14 hours out of hold time)for MTBE.The data has
been reported.
Page 2 of 18
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
NCDEQ-DWM-UST Section
Lot Number: TH16018

Project Name: Billy Barber
Project Number: NC0256 TF#3831
Sample Number Sample ID Matrix Date Sampled Date Received
001 08/13/2018 1215D1Aqueous 08/16/2018
002 08/13/2018 1220D3Aqueous 08/16/2018
(2 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 18
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
NCDEQ-DWM-UST Section
Lot Number: TH16018

Project Name: Billy Barber
Project Number: NC0256 TF#3831
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 D1 Aqueous 1,2-Dichloroethane SM 6200B-0.70 ug/L 5
001 D1 Aqueous Diisopropyl ether (IPE)SM 6200B-7.3 ug/L 5
001 D1 Aqueous Methyl tertiary butyl ether SM 6200B-260 H ug/L 5
(3 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 18
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D1
TH16018-001
08/13/2018 1215
08/16/2018
Aqueous
Project Name: Billy Barber
Project Number: NC0256 TF#3831
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/26/2018 1305 JJG 81915
2 SM 6200B-SM 6200B-2011 5 08/28/2018 0157 KGT 82070
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzene 71-43-2 SM 6200B-ND 1ug/L0.400.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.400.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.400.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.400.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.400.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.400.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.400.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.400.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.400.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.400.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.400.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.400.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.400.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.400.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.400.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 SM 6200B-0.70 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.400.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.400.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.400.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-7.3 1ug/L0.400.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.400.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.400.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.400.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.400.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-260 H 2ug/L2.02.5
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.400.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.400.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.400.50
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 18
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D1
TH16018-001
08/13/2018 1215
08/16/2018
Aqueous
Project Name: Billy Barber
Project Number: NC0256 TF#3831
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/26/2018 1305 JJG 81915
2 SM 6200B-SM 6200B-2011 5 08/28/2018 0157 KGT 82070
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Styrene 100-42-5 SM 6200B-ND 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.400.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.400.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.400.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.400.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.400.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.400.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.400.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.400.50
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 98 70-130 H 96 70-130
Bromofluorobenzene 104 70-130 H 101 70-130
Toluene-d8 106 70-130 H 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 18
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D3
TH16018-002
08/13/2018 1220
08/16/2018
Aqueous
Project Name: Billy Barber
Project Number: NC0256 TF#3831
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/26/2018 1326 JJG 81915
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzene 71-43-2 SM 6200B-ND 1ug/L0.400.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.400.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.400.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.400.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.400.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.400.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.400.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.400.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.400.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.400.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.400.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.400.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.400.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.400.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.400.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.400.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.400.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.400.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.400.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.400.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.400.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.400.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.400.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.400.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.400.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.400.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.400.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.400.50
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 18
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D3
TH16018-002
08/13/2018 1220
08/16/2018
Aqueous
Project Name: Billy Barber
Project Number: NC0256 TF#3831
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/26/2018 1326 JJG 81915
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.400.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.400.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.400.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.400.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.400.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.400.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.400.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.400.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 70-130
Bromofluorobenzene 102 70-130
Toluene-d8 104 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 18
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 18
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ81915-001
81915 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Benzene ND 08/26/2018 11170.50 0.40 ug/L1
Bromobenzene ND 08/26/2018 11170.50 0.40 ug/L1
Bromochloromethane ND 08/26/2018 11170.50 0.40 ug/L1
Bromodichloromethane ND 08/26/2018 11170.50 0.40 ug/L1
Bromoform ND 08/26/2018 11170.50 0.40 ug/L1
Bromomethane (Methyl bromide)ND 08/26/2018 11170.50 0.40 ug/L1
n-Butylbenzene ND 08/26/2018 11170.50 0.40 ug/L1
sec-Butylbenzene ND 08/26/2018 11170.50 0.40 ug/L1
tert-Butylbenzene ND 08/26/2018 11170.50 0.40 ug/L1
Carbon tetrachloride ND 08/26/2018 11170.50 0.40 ug/L1
Chlorobenzene ND 08/26/2018 11170.50 0.40 ug/L1
Chloroethane ND 08/26/2018 11170.50 0.40 ug/L1
Chloroform ND 08/26/2018 11170.50 0.40 ug/L1
Chloromethane (Methyl chloride)ND 08/26/2018 11170.50 0.40 ug/L1
2-Chlorotoluene ND 08/26/2018 11170.50 0.40 ug/L1
4-Chlorotoluene ND 08/26/2018 11170.50 0.40 ug/L1
Dibromochloromethane ND 08/26/2018 11170.50 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 08/26/2018 11170.50 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 08/26/2018 11170.50 0.40 ug/L1
1,2-Dichlorobenzene ND 08/26/2018 11170.50 0.40 ug/L1
1,3-Dichlorobenzene ND 08/26/2018 11170.50 0.40 ug/L1
1,4-Dichlorobenzene ND 08/26/2018 11170.50 0.40 ug/L1
Dichlorodifluoromethane ND 08/26/2018 11170.50 0.40 ug/L1
1,1-Dichloroethane ND 08/26/2018 11170.50 0.40 ug/L1
1,2-Dichloroethane ND 08/26/2018 11170.50 0.40 ug/L1
1,1-Dichloroethene ND 08/26/2018 11170.50 0.40 ug/L1
cis-1,2-Dichloroethene ND 08/26/2018 11170.50 0.40 ug/L1
trans-1,2-Dichloroethene ND 08/26/2018 11170.50 0.40 ug/L1
1,2-Dichloropropane ND 08/26/2018 11170.50 0.40 ug/L1
1,3-Dichloropropane ND 08/26/2018 11170.50 0.40 ug/L1
2,2-Dichloropropane ND 08/26/2018 11170.50 0.40 ug/L1
1,1-Dichloropropene ND 08/26/2018 11170.50 0.40 ug/L1
cis-1,3-Dichloropropene ND 08/26/2018 11170.50 0.40 ug/L1
trans-1,3-Dichloropropene ND 08/26/2018 11170.50 0.40 ug/L1
Diisopropyl ether (IPE)ND 08/26/2018 11170.50 0.40 ug/L1
Ethylbenzene ND 08/26/2018 11170.50 0.40 ug/L1
Hexachlorobutadiene ND 08/26/2018 11170.50 0.40 ug/L1
Isopropylbenzene (Cumene)ND 08/26/2018 11170.50 0.40 ug/L1
p-Isopropyltoluene (p-Cymene)ND 08/26/2018 11170.50 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 08/26/2018 11170.50 0.40 ug/L1
Methylene chloride ND 08/26/2018 11170.50 0.40 ug/L1
Naphthalene ND 08/26/2018 11170.50 0.40 ug/L1
n-Propylbenzene ND 08/26/2018 11170.50 0.40 ug/L1
Styrene ND 08/26/2018 11170.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 18
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ81915-001
81915 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
1,1,1,2-Tetrachloroethane ND 08/26/2018 11170.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 08/26/2018 11170.50 0.40 ug/L1
Tetrachloroethene ND 08/26/2018 11170.50 0.40 ug/L1
Toluene ND 08/26/2018 11170.50 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 08/26/2018 11170.50 0.40 ug/L1
1,2,3-Trichlorobenzene ND 08/26/2018 11170.50 0.40 ug/L1
1,2,4-Trichlorobenzene ND 08/26/2018 11170.50 0.40 ug/L1
1,1,1-Trichloroethane ND 08/26/2018 11170.50 0.40 ug/L1
1,1,2-Trichloroethane ND 08/26/2018 11170.50 0.40 ug/L1
Trichloroethene ND 08/26/2018 11170.50 0.40 ug/L1
Trichlorofluoromethane ND 08/26/2018 11170.50 0.40 ug/L1
1,2,3-Trichloropropane ND 08/26/2018 11170.50 0.40 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 08/26/2018 11170.50 0.40 ug/L1
1,2,4-Trimethylbenzene ND 08/26/2018 11170.50 0.40 ug/L1
Vinyl chloride ND 08/26/2018 11170.50 0.40 ug/L1
m+p - Xylenes ND 08/26/2018 11170.50 0.40 ug/L1
o - Xylenes ND 08/26/2018 11170.50 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 97 70-130
Bromofluorobenzene 103 70-130
Toluene-d8 106 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 18
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ81915-002
81915 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 50 08/26/2018 09421015070-1301
Bromobenzene 51 08/26/2018 09421025070-1301
Bromochloromethane 50 08/26/2018 09421005070-1301
Bromodichloromethane 50 08/26/2018 09421005070-1301
Bromoform 50 08/26/2018 09421005070-1301
Bromomethane (Methyl bromide)49 08/26/2018 0942985060-1401
n-Butylbenzene 52 08/26/2018 09421055070-1301
sec-Butylbenzene 53 08/26/2018 09421075070-1301
tert-Butylbenzene 55 08/26/2018 09421095070-1301
Carbon tetrachloride 53 08/26/2018 09421055070-1301
Chlorobenzene 51 08/26/2018 09421035070-1301
Chloroethane 50 08/26/2018 09421005042-1631
Chloroform 49 08/26/2018 0942975070-1301
Chloromethane (Methyl chloride)49 08/26/2018 0942975020-1581
2-Chlorotoluene 52 08/26/2018 09421045070-1301
4-Chlorotoluene 52 08/26/2018 09421055070-1301
Dibromochloromethane 51 08/26/2018 09421015070-1301
1,2-Dibromoethane (EDB)49 08/26/2018 0942995070-1301
Dibromomethane (Methylene bromide)49 08/26/2018 0942985070-1301
1,2-Dichlorobenzene 50 08/26/2018 09421005070-1301
1,3-Dichlorobenzene 51 08/26/2018 09421025070-1301
1,4-Dichlorobenzene 50 08/26/2018 09421015070-1301
Dichlorodifluoromethane 48 08/26/2018 0942965060-1401
1,1-Dichloroethane 51 08/26/2018 09421035070-1301
1,2-Dichloroethane 50 08/26/2018 0942995070-1301
1,1-Dichloroethene 53 08/26/2018 09421055070-1301
cis-1,2-Dichloroethene 51 08/26/2018 09421025070-1301
trans-1,2-Dichloroethene 51 08/26/2018 09421025070-1301
1,2-Dichloropropane 51 08/26/2018 09421025070-1301
1,3-Dichloropropane 50 08/26/2018 09421015070-1301
2,2-Dichloropropane 51 08/26/2018 09421035070-1301
1,1-Dichloropropene 52 08/26/2018 09421055070-1301
cis-1,3-Dichloropropene 53 08/26/2018 09421075070-1301
trans-1,3-Dichloropropene 52 08/26/2018 09421045070-1301
Diisopropyl ether (IPE)51 08/26/2018 09421035070-1301
Ethylbenzene 52 08/26/2018 09421035070-1301
Hexachlorobutadiene 53 08/26/2018 09421065070-1301
Isopropylbenzene (Cumene)52 08/26/2018 09421045070-1301
p-Isopropyltoluene (p-Cymene)53 08/26/2018 09421075070-1301
Methyl tertiary butyl ether (MTBE)48 08/26/2018 0942965070-1301
Methylene chloride 49 08/26/2018 0942995070-1301
Naphthalene 45 08/26/2018 0942905050-1401
n-Propylbenzene 53 08/26/2018 09421065070-1301
Styrene 52 08/26/2018 09421045070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 18
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ81915-002
81915 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 50 08/26/2018 09421005070-1301
1,1,2,2-Tetrachloroethane 47 08/26/2018 0942955070-1301
Tetrachloroethene 51 08/26/2018 09421035070-1301
Toluene 52 08/26/2018 09421035070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 52 08/26/2018 09421045070-1301
1,2,3-Trichlorobenzene 47 08/26/2018 0942945070-1301
1,2,4-Trichlorobenzene 49 08/26/2018 0942985070-1301
1,1,1-Trichloroethane 52 08/26/2018 09421035070-1301
1,1,2-Trichloroethane 49 08/26/2018 0942985070-1301
Trichloroethene 51 08/26/2018 09421035070-1301
Trichlorofluoromethane 51 08/26/2018 09421015060-1401
1,2,3-Trichloropropane 48 08/26/2018 0942965070-1301
1,3,5-Trimethylbenzene (Mesitylene)53 08/26/2018 09421065070-1301
1,2,4-Trimethylbenzene 52 08/26/2018 09421055070-1301
Vinyl chloride 51 08/26/2018 09421025060-1401
m+p - Xylenes 52 08/26/2018 09421045070-1301
o - Xylenes 51 08/26/2018 09421035070-1301
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 96 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 18
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ82070-001
82070 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Methyl tertiary butyl ether (MTBE)ND 08/27/2018 21410.50 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 98 70-130
Bromofluorobenzene 104 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 18
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ82070-002
82070 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methyl tertiary butyl ether (MTBE)46 08/27/2018 2018925070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 18
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 18
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 17 of 18
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 18 of 18