RA-527_3327_CA_LAB_20150519_ESC Lab Report for WSWs

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Kevin Buchanan
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
Report Summary
Tuesday May 19, 2015
Report Number: L764375
Samples Received: 05/12/15
Client Project: 2140214.74
Description: Billy's Mini Mart
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By: ____________________________________
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TN002
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-01
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-1
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 11:00
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/l 6200B-1997 05/19/15 1
Acrolein BDL 50. ug/l 6200B-1997 05/19/15 1
Acrylonitrile BDL 10. ug/l 6200B-1997 05/19/15 1
Benzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromodichloromethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromoform BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromomethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chloroethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloroform BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloromethane BDL 2.5 ug/l 6200B-1997 05/19/15 1
2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Ethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Isopropylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
2-Butanone (MEK) BDL 10. ug/l 6200B-1997 05/19/15 1
Methylene Chloride BDL 5.0 ug/l 6200B-1997 05/19/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 2 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-01
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-1
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 11:00
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Naphthalene BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Propylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Styrene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Tetrachloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Toluene BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 05/19/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Vinyl chloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
o-Xylene BDL 1.0 ug/l 6200B-1997 05/19/15 1
m&p-Xylenes BDL 2.0 ug/l 6200B-1997 05/19/15 1
Surrogate Recovery
Toluene-d8 100. % Rec. 6200B-1997 05/19/15 1
Dibromofluoromethane 95.5 % Rec. 6200B-1997 05/19/15 1
a,a,a-Trifluorotoluene 103. % Rec. 6200B-1997 05/19/15 1
4-Bromofluorobenzene 105. % Rec. 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 05/19/15 17:00 Printed: 05/19/15 17:00
Page 3 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-02
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-2
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 16:45
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/l 6200B-1997 05/19/15 1
Acrolein BDL 50. ug/l 6200B-1997 05/19/15 1
Acrylonitrile BDL 10. ug/l 6200B-1997 05/19/15 1
Benzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromodichloromethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromoform BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromomethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chloroethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloroform BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloromethane BDL 2.5 ug/l 6200B-1997 05/19/15 1
2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Ethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Isopropylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
2-Butanone (MEK) BDL 10. ug/l 6200B-1997 05/19/15 1
Methylene Chloride BDL 5.0 ug/l 6200B-1997 05/19/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 4 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-02
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-2
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 16:45
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Naphthalene BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Propylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Styrene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Tetrachloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Toluene BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 05/19/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Vinyl chloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
o-Xylene BDL 1.0 ug/l 6200B-1997 05/19/15 1
m&p-Xylenes BDL 2.0 ug/l 6200B-1997 05/19/15 1
Surrogate Recovery
Toluene-d8 99.7 % Rec. 6200B-1997 05/19/15 1
Dibromofluoromethane 94.2 % Rec. 6200B-1997 05/19/15 1
a,a,a-Trifluorotoluene 104. % Rec. 6200B-1997 05/19/15 1
4-Bromofluorobenzene 105. % Rec. 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 05/19/15 17:00 Printed: 05/19/15 17:00
Page 5 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-03
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-3
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/06/15 08:32
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/l 6200B-1997 05/19/15 1
Acrolein BDL 50. ug/l 6200B-1997 05/19/15 1
Acrylonitrile BDL 10. ug/l 6200B-1997 05/19/15 1
Benzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromodichloromethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromoform BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromomethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chloroethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloroform BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloromethane BDL 2.5 ug/l 6200B-1997 05/19/15 1
2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Ethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Isopropylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
2-Butanone (MEK) BDL 10. ug/l 6200B-1997 05/19/15 1
Methylene Chloride BDL 5.0 ug/l 6200B-1997 05/19/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 6 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-03
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-3
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/06/15 08:32
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Naphthalene BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Propylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Styrene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Tetrachloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Toluene BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 05/19/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Vinyl chloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
o-Xylene BDL 1.0 ug/l 6200B-1997 05/19/15 1
m&p-Xylenes BDL 2.0 ug/l 6200B-1997 05/19/15 1
Surrogate Recovery
Toluene-d8 100. % Rec. 6200B-1997 05/19/15 1
Dibromofluoromethane 95.5 % Rec. 6200B-1997 05/19/15 1
a,a,a-Trifluorotoluene 104. % Rec. 6200B-1997 05/19/15 1
4-Bromofluorobenzene 103. % Rec. 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 05/19/15 17:00 Printed: 05/19/15 17:00
Page 7 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-04
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-4
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 10:45
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/l 6200B-1997 05/19/15 1
Acrolein BDL 50. ug/l 6200B-1997 05/19/15 1
Acrylonitrile BDL 10. ug/l 6200B-1997 05/19/15 1
Benzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromodichloromethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromoform BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromomethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chloroethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloroform BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloromethane BDL 2.5 ug/l 6200B-1997 05/19/15 1
2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Ethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Isopropylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
2-Butanone (MEK) BDL 10. ug/l 6200B-1997 05/19/15 1
Methylene Chloride BDL 5.0 ug/l 6200B-1997 05/19/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 8 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-04
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-4
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 10:45
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Naphthalene BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Propylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Styrene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Tetrachloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Toluene BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 05/19/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Vinyl chloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
o-Xylene BDL 1.0 ug/l 6200B-1997 05/19/15 1
m&p-Xylenes BDL 2.0 ug/l 6200B-1997 05/19/15 1
Surrogate Recovery
Toluene-d8 100. % Rec. 6200B-1997 05/19/15 1
Dibromofluoromethane 95.1 % Rec. 6200B-1997 05/19/15 1
a,a,a-Trifluorotoluene 104. % Rec. 6200B-1997 05/19/15 1
4-Bromofluorobenzene 103. % Rec. 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 05/19/15 17:00 Printed: 05/19/15 17:00
Page 9 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-05
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-5
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 10:10
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/l 6200B-1997 05/19/15 1
Acrolein BDL 50. ug/l 6200B-1997 05/19/15 1
Acrylonitrile BDL 10. ug/l 6200B-1997 05/19/15 1
Benzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromodichloromethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromoform BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromomethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chloroethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloroform BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloromethane BDL 2.5 ug/l 6200B-1997 05/19/15 1
2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Ethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Isopropylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
2-Butanone (MEK) BDL 10. ug/l 6200B-1997 05/19/15 1
Methylene Chloride BDL 5.0 ug/l 6200B-1997 05/19/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 10 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-05
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-5
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 10:10
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Naphthalene BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Propylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Styrene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Tetrachloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Toluene BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 05/19/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Vinyl chloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
o-Xylene BDL 1.0 ug/l 6200B-1997 05/19/15 1
m&p-Xylenes BDL 2.0 ug/l 6200B-1997 05/19/15 1
Surrogate Recovery
Toluene-d8 100. % Rec. 6200B-1997 05/19/15 1
Dibromofluoromethane 95.2 % Rec. 6200B-1997 05/19/15 1
a,a,a-Trifluorotoluene 105. % Rec. 6200B-1997 05/19/15 1
4-Bromofluorobenzene 104. % Rec. 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 05/19/15 17:00 Printed: 05/19/15 17:00
Page 11 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-06
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-6
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 10:25
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/l 6200B-1997 05/19/15 1
Acrolein BDL 50. ug/l 6200B-1997 05/19/15 1
Acrylonitrile BDL 10. ug/l 6200B-1997 05/19/15 1
Benzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromodichloromethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromoform BDL 1.0 ug/l 6200B-1997 05/19/15 1
Bromomethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Chloroethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloroform BDL 5.0 ug/l 6200B-1997 05/19/15 1
Chloromethane BDL 2.5 ug/l 6200B-1997 05/19/15 1
2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dibromomethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Ethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Isopropylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 05/19/15 1
2-Butanone (MEK) BDL 10. ug/l 6200B-1997 05/19/15 1
Methylene Chloride BDL 5.0 ug/l 6200B-1997 05/19/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 12 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Kevin Buchanan May 19,2015
Withers & Ravenel Eng. - Standard
115 MacKenan Drive
Cary, NC 27511
ESC Sample # : L764375-06
Date Received : May 12, 2015
Description : Billy's Mini Mart
Site ID :
Sample ID : WSW-6
Project # : 2140214.74
Collected By : P. Jones
Collection Date : 05/05/15 10:25
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 05/19/15 1
Naphthalene BDL 5.0 ug/l 6200B-1997 05/19/15 1
n-Propylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Styrene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Tetrachloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Toluene BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichloroethene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 05/19/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 05/19/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 05/19/15 1
Vinyl chloride BDL 1.0 ug/l 6200B-1997 05/19/15 1
o-Xylene BDL 1.0 ug/l 6200B-1997 05/19/15 1
m&p-Xylenes BDL 2.0 ug/l 6200B-1997 05/19/15 1
Surrogate Recovery
Toluene-d8 99.5 % Rec. 6200B-1997 05/19/15 1
Dibromofluoromethane 95.1 % Rec. 6200B-1997 05/19/15 1
a,a,a-Trifluorotoluene 104. % Rec. 6200B-1997 05/19/15 1
4-Bromofluorobenzene 103. % Rec. 6200B-1997 05/19/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
.
Reported: 05/19/15 17:00 Printed: 05/19/15 17:00
Page 13 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Laboratory Blank
Analyte Result Units % Rec Limit Batch Date Analyzed
1,1,1,2-Tetrachloroethane < .001 mg/l WG789089 05/19/15 10:22
1,1,1-Trichloroethane < .001 mg/l WG789089 05/19/15 10:22
1,1,2,2-Tetrachloroethane < .001 mg/l WG789089 05/19/15 10:22
1,1,2-Trichloroethane < .001 mg/l WG789089 05/19/15 10:22
1,1-Dichloroethane < .001 mg/l WG789089 05/19/15 10:22
1,1-Dichloroethene < .001 mg/l WG789089 05/19/15 10:22
1,1-Dichloropropene < .001 mg/l WG789089 05/19/15 10:22
1,2,3-Trichlorobenzene < .001 mg/l WG789089 05/19/15 10:22
1,2,3-Trichloropropane < .001 mg/l WG789089 05/19/15 10:22
1,2,4-Trichlorobenzene < .001 mg/l WG789089 05/19/15 10:22
1,2,4-Trimethylbenzene < .001 mg/l WG789089 05/19/15 10:22
1,2-Dibromo-3-Chloropropane < .005 mg/l WG789089 05/19/15 10:22
1,2-Dibromoethane < .001 mg/l WG789089 05/19/15 10:22
1,2-Dichlorobenzene < .001 mg/l WG789089 05/19/15 10:22
1,2-Dichloroethane < .001 mg/l WG789089 05/19/15 10:22
1,2-Dichloropropane < .001 mg/l WG789089 05/19/15 10:22
1,3,5-Trimethylbenzene < .001 mg/l WG789089 05/19/15 10:22
1,3-Dichlorobenzene < .001 mg/l WG789089 05/19/15 10:22
1,3-Dichloropropane < .001 mg/l WG789089 05/19/15 10:22
1,4-Dichlorobenzene < .001 mg/l WG789089 05/19/15 10:22
2,2-Dichloropropane < .001 mg/l WG789089 05/19/15 10:22
2-Butanone (MEK) < .01 mg/l WG789089 05/19/15 10:22
2-Chlorotoluene < .001 mg/l WG789089 05/19/15 10:22
4-Chlorotoluene < .001 mg/l WG789089 05/19/15 10:22
4-Methyl-2-pentanone (MIBK) < .01 mg/l WG789089 05/19/15 10:22
Acetone < .05 mg/l WG789089 05/19/15 10:22
Acrolein < .025 mg/l WG789089 05/19/15 10:22
Acrylonitrile < .01 mg/l WG789089 05/19/15 10:22
Benzene < .001 mg/l WG789089 05/19/15 10:22
Bromobenzene < .001 mg/l WG789089 05/19/15 10:22
Bromodichloromethane < .001 mg/l WG789089 05/19/15 10:22
Bromoform < .001 mg/l WG789089 05/19/15 10:22
Bromomethane < .005 mg/l WG789089 05/19/15 10:22
Carbon tetrachloride < .001 mg/l WG789089 05/19/15 10:22
Chlorobenzene < .001 mg/l WG789089 05/19/15 10:22
Chlorodibromomethane < .001 mg/l WG789089 05/19/15 10:22
Chloroethane < .005 mg/l WG789089 05/19/15 10:22
Chloroform < .005 mg/l WG789089 05/19/15 10:22
Chloromethane < .0025 mg/l WG789089 05/19/15 10:22
cis-1,2-Dichloroethene < .001 mg/l WG789089 05/19/15 10:22
Di-isopropyl ether < .001 mg/l WG789089 05/19/15 10:22
Dibromomethane < .001 mg/l WG789089 05/19/15 10:22
Dichlorodifluoromethane < .005 mg/l WG789089 05/19/15 10:22
Ethylbenzene < .001 mg/l WG789089 05/19/15 10:22
Hexachloro-1,3-butadiene < .001 mg/l WG789089 05/19/15 10:22
Isopropylbenzene < .001 mg/l WG789089 05/19/15 10:22
m&p-Xylenes < .002 mg/l WG789089 05/19/15 10:22
Methyl tert-butyl ether < .001 mg/l WG789089 05/19/15 10:22
Methylene Chloride < .005 mg/l WG789089 05/19/15 10:22
n-Butylbenzene < .001 mg/l WG789089 05/19/15 10:22
n-Propylbenzene < .001 mg/l WG789089 05/19/15 10:22
Naphthalene < .005 mg/l WG789089 05/19/15 10:22
o-Xylene < .001 mg/l WG789089 05/19/15 10:22
p-Isopropyltoluene < .001 mg/l WG789089 05/19/15 10:22
sec-Butylbenzene < .001 mg/l WG789089 05/19/15 10:22
Styrene < .001 mg/l WG789089 05/19/15 10:22
tert-Butylbenzene < .001 mg/l WG789089 05/19/15 10:22
Tetrachloroethene < .001 mg/l WG789089 05/19/15 10:22
Toluene < .005 mg/l WG789089 05/19/15 10:22
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 14 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Laboratory Blank
Analyte Result Units % Rec Limit Batch Date Analyzed
trans-1,2-Dichloroethene < .001 mg/l WG789089 05/19/15 10:22
Trichloroethene < .001 mg/l WG789089 05/19/15 10:22
Trichlorofluoromethane < .005 mg/l WG789089 05/19/15 10:22
Vinyl chloride < .001 mg/l WG789089 05/19/15 10:22
4-Bromofluorobenzene % Rec. 105.0 71-126 WG789089 05/19/15 10:22
Dibromofluoromethane % Rec. 95.40 78.3-121 WG789089 05/19/15 10:22
Toluene-d8 % Rec. 100.0 88.5-111 WG789089 05/19/15 10:22
a,a,a-Trifluorotoluene % Rec. 103.0 85-114 WG789089 05/19/15 10:22
Laboratory Control Sample
Analyte Units Known Val Result % Rec Limit Batch
1,1,1,2-Tetrachloroethane mg/l .025 0.0267 107. 74.2-124 WG789089
1,1,1-Trichloroethane mg/l .025 0.0275 110. 73.2-123 WG789089
1,1,2,2-Tetrachloroethane mg/l .025 0.0266 107. 70.7-122 WG789089
1,1,2-Trichloroethane mg/l .025 0.0264 106. 77.7-118 WG789089
1,1-Dichloroethane mg/l .025 0.0274 110. 70.7-126 WG789089
1,1-Dichloroethene mg/l .025 0.0275 110. 67.8-129 WG789089
1,1-Dichloropropene mg/l .025 0.0279 112. 73.1-125 WG789089
1,2,3-Trichlorobenzene mg/l .025 0.0237 94.6 64.9-135 WG789089
1,2,3-Trichloropropane mg/l .025 0.0272 109. 71.8-121 WG789089
1,2,4-Trichlorobenzene mg/l .025 0.0246 98.3 69.7-136 WG789089
1,2,4-Trimethylbenzene mg/l .025 0.0269 107. 75-123 WG789089
1,2-Dibromo-3-Chloropropane mg/l .025 0.0252 101. 65.4-128 WG789089
1,2-Dibromoethane mg/l .025 0.0275 110. 76.6-121 WG789089
1,2-Dichlorobenzene mg/l .025 0.0259 104. 78.4-117 WG789089
1,2-Dichloroethane mg/l .025 0.0273 109. 68.8-124 WG789089
1,2-Dichloropropane mg/l .025 0.0267 107. 76.5-119 WG789089
1,3,5-Trimethylbenzene mg/l .025 0.0272 109. 75.6-124 WG789089
1,3-Dichlorobenzene mg/l .025 0.0263 105. 70.8-128 WG789089
1,3-Dichloropropane mg/l .025 0.0254 101. 77.4-117 WG789089
1,4-Dichlorobenzene mg/l .025 0.0255 102. 78.8-115 WG789089
2,2-Dichloropropane mg/l .025 0.0272 109. 62.4-133 WG789089
2-Butanone (MEK) mg/l .125 0.134 107. 55-149 WG789089
2-Chlorotoluene mg/l .025 0.0269 108. 74.7-122 WG789089
4-Chlorotoluene mg/l .025 0.0264 106. 77.5-120 WG789089
4-Methyl-2-pentanone (MIBK) mg/l .125 0.138 110. 70.5-133 WG789089
Acetone mg/l .125 0.126 101. 35.6-163 WG789089
Acrolein mg/l .125 0.161 129. 10-190 WG789089
Acrylonitrile mg/l .125 0.144 116. 55.2-130 WG789089
Benzene mg/l .025 0.0268 107. 74.8-121 WG789089
Bromobenzene mg/l .025 0.0259 103. 77.5-116 WG789089
Bromodichloromethane mg/l .025 0.0264 105. 75.1-116 WG789089
Bromoform mg/l .025 0.0271 108. 67.5-130 WG789089
Bromomethane mg/l .025 0.0306 122. 49.9-162 WG789089
Carbon tetrachloride mg/l .025 0.0272 109. 70.2-123 WG789089
Chlorobenzene mg/l .025 0.0265 106. 78.1-119 WG789089
Chlorodibromomethane mg/l .025 0.0269 108. 74-121 WG789089
Chloroethane mg/l .025 0.0302 121. 61.7-135 WG789089
Chloroform mg/l .025 0.0268 107. 76-121 WG789089
Chloromethane mg/l .025 0.0296 118. 61.5-129 WG789089
cis-1,2-Dichloroethene mg/l .025 0.0270 108. 76-119 WG789089
Di-isopropyl ether mg/l .025 0.0268 107. 65.6-132 WG789089
Dibromomethane mg/l .025 0.0277 111. 79.5-118 WG789089
Dichlorodifluoromethane mg/l .025 0.0302 121. 54.8-135 WG789089
Ethylbenzene mg/l .025 0.0269 107. 78.8-122 WG789089
Hexachloro-1,3-butadiene mg/l .025 0.0255 102. 64.7-129 WG789089
Isopropylbenzene mg/l .025 0.0275 110. 78.6-132 WG789089
m&p-Xylenes mg/l .05 0.0534 107. 78.8-121 WG789089
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 15 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Laboratory Control Sample
Analyte Units Known Val Result % Rec Limit Batch
Methyl tert-butyl ether mg/l .025 0.0275 110. 71.2-126 WG789089
Methylene Chloride mg/l .025 0.0266 106. 70.3-120 WG789089
n-Butylbenzene mg/l .025 0.0272 109. 76.2-126 WG789089
n-Propylbenzene mg/l .025 0.0271 108. 78.2-122 WG789089
Naphthalene mg/l .025 0.0240 96.1 68.4-128 WG789089
o-Xylene mg/l .025 0.0266 106. 77.6-122 WG789089
p-Isopropyltoluene mg/l .025 0.0280 112. 74-131 WG789089
sec-Butylbenzene mg/l .025 0.0276 110. 74.4-127 WG789089
Styrene mg/l .025 0.0284 114. 80.4-126 WG789089
tert-Butylbenzene mg/l .025 0.0277 111. 75.3-126 WG789089
Tetrachloroethene mg/l .025 0.0273 109. 72.6-126 WG789089
Toluene mg/l .025 0.0251 100. 79.7-116 WG789089
trans-1,2-Dichloroethene mg/l .025 0.0277 111. 72.6-121 WG789089
Trichloroethene mg/l .025 0.0273 109. 77.7-118 WG789089
Trichlorofluoromethane mg/l .025 0.0299 119. 63.5-135 WG789089
Vinyl chloride mg/l .025 0.0301 121. 65.9-128 WG789089
4-Bromofluorobenzene 101.0 71-126 WG789089
Dibromofluoromethane 97.80 78.3-121 WG789089
Toluene-d8 100.0 88.5-111 WG789089
a,a,a-Trifluorotoluene 102.0 85-114 WG789089
Laboratory Control Sample Duplicate
Analyte Units Result Ref %Rec Limit RPD Limit Batch
1,1,1,2-Tetrachloroethane mg/l 0.0263 0.0267 105. 74.2-124 1.27 20 WG789089
1,1,1-Trichloroethane mg/l 0.0266 0.0275 106. 73.2-123 3.59 20 WG789089
1,1,2,2-Tetrachloroethane mg/l 0.0255 0.0266 102. 70.7-122 4.45 20 WG789089
1,1,2-Trichloroethane mg/l 0.0255 0.0264 102. 77.7-118 3.38 20 WG789089
1,1-Dichloroethane mg/l 0.0261 0.0274 104. 70.7-126 4.91 20 WG789089
1,1-Dichloroethene mg/l 0.0271 0.0275 108. 67.8-129 1.51 20 WG789089
1,1-Dichloropropene mg/l 0.0268 0.0279 107. 73.1-125 3.83 20 WG789089
1,2,3-Trichlorobenzene mg/l 0.0227 0.0237 91.0 64.9-135 4.00 20 WG789089
1,2,3-Trichloropropane mg/l 0.0262 0.0272 105. 71.8-121 3.82 20 WG789089
1,2,4-Trichlorobenzene mg/l 0.0235 0.0246 94.0 69.7-136 4.44 20 WG789089
1,2,4-Trimethylbenzene mg/l 0.0262 0.0269 105. 75-123 2.42 20 WG789089
1,2-Dibromo-3-Chloropropane mg/l 0.0240 0.0252 96.0 65.4-128 4.92 20 WG789089
1,2-Dibromoethane mg/l 0.0268 0.0275 107. 76.6-121 2.62 20 WG789089
1,2-Dichlorobenzene mg/l 0.0249 0.0259 99.0 78.4-117 4.25 20 WG789089
1,2-Dichloroethane mg/l 0.0261 0.0273 104. 68.8-124 4.45 20 WG789089
1,2-Dichloropropane mg/l 0.0261 0.0267 104. 76.5-119 2.16 20 WG789089
1,3,5-Trimethylbenzene mg/l 0.0268 0.0272 107. 75.6-124 1.73 20 WG789089
1,3-Dichlorobenzene mg/l 0.0259 0.0263 104. 70.8-128 1.33 20 WG789089
1,3-Dichloropropane mg/l 0.0250 0.0254 100. 77.4-117 1.36 20 WG789089
1,4-Dichlorobenzene mg/l 0.0245 0.0255 98.0 78.8-115 4.16 20 WG789089
2,2-Dichloropropane mg/l 0.0257 0.0272 103. 62.4-133 5.87 20 WG789089
2-Butanone (MEK) mg/l 0.123 0.134 98.0 55-149 8.47 20 WG789089
2-Chlorotoluene mg/l 0.0264 0.0269 105. 74.7-122 2.08 20 WG789089
4-Chlorotoluene mg/l 0.0257 0.0264 103. 77.5-120 2.86 20 WG789089
4-Methyl-2-pentanone (MIBK) mg/l 0.130 0.138 104. 70.5-133 6.12 20 WG789089
Acetone mg/l 0.118 0.126 94.0 35.6-163 6.46 23.9 WG789089
Acrolein mg/l 0.150 0.161 120. 10-190 6.74 28.1 WG789089
Acrylonitrile mg/l 0.137 0.144 109. 55.2-130 5.46 20 WG789089
Benzene mg/l 0.0259 0.0268 103. 74.8-121 3.60 20 WG789089
Bromobenzene mg/l 0.0254 0.0259 102. 77.5-116 1.77 20 WG789089
Bromodichloromethane mg/l 0.0259 0.0264 104. 75.1-116 1.65 20 WG789089
Bromoform mg/l 0.0260 0.0271 104. 67.5-130 3.99 20 WG789089
Bromomethane mg/l 0.0278 0.0306 111. 49.9-162 9.60 20 WG789089
Carbon tetrachloride mg/l 0.0266 0.0272 106. 70.2-123 2.52 20 WG789089
Chlorobenzene mg/l 0.0264 0.0265 106. 78.1-119 0.220 20 WG789089
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 16 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Laboratory Control Sample Duplicate
Analyte Units Result Ref %Rec Limit RPD Limit Batch
Chlorodibromomethane mg/l 0.0260 0.0269 104. 74-121 3.41 20 WG789089
Chloroethane mg/l 0.0285 0.0302 114. 61.7-135 5.60 20 WG789089
Chloroform mg/l 0.0258 0.0268 103. 76-121 3.96 20 WG789089
Chloromethane mg/l 0.0280 0.0296 112. 61.5-129 5.52 20 WG789089
cis-1,2-Dichloroethene mg/l 0.0261 0.0270 104. 76-119 3.43 20 WG789089
Di-isopropyl ether mg/l 0.0256 0.0268 102. 65.6-132 4.43 20 WG789089
Dibromomethane mg/l 0.0268 0.0277 107. 79.5-118 3.01 20 WG789089
Dichlorodifluoromethane mg/l 0.0291 0.0302 116. 54.8-135 3.92 20 WG789089
Ethylbenzene mg/l 0.0265 0.0269 106. 78.8-122 1.42 20 WG789089
Hexachloro-1,3-butadiene mg/l 0.0246 0.0255 98.0 64.7-129 3.56 20 WG789089
Isopropylbenzene mg/l 0.0271 0.0275 108. 78.6-132 1.71 20 WG789089
m&p-Xylenes mg/l 0.0523 0.0534 105. 78.8-121 2.12 20 WG789089
Methyl tert-butyl ether mg/l 0.0257 0.0275 103. 71.2-126 6.62 20 WG789089
Methylene Chloride mg/l 0.0255 0.0266 102. 70.3-120 4.27 20 WG789089
n-Butylbenzene mg/l 0.0261 0.0272 104. 76.2-126 4.07 20 WG789089
n-Propylbenzene mg/l 0.0265 0.0271 106. 78.2-122 2.15 20 WG789089
Naphthalene mg/l 0.0232 0.0240 93.0 68.4-128 3.47 20 WG789089
o-Xylene mg/l 0.0261 0.0266 104. 77.6-122 1.98 20 WG789089
p-Isopropyltoluene mg/l 0.0272 0.0280 109. 74-131 2.92 20 WG789089
sec-Butylbenzene mg/l 0.0272 0.0276 109. 74.4-127 1.32 20 WG789089
Styrene mg/l 0.0280 0.0284 112. 80.4-126 1.32 20 WG789089
tert-Butylbenzene mg/l 0.0273 0.0277 109. 75.3-126 1.57 20 WG789089
Tetrachloroethene mg/l 0.0273 0.0273 109. 72.6-126 0.330 20 WG789089
Toluene mg/l 0.0245 0.0251 98.0 79.7-116 2.48 20 WG789089
trans-1,2-Dichloroethene mg/l 0.0270 0.0277 108. 72.6-121 2.54 20 WG789089
Trichloroethene mg/l 0.0268 0.0273 107. 77.7-118 1.81 20 WG789089
Trichlorofluoromethane mg/l 0.0286 0.0299 114. 63.5-135 4.45 20 WG789089
Vinyl chloride mg/l 0.0288 0.0301 115. 65.9-128 4.39 20 WG789089
4-Bromofluorobenzene 102.0 71-126 WG789089
Dibromofluoromethane 96.40 78.3-121 WG789089
Toluene-d8 102.0 88.5-111 WG789089
a,a,a-Trifluorotoluene 103.0 85-114 WG789089
Matrix Spike
Analyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch
1,1,1,2-Tetrachloroethane mg/l 0.0263 0.0 .025 100. 64-128 L764375-01 WG789089
1,1,1-Trichloroethane mg/l 0.0268 0.0 .025 110. 58.7-134 L764375-01 WG789089
1,1,2,2-Tetrachloroethane mg/l 0.0268 0.0 .025 110. 56-132 L764375-01 WG789089
1,1,2-Trichloroethane mg/l 0.0256 0.0 .025 100. 66.3-125 L764375-01 WG789089
1,1-Dichloroethane mg/l 0.0266 0.0 .025 110. 58.5-132 L764375-01 WG789089
1,1-Dichloroethene mg/l 0.0276 0.0 .025 110. 51.1-140 L764375-01 WG789089
1,1-Dichloropropene mg/l 0.0273 0.0 .025 110. 57.3-136 L764375-01 WG789089
1,2,3-Trichlorobenzene mg/l 0.0236 0.0 .025 94.0 59.1-138 L764375-01 WG789089
1,2,3-Trichloropropane mg/l 0.0268 0.0 .025 110. 61.4-128 L764375-01 WG789089
1,2,4-Trichlorobenzene mg/l 0.0241 0.0 .025 97.0 63.6-143 L764375-01 WG789089
1,2,4-Trimethylbenzene mg/l 0.0269 0.0 .025 110. 57.4-137 L764375-01 WG789089
1,2-Dibromo-3-Chloropropane mg/l 0.0248 0.0 .025 99.0 57.3-136 L764375-01 WG789089
1,2-Dibromoethane mg/l 0.0266 0.0 .025 110. 67.1-125 L764375-01 WG789089
1,2-Dichlorobenzene mg/l 0.0248 0.0 .025 99.0 68.2-123 L764375-01 WG789089
1,2-Dichloroethane mg/l 0.0263 0.0 .025 100. 60-126 L764375-01 WG789089
1,2-Dichloropropane mg/l 0.0262 0.0 .025 100. 64.2-123 L764375-01 WG789089
1,3,5-Trimethylbenzene mg/l 0.0270 0.0 .025 110. 63.6-132 L764375-01 WG789089
1,3-Dichlorobenzene mg/l 0.0258 0.0 .025 100. 63.1-131 L764375-01 WG789089
1,3-Dichloropropane mg/l 0.0249 0.0 .025 100. 67.9-121 L764375-01 WG789089
1,4-Dichlorobenzene mg/l 0.0248 0.0 .025 99.0 68.6-123 L764375-01 WG789089
2,2-Dichloropropane mg/l 0.0254 0.0 .025 100. 50.5-144 L764375-01 WG789089
2-Butanone (MEK) mg/l 0.106 0.0 .125 84.0 22.4-138 L764375-01 WG789089
2-Chlorotoluene mg/l 0.0266 0.0 .025 110. 63.6-128 L764375-01 WG789089
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 17 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Matrix Spike
Analyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch
4-Chlorotoluene mg/l 0.0253 0.0 .025 100. 65.7-127 L764375-01 WG789089
4-Methyl-2-pentanone (MIBK) mg/l 0.136 0.0 .125 110. 60.8-140 L764375-01 WG789089
Acetone mg/l 0.0675 0.00137 .125 53.0 10-130 L764375-01 WG789089
Acrolein mg/l 0.128 0.0 .125 100. 10-200 L764375-01 WG789089
Acrylonitrile mg/l 0.143 0.0 .125 120. 49.4-133 L764375-01 WG789089
Benzene mg/l 0.0261 0.0 .025 100. 54.3-133 L764375-01 WG789089
Bromobenzene mg/l 0.0251 0.0 .025 100. 63.9-124 L764375-01 WG789089
Bromodichloromethane mg/l 0.0257 0.0 .025 100. 63.9-121 L764375-01 WG789089
Bromoform mg/l 0.0263 0.0 .025 100. 59.5-134 L764375-01 WG789089
Bromomethane mg/l 0.0268 0.0 .025 110. 41.7-155 L764375-01 WG789089
Carbon tetrachloride mg/l 0.0268 0.0 .025 110. 55.7-134 L764375-01 WG789089
Chlorobenzene mg/l 0.0261 0.0 .025 100. 67-125 L764375-01 WG789089
Chlorodibromomethane mg/l 0.0259 0.0 .025 100. 64.3-125 L764375-01 WG789089
Chloroethane mg/l 0.0286 0.0 .025 120. 51.5-136 L764375-01 WG789089
Chloroform mg/l 0.0260 0.0 .025 100. 63-129 L764375-01 WG789089
Chloromethane mg/l 0.0284 0.0 .025 110. 42.4-135 L764375-01 WG789089
cis-1,2-Dichloroethene mg/l 0.0264 0.0 .025 100. 59.2-129 L764375-01 WG789089
Di-isopropyl ether mg/l 0.0258 0.0 .025 100. 56.9-136 L764375-01 WG789089
Dibromomethane mg/l 0.0269 0.0 .025 110. 68.2-124 L764375-01 WG789089
Dichlorodifluoromethane mg/l 0.0310 0.0 .025 120. 40.6-144 L764375-01 WG789089
Ethylbenzene mg/l 0.0267 0.0 .025 110. 61.4-133 L764375-01 WG789089
Hexachloro-1,3-butadiene mg/l 0.0256 0.0 .025 100. 55.1-136 L764375-01 WG789089
Isopropylbenzene mg/l 0.0272 0.0 .025 110. 66.8-141 L764375-01 WG789089
m&p-Xylenes mg/l 0.0534 0.00 .05 107. 61.7-133 L764375-01 WG789089
Methyl tert-butyl ether mg/l 0.0270 0.0 .025 110. 57.7-134 L764375-01 WG789089
Methylene Chloride mg/l 0.0258 0.0 .025 100. 58.1-122 L764375-01 WG789089
n-Butylbenzene mg/l 0.0265 0.0 .025 110. 62.7-140 L764375-01 WG789089
n-Propylbenzene mg/l 0.0266 0.0 .025 110. 65.9-131 L764375-01 WG789089
Naphthalene mg/l 0.0245 0.0 .025 98.0 58-135 L764375-01 WG789089
o-Xylene mg/l 0.0265 0.00 .025 106. 63.3-130 L764375-01 WG789089
p-Isopropyltoluene mg/l 0.0276 0.0 .025 110. 63.2-139 L764375-01 WG789089
sec-Butylbenzene mg/l 0.0274 0.0 .025 110. 62.2-136 L764375-01 WG789089
Styrene mg/l 0.0270 0.0 .025 110. 66.8-133 L764375-01 WG789089
tert-Butylbenzene mg/l 0.0276 0.0 .025 110. 63.3-134 L764375-01 WG789089
Tetrachloroethene mg/l 0.0269 0.0 .025 110. 53-139 L764375-01 WG789089
Toluene mg/l 0.0248 0.0 .025 99.0 61.4-130 L764375-01 WG789089
trans-1,2-Dichloroethene mg/l 0.0272 0.0 .025 110. 56.5-129 L764375-01 WG789089
Trichloroethene mg/l 0.0266 0.0 .025 110. 44.1-149 L764375-01 WG789089
Trichlorofluoromethane mg/l 0.0291 0.0 .025 120. 49.6-145 L764375-01 WG789089
Vinyl chloride mg/l 0.0303 0.0 .025 120. 47.8-137 L764375-01 WG789089
4-Bromofluorobenzene 102.0 71-126 WG789089
Dibromofluoromethane 97.80 78.3-121 WG789089
Toluene-d8 100.0 88.5-111 WG789089
a,a,a-Trifluorotoluene 103.0 85-114 WG789089
Matrix Spike Duplicate
Analyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch
1,1,1,2-Tetrachloroethane mg/l 0.0264 0.0263 106. 64-128 0.260 20 L764375-01 WG789089
1,1,1-Trichloroethane mg/l 0.0266 0.0268 106. 58.7-134 0.550 20 L764375-01 WG789089
1,1,2,2-Tetrachloroethane mg/l 0.0268 0.0268 107. 56-132 0.130 22.2 L764375-01 WG789089
1,1,2-Trichloroethane mg/l 0.0260 0.0256 104. 66.3-125 1.79 20 L764375-01 WG789089
1,1-Dichloroethane mg/l 0.0263 0.0266 105. 58.5-132 1.04 20 L764375-01 WG789089
1,1-Dichloroethene mg/l 0.0267 0.0276 107. 51.1-140 3.41 20.2 L764375-01 WG789089
1,1-Dichloropropene mg/l 0.0269 0.0273 108. 57.3-136 1.53 20 L764375-01 WG789089
1,2,3-Trichlorobenzene mg/l 0.0245 0.0236 98.0 59.1-138 3.82 23.7 L764375-01 WG789089
1,2,3-Trichloropropane mg/l 0.0272 0.0268 109. 61.4-128 1.48 22.4 L764375-01 WG789089
1,2,4-Trichlorobenzene mg/l 0.0253 0.0241 101. 63.6-143 4.58 21.9 L764375-01 WG789089
1,2,4-Trimethylbenzene mg/l 0.0273 0.0269 109. 57.4-137 1.31 20 L764375-01 WG789089
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 18 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Matrix Spike Duplicate
Analyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch
1,2-Dibromo-3-Chloropropane mg/l 0.0253 0.0248 101. 57.3-136 1.75 27 L764375-01 WG789089
1,2-Dibromoethane mg/l 0.0271 0.0266 108. 67.1-125 2.16 20 L764375-01 WG789089
1,2-Dichlorobenzene mg/l 0.0255 0.0248 102. 68.2-123 3.01 20 L764375-01 WG789089
1,2-Dichloroethane mg/l 0.0263 0.0263 105. 60-126 0.0300 20 L764375-01 WG789089
1,2-Dichloropropane mg/l 0.0264 0.0262 106. 64.2-123 0.790 20 L764375-01 WG789089
1,3,5-Trimethylbenzene mg/l 0.0274 0.0270 110. 63.6-132 1.39 20.5 L764375-01 WG789089
1,3-Dichlorobenzene mg/l 0.0264 0.0258 106. 63.1-131 2.30 20 L764375-01 WG789089
1,3-Dichloropropane mg/l 0.0252 0.0249 101. 67.9-121 1.51 20 L764375-01 WG789089
1,4-Dichlorobenzene mg/l 0.0252 0.0248 101. 68.6-123 1.72 20 L764375-01 WG789089
2,2-Dichloropropane mg/l 0.0260 0.0254 104. 50.5-144 2.31 21.9 L764375-01 WG789089
2-Butanone (MEK) mg/l 0.105 0.106 83.7 22.4-138 0.910 27 L764375-01 WG789089
2-Chlorotoluene mg/l 0.0268 0.0266 107. 63.6-128 0.890 20 L764375-01 WG789089
4-Chlorotoluene mg/l 0.0258 0.0253 103. 65.7-127 1.65 20 L764375-01 WG789089
4-Methyl-2-pentanone (MIBK) mg/l 0.137 0.136 109. 60.8-140 0.460 25.1 L764375-01 WG789089
Acetone mg/l 0.0671 0.0675 52.6 10-130 0.570 27.9 L764375-01 WG789089
Acrolein mg/l 0.127 0.128 102. 10-200 0.870 27.7 L764375-01 WG789089
Acrylonitrile mg/l 0.143 0.143 114. 49.4-133 0.380 25.3 L764375-01 WG789089
Benzene mg/l 0.0259 0.0261 104. 54.3-133 0.650 20 L764375-01 WG789089
Bromobenzene mg/l 0.0256 0.0251 102. 63.9-124 1.75 20 L764375-01 WG789089
Bromodichloromethane mg/l 0.0260 0.0257 104. 63.9-121 1.17 20 L764375-01 WG789089
Bromoform mg/l 0.0266 0.0263 106. 59.5-134 1.21 20.5 L764375-01 WG789089
Bromomethane mg/l 0.0279 0.0268 112. 41.7-155 4.17 21.9 L764375-01 WG789089
Carbon tetrachloride mg/l 0.0266 0.0268 106. 55.7-134 0.860 20 L764375-01 WG789089
Chlorobenzene mg/l 0.0265 0.0261 106. 67-125 1.23 20 L764375-01 WG789089
Chlorodibromomethane mg/l 0.0261 0.0259 104. 64.3-125 1.02 20.8 L764375-01 WG789089
Chloroethane mg/l 0.0286 0.0286 114. 51.5-136 0.0100 40 L764375-01 WG789089
Chloroform mg/l 0.0261 0.0260 104. 63-129 0.110 20 L764375-01 WG789089
Chloromethane mg/l 0.0286 0.0284 114. 42.4-135 0.490 20 L764375-01 WG789089
cis-1,2-Dichloroethene mg/l 0.0263 0.0264 105. 59.2-129 0.330 20 L764375-01 WG789089
Di-isopropyl ether mg/l 0.0260 0.0258 104. 56.9-136 0.800 20 L764375-01 WG789089
Dibromomethane mg/l 0.0271 0.0269 108. 68.2-124 0.720 20 L764375-01 WG789089
Dichlorodifluoromethane mg/l 0.0304 0.0310 121. 40.6-144 1.97 20.2 L764375-01 WG789089
Ethylbenzene mg/l 0.0265 0.0267 106. 61.4-133 0.730 20 L764375-01 WG789089
Hexachloro-1,3-butadiene mg/l 0.0265 0.0256 106. 55.1-136 3.72 23.6 L764375-01 WG789089
Isopropylbenzene mg/l 0.0274 0.0272 110. 66.8-141 0.700 20 L764375-01 WG789089
m&p-Xylenes mg/l 0.0535 0.0534 107. 61.7-133 0.140 20 L764375-01 WG789089
Methyl tert-butyl ether mg/l 0.0274 0.0270 110. 57.7-134 1.44 20 L764375-01 WG789089
Methylene Chloride mg/l 0.0261 0.0258 104. 58.1-122 0.960 20 L764375-01 WG789089
n-Butylbenzene mg/l 0.0270 0.0265 108. 62.7-140 1.89 20.3 L764375-01 WG789089
n-Propylbenzene mg/l 0.0269 0.0266 108. 65.9-131 1.12 20 L764375-01 WG789089
Naphthalene mg/l 0.0252 0.0245 101. 58-135 3.05 25.5 L764375-01 WG789089
o-Xylene mg/l 0.0265 0.0265 106. 63.3-130 0.0100 20 L764375-01 WG789089
p-Isopropyltoluene mg/l 0.0282 0.0276 113. 63.2-139 2.18 20.4 L764375-01 WG789089
sec-Butylbenzene mg/l 0.0278 0.0274 111. 62.2-136 1.62 20.3 L764375-01 WG789089
Styrene mg/l 0.0273 0.0270 109. 66.8-133 1.06 20 L764375-01 WG789089
tert-Butylbenzene mg/l 0.0279 0.0276 112. 63.3-134 1.23 21 L764375-01 WG789089
Tetrachloroethene mg/l 0.0269 0.0269 108. 53-139 0.120 20 L764375-01 WG789089
Toluene mg/l 0.0247 0.0248 98.9 61.4-130 0.290 20 L764375-01 WG789089
trans-1,2-Dichloroethene mg/l 0.0270 0.0272 108. 56.5-129 0.610 20 L764375-01 WG789089
Trichloroethene mg/l 0.0264 0.0266 106. 44.1-149 0.550 20 L764375-01 WG789089
Trichlorofluoromethane mg/l 0.0284 0.0291 114. 49.6-145 2.18 21.2 L764375-01 WG789089
Vinyl chloride mg/l 0.0299 0.0303 120. 47.8-137 1.26 20 L764375-01 WG789089
4-Bromofluorobenzene 102.0 71-126 WG789089
Dibromofluoromethane 97.30 78.3-121 WG789089
Toluene-d8 100.0 88.5-111 WG789089
a,a,a-Trifluorotoluene 103.0 85-114 WG789089
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 19 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
Batch number /Run number / Sample number cross reference
WG789089: R3037990: L764375-01 02 03 04 05 06
* * Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 20 of 21
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Withers & Ravenel Eng. - Standard
Kevin Buchanan
115 MacKenan Drive Quality Assurance Report
Level II
Cary, NC 27511 May 19, 2015
L764375
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 21 of 21