RA-517_3274_CA_MRP_20190415

DRAFT

April 15, 2019 Mr. Mark Petermann NCDEQ, Division of Waste Management, UST Section 1646 Mail Service Center
Raleigh, North Carolina 27699-1646 Reference: Environmental Services Report – Petro Mart # 4
11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina NCDEQ Incident: TF-3274 NCDEQ Contract: N17006
ECS Project: 49:6230-B Dear Mr. Petermann:
As authorized by your acceptance of ECS Southeast, LLP (ECS) Task Authorization Request #3 dated January 30, 2019; ECS has completed the Comprehensive Site Assessment for the above-referenced site. Included in this report is a description of the field activities, the results obtained,
and our conclusions and recommendations. ECS appreciates the opportunity to provide our environmental consulting services to you on this project. If you have any questions concerning this report or this project, please contact us. Sincerely,
ECS SOUTHEAST, LLP

Samantha M. Szakasits, G.I.T. Matthew Gillis Assistant Staff Project Manager Sr. Environmental Project Manager
[e-mail] [e-mail] [phone] [phone] Matthew H. McDuffie, P.G.
Principal Geologist NC License No. 2269 [e-mail] [phone]

Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

SITE INFORMATION
Facility I.D.: #0-224946 UST Incident No.: TF-3274 Site Rank: H210A
Land Use Category: Commercial

Site Name and Location: Petro Mart #4
11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
Parcel Identification Number: 9776-23-9124
Latitude and Longitude: 35.846815° North, -79.091187° West
Contacts

Property Owner: Jean Williams PO Box 429 Carrboro, North Carolina 27510 [phone]
Property Owner Legal Representative: Benjamin D. Overby 522 South Lexington Ave. Burlington, NC 27216-2958 [phone] Consultant: ECS Southeast, LLP
9001 Glenwood Avenue Raleigh, North Carolina 27617 [phone] Attn: Matthew Gillis
Laboratory: Con-Test Analytical Laboratory 39 Spruce Street
East Longmeadow, MA 01028 [phone] NC Certification No. 652

Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

EXECUTIVE SUMMARY
The subject site is known as the Petro Mart #4 site and is located at 11455 NC Highway 15/501
North in Chapel Hill, Chatham County, North Carolina (Figure 1 and Figure 2). The subject site is further identified by Chatham County Geographic Information Systems (GIS) Parcel Identification Number (PIN) 9776-23-9124.
INCIDENT RISK EVALUATION SUMMARY
SOURCE INFORMATION
Source, Date, and Nature of Release 1 x 2,000-gallon UST (kerosene), 1 x 3,000-gallon UST (diesel), 1 x 6,000-gallon (gasoline), and 2 x 8,000-gallon USTs (gasoline) – removed March 7, 2001 Each Known Source Removed? Yes – 5 USTs removed in March 7, 2001
Additional Sources Likely Present? Yes – current USTs – 1 x 12,000-gallon UST (gasoline), 1 x 8,000-gallon UST (gasoline), and 1 x 6,000-gallon UST (diesel)
Known Sources Assessed (USTs, Piping, Dispensers)? Yes
FREE PRODUCT
Free Product Present? Currently, No. Historically, Yes in MW-3
SITE SOIL CONDITIONS
TPH Soil Data Available? Maximum concentration at site Unknown Risk-Based Soil Data Available? Yes Maximum Soil Contaminant Concentrations Aliphatics (C9-C12) at 3,080 mg/kg from SS-5B (2018) Current Extent of Soil Impact Delineated? Yes
SITE GROUNDWATER CONDITIONS
Average Depth to Groundwater? Approx. 34 feet below top of casing (btoc) Contaminants Present Above NC2L? Yes (Monitoring wells MW-1, MW-2, and MW-4)
Contaminants Present Above GCLs? Yes (Monitoring well MW-3)
Groundwater Plume Delineated? No, unknown south of monitoring well MW-3 and MW-4
Groundwater Plume Migrated Off-Site? Unknown south of monitoring well MW-3 and MW-4
Contaminant Level Trend Stable / Decreasing
RECEPTOR INFORMATION
Date of Most Current Receptor Survey August 10, 2015
Potable Water-Supply Wells within 1,000’? Yes – see section on water supply well information Water Available to Properties within 1,000’? Yes Non-Potable Wells within 250’? No Site within Wellhead Protection Area? No Surface Water Bodies within 500’? No
REMEDIAL ACTIVITIES
Remedial activities conducted? O-Sox Remedial Device Deployment and AFVR’s
VAPOR INTRUSION
Dissolved Contaminants exceeding
Groundwater Screening Levels for Vapors present within 5’ of Ground Surface?
No
Occupied Structures on the Site? Yes, Active Gas Station

Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

On February 20, 2019, ECS contracted with Zebra Environmental & Industrial Services (Zebra) to conduct an Aggressive Fluid and Vapor Recovery (AFVR) event at the site using monitoring well MW-3 as an extraction point.
On March 6, 2019, ECS collected a field blank and groundwater samples from monitoring wells MW-1 through MW-8. ECS deployed an O-Sox remedial device in monitoring well MW-3.
Laboratory analysis reported benzene at a concentration above its Gross Contamination Level (GCL) in monitoring well MW-3. Laboratory analysis reported several additional targeted analytes at concentrations above their respective North Carolina 2L Groundwater Quality Standard (NC2LGWQS) but below their respective GCL in the groundwater sample collected from monitoring well MW-3. Laboratory analysis reported several targeted analytes at concentrations above their respective
NC2LGWQS but below their respective GCL in the groundwater sample collected from monitoring well MW-4. Laboratory analysis reported several targeted analytes at concentrations above their respective
laboratory reporting limits but below their respective NC2LGWQS in the groundwater samples collected from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-7, and MW-8.
Laboratory analysis reported acetone at a concentration above its laboratory reporting limit but below its NC2LGWQS in the field blank. The concentration was denoted with a J-Flag, which is an estimated concentration. Acetone is a common laboratory artifact and ECS considers this detection to be a laboratory contaminant.
Based on the findings of this Environmental Services Report, ECS recommends the following:
• Obtain an access agreement to install two monitoring wells on the adjacent property to the south of subject site (See Figure 5). Based on review of the draft report, NCDEQ recommended installing two additional monitoring wells near the locations of monitoring
wells MW-4 and MW-7 25 to 30 feet below the existing monitoring wells.
• Conduct an updated receptor survey to determine the current status of the water supply wells in the area. It was observed that several houses appeared to be vacant in the area.
• Sample the two new monitoring wells and the eight existing monitoring wells.
• If funds are available, ECS recommends conducting an injection near monitoring wells MW-3, MW-4, MW-6, and MW-7 to promote the degradation of petroleum constituents in the site groundwater.

Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

TABLE OF CONTENTS

1.0 SITE HISTORY ......................................................................................................... 1 2.0 SITE GEOLOGY AND HYDROGEOLOGY............................................................... 4 3.0 RECEPTOR INFORMATION .................................................................................... 4 4.0 FILE REVIEW ............................................................................................................ 5
5.0 FIELD ACTIVITIES ................................................................................................... 5
6.0 RESULTS ................................................................................................................. 6
7.0 CONCLUSIONS ........................................................................................................ 8 8.0 RECOMMENDATIONS ............................................................................................. 8 FIGURES
Figure 1 Site Location Map Figure 2 Aerial Site Map Figure 3 2018 Soil Sample Location Map
Figure 4 Water Supply Well Location Map Figure 5 Monitoring Well Location Map Figure 6 Groundwater Elevation Map Figure 7 Pantry #294 Site Map Figure 8 Groundwater Concentration Map Figure 9 MTBE Isoconcentration Map
TABLES Table 1 UST Information
Table 2 Summary of Historical Soil Sample Analytical Results Table 3 Water Supply Well Survey Table 4 Aggressive Fluid and Vapor Recovery Measurements
Table 5 Aggressive Fluid and Vapor Recovery Calculations Table 6 Monitoring Well Construction and Groundwater Elevation Details Table 7 Geochemical Measurements Calculations Table 8 Summary of Current Groundwater Analytical Results
Table 9 Summary of Historical Groundwater Analytical Results
APPENDICIES
Appendix A ECS Personnel Field Notes and Sampling Data Sheets Appendix B Site Photographs Appendix C Laboratory Analytical Data Sheets and Chain of Custody (COC) Record
Appendix D Waste Manifest Appendix E Surveying Data
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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1.0 SITE HISTORY
The Petro Mart #4 site is located at 11455 NC Highway 15/501 North in Chapel Hill, Chatham County, North Carolina (Figures 1 and 2). According to information provided to ECS by the North Carolina Department of Environmental Quality (NCDEQ), the site is an active gasoline station that
formerly contained one 2,000-gallon kerosene UST, one 2,000-gallon diesel UST, one 6,000-gallon gasoline UST, and two 8,000-gallon gasoline USTs. The site currently contains one 12,000-gallon gasoline UST, one 8,000-gallon gasoline UST, and one 6,000-gallon diesel UST (Table 1).
In August 1986, a release of approximately 25-gallons of gasoline was reported on the site. In October 1986, two monitoring wells (*MW-1 and *MW-2) were installed at the site to depths of 20 and 30 ft bgs. Laboratory analysis of soil samples collected from the monitoring well borings did
not report petroleum-related contamination. The monitoring wells were determined to be dry and were not sampled. In 1987, laboratory analysis of soil samples collected by the NCDEQ reported benzene at 8.6
milligrams per kilogram (mg/kg) and methyl-ethyl ketone (MEK) at 120 mg/kg; however, the location of these soil borings is not known.
In September 1994, groundwater samples were collected from five off-site water supply wells. Laboratory analysis of the groundwater samples reported methyl tert-butyl ether (MTBE) at 72 ppb in the water supply well at the Park & Stay mobile home park (WSW-2) located approximately 800 feet south of the subject site. Water-supply well WSW-2 has subsequently been abandoned and
the Cole Park Plaza Shopping Center has been constructed at that location. In February 1995, two monitoring wells were installed at the site. Monitoring well MW-1 was
installed adjacent to the current tank basin and monitoring well MW-2 was installed on the southeast corner of the subject site. Laboratory analysis reported several targeted analytes at concentrations above their respective NC2LGWQS in the groundwater samples collected from monitoring wells MW-1 and MW-2.
In March 2001, five USTs were removed from the site. A total of eight soil samples were collected during closure activities. Laboratory analysis of seven of the eight soil samples reported total petroleum hydrocarbons (TPH) above the NCDEQ UST Sections Action Levels of 10 milligrams per kilogram (mg/kg). Monitoring wells *MW-1 and *MW-2 were abandoned. In December 2008, a receptor survey was conducted for the site. At that time, the site consisted
of an active gasoline station (Petro Mart) and one 20,000-gallon compartmentalized UST containing regular and premium gasoline and diesel. ECS could not determine the current status of this UST. The receptor survey did not identify monitoring wells or water supply wells on the subject site. The site was determined to utilize water obtained from water supply well WSW-1
located on an off-site property approximately 350 feet west and upgradient of the site. Water supply well WSW-1 is owned by Aqua who indicated that water supply well WSW-1 is sampled regularly for VOCs. Water supply well WSW-1 is approximately 410 feet deep, has a capacity of
60 gallons per minute (gpm), and has been in service since the late 1970s. Five additional water supply wells (WSW-2, WSW-3, and WSW-5 through WSW-7) were identified within 1,000 feet of the site. It was reported that these wells are inactive or have been abandoned.
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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In April 2010, a review of the active UST system compliance records for the site was conducted.
According to a February 2009 compliance inspection, three new USTs were installed on the site in May 2001 consisting of one 12,000-gallon gasoline, one 8,000-gallon gasoline, and one 6,000-gallon diesel UST. The inspection identified five violations consisting of the following:
1) Failure to provide secondary containment on UST systems installed or replaced after May 1, 2000 near wells and surface waters (the UST system is located within 500 feet of a public water supply well);
2) No leak detection for tanks;
3) Failure to conduct leak detection properly;
4) Failure to report a suspected release (weeps were reportedly observed beneath three of the four dispensing pumps); and,
5) Failure to investigate a suspected release.
In the compliance record file, there was a response letter from the property owner (K&M Services,
Inc.) regarding to the compliance report. Included in the letter were line and ELD test results, tank tightness testing results, copies of invoices for a continuous statistical leak detection system installed in the existing tank monitoring device, an invoice for seven sensors installed in sump pumps, and dispenser pans, and tank monitoring tapes. In addition, the letter indicates that all weeps beneath the dispensers had been repaired and that old filters had been removed from the containment sump. The 2010 compliance review report concluded that the UST system is in compliance and that residual soil and groundwater contamination may be present in the areas of
the former UST pit and dispensing pumps. The report indicates that groundwater contamination beneath the site may be originating from an adjoining leaking UST site (Pantry #294). On April 15 and 16, 2015, ECS installed monitoring wells (MW-1 and MW-2) to depths of 55
and 54 ft. bgs, respectively. Monitoring wells MW-1 and MW-2 are located near the current UST basin. ECS collected two soil samples from each monitoring well boring at depths of 3 to 5 ft bgs (SS-1A and SS-2A) and 8 to 10 ft bgs (SS-1B and SS-2B). Soil samples SS-1A and SS-1B
were collected from the boring for monitoring well MW-1 and soil samples SS-2A and SS-2B were collected from the boring for monitoring well MW-2. ECS also collected groundwater samples from monitoring wells MW-1 and MW-2.
Laboratory analysis reported methylene chloride at a concentration above its Soil-to-Groundwater Maximum Soil Contamination Concentration (MSCC) in the soil sample collected from SS-2A, as shown on Table 2. Laboratory analysis reported MTBE and lead at concentrations above their
respective NC2LGWQS but below their respective GCLs in the groundwater sample collected from monitoring well MW-1. Laboratory analysis reported benzene and MTBE at concentrations above their respective NC2LGWQS but below their respective GCLs in the groundwater sample collected from monitoring well MW-2.
On August 10-12, 2015, ECS installed four monitoring wells (MW-3 through MW-6) to depths ranging from 46 to 52 ft. bgs. ECS collected groundwater samples from monitoring wells MW-1
and MW-2 and the four newly installed monitoring wells. On August 24, 2015, Bateman Civil
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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Survey surveyed the site monitoring wells. Laboratory analysis reported benzene and MTBE at concentrations above their respective GCLs in the groundwater sample collected from monitoring well MW-3, which is located adjacent to the former UST basin. Laboratory analysis reported
several additional targeted analytes at concentrations above their respective NC2LGWQS but below their respective GCLs in the groundwater samples collected from monitoring wells MW-1 through MW-6.
ECS conducted a receptor survey update for the subject site. ECS observed two water supply well houses (WSW-1 and WSW-6) within 500 feet of the subject site and two water supply wells (WSW-5 and WSW-7) within 1,000 feet of the subject site. ECS spoke with Ms. Shonda, a representative of Aqua who confirmed that the subject site utilizes municipal water obtained from the community water supply well (WSW-1) located approximately 350 feet west and topographically upgradient of the site. Aqua also confirmed that the community water supply well WSW-1 supplies water to the residences within Cedar Terrace. Water supply well WSW-1 is
maintained by Aqua who indicated that WSW-1 is sampled regularly for VOCs. ECS spoke with Ms. Jean Williams, the owner of the properties associated with water supply wells WSW-5 through WSW-7, who confirmed that the water supply wells are active and are sampled regularly by an unknown agent. ECS was not provided with laboratory reports from this testing.
On March 7, 2018, ECS collected groundwater samples from monitoring wells MW-1, MW-2, MW-4, MW-5, and MW-6. Prior to sampling, ECS gauged each monitoring well for the presence
of free product. Free product was detected in monitoring well MW-3, and was therefore not sampled. The samples collected were shipped to Con-Test Analytical Laboratory for analyses for volatile organic compounds (VOCs) by SM 6200B. ECS subsequently deployed an O-Sox remedial device in monitoring well MW-4. Laboratory analysis of the groundwater samples
collected from monitoring wells MW-1, MW-2, and MW-4 detected petroleum-related hydrocarbons at concentrations that exceeded their respective North Carolina 2L Groundwater Quality Standards (NC2LGWQS), but did not exceed their respective Gross Contamination
Levels (GCLs). The groundwater results show similar concentrations as previous samplings events. In November 2018, ECS contracted with Quantex to advance eight soil borings to collect 24
total soil samples at depths ranging from 12 to 20 ft. bgs for risk-based analysis along the sidewalls of the investigate soil quality in the vicinity of the former UST basin (Table 2 and Figure 3). ECS also installed two Type II groundwater monitoring wells: MW-7 and MW-8,
conducted a groundwater monitoring event, and deployed O-Sox remedial device in monitoring well MW-4. Laboratory analysis detected benzene in monitoring well MW-3 at a concentration above its respective GCL and other petroleum-related compounds were detected in monitoring wells MW-1, MW-2, and MW-4, at concentrations exceeding their respective NC2LGWQS.
Laboratory analysis reported several targeted analytes at concentrations above their respective Soil-to-Water MSCCs in several soil samples collected at the site.
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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2.0 SITE GEOLOGY AND HYDROGEOLOGY

As determined from the USGS Topographic Map, Farrington, North Carolina Quadrangle dated 1993 (Figure 1), the site is at an approximate elevation of 550 feet above mean sea level.
The subject site is situated in the Piedmont Physiographic Province. The soils encountered in this area are the residual product of in-place chemical weathering of rock presently underlying the site and/or historic depositional events. In general, shallow unconfined groundwater movement within the overlying soils is controlled largely by topographic gradients. However, as
the groundwater percolates downward, it becomes controlled by the subsurface geologic conditions. Thus, the direction of groundwater movement in the deeper aquifers may not be consistent with the reflecting topography. In general, shallow unconfined groundwater movement within the overlying soils is controlled largely by topographic gradients. Recharge occurs primarily by infiltration along higher elevations and typically discharges into streams or other surface water bodies. The elevation of
the shallow water table is transient and can vary with seasonal fluctuations in precipitation. Movement of shallow groundwater is generally from higher to lower elevations. 3.0 RECEPTOR INFORMATION 3.1 Water Supply Wells On August 10, 2015, ECS conducted a receptor survey update for the subject site. ECS observed two water supply well houses (WSW-1 and WSW-6) within 500 feet of the subject site and two
water supply wells (WSW- 5 and WSW-7) within 1,000 feet of the subject site (Figure 4). ECS spoke with Ms. Shonda, a representative of Aqua who confirmed that the subject site utilizes municipal water obtained from the community water supply well (WSW-1) located approximately
350 feet west and topographically upgradient of the site. Aqua also confirmed that the community water supply well WSW-1 supplies water to the residences within Cedar Terrace. Water supply well WSW-1 is maintained by Aqua who indicated that WSW-1 is sampled regularly for VOCs. ECS spoke with Ms. Jean Williams, the owner of the properties associated with water supply wells
WSW-5 through WSW-7, who confirmed that the water supply wells are active and are sampled regularly by an unknown company. ECS was not provided with laboratory reports from this testing. During the March 2019 sampling event, it appeared several residences west of the subject site
appeared to be vacant and/or abandoned.

3.2 Public Water Supplies

ECS contacted Chatham County Public Works Utilities and Water Division to inquire if municipal water is available for the subject site and surrounding area. According to Chatham County personnel and the Chatham County GIS website, municipal water supply lines are located on Manns Chapel Road and NC Highway 15/501 which can supply municipal water to the subject site and surrounding area. The commercial properties located east of the subject site and some residences south and west of the subject site are currently connected to the municipal water supply.
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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3.3 Surface Water
As determined from the USGS Topographic Map, Farrington, North Carolina Quadrangle dated 1993 (Figure 1), the site is at an approximate elevation of 550 feet above mean sea level. Surface runoff on the site is generally to the southeast.
3.4 Subsurface Structures
ECS did not identify subsurface structures associated with the subject site.
3.5 Land Use

The subject site is developed with a commercial property and currently operates as a convenience store and gasoline station. The surrounding area is a mixture of residential and commercial properties.
3.6 Property Owners and Occupants
The Chatham County GIS website was utilized to identify the adjacent property owners. The names and addresses of the owners of adjacent properties and properties located within 500 feet of the site are shown on Table 3.
4.0 FILE REVIEW
A separate leaking gasoline UST site, identified as “the Pantry #294” (Incident #22718) (Facility ID #0-021416) is located across Manns Chapel Road, approximately 270 feet from the subject site.
ECS obtained and reviewed the Withers and Ravenel (WR) May 2013 Groundwater Monitoring Report and found that WR concluded that several VOCs were identified above their respective NC2LGWQS. WR reported, “The most concentrated contaminant area appears to be around
MW-3. MW-3 and deep well MW-4 were the only wells with contaminants exceeding 15A NCAC 2L groundwater standards.” Additionally, no analyzed VOCs were detected above their respective GCL. As shown in Figure 5, off-site monitoring wells MW-3 and deep well MW-4 associated with the Pantry #294 site are located near the eastern portion of the adjacent site. ECS determined
that it is unlikely that the current and former USTs located at the Pantry #294 have impacted the subject site based on the eastern plume delineation. 5.0 FIELD ACTIVITIES 5.1 AVFR Activities

On February 20, 2019, ECS contracted with Zebra Environmental & Industrial Services (Zebra) to conduct an AFVR event at the site using monitoring well MW-3 as an extraction point. Prior to the event, ECS did not measure free product in monitoring well MW-3. Zebra connected the
AFVR recovery pump and vacuum truck to monitoring well MW-3, and ran from 0845 through 1645 (8 hours). A total of 563 gallons of petroleum-impacted groundwater was removed from the monitoring well. The field measurements and calculations are summarized in Tables 4 and 5. ECS personnel field notes for the AFVR event are included in Appendix A. Site photographs
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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are included in Appendix B.
5.2 Monitoring Well Sampling and O-Sox Deployment
On March 6, 2019, ECS collected a field blank and groundwater samples from monitoring wells MW-1 through MW-8 (Figure 5). Purging and sampling of monitoring wells were accomplished using a disposable bailer. ECS collected geochemical measurements at each well for each well
volume purged using a YSI-556 multi-parameter meter. Geochemical measurements are shown in Table 6. Groundwater Monitoring Well Sampling Data sheets and Personnel Field Notes are provided in Appendix A. Site Photographs are included in Appendix B.
After purging the well, the groundwater samples were transferred into sample containers provided by the laboratory. The sample containers were labeled with ECS project number, sample identification, sample date and time, and requested analytical analysis. The containers were
placed into protective packaging material and placed into a cooler with ice to maintain the
samples at approximately 4° Celsius (C°). The samples were submitted to Con-test Analytical Laboratory located in East Longmeadow, MA for chemical analysis for VOCs using Standard Method 6200B. ECS maintained proper COC procedures throughout the sample collection and transportation process. Copies of the COC are included in Appendix C.
Before site departure on March 6, 2019, ECS deployed an O-Sox remedial device in monitoring well MW-3.
6.0 RESULTS
6.1 Free Product Characterization Type(s) of material released Gasoline
Summary of Free Product Recovery During the AFVR event on February 20, 2019, ECS recorded field measurements from the AFVR exhaust to calculate the free product as emissions. ECS collected a measurement of the
exhaust stack diameter and measurements of exhaust velocity, temperature and VOC concentrations. ECS used these measurements to calculate a mass-removal rate in pounds per hour. ECS then converted the mass-removal rate to gallons of free product at a ratio of 7.50
pounds per gallon of free product, in accordance with the Guidelines. This calculation is based on the molecular weight of gasoline and the weight of carbon in a gasoline molecule. The field measurements and calculations are summarized in Tables 4 and 5.
Estimated Quantity of Free Product (Liquid) Recovered The AFVR event recovered 563 total gallons of petroleum impacted groundwater.
Estimated Quantity of Free Product Emissions An estimated total of 20.59 pounds (2.75 gallons) of free product were emitted as vapor during the AFVR event. Emissions calculations are summarized in Tables 4 and 5.

Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B

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Permitting Petroleum emissions associated with AFVR are not required to have air permits in North Carolina. Therefore, no permits were issued.
Disposition of Recovered Free Product Recovered groundwater was disposed of by Zebra Environmental & Industrial Services at their waste disposal facility in Salisbury, North Carolina. The waste disposal manifest is included in
Appendix D. 6.2 Groundwater Flow Direction On March 6, 2019, ECS contracted with Bateman Civil Survey (Bateman) to conduct a
professional survey of the top of casing measurements for the site monitoring wells. The surveying data collected provided by Bateman is included in Appendix E. ECS measured the depth to groundwater in each of the wells (Table 7) and used this data to calculate groundwater flow direction.
The calculated groundwater flow direction is generally to the southeast across the site as determined between on-site monitoring wells MW-1 through MW-8. A potentiometric flow map
for the subject site is depicted as Figure 6. A 2013 potentiometric flow map for the adjacent Pantry #294 site (Figure 7) depicts groundwater flow northeast. 6.3 Monitoring Well Sampling Laboratory analysis reported benzene at a concentration above its GCL in monitoring well MW-3. Laboratory analysis reported several additional targeted analytes at concentrations above their
respective NC2LGWQS but below their respective GCL in the groundwater sample collected from monitoring well MW-3. Laboratory analysis reported MTBE at a concentration above its NC2LGWQS but below its GCL
in the groundwater samples collected from monitoring wells MW-1 and MW-2 Laboratory analysis reported several targeted analytes at concentrations above their respective NC2LGWQS but below their respective GCL in the groundwater samples collected from monitoring wells MW-1, MW-2, and MW-4. Laboratory analysis reported several targeted analytes at concentrations above their respective
laboratory reporting limits but below their respective NC2LGWQS in the groundwater samples collected from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-7, and MW-8. Laboratory analysis reported acetone at a concentration above its laboratory reporting limit but below its NC2LGWQS in the field blank. The concentration was denoted with a J-Flag, which is an estimated concentration. Acetone is a common laboratory artifact and ECS considers this detection to be a laboratory contaminant.
A summary of the current groundwater laboratory analytical results is included in Table 8 and depicted on Figure 8. Historical analytical data from groundwater assessment is included in Table
Environmental Services Report – Petro Mart # 4 11455 NC Highway 15/501 North Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274 NCDEQ Contract: N17006 ECS Project: 49:6230-B
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9.The laboratory data sheets and COC are included in Appendix C. Using the laboratoryanalytical results of the groundwater samples collected from the groundwater monitoring wells,isoconcentration maps showing the horizontal extent for benzene, which was detected above the
NC2LGWQS, is included as Figure 9.
7.0 CONCLUSIONS
Based on the results of this Environmental Services Report, ECS concludes the following:
•Based on the survey data the groundwater flow direction is generally to the southeastacross the site.
•Laboratory analysis detected benzene at a concentration above its GCL in the groundwatersample collected from monitoring well MW-3.
•Laboratory analysis detected several targeted analytes above their respective NC2LGWQS,but did not exceed their respective GCL in monitoring wells MW-1, MW-2, MW-3, and MW-4.
•An estimated total of 20.59 pounds (2.75 gallons) of free product was emitted as vaporduring the AFVR event. The AFVR event was marginally effective and did not significantly
reduce contaminant concentrations in the groundwater samples collected from monitoringwell MW-3. ECS concludes, AFVR events may not be a suitable remediation option for thissite.
•The majority of soil contamination appears to be present at a depth ranging from 14 feet to20 feet below ground surface; therefore, ECS concludes that the excavation of
contaminated soil is not feasible due to the close proximity of the site building and NCDOTRight-of-Way in relation to the former UST basin.
8.0 RECOMMENDATIONS
Based on the findings of this Environmental Services Report, ECS recommends the following:
•Obtain an access agreement to install two monitoring wells on the adjacent property to thesouth of subject site (See Figure 5). Based on review of the draft report, NCDEQ
recommended installing two additional monitoring wells near the locations of monitoringwells MW-4 and MW-7 25 to 30 feet below the existing monitoring wells.
•Conduct an updated receptor survey to determine the current status of the water supplywells in the area. It was observed that several houses appeared to be vacant in the area.
•Sample the two new monitoring wells and the eight existing monitoring wells.
•If funds are available, ECS recommends conducting an injection near monitoring wells MW-3, MW-4, MW-6, and MW-7 to promote the degradation of petroleum constituents in the sitegroundwater.
FIGURES
SOURCE:
USGS TOPOGRAPHIC MAP
FARRINGTON
NC QUADRANGLE
DATED 1993
SCALE: 1 : 24,000
FIGURE 1
SITE LOCATION MAP
PETRO MART #4
11455 NC HWY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
SITE
FIGURE 2
AERIAL SITE MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
Scale: 1 inch = 170 feet
SITE
COMMERCIAL
SINGLE-FAMILY
RESIDENCES
SINGLE-FAMILY
RESIDENCES
THE PANTRY #294
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Soil Sample Boring
Approximate Location of Former USTs
Approximate Location of Current USTs
SOURCE:
CHATHAM COUNTY GIS
DATED 2017
SCALE AS SHOWN
FIGURE 3
2018 SOIL SAMPLE LOCATION MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
Scale: 1 inch = 60 feet
MW-1
MW-2
MW-5MW-6
MW-3 MW-4
MW-7
MW-8
MW-1
SS-1
MW-6
MW-5
MW-8
MW-7
MW-4
MW-1
MW-2
MW-3
SS-1SS-2
SS-11SS-10
SS-8
SS-9
SS-3SS-4SS-5
SS-7
SS-6
SS-12
SOURCE:
CHATHAM COUNTY GIS
DATED 2017
SCALE AS SHOWN
FIGURE 4
WATER SUPPLY WELL LOCATION MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
Scale: 1 inch = 400 feet
LEGEND
Approximate Location of Water Supply Well
Approximate Location of Fire Hydrant
WSW-1
500 ft.
Radius
1,000 ft.
Radius
SITE
WSW-1
WSW-6
WSW-7
WSW-5
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 5
MONITORING WELL LOCATION MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
Scale: 1 inch = 80 feet
MW-1
MW-2
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Proposed Monitoring Well
Approximate Location of Former USTs
Approximate Location of Current USTs
MW-1
MW-5MW-6
MW-3 MW-4
MW-7
MW-8
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 6
GROUNDWATER ELEVATION MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
Scale: 1 inch = 80 feet
LEGEND
Approximate Location of Monitoring Well
Groundwater Elevation
Groundwater Contour Line
Estimated Groundwater Contour Line
Estimated Direction of Groundwater Flow
MW-1
520.82
MW-4
521.44
Approximate Location of
Current USTs
MW-7
522.04
MW-3
520.82
MW-8
522.67
522
MW-6
522.02
MW-5
521.30
MW-1
521.13
MW-2
521.41
521
Approximate Location of
Former USTs
FIGURE 7
PANTRY #294 SITE MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
SOURCE:
Withers and Ravenel (WR) May 2013
Groundwater Monitoring Report
SCALE AS SHOWN
SITE
COMMERCIAL
SINGLE-FAMILY
RESIDENCES
THE PANTRY 294
MW-3
MW-4
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 8
GROUNDWATER CONCENTRATION MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
Scale: 1 inch = 80 feet
MW-5
BRL
MW-6
BRL
MW-1
Diisopropyl ether 0.43 J
Methyl tert-butyl ether 41
MW-2
Diisopropyl ether 7.3
Methyl tert-butyl ether 100
MW-4
Benzene 420
Diisopropyl ether 77
Toluene 4.5 J
Ethylbenzene 28
Isopropylbenzene 1.3 J
Naphthalene 36
n-Propylbenzene 2.0 J
1,2,4-Trimethylbenzene 48
1,3,5-Trimethylbenzene 20
Total Xylenes 271
Methyl tert-butyl ether 830
MW-8
1,4-Dichlorobenzene 0.23 J
Methyl tert-butyl ether 3.6
Toluene 0.43 J
LEGEND
Approximate Location of Monitoring Well
3.6 Concentrations Above Laboratory Reporting
Limits (µg/L)
290 Bold Concentrations Above NC2LGWQS (µg/L)
28,000 Bold Underlined Concentrations Above GCL (µg/L)
BRL Below Reporting Limit
J Estimated Concentration
MW-1
MW-7
Benzene 0.17 J
1,4-Dichlorobenzene 0.50
Methyl tert-butyl ether 3.9
Toluene 0.65
Total Xylenes 0.31 J
MW-3
Acetone 10,000 J
Benzene 28,000
2-Butanone (MEK)2,700
Diisopropyl ether 290
Isopropylbenzene 100 J
Toluene 43,000
Ethylbenzene 3,300
Naphthalene 1,900
1,2,4-Trimethylbenzene 2,400
1,3,5-Trimethylbenzene 560
Total Xylenes 16,600
Methyl tert-butyl ether 7,200
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 9
MTBE ISOCONCENTRATION MAP
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-3274
ECS PROJECT: 49:6230-B
MW-3
Scale: 1 inch = 80 feet
LEGEND
Approximate Location of Monitoring Well
MTBE Isoconcentration Contour (µg/L)
830 Bold Concentration Above NC2LGWQS
BRL Below Reporting Limit
MW-1
MW-5
BRL
MW-6
BRL
Approximate Location of
Former USTs
Approximate Location of
Current USTs
MW-2
100
20MW-1
41
MW-8
3.6
MW-7
3.9
MW-3
7,200
MW-4
830
8,000
200
2,000
TABLES
UST ID
Number
Last
Contents
Previous
Contents
Capacity
(in Gallons)
Construction
Details
Tank
Dimensions
Installation
Date
Removal
Date Status
1 Kerosene Kerosene 2,000 Unknown 12.0' x 5.33' 11/10/1986 3/7/2001 Removed
2 Diesel Diesel 3,000 Unknown 12.0' x 5.33' 11/10/1986 3/7/2001 Removed
3 Gasoline Gasoline 6,000 Unknown 16.16' x 8.0' 11/10/1986 3/7/2001 Removed
4 Gasoline Gasoline 8,000 Unknown 20.66' x 8' 11/10/1986 3/7/2001 Removed
5 Gasoline Gasoline 8,000 Unknown 20.66' x 8' 11/10/1986 3/7/2001 Removed
6 Gasoline Gasoline 12,000 Unknown Unknown May 2001 Current Current
7 Gasoline Gasoline 8,000 Unknown Unknown May 2001 Current Current
8 Diesel Diesel 6,000 Unknown Unknown May 2001 Current Current
Chapel Hill, Chatham County, North Carolina
ECS Project: 49:6230-B
Table 1
UST Information
Petro Mart #4
11455 NC Highway 15/501 North
NCDEQ Incident: 3274
PARAMETER
Sample ID SS-1A SS-1B SS-2A SS-2B SS-1A SS-1B SS-2A SS-2B SS-3A SS-3B SS-4A SS-4B SS-5A SS-5B SS-6A SS-6B SS-7A SS-7B SS-8A SS-8B SS-9A SS-9B SS-10A SS-10B SS-11A SS-11B SS-12A SS-12B
Collection Date
Sample Depth (ft bgs)3-5 8-10 3-5 8-10 11.5-13.5 18.5-19.5 14.0-15.0 18.5-19.5 14.0-15.0 18.5-19.5 14.0-15.0 18.5-19.5 13.0-14.0 18.5-19.5 8.5-9.5 18.5-19.5 8.5-9.5 18.5-19.5 8.5-9.5 18.5-19.5 14.5-15.5 18.5-19.5 9.0-13.0 18.5-19.5 4.0-14.0 18.5-19.5 9.0-10.0 18.5-19.5
PID Reading (ppm)NA NA NA NA 3.2 7.2 8.4 5.7 38.0 40.8 33.7 24.5 21.7 22.1 20.0 18.4 0.4 5.1 2.2 68.0 9.5 62.7 25.2 41.1 33.3 31.3 6.6 33.8
Benzene BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.8 BRL 3.1 BRL 0.0064 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.0056 18 164
n-Butylbenzene BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.30 8.5 20.8 17.2 40.7 BRL 0.13 BRL BRL BRL BRL BRL BRL BRL 0.50 2.3 18.2 BRL BRL 4.3 626 16,350
Methylene chloride BRL BRL 0.032 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.02 85 763
Methyl-tert-butyl ether BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.010 BRL 0.011 0.0058 0.020 BRL 0.032 BRL BRL BRL BRL BRL BRL 0.091 350 3,100
sec-Butylbenzene BRL BRL BRL BRL BRL BRL BRL BRL 0.99 BRL 2.0 4.4 3.5 8.3 BRL 0.023 BRL BRL BRL BRL BRL BRL BRL BRL 0.55 4.7 BRL BRL 3.3 626 16,350
Isopropylbenzene BRL BRL BRL BRL BRL BRL BRL BRL 1.7 BRL 2.8 10.6 4.8 19.8 BRL 0.024 BRL BRL BRL BRL BRL BRL BRL BRL 0.71 8.9 BRL BRL 1.7 1,564 40,880
Ethylbenzene BRL BRL BRL BRL BRL BRL BRL BRL 10.8 0.32 11.0 101 27.4 176 BRL 0.12 BRL BRL BRL BRL 0.0062 BRL BRL BRL 2.7 42.7 BRL BRL 4.9 1,560 40,000
p-Isopropyltoluene BRL BRL BRL BRL BRL BRL BRL 1.6 3.6 0.18 5.3 BRL 9.0 20.8 BRL 0.066 BRL BRL BRL BRL BRL BRL 0.012 BRL 1.5 11.7 BRL BRL 0.12 100 4,000
Naphthalene BRL BRL BRL BRL BRL BRL BRL 10.7 14.1 1.2 30.0 121 48.6 149 BRL BRL BRL BRL BRL 0.024 0.038 0.081 0.56 3.3 8.6 45.3 BRL 0.059 0.16 313 8,176
Acetone BRL BRL BRL BRL BRL BRL BRL 31.0 11.8 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 24 14,000 360,000
n-Propylbenzene BRL BRL BRL BRL BRL BRL BRL 2.3 7.3 0.34 11.6 44.7 25.4 90.3 BRL 0.12 BRL BRL BRL BRL BRL BRL 0.0098 BRL 3.2 BRL BRL BRL 1.7 626 16,350
Toluene BRL BRL BRL BRL BRL BRL BRL BRL 6.9 0.20 3.0 170 16.6 245 BRL 0.11 BRL BRL BRL 0.0096 BRL 0.012 BRL BRL 0.60 22.6 BRL BRL 4.3 1,200 32,000
1,2,3-Trichloropropane BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS NS NS
1,2,4-Trimethylbenzene BRL BRL BRL BRL BRL BRL BRL 21.2 59.1 3.3 100 272 182 592 BRL 0.23 BRL BRL BRL 0.0064 0.039 0.022 0.15 3.0 24.3 190 0.0073 0.0062 8.5 782 20,440
1,3,5-Trimethylbenzene BRL BRL BRL BRL BRL BRL BRL 6.2 18.3 0.96 29.9 81.8 51.7 177 BRL BRL BRL BRL BRL BRL 0.010 BRL 0.036 0.80 7.4 57.7 BRL BRL 8.5 782 20,440
Total Xylenes BRL BRL BRL BRL BRL BRL BRL 7.0 61.4 2.4 66.3 506 128 943 BRL BRL BRL BRL BRL BRL 0.017 0.022 0.023 0.32 15.5 234 BRL BRL 4.6 3,129 81,760
All Other VOCs BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1-Methylnaphthalene NS NS NS NS BRL BRL BRL 7.1 6.0 BRL 7.8 23.5 21.5 25.2 BRL 0.51 BRL BRL BRL BRL BRL BRL BRL 1.3 1.8 11.5 BRL BRL 0.004 20 100
2-Methylnaphthalene NS NS NS NS BRL BRL BRL 13.8 12.0 0.63 15.5 64.5 45.0 54.9 BRL 0.96 BRL BRL BRL BRL BRL BRL 0.73 2.6 3.8 24.6 BRL BRL 3.6 63 1,635
Naphthalene NS NS NS NS BRL BRL BRL 12.2 10.3 0.63 14.3 62.7 34.4 59.6 BRL 0.44 BRL BRL BRL BRL BRL BRL BRL 1.6 3.3 24.7 BRL BRL 0.16 313 8,176
Phrenanthene NS NS NS NS BRL BRL BRL 0.65 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 56 469 12,264
All other SVOCs NS NS NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
Aliphatics (C5-C8)NS NS NS NS BRL BRL BRL 10.3 31.9 BRL 166 736 113 573 BRL BRL BRL BRL BRL BRL BRL BRL BRL 7.6 70.7 118 BRL BRL 68 939 24,528
Aliphatics (C9-C18)NS NS NS NS BRL BRL 2.8 422.1 287 6.8 576 1,353 868 1,900 BRL 5.7 BRL BRL BRL BRL BRL BRL 3.2 15.3 337 898 BRL BRL 540 1,500 40,000
Aliphatics (C19-C36)NS NS NS NS BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Immobile 31,000 810,000
Aromatics (C9-C22)NS NS NS NS BRL BRL 5.2 220.7 272 4.8 539 1,154 896 1,993 BRL BRL BRL BRL BRL BRL BRL BRL 3.4 9.8 318.2 509 BRL BRL 31 469 12,264
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
mg/kg = Milligrams per Kilogram
Underlined = Detected above the Soil-to-Water Maximum Contaminant Concentration and Residential Soil Cleanup Level
Bold = Detected above the Action Level or Soil-to-Water Maximum Contaminant Concentration
BRL = Below Laboratory Reporting Limit
NS = Not Standard
NA = Not Applicable
Soil-to-Water
Maximum
Contaminant
Concentration
Residential
Soil
Cleanup
Level
Industrial/
Commercial
Soil Cleanup
Level
Table 2
Summary of Historical Soil Analytical Results
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: 3274
ANALYTICAL RESULTS
4/15/2015
NCDEQ = North Carolina Department of Environmental Quality
11/5/2018
Volitile Petroluem Hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons (EPH) by MADEP
ECS Project: 49:6230-A
Volatile Organic Compounds (VOCs) by EPA Method 8260
--
Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270
--
Water Supply
Well ID Well Owner / Address**Well Address Well Use
Well Depth
(ft bgs)Type of Well
Approximate Distance
from Source Area of
Release (ft)
WSW-1
Jean Williams (AQUA)
PO Box 429
Carrboro, NC 27510
Cedar Terrace Chapel
Hill, NC 27514 Potable Unknown Drilled
Approximately
380 ft west
WSW-5
Jean Williams
PO Box 429
Carrboro, NC 27510
29 Cedar Lake Road
Chapel Hill, NC 27514 Potable Unknown Drilled
Approximately
680 ft west
WSW-6
Cheryl Curl Atwater and Toni Buck Curl
709 Reserve Estates Drive
Wake Forest, NC 27586
Cedar Village Road
Chapel Hill, NC 27514 Unknown Unknown Drilled
Approximately
280 ft southwest
WSW-7
Cheryl Curl Atwater and Toni Buck Curl
709 Reserve Estates Drive
Wake Forest, NC 27587
103 Cedar Village Road
Chapel Hill, NC 27514 Unknown Unknown Drilled
Approximately
930 ft southwest
** ECS confirmed ownership details via Chatham County GIS on November 15, 2018.
ECS Project: 49:6230-B
Table 3
Water Supply Well Survey
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: TF-3274
IDENTIFY THE WELL AND THE I.D. OF EACH WELL USED FOR AFVR:
PROVIDE BLOWER SPECIFICATIONS OF THE VACUUM TRUCK (cfm @ in Hg): See Attached
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS
Qstd
(ft3/min)
0:15 -20 2027 135 21.3 <0.1% 318
0:30 -22 2126 155 33.2 <0.1% 323
0:45 -22 2080 155 37.4 <0.1% 316
1:00 -22 1712 155 40.0 <0.1% 260
1:15 -22 1960 160 27.2 <0.1% 295
1:30 -22 1870 160 10.2 <0.1% 281
1:45 -22 2126 235 8.9 <0.1% 285
2:00 -22 2106 240 9.6 <0.1% 281
2:30 -23 1820 245 8.7 <0.1% 241
3:00 -23 2067 245 8.2 <0.1% 274
3:30 -23 1909 245 8.3 <0.1% 253
4:00 -23 1968 245 8.1 <0.1% 260
4:30 -23 2086 250 8.3 <0.1% 274
5:00 -24 2025 250 8.4 <0.1% 266
5:30 -24 2068 248 8.5 <0.1% 273
6:00 -24 2086 250 8.4 <0.1% 274
6:30 -25 2244 249 8.1 <0.1% 295
7:00 -24 2204 250 8.1 <0.1% 290
7:30 -24 2765 250 8.1 <0.1% 363
8:00 -24 1988 250 8.0 <0.1%261
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart
EQUATION
Qstd (ft3/min) = (1-Water Vapor) * velocity (ft/min) * (PI * (diameter(in)/24)^2) * (528R°/(Temp + 460°))
Vacuum (in
Hg)
Velocity
(ft/min)
Pipe ID
(in)Temp (°F)
Table 4
Aggressive Fluid Vapor Recovery Measurements
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: 3274
Rel Humid
(%)
Water Vapor
(%)
2/14/2019 6
ECS Project: 49:6230-B
MW-3
START OF TEST: 0845
Date Elapsed
Time
IDENTIFY THE WELL AND THE I.D. OF EACH WELL USED FOR AFVR:
PROVIDE BLOWER SPECIFICATIONS OF THE VACUUM TRUCK (cfm @ in Hg): See Attached
START OF TEST: 0845
EMISSION CALCULATIONS
Elapsed Interval
Time PPM measured K PPMc Cg:m Cc PMRc PMRg PMR
(min) (ppm) (#C - gas)(mg/dsm^3) (lb/dscf) (lb/hr) (lb/hr) (lb)
15 30.1 4 120.40 1000 62.5E-6 0.35 0.82 0.204
30 9.7 4 38.80 322 20.1E-6 0.20 0.47 0.118
45 16.2 4 64.80 538 33.6E-6 0.37 0.87 0.218
60 56.1 4 224.40 1865 116.4E-6 0.97 2.28 0.569
75 33.3 4 133.20 1107 69.1E-6 0.60 1.40 0.351
90 56.4 4 225.60 1875 117.0E-6 0.98 2.30 0.576
135 70.8 4 283.20 2353 146.9E-6 1.11 2.60 1.947
150 35.5 4 142.00 1180 73.7E-6 0.60 1.39 0.349
165 86.7 4 346.80 2882 179.9E-6 1.53 3.58 0.894
180 59.0 4 236.00 1961 122.4E-6 1.01 2.36 0.591
210 33.4 4 133.60 1110 69.3E-6 0.66 1.54 0.769
240 56.7 4 226.80 1885 117.6E-6 1.38 3.23 1.617
270 75.0 4 300.00 2493 155.6E-6 1.82 4.25 2.127
300 27.8 4 111.20 924 57.7E-6 0.67 1.57 0.786
330 14.0 4 56.00 465 29.0E-6 0.36 0.84 0.422
360 3.1 4 12.40 103 6.4E-6 0.07 0.17 0.086
390 58.5 4 234.00 1944 121.4E-6 1.52 3.56 1.779
420 260.0 4 1040.00 8641 539.5E-6 5.29 12.37 6.185
450 14.8 4 59.20 492 30.7E-6 0.34 0.79 0.790
480 3.9 4 15.60 130 8.1E-6 0.09 0.21 0.214
Total emissions in pounds 20.59
Total emissions in gallons 2.75
NOTES
PPM measured = Actual measurements (ppm) taken with a PID at the blower discharge piping
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, Isobutylene K = 4, or Hexane K = 6)
PPMc = PPMv, Volumetric concentration as gasoline emission, dry basis at STP
Cc:m = mg/dsm3, mass concentration of gasoline emission
Mg = 200 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant) *
Mc = 12.01mg/mg-mole, molecular weight of carbon
K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP
Cc = lb/dcsf, mass concentration of VOC emissions as carbon, dry basis at STP
PMRc = lb/hr, pollutant mass removal rate as carbon
PMRg = pollutant mass removal of gasoline
PMR = pollutant mass removal of gasoline for the elapsed time interval
Mcg = 85.5 mg/mg-mole, weight of carbon in gasoline molecule
EQUATIONS
PPMc = PPM measured * K PMRc = Cc * Qstd * 60 min/hr
Cg:m = PPMc * (Mg / K3)PMRg=PMRc(Mg/Mcg)
Cc = Cg:m * 62.43E-09 lb-m^3/mg-ft^3 PMR = PMRg * ((T2 - T1) / 60)
Note: Equations obtained from Appendix A, Section 2.1 (A) of Groundwater Section Guidelines for the Investigation
and Remediation of Soil and Groundwater, Volume II, Petroleum Underground Storage Tanks, January 2, 1998.
ECS Project: 49:6230-B
MW-3
Table 5
Aggressive Fluid Vapor Recovery Calculations
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: 3274
SAMPLE ID MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8
Date Sampled
pH 7.95 8.10 8.20 8.08 8.03 8.45 8.32 8.13
Temperature (oC)18.04 18.49 18.15 18.81 18.05 17.07 17.18 16.23
Conductivity (mS/cm) 0.126 0.111 0.259 0.351 0.127 0.215 0.225 0.298
Dissolved O2 (mg/L) 3.41 2.79 5.52 5.30 6.01 7.01 5.16 5.24
Turbidity (Observed)ST ST ST ST T T VT T
Notes:
mS/cm = milliseimens per centimeter
mV = millivolts
°C = degress Celsius
VT= Very Turbid
T= Turbid
ST= Slightly Turbid
mg/L= milligrams per Liter
Measured using YSI model 560 Meter
3/6/2019
ECS Project: 49:6230-B
Table 6
Geochemical Measurements
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: 3274
Monitoring
Well ID
Date
Measured
Depth to
Groundwater
(ft. btoc)
Date
Installed
Total Well
Depth
(ft. btoc)
Screen
Interval
(ft. btoc)
TOC
Elevation*
Groundwater
Elevation (ft)
MW-1 3/6/2019 32.30 4/15/2015 55 40-55 553.43 521.13
MW-2 3/6/2019 31.03 4/15/2015 54 39-54 552.44 521.41
MW-3 3/6/2019 32.21 8/10/2015 49 29-49 553.03 520.82
MW-4 3/6/2019 30.32 8/10/2015 46 26-46 551.76 521.44
MW-5 3/6/2019 32.10 8/10/2015 52 32-52 553.40 521.30
MW-6 3/6/2019 29.92 8/10/2015 52 32-52 551.94 522.02
MW-7 3/6/2019 32.14 11/6/2018 45 30-45 554.18 522.04
MW-8 3/6/2019 29.27 11/6/2018 45 30-45 551.94 522.67
Notes:
ft. btoc = Feet Below Top of Casing
* = Survey performed by Bateman Civil Survey on March 6, 2019. The site vertical datum is based on NAV88 and
the horizontal datum is based on NAD83.
TOC = Top of Casing
Table 7
Monitoring Well Construction and Groundwater Elevation Details
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
ECS Project: 49:6230-B
NCDEQ Incident: 3274
MW-1 3/6/2019 BRL BRL BRL BRL 0.43 J BRL BRL 41 BRL BRL BRL BRL BRL BRL
MW-2 3/6/2019 BRL BRL BRL BRL 7.3 BRL BRL 100 BRL BRL BRL BRL BRL BRL
MW-3 3/6/2019 10,000 J 28,000 2,700 BRL 290 3,300 100 J 7,200 1,900 290 43,000 2,400 560 16,600
MW-4 3/6/2019 BRL 420 BRL BRL 77 28 1.3 J 830 36 2.0 J 4.5 J 48 20 271
MW-5 3/6/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-6 3/6/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-7 3/6/2019 BRL 0.17 J BRL 0.50 BRL BRL BRL 3.9 BRL BRL 0.65 BRL BRL 0.31 J
MW-8 3/6/2019 BRL BRL BRL 0.23 J BRL BRL BRL 3.6 BRL BRL 0.43 J BRL BRL BRL
Field Blank 3/6/2019 12 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
6,000 1 4,000 6 70 600 70 20 6 70 600 400 400 500
6,000,000 5,000 4,000,000 6,000 70,000 84,500 25,000 20,000 6,000 30,000 260,000 28,500 25,000 85,500
Notes:
J = Estimated Concentration
Table 8
Summary of Current Groundwater Analytical Results
Petro Mart #4
11455 NC Highway 15/501 North
Chapel Hill, Chatham County, North Carolina
NCDEQ Incident: 3274
BRL = Below Laboratory Reporting Limit Methyl-tert-butyl-etherSample Date
NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012
(µg/L) = Micrograms per Liter
Bold = Reported above the NC2LGWQS
GCL (µg/L)
NC2LGWQS (µg/L)BenzeneIsopropylbenzeneNaphthalene1,3,5- TrimethylbenzeneDiisopropyl etherSample ID 1,4-DichlorobenzeneAcetoneStandard Method 6200B
2-Butanone (MEK)Underline = Reported above the NC2LGWQS and GCL
ECS Project: 49:6230-B
EthylbenzeneAnalytical Method
n-PropylbenzeneToluene1,2,4-TrimethylbenzeneTotal Xylenes
Sample ID Date Collected
*MW-1 2/8/1995 BRL 1,800 BRL BRL BRL 3,400 300 BRL BRL BRL BRL BRL BRL 760 1,200 BRL BRL
*MW-2 2/8/1995 BRL 1.0 BRL BRL BRL 1.6 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
4/16/2015 BRL BRL BRL BRL 0.90 BRL BRL BRL BRL BRL BRL BRL BRL BRL 53.5 12,830 BRL
8/12/2015 BRL BRL BRL BRL 1.2 BRL BRL BRL BRL BRL BRL BRL BRL BRL 76.5 BRL BRL
3/7/2018 BRL BRL BRL BRL 0.64 BRL BRL BRL BRL BRL BRL BRL BRL BRL 53 BRL BRL
11/5/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 37.2 BRL BRL
3/6/2019 BRL BRL BRL BRL 0.43 J BRL BRL BRL BRL BRL BRL BRL BRL BRL 41 BRL BRL
4/16/2015 BRL 73.3 BRL BRL 17.3 0.64 2.7 1.7 BRL 1.4 BRL 6.2 BRL 83.8 296 BRL BRL
8/12/2015 BRL BRL BRL BRL 13.5 BRL BRL BRL BRL BRL BRL BRL BRL BRL 250 BRL BRL
3/7/2018 BRL BRL BRL BRL 9.9 BRL BRL BRL BRL BRL BRL BRL BRL BRL 130 BRL BRL
11/5/2018 BRL BRL BRL BRL 6.9 BRL BRL BRL BRL BRL BRL BRL BRL BRL 84.4 BRL BRL
3/6/2019 BRL BRL BRL BRL 7.3 BRL BRL BRL BRL BRL BRL BRL BRL BRL 100 BRL BRL
8/12/2015 BRL 29,900 BRL BRL 229 32,800 1,860 50.3 733 188 34.4 1,350 340 9,140 22,700 BRL BRL
3/7/2018
11/5/2018 BRL 31,900 BRL BRL 130 38,700 2,880 BRL 758 BRL BRL 2,150 BRL 13,830 7,760 BRL BRL
3/6/2019 10,000 J 28,000 2,700 BRL 290 43,000 3,300 100 J 1,900 290 BRL 2,400 560 16,600 7,200 BRL BRL
8/12/2015 BRL 1,410 BRL BRL 296 1,680 98.9 BRL 26.2 7.5 BRL 306 124 2,497 4,950 BRL BRL
3/7/2018 BRL 1,200 BRL BRL 160 620 74 3.6 J BRL 11 BRL 200 74 1,730 2,100 320 47 J
11/5/2018 BRL 309 BRL BRL 76.4 24.3 37 BRL 10.1 BRL BRL 47.9 BRL 311 834 BRL BRL
3/6/2019 BRL 420 BRL BRL 77 4.5 J 28 1.3 J 36 2.0 J BRL 48 20 271 830 BRL BRL
8/12/2015 BRL 1.3 BRL BRL BRL 2.8 0.53 BRL BRL BRL BRL BRL BRL 2.55 BRL BRL BRL
3/7/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
11/5/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
3/6/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
8/12/2015 BRL 2.4 BRL BRL BRL 5.2 0.76 BRL BRL BRL BRL BRL BRL 3.7 0.76 BRL BRL
3/7/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
11/5/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
3/6/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
11/8/2018 BRL BRL BRL 0.9 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 5.1 BRL BRL
3/6/2019 BRL 0.17 J BRL 0.50 BRL 0.65 BRL BRL BRL BRL BRL BRL BRL 0.31 J 3.9 BRL BRL
11/8/2018 BRL BRL BRL 0.57 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 4.8 BRL BRL
3/6/2019 BRL BRL BRL 0.23 J BRL 0.43 J BRL BRL BRL BRL BRL BRL BRL BRL 3.6 BRL BRL
6,000 1 4,000 6 70 600 600 70 6 70 70 400 400 500 20 40 100
6,000,000 5,000 4,000,000 6,000 70,000 260,000 84,500 25,000 6,000 30,000 70,000 28,500 25,000 85,500 20,000 40,000 100,000
Notes:
J = Estimated Concentration
BRL = Below Laboratory Reporting
GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012 2-Hexanone4-Methyl-2-pentanone (MIBK)Bold = Reported above the NC2LGWQS or NCDEQ Final and Interim GWQS Styrene1,3,5-Trimethylbenzene1,4-DichlorobenzeneTotal XylenesNC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
MW-1
MW-3
MW-4
NS = Not Sampled
NC2LGWQS (µg/L)
Gross Contamination Level (µg/L)BenzeneTolueneEthylbenzene(µg/L) = Micrograms per Liter
NCDEQ Incident: 3274
ECS Project: 49:6230-B
AcetoneFree Product ≈ 0.36''2-Butanone (MEK)MW-2
* = Monitoring wells were abandoned in March 2001 Diisopropyl etherIsopropylbenzenen-Propylbenzene1,2,4- TrimethylbenzeneUnderline = Reported above the NC2LGWQS and GCL
MW-5
MW-6
MW-7
MW-8 Methyl tert-butyl etherNaphthaleneTable 9
Summary of Historical Groundwater Analytical Results
Petro Mart #4
11455 NC Highway 15/501 North
Analytical Method
Chapel Hill, Chatham County, North Carolina
Standard Method 6200B (or equivalent)
Contaminant of Concern (µg/L)
APPENDIX A
APPENDIX B
SITE PHOTOGRAPHS
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY
NORTH CAROLINA
NCDEQ INCIDENT: 3274
ECS PROJECT NO.: 49:6230-B
Photograph 1: View of the subject site. View is to the southwest.
Photograph 2: View of monitoring well MW-1. View is to the north.
SITE PHOTOGRAPHS
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY
NORTH CAROLINA
NCDEQ INCIDENT: 3274
ECS PROJECT NO.: 49:6230-B
Photograph 3: View of the monitoring well MW-2. View is to the southwest.
Photograph 4: View of the monitoring well MW-3 with free product in bailer. View is to the west.
SITE PHOTOGRAPHS
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY
NORTH CAROLINA
NCDEQ INCIDENT: 3274
ECS PROJECT NO.: 49:6230-B
Photograph 5: View of the monitoring well MW-4. View is to the northwest.
Photograph 6: View of the monitoring well MW-5. View is to the north.
SITE PHOTOGRAPHS
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY
NORTH CAROLINA
NCDEQ INCIDENT: 3274
ECS PROJECT NO.: 49:6230-B
Photograph 7: View of the monitoring well MW-6. View is to the west.
Photograph 8: View of the monitoring well MW-7. View is to the southeast.
SITE PHOTOGRAPHS
PETRO MART #4
11455 NC HIGHWAY 15/501 NORTH
CHAPEL HILL, CHATHAM COUNTY
NORTH CAROLINA
NCDEQ INCIDENT: 3274
ECS PROJECT NO.: 49:6230-B
Photograph 9: View of the monitoring well MW-8. View is to the southeast.
Photograph 10: View of the monitoring well MW-7 and MW-8. View is to the north.
M
APPENDIX C
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 13, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Chatham County
Client Job Number:
Project Number: 49:6230-B
Laboratory Work Order Number: 19C0264
Enclosed are results of analyses for samples received by the laboratory on March 7, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 40
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
19C0264-01 8
19C0264-02 10
19C0264-03 12
19C0264-04 14
19C0264-05 16
19C0264-06 18
19C0264-07 20
19C0264-08 22
19C0264-09 24
Sample Preparation Information 26
QC Data 27
Volatile Organic Compounds by GC/MS 27
B225391 27
B225511 31
Flag/Qualifier Summary 35
Certifications 36
Chain of Custody/Sample Receipt 38
Page 2 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/13/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:6230-B
19C0264
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Chatham County
Field Blank 19C0264-01 Field Blank SM21-22 6200B
MW-1 19C0264-02 Ground Water SM21-22 6200B
MW-2 19C0264-03 Ground Water SM21-22 6200B
MW-3 19C0264-04 Ground Water SM21-22 6200B
MW-4 19C0264-05 Ground Water SM21-22 6200B
MW-5 19C0264-06 Ground Water SM21-22 6200B
MW-6 19C0264-07 Ground Water SM21-22 6200B
MW-7 19C0264-08 Ground Water SM21-22 6200B
MW-8 19C0264-09 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:19C0264-06MW-5
No Results Detected
Client ID:Lab ID:19C0264-07MW-6
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-01Field Blank
DL
Acetone 12 50 g/L SM21-22 6200BJ9.7
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-02MW-1
DL
Diisopropyl Ether (DIPE)0.43 0.50 g/L SM21-22 6200BJ0.18
Methyl tert-Butyl Ether (MTBE)41 0.50 g/L SM21-22 6200B0.090
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-03MW-2
DL
Diisopropyl Ether (DIPE)7.3 0.50 g/L SM21-22 6200B0.18
Methyl tert-Butyl Ether (MTBE)100 0.50 g/L SM21-22 6200B0.090
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-04MW-3
DL
1,2,4-Trimethylbenzene 2400 250 g/L SM21-22 6200B90
1,3,5-Trimethylbenzene 560 250 g/L SM21-22 6200B65
2-Butanone (MEK)2700 2500 g/L SM21-22 6200B1200
Acetone 10000 25000 g/L SM21-22 6200BJ4800
Benzene 28000 250 g/L SM21-22 6200B60
Diisopropyl Ether (DIPE)290 250 g/L SM21-22 6200B90
Ethylbenzene 3300 250 g/L SM21-22 6200B65
Isopropylbenzene (Cumene)100 250 g/L SM21-22 6200BJ60
m+p Xylene 11000 500 g/L SM21-22 6200B130
Methyl tert-Butyl Ether (MTBE)7200 250 g/L SM21-22 6200B45
Naphthalene 1900 1000 g/L SM21-22 6200B60
n-Propylbenzene 290 250 g/L SM21-22 6200B65
o-Xylene 5600 250 g/L SM21-22 6200B66
Toluene 43000 250 g/L SM21-22 6200B85
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-05MW-4
DL
1,2,4-Trimethylbenzene 48 5.0 g/L SM21-22 6200B1.8
1,3,5-Trimethylbenzene 20 5.0 g/L SM21-22 6200B1.3
Benzene 420 5.0 g/L SM21-22 6200B1.2
Diisopropyl Ether (DIPE)77 5.0 g/L SM21-22 6200B1.8
Ethylbenzene 28 5.0 g/L SM21-22 6200B1.3
Isopropylbenzene (Cumene)1.3 5.0 g/L SM21-22 6200BJ1.2
m+p Xylene 210 10 g/L SM21-22 6200B2.6
Methyl tert-Butyl Ether (MTBE)830 5.0 g/L SM21-22 6200B0.90
Naphthalene 36 20 g/L SM21-22 6200B1.2
n-Propylbenzene 2.0 5.0 g/L SM21-22 6200BJ1.3
o-Xylene 61 5.0 g/L SM21-22 6200B1.3
Toluene 4.5 5.0 g/L SM21-22 6200BJ1.7
Page 5 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-08MW-7
DL
1,4-Dichlorobenzene 0.50 0.50 g/L SM21-22 6200B0.15
Benzene 0.17 0.50 g/L SM21-22 6200BJ0.12
m+p Xylene 0.31 1.0 g/L SM21-22 6200BJ0.26
Methyl tert-Butyl Ether (MTBE)3.9 0.50 g/L SM21-22 6200B0.090
Toluene 0.65 0.50 g/L SM21-22 6200B0.17
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19C0264-09MW-8
DL
1,4-Dichlorobenzene 0.23 0.50 g/L SM21-22 6200BJ0.15
Methyl tert-Butyl Ether (MTBE)3.6 0.50 g/L SM21-22 6200B0.090
Toluene 0.43 0.50 g/L SM21-22 6200BJ0.17
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 19C0264-04+05 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Vinyl Acetate
19C0264-01[Field Blank], 19C0264-02[MW-1], 19C0264-03[MW-2], 19C0264-04[MW-3], 19C0264-05[MW-4], 19C0264-06[MW-5], 19C0264-07[MW-6],
19C0264-08[MW-7], 19C0264-09[MW-8], B225391-BLK1, B225391-BS1, B225391-BSD1, B225511-BLK1, B225511-BS1, B225511-BSD1, S033428-CCV1
pH of sample (pH 5) is outside of method specified preservation criteria.
Analyte & Samples(s) Qualified:
PR-08
19C0264-08[MW-7]
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19C0264-04[MW-3], 19C0264-05[MW-4]
Sample poured off into another vial with headspace due to high level of sediment in sample.
Analyte & Samples(s) Qualified:
Z-01
19C0264-08[MW-7]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 7 of 40
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-01
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 3/6/2019 17:25
[TOC_2]19C0264-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
12 50 3/11/19 12:01 EEHg/L9.7 3/8/19SM21-22 6200B1JAcetone
ND 0.50 3/11/19 12:01 EEHg/L0.12 3/8/19SM21-22 6200B1Benzene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 12:01 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 12:01 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 12:01 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 12:01 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 12:01 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 12:01 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 12:01 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 12:01 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 12:01 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 12:01 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 12:01 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 12:01 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 12:01 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 12:01 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 12:01 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 12:01 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 12:01 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/11/19 12:01 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 12:01 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 12:01 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 12:01 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 12:01 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 12:01 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 12:01 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/11/19 12:01 EEHg/L0.18 3/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 12:01 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 12:01 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/11/19 12:01 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 12:01 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 12:01 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 8 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-01
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 3/6/2019 17:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 12:01 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 12:01 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 12:01 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/11/19 12:01 EEHg/L0.17 3/8/19SM21-22 6200B1Toluene
ND 5.0 3/11/19 12:01 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 12:01 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 12:01 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 12:01 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 12:01 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 12:01 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 12:01 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 12:01 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 3/11/19 12:01 EEHg/L0.26 3/8/19SM21-22 6200B1m+p Xylene
ND 0.50 3/11/19 12:01 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 102 3/11/19 12:0170-130
Toluene-d8 100 3/11/19 12:0170-130
4-Bromofluorobenzene 98.1 3/11/19 12:0170-130
Page 9 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/6/2019 12:45
[TOC_2]19C0264-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/11/19 17:26 EEHg/L9.7 3/8/19SM21-22 6200B1Acetone
ND 0.50 3/11/19 17:26 EEHg/L0.12 3/8/19SM21-22 6200B1Benzene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 17:26 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 17:26 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 17:26 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 17:26 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 17:26 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 17:26 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 17:26 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 17:26 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 17:26 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 17:26 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 17:26 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 17:26 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 17:26 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 17:26 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 17:26 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 17:26 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 17:26 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/11/19 17:26 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 17:26 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 17:26 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 17:26 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 17:26 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 17:26 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 17:26 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
0.43 0.50 3/11/19 17:26 EEHg/L0.18 3/8/19SM21-22 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 17:26 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 17:26 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
41 0.50 3/11/19 17:26 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 17:26 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 17:26 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 10 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/6/2019 12:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 17:26 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 17:26 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 17:26 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/11/19 17:26 EEHg/L0.17 3/8/19SM21-22 6200B1Toluene
ND 5.0 3/11/19 17:26 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 17:26 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 17:26 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 17:26 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 17:26 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 17:26 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 17:26 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 17:26 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 3/11/19 17:26 EEHg/L0.26 3/8/19SM21-22 6200B1m+p Xylene
ND 0.50 3/11/19 17:26 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 104 3/11/19 17:2670-130
Toluene-d8 99.0 3/11/19 17:2670-130
4-Bromofluorobenzene 96.6 3/11/19 17:2670-130
Page 11 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-03
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/6/2019 13:33
[TOC_2]19C0264-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/11/19 17:53 EEHg/L9.7 3/8/19SM21-22 6200B1Acetone
ND 0.50 3/11/19 17:53 EEHg/L0.12 3/8/19SM21-22 6200B1Benzene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 17:53 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 17:53 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 17:53 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 17:53 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 17:53 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 17:53 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 17:53 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 17:53 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 17:53 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 17:53 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 17:53 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 17:53 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 17:53 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 17:53 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 17:53 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 17:53 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 17:53 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/11/19 17:53 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 17:53 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 17:53 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 17:53 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 17:53 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 17:53 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 17:53 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
7.3 0.50 3/11/19 17:53 EEHg/L0.18 3/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 17:53 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 17:53 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
100 0.50 3/11/19 17:53 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 17:53 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 17:53 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 12 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-03
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/6/2019 13:33
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 17:53 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 17:53 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 17:53 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/11/19 17:53 EEHg/L0.17 3/8/19SM21-22 6200B1Toluene
ND 5.0 3/11/19 17:53 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 17:53 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 17:53 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 17:53 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 17:53 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 17:53 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 17:53 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 17:53 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 3/11/19 17:53 EEHg/L0.26 3/8/19SM21-22 6200B1m+p Xylene
ND 0.50 3/11/19 17:53 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 3/11/19 17:5370-130
Toluene-d8 100 3/11/19 17:5370-130
4-Bromofluorobenzene 95.0 3/11/19 17:5370-130
Page 13 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-04
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/6/2019 16:06
[TOC_2]19C0264-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
10000 25000 3/12/19 19:40 EEHg/L4800 3/12/19SM21-22 6200B500JAcetone
28000 250 3/12/19 19:40 EEHg/L60 3/12/19SM21-22 6200B500Benzene
ND 250 3/12/19 19:40 EEHg/L75 3/12/19SM21-22 6200B500Bromobenzene
ND 250 3/12/19 19:40 EEHg/L110 3/12/19SM21-22 6200B500Bromochloromethane
ND 250 3/12/19 19:40 EEHg/L150 3/12/19SM21-22 6200B500Bromodichloromethane
ND 1000 3/12/19 19:40 EEHg/L100 3/12/19SM21-22 6200B500Bromoform
ND 1000 3/12/19 19:40 EEHg/L470 3/12/19SM21-22 6200B500Bromomethane
2700 2500 3/12/19 19:40 EEHg/L1200 3/12/19SM21-22 6200B5002-Butanone (MEK)
ND 250 3/12/19 19:40 EEHg/L75 3/12/19SM21-22 6200B500n-Butylbenzene
ND 250 3/12/19 19:40 EEHg/L65 3/12/19SM21-22 6200B500sec-Butylbenzene
ND 250 3/12/19 19:40 EEHg/L60 3/12/19SM21-22 6200B500tert-Butylbenzene
ND 250 3/12/19 19:40 EEHg/L120 3/12/19SM21-22 6200B500Carbon Tetrachloride
ND 250 3/12/19 19:40 EEHg/L80 3/12/19SM21-22 6200B500Chlorobenzene
ND 25000 3/12/19 19:40 EEHg/L14000 3/12/19SM21-22 6200B500Ethanol
ND 250 3/12/19 19:40 EEHg/L52 3/12/19SM21-22 6200B500Chlorodibromomethane
ND 250 3/12/19 19:40 EEHg/L140 3/12/19SM21-22 6200B500Chloroethane
ND 250 3/12/19 19:40 EEHg/L110 3/12/19SM21-22 6200B500Chloroform
ND 300 3/12/19 19:40 EEHg/L280 3/12/19SM21-22 6200B500Chloromethane
ND 250 3/12/19 19:40 EEHg/L60 3/12/19SM21-22 6200B5002-Chlorotoluene
ND 250 3/12/19 19:40 EEHg/L70 3/12/19SM21-22 6200B5004-Chlorotoluene
ND 250 3/12/19 19:40 EEHg/L74 3/12/19SM21-22 6200B5001,2-Dibromoethane (EDB)
ND 250 3/12/19 19:40 EEHg/L85 3/12/19SM21-22 6200B5001,2-Dichlorobenzene
ND 250 3/12/19 19:40 EEHg/L85 3/12/19SM21-22 6200B5001,3-Dichlorobenzene
ND 250 3/12/19 19:40 EEHg/L75 3/12/19SM21-22 6200B5001,4-Dichlorobenzene
ND 250 3/12/19 19:40 EEHg/L140 3/12/19SM21-22 6200B500Dichlorodifluoromethane (Freon 12)
ND 250 3/12/19 19:40 EEHg/L79 3/12/19SM21-22 6200B5001,1-Dichloroethane
ND 250 3/12/19 19:40 EEHg/L97 3/12/19SM21-22 6200B5001,2-Dichloroethane
ND 250 3/12/19 19:40 EEHg/L100 3/12/19SM21-22 6200B5001,1-Dichloroethylene
ND 250 3/12/19 19:40 EEHg/L74 3/12/19SM21-22 6200B500cis-1,2-Dichloroethylene
ND 250 3/12/19 19:40 EEHg/L75 3/12/19SM21-22 6200B500trans-1,2-Dichloroethylene
ND 250 3/12/19 19:40 EEHg/L65 3/12/19SM21-22 6200B5001,2-Dichloropropane
ND 250 3/12/19 19:40 EEHg/L65 3/12/19SM21-22 6200B5001,3-Dichloropropane
ND 250 3/12/19 19:40 EEHg/L110 3/12/19SM21-22 6200B5002,2-Dichloropropane
ND 250 3/12/19 19:40 EEHg/L64 3/12/19SM21-22 6200B5001,1-Dichloropropene
ND 250 3/12/19 19:40 EEHg/L60 3/12/19SM21-22 6200B500cis-1,3-Dichloropropene
ND 250 3/12/19 19:40 EEHg/L56 3/12/19SM21-22 6200B500trans-1,3-Dichloropropene
290 250 3/12/19 19:40 EEHg/L90 3/12/19SM21-22 6200B500Diisopropyl Ether (DIPE)
3300 250 3/12/19 19:40 EEHg/L65 3/12/19SM21-22 6200B500Ethylbenzene
ND 2500 3/12/19 19:40 EEHg/L760 3/12/19SM21-22 6200B5002-Hexanone (MBK)
100 250 3/12/19 19:40 EEHg/L60 3/12/19SM21-22 6200B500JIsopropylbenzene (Cumene)
ND 250 3/12/19 19:40 EEHg/L75 3/12/19SM21-22 6200B500p-Isopropyltoluene (p-Cymene)
7200 250 3/12/19 19:40 EEHg/L45 3/12/19SM21-22 6200B500Methyl tert-Butyl Ether (MTBE)
ND 2500 3/12/19 19:40 EEHg/L1600 3/12/19SM21-22 6200B500Methylene Chloride
ND 2500 3/12/19 19:40 EEHg/L730 3/12/19SM21-22 6200B5004-Methyl-2-pentanone (MIBK)
Page 14 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-04
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/6/2019 16:06
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
1900 1000 3/12/19 19:40 EEHg/L60 3/12/19SM21-22 6200B500Naphthalene
290 250 3/12/19 19:40 EEHg/L65 3/12/19SM21-22 6200B500n-Propylbenzene
ND 250 3/12/19 19:40 EEHg/L75 3/12/19SM21-22 6200B500Styrene
ND 250 3/12/19 19:40 EEHg/L80 3/12/19SM21-22 6200B5001,1,2,2-Tetrachloroethane
ND 250 3/12/19 19:40 EEHg/L140 3/12/19SM21-22 6200B500Tetrachloroethylene
43000 250 3/12/19 19:40 EEHg/L85 3/12/19SM21-22 6200B500Toluene
ND 2500 3/12/19 19:40 EEHg/L70 3/12/19SM21-22 6200B5001,2,3-Trichlorobenzene
ND 1000 3/12/19 19:40 EEHg/L95 3/12/19SM21-22 6200B5001,2,4-Trichlorobenzene
ND 250 3/12/19 19:40 EEHg/L66 3/12/19SM21-22 6200B5001,1,1-Trichloroethane
ND 250 3/12/19 19:40 EEHg/L120 3/12/19SM21-22 6200B5001,1,2-Trichloroethane
ND 250 3/12/19 19:40 EEHg/L100 3/12/19SM21-22 6200B500Trichloroethylene
ND 250 3/12/19 19:40 EEHg/L74 3/12/19SM21-22 6200B500Trichlorofluoromethane (Freon 11)
ND 250 3/12/19 19:40 EEHg/L110 3/12/19SM21-22 6200B5001,2,3-Trichloropropane
2400 250 3/12/19 19:40 EEHg/L90 3/12/19SM21-22 6200B5001,2,4-Trimethylbenzene
560 250 3/12/19 19:40 EEHg/L65 3/12/19SM21-22 6200B5001,3,5-Trimethylbenzene
ND 2500 3/12/19 19:40 EEHg/L720 3/12/19SM21-22 6200B500L-04Vinyl Acetate
ND 250 3/12/19 19:40 EEHg/L66 3/12/19SM21-22 6200B500Vinyl Chloride
11000 500 3/12/19 19:40 EEHg/L130 3/12/19SM21-22 6200B500m+p Xylene
5600 250 3/12/19 19:40 EEHg/L66 3/12/19SM21-22 6200B500o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 3/12/19 19:4070-130
Toluene-d8 99.7 3/12/19 19:4070-130
4-Bromofluorobenzene 98.1 3/12/19 19:4070-130
Page 15 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-05
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/6/2019 15:18
[TOC_2]19C0264-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 3/12/19 19:13 EEHg/L97 3/12/19SM21-22 6200B10Acetone
420 5.0 3/12/19 19:13 EEHg/L1.2 3/12/19SM21-22 6200B10Benzene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10Bromobenzene
ND 5.0 3/12/19 19:13 EEHg/L2.2 3/12/19SM21-22 6200B10Bromochloromethane
ND 5.0 3/12/19 19:13 EEHg/L3.0 3/12/19SM21-22 6200B10Bromodichloromethane
ND 20 3/12/19 19:13 EEHg/L2.1 3/12/19SM21-22 6200B10Bromoform
ND 20 3/12/19 19:13 EEHg/L9.4 3/12/19SM21-22 6200B10Bromomethane
ND 50 3/12/19 19:13 EEHg/L24 3/12/19SM21-22 6200B102-Butanone (MEK)
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10n-Butylbenzene
ND 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B10sec-Butylbenzene
ND 5.0 3/12/19 19:13 EEHg/L1.2 3/12/19SM21-22 6200B10tert-Butylbenzene
ND 5.0 3/12/19 19:13 EEHg/L2.5 3/12/19SM21-22 6200B10Carbon Tetrachloride
ND 5.0 3/12/19 19:13 EEHg/L1.6 3/12/19SM21-22 6200B10Chlorobenzene
ND 500 3/12/19 19:13 EEHg/L280 3/12/19SM21-22 6200B10Ethanol
ND 5.0 3/12/19 19:13 EEHg/L1.0 3/12/19SM21-22 6200B10Chlorodibromomethane
ND 5.0 3/12/19 19:13 EEHg/L2.8 3/12/19SM21-22 6200B10Chloroethane
ND 5.0 3/12/19 19:13 EEHg/L2.2 3/12/19SM21-22 6200B10Chloroform
ND 6.0 3/12/19 19:13 EEHg/L5.5 3/12/19SM21-22 6200B10Chloromethane
ND 5.0 3/12/19 19:13 EEHg/L1.2 3/12/19SM21-22 6200B102-Chlorotoluene
ND 5.0 3/12/19 19:13 EEHg/L1.4 3/12/19SM21-22 6200B104-Chlorotoluene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 3/12/19 19:13 EEHg/L1.7 3/12/19SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 3/12/19 19:13 EEHg/L1.7 3/12/19SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 3/12/19 19:13 EEHg/L2.8 3/12/19SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 3/12/19 19:13 EEHg/L1.6 3/12/19SM21-22 6200B101,1-Dichloroethane
ND 5.0 3/12/19 19:13 EEHg/L1.9 3/12/19SM21-22 6200B101,2-Dichloroethane
ND 5.0 3/12/19 19:13 EEHg/L2.1 3/12/19SM21-22 6200B101,1-Dichloroethylene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B101,2-Dichloropropane
ND 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B101,3-Dichloropropane
ND 5.0 3/12/19 19:13 EEHg/L2.1 3/12/19SM21-22 6200B102,2-Dichloropropane
ND 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B101,1-Dichloropropene
ND 5.0 3/12/19 19:13 EEHg/L1.2 3/12/19SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 3/12/19 19:13 EEHg/L1.1 3/12/19SM21-22 6200B10trans-1,3-Dichloropropene
77 5.0 3/12/19 19:13 EEHg/L1.8 3/12/19SM21-22 6200B10Diisopropyl Ether (DIPE)
28 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B10Ethylbenzene
ND 50 3/12/19 19:13 EEHg/L15 3/12/19SM21-22 6200B102-Hexanone (MBK)
1.3 5.0 3/12/19 19:13 EEHg/L1.2 3/12/19SM21-22 6200B10JIsopropylbenzene (Cumene)
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10p-Isopropyltoluene (p-Cymene)
830 5.0 3/12/19 19:13 EEHg/L0.90 3/12/19SM21-22 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 3/12/19 19:13 EEHg/L32 3/12/19SM21-22 6200B10Methylene Chloride
ND 50 3/12/19 19:13 EEHg/L15 3/12/19SM21-22 6200B104-Methyl-2-pentanone (MIBK)
Page 16 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-05
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/6/2019 15:18
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
36 20 3/12/19 19:13 EEHg/L1.2 3/12/19SM21-22 6200B10Naphthalene
2.0 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B10Jn-Propylbenzene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10Styrene
ND 5.0 3/12/19 19:13 EEHg/L1.6 3/12/19SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 3/12/19 19:13 EEHg/L2.7 3/12/19SM21-22 6200B10Tetrachloroethylene
4.5 5.0 3/12/19 19:13 EEHg/L1.7 3/12/19SM21-22 6200B10JToluene
ND 50 3/12/19 19:13 EEHg/L1.4 3/12/19SM21-22 6200B101,2,3-Trichlorobenzene
ND 20 3/12/19 19:13 EEHg/L1.9 3/12/19SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 3/12/19 19:13 EEHg/L2.4 3/12/19SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 3/12/19 19:13 EEHg/L2.0 3/12/19SM21-22 6200B10Trichloroethylene
ND 5.0 3/12/19 19:13 EEHg/L1.5 3/12/19SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 3/12/19 19:13 EEHg/L2.2 3/12/19SM21-22 6200B101,2,3-Trichloropropane
48 5.0 3/12/19 19:13 EEHg/L1.8 3/12/19SM21-22 6200B101,2,4-Trimethylbenzene
20 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B101,3,5-Trimethylbenzene
ND 50 3/12/19 19:13 EEHg/L14 3/12/19SM21-22 6200B10L-04Vinyl Acetate
ND 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B10Vinyl Chloride
210 10 3/12/19 19:13 EEHg/L2.6 3/12/19SM21-22 6200B10m+p Xylene
61 5.0 3/12/19 19:13 EEHg/L1.3 3/12/19SM21-22 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 3/12/19 19:1370-130
Toluene-d8 99.3 3/12/19 19:1370-130
4-Bromofluorobenzene 98.6 3/12/19 19:1370-130
Page 17 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-06
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/6/2019 11:50
[TOC_2]19C0264-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/11/19 18:20 EEHg/L9.7 3/8/19SM21-22 6200B1Acetone
ND 0.50 3/11/19 18:20 EEHg/L0.12 3/8/19SM21-22 6200B1Benzene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 18:20 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 18:20 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 18:20 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 18:20 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 18:20 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 18:20 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 18:20 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 18:20 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 18:20 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 18:20 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 18:20 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 18:20 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 18:20 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 18:20 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 18:20 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 18:20 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 18:20 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/11/19 18:20 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 18:20 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 18:20 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 18:20 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 18:20 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 18:20 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 18:20 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/11/19 18:20 EEHg/L0.18 3/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 18:20 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 18:20 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/11/19 18:20 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 18:20 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 18:20 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 18 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-06
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/6/2019 11:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 18:20 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 18:20 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 18:20 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/11/19 18:20 EEHg/L0.17 3/8/19SM21-22 6200B1Toluene
ND 5.0 3/11/19 18:20 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 18:20 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 18:20 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 18:20 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 18:20 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 18:20 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 18:20 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 18:20 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 3/11/19 18:20 EEHg/L0.26 3/8/19SM21-22 6200B1m+p Xylene
ND 0.50 3/11/19 18:20 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 3/11/19 18:2070-130
Toluene-d8 100 3/11/19 18:2070-130
4-Bromofluorobenzene 97.7 3/11/19 18:2070-130
Page 19 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-07
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 3/6/2019 11:03
[TOC_2]19C0264-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/11/19 18:47 EEHg/L9.7 3/8/19SM21-22 6200B1Acetone
ND 0.50 3/11/19 18:47 EEHg/L0.12 3/8/19SM21-22 6200B1Benzene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 18:47 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 18:47 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 18:47 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 18:47 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 18:47 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 18:47 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 18:47 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 18:47 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 18:47 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 18:47 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 18:47 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 18:47 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 18:47 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 18:47 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 18:47 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 18:47 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 18:47 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/11/19 18:47 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 18:47 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 18:47 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 18:47 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 18:47 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 18:47 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 18:47 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/11/19 18:47 EEHg/L0.18 3/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 18:47 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 18:47 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/11/19 18:47 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 18:47 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 18:47 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 20 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-07
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 3/6/2019 11:03
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 18:47 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 18:47 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 18:47 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/11/19 18:47 EEHg/L0.17 3/8/19SM21-22 6200B1Toluene
ND 5.0 3/11/19 18:47 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 18:47 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 18:47 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 18:47 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 18:47 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 18:47 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 18:47 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 18:47 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 3/11/19 18:47 EEHg/L0.26 3/8/19SM21-22 6200B1m+p Xylene
ND 0.50 3/11/19 18:47 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 102 3/11/19 18:4770-130
Toluene-d8 100 3/11/19 18:4770-130
4-Bromofluorobenzene 97.1 3/11/19 18:4770-130
Page 21 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-08
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 3/6/2019 16:42
[TOC_2]19C0264-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: PR-08, Z-01 Volatile Organic Compounds by GC/MS
ND 50 3/11/19 19:14 EEHg/L9.7 3/8/19SM21-22 6200B1Acetone
0.17 0.50 3/11/19 19:14 EEHg/L0.12 3/8/19SM21-22 6200B1JBenzene
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 19:14 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 19:14 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 19:14 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 19:14 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 19:14 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 19:14 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 19:14 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 19:14 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 19:14 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 19:14 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 19:14 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 19:14 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 19:14 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 19:14 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 19:14 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 19:14 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 19:14 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
0.50 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/11/19 19:14 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 19:14 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 19:14 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 19:14 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 19:14 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 19:14 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 19:14 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/11/19 19:14 EEHg/L0.18 3/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 19:14 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 19:14 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
3.9 0.50 3/11/19 19:14 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 19:14 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 19:14 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 22 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-08
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 3/6/2019 16:42
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: PR-08, Z-01 Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 19:14 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 19:14 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 19:14 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
0.65 0.50 3/11/19 19:14 EEHg/L0.17 3/8/19SM21-22 6200B1Toluene
ND 5.0 3/11/19 19:14 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 19:14 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 19:14 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 19:14 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 19:14 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 19:14 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 19:14 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 19:14 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
0.31 1.0 3/11/19 19:14 EEHg/L0.26 3/8/19SM21-22 6200B1Jm+p Xylene
ND 0.50 3/11/19 19:14 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 3/11/19 19:1470-130
Toluene-d8 100 3/11/19 19:1470-130
4-Bromofluorobenzene 96.0 3/11/19 19:1470-130
Page 23 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-09
Field Sample #: MW-8
Sample Matrix: Ground Water
Sampled: 3/6/2019 17:17
[TOC_2]19C0264-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/11/19 19:41 EEHg/L9.7 3/8/19SM21-22 6200B1Acetone
ND 0.50 3/11/19 19:41 EEHg/L0.12 3/8/19SM21-22 6200B1Benzene
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1Bromobenzene
ND 0.50 3/11/19 19:41 EEHg/L0.22 3/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 3/11/19 19:41 EEHg/L0.30 3/8/19SM21-22 6200B1Bromodichloromethane
ND 2.0 3/11/19 19:41 EEHg/L0.21 3/8/19SM21-22 6200B1Bromoform
ND 2.0 3/11/19 19:41 EEHg/L0.94 3/8/19SM21-22 6200B1Bromomethane
ND 5.0 3/11/19 19:41 EEHg/L2.4 3/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/11/19 19:41 EEHg/L0.12 3/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/11/19 19:41 EEHg/L0.25 3/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/11/19 19:41 EEHg/L0.16 3/8/19SM21-22 6200B1Chlorobenzene
ND 50 3/11/19 19:41 EEHg/L28 3/8/19SM21-22 6200B1Ethanol
ND 0.50 3/11/19 19:41 EEHg/L0.10 3/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/11/19 19:41 EEHg/L0.28 3/8/19SM21-22 6200B1Chloroethane
ND 0.50 3/11/19 19:41 EEHg/L0.22 3/8/19SM21-22 6200B1Chloroform
ND 0.60 3/11/19 19:41 EEHg/L0.55 3/8/19SM21-22 6200B1Chloromethane
ND 0.50 3/11/19 19:41 EEHg/L0.12 3/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 3/11/19 19:41 EEHg/L0.14 3/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/11/19 19:41 EEHg/L0.17 3/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/11/19 19:41 EEHg/L0.17 3/8/19SM21-22 6200B11,3-Dichlorobenzene
0.23 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1J1,4-Dichlorobenzene
ND 0.50 3/11/19 19:41 EEHg/L0.28 3/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/11/19 19:41 EEHg/L0.16 3/8/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/11/19 19:41 EEHg/L0.19 3/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/11/19 19:41 EEHg/L0.21 3/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/11/19 19:41 EEHg/L0.21 3/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/11/19 19:41 EEHg/L0.12 3/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/11/19 19:41 EEHg/L0.11 3/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/11/19 19:41 EEHg/L0.18 3/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 3/11/19 19:41 EEHg/L1.5 3/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/11/19 19:41 EEHg/L0.12 3/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
3.6 0.50 3/11/19 19:41 EEHg/L0.090 3/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/11/19 19:41 EEHg/L3.2 3/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 3/11/19 19:41 EEHg/L1.5 3/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/7/2019
Work Order: 19C0264Sample Description:Project Location: Chatham County
Sample ID: 19C0264-09
Field Sample #: MW-8
Sample Matrix: Ground Water
Sampled: 3/6/2019 17:17
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/11/19 19:41 EEHg/L0.12 3/8/19SM21-22 6200B1Naphthalene
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1Styrene
ND 0.50 3/11/19 19:41 EEHg/L0.16 3/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/11/19 19:41 EEHg/L0.27 3/8/19SM21-22 6200B1Tetrachloroethylene
0.43 0.50 3/11/19 19:41 EEHg/L0.17 3/8/19SM21-22 6200B1JToluene
ND 5.0 3/11/19 19:41 EEHg/L0.14 3/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 2.0 3/11/19 19:41 EEHg/L0.19 3/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/11/19 19:41 EEHg/L0.24 3/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/11/19 19:41 EEHg/L0.20 3/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 3/11/19 19:41 EEHg/L0.15 3/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/11/19 19:41 EEHg/L0.22 3/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/11/19 19:41 EEHg/L0.18 3/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/11/19 19:41 EEHg/L1.4 3/8/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 3/11/19 19:41 EEHg/L0.26 3/8/19SM21-22 6200B1m+p Xylene
ND 0.50 3/11/19 19:41 EEHg/L0.13 3/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 3/11/19 19:4170-130
Toluene-d8 102 3/11/19 19:4170-130
4-Bromofluorobenzene 99.0 3/11/19 19:4170-130
Page 25 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B225391 03/08/1955.0019C0264-01 [Field Blank]
B225391 03/08/1955.0019C0264-02 [MW-1]
B225391 03/08/1955.0019C0264-03 [MW-2]
B225391 03/08/1955.0019C0264-06 [MW-5]
B225391 03/08/1955.0019C0264-07 [MW-6]
B225391 03/08/1955.0019C0264-08 [MW-7]
B225391 03/08/1955.0019C0264-09 [MW-8]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B225511 03/12/190.01 5.0019C0264-04 [MW-3]
B225511 03/12/190.5 5.0019C0264-05 [MW-4]
[TOC_1]Sample Preparation Information[TOC]
Page 26 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B225391 - SW-846 5030B
[TOC_3]B225391[TOC]
Blank (B225391-BLK1) Prepared & Analyzed: 03/11/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 27 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225391 - SW-846 5030B
Blank (B225391-BLK1) Prepared & Analyzed: 03/11/19
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0 L-04ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10125.2
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.423.6
LCS (B225391-BS1) Prepared & Analyzed: 03/11/19
Acetone g/L50 100 70-13098.298.2
Benzene g/L0.50 10.0 70-13096.39.63
Bromobenzene g/L0.50 10.0 70-13010510.5
Bromochloromethane g/L0.50 10.0 70-13097.59.75
Bromodichloromethane g/L0.50 10.0 70-13096.59.65
Bromoform g/L0.50 10.0 70-13097.69.76
Bromomethane g/L1.0 10.0 60-14062.76.27
2-Butanone (MEK)g/L5.0 100 70-13071.671.6
n-Butylbenzene g/L0.50 10.0 70-13011211.2
sec-Butylbenzene g/L0.50 10.0 70-13011411.4
tert-Butylbenzene g/L0.50 10.0 70-13011111.1
Carbon Tetrachloride g/L0.50 10.0 70-13096.19.61
Chlorobenzene g/L0.50 10.0 70-13010410.4
Ethanol g/L50 100 70-130121121
Chlorodibromomethane g/L0.50 10.0 70-13099.89.98
Chloroethane g/L0.50 10.0 60-14010710.7
Chloroform g/L0.50 10.0 70-13095.29.52
Chloromethane g/L0.60 10.0 60-14076.07.60
2-Chlorotoluene g/L0.50 10.0 70-13010110.1
4-Chlorotoluene g/L0.50 10.0 70-13010910.9
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13093.09.30
1,2-Dichlorobenzene g/L0.50 10.0 70-13011111.1
1,3-Dichlorobenzene g/L0.50 10.0 70-13011111.1
1,4-Dichlorobenzene g/L0.50 10.0 70-13010910.9
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14078.87.88
1,1-Dichloroethane g/L0.50 10.0 70-13010010.0
1,2-Dichloroethane g/L0.50 10.0 70-13084.68.46
1,1-Dichloroethylene g/L0.50 10.0 70-13011211.2
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13098.39.83
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010410.4
1,2-Dichloropropane g/L0.50 10.0 70-13093.19.31
1,3-Dichloropropane g/L0.50 10.0 70-13095.19.51
2,2-Dichloropropane g/L0.50 10.0 70-13099.89.98
1,1-Dichloropropene g/L0.50 10.0 70-13094.19.41
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010410.4
trans-1,3-Dichloropropene g/L0.50 10.0 70-13011111.1
Page 28 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225391 - SW-846 5030B
LCS (B225391-BS1) Prepared & Analyzed: 03/11/19
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010310.3
Ethylbenzene g/L0.50 10.0 70-13010310.3
2-Hexanone (MBK)g/L5.0 100 70-13080.180.1
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010410.4
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011311.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13010210.2
Methylene Chloride g/L5.0 10.0 70-13011711.7
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13082.882.8
Naphthalene g/L0.50 10.0 70-13092.19.21
n-Propylbenzene g/L0.50 10.0 70-13010510.5
Styrene g/L0.50 10.0 70-13011111.1
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010510.5
Tetrachloroethylene g/L0.50 10.0 70-13094.39.43
Toluene g/L0.50 10.0 70-13096.69.66
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13010910.9
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13094.79.47
1,1,1-Trichloroethane g/L0.50 10.0 70-13095.39.53
1,1,2-Trichloroethane g/L0.50 10.0 70-13010210.2
Trichloroethylene g/L0.50 10.0 70-13095.29.52
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13094.29.42
1,2,3-Trichloropropane g/L0.50 10.0 70-13095.69.56
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011211.2
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010410.4
Vinyl Acetate g/L5.0 100 L-0470-13063.3 *63.3
Vinyl Chloride g/L0.50 10.0 60-14010410.4
m+p Xylene g/L1.0 20.0 70-13010621.1
o-Xylene g/L0.50 10.0 70-13011011.0
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.6
g/L 25.0 70-130Surrogate: Toluene-d8 99.424.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.2
LCS Dup (B225391-BSD1) Prepared & Analyzed: 03/11/19
Acetone g/L50 100 2570-13097.6 0.60297.6
Benzene g/L0.50 10.0 2570-13095.3 1.049.53
Bromobenzene g/L0.50 10.0 2570-130103 1.4410.3
Bromochloromethane g/L0.50 10.0 2570-130101 3.4310.1
Bromodichloromethane g/L0.50 10.0 2570-13095.2 1.369.52
Bromoform g/L0.50 10.0 2570-13099.2 1.639.92
Bromomethane g/L1.0 10.0 2560-14074.7 17.57.47
2-Butanone (MEK)g/L5.0 100 2570-13072.1 0.68272.1
n-Butylbenzene g/L0.50 10.0 2570-130112 0.089411.2
sec-Butylbenzene g/L0.50 10.0 2570-130115 0.26211.5
tert-Butylbenzene g/L0.50 10.0 2570-130111 0.36011.1
Carbon Tetrachloride g/L0.50 10.0 2570-13094.5 1.689.45
Chlorobenzene g/L0.50 10.0 2570-130104 0.19210.4
Ethanol g/L50 100 2570-130121 0.355121
Chlorodibromomethane g/L0.50 10.0 2570-130100 0.20010.0
Chloroethane g/L0.50 10.0 2560-140111 3.7711.1
Chloroform g/L0.50 10.0 2570-13095.6 0.4199.56
Chloromethane g/L0.60 10.0 2560-14079.2 4.127.92
2-Chlorotoluene g/L0.50 10.0 2570-13099.0 2.209.90
4-Chlorotoluene g/L0.50 10.0 2570-130108 0.73710.8
Page 29 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225391 - SW-846 5030B
LCS Dup (B225391-BSD1) Prepared & Analyzed: 03/11/19
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13095.2 2.349.52
1,2-Dichlorobenzene g/L0.50 10.0 2570-130109 1.5410.9
1,3-Dichlorobenzene g/L0.50 10.0 2570-130111 0.0011.1
1,4-Dichlorobenzene g/L0.50 10.0 2570-130107 1.7610.7
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14078.9 0.1277.89
1,1-Dichloroethane g/L0.50 10.0 2570-13098.1 2.229.81
1,2-Dichloroethane g/L0.50 10.0 2570-13083.3 1.558.33
1,1-Dichloroethylene g/L0.50 10.0 2570-130113 0.26711.3
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.9 1.439.69
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130104 0.0010.4
1,2-Dichloropropane g/L0.50 10.0 2570-13091.6 1.629.16
1,3-Dichloropropane g/L0.50 10.0 2570-13095.6 0.5249.56
2,2-Dichloropropane g/L0.50 10.0 2570-13096.8 3.059.68
1,1-Dichloropropene g/L0.50 10.0 2570-13094.4 0.3189.44
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130107 2.7610.7
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130111 0.36011.1
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13097.7 5.679.77
Ethylbenzene g/L0.50 10.0 2570-130104 0.96610.4
2-Hexanone (MBK)g/L5.0 100 2570-13079.7 0.51379.7
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130103 0.67610.3
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130112 1.3411.2
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130103 0.87810.3
Methylene Chloride g/L5.0 10.0 2570-130116 0.51411.6
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13080.8 2.4380.8
Naphthalene g/L0.50 10.0 2570-13092.6 0.5419.26
n-Propylbenzene g/L0.50 10.0 2570-130105 0.19010.5
Styrene g/L0.50 10.0 2570-130109 2.1810.9
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130104 0.76310.4
Tetrachloroethylene g/L0.50 10.0 2570-13092.9 1.509.29
Toluene g/L0.50 10.0 2570-13096.5 0.1049.65
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-130107 1.5710.7
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13095.4 0.7369.54
1,1,1-Trichloroethane g/L0.50 10.0 2570-13096.0 0.7329.60
1,1,2-Trichloroethane g/L0.50 10.0 2570-130102 0.29510.2
Trichloroethylene g/L0.50 10.0 2570-13090.1 5.509.01
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13094.3 0.1069.43
1,2,3-Trichloropropane g/L0.50 10.0 2570-13093.6 2.119.36
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130112 0.62511.2
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130102 1.7510.2
Vinyl Acetate g/L5.0 100 25 L-0470-13064.2 1.51*64.2
Vinyl Chloride g/L0.50 10.0 2560-140101 3.2110.1
m+p Xylene g/L1.0 20.0 2570-130105 0.95120.9
o-Xylene g/L0.50 10.0 2570-130108 1.5610.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10325.9
g/L 25.0 70-130Surrogate: Toluene-d8 98.824.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10025.0
Page 30 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225511 - SW-846 5030B
[TOC_3]B225511[TOC]
Blank (B225511-BLK1) Prepared & Analyzed: 03/12/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 31 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225511 - SW-846 5030B
Blank (B225511-BLK1) Prepared & Analyzed: 03/12/19
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0 L-04ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 99.925.0
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.124.3
LCS (B225511-BS1) Prepared & Analyzed: 03/12/19
Acetone g/L50 100 70-13099.699.6
Benzene g/L0.50 10.0 70-13096.39.63
Bromobenzene g/L0.50 10.0 70-13011011.0
Bromochloromethane g/L0.50 10.0 70-13010610.6
Bromodichloromethane g/L0.50 10.0 70-13010210.2
Bromoform g/L0.50 10.0 70-13010410.4
Bromomethane g/L1.0 10.0 60-14070.47.04
2-Butanone (MEK)g/L5.0 100 70-13070.470.4
n-Butylbenzene g/L0.50 10.0 70-13011411.4
sec-Butylbenzene g/L0.50 10.0 70-13011411.4
tert-Butylbenzene g/L0.50 10.0 70-13011211.2
Carbon Tetrachloride g/L0.50 10.0 70-13094.69.46
Chlorobenzene g/L0.50 10.0 70-13011111.1
Ethanol g/L50 100 70-130108108
Chlorodibromomethane g/L0.50 10.0 70-13010810.8
Chloroethane g/L0.50 10.0 60-14010510.5
Chloroform g/L0.50 10.0 70-13099.69.96
Chloromethane g/L0.60 10.0 60-14076.47.64
2-Chlorotoluene g/L0.50 10.0 70-13010710.7
4-Chlorotoluene g/L0.50 10.0 70-13011311.3
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010210.2
1,2-Dichlorobenzene g/L0.50 10.0 70-13011511.5
1,3-Dichlorobenzene g/L0.50 10.0 70-13011611.6
1,4-Dichlorobenzene g/L0.50 10.0 70-13011311.3
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14072.97.29
1,1-Dichloroethane g/L0.50 10.0 70-13010110.1
1,2-Dichloroethane g/L0.50 10.0 70-13089.88.98
1,1-Dichloroethylene g/L0.50 10.0 70-13011211.2
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010310.3
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010510.5
1,2-Dichloropropane g/L0.50 10.0 70-13096.79.67
1,3-Dichloropropane g/L0.50 10.0 70-13010410.4
2,2-Dichloropropane g/L0.50 10.0 70-13094.89.48
1,1-Dichloropropene g/L0.50 10.0 70-13093.49.34
cis-1,3-Dichloropropene g/L0.50 10.0 70-13011111.1
trans-1,3-Dichloropropene g/L0.50 10.0 70-13011711.7
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225511 - SW-846 5030B
LCS (B225511-BS1) Prepared & Analyzed: 03/12/19
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13098.79.87
Ethylbenzene g/L0.50 10.0 70-13010610.6
2-Hexanone (MBK)g/L5.0 100 70-13083.583.5
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010710.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011411.4
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13010510.5
Methylene Chloride g/L5.0 10.0 70-13012112.1
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13087.787.7
Naphthalene g/L0.50 10.0 70-13091.49.14
n-Propylbenzene g/L0.50 10.0 70-13010710.7
Styrene g/L0.50 10.0 70-13011611.6
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13011011.0
Tetrachloroethylene g/L0.50 10.0 70-13097.09.70
Toluene g/L0.50 10.0 70-13010210.2
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13011011.0
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13099.59.95
1,1,1-Trichloroethane g/L0.50 10.0 70-13095.29.52
1,1,2-Trichloroethane g/L0.50 10.0 70-13010810.8
Trichloroethylene g/L0.50 10.0 70-13010010.0
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13093.69.36
1,2,3-Trichloropropane g/L0.50 10.0 70-13010210.2
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011311.3
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010710.7
Vinyl Acetate g/L5.0 100 L-0470-13065.5 *65.5
Vinyl Chloride g/L0.50 10.0 60-14097.39.73
m+p Xylene g/L1.0 20.0 70-13010721.4
o-Xylene g/L0.50 10.0 70-13011311.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10025.0
g/L 25.0 70-130Surrogate: Toluene-d8 99.224.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.2
LCS Dup (B225511-BSD1) Prepared & Analyzed: 03/12/19
Acetone g/L50 100 2570-130125 22.9125
Benzene g/L0.50 10.0 2570-13095.0 1.369.50
Bromobenzene g/L0.50 10.0 2570-130110 0.091011.0
Bromochloromethane g/L0.50 10.0 2570-130103 2.7710.3
Bromodichloromethane g/L0.50 10.0 2570-13099.7 2.779.97
Bromoform g/L0.50 10.0 2570-13099.3 5.109.93
Bromomethane g/L1.0 10.0 2560-14080.4 13.38.04
2-Butanone (MEK)g/L5.0 100 2570-13078.4 10.878.4
n-Butylbenzene g/L0.50 10.0 2570-130111 2.4011.1
sec-Butylbenzene g/L0.50 10.0 2570-130112 1.2411.2
tert-Butylbenzene g/L0.50 10.0 2570-130111 0.54011.1
Carbon Tetrachloride g/L0.50 10.0 2570-13092.9 1.819.29
Chlorobenzene g/L0.50 10.0 2570-130111 0.45011.1
Ethanol g/L50 100 2570-130105 3.46105
Chlorodibromomethane g/L0.50 10.0 2570-130102 5.1310.2
Chloroethane g/L0.50 10.0 2560-140108 3.0910.8
Chloroform g/L0.50 10.0 2570-13097.8 1.829.78
Chloromethane g/L0.60 10.0 2560-14077.6 1.567.76
2-Chlorotoluene g/L0.50 10.0 2570-130103 3.2410.3
4-Chlorotoluene g/L0.50 10.0 2570-130112 0.79911.2
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B225511 - SW-846 5030B
LCS Dup (B225511-BSD1) Prepared & Analyzed: 03/12/19
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13098.7 3.489.87
1,2-Dichlorobenzene g/L0.50 10.0 2570-130116 1.0411.6
1,3-Dichlorobenzene g/L0.50 10.0 2570-130116 0.51711.6
1,4-Dichlorobenzene g/L0.50 10.0 2570-130113 0.17711.3
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14070.9 2.787.09
1,1-Dichloroethane g/L0.50 10.0 2570-13099.8 1.599.98
1,2-Dichloroethane g/L0.50 10.0 2570-13087.3 2.828.73
1,1-Dichloroethylene g/L0.50 10.0 2570-130112 0.089111.2
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13099.5 3.659.95
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130102 2.6110.2
1,2-Dichloropropane g/L0.50 10.0 2570-13094.6 2.209.46
1,3-Dichloropropane g/L0.50 10.0 2570-130100 3.4310.0
2,2-Dichloropropane g/L0.50 10.0 2570-13091.9 3.119.19
1,1-Dichloropropene g/L0.50 10.0 2570-13091.3 2.279.13
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130108 3.0210.8
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130110 5.5511.0
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13098.5 0.2039.85
Ethylbenzene g/L0.50 10.0 2570-130106 0.28410.6
2-Hexanone (MBK)g/L5.0 100 2570-13081.7 2.1981.7
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130107 0.46810.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130112 1.5011.2
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130105 0.57110.5
Methylene Chloride g/L5.0 10.0 2570-130120 1.0812.0
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13082.8 5.7482.8
Naphthalene g/L0.50 10.0 2570-13096.9 5.849.69
n-Propylbenzene g/L0.50 10.0 2570-130107 0.0010.7
Styrene g/L0.50 10.0 2570-130115 0.34611.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130108 1.5510.8
Tetrachloroethylene g/L0.50 10.0 2570-13096.1 0.9329.61
Toluene g/L0.50 10.0 2570-13098.4 3.989.84
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-130117 6.3511.7
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130103 3.8410.3
1,1,1-Trichloroethane g/L0.50 10.0 2570-13092.1 3.319.21
1,1,2-Trichloroethane g/L0.50 10.0 2570-130105 2.5410.5
Trichloroethylene g/L0.50 10.0 2570-13092.0 8.839.20
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13091.9 1.839.19
1,2,3-Trichloropropane g/L0.50 10.0 2570-13097.6 4.029.76
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130112 1.4211.2
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130106 0.84510.6
Vinyl Acetate g/L5.0 100 25 L-0470-13062.4 4.92*62.4
Vinyl Chloride g/L0.50 10.0 2560-140104 6.1810.4
m+p Xylene g/L1.0 20.0 2570-130107 0.093621.4
o-Xylene g/L0.50 10.0 2570-130111 1.8711.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 96.124.0
g/L 25.0 70-130Surrogate: Toluene-d8 99.624.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
pH of sample (pH 5) is outside of method specified preservation criteria.PR-08
Elevated reporting limit due to high concentration of target compounds.RL-11
Sample poured off into another vial with headspace due to high level of sediment in sample.Z-01
[TOC_1]Flag/Qualifier Summary[TOC]
Page 35 of 40
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 36 of 40
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
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APPENDIX D