RA-493_1943_CA_MRP_20160302_SME FINAL GWM Report

GROUNDWATER MONITORING REPORT
WISE CONVENIENT MART, INCIDENT #1943
2027 US HIGHWAY 1 NORTH
WISE, WARREN COUNTY, NORTH CAROLINA
S&ME PROJECT # 4305-15-094
MARCH 2, 2016

Prepared For:

North Carolina Department of Environmental Quality
Division of Waste Management
Underground Storage Tank Section
1637 Mail Service Center
Raleigh, North Carolina 27699

Prepared by:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, North Carolina 27616

___________________________ _______________________________
Alexander R. Culpepper, P.G. Thomas P. Raymond, P.E., P.M.P.
Project Geologist Senior Consultant

S&ME is licensed to practice geology/engineering in North Carolina. Geology License Certification #C-145 and
Engineering License Certification #F-0176.

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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TABLE OF CONTENTS
1. FEDERAL/STATE-LEAD MONITORING REPORT ......................................... 3
2. EXECUTIVE SUMMARY ....................................................................................... 4
3. SCOPE OF SERVICES ............................................................................................ 6
3.1 Contract Information ........................................................................................... 6
3.2 Approved Scope of Services ............................................................................... 6
4. SITE HISTORY AND CHARACTERIZATION ................................................... 7
4.1 UST Owner and Operator Information. .............................................................. 8
4.2 UST Information ................................................................................................. 8
4.3 Description of the UST Release .......................................................................... 8
5. CURRENT SITE ASSESSMENT INFORMATION ............................................. 9
5.1 Current Liquid Levels ......................................................................................... 9
5.2 Groundwater Monitoring Events ........................................................................ 9
5.3 Water Supply Wells ............................................................................................ 9
5.4 Water Supply Well Monitoring Event ................................................................ 9
5.5 Summary of Groundwater and Free Product Assessment Information .............. 9
5.6 Summary of Water Supply Well Assessment Information ............................... 10
5.7 Regional and Site Geology and Hydrogeology ................................................ 10
5.7.1 Soil and Bedrock ................................................................................. 10
5.7.2 Hydrogeology ...................................................................................... 10
5.8 Evaluation of Groundwater Assessment Information ....................................... 10
5.8.1 Current Extent and Severity of Contamination ................................... 10
5.8.2 Cleanup Levels Achieved .................................................................... 11
6. CONCLUSIONS AND RECOMMENDATIONS ................................................ 12

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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TABLE OF CONTENTS (continued)

FIGURES

1 Vicinity Map
2 Site Map
3 Groundwater Elevation Map
4 Water Supply Well Map
5 Groundwater Elevation Map
6 Groundwater Constituent Map

TABLES

1 UST Owner/Operator Information
2 UST Information
3 Water Supply Well Information
4 Monitor Well Construction and Liquid Level Data
5 Summary of Groundwater Sampling Results
6 Summary of Water Supply Well Sampling Results

APPENDICES

I Photographic Log
III Field Sampling Forms
IV Laboratory Analytical Report and Chain-of-Custody Record

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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2. EXECUTIVE SUMMARY
On October 26, 2015, S&ME collected groundwater samples from eight monitor wells (MW-1
through MW-7, and DW-1) located at the former Wise Convenient Mart site, located at 2027 US
Highway 1 North in Wise, Warren County, North Carolina. S&ME also collected samples from
two water supply wells WSW-1 and WSW-11. The following summarizes the results of the
sampling event:

 Free product has historically been reported in monitor well MW-1. During the October
26, 2015 sampling event no free product was measured in MW-1.

 The following constituents were the highest reported at concentrations above the 15A
NCAC 2L.0202 Groundwater Standards (2L Standards) in groundwater samples collected
from monitor wells (MW-1 through MW-7, and DW-1) on October 26, 2015:

Contaminant
2L
Standard
(µg/L)
Concentration
(µg/L) Well ID Date
Benzene 1 650 MW-5 10/26/2015
1,2-dibromoethane 0.02 5.9 MW-1 10/26/2015
Ethylbenzene 600 1,200 MW-1 10/26/2015
p-Isopropyltoluene 25 36 MW-1 10/26/2015
n-Propylbenzene 70 180 MW-1 10/26/2015
Naphthalene 6 340 MW-1 10/26/2015
Toluene 600 7,600 MW-1 10/26/2015
1,2,4-Trimethylbenzene 400 1,500 MW-1 10/26/2015
1,3,5-Trimethylbenzene 400 510 MW-1 10/26/2015
Total Xylenes 500 7,700 MW-1 10/26/2015

 According to an S&ME Groundwater Monitoring Report, dated April 21, 2014, the
following water supply wells were identified within 1,000 feet of the site:

Distance from
source (ft)
Municipal
Water
Available
Active Drinking
Water Well
Inactive
Drinking
Water Well
Irrigation
Well
Surface
Water Body
0 – 500 Yes
WSW-1, WSW-4*,
WSW-7, WSW-8,
WSW-10, WSW-11
WSW-2 and
WSW-3
None
observed
None
observed
500 – 1000 Yes WSW-5A, WSW-6,
and WSW-9
None
observed
None
observed
None
observed
*WSW-4 has a point of entry (POE) treatment system.

 Municipal water is available to the site and surrounding properties.

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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Recommendations:

 Determine if water supply well owners will connect to the municipal service.

 Delineate the extent of soil contamination by advancing additional soil borings and
collecting soil samples for laboratory analysis.

 Delineate the extent of groundwater contamination by obtaining access to surrounding
properties and installing additional groundwater wells.

 Continue periodic sampling of water supply wells.

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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3. SCOPE OF SERVICES
3.1 Contract Information

The scope of services for this report was performed in general accordance with S&ME’s
proposal number 43-1500743, dated March 3, 2015. The scope of services was authorized by the
North Carolina Department of Environment Quality (NCDEQ) Task Authorization TA-01, dated
March 10, 2015, and within contract number N14005i. Project delays were encountered because
of multiple attempts by NCDEQ to obtain access agreements.

3.2 Approved Scope of Services

S&ME’s approved Scope of Services for this Task Authorization included installing two monitor
wells (MW-8 and MW-9) collecting groundwater samples from up to 10 monitor wells (MW-1
through MW-9, and DW-1), collecting samples from up to eight water supply wells (WSW-1,
WSW-4 (influent and effluent), WSW-5A, WSW-7, WSW-8, WSW-10, and WSW-11), and
preparing this report. These services were completed with the following exceptions:

 NCDEQ was unable to obtain access agreements to install two new monitor wells MW-8
and MW-9, therefore no groundwater samples were collected.
 S&ME was unable to gain permission to sample water supply wells WSW-4 (influent and
effluent), WSW-5A, WSW-7, WSW-8, and WSW-10; therefore, no samples were
collected from these wells.

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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4. SITE HISTORY AND CHARACTERIZATION
The subject site is located at 2027 US Highway 1 North in Wise, Warren County, North Carolina. A
vicinity map of the site is shown on Figure 1, and the site and pertinent features are shown on
Figure 2. Photographs of the site are provided in Appendix I.

The site consists of the former Wise Convenient Mart structure (now vacant), three occupied
residential homes, and several storage sheds and outbuildings. The adjoining properties consist
of rural residential development and agricultural fields.

According to a Groundwater Monitoring Report prepared by Terraquest Environmental
Consultants, P.C. (Terraquest), and dated January 4, 2011, two 550-gallon gasoline underground
storage tanks (USTs) were installed at the site prior to 1954. The USTs were reportedly removed
from the site in 1988, prior to the existence of UST regulations. The Terraquest report references
a Phase II Limited Site Assessment prepared by ATC Associates on May 19, 2006 (S&ME did
not receive a copy of this report for review). According to the ATC report, 11 private water
supply wells were identified in the vicinity of the site. Municipal water service is reportedly
available to the site and surrounding properties. ATC installed five groundwater monitor wells
(labeled as MW-1 through MW-5) at the site and collected groundwater and soil samples. The
laboratory analytical results of the groundwater samples collected by ATC indicated that several
volatile organic compounds (VOCs) were detected in concentrations exceeding their respective
North Carolina 2L Groundwater Standards (2LStandards) in monitor wells MW-1, MW-2, and
MW-5. The laboratory analytical results of soil samples collected by ATC were not available.
One additional monitor well (MW-6) was installed to further delineate the extent of groundwater
contamination.

On November 11, 2010, Terraquest completed a Comprehensive Site Assessment (CSA) at the
site. During this investigation, one additional Type II shallow monitor well (MW-7) and Type
III deep monitor well (DW-1) were installed at the site. During the investigation, approximately
0.75 feet of free product was measured in MW-1.

Between April 12 and 16, 2010, Terraquest conducted a mobile multi-phase extraction (MMPE)
event at the site. During the event, 8,559 gallons of contaminated groundwater were recovered.
A total of 708.15 pounds (approximately 131.38 gallons) of petroleum as gasoline were
calculated to have been discharged as vapor.

On October 22, 2012, Crawford Environmental Services (CES) collected groundwater samples
from the monitor well network. The laboratory analytical results of the groundwater samples
indicated that several VOCs were detected in concentrations exceeding their respective 2L
Standards in the samples collected from MW-1, MW-2, and MW-5. Five water supply wells
were sampled (WSW-1, WSW-4, WSW-5A, and WSW-6). Concentrations of VOCs were
detected in concentrations below their respective 2L Standards in the samples collected from
water supply wells WSW-1, WSW-4 (post POE), and WSW-5A.

On March 13, 2014, S&ME collected groundwater samples from seven groundwater monitor
wells at the site (MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, and DW-1). Monitor well MW-
1 contained approximately 0.25 inches of free product and was not sampled. The laboratory

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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analytical results of the groundwater samples indicated that several VOCs were detected in
concentrations exceeding their respective 2L Standards in MW-5. In addition, benzene was also
detected above the 2L Standard in monitor wells MW-2 and MW-6.

On March 13, 2014, S&ME collected water samples from six water supply wells (WSW-1,
WSW-5A, WSW-6, WSW-7, WSW-8, and WSW-11). Six other water supply wells (WSW-2,
WSW-3, WSW-4, WSW-5, WSW-9, and WSW-10) were not sampled because they were either
inactive or the homeowner was not present at the time of sampling. The laboratory analytical
results of the water supply well samples indicated that MTBE was detected below the 2L
Standard in WSW-1 and WSW-7 and 1,2-dichloroethane and di-isopropyl ether were detected
below their respective 2L Standards in the water sample collected from WSW-5A.

4.1 UST Owner and Operator Information.
The former owner/operator of the UST system in unknown. The property is now owned by Mr.
Donald Paynter. Information about the owner/operator of the UST system and the dates of
operation are provided in Table 1.

4.2 UST Information
According to a Groundwater Monitoring Report prepared by Terraquest Environmental
Consultants, P.C. (Terraquest), and dated January 4, 2011, two 550-gallon gasoline underground
storage tanks (USTs) were installed at the site prior to 1954. The USTs were reportedly removed
from the site in 1988, prior to the existence of UST regulations. Information about the UST
System is provided in Table 2.

4.3 Description of the UST Release
The Terraquest report references a Phase II Limited Site Assessment prepared by ATC
Associates on May 19, 2006 (S&ME did not receive a copy of this report for review). According
to the ATC report, 11 private water supply wells were identified in the vicinity of the site.
Municipal water service is reportedly available to the site and surrounding properties. ATC
installed five groundwater monitor wells (labeled as MW-1 through MW-5) at the site and
collected groundwater and soil samples.

The laboratory analytical results of the groundwater samples collected by ATC indicated that
several volatile organic compounds (VOCs) were detected in concentrations exceeding their
respective 2LStandards in monitor wells MW-1, MW-2, and MW-5. The laboratory analytical
results of soil samples collected by ATC were not available. One additional monitor well (MW-
6) was installed to further delineate the extent of groundwater contamination.

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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5. CURRENT SITE ASSESSMENT INFORMATION
5.1 Current Liquid Levels
On October 26, 2015, S&ME personnel measured depth to groundwater from the top of casing in
monitoring wells (MW-1 through MW-7, and DW-1). Depth to groundwater was measured
using an electronic interface probe, which emits an audible tone when encountering free product,
and a distinctly different tone when encountering groundwater. The depth to groundwater ranged
from 15.18 feet below top of casing (ft-btoc) in monitor well MW-3 to 19.06 ft-btoc in monitor
well MW-5. S&ME used the depth to groundwater measurements to generate a depth to
groundwater elevation map (Figure 3). The monitor well construction details, depth to
groundwater measurements are provided in Table 3.
5.2 Groundwater Monitoring Events
On October 26, 2015, S&ME collected groundwater samples from eight monitor wells (MW-1
through MW-7, and DW-1). The monitor wells were purged and sampled using new
polyethylene bailers. The wells were purged approximately three casing volumes or bailed dry
and allowed to recover prior to sampling. The field parameters consisting of temperature, pH,
and specific conductance were measured and recorded for each casing volume removed. The
groundwater samples were collected directly into laboratory-supplied containers, placed in a
cooler on ice, and shipped under standard chain-of-custody protocol to Con-Test Analytical
Services, Inc. (Con-Test) of East Longmeadow, Massachusetts, a North Carolina certified
laboratory, for analysis. The samples were analyzed for VOCs by EPA Method 6200B. The
field sampling sheets are provided in Appendix II.
5.3 Water Supply Wells
S&ME was granted permission to collect a sample from water supply wells WSW-1 and WSW-
11. S&ME was unsuccessful in obtaining permission from the property owners associated with
water supply wells WSW-4 (influent and effluent), WSW-5A, WSW-7, WSW-8, and WSW-10.
Information pertaining to the water supply wells and adjacent property owners is included in
Table 4. Well locations are shown on Figure 4.
5.4 Water Supply Well Monitoring Event
On October 26, 2015, S&ME sampled WSW-1 and WSW-11. The samples from the water
supply wells was collected from spigot at the well houses. The tap was opened and the water was
allowed to run for approximately 15 minutes prior to sample collection. The samples were
collected directly into laboratory-supplied containers, placed in a cooler on ice, and shipped
under standard chain-of-custody procedure to Con-Test for analysis. The samples were analyzed
for VOCs by EPA Method 6200B. The field sampling sheets are provided in Appendix II.
Water supply well information is provided in Table 4.
5.5 Summary of Groundwater and Free Product Assessment Information
The laboratory analytical results for the groundwater samples collected from monitor wells MW-
1 through MW-7, and DW-1 indicated that the following constituents were reported at
concentrations above the 2L Standards:

 Benzene in monitor wells MW-1, MW-2, MW-5, and MW-6;

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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 1,2-dibromoethane (EDB) in MW-5, and MW-6;
 Ethylbezene in MW-1;
 P-Isopropyltoluene in MW-1;
 Naphthalene in MW-1, MW-2, and MW-5;
 N-propylbenzene in MW-1;
 Toluene in MW-1;
 1,2,4-Trimethylbenzene in MW-1;
 1,3,5-Trimethylbenzene in MW-1; and,
 Total Xylenes in MW-1 and MW-5.

Additional constituents were reported in groundwater samples collected from MW-1, MW-2,
MW-5 and MW-6 in concentrations below their respective 2L Standards. No targeted
constituents were reported at concentrations above the laboratory analytical method detection
limits in the groundwater samples collected from monitor wells MW-3, MW-4, MW-7 and DW-
1. No free product was measured in any of the monitor wells. A summary of the groundwater
analytical results is provided in Table 5, and are shown in Figure 5. A copy of the laboratory
analytical report and chain-of-custody record in provided in Appendix III.

5.6 Summary of Water Supply Well Assessment Information
No targeted constituents were reported at concentrations above the laboratory analytical method
detection limits in the groundwater samples collected from WSW-1 and WSW-11. A summary
of the water supply well analytical results is presented in Table 6. A copy of the laboratory
analytical report and chain-of-custody record are provided in Appendix III.

5.7 Regional and Site Geology and Hydrogeology
5.7.1 Soil and Bedrock
According to the Geologic Map of North Carolina, dated 1985, the site lies within Raleigh Belt
of the Piedmont Physiographic Province, which is categorized by broadly sloping plains of
moderate topographic relief with good drainage and soil development. The site is underlain by
Permian to Pennsylvanian granitic rock.
5.7.2 Hydrogeology
S&ME used the depth to groundwater measurements to generate a depth to groundwater
elevation map (Figure 3). Groundwater flow direction at the site is generally north. The
hydraulic conductivity at the site has not been measured; therefore, the linear groundwater
velocity was not calculated.

5.8 Evaluation of Groundwater Assessment Information
5.8.1 Current Extent and Severity of Contamination
Historically, the highest concentrations of contaminants have been detected in monitor well
MW-1. MW-1 is located in front of the Wise convenient mart store. No contaminants have been

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

11
detected at concentrations exceeding the Gross Contaminant Levels (GCLs) and free product was
not been detected in any monitor well during this event. However, free product was previously
measured in MW-1 (March 2014). Contaminant concentrations in monitor wells MW-1, MW-2,
MW-5 and MW-6 have decreased. No contaminants were detected in monitor well MW-3, MW-
4, MW-7, and DW-1 at concentrations above their laboratory method detection limits. The
impacted groundwater plume is not delineated in the down-gradient direction east of US
Highway 1 North.

5.8.2 Cleanup Levels Achieved
 Soil (soil-to-groundwater maximum soil contaminant concentrations) No
 Groundwater (2L standard concentrations) No
 Free Product (Measured greater than 0.01’) Yes

Groundwater Monitoring Report S&ME Project No. 4305-15-094
TF-1943 Wise Convenience Mart, Wise, Warren County, NC March 2, 2016

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6. CONCLUSIONS AND RECOMMENDATIONS
Based on the current and historical assessment information for the site, the following conclusions
are presented:

1. The UST Incident meets the following conditions for a High Risk classification:
a. There are active drinking water supply wells within 1,000 feet of the source area.
b. Contaminant levels in the groundwater exceed the 2L Standards
2. Groundwater contaminant concentrations do not appear to be decreasing in a consistent
trend.

Based on the above, the following recommendations are presented:

1. Determine if water supply well owners will connect to the municipal service;
2. Delineate the extent of soil contamination by advancing additional soil borings and
collecting soil samples for laboratory analysis.
3. Delineate the extent of groundwater contamination by obtaining access to surrounding
properties and installing additional groundwater wells either on the adjacent property to
the north of the site, or, if permission cannot be obtained, within the NCDOT right-of-
way to the north of the site; and,
4. Continue periodic sampling of water supply wells located down-gradient from the site
(WSW-4, WSW-5A, WSW-6).

TABLES

UST ID
Number UST Information Owner/ Operator Dates of Operation
T1 550 Unknown - 1988
T2 550 Unknown - 1988
Notes:
Current Property Owner: Donald Paynter, P.O. Box 714, Nolina, NC, 27563
TABLE 1
UST owner/operator information from Groundwater Monitoring Report summitted by TerraQuest Environmental on 1/4/11.
Unknown
Wise Convenient Mart
2027 US Highway 1 North
Wise, Warren County, North Carolina
NCDEQ Incident No. 1943
S&ME Project No. 4305-15-094
UST Owner/Operator Information
UST ID
Number Contents Capacity
(gallons)
Tank
Dimensions Date Installed Date Closed Release from
System
T1 gasoline 550 Unknown Unknown 1988 Yes
T2 gasoline 550 Unknown Unknown 1988 Yes
Notes:
UST information from Groundwater Monitoring Report summitted by TerraQuest Environmental on 1/4/11.
S&ME Project No. 4305-15-094
TABLE 2
UST Information
Wise Convenient Mart
2027 US Highway 1 North
Wise, Warren County, North Carolina
NCDEQ Incident No. 1943
9/25/2012 19.42 0.00 78.04
3/13/2014 17.15 0.25 80.32
10/26/2015 16.06 0.00 81.40
9/25/2012 21.26 0.00 77.54
3/13/2014 18.88 0.00 79.92
10/26/2015 17.70 0.00 81.10
9/25/2012 18.43 0.00 78.39
3/13/2014 16.21 0.00 80.61
10/26/2015 15.18 0.00 81.64
9/25/2012 19.37 0.00 77.63
3/13/2014 16.97 0.00 80.03
10/26/2015 15.80 0.00 81.20
9/25/2012 22.71 0.00 77.27
3/13/2014 20.29 0.00 79.69
10/26/2015 19.06 0.00 80.92
9/25/2012 21.48 0.00 75.48
3/13/2014 18.82 0.00 78.14
10/26/2015 17.49 0.00 79.47
9/25/2012 19.94 0.00 67.73
3/13/2014 16.74 0.00 70.93
10/26/2015 15.90 0.00 71.77
9/25/2012 Not Measured N/A N/A
3/13/2014 17.21 0.00 N/A
10/26/2015 16.22 0.00 N/A
NOTES:
1. Top of Casing elevations and data previous to 3/13/2014 is from Crawford Environmental Services, October 22, 201 Groundwater Monitoring Report.
2. BTOC - Below top of casing
3. Ft-bgs - Feet below ground surface
4. The relative elevation for DW-1 has not been measured.
5. N/A - not applicable
NCDEQ Incident No. 1943
TABLE 3
Monitoring Well Construction Details and Groundwater Elevation Measurements
Wise Convenient Mart
2027 US Highway 1 North
Wise, Warren County, North Carolina
S&ME Project No. 4305-15-094
Well ID Date
Installed
Well Casing
Depth (ft.-bgs)
Well Screened
Interval (ft.-bgs)
Total Depth
(ft)
Top of Casing
Elevation
(ft-rel)
Date of
Measurement
Depth to Water
(ft BTOC)
Free Product
Thickness (inches)
10.0 - 25.0 25.0 98.80
25.0
Groundwater
Elevation
(ft)
96.82MW-3 3/6/2006 10.0 10.0 - 25.0
MW-5 3/6/2006 10.0 10.0 - 30.0
MW-4 3/6/2006 10.0 10.0 - 25.0
6. Groundwater elevation data for wells with measurable free product was calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness (ft) x 0.729]
MW-1 11/18/2005 10.0 10.0 - 25.0 25.0 97.46
MW-2 11/18/2005 10.0
DW-1 6/12/2009 55.0 55.0 - 60.0 60.0 Not Measured
97.00
25.0 96.96
MW-7 8/26/2009 10.0 10.0 - 25.0 25.0 87.67
MW-6 9/7/2007 10.0 10.0 - 25.0
99.9830.0
25.0
Private Water Supply Wells
Map ID
/Well ID Parcel Number Property Address Well Owner Owner Address Phone Number Well Use Sampled
Distance from
source area of
release*
(feet)
Comment
WSW-1 2040131168 2027 US Highway 1 North, Wise, NC Donald and Edward Paynter P.O. Box 714, Norlina, NC 252-456-2139 Potable Yes 300' SW Sample Collected
WSW-2 2040131168 2027 US Highway 1 North, Wise, NC Donald and Edward Paynter P.O. Box 714, Norlina, NC 252-456-2139 Not in Service No 80' W Well not in service.
WSW-3 2040030515 2041 US Highway 1 North, Wise, NC Walter and Joanne Paynter 2041 US Highway 1 North, Wise, NC 252-456-2408 Not in Service No 360' NW Well not in service.
WSW-4 2040030515 2041 US Highway 1 North, Wise, NC Walter and Joanne Paynter 2041 US Highway 1 North, Wise, NC 252-456-2408 Potable No 600' NW POE system present at well. Resident not home at time of
sampling - no sample collected.
WSW-5 2030945267 2049 US Highway 1 North, Wise, NC Willie Felts, Jr.2049 US Highway 1 North, Wise, NC 252-456-4809 Not in Service No 640' NW Well not in service.
WSW-5A 2040042185 2061 US Highway 1 North, Wise, NC Willie Felts, Jr.2049 US Highway 1 North, Wise, NC 252-456-4809 Potable Yes 1,100' NW Resident/Occupant not home at time of sampling - no
sample collected.
WSW-6 2040038915 2061 US Highway 1 North, Wise, NC Willie Felts, Jr.2049 US Highway 1 North, Wise, NC 252-456-4809 Potable Yes 720' NW Resident/Occupant not home at time of sampling - no
sample collected.
WSW-7 2040122925 2007 US Highway 1 North, Wise, NC Joe and Mary Ann Hunt P.O. Box 153, Wise, NC 252-456-4256 Potable Yes 400' S Resident/Occupant not home at time of sampling - no
sample collected.
WSW-8 2040123522 1989 US Highway 1 North, Wise, NC Annie Morris 1989 US Highway 1 North, Wise, NC 252-456-2540 Potable Yes 740' S Resident/Occupant not home at time of sampling - no
sample collected.
WSW-9 2040124079 1971 US Highway 1 North, Wise, NC Ashley and Stuart White 807 Rocker Dairy Rd., Norlina, NC 252-456-4261 Potable No 1,080' SE Resident/Occupant not home at time of sampling - no
sample collected.
WSW-10 2040125855 2002 US Highway 1 North, Wise, NC Ashley and Stuart White 807 Rocker Dairy Rd., Norlina, NC 252-456-4261 Potable No 560' SE Resident/Occupant not home at time of sampling - no
sample collected.
WSW-11 2040135011 2004 US Highway 1 North, Wise, NC Judith Sammons 2004 US Highway 1 North, Wise, NC 252-456-2028 Potable Yes 540' SE Sample Collected
Notes:
1. Water SupplyWells (WSW).
2. Refer toFigure 3for WSW locations
3. Site identification/ownership information is from Warren County's GIS website accessed November 9, 2015.
4. P.O.E. = Point of EntrySystem
TABLE 4
Water Supply Well Information
Wise Convenient Mart
2027 US Highway 1 North
Wise, Warren County, North Carolina
NCDEQ Incident No. 1943
S&ME Project No. 4305-15-094
Contaminant ofConcern
benzenen-butylbenzenesec-butylbenzenetert-butylbenzene1,2-dichloroethane1,2-dibromoethane(EDB)di-isopropyletherethylbenzeneisopropylbenzenep-Isopropyltoluenemethyl-tert-butylethernaphthalenen-propylbenzenetetrachloroethylenestyrenetoluene1,1,2-trichloroethane1,2,4-trimethylbenzene1,3,5-trimethylbenzenetotalxylenesDate
9/25/2012 1,100 57 BDL BDL BDL BDL BDL 2,090 120 BDL BDL 589 254 BDL BDL 13,600 BDL 2,200 618 12,310
3/13/2014
10/26/2015 180 65 9.7 1.4 BDL 5.9 BDL 1,200 60 36 BDL 340 180 BDL BDL 7,600 BDL 1,500 510 7,700
9/25/2012 82.3 BDL BDL BDL 2 0.71 82.2 183 6.9 BDL 1.1 49.4 14.5 BDL BDL 714 BDL 113 36.4 646
3/13/2014 28 1 BDL BDL BDL BDL 25 87 2.6 BDL BDL 13 5.6 BDL BDL 200 BDL 39 14 239
10/26/2015 15 BDL 0.19 BDL 0.39 BDL 13 71 2.2 0.4 0.15 15 4.5 BDL 2.3 13 BDL 23 11 147
9/25/2012 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/13/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
10/26/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/25/2012 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/13/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.12 BDL BDL BDL BDL BDL BDL
10/26/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/25/2012 1,770 BDL BDL BDL 51.6 BDL 427 374 21.2 BDL 38.4 173 32.6 BDL BDL 1,530 BDL 473 145 2,749
3/13/2014 1,900 6.5 BDL BDL 58 BDL 250 370 21 BDL 11 60 30 BDL BDL 1,400 BDL 380 110 2,350
10/26/2015 650 2.9 BDL BDL BDL BDL 56 130 8 1.4 2.1 53 11 BDL BDL 470 BDL 140 46 900
9/25/2012 BDL BDL BDL BDL 1.6 BDL 12.1 BDL BDL BDL 2.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/13/2014 5.4 BDL BDL BDL 7.1 0.37 54 0.41 BDL BDL 3.4 BDL BDL BDL BDL 0.28 0.22 0.49 BDL 2.9
10/26/2015 15 BDL BDL BDL 5 0.31 23 1.8 0.22 BDL 2.8 0.88 0.21 BDL BDL 1.6 BDL 1.90 BDL 10.8
9/25/2012 BDL BDL BDL BDL BDL BDL 6.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/13/2014 BDL BDL BDL BDL BDL BDL 1.9 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
10/26/2015 BDL BDL BDL BDL BDL BDL 0.63 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/25/2012
3/13/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
10/26/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1 70 70 70 6 0.02 70 600 70 25 20 6 70 0.7 70 600 0.6 400 400 500
5,000 6,900 8,500 15,000 6,000 50 70,000 84,500 25,000 11,700 20,000 6,000 30,000 7,000 70,000 260,000 600 28,500 25,000 85,500
Notes:1. Analytes that are not shown were not detected for the method.2. All concentrations are reported in micrograms per liter (µg/L).3. 2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.02024. VOCs: Volatile Organic Compounds5. Concentrations exceeding the 2L Standards are shown in Shaded andBOLDfields.6. Concentrations exceeding the laboratory's reporting limits are shown inBOLDfields.
7. Analysis for parameter not requested.
8. Data prior to 3/13/2014 was collected by others.9. BDL: Below laboratory detection limits
NCDEQ Incident No. 1943
TABLE 5Summary of Groundwater Analytical Results
Wise Convenient Mart
2201 US Highway 1 NorthWise, Warren County, North Carolina
S&ME Project No. 4305-15-094
Volatile Organic Compounds (VOCs) by EPA Method 6200B or Equivalent (µg/L)
Sample ID
Not Sampled - Approximately 0.25 inches of Free Product
Not Sampled
2L Standards
Gross Contamination Levels
MW-1
MW-2
MW-3
MW-4
MW-5
MW-6
MW-7
DW-1
Contaminant of
Concern
benzeneethylbenzenetotalxylenesdi-isopropylethermethyltert-butylethernaphthalene1,2-dichloroethane1,2,4-trimethylbenzene1,3,5-trimethylbenzeneDate
9/25/2012 BDL BDL BDL BDL 0.92 BDL BDL BDL BDL
3/13/2014 BDL BDL BDL BDL 0.18 BDL BDL BDL BDL
10/26/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL
WSW-3 10/26/2015
9/25/2012
3/13/2014
10/26/2015
9/25/2012 BDL BDL BDL BDL BDL BDL 1.3 BDL BDL
3/13/2014
10/26/2015
WSW-5 10/26/2015
9/25/2012 BDL BDL BDL 5.6 BDL BDL 1.6 BDL BDL
3/13/2014 BDL BDL BDL 4.5 BDL BDL 1.1 BDL BDL
10/26/2015
WSW-6 10/26/2015
3/13/2014 BDL BDL BDL BDL 0.40 BDL BDL BDL BDL
10/26/2015
3/13/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL
10/26/2015
WSW-9 10/26/2015
WSW-10 10/26/2015
3/13/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL
10/26/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL
1 600 500 70 20 6 6 400 400
5,000 84,500 85,500 70,000 20,000 6,000 6,000 28,500 25,000
Notes:
1. Analytes that are not shown were not detected.
2. All concentrations are reported in micrograms per liter (µg/L).
3. 2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
4. VOCs: Volatile Organic Compounds
5. All samples that exceed the 2L Standards are shown in Shaded andBOLDfields.
6. Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.
7. WSW-4 has a point of entry (POE) system installed at the wellhead.
NCDEQ Incident No. 1943
TABLE 6
Summary of Water Supply Well Analytical Results
Wise Convenient Mart
2027 US Highway 1 North
Wise, Warren County, North Carolina
S&ME Project No. 4305-15-094
Volatile Organic Compounds (VOCs) by EPA Method 6200B or Equivalent
Sample ID
WSW-1
WSW-4 Influent
Sample Not Collected
Sample Not Collected
WSW-4 Effluent Sample Not Collected
Gross Contamination Levels
Sample Not Requested - Well is Out of Service
Sample Not Collected
Sample Not Collected
Sample Not Collected
Sample Not Requested - Well is Out of Service
Sample Not Requested
WSW-11
WSW-5A
Sample Not Requested
Sample Not Collected- Connected to Municipal Water
2L Standards
Sample Not CollectedWSW-8
Sample Not CollectedWSW-7

FIGURES

SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
VICINITY MAP
2027 US HWY 1 NORTH
WISE, NORTH CAROLINA
1" = 2000'
BTR
NOV 2015
4305-15-094
1
A-5595
WISE CONVENIENT MART TF-1943
2000 4000
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-094\CAD\A5595.dwg, FIG1, 12/16/2015 3:47:49 PM, 1:1
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
SITE MAP
2027 US HWY 1 NORTH
WISE, NORTH CAROLINA
1" = 120'
BTR
NOV 2015
4305-15-094
2
A-5596
WISE CONVENIENT MART TF-1943
120 240
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-094\CAD\A5596.dwg, FIG2, 12/16/2015 3:47:36 PM, 1:1
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
GROUNDWATER ELEVATION MAP
2027 US HWY 1 NORTH
WISE, NORTH CAROLINA
1" = 120'
BTR
NOV 2015
4305-15-094
3
A-5598
WISE CONVENIENT MART TF-1943
120 240
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-094\CAD\A5598.dwg, FIG3, 1/4/2016 1:26:45 PM, 1:1
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM 2027 US HWY 1 NORTH
WISE, NORTH CAROLINA
1" = 400'
BTR
NOV 2015
4305-15-094
4
A-5597
WATER SUPPLY WELL
CONSTITUENT MAP
WISE CONVENIENT MART TF-1943
400 800
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-094\CAD\A5597.dwg, FIG4, 1/4/2016 1:27:04 PM, 1:1
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
GROUNDWATER CONSTITUENT MAP
2027 US HWY 1 NORTH
WISE, NORTH CAROLINA
1" = 120'
BTR
NOV 2015
4305-15-094
5
A-5599
WISE CONVENIENT MART TF-1943
120 240
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-094\CAD\A5599.dwg, FIG5, 12/16/2015 3:48:03 PM, 1:1

APPENDICES

APPENDIX I

Photographic Log

Groundwater Monitoring Report Wise Convenient Mart TF-1943
Wise, Warren County, North Carolina
S&ME Project No. 4305-15-094
Taken by: 10/26/15 Date Taken: BB
1

1 MW-1 and DW-1 2 MW-2

3 MW-3

4 MW-4

Groundwater Monitoring Report Wise Convenient Mart TF-1943
Wise, Warren County, North Carolina
S&ME Project No. 4305-15-094
Taken by: 10/26/15 Date Taken: BB
2

5 MW-5 6 MW-6

7 MW-7 8 WSW-1

APPENDIX II

Field Sampling Forms

APPENDIX III

Laboratory Analytical Report and Chain-of-Custody Record
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
November 9, 2015
Alan Culpepper
S&ME, Inc - Raleigh, NC
3201 Spring Forest Rd.
Raleigh, NC 27616
Project Location: Wise Convenient Mart, NC
Client Job Number:
Project Number: 4305-15-094
Laboratory Work Order Number: 15J1337
Enclosed are results of analyses for samples received by the laboratory on October 27, 2015. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 45
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 10
15J1337-01 10
15J1337-02 12
15J1337-03 14
15J1337-04 16
15J1337-05 18
15J1337-06 20
15J1337-07 22
15J1337-08 24
15J1337-09 26
15J1337-10 28
Sample Preparation Information 30
QC Data 31
Volatile Organic Compounds by GC/MS 31
B134679 31
B134803 35
Flag/Qualifier Summary 39
Certifications 40
Chain of Custody/Sample Receipt 42
Page 2 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
11/9/2015
S&ME, Inc - Raleigh, NC
3201 Spring Forest Rd.
Raleigh, NC 27616
ATTN: Alan Culpepper
4305-15-094
15J1337
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Wise Convenient Mart, NC
DW-1 15J1337-01 Ground Water SM21-22 6200B
MW-1 15J1337-02 Ground Water SM21-22 6200B
MW-4 15J1337-03 Ground Water SM21-22 6200B
MW-3 15J1337-04 Ground Water SM21-22 6200B
MW-2 15J1337-05 Ground Water SM21-22 6200B
MW-5 15J1337-06 Ground Water SM21-22 6200B
MW-7 15J1337-07 Ground Water SM21-22 6200B
MW-6 15J1337-08 Ground Water SM21-22 6200B
WSW-1 15J1337-09 Ground Water SM21-22 6200B
WSW-11 15J1337-10 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:15J1337-01DW-1
No Results Detected
Client ID:Lab ID:15J1337-03MW-4
No Results Detected
Client ID:Lab ID:15J1337-04MW-3
No Results Detected
Client ID:Lab ID:15J1337-09WSW-1
No Results Detected
Client ID:Lab ID:15J1337-10WSW-11
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
15J1337-02MW-1
DL
1,2,4-Trimethylbenzene 1500 5.0 g/L SM21-22 6200B1.8
1,2-Dibromoethane (EDB)5.9 5.0 g/L SM21-22 6200B0.89
1,3,5-Trimethylbenzene 510 5.0 g/L SM21-22 6200B1.0
Benzene 180 5.0 g/L SM21-22 6200B0.79
Ethylbenzene 1200 5.0 g/L SM21-22 6200B1.3
Isopropylbenzene (Cumene)60 5.0 g/L SM21-22 6200B1.2
m+p Xylene 4400 10 g/L SM21-22 6200BE2.5
Naphthalene 340 5.0 g/L SM21-22 6200B1.2
n-Butylbenzene 65 5.0 g/L SM21-22 6200B1.0
n-Propylbenzene 180 5.0 g/L SM21-22 6200B1.1
p-Isopropyltoluene (p-Cymene)36 5.0 g/L SM21-22 6200B1.2
sec-Butylbenzene 9.7 5.0 g/L SM21-22 6200B1.1
tert-Butylbenzene 1.4 5.0 g/L SM21-22 6200BJ1.1
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
15J1337-05MW-2
DL
1,2,4-Trimethylbenzene 23 0.50 g/L SM21-22 6200B0.18
1,2-Dichloroethane 0.39 0.50 g/L SM21-22 6200BJ0.19
1,3,5-Trimethylbenzene 11 0.50 g/L SM21-22 6200B0.10
Benzene 15 0.50 g/L SM21-22 6200B0.079
Diisopropyl Ether (DIPE)13 0.50 g/L SM21-22 6200B0.18
Ethylbenzene 71 0.50 g/L SM21-22 6200B0.13
Isopropylbenzene (Cumene)2.2 0.50 g/L SM21-22 6200B0.12
m+p Xylene 67 1.0 g/L SM21-22 6200B0.25
Methyl tert-Butyl Ether (MTBE)0.15 0.50 g/L SM21-22 6200BJ0.090
Naphthalene 15 0.50 g/L SM21-22 6200B0.12
n-Propylbenzene 4.5 0.50 g/L SM21-22 6200B0.11
o-Xylene 80 0.50 g/L SM21-22 6200B0.13
p-Isopropyltoluene (p-Cymene)0.40 0.50 g/L SM21-22 6200BJ0.12
sec-Butylbenzene 0.19 0.50 g/L SM21-22 6200BJ0.11
Styrene 2.3 0.50 g/L SM21-22 6200B0.15
Toluene 13 0.50 g/L SM21-22 6200B0.10
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
15J1337-06MW-5
DL
1,2,4-Trimethylbenzene 140 5.0 g/L SM21-22 6200B1.8
1,3,5-Trimethylbenzene 46 5.0 g/L SM21-22 6200B1.0
Benzene 650 5.0 g/L SM21-22 6200B0.79
Diisopropyl Ether (DIPE)56 5.0 g/L SM21-22 6200B1.8
Ethylbenzene 130 5.0 g/L SM21-22 6200B1.3
Isopropylbenzene (Cumene)8.3 5.0 g/L SM21-22 6200B1.2
m+p Xylene 630 10 g/L SM21-22 6200B2.5
Methyl tert-Butyl Ether (MTBE)2.1 5.0 g/L SM21-22 6200BJ0.90
Naphthalene 53 5.0 g/L SM21-22 6200B1.2
n-Butylbenzene 2.9 5.0 g/L SM21-22 6200BJ1.0
n-Propylbenzene 11 5.0 g/L SM21-22 6200B1.1
o-Xylene 270 5.0 g/L SM21-22 6200B1.3
p-Isopropyltoluene (p-Cymene)1.4 5.0 g/L SM21-22 6200BJ1.2
Toluene 470 5.0 g/L SM21-22 6200B1.0
Page 5 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
15J1337-07MW-7
DL
Diisopropyl Ether (DIPE)0.63 0.50 g/L SM21-22 6200B0.18
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
15J1337-08MW-6
DL
1,2,4-Trimethylbenzene 1.9 0.50 g/L SM21-22 6200B0.18
1,2-Dibromoethane (EDB)0.31 0.50 g/L SM21-22 6200BJ0.089
1,2-Dichloroethane 5.0 0.50 g/L SM21-22 6200B0.19
Benzene 15 0.50 g/L SM21-22 6200B0.079
Diisopropyl Ether (DIPE)23 0.50 g/L SM21-22 6200B0.18
Ethylbenzene 1.8 0.50 g/L SM21-22 6200B0.13
Isopropylbenzene (Cumene)0.22 0.50 g/L SM21-22 6200BJ0.12
m+p Xylene 7.3 1.0 g/L SM21-22 6200B0.25
Methyl tert-Butyl Ether (MTBE)2.8 0.50 g/L SM21-22 6200B0.090
Naphthalene 0.88 0.50 g/L SM21-22 6200B0.12
n-Propylbenzene 0.21 0.50 g/L SM21-22 6200BJ0.11
o-Xylene 3.5 0.50 g/L SM21-22 6200B0.13
Toluene 1.6 0.50 g/L SM21-22 6200B0.10
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
Page 7 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SM21-22 6200B
Qualifications:
Reported result is estimated. Value reported over verified calibration range.
Analyte & Samples(s) Qualified:
E
m+p Xylene
15J1337-02[MW-1]
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Acetate
B134679-BS1, B134679-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
2,2-Dichloropropane
15J1337-01[DW-1], 15J1337-02[MW-1], 15J1337-03[MW-4], 15J1337-04[MW-3], 15J1337-05[MW-2], 15J1337-06[MW-5], 15J1337-07[MW-7], 15J1337-08[MW-6],
15J1337-09[WSW-1], 15J1337-10[WSW-11], B134679-BLK1, B134679-BS1, B134679-BSD1, B134803-BLK1, B134803-BS1, B134803-BSD1
Bromoform
15J1337-01[DW-1], 15J1337-02[MW-1], 15J1337-03[MW-4], 15J1337-04[MW-3], 15J1337-05[MW-2], 15J1337-06[MW-5], 15J1337-07[MW-7], 15J1337-08[MW-6],
15J1337-09[WSW-1], 15J1337-10[WSW-11], B134679-BLK1, B134679-BS1, B134679-BSD1, B134803-BLK1, B134803-BS1, B134803-BSD1
Carbon Tetrachloride
15J1337-01[DW-1], 15J1337-02[MW-1], 15J1337-03[MW-4], 15J1337-04[MW-3], 15J1337-05[MW-2], 15J1337-06[MW-5], 15J1337-07[MW-7], 15J1337-08[MW-6],
15J1337-09[WSW-1], 15J1337-10[WSW-11], B134679-BLK1, B134679-BS1, B134679-BSD1, B134803-BLK1, B134803-BS1, B134803-BSD1
Chlorodibromomethane
15J1337-01[DW-1], 15J1337-02[MW-1], 15J1337-03[MW-4], 15J1337-04[MW-3], 15J1337-05[MW-2], 15J1337-06[MW-5], 15J1337-07[MW-7], 15J1337-08[MW-6],
15J1337-09[WSW-1], 15J1337-10[WSW-11], B134679-BLK1, B134679-BS1, B134679-BSD1, B134803-BLK1, B134803-BS1, B134803-BSD1
trans-1,3-Dichloropropene
15J1337-05[MW-2], B134803-BLK1, B134803-BS1, B134803-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Acetone
B134679-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Bromomethane
15J1337-01[DW-1], 15J1337-02[MW-1], 15J1337-03[MW-4], 15J1337-04[MW-3], 15J1337-06[MW-5], 15J1337-07[MW-7], 15J1337-08[MW-6], 15J1337-09[WSW-1],
15J1337-10[WSW-11], B134679-BLK1, B134679-BS1, B134679-BSD1
Methylene Chloride
15J1337-01[DW-1], 15J1337-02[MW-1], 15J1337-03[MW-4], 15J1337-04[MW-3], 15J1337-06[MW-5], 15J1337-07[MW-7], 15J1337-08[MW-6], 15J1337-09[WSW-1],
15J1337-10[WSW-11], B134679-BLK1, B134679-BS1, B134679-BSD1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
15J1337-02[MW-1], 15J1337-06[MW-5]
Page 8 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 9 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-01
Field Sample #: DW-1
Sample Matrix: Ground Water
Sampled: 10/26/2015 12:15
[TOC_2]15J1337-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 4:15 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
ND 0.50 11/6/15 4:15 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 4:15 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 4:15 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 4:15 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 4:15 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 4:15 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 4:15 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 4:15 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 4:15 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 4:15 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 4:15 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 4:15 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 4:15 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 4:15 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 4:15 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 4:15 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 4:15 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 4:15 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/6/15 4:15 MFFg/L0.089 11/5/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/6/15 4:15 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 4:15 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 4:15 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 4:15 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 4:15 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/6/15 4:15 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 4:15 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 4:15 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 4:15 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 4:15 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 4:15 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 4:15 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 4:15 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/6/15 4:15 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 4:15 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/6/15 4:15 MFFg/L0.12 11/5/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/6/15 4:15 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/6/15 4:15 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 4:15 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 4:15 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 10 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-01
Field Sample #: DW-1
Sample Matrix: Ground Water
Sampled: 10/26/2015 12:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/6/15 4:15 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
ND 0.50 11/6/15 4:15 MFFg/L0.11 11/5/15SM21-22 6200B1n-Propylbenzene
ND 0.50 11/6/15 4:15 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 4:15 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/6/15 4:15 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 4:15 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 4:15 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 4:15 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 4:15 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 4:15 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 4:15 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 4:15 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/6/15 4:15 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 4:15 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 4:15 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
ND 1.0 11/6/15 4:15 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
ND 0.50 11/6/15 4:15 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.4 11/6/15 4:1570-130
Toluene-d8 101 11/6/15 4:1570-130
4-Bromofluorobenzene 98.7 11/6/15 4:1570-130
Page 11 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 10/26/2015 12:40
[TOC_2]15J1337-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 11/6/15 8:10 MFFg/L49 11/5/15SM21-22 6200B10Acetone
180 5.0 11/6/15 8:10 MFFg/L0.79 11/5/15SM21-22 6200B10Benzene
ND 5.0 11/6/15 8:10 MFFg/L1.5 11/5/15SM21-22 6200B10Bromobenzene
ND 5.0 11/6/15 8:10 MFFg/L2.2 11/5/15SM21-22 6200B10Bromochloromethane
ND 5.0 11/6/15 8:10 MFFg/L0.88 11/5/15SM21-22 6200B10Bromodichloromethane
ND 10 11/6/15 8:10 MFFg/L2.1 11/5/15SM21-22 6200B10L-04Bromoform
ND 10 11/6/15 8:10 MFFg/L9.4 11/5/15SM21-22 6200B10R-05Bromomethane
ND 50 11/6/15 8:10 MFFg/L24 11/5/15SM21-22 6200B102-Butanone (MEK)
65 5.0 11/6/15 8:10 MFFg/L1.0 11/5/15SM21-22 6200B10n-Butylbenzene
9.7 5.0 11/6/15 8:10 MFFg/L1.1 11/5/15SM21-22 6200B10sec-Butylbenzene
1.4 5.0 11/6/15 8:10 MFFg/L1.1 11/5/15SM21-22 6200B10Jtert-Butylbenzene
ND 5.0 11/6/15 8:10 MFFg/L1.2 11/5/15SM21-22 6200B10L-04Carbon Tetrachloride
ND 5.0 11/6/15 8:10 MFFg/L1.6 11/5/15SM21-22 6200B10Chlorobenzene
ND 500 11/6/15 8:10 MFFg/L280 11/5/15SM21-22 6200B10Ethanol
ND 5.0 11/6/15 8:10 MFFg/L1.0 11/5/15SM21-22 6200B10L-04Chlorodibromomethane
ND 5.0 11/6/15 8:10 MFFg/L2.8 11/5/15SM21-22 6200B10Chloroethane
ND 5.0 11/6/15 8:10 MFFg/L2.2 11/5/15SM21-22 6200B10Chloroform
ND 5.0 11/6/15 8:10 MFFg/L3.2 11/5/15SM21-22 6200B10Chloromethane
ND 5.0 11/6/15 8:10 MFFg/L1.2 11/5/15SM21-22 6200B102-Chlorotoluene
ND 5.0 11/6/15 8:10 MFFg/L1.3 11/5/15SM21-22 6200B104-Chlorotoluene
5.9 5.0 11/6/15 8:10 MFFg/L0.89 11/5/15SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 11/6/15 8:10 MFFg/L1.0 11/5/15SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 11/6/15 8:10 MFFg/L1.7 11/5/15SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 11/6/15 8:10 MFFg/L1.5 11/5/15SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 11/6/15 8:10 MFFg/L1.8 11/5/15SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 11/6/15 8:10 MFFg/L1.6 11/5/15SM21-22 6200B101,1-Dichloroethane
ND 5.0 11/6/15 8:10 MFFg/L1.9 11/5/15SM21-22 6200B101,2-Dichloroethane
ND 5.0 11/6/15 8:10 MFFg/L2.1 11/5/15SM21-22 6200B101,1-Dichloroethylene
ND 5.0 11/6/15 8:10 MFFg/L1.5 11/5/15SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 11/6/15 8:10 MFFg/L1.5 11/5/15SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 11/6/15 8:10 MFFg/L1.3 11/5/15SM21-22 6200B101,2-Dichloropropane
ND 5.0 11/6/15 8:10 MFFg/L1.1 11/5/15SM21-22 6200B101,3-Dichloropropane
ND 5.0 11/6/15 8:10 MFFg/L1.6 11/5/15SM21-22 6200B10L-042,2-Dichloropropane
ND 5.0 11/6/15 8:10 MFFg/L1.3 11/5/15SM21-22 6200B101,1-Dichloropropene
ND 5.0 11/6/15 8:10 MFFg/L0.62 11/5/15SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 11/6/15 8:10 MFFg/L1.1 11/5/15SM21-22 6200B10trans-1,3-Dichloropropene
ND 5.0 11/6/15 8:10 MFFg/L1.8 11/5/15SM21-22 6200B10Diisopropyl Ether (DIPE)
1200 5.0 11/6/15 8:10 MFFg/L1.3 11/5/15SM21-22 6200B10Ethylbenzene
ND 50 11/6/15 8:10 MFFg/L15 11/5/15SM21-22 6200B102-Hexanone (MBK)
60 5.0 11/6/15 8:10 MFFg/L1.2 11/5/15SM21-22 6200B10Isopropylbenzene (Cumene)
36 5.0 11/6/15 8:10 MFFg/L1.2 11/5/15SM21-22 6200B10p-Isopropyltoluene (p-Cymene)
ND 5.0 11/6/15 8:10 MFFg/L0.90 11/5/15SM21-22 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 11/6/15 8:10 MFFg/L32 11/5/15SM21-22 6200B10R-05Methylene Chloride
ND 50 11/6/15 8:10 MFFg/L15 11/5/15SM21-22 6200B104-Methyl-2-pentanone (MIBK)
Page 12 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 10/26/2015 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
340 5.0 11/6/15 8:10 MFFg/L1.2 11/5/15SM21-22 6200B10Naphthalene
180 5.0 11/6/15 8:10 MFFg/L1.1 11/5/15SM21-22 6200B10n-Propylbenzene
ND 5.0 11/6/15 8:10 MFFg/L1.5 11/5/15SM21-22 6200B10Styrene
ND 20 11/6/15 8:10 MFFg/L1.3 11/5/15SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 11/6/15 8:10 MFFg/L1.7 11/5/15SM21-22 6200B10Tetrachloroethylene
7600 250 11/7/15 8:49 WSDg/L50 11/5/15SM21-22 6200B500Toluene
ND 5.0 11/6/15 8:10 MFFg/L1.4 11/5/15SM21-22 6200B101,2,3-Trichlorobenzene
ND 5.0 11/6/15 8:10 MFFg/L1.9 11/5/15SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 11/6/15 8:10 MFFg/L0.94 11/5/15SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 11/6/15 8:10 MFFg/L1.2 11/5/15SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 11/6/15 8:10 MFFg/L2.0 11/5/15SM21-22 6200B10Trichloroethylene
ND 5.0 11/6/15 8:10 MFFg/L1.5 11/5/15SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 11/6/15 8:10 MFFg/L1.9 11/5/15SM21-22 6200B101,2,3-Trichloropropane
1500 5.0 11/6/15 8:10 MFFg/L1.8 11/5/15SM21-22 6200B101,2,4-Trimethylbenzene
510 5.0 11/6/15 8:10 MFFg/L1.0 11/5/15SM21-22 6200B101,3,5-Trimethylbenzene
ND 50 11/6/15 8:10 MFFg/L14 11/5/15SM21-22 6200B10Vinyl Acetate
ND 5.0 11/6/15 8:10 MFFg/L1.3 11/5/15SM21-22 6200B10Vinyl Chloride
4400 10 11/6/15 8:10 MFFg/L2.5 11/5/15SM21-22 6200B10Em+p Xylene
6900 500 11/7/15 8:49 WSDg/L120 11/5/15SM21-22 6200B500m+p Xylene
3300 250 11/7/15 8:49 WSDg/L65 11/5/15SM21-22 6200B500o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.0 11/7/15 8:4970-130
1,2-Dichloroethane-d4 90.5 11/6/15 8:1070-130
Toluene-d8 101 11/6/15 8:1070-130
Toluene-d8 102 11/7/15 8:4970-130
4-Bromofluorobenzene 98.1 11/7/15 8:4970-130
4-Bromofluorobenzene 94.2 11/6/15 8:1070-130
Page 13 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-03
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 10/26/2015 13:20
[TOC_2]15J1337-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 4:45 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
ND 0.50 11/6/15 4:45 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 4:45 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 4:45 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 4:45 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 4:45 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 4:45 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 4:45 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 4:45 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 4:45 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 4:45 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 4:45 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 4:45 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 4:45 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 4:45 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 4:45 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 4:45 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 4:45 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 4:45 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/6/15 4:45 MFFg/L0.089 11/5/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/6/15 4:45 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 4:45 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 4:45 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 4:45 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 4:45 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/6/15 4:45 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 4:45 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 4:45 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 4:45 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 4:45 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 4:45 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 4:45 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 4:45 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/6/15 4:45 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 4:45 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/6/15 4:45 MFFg/L0.12 11/5/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/6/15 4:45 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/6/15 4:45 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 4:45 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 4:45 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 14 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-03
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 10/26/2015 13:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/6/15 4:45 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
ND 0.50 11/6/15 4:45 MFFg/L0.11 11/5/15SM21-22 6200B1n-Propylbenzene
ND 0.50 11/6/15 4:45 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 4:45 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/6/15 4:45 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 4:45 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 4:45 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 4:45 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 4:45 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 4:45 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 4:45 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 4:45 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/6/15 4:45 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 4:45 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 4:45 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
ND 1.0 11/6/15 4:45 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
ND 0.50 11/6/15 4:45 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.8 11/6/15 4:4570-130
Toluene-d8 100 11/6/15 4:4570-130
4-Bromofluorobenzene 97.6 11/6/15 4:4570-130
Page 15 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-04
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 10/26/2015 13:45
[TOC_2]15J1337-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 5:14 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
ND 0.50 11/6/15 5:14 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 5:14 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 5:14 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 5:14 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 5:14 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 5:14 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 5:14 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 5:14 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 5:14 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 5:14 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 5:14 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 5:14 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 5:14 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 5:14 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 5:14 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 5:14 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 5:14 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 5:14 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/6/15 5:14 MFFg/L0.089 11/5/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/6/15 5:14 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 5:14 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 5:14 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 5:14 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 5:14 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/6/15 5:14 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 5:14 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 5:14 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 5:14 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 5:14 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 5:14 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 5:14 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 5:14 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/6/15 5:14 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 5:14 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/6/15 5:14 MFFg/L0.12 11/5/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/6/15 5:14 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/6/15 5:14 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 5:14 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 5:14 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 16 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-04
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 10/26/2015 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/6/15 5:14 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
ND 0.50 11/6/15 5:14 MFFg/L0.11 11/5/15SM21-22 6200B1n-Propylbenzene
ND 0.50 11/6/15 5:14 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 5:14 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/6/15 5:14 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 5:14 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 5:14 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 5:14 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 5:14 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 5:14 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 5:14 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 5:14 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/6/15 5:14 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 5:14 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 5:14 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
ND 1.0 11/6/15 5:14 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
ND 0.50 11/6/15 5:14 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.6 11/6/15 5:1470-130
Toluene-d8 102 11/6/15 5:1470-130
4-Bromofluorobenzene 98.7 11/6/15 5:1470-130
Page 17 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-05
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 10/26/2015 14:10
[TOC_2]15J1337-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/7/15 8:19 WSDg/L4.9 11/6/15SM21-22 6200B1Acetone
15 0.50 11/7/15 8:19 WSDg/L0.079 11/6/15SM21-22 6200B1Benzene
ND 0.50 11/7/15 8:19 WSDg/L0.15 11/6/15SM21-22 6200B1Bromobenzene
ND 0.50 11/7/15 8:19 WSDg/L0.22 11/6/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/7/15 8:19 WSDg/L0.088 11/6/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/7/15 8:19 WSDg/L0.21 11/6/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/7/15 8:19 WSDg/L0.94 11/6/15SM21-22 6200B1Bromomethane
ND 5.0 11/7/15 8:19 WSDg/L2.4 11/6/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/7/15 8:19 WSDg/L0.10 11/6/15SM21-22 6200B1n-Butylbenzene
0.19 0.50 11/7/15 8:19 WSDg/L0.11 11/6/15SM21-22 6200B1Jsec-Butylbenzene
ND 0.50 11/7/15 8:19 WSDg/L0.11 11/6/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/7/15 8:19 WSDg/L0.12 11/6/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/7/15 8:19 WSDg/L0.16 11/6/15SM21-22 6200B1Chlorobenzene
ND 50 11/7/15 8:19 WSDg/L28 11/6/15SM21-22 6200B1Ethanol
ND 0.50 11/7/15 8:19 WSDg/L0.10 11/6/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/7/15 8:19 WSDg/L0.28 11/6/15SM21-22 6200B1Chloroethane
ND 0.50 11/7/15 8:19 WSDg/L0.22 11/6/15SM21-22 6200B1Chloroform
ND 0.50 11/7/15 8:19 WSDg/L0.32 11/6/15SM21-22 6200B1Chloromethane
ND 0.50 11/7/15 8:19 WSDg/L0.12 11/6/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/7/15 8:19 WSDg/L0.089 11/6/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/7/15 8:19 WSDg/L0.10 11/6/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/7/15 8:19 WSDg/L0.17 11/6/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/7/15 8:19 WSDg/L0.15 11/6/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/7/15 8:19 WSDg/L0.18 11/6/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/7/15 8:19 WSDg/L0.16 11/6/15SM21-22 6200B11,1-Dichloroethane
0.39 0.50 11/7/15 8:19 WSDg/L0.19 11/6/15SM21-22 6200B1J1,2-Dichloroethane
ND 0.50 11/7/15 8:19 WSDg/L0.21 11/6/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/7/15 8:19 WSDg/L0.15 11/6/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/7/15 8:19 WSDg/L0.15 11/6/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/7/15 8:19 WSDg/L0.11 11/6/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/7/15 8:19 WSDg/L0.16 11/6/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/7/15 8:19 WSDg/L0.062 11/6/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/7/15 8:19 WSDg/L0.11 11/6/15SM21-22 6200B1L-04trans-1,3-Dichloropropene
13 0.50 11/7/15 8:19 WSDg/L0.18 11/6/15SM21-22 6200B1Diisopropyl Ether (DIPE)
71 0.50 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/7/15 8:19 WSDg/L1.5 11/6/15SM21-22 6200B12-Hexanone (MBK)
2.2 0.50 11/7/15 8:19 WSDg/L0.12 11/6/15SM21-22 6200B1Isopropylbenzene (Cumene)
0.40 0.50 11/7/15 8:19 WSDg/L0.12 11/6/15SM21-22 6200B1Jp-Isopropyltoluene (p-Cymene)
0.15 0.50 11/7/15 8:19 WSDg/L0.090 11/6/15SM21-22 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 11/7/15 8:19 WSDg/L3.2 11/6/15SM21-22 6200B1Methylene Chloride
ND 5.0 11/7/15 8:19 WSDg/L1.5 11/6/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 18 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-05
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 10/26/2015 14:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
15 0.50 11/7/15 8:19 WSDg/L0.12 11/6/15SM21-22 6200B1Naphthalene
4.5 0.50 11/7/15 8:19 WSDg/L0.11 11/6/15SM21-22 6200B1n-Propylbenzene
2.3 0.50 11/7/15 8:19 WSDg/L0.15 11/6/15SM21-22 6200B1Styrene
ND 2.0 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/7/15 8:19 WSDg/L0.17 11/6/15SM21-22 6200B1Tetrachloroethylene
13 0.50 11/7/15 8:19 WSDg/L0.10 11/6/15SM21-22 6200B1Toluene
ND 0.50 11/7/15 8:19 WSDg/L0.14 11/6/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/7/15 8:19 WSDg/L0.19 11/6/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/7/15 8:19 WSDg/L0.094 11/6/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/7/15 8:19 WSDg/L0.12 11/6/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/7/15 8:19 WSDg/L0.20 11/6/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/7/15 8:19 WSDg/L0.15 11/6/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/7/15 8:19 WSDg/L0.19 11/6/15SM21-22 6200B11,2,3-Trichloropropane
23 0.50 11/7/15 8:19 WSDg/L0.18 11/6/15SM21-22 6200B11,2,4-Trimethylbenzene
11 0.50 11/7/15 8:19 WSDg/L0.10 11/6/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/7/15 8:19 WSDg/L1.4 11/6/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B1Vinyl Chloride
67 1.0 11/7/15 8:19 WSDg/L0.25 11/6/15SM21-22 6200B1m+p Xylene
80 0.50 11/7/15 8:19 WSDg/L0.13 11/6/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.1 11/7/15 8:1970-130
Toluene-d8 101 11/7/15 8:1970-130
4-Bromofluorobenzene 99.5 11/7/15 8:1970-130
Page 19 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-06
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 10/26/2015 14:45
[TOC_2]15J1337-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 11/6/15 9:09 MFFg/L49 11/5/15SM21-22 6200B10Acetone
650 5.0 11/6/15 9:09 MFFg/L0.79 11/5/15SM21-22 6200B10Benzene
ND 5.0 11/6/15 9:09 MFFg/L1.5 11/5/15SM21-22 6200B10Bromobenzene
ND 5.0 11/6/15 9:09 MFFg/L2.2 11/5/15SM21-22 6200B10Bromochloromethane
ND 5.0 11/6/15 9:09 MFFg/L0.88 11/5/15SM21-22 6200B10Bromodichloromethane
ND 10 11/6/15 9:09 MFFg/L2.1 11/5/15SM21-22 6200B10L-04Bromoform
ND 10 11/6/15 9:09 MFFg/L9.4 11/5/15SM21-22 6200B10R-05Bromomethane
ND 50 11/6/15 9:09 MFFg/L24 11/5/15SM21-22 6200B102-Butanone (MEK)
2.9 5.0 11/6/15 9:09 MFFg/L1.0 11/5/15SM21-22 6200B10Jn-Butylbenzene
ND 5.0 11/6/15 9:09 MFFg/L1.1 11/5/15SM21-22 6200B10sec-Butylbenzene
ND 5.0 11/6/15 9:09 MFFg/L1.1 11/5/15SM21-22 6200B10tert-Butylbenzene
ND 5.0 11/6/15 9:09 MFFg/L1.2 11/5/15SM21-22 6200B10L-04Carbon Tetrachloride
ND 5.0 11/6/15 9:09 MFFg/L1.6 11/5/15SM21-22 6200B10Chlorobenzene
ND 500 11/6/15 9:09 MFFg/L280 11/5/15SM21-22 6200B10Ethanol
ND 5.0 11/6/15 9:09 MFFg/L1.0 11/5/15SM21-22 6200B10L-04Chlorodibromomethane
ND 5.0 11/6/15 9:09 MFFg/L2.8 11/5/15SM21-22 6200B10Chloroethane
ND 5.0 11/6/15 9:09 MFFg/L2.2 11/5/15SM21-22 6200B10Chloroform
ND 5.0 11/6/15 9:09 MFFg/L3.2 11/5/15SM21-22 6200B10Chloromethane
ND 5.0 11/6/15 9:09 MFFg/L1.2 11/5/15SM21-22 6200B102-Chlorotoluene
ND 5.0 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B104-Chlorotoluene
ND 5.0 11/6/15 9:09 MFFg/L0.89 11/5/15SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 11/6/15 9:09 MFFg/L1.0 11/5/15SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 11/6/15 9:09 MFFg/L1.7 11/5/15SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 11/6/15 9:09 MFFg/L1.5 11/5/15SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 11/6/15 9:09 MFFg/L1.8 11/5/15SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 11/6/15 9:09 MFFg/L1.6 11/5/15SM21-22 6200B101,1-Dichloroethane
ND 5.0 11/6/15 9:09 MFFg/L1.9 11/5/15SM21-22 6200B101,2-Dichloroethane
ND 5.0 11/6/15 9:09 MFFg/L2.1 11/5/15SM21-22 6200B101,1-Dichloroethylene
ND 5.0 11/6/15 9:09 MFFg/L1.5 11/5/15SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 11/6/15 9:09 MFFg/L1.5 11/5/15SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B101,2-Dichloropropane
ND 5.0 11/6/15 9:09 MFFg/L1.1 11/5/15SM21-22 6200B101,3-Dichloropropane
ND 5.0 11/6/15 9:09 MFFg/L1.6 11/5/15SM21-22 6200B10L-042,2-Dichloropropane
ND 5.0 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B101,1-Dichloropropene
ND 5.0 11/6/15 9:09 MFFg/L0.62 11/5/15SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 11/6/15 9:09 MFFg/L1.1 11/5/15SM21-22 6200B10trans-1,3-Dichloropropene
56 5.0 11/6/15 9:09 MFFg/L1.8 11/5/15SM21-22 6200B10Diisopropyl Ether (DIPE)
130 5.0 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B10Ethylbenzene
ND 50 11/6/15 9:09 MFFg/L15 11/5/15SM21-22 6200B102-Hexanone (MBK)
8.3 5.0 11/6/15 9:09 MFFg/L1.2 11/5/15SM21-22 6200B10Isopropylbenzene (Cumene)
1.4 5.0 11/6/15 9:09 MFFg/L1.2 11/5/15SM21-22 6200B10Jp-Isopropyltoluene (p-Cymene)
2.1 5.0 11/6/15 9:09 MFFg/L0.90 11/5/15SM21-22 6200B10JMethyl tert-Butyl Ether (MTBE)
ND 50 11/6/15 9:09 MFFg/L32 11/5/15SM21-22 6200B10R-05Methylene Chloride
ND 50 11/6/15 9:09 MFFg/L15 11/5/15SM21-22 6200B104-Methyl-2-pentanone (MIBK)
Page 20 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-06
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 10/26/2015 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
53 5.0 11/6/15 9:09 MFFg/L1.2 11/5/15SM21-22 6200B10Naphthalene
11 5.0 11/6/15 9:09 MFFg/L1.1 11/5/15SM21-22 6200B10n-Propylbenzene
ND 5.0 11/6/15 9:09 MFFg/L1.5 11/5/15SM21-22 6200B10Styrene
ND 20 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 11/6/15 9:09 MFFg/L1.7 11/5/15SM21-22 6200B10Tetrachloroethylene
470 5.0 11/6/15 9:09 MFFg/L1.0 11/5/15SM21-22 6200B10Toluene
ND 5.0 11/6/15 9:09 MFFg/L1.4 11/5/15SM21-22 6200B101,2,3-Trichlorobenzene
ND 5.0 11/6/15 9:09 MFFg/L1.9 11/5/15SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 11/6/15 9:09 MFFg/L0.94 11/5/15SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 11/6/15 9:09 MFFg/L1.2 11/5/15SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 11/6/15 9:09 MFFg/L2.0 11/5/15SM21-22 6200B10Trichloroethylene
ND 5.0 11/6/15 9:09 MFFg/L1.5 11/5/15SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 11/6/15 9:09 MFFg/L1.9 11/5/15SM21-22 6200B101,2,3-Trichloropropane
140 5.0 11/6/15 9:09 MFFg/L1.8 11/5/15SM21-22 6200B101,2,4-Trimethylbenzene
46 5.0 11/6/15 9:09 MFFg/L1.0 11/5/15SM21-22 6200B101,3,5-Trimethylbenzene
ND 50 11/6/15 9:09 MFFg/L14 11/5/15SM21-22 6200B10Vinyl Acetate
ND 5.0 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B10Vinyl Chloride
630 10 11/6/15 9:09 MFFg/L2.5 11/5/15SM21-22 6200B10m+p Xylene
270 5.0 11/6/15 9:09 MFFg/L1.3 11/5/15SM21-22 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.6 11/6/15 9:0970-130
Toluene-d8 101 11/6/15 9:0970-130
4-Bromofluorobenzene 98.4 11/6/15 9:0970-130
Page 21 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-07
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 10/26/2015 16:00
[TOC_2]15J1337-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 5:43 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
ND 0.50 11/6/15 5:43 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 5:43 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 5:43 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 5:43 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 5:43 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 5:43 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 5:43 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 5:43 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 5:43 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 5:43 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 5:43 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 5:43 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 5:43 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 5:43 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 5:43 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 5:43 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 5:43 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 5:43 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/6/15 5:43 MFFg/L0.089 11/5/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/6/15 5:43 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 5:43 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 5:43 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 5:43 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 5:43 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/6/15 5:43 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 5:43 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 5:43 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 5:43 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 5:43 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 5:43 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 5:43 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 5:43 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
0.63 0.50 11/6/15 5:43 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 5:43 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/6/15 5:43 MFFg/L0.12 11/5/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/6/15 5:43 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/6/15 5:43 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 5:43 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 5:43 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 22 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-07
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 10/26/2015 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/6/15 5:43 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
ND 0.50 11/6/15 5:43 MFFg/L0.11 11/5/15SM21-22 6200B1n-Propylbenzene
ND 0.50 11/6/15 5:43 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 5:43 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/6/15 5:43 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 5:43 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 5:43 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 5:43 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 5:43 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 5:43 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 5:43 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 5:43 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/6/15 5:43 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 5:43 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 5:43 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
ND 1.0 11/6/15 5:43 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
ND 0.50 11/6/15 5:43 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.6 11/6/15 5:4370-130
Toluene-d8 101 11/6/15 5:4370-130
4-Bromofluorobenzene 98.4 11/6/15 5:4370-130
Page 23 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-08
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 10/26/2015 16:25
[TOC_2]15J1337-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 6:13 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
15 0.50 11/6/15 6:13 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 6:13 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 6:13 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 6:13 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 6:13 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 6:13 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 6:13 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 6:13 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 6:13 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 6:13 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 6:13 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 6:13 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 6:13 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 6:13 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 6:13 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 6:13 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 6:13 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 6:13 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
0.31 0.50 11/6/15 6:13 MFFg/L0.089 11/5/15SM21-22 6200B1J1,2-Dibromoethane (EDB)
ND 0.50 11/6/15 6:13 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 6:13 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 6:13 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 6:13 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 6:13 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
5.0 0.50 11/6/15 6:13 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 6:13 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 6:13 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 6:13 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 6:13 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 6:13 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 6:13 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 6:13 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
23 0.50 11/6/15 6:13 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
1.8 0.50 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 6:13 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
0.22 0.50 11/6/15 6:13 MFFg/L0.12 11/5/15SM21-22 6200B1JIsopropylbenzene (Cumene)
ND 0.50 11/6/15 6:13 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
2.8 0.50 11/6/15 6:13 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 6:13 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 6:13 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-08
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 10/26/2015 16:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.88 0.50 11/6/15 6:13 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
0.21 0.50 11/6/15 6:13 MFFg/L0.11 11/5/15SM21-22 6200B1Jn-Propylbenzene
ND 0.50 11/6/15 6:13 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 6:13 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
1.6 0.50 11/6/15 6:13 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 6:13 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 6:13 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 6:13 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 6:13 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 6:13 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 6:13 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 6:13 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
1.9 0.50 11/6/15 6:13 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 6:13 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 6:13 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
7.3 1.0 11/6/15 6:13 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
3.5 0.50 11/6/15 6:13 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.1 11/6/15 6:1370-130
Toluene-d8 102 11/6/15 6:1370-130
4-Bromofluorobenzene 99.0 11/6/15 6:1370-130
Page 25 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-09
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 10/26/2015 17:00
[TOC_2]15J1337-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 6:42 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
ND 0.50 11/6/15 6:42 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 6:42 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 6:42 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 6:42 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 6:42 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 6:42 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 6:42 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 6:42 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 6:42 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 6:42 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 6:42 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 6:42 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 6:42 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 6:42 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 6:42 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 6:42 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 6:42 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 6:42 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/6/15 6:42 MFFg/L0.089 11/5/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/6/15 6:42 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 6:42 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 6:42 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 6:42 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 6:42 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/6/15 6:42 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 6:42 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 6:42 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 6:42 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 6:42 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 6:42 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 6:42 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 6:42 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/6/15 6:42 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 6:42 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/6/15 6:42 MFFg/L0.12 11/5/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/6/15 6:42 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/6/15 6:42 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 6:42 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 6:42 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 26 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-09
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 10/26/2015 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/6/15 6:42 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
ND 0.50 11/6/15 6:42 MFFg/L0.11 11/5/15SM21-22 6200B1n-Propylbenzene
ND 0.50 11/6/15 6:42 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 6:42 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/6/15 6:42 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 6:42 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 6:42 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 6:42 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 6:42 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 6:42 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 6:42 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 6:42 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/6/15 6:42 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 6:42 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 6:42 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
ND 1.0 11/6/15 6:42 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
ND 0.50 11/6/15 6:42 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.4 11/6/15 6:4270-130
Toluene-d8 101 11/6/15 6:4270-130
4-Bromofluorobenzene 99.2 11/6/15 6:4270-130
Page 27 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-10
Field Sample #: WSW-11
Sample Matrix: Ground Water
Sampled: 10/26/2015 17:25
[TOC_2]15J1337-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/6/15 7:12 MFFg/L4.9 11/5/15SM21-22 6200B1Acetone
ND 0.50 11/6/15 7:12 MFFg/L0.079 11/5/15SM21-22 6200B1Benzene
ND 0.50 11/6/15 7:12 MFFg/L0.15 11/5/15SM21-22 6200B1Bromobenzene
ND 0.50 11/6/15 7:12 MFFg/L0.22 11/5/15SM21-22 6200B1Bromochloromethane
ND 0.50 11/6/15 7:12 MFFg/L0.088 11/5/15SM21-22 6200B1Bromodichloromethane
ND 1.0 11/6/15 7:12 MFFg/L0.21 11/5/15SM21-22 6200B1L-04Bromoform
ND 1.0 11/6/15 7:12 MFFg/L0.94 11/5/15SM21-22 6200B1R-05Bromomethane
ND 5.0 11/6/15 7:12 MFFg/L2.4 11/5/15SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/6/15 7:12 MFFg/L0.10 11/5/15SM21-22 6200B1n-Butylbenzene
ND 0.50 11/6/15 7:12 MFFg/L0.11 11/5/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/6/15 7:12 MFFg/L0.11 11/5/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/6/15 7:12 MFFg/L0.12 11/5/15SM21-22 6200B1L-04Carbon Tetrachloride
ND 0.50 11/6/15 7:12 MFFg/L0.16 11/5/15SM21-22 6200B1Chlorobenzene
ND 50 11/6/15 7:12 MFFg/L28 11/5/15SM21-22 6200B1Ethanol
ND 0.50 11/6/15 7:12 MFFg/L0.10 11/5/15SM21-22 6200B1L-04Chlorodibromomethane
ND 0.50 11/6/15 7:12 MFFg/L0.28 11/5/15SM21-22 6200B1Chloroethane
ND 0.50 11/6/15 7:12 MFFg/L0.22 11/5/15SM21-22 6200B1Chloroform
ND 0.50 11/6/15 7:12 MFFg/L0.32 11/5/15SM21-22 6200B1Chloromethane
ND 0.50 11/6/15 7:12 MFFg/L0.12 11/5/15SM21-22 6200B12-Chlorotoluene
ND 0.50 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B14-Chlorotoluene
ND 0.50 11/6/15 7:12 MFFg/L0.089 11/5/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/6/15 7:12 MFFg/L0.10 11/5/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/6/15 7:12 MFFg/L0.17 11/5/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/6/15 7:12 MFFg/L0.15 11/5/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/6/15 7:12 MFFg/L0.18 11/5/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/6/15 7:12 MFFg/L0.16 11/5/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/6/15 7:12 MFFg/L0.19 11/5/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/6/15 7:12 MFFg/L0.21 11/5/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/6/15 7:12 MFFg/L0.15 11/5/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/6/15 7:12 MFFg/L0.15 11/5/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/6/15 7:12 MFFg/L0.11 11/5/15SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/6/15 7:12 MFFg/L0.16 11/5/15SM21-22 6200B1L-042,2-Dichloropropane
ND 0.50 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/6/15 7:12 MFFg/L0.062 11/5/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/6/15 7:12 MFFg/L0.11 11/5/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/6/15 7:12 MFFg/L0.18 11/5/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B1Ethylbenzene
ND 5.0 11/6/15 7:12 MFFg/L1.5 11/5/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/6/15 7:12 MFFg/L0.12 11/5/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/6/15 7:12 MFFg/L0.12 11/5/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/6/15 7:12 MFFg/L0.090 11/5/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/6/15 7:12 MFFg/L3.2 11/5/15SM21-22 6200B1R-05Methylene Chloride
ND 5.0 11/6/15 7:12 MFFg/L1.5 11/5/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/27/2015
Work Order: 15J1337Sample Description:Project Location: Wise Convenient Mart, NC
Sample ID: 15J1337-10
Field Sample #: WSW-11
Sample Matrix: Ground Water
Sampled: 10/26/2015 17:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/6/15 7:12 MFFg/L0.12 11/5/15SM21-22 6200B1Naphthalene
ND 0.50 11/6/15 7:12 MFFg/L0.11 11/5/15SM21-22 6200B1n-Propylbenzene
ND 0.50 11/6/15 7:12 MFFg/L0.15 11/5/15SM21-22 6200B1Styrene
ND 2.0 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/6/15 7:12 MFFg/L0.17 11/5/15SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/6/15 7:12 MFFg/L0.10 11/5/15SM21-22 6200B1Toluene
ND 0.50 11/6/15 7:12 MFFg/L0.14 11/5/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/6/15 7:12 MFFg/L0.19 11/5/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/6/15 7:12 MFFg/L0.094 11/5/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/6/15 7:12 MFFg/L0.12 11/5/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/6/15 7:12 MFFg/L0.20 11/5/15SM21-22 6200B1Trichloroethylene
ND 0.50 11/6/15 7:12 MFFg/L0.15 11/5/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/6/15 7:12 MFFg/L0.19 11/5/15SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/6/15 7:12 MFFg/L0.18 11/5/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/6/15 7:12 MFFg/L0.10 11/5/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 11/6/15 7:12 MFFg/L1.4 11/5/15SM21-22 6200B1Vinyl Acetate
ND 0.50 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B1Vinyl Chloride
ND 1.0 11/6/15 7:12 MFFg/L0.25 11/5/15SM21-22 6200B1m+p Xylene
ND 0.50 11/6/15 7:12 MFFg/L0.13 11/5/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.1 11/6/15 7:1270-130
Toluene-d8 100 11/6/15 7:1270-130
4-Bromofluorobenzene 97.9 11/6/15 7:1270-130
Page 29 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B134679 11/05/155 5.0015J1337-01 [DW-1]
B134679 11/05/150.5 5.0015J1337-02 [MW-1]
B134679 11/05/155 5.0015J1337-03 [MW-4]
B134679 11/05/155 5.0015J1337-04 [MW-3]
B134679 11/05/150.5 5.0015J1337-06 [MW-5]
B134679 11/05/155 5.0015J1337-07 [MW-7]
B134679 11/05/155 5.0015J1337-08 [MW-6]
B134679 11/05/155 5.0015J1337-09 [WSW-1]
B134679 11/05/155 5.0015J1337-10 [WSW-11]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B134803 11/05/150.01 5.0015J1337-02RE1 [MW-1]
B134803 11/06/155 5.0015J1337-05 [MW-2]
[TOC_1]Sample Preparation Information[TOC]
Page 30 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B134679 - SW-846 5030B
[TOC_3]B134679[TOC]
Blank (B134679-BLK1) Prepared: 11/05/15 Analyzed: 11/06/15
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50 L-04ND
Bromomethane g/L1.0 R-05ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50 L-04ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50 L-04ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.50ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50 L-04ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0 R-05ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 31 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134679 - SW-846 5030B
Blank (B134679-BLK1) Prepared: 11/05/15 Analyzed: 11/06/15
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.022.3
g/L 25.0 70-130Surrogate: Toluene-d8 10225.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.424.9
LCS (B134679-BS1) Prepared: 11/05/15 Analyzed: 11/06/15
Acetone g/L50 100 70-13070.470.4
Benzene g/L0.50 10.0 70-13097.09.70
Bromobenzene g/L0.50 10.0 70-13010210.2
Bromochloromethane g/L0.50 10.0 70-13091.89.18
Bromodichloromethane g/L0.50 10.0 70-13085.48.54
Bromoform g/L0.50 10.0 L-0470-13059.6 *5.96
Bromomethane g/L1.0 10.0 R-0560-14010610.6
2-Butanone (MEK)g/L5.0 100 70-13080.280.2
n-Butylbenzene g/L0.50 10.0 70-13099.59.95
sec-Butylbenzene g/L0.50 10.0 70-13010310.3
tert-Butylbenzene g/L0.50 10.0 70-13010310.3
Carbon Tetrachloride g/L0.50 10.0 L-0470-13062.0 *6.20
Chlorobenzene g/L0.50 10.0 70-13010810.8
Ethanol g/L50 100 70-13082.682.6
Chlorodibromomethane g/L0.50 10.0 L-0470-13065.7 *6.57
Chloroethane g/L0.50 10.0 60-14095.09.50
Chloroform g/L0.50 10.0 70-13097.89.78
Chloromethane g/L0.50 10.0 60-14083.28.32
2-Chlorotoluene g/L0.50 10.0 70-13010510.5
4-Chlorotoluene g/L0.50 10.0 70-13010810.8
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13094.49.44
1,2-Dichlorobenzene g/L0.50 10.0 70-13010210.2
1,3-Dichlorobenzene g/L0.50 10.0 70-13010110.1
1,4-Dichlorobenzene g/L0.50 10.0 70-13010210.2
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14072.37.23
1,1-Dichloroethane g/L0.50 10.0 70-13091.79.17
1,2-Dichloroethane g/L0.50 10.0 70-13096.39.63
1,1-Dichloroethylene g/L0.50 10.0 70-13093.79.37
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13091.29.12
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13094.79.47
1,2-Dichloropropane g/L0.50 10.0 70-13097.39.73
1,3-Dichloropropane g/L0.50 10.0 70-13099.69.96
2,2-Dichloropropane g/L0.50 10.0 L-0470-13060.1 *6.01
1,1-Dichloropropene g/L0.50 10.0 70-13097.19.71
cis-1,3-Dichloropropene g/L0.50 10.0 70-13078.37.83
trans-1,3-Dichloropropene g/L0.50 10.0 70-13072.77.27
Page 32 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134679 - SW-846 5030B
LCS (B134679-BS1) Prepared: 11/05/15 Analyzed: 11/06/15
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13091.89.18
Ethylbenzene g/L0.50 10.0 70-13010710.7
2-Hexanone (MBK)g/L5.0 100 70-13092.592.5
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011011.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010310.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13087.88.78
Methylene Chloride g/L5.0 10.0 R-0570-13090.79.07
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13096.696.6
Naphthalene g/L0.50 10.0 70-13097.89.78
n-Propylbenzene g/L0.50 10.0 70-13010710.7
Styrene g/L0.50 10.0 70-13010710.7
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010110.1
Tetrachloroethylene g/L0.50 10.0 70-13010810.8
Toluene g/L0.50 10.0 70-13011011.0
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13098.59.85
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13098.19.81
1,1,1-Trichloroethane g/L0.50 10.0 70-13080.58.05
1,1,2-Trichloroethane g/L0.50 10.0 70-13098.29.82
Trichloroethylene g/L0.50 10.0 70-13091.19.11
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13091.99.19
1,2,3-Trichloropropane g/L0.50 10.0 70-13097.19.71
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010210.2
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010810.8
Vinyl Acetate g/L5.0 100 L-0270-130190*190
Vinyl Chloride g/L0.50 10.0 60-14087.78.77
m+p Xylene g/L1.0 20.0 70-13011022.0
o-Xylene g/L0.50 10.0 70-13010910.9
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.622.2
g/L 25.0 70-130Surrogate: Toluene-d8 10325.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.124.8
LCS Dup (B134679-BSD1) Prepared: 11/05/15 Analyzed: 11/06/15
Acetone g/L50 100 25 L-0770-13064.9 8.11*64.9
Benzene g/L0.50 10.0 2570-13093.3 3.899.33
Bromobenzene g/L0.50 10.0 2570-13097.5 4.619.75
Bromochloromethane g/L0.50 10.0 2570-13090.0 1.989.00
Bromodichloromethane g/L0.50 10.0 2570-13087.2 2.098.72
Bromoform g/L0.50 10.0 25 L-0470-13060.9 2.16*6.09
Bromomethane g/L1.0 10.0 25 R-0560-14061.4 53.2 *6.14
2-Butanone (MEK)g/L5.0 100 2570-13080.1 0.099880.1
n-Butylbenzene g/L0.50 10.0 2570-13092.9 6.869.29
sec-Butylbenzene g/L0.50 10.0 2570-13095.4 7.379.54
tert-Butylbenzene g/L0.50 10.0 2570-13095.3 7.969.53
Carbon Tetrachloride g/L0.50 10.0 25 L-0470-13060.0 3.28*6.00
Chlorobenzene g/L0.50 10.0 2570-130101 6.0410.1
Ethanol g/L50 100 2570-13082.0 0.64482.0
Chlorodibromomethane g/L0.50 10.0 25 L-0470-13069.1 5.04*6.91
Chloroethane g/L0.50 10.0 2560-14088.6 6.978.86
Chloroform g/L0.50 10.0 2570-13093.7 4.289.37
Chloromethane g/L0.50 10.0 2560-14078.2 6.207.82
2-Chlorotoluene g/L0.50 10.0 2570-13097.3 7.999.73
4-Chlorotoluene g/L0.50 10.0 2570-130102 6.1110.2
Page 33 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134679 - SW-846 5030B
LCS Dup (B134679-BSD1) Prepared: 11/05/15 Analyzed: 11/06/15
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13093.0 1.499.30
1,2-Dichlorobenzene g/L0.50 10.0 2570-13097.3 4.329.73
1,3-Dichlorobenzene g/L0.50 10.0 2570-13094.3 7.069.43
1,4-Dichlorobenzene g/L0.50 10.0 2570-13096.7 4.949.67
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14063.9 12.36.39
1,1-Dichloroethane g/L0.50 10.0 2570-13088.1 4.008.81
1,2-Dichloroethane g/L0.50 10.0 2570-13096.5 0.2079.65
1,1-Dichloroethylene g/L0.50 10.0 2570-13082.2 13.18.22
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13087.2 4.488.72
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13088.8 6.438.88
1,2-Dichloropropane g/L0.50 10.0 2570-13094.9 2.509.49
1,3-Dichloropropane g/L0.50 10.0 2570-13095.8 3.899.58
2,2-Dichloropropane g/L0.50 10.0 25 L-0470-13055.8 7.42*5.58
1,1-Dichloropropene g/L0.50 10.0 2570-13091.3 6.169.13
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13077.8 0.6417.78
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13071.9 1.117.19
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13091.1 0.7659.11
Ethylbenzene g/L0.50 10.0 2570-13099.0 7.779.90
2-Hexanone (MBK)g/L5.0 100 2570-13090.3 2.4290.3
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13099.5 9.759.95
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13094.6 8.419.46
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13087.8 0.008.78
Methylene Chloride g/L5.0 10.0 25 R-0570-130119 27.3 *11.9
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13095.5 1.1595.5
Naphthalene g/L0.50 10.0 2570-13094.0 3.969.40
n-Propylbenzene g/L0.50 10.0 2570-13098.6 7.809.86
Styrene g/L0.50 10.0 2570-130102 4.8910.2
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130100 0.59610.0
Tetrachloroethylene g/L0.50 10.0 2570-130101 6.9810.1
Toluene g/L0.50 10.0 2570-130104 5.7010.4
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13097.2 1.339.72
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13094.2 4.069.42
1,1,1-Trichloroethane g/L0.50 10.0 2570-13077.3 4.067.73
1,1,2-Trichloroethane g/L0.50 10.0 2570-13097.6 0.6139.76
Trichloroethylene g/L0.50 10.0 2570-13083.8 8.358.38
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13080.7 13.08.07
1,2,3-Trichloropropane g/L0.50 10.0 2570-13091.7 5.729.17
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13095.5 6.399.55
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130100 7.1010.0
Vinyl Acetate g/L5.0 100 25 L-0270-130201 5.47*201
Vinyl Chloride g/L0.50 10.0 2560-14081.0 7.948.10
m+p Xylene g/L1.0 20.0 2570-130100 9.1520.0
o-Xylene g/L0.50 10.0 2570-130101 7.9210.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.422.4
g/L 25.0 70-130Surrogate: Toluene-d8 10325.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.724.7
Page 34 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134803 - SW-846 5030B
[TOC_3]B134803[TOC]
Blank (B134803-BLK1) Prepared: 11/06/15 Analyzed: 11/07/15
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50 L-04ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50 L-04ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50 L-04ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.50ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50 L-04ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50 L-04ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 35 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134803 - SW-846 5030B
Blank (B134803-BLK1) Prepared: 11/06/15 Analyzed: 11/07/15
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.422.3
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.424.1
LCS (B134803-BS1) Prepared: 11/06/15 Analyzed: 11/07/15
Acetone g/L50 100 70-13072.172.1
Benzene g/L0.50 10.0 70-13090.29.02
Bromobenzene g/L0.50 10.0 70-13092.99.29
Bromochloromethane g/L0.50 10.0 70-13088.28.82
Bromodichloromethane g/L0.50 10.0 70-13084.58.45
Bromoform g/L0.50 10.0 L-0470-13058.7 *5.87
Bromomethane g/L1.0 10.0 60-14010010.0
2-Butanone (MEK)g/L5.0 100 70-13080.580.5
n-Butylbenzene g/L0.50 10.0 70-13088.98.89
sec-Butylbenzene g/L0.50 10.0 70-13093.89.38
tert-Butylbenzene g/L0.50 10.0 70-13095.29.52
Carbon Tetrachloride g/L0.50 10.0 L-0470-13058.0 *5.80
Chlorobenzene g/L0.50 10.0 70-13010110.1
Ethanol g/L50 100 70-13079.179.1
Chlorodibromomethane g/L0.50 10.0 L-0470-13064.6 *6.46
Chloroethane g/L0.50 10.0 60-14086.18.61
Chloroform g/L0.50 10.0 70-13091.19.11
Chloromethane g/L0.50 10.0 60-14085.98.59
2-Chlorotoluene g/L0.50 10.0 70-13097.39.73
4-Chlorotoluene g/L0.50 10.0 70-13098.89.88
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13090.99.09
1,2-Dichlorobenzene g/L0.50 10.0 70-13095.29.52
1,3-Dichlorobenzene g/L0.50 10.0 70-13093.39.33
1,4-Dichlorobenzene g/L0.50 10.0 70-13092.79.27
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14076.07.60
1,1-Dichloroethane g/L0.50 10.0 70-13083.88.38
1,2-Dichloroethane g/L0.50 10.0 70-13093.99.39
1,1-Dichloroethylene g/L0.50 10.0 70-13081.78.17
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13083.58.35
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13086.28.62
1,2-Dichloropropane g/L0.50 10.0 70-13090.79.07
1,3-Dichloropropane g/L0.50 10.0 70-13095.39.53
2,2-Dichloropropane g/L0.50 10.0 L-0470-13043.9 *4.39
1,1-Dichloropropene g/L0.50 10.0 70-13088.38.83
cis-1,3-Dichloropropene g/L0.50 10.0 70-13072.37.23
trans-1,3-Dichloropropene g/L0.50 10.0 L-0470-13064.7 *6.47
Page 36 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134803 - SW-846 5030B
LCS (B134803-BS1) Prepared: 11/06/15 Analyzed: 11/07/15
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13085.68.56
Ethylbenzene g/L0.50 10.0 70-13097.79.77
2-Hexanone (MBK)g/L5.0 100 70-13088.688.6
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13096.29.62
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13092.09.20
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13085.68.56
Methylene Chloride g/L5.0 10.0 70-13011711.7
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13093.793.7
Naphthalene g/L0.50 10.0 70-13092.99.29
n-Propylbenzene g/L0.50 10.0 70-13094.19.41
Styrene g/L0.50 10.0 70-13098.39.83
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13082.48.24
Tetrachloroethylene g/L0.50 10.0 70-13094.29.42
Toluene g/L0.50 10.0 70-13099.89.98
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13094.79.47
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13091.79.17
1,1,1-Trichloroethane g/L0.50 10.0 70-13073.17.31
1,1,2-Trichloroethane g/L0.50 10.0 70-13093.59.35
Trichloroethylene g/L0.50 10.0 70-13093.19.31
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13083.18.31
1,2,3-Trichloropropane g/L0.50 10.0 70-13091.79.17
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13093.59.35
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13098.09.80
Vinyl Acetate g/L5.0 100 70-130104104
Vinyl Chloride g/L0.50 10.0 60-14085.38.53
m+p Xylene g/L1.0 20.0 70-13099.019.8
o-Xylene g/L0.50 10.0 70-13097.99.79
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.622.4
g/L 25.0 70-130Surrogate: Toluene-d8 10225.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.424.6
LCS Dup (B134803-BSD1) Prepared: 11/06/15 Analyzed: 11/07/15
Acetone g/L50 100 2570-13076.2 5.5476.2
Benzene g/L0.50 10.0 2570-13090.4 0.2219.04
Bromobenzene g/L0.50 10.0 2570-13093.8 0.9649.38
Bromochloromethane g/L0.50 10.0 2570-13089.8 1.808.98
Bromodichloromethane g/L0.50 10.0 2570-13083.3 1.438.33
Bromoform g/L0.50 10.0 25 L-0470-13063.3 7.54*6.33
Bromomethane g/L1.0 10.0 2560-14085.2 16.08.52
2-Butanone (MEK)g/L5.0 100 2570-13083.2 3.3383.2
n-Butylbenzene g/L0.50 10.0 2570-13089.9 1.128.99
sec-Butylbenzene g/L0.50 10.0 2570-13094.9 1.179.49
tert-Butylbenzene g/L0.50 10.0 2570-13095.5 0.3159.55
Carbon Tetrachloride g/L0.50 10.0 25 L-0470-13060.6 4.38*6.06
Chlorobenzene g/L0.50 10.0 2570-13099.2 1.409.92
Ethanol g/L50 100 2570-13075.6 4.5075.6
Chlorodibromomethane g/L0.50 10.0 25 L-0470-13066.6 3.05*6.66
Chloroethane g/L0.50 10.0 2560-14087.0 1.048.70
Chloroform g/L0.50 10.0 2570-13093.0 2.069.30
Chloromethane g/L0.50 10.0 2560-14083.1 3.318.31
2-Chlorotoluene g/L0.50 10.0 2570-13095.7 1.669.57
4-Chlorotoluene g/L0.50 10.0 2570-13099.4 0.6059.94
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B134803 - SW-846 5030B
LCS Dup (B134803-BSD1) Prepared: 11/06/15 Analyzed: 11/07/15
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13090.9 0.009.09
1,2-Dichlorobenzene g/L0.50 10.0 2570-13096.0 0.8379.60
1,3-Dichlorobenzene g/L0.50 10.0 2570-13094.0 0.7479.40
1,4-Dichlorobenzene g/L0.50 10.0 2570-13094.5 1.929.45
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14077.9 2.477.79
1,1-Dichloroethane g/L0.50 10.0 2570-13085.5 2.018.55
1,2-Dichloroethane g/L0.50 10.0 2570-13094.0 0.1069.40
1,1-Dichloroethylene g/L0.50 10.0 2570-13084.2 3.018.42
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13084.7 1.438.47
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13087.9 1.958.79
1,2-Dichloropropane g/L0.50 10.0 2570-13090.8 0.1109.08
1,3-Dichloropropane g/L0.50 10.0 2570-13095.8 0.5239.58
2,2-Dichloropropane g/L0.50 10.0 25 L-0470-13044.5 1.36*4.45
1,1-Dichloropropene g/L0.50 10.0 2570-13089.3 1.138.93
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13071.7 0.8337.17
trans-1,3-Dichloropropene g/L0.50 10.0 25 L-0470-13065.2 0.770*6.52
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13086.5 1.058.65
Ethylbenzene g/L0.50 10.0 2570-13099.3 1.629.93
2-Hexanone (MBK)g/L5.0 100 2570-13090.5 2.1190.5
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13097.5 1.349.75
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13093.0 1.089.30
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13085.0 0.7038.50
Methylene Chloride g/L5.0 10.0 2570-130115 1.2911.5
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13094.1 0.50194.1
Naphthalene g/L0.50 10.0 2570-13094.3 1.509.43
n-Propylbenzene g/L0.50 10.0 2570-13094.4 0.3189.44
Styrene g/L0.50 10.0 2570-13098.7 0.4069.87
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13080.8 1.968.08
Tetrachloroethylene g/L0.50 10.0 2570-13095.2 1.069.52
Toluene g/L0.50 10.0 2570-130100 0.50010.0
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13095.8 1.159.58
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13091.2 0.5479.12
1,1,1-Trichloroethane g/L0.50 10.0 2570-13075.9 3.767.59
1,1,2-Trichloroethane g/L0.50 10.0 2570-13094.0 0.5339.40
Trichloroethylene g/L0.50 10.0 2570-13095.3 2.349.53
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13086.4 3.898.64
1,2,3-Trichloropropane g/L0.50 10.0 2570-13095.7 4.279.57
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13093.6 0.1079.36
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13098.6 0.6109.86
Vinyl Acetate g/L5.0 100 2570-130104 0.741104
Vinyl Chloride g/L0.50 10.0 2560-14088.4 3.578.84
m+p Xylene g/L1.0 20.0 2570-13099.0 0.050519.8
o-Xylene g/L0.50 10.0 2570-13098.7 0.8149.87
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.522.6
g/L 25.0 70-130Surrogate: Toluene-d8 10325.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.224.6
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Reported result is estimated. Value reported over verified calibration range.E
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2016
M-MA100Massachusetts DEPMA 06/30/2016
PH-0567Connecticut Department of Publilc HealthCT 09/30/2017
10899 NELAPNew York State Department of HealthNY 04/1/2016
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2016
LAO00112Rhode Island Department of HealthRI 12/30/2015
652North Carolina Div. of Water QualityNC 12/31/2015
MA007 NELAPNew Jersey DEPNJ 06/30/2016
E871027 NELAPFlorida Department of HealthFL 06/30/2016
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2016
C2065State of Washington Department of EcologyWA 02/23/2016
2011028State of MaineME 06/9/2017
460217Commonwealth of VirginiaVA 12/14/2015
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2016
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