MO-7545_36185_CA_MRP_20231013

Monitoring Report

Dot’s Place Too
1484 Mecklenburg Highway
Mount Mourne, Iredell County, North Carolina 28115
NCDEQ Incident No. 36185
ATC Project No: STL3618501

Submittal Date:

October 13, 2023

Prepared By:

ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, North Carolina 28273
p: [phone] / f: [phone]

www.atcgroupservices.com
7606 Whitehall Executive Center Drive
Suite 800
Charlotte, NC 28273
Tel: [phone]
www.atcassociates.com
Fax: [phone]
N.C. Engineering License No. C-1598

October 13, 2023

Mr. Scott Ryals, P.E.
North Carolina Department of Environmental Quality
Division of Waste Management - Underground Storage Tank Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Re: Monitoring Report
Dot’s Place Too
1484 Mecklenburg Highway
Mount Mourne, Iredell County, North Carolina 28115
NCDEQ Incident # 36185
ATC Project # STL3618501
Task Authorization: TA-01

Dear Mr. Ryals:

ATC Associates of North Carolina, P.C. is submitting the enclosed Monitoring Report for Dot’s
Place Too. The report presents a summary of field activities and laboratory analytical results for
work conducted in July and August 2023. Field activities included collection of groundwater
samples from monitoring wells and supply wells for laboratory analysis. If you have any questions
or require additional information, please contact our office at [phone].

Sincerely,

ATC Associates of North Carolina, P.C.

Noelle France, P.G. Al Quarles, P.G.
Senior Project Manager Senior Project Manager

Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION ............................................................................... 1 
2.0 EXECUTIVE SUMMARY ............................................................................. 2 
3.0 SITE DESCRIPTION ................................................................................... 3 
3.1 Site Characterization .................................................................... 3 
3.2 Site Background ........................................................................... 3 
3.3 Site and Regional Geology .......................................................... 5 
3.4 Site and Regional Hydrogeology .................................................. 6 
4.0 GROUNDWATER CHARACTERIZATION .................................................. 6 
4.1 Water Supply Wells ...................................................................... 6 
4.2 Groundwater Levels ..................................................................... 7 
4.3 Groundwater Quality .................................................................... 7 
5.0 CONCLUSIONS AND RECOMMENDATIONS ........................................... 9 
TABLES
Table 1 Water Supply Well Information
Table 2 Monitoring Well Construction
Table 3 Groundwater Elevation Data
Table 4 Field Parameters
Table 5 Recent Groundwater Analytical Data
Table 6 Historical Water Supply Well Analytical Data
Table 7 Historical Monitoring Well Analytical Data
FIGURES
Figure 1 Site Location Map
Figure 2 Site Vicinity Map with Water Supply Well Locations
Figure 3 Site Map
Figure 4 Groundwater Elevation Map
Figure 5 Benzene Isoconcentration Contour Map
Figure 6 EDB Isoconcentration Contour Map
Figure 7 Contaminants of Concern Map
APPENDICES
Appendix A Conceptual Site Model
Appendix B Field Notes & Photographs
Appendix C Laboratory Analytical Reports
Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501
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1.0 SITE IDENTIFICATION
1. Site Identification
Date of Report: October 13, 2023
Facility I.D.: Not Listed UST Incident Number (if known): 36185
Site Risk: High Site Rank: 0330D Land Use Category: Commercial
Site Name: Dot’s Place Too
Site Street Address: 1484 Mecklenburg Highway
City/Town: Mount Mourne Zip Code: 28115 County: Iredell County
Description of Geographical Data Point: Store___
Location Method: __Google Earth______________________________
Latitude (decimal degrees): 35.54393 Longitude (decimal degrees): -80.84722

2. Information about Contacts Associated with the Leaking UST System
UST Owner: Bill Bolmer
Address: 220 Chandeleur Drive, Mooresville, North Carolina 28117 Tel.: Unknown
UST Operator: Bill Bolmer
Address: 220 Chandeleur Drive, Mooresville, North Carolina 28117 Tel.: Unknown
Property Owner: Grant William Bolmer Jr. (Bolmer Group)
Address: 17750 Mooresville Road, Mooresville, North Carolina 28125 Tel.: Unknown
Property Occupant: Vacant
Address: 1484 Mecklenburg Highway, Mount Mourne, North Carolina, 28115 Tel: Unknown
Consultant/Contractor: ATC Associates of North Carolina, P.C.
Address: 7606 Whitehall Exec. Cntr Dr. Ste 800, Charlotte, NC Tel.: [phone]
Analytical Laboratory: Pace Analytical Laboratory State Certification No.: 12
Address: 9800 Kincey Ave, Suite 100, Huntersville NC 28078 Tel: [phone]

3. Information about Release
Date Discovered: October 2006
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): Leaking UST System
Sizes and contents of UST system(s) from which the release occurred: Three 550-gallon
gasoline USTs and one 100-gallon hydraulic oil UST.
Criteria Used to Classify Risk: Water supply wells within 1,000 feet of the source area.

4. Information about the Monitoring Report
Date(s) of Groundwater Monitoring & Supply Well Sampling Events(s): 7/25/23 and 8/4/23

5. Certification
I, Al Quarles, a Licensed Geologist for ATC Associates of
North Carolina, P.C., do certify that the information contained
in this report is correct and accurate to the best of my
knowledge.

ATC Associates of North Carolina, P.C. is licensed to practice
engineering and geology in North Carolina. The certification
number of the company or corporation is C-1598 for
engineering and C-294 for geology.
Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501
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2.0 EXECUTIVE SUMMARY
ATC Associates of North Carolina, P.C. (ATC) has completed a Groundwater Monitoring Report
(GMR) documenting site assessment activity conducted in July and August 2023, at Dot’s Place
Too, located at 1484 Mecklenburg Highway in Mount Mourne, Iredell County, North Carolina.
The GMR was performed based on the June 22, 2023, Task Authorization (TA-01) by the Trust
Fund Branch of the Underground Storage Tank (UST) Section, Division of Waste Management,
North Carolina Department of Environmental Quality (NCDEQ) and an August 4, 2023 Change
Order for the resampling of water supply well WSW-8. The work was performed as part of the
State Lead Contract #N70522-B between NCDEQ and ATC. Former petroleum USTs at the site
released petroleum product to the subsurface prior to their removal in 2006. This GMR
documents impacts to the site related to the former UST system.

The approved scope of services included the sampling of five monitoring wells (MW-1R, MW-4,
MW-5, MW-6, and DW-1), and two active potable water supply wells (WSW-8, and WSW-9),
with analysis of all samples for volatile organic compounds (VOCs) by Standard Method (SM)
6200B. All samples were collected on July 25, 2023, and water supply well WSW-8 was
resampled on August 4, 2023, that also included the analysis of 1,2-dibromoethane or ethylene
dibromide (EDB) using EPA Method 504.1. Analytical results were compared to the 15A NCAC
02L .0202 Groundwater Quality Standards (2L Standards) and Gross Contamination Levels
(GCLs). Due to an oversight, the sampling of the on-site water supply well or water supply well
WSW-4 was not included in the proposed scope of services.

Analytical results from the July 25, 2023 sampling indicated that the reported results for
monitoring well MW-5 (with no VOCs) and water supply well WSW-8 (with multiple VOCs) had
been swapped by the laboratory. Confirmation sampling of WSW-8 on August 4, 2023 indicated
no VOCs with the exception of chloroform. For the purposes of this report, the analytical data
discussed used, assumes that the results from MW-5 and WSW-8 had been switched.

A summary of the site conditions based on the recent and historical assessment are presented
below and in the Conceptual Site Model (CSM) in Appendix A.

 Six active water supply wells are located within 500 feet of the source area, including two
wells within 250 feet (WSW-SITE and WSW-4). While municipal water is available those
properties, none the properties are not within the Town of Mooresville limits and cannot
access the water line at this time. Additional active water supply wells are likely present
between 500 and 1,000 feet of the source area;
 Water supply well WSW-8 contained chloroform (August 4, 2023 sample) at an estimated
concentration of 0.22 micrograms per liter (µg/L), less than the 2L Standard;
 The water supply well WSW-9 sample contained trihalomethanes typically found in
treated municipal water and no other VOCs. The sample is presumed to be a municipal
water sample;
 Light non-aqueous phase liquid (LNAPL) was not detected in the monitoring wells;
 EDB was detected in wells MW-1R at a concentration of 209 µg/L, exceeding the GCL of
50 µg/L;
 Each of the shallow monitoring wells sampled contained several VOCs at concentrations
exceeding the 2L Standards;
 The depth to groundwater ranged from 28.84 feet below top of casing (ft-toc) in well MW-6
to 31.22 ft-toc in well MW-5 on July 25, 2023. Groundwater levels are approximately 5.5 to
6.8 feet lower than those observed in March 2021; and,
Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501
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 Historically, groundwater flow has been indicated to be the southeast. The recent data
suggest a groundwater mound at well MW-1R with flow to the west toward MW-6 from MW-
1 and to the southeast toward MW-5 from MW-1.

The contaminant plume appears to be generally stable with overall decreasing concentrations
with time except for well MW-6. VOC concentrations in well MW-6 increased since first sampled
in March 2021 possibly due to the use of the on-site water supply well. VOC concentrations
were below laboratory detection limits in the deep well DMW-1. Contaminant concentrations
have fluctuated with time but are generally decreasing.

The reduction of VOCs following prior aggressive fluid vapor recovery (AFVR) events does not
appear to be sustained, and the use of oxygen releasing socks has not been effective at
reducing the contaminant concentrations in groundwater monitoring wells. Based on the current
and historical findings, ATC recommends the following:

 Sample the on-site water supply well WSW-SITE and WSW-4 located within 500 feet of the
source area.
 Consider conducting a qualitative high resolution site characterization (qHRSC) for possible
chemical injection to reduce the petroleum VOCs including EDB that exceeds the GCL.
 Consider conducting a combined mobile multi-phase extraction / air sparge (MMPE/AS)
event using MW-1, MW-4, and MW-6 as extraction wells and DMW-1 as the sparge well.

3.0 SITE DESCRIPTION
3.1 Site Characterization
The NCDEQ retained ATC to provide environmental consulting services for Dot’s Place Too,
which is located at 1484 Mecklenburg Highway in Mount Mourne, Iredell County, North
Carolina. Figure 1 depicts the site location on a topographic map. The site is currently used as
a plant nursery with retail sales of lawn care and landscaping products.

Twenty-four water supply wells were identified within 1,000 feet of the site in 2008. Data from
the 2015 receptor update indicated four active water supply wells within 500 feet of the site, and
current site activities identified six active water supply wells within 500 feet of the source area,
including an on-site wells (WSW-SITE) and WSW-4 within 250 feet of the source area.
Municipal water lines from the Town of Mooresville are located along the properties with the
water supply wells, however, the properties are not within the Town of Mooresville limits. Thus,
access to the municipal water line is not available at this time and would require that the
properties be annexed into the Town of Mooresville. Figure 2 indicates the location of water
supply wells in the site vicinity, and Table 1 provides the water supply well information. Figure 3
presents the locations of the monitoring wells and prior locations of the former USTs and
building.

3.2 Site Background
The former Dot’s Place Too served as a gasoline station in the 1970’s and 1980s. Four
underground storage tanks (USTs) were formerly utilized at the site. Three 550-gallon gasoline
USTs and one 100-gallon hydraulic oil UST were removed in October 2006. During UST
closure activities, concentrations of diesel range organic and gasoline range organic total
petroleum hydrocarbons were detected exceeding the North Carolina action levels for soil.

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Between February 13 and April 1, 2008, Geological Resources, Inc. completed Phase I and II
Limited Site Assessments (LSA) at the site. During the investigations, four groundwater
monitoring wells were installed (MW-1, MW-2, MW-3, and MW-4). Groundwater sampling from
the Phase II LSA indicated petroleum impact to the monitoring wells, including a concentration
of EDB exceeding the GCL in monitoring well MW-1.

Subsequent groundwater monitoring events have been conducted at the site from 2009 through
2013, which indicated remaining petroleum impact above the 2L Standards. In November 2009,
monitoring well MW-1R was installed to replace monitoring well MW-1 which was destroyed
during the installation of a water main near the western edge of the site. In February 2010,
monitoring well MW-5 was installed to the west of the site in a vacant lot.

On January 4, 2013, Force Environmental Service Company, LLC performed an 8-hour
aggressive fluid-vapor recovery (AFVR) event utilizing well MW-1R as the extraction point.
According to an Initial Abatement Action Report (IAAR) performed by Schnabel Engineering
South, P.C, the AFVR event recovered approximately 825 gallons of petroleum impacted
groundwater. Calculations to determine the volume of VOCs recovered as vapor were not
provided. Post-AFVR groundwater monitoring indicated that the AFVR had aided in reducing the
dissolved petroleum constituent concentrations below GCLs; however, petroleum impact
remained above 2L Standards.

In April 2015, ATC and A&D Environmental Services conducted an 8-hour AFVR event using
well MW-4 as the extraction point. The AFVR generated approximately 1,019 gallons of
petroleum impacted groundwater and recovered an estimated 5.75 gallons of petroleum as
vapor. In May 2015, ATC completed a comprehensive groundwater sampling event and
updated the sensitive receptor and water supply well survey previously completed in 2008. VOC
concentrations were reduced slightly. Table 1 lists water supply wells within 500 feet of the
source area.

Adventus remedial O-sox were installed in monitoring wells MW-1R, MW-4, and MW-5 in
August 2015 and a subsequent monitoring event was performed in February 2016. The
subsequent sampling event was performed to monitor groundwater conditions following an
updated O-sox installation in June 2016.

In August 2017, groundwater monitoring wells MW-1R, MW-4, and MW-5, and water supply
wells WSW-3 and WSW-9/WSW-26 were sampled. Several petroleum constituents were
detected in wells MW-1R, MW-4, and MW-5 above the 2L Standards.

Provectus Oxygen Releasing Substrate (ORS) were installed in monitoring wells MW-1R, MW-
4, and MW-5 in September 2018.

Groundwater monitoring wells MW-1R, MW-3, MW-4, and MW-5 were sampled in September
2019. The ORS was removed from monitoring wells MW-1R, MW-4, and MW-5 prior to
sampling. EDB was detected in wells MW-1R and MW-4 at concentrations exceeding the GCLs.
Several petroleum constituents were detected in wells MW-1R, MW-3, and MW-5 at
concentrations exceeding the 2L Standards.

In April 2020, groundwater samples were collected from water supply wells WSW-2, WSW-3,
WSW-5 and WSW-9/WSW-26. No petroleum constituents were detected in the April 2020 water
supply well samples with the exception of chloroform (0.47 µg/L) in WSW-9/WSW-26 which was
Monitoring Report October 13, 2023
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below the 2L Standard. ATC recommended the installation of a shallow monitoring well at the
former kerosene/gasoline UST basin, and a deep monitoring well in the former gasoline
dispenser/UST basin to further evaluate the horizontal and vertical extent of groundwater impact,
and four additional soil borings around the former gasoline dispenser/UST basin to evaluate the
extent and magnitude of soil contamination.

On March 11, 2021, ATC oversaw the advancement of four soil borings for the collection of soil
samples. On March 11 and 12, 2021, ATC supervised the installation of monitoring wells MW-6
and DW-1. On March 11, 2021, soil samples were collected from four soil borings (SB-A, SB-B,
SB-C, and SB-D) and two monitoring wells (MW-6 and DW-1) at select intervals. One soil
sample from each boring was selected for laboratory analysis based on the highest potential for
soil impacts based on visual and olfactory observations, as well as PID screening results. The
VOCs detected in soils included, p-Isopropyltoluene, methyl isobutyl ketone (MIBK), and C5-C8
Aliphatics in soil samples SB-A, MW-6, and DW-1; naphthalene in soil samples MW-6 and DW-
1; and 1,2,4-trimethylbenzene in soil sample MW-6 were detected at concentrations above the
Soil-to-Water MSCCs, but below the Residential cleanup levels. SVOCs and EPH were not
detected in the sample collected from MW-6, and the sample collected from SB-D did not
contain detectable concentrations of petroleum constituents.

On March 18, 2021, ATC collected groundwater samples from five monitoring wells (MW-1R, MW-
4, MW-5, MW-6, and DW-1), and two active potable water supply wells (WSW-8, and WSW-
9/WSW-26) located within 500 feet of the source area. Groundwater monitoring wells MW-2 and
MW-3 were not located for sampling, and ATC was unable to obtain permission to sample water
supply wells WSW-2 and WSW-3. Six active water supply wells are located within 500 feet of the
source area. Municipal water is available to properties located along Mecklenburg Highway;
however, none of the properties with identified water supply wells have an active municipal water
account. Additional active water supply wells are likely present between 500 and 1,000 feet of the
source area.

An active water supply well, presumed to be used for drinking water and irrigation, was observed
on site during the March 2021 assessment activities, and appears to have been installed at the site
at some time since 2019. The site does not have an active municipal water account. Light non-
aqueous phase liquid (LNAPL) was not detected in the monitoring wells,1,2-Dibromoethane
(ethylene dibromide or EDB) was detected in wells MW-1R and MW-4 at concentrations
exceeding the GCL. Each of the sampled monitoring wells contained several VOCs at
concentrations exceeding the 2L Standards. The water supply wells contained toluene (WSW-8 at
0.6 micrograms per liter or µg/L) and chloroform (WSW-9 at 0.43J µg/L), at concentrations less
than the 2L Standards.

3.3 Site and Regional Geology
According to the Geologic Map of North Carolina, produced by the State of North Carolina in
1985, the site lies in the Charlotte Belt of the Piedmont Physiographic Province of North
Carolina. The rock type in this area has been identified as granite, a crystalline igneous rock.
The shallow subsurface in most areas of the Piedmont contains residual soil overburden,
including structure-free residuum, saprolite, and partially weathered rock (PWR) that derive from
in-place weathering of the crystalline bedrock. Occasional areas containing recent deposits of
alluvium in the uppermost subsurface are found near streams and rivers. Saprolite and PWR
typically contain some relict structures from the original rock material. Depth to rock ranges from
ground surface at occasional outcrops to depths of greater than 100 feet in areas of easily
weathered rock.
Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501
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According to geological data collected during the installation of the monitoring wells during the
Phase II LSA performed by Geological Resources, Inc., the site soils consist of undifferentiated
silts to approximately 22 ft-bgs, transitioning to saprolite and granitic rock at a depth of 40 ft-bgs.
Based on ATC’s observations during the installation of monitoring wells MW-6 and DW-1, PWR
extended to a depth of approximately 55 ft-bgs, and bedrock was encountered from 55 ft-bgs to
65 ft-bgs.

On March 11 and 12, 2021, ATC supervised the installation of monitoring wells MW-6 and DW-
1. The boring for monitoring well MW-6 was extended to a depth of approximately 35 ft-bgs. The
boring for the outer casing of DW-1 was extended to a depth of approximately 55 ft-bgs. The
boring for monitoring well DW-1 was extended to approximately 65 ft-bgs. Evidence of PWR
was observed from approximately 25 ft-bgs to 55 ft-bgs, and the top of bedrock was
encountered at a depth of approximately 55 ft-bgs.

3.4 Site and Regional Hydrogeology
The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and
rivers to as deep as 50 feet or more beneath upland surfaces in some parts of the Piedmont.
Water in the alluvium or unconsolidated residual material, including saprolite and PWR, usually
behaves as an unconfined aquifer, or water table, and will yield water with head elevation
equivalent to the first elevation where water was encountered. Permeability varies with lithology
and is typically relatively low in residual soils, with higher permeability in saprolite or PWR due
to relict rock texture and variable susceptibility to weathering exhibited by different minerals in
the rock. Groundwater flow in residual soils or alluvium generally follows local topographic
conditions toward local drainage features. Based on the data from the monitoring well network,
shallow groundwater flows generally to the east. The depth to groundwater ranged from 28.84
feet below top of casing (ft-toc) in well MW-6 to 31.22 ft-toc in well MW-5, during the groundwater
monitoring event. Historical groundwater levels have ranged from approximately 22 ft-bgs to 35 ft-
bgs.

Modern water supply wells in the Piedmont, likely including those in the site vicinity, are typically
installed with a surface casing through the unconsolidated material, and an open borehole into
the bedrock where water-bearing fractures are encountered.

4.0 GROUNDWATER CHARACTERIZATION
4.1 Water Supply Wells
On July 25, 2023, ATC collected samples from water supply wells WSW-8 and WSW-9. On August
4, 2023, ATC collected a confirmatory sample from water supply well WSW-8. No sample was
proposed to be collected from water supply wells WSW-SITE or WSW-4 located within 250 of the
source area. Water supply well information is included in Table 1 and locations are depicted on
Figure 2.

During sampling activities, the water supply wells were purged for 15 minutes prior to sampling.
The water samples were collected in laboratory-supplied, preserved containers; entered into
chain of custody control; placed on ice; and shipped to Pace Analytical Services, LLC in
Huntersville, North Carolina. The water supply well samples were analyzed by Standard Method
6200B for VOCs including petroleum constituents. Field notes from the groundwater monitoring
event are included in Appendix B. The analytical report is included in Appendix C.

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ATC received the analytical results for these wells on August 2, 2023. Analytical results from
MW-5 did not indicate the presence of VOCs, where they had been present during the previous
sampling event. The analytical results from WSW-8 indicated the presence of various VOCs
where none had been present previously. Based on these results, ATC concluded that the
samples had been switched at some point.

ATC reviewed field notes and laboratory report, and asked field and laboratory staff about
possible mislabeling of sample identifications between sample MW-5 and WSW-8. The sample
containers were labeled in the field at the time of sample collection of each sample, and
therefore, mislabeling by the field staff does not appear to be the cause. The laboratory
indicated that they checked their system and found no indication of mislabeling, although ATC
suspects that to be the case. To confirm the results for WSW-8, ATC resampled WSW-8 on
August 4, 2023, and those results indicated no VOCs except for an estimated concentration of
chloroform.

For the purposes of this report, the analytical results of the July 25, 2023 sampling of WSW-8
and MW-5 are reported as if the sample identifications were mislabeled.

4.2 Groundwater Levels
On July 25, 2023, a groundwater gauging event was conducted for monitoring wells MW-1R,
MW-4, MW-5, MW-6, and DW-1. Monitoring wells MW-2 and MW-3 were not located and are
likely covered by landscaping supplies. Depth to groundwater and total well depths were
measured from TOC using an electronic water level indicator. Figure 3 depicts a site map with
pertinent site features and monitoring well locations. Monitoring well construction details are
summarized in Table 2.

Groundwater flow has previously been reported to be the southeast. The depth to groundwater
ranged from 28.84 feet below top of casing (ft-toc) in well MW-6 to 31.22 ft-toc in well MW-5.
Historical groundwater levels have ranged from approximately 22 ft-bgs to 35 ft-bgs. Recent and
historical depth to groundwater and groundwater elevation data are summarized in Table 3. A
groundwater elevation map is presented in Figure 4. Field notes from the groundwater
monitoring event are included in Appendix B.

4.3 Groundwater Quality
On July 25, 2023, a groundwater sampling event was conducted for monitoring wells MW-1R,
MW-4, MW-5, MW-6, DW-1, WSW-8, and WSW-9. LNAPL was not detected in the monitoring
wells.

During sampling activities, the monitoring wells were purged of three standing well volumes, or
purged dry and allowed to recharge, to ensure a representative groundwater sample was collected.
After purging, field parameters were measured and recorded at the time of sampling and are
presented in Table 4 and in the field notes included in Appendix B.

The water samples were collected in laboratory-supplied, preserved containers; placed on ice;
entered into chain of custody control; and transported to Pace Analytical Services, LLC in
Huntersville, North Carolina. The monitoring well samples, a field blank, and a trip blank were
analyzed by Standard Method 6200B for VOCs including petroleum constituents.

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Groundwater analytical results for the groundwater monitoring wells, assuming the original WSW-8
data is actually that of MW-5, were compared to the 2L Standards and GCLs. The findings from the
groundwater monitoring event indicate the following:

 Water supply well WSW-8 contained chloroform (August 4, 2023 sample) at an estimated
concentration of 0.22 µg/L, less than the 2L Standard;
 The water supply well WSW-9 sample contained trihalomethanes typically found in
chlorinated water. The property with this well does not have an active municipal water
account;
 LNAPL was not detected in the monitoring wells;
 Monitoring wells MW-1R contained EDB at 209 µg/L, exceeding the GCL of 50 µg/L;
 Each of the shallow monitoring wells contained several VOCs at concentrations exceeding
the 2L Standards; and
 VOCs were not detected in the deep monitoring well DMW-1, except for chloroform at an
estimated concentration less than the 2L Standard.

Recent groundwater analytical results for the monitoring and water supply wells are summarized
in Table 5. Historical water supply well and monitoring well analytical data are included in Table
6 and Table 7, respectively. Figure 5, Figure 6, and Figure 7 depict the concentrations for
benzene, EDB, and VOCs exceeding the 2L Standards in groundwater. Field notes and
photographs from the groundwater monitoring event are included in Appendix B. The
laboratory analytical report is included in Appendix C.

The contaminant plume appears to be generally stable with overall decreasing concentrations
with time except for well MW-6. VOC concentrations in well MW-6 increased since first sampled
in March 2021 possibly due to the use of the on-site water supply well. VOC concentrations
were below laboratory detection limits in the deep well DMW-1. Contaminant concentrations
have fluctuated with time but are generally decreasing.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of
the laboratory reports was conducted. During the review, it was found that the samples were
received from the laboratory in acceptable condition and properly preserved. The samples were
analyzed within correct holding times and reported within the lab report, and the chain of
custody was properly completed by all parties. The field blank sample, FB-1, and a laboratory
provided Trip Blank were analyzed for VOCs, neither of which contained detectable
concentrations of petroleum constituents. The laboratory QC report shows that two internal
method blanks were analyzed for each method that was used for the original samples. The
laboratory fortified blank (LFB) and laboratory control sample (LCS) data results were also
provided for each analytical method. Some samples had to be diluted during analysis, resulting in
method detection limits that exceeded the 2L Standard; however, the wells with higher dilutions
had other compounds with confirmed detections above 2L Standards. Refer to the laboratory
reports in Appendix C for details regarding QA results for the laboratory samples and any noted
exceptions. Overall, ATC concludes that the laboratory results are usable. Lab qualifications are
defined on the corresponding tables.

Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501
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5.0 CONCLUSIONS AND RECOMMENDATIONS
On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Groundwater
Monitoring Report documenting assessment activities conducted in July and August 2023, at
Dot’s Place Too, located at 1484 Mecklenburg Highway in Mount Mourne, Iredell County, North
Carolina.
The approved scope of services included the sampling of five monitoring wells (MW-1R, MW-4,
MW-5, MW-6, and DW-1), and two active potable water supply wells (WSW-8, and WSW-9),
with analysis of all samples for VOCs by SM 6200B. All samples were collected on July 25,
2023, and water supply well WSW-8 was resampled on August 4, 2023, that also included the
analysis of EDB using EPA Method 504.1. Analytical results were compared to the 2L
Standards and GCLs.

Analytical results from the July 25, 2023 sampling indicated that the reported results for
monitoring well MW-5 (with no VOCs) and water supply well WSW-8 (with multiple VOCs) had
been mislabeled by the laboratory. Confirmation sampling of WSW-8 on August 4, 2023
indicated no VOCs with the exception of chloroform. For the purposes of this report, the
analytical data discussed used, assumes that the results from MW-5 and WSW-8 had been
switched.

A summary of the site conditions based on the recent and historical assessment are presented
below and in the CSM in Appendix A.

 Six active water supply wells are located within 500 feet of the source area, including two
wells within 250 feet (WSW-SITE and WSW-4). While municipal water is available those
properties, none the properties are not within the Town of Mooresville limits and cannot
access the water line at this time. Additional active water supply wells are likely present
between 500 and 1,000 feet of the source area;
 Water supply well WSW-8 contained chloroform (August 4, 2023 sample) at an estimated
concentration of 0.22 µg/L, less than the 2L Standard;
 The water supply well WSW-9 sample contained trihalomethanes typically found in
chlorinated water. The property with this well does not have an active municipal water
account;
 LNAPL was not detected in the monitoring wells;
 EDB was detected in wells MW-1R at a concentration of 209 µg/L, exceeding the GCL of
50 µg/L;
 Each of the shallow monitoring wells sampled contained several VOCs at concentrations
exceeding the 2L Standards;
 The depth to groundwater ranged from 28.84 feet below top of casing (ft-toc) in well MW-6
to 31.22 ft-toc in well MW-5 on July 25, 2023. Groundwater levels are approximately 5.5 to
6.8 feet lower than those observed in March 2021; and,
 Historically, groundwater flow has been indicated to be the southeast. The recent data
suggest a groundwater mound at well MW-1R with flow to the west toward MW-6 from MW-
1 and to the southeast toward MW-5 from MW-1.

The contaminant plume appears to be generally stable with overall decreasing concentrations
with time except for well MW-6. VOC concentrations in well MW-6 increased since first sampled
in March 2021 possibly due to the use of the on-site water supply well. VOC concentrations
were below laboratory detection limits in the deep well DMW-1. Contaminant concentrations
have fluctuated with time but are generally decreasing.
Monitoring Report October 13, 2023
Dot’s Place Too, Incident # 36185, Mooresville, NC ATC Project No. STL3618501
10
The reduction of VOCs following prior AFVR events does not appear to be sustained, and the
use of oxygen releasing socks has not been effective at reducing the contaminant
concentrations in groundwater monitoring wells. Based on the current and historical findings,
ATC recommends the following:
Sample the on-site water supply well WELL-SITE and WSW-4 located within 250 feet of
the source area;
Consider conducting a qHRSC for possible chemical injection to reduce the petroleum
VOCs including EDB that exceeds the GCL.
Consider conducting a combined MMPE/AS event using MW-1, MW-4, and MW-6 as
extraction wells and DMW-1 as the sparge well.

TABLES
TABLE 1WATER-SUPPLY WELL INFORMATIONDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well Well / Property OwnerProperty AddressOwner AddressWell Use (P/I/A/N)Active Municipal Water Account (Y/N)Available Water Connection (Y/N)WSW-SITE Bolmer Group LLC1484 Mecklenburg HighwayMooresville, NC 2811717750 Mooresville RoadMooresville, NC 28115P / INYWSW-2RKWP LLCMoser Brothers Enterprises Inc.1488 Mecklenburg HighwayMooresville, NC 28117444 Williamson Rd, Suite AMooresville, NC 28117130 SWPNYWSW-3 HWG Mt. Mourne LLC1477 Mecklenburg HighwayMooresville, NC 28117130 Valleymist LaneMooresville, NC 28117295 NE UnknownVacant with no structures on-siteYWSW-4 Bolmer Group LLC1478 Mecklenburg HighwayMooresville, NC 2811717750 Mooresville RoadMooresville, NC 28115220 NPNYWSW-5 HWG Mt. Mourne LLC1489/1495 Mecklenburg HighwayMooresville, NC 28117130 Valleymist LaneMooresville, NC 28117275 SSE N *Vacant with no structures on-siteYWSW-6 HWG Mt. Mourne LLCVacant - Mecklenburg HighwayMooresville, NC 28117130 Valleymist LaneMooresville, NC 28117290 SEAVacant with no structures on-siteYWSW-8 Joseph Albert Wilson Heirs117 Faith RoadMooresville, NC 28117P.O. Box 66Mount Mourne, NC 28123475 ESE PNYWSW-9Gaston Tuck1467 Mecklenburg HighwayMooresville, NC 28117P.O. Box 444Mount Mourne, NC 28123450 NNE PNYNotes:P / I / A / N = Potable / Irrigation / Abandoned / Not ActiveNote: All properties with the active water supply wells are outside of the Town of Mooresville, and the properties would need to be annexed to access the water line.Distance/Direction From Source Area(ft)SITE
TABLE 2
MONITORING WELL CONSTRUCTION DETAILS
DOT'S PLACE TOO
1484 Mecklenburg Highway
Mount Mourne, Iredell County, North Carolina
NCDEQ Incident #36185
MW-1R 11/17/09 30-40 2 40 100.02
DMW-1 03/12/21 60-65 2 65 100.04
MW-2 03/31/08 25-40 2 40 99.34
MW-3 03/31/08 25-40 2 40 98.83
MW-4 03/31/08 25-40 2 40 100.23
MW-5 02/11/10 20-35 2 35 100.68
MW-6 03/11/21 18-33 2 33 98.23
Notes:
Top of casing elevation relative to arbitrary benchmark elevation of 100 feet
Top of Casing
Elevation
(feet)
Well
ID
Date
Installed
Screen
Interval
(feet)
Well
Diameter
(inches)
Total
Depth
(feet)

TABLE 3
GROUNDWATER ELEVATION DATA
DOT'S PLACE TOO
1484 Mecklenburg Highway
Mount Mourne, Iredell County, North Carolina
NCDEQ Incident #36185
11/17/09 31.71 68.31
02/11/10 28.66 71.36
01/07/11 29.01 71.01
05/10/11 28.02 72.00
10/19/11 30.19 69.83
07/20/12 29.96 70.06
02/07/13 33.67 66.35
08/25/14 29.64 70.38
05/18/15 30.49 69.53
02/15/16 32.15 67.87
08/22/17 31.99 68.03
09/03/19 25.55 74.47
03/18/21 23.96 76.06
07/25/23 29.53 70.49
05/21/09 29.75 69.59
11/06/09 31.02 68.32
02/11/10 27.22 72.12
01/07/11 27.95 71.39
05/10/11 26.65 72.69
10/19/11 29.43 69.91
07/20/12 29.49 69.85
02/07/13 32.99 66.35
08/25/14 29.35 69.99
05/18/15 29.63 69.71
02/15/16 31.27 68.07
08/22/17 Obstruction- Well not accessible
09/03/19 Could Not Find
03/18/21 Could Not Find
07/25/23
99.34
Well
ID
MW-1R 30-40
MW-2 25-40
Groundwater
Elevation
Depth to
Groundwater
TOC
Elevation
Screen
Interval
Gauging
Date
100.02
Not Required
Page 1 of 3

TABLE 3
GROUNDWATER ELEVATION DATA
DOT'S PLACE TOO
1484 Mecklenburg Highway
Mount Mourne, Iredell County, North Carolina
NCDEQ Incident #36185
Well
ID
Groundwater
Elevation
Depth to
Groundwater
TOC
Elevation
Screen
Interval
Gauging
Date
05/21/09 27.91 70.92
11/06/09 28.90 69.93
02/11/10 23.86 74.97
01/07/11 27.75 71.08
05/10/11 25.96 72.87
10/19/11 28.54 70.29
07/20/12 27.96 70.87
02/07/13 30.84 67.99
08/25/14 27.78 71.05
05/18/15 27.31 71.52
02/15/16 27.02 71.81
08/22/17 Obstruction- Well not accessible
09/03/19 24.17 74.66
03/18/21 Could Not Find
07/25/23
05/21/09 31.71 68.52
11/06/09 32.44 67.79
02/11/10 29.59 70.64
01/07/11 29.81 70.42
05/10/11 29.99 70.24
10/19/11 30.93 69.30
07/20/12 30.50 69.73
02/07/13 34.30 65.93
08/25/14 30.12 70.11
04/27/15 NM NM
05/18/15 31.22 69.01
02/15/16 32.78 67.45
08/22/17 32.73 67.50
09/03/19 26.30 73.93
03/18/21 24.70 75.53
07/25/23 30.38 69.85
MW-3 25-40 98.83
Not Required
MW-4 25-40 100.23
Page 2 of 3

TABLE 3
GROUNDWATER ELEVATION DATA
DOT'S PLACE TOO
1484 Mecklenburg Highway
Mount Mourne, Iredell County, North Carolina
NCDEQ Incident #36185
Well
ID
Groundwater
Elevation
Depth to
Groundwater
TOC
Elevation
Screen
Interval
Gauging
Date
02/11/10 30.31 70.37
01/07/11 30.52 70.16
05/10/11 29.70 70.98
10/19/11 31.61 69.07
07/20/12 31.18 69.50
02/07/13 34.89 65.79
08/25/14 30.79 69.89
05/18/15 31.93 68.75
02/15/16 33.76 66.92
08/22/17 33.83 66.85
09/03/19 27.03 73.65
03/18/21 25.47 75.21
07/25/23 31.22 69.46
03/18/21 22.10 76.13
07/25/23 28.84 69.39
03/18/21 24.00 76.04
07/25/23 30.14 69.90
Notes:
All measurements expressed in feet
TOC = Top of Casing
NM = Not Measured
MW-5 20-35 100.68
MW-6
DMW-1 60-65 100.04
98.2318-33
Page 3 of 3
TABLE 4FIELD PARAMETERSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185MW-1R 07/25/2320.710.153.6535.7MW-4 07/25/2323.110.352.7314.9MW-5 07/25/2323.560.205.0765.6MW-6 07/25/2319.160.273.5215.2DW-107/25/2320.930.189.8-436.4Notes:°C = degrees CelsiusmS/cm = milliSiemens per centimetermg/L = milligrams per literORP = oxidation-reduction potentialmV= millivoltssu = standard unitspH(su)Well IDSample DateTemperature (°C)Conductivity (mS/cm)Dissolved Oxygen(mg/L)ORP(mV)Page 1 of 1
TABLE 5RECENT GROUNDWATER ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Sample IDConstituent of ConcernBenzeneTolueneEthylbenzeneTotal XylenesChloroformNaphthalene1,2-Dibromoethane (EDB)1,2-DichloroethaneIsopropylbenzene n-Propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1 600 600 50070 6 0.02 0.4 70 70 400 4005,000260,00080,00050,00070,0006,0005040025,00026,10028,50024,100MW-1R 07/25/231,680 35,400 2,210 23,650<13.8484 209<21.272.2J 134 2,770 714MW-4 07/25/23361 7,480 3,230 17,230<3.5371<7.4 <5.3190 498 3,210 858MW-5 07/25/2314.555.2 369 1,716 <0.06940.6 0.37J 1.035.381.2 770<0.71MW-6 07/25/2327.91379472,910 <1.4104<2.9 <2.1140 4442570784DW-107/25/23 <0.079 <0.090 <0.081 <0.234 0.26J <0.10 <0.15 <0.11 <0.11 <0.10 <0.031 <0.07107/25/23 <0.079 <0.090 <0.081 <0.234 <0.069 <0.10 <0.15 <0.11 <0.11 <0.10 <0.031 <0.07108/04/23 <0.079 <0.090 <0.081 <0.234 0.22J <0.10 <0.15 <0.11 <0.11 <0.10 <0.031 <0.071WSW-9 07/25/23 <0.079 <0.090 <0.081 <0.234 40.9* <0.10 <0.15 <0.11 <0.11 <0.10 <0.031 <0.071Notes:Concentrations are reported in micrograms per liter (µg/L)."<" = Not detected at or above the laboratory detection limit2L Standard = 15A NCAC 2L .0202 Groundwater Quality StandardsGCL = Gross Contamination LevelJ = Estimated value between laboratory method detection limit and reporting limitValues in BOLD exceed 2L StandardsValues In UNDERLINED AND BOLD text exceed GCL standards.NE - Not Established* Chloroform and other trihalomethanes reported in the water supply well sample WSW-9, presumed to be municipal water.2L StandardsGCL StandardsWSW-8
TABLE 6HISTORICAL WATER SUPPLY WELL ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well IDSampleDateBenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl Ether1,2-Dibromoethane (EDB)Naphthalenen-ButylbenzeneMethylene ChlorideChloroformIsopropylbenzenen-propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1 600 600 500 20 70 0.02 6 70 5 70 70 70 400 40005/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.21 <0.019 <0.39 <0.20 1.2 0.77 <0.24 <0.30 <0.20 <0.2511/05/09 <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 <0.5 3.2 <0.5 <2.0 0.88 <0.5 <0.5 <0.5 <0.502/11/10 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.5001/07/11 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.061 <0.50 <0.50 <0.50 <0.17 <0.50 <0.50 <0.50 <0.5005/10/11 <0.27 <1.7 <1.7 <1.7 <0.19 0.38 J <0.61 <1.7 <0.17 <0.17 <1.7 <0.29 <0.24 <1.7 <1.710/19/11 <0.27 <1.7 <1.7 <1.7 0.22 J <0.052 <0.61 <1.7 <0.17 <0.17 0.6 <0.29 <0.24 <1.7 <1.704/27/20 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <2.0 <0.50 2.0 <0.50 <0.50 <0.50 <0.50 <0.5003/18/21Not Sampled05/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.21 <0.019 <0.39 <0.20 0.69 <0.20 <0.24 <0.30 <0.20 <0.2511/05/09 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.5002/11/10 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.5001/07/11 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.061 <0.50 <0.50 <0.50 <0.17 <0.50 <0.50 <0.50 <0.5005/10/11 <0.027 9.5 13 <0.17 <0.019 <0.052 <0.061 <0.17 0.81 <0.17 <0.17 1.8 3.8 45 1310/19/11 <0.027 <0.17 <0.17 <0.17 <0.019 <0.052 <0.061 <0.17 <0.50 <0.17 <0.17 <0.029 <0.024 <0.17 <0.1705/18/15 <0.079 <0.090 <0.092 <0.29 <0.090 <0.18 <0.089 <0.12 <0.054 <3.2 <0.14 <0.11 <0.094 <0.18 <0.1003/02/16 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <5.0 <1.0 <0.50 <0.50 <0.50 <0.5008/22/17 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <1.0 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.5004/27/20 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <2.0 <0.50 2.0 <0.50 <0.50 <0.50 <0.50 <0.5003/18/21Not SampledWSW-3(1477 Meck. Hwy)WSW-2 (1488 Meck. Hwy)2L StandardPage 1 of 3
TABLE 6HISTORICAL WATER SUPPLY WELL ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well IDSampleDateBenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl Ether1,2-Dibromoethane (EDB)Naphthalenen-ButylbenzeneMethylene ChlorideChloroformIsopropylbenzenen-propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1 600 600 500 20 70 0.02 6 70 5 70 70 70 400 4002L Standard05/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.21 <0.020 <0.39 <0.20 0.68 <0.20 <0.24 <0.30 <0.20 <0.2511/05/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.21 <0.019 <0.39 <0.20 0.75 <0.20 <0.24 <0.30 <0.20 <0.2505/10/11 <0.027 0.92 0.45 J 4.2 <0.019 <0.052 <0.061 2.0 <0.017 <0.17 <0.17 <0.29 <0.015 2.6 0.7908/25/14 <0.079 <0.090 <0.092 <0.29 <0.090 <0.18 <0.089 <0.12 <0.054 <3.2 <0.14 <0.11 <0.094 <0.18 <0.1005/18/15 <0.079 <0.090 <0.092 <0.29 <0.090 <0.18 <0.089 <0.12 <0.054 <3.2 <0.14 <0.11 <0.094 <0.18 <0.1003/02/16 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <5.0 <1.0 <0.50 <0.50 <0.50 <0.5005/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.21 <0.019 <0.39 <0.20 0.75 <0.20 <0.24 <0.30 <0.20 <0.2511/05/09 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.5002/11/10 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.5001/07/11 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.061 <0.50 <0.50 <0.50 <0.17 <0.50 <0.50 <0.50 <0.5005/10/11 <0.027 0.58 <0.17 0.81 <0.019 <0.052 <0.061 <0.17 <0.017 <0.17 <0.17 <0.029 <0.015 <0.17 <0.1710/19/11 <0.027 <0.17 <0.17 <0.17 <0.019 <0.052 <0.061 <0.17 0.81 <0.17 0.24 J <0.029 <0.024 <0.17 <0.1707/20/12 <0.027 <0.17 <0.17 <0.17 <0.019 <0.052 <0.061 <0.17 <0.017 <0.17 0.24 J <0.029 <0.024 <0.17 <0.1708/22/17 Not Sampled- Well Not Found- Does Not ExistWSW-5(1495 Meck. Hwy)WSW-4(1478 Meck. Hwy)Page 2 of 3
TABLE 6HISTORICAL WATER SUPPLY WELL ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well IDSampleDateBenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl Ether1,2-Dibromoethane (EDB)Naphthalenen-ButylbenzeneMethylene ChlorideChloroformIsopropylbenzenen-propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1 600 600 500 20 70 0.02 6 70 5 70 70 70 400 4002L Standard05/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.21 <0.019 <0.39 <0.20 <0.53 <0.20 <0.24 <0.30 <0.20 <0.2511/05/09 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.5002/11/10 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.5001/07/11 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.061 <0.50 <0.50 <0.50 0.20 J <0.50 <0.50 <0.50 <0.5005/10/11 <0.27 0.41 J <0.17 <0.17 <0.019 <0.052 <0.061 <0.17 <0.017 <0.17 0.22 J <0.029 <0.015 <0.17 <0.1710/19/11 <0.27 <0.17 <0.17 <0.17 <0.019 <0.052 <0.061 <0.17 0.81 <0.17 0.20 J <0.029 <0.024 <0.17 <0.1708/25/14 <0.079 <0.090 <0.092 <0.29 <0.090 <0.18 <0.089 <0.12 <0.054 <3.2 <0.14 <0.11 <0.094 <0.18 <0.1005/18/15 <0.079 <0.090 <0.092 <0.29 <0.090 <0.18 <0.089 <0.12 <0.054 <3.2 0.19 J <0.11 <0.094 <0.18 <0.1004/27/20 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <2.0 <0.50 2.0 <0.50 <0.50 <0.50 <0.50 <0.5003/18/21 <0.34 0.60 <0.30 <0.34 <0.42 <0.31 <0.27 <0.64 <0.49 <2.0 <0.35 <0.33 <0.34 <0.50 <0.3307/25/23 <0.079 <0.090 <0.081 <0.234 <0.053 <0.072 <0.15 <0.10 <0.066 <1.9 <0.069 <0.11 <0.10 <0.031 <0.07108/04/23 <0.079 <0.090 <0.081 <0.234 <0.053 <0.072 <0.15 <0.10 <0.066 <1.9 0.22J <0.11 <0.10 <0.031 <0.07102/11/10 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.64 <0.50 <0.50 <0.50 <0.5008/22/17 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <1.0 <0.50 <5.0 0.36 J <0.50 <0.50 <0.50 <0.5004/27/20 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <2.0 <0.50 <2.0 0.47 J <0.50 <0.50 <0.50 <0.5003/18/21 <0.34 <0.48 <0.30 <0.34 <0.42 <0.31 <0.27 <0.64 <0.49 <2.0 0.43 J <0.33 <0.34 <0.50 <0.3307/25/23 <0.079 <0.090 <0.081 <0.234 <0.053 <0.072 <0.15 <0.10 <0.066 <1.9 40.9 <0.11 <0.10 <0.031 <0.071Notes:ND = Not detected at or above the laboratory detection limitNE = Not EstablishedConcentrations are reported in micrograms per liter (µg/L) .Values in BOLD print indicate levels above 2L Standards* Chloroform and other trihalomethanes reported in the water supply well sample WSW-9, presumed to be municipal water.J = Estimated value below method reporting limitWSW-9/WSW-26(1467 Meck. Hwy) WSW-8 (117 Faith Rd)Page 3 of 3
TABLE 7HISTORICAL MONITORING WELL ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well IDSampleDateBenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthalene1,2-Dibromoethane (EDB)n-Butylbenzenesec-Butylbenzene1,2-DichloroethaneIsopropylbenzenen-propylbenzeneTetrachloroetheneTrichloroethene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenep-IsopropyltolueneIsopropyl EtherMethylene ChlorideEthanol1,1-Dichloroethane1,1,2,2-Tetrachloroethane1,2,3-Trichloropropane2L Standard 1 600 600 500 20 6 0.02 70 70 0.04 70 70 0.7 3.0 400 400 25 70 5 4,000 6 0.2 0.005GCL Standard 5,000260,00080,00050,00020,0006,000505,9008,80040025,00026,1007003,00028,50024,10011,70070,0005,0004,000,0006,000200NEMW-1 02/14/081,730 31,900 5,150 25,500<104390.000470.8--19.8 274 708-- --3,140 98513.3 <50 -- -- -- -- --11/17/091,060 16,200 2,980 15,590<12.5306 18<12.5 <12.525<12.5483<12.5 --3,090 780NS <12.5 <50.0 ND -- -- --02/11/10460 6,100 1,700 6,800<10.086<10.0 40 14 <10.0120 320<10.0 --1,700 460<10.0 <10.0 <10.0 <2,000 -- -- --01/07/11 <11.053,000 5,500 27,800<200300 360<6.7 <4.2 <9.3210 570<5.7 --3,100 770<7.1 <21.0 <68.0 <13,000 -- -- --05/10/112,500 23,000 3,700 15,600<0.38280 15053.0 <0.2173 170.0 450<0.29 --2,500 69013.0 <1.0 <3.44,200-- -- --10/19/114,900 52,000 4,700 23,000<9.5240 J 200 J<8.4 <5.2 <12150 J 390<7.2 --2,300 670<8.9 <26 <85 <17,000 -- -- --07/20/125,60049,000 5,200 27,200<3.8280 300<3.3 <2.1270 160 420<2.9 --2,600 690<3.5 <10 <34 <6,600 -- -- --02/07/132,600 30,800 3,510 19,400<50.0405<50.0 <50.0 <50.0 <50.0253 312<50.0 --2,140 494NA <50.0 <200 NA -- ----08/25/143,800 64,000 4,400 24,600<18290 29024 J 22 J170 J 150 380 52 J 180 2,800 700<25 <36 <640 <5,600 <32 <25 <2405/18/152,500 35,000 4,500 29,900<45 <60140 J<27 <42 <97180 J 380<40 <383,100 660<62 <90 <1,600 <14,000 <79 <62 <6002/15/161,200 16,000 2,000 22,800<120280<120 60 J <120 <120110 J 220<120 <2503,500 760<120 <120 <120 <120 <120 <120 <12008/22/171,600 25,000 2,300 21,700<200 <400 <200 <200 <200 <800140 250<200 <2003,000 770<200 <200 <2,000 <20,000 <200 <200 <20009/03/193,030 39,500 2,080 16,500<500 <500316 J<500 <500 <500 <500 <500 <500 <5001,200 408 J<500 <500 <2,000 <100,000 <500 <500 <50003/18/21792 21,400 2,320 15,500<84.4317J 70.2J<98.0 <80.0 <64.492.4J<68.0 <58.4 <76.61,910<66.4 NA <61.6 <390 NA <73.4 <45.0 <52.207/25/231,680 35,400 2,210 23,650<10.7484 209<13.3 <17.0 <21.272.2J 134<17.1 <34.22,770 714NA <14.5 <378 <1010 <11.2 <14.8 <34.603/18/2112214 67.6 303 <0.846.7<0.54 3.4 <0.80 <0.64 8.8 <0.68 <0.58 <0.77 79.3 30.8 NA <0.62 <3.9 NA <0.73 <0.45 <0.5207/25/23 <0.079 <0.090 <0.081 <0.234 <0.053 <0.10 <0.15 <0.066 <0.085 <0.11 <0.11 <0.10 <0.086 <0.17 <0.031 <0.071 NA <0.072 <1.9 <5.0 <0.056 <0.074 <0.1704/01/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <0.010 <1.0 -- <1.0 <1.0 <1.0 -- -- <1.0 <1.0 <1.0 <5.0 -- -- -- -- --04/15/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <0.010 <1.0 NS NS <1.0 <1.0 NS -- <1.0 <1.0 <1.0 NS NS -- -- -- --05/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.39 <0.020 <0.20 <0.24 NS <0.24 <0.30 <0.36 -- <0.20 <0.25 <0.26 <0.21 0.72 -- -- -- --11/06/09 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 -- <0.50 <0.50 NS <0.50 <2.0 -- -- -- --02/11/10 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 -- <0.50 <0.50 <0.50 <0.50 <0.50 -- -- -- --01/07/11 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.061 <0.50 <0.50 <0.023 <0.50 <0.50 <0.50 -- <0.50 <0.50 <0.50 <0.50 <0.50 -- -- -- --05/10/11 <0.027 <0.17 <0.17 <0.17 <0.019 <0.17 <0.061 <0.017 <0.010 <0.023 <0.029 <0.024 <0.014 -- <0.17 <0.17 <0.018 <0.052 <0.17 -- -- -- --10/19/11 <0.027 <0.17 <0.17 <0.17 <0.019 <0.17 <0.061 <0.017 <0.010 <0.023 <0.029 <0.024 <0.014 -- <0.17 <0.17 <0.018 <0.052 <0.17 -- -- -- --07/20/12 <0.027 <0.17 <0.17 <0.17 <0.019 <0.17 <0.061 <0.017 <0.010 <0.023 <0.029 <0.024 <0.014 -- <0.17 <0.17 <0.018 <0.052 <0.17 -- -- -- --02/07/13 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 -- <0.50 <0.50 NA <0.50 2.0 -- -- -- --08/25/14 <0.079 <0.090 <0.092 <0.29 <0.090 <0.12 <0.089 <0.054 <0.084 <0.19 <0.11 <0.094 <0.080 <0.077 <0.18 <0.10 <0.12 <0.18 <3.2 <28 <0.16 <0.12 <0.1205/18/15 <0.079 <0.090 <0.092 <0.29 <0.090 <0.12 <0.089 <0.054 <0.084 <0.19 <0.11 <0.094 <0.080 <0.077 <0.18 <0.10 <0.12 <0.18 <3.2 <28 <0.16 <0.12 <0.1202/15/16 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <50 <1.0 <0.50 <0.5008/22/17Not Sampled - Obstruction - Well Not Accessible09/03/19Not Sampled - Could Not Find03/18/21Not Sampled - Could Not FindDMW-1MW-2MW-1RPage 1 of 3
TABLE 7HISTORICAL MONITORING WELL ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well IDSampleDateBenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthalene1,2-Dibromoethane (EDB)n-Butylbenzenesec-Butylbenzene1,2-DichloroethaneIsopropylbenzenen-propylbenzeneTetrachloroetheneTrichloroethene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenep-IsopropyltolueneIsopropyl EtherMethylene ChlorideEthanol1,1-Dichloroethane1,1,2,2-Tetrachloroethane1,2,3-Trichloropropane2L Standard 1 600 600 500 20 6 0.02 70 70 0.04 70 70 0.7 3.0 400 400 25 70 5 4,000 6 0.2 0.005GCL Standard 5,000260,00080,00050,00020,0006,000505,9008,80040025,00026,1007003,00028,50024,10011,70070,0005,0004,000,0006,000200NE04/15/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <0.010 <1.0 NS NS <1.0 <1.0 NS -- <1.0 <1.0 <1.0 NS NS -- -- -- --05/21/09 <0.20 <0.27 <0.20 <0.40 <0.38 <0.39 <0.019 <0.20 <0.24 NS <0.24 <0.30 <0.36 -- <0.520 <0.25 <0.26 <0.21 0.84 -- -- -- --11/06/09 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 -- <0.50 <0.50 NS <0.50 <2.0 -- -- -- --02/11/101.1<0.50 <0.50 1.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 -- <0.50 <0.50 <0.50 <0.50 <0.50 -- -- -- --01/07/114.30.79 1.2 <0.50 <0.50 <0.50 <0.061 <0.50 <0.50 <0.023 0.94 0.63 <0.050 -- 2.1 <0.50 <0.50 <0.50 <0.50 -- -- -- --05/10/11 <1.4 320 120760<0.9550<3.1 <0.84 <0.52 <1.2 <1.4 33 <0.72 -- 300 94 <0.89 <2.6 <8.5 -- -- -- --10/19/11 0.13 J <0.17 <0.17 <0.17 <0.019 <0.17 <0.061 <0.017 <0.010 <0.023 <0.029 <0.024 <0.014 -- <0.17 <0.17 <0.018 <0.052 <0.17 -- -- -- --07/20/12 <0.27 2.1 J <0.17 <0.17 <0.019 <0.17 <0.061 <0.017 <0.010 <0.023 <0.029 <0.024 <0.014 -- <0.17 <0.17 <0.018 <0.052 <0.17 ------ --02/07/13 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 -- <0.50 <0.50 NA <0.50 <2.0 -- -- -- --08/25/14 <0.079 <0.090 <0.092 <0.29 <0.090 <0.12 <0.089 <0.054 <0.084 <0.19 <0.11 <0.094 <0.080 <0.077 <0.18 <0.10 <0.12 <0.18 <3.2 <28 <0.16 <0.12 <0.1205/18/15 <0.079 <0.090 <0.092 <0.29 <0.090 <0.12 <0.089 <0.054 <0.084 <0.19 <0.11 <0.094 <0.080 <0.077 <0.18 <0.10 <0.12 <0.18 <3.2 <28 <0.16 <0.12 <0.1202/15/16 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <50 <1.0 <0.50 <0.5008/22/17Not Sampled - Obstruction - Well Not Accessible09/03/19 0.16 J <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <100 <0.50 <0.50 <0.5003/18/21Not Sampled - Could Not Locate04/15/08226 1,790 866 4,160<1.047.3 0.952.92 NS NS 43.996.5NS --517119 6.37 NS NS -- -- -- --05/21/091,900 14,000 3,000 19,000<76.0 <78.055.9<40.0 <48.0 NS110 370<72.0 --1,700 410<0.26 <0.21 <110.0 -- <66 NS <11011/06/091,170 11,700 3,110 16,710<5.0160 16.8<5.0 <5.014.8 98.1 250<5.0 --1,510373 NS <5.0 <20.0 -- <5.0 <5.0 <5.002/11/101,900 19,000 4,500 25,000<25.0250 94<25.0 <25.0 <25.0170 450<25.0 --3,000 810 43<25.0 <25.0 -- <25.0 <25.0 <25.001/07/111,500 14,000 4,600 24,800<50.0270 6125 J <50.0 <2.3180 520<1.4 --2,900 760<5.2 <50.0 <17.0 -- <5.4 <1.3 <3305/10/111,300 4,900 2,800 10,000<0.019150 9921 <0.01079 110 340<0.014 --1,300380 3.6 5.3 <0.17 -- 1.25.02.110/19/111,200 10,000 3,700 19,000<1.9180 18 J33 J <1.025 J 130 350<1.4 --2,000 550<1.8 <5.2 <17 -- <5.4 <1.3 <3307/20/121,200 9,700 4,800 25,700<1.9260 33 J<1.7 <1.0 <2.3180 460<1.4 --2,700 710<1.8 <5.2 <17 -- <5.4 <1.3 <3302/07/13471 4,080 3,380 18,810<50.0364<50.0 <50.0 <50.0 <50.0252 292<50.0 --1,910 443NA <50.0 <200 -- <50.0 <50.0 <50.008/25/14750 8,800 4,700 26,500<18290<18 <11 <17 <39160 400<16 <153,100 830<25 <36 <640 <5,600 <32 <25 <2405/18/15520 3,300 4,800 23,000<9.0 <12 <8.9 39 J 14 J <19180 470<8.0 <7.73,000 700<12 <18 <320 <2,800 <16 <12 <1202/15/16540 2,200 2,400 18,400<25170<25 24 J 7.5 J <2592 220<25 <252,000 5407.5 J <25 <250 <2,500 <25 <25 <2508/22/17550 2,100 1,100 16,100<50120 30<50 <50 <200 47 97 <50 <501,500 490<50 <50 <500 <5,000 <200 <50 <5009/03/19978 11,100 2,920 18,700<130182 87.7 J<130 <13052.3 J 90.9 J 286<130 <1302,650 776<130 <130 <500 <25,000 <130 <130 <13003/18/21860 9,360 2,320 13,800<42.2283 121<49.0 <40.052.6 133<34.0 <29.2 <38.32,550<33.2 NA <30.8 <195 NA <36.7 <22.5 <26.107/25/23361 7,480 3,230 17,230<2.7371<7.4 <3.3 <4.3 <5.3190 498<4.3 <8.63,210 858NA <3.6 <94.5 <252 <2.8 <3.7 <8.6MW-3MW-4Page 2 of 3
TABLE 7HISTORICAL MONITORING WELL ANALYTICAL RESULTSDOT'S PLACE TOO1484 Mecklenburg HighwayMount Mourne, Iredell County, North CarolinaNCDEQ Incident #36185Well IDSampleDateBenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthalene1,2-Dibromoethane (EDB)n-Butylbenzenesec-Butylbenzene1,2-DichloroethaneIsopropylbenzenen-propylbenzeneTetrachloroetheneTrichloroethene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenep-IsopropyltolueneIsopropyl EtherMethylene ChlorideEthanol1,1-Dichloroethane1,1,2,2-Tetrachloroethane1,2,3-Trichloropropane2L Standard 1 600 600 500 20 6 0.02 70 70 0.04 70 70 0.7 3.0 400 400 25 70 5 4,000 6 0.2 0.005GCL Standard 5,000260,00080,00050,00020,0006,000505,9008,80040025,00026,1007003,00028,50024,10011,70070,0005,0004,000,0006,000200NE02/11/10590 5,100 4,200 23,600<25.0280<25.0 <25.0 <25.0 <25.0240 720<25.0 --3,800 980<25.0 <25.0 <25.0 -- <25.0 <0.50 <25.001/07/11270 3,100 2,400 13,900<50.0140 15 J<50.0 <50.028 J 130 360<1.4 --2,300 650<50.0 <50.0 <17.0 -- <5.4 <1.3 <3005/10/11250 1,900 1,600 5,700<0.019110 17<0.17 14 <0.023180 420<0.014 --1,200 68012 <0.052 <0.17 -- <0.094 <0.013 <0.3310/19/11530 6,200 3,400 19,400<1.9210 38 J43 J <1.073 160 500<1.4 --2,900 800<1.8 <5.2 <17 -- <5.4 <1.3 <3307/20/12560 4,900 2,900 15,400<0.95210 6551 16 J84 150 390<0.72 --2,300 6809.0 J <2.6 <8.5 -- <4.7 <0.65 <1702/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/25/1476 1,100 1,100 6,500<9.0100<8.9 12 J 11 J <1976 200<8.0 <7.71,500400 <12 <18 <320 <2,800 <16 <12 <1205/18/155.9140 2001,270<0.90 <1.2 <0.89 <0.54 4.3 J <1.9 2273<0.80 <0.77510180 4.6 J <1.8 <32 <500 <1.6 <1.2 <1.202/15/1662700 29016,400<50210<50 63 <50 <50 32 J77<50 <503,500 96016 J <50 <500 <5,000 <100 <50 <5008/22/177.0130 977,400<2572<25 <25 <25 <100 6.5 8.0 <25 <251,400 740<25 <25 <250 <2,500 <25 <25 <5009/03/197.9 J28.3 2831,890<1015.7<10 <10 <10 <10 12.7 38.9 <10 <10484140 <10 <10 <40 <2,000 <10 <10 <1003/18/2167.9249680 4,0408.068.7 5.8<4.9 <4.07.750.5 <3.4 <2.9 <3.81,070<3.3 NA <3.1 <19.5 NA <3.7 <2.2 <2.607/25/2314.555.2 3691,716<0.05340.6 0.37J<0.066 <0.0851.035.381.2<0.086 <0.17770<0.71 NA <0.072 <1.9 <5.0 <0.056 <0.074 <0.1703/18/21 <4.3 33.6 4681,260<5.344.2<3.4 <6.1 <5.0 <4.090.2<4.2 <3.6 <4.81,520 459NA <3.8 <24.4 NA <4.6 <2.8 <3.307/25/2327.9137947 2,910<1.1104<2.9 <1.3 <1.7 <2.1140 444<1.7 <3.42,570 784NA <1.4 <37.8 <101 <1.1 <1.5 <3.5Notes:Concentrations are reported in micrograms per liter (µg/L).GCL = Gross Contamination Level2L Standard = 15A NCAC 2L .0202 Groundwater Quality StandardsJ = Estimated valueNA = Not AnalyzedNE = Not EstablishedNS = Not SampledValues in BOLD exceed 2L StandardsValues In UNDERLINED AND BOLD text exceed GCL standards. -- = No analytical data reported for constituentSample results for MW-5 on July 25, 2023 reported as the laboratory WSW-8 results due to presumed swapping of sample identifications by the laboratoryMW-6MW-5Page 3 of 3

FIGURES
REFERENCE: USGS 7.5-MINUTE MAP, MOORESVILLE, NORTH
CAROLINA. DATED 1993
LATITUDE:ƒ1257+
LONGITUDE:ƒ:(67
SITE
CAD FILE PREP. BY REV. BY SCALE PROJECT NO.
TITLE
DATE
LB EG 05/06/2021 SLC3681501
500'1,000'LEGENDWATER SUPPLYWELL LOCATIONSource: NC GeospatialDatabaseWSW-31477 Mecklenburg HighwaySITEWSW-8117 Faith RoadWSW-41478 Mecklenburg HighwayWSW-6Vacant Parcel - Well AbandonedWSW-51493/1495 Mecklenburg HighwayWSW-21488 Mecklenburg HighwayWSW-91467 Mecklenburg HighwayASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE
S:\Administrative\ATC RETURNS!\ATC Logo - 2015\ATC Logo_Full Color_CMYK.jpgWSW-SITE
MW-1RMW-4MW-3MW-2MW-5FORMER DOT'S PLACE TOORESIDENCERESIDENCEEDGE OF PAVEMENTFORMER DOT'S PLACE TOOEDGE OF PAVEMENTMW-6MECKLE
N
B
U
R
G

H
I
G
H
W
A
YFORMER UST BASINFORMER UST BASINDW-1LEGENDMONITORING WELLLOCATIONPROPERTY BOUNDARYWATER SUPPLY WELL LOCATIONSource: GOOGLEEARTH PROCAD FILE
ASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE WSW-SITE
MW-1RMW-4MW-3MW-2MW-5FORMER DOT'S PLACE TOORESIDENCERESIDENCEEDGE OF PAVEMENTMW-2FORMER DOT'S PLACE TOOEDGE OF PAVEMENTMW-6MECKLE
N
B
U
R
G

H
I
G
H
W
A
YFORMER UST BASINFORMER UST BASINDW-1MW-3LEGEND69.39NRNOT REQUIREDMONITORING WELL LOCATIONPROPERTYBOUNDARYGROUNDWATER ELEVATIONGROUNDWATER ELEVATION CONTOUR LINE (DASHED WHERE INFERRED)GROUNDWATER DIRECTIONAL FLOWCAD FILE MW-3RESIDENCERESIDENCEASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE NR69.50
Source: GOOGLEEARTH PROGROUNDWATER ELEVATIONA MEASURED ON
07/25/2023
1.NR69.3969.8569.4669.7
5
70.25
70.00
69.75
69.50
70.49[69.90]
MW-1RMW-4MW-3MW-2MW-5FORMER DOT'S PLACE TOORESIDENCERESIDENCEEDGE OF PAVEMENTMW-2FORMER DOT'S PLACE TOOEDGE OF PAVEMENTMW-6MECKLE
N
B
U
R
G

H
I
G
H
W
A
YFORMER UST BASINFORMER UST BASINDW-1MW-3LEGENDMONITORING WELLLOCATIONISOCONCENTRATIONCONTOUR LINE (DASHEDWHERE INFERRED)PROPERTYBOUNDARYBENZENEISOCONCENTRATIONNOT REQUIREDNOT USED INCONTOURINGCAD FILERESIDENCE RESIDENCEASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE NR14.50Source: GOOGLEEARTH PROGROUNDWATER SAMPLES TAKEN 07/25/20231.NR361NR10 µg/L1 µg/L[<0.079][0.079]1,000 µg/L1,68027.9361100 µg/L
MW-1RMW-4MW-3MW-2MW-5FORMER DOT'S PLACE TOORESIDENCERESIDENCEEDGE OF PAVEMENTMW-2FORMER DOT'S PLACE TOOEDGE OF PAVEMENTMW-6MECKLE
N
B
U
R
G

H
I
G
H
W
A
YFORMER UST BASINFORMER UST BASINDW-1MW-3LEGENDMONITORING WELLLOCATIONISOCONCENTRATIONCONTOUR LINE (DASHEDWHERE INFERRED)PROPERTYBOUNDARYEDB ISOCONCENTRATIONNOT REQUIREDNOT USED INCONTOURINGCAD FILERESIDENCE RESIDENCEASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE NR<0.37JSource: GOOGLEEARTH PROGROUNDWATER SAMPLES TAKEN 07/25/20231.
2.NR209NR200 µg/L[<0.15]20.0 µg/L0.2 µg/L2.0 µg/L0.02 µg/L<7.4<2.9[<0.15]209
MW-1RMW-4MW-3MW-2MW-5FORMER DOT'S PLACE TOORESIDENCERESIDENCEEDGE OF PAVEMENTMW-2FORMER DOT'S PLACE TOOEDGE OF PAVEMENTMW-6MECKLE
N
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U
R
G

H
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G
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A
YFORMER UST BASINFORMER UST BASINDW-1MW-3LEGENDMONITORING WELLLOCATIONPROPERTYBOUNDARYNOT REQUIREDCAD FILERESIDENCE RESIDENCEASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE NRSource: GOOGLEEARTH PROGROUNDWATER SAMPLES TAKEN 07/25/20231.NRNR

APPENDIX A
CONCEPTUAL SITE MODEL

Site Name: Dot's Place Too Date:9/5/2023
Property Owner: Grant William Bolmer Jr. Last Field Event Date:8/4/2023
Site Name: Dot's Place Too Release Discovery Date: October 2006
NCDEQ UST Incident No.: 36185 Source of Release: Leaking UST System
Facility ID No.: Unknown Estimated Volume of Release: Unknown
Risk Classification: High
Risk Rank:0330D Gasoline (leaded)Yes
Site Address:1484 Mecklenburg Highway Gasoline (unleaded)No
Site City, ST ZIP:Mount Mourne Gasoline (ethanol blend)No
Site County:Iredell Diesel No
NCDEQ Regional Office:Mooresville Regional Office Kerosene No
Active UST Facility:No Heating Oil (#2)No
USTs Present:No Heating Oil (>#2)No
Motor Oil No
Hydraulic Oil Yes
Major Soil Type:Silt Used Oil No
Surface Cover over impacted soil: Unpaved soil
Utilities within plume (Y/N/U): U
>S‐W MSCCs (Y/N/U):Y
>Residential MSCCs (Y/N/U): N Site (Current):Landscaping Business
>Comm/Ind MSCCs (Y/N/U): N Site (Future):Landscaping Business
North Adjacent:Residential and agricultural
East Adjacent:Railroad and residential
Litho‐Tectonic Zone Charlotte Belt South Adjacent:Residential
Geologic Formation Unknown West Adjacent:Residential and agricultural
Rock Type Granite
Depth to Bedrock (ft bgs)~55 feet bgs Municipal Water (Y/N/U):Available
Active Potable Wells <1000 ft (#/U): 24
Active Potable Wells <500 ft (#/U): 4
Depth to water (ft‐bgs)Historically ~22 to 35 Impacted Wells (Y/N/U):N
Gradient (ft/ft):0.011 (SE) Any wells <250 ft (Y/N/U): WSW‐2 located on site
Direction (N E S W combo):Southeast (and partially) West
Hydraulic Conductivity (ft/day): Unknown <500 ft (Y/N):N
Total Porosity (%):Unknown Type of Surface Water:intermittent stream
Effective Porosity (%):Unknown Name of Nearest Stream:NA
Flow Rate (ft/year):Unknown Stream Classification:NA
COCs >2L (Y/N/U):Y Impacted Surface Water (Y/N/U): U
COCs >2L Extent Defined (Y/N): N ‐ >2L downgradient in MW‐5
COCs >GCLs (Y/N/U):Y
COCs >GCLs (Wells):MW‐1R (EDB)>LEL in Structures:Unknown
COCs >GCLs Extent Defined (Y/N): Y Vapors in Buildings:Unknown
COCs >2B Standards by 10X (Y/N/U): Yes Slab‐on‐grade or Crawlspace: Unknown
LNAPL (Y/N/U):N Dissolved VOCs <5 ft of Structures: Unknown
LNAPL (Max Thickness ft):NA LNAPL <15 ft of Structures:No
LNAPL (Wells):NA Basement <30 ft of Dissolved COCs: Unknown
LNAPL Extent Defined (Y/N): NA
LNAPL (<5 ft beneath buildings/U): NA
Utilities within plume (Y/N/U): Unknown
Alternative Water Source:Municipal water to WSW users
NORP:NA
Site Remediation:NA
Soil Excavation:NA
AFVR:NA
MMPE:NA
SVE/AS:NA
Other:NA
CONCEPTUAL SITE MODEL 
Soil Information
Possible Path(s) to Closure
Site Information Release Information
Petroleum Type Released
Geologic Information
Groundwater Information
Comments:
Receptor Information
Water Supply
Vapor
Additional Support Documentation Available / Data Gaps:
qHRSC if chemical injection pursued. Water supply well connection agreements to 
WSW users needed for all <500 feet to pursue this option. Fate & Transport 
modeling to evaluate potential impact to other WSWs >500 feet for consideration 
of an NFA.
Approach (general discussion): Address GCLs in groundwater
Surface Water
Land Use / Zoning
EDB > GCLS, multiple VOCs > 2L, multiple water supply wells within 500 feet. 
Additional assessment for chemical injection, or combined MMPE/AS event to 
reduce VOCs <GCLs and connection WSW users <500 feet to muncipal water. 
Possible replacement irrigation well on‐site.
Page 1 of 1

APPENDIX B
FIELD NOTES AND PHOTOGRAPHS
Proje t ·
{J
Dot’s Place Too July 2023
NCDEQ Incident No. 36185 ATC Project No. STL3618501

Photo 1: DMW-1. Photo 2 MW-1R.

Photo 3: MW-5. Photo 4: MW-4.

Photo 5: Sampling Point WSW-8. .

APPENDIX C
LABORATORY ANALYTICAL REPORTS

#=CL#
August 02, 2023
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92679292
92679292
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
DOT'S PLACE TOO MOUNT MOURNE N
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on July 26, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 38
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 38
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Lab ID Sample ID Matrix Date Collected Date Received
92679292001 MW-1R Water 07/25/23 09:40 07/26/23 06:00
92679292002 MW-4 Water 07/25/23 10:55 07/26/23 06:00
92679292003 MW-5 Water 07/25/23 11:35 07/26/23 06:00
92679292004 MW-6 Water 07/25/23 09:05 07/26/23 06:00
92679292005 DW-1 Water 07/25/23 10:19 07/26/23 06:00
92679292006 WSW-8 Water 07/25/23 11:50 07/26/23 06:00
92679292007 WSW-9 Water 07/25/23 12:05 07/26/23 06:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 38
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92679292001 MW-1R SM 6200B 69 PASI-CSAS
92679292002 MW-4 SM 6200B 69 PASI-CSAS
92679292003 MW-5 SM 6200B 69 PASI-CSAS
92679292004 MW-6 SM 6200B 69 PASI-CSAS
92679292005 DW-1 SM 6200B 69 PASI-CSAS
92679292006 WSW-8 SM 6200B 69 PASI-CSAS
92679292007 WSW-9 SM 6200B 69 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-1R Lab ID: 92679292001 Collected: 07/25/23 09:40 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <1490 ug/L 07/27/23 21:46 75-85-420000 1490 200
tert-Amylmethyl ether <24.8 ug/L 07/27/23 21:46 994-05-82000 24.8 200
Benzene 1680 ug/L 07/27/23 21:46 71-43-2100 15.7 200
Bromobenzene <27.0 ug/L 07/27/23 21:46 108-86-1100 27.0 200
Bromochloromethane <18.9 ug/L 07/27/23 21:46 74-97-5100 18.9 200
Bromodichloromethane <34.0 ug/L 07/27/23 21:46 75-27-4100 34.0 200
Bromoform <39.4 ug/L 07/27/23 21:46 75-25-2100 39.4 200
Bromomethane <44.4 ug/L 07/27/23 21:46 74-83-91000 44.4 200
tert-Butyl Alcohol <818 ug/L 07/27/23 21:46 75-65-010000 818 200
n-Butylbenzene <13.3 ug/L 07/27/23 21:46 104-51-8100 13.3 200
sec-Butylbenzene <17.0 ug/L 07/27/23 21:46 135-98-8100 17.0 200
tert-Butylbenzene <17.1 ug/L 07/27/23 21:46 98-06-6100 17.1 200
tert-Butyl Formate <60.0 ug/L 07/27/23 21:46 762-75-410000 60.0 200
Carbon tetrachloride <33.8 ug/L 07/27/23 21:46 56-23-5100 33.8 200
Chlorobenzene <16.9 ug/L 07/27/23 21:46 108-90-7100 16.9 200
Chloroethane <34.6 ug/L 07/27/23 21:46 75-00-3200 34.6 200
Chloroform <13.8 ug/L 07/27/23 21:46 67-66-3100 13.8 200
Chloromethane <35.0 ug/L 07/27/23 21:46 74-87-3200 35.0 200
2-Chlorotoluene <25.8 ug/L 07/27/23 21:46 95-49-8100 25.8 200
4-Chlorotoluene <19.1 ug/L 07/27/23 21:46 106-43-4100 19.1 200
1,2-Dibromo-3-chloropropane <35.8 ug/L 07/27/23 21:46 96-12-8200 35.8 200
Dibromochloromethane <29.6 ug/L 07/27/23 21:46 124-48-1100 29.6 200
1,2-Dibromoethane (EDB)209 ug/L 07/27/23 21:46 106-93-4100 29.4 200
Dibromomethane <37.4 ug/L 07/27/23 21:46 74-95-3100 37.4 200
1,2-Dichlorobenzene <18.8 ug/L 07/27/23 21:46 95-50-1100 18.8 200
1,3-Dichlorobenzene <19.6 ug/L 07/27/23 21:46 541-73-1100 19.6 200
1,4-Dichlorobenzene <17.9 ug/L 07/27/23 21:46 106-46-7100 17.9 200
Dichlorodifluoromethane <24.6 ug/L 07/27/23 21:46 75-71-8100 24.6 200
1,1-Dichloroethane <11.2 ug/L 07/27/23 21:46 75-34-3100 11.2 200
1,2-Dichloroethane <21.2 ug/L 07/27/23 21:46 107-06-2100 21.2 200
1,1-Dichloroethene <15.7 ug/L 07/27/23 21:46 75-35-4100 15.7 200
cis-1,2-Dichloroethene <22.2 ug/L 07/27/23 21:46 156-59-2100 22.2 200
trans-1,2-Dichloroethene <20.2 ug/L 07/27/23 21:46 156-60-5100 20.2 200
1,2-Dichloropropane <27.2 ug/L 07/27/23 21:46 78-87-5100 27.2 200
1,3-Dichloropropane <17.1 ug/L 07/27/23 21:46 142-28-9100 17.1 200
2,2-Dichloropropane <24.4 ug/L 07/27/23 21:46 594-20-7100 24.4 200
1,1-Dichloropropene <13.2 ug/L 07/27/23 21:46 563-58-6100 13.2 200
cis-1,3-Dichloropropene <17.9 ug/L 07/27/23 21:46 10061-01-5100 17.9 200
trans-1,3-Dichloropropene <26.4 ug/L 07/27/23 21:46 10061-02-6100 26.4 200
Diisopropyl ether <14.5 ug/L 07/27/23 21:46 108-20-3100 14.5 200
Ethanol <1010 ug/L 07/27/23 21:46 64-17-540000 1010 200
Ethylbenzene 2210 ug/L 07/27/23 21:46 100-41-4100 16.2 200
Ethyl-tert-butyl ether <22.4 ug/L 07/27/23 21:46 637-92-32000 22.4 200
Hexachloro-1,3-butadiene <70.2 ug/L 07/27/23 21:46 87-68-3400 70.2 200
Isopropylbenzene (Cumene)72.2J ug/L 07/27/23 21:46 98-82-8100 21.2 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-1R Lab ID: 92679292001 Collected: 07/25/23 09:40 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <378 ug/L 07/27/23 21:46 75-09-2400 378 200
Methyl-tert-butyl ether <10.7 ug/L 07/27/23 21:46 1634-04-4100 10.7 200
Naphthalene 484 ug/L 07/27/23 21:46 91-20-3400 20.2 200
n-Propylbenzene 134 ug/L 07/27/23 21:46 103-65-1100 21.0 200
Styrene <27.4 ug/L 07/27/23 21:46 100-42-5100 27.4 200
1,1,1,2-Tetrachloroethane <18.2 ug/L 07/27/23 21:46 630-20-6100 18.2 200
1,1,2,2-Tetrachloroethane <14.8 ug/L 07/27/23 21:46 79-34-5100 14.8 200
Tetrachloroethene <17.1 ug/L 07/27/23 21:46 127-18-4100 17.1 200
Toluene 35400 ug/L 07/27/23 21:46 108-88-3100 18.0 200
1,2,3-Trichlorobenzene <24.2 ug/L 07/27/23 21:46 87-61-6400 24.2 200
1,2,4-Trichlorobenzene <31.2 ug/L 07/27/23 21:46 120-82-1400 31.2 200
1,1,1-Trichloroethane <21.4 ug/L 07/27/23 21:46 71-55-6100 21.4 200
1,1,2-Trichloroethane <19.1 ug/L 07/27/23 21:46 79-00-5100 19.1 200
Trichloroethene <34.2 ug/L 07/27/23 21:46 79-01-6100 34.2 200
Trichlorofluoromethane <28.8 ug/L 07/27/23 21:46 75-69-4200 28.8 200
1,2,3-Trichloropropane <34.6 ug/L 07/27/23 21:46 96-18-4100 34.6 200
1,2,4-Trimethylbenzene 2770 ug/L 07/27/23 21:46 95-63-6100 6.1 200
1,3,5-Trimethylbenzene 714 ug/L 07/27/23 21:46 108-67-8100 14.3 200
Vinyl chloride <29.8 ug/L 07/27/23 21:46 75-01-4200 29.8 200
m&p-Xylene 15900 ug/L 07/27/23 21:46 179601-23-1200 18.7 200
o-Xylene 7750 ug/L 07/27/23 21:46 95-47-6100 28.8 200
Surrogates
1,2-Dichloroethane-d4 (S)99 %07/27/23 21:46 17060-07-070-130 200
4-Bromofluorobenzene (S)90 %07/27/23 21:46 460-00-470-130 200
Toluene-d8 (S)100 %07/27/23 21:46 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-4 Lab ID: 92679292002 Collected: 07/25/23 10:55 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <372 ug/L 07/28/23 17:06 75-85-45000 372 50
tert-Amylmethyl ether <6.2 ug/L 07/28/23 17:06 994-05-8500 6.2 50
Benzene 361 ug/L 07/28/23 17:06 71-43-225.0 3.9 50
Bromobenzene <6.8 ug/L 07/28/23 17:06 108-86-125.0 6.8 50
Bromochloromethane <4.7 ug/L 07/28/23 17:06 74-97-525.0 4.7 50
Bromodichloromethane <8.5 ug/L 07/28/23 17:06 75-27-425.0 8.5 50
Bromoform <9.8 ug/L 07/28/23 17:06 75-25-225.0 9.8 50
Bromomethane <11.1 ug/L 07/28/23 17:06 74-83-9250 11.1 50
tert-Butyl Alcohol <204 ug/L 07/28/23 17:06 75-65-02500 204 50
n-Butylbenzene <3.3 ug/L 07/28/23 17:06 104-51-825.0 3.3 50
sec-Butylbenzene <4.3 ug/L 07/28/23 17:06 135-98-825.0 4.3 50
tert-Butylbenzene <4.3 ug/L 07/28/23 17:06 98-06-625.0 4.3 50
tert-Butyl Formate <15.0 ug/L 07/28/23 17:06 762-75-42500 15.0 50
Carbon tetrachloride <8.4 ug/L 07/28/23 17:06 56-23-525.0 8.4 50
Chlorobenzene <4.2 ug/L 07/28/23 17:06 108-90-725.0 4.2 50
Chloroethane <8.6 ug/L 07/28/23 17:06 75-00-350.0 8.6 50
Chloroform <3.5 ug/L 07/28/23 17:06 67-66-325.0 3.5 50
Chloromethane <8.8 ug/L 07/28/23 17:06 74-87-350.0 8.8 50
2-Chlorotoluene <6.4 ug/L 07/28/23 17:06 95-49-825.0 6.4 50
4-Chlorotoluene <4.8 ug/L 07/28/23 17:06 106-43-425.0 4.8 50
1,2-Dibromo-3-chloropropane <9.0 ug/L 07/28/23 17:06 96-12-850.0 9.0 50
Dibromochloromethane <7.4 ug/L 07/28/23 17:06 124-48-125.0 7.4 50
1,2-Dibromoethane (EDB)<7.4 ug/L 07/28/23 17:06 106-93-425.0 7.4 50
Dibromomethane <9.4 ug/L 07/28/23 17:06 74-95-325.0 9.4 50
1,2-Dichlorobenzene <4.7 ug/L 07/28/23 17:06 95-50-125.0 4.7 50
1,3-Dichlorobenzene <4.9 ug/L 07/28/23 17:06 541-73-125.0 4.9 50
1,4-Dichlorobenzene <4.5 ug/L 07/28/23 17:06 106-46-725.0 4.5 50
Dichlorodifluoromethane <6.2 ug/L 07/28/23 17:06 75-71-825.0 6.2 50
1,1-Dichloroethane <2.8 ug/L 07/28/23 17:06 75-34-325.0 2.8 50
1,2-Dichloroethane <5.3 ug/L 07/28/23 17:06 107-06-225.0 5.3 50
1,1-Dichloroethene <3.9 ug/L 07/28/23 17:06 75-35-425.0 3.9 50
cis-1,2-Dichloroethene <5.6 ug/L 07/28/23 17:06 156-59-225.0 5.6 50
trans-1,2-Dichloroethene <5.0 ug/L 07/28/23 17:06 156-60-525.0 5.0 50
1,2-Dichloropropane <6.8 ug/L 07/28/23 17:06 78-87-525.0 6.8 50
1,3-Dichloropropane <4.3 ug/L 07/28/23 17:06 142-28-925.0 4.3 50
2,2-Dichloropropane <6.1 ug/L 07/28/23 17:06 594-20-725.0 6.1 50
1,1-Dichloropropene <3.3 ug/L 07/28/23 17:06 563-58-625.0 3.3 50
cis-1,3-Dichloropropene <4.5 ug/L 07/28/23 17:06 10061-01-525.0 4.5 50
trans-1,3-Dichloropropene <6.6 ug/L 07/28/23 17:06 10061-02-625.0 6.6 50
Diisopropyl ether <3.6 ug/L 07/28/23 17:06 108-20-325.0 3.6 50
Ethanol <252 ug/L 07/28/23 17:06 64-17-510000 252 50
Ethylbenzene 3230 ug/L 07/28/23 17:06 100-41-425.0 4.1 50
Ethyl-tert-butyl ether <5.6 ug/L 07/28/23 17:06 637-92-3500 5.6 50
Hexachloro-1,3-butadiene <17.6 ug/L 07/28/23 17:06 87-68-3100 17.6 50
Isopropylbenzene (Cumene)190 ug/L 07/28/23 17:06 98-82-825.0 5.3 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-4 Lab ID: 92679292002 Collected: 07/25/23 10:55 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <94.5 ug/L 07/28/23 17:06 75-09-2100 94.5 50
Methyl-tert-butyl ether <2.7 ug/L 07/28/23 17:06 1634-04-425.0 2.7 50
Naphthalene 371 ug/L 07/28/23 17:06 91-20-3100 5.0 50
n-Propylbenzene 498 ug/L 07/28/23 17:06 103-65-125.0 5.2 50
Styrene <6.8 ug/L 07/28/23 17:06 100-42-525.0 6.8 50
1,1,1,2-Tetrachloroethane <4.6 ug/L 07/28/23 17:06 630-20-625.0 4.6 50
1,1,2,2-Tetrachloroethane <3.7 ug/L 07/28/23 17:06 79-34-525.0 3.7 50
Tetrachloroethene <4.3 ug/L 07/28/23 17:06 127-18-425.0 4.3 50
Toluene 7480 ug/L 07/28/23 17:06 108-88-325.0 4.5 50
1,2,3-Trichlorobenzene <6.0 ug/L 07/28/23 17:06 87-61-6100 6.0 50
1,2,4-Trichlorobenzene <7.8 ug/L 07/28/23 17:06 120-82-1100 7.8 50
1,1,1-Trichloroethane <5.4 ug/L 07/28/23 17:06 71-55-625.0 5.4 50
1,1,2-Trichloroethane <4.8 ug/L 07/28/23 17:06 79-00-525.0 4.8 50
Trichloroethene <8.6 ug/L 07/28/23 17:06 79-01-625.0 8.6 50
Trichlorofluoromethane <7.2 ug/L 07/28/23 17:06 75-69-450.0 7.2 50
1,2,3-Trichloropropane <8.6 ug/L 07/28/23 17:06 96-18-425.0 8.6 50
1,2,4-Trimethylbenzene 3210 ug/L 07/28/23 17:06 95-63-625.0 1.5 50
1,3,5-Trimethylbenzene 858 ug/L 07/28/23 17:06 108-67-825.0 3.6 50
Vinyl chloride <7.4 ug/L 07/28/23 17:06 75-01-450.0 7.4 50
m&p-Xylene 12300 ug/L 07/28/23 17:06 179601-23-150.0 4.7 50
o-Xylene 4930 ug/L 07/28/23 17:06 95-47-625.0 7.2 50
Surrogates
1,2-Dichloroethane-d4 (S)97 %07/28/23 17:06 17060-07-070-130 50
4-Bromofluorobenzene (S)95 %07/28/23 17:06 460-00-470-130 50
Toluene-d8 (S)95 %07/28/23 17:06 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-5 Lab ID: 92679292003 Collected: 07/25/23 11:35 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <7.4 ug/L 07/28/23 15:53 75-85-4100 7.4 1
tert-Amylmethyl ether <0.12 ug/L 07/28/23 15:53 994-05-810.0 0.12 1
Benzene <0.079 ug/L 07/28/23 15:53 71-43-20.50 0.079 1
Bromobenzene <0.14 ug/L 07/28/23 15:53 108-86-10.50 0.14 1
Bromochloromethane <0.094 ug/L 07/28/23 15:53 74-97-50.50 0.094 1
Bromodichloromethane <0.17 ug/L 07/28/23 15:53 75-27-40.50 0.17 1
Bromoform <0.20 ug/L 07/28/23 15:53 75-25-20.50 0.20 1
Bromomethane <0.22 ug/L 07/28/23 15:53 74-83-95.0 0.22 1
tert-Butyl Alcohol <4.1 ug/L 07/28/23 15:53 75-65-050.0 4.1 1
n-Butylbenzene <0.066 ug/L 07/28/23 15:53 104-51-80.50 0.066 1
sec-Butylbenzene <0.085 ug/L 07/28/23 15:53 135-98-80.50 0.085 1
tert-Butylbenzene <0.086 ug/L 07/28/23 15:53 98-06-60.50 0.086 1
tert-Butyl Formate <0.30 ug/L 07/28/23 15:53 762-75-450.0 0.30 1
Carbon tetrachloride <0.17 ug/L 07/28/23 15:53 56-23-50.50 0.17 1
Chlorobenzene <0.085 ug/L 07/28/23 15:53 108-90-70.50 0.085 1
Chloroethane <0.17 ug/L 07/28/23 15:53 75-00-31.0 0.17 1
Chloroform <0.069 ug/L 07/28/23 15:53 67-66-30.50 0.069 1
Chloromethane 0.18J ug/L 07/28/23 15:53 74-87-31.0 0.18 1
2-Chlorotoluene <0.13 ug/L 07/28/23 15:53 95-49-80.50 0.13 1
4-Chlorotoluene <0.096 ug/L 07/28/23 15:53 106-43-40.50 0.096 1
1,2-Dibromo-3-chloropropane <0.18 ug/L 07/28/23 15:53 96-12-81.0 0.18 1
Dibromochloromethane <0.15 ug/L 07/28/23 15:53 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)<0.15 ug/L 07/28/23 15:53 106-93-40.50 0.15 1
Dibromomethane <0.19 ug/L 07/28/23 15:53 74-95-30.50 0.19 1
1,2-Dichlorobenzene <0.094 ug/L 07/28/23 15:53 95-50-10.50 0.094 1
1,3-Dichlorobenzene <0.098 ug/L 07/28/23 15:53 541-73-10.50 0.098 1
1,4-Dichlorobenzene <0.090 ug/L 07/28/23 15:53 106-46-70.50 0.090 1
Dichlorodifluoromethane <0.12 ug/L 07/28/23 15:53 75-71-80.50 0.12 1
1,1-Dichloroethane <0.056 ug/L 07/28/23 15:53 75-34-30.50 0.056 1
1,2-Dichloroethane <0.11 ug/L 07/28/23 15:53 107-06-20.50 0.11 1
1,1-Dichloroethene <0.079 ug/L 07/28/23 15:53 75-35-40.50 0.079 1
cis-1,2-Dichloroethene <0.11 ug/L 07/28/23 15:53 156-59-20.50 0.11 1
trans-1,2-Dichloroethene <0.10 ug/L 07/28/23 15:53 156-60-50.50 0.10 1
1,2-Dichloropropane <0.14 ug/L 07/28/23 15:53 78-87-50.50 0.14 1
1,3-Dichloropropane <0.085 ug/L 07/28/23 15:53 142-28-90.50 0.085 1
2,2-Dichloropropane <0.12 ug/L 07/28/23 15:53 594-20-70.50 0.12 1
1,1-Dichloropropene <0.066 ug/L 07/28/23 15:53 563-58-60.50 0.066 1
cis-1,3-Dichloropropene <0.090 ug/L 07/28/23 15:53 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene <0.13 ug/L 07/28/23 15:53 10061-02-60.50 0.13 1
Diisopropyl ether <0.072 ug/L 07/28/23 15:53 108-20-30.50 0.072 1
Ethanol <5.0 ug/L 07/28/23 15:53 64-17-5200 5.0 1
Ethylbenzene <0.081 ug/L 07/28/23 15:53 100-41-40.50 0.081 1
Ethyl-tert-butyl ether <0.11 ug/L 07/28/23 15:53 637-92-310.0 0.11 1
Hexachloro-1,3-butadiene <0.35 ug/L 07/28/23 15:53 87-68-32.0 0.35 1
Isopropylbenzene (Cumene)<0.11 ug/L 07/28/23 15:53 98-82-80.50 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-5 Lab ID: 92679292003 Collected: 07/25/23 11:35 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <1.9 ug/L 07/28/23 15:53 75-09-22.0 1.9 1
Methyl-tert-butyl ether <0.053 ug/L 07/28/23 15:53 1634-04-40.50 0.053 1
Naphthalene <0.10 ug/L 07/28/23 15:53 91-20-32.0 0.10 1
n-Propylbenzene <0.10 ug/L 07/28/23 15:53 103-65-10.50 0.10 1
Styrene <0.14 ug/L 07/28/23 15:53 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane <0.091 ug/L 07/28/23 15:53 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane <0.074 ug/L 07/28/23 15:53 79-34-50.50 0.074 1
Tetrachloroethene <0.086 ug/L 07/28/23 15:53 127-18-40.50 0.086 1
Toluene <0.090 ug/L 07/28/23 15:53 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene <0.12 ug/L 07/28/23 15:53 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene <0.16 ug/L 07/28/23 15:53 120-82-12.0 0.16 1
1,1,1-Trichloroethane <0.11 ug/L 07/28/23 15:53 71-55-60.50 0.11 1
1,1,2-Trichloroethane <0.096 ug/L 07/28/23 15:53 79-00-50.50 0.096 1
Trichloroethene <0.17 ug/L 07/28/23 15:53 79-01-60.50 0.17 1
Trichlorofluoromethane <0.14 ug/L 07/28/23 15:53 75-69-41.0 0.14 1
1,2,3-Trichloropropane <0.17 ug/L 07/28/23 15:53 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene <0.031 ug/L 07/28/23 15:53 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene <0.071 ug/L 07/28/23 15:53 108-67-80.50 0.071 1
Vinyl chloride <0.15 ug/L 07/28/23 15:53 75-01-41.0 0.15 1
m&p-Xylene <0.094 ug/L 07/28/23 15:53 179601-23-11.0 0.094 1
o-Xylene <0.14 ug/L 07/28/23 15:53 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %07/28/23 15:53 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %07/28/23 15:53 460-00-470-130 1
Toluene-d8 (S)96 %07/28/23 15:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-6 Lab ID: 92679292004 Collected: 07/25/23 09:05 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <149 ug/L 07/28/23 16:30 75-85-42000 149 20
tert-Amylmethyl ether <2.5 ug/L 07/28/23 16:30 994-05-8200 2.5 20
Benzene 27.9 ug/L 07/28/23 16:30 71-43-210.0 1.6 20
Bromobenzene <2.7 ug/L 07/28/23 16:30 108-86-110.0 2.7 20
Bromochloromethane <1.9 ug/L 07/28/23 16:30 74-97-510.0 1.9 20
Bromodichloromethane <3.4 ug/L 07/28/23 16:30 75-27-410.0 3.4 20
Bromoform <3.9 ug/L 07/28/23 16:30 75-25-210.0 3.9 20
Bromomethane <4.4 ug/L 07/28/23 16:30 74-83-9100 4.4 20
tert-Butyl Alcohol <81.8 ug/L 07/28/23 16:30 75-65-01000 81.8 20
n-Butylbenzene <1.3 ug/L 07/28/23 16:30 104-51-810.0 1.3 20
sec-Butylbenzene <1.7 ug/L 07/28/23 16:30 135-98-810.0 1.7 20
tert-Butylbenzene <1.7 ug/L 07/28/23 16:30 98-06-610.0 1.7 20
tert-Butyl Formate <6.0 ug/L 07/28/23 16:30 762-75-41000 6.0 20
Carbon tetrachloride <3.4 ug/L 07/28/23 16:30 56-23-510.0 3.4 20
Chlorobenzene <1.7 ug/L 07/28/23 16:30 108-90-710.0 1.7 20
Chloroethane <3.5 ug/L 07/28/23 16:30 75-00-320.0 3.5 20
Chloroform <1.4 ug/L 07/28/23 16:30 67-66-310.0 1.4 20
Chloromethane <3.5 ug/L 07/28/23 16:30 74-87-320.0 3.5 20
2-Chlorotoluene <2.6 ug/L 07/28/23 16:30 95-49-810.0 2.6 20
4-Chlorotoluene <1.9 ug/L 07/28/23 16:30 106-43-410.0 1.9 20
1,2-Dibromo-3-chloropropane <3.6 ug/L 07/28/23 16:30 96-12-820.0 3.6 20
Dibromochloromethane <3.0 ug/L 07/28/23 16:30 124-48-110.0 3.0 20
1,2-Dibromoethane (EDB)<2.9 ug/L 07/28/23 16:30 106-93-410.0 2.9 20
Dibromomethane <3.7 ug/L 07/28/23 16:30 74-95-310.0 3.7 20
1,2-Dichlorobenzene <1.9 ug/L 07/28/23 16:30 95-50-110.0 1.9 20
1,3-Dichlorobenzene <2.0 ug/L 07/28/23 16:30 541-73-110.0 2.0 20
1,4-Dichlorobenzene <1.8 ug/L 07/28/23 16:30 106-46-710.0 1.8 20
Dichlorodifluoromethane <2.5 ug/L 07/28/23 16:30 75-71-810.0 2.5 20
1,1-Dichloroethane <1.1 ug/L 07/28/23 16:30 75-34-310.0 1.1 20
1,2-Dichloroethane <2.1 ug/L 07/28/23 16:30 107-06-210.0 2.1 20
1,1-Dichloroethene <1.6 ug/L 07/28/23 16:30 75-35-410.0 1.6 20
cis-1,2-Dichloroethene <2.2 ug/L 07/28/23 16:30 156-59-210.0 2.2 20
trans-1,2-Dichloroethene <2.0 ug/L 07/28/23 16:30 156-60-510.0 2.0 20
1,2-Dichloropropane <2.7 ug/L 07/28/23 16:30 78-87-510.0 2.7 20
1,3-Dichloropropane <1.7 ug/L 07/28/23 16:30 142-28-910.0 1.7 20
2,2-Dichloropropane <2.4 ug/L 07/28/23 16:30 594-20-710.0 2.4 20
1,1-Dichloropropene <1.3 ug/L 07/28/23 16:30 563-58-610.0 1.3 20
cis-1,3-Dichloropropene <1.8 ug/L 07/28/23 16:30 10061-01-510.0 1.8 20
trans-1,3-Dichloropropene <2.6 ug/L 07/28/23 16:30 10061-02-610.0 2.6 20
Diisopropyl ether <1.4 ug/L 07/28/23 16:30 108-20-310.0 1.4 20
Ethanol <101 ug/L 07/28/23 16:30 64-17-54000 101 20
Ethylbenzene 947 ug/L 07/28/23 16:30 100-41-410.0 1.6 20
Ethyl-tert-butyl ether <2.2 ug/L 07/28/23 16:30 637-92-3200 2.2 20
Hexachloro-1,3-butadiene <7.0 ug/L 07/28/23 16:30 87-68-340.0 7.0 20
Isopropylbenzene (Cumene)140 ug/L 07/28/23 16:30 98-82-810.0 2.1 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: MW-6 Lab ID: 92679292004 Collected: 07/25/23 09:05 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <37.8 ug/L 07/28/23 16:30 75-09-240.0 37.8 20
Methyl-tert-butyl ether <1.1 ug/L 07/28/23 16:30 1634-04-410.0 1.1 20
Naphthalene 104 ug/L 07/28/23 16:30 91-20-340.0 2.0 20
n-Propylbenzene 444 ug/L 07/28/23 16:30 103-65-110.0 2.1 20
Styrene <2.7 ug/L 07/28/23 16:30 100-42-510.0 2.7 20
1,1,1,2-Tetrachloroethane <1.8 ug/L 07/28/23 16:30 630-20-610.0 1.8 20
1,1,2,2-Tetrachloroethane <1.5 ug/L 07/28/23 16:30 79-34-510.0 1.5 20
Tetrachloroethene <1.7 ug/L 07/28/23 16:30 127-18-410.0 1.7 20
Toluene 137 ug/L 07/28/23 16:30 108-88-310.0 1.8 20
1,2,3-Trichlorobenzene <2.4 ug/L 07/28/23 16:30 87-61-640.0 2.4 20
1,2,4-Trichlorobenzene <3.1 ug/L 07/28/23 16:30 120-82-140.0 3.1 20
1,1,1-Trichloroethane <2.1 ug/L 07/28/23 16:30 71-55-610.0 2.1 20
1,1,2-Trichloroethane <1.9 ug/L 07/28/23 16:30 79-00-510.0 1.9 20
Trichloroethene <3.4 ug/L 07/28/23 16:30 79-01-610.0 3.4 20
Trichlorofluoromethane <2.9 ug/L 07/28/23 16:30 75-69-420.0 2.9 20
1,2,3-Trichloropropane <3.5 ug/L 07/28/23 16:30 96-18-410.0 3.5 20
1,2,4-Trimethylbenzene 2570 ug/L 07/28/23 16:30 95-63-610.0 0.61 20
1,3,5-Trimethylbenzene 784 ug/L 07/28/23 16:30 108-67-810.0 1.4 20
Vinyl chloride <3.0 ug/L 07/28/23 16:30 75-01-420.0 3.0 20
m&p-Xylene 2050 ug/L 07/28/23 16:30 179601-23-120.0 1.9 20
o-Xylene 860 ug/L 07/28/23 16:30 95-47-610.0 2.9 20
Surrogates
1,2-Dichloroethane-d4 (S)98 %07/28/23 16:30 17060-07-070-130 20
4-Bromofluorobenzene (S)95 %07/28/23 16:30 460-00-470-130 20
Toluene-d8 (S)95 %07/28/23 16:30 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: DW-1 Lab ID: 92679292005 Collected: 07/25/23 10:19 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <7.4 ug/L 07/31/23 15:57 75-85-4100 7.4 1
tert-Amylmethyl ether <0.12 ug/L 07/31/23 15:57 994-05-810.0 0.12 1
Benzene <0.079 ug/L 07/31/23 15:57 71-43-20.50 0.079 1
Bromobenzene <0.14 ug/L 07/31/23 15:57 108-86-10.50 0.14 1
Bromochloromethane <0.094 ug/L 07/31/23 15:57 74-97-50.50 0.094 1
Bromodichloromethane <0.17 ug/L 07/31/23 15:57 75-27-40.50 0.17 1
Bromoform <0.20 ug/L 07/31/23 15:57 75-25-20.50 0.20 1
Bromomethane <0.22 ug/L 07/31/23 15:57 74-83-95.0 0.22 1
tert-Butyl Alcohol <4.1 ug/L 07/31/23 15:57 75-65-050.0 4.1 1
n-Butylbenzene <0.066 ug/L 07/31/23 15:57 104-51-80.50 0.066 1
sec-Butylbenzene <0.085 ug/L 07/31/23 15:57 135-98-80.50 0.085 1
tert-Butylbenzene <0.086 ug/L 07/31/23 15:57 98-06-60.50 0.086 1
tert-Butyl Formate <0.30 ug/L 07/31/23 15:57 762-75-450.0 0.30 1
Carbon tetrachloride <0.17 ug/L 07/31/23 15:57 56-23-50.50 0.17 1
Chlorobenzene <0.085 ug/L 07/31/23 15:57 108-90-70.50 0.085 1
Chloroethane <0.17 ug/L 07/31/23 15:57 75-00-31.0 0.17 1
Chloroform 0.26J ug/L 07/31/23 15:57 67-66-30.50 0.069 1
Chloromethane <0.18 ug/L 07/31/23 15:57 74-87-31.0 0.18 1
2-Chlorotoluene <0.13 ug/L 07/31/23 15:57 95-49-80.50 0.13 1
4-Chlorotoluene <0.096 ug/L 07/31/23 15:57 106-43-40.50 0.096 1
1,2-Dibromo-3-chloropropane <0.18 ug/L 07/31/23 15:57 96-12-81.0 0.18 1
Dibromochloromethane <0.15 ug/L 07/31/23 15:57 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)<0.15 ug/L 07/31/23 15:57 106-93-40.50 0.15 1
Dibromomethane <0.19 ug/L 07/31/23 15:57 74-95-30.50 0.19 1
1,2-Dichlorobenzene <0.094 ug/L 07/31/23 15:57 95-50-10.50 0.094 1
1,3-Dichlorobenzene <0.098 ug/L 07/31/23 15:57 541-73-10.50 0.098 1
1,4-Dichlorobenzene <0.090 ug/L 07/31/23 15:57 106-46-70.50 0.090 1
Dichlorodifluoromethane <0.12 ug/L 07/31/23 15:57 75-71-80.50 0.12 1
1,1-Dichloroethane <0.056 ug/L 07/31/23 15:57 75-34-30.50 0.056 1
1,2-Dichloroethane <0.11 ug/L 07/31/23 15:57 107-06-20.50 0.11 1
1,1-Dichloroethene <0.079 ug/L 07/31/23 15:57 75-35-40.50 0.079 1
cis-1,2-Dichloroethene <0.11 ug/L 07/31/23 15:57 156-59-20.50 0.11 1
trans-1,2-Dichloroethene <0.10 ug/L 07/31/23 15:57 156-60-50.50 0.10 1
1,2-Dichloropropane <0.14 ug/L 07/31/23 15:57 78-87-50.50 0.14 1
1,3-Dichloropropane <0.085 ug/L 07/31/23 15:57 142-28-90.50 0.085 1
2,2-Dichloropropane <0.12 ug/L 07/31/23 15:57 594-20-70.50 0.12 1
1,1-Dichloropropene <0.066 ug/L 07/31/23 15:57 563-58-60.50 0.066 1
cis-1,3-Dichloropropene <0.090 ug/L 07/31/23 15:57 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene <0.13 ug/L 07/31/23 15:57 10061-02-60.50 0.13 1
Diisopropyl ether <0.072 ug/L 07/31/23 15:57 108-20-30.50 0.072 1
Ethanol <5.0 ug/L 07/31/23 15:57 64-17-5200 5.0 1
Ethylbenzene <0.081 ug/L 07/31/23 15:57 100-41-40.50 0.081 1
Ethyl-tert-butyl ether <0.11 ug/L 07/31/23 15:57 637-92-310.0 0.11 1
Hexachloro-1,3-butadiene <0.35 ug/L 07/31/23 15:57 87-68-32.0 0.35 1
Isopropylbenzene (Cumene)<0.11 ug/L 07/31/23 15:57 98-82-80.50 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: DW-1 Lab ID: 92679292005 Collected: 07/25/23 10:19 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <1.9 ug/L 07/31/23 15:57 75-09-22.0 1.9 1
Methyl-tert-butyl ether <0.053 ug/L 07/31/23 15:57 1634-04-40.50 0.053 1
Naphthalene <0.10 ug/L 07/31/23 15:57 91-20-32.0 0.10 1
n-Propylbenzene <0.10 ug/L 07/31/23 15:57 103-65-10.50 0.10 1
Styrene <0.14 ug/L 07/31/23 15:57 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane <0.091 ug/L 07/31/23 15:57 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane <0.074 ug/L 07/31/23 15:57 79-34-50.50 0.074 1
Tetrachloroethene <0.086 ug/L 07/31/23 15:57 127-18-40.50 0.086 1
Toluene <0.090 ug/L 07/31/23 15:57 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene <0.12 ug/L 07/31/23 15:57 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene <0.16 ug/L 07/31/23 15:57 120-82-12.0 0.16 1
1,1,1-Trichloroethane <0.11 ug/L 07/31/23 15:57 71-55-60.50 0.11 1
1,1,2-Trichloroethane <0.096 ug/L 07/31/23 15:57 79-00-50.50 0.096 1
Trichloroethene <0.17 ug/L 07/31/23 15:57 79-01-60.50 0.17 1
Trichlorofluoromethane <0.14 ug/L 07/31/23 15:57 75-69-41.0 0.14 1
1,2,3-Trichloropropane <0.17 ug/L 07/31/23 15:57 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene <0.031 ug/L 07/31/23 15:57 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene <0.071 ug/L 07/31/23 15:57 108-67-80.50 0.071 1
Vinyl chloride <0.15 ug/L 07/31/23 15:57 75-01-41.0 0.15 1
m&p-Xylene <0.094 ug/L 07/31/23 15:57 179601-23-11.0 0.094 1
o-Xylene <0.14 ug/L 07/31/23 15:57 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %07/31/23 15:57 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %07/31/23 15:57 460-00-470-130 1
Toluene-d8 (S)94 %07/31/23 15:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: WSW-8 Lab ID: 92679292006 Collected: 07/25/23 11:50 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol 50.8J ug/L 07/27/23 17:15 75-85-4100 7.4 1
tert-Amylmethyl ether <0.12 ug/L 07/27/23 17:15 994-05-810.0 0.12 1
Benzene 14.5 ug/L 07/27/23 17:15 71-43-20.50 0.079 1
Bromobenzene <0.14 ug/L 07/27/23 17:15 108-86-10.50 0.14 1
Bromochloromethane <0.094 ug/L 07/27/23 17:15 74-97-50.50 0.094 1
Bromodichloromethane <0.17 ug/L 07/27/23 17:15 75-27-40.50 0.17 1
Bromoform <0.20 ug/L 07/27/23 17:15 75-25-20.50 0.20 1
Bromomethane <0.22 ug/L 07/27/23 17:15 74-83-9 M15.0 0.22 1
tert-Butyl Alcohol <4.1 ug/L 07/27/23 17:15 75-65-050.0 4.1 1
n-Butylbenzene <0.066 ug/L 07/27/23 17:15 104-51-8 M10.50 0.066 1
sec-Butylbenzene <0.085 ug/L 07/27/23 17:15 135-98-8 M10.50 0.085 1
tert-Butylbenzene <0.086 ug/L 07/27/23 17:15 98-06-60.50 0.086 1
tert-Butyl Formate <0.30 ug/L 07/27/23 17:15 762-75-450.0 0.30 1
Carbon tetrachloride <0.17 ug/L 07/27/23 17:15 56-23-50.50 0.17 1
Chlorobenzene <0.085 ug/L 07/27/23 17:15 108-90-70.50 0.085 1
Chloroethane <0.17 ug/L 07/27/23 17:15 75-00-3 M11.0 0.17 1
Chloroform <0.069 ug/L 07/27/23 17:15 67-66-30.50 0.069 1
Chloromethane <0.18 ug/L 07/27/23 17:15 74-87-31.0 0.18 1
2-Chlorotoluene <0.13 ug/L 07/27/23 17:15 95-49-8 M10.50 0.13 1
4-Chlorotoluene <0.096 ug/L 07/27/23 17:15 106-43-40.50 0.096 1
1,2-Dibromo-3-chloropropane <0.18 ug/L 07/27/23 17:15 96-12-81.0 0.18 1
Dibromochloromethane <0.15 ug/L 07/27/23 17:15 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)0.37J ug/L 07/27/23 17:15 106-93-40.50 0.15 1
Dibromomethane <0.19 ug/L 07/27/23 17:15 74-95-3 M10.50 0.19 1
1,2-Dichlorobenzene <0.094 ug/L 07/27/23 17:15 95-50-10.50 0.094 1
1,3-Dichlorobenzene <0.098 ug/L 07/27/23 17:15 541-73-10.50 0.098 1
1,4-Dichlorobenzene <0.090 ug/L 07/27/23 17:15 106-46-70.50 0.090 1
Dichlorodifluoromethane <0.12 ug/L 07/27/23 17:15 75-71-8 M10.50 0.12 1
1,1-Dichloroethane <0.056 ug/L 07/27/23 17:15 75-34-30.50 0.056 1
1,2-Dichloroethane 1.0 ug/L 07/27/23 17:15 107-06-2 M10.50 0.11 1
1,1-Dichloroethene <0.079 ug/L 07/27/23 17:15 75-35-4 M10.50 0.079 1
cis-1,2-Dichloroethene <0.11 ug/L 07/27/23 17:15 156-59-20.50 0.11 1
trans-1,2-Dichloroethene <0.10 ug/L 07/27/23 17:15 156-60-5 M10.50 0.10 1
1,2-Dichloropropane <0.14 ug/L 07/27/23 17:15 78-87-5 M10.50 0.14 1
1,3-Dichloropropane <0.085 ug/L 07/27/23 17:15 142-28-90.50 0.085 1
2,2-Dichloropropane <0.12 ug/L 07/27/23 17:15 594-20-70.50 0.12 1
1,1-Dichloropropene <0.066 ug/L 07/27/23 17:15 563-58-60.50 0.066 1
cis-1,3-Dichloropropene <0.090 ug/L 07/27/23 17:15 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene <0.13 ug/L 07/27/23 17:15 10061-02-6 M10.50 0.13 1
Diisopropyl ether <0.072 ug/L 07/27/23 17:15 108-20-30.50 0.072 1
Ethanol <5.0 ug/L 07/27/23 17:15 64-17-5 M1200 5.0 1
Ethylbenzene 369 ug/L 07/28/23 10:56 100-41-4 M15.0 0.81 10
Ethyl-tert-butyl ether <0.11 ug/L 07/27/23 17:15 637-92-310.0 0.11 1
Hexachloro-1,3-butadiene <0.35 ug/L 07/27/23 17:15 87-68-32.0 0.35 1
Isopropylbenzene (Cumene)35.3 ug/L 07/27/23 17:15 98-82-80.50 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: WSW-8 Lab ID: 92679292006 Collected: 07/25/23 11:50 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <1.9 ug/L 07/27/23 17:15 75-09-2 M12.0 1.9 1
Methyl-tert-butyl ether <0.053 ug/L 07/27/23 17:15 1634-04-40.50 0.053 1
Naphthalene 40.6 ug/L 07/27/23 17:15 91-20-32.0 0.10 1
n-Propylbenzene 81.2 ug/L 07/27/23 17:15 103-65-10.50 0.10 1
Styrene <0.14 ug/L 07/27/23 17:15 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane <0.091 ug/L 07/27/23 17:15 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane <0.074 ug/L 07/27/23 17:15 79-34-50.50 0.074 1
Tetrachloroethene <0.086 ug/L 07/27/23 17:15 127-18-40.50 0.086 1
Toluene 55.2 ug/L 07/27/23 17:15 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene <0.12 ug/L 07/27/23 17:15 87-61-6 M12.0 0.12 1
1,2,4-Trichlorobenzene <0.16 ug/L 07/27/23 17:15 120-82-12.0 0.16 1
1,1,1-Trichloroethane <0.11 ug/L 07/27/23 17:15 71-55-60.50 0.11 1
1,1,2-Trichloroethane <0.096 ug/L 07/27/23 17:15 79-00-5 M10.50 0.096 1
Trichloroethene <0.17 ug/L 07/27/23 17:15 79-01-60.50 0.17 1
Trichlorofluoromethane <0.14 ug/L 07/27/23 17:15 75-69-41.0 0.14 1
1,2,3-Trichloropropane <0.17 ug/L 07/27/23 17:15 96-18-4 M10.50 0.17 1
1,2,4-Trimethylbenzene 770 ug/L 07/28/23 10:56 95-63-6 M15.0 0.31 10
1,3,5-Trimethylbenzene <0.71 ug/L 07/28/23 10:56 108-67-8 M15.0 0.71 10
Vinyl chloride <0.15 ug/L 07/27/23 17:15 75-01-41.0 0.15 1
m&p-Xylene 941 ug/L 07/28/23 10:56 179601-23-1 M110.0 0.94 10
o-Xylene 775 ug/L 07/28/23 10:56 95-47-65.0 1.4 10
Surrogates
1,2-Dichloroethane-d4 (S)95 %07/27/23 17:15 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %07/27/23 17:15 460-00-470-130 1
Toluene-d8 (S)104 %07/27/23 17:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: WSW-9 Lab ID: 92679292007 Collected: 07/25/23 12:05 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <7.4 ug/L 07/28/23 13:44 75-85-4100 7.4 1
tert-Amylmethyl ether <0.12 ug/L 07/28/23 13:44 994-05-810.0 0.12 1
Benzene <0.079 ug/L 07/28/23 13:44 71-43-20.50 0.079 1
Bromobenzene <0.14 ug/L 07/28/23 13:44 108-86-10.50 0.14 1
Bromochloromethane <0.094 ug/L 07/28/23 13:44 74-97-50.50 0.094 1
Bromodichloromethane 8.6 ug/L 07/28/23 13:44 75-27-40.50 0.17 1
Bromoform <0.20 ug/L 07/28/23 13:44 75-25-20.50 0.20 1
Bromomethane 0.42J ug/L 07/28/23 13:44 74-83-95.0 0.22 1
tert-Butyl Alcohol <4.1 ug/L 07/28/23 13:44 75-65-050.0 4.1 1
n-Butylbenzene <0.066 ug/L 07/28/23 13:44 104-51-80.50 0.066 1
sec-Butylbenzene <0.085 ug/L 07/28/23 13:44 135-98-80.50 0.085 1
tert-Butylbenzene <0.086 ug/L 07/28/23 13:44 98-06-60.50 0.086 1
tert-Butyl Formate <0.30 ug/L 07/28/23 13:44 762-75-450.0 0.30 1
Carbon tetrachloride <0.17 ug/L 07/28/23 13:44 56-23-50.50 0.17 1
Chlorobenzene <0.085 ug/L 07/28/23 13:44 108-90-70.50 0.085 1
Chloroethane <0.17 ug/L 07/28/23 13:44 75-00-31.0 0.17 1
Chloroform 40.9 ug/L 07/28/23 13:44 67-66-3 M10.50 0.069 1
Chloromethane 0.18J ug/L 07/28/23 13:44 74-87-3 M11.0 0.18 1
2-Chlorotoluene <0.13 ug/L 07/28/23 13:44 95-49-80.50 0.13 1
4-Chlorotoluene <0.096 ug/L 07/28/23 13:44 106-43-40.50 0.096 1
1,2-Dibromo-3-chloropropane <0.18 ug/L 07/28/23 13:44 96-12-81.0 0.18 1
Dibromochloromethane 2.2 ug/L 07/28/23 13:44 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)<0.15 ug/L 07/28/23 13:44 106-93-40.50 0.15 1
Dibromomethane <0.19 ug/L 07/28/23 13:44 74-95-30.50 0.19 1
1,2-Dichlorobenzene <0.094 ug/L 07/28/23 13:44 95-50-10.50 0.094 1
1,3-Dichlorobenzene <0.098 ug/L 07/28/23 13:44 541-73-10.50 0.098 1
1,4-Dichlorobenzene <0.090 ug/L 07/28/23 13:44 106-46-70.50 0.090 1
Dichlorodifluoromethane <0.12 ug/L 07/28/23 13:44 75-71-80.50 0.12 1
1,1-Dichloroethane <0.056 ug/L 07/28/23 13:44 75-34-30.50 0.056 1
1,2-Dichloroethane <0.11 ug/L 07/28/23 13:44 107-06-20.50 0.11 1
1,1-Dichloroethene <0.079 ug/L 07/28/23 13:44 75-35-40.50 0.079 1
cis-1,2-Dichloroethene <0.11 ug/L 07/28/23 13:44 156-59-20.50 0.11 1
trans-1,2-Dichloroethene <0.10 ug/L 07/28/23 13:44 156-60-50.50 0.10 1
1,2-Dichloropropane <0.14 ug/L 07/28/23 13:44 78-87-50.50 0.14 1
1,3-Dichloropropane <0.085 ug/L 07/28/23 13:44 142-28-90.50 0.085 1
2,2-Dichloropropane <0.12 ug/L 07/28/23 13:44 594-20-70.50 0.12 1
1,1-Dichloropropene <0.066 ug/L 07/28/23 13:44 563-58-60.50 0.066 1
cis-1,3-Dichloropropene <0.090 ug/L 07/28/23 13:44 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene <0.13 ug/L 07/28/23 13:44 10061-02-60.50 0.13 1
Diisopropyl ether <0.072 ug/L 07/28/23 13:44 108-20-30.50 0.072 1
Ethanol <5.0 ug/L 07/28/23 13:44 64-17-5200 5.0 1
Ethylbenzene <0.081 ug/L 07/28/23 13:44 100-41-40.50 0.081 1
Ethyl-tert-butyl ether <0.11 ug/L 07/28/23 13:44 637-92-310.0 0.11 1
Hexachloro-1,3-butadiene <0.35 ug/L 07/28/23 13:44 87-68-32.0 0.35 1
Isopropylbenzene (Cumene)<0.11 ug/L 07/28/23 13:44 98-82-80.50 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Sample: WSW-9 Lab ID: 92679292007 Collected: 07/25/23 12:05 Received: 07/26/23 06:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <1.9 ug/L 07/28/23 13:44 75-09-22.0 1.9 1
Methyl-tert-butyl ether <0.053 ug/L 07/28/23 13:44 1634-04-40.50 0.053 1
Naphthalene <0.10 ug/L 07/28/23 13:44 91-20-3 R12.0 0.10 1
n-Propylbenzene <0.10 ug/L 07/28/23 13:44 103-65-10.50 0.10 1
Styrene <0.14 ug/L 07/28/23 13:44 100-42-5 M1,R10.50 0.14 1
1,1,1,2-Tetrachloroethane <0.091 ug/L 07/28/23 13:44 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane <0.074 ug/L 07/28/23 13:44 79-34-50.50 0.074 1
Tetrachloroethene <0.086 ug/L 07/28/23 13:44 127-18-40.50 0.086 1
Toluene <0.090 ug/L 07/28/23 13:44 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene <0.12 ug/L 07/28/23 13:44 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene <0.16 ug/L 07/28/23 13:44 120-82-12.0 0.16 1
1,1,1-Trichloroethane <0.11 ug/L 07/28/23 13:44 71-55-60.50 0.11 1
1,1,2-Trichloroethane <0.096 ug/L 07/28/23 13:44 79-00-50.50 0.096 1
Trichloroethene <0.17 ug/L 07/28/23 13:44 79-01-60.50 0.17 1
Trichlorofluoromethane <0.14 ug/L 07/28/23 13:44 75-69-41.0 0.14 1
1,2,3-Trichloropropane <0.17 ug/L 07/28/23 13:44 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene <0.031 ug/L 07/28/23 13:44 95-63-6 M1,R10.50 0.031 1
1,3,5-Trimethylbenzene <0.071 ug/L 07/28/23 13:44 108-67-8 M10.50 0.071 1
Vinyl chloride <0.15 ug/L 07/28/23 13:44 75-01-41.0 0.15 1
m&p-Xylene <0.094 ug/L 07/28/23 13:44 179601-23-1 R11.0 0.094 1
o-Xylene <0.14 ug/L 07/28/23 13:44 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %07/28/23 13:44 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %07/28/23 13:44 460-00-470-130 1
Toluene-d8 (S)95 %07/28/23 13:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
789623
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92679292001, 92679292006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4092585
Associated Lab Samples:92679292001, 92679292006
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.091 0.50 07/27/23 15:280.091
1,1,1-Trichloroethane ug/L <0.11 0.50 07/27/23 15:280.11
1,1,2,2-Tetrachloroethane ug/L <0.074 0.50 07/27/23 15:280.074
1,1,2-Trichloroethane ug/L <0.096 0.50 07/27/23 15:280.096
1,1-Dichloroethane ug/L <0.056 0.50 07/27/23 15:280.056
1,1-Dichloroethene ug/L <0.079 0.50 07/27/23 15:280.079
1,1-Dichloropropene ug/L <0.066 0.50 07/27/23 15:280.066
1,2,3-Trichlorobenzene ug/L <0.12 2.0 07/27/23 15:280.12
1,2,3-Trichloropropane ug/L <0.17 0.50 07/27/23 15:280.17
1,2,4-Trichlorobenzene ug/L <0.16 2.0 07/27/23 15:280.16
1,2,4-Trimethylbenzene ug/L <0.031 0.50 07/27/23 15:280.031
1,2-Dibromo-3-chloropropane ug/L <0.18 1.0 07/27/23 15:280.18
1,2-Dibromoethane (EDB)ug/L <0.15 0.50 07/27/23 15:280.15
1,2-Dichlorobenzene ug/L <0.094 0.50 07/27/23 15:280.094
1,2-Dichloroethane ug/L <0.11 0.50 07/27/23 15:280.11
1,2-Dichloropropane ug/L <0.14 0.50 07/27/23 15:280.14
1,3,5-Trimethylbenzene ug/L <0.071 0.50 07/27/23 15:280.071
1,3-Dichlorobenzene ug/L <0.098 0.50 07/27/23 15:280.098
1,3-Dichloropropane ug/L <0.085 0.50 07/27/23 15:280.085
1,4-Dichlorobenzene ug/L <0.090 0.50 07/27/23 15:280.090
2,2-Dichloropropane ug/L <0.12 0.50 07/27/23 15:280.12
2-Chlorotoluene ug/L <0.13 0.50 07/27/23 15:280.13
4-Chlorotoluene ug/L <0.096 0.50 07/27/23 15:280.096
Benzene ug/L <0.079 0.50 07/27/23 15:280.079
Bromobenzene ug/L <0.14 0.50 07/27/23 15:280.14
Bromochloromethane ug/L <0.094 0.50 07/27/23 15:280.094
Bromodichloromethane ug/L <0.17 0.50 07/27/23 15:280.17
Bromoform ug/L <0.20 0.50 07/27/23 15:280.20
Bromomethane ug/L <0.22 5.0 07/27/23 15:280.22
Carbon tetrachloride ug/L <0.17 0.50 07/27/23 15:280.17
Chlorobenzene ug/L <0.085 0.50 07/27/23 15:280.085
Chloroethane ug/L <0.17 1.0 07/27/23 15:280.17
Chloroform ug/L <0.069 0.50 07/27/23 15:280.069
Chloromethane ug/L <0.18 1.0 07/27/23 15:280.18
cis-1,2-Dichloroethene ug/L <0.11 0.50 07/27/23 15:280.11
cis-1,3-Dichloropropene ug/L <0.090 0.50 07/27/23 15:280.090
Dibromochloromethane ug/L <0.15 0.50 07/27/23 15:280.15
Dibromomethane ug/L <0.19 0.50 07/27/23 15:280.19
Dichlorodifluoromethane ug/L <0.12 0.50 07/27/23 15:280.12
Diisopropyl ether ug/L <0.072 0.50 07/27/23 15:280.072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4092585
Associated Lab Samples:92679292001, 92679292006
Matrix: Water
AnalyzedMDL
Ethanol ug/L <5.0 200 07/27/23 15:285.0
Ethyl-tert-butyl ether ug/L <0.11 10.0 07/27/23 15:280.11
Ethylbenzene ug/L <0.081 0.50 07/27/23 15:280.081
Hexachloro-1,3-butadiene ug/L <0.35 2.0 07/27/23 15:280.35
Isopropylbenzene (Cumene)ug/L <0.11 0.50 07/27/23 15:280.11
m&p-Xylene ug/L <0.094 1.0 07/27/23 15:280.094
Methyl-tert-butyl ether ug/L <0.053 0.50 07/27/23 15:280.053
Methylene Chloride ug/L <1.9 2.0 07/27/23 15:281.9
n-Butylbenzene ug/L <0.066 0.50 07/27/23 15:280.066
n-Propylbenzene ug/L <0.10 0.50 07/27/23 15:280.10
Naphthalene ug/L <0.10 2.0 07/27/23 15:280.10
o-Xylene ug/L <0.14 0.50 07/27/23 15:280.14
sec-Butylbenzene ug/L <0.085 0.50 07/27/23 15:280.085
Styrene ug/L <0.14 0.50 07/27/23 15:280.14
tert-Amyl Alcohol ug/L <7.4 100 07/27/23 15:287.4
tert-Amylmethyl ether ug/L <0.12 10.0 07/27/23 15:280.12
tert-Butyl Alcohol ug/L <4.1 50.0 07/27/23 15:284.1
tert-Butyl Formate ug/L <0.30 50.0 07/27/23 15:280.30
tert-Butylbenzene ug/L <0.086 0.50 07/27/23 15:280.086
Tetrachloroethene ug/L <0.086 0.50 07/27/23 15:280.086
Toluene ug/L <0.090 0.50 07/27/23 15:280.090
trans-1,2-Dichloroethene ug/L <0.10 0.50 07/27/23 15:280.10
trans-1,3-Dichloropropene ug/L <0.13 0.50 07/27/23 15:280.13
Trichloroethene ug/L <0.17 0.50 07/27/23 15:280.17
Trichlorofluoromethane ug/L <0.14 1.0 07/27/23 15:280.14
Vinyl chloride ug/L <0.15 1.0 07/27/23 15:280.15
1,2-Dichloroethane-d4 (S)%102 70-130 07/27/23 15:28
4-Bromofluorobenzene (S)%100 70-130 07/27/23 15:28
Toluene-d8 (S)%101 70-130 07/27/23 15:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4092586LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.620 98 60-140
1,1,1-Trichloroethane ug/L 20.220 101 60-140
1,1,2,2-Tetrachloroethane ug/L 20.120 100 60-140
1,1,2-Trichloroethane ug/L 19.920 99 60-140
1,1-Dichloroethane ug/L 20.520 103 60-140
1,1-Dichloroethene ug/L 21.320 106 60-140
1,1-Dichloropropene ug/L 21.220 106 60-140
1,2,3-Trichlorobenzene ug/L 21.120 105 60-140
1,2,3-Trichloropropane ug/L 19.020 95 60-140
1,2,4-Trichlorobenzene ug/L 20.820 104 60-140
1,2,4-Trimethylbenzene ug/L 19.320 97 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4092586LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 19.220 96 60-140
1,2-Dibromoethane (EDB)ug/L 19.820 99 60-140
1,2-Dichlorobenzene ug/L 19.120 95 60-140
1,2-Dichloroethane ug/L 20.320 102 60-140
1,2-Dichloropropane ug/L 20.320 102 60-140
1,3,5-Trimethylbenzene ug/L 19.420 97 60-140
1,3-Dichlorobenzene ug/L 18.720 94 60-140
1,3-Dichloropropane ug/L 18.820 94 60-140
1,4-Dichlorobenzene ug/L 18.420 92 60-140
2,2-Dichloropropane ug/L 19.720 98 60-140
2-Chlorotoluene ug/L 19.120 95 60-140
4-Chlorotoluene ug/L 19.020 95 60-140
Benzene ug/L 19.120 96 60-140
Bromobenzene ug/L 18.520 93 60-140
Bromochloromethane ug/L 20.620 103 60-140
Bromodichloromethane ug/L 19.220 96 60-140
Bromoform ug/L 18.620 93 60-140
Bromomethane ug/L 19.420 97 60-140
Carbon tetrachloride ug/L 19.220 96 60-140
Chlorobenzene ug/L 19.020 95 60-140
Chloroethane ug/L 21.620 108 60-140
Chloroform ug/L 19.920 99 60-140
Chloromethane ug/L 21.820 109 60-140
cis-1,2-Dichloroethene ug/L 20.520 103 60-140
cis-1,3-Dichloropropene ug/L 19.220 96 60-140
Dibromochloromethane ug/L 18.820 94 60-140
Dibromomethane ug/L 19.520 97 60-140
Dichlorodifluoromethane ug/L 25.420 127 60-140
Diisopropyl ether ug/L 21.020 105 60-140
Ethanol ug/L 891800 111 60-140
Ethyl-tert-butyl ether ug/L 39.240 98 60-140
Ethylbenzene ug/L 18.820 94 60-140
Hexachloro-1,3-butadiene ug/L 21.520 107 60-140
Isopropylbenzene (Cumene)ug/L 19.420 97 60-140
m&p-Xylene ug/L 38.040 95 60-140
Methyl-tert-butyl ether ug/L 19.320 96 60-140
Methylene Chloride ug/L 21.920 110 60-140
n-Butylbenzene ug/L 19.420 97 60-140
n-Propylbenzene ug/L 18.720 93 60-140
Naphthalene ug/L 21.420 107 60-140
o-Xylene ug/L 18.920 95 60-140
sec-Butylbenzene ug/L 19.020 95 60-140
Styrene ug/L 19.220 96 60-140
tert-Amyl Alcohol ug/L 419400 105 60-140
tert-Amylmethyl ether ug/L 39.840 99 60-140
tert-Butyl Alcohol ug/L 205200 103 60-140
tert-Butyl Formate ug/L 160160 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4092586LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 15.620 78 60-140
Tetrachloroethene ug/L 18.320 91 60-140
Toluene ug/L 18.420 92 60-140
trans-1,2-Dichloroethene ug/L 21.220 106 60-140
trans-1,3-Dichloropropene ug/L 19.820 99 60-140
Trichloroethene ug/L 19.620 98 60-140
Trichlorofluoromethane ug/L 19.820 99 60-140
Vinyl chloride ug/L 18.420 92 60-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4092587MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92679292006
4092588
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 25 128 60-140122 5 3025<0.091 32.1 30.4
1,1,1-Trichloroethane ug/L 25 132 60-140125 5 3025<0.11 33.0 31.2
1,1,2,2-Tetrachloroethane ug/L 25 136 60-140137 0 3025<0.074 34.0 34.2
1,1,2-Trichloroethane ug/L M12512160-140155 25 3025<0.096 30.1 38.8
1,1-Dichloroethane ug/L 25 137 60-140139 1 3025<0.056 34.4 34.8
1,1-Dichloroethene ug/L M12515760-140142 10 3025<0.079 39.2 35.5
1,1-Dichloropropene ug/L 25 134 60-140130 3 3025<0.066 33.6 32.5
1,2,3-Trichlorobenzene ug/L M12513560-140146 8 3025<0.12 33.9 36.6
1,2,3-Trichloropropane ug/L M12516660-140158 5 3025<0.17 41.4 39.4
1,2,4-Trichlorobenzene ug/L 25 131 60-140138 5 3025<0.16 32.7 34.4
1,2,4-Trimethylbenzene ug/L M12517360-140320 4 3025770813 850
1,2-Dibromo-3-
chloropropane ug/L 25 135 60-140137 2 3025<0.18 33.8 34.3
1,2-Dibromoethane (EDB) ug/L 25 130 60-140126 4 30250.37J 33.0 31.8
1,2-Dichlorobenzene ug/L 25 136 60-140137 1 3025<0.094 34.0 34.2
1,2-Dichloroethane ug/L M12514160-140137 3 30251.0 36.3 35.1
1,2-Dichloropropane ug/L M12514160-140140 0 3025<0.14 35.1 35.1
1,3,5-Trimethylbenzene ug/L M125107060-1401100 3 3025<0.71 267 274
1,3-Dichlorobenzene ug/L 25 133 60-140136 2 3025<0.098 33.2 33.9
1,3-Dichloropropane ug/L 25 127 60-140124 2 3025<0.085 31.8 31.0
1,4-Dichlorobenzene ug/L 25 131 60-140136 4 3025<0.090 32.9 34.1
2,2-Dichloropropane ug/L 25 129 60-140133 3 3025<0.12 32.1 33.2
2-Chlorotoluene ug/L M12515060-140146 3 3025<0.13 37.4 36.4
4-Chlorotoluene ug/L 25 124 60-140131 5 3025<0.096 31.1 32.7
Benzene ug/L 25 95 60-140111 10 302514.5 38.2 42.4
Bromobenzene ug/L 25 127 60-140138 8 3025<0.14 31.8 34.6
Bromochloromethane ug/L 25 139 60-140140 1 3025<0.094 34.8 35.0
Bromodichloromethane ug/L 25 119 60-140134 12 3025<0.17 29.7 33.4
Bromoform ug/L 25 115 60-140111 4 3025<0.20 28.6 27.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4092587MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92679292006
4092588
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M12518460-140167 3025<0.22 46.1J 41.9J
Carbon tetrachloride ug/L 25 111 60-140122 9 3025<0.17 27.9 30.6
Chlorobenzene ug/L 25 137 60-140133 3 3025<0.085 34.1 33.3
Chloroethane ug/L M12514960-140144 3 3025<0.17 37.2 36.1
Chloroform ug/L 25 135 60-140133 2 3025<0.069 33.8 33.2
Chloromethane ug/L 25 137 60-140139 1 3025<0.18 34.2 34.6
cis-1,2-Dichloroethene ug/L 25 136 60-140140 3 3025<0.11 34.1 35.0
cis-1,3-Dichloropropene ug/L 25 116 60-140136 15 3025<0.090 29.0 33.9
Dibromochloromethane ug/L 25 117 60-140120 2 3025<0.15 29.2 29.9
Dibromomethane ug/L M12514560-140139 4 3025<0.19 36.3 34.8
Dichlorodifluoromethane ug/L M12514060-140143 2 3025<0.12 35.0 35.7
Diisopropyl ether ug/L 25 139 60-140139 1 3025<0.072 34.7 34.9
Ethanol ug/L M1100017660-140159 301000<5.0 1760J 1590J
Ethyl-tert-butyl ether ug/L 50 131 60-140131 3050<0.11 65.3J 65.3J
Ethylbenzene ug/L M12514160-140120 1 3025369405 399
Hexachloro-1,3-butadiene ug/L 25 135 60-140133 2 3025<0.35 33.7 33.1
Isopropylbenzene
(Cumene)ug/L 25 112 60-140113 0 302535.3 63.3 63.6
m&p-Xylene ug/L M15014060-140154 1 30509411010 1020
Methyl-tert-butyl ether ug/L 25 129 60-140127 2 3025<0.053 32.2 31.7
Methylene Chloride ug/L M12515660-140155 1 3025<1.9 39.1 38.7
n-Butylbenzene ug/L M12519560-140201 3 3025<0.066 48.8 50.3
n-Propylbenzene ug/L 25 60 60-14078 4 302581.2 96.2 101
Naphthalene ug/L 25 105 60-140123 7 302540.6 66.8 71.4
o-Xylene ug/L 25 93 60-14079 0 3025775798 795
sec-Butylbenzene ug/L M12513760-140144 5 3025<0.085 34.1 36.0
Styrene ug/L 25 139 60-140138 1 3025<0.14 34.8 34.5
tert-Amyl Alcohol ug/L 500 113 60-140128 3050050.8J 618J 689J
tert-Amylmethyl ether ug/L 50 119 60-140138 3050<0.12 59.5J 69.1J
tert-Butyl Alcohol ug/L 250 132 60-140131 30250<4.1 329J 327J
tert-Butyl Formate ug/L 200 101 60-14098 30200<0.30 202J 195J
tert-Butylbenzene ug/L 25 104 60-140108 4 3025<0.086 26.1 27.1
Tetrachloroethene ug/L 25 124 60-140140 12 3025<0.086 31.0 35.1
Toluene ug/L 25 62 60-140110 16 302555.2 70.8 82.7
trans-1,2-Dichloroethene ug/L M12513960-140141 1 3025<0.10 34.8 35.3
trans-1,3-Dichloropropene ug/L M12511060-140141 25 3025<0.13 27.5 35.4
Trichloroethene ug/L 25 127 60-140127 0 3025<0.17 31.8 31.9
Trichlorofluoromethane ug/L 25 130 60-140131 1 3025<0.14 32.5 32.6
Vinyl chloride ug/L 25 117 60-140119 2 3025<0.15 29.2 29.7
1,2-Dichloroethane-d4 (S) %100 70-13098
4-Bromofluorobenzene (S) %100 70-13098
Toluene-d8 (S)%98 70-130113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
789971
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92679292002, 92679292003, 92679292004, 92679292007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4094183
Associated Lab Samples:92679292002, 92679292003, 92679292004, 92679292007
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.091 0.50 07/28/23 13:260.091
1,1,1-Trichloroethane ug/L <0.11 0.50 07/28/23 13:260.11
1,1,2,2-Tetrachloroethane ug/L <0.074 0.50 07/28/23 13:260.074
1,1,2-Trichloroethane ug/L <0.096 0.50 07/28/23 13:260.096
1,1-Dichloroethane ug/L <0.056 0.50 07/28/23 13:260.056
1,1-Dichloroethene ug/L <0.079 0.50 07/28/23 13:260.079
1,1-Dichloropropene ug/L <0.066 0.50 07/28/23 13:260.066
1,2,3-Trichlorobenzene ug/L <0.12 2.0 07/28/23 13:260.12
1,2,3-Trichloropropane ug/L <0.17 0.50 07/28/23 13:260.17
1,2,4-Trichlorobenzene ug/L <0.16 2.0 07/28/23 13:260.16
1,2,4-Trimethylbenzene ug/L <0.031 0.50 07/28/23 13:260.031
1,2-Dibromo-3-chloropropane ug/L <0.18 1.0 07/28/23 13:260.18
1,2-Dibromoethane (EDB)ug/L <0.15 0.50 07/28/23 13:260.15
1,2-Dichlorobenzene ug/L <0.094 0.50 07/28/23 13:260.094
1,2-Dichloroethane ug/L <0.11 0.50 07/28/23 13:260.11
1,2-Dichloropropane ug/L <0.14 0.50 07/28/23 13:260.14
1,3,5-Trimethylbenzene ug/L <0.071 0.50 07/28/23 13:260.071
1,3-Dichlorobenzene ug/L <0.098 0.50 07/28/23 13:260.098
1,3-Dichloropropane ug/L <0.085 0.50 07/28/23 13:260.085
1,4-Dichlorobenzene ug/L <0.090 0.50 07/28/23 13:260.090
2,2-Dichloropropane ug/L <0.12 0.50 07/28/23 13:260.12
2-Chlorotoluene ug/L <0.13 0.50 07/28/23 13:260.13
4-Chlorotoluene ug/L <0.096 0.50 07/28/23 13:260.096
Benzene ug/L <0.079 0.50 07/28/23 13:260.079
Bromobenzene ug/L <0.14 0.50 07/28/23 13:260.14
Bromochloromethane ug/L <0.094 0.50 07/28/23 13:260.094
Bromodichloromethane ug/L <0.17 0.50 07/28/23 13:260.17
Bromoform ug/L <0.20 0.50 07/28/23 13:260.20
Bromomethane ug/L <0.22 5.0 07/28/23 13:260.22
Carbon tetrachloride ug/L <0.17 0.50 07/28/23 13:260.17
Chlorobenzene ug/L <0.085 0.50 07/28/23 13:260.085
Chloroethane ug/L <0.17 1.0 07/28/23 13:260.17
Chloroform ug/L <0.069 0.50 07/28/23 13:260.069
Chloromethane ug/L <0.18 1.0 07/28/23 13:260.18
cis-1,2-Dichloroethene ug/L <0.11 0.50 07/28/23 13:260.11
cis-1,3-Dichloropropene ug/L <0.090 0.50 07/28/23 13:260.090
Dibromochloromethane ug/L <0.15 0.50 07/28/23 13:260.15
Dibromomethane ug/L <0.19 0.50 07/28/23 13:260.19
Dichlorodifluoromethane ug/L <0.12 0.50 07/28/23 13:260.12
Diisopropyl ether ug/L <0.072 0.50 07/28/23 13:260.072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4094183
Associated Lab Samples:92679292002, 92679292003, 92679292004, 92679292007
Matrix: Water
AnalyzedMDL
Ethanol ug/L <5.0 200 07/28/23 13:265.0
Ethyl-tert-butyl ether ug/L <0.11 10.0 07/28/23 13:260.11
Ethylbenzene ug/L <0.081 0.50 07/28/23 13:260.081
Hexachloro-1,3-butadiene ug/L <0.35 2.0 07/28/23 13:260.35
Isopropylbenzene (Cumene)ug/L <0.11 0.50 07/28/23 13:260.11
m&p-Xylene ug/L <0.094 1.0 07/28/23 13:260.094
Methyl-tert-butyl ether ug/L <0.053 0.50 07/28/23 13:260.053
Methylene Chloride ug/L <1.9 2.0 07/28/23 13:261.9
n-Butylbenzene ug/L <0.066 0.50 07/28/23 13:260.066
n-Propylbenzene ug/L <0.10 0.50 07/28/23 13:260.10
Naphthalene ug/L <0.10 2.0 07/28/23 13:260.10
o-Xylene ug/L <0.14 0.50 07/28/23 13:260.14
sec-Butylbenzene ug/L <0.085 0.50 07/28/23 13:260.085
Styrene ug/L <0.14 0.50 07/28/23 13:260.14
tert-Amyl Alcohol ug/L <7.4 100 07/28/23 13:267.4
tert-Amylmethyl ether ug/L <0.12 10.0 07/28/23 13:260.12
tert-Butyl Alcohol ug/L <4.1 50.0 07/28/23 13:264.1
tert-Butyl Formate ug/L <0.30 50.0 07/28/23 13:260.30
tert-Butylbenzene ug/L <0.086 0.50 07/28/23 13:260.086
Tetrachloroethene ug/L <0.086 0.50 07/28/23 13:260.086
Toluene ug/L <0.090 0.50 07/28/23 13:260.090
trans-1,2-Dichloroethene ug/L <0.10 0.50 07/28/23 13:260.10
trans-1,3-Dichloropropene ug/L <0.13 0.50 07/28/23 13:260.13
Trichloroethene ug/L <0.17 0.50 07/28/23 13:260.17
Trichlorofluoromethane ug/L <0.14 1.0 07/28/23 13:260.14
Vinyl chloride ug/L <0.15 1.0 07/28/23 13:260.15
1,2-Dichloroethane-d4 (S)%100 70-130 07/28/23 13:26
4-Bromofluorobenzene (S)%98 70-130 07/28/23 13:26
Toluene-d8 (S)%95 70-130 07/28/23 13:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4094184LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.720 94 60-140
1,1,1-Trichloroethane ug/L 17.920 89 60-140
1,1,2,2-Tetrachloroethane ug/L 18.820 94 60-140
1,1,2-Trichloroethane ug/L 16.520 83 60-140
1,1-Dichloroethane ug/L 17.220 86 60-140
1,1-Dichloroethene ug/L 17.720 88 60-140
1,1-Dichloropropene ug/L 18.720 94 60-140
1,2,3-Trichlorobenzene ug/L 19.220 96 60-140
1,2,3-Trichloropropane ug/L 18.020 90 60-140
1,2,4-Trichlorobenzene ug/L 19.420 97 60-140
1,2,4-Trimethylbenzene ug/L 18.220 91 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4094184LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 18.720 93 60-140
1,2-Dibromoethane (EDB)ug/L 18.720 94 60-140
1,2-Dichlorobenzene ug/L 19.220 96 60-140
1,2-Dichloroethane ug/L 18.020 90 60-140
1,2-Dichloropropane ug/L 17.520 87 60-140
1,3,5-Trimethylbenzene ug/L 18.320 91 60-140
1,3-Dichlorobenzene ug/L 18.820 94 60-140
1,3-Dichloropropane ug/L 18.120 90 60-140
1,4-Dichlorobenzene ug/L 18.620 93 60-140
2,2-Dichloropropane ug/L 17.520 88 60-140
2-Chlorotoluene ug/L 18.320 92 60-140
4-Chlorotoluene ug/L 18.320 91 60-140
Benzene ug/L 17.520 88 60-140
Bromobenzene ug/L 18.420 92 60-140
Bromochloromethane ug/L 17.820 89 60-140
Bromodichloromethane ug/L 15.920 79 60-140
Bromoform ug/L 18.620 93 60-140
Bromomethane ug/L 14.620 73 60-140
Carbon tetrachloride ug/L 17.520 88 60-140
Chlorobenzene ug/L 18.120 91 60-140
Chloroethane ug/L 15.720 78 60-140
Chloroform ug/L 17.620 88 60-140
Chloromethane ug/L 16.420 82 60-140
cis-1,2-Dichloroethene ug/L 17.620 88 60-140
cis-1,3-Dichloropropene ug/L 17.920 90 60-140
Dibromochloromethane ug/L 18.220 91 60-140
Dibromomethane ug/L 18.620 93 60-140
Dichlorodifluoromethane ug/L 17.520 88 60-140
Diisopropyl ether ug/L 17.220 86 60-140
Ethanol ug/L 696800 87 60-140
Ethyl-tert-butyl ether ug/L 35.940 90 60-140
Ethylbenzene ug/L 17.620 88 60-140
Hexachloro-1,3-butadiene ug/L 19.520 97 60-140
Isopropylbenzene (Cumene)ug/L 17.920 89 60-140
m&p-Xylene ug/L 35.440 89 60-140
Methyl-tert-butyl ether ug/L 17.420 87 60-140
Methylene Chloride ug/L 16.720 83 60-140
n-Butylbenzene ug/L 18.520 93 60-140
n-Propylbenzene ug/L 17.920 89 60-140
Naphthalene ug/L 19.920 99 60-140
o-Xylene ug/L 17.420 87 60-140
sec-Butylbenzene ug/L 17.320 87 60-140
Styrene ug/L 18.320 91 60-140
tert-Amyl Alcohol ug/L 359400 90 60-140
tert-Amylmethyl ether ug/L 37.040 93 60-140
tert-Butyl Alcohol ug/L 178200 89 60-140
tert-Butyl Formate ug/L 144160 90 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4094184LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 14.420 72 60-140
Tetrachloroethene ug/L 17.420 87 60-140
Toluene ug/L 17.520 87 60-140
trans-1,2-Dichloroethene ug/L 18.020 90 60-140
trans-1,3-Dichloropropene ug/L 18.220 91 60-140
Trichloroethene ug/L 18.020 90 60-140
Trichlorofluoromethane ug/L 16.620 83 60-140
Vinyl chloride ug/L 14.420 72 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4094185MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92679292007
4094186
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 113 60-140119 5 3020<0.091 22.6 23.8
1,1,1-Trichloroethane ug/L 20 123 60-140129 5 3020<0.11 24.6 25.9
1,1,2,2-Tetrachloroethane ug/L 20 109 60-140118 8 3020<0.074 21.8 23.7
1,1,2-Trichloroethane ug/L 20 129 60-140122 6 3020<0.096 25.9 24.4
1,1-Dichloroethane ug/L 20 123 60-140126 2 3020<0.056 24.5 25.1
1,1-Dichloroethene ug/L 20 132 60-140134 2 3020<0.079 26.4 26.8
1,1-Dichloropropene ug/L 20 131 60-140132 1 3020<0.066 26.2 26.4
1,2,3-Trichlorobenzene ug/L 20 112 60-140113 1 3020<0.12 22.4 22.7
1,2,3-Trichloropropane ug/L 20 102 60-140114 11 3020<0.17 20.4 22.8
1,2,4-Trichlorobenzene ug/L 20 114 60-140115 1 3020<0.16 22.7 23.0
1,2,4-Trimethylbenzene ug/L M1,R12013360-14010 171 3020<0.031 26.5 2.1
1,2-Dibromo-3-
chloropropane ug/L 20 100 60-140106 6 3020<0.18 20.0 21.3
1,2-Dibromoethane (EDB) ug/L 20 110 60-140118 7 3020<0.15 22.0 23.6
1,2-Dichlorobenzene ug/L 20 111 60-140114 3 3020<0.094 22.2 22.7
1,2-Dichloroethane ug/L 20 118 60-140126 6 3020<0.11 23.7 25.2
1,2-Dichloropropane ug/L 20 137 60-140126 9 3020<0.14 27.5 25.1
1,3,5-Trimethylbenzene ug/L M12010960-1401 3020<0.071 21.7 0.15J
1,3-Dichlorobenzene ug/L 20 109 60-140110 1 3020<0.098 21.9 22.0
1,3-Dichloropropane ug/L 20 105 60-140115 9 3020<0.085 21.1 23.1
1,4-Dichlorobenzene ug/L 20 109 60-140112 2 3020<0.090 21.8 22.3
2,2-Dichloropropane ug/L 20 126 60-140131 4 3020<0.12 25.1 26.2
2-Chlorotoluene ug/L 20 123 60-140116 6 3020<0.13 24.6 23.2
4-Chlorotoluene ug/L 20 125 60-140115 8 3020<0.096 25.1 23.1
Benzene ug/L 20 116 60-140120 3 3020<0.079 23.2 23.9
Bromobenzene ug/L 20 123 60-140111 10 3020<0.14 24.7 22.2
Bromochloromethane ug/L 20 119 60-140125 5 3020<0.094 23.8 25.0
Bromodichloromethane ug/L 20 132 60-140139 4 30208.6 35.0 36.4
Bromoform ug/L 20 110 60-140113 3 3020<0.20 22.0 22.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4094185MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92679292007
4094186
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 88 60-14083 6 30200.42J 18.1 17.0
Carbon tetrachloride ug/L 20 121 60-140124 2 3020<0.17 24.2 24.8
Chlorobenzene ug/L 20 111 60-140117 6 3020<0.085 22.1 23.4
Chloroethane ug/L 20 130 60-140134 3 3020<0.17 25.9 26.7
Chloroform ug/L M12014360-140151 2 302040.9 69.4 71.2
Chloromethane ug/L M12014260-140171 18 30200.18J 28.6 34.4
cis-1,2-Dichloroethene ug/L 20 121 60-140126 4 3020<0.11 24.3 25.3
cis-1,3-Dichloropropene ug/L 20 125 60-140130 4 3020<0.090 25.1 26.0
Dibromochloromethane ug/L 20 111 60-140118 5 30202.2 24.4 25.8
Dibromomethane ug/L 20 113 60-140119 6 3020<0.19 22.5 23.8
Dichlorodifluoromethane ug/L 20 132 60-140133 1 3020<0.12 26.5 26.7
Diisopropyl ether ug/L 20 120 60-140128 6 3020<0.072 24.0 25.5
Ethanol ug/L 800 128 60-140124 3 30800<5.0 1020 989
Ethyl-tert-butyl ether ug/L 40 114 60-140119 5 3040<0.11 45.6 47.8
Ethylbenzene ug/L 20 109 60-140115 6 3020<0.081 21.8 23.1
Hexachloro-1,3-butadiene ug/L 20 119 60-140117 2 3020<0.35 23.9 23.4
Isopropylbenzene
(Cumene)ug/L 20 114 60-140119 4 3020<0.11 22.9 23.8
m&p-Xylene ug/L R14010960-14065 50 3040<0.094 43.4 25.9
Methyl-tert-butyl ether ug/L 20 111 60-140118 6 3020<0.053 22.2 23.6
Methylene Chloride ug/L 20 114 60-140122 7 3020<1.9 22.8 24.4
n-Butylbenzene ug/L 20 123 60-140121 2 3020<0.066 24.5 24.1
n-Propylbenzene ug/L 20 123 60-140113 9 3020<0.10 24.6 22.5
Naphthalene ug/L R12010860-14067 47 3020<0.10 21.6 13.3
o-Xylene ug/L 20 110 60-140106 3 3020<0.14 22.0 21.3
sec-Butylbenzene ug/L 20 123 60-140114 8 3020<0.085 24.7 22.9
Styrene ug/L M1,R1201360-1403 126 3020<0.14 2.6 0.60
tert-Amyl Alcohol ug/L 400 112 60-140116 3 30400<7.4 450 464
tert-Amylmethyl ether ug/L 40 115 60-140120 4 3040<0.12 45.8 47.9
tert-Butyl Alcohol ug/L 200 115 60-140126 9 30200<4.1 230 252
tert-Butyl Formate ug/L 160 103 60-14094 9 30160<0.30 165 150
tert-Butylbenzene ug/L 20 107 60-14094 12 3020<0.086 21.3 18.9
Tetrachloroethene ug/L 20 116 60-140126 8 3020<0.086 23.2 25.2
Toluene ug/L 20 121 60-140125 3 3020<0.090 24.2 25.0
trans-1,2-Dichloroethene ug/L 20 130 60-140135 4 3020<0.10 26.0 27.1
trans-1,3-Dichloropropene ug/L 20 125 60-140122 3 3020<0.13 25.0 24.4
Trichloroethene ug/L 20 120 60-140124 3 3020<0.17 24.1 24.8
Trichlorofluoromethane ug/L 20 123 60-140127 3 3020<0.14 24.6 25.3
Vinyl chloride ug/L 20 109 60-140107 1 3020<0.15 21.8 21.5
1,2-Dichloroethane-d4 (S) %104 70-130101
4-Bromofluorobenzene (S) %100 70-130101
Toluene-d8 (S)%111 70-130110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
790354
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92679292005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4096169
Associated Lab Samples:92679292005
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.091 0.50 07/31/23 14:080.091
1,1,1-Trichloroethane ug/L <0.11 0.50 07/31/23 14:080.11
1,1,2,2-Tetrachloroethane ug/L <0.074 0.50 07/31/23 14:080.074
1,1,2-Trichloroethane ug/L <0.096 0.50 07/31/23 14:080.096
1,1-Dichloroethane ug/L <0.056 0.50 07/31/23 14:080.056
1,1-Dichloroethene ug/L <0.079 0.50 07/31/23 14:080.079
1,1-Dichloropropene ug/L <0.066 0.50 07/31/23 14:080.066
1,2,3-Trichlorobenzene ug/L <0.12 2.0 07/31/23 14:080.12
1,2,3-Trichloropropane ug/L <0.17 0.50 07/31/23 14:080.17
1,2,4-Trichlorobenzene ug/L <0.16 2.0 07/31/23 14:080.16
1,2,4-Trimethylbenzene ug/L <0.031 0.50 07/31/23 14:080.031
1,2-Dibromo-3-chloropropane ug/L <0.18 1.0 07/31/23 14:080.18
1,2-Dibromoethane (EDB)ug/L <0.15 0.50 07/31/23 14:080.15
1,2-Dichlorobenzene ug/L <0.094 0.50 07/31/23 14:080.094
1,2-Dichloroethane ug/L <0.11 0.50 07/31/23 14:080.11
1,2-Dichloropropane ug/L <0.14 0.50 07/31/23 14:080.14
1,3,5-Trimethylbenzene ug/L <0.071 0.50 07/31/23 14:080.071
1,3-Dichlorobenzene ug/L <0.098 0.50 07/31/23 14:080.098
1,3-Dichloropropane ug/L <0.085 0.50 07/31/23 14:080.085
1,4-Dichlorobenzene ug/L <0.090 0.50 07/31/23 14:080.090
2,2-Dichloropropane ug/L <0.12 0.50 07/31/23 14:080.12
2-Chlorotoluene ug/L <0.13 0.50 07/31/23 14:080.13
4-Chlorotoluene ug/L <0.096 0.50 07/31/23 14:080.096
Benzene ug/L <0.079 0.50 07/31/23 14:080.079
Bromobenzene ug/L <0.14 0.50 07/31/23 14:080.14
Bromochloromethane ug/L <0.094 0.50 07/31/23 14:080.094
Bromodichloromethane ug/L <0.17 0.50 07/31/23 14:080.17
Bromoform ug/L <0.20 0.50 07/31/23 14:080.20
Bromomethane ug/L <0.22 5.0 07/31/23 14:080.22
Carbon tetrachloride ug/L <0.17 0.50 07/31/23 14:080.17
Chlorobenzene ug/L <0.085 0.50 07/31/23 14:080.085
Chloroethane ug/L <0.17 1.0 07/31/23 14:080.17
Chloroform ug/L <0.069 0.50 07/31/23 14:080.069
Chloromethane ug/L <0.18 1.0 07/31/23 14:080.18
cis-1,2-Dichloroethene ug/L <0.11 0.50 07/31/23 14:080.11
cis-1,3-Dichloropropene ug/L <0.090 0.50 07/31/23 14:080.090
Dibromochloromethane ug/L <0.15 0.50 07/31/23 14:080.15
Dibromomethane ug/L <0.19 0.50 07/31/23 14:080.19
Dichlorodifluoromethane ug/L <0.12 0.50 07/31/23 14:080.12
Diisopropyl ether ug/L <0.072 0.50 07/31/23 14:080.072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4096169
Associated Lab Samples:92679292005
Matrix: Water
AnalyzedMDL
Ethanol ug/L <5.0 200 07/31/23 14:085.0
Ethyl-tert-butyl ether ug/L <0.11 10.0 07/31/23 14:080.11
Ethylbenzene ug/L <0.081 0.50 07/31/23 14:080.081
Hexachloro-1,3-butadiene ug/L <0.35 2.0 07/31/23 14:080.35
Isopropylbenzene (Cumene)ug/L <0.11 0.50 07/31/23 14:080.11
m&p-Xylene ug/L <0.094 1.0 07/31/23 14:080.094
Methyl-tert-butyl ether ug/L <0.053 0.50 07/31/23 14:080.053
Methylene Chloride ug/L <1.9 2.0 07/31/23 14:081.9
n-Butylbenzene ug/L <0.066 0.50 07/31/23 14:080.066
n-Propylbenzene ug/L <0.10 0.50 07/31/23 14:080.10
Naphthalene ug/L <0.10 2.0 07/31/23 14:080.10
o-Xylene ug/L <0.14 0.50 07/31/23 14:080.14
sec-Butylbenzene ug/L <0.085 0.50 07/31/23 14:080.085
Styrene ug/L <0.14 0.50 07/31/23 14:080.14
tert-Amyl Alcohol ug/L <7.4 100 07/31/23 14:087.4
tert-Amylmethyl ether ug/L <0.12 10.0 07/31/23 14:080.12
tert-Butyl Alcohol ug/L <4.1 50.0 07/31/23 14:084.1
tert-Butyl Formate ug/L <0.30 50.0 07/31/23 14:080.30
tert-Butylbenzene ug/L <0.086 0.50 07/31/23 14:080.086
Tetrachloroethene ug/L <0.086 0.50 07/31/23 14:080.086
Toluene ug/L <0.090 0.50 07/31/23 14:080.090
trans-1,2-Dichloroethene ug/L <0.10 0.50 07/31/23 14:080.10
trans-1,3-Dichloropropene ug/L <0.13 0.50 07/31/23 14:080.13
Trichloroethene ug/L <0.17 0.50 07/31/23 14:080.17
Trichlorofluoromethane ug/L <0.14 1.0 07/31/23 14:080.14
Vinyl chloride ug/L <0.15 1.0 07/31/23 14:080.15
1,2-Dichloroethane-d4 (S)%98 70-130 07/31/23 14:08
4-Bromofluorobenzene (S)%97 70-130 07/31/23 14:08
Toluene-d8 (S)%94 70-130 07/31/23 14:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4096170LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.920 94 60-140
1,1,1-Trichloroethane ug/L 17.420 87 60-140
1,1,2,2-Tetrachloroethane ug/L 18.220 91 60-140
1,1,2-Trichloroethane ug/L 16.320 82 60-140
1,1-Dichloroethane ug/L 16.520 83 60-140
1,1-Dichloroethene ug/L 16.920 84 60-140
1,1-Dichloropropene ug/L 17.520 87 60-140
1,2,3-Trichlorobenzene ug/L 18.820 94 60-140
1,2,3-Trichloropropane ug/L 17.520 88 60-140
1,2,4-Trichlorobenzene ug/L 19.120 96 60-140
1,2,4-Trimethylbenzene ug/L 17.920 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4096170LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 17.420 87 60-140
1,2-Dibromoethane (EDB)ug/L 18.520 93 60-140
1,2-Dichlorobenzene ug/L 19.320 97 60-140
1,2-Dichloroethane ug/L 17.520 88 60-140
1,2-Dichloropropane ug/L 17.220 86 60-140
1,3,5-Trimethylbenzene ug/L 18.020 90 60-140
1,3-Dichlorobenzene ug/L 18.520 93 60-140
1,3-Dichloropropane ug/L 17.820 89 60-140
1,4-Dichlorobenzene ug/L 18.720 94 60-140
2,2-Dichloropropane ug/L 16.720 84 60-140
2-Chlorotoluene ug/L 17.620 88 60-140
4-Chlorotoluene ug/L 17.920 89 60-140
Benzene ug/L 17.220 86 60-140
Bromobenzene ug/L 18.620 93 60-140
Bromochloromethane ug/L 17.620 88 60-140
Bromodichloromethane ug/L 15.920 79 60-140
Bromoform ug/L 18.520 93 60-140
Bromomethane ug/L 15.020 75 60-140
Carbon tetrachloride ug/L 17.720 89 60-140
Chlorobenzene ug/L 18.420 92 60-140
Chloroethane ug/L 15.120 76 60-140
Chloroform ug/L 17.220 86 60-140
Chloromethane ug/L 14.320 72 60-140
cis-1,2-Dichloroethene ug/L 16.820 84 60-140
cis-1,3-Dichloropropene ug/L 17.620 88 60-140
Dibromochloromethane ug/L 18.320 91 60-140
Dibromomethane ug/L 19.120 96 60-140
Dichlorodifluoromethane ug/L 18.520 93 60-140
Diisopropyl ether ug/L 15.720 79 60-140
Ethanol ug/L 608800 76 60-140
Ethyl-tert-butyl ether ug/L 33.640 84 60-140
Ethylbenzene ug/L 17.420 87 60-140
Hexachloro-1,3-butadiene ug/L 18.920 95 60-140
Isopropylbenzene (Cumene)ug/L 17.820 89 60-140
m&p-Xylene ug/L 34.840 87 60-140
Methyl-tert-butyl ether ug/L 16.420 82 60-140
Methylene Chloride ug/L 15.220 76 60-140
n-Butylbenzene ug/L 17.520 87 60-140
n-Propylbenzene ug/L 17.220 86 60-140
Naphthalene ug/L 19.020 95 60-140
o-Xylene ug/L 17.020 85 60-140
sec-Butylbenzene ug/L 16.820 84 60-140
Styrene ug/L 18.220 91 60-140
tert-Amyl Alcohol ug/L 327400 82 60-140
tert-Amylmethyl ether ug/L 36.540 91 60-140
tert-Butyl Alcohol ug/L 154200 77 60-140
tert-Butyl Formate ug/L 135160 84 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4096170LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 14.320 71 60-140
Tetrachloroethene ug/L 17.320 86 60-140
Toluene ug/L 17.320 86 60-140
trans-1,2-Dichloroethene ug/L 17.020 85 60-140
trans-1,3-Dichloropropene ug/L 17.720 89 60-140
Trichloroethene ug/L 18.620 93 60-140
Trichlorofluoromethane ug/L 17.020 85 60-140
Vinyl chloride ug/L 13.220 66 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4096171MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92679660013
4096172
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 116 60-140111 5 3020ND23.2 22.1
1,1,1-Trichloroethane ug/L 20 112 60-140107 5 3020ND22.3 21.3
1,1,2,2-Tetrachloroethane ug/L 20 107 60-140101 6 3020ND21.4 20.2
1,1,2-Trichloroethane ug/L 20 97 60-14091 6 3020ND19.4 18.3
1,1-Dichloroethane ug/L 20 101 60-14096 5 3020ND20.1 19.2
1,1-Dichloroethene ug/L 20 108 60-140103 5 3020ND21.6 20.5
1,1-Dichloropropene ug/L 20 113 60-140108 5 3020ND22.6 21.5
1,2,3-Trichlorobenzene ug/L 20 116 60-140107 8 3020ND23.2 21.4
1,2,3-Trichloropropane ug/L 20 103 60-14095 8 3020ND20.6 18.9
1,2,4-Trichlorobenzene ug/L 20 117 60-140110 6 3020ND23.5 22.1
1,2,4-Trimethylbenzene ug/L 20 110 60-140103 6 3020ND21.9 20.6
1,2-Dibromo-3-
chloropropane ug/L 20 102 60-14096 6 3020ND20.5 19.2
1,2-Dibromoethane (EDB) ug/L 20 111 60-140105 6 3020ND22.2 21.0
1,2-Dichlorobenzene ug/L 20 115 60-140108 6 3020ND23.0 21.6
1,2-Dichloroethane ug/L 20 105 60-140100 5 3020ND20.9 19.9
1,2-Dichloropropane ug/L 20 103 60-14098 5 3020ND20.6 19.7
1,3,5-Trimethylbenzene ug/L 20 111 60-140104 6 3020ND22.1 20.8
1,3-Dichlorobenzene ug/L 20 115 60-140107 7 3020ND22.9 21.5
1,3-Dichloropropane ug/L 20 107 60-140101 6 3020ND21.4 20.2
1,4-Dichlorobenzene ug/L 20 113 60-140105 7 3020ND22.5 21.1
2,2-Dichloropropane ug/L 20 110 60-140103 6 3020ND21.9 20.7
2-Chlorotoluene ug/L 20 108 60-140102 6 3020ND21.7 20.5
4-Chlorotoluene ug/L 20 110 60-140102 7 3020ND21.9 20.5
Benzene ug/L 20 106 60-140102 4 3020ND21.3 20.4
Bromobenzene ug/L 20 112 60-140107 4 3020ND22.3 21.3
Bromochloromethane ug/L 20 108 60-140102 6 3020ND21.6 20.3
Bromodichloromethane ug/L 20 95 60-14092 4 3020ND19.0 18.3
Bromoform ug/L 20 111 60-140105 6 3020ND22.2 20.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
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Huntersville, NC 28078
[phone]
Page 32 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4096171MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92679660013
4096172
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 86 60-14081 6 3020ND17.2 16.2
Carbon tetrachloride ug/L 20 116 60-140111 4 3020ND23.3 22.3
Chlorobenzene ug/L 20 113 60-140108 5 3020ND22.7 21.6
Chloroethane ug/L 20 90 60-14086 5 3020ND18.1 17.2
Chloroform ug/L 20 105 60-14098 7 3020ND21.0 19.7
Chloromethane ug/L 20 85 60-14080 7 3020ND17.1 15.9
cis-1,2-Dichloroethene ug/L 20 102 60-14096 6 3020ND20.4 19.2
cis-1,3-Dichloropropene ug/L 20 104 60-14099 5 3020ND20.8 19.8
Dibromochloromethane ug/L 20 110 60-140105 5 3020ND21.9 20.9
Dibromomethane ug/L 20 115 60-140110 4 3020ND23.0 22.1
Dichlorodifluoromethane ug/L 20 118 60-140111 7 3020ND23.7 22.2
Diisopropyl ether ug/L 20 93 60-14087 7 3020ND18.5 17.3
Ethanol ug/L 800 87 60-14084 4 30800ND697 669
Ethyl-tert-butyl ether ug/L 40 99 60-14094 6 3040ND39.7 37.4
Ethylbenzene ug/L 20 109 60-140104 5 3020ND21.8 20.8
Hexachloro-1,3-butadiene ug/L 20 134 60-140120 11 3020ND26.8 24.0
Isopropylbenzene
(Cumene)ug/L 20 112 60-140106 6 3020ND22.5 21.1
m&p-Xylene ug/L 40 109 60-140103 6 3040ND43.7 41.1
Methyl-tert-butyl ether ug/L 20 95 60-14091 5 3020ND19.0 18.1
Methylene Chloride ug/L 20 90 60-14084 7 3020ND18.0 16.8
n-Butylbenzene ug/L 20 114 60-140106 8 3020ND22.9 21.2
n-Propylbenzene ug/L 20 109 60-140101 7 3020ND21.8 20.3
Naphthalene ug/L 20 111 60-140106 5 3020ND22.2 21.1
o-Xylene ug/L 20 106 60-140100 5 3020ND21.1 20.1
sec-Butylbenzene ug/L 20 109 60-140101 7 3020ND21.8 20.2
Styrene ug/L 20 109 60-140105 5 3020ND21.9 20.9
tert-Amyl Alcohol ug/L 400 94 60-14089 6 30400ND376 355
tert-Amylmethyl ether ug/L 40 108 60-140103 5 3040ND43.1 41.2
tert-Butyl Alcohol ug/L 200 93 60-14093 1 30200ND187 185
tert-Butyl Formate ug/L 160 87 60-14073 18 30160ND140 116
tert-Butylbenzene ug/L 20 92 60-14085 8 3020ND18.3 16.9
Tetrachloroethene ug/L 20 116 60-140109 6 3020ND23.2 21.9
Toluene ug/L 20 108 60-140104 4 3020ND21.6 20.7
trans-1,2-Dichloroethene ug/L 20 106 60-14099 7 3020ND21.3 19.9
trans-1,3-Dichloropropene ug/L 20 104 60-14099 4 3020ND20.7 19.8
Trichloroethene ug/L 20 117 60-140114 3 3020ND23.4 22.7
Trichlorofluoromethane ug/L 20 112 60-140107 5 3020ND22.4 21.3
Vinyl chloride ug/L 20 85 60-14078 8 3020ND17.0 15.7
1,2-Dichloroethane-d4 (S) %94 70-13094
4-Bromofluorobenzene (S) %96 70-13097
Toluene-d8 (S)%96 70-13096
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
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Huntersville, NC 28078
[phone]
Page 33 of 38
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 34 of 38
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92679292
DOT'S PLACE TOO MOUNT MOURNE N
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92679292001 789623MW-1R SM 6200B
92679292002 789971MW-4 SM 6200B
92679292003 789971MW-5 SM 6200B
92679292004 789971MW-6 SM 6200B
92679292005 790354DW-1 SM 6200B
92679292006 789623WSW-8 SM 6200B
92679292007 789971WSW-9 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2023 10:40 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 38
Page 36 of 38
Page 37 of 38
Page 38 of 38
#=CL#
August 08, 2023
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92681018
92681018
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
DOT'S PLACE TOO
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on August 04, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 2 of 17
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Lab ID Sample ID Matrix Date Collected Date Received
92681018001 WSW-8 Water 08/04/23 15:10 08/04/23 15:36
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92681018001 WSW-8 EPA 504.1 2 PASI-CHH
SM 6200B 69 PASI-CTMH
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Sample: WSW-8 Lab ID: 92681018001 Collected: 08/04/23 15:10 Received: 08/04/23 15:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.0055 ug/L 08/07/23 21:40 106-93-408/07/23 10:310.019 0.0055 1
Surrogates
1-Chloro-2-bromopropane (S)70 %08/07/23 21:40 301-79-5608/07/23 10:3170-130 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <7.4 ug/L 08/07/23 15:10 75-85-4100 7.4 1
tert-Amylmethyl ether <0.12 ug/L 08/07/23 15:10 994-05-810.0 0.12 1
Benzene <0.079 ug/L 08/07/23 15:10 71-43-20.50 0.079 1
Bromobenzene <0.14 ug/L 08/07/23 15:10 108-86-10.50 0.14 1
Bromochloromethane <0.094 ug/L 08/07/23 15:10 74-97-50.50 0.094 1
Bromodichloromethane <0.17 ug/L 08/07/23 15:10 75-27-40.50 0.17 1
Bromoform <0.20 ug/L 08/07/23 15:10 75-25-20.50 0.20 1
Bromomethane <0.22 ug/L 08/07/23 15:10 74-83-95.0 0.22 1
tert-Butyl Alcohol <4.1 ug/L 08/07/23 15:10 75-65-050.0 4.1 1
n-Butylbenzene <0.066 ug/L 08/07/23 15:10 104-51-80.50 0.066 1
sec-Butylbenzene <0.085 ug/L 08/07/23 15:10 135-98-80.50 0.085 1
tert-Butylbenzene <0.086 ug/L 08/07/23 15:10 98-06-60.50 0.086 1
tert-Butyl Formate <0.30 ug/L 08/07/23 15:10 762-75-450.0 0.30 1
Carbon tetrachloride <0.17 ug/L 08/07/23 15:10 56-23-50.50 0.17 1
Chlorobenzene <0.085 ug/L 08/07/23 15:10 108-90-70.50 0.085 1
Chloroethane <0.17 ug/L 08/07/23 15:10 75-00-31.0 0.17 1
Chloroform 0.22J ug/L 08/07/23 15:10 67-66-30.50 0.069 1
Chloromethane <0.18 ug/L 08/07/23 15:10 74-87-31.0 0.18 1
2-Chlorotoluene <0.13 ug/L 08/07/23 15:10 95-49-80.50 0.13 1
4-Chlorotoluene <0.096 ug/L 08/07/23 15:10 106-43-40.50 0.096 1
1,2-Dibromo-3-chloropropane <0.18 ug/L 08/07/23 15:10 96-12-81.0 0.18 1
Dibromochloromethane <0.15 ug/L 08/07/23 15:10 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)<0.15 ug/L 08/07/23 15:10 106-93-40.50 0.15 1
Dibromomethane <0.19 ug/L 08/07/23 15:10 74-95-30.50 0.19 1
1,2-Dichlorobenzene <0.094 ug/L 08/07/23 15:10 95-50-10.50 0.094 1
1,3-Dichlorobenzene <0.098 ug/L 08/07/23 15:10 541-73-10.50 0.098 1
1,4-Dichlorobenzene <0.090 ug/L 08/07/23 15:10 106-46-70.50 0.090 1
Dichlorodifluoromethane <0.12 ug/L 08/07/23 15:10 75-71-80.50 0.12 1
1,1-Dichloroethane <0.056 ug/L 08/07/23 15:10 75-34-30.50 0.056 1
1,2-Dichloroethane <0.11 ug/L 08/07/23 15:10 107-06-20.50 0.11 1
1,1-Dichloroethene <0.079 ug/L 08/07/23 15:10 75-35-40.50 0.079 1
cis-1,2-Dichloroethene <0.11 ug/L 08/07/23 15:10 156-59-20.50 0.11 1
trans-1,2-Dichloroethene <0.10 ug/L 08/07/23 15:10 156-60-50.50 0.10 1
1,2-Dichloropropane <0.14 ug/L 08/07/23 15:10 78-87-50.50 0.14 1
1,3-Dichloropropane <0.085 ug/L 08/07/23 15:10 142-28-90.50 0.085 1
2,2-Dichloropropane <0.12 ug/L 08/07/23 15:10 594-20-70.50 0.12 1
1,1-Dichloropropene <0.066 ug/L 08/07/23 15:10 563-58-60.50 0.066 1
cis-1,3-Dichloropropene <0.090 ug/L 08/07/23 15:10 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene <0.13 ug/L 08/07/23 15:10 10061-02-60.50 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Sample: WSW-8 Lab ID: 92681018001 Collected: 08/04/23 15:10 Received: 08/04/23 15:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Diisopropyl ether <0.072 ug/L 08/07/23 15:10 108-20-30.50 0.072 1
Ethanol <5.0 ug/L 08/07/23 15:10 64-17-5200 5.0 1
Ethylbenzene <0.081 ug/L 08/07/23 15:10 100-41-40.50 0.081 1
Ethyl-tert-butyl ether <0.11 ug/L 08/07/23 15:10 637-92-310.0 0.11 1
Hexachloro-1,3-butadiene <0.35 ug/L 08/07/23 15:10 87-68-32.0 0.35 1
Isopropylbenzene (Cumene)<0.11 ug/L 08/07/23 15:10 98-82-80.50 0.11 1
Methylene Chloride <1.9 ug/L 08/07/23 15:10 75-09-22.0 1.9 1
Methyl-tert-butyl ether <0.053 ug/L 08/07/23 15:10 1634-04-40.50 0.053 1
Naphthalene <0.10 ug/L 08/07/23 15:10 91-20-32.0 0.10 1
n-Propylbenzene <0.10 ug/L 08/07/23 15:10 103-65-10.50 0.10 1
Styrene <0.14 ug/L 08/07/23 15:10 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane <0.091 ug/L 08/07/23 15:10 630-20-60.50 0.091 1
1,1,2,2-Tetrachloroethane <0.074 ug/L 08/07/23 15:10 79-34-50.50 0.074 1
Tetrachloroethene <0.086 ug/L 08/07/23 15:10 127-18-40.50 0.086 1
Toluene <0.090 ug/L 08/07/23 15:10 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene <0.12 ug/L 08/07/23 15:10 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene <0.16 ug/L 08/07/23 15:10 120-82-12.0 0.16 1
1,1,1-Trichloroethane <0.11 ug/L 08/07/23 15:10 71-55-60.50 0.11 1
1,1,2-Trichloroethane <0.096 ug/L 08/07/23 15:10 79-00-50.50 0.096 1
Trichloroethene <0.17 ug/L 08/07/23 15:10 79-01-60.50 0.17 1
Trichlorofluoromethane <0.14 ug/L 08/07/23 15:10 75-69-41.0 0.14 1
1,2,3-Trichloropropane <0.17 ug/L 08/07/23 15:10 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene <0.031 ug/L 08/07/23 15:10 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene <0.071 ug/L 08/07/23 15:10 108-67-80.50 0.071 1
Vinyl chloride <0.15 ug/L 08/07/23 15:10 75-01-41.0 0.15 1
m&p-Xylene <0.094 ug/L 08/07/23 15:10 179601-23-11.0 0.094 1
o-Xylene <0.14 ug/L 08/07/23 15:10 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %08/07/23 15:10 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %08/07/23 15:10 460-00-470-130 1
Toluene-d8 (S)104 %08/07/23 15:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Page 6 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791870
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92681018001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4103460
Associated Lab Samples:92681018001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.091 0.50 08/07/23 13:580.091
1,1,1-Trichloroethane ug/L <0.11 0.50 08/07/23 13:580.11
1,1,2,2-Tetrachloroethane ug/L <0.074 0.50 08/07/23 13:580.074
1,1,2-Trichloroethane ug/L <0.096 0.50 08/07/23 13:580.096
1,1-Dichloroethane ug/L <0.056 0.50 08/07/23 13:580.056
1,1-Dichloroethene ug/L <0.079 0.50 08/07/23 13:580.079
1,1-Dichloropropene ug/L <0.066 0.50 08/07/23 13:580.066
1,2,3-Trichlorobenzene ug/L <0.12 2.0 08/07/23 13:580.12
1,2,3-Trichloropropane ug/L <0.17 0.50 08/07/23 13:580.17
1,2,4-Trichlorobenzene ug/L <0.16 2.0 08/07/23 13:580.16
1,2,4-Trimethylbenzene ug/L <0.031 0.50 08/07/23 13:580.031
1,2-Dibromo-3-chloropropane ug/L <0.18 1.0 08/07/23 13:580.18
1,2-Dibromoethane (EDB)ug/L <0.15 0.50 08/07/23 13:580.15
1,2-Dichlorobenzene ug/L <0.094 0.50 08/07/23 13:580.094
1,2-Dichloroethane ug/L <0.11 0.50 08/07/23 13:580.11
1,2-Dichloropropane ug/L <0.14 0.50 08/07/23 13:580.14
1,3,5-Trimethylbenzene ug/L <0.071 0.50 08/07/23 13:580.071
1,3-Dichlorobenzene ug/L <0.098 0.50 08/07/23 13:580.098
1,3-Dichloropropane ug/L <0.085 0.50 08/07/23 13:580.085
1,4-Dichlorobenzene ug/L <0.090 0.50 08/07/23 13:580.090
2,2-Dichloropropane ug/L <0.12 0.50 08/07/23 13:580.12
2-Chlorotoluene ug/L <0.13 0.50 08/07/23 13:580.13
4-Chlorotoluene ug/L <0.096 0.50 08/07/23 13:580.096
Benzene ug/L <0.079 0.50 08/07/23 13:580.079
Bromobenzene ug/L <0.14 0.50 08/07/23 13:580.14
Bromochloromethane ug/L <0.094 0.50 08/07/23 13:580.094
Bromodichloromethane ug/L <0.17 0.50 08/07/23 13:580.17
Bromoform ug/L <0.20 0.50 08/07/23 13:580.20
Bromomethane ug/L <0.22 5.0 08/07/23 13:580.22
Carbon tetrachloride ug/L <0.17 0.50 08/07/23 13:580.17
Chlorobenzene ug/L <0.085 0.50 08/07/23 13:580.085
Chloroethane ug/L <0.17 1.0 08/07/23 13:580.17
Chloroform ug/L <0.069 0.50 08/07/23 13:580.069
Chloromethane ug/L <0.18 1.0 08/07/23 13:580.18
cis-1,2-Dichloroethene ug/L <0.11 0.50 08/07/23 13:580.11
cis-1,3-Dichloropropene ug/L <0.090 0.50 08/07/23 13:580.090
Dibromochloromethane ug/L <0.15 0.50 08/07/23 13:580.15
Dibromomethane ug/L <0.19 0.50 08/07/23 13:580.19
Dichlorodifluoromethane ug/L <0.12 0.50 08/07/23 13:580.12
Diisopropyl ether ug/L <0.072 0.50 08/07/23 13:580.072
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Page 7 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4103460
Associated Lab Samples:92681018001
Matrix: Water
AnalyzedMDL
Ethanol ug/L <5.0 200 08/07/23 13:585.0
Ethyl-tert-butyl ether ug/L <0.11 10.0 08/07/23 13:580.11
Ethylbenzene ug/L <0.081 0.50 08/07/23 13:580.081
Hexachloro-1,3-butadiene ug/L <0.35 2.0 08/07/23 13:580.35
Isopropylbenzene (Cumene)ug/L <0.11 0.50 08/07/23 13:580.11
m&p-Xylene ug/L <0.094 1.0 08/07/23 13:580.094
Methyl-tert-butyl ether ug/L <0.053 0.50 08/07/23 13:580.053
Methylene Chloride ug/L <1.9 2.0 08/07/23 13:581.9
n-Butylbenzene ug/L <0.066 0.50 08/07/23 13:580.066
n-Propylbenzene ug/L <0.10 0.50 08/07/23 13:580.10
Naphthalene ug/L <0.10 2.0 08/07/23 13:580.10
o-Xylene ug/L <0.14 0.50 08/07/23 13:580.14
sec-Butylbenzene ug/L <0.085 0.50 08/07/23 13:580.085
Styrene ug/L <0.14 0.50 08/07/23 13:580.14
tert-Amyl Alcohol ug/L <7.4 100 08/07/23 13:587.4
tert-Amylmethyl ether ug/L <0.12 10.0 08/07/23 13:580.12
tert-Butyl Alcohol ug/L <4.1 50.0 08/07/23 13:584.1
tert-Butyl Formate ug/L <0.30 50.0 08/07/23 13:580.30
tert-Butylbenzene ug/L <0.086 0.50 08/07/23 13:580.086
Tetrachloroethene ug/L <0.086 0.50 08/07/23 13:580.086
Toluene ug/L <0.090 0.50 08/07/23 13:580.090
trans-1,2-Dichloroethene ug/L <0.10 0.50 08/07/23 13:580.10
trans-1,3-Dichloropropene ug/L <0.13 0.50 08/07/23 13:580.13
Trichloroethene ug/L <0.17 0.50 08/07/23 13:580.17
Trichlorofluoromethane ug/L <0.14 1.0 08/07/23 13:580.14
Vinyl chloride ug/L <0.15 1.0 08/07/23 13:580.15
1,2-Dichloroethane-d4 (S)%95 70-130 08/07/23 13:58
4-Bromofluorobenzene (S)%94 70-130 08/07/23 13:58
Toluene-d8 (S)%105 70-130 08/07/23 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103461LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.620 103 60-140
1,1,1-Trichloroethane ug/L 19.220 96 60-140
1,1,2,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,2-Trichloroethane ug/L 19.720 98 60-140
1,1-Dichloroethane ug/L 17.820 89 60-140
1,1-Dichloroethene ug/L 18.420 92 60-140
1,1-Dichloropropene ug/L 17.520 87 60-140
1,2,3-Trichlorobenzene ug/L 20.520 102 60-140
1,2,3-Trichloropropane ug/L 18.520 93 60-140
1,2,4-Trichlorobenzene ug/L 20.320 101 60-140
1,2,4-Trimethylbenzene ug/L 19.920 100 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103461LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 19.020 95 60-140
1,2-Dibromoethane (EDB)ug/L 20.020 100 60-140
1,2-Dichlorobenzene ug/L 20.320 101 60-140
1,2-Dichloroethane ug/L 18.920 94 60-140
1,2-Dichloropropane ug/L 18.720 93 60-140
1,3,5-Trimethylbenzene ug/L 19.820 99 60-140
1,3-Dichlorobenzene ug/L 20.120 100 60-140
1,3-Dichloropropane ug/L 18.820 94 60-140
1,4-Dichlorobenzene ug/L 20.320 101 60-140
2,2-Dichloropropane ug/L 19.420 97 60-140
2-Chlorotoluene ug/L 19.320 96 60-140
4-Chlorotoluene ug/L 19.420 97 60-140
Benzene ug/L 18.920 95 60-140
Bromobenzene ug/L 19.920 99 60-140
Bromochloromethane ug/L 19.920 99 60-140
Bromodichloromethane ug/L 19.620 98 60-140
Bromoform ug/L 16.820 84 60-140
Bromomethane ug/L 25.420 127 60-140
Carbon tetrachloride ug/L 20.820 104 60-140
Chlorobenzene ug/L 19.820 99 60-140
Chloroethane ug/L 19.820 99 60-140
Chloroform ug/L 17.820 89 60-140
Chloromethane ug/L 15.320 76 60-140
cis-1,2-Dichloroethene ug/L 17.720 89 60-140
cis-1,3-Dichloropropene ug/L 19.220 96 60-140
Dibromochloromethane ug/L 20.120 101 60-140
Dibromomethane ug/L 20.220 101 60-140
Dichlorodifluoromethane ug/L 21.120 105 60-140
Diisopropyl ether ug/L 16.120 81 60-140
Ethanol ug/L 652800 81 60-140
Ethyl-tert-butyl ether ug/L 32.240 80 60-140
Ethylbenzene ug/L 19.420 97 60-140
Hexachloro-1,3-butadiene ug/L 21.320 107 60-140
Isopropylbenzene (Cumene)ug/L 20.520 102 60-140
m&p-Xylene ug/L 39.140 98 60-140
Methyl-tert-butyl ether ug/L 16.720 83 60-140
Methylene Chloride ug/L 18.620 93 60-140
n-Butylbenzene ug/L 20.720 104 60-140
n-Propylbenzene ug/L 19.020 95 60-140
Naphthalene ug/L 20.120 101 60-140
o-Xylene ug/L 19.120 96 60-140
sec-Butylbenzene ug/L 19.920 99 60-140
Styrene ug/L 20.120 101 60-140
tert-Amyl Alcohol ug/L 364400 91 60-140
tert-Amylmethyl ether ug/L 36.340 91 60-140
tert-Butyl Alcohol ug/L 169200 84 60-140
tert-Butyl Formate ug/L 135160 84 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103461LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 16.820 84 60-140
Tetrachloroethene ug/L 20.420 102 60-140
Toluene ug/L 18.120 91 60-140
trans-1,2-Dichloroethene ug/L 17.620 88 60-140
trans-1,3-Dichloropropene ug/L 19.420 97 60-140
Trichloroethene ug/L 20.720 104 60-140
Trichlorofluoromethane ug/L 20.220 101 60-140
Vinyl chloride ug/L 15.120 76 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4103462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681011001
4103463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 109 60-140122 11 3020ND21.8 24.4
1,1,1-Trichloroethane ug/L 20 102 60-140115 12 3020ND20.4 22.9
1,1,2,2-Tetrachloroethane ug/L 20 102 60-140111 8 3020ND20.4 22.1
1,1,2-Trichloroethane ug/L 20 103 60-140114 11 3020ND20.6 22.9
1,1-Dichloroethane ug/L 20 97 60-140111 13 3020ND19.5 22.1
1,1-Dichloroethene ug/L 20 107 60-140119 11 3020ND21.4 23.8
1,1-Dichloropropene ug/L 20 109 60-140120 10 3020ND21.8 24.1
1,2,3-Trichlorobenzene ug/L 20 114 60-140129 13 3020ND22.8 25.9
1,2,3-Trichloropropane ug/L 20 95 60-140103 9 3020ND18.9 20.6
1,2,4-Trichlorobenzene ug/L 20 114 60-140125 9 3020ND22.8 25.0
1,2,4-Trimethylbenzene ug/L 20 107 60-140117 9 3020ND21.4 23.4
1,2-Dibromo-3-
chloropropane ug/L 20 101 60-140114 12 3020ND20.1 22.8
1,2-Dibromoethane (EDB) ug/L 20 106 60-140117 10 3020ND21.2 23.4
1,2-Dichlorobenzene ug/L 20 107 60-140118 10 3020ND21.4 23.6
1,2-Dichloroethane ug/L 20 96 60-140108 12 3020ND19.3 21.7
1,2-Dichloropropane ug/L 20 103 60-140115 11 3020ND20.7 23.1
1,3,5-Trimethylbenzene ug/L 20 106 60-140117 10 3020ND21.2 23.5
1,3-Dichlorobenzene ug/L 20 107 60-140117 9 3020ND21.4 23.5
1,3-Dichloropropane ug/L 20 98 60-140110 12 3020ND19.5 21.9
1,4-Dichlorobenzene ug/L 20 106 60-140115 8 3020ND21.2 23.0
2,2-Dichloropropane ug/L 20 104 60-140117 12 3020ND20.9 23.5
2-Chlorotoluene ug/L 20 101 60-140110 9 3020ND20.2 22.1
4-Chlorotoluene ug/L 20 103 60-140111 7 3020ND20.6 22.2
Benzene ug/L 20 102 60-140115 12 3020ND20.5 23.0
Bromobenzene ug/L 20 103 60-140111 7 3020ND20.6 22.1
Bromochloromethane ug/L 20 103 60-140118 13 3020ND20.6 23.6
Bromodichloromethane ug/L 20 99 60-140111 12 3020ND19.8 22.3
Bromoform ug/L 20 106 60-140118 11 3020ND21.2 23.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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[phone]
Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4103462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681011001
4103463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 91 60-14099 8 3020ND18.2 19.8
Carbon tetrachloride ug/L 20 109 60-140121 10 3020ND21.8 24.2
Chlorobenzene ug/L 20 104 60-140112 7 3020ND20.8 22.4
Chloroethane ug/L 20 87 60-14097 12 3020ND17.3 19.4
Chloroform ug/L 20 98 60-140108 9 3020ND19.7 21.6
Chloromethane ug/L 20 85 60-14096 13 3020ND17.0 19.3
cis-1,2-Dichloroethene ug/L 20 99 60-140110 11 3020ND19.8 22.0
cis-1,3-Dichloropropene ug/L 20 101 60-140113 11 3020ND20.2 22.5
Dibromochloromethane ug/L 20 103 60-140114 10 3020ND20.6 22.8
Dibromomethane ug/L 20 110 60-140120 8 3020ND22.0 23.9
Dichlorodifluoromethane ug/L 20 95 60-140106 11 3020ND19.0 21.2
Diisopropyl ether ug/L 20 91 60-140106 15 3020ND18.1 21.1
Ethanol ug/L 800 85 60-14094 9 30800ND683 748
Ethyl-tert-butyl ether ug/L 40 86 60-14099 14 3040ND34.3 39.5
Ethylbenzene ug/L 20 102 60-140108 6 3020ND20.4 21.6
Hexachloro-1,3-butadiene ug/L M12012960-140148 14 3020ND25.7 29.6
Isopropylbenzene
(Cumene)ug/L 20 108 60-140116 8 3020ND21.5 23.2
m&p-Xylene ug/L 40 102 60-140109 7 3040ND40.9 43.7
Methyl-tert-butyl ether ug/L 20 88 60-140102 15 3020ND17.7 20.5
Methylene Chloride ug/L 20 89 60-140102 13 3020ND17.9 20.3
n-Butylbenzene ug/L 20 115 60-140128 11 3020ND23.0 25.6
n-Propylbenzene ug/L 20 104 60-140114 9 3020ND20.8 22.8
Naphthalene ug/L 20 106 60-140119 12 3020ND21.1 23.8
o-Xylene ug/L 20 104 60-140112 7 3020ND20.7 22.3
sec-Butylbenzene ug/L 20 108 60-140122 12 3020ND21.6 24.4
Styrene ug/L 20 104 60-140111 7 3020ND20.7 22.2
tert-Amyl Alcohol ug/L 400 87 60-14099 13 30400ND347 395
tert-Amylmethyl ether ug/L 40 95 60-140107 12 3040ND38.0 43.0
tert-Butyl Alcohol ug/L 200 86 60-140104 19 30200ND172 208
tert-Butyl Formate ug/L 160 72 60-14071 1 30160ND115 114
tert-Butylbenzene ug/L 20 89 60-140101 13 3020ND17.7 20.2
Tetrachloroethene ug/L 20 113 60-140116 2 3020ND22.7 23.3
Toluene ug/L 20 100 60-140110 9 3020ND20.1 22.0
trans-1,2-Dichloroethene ug/L 20 102 60-140115 11 3020ND20.4 22.9
trans-1,3-Dichloropropene ug/L 20 99 60-140111 11 3020ND19.8 22.2
Trichloroethene ug/L 20 112 60-140123 9 3020ND22.4 24.5
Trichlorofluoromethane ug/L 20 101 60-140110 8 3020ND20.2 21.9
Vinyl chloride ug/L 20 79 60-14090 13 3020ND15.9 18.0
1,2-Dichloroethane-d4 (S) %91 70-13096
4-Bromofluorobenzene (S) %98 70-13096
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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[phone]
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
791790
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92681018001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4103039
Associated Lab Samples:92681018001
Matrix: Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L <0.0056 0.020 08/07/23 15:140.0056
1-Chloro-2-bromopropane (S)%91 70-130 08/07/23 15:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4103040LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
4103041
1,2-Dibromoethane (EDB)ug/L 0.260.25 104 70-130880.22 17 20
1-Chloro-2-bromopropane (S)%122 70-130102
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4103043MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92680612002
4103044
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB) ug/L 0.24 92 65-13591 0 200.24ND 0.22 0.22
1-Chloro-2-bromopropane
(S)
%102 70-13099
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92680612001
4103042SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L <0.0055 20ND
1-Chloro-2-bromopropane (S)%108107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Page 12 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Huntersville, NC 28078
[phone]
Page 13 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92681018
DOT'S PLACE TOO
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92681018001 791790 791921WSW-8 EPA 504.1 EPA 504.1
92681018001 791870WSW-8 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2023 04:52 PM
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Huntersville, NC 28078
[phone]
Page 14 of 17
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