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HomeMy WebLinkAboutAS-3656_28791_CA_MRP_20231115_LSAA CONSULTECH ENVIRONMENTAL, LLC. P.O. Box 5306, Cary, NC 27512 (919) 234-4238, (919) 234-4239 Fax November 10, 2023 North Carolina Department of Environmental Quality Division of Waste Management, UST Section 1628 Mail Service Center Raleigh, NC 27699-1628 Attention: Mr. Scott Ryals Reference:Limited Site Assessment Report Former Kwik Stop #1 1024 South Trade Street, Tryon, Polk County, NC Incident No: 28791 Dear Mr. Ryals: Please find attached a Limited Site Assessment report for the above referenced facility. Please contact the undersigned if you have any questions or comments regarding the report. Respectively, Consultech Environmental, LLC. John D. Liebig Project Manager B CONSULTECH ENVIRONMENTAL, LLC. P.O. Box 5306, Cary, NC 27512 (919) 234-4238, (919) 234-4239 Fax Prepared by: Consultech Environmental, LLC. 2021 Energy Drive Apex, NC 27502 November 10, 2023 LIMITED SITE ASSESSMENT REPORT Former Kwik Stop #1 1024 South Trade Street Tryon,Polk County, North Carolina NCDEQ Incident No: 28791 i 2. Contact Information UST Owner/Operator: Address: Burrell’s Fuels, Inc. 231 North Trade Street Tryon, NC 28782 Tel:(828) 859-5875 Property Owner:Fredia and John Belk 14 Yancy Drive, Greenville, SC 29615 Consultant/Contractor:Consultech Environmental, LLC. Address: Tel: 2021 Energy Drive Apex, NC 27502 (919) 234-4238 Analytical Laboratory:Eurofins Test America. Cert # 314 Address: Tel: 3355 McLemore Drive Pensacola, FL 32514 (854) 474-1001 3. Information about Release Date Discovered:01/16/2009 Estimated Quantity of Release:Unknown Cause of Release:Leaks at gasoline pumps / dispensers Source of Release (Dispenser/Piping/UST):Piping/Dispensers for Gasoline Size and Contents of UST System(s) from which the release occurred: 8000-Gallon Gasoline USTs Criteria Used to Classify Risk 4. Certification Certification: Jeffrey L. Gerlock, L.G. I, ___________________, a Licensed Geologist (#1141) with Consultech Environmental, LLC, do certify that the information contained in this report is correct and accurate to the best of my knowledge. Consultech Environmental, LLC is licensed to practice geology in the State of North Carolina. Consultech Environmental, LLC currently holds North Carolina Corporate Geology license number C-0497 A SITE INFORMATION 1. Site Identification Former Kwik Stop #1 1024 South Trade Street Tryon,Polk County, North Carolina Date of Report:November 10, 2023 Facility I.D.:UST Incident No.: 28791 Site Risk:Unknown Land Use Classification: Commercial Site Name (NCDEQ Incident Name): Former Kwik Stop #1 Site Street Address:1024 South Trade Street City/Town:Tryon Zip Code:28782 County:Polk Description of Geographical Data Point:Approximate center of property Location Method:Google Earth Latitude (decimal degrees):N 35.197238 Longitude (decimal degrees):W -82.229932 ii B EXECUTIVE SUMMARY The following Limited Site Assessment (LSA) report was prepared by Consultech Environmental, LLC. (Consultech) for the Kwik Stop #1 (site) located at 1024 South Trade Street in Tryon, North Carolina. This LSA has been prepared to address the release of petroleum hydrocarbon compounds from an underground storage tank (UST) system that was located on the site. The site previously contained three 8000-gallon gasoline, one 2000-gallon diesel, and on 2000-gallon kerosene USTs operated by Burrell’s Fuels Inc. The USTs were removed from the site in November 2008. Soil samples collected beneath the UST systems indicated that petroleum impacted soil was present in the vicinity of the former pump island / dispensers for the gasoline USTs. The release was assigned Incident Number 28791 by the NCDEQ) UST Section. The results of the LSA are summarized below: Type of Contaminant Gasoline Source of Release Dispensers / Pump island Amount of Release Unknown Initial Abatement/Emergency Response Information None Hydrogeology Groundwater was encountered at 20 and 15 feet below ground surface (BGS) in wells MW-1 and MW-2, respectively. Soil and Groundwater Assessment Soil samples collected during the UST closure indicated gasoline and diesel range TPH concentrations above the State action levels in three of the twenty-one samples. The most impacted samples were located at the dispensers / pump island for the gasoline / diesel USTs. Low concentrations of several VOCs, VPH fractions, chromium, and lead were detected in one or more of the soil samples collected in the two borings drilled in the former source areas. No VOCs, SVOCs, VPH, or EPH were detected in the soil samples during this LSA at concentrations above the Soil to Water MSCCs. Chromium was detected in several of the soil samples in borings MW- 1 and MW-2 at concentrations above the soil to groundwater MSCCs. Chromium is naturally occurring in site soils. No constituents were detected in site soils at concentrations above the Residential or Commercial / Industrial MSCCs. Low concentrations of one VOC, three SVOCs, lead, and C9-C10 Aromatics were detected in the groundwater sample from well MW-1; none of the analyzed parameters were detected at concentrations above the 2L Groundwater standards. Low concentrations of several VOCs, one SVOC, lead, C9-C12 Aliphatics, and C9-C10 Aromatics were detected in the sample from well MW-2. Dibromochloromethane was the only constituent detected in the groundwater in well MW- 2 at a concentration above the 2L Standard. Dibromochloromethane is a common laboratory contaminant and its presence may not be indicative of groundwater impact. None of the analyzed parameters were detected in the groundwater from the two wells at concentrations above the GCLs. Risk Classification Low iii Current Soil and Groundwater Remediation Standards Soil: Soil to Groundwater MSCC. Groundwater: North Carolina Administrative Code, Title 15A, Department of Environmental Quality, Subchapter 2L, Classifications and Water Quality Standards Applicable to the Groundwaters of North Carolina, Revised April 1, 2023 (NC 2L groundwater standards). Recommendations No Further Action with a Notice of Residual Petroleum (NORP). iv C TABLE OF CONTENTS A SITE INFORMATION ............................................................................................I B EXECUTIVE SUMMARY......................................................................................II C TABLE OF CONTENTS......................................................................................IV D SITE HISTORY AND SOURCE CHARACTERIZATION......................................5 D.1 OWNER-OPERATOR INFORMATION ................................................................................ 5 D.2 UST SYSTEM INFORMATION.......................................................................................... 5 D.3 NON-UST INFORMATION............................................................................................... 5 D.4 PREVIOUS SITE ASSESSMENT ACTIVITY......................................................................... 5 D.5 SITE AND VICINITY CHARACTERISTICS (LAND USE OF THE SITE AND SURROUNDING AREA, TOPOGRAPHY,VEGETATION,SURFACE WATER,WELLS,BUILDINGS,SURFACE COVER,SOIL TYPE,DEPTH TO AND NATURE OF BEDROCK,DEPTH TO GROUNDWATER,DIRECTION OF GROUNDWATER FLOW).................................................................................................. 5 D.6 SUMMARY OF ABATEMENT ACTIONS,ASSESSMENT REPORTS AND CORRECTIVE ACTIONS6 E RISK CHARACTERIZATION...............................................................................6 F RECEPTOR INFORMATION ...............................................................................8 F.1 WATER SUPPLY WELLS................................................................................................ 8 F.2 PUBLIC WATER SUPPLIES ............................................................................................ 8 F.3 SURFACE WATER......................................................................................................... 8 F.4 WELLHEAD PROTECTION AREAS................................................................................... 8 F.5 DEEP AQUIFERS OF THE COASTAL PLAIN PHYSIOGRAPHIC PROVINCE ............................ 8 F.6 SUBSURFACE STRUCTURES.......................................................................................... 8 G LAND USE...........................................................................................................9 G.1 PROPERTY OWNERS AND OCCUPANTS.......................................................................... 9 H SITE GEOLOGY AND HYDROGEOLOGY..........................................................8 I SAMPLING RESULTS.........................................................................................8 J CONCLUSIONS AND RECOMMENDATIONS....................................................9 TABLES Table 1 Receptor Information Table 2 Property Owners/Occupants Table 3 Soil Analytical Results Table 4 Groundwater Analytical Results FIGURES Figure 1 Site Location Map Figure 2 Site Map Figure 3 Receptor Map LIST OF APPENDICES APPENDIX A Laboratory Analytical Reports APPENDIX B Well Construction Records 5 D SITE HISTORY AND SOURCE CHARACTERIZATION The site is located at 1024 South Trade Street in Tryon, North Carolina. The property location is shown on Figure 1. A.1 Owner-Operator Information The former operator of the UST is Burrell’s Fuels Inc. located at 231 North Trade Street in Tryon, North Carolina. There is no specific contact; the phone number is listed as (828) 859-5875. A.2 UST System Information Kwik Stop #1 was located at the subject site (currently an empty lot). Three 8,000-gallon gasoline, one 2000-gallon diesel, and one 2000-gallon kerosene USTs operated by Burrell’s Fuels Inc. were located at the site until they were removed from the property in November 2008. Soil sampling conducted at the time of the tank removal indicated gasoline and diesel range TPH concentrations above the State action levels in three of the twenty-one samples. The impacted soil was located in the samples collected at the former location of the gasoline pump island / dispensers. A.3 Non-UST Information No information wasfound in the conductance of the LSA that indicated the presence of aboveground storage tanks. A.4 Previous Site Assessment Activity In December 2008 Advanced Environmental Solutions collected soil samples in the former UST basins and at the former pump islands. Gasoline range and diesel range total petroleum hydrocarbons (TPH) were detected in three of the twenty-one soil samples collected beneath the former UST systems. TPH-GRO was detected at concentrations of 9390 and 84.1 milligrams per kilogram (mg/kg) and TPH-DRO was detected at concentrations of 258, 1560, and 19,900 mg/kg. The TPH-GRO action level was 50 mg/kg and the TPH-DRO action level was 100 mg/kg. No reports or recommendations were made aside from the tank closure form and a memo containing the soil sampling results. A.5 Site and Vicinity Characteristics (land use of the site and surrounding area, topography, vegetation, surface water, wells, buildings, surface cover, soil type, depthtoandnatureofbedrock, depthtogroundwater,directionofgroundwaterflow). The site is located at 1024 South Trade Street in Tryon, North Carolina. The site is currently an empty gravel lot; no buildings are located on the property. The site contains no structures aside from the concrete pad from the old convenience store and the asphalt driveway. The property around the site is amix of residentialand commercialproperties. Residential propertiesare locatedtothesouth. The topography in the region is relatively flat around the site with mountainous terrain to the south of the property. The surrounding area slopes to the southeast and southwest. Lake Lanier is located south of the site. During the boring of MW-1, fill material was encountered at 5 feet bgs, rocky fill and brown sandy soil was encountered at 10 feet bgs, brown to dark brown moist sandy soil was encountered at 15 feet bgs, and Brown mud and water was encountered at 20 feet bgs. Groundwater was encountered at 20 feet bgs and MW-1 was set at 25 feet. During the boring of MW-2, brown sandy clay was encountered at 5 feet bgs, brown to gray moist sandy clay soil was encountered at 10 feet bgs, and 6 brown moist clay soil was encountered at 15 feet bgs. Groundwater was encountered at 15 feet bgs andMW-2 wassetat20feet. Thesiteislocatedinavalleywithhilly/mountainousterrain surrounding it and groundwater flow is likely to the south. The site and surrounding properties utilize public water for drinking purposes. The sites relation to the surrounding property can be seen in Figure 3. A.6 Summary of Abatement Actions, Assessment Reports and Corrective Actions No previous abatement actions are known to have occurred. E RISK CHARACTERIZATION Limited Site Assessment Risk Classification and Land Use Form Part I – Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the release contaminated any water supply well including any well used for non- drinking purposes?NO 2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release?NO 3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of the release?NO 4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there is no other source of water supply other than the groundwater)?NO 5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment?NO If yes, describe.Not applicable. 6. Are there any other factors that would cause the release to pose an imminent danger to public health, public safety, or the environment?NO If yes, describe. Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the release?NO If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?NO 8. Is the source area of the release located within an approved or planned wellhead protection area as defined in 42 USC 300h-7(e)? NO If yes, describe.Not applicable. 9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology of North Carolina” published by the Department in 1985?NO If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of drinking water?No 7 10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels established by the Department?NO Part II - Land Use Property Containing Source Area of Release The questions below pertain to the property containing the source area of the release. 1. Does the property contain one or more primary or secondary residences (permanent or temporary)?NO Describe. 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly?NO Describe. 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped?NO Describe. 4. Do children visit the property?NO Explain. 5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)?NO Explain. The site is an empty lot with access from the main road. 6. Do pavement, buildings, or other structures cap the contaminated soil?NO Describe. If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future? What is the zoning status of the property? Commercial 7. Is the use of the property likely to change in the next 20 years?YES Explain. As the property is an empty lot, development is likely to happen in the next 20 years. Property Surrounding Source Area of Release The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing source area of the release): 1. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)? 300 feet south of the former tank basins. 8 2. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? Lake Lanier is located 1200 feet southwest of the site and is used for recreational purposes. 3. What is the zoning status of properties in the surrounding area? West: Commercial North: Commercial East: Commercial South: Residential 4. Briefly characterize the use and activities of the land in the surrounding area. Surrounding properties are utilized for both residential and commercial purposes. There are stores and restaurants located within close proximity to the site to the east, west, and north. Residences are located south, southeast, and southwest of the site. Land use and property owners/occupant information is Included in Table 2. F RECEPTOR INFORMATION A.7 Water Supply Wells No water supply wells were observed within 1,500 feet of the site. A.8 Public Water Supplies The site and adjoining properties are connected to the municipal / public water supply system. A.9 Surface Water Six surface water features are located within 1,500 feet of the site. Lake Lanier is located approximately 1,200 feet southwest of the site. Vaughn Creek is located within 500 feet of the site and its associated unnamed tributaries are located within 1500 feet of the site. Surface water information is summarized in Table 1 and the surface water locations are shown on Figure 3. A.10 Wellhead Protection Areas Wellhead Protection Areas are administered by the North Carolina Division of Environmental Quality, Public Water Supply (PWS) Section. According to the PWS, no Wellhead Protection Areas are located within 1,500 feet of the source area. A.11 Deep Aquifers of the Coastal Plain Physiographic Province The site property is not located in the Coastal Plain Physiographic Province. A.12 Subsurface Structures There is no basement at the site. The underground utilities at the site include underground/above ground electrical lines, water lines, and sanitary sewer lines. The utilities are located outside of the former UST locations. 9 G LAND USE A.13 Property Owners and Occupants The site is owned by Fredia and John Belk; there are no permanent occupants. A list of the adjacent property owners is Included in Table 2. H SITE GEOLOGY AND HYDROGEOLOGY According to the 1985 Geologic Map of North Carolina, underlying geology the site is located in the inner piedmont belt and consists of metamorphic rock with biotite gneiss and schist. Soil encountered at the site consisted of brown sandy soil from 4’-6’, brown sandy soil with intermittent rocks from 9’-11’, and brown clay from 14’-16’. Groundwater was encountered at 20 and 15 feet. Based on the topographic map of the area, the estimated groundwater flow direction is to the south and southeast. I SAMPLING RESULTS On October 10, 2023, South Atlantic Environmental Drilling and Construction Company (SAEDACCO) drilled two soil borings and installed monitoring wells within the former gasoline and diesel tank basin (MW-1) and near the former gasoline and diesel pump island (MW-2). The borings were drilled using hollow stem augers to a depth of 25 feet and 20 feet respectively. The soil boring/well locations are shown on Figure 2. On October 10, 2023 soil samples were collected from boring MW-1 at five-foot intervals (10, 15, and 20 feet) and from boring MW-2 at five-foot intervals (5, 10, and 15 feet). The soil samples were placed into appropriate laboratory- supplied containers, the samples were then placed on ice in a cooler, and shipped under chain- of-custody to Eurofins Environment Testing in Pensacola, FL for analysis for volatile organic compounds (VOCs) by EPA Method 8260, semi-VOCs by Method 8270, volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH) by the MADEP method. Three VOCs (acetone, toluene, 2-butanone), chromium, lead, and one VPH fraction (C19-C36 Aliphatics) were detected in the soil sample from 10 feet bgs in MW-1 at concentrations of 0.0879, 0.00134, 0.00688, 43.5, 8.7, and 12.3 mg/kg. No VOCs were detected in the soil sample from 15 feet bgs in boring MW-1. One VPH (C19-C36 Aliphatics) was detected in the soil sample from 15 feet bgs at a concentration of 7.24 mg/kg. One VOC (acetone), chromium, and lead were detected in the soil sample from 20 feet bgs in boring MW-1 at concentrations of 0.061, 15.7, and 6.87 mg/kg. No VPHs were detected in the soil sample from 20 feet bgs. No SVOCs or EPH were detected in the soil samples. Chromium was the only constituent detected in the soil samples in boring MW-1 at concentrations above the Soil to Water MSCCs. One VOC (acetone), chromium, lead, and two VPH fractions (C9-C18 Aliphatics and C19-C36 Aliphatics) were detected in the soil sample from 5 feet bgs in well MW-2 at concentrations of 0.0427, 32.8, 14.2, 15.5, and 3.43 mg/kg. No VOCs were detected in the soil sample from 10 feet bgs in well MW-2; two VPH fractions (C9-C18 Aliphatics and C19-C36 Aliphatics) were detected in the soil sample from 10 feet bgs at concentrations of 10.5 and 7.22 mg/kg. One VOC (acetone), chromium, lead, and one VPH fraction (C9-C10 aromatics) were detected in the soil sample from 15 feet bgs at concentrations of 0.0514, 20.4, 8.88, and 2.59 mg/kg. No SVOCs or EPH were detected in the soil samples. Chromium was the only constituent detected in the soil samples in boring MW-2 at concentrations above the Soil to Water MSCCs. Soil analytical data is summarized in Table 3 and the soil laboratory analytical report is contained in Appendix A. 10 Groundwater was encountered in boring MW-1 at 20 feet. On October 10, 2023 SAEDACCO installed a monitoring well in the boring to a depth of 25 feet; the well included a screened interval from 8 to 18 feet bgs. The well construction record is presented in Appendix B. A water sample was collected from the well on October 10, 2023 using a new polyethylene bailer. The sample was placed into appropriate laboratory- supplied containers, the samples were then placed on ice, and shipped under chain-of-custody to Eurofins Environment Testing in Pensacola, FL for analysis for VOCs by EPA Method 6200, semi-VOCs by Method 625, VPH and EPH by the MADEP method, and Lead by the SW 846 6010D Method. Groundwater was encountered in boring MW-2 at 15 feet. On October 10, 2023 SAEDACCO installed a monitoring well in the boring to a depth of 20 feet; the well included a screened interval from 9 to 19 feet bgs. The well construction record is presented in Appendix B. A water sample was collected from the well on October 10, 2023 using a new polyethylene bailer. The sample was placed into appropriate laboratory- supplied containers, the samples were then placed on ice, and shipped under chain-of-custody to Eurofins Environment Testing in Pensacola, FL for analysis for VOCs by EPA Method 6200, SVOCs by Method 625, VPH and EPH by the MADEP method, and Lead by the SW 846 6010D Method. One VOC (2-hexanone), three SVOCs (Benzoic acid, Diethyl phthalate, Phenol) and lead were detected in the groundwater sample from well MW-1 at concentrations ranging from 0.692 to 15.9 micrograms per liter - ug/L). One VPH fraction (C9-C10 Aromatics) was detected in the groundwater sample in well MW-1 at a concentration of 12.3 ug/L. EPH was not detected in the sample. None of the analyzed parameters were detected in the groundwater sample from well MW-1 at concentrations above the NCAC 2L groundwater quality standards or the Gross Contaminant Levels (GCLs). One SVOC (Diethyl phthalate), six VOCs (Bromodichloromethane, Bromoform, Chloroform, Dibromochloromethane, 2-hexanone, 4-Methyl-2-pentanone), and lead were detected in the groundwater sample from well MW-2 at concentrations ranging from of 0.977 to 11.8 ug/L. Two VPHs (C9-C12 Aliphatics and C9-C10 Aromatics) were detected in the groundwater sample in well MW-2 at concentrations of 12.6 and 14 ug/L. EPH was not detected in the well. Dibromochloromethane was found in well MW-2 at a concentration in exceedance of the NCAC 2L groundwater quality standard (0.4 ug/L). No other VOCs, SVOCs, VPH, EPH, or lead were detected in the groundwater sample from well MW-2 at concentrations above the NCAC 2L groundwater quality standards. None of the analyzed parameters were detected in the groundwater at concentrations above the NCDEQ Gross Contaminant Levels (GCLs). Groundwater analytical data is summarized in Table 4 while the groundwater laboratory analytical report is contained in Appendix A. J CONCLUSIONS AND RECOMMENDATIONS The following conclusions were reached regarding the release from the former Western Carolina Community Center: The site previously contained three 8000-gallon gasoline USTs, one 2000-gallon diesel UST, and one 2000-gallon kerosene UST operated by Burrell’s Fuels Inc. The USTs were removed in November 2008 and soil sampling conducted at the time of closure indicated high levels of TPH in the soil samples collected below the former gasoline pump island. No elevated levels of TPH were detected in soil samples collected beneath the 11 USTs. Thesurroundingpropertiesareamixofcommercialandresidentialpropertiesthat areconnected to the municipal water system; the site and surrounding properties do not use the groundwater as a drinking water source. No VOCs, SVOCs, VPH, or EPH were detected in the soil samples collected from borings drilled in the former source areas (tank basin and pump island) at concentrations above the Soil to Water MSCCs. Chromium was the only constituent detected in the soil samples from MW-1 and MW-2 at concentrations above the Soil to Water MSCCs. Chromium is naturally occurring in soils in the area. No VOCs, SVOCs, VPH, or EPH were detected in the groundwater sample from well MW-1 at concentrations above the 2L Groundwater Standards. One VOC (Dibromochloromethane) was detected in the water sample from MW-2 at a concentration above the 2L Groundwater Standard. Dibromochloromethane is a common laboratory contaminant and its presence may not be indicative of groundwater contamination. None of the analyzed parameters were detected in the groundwater at concentrations above the GCLs. Consultech recommends the incident be assigned a No Further Action status with a Notice of Residual Petroleum (NORP) TABLES Revision Date 10/11/2023 Incident Number/ Name: Public and Private Water Supply Wells Receptor ID DescriptionLatitude/ Longitude of any significant point(s)*Phone NumberUsageDistance from source area of release (ft.)Up or down-gradient1 Lake Lanier 35.194611, -82.233286 Not determined Lake 1,150 Not determined 2 Vaughn Creek 35.198169, -82.232661 Not determined Stream 450 Not determined 3 Unnamed Tributary 1 35.196872, -82.228519 Not determined Tributary 450 Not determined 4 Unnamed Tributary 2 35.199313, -82.226319 Not determined Tributary 1,350 Not determined 5 Unnamed Tributary 3 35.199583, -82.226152 Not determined Tributary 1,450 Not determined 6 Unnamed Tributary 4 35.199022, -82.234422 Not determined Tributary 1,460 Not determined Notes: Receptor distances were obtained from Google Earth and were approximated from the center of the former UST basin. Latitude and longitude obtained from field measurments, Wilkes County GIS or Google Earth. 28791/Former Kwik Stop #1 No Drinking Water Wells Located Within 1500 Feet. Table 1 Receptor Information Former Kwik Stop #1 1024 South Trade Street Tryon, Polk County, North Caolina AddressPhone NumberLatitude/ Longitude (Public water supplies, reservoirs, supply lines, surface water bodies, wellhead protection areas, recharge areas for deep aquifers, subsurface structures)Up or downgradientOther Receptors Well UseWell Depth (ft BGS)Type of WellWell Casing Depth (ft. BGS)Well Screen IntervalDistance from source area of release (ft.)Receptor ID Well Owner/ User Revision Date 10/11/2023 Incident Number/ Name: 28791/Former Kwik Stop #1 Tax Parcel Number/ Map ID Owner/ Occupant Name Property Address Owner Address 06424011000500 Haller, Paul O 99 Lanier Dr Not Listed 50188 Thompson, Nina P 101 E Lakeshore Dr PO Box 561 51427 McNutt Investments LLC 974 South Trade Street 975 South Trade Street 59018 Belk, Frida 1052 South Trade Street 14 Yancy Drive 6140 Garrett & Garrett 1005 South Trade Street PO Box 36 Table 2 Property Owners/Occupants Former Kwik Stop #1 1024 South Trade Street Tryon, Polk County, North Carolina 5030 3350 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8270 8270 8270 8270 8270 8270 VPH VPH VPH TPH-GROTPH-DRONapthalene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)AcetoneBenzeneEthylbenzeneMethyl tert-butyl etherTolueneEthanolIsopropylbenzene2-Butanone2-ChlorotolueneAnthraceneBenzo(a)pyreneChryseneFluorenePhenanthrene2-MethylnaphthaleneChromiumLeadC9-C10 AromaticsC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C12 AliphaticsSample ID Date Depth SS-1 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-2 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-3 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-4 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-5 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-6 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-7 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-8 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-9 12/22/2008 NL BDL 26.6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-10 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-11 12/22/2008 NL 11.4 258 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-12 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-13 12/22/2008 NL 9390 1560 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-14 12/22/2008 NL 84.1 19900 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-15 12/22/2008 NL 6.9 BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-16 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-17 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-18 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-19 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-20 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SS-21 12/22/2008 NL BDL BDL NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA MW-1 10/10/2023 10 ND ND ND ND ND ND 0.0879 ND ND ND 0.00134 J ND ND 0.00688 J ND ND ND ND ND ND ND 43.5 8.7 ND ND ND 12.3 ND MW-1 10/10/2023 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7.24 ND MW-1 10/10/2023 20 ND ND ND ND ND ND 0.061 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 15.7 6.87 ND ND ND ND ND MW-2 10/10/2023 5 ND ND ND ND ND ND 0.0427 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 32.8 14.2 ND ND 15.5 3.43 ND MW-2 10/10/2023 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10.5 7.22 ND MW-2 10/10/2023 15 ND ND ND ND ND ND 0.0514 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 20.4 8.88 2.59 ND ND ND ND 50 NS NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NS 100 NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL NL5.4 270NS TPH-GRO Action Level Incident Number/ Name: 28791/Former Kwik Stop #1Revision Date: 10/11/2023 NL688.3 4.6 24 0.0056 Analyses: Constituents (Units = mg/kg): Soil-to-Groundwater MSCCs (Units = mg/kg)0.16NS TPH-DRO Action Level 540 Notes: BOLD indicates exceedance of Soil-to-Groundwater MSCCs; NL = Not Listed, BDL = Below Detection Limits, NA = Not Analyzed 47 56 1.5 3116 NL 940 0.096 394.9 0.91 4.3 16 1.78.5 Table 3 Soil Analytical Results Former Kwik Stop #1 1024 South Trade Street Tryon, Polk County, North Carolina 625.1 625.1 625.1 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 6200B 6200B 6200B 6200B 6200B 6200B 6010D VPH VPH VPH Contaminant of Concern ->Sample LocationDate SampledBenzoic acidDiethyl phthalatePhenolBenzeneTolueneEthylbenzeneXylenes (total)MTBENaphthaleneEthanolT-amyl alcoholtert-amyl methyl etherTetrachloroethene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneBromodichloromethaneBromoformChloroformDibromochloromethane4-Methyl-2-pentanone (MIBK)2-HexanoneLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics MW-1 10/10/23 15.9 J 0.692 J 2.22 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.94 J 0.241 ND ND 12.3 MW-2 10/10/23 ND 0.977 J ND ND ND ND ND ND ND ND ND ND ND ND ND 5.07 1.09 J 11.8 2.57 2.30 J ND 0.388 ND 12.6 14 NC 2L GW Standard 30000 NS 30 1 600 600 500 20 6 4000 40 128 0.7 400 400 NS 4 70 0.4 100 40 15 400 700 200 GCL 1700000 NS 30000 5000 260000 84500 85500 20000 6000 4000000 40000 12800 700 28500 25000 NS 4000 70000 400 100000 40000 15000 NS NS NS Analytical results reported in ug/L. ND: Compound not detected above laboratory detection limit. NS No standard. J indicates estimated concentration above MDL but below RL Bold Values indicate concentrations above NC 2L GW Standard Analytical Method Revision Date: 10/11/2023 Table 4 Groundwater Analytical Results Former Kwik Stop #1 1024 South Trade Street Tryon, Polk County, North Carolina Incident Number/ Name: 28791/Former Kwik Stop #1 FIGURES Approximate Scale 1” = 2,000’ 1000’ 1994 Landrum, NC-SC 7.5’ USGS Topographic Map Site Location Map Former Kwik Stop #1 (#28791) 1024 S Trade Street, Polk County, Tryon, NC Consultech Environmental, LLC 2021 Energy Drive, Apex, NC 27502 Compiled By: CJP Figure No: 1 Checked By: RBS Date: October 9, 2023 SITE N Approximate Scale 1” = 40 m Google Earth 2022 Site Map Former Kwik Stop #1 Incident (#28791) 1024 S Trade St, Polk County, Tryon, NC Consultech Environmental, LLC 2021 Energy Drive, Apex, NC 27502 Compiled By: CJP Figure No: 2 Checked By: RBS Date: October 9, 2023 Map Key Monitoring Well Location Historical Soil Sample Location Former Dispenser Location Approximate location of Former USTs MW-1 Kwik Stop Building Location MW-2 SS-1 SS-2 SS-3 SS-4 SS-5 SS-6 SS-7 SS-8 SS-10 SS-17 SS-19 SS-18 SS-20 SS-21 Gasoline/Diesel UST Tank Basin Kerosene UST Tank Basin Approximate Scale 1” = 350 m Google Earth 2022 Receptor Map Former Kwik Stop #1 Incident (#28791) 1024 S Trade Street, Polk County, Tryon, NC Consultech Environmental, LLC 2021 Energy Drive, Apex, NC 27502 Compiled By: CJP Figure No: 3 Checked By: RBS Date: October 9, 2023 #1 Lake Lanier #4 Unnamed Tributary 2 APPENDIX A Laboratory Analytical Reports ANALYTICAL REPORT PREPARED FOR Attn: Raj Shah Consultech Environmental LLC 2021 Energy Drive Apex, North Carolina 27502 Generated 10/23/2023 6:14:07 PM JOB DESCRIPTION Kwik Stop JOB NUMBER 400-244922-1 See page two for job notes and contact information. Pensacola FL 32514 3355 McLemore Drive Eurofins Pensacola Page 1 of 39 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Pensacola Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 10/23/2023 6:14:07 PM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Consultech Environmental LLC Project/Site: Kwik Stop Laboratory Job ID: 400-244922-1 Page 3 of 39 Eurofins Pensacola10/23/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Job ID: 400-244922-1 Laboratory: Eurofins Pensacola Narrative Job Narrative 400-244922-1 Receipt The samples were received on 10/12/2023 9:41 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 4.6°C GC/MS VOA No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 625.1: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation batch 400-645683 and analytical batch 400-645849 recovered outside control limits for the following analyte: Benzidine. Method 625.1: The following analyte recovered outside control limits for the laboratory control sample / laboratory control sample duplicate (LCS/LCSD) associated with preparation batch 400-645683 and analytical batch 400-645849: 2,2'-oxybis(1-chloropropane). This is not indicative of a systematic control problem because this was a random marginal exceedance. Qualified results have been reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins PensacolaPage 4 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Client Sample ID: MW-1 Lab Sample ID: 400-244922-1 2-Hexanone RL 25.0 ug/L MDL 1.40 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J1.94 SM6200-B Benzoic acid 29.3 ug/L7.12 Total/NA115.9 J 625.1 Diethyl phthalate 9.75 ug/L0.234 Total/NA10.692 J 625.1 Phenol 9.75 ug/L1.07 Total/NA12.22 J 625.1 C9-C10 Aromatics 7.00 ug/L7.00 Total/NA112.3 MAVPH Lead 0.0500 mg/L0.0100 Total/NA10.241 6010D Client Sample ID: MW-2 Lab Sample ID: 400-244922-2 2-Hexanone RL 25.0 ug/L MDL 1.40 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J2.33 SM6200-B 4-Methyl-2-pentanone (MIBK)25.0 ug/L1.80 Total/NA12.30 J SM6200-B Bromodichloromethane 1.00 ug/L0.500 Total/NA15.07 SM6200-B Bromoform 5.00 ug/L0.250 Total/NA11.09 J SM6200-B Chloroform 1.00 ug/L0.900 Total/NA111.8 SM6200-B Dibromochloromethane 1.00 ug/L0.240 Total/NA12.57 SM6200-B Diethyl phthalate 10.3 ug/L0.246 Total/NA10.977 J 625.1 C9-C12 Aliphatics 11.0 ug/L11.0 Total/NA112.6 MAVPH C9-C10 Aromatics 7.00 ug/L7.00 Total/NA114.0 MAVPH Lead 0.0500 mg/L0.0100 Total/NA10.388 6010D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 5 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Lab Sample ID Client Sample ID Matrix Collected Received 400-244922-1 MW-1 Water 10/10/23 17:40 10/12/23 09:41 400-244922-2 MW-2 Water 10/10/23 17:20 10/12/23 09:41 Eurofins PensacolaPage 6 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 10/10/23 17:40 Date Received: 10/12/23 09:41 Method: SM6200-B - Volatile Organic Compounds RL MDL <0.160 U 1.00 0.160 ug/L 10/17/23 23:50 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 1.00 0.180 ug/L 10/17/23 23:50 1<0.180 U1,1,1-Trichloroethane 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,1,2,2-Tetrachloroethane 5.00 0.210 ug/L 10/17/23 23:50 1<0.210 U1,1,2-Trichloroethane 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,1-Dichloroethane 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,1-Dichloroethene 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,1-Dichloropropene 1.00 0.900 ug/L 10/17/23 23:50 1<0.900 U1,2,3-Trichlorobenzene 5.00 0.840 ug/L 10/17/23 23:50 1<0.840 U1,2,3-Trichloropropane 1.00 0.820 ug/L 10/17/23 23:50 1<0.820 U1,2,4-Trichlorobenzene 1.00 0.820 ug/L 10/17/23 23:50 1<0.820 U1,2,4-Trimethylbenzene 1.00 0.230 ug/L 10/17/23 23:50 1<0.230 U1,2-Dibromoethane (EDB) 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,2-Dichlorobenzene 1.00 0.190 ug/L 10/17/23 23:50 1<0.190 U1,2-Dichloroethane 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,2-Dichloropropane 1.00 0.560 ug/L 10/17/23 23:50 1<0.560 U1,3,5-Trimethylbenzene 1.00 0.540 ug/L 10/17/23 23:50 1<0.540 U1,3-Dichlorobenzene 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U1,3-Dichloropropane 1.00 0.640 ug/L 10/17/23 23:50 1<0.640 U1,4-Dichlorobenzene 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 U2,2-Dichloropropane 25.0 2.60 ug/L 10/17/23 23:50 1<2.60 U2-Butanone (MEK) 1.00 0.570 ug/L 10/17/23 23:50 1<0.570 U2-Chlorotoluene 25.0 1.40 ug/L 10/17/23 23:50 11.94 J2-Hexanone 20.0 12.0 ug/L 10/17/23 23:50 1<12.0 U3,3-Dimethyl-1-butanol 1.00 0.560 ug/L 10/17/23 23:50 1<0.560 U4-Chlorotoluene 25.0 1.80 ug/L 10/17/23 23:50 1<1.80 U4-Methyl-2-pentanone (MIBK) 25.0 10.0 ug/L 10/19/23 09:14 1<10.0 UAcetone 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 UBenzene 1.00 0.540 ug/L 10/17/23 23:50 1<0.540 UBromobenzene 1.00 0.210 ug/L 10/17/23 23:50 1<0.210 UBromochloromethane 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 UBromodichloromethane 5.00 0.250 ug/L 10/17/23 23:50 1<0.250 UBromoform 1.00 0.980 ug/L 10/17/23 23:50 1<0.980 UBromomethane 1.00 0.190 ug/L 10/17/23 23:50 1<0.190 UCarbon tetrachloride 1.00 0.900 ug/L 10/17/23 23:50 1<0.900 UChlorobenzene 1.00 0.760 ug/L 10/17/23 23:50 1<0.760 UChloroethane 1.00 0.900 ug/L 10/17/23 23:50 1<0.900 UChloroform 1.00 0.900 ug/L 10/17/23 23:50 1<0.900 UChloromethane 1.00 0.200 ug/L 10/17/23 23:50 1<0.200 Ucis-1,2-Dichloroethene 5.00 0.500 ug/L 10/17/23 23:50 1<0.500 Ucis-1,3-Dichloropropene 1.00 0.240 ug/L 10/17/23 23:50 1<0.240 UDibromochloromethane 1.00 0.850 ug/L 10/17/23 23:50 1<0.850 UDichlorodifluoromethane 1.00 0.200 ug/L 10/17/23 23:50 1<0.200 UDiisopropyl ether 100 24.0 ug/L 10/17/23 23:50 1<24.0 UEthanol 1.00 0.280 ug/L 10/17/23 23:50 1<0.280 UEthyl tert-butyl ether 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 UEthylbenzene 1.00 0.530 ug/L 10/17/23 23:50 1<0.530 UIsopropylbenzene 1.00 0.220 ug/L 10/17/23 23:50 1<0.220 UMethyl tert-butyl ether 5.00 3.00 ug/L 10/17/23 23:50 1<3.00 UMethylene Chloride Eurofins Pensacola Page 7 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 10/10/23 17:40 Date Received: 10/12/23 09:41 Method: SM6200-B - Volatile Organic Compounds (Continued) RL MDL <0.630 U 5.00 0.630 ug/L 10/17/23 23:50 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier m-Xylene & p-Xylene 5.00 3.00 ug/L 10/17/23 23:50 1<3.00 UNaphthalene 1.00 0.760 ug/L 10/17/23 23:50 1<0.760 Un-Butylbenzene 1.00 0.690 ug/L 10/17/23 23:50 1<0.690 UN-Propylbenzene 5.00 0.600 ug/L 10/17/23 23:50 1<0.600 Uo-Xylene 1.00 0.710 ug/L 10/17/23 23:50 1<0.710 Up-Cymene (p-Isopropyltoluene) 1.00 0.700 ug/L 10/17/23 23:50 1<0.700 Usec-Butylbenzene 1.00 1.00 ug/L 10/17/23 23:50 1<1.00 UStyrene 10.0 4.50 ug/L 10/17/23 23:50 1<4.50 Ut-Amyl alcohol 1.00 0.230 ug/L 10/17/23 23:50 1<0.230 UTert-amyl methyl ether 10.0 2.40 ug/L 10/17/23 23:50 1<2.40 Utert-Butyl Formate 1.00 0.630 ug/L 10/17/23 23:50 1<0.630 Utert-Butylbenzene 1.00 0.900 ug/L 10/17/23 23:50 1<0.900 UTetrachloroethene 1.00 0.900 ug/L 10/17/23 23:50 1<0.900 UToluene 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 Utrans-1,2-Dichloroethene 5.00 0.200 ug/L 10/17/23 23:50 1<0.200 Utrans-1,3-Dichloropropene 1.00 0.150 ug/L 10/17/23 23:50 1<0.150 UTrichloroethene 1.00 0.520 ug/L 10/17/23 23:50 1<0.520 UTrichlorofluoromethane 25.0 0.930 ug/L 10/17/23 23:50 1<0.930 UVinyl acetate 1.00 0.500 ug/L 10/17/23 23:50 1<0.500 UVinyl chloride 10.0 1.60 ug/L 10/17/23 23:50 1<1.60 UXylenes, Total 4-Bromofluorobenzene 93 72-130 10/17/23 23:50 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene 105 10/19/23 09:14 172-130 Dibromofluoromethane 117 10/17/23 23:50 175-126 Dibromofluoromethane 91 10/19/23 09:14 175-126 Toluene-d8 (Surr)98 10/17/23 23:50 164-132 Toluene-d8 (Surr)105 10/19/23 09:14 164-132 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) RL MDL <0.176 U 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 9.75 0.146 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.146 U1-Methylnaphthalene 9.75 0.156 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.156 U *-2,2'-oxybis(1-chloropropane) 9.75 3.61 ug/L 10/16/23 11:18 10/17/23 21:11 1<3.61 U2,4,5-Trichlorophenol 9.75 2.54 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.54 U2,4,6-Trichlorophenol 9.75 1.95 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.95 U2,4-Dichlorophenol 9.75 1.95 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.95 U2,4-Dimethylphenol 29.3 3.32 ug/L 10/16/23 11:18 10/17/23 21:11 1<3.32 U2,4-Dinitrophenol 9.75 1.85 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.85 U2,4-Dinitrotoluene 9.75 1.85 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.85 U2,6-Dinitrotoluene 9.75 0.137 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.137 U2-Chloronaphthalene 9.75 2.15 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.15 U2-Chlorophenol 9.75 0.127 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.127 U2-Methylnaphthalene 9.75 1.76 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.76 U2-Methylphenol 9.75 2.15 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.15 U2-Nitroaniline 9.75 2.34 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.34 U2-Nitrophenol 19.5 0.380 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.380 U3 & 4 Methylphenol 9.75 2.54 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.54 U3,3'-Dichlorobenzidine Eurofins Pensacola Page 8 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 10/10/23 17:40 Date Received: 10/12/23 09:41 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <1.76 U 9.75 1.76 ug/L 10/16/23 11:18 10/17/23 21:11 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 3-Nitroaniline 9.75 1.56 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.56 U4,6-Dinitro-2-methylphenol 9.75 0.195 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.195 U4-Bromophenyl phenyl ether 9.75 3.71 ug/L 10/16/23 11:18 10/17/23 21:11 1<3.71 U4-Chloro-3-methylphenol 9.75 3.32 ug/L 10/16/23 11:18 10/17/23 21:11 1<3.32 U4-Chloroaniline 9.75 1.95 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.95 U4-Chlorophenyl phenyl ether 9.75 1.46 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.46 U4-Nitroaniline 9.75 2.05 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.05 U4-Nitrophenol 9.75 0.156 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.156 UAcenaphthene 9.75 0.166 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.166 UAcenaphthylene 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.176 UAnthracene 24.4 19.5 ug/L 10/16/23 11:18 10/17/23 21:11 1<19.5 U *1Benzidine 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.176 UBenzo[a]anthracene 9.75 0.117 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.117 UBenzo[a]pyrene 9.75 0.146 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.146 UBenzo[b]fluoranthene 9.75 0.224 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.224 UBenzo[g,h,i]perylene 9.75 0.156 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.156 UBenzo[k]fluoranthene 29.3 7.12 ug/L 10/16/23 11:18 10/17/23 21:11 115.9 JBenzoic acid 9.75 1.95 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.95 UBenzyl alcohol 9.75 0.156 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.156 UBis(2-chloroethoxy)methane 9.75 2.63 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.63 UBis(2-chloroethyl)ether 9.75 4.88 ug/L 10/16/23 11:18 10/17/23 21:11 1<4.88 UBis(2-ethylhexyl) phthalate 9.75 0.185 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.185 UButyl benzyl phthalate 9.75 0.185 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.185 UChrysene 9.75 0.234 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.234 UDibenz(a,h)anthracene 9.75 0.166 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.166 UDibenzofuran 9.75 0.234 ug/L 10/16/23 11:18 10/17/23 21:11 10.692 JDiethyl phthalate 9.75 0.166 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.166 UDimethyl phthalate 9.75 1.37 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.37 UDi-n-butyl phthalate 9.75 0.166 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.166 UDi-n-octyl phthalate 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.176 UFluoranthene 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.176 UFluorene 9.75 0.166 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.166 UHexachlorobenzene 9.75 3.51 ug/L 10/16/23 11:18 10/17/23 21:11 1<3.51 UHexachlorobutadiene 19.5 2.54 ug/L 10/16/23 11:18 10/17/23 21:11 1<2.54 UHexachlorocyclopentadiene 9.75 4.10 ug/L 10/16/23 11:18 10/17/23 21:11 1<4.10 UHexachloroethane 9.75 0.215 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.215 UIndeno[1,2,3-cd]pyrene 9.75 0.137 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.137 UIsophorone 9.75 0.166 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.166 UNaphthalene 9.75 0.127 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.127 UNitrobenzene 9.75 3.22 ug/L 10/16/23 11:18 10/17/23 21:11 1<3.22 UN-Nitrosodi-n-propylamine 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.176 UN-Nitrosodiphenylamine 19.5 1.37 ug/L 10/16/23 11:18 10/17/23 21:11 1<1.37 UPentachlorophenol 9.75 0.176 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.176 UPhenanthrene 9.75 1.07 ug/L 10/16/23 11:18 10/17/23 21:11 12.22 JPhenol 9.75 0.205 ug/L 10/16/23 11:18 10/17/23 21:11 1<0.205 UPyrene 2,4,6-Tribromophenol 70 15-135 10/16/23 11:18 10/17/23 21:11 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 75 10/16/23 11:18 10/17/23 21:11 132-109 Eurofins Pensacola Page 9 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 10/10/23 17:40 Date Received: 10/12/23 09:41 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) 2-Fluorophenol 35 10-104 10/16/23 11:18 10/17/23 21:11 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 62 10/16/23 11:18 10/17/23 21:11 131-111 Phenol-d5 27 10/16/23 11:18 10/17/23 21:11 110-110 Terphenyl-d14 72 10/16/23 11:18 10/17/23 21:11 130-129 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <26.0 U 26.0 26.0 ug/L 10/19/23 22:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 11.0 11.0 ug/L 10/19/23 22:15 1<11.0 UC9-C12 Aliphatics 7.00 7.00 ug/L 10/19/23 22:15 112.3C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)81 70-130 10/19/23 22:15 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)83 10/19/23 22:15 170-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <144 U 144 144 ug/L 10/12/23 21:48 10/13/23 23:57 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 144 144 ug/L 10/12/23 21:48 10/13/23 23:57 1<144 UC19-C36 Aliphatics 296 296 ug/L 10/12/23 21:48 10/14/23 00:08 1<296 UC11-C22 Aromatics 1-Chlorooctadecane 64 40-140 10/12/23 21:48 10/13/23 23:57 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 78 10/12/23 21:48 10/14/23 00:08 140-140 2-Fluorobiphenyl 108 10/12/23 21:48 10/14/23 00:08 140-140 2-Bromonaphthalene 105 10/12/23 21:48 10/14/23 00:08 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 0.241 0.0500 0.0100 mg/L 10/17/23 07:58 10/18/23 23:25 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Lead Eurofins Pensacola Page 10 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 10/10/23 17:20 Date Received: 10/12/23 09:41 Method: SM6200-B - Volatile Organic Compounds RL MDL <0.160 U 1.00 0.160 ug/L 10/18/23 00:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 1.00 0.180 ug/L 10/18/23 00:08 1<0.180 U1,1,1-Trichloroethane 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,1,2,2-Tetrachloroethane 5.00 0.210 ug/L 10/18/23 00:08 1<0.210 U1,1,2-Trichloroethane 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,1-Dichloroethane 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,1-Dichloroethene 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,1-Dichloropropene 1.00 0.900 ug/L 10/18/23 00:08 1<0.900 U1,2,3-Trichlorobenzene 5.00 0.840 ug/L 10/18/23 00:08 1<0.840 U1,2,3-Trichloropropane 1.00 0.820 ug/L 10/18/23 00:08 1<0.820 U1,2,4-Trichlorobenzene 1.00 0.820 ug/L 10/18/23 00:08 1<0.820 U1,2,4-Trimethylbenzene 1.00 0.230 ug/L 10/18/23 00:08 1<0.230 U1,2-Dibromoethane (EDB) 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,2-Dichlorobenzene 1.00 0.190 ug/L 10/18/23 00:08 1<0.190 U1,2-Dichloroethane 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,2-Dichloropropane 1.00 0.560 ug/L 10/18/23 00:08 1<0.560 U1,3,5-Trimethylbenzene 1.00 0.540 ug/L 10/18/23 00:08 1<0.540 U1,3-Dichlorobenzene 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U1,3-Dichloropropane 1.00 0.640 ug/L 10/18/23 00:08 1<0.640 U1,4-Dichlorobenzene 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 U2,2-Dichloropropane 25.0 2.60 ug/L 10/18/23 00:08 1<2.60 U2-Butanone (MEK) 1.00 0.570 ug/L 10/18/23 00:08 1<0.570 U2-Chlorotoluene 25.0 1.40 ug/L 10/18/23 00:08 12.33 J2-Hexanone 20.0 12.0 ug/L 10/18/23 00:08 1<12.0 U3,3-Dimethyl-1-butanol 1.00 0.560 ug/L 10/18/23 00:08 1<0.560 U4-Chlorotoluene 25.0 1.80 ug/L 10/18/23 00:08 12.30 J4-Methyl-2-pentanone (MIBK) 25.0 10.0 ug/L 10/19/23 09:36 1<10.0 UAcetone 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 UBenzene 1.00 0.540 ug/L 10/18/23 00:08 1<0.540 UBromobenzene 1.00 0.210 ug/L 10/18/23 00:08 1<0.210 UBromochloromethane 1.00 0.500 ug/L 10/18/23 00:08 15.07Bromodichloromethane 5.00 0.250 ug/L 10/18/23 00:08 11.09 JBromoform 1.00 0.980 ug/L 10/18/23 00:08 1<0.980 UBromomethane 1.00 0.190 ug/L 10/18/23 00:08 1<0.190 UCarbon tetrachloride 1.00 0.900 ug/L 10/18/23 00:08 1<0.900 UChlorobenzene 1.00 0.760 ug/L 10/18/23 00:08 1<0.760 UChloroethane 1.00 0.900 ug/L 10/18/23 00:08 111.8Chloroform 1.00 0.900 ug/L 10/18/23 00:08 1<0.900 UChloromethane 1.00 0.200 ug/L 10/18/23 00:08 1<0.200 Ucis-1,2-Dichloroethene 5.00 0.500 ug/L 10/18/23 00:08 1<0.500 Ucis-1,3-Dichloropropene 1.00 0.240 ug/L 10/18/23 00:08 12.57Dibromochloromethane 1.00 0.850 ug/L 10/18/23 00:08 1<0.850 UDichlorodifluoromethane 1.00 0.200 ug/L 10/18/23 00:08 1<0.200 UDiisopropyl ether 100 24.0 ug/L 10/18/23 00:08 1<24.0 UEthanol 1.00 0.280 ug/L 10/18/23 00:08 1<0.280 UEthyl tert-butyl ether 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 UEthylbenzene 1.00 0.530 ug/L 10/18/23 00:08 1<0.530 UIsopropylbenzene 1.00 0.220 ug/L 10/18/23 00:08 1<0.220 UMethyl tert-butyl ether 5.00 3.00 ug/L 10/18/23 00:08 1<3.00 UMethylene Chloride Eurofins Pensacola Page 11 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 10/10/23 17:20 Date Received: 10/12/23 09:41 Method: SM6200-B - Volatile Organic Compounds (Continued) RL MDL <0.630 U 5.00 0.630 ug/L 10/18/23 00:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier m-Xylene & p-Xylene 5.00 3.00 ug/L 10/18/23 00:08 1<3.00 UNaphthalene 1.00 0.760 ug/L 10/18/23 00:08 1<0.760 Un-Butylbenzene 1.00 0.690 ug/L 10/18/23 00:08 1<0.690 UN-Propylbenzene 5.00 0.600 ug/L 10/18/23 00:08 1<0.600 Uo-Xylene 1.00 0.710 ug/L 10/18/23 00:08 1<0.710 Up-Cymene (p-Isopropyltoluene) 1.00 0.700 ug/L 10/18/23 00:08 1<0.700 Usec-Butylbenzene 1.00 1.00 ug/L 10/18/23 00:08 1<1.00 UStyrene 10.0 4.50 ug/L 10/18/23 00:08 1<4.50 Ut-Amyl alcohol 1.00 0.230 ug/L 10/18/23 00:08 1<0.230 UTert-amyl methyl ether 10.0 2.40 ug/L 10/18/23 00:08 1<2.40 Utert-Butyl Formate 1.00 0.630 ug/L 10/18/23 00:08 1<0.630 Utert-Butylbenzene 1.00 0.900 ug/L 10/18/23 00:08 1<0.900 UTetrachloroethene 1.00 0.900 ug/L 10/18/23 00:08 1<0.900 UToluene 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 Utrans-1,2-Dichloroethene 5.00 0.200 ug/L 10/18/23 00:08 1<0.200 Utrans-1,3-Dichloropropene 1.00 0.150 ug/L 10/18/23 00:08 1<0.150 UTrichloroethene 1.00 0.520 ug/L 10/18/23 00:08 1<0.520 UTrichlorofluoromethane 25.0 0.930 ug/L 10/18/23 00:08 1<0.930 UVinyl acetate 1.00 0.500 ug/L 10/18/23 00:08 1<0.500 UVinyl chloride 10.0 1.60 ug/L 10/18/23 00:08 1<1.60 UXylenes, Total 4-Bromofluorobenzene 96 72-130 10/18/23 00:08 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene 106 10/19/23 09:36 172-130 Dibromofluoromethane 115 10/18/23 00:08 175-126 Dibromofluoromethane 94 10/19/23 09:36 175-126 Toluene-d8 (Surr)99 10/18/23 00:08 164-132 Toluene-d8 (Surr)103 10/19/23 09:36 164-132 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) RL MDL <0.185 U 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 10.3 0.154 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.154 U1-Methylnaphthalene 10.3 0.164 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.164 U *-2,2'-oxybis(1-chloropropane) 10.3 3.80 ug/L 10/16/23 11:18 10/17/23 21:37 1<3.80 U2,4,5-Trichlorophenol 10.3 2.67 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.67 U2,4,6-Trichlorophenol 10.3 2.05 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.05 U2,4-Dichlorophenol 10.3 2.05 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.05 U2,4-Dimethylphenol 30.8 3.49 ug/L 10/16/23 11:18 10/17/23 21:37 1<3.49 U2,4-Dinitrophenol 10.3 1.95 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.95 U2,4-Dinitrotoluene 10.3 1.95 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.95 U2,6-Dinitrotoluene 10.3 0.144 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.144 U2-Chloronaphthalene 10.3 2.26 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.26 U2-Chlorophenol 10.3 0.133 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.133 U2-Methylnaphthalene 10.3 1.85 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.85 U2-Methylphenol 10.3 2.26 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.26 U2-Nitroaniline 10.3 2.46 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.46 U2-Nitrophenol 20.5 0.400 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.400 U3 & 4 Methylphenol 10.3 2.67 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.67 U3,3'-Dichlorobenzidine Eurofins Pensacola Page 12 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 10/10/23 17:20 Date Received: 10/12/23 09:41 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <1.85 U 10.3 1.85 ug/L 10/16/23 11:18 10/17/23 21:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 3-Nitroaniline 10.3 1.64 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.64 U4,6-Dinitro-2-methylphenol 10.3 0.205 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.205 U4-Bromophenyl phenyl ether 10.3 3.90 ug/L 10/16/23 11:18 10/17/23 21:37 1<3.90 U4-Chloro-3-methylphenol 10.3 3.49 ug/L 10/16/23 11:18 10/17/23 21:37 1<3.49 U4-Chloroaniline 10.3 2.05 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.05 U4-Chlorophenyl phenyl ether 10.3 1.54 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.54 U4-Nitroaniline 10.3 2.16 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.16 U4-Nitrophenol 10.3 0.164 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.164 UAcenaphthene 10.3 0.174 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.174 UAcenaphthylene 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.185 UAnthracene 25.7 20.5 ug/L 10/16/23 11:18 10/17/23 21:37 1<20.5 U *1Benzidine 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.185 UBenzo[a]anthracene 10.3 0.123 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.123 UBenzo[a]pyrene 10.3 0.154 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.154 UBenzo[b]fluoranthene 10.3 0.236 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.236 UBenzo[g,h,i]perylene 10.3 0.164 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.164 UBenzo[k]fluoranthene 30.8 7.49 ug/L 10/16/23 11:18 10/17/23 21:37 1<7.49 UBenzoic acid 10.3 2.05 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.05 UBenzyl alcohol 10.3 0.164 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.164 UBis(2-chloroethoxy)methane 10.3 2.77 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.77 UBis(2-chloroethyl)ether 10.3 5.13 ug/L 10/16/23 11:18 10/17/23 21:37 1<5.13 UBis(2-ethylhexyl) phthalate 10.3 0.195 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.195 UButyl benzyl phthalate 10.3 0.195 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.195 UChrysene 10.3 0.246 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.246 UDibenz(a,h)anthracene 10.3 0.174 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.174 UDibenzofuran 10.3 0.246 ug/L 10/16/23 11:18 10/17/23 21:37 10.977 JDiethyl phthalate 10.3 0.174 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.174 UDimethyl phthalate 10.3 1.44 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.44 UDi-n-butyl phthalate 10.3 0.174 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.174 UDi-n-octyl phthalate 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.185 UFluoranthene 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.185 UFluorene 10.3 0.174 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.174 UHexachlorobenzene 10.3 3.69 ug/L 10/16/23 11:18 10/17/23 21:37 1<3.69 UHexachlorobutadiene 20.5 2.67 ug/L 10/16/23 11:18 10/17/23 21:37 1<2.67 UHexachlorocyclopentadiene 10.3 4.31 ug/L 10/16/23 11:18 10/17/23 21:37 1<4.31 UHexachloroethane 10.3 0.226 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.226 UIndeno[1,2,3-cd]pyrene 10.3 0.144 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.144 UIsophorone 10.3 0.174 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.174 UNaphthalene 10.3 0.133 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.133 UNitrobenzene 10.3 3.39 ug/L 10/16/23 11:18 10/17/23 21:37 1<3.39 UN-Nitrosodi-n-propylamine 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.185 UN-Nitrosodiphenylamine 20.5 1.44 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.44 UPentachlorophenol 10.3 0.185 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.185 UPhenanthrene 10.3 1.13 ug/L 10/16/23 11:18 10/17/23 21:37 1<1.13 UPhenol 10.3 0.216 ug/L 10/16/23 11:18 10/17/23 21:37 1<0.216 UPyrene 2,4,6-Tribromophenol 82 15-135 10/16/23 11:18 10/17/23 21:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 72 10/16/23 11:18 10/17/23 21:37 132-109 Eurofins Pensacola Page 13 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244922-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 10/10/23 17:20 Date Received: 10/12/23 09:41 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) 2-Fluorophenol 32 10-104 10/16/23 11:18 10/17/23 21:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 69 10/16/23 11:18 10/17/23 21:37 131-111 Phenol-d5 27 10/16/23 11:18 10/17/23 21:37 110-110 Terphenyl-d14 72 10/16/23 11:18 10/17/23 21:37 130-129 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <26.0 U 26.0 26.0 ug/L 10/19/23 22:46 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 11.0 11.0 ug/L 10/19/23 22:46 112.6C9-C12 Aliphatics 7.00 7.00 ug/L 10/19/23 22:46 114.0C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)81 70-130 10/19/23 22:46 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)84 10/19/23 22:46 170-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <144 U 144 144 ug/L 10/12/23 21:48 10/14/23 00:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 144 144 ug/L 10/12/23 21:48 10/14/23 00:08 1<144 UC19-C36 Aliphatics 297 297 ug/L 10/12/23 21:48 10/14/23 00:20 1<297 UC11-C22 Aromatics 1-Chlorooctadecane 72 40-140 10/12/23 21:48 10/14/23 00:08 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 81 10/12/23 21:48 10/14/23 00:20 140-140 2-Fluorobiphenyl 118 10/12/23 21:48 10/14/23 00:20 140-140 2-Bromonaphthalene 114 10/12/23 21:48 10/14/23 00:20 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 0.388 0.0500 0.0100 mg/L 10/17/23 07:58 10/18/23 23:29 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Lead Eurofins Pensacola Page 14 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Qualifiers GC/MS VOA Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier U Indicates the analyte was analyzed for but not detected. GC/MS Semi VOA Qualifier Description *-LCS and/or LCSD is outside acceptance limits, low biased. Qualifier *1 LCS/LCSD RPD exceeds control limits. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. U Indicates the analyte was analyzed for but not detected. GC VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC Semi VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Metals Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) Eurofins Pensacola Page 15 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Glossary (Continued) These commonly used abbreviations may or may not be present in this report. TEQ Toxicity Equivalent Quotient (Dioxin) Abbreviation TNTC Too Numerous To Count Eurofins Pensacola Page 16 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: SM6200-B - Volatile Organic Compounds Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (72-130)(75-126)(64-132) BFB DBFM TOL 93 117 98400-244922-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 105 91 105400-244922-1 MW-1 96 115 99400-244922-2 MW-2 106 94 103400-244922-2 MW-2 103 103 100LCS 400-645916/1008 Lab Control Sample 105 90 104LCS 400-646204/1002 Lab Control Sample 99 112 99MB 400-645916/32 Method Blank 106 91 105MB 400-646204/5 Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) Method: 625.1 - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (15-135)(32-109)(10-104)(31-111)(10-110)(30-129) TBP FBP 2FP NBZ PHL TPHL 70 75 35 62 27 72400-244922-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 82 72 32 2769 72400-244922-2 MW-2 84 73 43 4386 73LCS 400-645683/2-A Lab Control Sample 81 72 44 4283 89LCSD 400-645683/3-A Lab Control Sample Dup 56 58 34 2750 56MB 400-645683/1-A Method Blank Surrogate Legend TBP = 2,4,6-Tribromophenol FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol NBZ = Nitrobenzene-d5 PHL = Phenol-d5 TPHL = Terphenyl-d14 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (70-130)(70-130) TFT-F1 TFT-P1 81 83400-244922-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 81 84400-244922-2 MW-2 88 88LCS 400-646250/3 Lab Control Sample 88 88LCSD 400-646250/4 Lab Control Sample Dup 85 87MB 400-646250/2 Method Blank Surrogate Legend TFT-F = a,a,a-Trifluorotoluene (fid) TFT-P = a,a,a-Trifluorotoluene (pid) Eurofins Pensacola Page 17 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (40-140) 1COD1 64400-244922-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 72400-244922-2 MW-2 81LCS 400-645382/2-A Lab Control Sample 86LCSD 400-645382/3-A Lab Control Sample Dup 82MB 400-645382/1-A Method Blank Surrogate Legend 1COD = 1-Chlorooctadecane Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 78 108 105400-244922-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 81 118 114400-244922-2 MW-2 101 133 129LCS 400-645382/2-A Lab Control Sample 87 111 106LCSD 400-645382/3-A Lab Control Sample Dup 92 124 119MB 400-645382/1-A Method Blank Surrogate Legend OTPH = o-Terphenyl FBP = 2-Fluorobiphenyl 2BN = 2-Bromonaphthalene Eurofins Pensacola Page 18 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop GC/MS VOA Analysis Batch: 645916 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water SM6200-B400-244922-1 MW-1 Total/NA Water SM6200-B400-244922-2 MW-2 Total/NA Water SM6200-BMB 400-645916/32 Method Blank Total/NA Water SM6200-BLCS 400-645916/1008 Lab Control Sample Total/NA Analysis Batch: 646204 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water SM6200-B400-244922-1 MW-1 Total/NA Water SM6200-B400-244922-2 MW-2 Total/NA Water SM6200-BMB 400-646204/5 Method Blank Total/NA Water SM6200-BLCS 400-646204/1002 Lab Control Sample Total/NA GC/MS Semi VOA Prep Batch: 645683 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 625400-244922-1 MW-1 Total/NA Water 625400-244922-2 MW-2 Total/NA Water 625MB 400-645683/1-A Method Blank Total/NA Water 625LCS 400-645683/2-A Lab Control Sample Total/NA Water 625LCSD 400-645683/3-A Lab Control Sample Dup Total/NA Analysis Batch: 645849 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 625.1 645683400-244922-1 MW-1 Total/NA Water 625.1 645683400-244922-2 MW-2 Total/NA Water 625.1 645683MB 400-645683/1-A Method Blank Total/NA Water 625.1 645683LCS 400-645683/2-A Lab Control Sample Total/NA Water 625.1 645683LCSD 400-645683/3-A Lab Control Sample Dup Total/NA GC VOA Analysis Batch: 646250 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MAVPH400-244922-1 MW-1 Total/NA Water MAVPH400-244922-2 MW-2 Total/NA Water MAVPHMB 400-646250/2 Method Blank Total/NA Water MAVPHLCS 400-646250/3 Lab Control Sample Total/NA Water MAVPHLCSD 400-646250/4 Lab Control Sample Dup Total/NA GC Semi VOA Prep Batch: 645382 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3511400-244922-1 MW-1 Total/NA Water 3511400-244922-2 MW-2 Total/NA Water 3511MB 400-645382/1-A Method Blank Total/NA Water 3511LCS 400-645382/2-A Lab Control Sample Total/NA Water 3511LCSD 400-645382/3-A Lab Control Sample Dup Total/NA Eurofins Pensacola Page 19 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop GC Semi VOA Analysis Batch: 645456 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MA-EPH 645382400-244922-1 MW-1 Total/NA Water MA-EPH 645382400-244922-2 MW-2 Total/NA Water MA-EPH 645382MB 400-645382/1-A Method Blank Total/NA Water MA-EPH 645382LCS 400-645382/2-A Lab Control Sample Total/NA Water MA-EPH 645382LCSD 400-645382/3-A Lab Control Sample Dup Total/NA Analysis Batch: 645458 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MA-EPH 645382400-244922-1 MW-1 Total/NA Water MA-EPH 645382400-244922-2 MW-2 Total/NA Water MA-EPH 645382MB 400-645382/1-A Method Blank Total/NA Water MA-EPH 645382LCS 400-645382/2-A Lab Control Sample Total/NA Water MA-EPH 645382LCSD 400-645382/3-A Lab Control Sample Dup Total/NA Metals Prep Batch: 645663 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3010A400-244922-1 MW-1 Total/NA Water 3010A400-244922-2 MW-2 Total/NA Water 3010AMB 400-645663/1-A Method Blank Total/NA Water 3010ALCS 400-645663/2-A Lab Control Sample Total/NA Analysis Batch: 646279 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 6010D 645663400-244922-1 MW-1 Total/NA Water 6010D 645663400-244922-2 MW-2 Total/NA Water 6010D 645663MB 400-645663/1-A Method Blank Total/NA Water 6010D 645663LCS 400-645663/2-A Lab Control Sample Total/NA Eurofins Pensacola Page 20 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: SM6200-B - Volatile Organic Compounds Client Sample ID: Method BlankLab Sample ID: MB 400-645916/32 Matrix: Water Prep Type: Total/NA Analysis Batch: 645916 RL MDL 1,1,1,2-Tetrachloroethane <0.160 U 1.00 0.160 ug/L 10/17/23 15:57 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.180 U 0.1801.00 ug/L 10/17/23 15:57 11,1,1-Trichloroethane <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,1,2,2-Tetrachloroethane <0.210 U 0.2105.00 ug/L 10/17/23 15:57 11,1,2-Trichloroethane <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,1-Dichloroethane <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,1-Dichloroethene <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,1-Dichloropropene <0.900 U 0.9001.00 ug/L 10/17/23 15:57 11,2,3-Trichlorobenzene <0.840 U 0.8405.00 ug/L 10/17/23 15:57 11,2,3-Trichloropropane <0.820 U 0.8201.00 ug/L 10/17/23 15:57 11,2,4-Trichlorobenzene <0.820 U 0.8201.00 ug/L 10/17/23 15:57 11,2,4-Trimethylbenzene <0.230 U 0.2301.00 ug/L 10/17/23 15:57 11,2-Dibromoethane (EDB) <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,2-Dichlorobenzene <0.190 U 0.1901.00 ug/L 10/17/23 15:57 11,2-Dichloroethane <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,2-Dichloropropane <0.560 U 0.5601.00 ug/L 10/17/23 15:57 11,3,5-Trimethylbenzene <0.540 U 0.5401.00 ug/L 10/17/23 15:57 11,3-Dichlorobenzene <0.500 U 0.5001.00 ug/L 10/17/23 15:57 11,3-Dichloropropane <0.640 U 0.6401.00 ug/L 10/17/23 15:57 11,4-Dichlorobenzene <0.500 U 0.5001.00 ug/L 10/17/23 15:57 12,2-Dichloropropane <2.60 U 2.6025.0 ug/L 10/17/23 15:57 12-Butanone (MEK) <0.570 U 0.5701.00 ug/L 10/17/23 15:57 12-Chlorotoluene <1.40 U 1.4025.0 ug/L 10/17/23 15:57 12-Hexanone <12.0 U 12.020.0 ug/L 10/17/23 15:57 13,3-Dimethyl-1-butanol <0.560 U 0.5601.00 ug/L 10/17/23 15:57 14-Chlorotoluene <1.80 U 1.8025.0 ug/L 10/17/23 15:57 14-Methyl-2-pentanone (MIBK) <0.500 U 0.5001.00 ug/L 10/17/23 15:57 1Benzene <0.540 U 0.5401.00 ug/L 10/17/23 15:57 1Bromobenzene <0.210 U 0.2101.00 ug/L 10/17/23 15:57 1Bromochloromethane <0.500 U 0.5001.00 ug/L 10/17/23 15:57 1Bromodichloromethane <0.250 U 0.2505.00 ug/L 10/17/23 15:57 1Bromoform <0.980 U 0.9801.00 ug/L 10/17/23 15:57 1Bromomethane <0.190 U 0.1901.00 ug/L 10/17/23 15:57 1Carbon tetrachloride <0.900 U 0.9001.00 ug/L 10/17/23 15:57 1Chlorobenzene <0.760 U 0.7601.00 ug/L 10/17/23 15:57 1Chloroethane <0.900 U 0.9001.00 ug/L 10/17/23 15:57 1Chloroform <0.900 U 0.9001.00 ug/L 10/17/23 15:57 1Chloromethane <0.200 U 0.2001.00 ug/L 10/17/23 15:57 1cis-1,2-Dichloroethene <0.500 U 0.5005.00 ug/L 10/17/23 15:57 1cis-1,3-Dichloropropene <0.240 U 0.2401.00 ug/L 10/17/23 15:57 1Dibromochloromethane <0.850 U 0.8501.00 ug/L 10/17/23 15:57 1Dichlorodifluoromethane <0.200 U 0.2001.00 ug/L 10/17/23 15:57 1Diisopropyl ether <24.0 U 24.0100 ug/L 10/17/23 15:57 1Ethanol <0.280 U 0.2801.00 ug/L 10/17/23 15:57 1Ethyl tert-butyl ether <0.500 U 0.5001.00 ug/L 10/17/23 15:57 1Ethylbenzene <0.530 U 0.5301.00 ug/L 10/17/23 15:57 1Isopropylbenzene <0.220 U 0.2201.00 ug/L 10/17/23 15:57 1Methyl tert-butyl ether <3.00 U 3.005.00 ug/L 10/17/23 15:57 1Methylene Chloride Eurofins Pensacola Page 21 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: SM6200-B - Volatile Organic Compounds (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-645916/32 Matrix: Water Prep Type: Total/NA Analysis Batch: 645916 RL MDL m-Xylene & p-Xylene <0.630 U 5.00 0.630 ug/L 10/17/23 15:57 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <3.00 U 3.005.00 ug/L 10/17/23 15:57 1Naphthalene <0.760 U 0.7601.00 ug/L 10/17/23 15:57 1n-Butylbenzene <0.690 U 0.6901.00 ug/L 10/17/23 15:57 1N-Propylbenzene <0.600 U 0.6005.00 ug/L 10/17/23 15:57 1o-Xylene <0.710 U 0.7101.00 ug/L 10/17/23 15:57 1p-Cymene (p-Isopropyltoluene) <0.700 U 0.7001.00 ug/L 10/17/23 15:57 1sec-Butylbenzene <1.00 U 1.001.00 ug/L 10/17/23 15:57 1Styrene <4.50 U 4.5010.0 ug/L 10/17/23 15:57 1t-Amyl alcohol <0.230 U 0.2301.00 ug/L 10/17/23 15:57 1Tert-amyl methyl ether <2.40 U 2.4010.0 ug/L 10/17/23 15:57 1tert-Butyl Formate <0.630 U 0.6301.00 ug/L 10/17/23 15:57 1tert-Butylbenzene <0.900 U 0.9001.00 ug/L 10/17/23 15:57 1Tetrachloroethene <0.900 U 0.9001.00 ug/L 10/17/23 15:57 1Toluene <0.500 U 0.5001.00 ug/L 10/17/23 15:57 1trans-1,2-Dichloroethene <0.200 U 0.2005.00 ug/L 10/17/23 15:57 1trans-1,3-Dichloropropene <0.150 U 0.1501.00 ug/L 10/17/23 15:57 1Trichloroethene <0.520 U 0.5201.00 ug/L 10/17/23 15:57 1Trichlorofluoromethane <0.930 U 0.93025.0 ug/L 10/17/23 15:57 1Vinyl acetate <0.500 U 0.5001.00 ug/L 10/17/23 15:57 1Vinyl chloride <1.60 U 1.6010.0 ug/L 10/17/23 15:57 1Xylenes, Total 4-Bromofluorobenzene 99 72-130 10/17/23 15:57 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 112 10/17/23 15:57 1Dibromofluoromethane75-126 99 10/17/23 15:57 1Toluene-d8 (Surr)64-132 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645916/1008 Matrix: Water Prep Type: Total/NA Analysis Batch: 645916 1,1,1,2-Tetrachloroethane 50.0 45.01 ug/L 90 67 -131 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 50.0 46.24 ug/L 92 68 -130 1,1,2,2-Tetrachloroethane 50.0 49.55 ug/L 99 70 -131 1,1,2-Trichloroethane 50.0 49.19 ug/L 98 70 -130 1,1-Dichloroethane 50.0 47.61 ug/L 95 70 -130 1,1-Dichloroethene 50.0 46.06 ug/L 92 63 -134 1,1-Dichloropropene 50.0 48.16 ug/L 96 70 -130 1,2,3-Trichlorobenzene 50.0 48.20 ug/L 96 60 -138 1,2,3-Trichloropropane 50.0 49.07 ug/L 98 70 -130 1,2,4-Trichlorobenzene 50.0 49.59 ug/L 99 60 -140 1,2,4-Trimethylbenzene 50.0 51.73 ug/L 103 70 -130 1,2-Dibromoethane (EDB)50.0 48.94 ug/L 98 70 -130 1,2-Dichlorobenzene 50.0 48.45 ug/L 97 67 -130 1,2-Dichloroethane 50.0 48.87 ug/L 98 69 -130 1,2-Dichloropropane 50.0 48.67 ug/L 97 70 -130 1,3,5-Trimethylbenzene 50.0 51.98 ug/L 104 69 -130 Eurofins Pensacola Page 22 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: SM6200-B - Volatile Organic Compounds (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645916/1008 Matrix: Water Prep Type: Total/NA Analysis Batch: 645916 1,3-Dichlorobenzene 50.0 48.99 ug/L 98 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,3-Dichloropropane 50.0 49.18 ug/L 98 70 -130 1,4-Dichlorobenzene 50.0 48.25 ug/L 96 70 -130 2,2-Dichloropropane 50.0 46.50 ug/L 93 52 -135 2-Butanone (MEK)200 221.4 ug/L 111 61 -145 2-Chlorotoluene 50.0 50.83 ug/L 102 70 -130 2-Hexanone 200 234.2 ug/L 117 65 -137 3,3-Dimethyl-1-butanol 250 231.6 ug/L 93 38 -144 4-Chlorotoluene 50.0 51.25 ug/L 103 70 -130 4-Methyl-2-pentanone (MIBK)200 222.6 ug/L 111 69 -138 Benzene 50.0 46.80 ug/L 94 70 -130 Bromobenzene 50.0 47.55 ug/L 95 70 -132 Bromochloromethane 50.0 46.19 ug/L 92 70 -130 Bromodichloromethane 50.0 47.96 ug/L 96 67 -133 Bromoform 50.0 47.35 ug/L 95 57 -140 Bromomethane 50.0 42.38 ug/L 85 10 -160 Carbon tetrachloride 50.0 45.94 ug/L 92 61 -137 Chlorobenzene 50.0 47.01 ug/L 94 70 -130 Chloroethane 50.0 44.64 ug/L 89 55 -141 Chloroform 50.0 47.62 ug/L 95 69 -130 Chloromethane 50.0 49.63 ug/L 99 58 -137 cis-1,2-Dichloroethene 50.0 48.76 ug/L 98 68 -130 cis-1,3-Dichloropropene 50.0 49.08 ug/L 98 69 -132 Dibromochloromethane 50.0 46.63 ug/L 93 67 -135 Dichlorodifluoromethane 50.0 44.67 ug/L 89 41 -146 Diisopropyl ether 50.0 52.59 ug/L 105 64 -132 Ethanol 2000 1201 ug/L 60 20 -160 Ethyl tert-butyl ether 50.0 50.14 ug/L 100 55 -133 Ethylbenzene 50.0 48.33 ug/L 97 70 -130 Isopropylbenzene 50.0 49.66 ug/L 99 70 -130 Methyl tert-butyl ether 50.0 49.25 ug/L 98 66 -130 Methylene Chloride 50.0 48.40 ug/L 97 66 -135 m-Xylene & p-Xylene 50.0 49.08 ug/L 98 70 -130 Naphthalene 50.0 47.95 ug/L 96 47 -149 n-Butylbenzene 50.0 54.68 ug/L 109 67 -130 N-Propylbenzene 50.0 49.71 ug/L 99 70 -130 o-Xylene 50.0 48.94 ug/L 98 70 -130 p-Cymene (p-Isopropyltoluene)50.0 52.37 ug/L 105 65 -130 sec-Butylbenzene 50.0 51.97 ug/L 104 66 -130 Styrene 50.0 47.60 ug/L 95 70 -130 t-Amyl alcohol 500 527.3 ug/L 105 38 -139 Tert-amyl methyl ether 50.0 50.17 ug/L 100 52 -132 tert-Butyl Formate 250 268.0 ug/L 107 10 -160 tert-Butylbenzene 50.0 50.08 ug/L 100 64 -139 Tetrachloroethene 50.0 43.21 ug/L 86 65 -130 Toluene 50.0 46.04 ug/L 92 70 -130 trans-1,2-Dichloroethene 50.0 47.36 ug/L 95 70 -130 trans-1,3-Dichloropropene 50.0 49.12 ug/L 98 63 -130 Trichloroethene 50.0 45.82 ug/L 92 70 -130 Eurofins Pensacola Page 23 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: SM6200-B - Volatile Organic Compounds (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645916/1008 Matrix: Water Prep Type: Total/NA Analysis Batch: 645916 Trichlorofluoromethane 50.0 46.86 ug/L 94 65 -138 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Vinyl acetate 100 131.0 ug/L 131 26 -160 Vinyl chloride 50.0 50.26 ug/L 101 59 -136 Xylenes, Total 100 98.01 ug/L 98 70 -130 4-Bromofluorobenzene 72 -130 Surrogate 103 LCS LCS Qualifier Limits%Recovery 103Dibromofluoromethane 75 -126 100Toluene-d8 (Surr)64 -132 Client Sample ID: Method BlankLab Sample ID: MB 400-646204/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 646204 RL MDL Acetone <10.0 U 25.0 10.0 ug/L 10/19/23 08:50 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 4-Bromofluorobenzene 106 72-130 10/19/23 08:50 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 91 10/19/23 08:50 1Dibromofluoromethane75-126 105 10/19/23 08:50 1Toluene-d8 (Surr)64-132 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646204/1002 Matrix: Water Prep Type: Total/NA Analysis Batch: 646204 Acetone 200 198.8 ug/L 99 43 -160 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 4-Bromofluorobenzene 72 -130 Surrogate 105 LCS LCS Qualifier Limits%Recovery 90Dibromofluoromethane 75 -126 104Toluene-d8 (Surr)64 -132 Method: 625.1 - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 400-645683/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 RL MDL 1,2,4-Trichlorobenzene <0.180 U 10.0 0.180 ug/L 10/16/23 11:18 10/17/23 18:08 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.150 U 0.15010.0 ug/L 10/16/23 11:18 10/17/23 18:08 11-Methylnaphthalene <0.160 U 0.16010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,2'-oxybis(1-chloropropane) <3.70 U 3.7010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,4,5-Trichlorophenol <2.60 U 2.6010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,4,6-Trichlorophenol <2.00 U 2.0010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,4-Dichlorophenol <2.00 U 2.0010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,4-Dimethylphenol Eurofins Pensacola Page 24 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-645683/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 RL MDL 2,4-Dinitrophenol <3.40 U 30.0 3.40 ug/L 10/16/23 11:18 10/17/23 18:08 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.90 U 1.9010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,4-Dinitrotoluene <1.90 U 1.9010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12,6-Dinitrotoluene <0.140 U 0.14010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12-Chloronaphthalene <2.20 U 2.2010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12-Chlorophenol <0.130 U 0.13010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12-Methylnaphthalene <1.80 U 1.8010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12-Methylphenol <2.20 U 2.2010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12-Nitroaniline <2.40 U 2.4010.0 ug/L 10/16/23 11:18 10/17/23 18:08 12-Nitrophenol <0.390 U 0.39020.0 ug/L 10/16/23 11:18 10/17/23 18:08 13 & 4 Methylphenol <2.60 U 2.6010.0 ug/L 10/16/23 11:18 10/17/23 18:08 13,3'-Dichlorobenzidine <1.80 U 1.8010.0 ug/L 10/16/23 11:18 10/17/23 18:08 13-Nitroaniline <1.60 U 1.6010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14,6-Dinitro-2-methylphenol <0.200 U 0.20010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14-Bromophenyl phenyl ether <3.80 U 3.8010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14-Chloro-3-methylphenol <3.40 U 3.4010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14-Chloroaniline <2.00 U 2.0010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14-Chlorophenyl phenyl ether <1.50 U 1.5010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14-Nitroaniline <2.10 U 2.1010.0 ug/L 10/16/23 11:18 10/17/23 18:08 14-Nitrophenol <0.160 U 0.16010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Acenaphthene <0.170 U 0.17010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Acenaphthylene <0.180 U 0.18010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Anthracene <20.0 U 20.025.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzidine <0.180 U 0.18010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzo[a]anthracene <0.120 U 0.12010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzo[a]pyrene <0.150 U 0.15010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzo[b]fluoranthene <0.230 U 0.23010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzo[g,h,i]perylene <0.160 U 0.16010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzo[k]fluoranthene <7.30 U 7.3030.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzoic acid <2.00 U 2.0010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Benzyl alcohol <0.160 U 0.16010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Bis(2-chloroethoxy)methane <2.70 U 2.7010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Bis(2-chloroethyl)ether <5.00 U 5.0010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Bis(2-ethylhexyl) phthalate <0.190 U 0.19010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Butyl benzyl phthalate <0.190 U 0.19010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Chrysene <0.240 U 0.24010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Dibenz(a,h)anthracene <0.170 U 0.17010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Dibenzofuran <0.240 U 0.24010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Diethyl phthalate <0.170 U 0.17010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Dimethyl phthalate <1.40 U 1.4010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Di-n-butyl phthalate <0.170 U 0.17010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Di-n-octyl phthalate <0.180 U 0.18010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Fluoranthene <0.180 U 0.18010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Fluorene <0.170 U 0.17010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Hexachlorobenzene <3.60 U 3.6010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Hexachlorobutadiene <2.60 U 2.6020.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Hexachlorocyclopentadiene <4.20 U 4.2010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Hexachloroethane <0.220 U 0.22010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Indeno[1,2,3-cd]pyrene <0.140 U 0.14010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Isophorone Eurofins Pensacola Page 25 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-645683/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 RL MDL Naphthalene <0.170 U 10.0 0.170 ug/L 10/16/23 11:18 10/17/23 18:08 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.130 U 0.13010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Nitrobenzene <3.30 U 3.3010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1N-Nitrosodi-n-propylamine <0.180 U 0.18010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1N-Nitrosodiphenylamine <1.40 U 1.4020.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Pentachlorophenol <0.180 U 0.18010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Phenanthrene <1.10 U 1.1010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Phenol <0.210 U 0.21010.0 ug/L 10/16/23 11:18 10/17/23 18:08 1Pyrene 2,4,6-Tribromophenol 56 15-135 10/17/23 18:08 1 MB MB Surrogate 10/16/23 11:18 Dil FacPreparedAnalyzedQualifierLimits%Recovery 58 10/16/23 11:18 10/17/23 18:08 12-Fluorobiphenyl 32-109 34 10/16/23 11:18 10/17/23 18:08 12-Fluorophenol 10-104 50 10/16/23 11:18 10/17/23 18:08 1Nitrobenzene-d5 31-111 27 10/16/23 11:18 10/17/23 18:08 1Phenol-d5 10-110 56 10/16/23 11:18 10/17/23 18:08 1Terphenyl-d14 30-129 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645683/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 1,2,4-Trichlorobenzene 120 82.10 ug/L 68 57 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1-Methylnaphthalene 120 91.34 ug/L 76 53 -130 2,2'-oxybis(1-chloropropane)120 62.15 *-ug/L 52 63 -139 2,4,5-Trichlorophenol 120 96.96 ug/L 81 55 -140 2,4,6-Trichlorophenol 120 88.45 ug/L 74 52 -129 2,4-Dichlorophenol 120 87.59 ug/L 73 53 -122 2,4-Dimethylphenol 120 132.7 ug/L 111 42 -120 2,4-Dinitrophenol 240 176.2 ug/L 73 10 -173 2,4-Dinitrotoluene 120 99.78 ug/L 83 48 -127 2,6-Dinitrotoluene 120 94.50 ug/L 79 68 -137 2-Chloronaphthalene 120 87.13 ug/L 73 65 -120 2-Chlorophenol 120 77.18 ug/L 64 36 -120 2-Methylnaphthalene 120 89.58 ug/L 75 53 -130 2-Methylphenol 120 85.86 ug/L 72 51 -130 2-Nitroaniline 120 98.66 ug/L 82 41 -130 2-Nitrophenol 120 87.56 ug/L 73 61 -163 3 & 4 Methylphenol 120 79.09 ug/L 66 49 -130 3,3'-Dichlorobenzidine 240 153.8 ug/L 64 10 -213 3-Nitroaniline 120 66.39 ug/L 55 25 -130 4,6-Dinitro-2-methylphenol 240 192.0 ug/L 80 53 -130 4-Bromophenyl phenyl ether 120 91.82 ug/L 77 65 -120 4-Chloro-3-methylphenol 120 90.08 ug/L 75 41 -128 4-Chloroaniline 120 61.09 ug/L 51 10 -130 4-Chlorophenyl phenyl ether 120 97.74 ug/L 81 38 -145 4-Nitroaniline 120 87.21 ug/L 73 28 -130 4-Nitrophenol 240 251.7 ug/L 105 13 -129 Eurofins Pensacola Page 26 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645683/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 Acenaphthene 120 96.06 ug/L 80 60 -132 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 120 92.68 ug/L 77 54 -126 Anthracene 120 96.97 ug/L 81 43 -120 Benzidine 659 137.9 ug/L 21 5-130 Benzo[a]anthracene 120 92.08 ug/L 77 42 -133 Benzo[a]pyrene 120 98.35 ug/L 82 32 -148 Benzo[b]fluoranthene 120 95.39 ug/L 79 42 -140 Benzo[g,h,i]perylene 120 76.34 ug/L 64 10 -195 Benzo[k]fluoranthene 120 104.0 ug/L 87 25 -146 Benzoic acid 522 183.5 ug/L 35 19 -126 Benzyl alcohol 120 76.05 ug/L 63 10 -130 Bis(2-chloroethoxy)methane 120 69.37 ug/L 58 49 -165 Bis(2-chloroethyl)ether 120 54.47 ug/L 45 43 -126 Bis(2-ethylhexyl) phthalate 120 103.0 ug/L 86 29 -137 Butyl benzyl phthalate 120 100.5 ug/L 84 10 -140 Chrysene 120 93.50 ug/L 78 44 -140 Dibenz(a,h)anthracene 120 84.53 ug/L 70 10 -200 Dibenzofuran 120 92.49 ug/L 77 59 -130 Diethyl phthalate 120 106.1 ug/L 88 10 -120 Dimethyl phthalate 120 95.42 ug/L 80 10 -120 Di-n-butyl phthalate 120 102.7 ug/L 86 10 -120 Di-n-octyl phthalate 120 97.32 ug/L 81 19 -132 Fluoranthene 120 101.5 ug/L 85 43 -121 Fluorene 120 97.18 ug/L 81 70 -120 Hexachlorobenzene 120 91.89 ug/L 77 10 -142 Hexachlorobutadiene 120 94.41 ug/L 79 38 -120 Hexachlorocyclopentadiene 120 79.00 ug/L 66 10 -130 Hexachloroethane 120 78.74 ug/L 66 55 -120 Indeno[1,2,3-cd]pyrene 120 74.16 ug/L 62 10 -151 Isophorone 120 81.77 ug/L 68 47 -180 Naphthalene 120 85.38 ug/L 71 36 -120 Nitrobenzene 120 82.75 ug/L 69 54 -158 N-Nitrosodi-n-propylamine 120 82.35 ug/L 69 14 -198 N-Nitrosodiphenylamine 119 86.46 ug/L 73 57 -130 Pentachlorophenol 240 167.5 ug/L 70 38 -152 Phenanthrene 120 92.46 ug/L 77 65 -120 Phenol 120 53.24 ug/L 44 17 -120 Pyrene 120 89.80 ug/L 75 70 -120 2,4,6-Tribromophenol 15 -135 Surrogate 84 LCS LCS Qualifier Limits%Recovery 732-Fluorobiphenyl 32 -109 432-Fluorophenol 10 -104 86Nitrobenzene-d5 31 -111 43Phenol-d5 10 -110 73Terphenyl-d14 30 -129 Eurofins Pensacola Page 27 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645683/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 1,2,4-Trichlorobenzene 120 83.48 ug/L 70 57 -130 2 40 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD 1-Methylnaphthalene 120 88.95 ug/L 74 53 -130 3 40 2,2'-oxybis(1-chloropropane)120 65.36 *-ug/L 54 63 -139 5 40 2,4,5-Trichlorophenol 120 96.96 ug/L 81 55 -140 0 40 2,4,6-Trichlorophenol 120 91.33 ug/L 76 52 -129 3 40 2,4-Dichlorophenol 120 86.71 ug/L 72 53 -122 1 40 2,4-Dimethylphenol 120 128.6 ug/L 107 42 -120 3 40 2,4-Dinitrophenol 240 181.8 ug/L 76 10 -173 3 40 2,4-Dinitrotoluene 120 98.41 ug/L 82 48 -127 1 40 2,6-Dinitrotoluene 120 95.67 ug/L 80 68 -137 1 40 2-Chloronaphthalene 120 87.15 ug/L 73 65 -120 0 24 2-Chlorophenol 120 78.11 ug/L 65 36 -120 1 40 2-Methylnaphthalene 120 87.10 ug/L 73 53 -130 3 40 2-Methylphenol 120 86.52 ug/L 72 51 -130 1 40 2-Nitroaniline 120 97.16 ug/L 81 41 -130 2 40 2-Nitrophenol 120 91.19 ug/L 76 61 -163 4 40 3 & 4 Methylphenol 120 77.73 ug/L 65 49 -130 2 40 3,3'-Dichlorobenzidine 240 153.6 ug/L 64 10 -213 0 40 3-Nitroaniline 120 65.40 ug/L 55 25 -130 1 40 4,6-Dinitro-2-methylphenol 240 189.2 ug/L 79 53 -130 2 40 4-Bromophenyl phenyl ether 120 93.95 ug/L 78 65 -120 2 40 4-Chloro-3-methylphenol 120 89.09 ug/L 74 41 -128 1 40 4-Chloroaniline 120 60.35 ug/L 50 10 -130 1 40 4-Chlorophenyl phenyl ether 120 98.67 ug/L 82 38 -145 1 40 4-Nitroaniline 120 89.28 ug/L 74 28 -130 2 40 4-Nitrophenol 240 244.9 ug/L 102 13 -129 3 40 Acenaphthene 120 95.21 ug/L 79 60 -132 1 40 Acenaphthylene 120 93.80 ug/L 78 54 -126 1 40 Anthracene 120 95.98 ug/L 80 43 -120 1 40 Benzidine 659 209.3 *1 ug/L 32 5-130 41 40 Benzo[a]anthracene 120 90.44 ug/L 75 42 -133 2 40 Benzo[a]pyrene 120 98.46 ug/L 82 32 -148 0 40 Benzo[b]fluoranthene 120 94.52 ug/L 79 42 -140 1 40 Benzo[g,h,i]perylene 120 79.65 ug/L 66 10 -195 4 40 Benzo[k]fluoranthene 120 100.0 ug/L 83 25 -146 4 40 Benzoic acid 522 175.6 ug/L 34 19 -126 4 40 Benzyl alcohol 120 74.52 ug/L 62 10 -130 2 40 Bis(2-chloroethoxy)methane 120 69.80 ug/L 58 49 -165 1 40 Bis(2-chloroethyl)ether 120 61.43 ug/L 51 43 -126 12 40 Bis(2-ethylhexyl) phthalate 120 99.22 ug/L 83 29 -137 4 40 Butyl benzyl phthalate 120 118.9 ug/L 99 10 -140 17 40 Chrysene 120 94.34 ug/L 79 44 -140 1 40 Dibenz(a,h)anthracene 120 88.67 ug/L 74 10 -200 5 40 Dibenzofuran 120 92.85 ug/L 77 59 -130 0 40 Diethyl phthalate 120 106.1 ug/L 88 10 -120 0 40 Dimethyl phthalate 120 93.31 ug/L 78 10 -120 2 40 Di-n-butyl phthalate 120 102.3 ug/L 85 10 -120 0 40 Di-n-octyl phthalate 120 101.5 ug/L 85 19 -132 4 40 Eurofins Pensacola Page 28 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645683/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645849 Prep Batch: 645683 Fluoranthene 120 115.6 ug/L 96 43 -121 13 40 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Fluorene 120 100.9 ug/L 84 70 -120 4 38 Hexachlorobenzene 120 90.98 ug/L 76 10 -142 1 40 Hexachlorobutadiene 120 90.07 ug/L 75 38 -120 5 40 Hexachlorocyclopentadiene 120 85.72 ug/L 71 10 -130 8 40 Hexachloroethane 120 79.30 ug/L 66 55 -120 1 40 Indeno[1,2,3-cd]pyrene 120 80.69 ug/L 67 10 -151 8 40 Isophorone 120 80.49 ug/L 67 47 -180 2 40 Naphthalene 120 84.42 ug/L 70 36 -120 1 40 Nitrobenzene 120 79.37 ug/L 66 54 -158 4 40 N-Nitrosodi-n-propylamine 120 86.32 ug/L 72 14 -198 5 40 N-Nitrosodiphenylamine 119 88.71 ug/L 75 57 -130 3 40 Pentachlorophenol 240 169.2 ug/L 70 38 -152 1 40 Phenanthrene 120 97.40 ug/L 81 65 -120 5 39 Phenol 120 52.09 ug/L 43 17 -120 2 40 Pyrene 120 108.7 ug/L 91 70 -120 19 40 2,4,6-Tribromophenol 15 -135 Surrogate 81 LCSD LCSD Qualifier Limits%Recovery 722-Fluorobiphenyl 32 -109 442-Fluorophenol 10 -104 83Nitrobenzene-d5 31 -111 42Phenol-d5 10 -110 89Terphenyl-d14 30 -129 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-646250/2 Matrix: Water Prep Type: Total/NA Analysis Batch: 646250 RL MDL C5-C8 Aliphatics <26.0 U 26.0 26.0 ug/L 10/19/23 19:08 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <11.0 U 11.011.0 ug/L 10/19/23 19:08 1C9-C12 Aliphatics <7.00 U 7.007.00 ug/L 10/19/23 19:08 1C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)85 70-130 10/19/23 19:08 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 87 10/19/23 19:08 1a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646250/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 646250 C5-C8 Aliphatics 300 368.4 ug/L 123 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 350 360.3 ug/L 103 70 -130 C9-C10 Aromatics 50.0 48.60 ug/L 97 70 -130 Eurofins Pensacola Page 29 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646250/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 646250 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 88 LCS LCS Qualifier Limits%Recovery 88a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-646250/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 646250 C5-C8 Aliphatics 300 364.6 ug/L 122 70 -130 1 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 350 342.8 ug/L 98 70 -130 5 25 C9-C10 Aromatics 50.0 46.98 ug/L 94 70 -130 3 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 88 LCSD LCSD Qualifier Limits%Recovery 88a,a,a-Trifluorotoluene (pid)70 -130 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-645382/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645456 Prep Batch: 645382 RL MDL C9-C18 Aliphatics <142 U 142 142 ug/L 10/12/23 21:48 10/13/23 23:22 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <142 U 142142 ug/L 10/12/23 21:48 10/13/23 23:22 1C19-C36 Aliphatics <293 U 293293 ug/L 10/12/23 21:48 10/13/23 23:22 1C11-C22 Aromatics 1-Chlorooctadecane 82 40-140 10/13/23 23:22 1 MB MB Surrogate 10/12/23 21:48 Dil FacPreparedAnalyzedQualifierLimits%Recovery 92 10/12/23 21:48 10/13/23 23:22 1o-Terphenyl 40-140 124 10/12/23 21:48 10/13/23 23:22 12-Fluorobiphenyl 40-140 119 10/12/23 21:48 10/13/23 23:22 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645382/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645456 Prep Batch: 645382 C9-C18 Aliphatics 1290 1164 ug/L 90 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 1720 1488 ug/L 86 40 -140 1-Chlorooctadecane 40 -140 Surrogate 81 LCS LCS Qualifier Limits%Recovery Eurofins Pensacola Page 30 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645382/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645458 Prep Batch: 645382 C11-C22 Aromatics 3660 3490 ug/L 95 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl 40 -140 Surrogate 101 LCS LCS Qualifier Limits%Recovery 1332-Fluorobiphenyl 40 -140 1292-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645382/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645456 Prep Batch: 645382 C9-C18 Aliphatics 1290 1189 ug/L 92 40 -140 2 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 1720 1694 ug/L 98 40 -140 13 50 1-Chlorooctadecane 40 -140 Surrogate 86 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645382/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 645458 Prep Batch: 645382 C11-C22 Aromatics 3660 3107 ug/L 85 40 -140 12 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 87 LCSD LCSD Qualifier Limits%Recovery 1112-Fluorobiphenyl 40 -140 1062-Bromonaphthalene 40 -140 Method: 6010D - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 400-645663/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 646279 Prep Batch: 645663 RL MDL Lead <0.00200 U 0.0100 0.00200 mg/L 10/17/23 07:58 10/18/23 22:06 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645663/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 646279 Prep Batch: 645663 Lead 1.00 0.9826 mg/L 98 80 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Eurofins Pensacola Page 31 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Client Sample ID: MW-1 Lab Sample ID: 400-244922-1 Matrix: WaterDate Collected: 10/10/23 17:40 Date Received: 10/12/23 09:41 Analysis SM6200-B WPD10/19/23 09:141 EET PEN646204 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Analysis SM6200-B 1 645916 10/17/23 23:50 CAR EET PENTotal/NA 5 mL 5 mL Prep 625 645683 10/16/23 11:18 SNG EET PENTotal/NA 256.4 mL 1 mL Analysis 625.1 1 645849 10/17/23 21:11 S1B EET PENTotal/NA 0.4 mL 0.4 mL Analysis MAVPH 1 646250 10/19/23 22:15 SRK EET PENTotal/NA 5 mL 5 mL Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 57.4 mL 2 mL Analysis MA-EPH 1 645456 10/13/23 23:57 MP EET PENTotal/NA Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 57.4 mL 2 mL Analysis MA-EPH 1 645458 10/14/23 00:08 MP EET PENTotal/NA 1 mL 1 mL Prep 3010A 645663 10/17/23 07:58 MS EET PENTotal/NA 10 mL 50 mL Completed:10/17/23 13:34 ¹ Analysis 6010D 1 646279 10/18/23 23:25 BAW EET PENTotal/NA Client Sample ID: MW-2 Lab Sample ID: 400-244922-2 Matrix: WaterDate Collected: 10/10/23 17:20 Date Received: 10/12/23 09:41 Analysis SM6200-B WPD10/19/23 09:361 EET PEN646204 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Analysis SM6200-B 1 645916 10/18/23 00:08 CAR EET PENTotal/NA 5 mL 5 mL Prep 625 645683 10/16/23 11:18 SNG EET PENTotal/NA 243.6 mL 1 mL Analysis 625.1 1 645849 10/17/23 21:37 S1B EET PENTotal/NA 0.4 mL 0.4 mL Analysis MAVPH 1 646250 10/19/23 22:46 SRK EET PENTotal/NA 5 mL 5 mL Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 57.2 mL 2 mL Analysis MA-EPH 1 645456 10/14/23 00:08 MP EET PENTotal/NA Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 57.2 mL 2 mL Analysis MA-EPH 1 645458 10/14/23 00:20 MP EET PENTotal/NA 1 mL 1 mL Prep 3010A 645663 10/17/23 07:58 MS EET PENTotal/NA 10 mL 50 mL Completed:10/17/23 13:34 ¹ Analysis 6010D 1 646279 10/18/23 23:29 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645382/1-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3511 JTC10/12/23 21:48 EET PEN645382 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 58 mL 2 mL Analysis MA-EPH 1 645456 10/13/23 23:22 MP EET PENTotal/NA Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 58 mL 2 mL Analysis MA-EPH 1 645458 10/13/23 23:22 MP EET PENTotal/NA 1 mL 1 mL Eurofins Pensacola Page 32 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Client Sample ID: Method Blank Lab Sample ID: MB 400-645663/1-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3010A MS10/17/23 07:58 EET PEN645663 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 50 mL 50 mL Completed:10/17/23 13:34 ¹ Analysis 6010D 1 646279 10/18/23 22:06 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645683/1-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 625 SNG10/16/23 11:18 EET PEN645683 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 250 mL 1 mL Analysis 625.1 1 645849 10/17/23 18:08 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-645916/32 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis SM6200-B CAR10/17/23 15:571 EET PEN645916 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-646204/5 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis SM6200-B WPD10/19/23 08:501 EET PEN646204 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-646250/2 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis MAVPH SRK10/19/23 19:081 EET PEN646250 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645382/2-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3511 JTC10/12/23 21:48 EET PEN645382 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 58 mL 2 mL Analysis MA-EPH 1 645456 10/13/23 23:34 MP EET PENTotal/NA Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 58 mL 2 mL Analysis MA-EPH 1 645458 10/13/23 23:45 MP EET PENTotal/NA 1 mL 1 mL Eurofins Pensacola Page 33 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645663/2-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3010A MS10/17/23 07:58 EET PEN645663 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 50 mL 50 mL Completed:10/17/23 13:34 ¹ Analysis 6010D 1 646279 10/18/23 22:10 BAW EET PENTotal/NA Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645683/2-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 625 SNG10/16/23 11:18 EET PEN645683 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 250 mL 1 mL Analysis 625.1 1 645849 10/17/23 18:34 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645916/1008 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis SM6200-B CAR10/17/23 15:011 EET PEN645916 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-646204/1002 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis SM6200-B WPD10/19/23 08:041 EET PEN646204 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-646250/3 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis MAVPH SRK10/19/23 19:391 EET PEN646250 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-645382/3-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3511 JTC10/12/23 21:48 EET PEN645382 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 58 mL 2 mL Analysis MA-EPH 1 645456 10/13/23 23:45 MP EET PENTotal/NA Prep 3511 645382 10/12/23 21:48 JTC EET PENTotal/NA 58 mL 2 mL Analysis MA-EPH 1 645458 10/13/23 23:57 MP EET PENTotal/NA 1 mL 1 mL Eurofins Pensacola Page 34 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-645683/3-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 625 SNG10/16/23 11:18 EET PEN645683 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 250 mL 1 mL Analysis 625.1 1 645849 10/17/23 19:00 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-646250/4 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis MAVPH SRK10/19/23 20:101 EET PEN646250 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL ¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 35 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 400-244922-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method Method Description LaboratoryProtocol SMSM6200-B Volatile Organic Compounds EET PEN EPA625.1 Semivolatile Organic Compounds (GC/MS)EET PEN MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN SW8466010DMetals (ICP)EET PEN SW8463010APreparation, Total Metals EET PEN SW8463511Microextraction of Organic Compounds EET PEN SW8465030BPurge and Trap EET PEN EPA625Liquid-Liquid Extraction EET PEN Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 36 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Consultech Environmental LLC Job ID: 400-244922-1 Project/Site: Kwik Stop Laboratory: Eurofins Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte SM6200-B Water 2-Butanone (MEK) SM6200-B Water 2-Hexanone SM6200-B Water 3,3-Dimethyl-1-butanol SM6200-B Water 4-Methyl-2-pentanone (MIBK) SM6200-B Water Acetone SM6200-B Water Ethyl tert-butyl ether SM6200-B Water t-Amyl alcohol SM6200-B Water Tert-amyl methyl ether SM6200-B Water tert-Butyl Formate SM6200-B Water Vinyl acetate Eurofins Pensacola Page 37 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 38 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Consultech Environmental LLC Job Number: 400-244922-1 Login Number: 244922 Question Answer Comment Creator: Roberts, Alexis J List Source: Eurofins Pensacola List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.4.6°C IR8 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Pensacola Page 39 of 39 10/23/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 ANALYTICAL REPORT PREPARED FOR Attn: Raj Shah Consultech Environmental LLC 2021 Energy Drive Apex, North Carolina 27502 Generated 10/25/2023 11:35:29 AM JOB DESCRIPTION Kwik Stop JOB NUMBER 400-244947-1 See page two for job notes and contact information. Pensacola FL 32514 3355 McLemore Drive Eurofins Pensacola Page 1 of 44 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Pensacola Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 10/25/2023 11:35:29 AM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Consultech Environmental LLC Project/Site: Kwik Stop Laboratory Job ID: 400-244947-1 Page 3 of 44 Eurofins Pensacola10/25/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Job ID: 400-244947-1 Laboratory: Eurofins Pensacola Narrative Job Narrative 400-244947-1 Receipt The samples were received on 10/12/2023 9:41 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 0.9°C GC/MS VOA No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 8270E: The following analyte recovered outside control limits for the LCS associated with preparation batch 400-645696 and analytical batch 400-645850: 4-Chloro-3-methylphenol. This is not indicative of a systematic control problem because this was a random marginal exceedance. Qualified results have been reported. Method 8270E: Physical properties (viscosity, color, odor) of the following sample extract preclude concentrated analysis which would jeopardize instrumentation: MW-2 5' (400-244947-1) Minimal dilution with elevated RLs is reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAVPH: The following samples were diluted because the base dilution for VPH soil analysis is 1:50:MW-2 5' (400-244947-1), MW-2 10' (400-244947-2) and MW-2 15' (400-244947-3). No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins PensacolaPage 4 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 ☼Acetone RL 0.0238 mg/Kg MDL 0.0114 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0427 8260D ☼C9-C18 Aliphatics 2.04 mg/Kg2.04 Total/NA115.5 F1 MA-EPH ☼C19-C36 Aliphatics 2.04 mg/Kg2.04 Total/NA13.43 MA-EPH ☼Chromium 1.24 mg/Kg0.384 Total/NA132.8 6010D ☼Lead 1.24 mg/Kg0.272 Total/NA114.2 6010D Client Sample ID: MW-2 10'Lab Sample ID: 400-244947-2 ☼C9-C18 Aliphatics RL 1.76 mg/Kg MDL 1.76 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA110.5 MA-EPH ☼C19-C36 Aliphatics 1.76 mg/Kg1.76 Total/NA17.22 MA-EPH Client Sample ID: MW-2 15'Lab Sample ID: 400-244947-3 ☼Acetone RL 0.0309 mg/Kg MDL 0.0148 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0514 8260D ☼C9-C10 Aromatics 0.616 mg/Kg0.616 Total/NA502.59 MAVPH ☼Chromium 1.12 mg/Kg0.348 Total/NA120.4 6010D ☼Lead 1.12 mg/Kg0.247 Total/NA18.88 6010D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 5 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Lab Sample ID Client Sample ID Matrix Collected Received 400-244947-1 MW-2 5'Solid 10/10/23 14:15 10/12/23 09:41 400-244947-2 MW-2 10'Solid 10/10/23 14:23 10/12/23 09:41 400-244947-3 MW-2 15'Solid 10/10/23 14:31 10/12/23 09:41 Eurofins PensacolaPage 6 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-1Client Sample ID: MW-2 5' Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL <0.00105 U 0.00476 0.00105 mg/Kg ☼10/18/23 10:10 10/18/23 17:18 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00476 0.00105 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00105 U1,1,1-Trichloroethane 0.00476 0.000781 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000781 U1,1,2,2-Tetrachloroethane 0.00476 0.000743 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000743 U1,1,2-Trichloroethane 0.00476 0.000791 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000791 U1,1-Dichloroethane 0.00476 0.000810 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000810 U1,1-Dichloroethene 0.00476 0.000791 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000791 U1,1-Dichloropropene 0.00476 0.00105 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00105 U1,2,3-Trichlorobenzene 0.00476 0.000762 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000762 U1,2,3-Trichloropropane 0.00476 0.000877 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000877 U1,2,4-Trichlorobenzene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 U1,2,4-Trimethylbenzene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 U1,2-Dibromoethane 0.00476 0.000677 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000677 U1,2-Dichlorobenzene 0.00476 0.000781 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000781 U1,2-Dichloroethane 0.00476 0.000724 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000724 U1,2-Dichloropropane 0.00476 0.000791 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000791 U1,3,5-Trimethylbenzene 0.00476 0.000905 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000905 U1,3-Dichlorobenzene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 U1,3-Dichloropropane 0.00476 0.000819 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000819 U1,4-Dichlorobenzene 0.00476 0.00105 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00105 U2,2-Dichloropropane 0.0238 0.00572 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00572 U2-Butanone (MEK) 0.00476 0.000772 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000772 U2-Chlorotoluene 0.0238 0.00476 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00476 U2-Hexanone 0.00476 0.000934 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000934 U4-Chlorotoluene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 U4-Isopropyltoluene 0.0238 0.00476 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00476 U4-Methyl-2-pentanone (MIBK) 0.0238 0.0114 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼0.0427Acetone 0.00476 0.000638 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000638 UBenzene 0.00476 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00124 UBromobenzene 0.00476 0.000772 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000772 UBromochloromethane 0.00476 0.000877 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000877 UBromodichloromethane 0.00476 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00124 UBromoform 0.00476 0.00238 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00238 UBromomethane 0.00476 0.00162 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00162 UCarbon tetrachloride 0.00476 0.000495 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000495 UChlorobenzene 0.00476 0.00114 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00114 UChloroethane 0.00476 0.00476 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00476 UChloroform 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 UChloromethane 0.00476 0.000724 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000724 Ucis-1,2-Dichloroethene 0.00476 0.00114 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00114 Ucis-1,3-Dichloropropene 0.00476 0.00114 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00114 UDibromochloromethane 0.00476 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00124 UDichlorodifluoromethane 0.0953 0.0705 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.0705 UEthanol 0.00476 0.000581 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000581 UEthylbenzene 0.00476 0.000524 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000524 UIsopropyl ether 0.00476 0.000648 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000648 UIsopropylbenzene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 UMethyl tert-butyl ether 0.0143 0.00953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00953 UMethylene Chloride 0.00476 0.00286 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00286 UNaphthalene Eurofins Pensacola Page 7 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-1Client Sample ID: MW-2 5' Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL <0.000915 U 0.00476 0.000915 mg/Kg ☼10/18/23 10:10 10/18/23 17:18 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00476 0.000858 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000858 UN-Propylbenzene 0.00476 0.000905 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000905 Usec-Butylbenzene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 UStyrene 0.00476 0.00105 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00105 Utert-Butylbenzene 0.00476 0.00286 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00286 UTetrachloroethene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 UToluene 0.00476 0.000915 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000915 Utrans-1,2-Dichloroethene 0.00476 0.00105 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00105 Utrans-1,3-Dichloropropene 0.00476 0.000953 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000953 UTrichloroethene 0.00476 0.000819 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000819 UTrichlorofluoromethane 0.0238 0.00181 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00181 UVinyl acetate 0.00476 0.000762 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.000762 UVinyl chloride 0.00953 0.00181 mg/Kg 10/18/23 10:10 10/18/23 17:18 1☼<0.00181 UXylenes, Total 4-Bromofluorobenzene 96 67-130 10/18/23 10:10 10/18/23 17:18 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 114 10/18/23 10:10 10/18/23 17:18 177-127 Toluene-d8 (Surr)96 10/18/23 10:10 10/18/23 17:18 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL <0.0831 U 0.831 0.0831 mg/Kg ☼10/16/23 12:06 10/17/23 16:49 2 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U1,2-Dichlorobenzene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U1,3-Dichlorobenzene 0.831 0.327 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.327 U1,4-Dichlorobenzene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U1-Methylnaphthalene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2,4,5-Trichlorophenol 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2,4,6-Trichlorophenol 0.831 0.176 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.176 U2,4-Dichlorophenol 0.831 0.237 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.237 U2,4-Dimethylphenol 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2,4-Dinitrotoluene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2,6-Dinitrotoluene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2-Chloronaphthalene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2-Chlorophenol 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2-Methylnaphthalene 0.831 0.202 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.202 U2-Methylphenol 0.831 0.176 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.176 U2-Nitroaniline 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U2-Nitrophenol 1.66 0.194 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.194 U3 & 4 Methylphenol 0.831 0.196 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.196 U3-Nitroaniline 0.831 0.605 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.605 U4,6-Dinitro-2-methylphenol 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U4-Bromophenyl phenyl ether 0.831 0.204 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.204 U *-4-Chloro-3-methylphenol 0.831 0.204 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.204 U4-Chloroaniline 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 U4-Chlorophenyl phenyl ether 0.831 0.285 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.285 U4-Nitroaniline 0.831 0.756 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.756 U4-Nitrophenol 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UAcenaphthene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UAcenaphthylene Eurofins Pensacola Page 8 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-1Client Sample ID: MW-2 5' Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <0.247 U 0.831 0.247 mg/Kg ☼10/16/23 12:06 10/17/23 16:49 2 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Aniline 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UAnthracene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UBenzo[a]anthracene 0.831 0.118 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.118 UBenzo[a]pyrene 0.831 0.249 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.249 UBenzo[b]fluoranthene 0.831 0.277 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.277 UBenzo[g,h,i]perylene 0.831 0.196 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.196 UBenzo[k]fluoranthene 2.49 0.882 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.882 U F1 F2Benzoic acid 0.831 0.317 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.317 Ubis (2-chloroisopropyl) ether 0.831 0.184 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.184 UBis(2-chloroethoxy)methane 0.831 0.116 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.116 U F1Bis(2-chloroethyl)ether 0.831 0.204 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.204 UBis(2-ethylhexyl) phthalate 0.831 0.179 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.179 UButyl benzyl phthalate 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UChrysene 0.831 0.144 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.144 UDibenz(a,h)anthracene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UDibenzofuran 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UDiethyl phthalate 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UDimethyl phthalate 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UDi-n-butyl phthalate 0.831 0.302 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.302 UDi-n-octyl phthalate 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UFluoranthene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UFluorene 0.831 0.252 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.252 UHexachlorobenzene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UHexachlorobutadiene 0.831 0.166 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.166 U F1Hexachlorocyclopentadiene 0.831 0.176 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.176 UHexachloroethane 0.831 0.166 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.166 UIndeno[1,2,3-cd]pyrene 0.831 0.169 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.169 UIsophorone 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UNaphthalene 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UNitrobenzene 0.831 0.264 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.264 UN-Nitrosodi-n-propylamine 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UN-Nitrosodiphenylamine 1.66 0.403 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.403 UPentachlorophenol 0.831 0.0831 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.0831 UPhenanthrene 0.831 0.224 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.224 UPhenol 0.831 0.196 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.196 UPyrene 0.831 0.378 mg/Kg 10/16/23 12:06 10/17/23 16:49 2☼<0.378 U F1Pyridine 2,4,6-Tribromophenol (Surr)68 10-150 10/16/23 12:06 10/17/23 16:49 2 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 62 10/16/23 12:06 10/17/23 16:49 227-127 2-Fluorophenol (Surr)40 10/16/23 12:06 10/17/23 16:49 225-128 Nitrobenzene-d5 (Surr)48 10/16/23 12:06 10/17/23 16:49 215-136 Phenol-d5 (Surr)41 10/16/23 12:06 10/17/23 16:49 229-130 Terphenyl-d14 (Surr)70 10/16/23 12:06 10/17/23 16:49 224-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <3.26 U 3.26 3.26 mg/Kg ☼10/16/23 16:00 10/16/23 20:15 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.69 1.69 mg/Kg 10/16/23 16:00 10/16/23 20:15 50☼<1.69 UC9-C12 Aliphatics Eurofins Pensacola Page 9 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-1Client Sample ID: MW-2 5' Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL <0.906 U 0.906 0.906 mg/Kg ☼10/16/23 16:00 10/16/23 20:15 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)94 70-130 10/16/23 16:00 10/16/23 20:15 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)91 10/16/23 16:00 10/16/23 20:15 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 15.5 F1 2.04 2.04 mg/Kg ☼10/17/23 08:04 10/18/23 20:27 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 2.04 2.04 mg/Kg 10/17/23 08:04 10/18/23 20:27 1☼3.43C19-C36 Aliphatics 3.82 3.82 mg/Kg 10/17/23 08:04 10/18/23 20:50 1☼<3.82 UC11-C22 Aromatics 1-Chlorooctadecane 60 40-140 10/17/23 08:04 10/18/23 20:27 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 63 10/17/23 08:04 10/18/23 20:50 140-140 2-Fluorobiphenyl 94 10/17/23 08:04 10/18/23 20:50 140-140 2-Bromonaphthalene 94 10/17/23 08:04 10/18/23 20:50 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 32.8 1.24 0.384 mg/Kg ☼10/13/23 13:18 10/19/23 13:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.24 0.272 mg/Kg 10/13/23 13:18 10/19/23 13:14 1☼14.2Lead General Chemistry RL MDL 78.1 0.01 0.01 %10/19/23 17:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %10/19/23 17:19 121.9Percent Moisture (EPA Moisture) Eurofins Pensacola Page 10 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-2Client Sample ID: MW-2 10' Matrix: SolidDate Collected: 10/10/23 14:23 Percent Solids: 89.3Date Received: 10/12/23 09:41 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <2.18 U 2.18 2.18 mg/Kg ☼10/16/23 16:00 10/16/23 20:55 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.13 1.13 mg/Kg 10/16/23 16:00 10/16/23 20:55 50☼<1.13 UC9-C12 Aliphatics 0.606 0.606 mg/Kg 10/16/23 16:00 10/16/23 20:55 50☼<0.606 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)97 70-130 10/16/23 16:00 10/16/23 20:55 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)94 10/16/23 16:00 10/16/23 20:55 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 10.5 1.76 1.76 mg/Kg ☼10/17/23 08:04 10/18/23 20:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.76 1.76 mg/Kg 10/17/23 08:04 10/18/23 20:39 1☼7.22C19-C36 Aliphatics 3.30 3.30 mg/Kg 10/17/23 08:04 10/18/23 21:02 1☼<3.30 UC11-C22 Aromatics 1-Chlorooctadecane 82 40-140 10/17/23 08:04 10/18/23 20:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 85 10/17/23 08:04 10/18/23 21:02 140-140 2-Fluorobiphenyl 99 10/17/23 08:04 10/18/23 21:02 140-140 2-Bromonaphthalene 99 10/17/23 08:04 10/18/23 21:02 140-140 General Chemistry RL MDL 89.3 0.01 0.01 %10/19/23 17:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %10/19/23 17:19 110.7Percent Moisture (EPA Moisture) Eurofins Pensacola Page 11 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-3Client Sample ID: MW-2 15' Matrix: SolidDate Collected: 10/10/23 14:31 Percent Solids: 86.2Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL <0.00136 U 0.00618 0.00136 mg/Kg ☼10/18/23 10:10 10/18/23 17:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00618 0.00136 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00136 U1,1,1-Trichloroethane 0.00618 0.00101 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00101 U1,1,2,2-Tetrachloroethane 0.00618 0.000964 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000964 U1,1,2-Trichloroethane 0.00618 0.00103 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00103 U1,1-Dichloroethane 0.00618 0.00105 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00105 U1,1-Dichloroethene 0.00618 0.00103 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00103 U1,1-Dichloropropene 0.00618 0.00136 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00136 U1,2,3-Trichlorobenzene 0.00618 0.000989 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000989 U1,2,3-Trichloropropane 0.00618 0.00114 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00114 U1,2,4-Trichlorobenzene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 U1,2,4-Trimethylbenzene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 U1,2-Dibromoethane 0.00618 0.000878 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000878 U1,2-Dichlorobenzene 0.00618 0.00101 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00101 U1,2-Dichloroethane 0.00618 0.000939 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000939 U1,2-Dichloropropane 0.00618 0.00103 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00103 U1,3,5-Trimethylbenzene 0.00618 0.00117 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00117 U1,3-Dichlorobenzene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 U1,3-Dichloropropane 0.00618 0.00106 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00106 U1,4-Dichlorobenzene 0.00618 0.00136 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00136 U2,2-Dichloropropane 0.0309 0.00742 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00742 U2-Butanone (MEK) 0.00618 0.00100 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00100 U2-Chlorotoluene 0.0309 0.00618 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00618 U2-Hexanone 0.00618 0.00121 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00121 U4-Chlorotoluene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 U4-Isopropyltoluene 0.0309 0.00618 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00618 U4-Methyl-2-pentanone (MIBK) 0.0309 0.0148 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼0.0514Acetone 0.00618 0.000828 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000828 UBenzene 0.00618 0.00161 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00161 UBromobenzene 0.00618 0.00100 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00100 UBromochloromethane 0.00618 0.00114 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00114 UBromodichloromethane 0.00618 0.00161 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00161 UBromoform 0.00618 0.00309 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00309 UBromomethane 0.00618 0.00210 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00210 UCarbon tetrachloride 0.00618 0.000643 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000643 UChlorobenzene 0.00618 0.00148 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00148 UChloroethane 0.00618 0.00618 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00618 UChloroform 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 UChloromethane 0.00618 0.000939 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000939 Ucis-1,2-Dichloroethene 0.00618 0.00148 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00148 Ucis-1,3-Dichloropropene 0.00618 0.00148 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00148 UDibromochloromethane 0.00618 0.00161 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00161 UDichlorodifluoromethane 0.124 0.0915 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.0915 UEthanol 0.00618 0.000754 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000754 UEthylbenzene 0.00618 0.000680 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000680 UIsopropyl ether 0.00618 0.000840 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000840 UIsopropylbenzene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 UMethyl tert-butyl ether 0.0185 0.0124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.0124 UMethylene Chloride 0.00618 0.00371 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00371 UNaphthalene Eurofins Pensacola Page 12 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-3Client Sample ID: MW-2 15' Matrix: SolidDate Collected: 10/10/23 14:31 Percent Solids: 86.2Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL <0.00119 U 0.00618 0.00119 mg/Kg ☼10/18/23 10:10 10/18/23 17:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00618 0.00111 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00111 UN-Propylbenzene 0.00618 0.00117 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00117 Usec-Butylbenzene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 UStyrene 0.00618 0.00136 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00136 Utert-Butylbenzene 0.00618 0.00371 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00371 UTetrachloroethene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 UToluene 0.00618 0.00119 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00119 Utrans-1,2-Dichloroethene 0.00618 0.00136 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00136 Utrans-1,3-Dichloropropene 0.00618 0.00124 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00124 UTrichloroethene 0.00618 0.00106 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00106 UTrichlorofluoromethane 0.0309 0.00235 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00235 UVinyl acetate 0.00618 0.000989 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.000989 UVinyl chloride 0.0124 0.00235 mg/Kg 10/18/23 10:10 10/18/23 17:41 1☼<0.00235 UXylenes, Total 4-Bromofluorobenzene 98 67-130 10/18/23 10:10 10/18/23 17:41 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 112 10/18/23 10:10 10/18/23 17:41 177-127 Toluene-d8 (Surr)97 10/18/23 10:10 10/18/23 17:41 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL <0.0381 U 0.381 0.0381 mg/Kg ☼10/16/23 12:06 10/17/23 17:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U1,2-Dichlorobenzene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U1,3-Dichlorobenzene 0.381 0.150 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.150 U1,4-Dichlorobenzene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U1-Methylnaphthalene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2,4,5-Trichlorophenol 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2,4,6-Trichlorophenol 0.381 0.0809 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0809 U2,4-Dichlorophenol 0.381 0.109 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.109 U2,4-Dimethylphenol 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2,4-Dinitrotoluene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2,6-Dinitrotoluene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2-Chloronaphthalene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2-Chlorophenol 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2-Methylnaphthalene 0.381 0.0924 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0924 U2-Methylphenol 0.381 0.0809 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0809 U2-Nitroaniline 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U2-Nitrophenol 0.763 0.0890 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0890 U3 & 4 Methylphenol 0.381 0.0901 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0901 U3-Nitroaniline 0.381 0.277 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.277 U4,6-Dinitro-2-methylphenol 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U4-Bromophenyl phenyl ether 0.381 0.0936 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0936 U *-4-Chloro-3-methylphenol 0.381 0.0936 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0936 U4-Chloroaniline 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 U4-Chlorophenyl phenyl ether 0.381 0.131 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.131 U4-Nitroaniline 0.381 0.347 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.347 U4-Nitrophenol 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UAcenaphthene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UAcenaphthylene Eurofins Pensacola Page 13 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-3Client Sample ID: MW-2 15' Matrix: SolidDate Collected: 10/10/23 14:31 Percent Solids: 86.2Date Received: 10/12/23 09:41 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <0.113 U 0.381 0.113 mg/Kg ☼10/16/23 12:06 10/17/23 17:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Aniline 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UAnthracene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UBenzo[a]anthracene 0.381 0.0543 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0543 UBenzo[a]pyrene 0.381 0.114 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.114 UBenzo[b]fluoranthene 0.381 0.127 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.127 UBenzo[g,h,i]perylene 0.381 0.0901 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0901 UBenzo[k]fluoranthene 1.14 0.404 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.404 UBenzoic acid 0.381 0.146 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.146 Ubis (2-chloroisopropyl) ether 0.381 0.0843 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0843 UBis(2-chloroethoxy)methane 0.381 0.0532 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0532 UBis(2-chloroethyl)ether 0.381 0.0936 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0936 UBis(2-ethylhexyl) phthalate 0.381 0.0820 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0820 UButyl benzyl phthalate 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UChrysene 0.381 0.0659 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0659 UDibenz(a,h)anthracene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UDibenzofuran 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UDiethyl phthalate 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UDimethyl phthalate 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UDi-n-butyl phthalate 0.381 0.139 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.139 UDi-n-octyl phthalate 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UFluoranthene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UFluorene 0.381 0.116 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.116 UHexachlorobenzene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UHexachlorobutadiene 0.381 0.0763 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0763 UHexachlorocyclopentadiene 0.381 0.0809 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0809 UHexachloroethane 0.381 0.0763 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0763 UIndeno[1,2,3-cd]pyrene 0.381 0.0774 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0774 UIsophorone 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UNaphthalene 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UNitrobenzene 0.381 0.121 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.121 UN-Nitrosodi-n-propylamine 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UN-Nitrosodiphenylamine 0.763 0.185 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.185 UPentachlorophenol 0.381 0.0381 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0381 UPhenanthrene 0.381 0.103 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.103 UPhenol 0.381 0.0901 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.0901 UPyrene 0.381 0.173 mg/Kg 10/16/23 12:06 10/17/23 17:15 1☼<0.173 UPyridine 2,4,6-Tribromophenol (Surr)68 10-150 10/16/23 12:06 10/17/23 17:15 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 70 10/16/23 12:06 10/17/23 17:15 127-127 2-Fluorophenol (Surr)52 10/16/23 12:06 10/17/23 17:15 125-128 Nitrobenzene-d5 (Surr)59 10/16/23 12:06 10/17/23 17:15 115-136 Phenol-d5 (Surr)55 10/16/23 12:06 10/17/23 17:15 129-130 Terphenyl-d14 (Surr)85 10/16/23 12:06 10/17/23 17:15 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <2.22 U 2.22 2.22 mg/Kg ☼10/16/23 16:00 10/16/23 21:34 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.15 1.15 mg/Kg 10/16/23 16:00 10/16/23 21:34 50☼<1.15 UC9-C12 Aliphatics Eurofins Pensacola Page 14 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244947-3Client Sample ID: MW-2 15' Matrix: SolidDate Collected: 10/10/23 14:31 Percent Solids: 86.2Date Received: 10/12/23 09:41 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL 2.59 0.616 0.616 mg/Kg ☼10/16/23 16:00 10/16/23 21:34 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)99 70-130 10/16/23 16:00 10/16/23 21:34 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)96 10/16/23 16:00 10/16/23 21:34 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <1.82 U 1.82 1.82 mg/Kg ☼10/17/23 08:04 10/18/23 20:50 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.82 1.82 mg/Kg 10/17/23 08:04 10/18/23 20:50 1☼<1.82 UC19-C36 Aliphatics 3.41 3.41 mg/Kg 10/17/23 08:04 10/18/23 21:14 1☼<3.41 UC11-C22 Aromatics 1-Chlorooctadecane 80 40-140 10/17/23 08:04 10/18/23 20:50 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 84 10/17/23 08:04 10/18/23 21:14 140-140 2-Fluorobiphenyl 99 10/17/23 08:04 10/18/23 21:14 140-140 2-Bromonaphthalene 99 10/17/23 08:04 10/18/23 21:14 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 20.4 1.12 0.348 mg/Kg ☼10/13/23 13:18 10/19/23 13:18 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.12 0.247 mg/Kg 10/13/23 13:18 10/19/23 13:18 1☼8.88Lead General Chemistry RL MDL 86.2 0.01 0.01 %10/19/23 17:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %10/19/23 17:19 113.8Percent Moisture (EPA Moisture) Eurofins Pensacola Page 15 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Qualifiers GC/MS VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC/MS Semi VOA Qualifier Description *-LCS and/or LCSD is outside acceptance limits, low biased. Qualifier F1 MS and/or MSD recovery exceeds control limits. F2 MS/MSD RPD exceeds control limits J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. U Indicates the analyte was analyzed for but not detected. GC VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC Semi VOA Qualifier Description F1 MS and/or MSD recovery exceeds control limits. Qualifier U Indicates the analyte was analyzed for but not detected. Metals Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points Eurofins Pensacola Page 16 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Glossary (Continued) These commonly used abbreviations may or may not be present in this report. TEF Toxicity Equivalent Factor (Dioxin) Abbreviation TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Pensacola Page 17 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (67-130)(77-127)(76-127) BFB DBFM TOL 96 114 96400-244947-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 5' 98 112 97400-244947-3 MW-2 15' 96 104 99LCS 400-646074/4-A Lab Control Sample 98 115 98MB 400-646074/25-A Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) Method: 8270E - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (10-150)(27-127)(25-128)(15-136)(29-130)(24-146) TBP FBP 2FP NBZ PHL TPHL 68 62 40 48 41 70400-244947-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 5' 77 67 52 5374 80400-244947-1 MS MW-2 5' 82 73 54 5780 81400-244947-1 MSD MW-2 5' 68 70 52 5559 85400-244947-3 MW-2 15' 80 61 52 5076 67LCS 400-645696/2-A Lab Control Sample 60 63 44 4653 64MB 400-645696/1-A Method Blank Surrogate Legend TBP = 2,4,6-Tribromophenol (Surr) FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol (Surr) NBZ = Nitrobenzene-d5 (Surr) PHL = Phenol-d5 (Surr) TPHL = Terphenyl-d14 (Surr) Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (70-130)(70-130) TFT-F1 TFT-P1 94 91400-244947-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 5' 97 94400-244947-2 MW-2 10' 99 96400-244947-3 MW-2 15' 101 106LCS 400-645692/2-A Lab Control Sample 98 100LCSD 400-645692/3-A Lab Control Sample Dup 97 94MB 400-645692/1-A Method Blank Surrogate Legend TFT-F = a,a,a-Trifluorotoluene (fid) TFT-P = a,a,a-Trifluorotoluene (pid) Eurofins Pensacola Page 18 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140) 1COD1 60400-244947-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 5' 59400-244947-1 MS MW-2 5' 67400-244947-1 MSD MW-2 5' 82400-244947-2 MW-2 10' 80400-244947-3 MW-2 15' 67LCS 400-645810/2-A Lab Control Sample 61LCSD 400-645810/18-A Lab Control Sample Dup 65MB 400-645810/1-A Method Blank Surrogate Legend 1COD = 1-Chlorooctadecane Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 63 94 94400-244947-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 5' 68 97 97400-244947-1 MS MW-2 5' 71 94 94400-244947-1 MSD MW-2 5' 85 99 99400-244947-2 MW-2 10' 84 99 99400-244947-3 MW-2 15' 74 101 98LCS 400-645810/2-A Lab Control Sample 70 99 99LCSD 400-645810/18-A Lab Control Sample Dup 74 96 92MB 400-645810/1-A Method Blank Surrogate Legend OTPH = o-Terphenyl FBP = 2-Fluorobiphenyl 2BN = 2-Bromonaphthalene Eurofins Pensacola Page 19 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop GC/MS VOA Prep Batch: 646074 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-244947-1 MW-2 5'Total/NA Solid 5035400-244947-3 MW-2 15'Total/NA Solid 5035MB 400-646074/25-A Method Blank Total/NA Solid 5035LCS 400-646074/4-A Lab Control Sample Total/NA Analysis Batch: 646100 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260D 646074400-244947-1 MW-2 5'Total/NA Solid 8260D 646074400-244947-3 MW-2 15'Total/NA Solid 8260D 646074MB 400-646074/25-A Method Blank Total/NA Solid 8260D 646074LCS 400-646074/4-A Lab Control Sample Total/NA GC/MS Semi VOA Prep Batch: 645696 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-244947-1 MW-2 5'Total/NA Solid 3546400-244947-3 MW-2 15'Total/NA Solid 3546MB 400-645696/1-A Method Blank Total/NA Solid 3546LCS 400-645696/2-A Lab Control Sample Total/NA Solid 3546400-244947-1 MS MW-2 5'Total/NA Solid 3546400-244947-1 MSD MW-2 5'Total/NA Analysis Batch: 645850 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 645696400-244947-1 MW-2 5'Total/NA Solid 8270E 645696400-244947-3 MW-2 15'Total/NA Solid 8270E 645696MB 400-645696/1-A Method Blank Total/NA Solid 8270E 645696LCS 400-645696/2-A Lab Control Sample Total/NA Solid 8270E 645696400-244947-1 MS MW-2 5'Total/NA Solid 8270E 645696400-244947-1 MSD MW-2 5'Total/NA GC VOA Analysis Batch: 645426 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MAVPH 645692400-244947-1 MW-2 5'Total/NA Solid MAVPH 645692400-244947-2 MW-2 10'Total/NA Solid MAVPH 645692400-244947-3 MW-2 15'Total/NA Solid MAVPH 645692MB 400-645692/1-A Method Blank Total/NA Solid MAVPH 645692LCS 400-645692/2-A Lab Control Sample Total/NA Solid MAVPH 645692LCSD 400-645692/3-A Lab Control Sample Dup Total/NA Prep Batch: 645692 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-244947-1 MW-2 5'Total/NA Solid 5035400-244947-2 MW-2 10'Total/NA Solid 5035400-244947-3 MW-2 15'Total/NA Solid 5035MB 400-645692/1-A Method Blank Total/NA Solid 5035LCS 400-645692/2-A Lab Control Sample Total/NA Solid 5035LCSD 400-645692/3-A Lab Control Sample Dup Total/NA Eurofins Pensacola Page 20 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop GC Semi VOA Prep Batch: 645810 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-244947-1 MW-2 5'Total/NA Solid 3546400-244947-2 MW-2 10'Total/NA Solid 3546400-244947-3 MW-2 15'Total/NA Solid 3546MB 400-645810/1-A Method Blank Total/NA Solid 3546LCS 400-645810/2-A Lab Control Sample Total/NA Solid 3546LCSD 400-645810/18-A Lab Control Sample Dup Total/NA Solid 3546400-244947-1 MS MW-2 5'Total/NA Solid 3546400-244947-1 MSD MW-2 5'Total/NA Analysis Batch: 646121 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 645810400-244947-1 MW-2 5'Total/NA Solid MA-EPH 645810400-244947-2 MW-2 10'Total/NA Solid MA-EPH 645810400-244947-3 MW-2 15'Total/NA Solid MA-EPH 645810MB 400-645810/1-A Method Blank Total/NA Solid MA-EPH 645810LCS 400-645810/2-A Lab Control Sample Total/NA Solid MA-EPH 645810LCSD 400-645810/18-A Lab Control Sample Dup Total/NA Solid MA-EPH 645810400-244947-1 MS MW-2 5'Total/NA Solid MA-EPH 645810400-244947-1 MSD MW-2 5'Total/NA Analysis Batch: 646124 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 645810400-244947-1 MW-2 5'Total/NA Solid MA-EPH 645810400-244947-2 MW-2 10'Total/NA Solid MA-EPH 645810400-244947-3 MW-2 15'Total/NA Solid MA-EPH 645810MB 400-645810/1-A Method Blank Total/NA Solid MA-EPH 645810LCS 400-645810/2-A Lab Control Sample Total/NA Solid MA-EPH 645810LCSD 400-645810/18-A Lab Control Sample Dup Total/NA Solid MA-EPH 645810400-244947-1 MS MW-2 5'Total/NA Solid MA-EPH 645810400-244947-1 MSD MW-2 5'Total/NA Metals Prep Batch: 645490 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3050B400-244947-1 MW-2 5'Total/NA Solid 3050B400-244947-3 MW-2 15'Total/NA Solid 3050BMB 400-645490/1-A Method Blank Total/NA Solid 3050BLCS 400-645490/2-A Lab Control Sample Total/NA Analysis Batch: 646339 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 645490400-244947-1 MW-2 5'Total/NA Solid 6010D 645490400-244947-3 MW-2 15'Total/NA Solid 6010D 645490MB 400-645490/1-A Method Blank Total/NA Solid 6010D 645490LCS 400-645490/2-A Lab Control Sample Total/NA General Chemistry Analysis Batch: 646393 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture400-244947-1 MW-2 5'Total/NA Eurofins Pensacola Page 21 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop General Chemistry (Continued) Analysis Batch: 646393 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture400-244947-2 MW-2 10'Total/NA Solid Moisture400-244947-3 MW-2 15'Total/NA Eurofins Pensacola Page 22 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS Client Sample ID: Method BlankLab Sample ID: MB 400-646074/25-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646100 Prep Batch: 646074 RL MDL 1,1,1,2-Tetrachloroethane <0.00110 U 0.00500 0.00110 mg/Kg 10/18/23 10:10 10/18/23 11:15 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.00110 U 0.001100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,1,1-Trichloroethane <0.000820 U 0.0008200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,1,2,2-Tetrachloroethane <0.000780 U 0.0007800.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,1,2-Trichloroethane <0.000830 U 0.0008300.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,1-Dichloroethane <0.000850 U 0.0008500.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,1-Dichloroethene <0.000830 U 0.0008300.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,1-Dichloropropene <0.00110 U 0.001100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2,3-Trichlorobenzene <0.000800 U 0.0008000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2,3-Trichloropropane <0.000920 U 0.0009200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2,4-Trichlorobenzene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2,4-Trimethylbenzene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2-Dibromoethane <0.000710 U 0.0007100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2-Dichlorobenzene <0.000820 U 0.0008200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2-Dichloroethane <0.000760 U 0.0007600.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,2-Dichloropropane <0.000830 U 0.0008300.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,3,5-Trimethylbenzene <0.000950 U 0.0009500.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,3-Dichlorobenzene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,3-Dichloropropane <0.000860 U 0.0008600.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 11,4-Dichlorobenzene <0.00110 U 0.001100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 12,2-Dichloropropane <0.00600 U 0.006000.0250 mg/Kg 10/18/23 10:10 10/18/23 11:15 12-Butanone (MEK) <0.000810 U 0.0008100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 12-Chlorotoluene <0.00500 U 0.005000.0250 mg/Kg 10/18/23 10:10 10/18/23 11:15 12-Hexanone <0.000980 U 0.0009800.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 14-Chlorotoluene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 14-Isopropyltoluene <0.00500 U 0.005000.0250 mg/Kg 10/18/23 10:10 10/18/23 11:15 14-Methyl-2-pentanone (MIBK) <0.0120 U 0.01200.0250 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Acetone <0.000670 U 0.0006700.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Benzene <0.00130 U 0.001300.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Bromobenzene <0.000810 U 0.0008100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Bromochloromethane <0.000920 U 0.0009200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Bromodichloromethane <0.00130 U 0.001300.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Bromoform <0.00250 U 0.002500.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Bromomethane <0.00170 U 0.001700.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Carbon tetrachloride <0.000520 U 0.0005200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Chlorobenzene <0.00120 U 0.001200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Chloroethane <0.00500 U 0.005000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Chloroform <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Chloromethane <0.000760 U 0.0007600.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1cis-1,2-Dichloroethene <0.00120 U 0.001200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1cis-1,3-Dichloropropene <0.00120 U 0.001200.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Dibromochloromethane <0.00130 U 0.001300.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Dichlorodifluoromethane <0.0740 U 0.07400.100 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Ethanol <0.000610 U 0.0006100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Ethylbenzene <0.000550 U 0.0005500.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Isopropyl ether <0.000680 U 0.0006800.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Isopropylbenzene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Methyl tert-butyl ether <0.0100 U 0.01000.0150 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Methylene Chloride Eurofins Pensacola Page 23 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-646074/25-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646100 Prep Batch: 646074 RL MDL Naphthalene <0.00300 U 0.00500 0.00300 mg/Kg 10/18/23 10:10 10/18/23 11:15 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.000960 U 0.0009600.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1n-Butylbenzene <0.000900 U 0.0009000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1N-Propylbenzene <0.000950 U 0.0009500.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1sec-Butylbenzene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Styrene <0.00110 U 0.001100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1tert-Butylbenzene <0.00300 U 0.003000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Tetrachloroethene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Toluene <0.000960 U 0.0009600.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1trans-1,2-Dichloroethene <0.00110 U 0.001100.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1trans-1,3-Dichloropropene <0.00100 U 0.001000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Trichloroethene <0.000860 U 0.0008600.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Trichlorofluoromethane <0.00190 U 0.001900.0250 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Vinyl acetate <0.000800 U 0.0008000.00500 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Vinyl chloride <0.00190 U 0.001900.0100 mg/Kg 10/18/23 10:10 10/18/23 11:15 1Xylenes, Total 4-Bromofluorobenzene 98 67-130 10/18/23 11:15 1 MB MB Surrogate 10/18/23 10:10 Dil FacPreparedAnalyzedQualifierLimits%Recovery 115 10/18/23 10:10 10/18/23 11:15 1Dibromofluoromethane77-127 98 10/18/23 10:10 10/18/23 11:15 1Toluene-d8 (Surr)76-127 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646074/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646100 Prep Batch: 646074 1,1,1,2-Tetrachloroethane 0.0500 0.05116 mg/Kg 102 65 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 0.0500 0.04599 mg/Kg 92 63 -130 1,1,2,2-Tetrachloroethane 0.0500 0.05331 mg/Kg 107 60 -131 1,1,2-Trichloroethane 0.0500 0.05330 mg/Kg 107 65 -130 1,1-Dichloroethane 0.0500 0.04561 mg/Kg 91 59 -130 1,1-Dichloroethene 0.0500 0.04428 mg/Kg 89 55 -137 1,1-Dichloropropene 0.0500 0.04646 mg/Kg 93 65 -130 1,2,3-Trichlorobenzene 0.0500 0.04818 mg/Kg 96 58 -135 1,2,3-Trichloropropane 0.0500 0.05154 mg/Kg 103 60 -130 1,2,4-Trichlorobenzene 0.0500 0.04739 mg/Kg 95 56 -138 1,2,4-Trimethylbenzene 0.0500 0.05159 mg/Kg 103 66 -130 1,2-Dibromoethane 0.0500 0.05328 mg/Kg 107 67 -130 1,2-Dichlorobenzene 0.0500 0.05414 mg/Kg 108 64 -130 1,2-Dichloroethane 0.0500 0.05157 mg/Kg 103 62 -130 1,2-Dichloropropane 0.0500 0.04719 mg/Kg 94 64 -130 1,3,5-Trimethylbenzene 0.0500 0.05089 mg/Kg 102 67 -130 1,3-Dichlorobenzene 0.0500 0.05355 mg/Kg 107 66 -130 1,3-Dichloropropane 0.0500 0.05381 mg/Kg 108 67 -130 1,4-Dichlorobenzene 0.0500 0.05374 mg/Kg 107 65 -130 2,2-Dichloropropane 0.0500 0.04207 mg/Kg 84 51 -132 2-Butanone (MEK)0.200 0.2045 mg/Kg 102 55 -130 2-Chlorotoluene 0.0500 0.05377 mg/Kg 108 67 -130 Eurofins Pensacola Page 24 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646074/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646100 Prep Batch: 646074 2-Hexanone 0.200 0.2092 mg/Kg 105 57 -131 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 4-Chlorotoluene 0.0500 0.05269 mg/Kg 105 66 -130 4-Isopropyltoluene 0.0500 0.05432 mg/Kg 109 68 -130 4-Methyl-2-pentanone (MIBK)0.200 0.1903 mg/Kg 95 58 -130 Acetone 0.200 0.2134 mg/Kg 107 48 -160 Benzene 0.0500 0.04719 mg/Kg 94 65 -130 Bromobenzene 0.0500 0.05079 mg/Kg 102 65 -130 Bromochloromethane 0.0500 0.05100 mg/Kg 102 65 -130 Bromodichloromethane 0.0500 0.04973 mg/Kg 99 61 -130 Bromoform 0.0500 0.04990 mg/Kg 100 52 -136 Bromomethane 0.0500 0.04530 mg/Kg 91 12 -160 Carbon tetrachloride 0.0500 0.04882 mg/Kg 98 60 -130 Chlorobenzene 0.0500 0.04976 mg/Kg 100 70 -130 Chloroethane 0.0500 0.05341 mg/Kg 107 55 -134 Chloroform 0.0500 0.04886 mg/Kg 98 62 -130 Chloromethane 0.0500 0.04139 mg/Kg 83 49 -136 cis-1,2-Dichloroethene 0.0500 0.04571 mg/Kg 91 53 -135 cis-1,3-Dichloropropene 0.0500 0.04889 mg/Kg 98 61 -130 Dibromochloromethane 0.0500 0.05292 mg/Kg 106 58 -132 Dichlorodifluoromethane 0.0500 0.04315 mg/Kg 86 34 -143 Ethanol 2.00 1.179 mg/Kg 59 29 -160 Ethylbenzene 0.0500 0.05038 mg/Kg 101 70 -130 Isopropyl ether 0.0500 0.05385 mg/Kg 108 62 -130 Isopropylbenzene 0.0500 0.05201 mg/Kg 104 70 -130 Methyl tert-butyl ether 0.0500 0.04779 mg/Kg 96 63 -130 Methylene Chloride 0.0500 0.04609 mg/Kg 92 57 -132 m-Xylene & p-Xylene 0.0500 0.05105 mg/Kg 102 70 -130 Naphthalene 0.0500 0.05005 mg/Kg 100 45 -144 n-Butylbenzene 0.0500 0.05871 mg/Kg 117 66 -130 N-Propylbenzene 0.0500 0.05298 mg/Kg 106 67 -130 o-Xylene 0.0500 0.05143 mg/Kg 103 70 -130 sec-Butylbenzene 0.0500 0.05350 mg/Kg 107 67 -130 Styrene 0.0500 0.05032 mg/Kg 101 68 -130 tert-Butylbenzene 0.0500 0.05176 mg/Kg 104 67 -130 Tetrachloroethene 0.0500 0.03876 mg/Kg 78 67 -130 Toluene 0.0500 0.04760 mg/Kg 95 70 -130 trans-1,2-Dichloroethene 0.0500 0.04586 mg/Kg 92 58 -134 trans-1,3-Dichloropropene 0.0500 0.05193 mg/Kg 104 60 -130 Trichloroethene 0.0500 0.04599 mg/Kg 92 65 -130 Trichlorofluoromethane 0.0500 0.05096 mg/Kg 102 61 -136 Vinyl acetate 0.100 0.1419 mg/Kg 142 24 -160 Vinyl chloride 0.0500 0.04752 mg/Kg 95 52 -132 Xylenes, Total 0.100 0.1025 mg/Kg 102 70 -130 4-Bromofluorobenzene 67 -130 Surrogate 96 LCS LCS Qualifier Limits%Recovery 104Dibromofluoromethane 77 -127 99Toluene-d8 (Surr)76 -127 Eurofins Pensacola Page 25 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 400-645696/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 RL MDL 1,2,4-Trichlorobenzene <0.0330 U 0.330 0.0330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11,2-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11,3-Dichlorobenzene <0.130 U 0.1300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11,4-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11-Methylnaphthalene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4,5-Trichlorophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4,6-Trichlorophenol <0.0700 U 0.07000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4-Dichlorophenol <0.0940 U 0.09400.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4-Dimethylphenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,6-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Chloronaphthalene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Chlorophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Methylnaphthalene <0.0800 U 0.08000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Methylphenol <0.0700 U 0.07000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Nitroaniline <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Nitrophenol <0.0770 U 0.07700.660 mg/Kg 10/16/23 12:06 10/17/23 15:05 13 & 4 Methylphenol <0.0780 U 0.07800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 13-Nitroaniline <0.240 U 0.2400.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14,6-Dinitro-2-methylphenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Bromophenyl phenyl ether <0.0810 U 0.08100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Chloro-3-methylphenol <0.0810 U 0.08100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Chloroaniline <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Chlorophenyl phenyl ether <0.113 U 0.1130.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Nitroaniline <0.300 U 0.3000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Nitrophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Acenaphthene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Acenaphthylene <0.0980 U 0.09800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Aniline <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Anthracene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[a]anthracene <0.0470 U 0.04700.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[a]pyrene <0.0990 U 0.09900.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[b]fluoranthene <0.110 U 0.1100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[g,h,i]perylene <0.0780 U 0.07800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[k]fluoranthene <0.350 U 0.3500.990 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzoic acid <0.126 U 0.1260.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1bis (2-chloroisopropyl) ether <0.0730 U 0.07300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Bis(2-chloroethoxy)methane <0.0460 U 0.04600.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Bis(2-chloroethyl)ether <0.0810 U 0.08100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Bis(2-ethylhexyl) phthalate <0.0710 U 0.07100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Butyl benzyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Chrysene <0.0570 U 0.05700.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Dibenz(a,h)anthracene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Dibenzofuran <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Diethyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Dimethyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Di-n-butyl phthalate <0.120 U 0.1200.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Di-n-octyl phthalate Eurofins Pensacola Page 26 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-645696/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 RL MDL Fluoranthene <0.0330 U 0.330 0.0330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Fluorene <0.100 U 0.1000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachlorobutadiene <0.0660 U 0.06600.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachlorocyclopentadiene <0.0700 U 0.07000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachloroethane <0.0660 U 0.06600.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Indeno[1,2,3-cd]pyrene <0.0670 U 0.06700.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Isophorone <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Naphthalene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Nitrobenzene <0.105 U 0.1050.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1N-Nitrosodi-n-propylamine <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1N-Nitrosodiphenylamine <0.160 U 0.1600.660 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Pentachlorophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Phenanthrene <0.0890 U 0.08900.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Phenol <0.0780 U 0.07800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Pyrene <0.150 U 0.1500.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Pyridine 2,4,6-Tribromophenol (Surr)60 10-150 10/17/23 15:05 1 MB MB Surrogate 10/16/23 12:06 Dil FacPreparedAnalyzedQualifierLimits%Recovery 63 10/16/23 12:06 10/17/23 15:05 12-Fluorobiphenyl 27-127 44 10/16/23 12:06 10/17/23 15:05 12-Fluorophenol (Surr)25-128 53 10/16/23 12:06 10/17/23 15:05 1Nitrobenzene-d5 (Surr)15-136 46 10/16/23 12:06 10/17/23 15:05 1Phenol-d5 (Surr)29-130 64 10/16/23 12:06 10/17/23 15:05 1Terphenyl-d14 (Surr)24-146 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645696/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 1,2,4-Trichlorobenzene 2.00 1.284 mg/Kg 64 41 -100 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,2-Dichlorobenzene 2.00 1.127 mg/Kg 56 49 -120 1,3-Dichlorobenzene 2.00 1.131 mg/Kg 57 45 -120 1,4-Dichlorobenzene 2.00 1.089 mg/Kg 54 48 -120 1-Methylnaphthalene 2.00 1.254 mg/Kg 63 40 -120 2,4,5-Trichlorophenol 2.00 1.329 mg/Kg 66 50 -118 2,4,6-Trichlorophenol 2.00 1.324 mg/Kg 66 49 -115 2,4-Dichlorophenol 2.00 1.313 mg/Kg 66 53 -120 2,4-Dimethylphenol 2.00 1.430 mg/Kg 72 45 -108 2,4-Dinitrotoluene 2.00 1.385 mg/Kg 69 53 -133 2,6-Dinitrotoluene 2.00 1.306 mg/Kg 65 51 -114 2-Chloronaphthalene 2.00 1.195 mg/Kg 60 48 -102 2-Chlorophenol 2.00 1.108 mg/Kg 55 50 -102 2-Methylnaphthalene 2.00 1.178 mg/Kg 59 40 -120 2-Methylphenol 2.00 1.139 mg/Kg 57 49 -111 2-Nitroaniline 2.00 1.336 mg/Kg 67 46 -108 2-Nitrophenol 2.00 1.280 mg/Kg 64 53 -120 Eurofins Pensacola Page 27 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645696/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 3 & 4 Methylphenol 2.00 1.125 mg/Kg 56 47 -123 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 3-Nitroaniline 2.00 1.103 mg/Kg 55 28 -119 4,6-Dinitro-2-methylphenol 4.00 2.006 mg/Kg 50 35 -135 4-Bromophenyl phenyl ether 2.00 1.283 mg/Kg 64 51 -120 4-Chloro-3-methylphenol 2.00 1.089 *-mg/Kg 54 57 -124 4-Chloroaniline 2.00 0.9874 mg/Kg 49 26 -102 4-Chlorophenyl phenyl ether 2.00 1.300 mg/Kg 65 53 -113 4-Nitroaniline 2.00 1.173 mg/Kg 59 32 -131 4-Nitrophenol 4.00 4.124 mg/Kg 103 35 -139 Acenaphthene 2.00 1.285 mg/Kg 64 50 -120 Acenaphthylene 2.00 1.273 mg/Kg 64 47 -110 Aniline 2.00 1.887 mg/Kg 94 15 -104 Anthracene 2.00 1.289 mg/Kg 64 52 -120 Benzo[a]anthracene 2.00 1.323 mg/Kg 66 55 -120 Benzo[a]pyrene 2.00 1.337 mg/Kg 67 54 -120 Benzo[b]fluoranthene 2.00 1.288 mg/Kg 64 47 -120 Benzo[g,h,i]perylene 2.00 1.329 mg/Kg 66 45 -120 Benzo[k]fluoranthene 2.00 1.282 mg/Kg 64 52 -120 Benzoic acid 8.69 2.655 mg/Kg 31 10 -139 bis (2-chloroisopropyl) ether 2.00 0.8106 mg/Kg 41 18 -105 Bis(2-chloroethoxy)methane 2.00 0.9612 mg/Kg 48 33 -100 Bis(2-chloroethyl)ether 2.00 1.399 mg/Kg 70 28 -120 Bis(2-ethylhexyl) phthalate 2.00 1.287 mg/Kg 64 40 -150 Butyl benzyl phthalate 2.00 1.304 mg/Kg 65 50 -126 Chrysene 2.00 1.313 mg/Kg 66 54 -120 Dibenz(a,h)anthracene 2.00 1.307 mg/Kg 65 47 -120 Dibenzofuran 2.00 1.301 mg/Kg 65 54 -105 Diethyl phthalate 2.00 1.460 mg/Kg 73 40 -128 Dimethyl phthalate 2.00 1.296 mg/Kg 65 58 -120 Di-n-butyl phthalate 2.00 1.369 mg/Kg 68 40 -122 Di-n-octyl phthalate 2.00 1.456 mg/Kg 73 40 -137 Fluoranthene 2.00 1.358 mg/Kg 68 49 -120 Fluorene 2.00 1.340 mg/Kg 67 47 -120 Hexachlorobenzene 2.00 1.249 mg/Kg 62 49 -127 Hexachlorobutadiene 2.00 1.269 mg/Kg 63 43 -120 Hexachlorocyclopentadiene 2.00 0.8947 mg/Kg 45 10 -140 Hexachloroethane 2.00 1.058 mg/Kg 53 45 -120 Indeno[1,2,3-cd]pyrene 2.00 1.304 mg/Kg 65 47 -120 Isophorone 2.00 1.102 mg/Kg 55 36 -120 Naphthalene 2.00 1.181 mg/Kg 59 41 -120 Nitrobenzene 2.00 1.179 mg/Kg 59 40 -120 N-Nitrosodi-n-propylamine 2.00 1.082 mg/Kg 54 39 -120 N-Nitrosodiphenylamine 1.98 1.195 mg/Kg 60 54 -120 Pentachlorophenol 4.00 2.187 mg/Kg 55 32 -131 Phenanthrene 2.00 1.276 mg/Kg 64 50 -120 Phenol 2.00 1.012 mg/Kg 51 40 -120 Pyrene 2.00 1.297 mg/Kg 65 54 -120 Pyridine 4.00 1.325 mg/Kg 33 29 -120 Eurofins Pensacola Page 28 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645696/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 80 LCS LCS Qualifier Limits%Recovery 612-Fluorobiphenyl 27 -127 522-Fluorophenol (Surr)25 -128 76Nitrobenzene-d5 (Surr)15 -136 50Phenol-d5 (Surr)29 -130 67Terphenyl-d14 (Surr)24 -146 Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 1,2,4-Trichlorobenzene <0.0831 U 2.55 1.520 mg/Kg 60 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits 1,2-Dichlorobenzene <0.0831 U 2.55 1.429 mg/Kg 56 40 -140☼ 1,3-Dichlorobenzene <0.0831 U 2.55 1.381 mg/Kg 54 40 -140☼ 1,4-Dichlorobenzene <0.327 U 2.55 1.398 mg/Kg 55 40 -140☼ 1-Methylnaphthalene <0.0831 U 2.55 1.581 mg/Kg 62 40 -140☼ 2,4,5-Trichlorophenol <0.0831 U 2.55 1.851 mg/Kg 73 40 -140☼ 2,4,6-Trichlorophenol <0.0831 U 2.55 1.811 mg/Kg 71 40 -140☼ 2,4-Dichlorophenol <0.176 U 2.55 1.657 mg/Kg 65 40 -140☼ 2,4-Dimethylphenol <0.237 U 2.55 1.691 mg/Kg 66 40 -140☼ 2,4-Dinitrotoluene <0.0831 U 2.55 1.856 mg/Kg 73 40 -140☼ 2,6-Dinitrotoluene <0.0831 U 2.55 1.855 mg/Kg 73 40 -140☼ 2-Chloronaphthalene <0.0831 U 2.55 1.612 mg/Kg 63 40 -140☼ 2-Chlorophenol <0.0831 U 2.55 1.489 mg/Kg 58 40 -140☼ 2-Methylnaphthalene <0.0831 U 2.55 1.496 mg/Kg 59 40 -140☼ 2-Methylphenol <0.202 U 2.55 1.461 mg/Kg 57 40 -140☼ 2-Nitroaniline <0.176 U 2.55 1.995 mg/Kg 78 40 -140☼ 2-Nitrophenol <0.0831 U 2.55 1.569 mg/Kg 62 40 -140☼ 3 & 4 Methylphenol <0.194 U 2.55 1.421 J mg/Kg 56 40 -140☼ 3-Nitroaniline <0.196 U 2.55 1.514 mg/Kg 59 40 -140☼ 4,6-Dinitro-2-methylphenol <0.605 U 5.09 2.929 mg/Kg 58 40 -140☼ 4-Bromophenyl phenyl ether <0.0831 U 2.55 1.854 mg/Kg 73 40 -140☼ 4-Chloro-3-methylphenol <0.204 U *-2.55 1.669 mg/Kg 66 40 -140☼ 4-Chloroaniline <0.204 U 2.55 1.223 mg/Kg 48 40 -140☼ 4-Chlorophenyl phenyl ether <0.0831 U 2.55 1.825 mg/Kg 72 40 -140☼ 4-Nitroaniline <0.285 U 2.55 1.514 mg/Kg 59 40 -140☼ 4-Nitrophenol <0.756 U 5.09 5.734 mg/Kg 113 40 -140☼ Acenaphthene <0.0831 U 2.55 1.750 mg/Kg 69 40 -140☼ Acenaphthylene <0.0831 U 2.55 1.664 mg/Kg 65 40 -140☼ Aniline <0.247 U 2.55 1.273 mg/Kg 50 40 -140☼ Anthracene <0.0831 U 2.55 1.836 mg/Kg 72 40 -140☼ Benzo[a]anthracene <0.0831 U 2.55 1.811 mg/Kg 71 40 -140☼ Benzo[a]pyrene <0.118 U 2.55 1.829 mg/Kg 72 40 -140☼ Benzo[b]fluoranthene <0.249 U 2.55 1.808 mg/Kg 71 40 -140☼ Benzo[g,h,i]perylene <0.277 U 2.55 1.512 mg/Kg 59 40 -140☼ Benzo[k]fluoranthene <0.196 U 2.55 1.989 mg/Kg 78 40 -140☼ Benzoic acid <0.882 U F1 F2 11.1 2.750 F1 mg/Kg 25 40 -140☼ Eurofins Pensacola Page 29 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 bis (2-chloroisopropyl) ether <0.317 U 2.55 1.081 mg/Kg 42 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits Bis(2-chloroethoxy)methane <0.184 U 2.55 1.219 mg/Kg 48 40 -140☼ Bis(2-chloroethyl)ether <0.116 U F1 2.55 1.006 F1 mg/Kg 39 40 -140☼ Bis(2-ethylhexyl) phthalate <0.204 U 2.55 1.796 mg/Kg 71 40 -140☼ Butyl benzyl phthalate <0.179 U 2.55 1.760 mg/Kg 69 40 -140☼ Chrysene <0.0831 U 2.55 1.887 mg/Kg 74 40 -140☼ Dibenz(a,h)anthracene <0.144 U 2.55 1.678 mg/Kg 66 40 -140☼ Dibenzofuran <0.0831 U 2.55 1.722 mg/Kg 68 40 -140☼ Diethyl phthalate <0.0831 U 2.55 1.954 mg/Kg 77 40 -140☼ Dimethyl phthalate <0.0831 U 2.55 1.775 mg/Kg 70 40 -140☼ Di-n-butyl phthalate <0.0831 U 2.55 1.931 mg/Kg 76 40 -140☼ Di-n-octyl phthalate <0.302 U 2.55 1.874 mg/Kg 74 40 -140☼ Fluoranthene <0.0831 U 2.55 1.835 mg/Kg 72 40 -140☼ Fluorene <0.0831 U 2.55 1.814 mg/Kg 71 40 -140☼ Hexachlorobenzene <0.252 U 2.55 1.884 mg/Kg 74 40 -140☼ Hexachlorobutadiene <0.0831 U 2.55 1.646 mg/Kg 65 40 -140☼ Hexachlorocyclopentadiene <0.166 U F1 2.55 0.9309 F1 mg/Kg 37 40 -140☼ Hexachloroethane <0.176 U 2.55 1.381 mg/Kg 54 40 -140☼ Indeno[1,2,3-cd]pyrene <0.166 U 2.55 1.629 mg/Kg 64 40 -140☼ Isophorone <0.169 U 2.55 1.397 mg/Kg 55 40 -140☼ Naphthalene <0.0831 U 2.55 1.490 mg/Kg 59 40 -140☼ Nitrobenzene <0.0831 U 2.55 1.498 mg/Kg 59 40 -140☼ N-Nitrosodi-n-propylamine <0.264 U 2.55 1.437 mg/Kg 56 40 -140☼ N-Nitrosodiphenylamine <0.0831 U 2.53 1.703 mg/Kg 67 40 -140☼ Pentachlorophenol <0.403 U 5.09 2.775 mg/Kg 54 40 -140☼ Phenanthrene <0.0831 U 2.55 1.839 mg/Kg 72 40 -140☼ Phenol <0.224 U 2.55 1.340 mg/Kg 53 40 -140☼ Pyrene <0.196 U 2.55 1.989 mg/Kg 78 40 -140☼ Pyridine <0.378 U F1 5.09 1.516 F1 mg/Kg 30 40 -140☼ 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 77 MS MS Qualifier Limits%Recovery 672-Fluorobiphenyl 27 -127 522-Fluorophenol (Surr)25 -128 74Nitrobenzene-d5 (Surr)15 -136 53Phenol-d5 (Surr)29 -130 80Terphenyl-d14 (Surr)24 -146 Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 1,2,4-Trichlorobenzene <0.0831 U 2.52 1.665 mg/Kg 66 40 -140 9 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD 1,2-Dichlorobenzene <0.0831 U 2.52 1.480 mg/Kg 59 40 -140 4 30☼ 1,3-Dichlorobenzene <0.0831 U 2.52 1.509 mg/Kg 60 40 -140 9 30☼ 1,4-Dichlorobenzene <0.327 U 2.52 1.419 mg/Kg 56 40 -140 2 30☼ 1-Methylnaphthalene <0.0831 U 2.52 1.674 mg/Kg 66 40 -140 6 30☼ Eurofins Pensacola Page 30 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 2,4,5-Trichlorophenol <0.0831 U 2.52 1.952 mg/Kg 77 40 -140 5 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD 2,4,6-Trichlorophenol <0.0831 U 2.52 1.923 mg/Kg 76 40 -140 6 30☼ 2,4-Dichlorophenol <0.176 U 2.52 1.767 mg/Kg 70 40 -140 6 30☼ 2,4-Dimethylphenol <0.237 U 2.52 1.887 mg/Kg 75 40 -140 11 30☼ 2,4-Dinitrotoluene <0.0831 U 2.52 1.927 mg/Kg 76 40 -140 4 30☼ 2,6-Dinitrotoluene <0.0831 U 2.52 1.942 mg/Kg 77 40 -140 5 30☼ 2-Chloronaphthalene <0.0831 U 2.52 1.750 mg/Kg 69 40 -140 8 30☼ 2-Chlorophenol <0.0831 U 2.52 1.596 mg/Kg 63 40 -140 7 30☼ 2-Methylnaphthalene <0.0831 U 2.52 1.659 mg/Kg 66 40 -140 10 30☼ 2-Methylphenol <0.202 U 2.52 1.559 mg/Kg 62 40 -140 7 30☼ 2-Nitroaniline <0.176 U 2.52 2.082 mg/Kg 83 40 -140 4 30☼ 2-Nitrophenol <0.0831 U 2.52 1.814 mg/Kg 72 40 -140 14 30☼ 3 & 4 Methylphenol <0.194 U 2.52 1.532 J mg/Kg 61 40 -140 8 30☼ 3-Nitroaniline <0.196 U 2.52 1.786 mg/Kg 71 40 -140 16 30☼ 4,6-Dinitro-2-methylphenol <0.605 U 5.04 2.394 mg/Kg 47 40 -140 20 30☼ 4-Bromophenyl phenyl ether <0.0831 U 2.52 1.915 mg/Kg 76 40 -140 3 30☼ 4-Chloro-3-methylphenol <0.204 U *-2.52 1.803 mg/Kg 71 40 -140 8 30☼ 4-Chloroaniline <0.204 U 2.52 1.386 mg/Kg 55 40 -140 12 30☼ 4-Chlorophenyl phenyl ether <0.0831 U 2.52 1.949 mg/Kg 77 40 -140 7 30☼ 4-Nitroaniline <0.285 U 2.52 1.752 mg/Kg 69 40 -140 15 30☼ 4-Nitrophenol <0.756 U 5.04 5.736 mg/Kg 114 40 -140 0 30☼ Acenaphthene <0.0831 U 2.52 1.865 mg/Kg 74 40 -140 6 30☼ Acenaphthylene <0.0831 U 2.52 1.851 mg/Kg 73 40 -140 11 30☼ Aniline <0.247 U 2.52 1.410 mg/Kg 56 40 -140 10 30☼ Anthracene <0.0831 U 2.52 1.916 mg/Kg 76 40 -140 4 30☼ Benzo[a]anthracene <0.0831 U 2.52 1.918 mg/Kg 76 40 -140 6 30☼ Benzo[a]pyrene <0.118 U 2.52 1.931 mg/Kg 77 40 -140 5 30☼ Benzo[b]fluoranthene <0.249 U 2.52 1.901 mg/Kg 75 40 -140 5 30☼ Benzo[g,h,i]perylene <0.277 U 2.52 1.386 mg/Kg 55 40 -140 9 30☼ Benzo[k]fluoranthene <0.196 U 2.52 1.960 mg/Kg 78 40 -140 1 30☼ Benzoic acid <0.882 U F1 F2 11.0 1.599 J F1 F2 mg/Kg 15 40 -140 53 30☼ bis (2-chloroisopropyl) ether <0.317 U 2.52 1.200 mg/Kg 48 40 -140 10 30☼ Bis(2-chloroethoxy)methane <0.184 U 2.52 1.381 mg/Kg 55 40 -140 12 30☼ Bis(2-chloroethyl)ether <0.116 U F1 2.52 1.068 mg/Kg 42 40 -140 6 30☼ Bis(2-ethylhexyl) phthalate <0.204 U 2.52 2.081 mg/Kg 82 40 -140 15 30☼ Butyl benzyl phthalate <0.179 U 2.52 2.021 mg/Kg 80 40 -140 14 30☼ Chrysene <0.0831 U 2.52 1.900 mg/Kg 75 40 -140 1 30☼ Dibenz(a,h)anthracene <0.144 U 2.52 1.610 mg/Kg 64 40 -140 4 30☼ Dibenzofuran <0.0831 U 2.52 1.818 mg/Kg 72 40 -140 5 30☼ Diethyl phthalate <0.0831 U 2.52 2.141 mg/Kg 85 40 -140 9 30☼ Dimethyl phthalate <0.0831 U 2.52 1.881 mg/Kg 75 40 -140 6 30☼ Di-n-butyl phthalate <0.0831 U 2.52 1.978 mg/Kg 78 40 -140 2 30☼ Di-n-octyl phthalate <0.302 U 2.52 2.062 mg/Kg 82 40 -140 10 30☼ Fluoranthene <0.0831 U 2.52 1.921 mg/Kg 76 40 -140 5 30☼ Fluorene <0.0831 U 2.52 1.860 mg/Kg 74 40 -140 3 30☼ Hexachlorobenzene <0.252 U 2.52 1.864 mg/Kg 74 40 -140 1 30☼ Hexachlorobutadiene <0.0831 U 2.52 1.861 mg/Kg 74 40 -140 12 30☼ Hexachlorocyclopentadiene <0.166 U F1 2.52 0.8801 F1 mg/Kg 35 40 -140 6 30☼ Hexachloroethane <0.176 U 2.52 1.536 mg/Kg 61 40 -140 11 30☼ Eurofins Pensacola Page 31 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 Indeno[1,2,3-cd]pyrene <0.166 U 2.52 1.639 mg/Kg 65 40 -140 1 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD Isophorone <0.169 U 2.52 1.514 mg/Kg 60 40 -140 8 30☼ Naphthalene <0.0831 U 2.52 1.636 mg/Kg 65 40 -140 9 30☼ Nitrobenzene <0.0831 U 2.52 1.615 mg/Kg 64 40 -140 8 30☼ N-Nitrosodi-n-propylamine <0.264 U 2.52 1.578 mg/Kg 63 40 -140 9 30☼ N-Nitrosodiphenylamine <0.0831 U 2.50 1.860 mg/Kg 74 40 -140 9 30☼ Pentachlorophenol <0.403 U 5.04 2.266 mg/Kg 45 40 -140 20 30☼ Phenanthrene <0.0831 U 2.52 1.934 mg/Kg 77 40 -140 5 30☼ Phenol <0.224 U 2.52 1.433 mg/Kg 57 40 -140 7 30☼ Pyrene <0.196 U 2.52 2.094 mg/Kg 83 40 -140 5 30☼ Pyridine <0.378 U F1 5.04 1.543 F1 mg/Kg 31 40 -140 2 30☼ 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 82 MSD MSD Qualifier Limits%Recovery 732-Fluorobiphenyl 27 -127 542-Fluorophenol (Surr)25 -128 80Nitrobenzene-d5 (Surr)15 -136 57Phenol-d5 (Surr)29 -130 81Terphenyl-d14 (Surr)24 -146 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-645692/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645426 Prep Batch: 645692 RL MDL C5-C8 Aliphatics <2.70 U 2.70 2.70 mg/Kg 10/13/23 08:59 10/13/23 10:00 50 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.40 U 1.401.40 mg/Kg 10/13/23 08:59 10/13/23 10:00 50C9-C12 Aliphatics <0.750 U 0.7500.750 mg/Kg 10/13/23 08:59 10/13/23 10:00 50C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)97 70-130 10/13/23 10:00 50 MB MB Surrogate 10/13/23 08:59 Dil FacPreparedAnalyzedQualifierLimits%Recovery 94 10/13/23 08:59 10/13/23 10:00 50a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645692/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645426 Prep Batch: 645692 C5-C8 Aliphatics 15.0 17.90 mg/Kg 119 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 17.5 19.21 mg/Kg 110 70 -130 C9-C10 Aromatics 2.50 2.869 mg/Kg 115 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 101 LCS LCS Qualifier Limits%Recovery 106a,a,a-Trifluorotoluene (pid)70 -130 Eurofins Pensacola Page 32 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645692/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645426 Prep Batch: 645692 C5-C8 Aliphatics 15.0 17.43 mg/Kg 116 70 -130 3 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 17.5 18.97 mg/Kg 108 70 -130 1 25 C9-C10 Aromatics 2.50 2.732 mg/Kg 109 70 -130 5 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 98 LCSD LCSD Qualifier Limits%Recovery 100a,a,a-Trifluorotoluene (pid)70 -130 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-645810/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 RL MDL C9-C18 Aliphatics <1.60 U 1.60 1.60 mg/Kg 10/17/23 08:04 10/18/23 19:29 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.60 U 1.601.60 mg/Kg 10/17/23 08:04 10/18/23 19:29 1C19-C36 Aliphatics 1-Chlorooctadecane 65 40-140 10/18/23 19:29 1 MB MB Surrogate 10/17/23 08:04 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-645810/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 RL MDL C11-C22 Aromatics <3.00 U 3.00 3.00 mg/Kg 10/17/23 08:04 10/18/23 19:40 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl 74 40-140 10/18/23 19:40 1 MB MB Surrogate 10/17/23 08:04 Dil FacPreparedAnalyzedQualifierLimits%Recovery 96 10/17/23 08:04 10/18/23 19:40 12-Fluorobiphenyl 40-140 92 10/17/23 08:04 10/18/23 19:40 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645810/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 C9-C18 Aliphatics 20.0 12.12 mg/Kg 61 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 26.7 19.61 mg/Kg 74 40 -140 1-Chlorooctadecane 40 -140 Surrogate 67 LCS LCS Qualifier Limits%Recovery Eurofins Pensacola Page 33 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645810/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 C11-C22 Aromatics 56.7 40.74 mg/Kg 72 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl 40 -140 Surrogate 74 LCS LCS Qualifier Limits%Recovery 1012-Fluorobiphenyl 40 -140 982-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645810/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 C9-C18 Aliphatics 20.0 11.63 mg/Kg 58 40 -140 4 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 26.7 18.31 mg/Kg 69 40 -140 7 50 1-Chlorooctadecane 40 -140 Surrogate 61 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645810/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 C11-C22 Aromatics 56.7 39.93 mg/Kg 70 40 -140 2 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 70 LCSD LCSD Qualifier Limits%Recovery 992-Fluorobiphenyl 40 -140 992-Bromonaphthalene 40 -140 Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 C9-C18 Aliphatics 15.5 F1 25.5 22.78 F1 mg/Kg 29 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits C19-C36 Aliphatics 3.43 34.0 26.50 mg/Kg 68 40 -140☼ 1-Chlorooctadecane 40 -140 Surrogate 59 MS MS Qualifier Limits%Recovery Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 C11-C22 Aromatics <3.82 U 72.3 48.76 mg/Kg 67 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits Eurofins Pensacola Page 34 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 o-Terphenyl 40 -140 Surrogate 68 MS MS Qualifier Limits%Recovery 972-Fluorobiphenyl 40 -140 972-Bromonaphthalene 40 -140 Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 C9-C18 Aliphatics 15.5 F1 25.3 33.56 mg/Kg 71 40 -140 38 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD C19-C36 Aliphatics 3.43 33.7 26.13 mg/Kg 67 40 -140 1 50☼ 1-Chlorooctadecane 40 -140 Surrogate 67 MSD MSD Qualifier Limits%Recovery Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 C11-C22 Aromatics <3.82 U 71.7 55.39 mg/Kg 77 40 -140 13 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 71 MSD MSD Qualifier Limits%Recovery 942-Fluorobiphenyl 40 -140 942-Bromonaphthalene 40 -140 Method: 6010D - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 400-645490/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646339 Prep Batch: 645490 RL MDL Chromium <0.310 U 1.00 0.310 mg/Kg 10/13/23 13:18 10/19/23 12:38 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.220 U 0.2201.00 mg/Kg 10/13/23 13:18 10/19/23 12:38 1Lead Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645490/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646339 Prep Batch: 645490 Chromium 99.4 97.90 mg/Kg 98 80 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Lead 99.4 93.83 mg/Kg 94 80 -120 Eurofins Pensacola Page 35 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 Matrix: SolidDate Collected: 10/10/23 14:15 Date Received: 10/12/23 09:41 Analysis Moisture TMP10/19/23 17:191 EET PEN646393 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Prep 5035 CH10/18/23 10:10 EET PEN646074 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.719 g 5.00 g Analysis 8260D 1 646100 10/18/23 17:18 CH EET PENTotal/NA 5 mL 5 mL Prep 3546 645696 10/16/23 12:06 LH EET PENTotal/NA 15.25 g 1 mL Analysis 8270E 2 645850 10/17/23 16:49 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 645692 10/16/23 16:00 SRK EET PENTotal/NA 6.903 g 5.00 g Analysis MAVPH 50 645426 10/16/23 20:15 SRK EET PENTotal/NA 5 mL 5 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.08 g 2 mL Analysis MA-EPH 1 646121 10/18/23 20:27 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.08 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:50 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 645490 10/13/23 13:18 KWN EET PENTotal/NA .517 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 13:14 BAW EET PENTotal/NA Client Sample ID: MW-2 10'Lab Sample ID: 400-244947-2 Matrix: SolidDate Collected: 10/10/23 14:23 Date Received: 10/12/23 09:41 Analysis Moisture TMP10/19/23 17:191 EET PEN646393 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: MW-2 10'Lab Sample ID: 400-244947-2 Matrix: SolidDate Collected: 10/10/23 14:23 Percent Solids: 89.3Date Received: 10/12/23 09:41 Prep 5035 SRK10/16/23 16:00 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 8.141 g 5.0 g Analysis MAVPH 50 645426 10/16/23 20:55 SRK EET PENTotal/NA 5 mL 5 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.26 g 2 mL Analysis MA-EPH 1 646121 10/18/23 20:39 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.26 g 2 mL Analysis MA-EPH 1 646124 10/18/23 21:02 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: MW-2 15'Lab Sample ID: 400-244947-3 Matrix: SolidDate Collected: 10/10/23 14:31 Date Received: 10/12/23 09:41 Analysis Moisture TMP10/19/23 17:191 EET PEN646393 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Eurofins Pensacola Page 36 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Client Sample ID: MW-2 15'Lab Sample ID: 400-244947-3 Matrix: SolidDate Collected: 10/10/23 14:31 Percent Solids: 86.2Date Received: 10/12/23 09:41 Prep 5035 CH10/18/23 10:10 EET PEN646074 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 4.693 g 5.00 g Analysis 8260D 1 646100 10/18/23 17:41 CH EET PENTotal/NA 5 mL 5 mL Prep 3546 645696 10/16/23 12:06 LH EET PENTotal/NA 15.06 g 1 mL Analysis 8270E 1 645850 10/17/23 17:15 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 645692 10/16/23 16:00 SRK EET PENTotal/NA 8.78 g 5.00 g Analysis MAVPH 50 645426 10/16/23 21:34 SRK EET PENTotal/NA 5 mL 5 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.30 g 2 mL Analysis MA-EPH 1 646121 10/18/23 20:50 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.30 g 2 mL Analysis MA-EPH 1 646124 10/18/23 21:14 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 645490 10/13/23 13:18 KWN EET PENTotal/NA .516 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 13:18 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645490/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN10/13/23 13:18 EET PEN645490 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA .500 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 12:38 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645692/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SRK10/13/23 08:59 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 mL Analysis MAVPH 50 645426 10/13/23 10:00 SRK EET PENTotal/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-645696/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH10/16/23 12:06 EET PEN645696 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 645850 10/17/23 15:05 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-645810/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646121 10/18/23 19:29 LHB EET PENTotal/NA Eurofins Pensacola Page 37 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Client Sample ID: Method Blank Lab Sample ID: MB 400-645810/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646124 10/18/23 19:40 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-646074/25-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 CH10/18/23 10:10 EET PEN646074 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 646100 10/18/23 11:15 CH EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645490/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN10/13/23 13:18 EET PEN645490 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA .503 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 12:50 BAW EET PENTotal/NA Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645692/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SRK10/13/23 08:59 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 mL Analysis MAVPH 50 645426 10/13/23 10:39 SRK EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645696/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH10/16/23 12:06 EET PEN645696 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 645850 10/17/23 15:30 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645810/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646121 10/18/23 19:40 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:04 MP EET PENTotal/NA 1 mL 1 mL Eurofins Pensacola Page 38 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-646074/4-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 CH10/18/23 10:10 EET PEN646074 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 646100 10/18/23 10:13 CH EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-645692/3-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SRK10/13/23 08:59 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 mL Analysis MAVPH 50 645426 10/16/23 13:49 SRK EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-645810/18-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646121 10/18/23 19:52 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:15 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MS Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Prep 3546 LH10/16/23 12:06 EET PEN645696 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.08 g 1 mL Analysis 8270E 2 645850 10/17/23 15:56 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.06 g 2 mL Analysis MA-EPH 1 646121 10/18/23 20:04 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.06 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:27 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: MW-2 5'Lab Sample ID: 400-244947-1 MSD Matrix: SolidDate Collected: 10/10/23 14:15 Percent Solids: 78.1Date Received: 10/12/23 09:41 Prep 3546 LH10/16/23 12:06 EET PEN645696 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.23 g 1 mL Analysis 8270E 2 645850 10/17/23 16:22 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.18 g 2 mL Analysis MA-EPH 1 646121 10/18/23 20:15 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.18 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:39 MP EET PENTotal/NA 1 mL 1 mL ¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Eurofins Pensacola Page 39 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 40 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 400-244947-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method Method Description LaboratoryProtocol SW8468260DVolatile Organic Compounds by GC/MS EET PEN SW8468270ESemivolatile Organic Compounds (GC/MS)EET PEN MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN SW8466010DMetals (ICP)EET PEN EPAMoisturePercent Moisture EET PEN SW8463050BPreparation, Metals EET PEN SW8463546Microwave Extraction EET PEN SW8465035Closed System Purge and Trap EET PEN Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 41 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Consultech Environmental LLC Job ID: 400-244947-1 Project/Site: Kwik Stop Laboratory: Eurofins Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte Moisture Solid Percent Moisture Moisture Solid Percent Solids Eurofins Pensacola Page 42 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 43 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Consultech Environmental LLC Job Number: 400-244947-1 Login Number: 244947 Question Answer Comment Creator: Earnest, Tamantha List Source: Eurofins Pensacola List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.0.9°C IR8 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Pensacola Page 44 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 ANALYTICAL REPORT PREPARED FOR Attn: Raj Shah Consultech Environmental LLC 2021 Energy Drive Apex, North Carolina 27502 Generated 10/25/2023 11:40:11 AM JOB DESCRIPTION Kwik Stop JOB NUMBER 400-244959-1 See page two for job notes and contact information. Pensacola FL 32514 3355 McLemore Drive Eurofins Pensacola Page 1 of 44 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Pensacola Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 10/25/2023 11:40:11 AM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Consultech Environmental LLC Project/Site: Kwik Stop Laboratory Job ID: 400-244959-1 Page 3 of 44 Eurofins Pensacola10/25/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Job ID: 400-244959-1 Laboratory: Eurofins Pensacola Narrative Job Narrative 400-244959-1 Receipt The samples were received on 10/12/2023 9:41 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 0.0°C GC/MS VOA No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 8270E: The following analyte recovered outside control limits for the LCS associated with preparation batch 400-645696 and analytical batch 400-645850: 4-Chloro-3-methylphenol. This is not indicative of a systematic control problem because this was a random marginal exceedance. Qualified results have been reported. Method 8270E: The method blank for preparation batch 400-646616 and analytical batch 400-646745 contained Di-n-butyl phthalate above the method detection limit. This target analyte concentration was less than the reporting limit (RL) in the method blank; therefore, re-extraction and/or re-analysis of samples was not performed. Method 8270E: Surrogate recovery for the following sample was outside control limits: MW-1 10' (400-244959-1). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAVPH: The following samples were diluted because the base dilution for VPH soil analysis is 1:50: MW-1 10' (400-244959-1), MW-1 15' (400-244959-2) and MW-1 20' (400-244959-3). No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins PensacolaPage 4 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Client Sample ID: MW-1 10'Lab Sample ID: 400-244959-1 ☼2-Butanone (MEK) RL 0.0261 mg/Kg MDL 0.00626 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J0.00688 8260D ☼Acetone 0.0261 mg/Kg0.0125 Total/NA10.0879 8260D ☼Toluene 0.00522 mg/Kg0.00104 Total/NA10.00134 J 8260D ☼C19-C36 Aliphatics 1.68 mg/Kg1.68 Total/NA112.3 MA-EPH ☼Chromium 1.04 mg/Kg0.322 Total/NA143.5 6010D ☼Lead 1.04 mg/Kg0.229 Total/NA18.70 6010D Client Sample ID: MW-1 15'Lab Sample ID: 400-244959-2 ☼C19-C36 Aliphatics RL 1.85 mg/Kg MDL 1.85 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA17.24 MA-EPH Client Sample ID: MW-1 20'Lab Sample ID: 400-244959-3 ☼Acetone RL 0.0247 mg/Kg MDL 0.0119 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0610 8260D ☼Chromium 1.32 mg/Kg0.408 Total/NA115.7 6010D ☼Lead 1.32 mg/Kg0.289 Total/NA16.87 6010D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 5 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Lab Sample ID Client Sample ID Matrix Collected Received 400-244959-1 MW-1 10'Solid 10/10/23 11:36 10/12/23 09:41 400-244959-2 MW-1 15'Solid 10/10/23 11:45 10/12/23 09:41 400-244959-3 MW-1 20'Solid 10/10/23 11:53 10/12/23 09:41 Eurofins PensacolaPage 6 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-1Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 10/10/23 11:36 Percent Solids: 92.2Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL <0.00115 U 0.00522 0.00115 mg/Kg ☼10/19/23 08:35 10/19/23 16:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00522 0.00115 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00115 U1,1,1-Trichloroethane 0.00522 0.000856 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000856 U1,1,2,2-Tetrachloroethane 0.00522 0.000814 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000814 U1,1,2-Trichloroethane 0.00522 0.000866 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000866 U1,1-Dichloroethane 0.00522 0.000887 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000887 U1,1-Dichloroethene 0.00522 0.000866 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000866 U1,1-Dichloropropene 0.00522 0.00115 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00115 U1,2,3-Trichlorobenzene 0.00522 0.000835 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000835 U1,2,3-Trichloropropane 0.00522 0.000960 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000960 U1,2,4-Trichlorobenzene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 U1,2,4-Trimethylbenzene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 U1,2-Dibromoethane 0.00522 0.000741 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000741 U1,2-Dichlorobenzene 0.00522 0.000856 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000856 U1,2-Dichloroethane 0.00522 0.000793 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000793 U1,2-Dichloropropane 0.00522 0.000866 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000866 U1,3,5-Trimethylbenzene 0.00522 0.000991 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000991 U1,3-Dichlorobenzene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 U1,3-Dichloropropane 0.00522 0.000897 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000897 U1,4-Dichlorobenzene 0.00522 0.00115 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00115 U2,2-Dichloropropane 0.0261 0.00626 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼0.00688 J2-Butanone (MEK) 0.00522 0.000845 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000845 U2-Chlorotoluene 0.0261 0.00522 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00522 U2-Hexanone 0.00522 0.00102 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00102 U4-Chlorotoluene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 U4-Isopropyltoluene 0.0261 0.00522 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00522 U4-Methyl-2-pentanone (MIBK) 0.0261 0.0125 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼0.0879Acetone 0.00522 0.000699 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000699 UBenzene 0.00522 0.00136 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00136 UBromobenzene 0.00522 0.000845 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000845 UBromochloromethane 0.00522 0.000960 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000960 UBromodichloromethane 0.00522 0.00136 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00136 UBromoform 0.00522 0.00261 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00261 UBromomethane 0.00522 0.00177 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00177 UCarbon tetrachloride 0.00522 0.000543 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000543 UChlorobenzene 0.00522 0.00125 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00125 UChloroethane 0.00522 0.00522 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00522 UChloroform 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 UChloromethane 0.00522 0.000793 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000793 Ucis-1,2-Dichloroethene 0.00522 0.00125 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00125 Ucis-1,3-Dichloropropene 0.00522 0.00125 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00125 UDibromochloromethane 0.00522 0.00136 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00136 UDichlorodifluoromethane 0.104 0.0772 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.0772 UEthanol 0.00522 0.000637 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000637 UEthylbenzene 0.00522 0.000574 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000574 UIsopropyl ether 0.00522 0.000710 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000710 UIsopropylbenzene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 UMethyl tert-butyl ether 0.0157 0.0104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.0104 UMethylene Chloride 0.00522 0.00313 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00313 UNaphthalene Eurofins Pensacola Page 7 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-1Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 10/10/23 11:36 Percent Solids: 92.2Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL <0.00100 U 0.00522 0.00100 mg/Kg ☼10/19/23 08:35 10/19/23 16:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00522 0.000939 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000939 UN-Propylbenzene 0.00522 0.000991 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000991 Usec-Butylbenzene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 UStyrene 0.00522 0.00115 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00115 Utert-Butylbenzene 0.00522 0.00313 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00313 UTetrachloroethene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼0.00134 JToluene 0.00522 0.00100 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00100 Utrans-1,2-Dichloroethene 0.00522 0.00115 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00115 Utrans-1,3-Dichloropropene 0.00522 0.00104 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00104 UTrichloroethene 0.00522 0.000897 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000897 UTrichlorofluoromethane 0.0261 0.00198 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00198 UVinyl acetate 0.00522 0.000835 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.000835 UVinyl chloride 0.0104 0.00198 mg/Kg 10/19/23 08:35 10/19/23 16:15 1☼<0.00198 UXylenes, Total 4-Bromofluorobenzene 99 67-130 10/19/23 08:35 10/19/23 16:15 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 114 10/19/23 08:35 10/19/23 16:15 177-127 Toluene-d8 (Surr)98 10/19/23 08:35 10/19/23 16:15 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL <0.0357 U 0.357 0.0357 mg/Kg ☼10/21/23 23:58 10/23/23 22:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U1,2-Dichlorobenzene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U1,3-Dichlorobenzene 0.357 0.141 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.141 U1,4-Dichlorobenzene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U1-Methylnaphthalene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2,4,5-Trichlorophenol 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2,4,6-Trichlorophenol 0.357 0.0758 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0758 U2,4-Dichlorophenol 0.357 0.102 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.102 U2,4-Dimethylphenol 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2,4-Dinitrotoluene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2,6-Dinitrotoluene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2-Chloronaphthalene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2-Chlorophenol 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2-Methylnaphthalene 0.357 0.0866 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0866 U2-Methylphenol 0.357 0.0758 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0758 U2-Nitroaniline 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U2-Nitrophenol 0.714 0.0833 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0833 U3 & 4 Methylphenol 0.357 0.0844 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0844 U3-Nitroaniline 0.357 0.260 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.260 U4,6-Dinitro-2-methylphenol 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U4-Bromophenyl phenyl ether 0.357 0.0877 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0877 U4-Chloro-3-methylphenol 0.357 0.0877 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0877 U4-Chloroaniline 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 U4-Chlorophenyl phenyl ether 0.357 0.122 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.122 U4-Nitroaniline 0.357 0.325 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.325 U4-Nitrophenol 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UAcenaphthene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UAcenaphthylene Eurofins Pensacola Page 8 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-1Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 10/10/23 11:36 Percent Solids: 92.2Date Received: 10/12/23 09:41 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <0.106 U 0.357 0.106 mg/Kg ☼10/21/23 23:58 10/23/23 22:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Aniline 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UAnthracene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UBenzo[a]anthracene 0.357 0.0509 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0509 UBenzo[a]pyrene 0.357 0.107 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.107 UBenzo[b]fluoranthene 0.357 0.119 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.119 UBenzo[g,h,i]perylene 0.357 0.0844 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0844 UBenzo[k]fluoranthene 1.07 0.379 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.379 UBenzoic acid 0.357 0.136 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.136 Ubis (2-chloroisopropyl) ether 0.357 0.0790 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0790 UBis(2-chloroethoxy)methane 0.357 0.0498 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0498 UBis(2-chloroethyl)ether 0.357 0.0877 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0877 UBis(2-ethylhexyl) phthalate 0.357 0.0768 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0768 UButyl benzyl phthalate 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UChrysene 0.357 0.0617 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0617 UDibenz(a,h)anthracene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UDibenzofuran 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UDiethyl phthalate 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UDimethyl phthalate 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UDi-n-butyl phthalate 0.357 0.130 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.130 UDi-n-octyl phthalate 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UFluoranthene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UFluorene 0.357 0.108 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.108 UHexachlorobenzene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UHexachlorobutadiene 0.357 0.0714 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0714 UHexachlorocyclopentadiene 0.357 0.0758 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0758 UHexachloroethane 0.357 0.0714 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0714 UIndeno[1,2,3-cd]pyrene 0.357 0.0725 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0725 UIsophorone 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UNaphthalene 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UNitrobenzene 0.357 0.114 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.114 UN-Nitrosodi-n-propylamine 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UN-Nitrosodiphenylamine 0.714 0.173 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.173 UPentachlorophenol 0.357 0.0357 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0357 UPhenanthrene 0.357 0.0963 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0963 UPhenol 0.357 0.0844 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.0844 UPyrene 0.357 0.162 mg/Kg 10/21/23 23:58 10/23/23 22:02 1☼<0.162 UPyridine 2,4,6-Tribromophenol (Surr)0.8 S1-10-150 10/21/23 23:58 10/23/23 22:02 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 65 10/21/23 23:58 10/23/23 22:02 127-127 2-Fluorophenol (Surr)0 S1-10/21/23 23:58 10/23/23 22:02 125-128 Nitrobenzene-d5 (Surr)47 10/21/23 23:58 10/23/23 22:02 115-136 Phenol-d5 (Surr)34 10/21/23 23:58 10/23/23 22:02 129-130 Terphenyl-d14 (Surr)70 10/21/23 23:58 10/23/23 22:02 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <3.29 U 3.29 3.29 mg/Kg ☼10/16/23 16:00 10/16/23 22:14 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.70 1.70 mg/Kg 10/16/23 16:00 10/16/23 22:14 50☼<1.70 UC9-C12 Aliphatics Eurofins Pensacola Page 9 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-1Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 10/10/23 11:36 Percent Solids: 92.2Date Received: 10/12/23 09:41 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL <0.913 U 0.913 0.913 mg/Kg ☼10/16/23 16:00 10/16/23 22:14 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)97 70-130 10/16/23 16:00 10/16/23 22:14 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)94 10/16/23 16:00 10/16/23 22:14 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <1.68 U 1.68 1.68 mg/Kg ☼10/17/23 08:04 10/18/23 21:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.68 1.68 mg/Kg 10/17/23 08:04 10/18/23 21:02 1☼12.3C19-C36 Aliphatics 3.16 3.16 mg/Kg 10/17/23 08:04 10/18/23 21:25 1☼<3.16 UC11-C22 Aromatics 1-Chlorooctadecane 69 40-140 10/17/23 08:04 10/18/23 21:02 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 67 10/17/23 08:04 10/18/23 21:25 140-140 2-Fluorobiphenyl 92 10/17/23 08:04 10/18/23 21:25 140-140 2-Bromonaphthalene 91 10/17/23 08:04 10/18/23 21:25 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 43.5 1.04 0.322 mg/Kg ☼10/13/23 13:18 10/19/23 13:22 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.04 0.229 mg/Kg 10/13/23 13:18 10/19/23 13:22 1☼8.70Lead General Chemistry RL MDL 92.2 0.01 0.01 %10/19/23 17:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %10/19/23 17:19 17.8Percent Moisture (EPA Moisture) Eurofins Pensacola Page 10 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-2Client Sample ID: MW-1 15' Matrix: SolidDate Collected: 10/10/23 11:45 Percent Solids: 85.6Date Received: 10/12/23 09:41 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <2.84 U 2.84 2.84 mg/Kg ☼10/16/23 16:00 10/16/23 22:53 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.47 1.47 mg/Kg 10/16/23 16:00 10/16/23 22:53 50☼<1.47 UC9-C12 Aliphatics 0.789 0.789 mg/Kg 10/16/23 16:00 10/16/23 22:53 50☼<0.789 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)96 70-130 10/16/23 16:00 10/16/23 22:53 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)94 10/16/23 16:00 10/16/23 22:53 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <1.85 U 1.85 1.85 mg/Kg ☼10/17/23 08:04 10/18/23 21:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.85 1.85 mg/Kg 10/17/23 08:04 10/18/23 21:14 1☼7.24C19-C36 Aliphatics 3.47 3.47 mg/Kg 10/17/23 08:04 10/18/23 21:37 1☼<3.47 UC11-C22 Aromatics 1-Chlorooctadecane 74 40-140 10/17/23 08:04 10/18/23 21:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 84 10/17/23 08:04 10/18/23 21:37 140-140 2-Fluorobiphenyl 96 10/17/23 08:04 10/18/23 21:37 140-140 2-Bromonaphthalene 96 10/17/23 08:04 10/18/23 21:37 140-140 General Chemistry RL MDL 85.6 0.01 0.01 %10/19/23 17:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %10/19/23 17:19 114.4Percent Moisture (EPA Moisture) Eurofins Pensacola Page 11 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-3Client Sample ID: MW-1 20' Matrix: SolidDate Collected: 10/10/23 11:53 Percent Solids: 73.4Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL <0.00109 U 0.00495 0.00109 mg/Kg ☼10/19/23 08:35 10/19/23 16:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00495 0.00109 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00109 U1,1,1-Trichloroethane 0.00495 0.000812 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000812 U1,1,2,2-Tetrachloroethane 0.00495 0.000772 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000772 U1,1,2-Trichloroethane 0.00495 0.000822 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000822 U1,1-Dichloroethane 0.00495 0.000841 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000841 U1,1-Dichloroethene 0.00495 0.000822 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000822 U1,1-Dichloropropene 0.00495 0.00109 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00109 U1,2,3-Trichlorobenzene 0.00495 0.000792 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000792 U1,2,3-Trichloropropane 0.00495 0.000911 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000911 U1,2,4-Trichlorobenzene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 U1,2,4-Trimethylbenzene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 U1,2-Dibromoethane 0.00495 0.000703 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000703 U1,2-Dichlorobenzene 0.00495 0.000812 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000812 U1,2-Dichloroethane 0.00495 0.000752 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000752 U1,2-Dichloropropane 0.00495 0.000822 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000822 U1,3,5-Trimethylbenzene 0.00495 0.000940 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000940 U1,3-Dichlorobenzene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 U1,3-Dichloropropane 0.00495 0.000851 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000851 U1,4-Dichlorobenzene 0.00495 0.00109 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00109 U2,2-Dichloropropane 0.0247 0.00594 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00594 U2-Butanone (MEK) 0.00495 0.000802 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000802 U2-Chlorotoluene 0.0247 0.00495 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00495 U2-Hexanone 0.00495 0.000970 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000970 U4-Chlorotoluene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 U4-Isopropyltoluene 0.0247 0.00495 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00495 U4-Methyl-2-pentanone (MIBK) 0.0247 0.0119 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼0.0610Acetone 0.00495 0.000663 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000663 UBenzene 0.00495 0.00129 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00129 UBromobenzene 0.00495 0.000802 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000802 UBromochloromethane 0.00495 0.000911 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000911 UBromodichloromethane 0.00495 0.00129 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00129 UBromoform 0.00495 0.00247 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00247 UBromomethane 0.00495 0.00168 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00168 UCarbon tetrachloride 0.00495 0.000515 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000515 UChlorobenzene 0.00495 0.00119 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00119 UChloroethane 0.00495 0.00495 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00495 UChloroform 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 UChloromethane 0.00495 0.000752 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000752 Ucis-1,2-Dichloroethene 0.00495 0.00119 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00119 Ucis-1,3-Dichloropropene 0.00495 0.00119 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00119 UDibromochloromethane 0.00495 0.00129 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00129 UDichlorodifluoromethane 0.0990 0.0732 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.0732 UEthanol 0.00495 0.000604 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000604 UEthylbenzene 0.00495 0.000544 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000544 UIsopropyl ether 0.00495 0.000673 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000673 UIsopropylbenzene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 UMethyl tert-butyl ether 0.0148 0.00990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00990 UMethylene Chloride 0.00495 0.00297 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00297 UNaphthalene Eurofins Pensacola Page 12 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-3Client Sample ID: MW-1 20' Matrix: SolidDate Collected: 10/10/23 11:53 Percent Solids: 73.4Date Received: 10/12/23 09:41 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL <0.000950 U 0.00495 0.000950 mg/Kg ☼10/19/23 08:35 10/19/23 16:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00495 0.000891 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000891 UN-Propylbenzene 0.00495 0.000940 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000940 Usec-Butylbenzene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 UStyrene 0.00495 0.00109 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00109 Utert-Butylbenzene 0.00495 0.00297 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00297 UTetrachloroethene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 UToluene 0.00495 0.000950 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000950 Utrans-1,2-Dichloroethene 0.00495 0.00109 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00109 Utrans-1,3-Dichloropropene 0.00495 0.000990 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000990 UTrichloroethene 0.00495 0.000851 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000851 UTrichlorofluoromethane 0.0247 0.00188 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00188 UVinyl acetate 0.00495 0.000792 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.000792 UVinyl chloride 0.00990 0.00188 mg/Kg 10/19/23 08:35 10/19/23 16:37 1☼<0.00188 UXylenes, Total 4-Bromofluorobenzene 97 67-130 10/19/23 08:35 10/19/23 16:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 113 10/19/23 08:35 10/19/23 16:37 177-127 Toluene-d8 (Surr)97 10/19/23 08:35 10/19/23 16:37 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL <0.0448 U 0.448 0.0448 mg/Kg ☼10/16/23 12:06 10/17/23 17:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U1,2-Dichlorobenzene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U1,3-Dichlorobenzene 0.448 0.176 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.176 U1,4-Dichlorobenzene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U1-Methylnaphthalene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2,4,5-Trichlorophenol 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2,4,6-Trichlorophenol 0.448 0.0949 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0949 U2,4-Dichlorophenol 0.448 0.127 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.127 U2,4-Dimethylphenol 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2,4-Dinitrotoluene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2,6-Dinitrotoluene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2-Chloronaphthalene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2-Chlorophenol 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2-Methylnaphthalene 0.448 0.108 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.108 U2-Methylphenol 0.448 0.0949 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0949 U2-Nitroaniline 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U2-Nitrophenol 0.895 0.104 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.104 U3 & 4 Methylphenol 0.448 0.106 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.106 U3-Nitroaniline 0.448 0.325 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.325 U4,6-Dinitro-2-methylphenol 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U4-Bromophenyl phenyl ether 0.448 0.110 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.110 U *-4-Chloro-3-methylphenol 0.448 0.110 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.110 U4-Chloroaniline 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 U4-Chlorophenyl phenyl ether 0.448 0.153 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.153 U4-Nitroaniline 0.448 0.407 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.407 U4-Nitrophenol 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UAcenaphthene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UAcenaphthylene Eurofins Pensacola Page 13 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-3Client Sample ID: MW-1 20' Matrix: SolidDate Collected: 10/10/23 11:53 Percent Solids: 73.4Date Received: 10/12/23 09:41 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <0.133 U 0.448 0.133 mg/Kg ☼10/16/23 12:06 10/17/23 17:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Aniline 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UAnthracene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UBenzo[a]anthracene 0.448 0.0637 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0637 UBenzo[a]pyrene 0.448 0.134 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.134 UBenzo[b]fluoranthene 0.448 0.149 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.149 UBenzo[g,h,i]perylene 0.448 0.106 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.106 UBenzo[k]fluoranthene 1.34 0.475 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.475 UBenzoic acid 0.448 0.171 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.171 Ubis (2-chloroisopropyl) ether 0.448 0.0990 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0990 UBis(2-chloroethoxy)methane 0.448 0.0624 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0624 UBis(2-chloroethyl)ether 0.448 0.110 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.110 UBis(2-ethylhexyl) phthalate 0.448 0.0963 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0963 UButyl benzyl phthalate 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UChrysene 0.448 0.0773 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0773 UDibenz(a,h)anthracene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UDibenzofuran 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UDiethyl phthalate 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UDimethyl phthalate 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UDi-n-butyl phthalate 0.448 0.163 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.163 UDi-n-octyl phthalate 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UFluoranthene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UFluorene 0.448 0.136 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.136 UHexachlorobenzene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UHexachlorobutadiene 0.448 0.0895 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0895 UHexachlorocyclopentadiene 0.448 0.0949 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0949 UHexachloroethane 0.448 0.0895 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0895 UIndeno[1,2,3-cd]pyrene 0.448 0.0909 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0909 UIsophorone 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UNaphthalene 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UNitrobenzene 0.448 0.142 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.142 UN-Nitrosodi-n-propylamine 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UN-Nitrosodiphenylamine 0.895 0.217 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.217 UPentachlorophenol 0.448 0.0448 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.0448 UPhenanthrene 0.448 0.121 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.121 UPhenol 0.448 0.106 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.106 UPyrene 0.448 0.203 mg/Kg 10/16/23 12:06 10/17/23 17:41 1☼<0.203 UPyridine 2,4,6-Tribromophenol (Surr)62 10-150 10/16/23 12:06 10/17/23 17:41 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 66 10/16/23 12:06 10/17/23 17:41 127-127 2-Fluorophenol (Surr)52 10/16/23 12:06 10/17/23 17:41 125-128 Nitrobenzene-d5 (Surr)54 10/16/23 12:06 10/17/23 17:41 115-136 Phenol-d5 (Surr)47 10/16/23 12:06 10/17/23 17:41 129-130 Terphenyl-d14 (Surr)71 10/16/23 12:06 10/17/23 17:41 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <3.95 U 3.95 3.95 mg/Kg ☼10/16/23 16:00 10/16/23 23:33 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 2.05 2.05 mg/Kg 10/16/23 16:00 10/16/23 23:33 50☼<2.05 UC9-C12 Aliphatics Eurofins Pensacola Page 14 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Lab Sample ID: 400-244959-3Client Sample ID: MW-1 20' Matrix: SolidDate Collected: 10/10/23 11:53 Percent Solids: 73.4Date Received: 10/12/23 09:41 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL <1.10 U 1.10 1.10 mg/Kg ☼10/16/23 16:00 10/16/23 23:33 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)96 70-130 10/16/23 16:00 10/16/23 23:33 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)94 10/16/23 16:00 10/16/23 23:33 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <2.15 U 2.15 2.15 mg/Kg ☼10/17/23 08:04 10/18/23 21:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 2.15 2.15 mg/Kg 10/17/23 08:04 10/18/23 21:37 1☼<2.15 UC19-C36 Aliphatics 4.04 4.04 mg/Kg 10/17/23 08:04 10/18/23 22:00 1☼<4.04 UC11-C22 Aromatics 1-Chlorooctadecane 81 40-140 10/17/23 08:04 10/18/23 21:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 89 10/17/23 08:04 10/18/23 22:00 140-140 2-Fluorobiphenyl 100 10/17/23 08:04 10/18/23 22:00 140-140 2-Bromonaphthalene 101 10/17/23 08:04 10/18/23 22:00 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 15.7 1.32 0.408 mg/Kg ☼10/16/23 12:39 10/17/23 17:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.32 0.289 mg/Kg 10/16/23 12:39 10/17/23 17:41 1☼6.87Lead General Chemistry RL MDL 73.4 0.01 0.01 %10/19/23 17:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %10/19/23 17:19 126.6Percent Moisture (EPA Moisture) Eurofins Pensacola Page 15 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Qualifiers GC/MS VOA Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier U Indicates the analyte was analyzed for but not detected. GC/MS Semi VOA Qualifier Description *-LCS and/or LCSD is outside acceptance limits, low biased. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. S1-Surrogate recovery exceeds control limits, low biased. U Indicates the analyte was analyzed for but not detected. GC VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC Semi VOA Qualifier Description *-LCS and/or LCSD is outside acceptance limits, low biased. Qualifier U Indicates the analyte was analyzed for but not detected. Metals Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points Eurofins Pensacola Page 16 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Glossary (Continued) These commonly used abbreviations may or may not be present in this report. TEF Toxicity Equivalent Factor (Dioxin) Abbreviation TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Pensacola Page 17 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (67-130)(77-127)(76-127) BFB DBFM TOL 99 114 98400-244959-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 10' 97 113 97400-244959-3 MW-1 20' 97 105 100LCS 400-646314/10-A Lab Control Sample 96 116 97MB 400-646314/9-A Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) Method: 8270E - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (10-150)(27-127)(25-128)(15-136)(29-130)(24-146) TBP FBP 2FP NBZ PHL TPHL 0.8 S1-65 0 S1-47 34 70400-244959-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 10' 62 66 52 4754 71400-244959-3 MW-1 20' 80 61 52 5076 67LCS 400-645696/2-A Lab Control Sample 93 71 45 4575 77LCS 400-646616/2-A Lab Control Sample 60 63 44 4653 64MB 400-645696/1-A Method Blank 82 71 41 4355 78MB 400-646616/1-A Method Blank Surrogate Legend TBP = 2,4,6-Tribromophenol (Surr) FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol (Surr) NBZ = Nitrobenzene-d5 (Surr) PHL = Phenol-d5 (Surr) TPHL = Terphenyl-d14 (Surr) Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (70-130)(70-130) TFT-F1 TFT-P1 97 94400-244959-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 10' 96 94400-244959-2 MW-1 15' 96 94400-244959-3 MW-1 20' 101 106LCS 400-645692/2-A Lab Control Sample 98 100LCSD 400-645692/3-A Lab Control Sample Dup 97 94MB 400-645692/1-A Method Blank Surrogate Legend TFT-F = a,a,a-Trifluorotoluene (fid) TFT-P = a,a,a-Trifluorotoluene (pid) Eurofins Pensacola Page 18 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140) 1COD1 69400-244959-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 10' 74400-244959-2 MW-1 15' 81400-244959-3 MW-1 20' 67LCS 400-645810/2-A Lab Control Sample 61LCSD 400-645810/18-A Lab Control Sample Dup 65MB 400-645810/1-A Method Blank Surrogate Legend 1COD = 1-Chlorooctadecane Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 67 92 91400-244959-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 10' 84 96 96400-244959-2 MW-1 15' 89 100 101400-244959-3 MW-1 20' 74 101 98LCS 400-645810/2-A Lab Control Sample 70 99 99LCSD 400-645810/18-A Lab Control Sample Dup 74 96 92MB 400-645810/1-A Method Blank Surrogate Legend OTPH = o-Terphenyl FBP = 2-Fluorobiphenyl 2BN = 2-Bromonaphthalene Eurofins Pensacola Page 19 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop GC/MS VOA Analysis Batch: 646236 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260D 646314400-244959-1 MW-1 10'Total/NA Solid 8260D 646314400-244959-3 MW-1 20'Total/NA Solid 8260D 646314MB 400-646314/9-A Method Blank Total/NA Solid 8260D 646314LCS 400-646314/10-A Lab Control Sample Total/NA Prep Batch: 646314 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-244959-1 MW-1 10'Total/NA Solid 5035400-244959-3 MW-1 20'Total/NA Solid 5035MB 400-646314/9-A Method Blank Total/NA Solid 5035LCS 400-646314/10-A Lab Control Sample Total/NA GC/MS Semi VOA Prep Batch: 645696 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-244959-3 MW-1 20'Total/NA Solid 3546MB 400-645696/1-A Method Blank Total/NA Solid 3546LCS 400-645696/2-A Lab Control Sample Total/NA Analysis Batch: 645850 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 645696400-244959-3 MW-1 20'Total/NA Solid 8270E 645696MB 400-645696/1-A Method Blank Total/NA Solid 8270E 645696LCS 400-645696/2-A Lab Control Sample Total/NA Prep Batch: 646616 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-244959-1 MW-1 10'Total/NA Solid 3546MB 400-646616/1-A Method Blank Total/NA Solid 3546LCS 400-646616/2-A Lab Control Sample Total/NA Analysis Batch: 646745 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 646616400-244959-1 MW-1 10'Total/NA Solid 8270E 646616MB 400-646616/1-A Method Blank Total/NA Solid 8270E 646616LCS 400-646616/2-A Lab Control Sample Total/NA GC VOA Analysis Batch: 645426 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MAVPH 645692400-244959-1 MW-1 10'Total/NA Solid MAVPH 645692400-244959-2 MW-1 15'Total/NA Solid MAVPH 645692400-244959-3 MW-1 20'Total/NA Solid MAVPH 645692MB 400-645692/1-A Method Blank Total/NA Solid MAVPH 645692LCS 400-645692/2-A Lab Control Sample Total/NA Solid MAVPH 645692LCSD 400-645692/3-A Lab Control Sample Dup Total/NA Prep Batch: 645692 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-244959-1 MW-1 10'Total/NA Eurofins Pensacola Page 20 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop GC VOA (Continued) Prep Batch: 645692 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-244959-2 MW-1 15'Total/NA Solid 5035400-244959-3 MW-1 20'Total/NA Solid 5035MB 400-645692/1-A Method Blank Total/NA Solid 5035LCS 400-645692/2-A Lab Control Sample Total/NA Solid 5035LCSD 400-645692/3-A Lab Control Sample Dup Total/NA GC Semi VOA Prep Batch: 645810 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-244959-1 MW-1 10'Total/NA Solid 3546400-244959-2 MW-1 15'Total/NA Solid 3546400-244959-3 MW-1 20'Total/NA Solid 3546MB 400-645810/1-A Method Blank Total/NA Solid 3546LCS 400-645810/2-A Lab Control Sample Total/NA Solid 3546LCSD 400-645810/18-A Lab Control Sample Dup Total/NA Analysis Batch: 646121 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 645810400-244959-1 MW-1 10'Total/NA Solid MA-EPH 645810400-244959-2 MW-1 15'Total/NA Solid MA-EPH 645810400-244959-3 MW-1 20'Total/NA Solid MA-EPH 645810MB 400-645810/1-A Method Blank Total/NA Solid MA-EPH 645810LCS 400-645810/2-A Lab Control Sample Total/NA Solid MA-EPH 645810LCSD 400-645810/18-A Lab Control Sample Dup Total/NA Analysis Batch: 646124 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 645810400-244959-1 MW-1 10'Total/NA Solid MA-EPH 645810400-244959-2 MW-1 15'Total/NA Solid MA-EPH 645810400-244959-3 MW-1 20'Total/NA Solid MA-EPH 645810MB 400-645810/1-A Method Blank Total/NA Solid MA-EPH 645810LCS 400-645810/2-A Lab Control Sample Total/NA Solid MA-EPH 645810LCSD 400-645810/18-A Lab Control Sample Dup Total/NA Metals Prep Batch: 645490 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3050B400-244959-1 MW-1 10'Total/NA Solid 3050BMB 400-645490/1-A Method Blank Total/NA Solid 3050BLCS 400-645490/2-A Lab Control Sample Total/NA Prep Batch: 645677 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3050B400-244959-3 MW-1 20'Total/NA Solid 3050BMB 400-645677/1-A Method Blank Total/NA Solid 3050BLCS 400-645677/2-A Lab Control Sample Total/NA Analysis Batch: 646016 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 645677400-244959-3 MW-1 20'Total/NA Eurofins Pensacola Page 21 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Metals (Continued) Analysis Batch: 646016 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 645677MB 400-645677/1-A Method Blank Total/NA Solid 6010D 645677LCS 400-645677/2-A Lab Control Sample Total/NA Analysis Batch: 646339 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 645490400-244959-1 MW-1 10'Total/NA Solid 6010D 645490MB 400-645490/1-A Method Blank Total/NA Solid 6010D 645490LCS 400-645490/2-A Lab Control Sample Total/NA General Chemistry Analysis Batch: 646393 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture400-244959-1 MW-1 10'Total/NA Solid Moisture400-244959-2 MW-1 15'Total/NA Solid Moisture400-244959-3 MW-1 20'Total/NA Eurofins Pensacola Page 22 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS Client Sample ID: Method BlankLab Sample ID: MB 400-646314/9-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646236 Prep Batch: 646314 RL MDL 1,1,1,2-Tetrachloroethane <0.00110 U 0.00500 0.00110 mg/Kg 10/19/23 08:35 10/19/23 09:48 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.00110 U 0.001100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,1,1-Trichloroethane <0.000820 U 0.0008200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,1,2,2-Tetrachloroethane <0.000780 U 0.0007800.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,1,2-Trichloroethane <0.000830 U 0.0008300.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,1-Dichloroethane <0.000850 U 0.0008500.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,1-Dichloroethene <0.000830 U 0.0008300.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,1-Dichloropropene <0.00110 U 0.001100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2,3-Trichlorobenzene <0.000800 U 0.0008000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2,3-Trichloropropane <0.000920 U 0.0009200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2,4-Trichlorobenzene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2,4-Trimethylbenzene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2-Dibromoethane <0.000710 U 0.0007100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2-Dichlorobenzene <0.000820 U 0.0008200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2-Dichloroethane <0.000760 U 0.0007600.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,2-Dichloropropane <0.000830 U 0.0008300.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,3,5-Trimethylbenzene <0.000950 U 0.0009500.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,3-Dichlorobenzene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,3-Dichloropropane <0.000860 U 0.0008600.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 11,4-Dichlorobenzene <0.00110 U 0.001100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 12,2-Dichloropropane <0.00600 U 0.006000.0250 mg/Kg 10/19/23 08:35 10/19/23 09:48 12-Butanone (MEK) <0.000810 U 0.0008100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 12-Chlorotoluene <0.00500 U 0.005000.0250 mg/Kg 10/19/23 08:35 10/19/23 09:48 12-Hexanone <0.000980 U 0.0009800.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 14-Chlorotoluene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 14-Isopropyltoluene <0.00500 U 0.005000.0250 mg/Kg 10/19/23 08:35 10/19/23 09:48 14-Methyl-2-pentanone (MIBK) <0.0120 U 0.01200.0250 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Acetone <0.000670 U 0.0006700.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Benzene <0.00130 U 0.001300.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Bromobenzene <0.000810 U 0.0008100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Bromochloromethane <0.000920 U 0.0009200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Bromodichloromethane <0.00130 U 0.001300.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Bromoform <0.00250 U 0.002500.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Bromomethane <0.00170 U 0.001700.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Carbon tetrachloride <0.000520 U 0.0005200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Chlorobenzene <0.00120 U 0.001200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Chloroethane <0.00500 U 0.005000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Chloroform <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Chloromethane <0.000760 U 0.0007600.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1cis-1,2-Dichloroethene <0.00120 U 0.001200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1cis-1,3-Dichloropropene <0.00120 U 0.001200.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Dibromochloromethane <0.00130 U 0.001300.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Dichlorodifluoromethane <0.0740 U 0.07400.100 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Ethanol <0.000610 U 0.0006100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Ethylbenzene <0.000550 U 0.0005500.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Isopropyl ether <0.000680 U 0.0006800.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Isopropylbenzene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Methyl tert-butyl ether <0.0100 U 0.01000.0150 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Methylene Chloride Eurofins Pensacola Page 23 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-646314/9-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646236 Prep Batch: 646314 RL MDL Naphthalene <0.00300 U 0.00500 0.00300 mg/Kg 10/19/23 08:35 10/19/23 09:48 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.000960 U 0.0009600.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1n-Butylbenzene <0.000900 U 0.0009000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1N-Propylbenzene <0.000950 U 0.0009500.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1sec-Butylbenzene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Styrene <0.00110 U 0.001100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1tert-Butylbenzene <0.00300 U 0.003000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Tetrachloroethene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Toluene <0.000960 U 0.0009600.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1trans-1,2-Dichloroethene <0.00110 U 0.001100.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1trans-1,3-Dichloropropene <0.00100 U 0.001000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Trichloroethene <0.000860 U 0.0008600.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Trichlorofluoromethane <0.00190 U 0.001900.0250 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Vinyl acetate <0.000800 U 0.0008000.00500 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Vinyl chloride <0.00190 U 0.001900.0100 mg/Kg 10/19/23 08:35 10/19/23 09:48 1Xylenes, Total 4-Bromofluorobenzene 96 67-130 10/19/23 09:48 1 MB MB Surrogate 10/19/23 08:35 Dil FacPreparedAnalyzedQualifierLimits%Recovery 116 10/19/23 08:35 10/19/23 09:48 1Dibromofluoromethane77-127 97 10/19/23 08:35 10/19/23 09:48 1Toluene-d8 (Surr)76-127 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646314/10-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646236 Prep Batch: 646314 1,1,1,2-Tetrachloroethane 0.0500 0.05417 mg/Kg 108 65 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 0.0500 0.04858 mg/Kg 97 63 -130 1,1,2,2-Tetrachloroethane 0.0500 0.05507 mg/Kg 110 60 -131 1,1,2-Trichloroethane 0.0500 0.05632 mg/Kg 113 65 -130 1,1-Dichloroethane 0.0500 0.04808 mg/Kg 96 59 -130 1,1-Dichloroethene 0.0500 0.04712 mg/Kg 94 55 -137 1,1-Dichloropropene 0.0500 0.04898 mg/Kg 98 65 -130 1,2,3-Trichlorobenzene 0.0500 0.05157 mg/Kg 103 58 -135 1,2,3-Trichloropropane 0.0500 0.05307 mg/Kg 106 60 -130 1,2,4-Trichlorobenzene 0.0500 0.05178 mg/Kg 104 56 -138 1,2,4-Trimethylbenzene 0.0500 0.05540 mg/Kg 111 66 -130 1,2-Dibromoethane 0.0500 0.05560 mg/Kg 111 67 -130 1,2-Dichlorobenzene 0.0500 0.05589 mg/Kg 112 64 -130 1,2-Dichloroethane 0.0500 0.05353 mg/Kg 107 62 -130 1,2-Dichloropropane 0.0500 0.04947 mg/Kg 99 64 -130 1,3,5-Trimethylbenzene 0.0500 0.05420 mg/Kg 108 67 -130 1,3-Dichlorobenzene 0.0500 0.05601 mg/Kg 112 66 -130 1,3-Dichloropropane 0.0500 0.05628 mg/Kg 113 67 -130 1,4-Dichlorobenzene 0.0500 0.05657 mg/Kg 113 65 -130 2,2-Dichloropropane 0.0500 0.04596 mg/Kg 92 51 -132 2-Butanone (MEK)0.200 0.2087 mg/Kg 104 55 -130 2-Chlorotoluene 0.0500 0.05492 mg/Kg 110 67 -130 Eurofins Pensacola Page 24 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646314/10-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646236 Prep Batch: 646314 2-Hexanone 0.200 0.2091 mg/Kg 105 57 -131 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 4-Chlorotoluene 0.0500 0.05475 mg/Kg 110 66 -130 4-Isopropyltoluene 0.0500 0.05644 mg/Kg 113 68 -130 4-Methyl-2-pentanone (MIBK)0.200 0.1917 mg/Kg 96 58 -130 Acetone 0.200 0.2144 mg/Kg 107 48 -160 Benzene 0.0500 0.04952 mg/Kg 99 65 -130 Bromobenzene 0.0500 0.05381 mg/Kg 108 65 -130 Bromochloromethane 0.0500 0.05445 mg/Kg 109 65 -130 Bromodichloromethane 0.0500 0.05155 mg/Kg 103 61 -130 Bromoform 0.0500 0.05314 mg/Kg 106 52 -136 Bromomethane 0.0500 0.03884 mg/Kg 78 12 -160 Carbon tetrachloride 0.0500 0.05086 mg/Kg 102 60 -130 Chlorobenzene 0.0500 0.05253 mg/Kg 105 70 -130 Chloroethane 0.0500 0.04729 mg/Kg 95 55 -134 Chloroform 0.0500 0.05067 mg/Kg 101 62 -130 Chloromethane 0.0500 0.04095 mg/Kg 82 49 -136 cis-1,2-Dichloroethene 0.0500 0.04816 mg/Kg 96 53 -135 cis-1,3-Dichloropropene 0.0500 0.05243 mg/Kg 105 61 -130 Dibromochloromethane 0.0500 0.05541 mg/Kg 111 58 -132 Dichlorodifluoromethane 0.0500 0.03931 mg/Kg 79 34 -143 Ethanol 2.00 1.179 mg/Kg 59 29 -160 Ethylbenzene 0.0500 0.05320 mg/Kg 106 70 -130 Isopropyl ether 0.0500 0.05118 mg/Kg 102 62 -130 Isopropylbenzene 0.0500 0.05448 mg/Kg 109 70 -130 Methyl tert-butyl ether 0.0500 0.05103 mg/Kg 102 63 -130 Methylene Chloride 0.0500 0.04869 mg/Kg 97 57 -132 m-Xylene & p-Xylene 0.0500 0.05380 mg/Kg 108 70 -130 Naphthalene 0.0500 0.05312 mg/Kg 106 45 -144 n-Butylbenzene 0.0500 0.05899 mg/Kg 118 66 -130 N-Propylbenzene 0.0500 0.05500 mg/Kg 110 67 -130 o-Xylene 0.0500 0.05486 mg/Kg 110 70 -130 sec-Butylbenzene 0.0500 0.05565 mg/Kg 111 67 -130 Styrene 0.0500 0.05275 mg/Kg 105 68 -130 tert-Butylbenzene 0.0500 0.05355 mg/Kg 107 67 -130 Tetrachloroethene 0.0500 0.04091 mg/Kg 82 67 -130 Toluene 0.0500 0.05585 mg/Kg 112 70 -130 trans-1,2-Dichloroethene 0.0500 0.04863 mg/Kg 97 58 -134 trans-1,3-Dichloropropene 0.0500 0.05618 mg/Kg 112 60 -130 Trichloroethene 0.0500 0.04917 mg/Kg 98 65 -130 Trichlorofluoromethane 0.0500 0.04650 mg/Kg 93 61 -136 Vinyl acetate 0.100 0.1303 mg/Kg 130 24 -160 Vinyl chloride 0.0500 0.04484 mg/Kg 90 52 -132 Xylenes, Total 0.100 0.1087 mg/Kg 109 70 -130 4-Bromofluorobenzene 67 -130 Surrogate 97 LCS LCS Qualifier Limits%Recovery 105Dibromofluoromethane 77 -127 100Toluene-d8 (Surr)76 -127 Eurofins Pensacola Page 25 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 400-645696/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 RL MDL 1,2,4-Trichlorobenzene <0.0330 U 0.330 0.0330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11,2-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11,3-Dichlorobenzene <0.130 U 0.1300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11,4-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 11-Methylnaphthalene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4,5-Trichlorophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4,6-Trichlorophenol <0.0700 U 0.07000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4-Dichlorophenol <0.0940 U 0.09400.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4-Dimethylphenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,4-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12,6-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Chloronaphthalene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Chlorophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Methylnaphthalene <0.0800 U 0.08000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Methylphenol <0.0700 U 0.07000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Nitroaniline <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 12-Nitrophenol <0.0770 U 0.07700.660 mg/Kg 10/16/23 12:06 10/17/23 15:05 13 & 4 Methylphenol <0.0780 U 0.07800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 13-Nitroaniline <0.240 U 0.2400.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14,6-Dinitro-2-methylphenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Bromophenyl phenyl ether <0.0810 U 0.08100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Chloro-3-methylphenol <0.0810 U 0.08100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Chloroaniline <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Chlorophenyl phenyl ether <0.113 U 0.1130.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Nitroaniline <0.300 U 0.3000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 14-Nitrophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Acenaphthene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Acenaphthylene <0.0980 U 0.09800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Aniline <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Anthracene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[a]anthracene <0.0470 U 0.04700.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[a]pyrene <0.0990 U 0.09900.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[b]fluoranthene <0.110 U 0.1100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[g,h,i]perylene <0.0780 U 0.07800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzo[k]fluoranthene <0.350 U 0.3500.990 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Benzoic acid <0.126 U 0.1260.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1bis (2-chloroisopropyl) ether <0.0730 U 0.07300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Bis(2-chloroethoxy)methane <0.0460 U 0.04600.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Bis(2-chloroethyl)ether <0.0810 U 0.08100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Bis(2-ethylhexyl) phthalate <0.0710 U 0.07100.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Butyl benzyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Chrysene <0.0570 U 0.05700.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Dibenz(a,h)anthracene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Dibenzofuran <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Diethyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Dimethyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Di-n-butyl phthalate <0.120 U 0.1200.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Di-n-octyl phthalate Eurofins Pensacola Page 26 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-645696/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 RL MDL Fluoranthene <0.0330 U 0.330 0.0330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Fluorene <0.100 U 0.1000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachlorobutadiene <0.0660 U 0.06600.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachlorocyclopentadiene <0.0700 U 0.07000.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Hexachloroethane <0.0660 U 0.06600.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Indeno[1,2,3-cd]pyrene <0.0670 U 0.06700.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Isophorone <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Naphthalene <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Nitrobenzene <0.105 U 0.1050.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1N-Nitrosodi-n-propylamine <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1N-Nitrosodiphenylamine <0.160 U 0.1600.660 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Pentachlorophenol <0.0330 U 0.03300.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Phenanthrene <0.0890 U 0.08900.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Phenol <0.0780 U 0.07800.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Pyrene <0.150 U 0.1500.330 mg/Kg 10/16/23 12:06 10/17/23 15:05 1Pyridine 2,4,6-Tribromophenol (Surr)60 10-150 10/17/23 15:05 1 MB MB Surrogate 10/16/23 12:06 Dil FacPreparedAnalyzedQualifierLimits%Recovery 63 10/16/23 12:06 10/17/23 15:05 12-Fluorobiphenyl 27-127 44 10/16/23 12:06 10/17/23 15:05 12-Fluorophenol (Surr)25-128 53 10/16/23 12:06 10/17/23 15:05 1Nitrobenzene-d5 (Surr)15-136 46 10/16/23 12:06 10/17/23 15:05 1Phenol-d5 (Surr)29-130 64 10/16/23 12:06 10/17/23 15:05 1Terphenyl-d14 (Surr)24-146 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645696/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 1,2,4-Trichlorobenzene 2.00 1.284 mg/Kg 64 41 -100 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,2-Dichlorobenzene 2.00 1.127 mg/Kg 56 49 -120 1,3-Dichlorobenzene 2.00 1.131 mg/Kg 57 45 -120 1,4-Dichlorobenzene 2.00 1.089 mg/Kg 54 48 -120 1-Methylnaphthalene 2.00 1.254 mg/Kg 63 40 -120 2,4,5-Trichlorophenol 2.00 1.329 mg/Kg 66 50 -118 2,4,6-Trichlorophenol 2.00 1.324 mg/Kg 66 49 -115 2,4-Dichlorophenol 2.00 1.313 mg/Kg 66 53 -120 2,4-Dimethylphenol 2.00 1.430 mg/Kg 72 45 -108 2,4-Dinitrotoluene 2.00 1.385 mg/Kg 69 53 -133 2,6-Dinitrotoluene 2.00 1.306 mg/Kg 65 51 -114 2-Chloronaphthalene 2.00 1.195 mg/Kg 60 48 -102 2-Chlorophenol 2.00 1.108 mg/Kg 55 50 -102 2-Methylnaphthalene 2.00 1.178 mg/Kg 59 40 -120 2-Methylphenol 2.00 1.139 mg/Kg 57 49 -111 2-Nitroaniline 2.00 1.336 mg/Kg 67 46 -108 2-Nitrophenol 2.00 1.280 mg/Kg 64 53 -120 Eurofins Pensacola Page 27 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645696/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 3 & 4 Methylphenol 2.00 1.125 mg/Kg 56 47 -123 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 3-Nitroaniline 2.00 1.103 mg/Kg 55 28 -119 4,6-Dinitro-2-methylphenol 4.00 2.006 mg/Kg 50 35 -135 4-Bromophenyl phenyl ether 2.00 1.283 mg/Kg 64 51 -120 4-Chloro-3-methylphenol 2.00 1.089 *-mg/Kg 54 57 -124 4-Chloroaniline 2.00 0.9874 mg/Kg 49 26 -102 4-Chlorophenyl phenyl ether 2.00 1.300 mg/Kg 65 53 -113 4-Nitroaniline 2.00 1.173 mg/Kg 59 32 -131 4-Nitrophenol 4.00 4.124 mg/Kg 103 35 -139 Acenaphthene 2.00 1.285 mg/Kg 64 50 -120 Acenaphthylene 2.00 1.273 mg/Kg 64 47 -110 Aniline 2.00 1.887 mg/Kg 94 15 -104 Anthracene 2.00 1.289 mg/Kg 64 52 -120 Benzo[a]anthracene 2.00 1.323 mg/Kg 66 55 -120 Benzo[a]pyrene 2.00 1.337 mg/Kg 67 54 -120 Benzo[b]fluoranthene 2.00 1.288 mg/Kg 64 47 -120 Benzo[g,h,i]perylene 2.00 1.329 mg/Kg 66 45 -120 Benzo[k]fluoranthene 2.00 1.282 mg/Kg 64 52 -120 Benzoic acid 8.69 2.655 mg/Kg 31 10 -139 bis (2-chloroisopropyl) ether 2.00 0.8106 mg/Kg 41 18 -105 Bis(2-chloroethoxy)methane 2.00 0.9612 mg/Kg 48 33 -100 Bis(2-chloroethyl)ether 2.00 1.399 mg/Kg 70 28 -120 Bis(2-ethylhexyl) phthalate 2.00 1.287 mg/Kg 64 40 -150 Butyl benzyl phthalate 2.00 1.304 mg/Kg 65 50 -126 Chrysene 2.00 1.313 mg/Kg 66 54 -120 Dibenz(a,h)anthracene 2.00 1.307 mg/Kg 65 47 -120 Dibenzofuran 2.00 1.301 mg/Kg 65 54 -105 Diethyl phthalate 2.00 1.460 mg/Kg 73 40 -128 Dimethyl phthalate 2.00 1.296 mg/Kg 65 58 -120 Di-n-butyl phthalate 2.00 1.369 mg/Kg 68 40 -122 Di-n-octyl phthalate 2.00 1.456 mg/Kg 73 40 -137 Fluoranthene 2.00 1.358 mg/Kg 68 49 -120 Fluorene 2.00 1.340 mg/Kg 67 47 -120 Hexachlorobenzene 2.00 1.249 mg/Kg 62 49 -127 Hexachlorobutadiene 2.00 1.269 mg/Kg 63 43 -120 Hexachlorocyclopentadiene 2.00 0.8947 mg/Kg 45 10 -140 Hexachloroethane 2.00 1.058 mg/Kg 53 45 -120 Indeno[1,2,3-cd]pyrene 2.00 1.304 mg/Kg 65 47 -120 Isophorone 2.00 1.102 mg/Kg 55 36 -120 Naphthalene 2.00 1.181 mg/Kg 59 41 -120 Nitrobenzene 2.00 1.179 mg/Kg 59 40 -120 N-Nitrosodi-n-propylamine 2.00 1.082 mg/Kg 54 39 -120 N-Nitrosodiphenylamine 1.98 1.195 mg/Kg 60 54 -120 Pentachlorophenol 4.00 2.187 mg/Kg 55 32 -131 Phenanthrene 2.00 1.276 mg/Kg 64 50 -120 Phenol 2.00 1.012 mg/Kg 51 40 -120 Pyrene 2.00 1.297 mg/Kg 65 54 -120 Pyridine 4.00 1.325 mg/Kg 33 29 -120 Eurofins Pensacola Page 28 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645696/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645850 Prep Batch: 645696 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 80 LCS LCS Qualifier Limits%Recovery 612-Fluorobiphenyl 27 -127 522-Fluorophenol (Surr)25 -128 76Nitrobenzene-d5 (Surr)15 -136 50Phenol-d5 (Surr)29 -130 67Terphenyl-d14 (Surr)24 -146 Client Sample ID: Method BlankLab Sample ID: MB 400-646616/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646745 Prep Batch: 646616 RL MDL 1,2,4-Trichlorobenzene <0.0330 U 0.330 0.0330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 11,2-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 11,3-Dichlorobenzene <0.130 U 0.1300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 11,4-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 11-Methylnaphthalene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12,4,5-Trichlorophenol <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12,4,6-Trichlorophenol <0.0700 U 0.07000.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12,4-Dichlorophenol <0.0940 U 0.09400.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12,4-Dimethylphenol <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12,4-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12,6-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12-Chloronaphthalene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12-Chlorophenol <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12-Methylnaphthalene <0.0800 U 0.08000.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12-Methylphenol <0.0700 U 0.07000.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12-Nitroaniline <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 12-Nitrophenol <0.0770 U 0.07700.660 mg/Kg 10/21/23 23:58 10/23/23 19:49 13 & 4 Methylphenol <0.0780 U 0.07800.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 13-Nitroaniline <0.240 U 0.2400.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14,6-Dinitro-2-methylphenol <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14-Bromophenyl phenyl ether <0.0810 U 0.08100.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14-Chloro-3-methylphenol <0.0810 U 0.08100.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14-Chloroaniline <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14-Chlorophenyl phenyl ether <0.113 U 0.1130.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14-Nitroaniline <0.300 U 0.3000.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 14-Nitrophenol <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Acenaphthene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Acenaphthylene <0.0980 U 0.09800.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Aniline <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Anthracene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Benzo[a]anthracene <0.0470 U 0.04700.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Benzo[a]pyrene <0.0990 U 0.09900.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Benzo[b]fluoranthene <0.110 U 0.1100.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Benzo[g,h,i]perylene <0.0780 U 0.07800.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Benzo[k]fluoranthene <0.350 U 0.3500.990 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Benzoic acid Eurofins Pensacola Page 29 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-646616/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646745 Prep Batch: 646616 RL MDL bis (2-chloroisopropyl) ether <0.126 U 0.330 0.126 mg/Kg 10/21/23 23:58 10/23/23 19:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0730 U 0.07300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Bis(2-chloroethoxy)methane <0.0460 U 0.04600.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Bis(2-chloroethyl)ether <0.0810 U 0.08100.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Bis(2-ethylhexyl) phthalate <0.0710 U 0.07100.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Butyl benzyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Chrysene <0.0570 U 0.05700.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Dibenz(a,h)anthracene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Dibenzofuran <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Diethyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Dimethyl phthalate 0.09722 J 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Di-n-butyl phthalate <0.120 U 0.1200.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Di-n-octyl phthalate <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Fluoranthene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Fluorene <0.100 U 0.1000.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Hexachlorobenzene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Hexachlorobutadiene <0.0660 U 0.06600.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Hexachlorocyclopentadiene <0.0700 U 0.07000.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Hexachloroethane <0.0660 U 0.06600.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Indeno[1,2,3-cd]pyrene <0.0670 U 0.06700.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Isophorone <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Naphthalene <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Nitrobenzene <0.105 U 0.1050.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1N-Nitrosodi-n-propylamine <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1N-Nitrosodiphenylamine <0.160 U 0.1600.660 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Pentachlorophenol <0.0330 U 0.03300.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Phenanthrene <0.0890 U 0.08900.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Phenol <0.0780 U 0.07800.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Pyrene <0.150 U 0.1500.330 mg/Kg 10/21/23 23:58 10/23/23 19:49 1Pyridine 2,4,6-Tribromophenol (Surr)82 10-150 10/23/23 19:49 1 MB MB Surrogate 10/21/23 23:58 Dil FacPreparedAnalyzedQualifierLimits%Recovery 71 10/21/23 23:58 10/23/23 19:49 12-Fluorobiphenyl 27-127 41 10/21/23 23:58 10/23/23 19:49 12-Fluorophenol (Surr)25-128 55 10/21/23 23:58 10/23/23 19:49 1Nitrobenzene-d5 (Surr)15-136 43 10/21/23 23:58 10/23/23 19:49 1Phenol-d5 (Surr)29-130 78 10/21/23 23:58 10/23/23 19:49 1Terphenyl-d14 (Surr)24-146 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646616/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646745 Prep Batch: 646616 1,2,4-Trichlorobenzene 2.00 1.389 mg/Kg 69 41 -100 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,2-Dichlorobenzene 2.00 1.249 mg/Kg 62 49 -120 1,3-Dichlorobenzene 2.00 1.212 mg/Kg 61 45 -120 1,4-Dichlorobenzene 2.00 1.194 mg/Kg 60 48 -120 1-Methylnaphthalene 2.00 1.452 mg/Kg 73 40 -120 Eurofins Pensacola Page 30 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646616/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646745 Prep Batch: 646616 2,4,5-Trichlorophenol 2.00 1.500 mg/Kg 75 50 -118 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 2,4,6-Trichlorophenol 2.00 1.391 mg/Kg 70 49 -115 2,4-Dichlorophenol 2.00 1.309 mg/Kg 65 53 -120 2,4-Dimethylphenol 2.00 1.218 mg/Kg 61 45 -108 2,4-Dinitrotoluene 2.00 1.483 mg/Kg 74 53 -133 2,6-Dinitrotoluene 2.00 1.427 mg/Kg 71 51 -114 2-Chloronaphthalene 2.00 1.331 mg/Kg 67 48 -102 2-Chlorophenol 2.00 1.150 mg/Kg 58 50 -102 2-Methylnaphthalene 2.00 1.410 mg/Kg 70 40 -120 2-Methylphenol 2.00 1.286 mg/Kg 64 49 -111 2-Nitroaniline 2.00 1.392 mg/Kg 70 46 -108 2-Nitrophenol 2.00 1.318 mg/Kg 66 53 -120 3 & 4 Methylphenol 2.00 1.165 mg/Kg 58 47 -123 3-Nitroaniline 2.00 1.341 mg/Kg 67 28 -119 4,6-Dinitro-2-methylphenol 4.00 2.018 mg/Kg 50 35 -135 4-Bromophenyl phenyl ether 2.00 1.595 mg/Kg 80 51 -120 4-Chloro-3-methylphenol 2.00 1.200 mg/Kg 60 57 -124 4-Chloroaniline 2.00 1.021 mg/Kg 51 26 -102 4-Chlorophenyl phenyl ether 2.00 1.667 mg/Kg 83 53 -113 4-Nitroaniline 2.00 1.277 mg/Kg 64 32 -131 4-Nitrophenol 4.00 4.083 mg/Kg 102 35 -139 Acenaphthene 2.00 1.475 mg/Kg 74 50 -120 Acenaphthylene 2.00 1.354 mg/Kg 68 47 -110 Aniline 2.00 1.164 mg/Kg 58 15 -104 Anthracene 2.00 1.476 mg/Kg 74 52 -120 Benzo[a]anthracene 2.00 1.529 mg/Kg 76 55 -120 Benzo[a]pyrene 2.00 1.525 mg/Kg 76 54 -120 Benzo[b]fluoranthene 2.00 1.435 mg/Kg 72 47 -120 Benzo[g,h,i]perylene 2.00 1.604 mg/Kg 80 45 -120 Benzo[k]fluoranthene 2.00 1.611 mg/Kg 81 52 -120 Benzoic acid 8.69 1.514 mg/Kg 17 10 -139 bis (2-chloroisopropyl) ether 2.00 0.7982 mg/Kg 40 18 -105 Bis(2-chloroethoxy)methane 2.00 0.8875 mg/Kg 44 33 -100 Bis(2-chloroethyl)ether 2.00 0.7672 mg/Kg 38 28 -120 Bis(2-ethylhexyl) phthalate 2.00 1.389 mg/Kg 69 40 -150 Butyl benzyl phthalate 2.00 1.277 mg/Kg 64 50 -126 Chrysene 2.00 1.528 mg/Kg 76 54 -120 Dibenz(a,h)anthracene 2.00 1.689 mg/Kg 84 47 -120 Dibenzofuran 2.00 1.449 mg/Kg 72 54 -105 Diethyl phthalate 2.00 1.680 mg/Kg 84 40 -128 Dimethyl phthalate 2.00 1.480 mg/Kg 74 58 -120 Di-n-butyl phthalate 2.00 1.603 mg/Kg 80 40 -122 Di-n-octyl phthalate 2.00 1.412 mg/Kg 71 40 -137 Fluoranthene 2.00 1.636 mg/Kg 82 49 -120 Fluorene 2.00 1.545 mg/Kg 77 47 -120 Hexachlorobenzene 2.00 1.593 mg/Kg 80 49 -127 Hexachlorobutadiene 2.00 1.524 mg/Kg 76 43 -120 Hexachlorocyclopentadiene 2.00 0.6946 mg/Kg 35 10 -140 Hexachloroethane 2.00 1.171 mg/Kg 59 45 -120 Eurofins Pensacola Page 31 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-646616/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646745 Prep Batch: 646616 Indeno[1,2,3-cd]pyrene 2.00 1.602 mg/Kg 80 47 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Isophorone 2.00 1.026 mg/Kg 51 36 -120 Naphthalene 2.00 1.304 mg/Kg 65 41 -120 Nitrobenzene 2.00 1.105 mg/Kg 55 40 -120 N-Nitrosodi-n-propylamine 2.00 1.072 mg/Kg 54 39 -120 N-Nitrosodiphenylamine 1.98 1.376 mg/Kg 69 54 -120 Pentachlorophenol 4.00 2.329 mg/Kg 58 32 -131 Phenanthrene 2.00 1.529 mg/Kg 76 50 -120 Phenol 2.00 0.9117 mg/Kg 46 40 -120 Pyrene 2.00 1.388 mg/Kg 69 54 -120 Pyridine 4.00 1.152 mg/Kg 29 29 -120 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 93 LCS LCS Qualifier Limits%Recovery 712-Fluorobiphenyl 27 -127 452-Fluorophenol (Surr)25 -128 75Nitrobenzene-d5 (Surr)15 -136 45Phenol-d5 (Surr)29 -130 77Terphenyl-d14 (Surr)24 -146 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-645692/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645426 Prep Batch: 645692 RL MDL C5-C8 Aliphatics <2.70 U 2.70 2.70 mg/Kg 10/13/23 08:59 10/13/23 10:00 50 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.40 U 1.401.40 mg/Kg 10/13/23 08:59 10/13/23 10:00 50C9-C12 Aliphatics <0.750 U 0.7500.750 mg/Kg 10/13/23 08:59 10/13/23 10:00 50C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)97 70-130 10/13/23 10:00 50 MB MB Surrogate 10/13/23 08:59 Dil FacPreparedAnalyzedQualifierLimits%Recovery 94 10/13/23 08:59 10/13/23 10:00 50a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645692/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645426 Prep Batch: 645692 C5-C8 Aliphatics 15.0 17.90 mg/Kg 119 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 17.5 19.21 mg/Kg 110 70 -130 C9-C10 Aromatics 2.50 2.869 mg/Kg 115 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 101 LCS LCS Qualifier Limits%Recovery 106a,a,a-Trifluorotoluene (pid)70 -130 Eurofins Pensacola Page 32 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645692/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 645426 Prep Batch: 645692 C5-C8 Aliphatics 15.0 17.43 mg/Kg 116 70 -130 3 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 17.5 18.97 mg/Kg 108 70 -130 1 25 C9-C10 Aromatics 2.50 2.732 mg/Kg 109 70 -130 5 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 98 LCSD LCSD Qualifier Limits%Recovery 100a,a,a-Trifluorotoluene (pid)70 -130 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-645810/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 RL MDL C9-C18 Aliphatics <1.60 U 1.60 1.60 mg/Kg 10/17/23 08:04 10/18/23 19:29 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.60 U 1.601.60 mg/Kg 10/17/23 08:04 10/18/23 19:29 1C19-C36 Aliphatics 1-Chlorooctadecane 65 40-140 10/18/23 19:29 1 MB MB Surrogate 10/17/23 08:04 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-645810/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 RL MDL C9-C18 Aliphatics <1.60 U 1.60 1.60 mg/Kg 10/17/23 08:04 10/18/23 19:40 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.60 U 1.601.60 mg/Kg 10/17/23 08:04 10/18/23 19:40 1C19-C36 Aliphatics <3.00 U 3.003.00 mg/Kg 10/17/23 08:04 10/18/23 19:40 1C11-C22 Aromatics o-Terphenyl 74 40-140 10/18/23 19:40 1 MB MB Surrogate 10/17/23 08:04 Dil FacPreparedAnalyzedQualifierLimits%Recovery 96 10/17/23 08:04 10/18/23 19:40 12-Fluorobiphenyl 40-140 92 10/17/23 08:04 10/18/23 19:40 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645810/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 C9-C18 Aliphatics 20.0 12.12 mg/Kg 61 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 26.7 19.61 mg/Kg 74 40 -140 1-Chlorooctadecane 40 -140 Surrogate 67 LCS LCS Qualifier Limits%Recovery Eurofins Pensacola Page 33 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645810/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 C9-C18 Aliphatics 20.0 <1.60 U *-mg/Kg 0 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 26.7 <1.60 U *-mg/Kg 0 40 -140 C11-C22 Aromatics 56.7 40.74 mg/Kg 72 40 -140 o-Terphenyl 40 -140 Surrogate 74 LCS LCS Qualifier Limits%Recovery 1012-Fluorobiphenyl 40 -140 982-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645810/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646121 Prep Batch: 645810 C9-C18 Aliphatics 20.0 11.63 mg/Kg 58 40 -140 4 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 26.7 18.31 mg/Kg 69 40 -140 7 50 1-Chlorooctadecane 40 -140 Surrogate 61 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-645810/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646124 Prep Batch: 645810 C9-C18 Aliphatics 20.0 <1.60 U *-mg/Kg 0 40 -140 NC 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 26.7 <1.60 U *-mg/Kg 0 40 -140 NC 50 C11-C22 Aromatics 56.7 39.93 mg/Kg 70 40 -140 2 50 o-Terphenyl 40 -140 Surrogate 70 LCSD LCSD Qualifier Limits%Recovery 992-Fluorobiphenyl 40 -140 992-Bromonaphthalene 40 -140 Method: 6010D - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 400-645490/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646339 Prep Batch: 645490 RL MDL Chromium <0.310 U 1.00 0.310 mg/Kg 10/13/23 13:18 10/19/23 12:38 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.220 U 0.2201.00 mg/Kg 10/13/23 13:18 10/19/23 12:38 1Lead Eurofins Pensacola Page 34 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method: 6010D - Metals (ICP) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645490/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646339 Prep Batch: 645490 Chromium 99.4 97.90 mg/Kg 98 80 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Lead 99.4 93.83 mg/Kg 94 80 -120 Client Sample ID: Method BlankLab Sample ID: MB 400-645677/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646016 Prep Batch: 645677 RL MDL Chromium <0.311 U 1.00 0.311 mg/Kg 10/16/23 12:39 10/17/23 16:42 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.220 U 0.2201.00 mg/Kg 10/16/23 12:39 10/17/23 16:42 1Lead Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-645677/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 646016 Prep Batch: 645677 Chromium 100 94.95 mg/Kg 95 80 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Lead 100 93.11 mg/Kg 93 80 -120 Eurofins Pensacola Page 35 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Client Sample ID: MW-1 10'Lab Sample ID: 400-244959-1 Matrix: SolidDate Collected: 10/10/23 11:36 Date Received: 10/12/23 09:41 Analysis Moisture TMP10/19/23 17:191 EET PEN646393 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: MW-1 10'Lab Sample ID: 400-244959-1 Matrix: SolidDate Collected: 10/10/23 11:36 Percent Solids: 92.2Date Received: 10/12/23 09:41 Prep 5035 CH10/19/23 08:35 EET PEN646314 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.196 g 5.00 g Analysis 8260D 1 646236 10/19/23 16:15 CH EET PENTotal/NA 5 mL 5 mL Prep 3546 646616 10/21/23 23:58 JTC EET PENTotal/NA 15.03 g 1 mL Analysis 8270E 1 646745 10/23/23 22:02 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 645692 10/16/23 16:00 SRK EET PENTotal/NA 4.787 g 5.00 g Analysis MAVPH 50 645426 10/16/23 22:14 SRK EET PENTotal/NA 5 mL 5 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.46 g 2 mL Analysis MA-EPH 1 646121 10/18/23 21:02 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.46 g 2 mL Analysis MA-EPH 1 646124 10/18/23 21:25 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 645490 10/13/23 13:18 KWN EET PENTotal/NA .522 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 13:22 BAW EET PENTotal/NA Client Sample ID: MW-1 15'Lab Sample ID: 400-244959-2 Matrix: SolidDate Collected: 10/10/23 11:45 Date Received: 10/12/23 09:41 Analysis Moisture TMP10/19/23 17:191 EET PEN646393 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: MW-1 15'Lab Sample ID: 400-244959-2 Matrix: SolidDate Collected: 10/10/23 11:45 Percent Solids: 85.6Date Received: 10/12/23 09:41 Prep 5035 SRK10/16/23 16:00 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.606 g 5.0 g Analysis MAVPH 50 645426 10/16/23 22:53 SRK EET PENTotal/NA 5 mL 5 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.16 g 2 mL Analysis MA-EPH 1 646121 10/18/23 21:14 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.16 g 2 mL Analysis MA-EPH 1 646124 10/18/23 21:37 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: MW-1 20'Lab Sample ID: 400-244959-3 Matrix: SolidDate Collected: 10/10/23 11:53 Date Received: 10/12/23 09:41 Analysis Moisture TMP10/19/23 17:191 EET PEN646393 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Eurofins Pensacola Page 36 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Client Sample ID: MW-1 20'Lab Sample ID: 400-244959-3 Matrix: SolidDate Collected: 10/10/23 11:53 Percent Solids: 73.4Date Received: 10/12/23 09:41 Prep 5035 CH10/19/23 08:35 EET PEN646314 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.882 g 5.00 g Analysis 8260D 1 646236 10/19/23 16:37 CH EET PENTotal/NA 5 mL 5 mL Prep 3546 645696 10/16/23 12:06 LH EET PENTotal/NA 15.07 g 1 mL Analysis 8270E 1 645850 10/17/23 17:41 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 645692 10/16/23 16:00 SRK EET PENTotal/NA 6.191 g 5.00 g Analysis MAVPH 50 645426 10/16/23 23:33 SRK EET PENTotal/NA 5 mL 5 mL Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.18 g 2 mL Analysis MA-EPH 1 646121 10/18/23 21:37 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.18 g 2 mL Analysis MA-EPH 1 646124 10/18/23 22:00 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 645677 10/16/23 12:39 KWN EET PENTotal/NA .518 g 50 mL Completed:10/16/23 16:15 ¹ Analysis 6010D 1 646016 10/17/23 17:41 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645490/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN10/13/23 13:18 EET PEN645490 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA .500 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 12:38 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645677/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN10/16/23 12:39 EET PEN645677 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA .499 g 50 mL Completed:10/16/23 16:15 ¹ Analysis 6010D 1 646016 10/17/23 16:42 BAW EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-645692/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SRK10/13/23 08:59 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 mL Analysis MAVPH 50 645426 10/13/23 10:00 SRK EET PENTotal/NA 5 mL 5 mL Eurofins Pensacola Page 37 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Client Sample ID: Method Blank Lab Sample ID: MB 400-645696/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH10/16/23 12:06 EET PEN645696 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 645850 10/17/23 15:05 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-645810/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646121 10/18/23 19:29 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 646124 10/18/23 19:40 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-646314/9-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 CH10/19/23 08:35 EET PEN646314 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 646236 10/19/23 09:48 CH EET PENTotal/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-646616/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 JTC10/21/23 23:58 EET PEN646616 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 646745 10/23/23 19:49 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645490/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN10/13/23 13:18 EET PEN645490 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA .503 g 50 mL Completed:10/13/23 16:35 ¹ Analysis 6010D 1 646339 10/19/23 12:50 BAW EET PENTotal/NA Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645677/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN10/16/23 12:39 EET PEN645677 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA .499 g 50 mL Completed:10/16/23 16:15 ¹ Analysis 6010D 1 646016 10/17/23 16:46 BAW EET PENTotal/NA Eurofins Pensacola Page 38 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645692/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SRK10/13/23 08:59 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 mL Analysis MAVPH 50 645426 10/13/23 10:39 SRK EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645696/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH10/16/23 12:06 EET PEN645696 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 645850 10/17/23 15:30 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-645810/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646121 10/18/23 19:40 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:04 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-646314/10-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 CH10/19/23 08:35 EET PEN646314 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 646236 10/19/23 08:41 CH EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-646616/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 JTC10/21/23 23:58 EET PEN646616 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 646745 10/23/23 20:16 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-645692/3-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SRK10/13/23 08:59 EET PEN645692 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 mL Analysis MAVPH 50 645426 10/16/23 13:49 SRK EET PENTotal/NA 5 mL 5 mL Eurofins Pensacola Page 39 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-645810/18-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR10/17/23 08:04 EET PEN645810 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 646121 10/18/23 19:52 LHB EET PENTotal/NA Prep 3546 645810 10/17/23 08:04 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 646124 10/18/23 20:15 MP EET PENTotal/NA 1 mL 1 mL ¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 40 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 400-244959-1Client: Consultech Environmental LLC Project/Site: Kwik Stop Method Method Description LaboratoryProtocol SW8468260DVolatile Organic Compounds by GC/MS EET PEN SW8468270ESemivolatile Organic Compounds (GC/MS)EET PEN MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN SW8466010DMetals (ICP)EET PEN EPAMoisturePercent Moisture EET PEN SW8463050BPreparation, Metals EET PEN SW8463546Microwave Extraction EET PEN SW8465035Closed System Purge and Trap EET PEN Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 41 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Consultech Environmental LLC Job ID: 400-244959-1 Project/Site: Kwik Stop Laboratory: Eurofins Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte Moisture Solid Percent Moisture Moisture Solid Percent Solids Eurofins Pensacola Page 42 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 43 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Consultech Environmental LLC Job Number: 400-244959-1 Login Number: 244959 Question Answer Comment Creator: Earnest, Tamantha List Source: Eurofins Pensacola List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.0.0°C IR8 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Pensacola Page 44 of 44 10/25/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 APPENDIX B Well Construction Record Stefan Smith 3576A SAEDACCO X 10-10-23 MW1 1024 South Trade St. , Tryon, NC, 28782 Polk 35.197469 82.229989 X X 1 18 8 HSA 0 8 2 SCH 40 PVC 8 18 2 .010 SCH 40 PVC 0 4 Portland Pour 6 18 Sand #2 0 12 Fill 12 18 Silt 2 foot bentonite seal from 4 to 6' 10/16/2023 Stefan Smith 3576A SAEDACCO X 10-10-23 MW2 1024 South Trade St. , Tryon, NC, 28782 Polk 35.197372 82.229868 X X 1 19 8 HSA 0 9 2 SCH 40 PVC 9 19 2 .010 SCH 40 PVC 0 5 Portland Pour 7 19 Sand #2 0 8 Silt 8 14 Clayey silt 14 19 Clayey sandy silt. 2 foot bentonite seal from 5 to 7' 10/16/2023