AS-243_3701_CA_RPTS_20180920_HRP Fmr Stamey Stores Pty

LIMITED PHASE 2
ENVIRONMENTAL SITE ASSESSMENT
REPORT

Former Stamey Stores, Inc. Property
4726 Fallston Road
Fallston, NC 28090

Prepared For:

Sirron Preservation, LLC
c\o: Mae Beth Boggs
203 Spurling Road
Fallston, NC 28042

Prepared By:

HRP Associates, Inc.
1327 Miller Road, Suite D
Greenville, SC 29607

Consultant Project #: SIR8000.P2

Issued On: September 20, 2018
Limited Phase 2 ESA
Sirron Preservation, LLC
Fallston, North Carolina
Page i of ii

H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
TABLE OF CONTENTS
1.0 INTRODUCTION ......................................................................................................... 1 
2.0 UTILITY MARKOUT AND GROUND PENETRATING RADAR SURVEY .......................... 3 
2.1 Utility Mark-out ........................................................................................................ 3 
2.2 Ground Penetrating Radar ........................................................................................ 3 
3.0 LIMITED SOIL AND GROUNDWATER INVESTIGATION ............................................. 4 
3.1 Soil Boring Investigation .......................................................................................... 4 
3.2 Groundwater Investigation ....................................................................................... 5 
3.3 Boring Abandonment ............................................................................................... 5 
3.4 Investigation Derived Wastes ................................................................................... 5 
3.5 Equipment Decontamination ..................................................................................... 5 
4.0 ANALYTICAL RESULTS ............................................................................................... 6 
4.1 Soil Analytical Results .............................................................................................. 6 
4.2 Groundwater Analytical Results ................................................................................. 6 
4.3 Quality Assurance/Quality Control ............................................................................. 7 
5.0 CONCLUSIONS ........................................................................................................... 8 
6.0 REFERENCES ............................................................................................................ 10 

Figures

Figure 1 Site Location
Figure 2 Site Plan
Figure 3 Soil Analytical Results
Figure 4 Groundwater Analytical Results

Tables

Table 1 Soil Boring Summary
Table 2 Soil Analytical Data Summary
Table 3 Groundwater Analytical Data Summary

Appendices

Appendix A Soil Boring Logs and Field Data Sheets
Appendix B Laboratory Analytical Report

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 1 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
1.0 INTRODUCTION

On behalf of Sirron Preservation, LLC, HRP Associates Engineering and Environmental
Management, PLLC, a Connecticut limited liability company, doing business in North Carolina as
HRP Associates Engineering and Environmental Management, PLLC, referred to herein as HRP,
has completed a Limited Phase 2 Environmental Site Assessment (ESA) of the Former Stamey
Stores, Inc. Property located at 4726 Fallston Road in Fallston, North Carolina (herein referred
to as the “Site”). A Site location map is included as Figure 1.

The Site consists of an approximately 1.48-acre parcel of land identified by the Cleveland
County Tax Assessor as Parcel 34895. The Site is developed with one (1) approximately 15,400
square foot Site building constructed in 1925. The Site building is of steel frame construction
supported by masonry brick walls over a raised foundation. The building was most recently
operational as a department store and is currently undergoing renovation for the purpose of
operating as an event venue. The remainder of the Site consists of a paved parking lot.

On June 25, 2018, HRP conducted a Phase 1 Environmental Site Assessment (ESA) on the Site
to assess potential environmental issues. The Phase 1 ESA indicated the following:

 The Site building was constructed in 1925 and has historically operated as a department
store, butchery, and as a furniture retailer.
 The Site was listed on the leaking underground storage tank (LUST) database due to the
former operation of a 550-gallon underground storage tank (UST) utilized for the retail sale
of kerosene. The UST is located adjacent to the southern exterior wall of the Site building
and was installed on March 7, 1946 according to the North Carolina Department of
Environmental Quality (NCDEQ) UST Database. A release from the kerosene UST was
discovered during soil sampling activities for an in-place UST closure on December 8, 1993.
HRP accessed the NCDEQ’s (formerly NCDEHNR & NCDENR) Laser fiche online file database
and contacted Mr. Mike Streeter, Hydrogeologist for the NCDEQ UST Division based out of
Mooresville, NC to obtain information relating to historical assessment activities.
HRP reviewed multiple files including a document titled “Extent of Soil Contamination,
Groundwater Analysis, Site Sensitivity Evaluation” by Southeastern Geological Services
(SGS) and dated July 13, 1994. The document indicated that five (5) borings were advanced
at the Site, one of which was converted to a permanent groundwater monitoring well,
between May 31 and June 1, 1994. Field screening results indicated that kerosene had
impacted approximately 200 cubic yards of soil from the UST (situated approximately 5 feet
below grade) to the water table located approximately 22 feet below the ground surface.
The contaminated soil was noted to extend radially around the UST, and that approximately
one-third of the estimated contamination plume was located beneath the Site building.
Further, the concentrations of benzene, ethylbenzene, xylenes, and naphthalene detected in
groundwater exceeded regulatory limits.
A “Corrective Action Plan” (CAP) dated April 1995 prepared by SGS recommended utilizing
air sparging combined with vapor extraction as a viable means for remediating the Site. The
CAP was approved by NCDENR in 1995; however, multiple setbacks occurred in getting the
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 2 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
system operational at the Site. No documents stating that the remediation was successfully
setup were identified. However, a correspondence letter dated February, 1997 from SGS to
the NCDENR requested a No Further Action (NFA) designation based on a change in
regulatory standards. The NCDENR replied with a request to sample the five (5)
groundwater wells located on the Site, collect and analyze one (1) soil sample, and submit
an updated water well survey. SGS complied with the requests and submitted a final
groundwater monitoring report on July 5, 1998.
On July 23, 1998, the NCDENR issued a “Notice of NFA” letter to the Site. The NFA letter
noted that the soils at the Site did not exceed industrial/commercial criteria, and that the
groundwater results were below their applicable standards. The NFA letter further stated
that “because contaminated soil was not cleaned up to the residential maximum soil
contaminant concentrations, the property containing soil contamination is not suitable for
residential use.” The reported remaining soil and groundwater contamination in connection
with land use restrictions for residential use is considered a Conditional Recognized
Environmental Condition (CREC).
 Two (2) adjacent and up-gradient properties with confirmed UST releases were identified to
have historically impacted the Site. Recent assessment activities indicate that petroleum
constituents are still present above regulatory standards on the western adjoining
properties.
The purpose of this Phase 2 ESA was to assess soil and groundwater in the area of the on-Site
UST and to assess groundwater down-gradient of the off-Site LUST facilities.

Work conducted by HRP in connection with the performance of this Limited Phase 2 ESA was
performed in accordance with the HRP proposal dated August 1, 2018, authorized on August 9,
2018. HRP’s proposal provided the guidelines with respect to evaluation of the areas of
environmental concern.

It should be noted that the westernmost boring (HA-1) could not be advanced to groundwater
due to the inability to use the drill rig with the limited clearance allowed by the awning on the
western side of the Site building. Additionally, the groundwater monitoring well located
southwest of the Site building (MW-7) could not be sampled due to the well being dry. These
limitations are not anticipated to affect our assessment of this area as the remaining borings
and wells were successfully sampled.

This report presents information regarding the following tasks:

 Utility Markout and a Ground Penetrating Radar (GPR) Survey;

 Limited Subsurface Soil and Groundwater Investigation; and,

 Data Summary and Evaluation.

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 3 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
2.0 UTILITY MARKOUT AND GROUND PENETRATING RADAR SURVEY

The following section provides information on how subsurface utilities were located.

2.1 Utility Mark-out

North Carolina 811 (a utility protection service) was contacted to identify public underground
utilities at the Site prior to initiation of the subsurface investigation. HRP contacted North
Carolina 811 on August 9, 2018 and was issued ticket # A182210995. As a result, eight (8)
utility providers were notified to mark their assets, if present, on the Site.

2.2 Ground Penetrating Radar

A GPR survey was performed at the Site prior to drilling activities to protect unidentified
subsurface utility lines and other unforeseen subsurface obstructions. GPR involves scanning
the subsurface with a device that emits and records the return signals of electromagnetic
energy in the radar wavelength.

HRP representatives established a survey grid of the anticipated areas of investigation in an
attempt to identify utility lines or other buried objects located in the area prior to advancement
of soil borings. A site-wide GPR survey was not completed as the survey grid was limited to the
approximate location of each boring.

No unusual anomalies were identified during the GPR survey. At the time of the GPR Survey, an
approximately 2 foot wide by 2 feet deep excavation area located adjacent to the southern wall
of the Site building was observed. The excavation area was reportedly constructed for the
installation of new plumbing lines for the Site building. The excavation debris was observed to
be in the area of the abandoned-in-place UST; as well as in an area of a proposed boring.
Therefore, the GPR was unable to accurately locate the area of the UST.
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 4 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
3.0 LIMITED SOIL AND GROUNDWATER INVESTIGATION

The following section outlines the methods used to investigate the subsurface.

3.1 Soil Boring Investigation

On August 19, 2018, one (1) soil boring and two (2) hand auger borings were advanced on the
Site to assess soil and groundwater conditions. The location of each of the borings is shown on
Figure 2.

A track-mounted Geoprobe® 7822DT drill rig was used to install the soil boring (SB-1) in an up-
gradient location. Continuous soil samples were collected beginning at ground surface in four-
foot HDPE liners during boring advancement.

A manually-operated hand auger was used to collect soil samples at each of the two (2) hand
auger borings (HA-1 and HA-2). Each soil-core was screened for volatile organic vapor at one-
or two-foot intervals using a MiniRae 3000 photo-ionization detector (PID). Soil logs are
included in Appendix A.

Table 1 provides a description of each location, boring depth, whether groundwater was
encountered, and the maximum PID reading at each location. A brief description of each boring
is provided below:

 SB-1: located in the southern portion of the site, up-gradient area, highest PID detection
of 0.6 ppm, no odor was noted in the soil, one (1) soil and one (1) groundwater sample
were collected based on its up-gradient location;

 HA-1: located west of the Site building, highest PID detection of 0.9 ppm, no odor was
noted in the soil, one (1) soil sample was collected to assess soil quality;

 HA-2: located adjacent to the southern exterior wall in the area of the UST, highest PID
detection of 909.1 ppm, heavy petroleum odor was noted in the soil, one (1) soil sample
was collected to measure level of petroleum contamination;

According to the United States Department of Agriculture (USDA), the soils at the Site consist
primarily of Cecil sandy clay loam (USDA 2018).

Subsurface observations during the field investigation indicated that soils at the Site consist of
primarily sandy fat clay and silty sand. Bedrock was not encountered at the Site. Boring logs are
provided in Appendix A. Based on the topographic map presented as Figure 1, the ground
surface slopes to the northeast towards the Stillwater River.

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 5 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
3.2 Groundwater Investigation

Groundwater was encountered in one (1) direct-push boring and within three (3) existing
permanent (MW-4, SE-MW-4, and MW-5) monitoring wells at depths ranging from 23.56 ft
below ground surface (bgs) to 34.08 ft bgs. The direct-push boring was converted to a
temporary groundwater monitoring well identified as “TMW-1.” The existing permanent
monitoring wells were identified with the “MW” nomenclature as identified in Figure 2. The
temporary monitoring well was constructed of a 1-inch PVC riser with a 10-foot screen. The
existing permanent monitoring wells were constructed of a 2-inc PVC riser with a 5-foot screen.

One (1) groundwater sample was collected from the temporary monitoring well using a low-flow
sampling technique with a peristaltic pump. Groundwater samples were collected from MW-4,
SE-MW-4, and MW-5 well using a volume purge technique with a typhoon pump. Water quality
parameters pH, conductivity, temperature, and turbidity were measured prior to sample
collection. The Well Installation Log is included with HRP’s Field Data Sheets, included in
Appendix A.

Groundwater flow direction was inferred to be to the northeast based on topography and Site
observations. A calculated groundwater flow gradient and flow direction could not be
determined based on Site conditions and lack of a Site survey.

3.3 Boring Abandonment

Following the collection of all soil and groundwater samples, each of the three (3) borings
drilled by HRP was abandoned in accordance with the North Carolina well abandonment
standards.

3.4 Investigation Derived Wastes

Soil cuttings and purge water generated during this assessment were temporarily staged on-
Site in one 55-gallon steel drum and positioned on the eastern Site boundary. A label was
placed on the drum noting its contents. The drum was sampled and proper disposal is pending.
The laboratory analytical reports are included in Appendix B.

3.5 Equipment Decontamination
Reusable down-hole investigative equipment was decontaminated before first use and between
sampling locations. Disposable HDPE liners were used to collect soil during borehole
advancement. Samples were collected from the cores using disposable nitrile gloves and all
appropriate measures were taken to ensure the proper collection and handling of samples in
order to provide representative Site data.
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 6 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
4.0 ANALYTICAL RESULTS

The following section describes the analytical procedures and data generated during the Limited
Phase 2 ESA. The laboratory analytical reports are included in Appendix B.

4.1 Soil Analytical Results

A total of three (3) soil samples were submitted under chain-of-custody to a laboratory certified
in North Carolina and analyzed for the following constituents:
 Volatile Organic Compounds (VOCs list) via EPA Method 8260B; and
 Polycyclic Aromatic Hydrocarbons (PAHs) via EPA Method 8270 SIM
Analytical data from the soil samples were compared to the Environmental Protection Agency’s
(EPA) Residential Soil Screening Levels (SSL) and the North Carolina Department of
Environmental Quality (NCDEQ) Maximum Soil Contaminant Concentration Levels (MSCCs)
(NCDEQ 2017). HRP believes that these screening criteria are appropriate for determining
environmental risk at the Site related to past releases at the Site and adjoining properties.
Table 2 provides a tabulation of the constituents detected above their laboratory detection limit
in each soil sample.
 VOCs: A total of 12 VOCs were present above the laboratory detection limit in the three
(3) soil samples collected. Naphthalene was detected at a concentration exceeding the
NCDEQ MSCC in the sample collected from HA-2.
 PAHs: A total of seven PAHs were present above the laboratory detection limit in the
three (3) soil samples collected. However, none of the PAHs exceeded either the
NCDEQ MSCCs or the US EPA Residential SSLs.
The concentration of naphthalene from the VOC analysis in the sample collected from HA-2 was
7,120 micrograms per liter (µg/kg), greater than the US EPA Residential SSL of 3,800 µg/kg.
This sample was collected from a depth of 7-8 feet bgs and was located adjacent to the
abandoned-in-place UST. Naphthalene was also detected in the PAH analysis of this sample, at
a concentration of 334 µg/kg. The VOC result is considered more accurate. No other
exceedances were detected.
4.2 Groundwater Analytical Results

A total of four (4) groundwater samples were submitted under chain-of-custody to a laboratory
certified in North Carolina and analyzed for the following constituents:
 VOCs via EPA Method 8260B; and
 PAHs via EPA Method 8270 SIM.
Table 3 provides a summary of analytical data from the groundwater samples, conservatively
compared to NCDEQ 15A NCAC 02L Groundwater Standards and the EPA’s Maximum
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 7 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
Contaminant Level (MCL). HRP believes that these screening criteria are appropriate for
determining environmental risk at the Site related to past releases at the Site and adjoining
properties.
 VOCs: A total of nine VOCs were present above the laboratory detection limit in the four
(4) groundwater samples collected. Benzene, 1,2-Dichloroethane, methyl tert-butyl ether
(MTBE), and naphthalene were detected at concentrations exceeding the NCDEQ 2L
groundwater standards in the sample collected from MW-5. Chloromethane was
detected at a concentration slightly greater than the NCDEQ 2L groundwater standard
within TMW-1.
 PAHs: PAHs were not present above detection limits in samples collected from TMW-1,
MW-4, and SE-MW-4. A total of four (4) PAHs (anthracene, 1-methylnaphthalene, 2-
methylnaphthalene, and naphthalene) were present above the laboratory detection limit
in MW-5. Of these, 2-methylnaphthalene and naphthalene were detected at
concentrations exceeding the NCDEQ 2L groundwater standards. No other exceedances
were observed.
4.3 Quality Assurance/Quality Control
Field instruments used as part of this assessment were calibrated in accordance with HRP’s
internal quality control procedures and laboratory certification requirements.

Typical laboratory quality assurance/quality control (QA/QC) procedures were conducted and
included a laboratory blank, standard, duplicate, and spike samples. The results of the
laboratory QA/QC samples indicate that the laboratory data for the submitted soil and
groundwater samples are considered reliable, valid and sufficient for the purpose of this
assessment.

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 8 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
5.0 CONCLUSIONS

A Limited Phase 2 Environmental Site Assessment was performed at the former Stamey Stores,
Inc. Property on August 19, 2018 to assess soil and groundwater in the area of the on-Site UST
and to assess groundwater down-gradient of the off-Site LUST sites.

Based upon the results of this investigation, HRP concludes the following:
 Three soil borings were advanced at the Site, one of which was converted to a
temporary monitoring well. One soil sample was collected from each boring and
analyzed for VOCs and PAHs. Three existing permanent monitoring wells located on the
Site and one temporary monitoring well were sampled for VOCs and PAHs.
 A total of seven PAHs and twelve VOCs were present above the laboratory detection
limit in the three soil samples collected. No PAHs were detected in concentrations
exceeding the NCDEQ MSCCs or the US EPA Residential SSLs; however, one constituent
(naphthalene, as a VOC) was detected at a concentration exceeding the US EPA
Residential SSL in the sample collected from HA-2.
 Thirteen constituents were detected in one of the groundwater samples (MW-5)
collected at the Site. Two PAHs (2-methylnaphthalene and naphthalene) were present at
concentrations exceeding the NCDEQ 2L groundwater standards. The remaining three
groundwater samples did not contain any PAHs at concentrations above method
detection limits.
 A total of nine VOCs were present above the laboratory detection limit in the four
groundwater samples. Benzene, 1,2-Dichloroethane, MTBE, and naphthalene were
detected in exceedance of the NCDEQ 2L groundwater standards in the sample collected
from MW-5. Chloromethane was detected in exceedance of the NCDEQ 2L groundwater
standard in the sample collected from TMW-1. The remaining two groundwater samples
did not contain any constituents at concentrations above reporting limits.
The soil data obtained during this Limited Phase 2 ESA is generally consistent with historical
data that formed the basis of the No Further Action (NFA) designation that was issued by
NCDEQ in 1998.

The groundwater data indicates that VOC and PAH concentrations have increased in well MW-5,
which is reportedly a bedrock well, since the 1998 sampling event conducted by Southeastern
Geological Services (Southeastern Geological Services, 1998). It is important to note that the
up-gradient property (“Lewis Service Station”) continues to have significantly high
concentrations of VOCs in groundwater, with benzene as high as 5,900 µg/L as recently as
August 2017. A report prepared by Terracon states that constituent concentrations appear to be
increasing at the Lewis Service Station property and that the plume appears to be migrating
vertically downward (Terracon, 2017).

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 9 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
Based on the above, HRP infers from the minimal amount of data obtained during this Limited
Phase 2 ESA that the impacted groundwater in the vicinity of MW-5 is attributable to the up-
gradient/off-site plume and is not related to the on-site kerosene UST that was closed in 1993.
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
Page 10 of 10
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
6.0 REFERENCES

Environmental Protection Agency, 2018. Regional Screening Level Tables, May 2018.

North Carolina Department of Commerce, 2017. Technical Guidance Manual for the 2017
Closure, Corrective Action, and Petroleum Contaminated Soil Rules.

Soil Survey Staff, Natural Resources Conservation Service, United States Department of
Agriculture. Web Soil Survey. Available online at the following link:
https://websoilsurvey.sc.egov.usda.gov/. Accessed: August 22, 2018.

Southeastern Geological Services, 1998. Monitor Well and Soil Sampling Water Well Survey,
Incident #12004, 4726 Fallston Road, Fallston, Cleveland County, July 5, 1998.

Terracon Consultants, Inc., 2017. Federal/State-Lead Monitoring Report, Lewis Service Station
(Incident #3701), 4733 Fallston Road, Fallston, Cleveland County, NC; September 27, 2017.

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
FIGURES

Copyright:© 2013 National Geographic Society, i-cubed
0 2,000 4,000 6,000 8,0001,000
Feet
1 inch = 2,000 feet
Path: H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Figures\Figure 1 - Site Location.mxdFigure 1Site Location4726 Fallston RoadFallston, North CarolinaHRP # SIR8000.P2Scale 1"=2,000'
Site Location
USGS Quadrangle Data
USGS ID: 35081-D5
Quad Name: Lawndale, North Carolina
Date Pub: 1983
Map Edit: 1
FallstonRoadE.StageCoachTrail
GW-12WSW-4
GW-10
GW-11
GW-4
GW-3
GW-15
GW-2
GW-1
GW-8
GW-7
WSW-3WSW-2
WSW-1
GW-5
GW-13
GW-9
GW-14
MW-5
MW-4
MW-3 MW-1
MW-2
MW-8
SE-MW-4
MW-4
MW-7
SE-MW-2
SE-MW-1
SE-MW-3
MW-5
VMW-1
GW-6
Residential
Residential
FallstonElementarySchool
Stamey StoreLUSTFacility ID: 12004
Lewis Service StationLUST TRUSTFacility ID: 12873
Commercial
Location of crushed asphalt,household trash, constructiondebris, railroad ties
(3) Former 1,000-Gal. Gasoline USTs
Former 1,000-Gal. Kerosene UST
Former 1,000-Gal. Gasoline USTs(abandoned in place)Former 1,000-Gal. Gasoline USTs(abandoned in place)
550-Gal. GasolineUST (not in use)550-Gal. GasolineUST (not in use)
Fallston SalesLUST, IMFacility ID: 16105
Abandoned-in-place 550-Gal. Kerosene UST
UST (Unknown capacity)
HA-2(Soil Only)
SB-1 (Temporary Well (TMW-1) & Soil Sample)
HA-1(Soil Only)
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the
GIS User Community
0 6030
Feet
Path: H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Figures\Figure 2 - Site Plan.mxdFIGURE NO.2Site PlanIssue Date:Project No:Sheet Size:Designed By:Drawn By:Reviewed By:08/23/2018SIR8000.P211x17AJHBOBSCMRevisionsNo.DateNorth
Legend
Temporary Well & Soil
Boring (HRP)
Hand Auger (HRP)
Water Supply Well
(abandoned or not in
use)
Existing Type III
Monitoring Well
Existing Type II
Monitoring Well
Previous Geoprobe
Groundwater Sample
Inferred Groundwater
Flow Direction
AST
UST
Approx. Site Boundary
4726 Fallston RoadFallston, North Carolina
FallstonRoadE.StageCoachTrail
Residential
Residential
FallstonElementarySchool
Stamey StoreLUSTFacility ID: 12004
Lewis Service StationLUST TRUSTFacility ID: 12873
Commercial
Location of crushed asphalt,household trash, constructiondebris, railroad ties
(3) Former 1,000-Gal. Gasoline USTs
Former 1,000-Gal. Kerosene UST
Former 1,000-Gal. Gasoline USTs(abandoned in place)Former 1,000-Gal. Gasoline USTs(abandoned in place)
550-Gal. GasolineUST (not in use)550-Gal. GasolineUST (not in use)
Fallston SalesLUST, IMFacility ID: 16105
Abandoned-in-place 550-Gal. Kerosene UST
UST (Unknown capacity)
HA-2(Soil Only)
SB-1 (Temporary Well (TMW-1) & Soil Sample)
HA-1(Soil Only)
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the
GIS User Community
0 6030
Feet
Path: H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Figures\Figure 3 - Soil Borings and Hand Augers.mxdFIGURE NO.3Soil Analytical Data SummaryIssue Date:Project No:Sheet Size:Designed By:Drawn By:Reviewed By:08/23/2018SIR8000.P211x17AJHBOBSCMRevisionsNo.DateNorth
Legend
Temporary Well & Soil
Boring
Hand Auger
UST
Approx. Site Boundary
4726 Fallston RoadFallston, North Carolina
FallstonRoadE.StageCoachTrail
SE-MW-4
MW-4
MW-7(Dry)
MW-5
Residential
Residential
FallstonElementarySchool
Stamey StoreLUSTFacility ID: 12004
Lewis Service StationLUST TRUSTFacility ID: 12873
Commercial
Location of crushed asphalt,household trash, constructiondebris, railroad ties
(3) Former 1,000-Gal. Gasoline USTs
Former 1,000-Gal. Kerosene UST
Former 1,000-Gal. Gasoline USTs(abandoned in place)Former 1,000-Gal. Gasoline USTs(abandoned in place)
550-Gal. GasolineUST (not in use)550-Gal. GasolineUST (not in use)
Fallston SalesLUST, IMFacility ID: 16105
Abandoned-in-place 550-Gal. Kerosene UST
UST (Unknown capacity)
SB-1 (Temporary Well (TMW-1) & Soil Sample)
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the
GIS User Community
0 6030
Feet
Path: H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Figures\Figure 4 - Sampled Wells.mxdFIGURE NO.4Groundwater Analytical DataSummaryIssue Date:Project No:Sheet Size:Designed By:Drawn By:Reviewed By:08/23/2018SIR8000.P211x17AJHBOBSCMRevisionsNo.DateNorth
Legend
Type III Monitoring
Well
Type II Monitoring
Well
Temporary Well & Soil
Boring
UST
Approx. Site Boundary
4726 Fallston RoadFallston, North Carolina
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
TABLES
TABLE 1: Soil Boring SummaryFormer Stamey Stores, Inc. Property4726 Fallston RoadFallston, NCBoring Designation Sample Description Total Boring Depth (ft bgs)Depth to Groundwater (ft bgs)Maximum Field Screening Results (ppm) / Depth (ft bgs)Sample MatrixSoil Sample Depth (ft bgs)HA-1Located west of the Site building down-gradient of the western adjacent properties.14 NE 0.9 / 0-1 Soil 13-14HA-2Located near the southern exterior wall near an abandoned-in-place underground storage tank.16 NE909.1 / 7-8 Soil7-8SB-1Located on the southern portion of the Site in a suspected up-gradient location.30 23 1.0 / 1.5 Soil & Groudwater 20-21Notes:ft bgs = feet below ground surfaceNE: Not Encounteredppm = parts per millionH:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Tables\Data Tables_v2
Table 2: Soil Analytical Data Summary
Former Stamey Stores, Inc. Property
4726 Fallston Road
Fallston, NC

Sample ID:
EPA
Residential
SSL [1]
NCDEQ MSCCs
Residential
Soil Cleanup
Levels [2]
HA-1
(13-14)
HA-2
(7-8)SB-1
Acenaphthene 3,600,000 940,000 < 12.0 39.1 < 12.3
Anthracene 18,000,000 4,600,000 < 12.0 5.2 J < 12.3
Fluorene 2,400,000 620,000 < 12.0 41.3 < 12.3
1-Methylnaphthalene 18,000 20,000 < 12.0 461 < 12.3
2-Methylnaphthalene 240,000 63,000 < 12.0 557 < 12.3
Naphthalene 3,800 313,000 < 12.0 334 < 12.3
Phenanthrene NE 469,000 < 12.0 17.5 < 12.3
Acetone 61,000,000 14,000,000 < 91.1 232 < 109
n-Butylbenzene 3,900,000 626,000 < 4.6 7,330 < 5.4
sec-Butylbenzene 7,800,000 626,000 < 4.6 4,440 < 5.4
Ethylbenzene 5,800 626,000.0 < 4.6 1,210 < 5.4
p-Isopropylbenzene (Cumene) 1,900,000 1,564,000 < 4.6 1,490 < 5.4
p-Isopropyltoluene NE 100,000 < 4.6 7,760 < 5.4
Methylene Chloride 57,000 85,000 < 18.2 38.7 < 21.7
Naphthalene 3,800 313,000 < 4.6 7,120 10.1
n-Propylbenzene 3,800,000 626,000 < 4.6 3,340 < 5.4
1,2,4-Trimethylbenzene 300,000 782,000 < 4.6 29,700 < 5.4
1,3,5-Trimethylbenzene 270,000 782,000 < 4.6 6,810 < 5.4
Xylene (Total) 580,000 3,129,000 < 9.1 3,790 < 10.9
Notes:
PAHs - polycyclic aromatic hydrocarbons
VOCs - volatile organic compounds
- Bolded values indicate laboratory detections above the laboratory detection limits.
- Shaded values indicate exceedance of the EPA RSLs.
NE - Not Established
< - less than the laboratory detection limit.
- J values indicate estimated concentrations above the laboratory detection limit, but below the laboratory reporting
li it
VOCs (µg/kg)
PAHs (µg/kg)
[1] US Environmental Protection Agency (USEPA) Regional Screening Levels (RSLs) Residential Soil Screening
Levels (May 2018)
[*] North Carolina Department of Environmental Quality Maximum Soil Contaminant Concentration Levels
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Tables\Data Tables_v2-
Table 3: Groundwater Analytical Data Summary Former Stamey Stores, Inc. Property4726 Fallston RoadFallston, NCSample ID:EPA MCL[1]NCDEQ 2L Standards [2]TMW-1 MW-4 SE-MW-4 MW-5AnthraceneNE 2000 <0.050 <0.050 <0.0500.271-MethylnaphthaleneNE NE <2.0 <2.0 <2.037.62-MethylnaphthaleneNE 30 <2.0 <2.0 <2.038.1NaphthaleneNE 6 <1.5 <1.5 <1.558.2Benzene51< 1.0 < 1.0 < 1.0585ChloromethaneNE33.7 0.59 J 0.52 J< 4.01,2-Dichloroethane5 0.4< 1.0 < 1.0 < 1.073.0Diisopropyl etherNE NE< 1.0 < 1.0 < 1.026.12-HexanoneNE NE18.8< 5.0 < 5.0 < 20p-IsopropyltolueneNENE< 1.0 < 1.0 < 1.011.5Methyl Tertiary-butyl Ether (MTBE)NE20< 1.0 < 1.0 < 1.0519NaphthaleneNE6< 1.0 < 1.0 < 1.071.1Xylenes (total)10,000500< 1.0 < 1.0 < 1.030.5[2] North Carolina Department of Environmental Quality 15A NCAC 02L .0202 Groundwater Quality Standards Class GA Standards- Bold values indicate laboratory detections above the laboratory detection limits.- NE - Not Established- VOCs - Volatile Organic Compounds- PAHs - Polycyclic Aromatic Hyrdocarbons< - less than the laboratory method detection limit.- TMW - Temporary Monitoring Well- µg/L - micrograms per liter (also known as parts per billion)- 'J' values indicate estimated concentrations above the method detection limit, but below the laboratory reporting limit[1] Environmental Protection Agency (EPA) Maximum Contaminant Levels (May 2018)PAHs (µg/L)VOCs (µg/L)H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Tables\Data Tables_v2
Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx

APPENDIX A
Soil Boring Logs and Field Data Sheets

Limited Phase 2 ESA
Sirron Preservation, LLC
4726 Fallston Road
Fallston, NC
H:\S\Sirron Preservation\SIR8000.P2 - 4726 Fallston Rd, Fallston NC P2\05. Reports\Sirron Preservation Fallston NC P2 Report 9 20 18.docx
APPENDIX B
Laboratory Analytical Report
#=CL#
September 10, 2018
LIMS USE: FR - ANTHONY
LIMS OBJECT ID: 92396262
92396262
Project:
Pace Project No.:
RE:
Anthony Herrmann
HRP Associates
1327 Miller Rd.
Greenville, SC 29609
SIRRON P2
Dear Anthony Herrmann:
Enclosed are the analytical results for sample(s) received by the laboratory between August 17,
2018 and August 20, 2018. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Daniel McDonnell, HRP Associates
EDD and Report, HRP Associates
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 54
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92396262
SIRRON P2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 54
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92396262
SIRRON P2
Lab ID Sample ID Matrix Date Collected Date Received
92396262001 HA-1 (13-14)Solid 08/16/18 11:45 08/17/18 11:32
92396262002 HA-2 (7-8)Solid 08/16/18 15:50 08/17/18 11:32
92396262003 SB-1 (20-21)Solid 08/16/18 12:55 08/17/18 11:32
92396262004 TMW-1 Water 08/16/18 17:00 08/17/18 11:32
92396262005 MW-4 Water 08/16/18 20:43 08/17/18 11:32
92396262006 SE-MW-4 Water 08/16/18 20:15 08/17/18 11:32
92396262007 MW-5 Water 08/16/18 18:28 08/17/18 11:32
92396262008 TCLP Solid 08/16/18 21:00 08/20/18 12:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 54
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92396262
SIRRON P2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92396262001 HA-1 (13-14)EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92396262002 HA-2 (7-8)EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92396262003 SB-1 (20-21)EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92396262004 TMW-1 EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 63 PASI-CGAW
92396262005 MW-4 EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 63 PASI-CGAW
92396262006 SE-MW-4 EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 63 PASI-CGAW
92396262007 MW-5 EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 54
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92396262
SIRRON P2
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92396262001 HA-1 (13-14)
Percent Moisture 17.1 %08/20/18 12:200.10ASTM D2974-87
92396262002 HA-2 (7-8)
Acenaphthene 39.1 ug/kg 08/25/18 11:0212.9EPA 8270D by SIM
Anthracene 5.2J ug/kg 08/25/18 11:0212.9EPA 8270D by SIM
Fluorene 41.3 ug/kg 08/25/18 11:0212.9EPA 8270D by SIM
1-Methylnaphthalene 461 ug/kg 08/25/18 11:02 D612.9EPA 8270D by SIM
2-Methylnaphthalene 557 ug/kg 08/25/18 11:02 D612.9EPA 8270D by SIM
Naphthalene 334 ug/kg 08/25/18 11:02 D612.9EPA 8270D by SIM
Phenanthrene 17.5 ug/kg 08/25/18 11:0212.9EPA 8270D by SIM
Acetone 232 ug/kg 08/21/18 15:08122EPA 8260B
n-Butylbenzene 7330 ug/kg 08/21/18 23:31305EPA 8260B
sec-Butylbenzene 4440 ug/kg 08/21/18 23:31305EPA 8260B
Ethylbenzene 1210 ug/kg 08/21/18 23:31305EPA 8260B
Isopropylbenzene (Cumene)1490 ug/kg 08/21/18 23:31305EPA 8260B
p-Isopropyltoluene 7760 ug/kg 08/21/18 23:31305EPA 8260B
Methylene Chloride 38.7 ug/kg 08/21/18 15:08 C924.4EPA 8260B
Naphthalene 7120 ug/kg 08/21/18 23:31305EPA 8260B
n-Propylbenzene 3340 ug/kg 08/21/18 23:31305EPA 8260B
1,2,4-Trimethylbenzene 29700 ug/kg 08/22/18 13:341220EPA 8260B
1,3,5-Trimethylbenzene 6810 ug/kg 08/21/18 23:31305EPA 8260B
Xylene (Total)3790 ug/kg 08/21/18 23:31610EPA 8260B
m&p-Xylene 2940 ug/kg 08/21/18 23:31610EPA 8260B
o-Xylene 851 ug/kg 08/21/18 23:31305EPA 8260B
Percent Moisture 22.7 %08/20/18 12:200.10ASTM D2974-87
92396262003 SB-1 (20-21)
Naphthalene 10.1 ug/kg 08/21/18 15:28 M15.4EPA 8260B
Percent Moisture 18.4 %08/20/18 12:200.10ASTM D2974-87
92396262004 TMW-1
Chloromethane 3.7 ug/L 08/24/18 10:561.0EPA 8260B
2-Hexanone 18.8 ug/L 08/24/18 10:565.0EPA 8260B
92396262005 MW-4
Chloromethane 0.59J ug/L 08/23/18 16:111.0EPA 8260B
92396262006 SE-MW-4
Chloromethane 0.52J ug/L 08/23/18 16:281.0EPA 8260B
92396262007 MW-5
Anthracene 0.27 ug/L 09/08/18 19:020.25EPA 8270D by SIM
1-Methylnaphthalene 37.6 ug/L 09/08/18 19:0210.0EPA 8270D by SIM
2-Methylnaphthalene 38.1 ug/L 09/08/18 19:02 D310.0EPA 8270D by SIM
Naphthalene 58.2 ug/L 09/08/18 19:027.5EPA 8270D by SIM
Benzene 585 ug/L 08/24/18 11:29 M14.0EPA 8260B
1,2-Dichloroethane 73.0 ug/L 08/24/18 11:294.0EPA 8260B
Diisopropyl ether 26.1 ug/L 08/24/18 11:294.0EPA 8260B
p-Isopropyltoluene 11.5 ug/L 08/24/18 11:294.0EPA 8260B
Methyl-tert-butyl ether 519 ug/L 08/24/18 11:29 M14.0EPA 8260B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 54
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92396262
SIRRON P2
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92396262007 MW-5
Naphthalene 71.1 ug/L 08/24/18 11:294.0EPA 8260B
Xylene (Total)30.5 ug/L 08/24/18 11:294.0EPA 8260B
m&p-Xylene 5.4J ug/L 08/24/18 11:298.0EPA 8260B
o-Xylene 30.5 ug/L 08/24/18 11:294.0EPA 8260B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:HA-1 (13-14)Lab ID:92396262001 Collected:08/16/18 11:45 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 08/25/18 10:16 83-32-908/21/18 14:4112.0 1.8 1
Acenaphthylene ND ug/kg 08/25/18 10:16 208-96-808/21/18 14:4112.0 1.6 1
Anthracene ND ug/kg 08/25/18 10:16 120-12-708/21/18 14:4112.0 1.7 1
Benzo(a)anthracene ND ug/kg 08/25/18 10:16 56-55-308/21/18 14:4112.0 0.85 1
Benzo(a)pyrene ND ug/kg 08/25/18 10:16 50-32-808/21/18 14:4112.0 1.3 1
Benzo(b)fluoranthene ND ug/kg 08/25/18 10:16 205-99-208/21/18 14:4112.0 0.80 1
Benzo(g,h,i)perylene ND ug/kg 08/25/18 10:16 191-24-208/21/18 14:4112.0 3.1 1
Benzo(k)fluoranthene ND ug/kg 08/25/18 10:16 207-08-908/21/18 14:4112.0 1.8 1
Chrysene ND ug/kg 08/25/18 10:16 218-01-908/21/18 14:4112.0 2.2 1
Dibenz(a,h)anthracene ND ug/kg 08/25/18 10:16 53-70-308/21/18 14:4112.0 2.2 1
Fluoranthene ND ug/kg 08/25/18 10:16 206-44-008/21/18 14:4112.0 0.99 1
Fluorene ND ug/kg 08/25/18 10:16 86-73-708/21/18 14:4112.0 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/25/18 10:16 193-39-508/21/18 14:4112.0 3.4 1
1-Methylnaphthalene ND ug/kg 08/25/18 10:16 90-12-008/21/18 14:4112.0 1.4 1
2-Methylnaphthalene ND ug/kg 08/25/18 10:16 91-57-608/21/18 14:4112.0 1.3 1
Naphthalene ND ug/kg 08/25/18 10:16 91-20-308/21/18 14:4112.0 2.8 1
Phenanthrene ND ug/kg 08/25/18 10:16 85-01-808/21/18 14:4112.0 1.8 1
Pyrene ND ug/kg 08/25/18 10:16 129-00-008/21/18 14:4112.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)73 %08/25/18 10:16 4165-60-008/21/18 14:4110-128 1
2-Fluorobiphenyl (S)55 %08/25/18 10:16 321-60-808/21/18 14:4110-110 1
Terphenyl-d14 (S)85 %08/25/18 10:16 1718-51-008/21/18 14:4139-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
Acetone ND ug/kg 08/21/18 14:49 67-64-108/20/18 13:4491.1 9.1 1
Benzene ND ug/kg 08/21/18 14:49 71-43-208/20/18 13:444.6 1.5 1
Bromobenzene ND ug/kg 08/21/18 14:49 108-86-108/20/18 13:444.6 1.8 1
Bromochloromethane ND ug/kg 08/21/18 14:49 74-97-508/20/18 13:444.6 1.5 1
Bromodichloromethane ND ug/kg 08/21/18 14:49 75-27-408/20/18 13:444.6 1.7 1
Bromoform ND ug/kg 08/21/18 14:49 75-25-208/20/18 13:444.6 2.1 1
Bromomethane ND ug/kg 08/21/18 14:49 74-83-908/20/18 13:449.1 2.3 1
2-Butanone (MEK)ND ug/kg 08/21/18 14:49 78-93-308/20/18 13:4491.1 2.6 1
n-Butylbenzene ND ug/kg 08/21/18 14:49 104-51-808/20/18 13:444.6 1.6 1
sec-Butylbenzene ND ug/kg 08/21/18 14:49 135-98-808/20/18 13:444.6 1.5 1
tert-Butylbenzene ND ug/kg 08/21/18 14:49 98-06-608/20/18 13:444.6 1.8 1
Carbon tetrachloride ND ug/kg 08/21/18 14:49 56-23-508/20/18 13:444.6 2.4 1
Chlorobenzene ND ug/kg 08/21/18 14:49 108-90-708/20/18 13:444.6 1.7 1
Chloroethane ND ug/kg 08/21/18 14:49 75-00-308/20/18 13:449.1 2.2 1
Chloroform ND ug/kg 08/21/18 14:49 67-66-308/20/18 13:444.6 1.5 1
Chloromethane ND ug/kg 08/21/18 14:49 74-87-308/20/18 13:449.1 2.2 1
2-Chlorotoluene ND ug/kg 08/21/18 14:49 95-49-808/20/18 13:444.6 1.5 1
4-Chlorotoluene ND ug/kg 08/21/18 14:49 106-43-408/20/18 13:444.6 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/18 14:49 96-12-808/20/18 13:444.6 3.3 1
Dibromochloromethane ND ug/kg 08/21/18 14:49 124-48-108/20/18 13:444.6 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/18 14:49 106-93-408/20/18 13:444.6 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:HA-1 (13-14)Lab ID:92396262001 Collected:08/16/18 11:45 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
Dibromomethane ND ug/kg 08/21/18 14:49 74-95-308/20/18 13:444.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 08/21/18 14:49 95-50-108/20/18 13:444.6 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/21/18 14:49 541-73-108/20/18 13:444.6 1.8 1
1,4-Dichlorobenzene ND ug/kg 08/21/18 14:49 106-46-708/20/18 13:444.6 1.5 1
Dichlorodifluoromethane ND ug/kg 08/21/18 14:49 75-71-808/20/18 13:449.1 3.3 1
1,1-Dichloroethane ND ug/kg 08/21/18 14:49 75-34-308/20/18 13:444.6 1.4 1
1,2-Dichloroethane ND ug/kg 08/21/18 14:49 107-06-208/20/18 13:444.6 2.0 1
1,1-Dichloroethene ND ug/kg 08/21/18 14:49 75-35-408/20/18 13:444.6 1.6 1
cis-1,2-Dichloroethene ND ug/kg 08/21/18 14:49 156-59-208/20/18 13:444.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 08/21/18 14:49 156-60-508/20/18 13:444.6 1.7 1
1,2-Dichloropropane ND ug/kg 08/21/18 14:49 78-87-508/20/18 13:444.6 1.5 1
1,3-Dichloropropane ND ug/kg 08/21/18 14:49 142-28-908/20/18 13:444.6 1.7 1
2,2-Dichloropropane ND ug/kg 08/21/18 14:49 594-20-708/20/18 13:444.6 1.5 1
1,1-Dichloropropene ND ug/kg 08/21/18 14:49 563-58-608/20/18 13:444.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 08/21/18 14:49 10061-01-508/20/18 13:444.6 1.6 1
trans-1,3-Dichloropropene ND ug/kg 08/21/18 14:49 10061-02-608/20/18 13:444.6 1.4 1
Diisopropyl ether ND ug/kg 08/21/18 14:49 108-20-308/20/18 13:444.6 1.5 1
Ethylbenzene ND ug/kg 08/21/18 14:49 100-41-408/20/18 13:444.6 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/18 14:49 87-68-308/20/18 13:444.6 1.8 1
2-Hexanone ND ug/kg 08/21/18 14:49 591-78-608/20/18 13:4445.5 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/18 14:49 98-82-808/20/18 13:444.6 1.7 1
p-Isopropyltoluene ND ug/kg 08/21/18 14:49 99-87-608/20/18 13:444.6 1.5 1
Methylene Chloride ND ug/kg 08/21/18 14:49 75-09-208/20/18 13:4418.2 2.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/18 14:49 108-10-108/20/18 13:4445.5 3.4 1
Methyl-tert-butyl ether ND ug/kg 08/21/18 14:49 1634-04-408/20/18 13:444.6 1.4 1
Naphthalene ND ug/kg 08/21/18 14:49 91-20-308/20/18 13:444.6 1.1 1
n-Propylbenzene ND ug/kg 08/21/18 14:49 103-65-108/20/18 13:444.6 1.5 1
Styrene ND ug/kg 08/21/18 14:49 100-42-508/20/18 13:444.6 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/18 14:49 630-20-608/20/18 13:444.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/18 14:49 79-34-508/20/18 13:444.6 1.7 1
Tetrachloroethene ND ug/kg 08/21/18 14:49 127-18-408/20/18 13:444.6 1.5 1
Toluene ND ug/kg 08/21/18 14:49 108-88-308/20/18 13:444.6 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/18 14:49 87-61-608/20/18 13:444.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/18 14:49 120-82-108/20/18 13:444.6 1.5 1
1,1,1-Trichloroethane ND ug/kg 08/21/18 14:49 71-55-608/20/18 13:444.6 1.6 1
1,1,2-Trichloroethane ND ug/kg 08/21/18 14:49 79-00-508/20/18 13:444.6 1.9 1
Trichloroethene ND ug/kg 08/21/18 14:49 79-01-608/20/18 13:444.6 1.9 1
Trichlorofluoromethane ND ug/kg 08/21/18 14:49 75-69-408/20/18 13:444.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 08/21/18 14:49 96-18-408/20/18 13:444.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/18 14:49 95-63-608/20/18 13:444.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/18 14:49 108-67-808/20/18 13:444.6 1.6 1
Vinyl acetate ND ug/kg 08/21/18 14:49 108-05-408/20/18 13:4445.5 8.0 1
Vinyl chloride ND ug/kg 08/21/18 14:49 75-01-408/20/18 13:449.1 1.6 1
Xylene (Total)ND ug/kg 08/21/18 14:49 1330-20-708/20/18 13:449.1 3.3 1
m&p-Xylene ND ug/kg 08/21/18 14:49 179601-23-108/20/18 13:449.1 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:HA-1 (13-14)Lab ID:92396262001 Collected:08/16/18 11:45 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
o-Xylene ND ug/kg 08/21/18 14:49 95-47-608/20/18 13:444.6 1.7 1
Surrogates
Toluene-d8 (S)102 %08/21/18 14:49 2037-26-508/20/18 13:4470-130 1
4-Bromofluorobenzene (S)100 %08/21/18 14:49 460-00-408/20/18 13:4470-130 1
1,2-Dichloroethane-d4 (S)121 %08/21/18 14:49 17060-07-008/20/18 13:4470-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.1 %08/20/18 12:200.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:HA-2 (7-8)Lab ID:92396262002 Collected:08/16/18 15:50 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 39.1 ug/kg 08/25/18 11:02 83-32-908/21/18 14:4112.9 1.9 1
Acenaphthylene ND ug/kg 08/25/18 11:02 208-96-808/21/18 14:4112.9 1.7 1
Anthracene 5.2J ug/kg 08/25/18 11:02 120-12-708/21/18 14:4112.9 1.8 1
Benzo(a)anthracene ND ug/kg 08/25/18 11:02 56-55-308/21/18 14:4112.9 0.91 1
Benzo(a)pyrene ND ug/kg 08/25/18 11:02 50-32-808/21/18 14:4112.9 1.4 1
Benzo(b)fluoranthene ND ug/kg 08/25/18 11:02 205-99-208/21/18 14:4112.9 0.86 1
Benzo(g,h,i)perylene ND ug/kg 08/25/18 11:02 191-24-208/21/18 14:4112.9 3.3 1
Benzo(k)fluoranthene ND ug/kg 08/25/18 11:02 207-08-908/21/18 14:4112.9 1.9 1
Chrysene ND ug/kg 08/25/18 11:02 218-01-908/21/18 14:4112.9 2.3 1
Dibenz(a,h)anthracene ND ug/kg 08/25/18 11:02 53-70-308/21/18 14:4112.9 2.3 1
Fluoranthene ND ug/kg 08/25/18 11:02 206-44-008/21/18 14:4112.9 1.1 1
Fluorene 41.3 ug/kg 08/25/18 11:02 86-73-708/21/18 14:4112.9 2.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/25/18 11:02 193-39-508/21/18 14:4112.9 3.6 1
1-Methylnaphthalene 461 ug/kg 08/25/18 11:02 90-12-0 D608/21/18 14:4112.9 1.5 1
2-Methylnaphthalene 557 ug/kg 08/25/18 11:02 91-57-6 D608/21/18 14:4112.9 1.4 1
Naphthalene 334 ug/kg 08/25/18 11:02 91-20-3 D608/21/18 14:4112.9 3.0 1
Phenanthrene 17.5 ug/kg 08/25/18 11:02 85-01-808/21/18 14:4112.9 1.9 1
Pyrene ND ug/kg 08/25/18 11:02 129-00-008/21/18 14:4112.9 2.3 1
Surrogates
Nitrobenzene-d5 (S)0 %08/25/18 11:02 4165-60-0 S208/21/18 14:4110-128 1
2-Fluorobiphenyl (S)30 %08/25/18 11:02 321-60-808/21/18 14:4110-110 1
Terphenyl-d14 (S)44 %08/25/18 11:02 1718-51-008/21/18 14:4139-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
Acetone 232 ug/kg 08/21/18 15:08 67-64-108/20/18 13:4412212.2 1
Benzene ND ug/kg 08/21/18 15:08 71-43-208/20/18 13:446.1 2.0 1
Bromobenzene ND ug/kg 08/21/18 15:08 108-86-108/20/18 13:446.1 2.4 1
Bromochloromethane ND ug/kg 08/21/18 15:08 74-97-508/20/18 13:446.1 2.1 1
Bromodichloromethane ND ug/kg 08/21/18 15:08 75-27-408/20/18 13:446.1 2.3 1
Bromoform ND ug/kg 08/21/18 15:08 75-25-208/20/18 13:446.1 2.8 1
Bromomethane ND ug/kg 08/21/18 15:08 74-83-908/20/18 13:4412.2 3.1 1
2-Butanone (MEK)ND ug/kg 08/21/18 15:08 78-93-308/20/18 13:441223.5 1
n-Butylbenzene 7330 ug/kg 08/21/18 23:31 104-51-808/20/18 13:4430511050
sec-Butylbenzene 4440 ug/kg 08/21/18 23:31 135-98-808/20/18 13:4430597.7 50
tert-Butylbenzene ND ug/kg 08/21/18 15:08 98-06-608/20/18 13:446.1 2.4 1
Carbon tetrachloride ND ug/kg 08/21/18 15:08 56-23-508/20/18 13:446.1 3.2 1
Chlorobenzene ND ug/kg 08/21/18 15:08 108-90-708/20/18 13:446.1 2.3 1
Chloroethane ND ug/kg 08/21/18 15:08 75-00-308/20/18 13:4412.2 2.9 1
Chloroform ND ug/kg 08/21/18 15:08 67-66-308/20/18 13:446.1 2.0 1
Chloromethane ND ug/kg 08/21/18 15:08 74-87-308/20/18 13:4412.2 2.9 1
2-Chlorotoluene ND ug/kg 08/21/18 15:08 95-49-808/20/18 13:446.1 2.1 1
4-Chlorotoluene ND ug/kg 08/21/18 15:08 106-43-408/20/18 13:446.1 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/18 15:08 96-12-808/20/18 13:446.1 4.4 1
Dibromochloromethane ND ug/kg 08/21/18 15:08 124-48-108/20/18 13:446.1 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/18 15:08 106-93-408/20/18 13:446.1 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:HA-2 (7-8)Lab ID:92396262002 Collected:08/16/18 15:50 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
Dibromomethane ND ug/kg 08/21/18 15:08 74-95-308/20/18 13:446.1 3.1 1
1,2-Dichlorobenzene ND ug/kg 08/21/18 15:08 95-50-108/20/18 13:446.1 2.3 1
1,3-Dichlorobenzene ND ug/kg 08/21/18 15:08 541-73-108/20/18 13:446.1 2.4 1
1,4-Dichlorobenzene ND ug/kg 08/21/18 15:08 106-46-708/20/18 13:446.1 2.1 1
Dichlorodifluoromethane ND ug/kg 08/21/18 15:08 75-71-808/20/18 13:4412.2 4.4 1
1,1-Dichloroethane ND ug/kg 08/21/18 15:08 75-34-308/20/18 13:446.1 1.8 1
1,2-Dichloroethane ND ug/kg 08/21/18 15:08 107-06-208/20/18 13:446.1 2.7 1
1,1-Dichloroethene ND ug/kg 08/21/18 15:08 75-35-408/20/18 13:446.1 2.2 1
cis-1,2-Dichloroethene ND ug/kg 08/21/18 15:08 156-59-208/20/18 13:446.1 1.7 1
trans-1,2-Dichloroethene ND ug/kg 08/21/18 15:08 156-60-508/20/18 13:446.1 2.3 1
1,2-Dichloropropane ND ug/kg 08/21/18 15:08 78-87-508/20/18 13:446.1 2.1 1
1,3-Dichloropropane ND ug/kg 08/21/18 15:08 142-28-908/20/18 13:446.1 2.3 1
2,2-Dichloropropane ND ug/kg 08/21/18 15:08 594-20-708/20/18 13:446.1 2.1 1
1,1-Dichloropropene ND ug/kg 08/21/18 15:08 563-58-608/20/18 13:446.1 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/21/18 15:08 10061-01-508/20/18 13:446.1 2.2 1
trans-1,3-Dichloropropene ND ug/kg 08/21/18 15:08 10061-02-608/20/18 13:446.1 1.8 1
Diisopropyl ether ND ug/kg 08/21/18 15:08 108-20-308/20/18 13:446.1 2.1 1
Ethylbenzene 1210 ug/kg 08/21/18 23:31 100-41-408/20/18 13:4430511050
Hexachloro-1,3-butadiene ND ug/kg 08/21/18 15:08 87-68-308/20/18 13:446.1 2.4 1
2-Hexanone ND ug/kg 08/21/18 15:08 591-78-608/20/18 13:4461.0 4.8 1
Isopropylbenzene (Cumene)1490 ug/kg 08/21/18 23:31 98-82-808/20/18 13:4430511650
p-Isopropyltoluene 7760 ug/kg 08/21/18 23:31 99-87-608/20/18 13:4430510450
Methylene Chloride 38.7 ug/kg 08/21/18 15:08 75-09-2 C908/20/18 13:4424.4 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/18 15:08 108-10-108/20/18 13:4461.0 4.5 1
Methyl-tert-butyl ether ND ug/kg 08/21/18 15:08 1634-04-408/20/18 13:446.1 1.8 1
Naphthalene 7120 ug/kg 08/21/18 23:31 91-20-308/20/18 13:4430573.3 50
n-Propylbenzene 3340 ug/kg 08/21/18 23:31 103-65-108/20/18 13:4430510450
Styrene ND ug/kg 08/21/18 15:08 100-42-508/20/18 13:446.1 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/18 15:08 630-20-608/20/18 13:446.1 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/18 15:08 79-34-508/20/18 13:446.1 2.3 1
Tetrachloroethene ND ug/kg 08/21/18 15:08 127-18-408/20/18 13:446.1 2.1 1
Toluene ND ug/kg 08/21/18 15:08 108-88-308/20/18 13:446.1 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/18 15:08 87-61-608/20/18 13:446.1 2.7 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/18 15:08 120-82-108/20/18 13:446.1 2.0 1
1,1,1-Trichloroethane ND ug/kg 08/21/18 15:08 71-55-608/20/18 13:446.1 2.2 1
1,1,2-Trichloroethane ND ug/kg 08/21/18 15:08 79-00-508/20/18 13:446.1 2.6 1
Trichloroethene ND ug/kg 08/21/18 15:08 79-01-608/20/18 13:446.1 2.6 1
Trichlorofluoromethane ND ug/kg 08/21/18 15:08 75-69-408/20/18 13:446.1 2.7 1
1,2,3-Trichloropropane ND ug/kg 08/21/18 15:08 96-18-408/20/18 13:446.1 2.0 1
1,2,4-Trimethylbenzene 29700 ug/kg 08/22/18 13:34 95-63-608/20/18 13:441220488200
1,3,5-Trimethylbenzene 6810 ug/kg 08/21/18 23:31 108-67-808/20/18 13:4430511050
Vinyl acetate ND ug/kg 08/21/18 15:08 108-05-408/20/18 13:4461.0 10.7 1
Vinyl chloride ND ug/kg 08/21/18 15:08 75-01-408/20/18 13:4412.2 2.2 1
Xylene (Total)3790 ug/kg 08/21/18 23:31 1330-20-708/20/18 13:4461022050
m&p-Xylene 2940 ug/kg 08/21/18 23:31 179601-23-108/20/18 13:4461022050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:HA-2 (7-8)Lab ID:92396262002 Collected:08/16/18 15:50 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
o-Xylene 851 ug/kg 08/21/18 23:31 95-47-608/20/18 13:4430511650
Surrogates
Toluene-d8 (S)145 %08/21/18 15:08 2037-26-5 IO,S108/20/18 13:4470-130 1
4-Bromofluorobenzene (S)541 %08/21/18 15:08 460-00-4 S108/20/18 13:4470-130 1
1,2-Dichloroethane-d4 (S)172 %08/21/18 15:08 17060-07-0 S108/20/18 13:4470-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.7 %08/20/18 12:200.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:SB-1 (20-21)Lab ID:92396262003 Collected:08/16/18 12:55 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 08/25/18 11:49 83-32-908/21/18 14:4112.3 1.8 1
Acenaphthylene ND ug/kg 08/25/18 11:49 208-96-808/21/18 14:4112.3 1.6 1
Anthracene ND ug/kg 08/25/18 11:49 120-12-708/21/18 14:4112.3 1.7 1
Benzo(a)anthracene ND ug/kg 08/25/18 11:49 56-55-308/21/18 14:4112.3 0.88 1
Benzo(a)pyrene ND ug/kg 08/25/18 11:49 50-32-808/21/18 14:4112.3 1.4 1
Benzo(b)fluoranthene ND ug/kg 08/25/18 11:49 205-99-208/21/18 14:4112.3 0.83 1
Benzo(g,h,i)perylene ND ug/kg 08/25/18 11:49 191-24-208/21/18 14:4112.3 3.2 1
Benzo(k)fluoranthene ND ug/kg 08/25/18 11:49 207-08-908/21/18 14:4112.3 1.8 1
Chrysene ND ug/kg 08/25/18 11:49 218-01-908/21/18 14:4112.3 2.2 1
Dibenz(a,h)anthracene ND ug/kg 08/25/18 11:49 53-70-308/21/18 14:4112.3 2.2 1
Fluoranthene ND ug/kg 08/25/18 11:49 206-44-008/21/18 14:4112.3 1.0 1
Fluorene ND ug/kg 08/25/18 11:49 86-73-708/21/18 14:4112.3 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/25/18 11:49 193-39-508/21/18 14:4112.3 3.5 1
1-Methylnaphthalene ND ug/kg 08/25/18 11:49 90-12-008/21/18 14:4112.3 1.5 1
2-Methylnaphthalene ND ug/kg 08/25/18 11:49 91-57-608/21/18 14:4112.3 1.4 1
Naphthalene ND ug/kg 08/25/18 11:49 91-20-308/21/18 14:4112.3 2.8 1
Phenanthrene ND ug/kg 08/25/18 11:49 85-01-808/21/18 14:4112.3 1.8 1
Pyrene ND ug/kg 08/25/18 11:49 129-00-008/21/18 14:4112.3 2.2 1
Surrogates
Nitrobenzene-d5 (S)66 %08/25/18 11:49 4165-60-008/21/18 14:4110-128 1
2-Fluorobiphenyl (S)53 %08/25/18 11:49 321-60-808/21/18 14:4110-110 1
Terphenyl-d14 (S)65 %08/25/18 11:49 1718-51-008/21/18 14:4139-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
Acetone ND ug/kg 08/21/18 15:28 67-64-108/20/18 13:4410910.9 1
Benzene ND ug/kg 08/21/18 15:28 71-43-208/20/18 13:445.4 1.7 1
Bromobenzene ND ug/kg 08/21/18 15:28 108-86-108/20/18 13:445.4 2.2 1
Bromochloromethane ND ug/kg 08/21/18 15:28 74-97-508/20/18 13:445.4 1.8 1
Bromodichloromethane ND ug/kg 08/21/18 15:28 75-27-408/20/18 13:445.4 2.1 1
Bromoform ND ug/kg 08/21/18 15:28 75-25-208/20/18 13:445.4 2.5 1
Bromomethane ND ug/kg 08/21/18 15:28 74-83-908/20/18 13:4410.9 2.7 1
2-Butanone (MEK)ND ug/kg 08/21/18 15:28 78-93-308/20/18 13:441093.1 1
n-Butylbenzene ND ug/kg 08/21/18 15:28 104-51-808/20/18 13:445.4 2.0 1
sec-Butylbenzene ND ug/kg 08/21/18 15:28 135-98-808/20/18 13:445.4 1.7 1
tert-Butylbenzene ND ug/kg 08/21/18 15:28 98-06-608/20/18 13:445.4 2.2 1
Carbon tetrachloride ND ug/kg 08/21/18 15:28 56-23-508/20/18 13:445.4 2.8 1
Chlorobenzene ND ug/kg 08/21/18 15:28 108-90-708/20/18 13:445.4 2.1 1
Chloroethane ND ug/kg 08/21/18 15:28 75-00-308/20/18 13:4410.9 2.6 1
Chloroform ND ug/kg 08/21/18 15:28 67-66-308/20/18 13:445.4 1.7 1
Chloromethane ND ug/kg 08/21/18 15:28 74-87-308/20/18 13:4410.9 2.6 1
2-Chlorotoluene ND ug/kg 08/21/18 15:28 95-49-808/20/18 13:445.4 1.8 1
4-Chlorotoluene ND ug/kg 08/21/18 15:28 106-43-408/20/18 13:445.4 2.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/18 15:28 96-12-808/20/18 13:445.4 3.9 1
Dibromochloromethane ND ug/kg 08/21/18 15:28 124-48-108/20/18 13:445.4 2.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/18 15:28 106-93-408/20/18 13:445.4 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:SB-1 (20-21)Lab ID:92396262003 Collected:08/16/18 12:55 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
Dibromomethane ND ug/kg 08/21/18 15:28 74-95-308/20/18 13:445.4 2.7 1
1,2-Dichlorobenzene ND ug/kg 08/21/18 15:28 95-50-108/20/18 13:445.4 2.1 1
1,3-Dichlorobenzene ND ug/kg 08/21/18 15:28 541-73-108/20/18 13:445.4 2.2 1
1,4-Dichlorobenzene ND ug/kg 08/21/18 15:28 106-46-708/20/18 13:445.4 1.8 1
Dichlorodifluoromethane ND ug/kg 08/21/18 15:28 75-71-808/20/18 13:4410.9 3.9 1
1,1-Dichloroethane ND ug/kg 08/21/18 15:28 75-34-308/20/18 13:445.4 1.6 1
1,2-Dichloroethane ND ug/kg 08/21/18 15:28 107-06-208/20/18 13:445.4 2.4 1
1,1-Dichloroethene ND ug/kg 08/21/18 15:28 75-35-408/20/18 13:445.4 2.0 1
cis-1,2-Dichloroethene ND ug/kg 08/21/18 15:28 156-59-208/20/18 13:445.4 1.5 1
trans-1,2-Dichloroethene ND ug/kg 08/21/18 15:28 156-60-508/20/18 13:445.4 2.1 1
1,2-Dichloropropane ND ug/kg 08/21/18 15:28 78-87-508/20/18 13:445.4 1.8 1
1,3-Dichloropropane ND ug/kg 08/21/18 15:28 142-28-908/20/18 13:445.4 2.1 1
2,2-Dichloropropane ND ug/kg 08/21/18 15:28 594-20-708/20/18 13:445.4 1.8 1
1,1-Dichloropropene ND ug/kg 08/21/18 15:28 563-58-608/20/18 13:445.4 1.6 1
cis-1,3-Dichloropropene ND ug/kg 08/21/18 15:28 10061-01-508/20/18 13:445.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 08/21/18 15:28 10061-02-608/20/18 13:445.4 1.6 1
Diisopropyl ether ND ug/kg 08/21/18 15:28 108-20-308/20/18 13:445.4 1.8 1
Ethylbenzene ND ug/kg 08/21/18 15:28 100-41-408/20/18 13:445.4 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/18 15:28 87-68-308/20/18 13:445.4 2.2 1
2-Hexanone ND ug/kg 08/21/18 15:28 591-78-608/20/18 13:4454.3 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/18 15:28 98-82-808/20/18 13:445.4 2.1 1
p-Isopropyltoluene ND ug/kg 08/21/18 15:28 99-87-608/20/18 13:445.4 1.8 1
Methylene Chloride ND ug/kg 08/21/18 15:28 75-09-208/20/18 13:4421.7 3.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/18 15:28 108-10-108/20/18 13:4454.3 4.0 1
Methyl-tert-butyl ether ND ug/kg 08/21/18 15:28 1634-04-408/20/18 13:445.4 1.6 1
Naphthalene 10.1 ug/kg 08/21/18 15:28 91-20-3 M108/20/18 13:445.4 1.3 1
n-Propylbenzene ND ug/kg 08/21/18 15:28 103-65-108/20/18 13:445.4 1.8 1
Styrene ND ug/kg 08/21/18 15:28 100-42-508/20/18 13:445.4 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/18 15:28 630-20-608/20/18 13:445.4 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/18 15:28 79-34-508/20/18 13:445.4 2.1 1
Tetrachloroethene ND ug/kg 08/21/18 15:28 127-18-408/20/18 13:445.4 1.8 1
Toluene ND ug/kg 08/21/18 15:28 108-88-308/20/18 13:445.4 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/18 15:28 87-61-608/20/18 13:445.4 2.4 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/18 15:28 120-82-108/20/18 13:445.4 1.7 1
1,1,1-Trichloroethane ND ug/kg 08/21/18 15:28 71-55-608/20/18 13:445.4 2.0 1
1,1,2-Trichloroethane ND ug/kg 08/21/18 15:28 79-00-508/20/18 13:445.4 2.3 1
Trichloroethene ND ug/kg 08/21/18 15:28 79-01-608/20/18 13:445.4 2.3 1
Trichlorofluoromethane ND ug/kg 08/21/18 15:28 75-69-408/20/18 13:445.4 2.4 1
1,2,3-Trichloropropane ND ug/kg 08/21/18 15:28 96-18-408/20/18 13:445.4 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/18 15:28 95-63-608/20/18 13:445.4 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/18 15:28 108-67-808/20/18 13:445.4 2.0 1
Vinyl acetate ND ug/kg 08/21/18 15:28 108-05-408/20/18 13:4454.3 9.6 1
Vinyl chloride ND ug/kg 08/21/18 15:28 75-01-4 M108/20/18 13:4410.9 2.0 1
Xylene (Total)ND ug/kg 08/21/18 15:28 1330-20-708/20/18 13:4410.9 3.9 1
m&p-Xylene ND ug/kg 08/21/18 15:28 179601-23-108/20/18 13:4410.9 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:SB-1 (20-21)Lab ID:92396262003 Collected:08/16/18 12:55 Received:08/17/18 11:32 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A SC Volatile Org
o-Xylene ND ug/kg 08/21/18 15:28 95-47-608/20/18 13:445.4 2.1 1
Surrogates
Toluene-d8 (S)97 %08/21/18 15:28 2037-26-508/20/18 13:4470-130 1
4-Bromofluorobenzene (S)100 %08/21/18 15:28 460-00-408/20/18 13:4470-130 1
1,2-Dichloroethane-d4 (S)105 %08/21/18 15:28 17060-07-008/20/18 13:4470-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.4 %08/20/18 12:200.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:TMW-1 Lab ID:92396262004 Collected:08/16/18 17:00 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35118270 Low Volume PAH SIM
Acenaphthene ND ug/L 09/08/18 17:59 83-32-908/22/18 14:170.50 0.50 1
Acenaphthylene ND ug/L 09/08/18 17:59 208-96-808/22/18 14:170.50 0.50 1
Anthracene ND ug/L 09/08/18 17:59 120-12-708/22/18 14:170.050 0.050 1
Benzo(a)anthracene ND ug/L 09/08/18 17:59 56-55-308/22/18 14:170.050 0.050 1
Benzo(a)pyrene ND ug/L 09/08/18 17:59 50-32-808/22/18 14:170.10 0.10 1
Benzo(b)fluoranthene ND ug/L 09/08/18 17:59 205-99-208/22/18 14:170.050 0.050 1
Benzo(g,h,i)perylene ND ug/L 09/08/18 17:59 191-24-2 L108/22/18 14:170.20 0.20 1
Benzo(k)fluoranthene ND ug/L 09/08/18 17:59 207-08-908/22/18 14:170.20 0.20 1
Chrysene ND ug/L 09/08/18 17:59 218-01-908/22/18 14:170.10 0.10 1
Dibenz(a,h)anthracene ND ug/L 09/08/18 17:59 53-70-3 L108/22/18 14:170.15 0.15 1
Fluoranthene ND ug/L 09/08/18 17:59 206-44-008/22/18 14:170.30 0.30 1
Fluorene ND ug/L 09/08/18 17:59 86-73-708/22/18 14:170.31 0.31 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/08/18 17:59 193-39-5 L108/22/18 14:170.050 0.050 1
1-Methylnaphthalene ND ug/L 09/08/18 17:59 90-12-008/22/18 14:172.0 2.0 1
2-Methylnaphthalene ND ug/L 09/08/18 17:59 91-57-608/22/18 14:172.0 2.0 1
Naphthalene ND ug/L 09/08/18 17:59 91-20-308/22/18 14:171.5 1.5 1
Phenanthrene ND ug/L 09/08/18 17:59 85-01-808/22/18 14:170.20 0.20 1
Pyrene ND ug/L 09/08/18 17:59 129-00-008/22/18 14:170.10 0.10 1
Surrogates
Nitrobenzene-d5 (S)116 %09/08/18 17:59 4165-60-0 H508/22/18 14:1770-130 1
2-Fluorobiphenyl (S)105 %09/08/18 17:59 321-60-808/22/18 14:1770-130 1
Terphenyl-d14 (S)56 %09/08/18 17:59 1718-51-0 S008/22/18 14:1770-130 1
Analytical Method: EPA 8260B8260 MSV Low Level SC
Acetone ND ug/L 08/24/18 10:56 67-64-125.0 10.0 1
Benzene ND ug/L 08/24/18 10:56 71-43-21.0 0.25 1
Bromobenzene ND ug/L 08/24/18 10:56 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 08/24/18 10:56 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 08/24/18 10:56 75-27-41.0 0.18 1
Bromoform ND ug/L 08/24/18 10:56 75-25-21.0 0.26 1
Bromomethane ND ug/L 08/24/18 10:56 74-83-95.0 0.29 1
2-Butanone (MEK)ND ug/L 08/24/18 10:56 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 08/24/18 10:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 08/24/18 10:56 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/24/18 10:56 75-00-31.0 0.54 1
Chloroform ND ug/L 08/24/18 10:56 67-66-31.0 0.14 1
Chloromethane 3.7 ug/L 08/24/18 10:56 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 08/24/18 10:56 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 08/24/18 10:56 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/18 10:56 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 08/24/18 10:56 124-48-11.0 0.21 1
Dibromomethane ND ug/L 08/24/18 10:56 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 08/24/18 10:56 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 08/24/18 10:56 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 08/24/18 10:56 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/24/18 10:56 75-71-81.0 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:TMW-1 Lab ID:92396262004 Collected:08/16/18 17:00 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level SC
1,1-Dichloroethane ND ug/L 08/24/18 10:56 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 08/24/18 10:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 08/24/18 10:56 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 08/24/18 10:56 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 08/24/18 10:56 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 08/24/18 10:56 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 08/24/18 10:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/24/18 10:56 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 08/24/18 10:56 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 08/24/18 10:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 08/24/18 10:56 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 08/24/18 10:56 108-20-31.0 0.12 1
1,4-Dioxane (p-Dioxane)ND ug/L 08/24/18 10:56 123-91-115078.4 1
Ethylbenzene ND ug/L 08/24/18 10:56 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/24/18 10:56 87-68-31.0 0.71 1
2-Hexanone 18.8 ug/L 08/24/18 10:56 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 08/24/18 10:56 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 08/24/18 10:56 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/18 10:56 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 08/24/18 10:56 1634-04-41.0 0.21 1
Naphthalene ND ug/L 08/24/18 10:56 91-20-31.0 0.24 1
Styrene ND ug/L 08/24/18 10:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/18 10:56 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/18 10:56 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 08/24/18 10:56 127-18-41.0 0.46 1
Toluene ND ug/L 08/24/18 10:56 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 08/24/18 10:56 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 08/24/18 10:56 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 08/24/18 10:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 08/24/18 10:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 08/24/18 10:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 08/24/18 10:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 08/24/18 10:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 08/24/18 10:56 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 08/24/18 10:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 08/24/18 10:56 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 08/24/18 10:56 179601-23-12.0 0.66 1
o-Xylene ND ug/L 08/24/18 10:56 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)104 %08/24/18 10:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %08/24/18 10:56 17060-07-070-130 1
Toluene-d8 (S)108 %08/24/18 10:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:MW-4 Lab ID:92396262005 Collected:08/16/18 20:43 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35118270 Low Volume PAH SIM
Acenaphthene ND ug/L 09/08/18 18:20 83-32-908/22/18 14:170.50 0.50 1
Acenaphthylene ND ug/L 09/08/18 18:20 208-96-808/22/18 14:170.50 0.50 1
Anthracene ND ug/L 09/08/18 18:20 120-12-708/22/18 14:170.050 0.050 1
Benzo(a)anthracene ND ug/L 09/08/18 18:20 56-55-308/22/18 14:170.050 0.050 1
Benzo(a)pyrene ND ug/L 09/08/18 18:20 50-32-808/22/18 14:170.10 0.10 1
Benzo(b)fluoranthene ND ug/L 09/08/18 18:20 205-99-208/22/18 14:170.050 0.050 1
Benzo(g,h,i)perylene ND ug/L 09/08/18 18:20 191-24-2 L108/22/18 14:170.20 0.20 1
Benzo(k)fluoranthene ND ug/L 09/08/18 18:20 207-08-908/22/18 14:170.20 0.20 1
Chrysene ND ug/L 09/08/18 18:20 218-01-908/22/18 14:170.10 0.10 1
Dibenz(a,h)anthracene ND ug/L 09/08/18 18:20 53-70-3 L108/22/18 14:170.15 0.15 1
Fluoranthene ND ug/L 09/08/18 18:20 206-44-008/22/18 14:170.30 0.30 1
Fluorene ND ug/L 09/08/18 18:20 86-73-708/22/18 14:170.31 0.31 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/08/18 18:20 193-39-5 L108/22/18 14:170.050 0.050 1
1-Methylnaphthalene ND ug/L 09/08/18 18:20 90-12-008/22/18 14:172.0 2.0 1
2-Methylnaphthalene ND ug/L 09/08/18 18:20 91-57-608/22/18 14:172.0 2.0 1
Naphthalene ND ug/L 09/08/18 18:20 91-20-308/22/18 14:171.5 1.5 1
Phenanthrene ND ug/L 09/08/18 18:20 85-01-808/22/18 14:170.20 0.20 1
Pyrene ND ug/L 09/08/18 18:20 129-00-008/22/18 14:170.10 0.10 1
Surrogates
Nitrobenzene-d5 (S)127 %09/08/18 18:20 4165-60-0 H508/22/18 14:1770-130 1
2-Fluorobiphenyl (S)115 %09/08/18 18:20 321-60-808/22/18 14:1770-130 1
Terphenyl-d14 (S)72 %09/08/18 18:20 1718-51-008/22/18 14:1770-130 1
Analytical Method: EPA 8260B8260 MSV Low Level SC
Acetone ND ug/L 08/23/18 16:11 67-64-125.0 10.0 1
Benzene ND ug/L 08/23/18 16:11 71-43-21.0 0.25 1
Bromobenzene ND ug/L 08/23/18 16:11 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 08/23/18 16:11 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 08/23/18 16:11 75-27-41.0 0.18 1
Bromoform ND ug/L 08/23/18 16:11 75-25-21.0 0.26 1
Bromomethane ND ug/L 08/23/18 16:11 74-83-95.0 0.29 1
2-Butanone (MEK)ND ug/L 08/23/18 16:11 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 08/23/18 16:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 08/23/18 16:11 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/23/18 16:11 75-00-31.0 0.54 1
Chloroform ND ug/L 08/23/18 16:11 67-66-31.0 0.14 1
Chloromethane 0.59J ug/L 08/23/18 16:11 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 08/23/18 16:11 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 08/23/18 16:11 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 08/23/18 16:11 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 08/23/18 16:11 124-48-11.0 0.21 1
Dibromomethane ND ug/L 08/23/18 16:11 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 08/23/18 16:11 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 08/23/18 16:11 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 08/23/18 16:11 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/23/18 16:11 75-71-81.0 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:MW-4 Lab ID:92396262005 Collected:08/16/18 20:43 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level SC
1,1-Dichloroethane ND ug/L 08/23/18 16:11 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 08/23/18 16:11 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 08/23/18 16:11 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 08/23/18 16:11 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 08/23/18 16:11 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 08/23/18 16:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 08/23/18 16:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/23/18 16:11 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 08/23/18 16:11 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 08/23/18 16:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 08/23/18 16:11 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 08/23/18 16:11 108-20-31.0 0.12 1
1,4-Dioxane (p-Dioxane)ND ug/L 08/23/18 16:11 123-91-115078.4 1
Ethylbenzene ND ug/L 08/23/18 16:11 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/23/18 16:11 87-68-31.0 0.71 1
2-Hexanone ND ug/L 08/23/18 16:11 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 08/23/18 16:11 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 08/23/18 16:11 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/23/18 16:11 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 08/23/18 16:11 1634-04-41.0 0.21 1
Naphthalene ND ug/L 08/23/18 16:11 91-20-31.0 0.24 1
Styrene ND ug/L 08/23/18 16:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 08/23/18 16:11 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 08/23/18 16:11 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 08/23/18 16:11 127-18-41.0 0.46 1
Toluene ND ug/L 08/23/18 16:11 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 08/23/18 16:11 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 08/23/18 16:11 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 08/23/18 16:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 08/23/18 16:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 08/23/18 16:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 08/23/18 16:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 08/23/18 16:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 08/23/18 16:11 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 08/23/18 16:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 08/23/18 16:11 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 08/23/18 16:11 179601-23-12.0 0.66 1
o-Xylene ND ug/L 08/23/18 16:11 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)104 %08/23/18 16:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %08/23/18 16:11 17060-07-070-130 1
Toluene-d8 (S)109 %08/23/18 16:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:SE-MW-4 Lab ID:92396262006 Collected:08/16/18 20:15 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35118270 Low Volume PAH SIM
Acenaphthene ND ug/L 09/08/18 18:41 83-32-908/22/18 14:170.50 0.50 1
Acenaphthylene ND ug/L 09/08/18 18:41 208-96-808/22/18 14:170.50 0.50 1
Anthracene ND ug/L 09/08/18 18:41 120-12-708/22/18 14:170.050 0.050 1
Benzo(a)anthracene ND ug/L 09/08/18 18:41 56-55-308/22/18 14:170.050 0.050 1
Benzo(a)pyrene ND ug/L 09/08/18 18:41 50-32-808/22/18 14:170.10 0.10 1
Benzo(b)fluoranthene ND ug/L 09/08/18 18:41 205-99-208/22/18 14:170.050 0.050 1
Benzo(g,h,i)perylene ND ug/L 09/08/18 18:41 191-24-2 L108/22/18 14:170.20 0.20 1
Benzo(k)fluoranthene ND ug/L 09/08/18 18:41 207-08-908/22/18 14:170.20 0.20 1
Chrysene ND ug/L 09/08/18 18:41 218-01-908/22/18 14:170.10 0.10 1
Dibenz(a,h)anthracene ND ug/L 09/08/18 18:41 53-70-3 L108/22/18 14:170.15 0.15 1
Fluoranthene ND ug/L 09/08/18 18:41 206-44-008/22/18 14:170.30 0.30 1
Fluorene ND ug/L 09/08/18 18:41 86-73-708/22/18 14:170.31 0.31 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/08/18 18:41 193-39-5 L108/22/18 14:170.050 0.050 1
1-Methylnaphthalene ND ug/L 09/08/18 18:41 90-12-008/22/18 14:172.0 2.0 1
2-Methylnaphthalene ND ug/L 09/08/18 18:41 91-57-608/22/18 14:172.0 2.0 1
Naphthalene ND ug/L 09/08/18 18:41 91-20-308/22/18 14:171.5 1.5 1
Phenanthrene ND ug/L 09/08/18 18:41 85-01-808/22/18 14:170.20 0.20 1
Pyrene ND ug/L 09/08/18 18:41 129-00-008/22/18 14:170.10 0.10 1
Surrogates
Nitrobenzene-d5 (S)107 %09/08/18 18:41 4165-60-0 H508/22/18 14:1770-130 1
2-Fluorobiphenyl (S)94 %09/08/18 18:41 321-60-808/22/18 14:1770-130 1
Terphenyl-d14 (S)43 %09/08/18 18:41 1718-51-0 S008/22/18 14:1770-130 1
Analytical Method: EPA 8260B8260 MSV Low Level SC
Acetone ND ug/L 08/23/18 16:28 67-64-125.0 10.0 1
Benzene ND ug/L 08/23/18 16:28 71-43-21.0 0.25 1
Bromobenzene ND ug/L 08/23/18 16:28 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 08/23/18 16:28 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 08/23/18 16:28 75-27-41.0 0.18 1
Bromoform ND ug/L 08/23/18 16:28 75-25-21.0 0.26 1
Bromomethane ND ug/L 08/23/18 16:28 74-83-95.0 0.29 1
2-Butanone (MEK)ND ug/L 08/23/18 16:28 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 08/23/18 16:28 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 08/23/18 16:28 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/23/18 16:28 75-00-31.0 0.54 1
Chloroform ND ug/L 08/23/18 16:28 67-66-31.0 0.14 1
Chloromethane 0.52J ug/L 08/23/18 16:28 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 08/23/18 16:28 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 08/23/18 16:28 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 08/23/18 16:28 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 08/23/18 16:28 124-48-11.0 0.21 1
Dibromomethane ND ug/L 08/23/18 16:28 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 08/23/18 16:28 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 08/23/18 16:28 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 08/23/18 16:28 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/23/18 16:28 75-71-81.0 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:SE-MW-4 Lab ID:92396262006 Collected:08/16/18 20:15 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level SC
1,1-Dichloroethane ND ug/L 08/23/18 16:28 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 08/23/18 16:28 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 08/23/18 16:28 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 08/23/18 16:28 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 08/23/18 16:28 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 08/23/18 16:28 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 08/23/18 16:28 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/23/18 16:28 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 08/23/18 16:28 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 08/23/18 16:28 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 08/23/18 16:28 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 08/23/18 16:28 108-20-31.0 0.12 1
1,4-Dioxane (p-Dioxane)ND ug/L 08/23/18 16:28 123-91-115078.4 1
Ethylbenzene ND ug/L 08/23/18 16:28 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/23/18 16:28 87-68-31.0 0.71 1
2-Hexanone ND ug/L 08/23/18 16:28 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 08/23/18 16:28 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 08/23/18 16:28 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/23/18 16:28 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 08/23/18 16:28 1634-04-41.0 0.21 1
Naphthalene ND ug/L 08/23/18 16:28 91-20-31.0 0.24 1
Styrene ND ug/L 08/23/18 16:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 08/23/18 16:28 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 08/23/18 16:28 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 08/23/18 16:28 127-18-41.0 0.46 1
Toluene ND ug/L 08/23/18 16:28 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 08/23/18 16:28 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 08/23/18 16:28 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 08/23/18 16:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 08/23/18 16:28 79-00-51.0 0.29 1
Trichloroethene ND ug/L 08/23/18 16:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 08/23/18 16:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 08/23/18 16:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 08/23/18 16:28 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 08/23/18 16:28 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 08/23/18 16:28 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 08/23/18 16:28 179601-23-12.0 0.66 1
o-Xylene ND ug/L 08/23/18 16:28 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %08/23/18 16:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %08/23/18 16:28 17060-07-070-130 1
Toluene-d8 (S)107 %08/23/18 16:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:MW-5 Lab ID:92396262007 Collected:08/16/18 18:28 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35118270 Low Volume PAH SIM
Acenaphthene ND ug/L 09/08/18 19:02 83-32-908/22/18 14:172.5 2.5 5
Acenaphthylene ND ug/L 09/08/18 19:02 208-96-808/22/18 14:172.5 2.5 5
Anthracene 0.27 ug/L 09/08/18 19:02 120-12-708/22/18 14:170.25 0.25 5
Benzo(a)anthracene ND ug/L 09/08/18 19:02 56-55-308/22/18 14:170.25 0.25 5
Benzo(a)pyrene ND ug/L 09/08/18 19:02 50-32-808/22/18 14:170.50 0.50 5
Benzo(b)fluoranthene ND ug/L 09/08/18 19:02 205-99-208/22/18 14:170.25 0.25 5
Benzo(g,h,i)perylene ND ug/L 09/08/18 19:02 191-24-2 L108/22/18 14:171.0 1.0 5
Benzo(k)fluoranthene ND ug/L 09/08/18 19:02 207-08-908/22/18 14:171.0 1.0 5
Chrysene ND ug/L 09/08/18 19:02 218-01-908/22/18 14:170.50 0.50 5
Dibenz(a,h)anthracene ND ug/L 09/08/18 19:02 53-70-3 L108/22/18 14:170.75 0.75 5
Fluoranthene ND ug/L 09/08/18 19:02 206-44-008/22/18 14:171.5 1.5 5
Fluorene ND ug/L 09/08/18 19:02 86-73-708/22/18 14:171.6 1.6 5
Indeno(1,2,3-cd)pyrene ND ug/L 09/08/18 19:02 193-39-5 L108/22/18 14:170.25 0.25 5
1-Methylnaphthalene 37.6 ug/L 09/08/18 19:02 90-12-008/22/18 14:1710.0 10.0 5
2-Methylnaphthalene 38.1 ug/L 09/08/18 19:02 91-57-6 D308/22/18 14:1710.0 10.0 5
Naphthalene 58.2 ug/L 09/08/18 19:02 91-20-308/22/18 14:177.5 7.5 5
Phenanthrene ND ug/L 09/08/18 19:02 85-01-808/22/18 14:171.0 1.0 5
Pyrene ND ug/L 09/08/18 19:02 129-00-008/22/18 14:170.50 0.50 5
Surrogates
Nitrobenzene-d5 (S)94 %09/08/18 19:02 4165-60-0 H508/22/18 14:1770-130 5
2-Fluorobiphenyl (S)79 %09/08/18 19:02 321-60-808/22/18 14:1770-130 5
Terphenyl-d14 (S)80 %09/08/18 19:02 1718-51-008/22/18 14:1770-130 5
Analytical Method: EPA 8260B8260 MSV Low Level SC
Acetone ND ug/L 08/24/18 11:29 67-64-110040.0 4
Benzene 585 ug/L 08/24/18 11:29 71-43-2 M14.0 1.0 4
Bromobenzene ND ug/L 08/24/18 11:29 108-86-14.0 1.2 4
Bromochloromethane ND ug/L 08/24/18 11:29 74-97-54.0 0.68 4
Bromodichloromethane ND ug/L 08/24/18 11:29 75-27-44.0 0.72 4
Bromoform ND ug/L 08/24/18 11:29 75-25-24.0 1.0 4
Bromomethane ND ug/L 08/24/18 11:29 74-83-920.0 1.2 4
2-Butanone (MEK)ND ug/L 08/24/18 11:29 78-93-320.0 3.8 4
Carbon tetrachloride ND ug/L 08/24/18 11:29 56-23-54.0 1.0 4
Chlorobenzene ND ug/L 08/24/18 11:29 108-90-74.0 0.92 4
Chloroethane ND ug/L 08/24/18 11:29 75-00-34.0 2.2 4
Chloroform ND ug/L 08/24/18 11:29 67-66-34.0 0.56 4
Chloromethane ND ug/L 08/24/18 11:29 74-87-34.0 0.44 4
2-Chlorotoluene ND ug/L 08/24/18 11:29 95-49-84.0 1.4 4
4-Chlorotoluene ND ug/L 08/24/18 11:29 106-43-44.0 1.2 4
1,2-Dibromo-3-chloropropane ND ug/L 08/24/18 11:29 96-12-88.0 8.0 4
Dibromochloromethane ND ug/L 08/24/18 11:29 124-48-14.0 0.84 4
Dibromomethane ND ug/L 08/24/18 11:29 74-95-34.0 0.84 4
1,2-Dichlorobenzene ND ug/L 08/24/18 11:29 95-50-14.0 1.2 4
1,3-Dichlorobenzene ND ug/L 08/24/18 11:29 541-73-14.0 0.96 4
1,4-Dichlorobenzene ND ug/L 08/24/18 11:29 106-46-74.0 1.3 4
Dichlorodifluoromethane ND ug/L 08/24/18 11:29 75-71-84.0 0.84 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92396262
SIRRON P2
Sample:MW-5 Lab ID:92396262007 Collected:08/16/18 18:28 Received:08/17/18 11:32 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level SC
1,1-Dichloroethane ND ug/L 08/24/18 11:29 75-34-34.0 1.3 4
1,2-Dichloroethane 73.0 ug/L 08/24/18 11:29 107-06-24.0 0.96 4
1,1-Dichloroethene ND ug/L 08/24/18 11:29 75-35-44.0 2.2 4
cis-1,2-Dichloroethene ND ug/L 08/24/18 11:29 156-59-24.0 0.76 4
trans-1,2-Dichloroethene ND ug/L 08/24/18 11:29 156-60-54.0 2.0 4
1,2-Dichloropropane ND ug/L 08/24/18 11:29 78-87-54.0 1.1 4
1,3-Dichloropropane ND ug/L 08/24/18 11:29 142-28-94.0 1.1 4
2,2-Dichloropropane ND ug/L 08/24/18 11:29 594-20-74.0 0.52 4
1,1-Dichloropropene ND ug/L 08/24/18 11:29 563-58-64.0 2.0 4
cis-1,3-Dichloropropene ND ug/L 08/24/18 11:29 10061-01-54.0 0.52 4
trans-1,3-Dichloropropene ND ug/L 08/24/18 11:29 10061-02-64.0 1.0 4
Diisopropyl ether 26.1 ug/L 08/24/18 11:29 108-20-34.0 0.48 4
1,4-Dioxane (p-Dioxane)ND ug/L 08/24/18 11:29 123-91-16003134
Ethylbenzene ND ug/L 08/24/18 11:29 100-41-44.0 1.2 4
Hexachloro-1,3-butadiene ND ug/L 08/24/18 11:29 87-68-34.0 2.8 4
2-Hexanone ND ug/L 08/24/18 11:29 591-78-620.0 1.8 4
p-Isopropyltoluene 11.5 ug/L 08/24/18 11:29 99-87-64.0 1.2 4
Methylene Chloride ND ug/L 08/24/18 11:29 75-09-28.0 3.9 4
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/18 11:29 108-10-120.0 1.3 4
Methyl-tert-butyl ether 519 ug/L 08/24/18 11:29 1634-04-4 M14.0 0.84 4
Naphthalene 71.1 ug/L 08/24/18 11:29 91-20-34.0 0.96 4
Styrene ND ug/L 08/24/18 11:29 100-42-54.0 1.0 4
1,1,1,2-Tetrachloroethane ND ug/L 08/24/18 11:29 630-20-64.0 1.3 4
1,1,2,2-Tetrachloroethane ND ug/L 08/24/18 11:29 79-34-54.0 1.6 4
Tetrachloroethene ND ug/L 08/24/18 11:29 127-18-44.0 1.8 4
Toluene ND ug/L 08/24/18 11:29 108-88-34.0 1.0 4
1,2,3-Trichlorobenzene ND ug/L 08/24/18 11:29 87-61-64.0 1.3 4
1,2,4-Trichlorobenzene ND ug/L 08/24/18 11:29 120-82-14.0 1.4 4
1,1,1-Trichloroethane ND ug/L 08/24/18 11:29 71-55-64.0 1.9 4
1,1,2-Trichloroethane ND ug/L 08/24/18 11:29 79-00-54.0 1.2 4
Trichloroethene ND ug/L 08/24/18 11:29 79-01-64.0 1.9 4
Trichlorofluoromethane ND ug/L 08/24/18 11:29 75-69-44.0 0.80 4
1,2,3-Trichloropropane ND ug/L 08/24/18 11:29 96-18-44.0 1.6 4
Vinyl acetate ND ug/L 08/24/18 11:29 108-05-48.0 1.4 4
Vinyl chloride ND ug/L 08/24/18 11:29 75-01-44.0 2.5 4
Xylene (Total)30.5 ug/L 08/24/18 11:29 1330-20-74.0 4.0 4
m&p-Xylene 5.4J ug/L 08/24/18 11:29 179601-23-18.0 2.6 4
o-Xylene 30.5 ug/L 08/24/18 11:29 95-47-64.0 0.92 4
Surrogates
4-Bromofluorobenzene (S)104 %08/24/18 11:29 460-00-470-130 4
1,2-Dichloroethane-d4 (S)109 %08/24/18 11:29 17060-07-070-130 4
Toluene-d8 (S)104 %08/24/18 11:29 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
426703
EPA 8260B
EPA 8260B
8260 MSV Low Level SC
Associated Lab Samples:92396262005, 92396262006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2358029
Associated Lab Samples:92396262005, 92396262006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/23/18 08:380.33
1,1,1-Trichloroethane ug/L ND 1.0 08/23/18 08:380.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/23/18 08:380.40
1,1,2-Trichloroethane ug/L ND 1.0 08/23/18 08:380.29
1,1-Dichloroethane ug/L ND 1.0 08/23/18 08:380.32
1,1-Dichloroethene ug/L ND 1.0 08/23/18 08:380.56
1,1-Dichloropropene ug/L ND 1.0 08/23/18 08:380.49
1,2,3-Trichlorobenzene ug/L ND 1.0 08/23/18 08:380.33
1,2,3-Trichloropropane ug/L ND 1.0 08/23/18 08:380.41
1,2,4-Trichlorobenzene ug/L ND 1.0 08/23/18 08:380.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/23/18 08:382.0
1,2-Dichlorobenzene ug/L ND 1.0 08/23/18 08:380.30
1,2-Dichloroethane ug/L ND 1.0 08/23/18 08:380.24
1,2-Dichloropropane ug/L ND 1.0 08/23/18 08:380.27
1,3-Dichlorobenzene ug/L ND 1.0 08/23/18 08:380.24
1,3-Dichloropropane ug/L ND 1.0 08/23/18 08:380.28
1,4-Dichlorobenzene ug/L ND 1.0 08/23/18 08:380.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 08/23/18 08:3878.4
2,2-Dichloropropane ug/L ND 1.0 08/23/18 08:380.13
2-Butanone (MEK)ug/L ND 5.0 08/23/18 08:380.96
2-Chlorotoluene ug/L ND 1.0 08/23/18 08:380.35
2-Hexanone ug/L ND 5.0 08/23/18 08:380.46
4-Chlorotoluene ug/L ND 1.0 08/23/18 08:380.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/23/18 08:380.33
Acetone ug/L ND 25.0 08/23/18 08:3810.0
Benzene ug/L ND 1.0 08/23/18 08:380.25
Bromobenzene ug/L ND 1.0 08/23/18 08:380.30
Bromochloromethane ug/L ND 1.0 08/23/18 08:380.17
Bromodichloromethane ug/L ND 1.0 08/23/18 08:380.18
Bromoform ug/L ND 1.0 08/23/18 08:380.26
Bromomethane ug/L ND 5.0 08/23/18 08:380.29
Carbon tetrachloride ug/L ND 1.0 08/23/18 08:380.25
Chlorobenzene ug/L ND 1.0 08/23/18 08:380.23
Chloroethane ug/L ND 1.0 08/23/18 08:380.54
Chloroform ug/L ND 1.0 08/23/18 08:380.14
Chloromethane ug/L ND 1.0 08/23/18 08:380.11
cis-1,2-Dichloroethene ug/L ND 1.0 08/23/18 08:380.19
cis-1,3-Dichloropropene ug/L ND 1.0 08/23/18 08:380.13
Dibromochloromethane ug/L ND 1.0 08/23/18 08:380.21
Dibromomethane ug/L ND 1.0 08/23/18 08:380.21
Dichlorodifluoromethane ug/L ND 1.0 08/23/18 08:380.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2358029
Associated Lab Samples:92396262005, 92396262006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 08/23/18 08:380.12
Ethylbenzene ug/L ND 1.0 08/23/18 08:380.30
Hexachloro-1,3-butadiene ug/L ND 1.0 08/23/18 08:380.71
m&p-Xylene ug/L ND 2.0 08/23/18 08:380.66
Methyl-tert-butyl ether ug/L ND 1.0 08/23/18 08:380.21
Methylene Chloride ug/L ND 2.0 08/23/18 08:380.97
Naphthalene ug/L ND 1.0 08/23/18 08:380.24
o-Xylene ug/L ND 1.0 08/23/18 08:380.23
p-Isopropyltoluene ug/L ND 1.0 08/23/18 08:380.31
Styrene ug/L ND 1.0 08/23/18 08:380.26
Tetrachloroethene ug/L ND 1.0 08/23/18 08:380.46
Toluene ug/L ND 1.0 08/23/18 08:380.26
trans-1,2-Dichloroethene ug/L ND 1.0 08/23/18 08:380.49
trans-1,3-Dichloropropene ug/L ND 1.0 08/23/18 08:380.26
Trichloroethene ug/L ND 1.0 08/23/18 08:380.47
Trichlorofluoromethane ug/L ND 1.0 08/23/18 08:380.20
Vinyl acetate ug/L ND 2.0 08/23/18 08:380.35
Vinyl chloride ug/L ND 1.0 08/23/18 08:380.62
Xylene (Total)ug/L ND 1.0 08/23/18 08:381.0
1,2-Dichloroethane-d4 (S)%90 70-130 08/23/18 08:38
4-Bromofluorobenzene (S)%105 70-130 08/23/18 08:38
Toluene-d8 (S)%108 70-130 08/23/18 08:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2358030LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.150 106 70-130
1,1,1-Trichloroethane ug/L 47.750 95 70-130
1,1,2,2-Tetrachloroethane ug/L 49.950 100 70-130
1,1,2-Trichloroethane ug/L 50.850 102 70-130
1,1-Dichloroethane ug/L 44.850 90 70-130
1,1-Dichloroethene ug/L 49.750 99 70-130
1,1-Dichloropropene ug/L 50.1 1g5010070-130
1,2,3-Trichlorobenzene ug/L 47.350 95 70-130
1,2,3-Trichloropropane ug/L 52.450 105 70-130
1,2,4-Trichlorobenzene ug/L 46.450 93 70-130
1,2-Dibromo-3-chloropropane ug/L 49.0 1g509870-130
1,2-Dichlorobenzene ug/L 50.150 100 70-130
1,2-Dichloroethane ug/L 50.050 100 70-130
1,2-Dichloropropane ug/L 54.950 110 70-130
1,3-Dichlorobenzene ug/L 48.850 98 70-130
1,3-Dichloropropane ug/L 51.250 102 70-130
1,4-Dichlorobenzene ug/L 49.750 99 70-130
1,4-Dioxane (p-Dioxane)ug/L 9981000 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2358030LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 43.250 86 70-130
2-Butanone (MEK)ug/L 88.6100 89 70-130
2-Chlorotoluene ug/L 50.650 101 70-130
2-Hexanone ug/L 94.9100 95 70-130
4-Chlorotoluene ug/L 49.250 98 70-130
4-Methyl-2-pentanone (MIBK)ug/L 93.5100 94 70-130
Acetone ug/L 94.1100 94 70-130
Benzene ug/L 52.450 105 70-130
Bromobenzene ug/L 50.550 101 70-130
Bromochloromethane ug/L 48.350 97 70-130
Bromodichloromethane ug/L 52.050 104 70-130
Bromoform ug/L 47.950 96 70-130
Bromomethane ug/L 42.3 1g508570-130
Carbon tetrachloride ug/L 49.550 99 70-130
Chlorobenzene ug/L 50.850 102 70-130
Chloroethane ug/L 47.8 1g509670-130
Chloroform ug/L 48.950 98 70-130
Chloromethane ug/L 35.550 71 70-130
cis-1,2-Dichloroethene ug/L 46.650 93 70-130
cis-1,3-Dichloropropene ug/L 54.050 108 70-130
Dibromochloromethane ug/L 47.7 1g509570-130
Dibromomethane ug/L 48.350 97 70-130
Dichlorodifluoromethane ug/L 45.350 91 70-130
Diisopropyl ether ug/L 42.9 1g508670-130
Ethylbenzene ug/L 49.950 100 70-130
Hexachloro-1,3-butadiene ug/L 46.050 92 70-130
m&p-Xylene ug/L 97.0100 97 70-130
Methyl-tert-butyl ether ug/L 46.9 1g509470-130
Methylene Chloride ug/L 47.0 1g509470-130
Naphthalene ug/L 51.850 104 70-130
o-Xylene ug/L 49.450 99 70-130
p-Isopropyltoluene ug/L 48.750 97 70-130
Styrene ug/L 47.350 95 70-130
Tetrachloroethene ug/L 47.650 95 70-130
Toluene ug/L 51.4 1g5010370-130
trans-1,2-Dichloroethene ug/L 49.450 99 70-130
trans-1,3-Dichloropropene ug/L 52.550 105 70-130
Trichloroethene ug/L 52.1 1g5010470-130
Trichlorofluoromethane ug/L 47.950 96 70-130
Vinyl acetate ug/L 88.6 1g1008970-130
Vinyl chloride ug/L 47.450 95 70-130
Xylene (Total)ug/L 146150 98 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2358871MATRIX SPIKE SAMPLE:
MSSpike
Result
92396260011
1,1,1,2-Tetrachloroethane ug/L 23.920 120 70-130ND
1,1,1-Trichloroethane ug/L 26.7 M12013470-130ND
1,1,2,2-Tetrachloroethane ug/L 23.820 119 70-130ND
1,1,2-Trichloroethane ug/L 23.320 116 70-130ND
1,1-Dichloroethane ug/L 25.220 126 70-130ND
1,1-Dichloroethene ug/L 30.1 M12015170-130ND
1,1-Dichloropropene ug/L 26.5 M12013370-130ND
1,2,3-Trichlorobenzene ug/L 19.820 99 70-130ND
1,2,3-Trichloropropane ug/L 25.420 127 70-130ND
1,2,4-Trichlorobenzene ug/L 20.920 104 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.420 112 70-130ND
1,2-Dichlorobenzene ug/L 22.820 114 70-130ND
1,2-Dichloroethane ug/L 25.420 127 70-130ND
1,2-Dichloropropane ug/L 27.9 M12013970-130ND
1,3-Dichlorobenzene ug/L 23.020 115 70-130ND
1,3-Dichloropropane ug/L 24.320 121 70-130ND
1,4-Dichlorobenzene ug/L 23.220 116 70-130ND
1,4-Dioxane (p-Dioxane)ug/L 539 M140013570-130ND
2,2-Dichloropropane ug/L 28.2 M12014170-130ND
2-Butanone (MEK)ug/L 45.640 114 70-130ND
2-Chlorotoluene ug/L 24.520 122 70-130ND
2-Hexanone ug/L 48.140 120 70-130ND
4-Chlorotoluene ug/L 24.820 124 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.940 112 70-130ND
Acetone ug/L 47.840 119 70-130ND
Benzene ug/L 27.3 M12013670-130ND
Bromobenzene ug/L 24.620 123 70-130ND
Bromochloromethane ug/L 27.2 M12013670-130ND
Bromodichloromethane ug/L 26.020 130 70-130ND
Bromoform ug/L 21.120 105 70-130ND
Bromomethane ug/L 27.2 M12013670-130ND
Carbon tetrachloride ug/L 27.4 M12013770-130ND
Chlorobenzene ug/L 26.3 M12013170-130ND
Chloroethane ug/L 28.3 M12014170-130ND
Chloroform ug/L 25.920 130 70-130ND
Chloromethane ug/L 18.320 91 70-130ND
cis-1,2-Dichloroethene ug/L 26.2 M12013170-130ND
cis-1,3-Dichloropropene ug/L 26.1 M12013170-130ND
Dibromochloromethane ug/L 22.120 111 70-130ND
Dibromomethane ug/L 24.620 123 70-130ND
Dichlorodifluoromethane ug/L 25.120 126 70-130ND
Diisopropyl ether ug/L 20.420 102 70-130ND
Ethylbenzene ug/L 26.020 130 70-130ND
Hexachloro-1,3-butadiene ug/L 27.8 M12013970-130ND
m&p-Xylene ug/L 51.940 130 70-130ND
Methyl-tert-butyl ether ug/L 21.420 107 70-130ND
Methylene Chloride ug/L 24.220 121 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2358871MATRIX SPIKE SAMPLE:
MSSpike
Result
92396260011
Naphthalene ug/L 20.320 102 70-130ND
o-Xylene ug/L 26.2 M12013170-130ND
p-Isopropyltoluene ug/L 23.420 117 70-130ND
Styrene ug/L 24.720 124 70-130ND
Tetrachloroethene ug/L 24.220 121 70-130ND
Toluene ug/L 27.9 M12014070-130ND
trans-1,2-Dichloroethene ug/L 28.1 M12014170-130ND
trans-1,3-Dichloropropene ug/L 25.320 127 70-130ND
Trichloroethene ug/L 26.9 M12013470-130ND
Trichlorofluoromethane ug/L 28.6 M12014370-130ND
Vinyl acetate ug/L 40.740 102 70-130ND
Vinyl chloride ug/L 28.2 M12014170-130ND
Xylene (Total)ug/L 78.1 MS6013070-130ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396260010
2358870SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1,4-Dioxane (p-Dioxane)ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396260010
2358870SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%92 698
4-Bromofluorobenzene (S)%104 0104
Toluene-d8 (S)%107 1108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
426920
EPA 8260B
EPA 8260B
8260 MSV Low Level SC
Associated Lab Samples:92396262004, 92396262007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2358964
Associated Lab Samples:92396262004, 92396262007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/24/18 07:350.33
1,1,1-Trichloroethane ug/L ND 1.0 08/24/18 07:350.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/24/18 07:350.40
1,1,2-Trichloroethane ug/L ND 1.0 08/24/18 07:350.29
1,1-Dichloroethane ug/L ND 1.0 08/24/18 07:350.32
1,1-Dichloroethene ug/L ND 1.0 08/24/18 07:350.56
1,1-Dichloropropene ug/L ND 1.0 08/24/18 07:350.49
1,2,3-Trichlorobenzene ug/L ND 1.0 08/24/18 07:350.33
1,2,3-Trichloropropane ug/L ND 1.0 08/24/18 07:350.41
1,2,4-Trichlorobenzene ug/L ND 1.0 08/24/18 07:350.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/24/18 07:352.0
1,2-Dichlorobenzene ug/L ND 1.0 08/24/18 07:350.30
1,2-Dichloroethane ug/L ND 1.0 08/24/18 07:350.24
1,2-Dichloropropane ug/L ND 1.0 08/24/18 07:350.27
1,3-Dichlorobenzene ug/L ND 1.0 08/24/18 07:350.24
1,3-Dichloropropane ug/L ND 1.0 08/24/18 07:350.28
1,4-Dichlorobenzene ug/L ND 1.0 08/24/18 07:350.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 08/24/18 07:3578.4
2,2-Dichloropropane ug/L ND 1.0 08/24/18 07:350.13
2-Butanone (MEK)ug/L ND 5.0 08/24/18 07:350.96
2-Chlorotoluene ug/L ND 1.0 08/24/18 07:350.35
2-Hexanone ug/L ND 5.0 08/24/18 07:350.46
4-Chlorotoluene ug/L ND 1.0 08/24/18 07:350.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/24/18 07:350.33
Acetone ug/L ND 25.0 08/24/18 07:3510.0
Benzene ug/L ND 1.0 08/24/18 07:350.25
Bromobenzene ug/L ND 1.0 08/24/18 07:350.30
Bromochloromethane ug/L ND 1.0 08/24/18 07:350.17
Bromodichloromethane ug/L ND 1.0 08/24/18 07:350.18
Bromoform ug/L ND 1.0 08/24/18 07:350.26
Bromomethane ug/L ND 5.0 08/24/18 07:350.29
Carbon tetrachloride ug/L ND 1.0 08/24/18 07:350.25
Chlorobenzene ug/L ND 1.0 08/24/18 07:350.23
Chloroethane ug/L ND 1.0 08/24/18 07:350.54
Chloroform ug/L ND 1.0 08/24/18 07:350.14
Chloromethane ug/L ND 1.0 08/24/18 07:350.11
cis-1,2-Dichloroethene ug/L ND 1.0 08/24/18 07:350.19
cis-1,3-Dichloropropene ug/L ND 1.0 08/24/18 07:350.13
Dibromochloromethane ug/L ND 1.0 08/24/18 07:350.21
Dibromomethane ug/L ND 1.0 08/24/18 07:350.21
Dichlorodifluoromethane ug/L ND 1.0 08/24/18 07:350.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2358964
Associated Lab Samples:92396262004, 92396262007
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 08/24/18 07:350.12
Ethylbenzene ug/L ND 1.0 08/24/18 07:350.30
Hexachloro-1,3-butadiene ug/L ND 1.0 08/24/18 07:350.71
m&p-Xylene ug/L ND 2.0 08/24/18 07:350.66
Methyl-tert-butyl ether ug/L ND 1.0 08/24/18 07:350.21
Methylene Chloride ug/L ND 2.0 08/24/18 07:350.97
Naphthalene ug/L ND 1.0 08/24/18 07:350.24
o-Xylene ug/L ND 1.0 08/24/18 07:350.23
p-Isopropyltoluene ug/L ND 1.0 08/24/18 07:350.31
Styrene ug/L ND 1.0 08/24/18 07:350.26
Tetrachloroethene ug/L ND 1.0 08/24/18 07:350.46
Toluene ug/L ND 1.0 08/24/18 07:350.26
trans-1,2-Dichloroethene ug/L ND 1.0 08/24/18 07:350.49
trans-1,3-Dichloropropene ug/L ND 1.0 08/24/18 07:350.26
Trichloroethene ug/L ND 1.0 08/24/18 07:350.47
Trichlorofluoromethane ug/L ND 1.0 08/24/18 07:350.20
Vinyl acetate ug/L ND 2.0 08/24/18 07:350.35
Vinyl chloride ug/L ND 1.0 08/24/18 07:350.62
Xylene (Total)ug/L ND 1.0 08/24/18 07:351.0
1,2-Dichloroethane-d4 (S)%104 70-130 08/24/18 07:35
4-Bromofluorobenzene (S)%105 70-130 08/24/18 07:35
Toluene-d8 (S)%109 70-130 08/24/18 07:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2358965LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.350 107 70-130
1,1,1-Trichloroethane ug/L 49.350 99 70-130
1,1,2,2-Tetrachloroethane ug/L 48.850 98 70-130
1,1,2-Trichloroethane ug/L 51.650 103 70-130
1,1-Dichloroethane ug/L 46.150 92 70-130
1,1-Dichloroethene ug/L 53.150 106 70-130
1,1-Dichloropropene ug/L 51.9 1g5010470-130
1,2,3-Trichlorobenzene ug/L 48.650 97 70-130
1,2,3-Trichloropropane ug/L 52.450 105 70-130
1,2,4-Trichlorobenzene ug/L 46.950 94 70-130
1,2-Dibromo-3-chloropropane ug/L 47.4 1g509570-130
1,2-Dichlorobenzene ug/L 50.350 101 70-130
1,2-Dichloroethane ug/L 52.250 104 70-130
1,2-Dichloropropane ug/L 54.950 110 70-130
1,3-Dichlorobenzene ug/L 49.350 99 70-130
1,3-Dichloropropane ug/L 51.650 103 70-130
1,4-Dichlorobenzene ug/L 50.250 100 70-130
1,4-Dioxane (p-Dioxane)ug/L 9951000 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2358965LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 44.550 89 70-130
2-Butanone (MEK)ug/L 91.0100 91 70-130
2-Chlorotoluene ug/L 50.950 102 70-130
2-Hexanone ug/L 96.0100 96 70-130
4-Chlorotoluene ug/L 49.850 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 91.7100 92 70-130
Acetone ug/L 99.6100 100 70-130
Benzene ug/L 53.950 108 70-130
Bromobenzene ug/L 52.250 104 70-130
Bromochloromethane ug/L 47.850 96 70-130
Bromodichloromethane ug/L 49.750 99 70-130
Bromoform ug/L 46.950 94 70-130
Bromomethane ug/L 44.2 1g508870-130
Carbon tetrachloride ug/L 50.050 100 70-130
Chlorobenzene ug/L 50.750 101 70-130
Chloroethane ug/L 50.6 1g5010170-130
Chloroform ug/L 49.650 99 70-130
Chloromethane ug/L 39.750 79 70-130
cis-1,2-Dichloroethene ug/L 48.550 97 70-130
cis-1,3-Dichloropropene ug/L 53.850 108 70-130
Dibromochloromethane ug/L 46.7 1g509370-130
Dibromomethane ug/L 48.350 97 70-130
Dichlorodifluoromethane ug/L 52.050 104 70-130
Diisopropyl ether ug/L 45.0 1g509070-130
Ethylbenzene ug/L 49.850 100 70-130
Hexachloro-1,3-butadiene ug/L 45.850 92 70-130
m&p-Xylene ug/L 97.4100 97 70-130
Methyl-tert-butyl ether ug/L 49.650 99 70-130
Methylene Chloride ug/L 50.5 1g5010170-130
Naphthalene ug/L 51.150 102 70-130
o-Xylene ug/L 50.450 101 70-130
p-Isopropyltoluene ug/L 48.850 98 70-130
Styrene ug/L 47.450 95 70-130
Tetrachloroethene ug/L 48.750 97 70-130
Toluene ug/L 51.2 1g5010270-130
trans-1,2-Dichloroethene ug/L 49.750 99 70-130
trans-1,3-Dichloropropene ug/L 51.950 104 70-130
Trichloroethene ug/L 52.9 1g5010670-130
Trichlorofluoromethane ug/L 52.450 105 70-130
Vinyl acetate ug/L 95.5 1g1009670-130
Vinyl chloride ug/L 53.850 108 70-130
Xylene (Total)ug/L 148150 99 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2358967MATRIX SPIKE SAMPLE:
MSSpike
Result
92396262007
1,1,1,2-Tetrachloroethane ug/L 86.280 108 70-130ND
1,1,1-Trichloroethane ug/L 92.780 116 70-130ND
1,1,2,2-Tetrachloroethane ug/L 80.380 100 70-130ND
1,1,2-Trichloroethane ug/L 85.180 106 70-130ND
1,1-Dichloroethane ug/L 82.080 102 70-130ND
1,1-Dichloroethene ug/L 10080 125 70-130ND
1,1-Dichloropropene ug/L 96.180 120 70-130ND
1,2,3-Trichlorobenzene ug/L 78.780 98 70-130ND
1,2,3-Trichloropropane ug/L 87.580 109 70-130ND
1,2,4-Trichlorobenzene ug/L 77.080 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 78.680 98 70-130ND
1,2-Dichlorobenzene ug/L 84.580 106 70-130ND
1,2-Dichloroethane ug/L 16080 109 70-13073.0
1,2-Dichloropropane ug/L 98.880 124 70-130ND
1,3-Dichlorobenzene ug/L 86.580 108 70-130ND
1,3-Dichloropropane ug/L 87.480 109 70-130ND
1,4-Dichlorobenzene ug/L 87.180 109 70-130ND
1,4-Dioxane (p-Dioxane)ug/L 15701600 98 70-130ND
2,2-Dichloropropane ug/L 93.180 116 70-130ND
2-Butanone (MEK)ug/L 163160 102 70-130ND
2-Chlorotoluene ug/L 89.680 112 70-130ND
2-Hexanone ug/L 158160 99 70-130ND
4-Chlorotoluene ug/L 88.180 110 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 151160 94 70-130ND
Acetone ug/L 141160 88 70-130ND
Benzene ug/L 628 M1805570-130585
Bromobenzene ug/L 89.780 112 70-130ND
Bromochloromethane ug/L 84.380 105 70-130ND
Bromodichloromethane ug/L 87.880 110 70-130ND
Bromoform ug/L 71.780 90 70-130ND
Bromomethane ug/L 87.380 109 70-130ND
Carbon tetrachloride ug/L 93.480 117 70-130ND
Chlorobenzene ug/L 87.180 109 70-130ND
Chloroethane ug/L 95.780 120 70-130ND
Chloroform ug/L 87.080 109 70-130ND
Chloromethane ug/L 72.980 91 70-130ND
cis-1,2-Dichloroethene ug/L 86.380 108 70-130ND
cis-1,3-Dichloropropene ug/L 91.380 114 70-130ND
Dibromochloromethane ug/L 77.980 97 70-130ND
Dibromomethane ug/L 82.980 104 70-130ND
Dichlorodifluoromethane ug/L 96.380 120 70-130ND
Diisopropyl ether ug/L 98.080 90 70-13026.1
Ethylbenzene ug/L 90.180 113 70-130ND
Hexachloro-1,3-butadiene ug/L 80.180 100 70-130ND
m&p-Xylene ug/L 182160 110 70-1305.4J
Methyl-tert-butyl ether ug/L 659 M18017570-130519
Methylene Chloride ug/L 91.880 115 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2358967MATRIX SPIKE SAMPLE:
MSSpike
Result
92396262007
Naphthalene ug/L 15080 99 70-13071.1
o-Xylene ug/L 11780 108 70-13030.5
p-Isopropyltoluene ug/L 98.880 109 70-13011.5
Styrene ug/L 83.680 105 70-130ND
Tetrachloroethene ug/L 87.680 110 70-130ND
Toluene ug/L 91.580 114 70-130ND
trans-1,2-Dichloroethene ug/L 92.680 116 70-130ND
trans-1,3-Dichloropropene ug/L 87.880 110 70-130ND
Trichloroethene ug/L 92.580 116 70-130ND
Trichlorofluoromethane ug/L 95.580 119 70-130ND
Vinyl acetate ug/L 165160 103 70-130ND
Vinyl chloride ug/L 98.580 123 70-130ND
Xylene (Total)ug/L 298240 112 70-13030.5
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396956001
2358966SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1,4-Dioxane (p-Dioxane)ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396956001
2358966SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%90 595
4-Bromofluorobenzene (S)%104 2106
Toluene-d8 (S)%107 3110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
425903
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92396262001, 92396262002, 92396262003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2354553
Associated Lab Samples:92396262001, 92396262002, 92396262003
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 4.9 08/21/18 12:312.1
1,1,1-Trichloroethane ug/kg ND 4.9 08/21/18 12:311.8
1,1,2,2-Tetrachloroethane ug/kg ND 4.9 08/21/18 12:311.9
1,1,2-Trichloroethane ug/kg ND 4.9 08/21/18 12:312.1
1,1-Dichloroethane ug/kg ND 4.9 08/21/18 12:311.5
1,1-Dichloroethene ug/kg ND 4.9 08/21/18 12:311.8
1,1-Dichloropropene ug/kg ND 4.9 08/21/18 12:311.5
1,2,3-Trichlorobenzene ug/kg ND 4.9 08/21/18 12:312.1
1,2,3-Trichloropropane ug/kg ND 4.9 08/21/18 12:311.6
1,2,4-Trichlorobenzene ug/kg ND 4.9 08/21/18 12:311.6
1,2,4-Trimethylbenzene ug/kg ND 4.9 08/21/18 12:312.0
1,2-Dibromo-3-chloropropane ug/kg ND 4.9 08/21/18 12:313.5
1,2-Dibromoethane (EDB)ug/kg ND 4.9 08/21/18 12:311.8
1,2-Dichlorobenzene ug/kg ND 4.9 08/21/18 12:311.9
1,2-Dichloroethane ug/kg ND 4.9 08/21/18 12:312.1
1,2-Dichloropropane ug/kg ND 4.9 08/21/18 12:311.7
1,3,5-Trimethylbenzene ug/kg ND 4.9 08/21/18 12:311.8
1,3-Dichlorobenzene ug/kg ND 4.9 08/21/18 12:312.0
1,3-Dichloropropane ug/kg ND 4.9 08/21/18 12:311.9
1,4-Dichlorobenzene ug/kg ND 4.9 08/21/18 12:311.7
2,2-Dichloropropane ug/kg ND 4.9 08/21/18 12:311.7
2-Butanone (MEK)ug/kg ND 97.7 08/21/18 12:312.8
2-Chlorotoluene ug/kg ND 4.9 08/21/18 12:311.7
2-Hexanone ug/kg ND 48.8 08/21/18 12:313.8
4-Chlorotoluene ug/kg ND 4.9 08/21/18 12:311.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 48.8 08/21/18 12:313.6
Acetone ug/kg ND 97.7 08/21/18 12:319.8
Benzene ug/kg ND 4.9 08/21/18 12:311.6
Bromobenzene ug/kg ND 4.9 08/21/18 12:312.0
Bromochloromethane ug/kg ND 4.9 08/21/18 12:311.7
Bromodichloromethane ug/kg ND 4.9 08/21/18 12:311.9
Bromoform ug/kg ND 4.9 08/21/18 12:312.2
Bromomethane ug/kg ND 9.8 08/21/18 12:312.4
Carbon tetrachloride ug/kg ND 4.9 08/21/18 12:312.5
Chlorobenzene ug/kg ND 4.9 08/21/18 12:311.9
Chloroethane ug/kg ND 9.8 08/21/18 12:312.3
Chloroform ug/kg ND 4.9 08/21/18 12:311.6
Chloromethane ug/kg ND 9.8 08/21/18 12:312.3
cis-1,2-Dichloroethene ug/kg ND 4.9 08/21/18 12:311.4
cis-1,3-Dichloropropene ug/kg ND 4.9 08/21/18 12:311.8
Dibromochloromethane ug/kg ND 4.9 08/21/18 12:311.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2354553
Associated Lab Samples:92396262001, 92396262002, 92396262003
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 4.9 08/21/18 12:312.4
Dichlorodifluoromethane ug/kg ND 9.8 08/21/18 12:313.5
Diisopropyl ether ug/kg ND 4.9 08/21/18 12:311.7
Ethylbenzene ug/kg ND 4.9 08/21/18 12:311.8
Hexachloro-1,3-butadiene ug/kg ND 4.9 08/21/18 12:312.0
Isopropylbenzene (Cumene)ug/kg ND 4.9 08/21/18 12:311.9
m&p-Xylene ug/kg ND 9.8 08/21/18 12:313.5
Methyl-tert-butyl ether ug/kg ND 4.9 08/21/18 12:311.5
Methylene Chloride ug/kg ND 19.5 08/21/18 12:312.9
n-Butylbenzene ug/kg ND 4.9 08/21/18 12:311.8
n-Propylbenzene ug/kg ND 4.9 08/21/18 12:311.7
Naphthalene ug/kg ND 4.9 08/21/18 12:311.2
o-Xylene ug/kg ND 4.9 08/21/18 12:311.9
p-Isopropyltoluene ug/kg ND 4.9 08/21/18 12:311.7
sec-Butylbenzene ug/kg ND 4.9 08/21/18 12:311.6
Styrene ug/kg ND 4.9 08/21/18 12:311.8
tert-Butylbenzene ug/kg ND 4.9 08/21/18 12:312.0
Tetrachloroethene ug/kg ND 4.9 08/21/18 12:311.7
Toluene ug/kg ND 4.9 08/21/18 12:311.8
trans-1,2-Dichloroethene ug/kg ND 4.9 08/21/18 12:311.9
trans-1,3-Dichloropropene ug/kg ND 4.9 08/21/18 12:311.5
Trichloroethene ug/kg ND 4.9 08/21/18 12:312.1
Trichlorofluoromethane ug/kg ND 4.9 08/21/18 12:312.1
Vinyl acetate ug/kg ND 48.8 08/21/18 12:318.6
Vinyl chloride ug/kg ND 9.8 08/21/18 12:311.8
Xylene (Total)ug/kg ND 9.8 08/21/18 12:313.5
1,2-Dichloroethane-d4 (S)%111 70-130 08/21/18 12:31
4-Bromofluorobenzene (S)%99 70-130 08/21/18 12:31
Toluene-d8 (S)%101 70-130 08/21/18 12:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2354554LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 50.751.8 98 70-130
1,1,1-Trichloroethane ug/kg 49.851.8 96 70-130
1,1,2,2-Tetrachloroethane ug/kg 51.051.8 99 70-130
1,1,2-Trichloroethane ug/kg 49.451.8 95 70-130
1,1-Dichloroethane ug/kg 48.651.8 94 70-130
1,1-Dichloroethene ug/kg 54.251.8 105 70-130
1,1-Dichloropropene ug/kg 50.351.8 97 70-130
1,2,3-Trichlorobenzene ug/kg 51.551.8 100 70-130
1,2,3-Trichloropropane ug/kg 51.451.8 99 70-130
1,2,4-Trichlorobenzene ug/kg 52.051.8 101 70-130
1,2,4-Trimethylbenzene ug/kg 46.351.8 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2354554LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 51.451.8 99 70-130
1,2-Dibromoethane (EDB)ug/kg 49.451.8 95 70-130
1,2-Dichlorobenzene ug/kg 47.851.8 92 70-130
1,2-Dichloroethane ug/kg 50.951.8 98 70-130
1,2-Dichloropropane ug/kg 48.851.8 94 70-130
1,3,5-Trimethylbenzene ug/kg 48.151.8 93 70-130
1,3-Dichlorobenzene ug/kg 46.451.8 90 70-130
1,3-Dichloropropane ug/kg 50.951.8 98 70-130
1,4-Dichlorobenzene ug/kg 46.751.8 90 70-130
2,2-Dichloropropane ug/kg 48.851.8 94 70-130
2-Butanone (MEK)ug/kg 99.2J104 96 70-130
2-Chlorotoluene ug/kg 49.151.8 95 70-130
2-Hexanone ug/kg 104104 101 70-130
4-Chlorotoluene ug/kg 47.351.8 91 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 103104 100 70-130
Acetone ug/kg 102J104 98 70-130
Benzene ug/kg 49.451.8 95 70-130
Bromobenzene ug/kg 50.151.8 97 70-130
Bromochloromethane ug/kg 49.151.8 95 70-130
Bromodichloromethane ug/kg 51.351.8 99 70-130
Bromoform ug/kg 54.751.8 106 70-130
Bromomethane ug/kg 54.6 2g51.8 105 70-130
Carbon tetrachloride ug/kg 50.451.8 97 70-130
Chlorobenzene ug/kg 49.451.8 95 70-130
Chloroethane ug/kg 50.951.8 98 70-130
Chloroform ug/kg 47.451.8 92 70-130
Chloromethane ug/kg 51.3 2g51.8 99 70-130
cis-1,2-Dichloroethene ug/kg 50.051.8 97 70-130
cis-1,3-Dichloropropene ug/kg 50.351.8 97 70-130
Dibromochloromethane ug/kg 52.751.8 102 70-130
Dibromomethane ug/kg 48.451.8 94 70-130
Dichlorodifluoromethane ug/kg 48.4 2g51.8 93 70-130
Diisopropyl ether ug/kg 49.251.8 95 70-130
Ethylbenzene ug/kg 49.851.8 96 70-130
Hexachloro-1,3-butadiene ug/kg 49.251.8 95 70-130
Isopropylbenzene (Cumene)ug/kg 51.051.8 98 70-130
m&p-Xylene ug/kg 101104 97 70-130
Methyl-tert-butyl ether ug/kg 48.151.8 93 70-130
Methylene Chloride ug/kg 48.951.8 94 70-130
n-Butylbenzene ug/kg 48.551.8 94 70-130
n-Propylbenzene ug/kg 48.551.8 94 70-130
Naphthalene ug/kg 54.051.8 104 70-130
o-Xylene ug/kg 51.351.8 99 70-130
p-Isopropyltoluene ug/kg 47.451.8 92 70-130
sec-Butylbenzene ug/kg 46.351.8 89 70-130
Styrene ug/kg 50.051.8 97 70-130
tert-Butylbenzene ug/kg 42.851.8 83 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2354554LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 43.251.8 84 70-130
Toluene ug/kg 48.751.8 94 70-130
trans-1,2-Dichloroethene ug/kg 51.451.8 99 70-130
trans-1,3-Dichloropropene ug/kg 51.251.8 99 70-130
Trichloroethene ug/kg 50.051.8 97 70-130
Trichlorofluoromethane ug/kg 53.751.8 104 70-130
Vinyl acetate ug/kg 85.6104 83 70-130
Vinyl chloride ug/kg 54.551.8 105 70-130
Xylene (Total)ug/kg 152155 98 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2354556MATRIX SPIKE SAMPLE:
MSSpike
Result
92396262003
1,1,1,2-Tetrachloroethane ug/kg 22.423.6 95 70-130ND
1,1,1-Trichloroethane ug/kg 26.223.6 111 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 25.323.6 107 70-130ND
1,1,2-Trichloroethane ug/kg 22.523.6 95 70-130ND
1,1-Dichloroethane ug/kg 27.123.6 115 70-130ND
1,1-Dichloroethene ug/kg 30.423.6 129 70-130ND
1,1-Dichloropropene ug/kg 26.223.6 111 70-130ND
1,2,3-Trichlorobenzene ug/kg 21.323.6 90 70-130ND
1,2,3-Trichloropropane ug/kg 23.423.6 99 70-130ND
1,2,4-Trichlorobenzene ug/kg 19.423.6 82 70-130ND
1,2,4-Trimethylbenzene ug/kg 20.723.6 80 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 23.723.6 100 70-130ND
1,2-Dibromoethane (EDB)ug/kg 21.723.6 92 70-130ND
1,2-Dichlorobenzene ug/kg 21.123.6 89 70-130ND
1,2-Dichloroethane ug/kg 25.323.6 107 70-130ND
1,2-Dichloropropane ug/kg 23.023.6 97 70-130ND
1,3,5-Trimethylbenzene ug/kg 21.523.6 91 70-130ND
1,3-Dichlorobenzene ug/kg 19.323.6 82 70-130ND
1,3-Dichloropropane ug/kg 23.423.6 99 70-130ND
1,4-Dichlorobenzene ug/kg 19.223.6 81 70-130ND
2,2-Dichloropropane ug/kg 22.523.6 95 70-130ND
2-Butanone (MEK)ug/kg 48.9J47.3 103 70-130ND
2-Chlorotoluene ug/kg 19.923.6 84 70-130ND
2-Hexanone ug/kg 49.0J47.3 104 70-130ND
4-Chlorotoluene ug/kg 20.123.6 85 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 48.2J47.3 102 70-130ND
Acetone ug/kg 60.8J47.3 129 70-130ND
Benzene ug/kg 24.023.6 102 70-130ND
Bromobenzene ug/kg 22.223.6 94 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2354556MATRIX SPIKE SAMPLE:
MSSpike
Result
92396262003
Bromochloromethane ug/kg 25.023.6 106 70-130ND
Bromodichloromethane ug/kg 21.823.6 92 70-130ND
Bromoform ug/kg 21.923.6 93 70-130ND
Bromomethane ug/kg 25.323.6 107 70-130ND
Carbon tetrachloride ug/kg 23.323.6 98 70-130ND
Chlorobenzene ug/kg 22.023.6 93 70-130ND
Chloroethane ug/kg 27.523.6 116 70-130ND
Chloroform ug/kg 24.323.6 103 70-130ND
Chloromethane ug/kg 29.623.6 125 70-130ND
cis-1,2-Dichloroethene ug/kg 25.523.6 108 70-130ND
cis-1,3-Dichloropropene ug/kg 20.623.6 87 70-130ND
Dibromochloromethane ug/kg 21.523.6 91 70-130ND
Dibromomethane ug/kg 21.623.6 91 70-130ND
Dichlorodifluoromethane ug/kg 28.523.6 121 70-130ND
Diisopropyl ether ug/kg 27.523.6 116 70-130ND
Ethylbenzene ug/kg 22.623.6 96 70-130ND
Hexachloro-1,3-butadiene ug/kg 22.723.6 96 70-130ND
Isopropylbenzene (Cumene)ug/kg 23.523.6 99 70-130ND
m&p-Xylene ug/kg 44.947.3 95 70-130ND
Methyl-tert-butyl ether ug/kg 25.423.6 107 70-130ND
Methylene Chloride ug/kg 27.023.6 114 70-130ND
n-Butylbenzene ug/kg 20.423.6 86 70-130ND
n-Propylbenzene ug/kg 22.223.6 94 70-130ND
Naphthalene ug/kg 26.4 M123.6 69 70-13010.1
o-Xylene ug/kg 22.523.6 95 70-130ND
p-Isopropyltoluene ug/kg 21.623.6 91 70-130ND
sec-Butylbenzene ug/kg 22.823.6 96 70-130ND
Styrene ug/kg 21.323.6 90 70-130ND
tert-Butylbenzene ug/kg 20.923.6 89 70-130ND
Tetrachloroethene ug/kg 19.923.6 84 70-130ND
Toluene ug/kg 22.723.6 96 70-130ND
trans-1,2-Dichloroethene ug/kg 28.223.6 119 70-130ND
trans-1,3-Dichloropropene ug/kg 20.123.6 85 70-130ND
Trichloroethene ug/kg 22.723.6 96 70-130ND
Trichlorofluoromethane ug/kg 29.623.6 125 70-130ND
Vinyl acetate ug/kg 49.6J47.3 105 70-130ND
Vinyl chloride ug/kg 33.6 M123.6 142 70-130ND
Xylene (Total)ug/kg 67.370.9 95 70-130ND
1,2-Dichloroethane-d4 (S)%115 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396127001
2354555SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396127001
2354555SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 304.0J
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%128 S14119
4-Bromofluorobenzene (S)%91 190
Toluene-d8 (S)%96 397
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
426122
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92396262001, 92396262002, 92396262003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2355587
Associated Lab Samples:92396262001, 92396262002, 92396262003
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10.0 08/25/18 09:301.2
2-Methylnaphthalene ug/kg ND 10.0 08/25/18 09:301.1
Acenaphthene ug/kg ND 10.0 08/25/18 09:301.5
Acenaphthylene ug/kg ND 10.0 08/25/18 09:301.3
Anthracene ug/kg ND 10.0 08/25/18 09:301.4
Benzo(a)anthracene ug/kg ND 10.0 08/25/18 09:300.71
Benzo(a)pyrene ug/kg ND 10.0 08/25/18 09:301.1
Benzo(b)fluoranthene ug/kg ND 10.0 08/25/18 09:300.67
Benzo(g,h,i)perylene ug/kg ND 10.0 08/25/18 09:302.6
Benzo(k)fluoranthene ug/kg ND 10.0 08/25/18 09:301.5
Chrysene ug/kg ND 10.0 08/25/18 09:301.8
Dibenz(a,h)anthracene ug/kg ND 10.0 08/25/18 09:301.8
Fluoranthene ug/kg ND 10.0 08/25/18 09:300.83
Fluorene ug/kg ND 10.0 08/25/18 09:301.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10.0 08/25/18 09:302.8
Naphthalene ug/kg ND 10.0 08/25/18 09:302.3
Phenanthrene ug/kg ND 10.0 08/25/18 09:301.5
Pyrene ug/kg ND 10.0 08/25/18 09:301.8
2-Fluorobiphenyl (S)%81 10-110 08/25/18 09:30
Nitrobenzene-d5 (S)%107 10-128 08/25/18 09:30
Terphenyl-d14 (S)%101 39-119 08/25/18 09:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2355588LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 26.633.1 80 44-130
2-Methylnaphthalene ug/kg 26.133.1 79 41-134
Acenaphthene ug/kg 27.433.1 83 52-123
Acenaphthylene ug/kg 27.333.1 83 49-116
Anthracene ug/kg 30.633.1 92 41-133
Benzo(a)anthracene ug/kg 27.633.1 83 56-130
Benzo(a)pyrene ug/kg 28.933.1 87 51-136
Benzo(b)fluoranthene ug/kg 27.033.1 81 37-149
Benzo(g,h,i)perylene ug/kg 26.033.1 78 39-127
Benzo(k)fluoranthene ug/kg 33.133.1 100 45-139
Chrysene ug/kg 29.933.1 90 59-127
Dibenz(a,h)anthracene ug/kg 27.433.1 83 37-139
Fluoranthene ug/kg 27.533.1 83 53-132
Fluorene ug/kg 27.233.1 82 45-127
Indeno(1,2,3-cd)pyrene ug/kg 28.433.1 86 35-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2355588LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/kg 26.433.1 80 45-123
Phenanthrene ug/kg 25.933.1 78 50-125
Pyrene ug/kg 26.833.1 81 52-132
2-Fluorobiphenyl (S)%81 10-110
Nitrobenzene-d5 (S)%106 10-128
Terphenyl-d14 (S)%94 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2355589MATRIX SPIKE SAMPLE:
MSSpike
Result
92396262001
1-Methylnaphthalene ug/kg 28.539.9 71 50-150ND
2-Methylnaphthalene ug/kg 28.039.9 70 50-150ND
Acenaphthene ug/kg 29.239.9 73 50-150ND
Acenaphthylene ug/kg 29.739.9 74 50-150ND
Anthracene ug/kg 30.739.9 77 50-150ND
Benzo(a)anthracene ug/kg 25.939.9 65 50-150ND
Benzo(a)pyrene ug/kg 26.339.9 66 50-150ND
Benzo(b)fluoranthene ug/kg 25.839.9 65 50-150ND
Benzo(g,h,i)perylene ug/kg 23.339.9 58 50-150ND
Benzo(k)fluoranthene ug/kg 28.839.9 72 50-150ND
Chrysene ug/kg 28.739.9 72 50-150ND
Dibenz(a,h)anthracene ug/kg 24.539.9 61 50-150ND
Fluoranthene ug/kg 26.839.9 67 50-150ND
Fluorene ug/kg 29.139.9 73 50-150ND
Indeno(1,2,3-cd)pyrene ug/kg 25.339.9 63 50-150ND
Naphthalene ug/kg 28.539.9 71 50-150ND
Phenanthrene ug/kg 27.639.9 69 50-150ND
Pyrene ug/kg 26.639.9 67 50-150ND
2-Fluorobiphenyl (S)%72 10-110
Nitrobenzene-d5 (S)%95 10-128
Terphenyl-d14 (S)%82 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396262002
2355590SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg 812 D65530461
2-Methylnaphthalene ug/kg 1040 D66030557
Acenaphthene ug/kg ND 3039.1
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg 5.4J 305.2J
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396262002
2355590SAMPLE DUPLICATE:
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg 44.9 8 3041.3
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg 639 D66330334
Phenanthrene ug/kg 20.0 14 3017.5
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%39 2530
Nitrobenzene-d5 (S)%0 S20
Terphenyl-d14 (S)%52 1944
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
426382
EPA 3511
EPA 8270D by SIM
8270 3511 Low Volume PAH SIM
Associated Lab Samples:92396262004, 92396262005, 92396262006, 92396262007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2356654
Associated Lab Samples:92396262004, 92396262005, 92396262006, 92396262007
Matrix:Water
AnalyzedMDL
1-Methylnaphthalene ug/L ND 2.0 09/08/18 16:562.0
2-Methylnaphthalene ug/L ND 2.0 09/08/18 16:562.0
Acenaphthene ug/L ND 0.50 09/08/18 16:560.50
Acenaphthylene ug/L ND 0.50 09/08/18 16:560.50
Anthracene ug/L ND 0.050 09/08/18 16:560.050
Benzo(a)anthracene ug/L ND 0.050 09/08/18 16:560.050
Benzo(a)pyrene ug/L ND 0.10 09/08/18 16:560.10
Benzo(b)fluoranthene ug/L ND 0.050 09/08/18 16:560.050
Benzo(g,h,i)perylene ug/L ND 0.20 09/08/18 16:560.20
Benzo(k)fluoranthene ug/L ND 0.20 09/08/18 16:560.20
Chrysene ug/L ND 0.10 09/08/18 16:560.10
Dibenz(a,h)anthracene ug/L ND 0.15 09/08/18 16:560.15
Fluoranthene ug/L ND 0.30 09/08/18 16:560.30
Fluorene ug/L ND 0.31 09/08/18 16:560.31
Indeno(1,2,3-cd)pyrene ug/L ND 0.050 09/08/18 16:560.050
Naphthalene ug/L ND 1.5 09/08/18 16:561.5
Phenanthrene ug/L ND 0.20 09/08/18 16:560.20
Pyrene ug/L ND 0.10 09/08/18 16:560.10
2-Fluorobiphenyl (S)%115 70-130 09/08/18 16:56
Nitrobenzene-d5 (S)%142 70-130 S309/08/18 16:56
Terphenyl-d14 (S)%61 70-130 S009/08/18 16:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2356655LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2356656
1-Methylnaphthalene ug/L 2.72.5 109 70-130992.5 10 30
2-Methylnaphthalene ug/L 2.82.5 112 70-1301032.6 9 30
Acenaphthene ug/L 2.72.5 108 70-1301012.5 7 30
Acenaphthylene ug/L 2.82.5 111 70-1301032.6 7 30
Anthracene ug/L 2.62.5 105 70-1301002.5 5 30
Benzo(a)anthracene ug/L 2.42.5 95 70-130922.3 4 30
Benzo(a)pyrene ug/L 2.62.5 103 70-130892.2 14 30
Benzo(b)fluoranthene ug/L 2.62.5 103 70-130982.5 5 30
Benzo(g,h,i)perylene ug/L 3.4 L12.5 134 70-1301203.0 12 30
Benzo(k)fluoranthene ug/L 2.52.5 98 70-130962.4 3 30
Chrysene ug/L 2.52.5 100 70-130962.4 4 30
Dibenz(a,h)anthracene ug/L 3.3 L12.5 133 70-1301213.0 10 30
Fluoranthene ug/L 2.62.5 105 70-130972.4 8 30
Fluorene ug/L 2.82.5 111 70-1301042.6 7 30
Indeno(1,2,3-cd)pyrene ug/L 3.6 L12.5 145 70-1301293.2 12 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2356655LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2356656
Naphthalene ug/L 2.92.5 115 70-1301052.6 9 30
Phenanthrene ug/L 2.62.5 105 70-1301032.6 2 30
Pyrene ug/L 2.62.5 103 70-130962.4 7 30
2-Fluorobiphenyl (S)%S013270-130105
Nitrobenzene-d5 (S)%S015170-130119
Terphenyl-d14 (S)%S08170-13067
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92396262
SIRRON P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
425891
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92396262001, 92396262002, 92396262003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92395938002
2354468SAMPLE DUPLICATE:
Percent Moisture %15.2 4 2514.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92396313001
2354469SAMPLE DUPLICATE:
Percent Moisture %18.6 1 2518.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 54
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92396262
SIRRON P2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Initial calibration evaluation met acceptance criteria. Compound did not meet additional accuracy assessment for percent
error1g
Initial calibration evaluation met acceptance criteria. Compound did not meet additional accuracy assessment for percent
error.2g
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.IO
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 54
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92396262
SIRRON P2
ANALYTE QUALIFIERS
Surrogate recovery outside laboratory control limits (confirmed by re-analysis).S1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 54
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92396262
SIRRON P2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92396262001 426122 426370HA-1 (13-14)EPA 3546 EPA 8270D by SIM
92396262002 426122 426370HA-2 (7-8)EPA 3546 EPA 8270D by SIM
92396262003 426122 426370SB-1 (20-21)EPA 3546 EPA 8270D by SIM
92396262004 426382 427014TMW-1 EPA 3511 EPA 8270D by SIM
92396262005 426382 427014MW-4 EPA 3511 EPA 8270D by SIM
92396262006 426382 427014SE-MW-4 EPA 3511 EPA 8270D by SIM
92396262007 426382 427014MW-5 EPA 3511 EPA 8270D by SIM
92396262004 426920TMW-1 EPA 8260B
92396262005 426703MW-4 EPA 8260B
92396262006 426703SE-MW-4 EPA 8260B
92396262007 426920MW-5 EPA 8260B
92396262001 425903 425924HA-1 (13-14)EPA 5035A EPA 8260B
92396262002 425903 425924HA-2 (7-8)EPA 5035A EPA 8260B
92396262003 425903 425924SB-1 (20-21)EPA 5035A EPA 8260B
92396262001 425891HA-1 (13-14)ASTM D2974-87
92396262002 425891HA-2 (7-8)ASTM D2974-87
92396262003 425891SB-1 (20-21)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/10/2018 10:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 54
Page 52 of 54
Page 53 of 54
Page 54 of 54