MO-7074_40162_CA_MRP_20210331

SUBSEQUENT MONITORING REPORT
Hull’s 66 (Incident #40162)
6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
March 31, 2021
Terracon Project No. 71179011A

Prepared for:
North Carolina Department of Environmental Quality
Division of Waste Management
Raleigh, North Carolina

Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina

Terracon Consultants, Inc. 2701 Westport Road Charlotte, NC 28208
P 704-509-1777 F 704-509-1888 terracon.com
March 31, 2021
Mr. Mark Petermann
North Carolina Department of Environmental Quality
Division of Waste Management
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Email: [e-mail]
Re: Subsequent Monitoring Report
Hull’s 66
6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
UST Incident Number: 40162
Terracon Project No. 71179011A
Dear Mr. Petermann:
Terracon Consultants, Inc. (Terracon) is pleased to submit this Subsequent Monitoring Report for
the above referenced property. This report has been prepared in general accordance with North
Carolina Department of Environmental Quality (NCDEQ), UST Section Guidelines for Assessment
and Corrective Action for UST Releases, dated July 15, 2008, revised December 2020 and Task
Authorization No. 01, approved on January 13, 2021.
If you have any questions regarding this report or the assessment activities, please contact us at
704-509-1777.
Sincerely,
Terracon Consultants, Inc.
Victoria M. Larson, GIT M.Neal McElveen, P.E
Field Geologist Principal/Environmental Services Manager
Attachments

Table of Contents
A. SITE INFORMATION ...................................................................................................................... 1
B. EXECUTIVE SUMMARY ................................................................................................................. 2
C. SITE HISTORY AND CHARACTERIZATION ............................................................................. 4
C.1 Site Setting ................................................................................................................................................ 4
C.2 Release Summary ...................................................................................................................................... 4
C.3 Previous Investigations ............................................................................................................................. 4
C.4 Water Supply Wells ................................................................................................................................... 7
C.5 Surface Water ........................................................................................................................................... 7
C.6 Land Use Information ................................................................................................................................ 7
D. ASSESSMENT INFORMATION ................................................................................................. 7
D.1 Site Geology and Hydrogeology ....................................................................................................................... 7
D.2 Sampling Activities .................................................................................................................................... 8 D.2.1 Free Product Evaluation ............................................................................................................................... 8
D.2.2 Groundwater Sampling Activities ................................................................................................................. 8
D.2.3 Analytical Results ......................................................................................................................................... 9
E. CONCLUSIONS AND RECOMMENDATIONS ................................................................ 9
FIGURES
Figure 1: Site Location Map
Figure 2: Site Plan
Figure 3: Water Supply Well Location Map
Figure 4: Groundwater Contour Map
Figure 5: Groundwater Analytical Results

TABLES
Table 1: Historical UST Information
Table 2: Water Supply Well Information
Table 3: Summary of Groundwater Analytical Results
Table 4: Monitoring Well Construction Information and Historical Groundwater
Elevations
APPENDIX
Appendix A: Laboratory Analytical Results and Chain of Custody Forms
Appendix B: Field Notes
Appendix C: Photographs
Hull’s 66 Vale, North Carolina Project Number 71179011A Incident No. 40162 March 31, 2021

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SUBSEQUENT MONITORING REPORT
A. SITE INFORMATION
Date of Report: March 31, 2021
NCDEQ Incident No: 40162
Facility ID: 0-014302
Site Name: Hull’s 66
Site Location: 6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
Latitude: N 35o 30’ 33.31”
Longitude: W 81o 27’ 29.63”
UST Owner/Operator: Petroleum World, Inc.
681 NC Highway 120
Mooresboro, North Carolina 28114
Current Property Owner: Mr. Harrel D. Hull
6711 Highway 27 West
Vale, North Carolina 28168

Current Property
Occupant: Automotive Repair Facility
Consultant: Terracon Consultants, Inc. (Contact: Victoria Larson) 2701 Westport Road
Charlotte, North Carolina 28208 [phone]
Laboratory: Pace Analytical (NCDEQ No. 5342)
9800 Kincey Avenue
Huntersville, North Carolina 28028
704-875-9092
Release Information: Release Discovery Date: January 22, 2013
Estimated Quantity: Unknown
Cause of Release: Unknown
Source of Release: Former UST System
Currently Active Tanks: None – Tanks were reportedly removed in
January 2013

Hull’s 66 Vale, North Carolina Project Number 71179011A Incident No. 40162 March 31, 2021

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I, M. Neal McElveen, a Professional Engineer for Terracon Consultants, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.

M. Neal McElveen, P.E.
NC License No. 20699

Terracon Consultants, Inc. is licensed to practice geology/engineering in North Carolina. The certification number of the corporation is F-0869.
B. EXECUTIVE SUMMARY
The purpose of this report is to evaluate the current status of the groundwater quality at the Hull’s 66
site. Terracon completed this report to summarize the findings of assessment activities performed
on February 3, 2021. The site is located at 6711 NC Highway 27 West in Vale, Lincoln County,
North Carolina in an area primarily developed as rural residential. The former on-site gasoline
station is currently occupied by an automotive repair shop.

Based on regulatory file review information, the site formerly operated one 4,000-gallon gasoline
UST, one 6,000-gallon gasoline UST, one 10,000-gallon gasoline UST, one 4,000-gallon diesel
UST, and one 2,000-gallon kerosene UST associated with former on-site fueling operations. A
potential release was discovered in January 2013 during the removal of the five USTs by Shield
Engineering, Inc. (Shield). A 24-Hour Release and UST Leak Reporting Form (UST-61) was
submitted to the NCDEQ on January 22, 2013. The suspected release(s) were associated with the
operations of the five USTs and the associated fuel dispensers. Shield also removed accessible
petroleum impacted soils from the Hull’s 66 property in January 2013.

Terracon mobilized to the site on February 3, 2021 to sample monitoring wells MW-1 through MW-
10, DMW-1, and water supply well WSW-10. Terracon personnel also exchanged the ORC inserts
in wells MW-2, MW-4 and MW-10 with new inserts. Initially, Terracon gauged the groundwater
levels in the monitoring wells and then purged a minimum of three well volumes from each well.
During this sampling event, depth to groundwater ranged from approximately 15.07 feet below top of
casing (btoc) in well MW-9 to 19.38 feet btoc in well MW-2. Based on the water level
measurements, the groundwater flow direction is to the north-northwest. Prior to collecting a sample
from well WSW-10, water was allowed to flow for about 15 minutes from the spigot. Flow was
reduced when the sample was collected.

According to the laboratory analytical report the following constituents were detected above their
respective 15A NCAC 2L groundwater standards: EDB (1.0 micrograms per liter [µg/L]) and 1,2-
dichloroethane (0.80 µg/L) in well MW-2; bromodichloromethane (0.92 µg/L), EDB (0.46J µg/L) and
Hull’s 66 Vale, North Carolina Project Number 71179011A Incident No. 40162 March 31, 2021

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1,2-dichloroethane (0.65 µg/L) in well MW-5; bromodichloromethane in well MW-6 (1.8 µg/L); and,
benzene (42.7 µg/L) in well MW-10. Various other constituents were detected in wells MW-1, MW-2,
MW-5, MW-6, MW-, MW-10 and DMW-1 at concentrations below their respective 2L standards. No
petroleum constituents were identified in monitoring wells MW-3, MW-4, MW-7 and MW-9 or water
supply well WSW-10 at concentrations above the laboratory minimum detection limits (MDLs).

Based on information obtained during the completion of these assessment activities, Terracon
provides the following conclusions and findings.

Free product was not encountered at the site.
None of the detected constituents exceeded the Gross Contaminant Levels (GCLs).
Benzene, bromodichloromethane, 1,2-dichloroethane and EDB were detected at concentrations
above their respective 2L standards in one or more on-site wells.
Various petroleum constituents were detected in on-site wells MW-1, MW-2, MW-5, MW-6, MW-8,
MW-10 and DMW-1 at concentrations below their respective 2L standards. No petroleum
constituents were identified in monitoring wells MW-3, MW-4, MW-7 and MW-9 at concentrations
above the MDLs.
O-Sox inserts were replaced in wells MW-2, MW-4 and MW-10 during this sampling event.
The estimated groundwater flow direction at the site is to the northwest.
Generally, constituent concentrations appear to be stable or are decreasing in the wells on the site
but appear to have increased slightly during this sampling event.
Low levels of Chloroform and/or bromodichloromethane were detected in wells MW-2, MW-5, MW-
6, MW-8 and DMW-1. Chloroform and bromodichloromethane are compounds often found in
disinfection of public water supply and the detected concentrations could be related to a public
water supply line leak.
No constituents of concern were detected in water supply well WSW-10 above the MDLs.
Thirty-four water supply wells are reportedly located within 1500 feet of the source area including
on-site inactive well WSW-1 and WSW-2 which was demolished in 2019.
Based on the findings of our assessment activities, the following comments and recommendations are
provided for the site.
Terracon recommends performing a Fate and Transport model on the site to provide
documentation that down-gradient receptors will be unaffected by site contaminants.
Terracon recommends that the on-site water supply well (WSW-1) be abandoned.
Terracon recommends performing a in depth file review on the adjacent eastern property across
Highway 274 to determine the if the contamination source effecting well MW-10 is associated with
a unrelated incident. MW-10 has abnormally high concentration of petroleum constituents
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compared to other on-site wells considering undetectable levels of petroleum constituents in wells
MW-3 and MW-4 which are positioned between the source area and MW-10.
C. SITE HISTORY AND CHARACTERIZATION
The purpose of this report is to evaluate the current status of the groundwater quality at the Hull’s 66
site. Terracon completed this report to summarize the findings of assessment activities performed
on February 3, 2021. The site is located at 6711 NC Highway 27 West in Vale, Lincoln County,
North Carolina (Figure 1). This Subsequent Monitoring Report was prepared for the site in response
to a request by NCDEQ Incident Manager, Mr. Mark Peterman with the NCDEQ Division of Waste
Management, State Lead Program.

The Subsequent Monitoring Report was prepared in general accordance with the 15A NCAC
2L.0115 regulations and the NCDEQ Underground Storage Tank (UST) Section Guidelines for
Assessment and Corrective Action for UST Releases, dated July 15, 2008, revised December 2020,
under the supervision of Mr. M. Neal McElveen, a North Carolina registered professional engineer
(North Carolina License No. 20699).

C.1 Site Setting
The site is located within an area primarily developed as rural residential with a few commercial
properties. A church is located approximately 400 feet to the northeast and a commercial building is
located on the adjacent property to the west. Specific land uses are further described in Section C.6
below.

C.2 Release Summary
Based on regulatory file review information, the site formerly operated one 4,000-gallon gasoline
UST, one 6,000-gallon gasoline UST, one 10,000-gallon gasoline UST, one 4,000-gallon diesel
UST, and one 2,000-gallon kerosene UST associated with former on-site fueling operations. A
potential release was discovered in January 2013 during the removal of the five USTs by Shield. A
24-Hour Release and UST Leak Reporting Form (UST-61) was submitted to the NCDEQ on
January 22, 2013. The suspected release(s) were associated with the operations of the five USTs
and the associated fuel dispensers. Shield also removed accessible petroleum impacted soils from
the Hull’s 66 property in January 2013. Historical UST information is provided in Table 1.

C.3 Previous Investigations
On January 7 and 8, 2013, Shield removed five USTs, the associated product lines and fuel
dispensers from the site. The USTs included one diesel UST, three gasoline USTs, and one
kerosene UST. Nine of the 25 confirmation soil samples collected beneath the tanks and product
lines indicated TPH-GRO and TPH-DRO concentrations above the NCDEQ action levels. Over-
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excavation of petroleum impacted soils was conducted in the areas of the product lines and fuel
dispensers in January 2013. The total depths of the excavations ranged from 5 feet to 15 feet bgs.

In July 2013, Shield completed a Limited Site Assessment (LSA) at the site by installing monitoring
well MW-1 south of the former dispenser island. According to the LSA, aliphatic range compounds,
methyl tert-butyl ether (MTBE) and acetone were detected in soil samples collected from the boring
for well MW-1 at concentrations below the NCDEQ Soil-to-Water Maximum Soil Contaminant
Concentrations (MSCCs). The groundwater sample collected from well MW-1 indicated
concentrations of lead, EDB, and dibromochloromethane were detected above their respective 2L
standards. As part of the LSA, Shield conducted a receptor survey. The closest active water supply
well, WSW-10, is located approximately 270 feet southwest of the source area. A pond located
approximately 420 feet north of the source area appears to be the closest surface water.

Based on the results from the 2013 LSA, the NCDEQ requested a Comprehensive Site Assessment
(CSA) for the Hull’s 66 site. In May and December 2014, fifteen soil borings were advanced at the
site to delineate the petroleum impacted soils near the former fuel dispensers and tank basins.
Shield determined soil contamination was limited laterally to areas beneath the former dispenser
island and did not extend vertically more than 15 feet below the ground surface (bgs). Delineation
activities determined contamination in the soils did not extend beyond the site boundaries.

In May 2014, Shield installed shallow monitoring wells MW-2 through MW-5 at the site. Analytical
results of the groundwater samples collected from wells MW-1 through MW-5 detected EDB,
benzene, total xylenes, 1,2-dichloroethane, naphthalene, and MTBE at concentrations exceeding
their respective 2L standards. EDB was also detected in well MW-5 above its GCL.

In December 2014, monitoring wells MW-6 through MW-9 and deep monitoring well DMW-1 were
installed at the site. Based on the laboratory results, dibromochloromethane was detected in well
MW-6 and EDB was detected in monitoring well MW-9 above their respective 2L standards. During
this sampling event, the average horizontal hydraulic gradient was calculated at approximately 0.022
feet/foot at the site. Additionally, water supply wells WSW-1, WSW-2 and WSW-10 were sampled.
No analyzed constituents were detected above the MDLs in the three water supply wells.

In April 2015, Shield conducted slug testing at monitoring wells MW-2, MW-5 and DMW-1. The
average estimated groundwater velocity for the shallow aquifer was calculated at 18.29 feet/year
while the groundwater velocity of the bedrock aquifer was estimated at 247.68 feet/year.

In July and October 2015, groundwater samples were collected from wells MW-1 through MW-5 and
DWM-1. Various petroleum constituents were detected above their respective 2L standards in the
wells and EDB was detected above its GCL in monitoring well MW-2.

In August 2017, groundwater samples were collected from monitoring wells MW-1 through MW-5
and water supply well WSW-10. Various petroleum constituents were detected above their
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respective 2L standards in wells MW-2, MW-4 and MW-5.

In March 2018, Terracon mobilized to the site to collect groundwater samples from wells MW-1
through MW-5. During this sampling event, depth to groundwater ranged from approximately 22.72
feet (well MW-4) to 24.50 feet (well MW-1) btoc. Terracon was unable to sample water supply wells
WSW-2 and WSW-10. Petroleum constituents were detected above their respective 2L standards
in wells MW-2 and MW-5. Various other constituents were detected in wells MW-2, MW-4 and MW-
5 at concentrations below their respective 2L standards. No petroleum constituents were identified in
wells MW-1 or MW-3 above the MDLs. Terracon recommended installing O-Sox inserts in wells
MW-2 and MW-5, abandonment of the inactive on-site water supply well, and semi-annual sampling
of the on-site groundwater monitoring wells.

In October 2018, Terracon collected groundwater samples from wells MW-1 through MW-5 and
water supply wells WSW-10. During this sampling event, depth to groundwater ranged from
approximately 21.13 feet (well MW-5) to 23.24 feet (well MW-2) btoc. Terracon was unable to
sample water supply well WSW-2. Petroleum constituents were detected above their respective 2L
standards in wells MW-2, MW-4 and MW-5. No petroleum constituents were identified in wells MW-
1 or MW-3 above the MDLs. Terracon recommended installing O-Sox inserts in wells MW-2, MW-4
and MW-5, abandonment of the inactive on-site water supply well, semi-annual sampling of the
groundwater monitoring wells, and installation of a monitoring well to the northeast of well MW-4.

In June 2019, Terracon mobilized to sample monitoring wells MW-1 through MW-9 and DMW-1, and
water supply wells WSW-2 and WSW-10. During this sampling event, depth to groundwater ranged
from approximately 15.30 feet btoc in well MW-9 to 19.33 feet btoc in well MW-2. Terracon was
unable to sample water supply wells WSW-2 and WSW-10. Later in June 2019, Terracon re-
mobilized to the site to install and collect water samples from monitoring well MW-10 located
northeast of the site, across NC Highway 27. Various petroleum constituents were detected above
their respective 2L groundwater standards in wells MW-1, MW-2, MW-4, MW-5, MW-6 and MW-10.
No petroleum constituents were identified in monitoring wells MW-3 and MW-8 at concentrations
above the MDLs. Terracon recommended semi-annual sampling of the groundwater monitoring
wells at the site.

In March 2020, Terracon mobilized to sample monitoring wells MW-1 through MW-10, DMW-1, and
water supply wells WSW-2 and WSW-10. Terracon personnel also exchanged the ORC inserts in
wells MW-2, MW-4, MW-5 and MW-10 with new inserts. The residence associated with well WSW-2
had been demolished and the well was no longer active; thus, the well was not sampled. During this
sampling event, depth to groundwater ranged from approximately 15.81 btoc in well MW-9 to 19.62
feet btoc in well MW-2. Various petroleum constituents were detected above their respective 2L
groundwater standards in wells MW-2, MW-5, MW-6 and MW-10. Various other constituents were
detected in wells MW-1, MW-2, MW-5, MW-6, MW-8, MW-10 and DMW-1 at concentrations below
their respective 2L standards. No petroleum constituents were identified in monitoring wells MW-3,
MW-4, MW-7 and MW-9 or water supply well WSW-10 at concentrations above MDLs.
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C.4 Water Supply Wells
Thirty-four water supply wells have been identified within 1,500 feet of the source area. Five water
supply wells (WSW-1, WSW-2, WSW-9, WSW-10 and WSW-16) were identified within 500 feet of
the source area. Well WSW-1 is located on the site but is currently inactive. Well WSW-2 was
destroyed in 2019. The closest active water supply well, WSW-10, is located approximately 270 feet
south of the source area. Thirteen water supply wells are located between 500 and 1,000 feet of
the source area while 16 water supply wells are located between 1,000 and 1,500 feet from the
source area. Municipal water is available to properties located east of the site and to the site itself.
Water supply well information is summarized in Table 2. The approximate locations of the identified
water supply wells are shown on Figure 3.

C.5 Surface Water
A pond and an unnamed tributary of Little Indian Creek are located approximately 370 feet north of
the site. Surface waters are depicted on Figure 1.

C.6 Land Use Information
The site is currently occupied by an automotive repair facility. The adjoining properties to the north,
across NC Highway 27 West, are primarily wooded land. A church is located to the northeast. The
adjoining properties to the east and south are a mixture of single-family residences, storage
buildings, and grass-covered land. The adjacent properties to the west consist of grass and gravel
covered land and a commercial building. The site and surrounding properties are depicted in
Figures 1 and 2.

D. ASSESSMENT INFORMATION
D.1 Site Geology and Hydrogeology
The following resources were reviewed to evaluate site-specific geological and hydrogeological
characteristics.
Banoak, North Carolina, USGS 7.5-minute topographic map, dated 2003 (Figure 1).
Geologic Map of North Carolina, dated 1985.
The Geology of the Carolinas, Carolina Geological Society Fiftieth Anniversary Volume, edited by
J. Wright Horton, Jr., and Victor A. Zullo, The University of Tennessee Press, dated 1991.
Soil Survey of Lincoln County, North Carolina, US Department of Agriculture, Natural Resources
Conservation Service, Web Soil Survey via the Internet, http://websoilsurvey.nrcs.usda.gov/app/.

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The site is located within the Inner Piedmont Belt of the Piedmont Physiographic Province. The
Piedmont Physiographic Province generally consists of low to medium elevation, rounded hills and
long rolling northeast to southwest trending ridges with incised creeks and river channels.
Underlying bedrock in the site area consists of mica schist intruded by pegmatites.

In-place chemical and physical weathering of parent rocks typically form residual soils in the
Piedmont region. Weathering is facilitated by the presence of fractures, joints, and less resistant
minerals in the rock. In areas not altered by erosion, alluvial deposition or the activities of man, the
typical residual soil profile consists of clay-rich unconsolidated materials at the surface, transitioning
to sandy silts and silty sands at depth. Typically, the boundary between soil and rock is not sharply
defined. This transitional zone is termed “partially weathered rock” or saprolite. Information obtained
from the Web Soil Survey for Lincoln County, depicts soils at the site as Cecil sandy clay loam
(CeB2).

In the Piedmont, groundwater generally occurs in pore spaces within soils and in the structural
features present in the underlying rock (i.e. joints, fractures, and faults). Recharge to the water table
is primarily by precipitation infiltrating the surficial soils and percolating downward under the
influence of gravity to the water table (vadose zone). Typically, the water table is not a level surface,
but a subdued reflection of the land surface. The depth to the water table is not consistent and is
dependent upon several factors that include the amount of rainfall, permeability of the soil, the
extent of fracturing in the underlying rock and the influences of groundwater pumping. Groundwater
typically flows in directions parallel to the ground surface and under the influence of gravity, migrates
to discharge points such as surface water features, the toes of slopes or natural springs.

Fluctuations in the depth of the water table can be expected depending on variations in precipitation,
surface water run-off and other factors not evident at the time of our subsurface exploration.
Normally, the highest levels of the water table occur in late winter and spring and the lowest levels
occur in the late summer and fall. Based on an interpreted groundwater flow direction from historical
data, groundwater is expected to flow to the northwest from the site. Currently, groundwater
appears to flow to the northwest.

D.2 Sampling Activities
D.2.1 Free Product Evaluation
Free product was not encountered at the site.

D.2.2 Groundwater Sampling Activities
Terracon mobilized to the site on February 3, 2021 to sample monitoring wells MW-1 through MW-
10, DMW-1, and water supply well WSW-10. The approximate locations of the monitoring wells are
shown on Figure 2. Terracon personnel also exchanged the ORC inserts in wells MW-2, MW-4 and
MW-10 with new inserts. Initially, Terracon gauged the groundwater levels in the monitoring wells
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and then purged a minimum of three well volumes from each well. During this sampling event, depth
to groundwater ranged from approximately 15.07 feet btoc in well MW-9 to 19.38 feet btoc in well
MW-2. Based on the water level measurements, the groundwater flow direction is to the north-
northwest (Figure 4). Current and historical groundwater depth measurements are provided in
Table 4. Prior to collecting a sample from well WSW-10, water was allowed to flow for about 15
minutes from the spigot. Flow was reduced when the sample was collected. A copy of Terracon’s
field notes is included in Appendix B.

The groundwater samples were placed in laboratory-supplied glassware, labeled and stored in an
ice-packed cooler. The samples, along with chain-of-custody documentation, were delivered to Pace
Analytical Services, Inc. in Huntersville, North Carolina for analysis of VOCs by Standard Method
6200B including MTBE, IPE and EDB.

D.2.3 Analytical Results
According to the laboratory analytical report the following constituents were detected above their
respective 15A NCAC 2L groundwater standards: EDB (1.0 µg/L) and 1,2-dichloroethane (0.80
µg/L) in well MW-2; bromodichloromethane (0.92 µg/L), EDB (0.46J µg/L) and 1,2-dichloroethane
(0.65 µg/L) in well MW-5; bromodichloromethane in well MW-6 (1.8 µg/L); and, benzene (42.7 µg/L)
in well MW-10. Various other constituents were detected in wells MW-1, MW-2, MW-5, MW-6, MW-,
MW-10 and DMW-1 at concentrations below their respective 2L standards. No petroleum
constituents were identified in monitoring wells MW-3, MW-4, MW-7 and MW-9 or water supply well
WSW-10 at concentrations above the laboratory MDLs. The groundwater analytical results are
summarized in Table 3 and are depicted on Figure 5. A copy of the laboratory analytical report is
provided in Appendix A.
E. CONCLUSIONS AND RECOMMENDATIONS
Based on information obtained during the completion of these assessment activities, Terracon
provides the following conclusions and findings.

Free product was not encountered at the site.
None of the detected constituents exceeded the Gross Contaminant Levels (GCLs).
Benzene, bromodichloromethane, 1,2-dichloroethane and EDB were detected at concentrations
above their respective 2L standards in one or more on-site wells.
Various petroleum constituents were detected in on-site wells MW-1, MW-2, MW-5, MW-6, MW-8,
MW-10 and DMW-1 at concentrations below their respective 2L standards. No petroleum
constituents were identified in monitoring wells MW-3, MW-4, MW-7 and MW-9 at concentrations
above the MDLs.
O-Sox inserts were replaced in wells MW-2, MW-4 and MW-10 during this sampling event.
Hull’s 66 Vale, North Carolina Project Number 71179011A Incident No. 40162 March 31, 2021
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The estimated groundwater flow direction at the site is to the northwest.
Generally, constituent concentrations appear to be stable or are decreasing in the wells on the site
but appear to have increased slightly during this sampling event.
Low levels of Chloroform and/or bromodichloromethane were detected in wells MW-2, MW-5, MW-
6, MW-8 and DMW-1. Chloroform and bromodichloromethane are compounds often found in
disinfection of public water supply and the detected concentrations could be related to a public
water supply line leak.
No constituents of concern were detected in water supply well WSW-10 above the MDLs.
Thirty-four water supply wells are reportedly located within 1500 feet of the source area including
on-site inactive well WSW-1 and WSW-2 which was demolished in 2019.
Based on the findings of our assessment activities, the following comments and recommendations are
provided for the site.
Terracon recommends performing a Fate and Transport model on the site to provide
documentation that down-gradient receptors will be unaffected by site contaminants.
Terracon recommends that the on-site water supply well (WSW-1) be abandoned.
Terracon recommends performing a in depth file review on the adjacent eastern property across
Highway 274 to determine the if the contamination source effecting well MW-10 is associated with
a unrelated incident. MW-10 has abnormally high concentration of petroleum constituents
compared to other on-site wells considering undetectable levels of petroleum constituents in wells
MW-3 and MW-4 which are positioned between the source area and MW-10.

FIGURES
SITE LOCATION MAP
Hull’s 66 (Incident #40162)
6711 NC Highway 27 West
Vale, Lincoln County, NC
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY
QUADRANGLES INCLUDE: BANOAK, NC (1/1/2003) and CHERRYVILLE, NC (1/1/2003).
2701 Westport Road
Charlotte, NC
71179011A
Project Manager:
Drawn by:
Checked by:
Approved by:
VML
MNM
MNM
1”=2,000’
71179011A.1
March 2021
Project No.
Scale:
File Name:
Date: 1
ExhibitVML
APPROXIMATE
SITE BOUNDARY
2
Figure
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES 2701 Westport Road
Charlotte, NC
Site PlanProject Manager:
Drawn by:
Checked by:
Approved by:
VML
Project No.
File Name:
Date:
Scale:
71179011
VML
March 2021MNM
MNM 71179011.2
Hull’s 66 (Incident #40162)
6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
denotes groundwater
monitoring well.
1” = 35 ft.
Parking Lot
Parking Lot
Grassed Area
Grassed Area
Grassed Area
MW-8
MW-9
MW-7
MW-6
MW-5
MW-4
MW-3
DMW-1
MW-2
MW-1
Auto Repair Shop
Former UST
Basin
Former Dispenser
Island
MW-10
Water Supply Well Location Map
2701 Westport Road
Charlotte, NC 28208
DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS
NOT INTENDED FOR CONSTRUCTION PURPOSES
3
Figure
denotes water supply well
1,500 ft. Radius
(from release location)
1,000 ft. Radius
(from release location)
500 ft. Radius
(from release location)
Hull’s 66 (Incident #40162)
6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
Project Manager:
Drawn by:
Checked by:
Approved by:
VML Project No.
File Name:
Date:
Scale:
71179011A
VML
MNM March 2021
MNM
1”~ 375’
71179011A.3
WSW-29
WSW-31
WSW-30 WSW-35
WSW-32
WSW-34
WSW-33
WSW-28
WSW-1
WSW-10
WSW-16
WSW-2
WSW-9
WSW-15
WSW-14
WSW-13
WSW-12
WSW-11 WSW-17
WSW-4
WSW-3WSW-18WSW-19
WSW-21
WSW-22
WSW-25
WSW-23 WSW-5
WSW-24 WSW-7
WSW-8
WSW-6
WSW-27
WSW-26
4
Figure
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES 2701 Westport Road
Charlotte, NC
Groundwater Contour MapProject Manager:
Drawn by:
Checked by:
Approved by:
VML
Project No.
File Name:
Date:
Scale:
71179011A
VML
March 2021MNM
MNM 71179011A.4
Hull’s 66 (Incident #40162)
6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
denotes approximate site
boundary
denotes groundwater
monitoring well.
1” = 35 ft.
estimated groundwater contour
estimated groundwater flow
direction
Parking Lot
Parking Lot
Grassed Area
Grassed Area
Grassed Area
MW-8
MW-9
MW-7
MW-6
MW-5
MW-4
MW-3
DMW-1
MW-2
MW-180.30’80.60’
79.03’
78.99’
80.70’
80.5’
80’
Auto Repair Shop
Former UST
Basin
MW-10
80.31’
80.34’
80.29’
80.51’
80.71’
5
Figure
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES 2701 Westport Road
Charlotte, NC
Groundwater Analytical ResultsProject Manager:
Drawn by:
Checked by:
Approved by:
VML
Project No.
File Name:
Date:
Scale:
71179011A
VML
March 2021MNM
MNM 71179011A.5
Hull’s 66 (Incident #40162)
6711 NC Highway 27 West
Vale, Lincoln County, North Carolina
denotes groundwater
monitoring well.
1” = 35 ft.
Parking Lot
Parking Lot
Grassed Area
Grassed Area
Grassed Area
MW-8
MW-9
MW-7
MW-6
MW-5
MW-4
MW-3
DMW-1
MW-2
MW-1
Auto Repair Shop
Sample ID: MW-5
Groundwater Sample
6200 –Bromodichloromethane: 0.92 µg/L
Chloroform: 7.2 µg/L
EDB: 0.46J µg/L
1,2-Dichloroethane: 0.65 µg/L
Ethylbenzene: 0.62 µg/L
Isopropylbenzene: 0.60 µg/L
MTBE: 0.69 µg/L
Naphthalene: 3.2 µg/L
1,3,5-Trimethylbenzene: 8.6 µg/L
Total Xylenes: 9.1 µg/L
*Values above 2L Standards are in bold.
Sample ID: MW-4
Groundwater Sample
6200 – No target analytes detected.
Sample ID: MW-2
Groundwater Sample
6200 – Chloroform: 0.62 µg/L
EDB: 1.0 µg/L
1,2-Dichloroethane: 0.80 µg/L
Ethylbenzene: 23.5 µg/L
Isopropylbenzene: 1.6 µg/L
MTBE: 0.92 µg/L
Naphthalene: 22.8 µg/L
Toluene: 18.0 µg/L
1,2,4-Trimethylbenzene: 113 µg/L
1,3,5-Trimethylbenzene: 75.8 µg/L
Total Xylenes: 430 µg/L
*Values above 2L Standards are in bold.
Sample ID: MW-3
Groundwater Sample
6200 – No target analytes detected.
MW-10
Sample ID: MW-1
Groundwater Sample
6200 – 1,2-Dichloroethane: 0.38J µg/L
*Values above 2L Standards are in bold.
Sample ID: MW-6
Groundwater Sample
6200 –Bromodichloromethane: 1.8 µg/L
Chloroform: 21.2 µg/L
1,2-Dichloroethane: 0.27J µg/L
*Values above 2L Standards are in bold.
Sample ID: MW-7
Groundwater Sample
6200 – No target analytes detected.
Sample ID: MW-8
Groundwater Sample
6200 – Chloroform: 0.75 µg/L
Sample ID: DMW-1
Groundwater Sample
6200 – Chloroform: 0.82 µg/L
Ethylbenzene: 0.36J µg/L
Naphthalene: 0.87J µg/L
1,2,4-Trimethylbenzene: 0.5 µg/L
*Values above 2L Standards are in bold.
Sample ID: MW-9
Groundwater Sample
6200 – No target analytes detected.
Sample ID: MW-10
Groundwater Sample
6200 –Benzene : 42.7 µg/L
n-Butylbenzene: 2.5 µg/L
Ethylbenzene: 103 µg/L
Isopropylbenzene: 26.3 µg/L
Naphthalene: 10.4 µg/L
n-Propylbenzene: 10 µg/L
Toluene: 1.7 µg/L
1,2,4-Trimethylbenzene: 34.8 µg/L
1,3,5-Trimethylbenzene: 19.2 µg/L
Total Xylenes: 55.9 µg/L
*Values above 2L Standards are in bold.

TABLES

TABLE 1
Historical UST Information
Hull's 66
Vale, North Carolina
Terracon Project No. 71179011A
NCDEQ Incident No. 40162
Contents Capacity (gallons)Date Installed Date Closed Closed/Active Release from
System
Gasoline 4,000 Unknown 1/7-8/2013 Closed Yes
Gasoline 6,000 Unknown 1/7-8/2013 Closed Yes
Gasoline 10,000 Unknown 1/7-8/2013 Closed Yes
Diesel 4,000 Unknown 1/7-8/2013 Closed Yes
Kerosene 2,000 Unknown 1/7-8/2013 Closed Yes
TABLE 2Water Supply Well Information
Hull's 66Vale, North Carolina
Terracon Project No. 71179011ANCDEQ Incident No. 40162
Well ID Property Owner Property Address Mailing Address Distance/Direction from source area (in feet)Well Status/Use Parcel No.Notes
WSW-1 Harrel Daniel Hull 6711 NC 27 West 6711 NC 27 West Site Inactive 2664-89-5311 Not in use. Pump removed.
WSW-2 Sandra R. Baxter 6757 NC 27 West 6964 Gene Baxter Lane 425 ft / northwest Inactive 2664-89-1505 No structures on site.
WSW-3 & WSW-4 Ruby & Kenneth Lingerfelt 7229 Hallman Mill road 7229 Hallman Mill Road 960 ft / west & 1,045 ft / west Active 2664-79-6269
WSW-5 Jerry & Crystal Tallent 6789 NC 27 West 6871 NC 27 West 730 ft / northwest Active 2664-79-8710
WSW-6 Ginger & Dean Lutz 6810 NC 27 West PO Box 936, Lincolnton, NC 28093 940 ft / northwest Inactive 2664-70-6094 No structures on site.
WSW-7 Tonga Sheena & Nioka Hoppenjans 6762 NC 27 West 6762 NC 27 West 740 ft / northwest Active 2664-89-1933
WSW-8 Wendy Clarke 6766 NC 27 West 6766 NC 27 West 600 ft / northwest Active 2664-89-0797
WSW-9 Johnny & Kathleen Campa 6752 NC 27 West 1081 Cedar Grove Church Road 365 ft / northwest Active 2664-89-5935
WSW-10 Joshua & Geneva Leatherman 118 NC Highway 274 7764 Matthew Miller Road 270 ft / south Active 2664-89-4127
WSW-11 Carrol Mitchem 167 NC Highway 274 7868 Hallman Mill Road 700 ft / southeast Active 2664-88-8784
WSW-12 Jennifer & Robert Bowen 201 NC Highway 274 201 NC Highway 274 960 ft / southeast Active 2664-88-9488
WSW-13 James & Mary Williams 192 NC Highway 274 192 Highway 274 930 ft / south Active 2664-88-6441
WSW-14 Stanley & Linda Friedland 152 NC Highway 274 7510 Ed Willis Road, Lawndale, NC 28090 725 ft / southwest Unknown 2664-78-8337 Well not observed. Identified on the 2013 Shield survey. Lincoln County could not confirm a well permit.
WSW-15 Jerome K. Brewer 114 NC Highway 274 144 NC Highway 274 570 ft / south Active 2664-89-5814
WSW-16 Grover Graig 134 Nighway 274 134 NC Highway 274 310 ft / southeast Active 2664-89-5020
WSW-17 Ronald M. Taylor 6635 NC Highway 27 West 6635 NC 27 West 880 ft / east Active 2664-98-2867
WSW-18 Lois S. Cook Life Estate c/o Sain Hazel 7253 Hallmand Mill Road 7172 Lackey Road 1,150 ft / west Active 2664-79-4221
WSW-19 Crystal R. Cook 7271 Hallman Mill Road 7172 Lackey Road 1,280 ft / west Active 2664-79-2213
WSW-21 Craig Erneest 291 Cooper Road 291 Cooper Road 1,430 ft / west Active 2664-78-1727
WSW-22 Helen & Jimmy Harbison 7266 Hallmand Mill Road 7266 Hallman Mill Road 1,300 ft / west Active 2664-79-1441
WSW-23 Jerry & Crystal Tallent 0 Hallman Mill Road 6871 NC 27 West 1,150 ft / northwest Active 2664-79-5665
WSW-24 Jeffery D. Tallent 6813 NC 27 West 112 Washington Way, Lagrange, GA 30240 1,110 ft / northwest Active 2664-79-5885
WSW-25 Judy T. Living Trust c/o Fred Houser 6849 NC 27 West 7416 Hallman Mill Road 1,410 ft / nothwest Active 2665-79-3981
WSW-26 Jason L. Willis 130 & 142 North Brook III School Road 131 Morningstar Lane, Lawndale, NC 28090 1,338 ft / north west Active 2664-70-5267
WSW-27 Sheena Willis 6790 NC 27 West 6762 NC 27 West 910 ft / northwest Unknown 2665-70-9315 Well not observed. Identified on the 2013 Shield survey. Lincoln County could not confirm a well permit.
WSW-28 Hull's Grove Baptist Church Hulls Grove Church Road 6670 NC 27 West 1,030 ft / northeast Active 2665-90-1222
WSW-29 Robert A. Bowen Life Estate 217 NC Highway 274 217 NC Highway 274 1,240 ft / southeast Active 2665-98-0273
WSW-30 Mary Wood Powell 6618 NC 27 West 6618 NC 27 West 950 ft / east Active 2664-99-4473
WSW-31 Ronald M. Taylor NC 27 West 6635 NC 27 West 1,080 ft / southeast Active 2664-98-3671
WSW-32 Annita Craig 178 Hulls Grove Church Road 178 Hulls Grove Church Road 1,100 ft / northeast Active 2664-99-6868
WSW-33 Gary & Sharon Crowder 200 Hulls Grove Church Road 200 Hulls Grove Church Road 1,450 ft / east Active 2665-90-7039
WSW-34 Donald B. Craig 216 Hulls Grove Church Road 3171 Cat Square Road 1,450 ft / east Active 2665-90-6167
WSW-35 Doyle & Sheri Boyles 7110 Jake Seagle Road 7110 Jake Seagle Road 1,380 ft / east Active 2664-99-9252
*All addresses are in Vale, Lincoln County unless otherwise indicated.
TABLE 3Summary of Groundwater Analytical Results
Hull's 66 Vale, North Carolina
Terracon Project No. 71179011ANCDEQ Incident No. 40162
EPA 504.1
Contaminant of Concern →
Well/SampleI.D.Date Collected (mm/dd/yy)
1 0.6 70 70 70 70 100 0.4 0.02 0.4 0.6 70 600 70 5 20 6 70 600 0.005 400 400 500 0.02
5,000 400 6,900 8,500 15,000 70,000 NE 400 50 400 600 70,000 84,500 25,000 5,000 20,000 6,000 30,000 260,000 NE 28,500 25,000 85,500 50
7/2/2013 0.94 ND ND ND ND 3.0 ND 1.4 NA ND ND ND ND ND ND 0.79 ND ND 1.9 ND ND 0.98 ND 0.0975/9/2014 ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND 0.54 ND ND ND ND ND ND ND 0.047/17/2015 ND ND ND ND ND 0.51 ND ND NA 0.97 ND ND ND ND ND 1.5 ND ND ND ND ND ND ND 0.05110/19/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.5 ND ND ND ND ND ND ND 0.0338/2/2017 <0.25 ND <0.25 <0.25 ND <0.25 ND <0.25 <0.25 <0.25 ND <0.25 <0.25 <0.25 ND <0.25 <1.0 <0.25 <0.25 ND <0.25 <0.25 <0.50 NA3/2/2018 <0.50 ND <0.50 <0.50 ND <0.50 ND <0.50 <0.50 <0.50 ND <0.50 <0.50 <0.50 ND <0.50 <2.0 <0.50 <0.50 ND <0.50 <0.50 <1.0 NA10/3/2018 <0.25 ND <0.25 <0.25 ND <0.25 <0.25 <0.25 <0.25 <0.25 ND <0.25 <0.25 <0.25 <1.0 <0.25 <1.0 <0.25 <0.25 ND <0.25 <0.25 <0.50 NA
6/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 <0.25 0.51 <0.25 <0.25 <0.25 <0.25 <1.0 0.87 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA
3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 1.5J <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 0.38J <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA5/9/2014 2.2 ND ND ND ND 2.9 ND ND NA 8 ND 1.9 66.3 7.6 ND 7.7 49.8 21.6 137 ND 162 100 454 33.87/17/2015 7.2 ND ND ND ND 5.3 ND ND NA 15.9 ND 4.2 232 16.8 ND 17.0 159 45.9 199 ND 281 184 1,597 59.910/19/2015 7.7 ND ND ND ND 5.4 ND ND 48.3 21.4 ND 6.3 374 25.1 ND 27 102 67.5 394 ND 425 312 2,548 58.38/2/2017 2.1 ND <1.0 <1.0 ND 2.1 ND <1.0 16.1 5.8 ND 1.5J 222 15.4 ND 6.5 87.4 <1.0 107 ND 296 169 1,587 NA
3/2/2018 0.59J ND <1.0 <1.0 ND 1.1 ND <1.0 3.5 2.7 ND 0.59 J 86.9 7.5 ND 2.9 62.5 <1.0 31.8 ND 187 90.9 654 NA
10/3/2018 2.5J ND <1.2 <1.2 ND <1.2 56.7 <1.2 3.7 5.9 ND 1.4J 152 10.5 14.2 6.4 126 <1.2 90.5 ND 371 230 2,076 NA
6/6/2019 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <1.0 <1.0 8.9 3.8 <1.0 <1.0 92.0 6.4 <4.0 4.2 106 18.6 82.6 <1.0 251 183 1,104 NA
3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 0.42J <0.21 <0.40 0.69 0.42J <0.18 <0.33 1.2 <0.24 <1.5 <0.44 1.5J <0.24 0.84 <0.27 <0.19 9.0 24.6 NA
2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 0.62 <0.21 <0.40 1.0 0.80 <0.18 <0.33 23.5 1.6 <1.5 0.92 22.8 <0.24 18.0 <0.27 113 75.8 430.0 NA5/9/2014 ND ND ND ND ND 0.94 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.9 0.91 0.0997/17/2015 ND ND ND ND ND 0.62 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.6 0.92 0.1110/19/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.4 0.78 0.328/2/2017 <0.25 ND <0.25 <0.25 ND <0.25 ND <0.25 <0.25 <0.25 ND <0.25 <0.25 <0.25 ND <0.25 <1.0 <0.25 <0.25 ND <0.25 0.57 <0.50 NA3/2/2018 <0.50 ND <0.50 <0.50 ND <0.50 ND <0.50 <0.50 <0.50 ND <0.50 <0.50 <0.50 ND <0.50 <2.0 <0.50 <0.50 ND <0.50 0.57 <1.0 NA10/3/2018 <0.25 ND <0.25 <0.25 ND <0.25 <0.25 <0.25 <0.25 <0.25 ND <0.25 <0.25 <0.25 <1.0 <0.25 <1.0 <0.25 <0.25 ND <0.25 <0.25 <0.50 NA6/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <1.0 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA5/9/2014 ND ND ND ND ND 1.8 ND ND NA 3.3 ND 0.64 2.4 1.1 ND 2 7.8 0.82 2.7 ND 15.9 14.8 54.6 6.67/17/2015 0.65 ND ND ND ND 1.9 ND ND NA 2.2 ND ND 6.6 1.9 ND 1.5 5.5 1.5 1.5 ND 14.6 14.8 21.5 0.7410/19/2015 1.3 ND 0.84 ND ND 1.8 ND ND ND 1.7 ND ND 6.9 5 ND 0.99 ND 2.7 ND ND 5.6 7 9.91 0.268/2/2017 <0.25 ND <0.25 <0.25 ND 0.66 ND <0.25 <0.25 0.66 ND <0.25 <0.25 0.33J ND <0.25 <1.0 <0.25 <0.25 ND <0.25 0.33J <0.50 NA3/2/2018 <0.50 ND <0.50 <0.50 ND 0.48 J ND <0.50 <0.50 0.36 J ND <0.50 <0.50 <0.50 ND <0.50 <2.0 <0.50 <0.50 ND <0.50 <0.50 <1.0 NA10/3/2018 <0.25 ND <0.25 <0.25 ND <0.25 <0.25 <0.25 <0.25 0.50J ND <0.25 <0.25 0.50J <1.0 <0.25 <1.0 <0.25 <0.25 ND 0.32J 1.2 <0.50 NA6/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 0.52 0.52 <0.25 <0.25 <0.25 <0.25 <1.0 <1.0 <1.0 <0.25 <0.25 <0.25 <0.25 2.2 <0.5 NA3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA
2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA5/9/2014 6.7 ND ND ND ND 21.7 ND 0.84 NA 29.1 ND 6.1 134 10.9 ND 32 141 26.4 44.3 ND 217 183 944 65.97/17/2015 4.3 ND ND ND ND 5.2 ND ND NA 19.1 ND 4.5 108 7.4 ND 24.8 105 18.9 17.3 ND 43.6 47.9 323 0.8810/19/2015 5.4 ND ND ND ND 6.1 ND ND ND 23.4 ND 6.8 111 10 ND 39.2 160 21.3 2.5 ND ND 13.1 51.6 0.238/2/2017 2.6 ND <0.25 <0.25 ND 2.2 ND <0.25 <0.25 9.9 ND 2.4 32 4.9 ND 12.5 20 6.2 0.30J ND <0.25 1.4 1.63 NA3/2/2018 3.3 ND <0.50 <0.50 ND 1.2 ND <0.50 0.30 J 10.5 ND 2.6 19.6 7.9 ND 12.8 17.2 4.5 <0.50 ND <0.50 1.4 9.1 NA10/3/2018 0.56 ND <0.25 0.52 ND 2.3 <0.25 <0.25 <0.25 2.5 ND 0.48J 1.2 2.5 <1.0 2.2 <1.0 <0.25 <0.25 ND <0.25 <0.25 <0.50 NA6/6/2019 <0.25 2.0 <0.25 <0.25 <0.25 15.5 <0.25 <0.25 5.8 1.8 <0.25 0.40J 1.4 0.86 <1.0 2.1 5.3 0.25J 0.67 0.97 11.1 32.8 49.0 NA3/27/2020 <0.24 0.95 <0.35 <0.25 <0.25 8.0 <0.21 <0.40 0.93 0.85 <0.18 <0.33 <0.24 <0.24 <1.5 0.62 1.6J <0.24 <0.23 <0.27 <0.19 1.8 2.4J NA2/3/2021 <0.24 0.92 <0.35 <0.25 <0.25 7.2 <0.21 <0.40 0.46J 0.65 <0.18 <0.33 0.62 0.60 <1.5 0.69 3.2 <0.24 <0.23 <0.27 <0.19 8.6 9.1 NA12/11/2014 ND ND ND ND ND 16.9 ND 3.2 NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/19/2015 ND ND ND ND ND 10.8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA8/2/20173/2/2018
10/3/2018
6/6/2019 <0.25 3.1 <0.25 <0.25 <0.25 27.7 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <1.0 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA
3/27/2020 <0.24 1.4 <0.35 <0.25 <0.25 18.7 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA
2/3/2021 <0.24 1.8 <0.35 <0.25 <0.25 21.2 <0.21 <0.40 <0.23 0.27J <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA
Notes: µg/L = Micrograms per literNA = Not analyzedND = Not detected at or above laboratory reporting limits.
NE = No standard establishedContaminants that exceed their respective GCL are highlighted in yellow. Contaminants that exceed the NCDEQ - NCAC 15A 2L Groundwater Standards are in BOLD.
GCL = Gross contamination levels for groundwater
MW-5
MW-6 Dibromochloromethane1,3,5-Trimethylbenzene1,2-Dibromoethane (EDB)Bromodichloromethane1,2,3-Trichloropropanetert-Butylbenzene1,2-Dichloropropanesec-Butylbenzenen-Butylbenzenen-Propylbenzene1,2,4-Trimethylbenzene1,2-DichloroethaneMW-1
MW-2
MW-3
MW-4
Analytical Method
2L Standard (ug/L)
GCL (ug/L)
6200B
Not Sampled
Not SampledNot Sampled Methyl-tert-butyl ether (MTBE)Chloroform1,2-Dibromoethane (EDB)BenzeneTotal XylenesEthylbenzeneDiisopropyl Ether IsopropylbenzeneNaphthaleneTolueneMethylene Chloride2-Chlorotoluene
TABLE 3Summary of Groundwater Analytical Results
Hull's 66 Vale, North Carolina
Terracon Project No. 71179011ANCDEQ Incident No. 40162
EPA 504.1
Contaminant of Concern →
Well/SampleI.D.Date Collected (mm/dd/yy)Dibromochloromethane1,3,5-Trimethylbenzene1,2-Dibromoethane (EDB)Bromodichloromethane1,2,3-Trichloropropanetert-Butylbenzene1,2-Dichloropropanesec-Butylbenzenen-Butylbenzenen-Propylbenzene1,2,4-Trimethylbenzene1,2-DichloroethaneAnalytical Method
2L St d d ( /L)
6200B
Methyl-tert-butyl ether (MTBE)Chloroform1,2-Dibromoethane (EDB)BenzeneTotal XylenesEthylbenzeneDiisopropyl Ether IsopropylbenzeneNaphthaleneTolueneMethylene Chloride2-Chlorotoluene1 0.6 70 70 70 70 100 0.4 0.02 0.4 0.6 70 600 70 5 20 6 70 600 0.005 400 400 500 0.02
5,000 400 6,900 8,500 15,000 70,000 NE 400 50 400 600 70,000 84,500 25,000 5,000 20,000 6,000 30,000 260,000 NE 28,500 25,000 85,500 5012/11/2014 ND ND ND ND ND 0.67 ND ND NA ND ND ND ND ND ND 0.7 ND ND ND ND ND ND ND ND10/19/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA8/2/20173/2/201810/3/20186/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 0.47J <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA
2/3/2021 <0.22 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA12/11/2014 ND ND ND ND ND 0.67 ND ND NA ND ND ND ND ND ND 1.7 ND ND ND ND ND ND ND ND10/19/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.74 ND ND ND ND ND ND ND NA8/2/2017
3/2/201810/3/20186/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 0.42J <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA
3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 1 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 0.75 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA12/11/2014 ND ND ND ND ND 3.2 ND ND NA ND ND ND ND ND ND 3.5 ND ND ND ND ND ND ND 0.047/17/2015 ND ND ND ND ND 1.4 ND ND NA ND ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND10/19/2015 ND ND ND ND ND 1.8 ND ND ND ND ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND8/2/20173/2/201810/3/20186/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 0.42J <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA3/27/2020 <0.24 <0.26 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA
6/7/2019 62.2 <0.25 3 3 0.96 <2.5 <0.25 <0.25 0.35J <0.25 0.36J <0.25 129 31.4 <1.0 <1.0 26.8 17.4 2.6 1.3 46.8 46.5 72.9 NA
3/27/2020 20.3 <0.18 0.64 0.8 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 32 9.5 <1.5 <0.44 2.3 4 0.7 <0.27 2.8 <0.23 12.7 NA
2/3/2021 42.7 <0.18 2.5 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 103 26.3 <1.5 <0.44 10.4 10 1.7 <0.27 34.8 19.2 55.9 NA12/11/2014 ND ND ND ND ND 1.1 ND ND NA ND ND ND ND ND ND 1.2 ND ND ND ND ND ND ND ND10/19/2015 ND ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND 0.85 ND ND ND ND ND ND ND NA8/2/20173/2/201810/3/20186/6/2019 <0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 0.39J <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.5 NA3/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 1.4 <0.21 <0.40 <0.23 0.30J <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 NA
2/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 0.82 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 0.36J <0.24 <1.5 <0.44 0.87J <0.24 <0.23 <0.27 0.5 <0.23 <0.24 NA12/11/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND8/2/2017 <0.25 ND <0.25 <0.25 ND <0.25 ND <0.25 <0.25 <0.25 ND <0.25 <0.25 <0.25 ND <0.25 <1.0 <0.25 <0.25 ND <0.25 <0.25 <0.50 <0.253/2/201810/3/20186/6/20193/27/202010/3/2018 <0.25 ND <0.25 <0.25 ND <0.25 <0.25 <0.25 <0.25 <0.25 ND <0.25 <0.25 <0.25 <1.0 <0.25 <1.0 <0.25 <0.25 ND <0.25 <0.25 <0.25 NA6/6/20193/27/2020 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.68 <0.0112/3/2021 <0.24 <0.18 <0.35 <0.25 <0.25 <0.35 <0.21 <0.40 <0.23 <0.26 <0.18 <0.33 <0.24 <0.24 <1.5 <0.44 <0.66 <0.24 <0.23 <0.27 <0.19 <0.23 <0.24 NA
Notes:
µg/L = Micrograms per literNA = Not analyzedND = Not detected at or above laboratory reporting limits. NE = No standard establishedContaminants that exceed their respective GCL are highlighted in yellow. Contaminants that exceed the NCDEQ - NCAC 15A 2L Groundwater Standards are in BOLD. GCL = Gross contamination levels for groundwater
WSW-10
MW-7
MW-8
MW-9
MW-10
DMW-1
WSW-2
2L Standard (ug/L)
GCL (ug/L)
Not Sampled
Not SampledNot Sampled
Not SampledNot SampledNot Sampled
Not SampledNot SampledNot Sampled
Not SampledNot Sampled
Not Sampled
Not SampledNot SampledNot Sampled
Not Sampled
Well Destroyed
TABLE 4Monitoring Well Construction Informationand Historical Groundwater Elevations
Hull's 66Vale, North Carolina
Terracon Project No. 71179011ANCDEQ Incident No. 40162
Well Id Date Installed (mm/dd/yy)
Date Water Level Measured (mm/dd/yy)
Well Casing Diameter (in.)
Screen Interval (ft-TOC)
Depth of Well (ft-TOC)
Top of
Casing Elevation (ft.)
Depth to Water from Top of Casing (ft.)
Groundwater Elevation (ft.)Comments
7/2/2013 22.76 77.245/9/2014 20.78 79.2212/11/2014 23.54 76.467/17/2015 23.01 76.9910/19/2015 24.44 75.568/2/2017 24.24 75.763/2/2018 24.50 75.5010/3/2018 22.95 77.056/6/2019 19.25 80.753/27/2020 19.43 80.572/3/2021 19.30 80.705/9/2014 20.89 78.7912/11/2014 23.50 76.187/17/2015 22.98 76.7010/19/2015 24.4 75.288/2/2017 24.16 75.523/2/2018 24.39 75.2910/3/2018 23.24 76.446/6/2019 19.33 80.353/27/2020 19.62 80.062/3/2021 19.38 80.305/9/2014 19.76 79.1312/11/2014 22.45 76.447/17/2015 21.92 76.9710/19/2015 23.37 75.528/2/2017 23.07 75.823/2/2018 23.28 75.6110/3/2018 21.82 77.076/6/2019 18.19 80.70
3/27/2020 18.38 80.512/3/2021 18.29 80.605/9/2014 19.14 78.8612/11/2014 21.84 76.167/17/2015 21.35 76.6510/19/2015 22.78 75.22
8/2/2017 22.53 75.473/2/2018 22.72 75.2810/3/2018 21.63 76.37
6/6/2019 17.62 80.383/27/2020 17.84 80.162/3/2021 17.69 80.315/9/2014 19.77 78.7712/11/2014 22.35 76.197/17/2015 21.87 76.6710/19/2015 23.26 75.288/2/2017 23.12 75.423/2/2018 23.33 75.21
10/3/2018 21.13 77.416/6/2019 18.20 80.343/27/2020 18.44 80.102/3/2021 18.25 80.2912/11/2014 23.98 75.5010/19/2015 24.08 75.408/2/20173/2/201810/3/20186/6/2019 19.09 80.393/27/2020 19.28 80.202/3/2021 19.14 80.34
12/11/2014 23.28 76.3610/19/2015 24.26 75.388/2/2017
3/2/201810/3/20186/6/2019 19.08 80.523/27/2020 19.28 80.362/3/2021 19.13 80.5112/11/2014 22.33 75.7710/19/2015 22.98 75.128/2/2017
3/2/201810/3/20186/6/2019 18.08 80.023/27/2020 18.22 79.88
2/3/2021 19.07 79.0312/11/2014 18.80 75.267/17/2015 18.51 75.5510/19/2015 19.66 74.408/2/20173/2/201810/3/2018
6/6/2019 15.30 78.80
3/27/2020 15.81 78.252/3/2021 15.07 78.99
6/7/2019 17.54 80.713/27/2020 17.78 80.472/3/2021 17.54 80.7112/11/2014 22.99 76.03
10/19/2015 23.93 75.098/2/20173/2/201810/3/2018
6/6/2019 19.00 80.003/27/2020 19.31 79.712/3/2021 19.00 80.02Notes: Depth of Well and Top of Casing elevations taken from Corrective Action Plan, Hull's 66 dated January 29, 2016 by Shield Engineering, Inc.Top of casing elevations are based on an assumed elevation of 100 feet at well MW-1.
6/7/2019 2 15-30 20 98.25
98.1
MW-7 12/3/2014 2 20-35 35
MW-8 10/4/2015 2 2914-29
99.48
MW-5 5/6/2014
99.64
MW-6 12/3/2014 2 18-33 33
30 98.00
30 98.54
99.68
MW-3 5/6/2014 2 11-26 26 98.89
MW-2 5/6/2014 2 15-30 30
DMW-1 12/4/2014 2 45-50 50
MW-10
Not MeasuredNot Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not MeasuredNot MeasuredMW-9 10/4/2015 2 10-25 25 94.06
MW-4 5/6/2014
MW-1 7/1/2013
Not MeasuredNot Measured
Not MeasuredNot Measured
2 15-30
2 15-30 30 100.00
2 15-30
Not MeasuredNot Measured
Not Measured
99.02

APPENDIX A
LABORATORY ANALYTICAL RESULTS AND
CHAIN-OF-CUSTODY FORMS
#=CL#
February 11, 2021
LIMS USE: FR - VICTORIA LARSON
LIMS OBJECT ID: 92520378
92520378
Project:
Pace Project No.:
RE:
Victoria Larson
2020 Starita Rd
Suite E
Charlotte, NC 28206
HULL'S 66
Dear Victoria Larson:
Enclosed are the analytical results for sample(s) received by the laboratory on February 04, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 58
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92520378
HULL'S 66
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 58
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92520378
HULL'S 66
Lab ID Sample ID Matrix Date Collected Date Received
92520378001 MW-1 Water 02/03/21 10:10 02/04/21 13:17
92520378002 MW-2 Water 02/03/21 11:50 02/04/21 13:17
92520378003 MW-3 Water 02/03/21 11:25 02/04/21 13:17
92520378004 MW-4 Water 02/03/21 12:15 02/04/21 13:17
92520378005 MW-5 Water 02/03/21 11:45 02/04/21 13:17
92520378006 MW-6 Water 02/03/21 11:55 02/04/21 13:17
92520378007 MW-7 Water 02/03/21 10:55 02/04/21 13:17
92520378008 MW-8 Water 02/03/21 10:00 02/04/21 13:17
92520378009 MW-9 Water 02/03/21 10:30 02/04/21 13:17
92520378010 MW-10 Water 02/03/21 10:45 02/04/21 13:17
92520378011 DMW-1 Water 02/03/21 09:55 02/04/21 13:17
92520378012 FB Water 02/03/21 09:00 02/04/21 13:17
92520378013 WSW-10 Water 02/03/21 12:15 02/04/21 13:17
92520378014 TB Water 02/04/21 00:00 02/04/21 13:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 58
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92520378
HULL'S 66
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92520378001 MW-1 SM 6200B 63 PASI-CSAS
92520378002 MW-2 SM 6200B 63 PASI-CSAS
92520378003 MW-3 SM 6200B 63 PASI-CSAS
92520378004 MW-4 SM 6200B 63 PASI-CSAS
92520378005 MW-5 SM 6200B 63 PASI-CSAS
92520378006 MW-6 SM 6200B 63 PASI-CSAS
92520378007 MW-7 SM 6200B 63 PASI-CSAS
92520378008 MW-8 SM 6200B 63 PASI-CSAS
92520378009 MW-9 SM 6200B 63 PASI-CSAS
92520378010 MW-10 SM 6200B 63 PASI-CSAS
92520378011 DMW-1 SM 6200B 63 PASI-CSAS
92520378012 FB SM 6200B 63 PASI-CSAS
92520378013 WSW-10 SM 6200B 63 PASI-CSAS
92520378014 TB SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 58
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92520378
HULL'S 66
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92520378001 MW-1
1,2-Dichloroethane 0.38J ug/L 02/09/21 17:490.50SM 6200B
92520378002 MW-2
Chloroform 0.62 ug/L 02/09/21 18:070.50SM 6200B
1,2-Dibromoethane (EDB)1.0 ug/L 02/09/21 18:070.50SM 6200B
1,2-Dichloroethane 0.80 ug/L 02/09/21 18:070.50SM 6200B
Ethylbenzene 23.5 ug/L 02/09/21 18:070.50SM 6200B
Isopropylbenzene (Cumene)1.6 ug/L 02/09/21 18:070.50SM 6200B
Methyl-tert-butyl ether 0.92 ug/L 02/09/21 18:070.50SM 6200B
Naphthalene 22.8 ug/L 02/09/21 18:072.0SM 6200B
Toluene 18.0 ug/L 02/09/21 18:070.50SM 6200B
1,2,4-Trimethylbenzene 113 ug/L 02/09/21 18:070.50SM 6200B
1,3,5-Trimethylbenzene 75.8 ug/L 02/09/21 18:070.50SM 6200B
m&p-Xylene 264 ug/L 02/09/21 18:071.0SM 6200B
o-Xylene 166 ug/L 02/09/21 18:070.50SM 6200B
92520378005 MW-5
Bromodichloromethane 0.92 ug/L 02/09/21 19:010.50SM 6200B
Chloroform 7.2 ug/L 02/09/21 19:010.50SM 6200B
1,2-Dibromoethane (EDB)0.46J ug/L 02/09/21 19:010.50SM 6200B
1,2-Dichloroethane 0.65 ug/L 02/09/21 19:010.50SM 6200B
Ethylbenzene 0.62 ug/L 02/09/21 19:010.50SM 6200B
Isopropylbenzene (Cumene)0.60 ug/L 02/09/21 19:010.50SM 6200B
Methyl-tert-butyl ether 0.69 ug/L 02/09/21 19:010.50SM 6200B
Naphthalene 3.2 ug/L 02/09/21 19:012.0SM 6200B
1,3,5-Trimethylbenzene 8.6 ug/L 02/09/21 19:010.50SM 6200B
m&p-Xylene 3.6 ug/L 02/09/21 19:011.0SM 6200B
o-Xylene 5.5 ug/L 02/09/21 19:010.50SM 6200B
92520378006 MW-6
Bromodichloromethane 1.8 ug/L 02/09/21 19:190.50SM 6200B
Chloroform 21.2 ug/L 02/09/21 19:190.50SM 6200B
1,2-Dichloroethane 0.27J ug/L 02/09/21 19:190.50SM 6200B
92520378008 MW-8
Chloroform 0.75 ug/L 02/09/21 19:550.50SM 6200B
92520378010 MW-10
Benzene 42.7 ug/L 02/09/21 20:310.50SM 6200B
n-Butylbenzene 2.5 ug/L 02/09/21 20:310.50SM 6200B
Ethylbenzene 103 ug/L 02/09/21 20:310.50SM 6200B
Isopropylbenzene (Cumene)26.3 ug/L 02/09/21 20:310.50SM 6200B
Naphthalene 10.4 ug/L 02/09/21 20:312.0SM 6200B
n-Propylbenzene 10 ug/L 02/09/21 20:310.50SM 6200B
Toluene 1.7 ug/L 02/09/21 20:310.50SM 6200B
1,2,4-Trimethylbenzene 34.8 ug/L 02/09/21 20:310.50SM 6200B
1,3,5-Trimethylbenzene 19.2 ug/L 02/09/21 20:310.50SM 6200B
m&p-Xylene 52.9 ug/L 02/09/21 20:311.0SM 6200B
o-Xylene 3.0 ug/L 02/09/21 20:310.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 58
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92520378
HULL'S 66
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92520378011 DMW-1
Chloroform 0.82 ug/L 02/09/21 20:490.50SM 6200B
Ethylbenzene 0.36J ug/L 02/09/21 20:490.50SM 6200B
Naphthalene 0.87J ug/L 02/09/21 20:492.0SM 6200B
1,2,4-Trimethylbenzene 0.50 ug/L 02/09/21 20:490.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 58
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92520378
HULL'S 66
Method:
Client:Terracon - Charlotte, NC
SM 6200B
Date:February 11, 2021
Description:6200B MSV
General Information:
14 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 598767
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 3156848)
• 1,1,2-Trichloroethane
• 1,2-Dibromo-3-chloropropane
• 1,2-Dibromoethane (EDB)
• Bromoform
• Dibromochloromethane
• Dibromomethane
• Naphthalene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 598656
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92519777002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MSD (Lab ID: 3156162)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 58
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92520378
HULL'S 66
Method:
Client:Terracon - Charlotte, NC
SM 6200B
Date:February 11, 2021
Description:6200B MSV
QC Batch: 598656
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92519777002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• 1,2,4-Trimethylbenzene
• Benzene
• Ethylbenzene
• Naphthalene
• Toluene
• m&p-Xylene
• o-Xylene
R1: RPD value was outside control limits.
• MSD (Lab ID: 3156162)
• 1,2,4-Trimethylbenzene
• Toluene
• m&p-Xylene
• o-Xylene
QC Batch: 598947
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92520734001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3159201)
• Toluene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-1 Lab ID: 92520378001 Collected: 02/03/21 10:10 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 17:49 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 17:49 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 17:49 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 17:49 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 17:49 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 17:49 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 17:49 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 17:49 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 17:49 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 17:49 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 17:49 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 17:49 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 17:49 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 17:49 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 17:49 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 17:49 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 17:49 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 17:49 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 17:49 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 17:49 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 17:49 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 17:49 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 17:49 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 17:49 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 17:49 75-34-30.50 0.24 1
1,2-Dichloroethane 0.38J ug/L 02/09/21 17:49 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 17:49 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 17:49 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 17:49 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 17:49 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 17:49 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 17:49 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 17:49 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 17:49 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 17:49 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 17:49 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 17:49 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 17:49 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 17:49 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 17:49 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 17:49 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 17:49 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 17:49 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 17:49 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 17:49 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-1 Lab ID: 92520378001 Collected: 02/03/21 10:10 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 17:49 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 17:49 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 17:49 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 17:49 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 17:49 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 17:49 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 17:49 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 17:49 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 17:49 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 17:49 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 17:49 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 17:49 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 17:49 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 17:49 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 17:49 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/09/21 17:49 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %02/09/21 17:49 460-00-470-130 1
Toluene-d8 (S)100 %02/09/21 17:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-2 Lab ID: 92520378002 Collected: 02/03/21 11:50 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 18:07 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 18:07 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 18:07 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 18:07 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 18:07 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 18:07 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 18:07 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 18:07 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 18:07 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 18:07 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 18:07 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 18:07 75-00-31.0 0.58 1
Chloroform 0.62 ug/L 02/09/21 18:07 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 18:07 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 18:07 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 18:07 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 18:07 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 18:07 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)1.0 ug/L 02/09/21 18:07 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 18:07 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 18:07 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 18:07 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 18:07 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 18:07 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 18:07 75-34-30.50 0.24 1
1,2-Dichloroethane 0.80 ug/L 02/09/21 18:07 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 18:07 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 18:07 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 18:07 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 18:07 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 18:07 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 18:07 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 18:07 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 18:07 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 18:07 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 18:07 108-20-30.50 0.33 1
Ethylbenzene 23.5 ug/L 02/09/21 18:07 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 18:07 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)1.6 ug/L 02/09/21 18:07 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 18:07 75-09-22.0 1.5 1
Methyl-tert-butyl ether 0.92 ug/L 02/09/21 18:07 1634-04-40.50 0.44 1
Naphthalene 22.8 ug/L 02/09/21 18:07 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 18:07 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 18:07 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 18:07 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-2 Lab ID: 92520378002 Collected: 02/03/21 11:50 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 18:07 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 18:07 127-18-40.50 0.23 1
Toluene 18.0 ug/L 02/09/21 18:07 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 18:07 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 18:07 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 18:07 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 18:07 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 18:07 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 18:07 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 18:07 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene 113 ug/L 02/09/21 18:07 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene 75.8 ug/L 02/09/21 18:07 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 18:07 75-01-41.0 0.41 1
m&p-Xylene 264 ug/L 02/09/21 18:07 179601-23-11.0 0.44 1
o-Xylene 166 ug/L 02/09/21 18:07 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/09/21 18:07 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/09/21 18:07 460-00-470-130 1
Toluene-d8 (S)100 %02/09/21 18:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-3 Lab ID: 92520378003 Collected: 02/03/21 11:25 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/10/21 23:33 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/10/21 23:33 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/10/21 23:33 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/10/21 23:33 75-27-40.50 0.18 1
Bromoform ND ug/L 02/10/21 23:33 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/10/21 23:33 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/10/21 23:33 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/10/21 23:33 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/10/21 23:33 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/10/21 23:33 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/10/21 23:33 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/10/21 23:33 75-00-31.0 0.58 1
Chloroform ND ug/L 02/10/21 23:33 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/10/21 23:33 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/10/21 23:33 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/10/21 23:33 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/10/21 23:33 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/10/21 23:33 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/10/21 23:33 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/10/21 23:33 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/10/21 23:33 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/10/21 23:33 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/10/21 23:33 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/10/21 23:33 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/10/21 23:33 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/10/21 23:33 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/10/21 23:33 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/10/21 23:33 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/10/21 23:33 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/10/21 23:33 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/10/21 23:33 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/10/21 23:33 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/10/21 23:33 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/10/21 23:33 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/10/21 23:33 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/10/21 23:33 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/10/21 23:33 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/10/21 23:33 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/10/21 23:33 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/10/21 23:33 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/10/21 23:33 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/10/21 23:33 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/10/21 23:33 103-65-10.50 0.24 1
Styrene ND ug/L 02/10/21 23:33 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/10/21 23:33 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-3 Lab ID: 92520378003 Collected: 02/03/21 11:25 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/10/21 23:33 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/10/21 23:33 127-18-40.50 0.23 1
Toluene ND ug/L 02/10/21 23:33 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/10/21 23:33 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/10/21 23:33 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/10/21 23:33 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/10/21 23:33 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/10/21 23:33 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/10/21 23:33 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/10/21 23:33 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/10/21 23:33 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/10/21 23:33 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/10/21 23:33 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/10/21 23:33 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/10/21 23:33 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %02/10/21 23:33 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %02/10/21 23:33 460-00-470-130 1
Toluene-d8 (S)98 %02/10/21 23:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-4 Lab ID: 92520378004 Collected: 02/03/21 12:15 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 18:43 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 18:43 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 18:43 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 18:43 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 18:43 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 18:43 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 18:43 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 18:43 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 18:43 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 18:43 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 18:43 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 18:43 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 18:43 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 18:43 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 18:43 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 18:43 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 18:43 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 18:43 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 18:43 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 18:43 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 18:43 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 18:43 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 18:43 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 18:43 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 18:43 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 18:43 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 18:43 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 18:43 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 18:43 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 18:43 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 18:43 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 18:43 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 18:43 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 18:43 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 18:43 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 18:43 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 18:43 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 18:43 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 18:43 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 18:43 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 18:43 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 18:43 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 18:43 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 18:43 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 18:43 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 15 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-4 Lab ID: 92520378004 Collected: 02/03/21 12:15 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 18:43 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 18:43 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 18:43 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 18:43 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 18:43 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 18:43 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 18:43 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 18:43 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 18:43 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 18:43 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 18:43 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 18:43 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 18:43 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 18:43 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 18:43 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %02/09/21 18:43 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %02/09/21 18:43 460-00-470-130 1
Toluene-d8 (S)101 %02/09/21 18:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-5 Lab ID: 92520378005 Collected: 02/03/21 11:45 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 19:01 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 19:01 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 19:01 74-97-50.50 0.26 1
Bromodichloromethane 0.92 ug/L 02/09/21 19:01 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 19:01 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 19:01 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 19:01 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 19:01 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 19:01 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 19:01 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 19:01 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 19:01 75-00-31.0 0.58 1
Chloroform 7.2 ug/L 02/09/21 19:01 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 19:01 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 19:01 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 19:01 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 19:01 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 19:01 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)0.46J ug/L 02/09/21 19:01 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 19:01 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 19:01 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 19:01 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 19:01 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 19:01 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 19:01 75-34-30.50 0.24 1
1,2-Dichloroethane 0.65 ug/L 02/09/21 19:01 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 19:01 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 19:01 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 19:01 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 19:01 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 19:01 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 19:01 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 19:01 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 19:01 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 19:01 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 19:01 108-20-30.50 0.33 1
Ethylbenzene 0.62 ug/L 02/09/21 19:01 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 19:01 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)0.60 ug/L 02/09/21 19:01 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 19:01 75-09-22.0 1.5 1
Methyl-tert-butyl ether 0.69 ug/L 02/09/21 19:01 1634-04-40.50 0.44 1
Naphthalene 3.2 ug/L 02/09/21 19:01 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 19:01 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 19:01 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 19:01 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-5 Lab ID: 92520378005 Collected: 02/03/21 11:45 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 19:01 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 19:01 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 19:01 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 19:01 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 19:01 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 19:01 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 19:01 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 19:01 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 19:01 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 19:01 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 19:01 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene 8.6 ug/L 02/09/21 19:01 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 19:01 75-01-41.0 0.41 1
m&p-Xylene 3.6 ug/L 02/09/21 19:01 179601-23-11.0 0.44 1
o-Xylene 5.5 ug/L 02/09/21 19:01 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %02/09/21 19:01 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/09/21 19:01 460-00-470-130 1
Toluene-d8 (S)99 %02/09/21 19:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-6 Lab ID: 92520378006 Collected: 02/03/21 11:55 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 19:19 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 19:19 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 19:19 74-97-50.50 0.26 1
Bromodichloromethane 1.8 ug/L 02/09/21 19:19 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 19:19 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 19:19 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 19:19 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 19:19 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 19:19 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 19:19 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 19:19 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 19:19 75-00-31.0 0.58 1
Chloroform 21.2 ug/L 02/09/21 19:19 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 19:19 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 19:19 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 19:19 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 19:19 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 19:19 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 19:19 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 19:19 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 19:19 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 19:19 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 19:19 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 19:19 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 19:19 75-34-30.50 0.24 1
1,2-Dichloroethane 0.27J ug/L 02/09/21 19:19 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 19:19 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 19:19 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 19:19 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 19:19 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 19:19 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 19:19 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 19:19 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 19:19 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 19:19 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 19:19 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 19:19 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 19:19 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 19:19 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 19:19 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 19:19 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 19:19 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 19:19 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 19:19 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 19:19 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-6 Lab ID: 92520378006 Collected: 02/03/21 11:55 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 19:19 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 19:19 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 19:19 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 19:19 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 19:19 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 19:19 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 19:19 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 19:19 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 19:19 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 19:19 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 19:19 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 19:19 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 19:19 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 19:19 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 19:19 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %02/09/21 19:19 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %02/09/21 19:19 460-00-470-130 1
Toluene-d8 (S)101 %02/09/21 19:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-7 Lab ID: 92520378007 Collected: 02/03/21 10:55 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 19:37 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 19:37 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 19:37 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 19:37 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 19:37 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 19:37 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 19:37 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 19:37 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 19:37 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 19:37 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 19:37 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 19:37 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 19:37 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 19:37 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 19:37 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 19:37 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 19:37 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 19:37 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 19:37 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 19:37 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 19:37 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 19:37 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 19:37 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 19:37 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 19:37 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 19:37 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 19:37 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 19:37 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 19:37 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 19:37 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 19:37 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 19:37 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 19:37 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 19:37 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 19:37 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 19:37 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 19:37 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 19:37 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 19:37 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 19:37 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 19:37 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 19:37 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 19:37 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 19:37 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 19:37 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-7 Lab ID: 92520378007 Collected: 02/03/21 10:55 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 19:37 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 19:37 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 19:37 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 19:37 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 19:37 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 19:37 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 19:37 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 19:37 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 19:37 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 19:37 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 19:37 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 19:37 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 19:37 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 19:37 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 19:37 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %02/09/21 19:37 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %02/09/21 19:37 460-00-470-130 1
Toluene-d8 (S)100 %02/09/21 19:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-8 Lab ID: 92520378008 Collected: 02/03/21 10:00 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 19:55 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 19:55 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 19:55 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 19:55 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 19:55 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 19:55 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 19:55 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 19:55 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 19:55 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 19:55 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 19:55 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 19:55 75-00-31.0 0.58 1
Chloroform 0.75 ug/L 02/09/21 19:55 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 19:55 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 19:55 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 19:55 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 19:55 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 19:55 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 19:55 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 19:55 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 19:55 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 19:55 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 19:55 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 19:55 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 19:55 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 19:55 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 19:55 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 19:55 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 19:55 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 19:55 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 19:55 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 19:55 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 19:55 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 19:55 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 19:55 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 19:55 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 19:55 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 19:55 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 19:55 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 19:55 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 19:55 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 19:55 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 19:55 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 19:55 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 19:55 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-8 Lab ID: 92520378008 Collected: 02/03/21 10:00 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 19:55 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 19:55 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 19:55 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 19:55 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 19:55 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 19:55 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 19:55 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 19:55 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 19:55 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 19:55 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 19:55 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 19:55 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 19:55 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 19:55 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 19:55 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %02/09/21 19:55 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %02/09/21 19:55 460-00-470-130 1
Toluene-d8 (S)99 %02/09/21 19:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-9 Lab ID: 92520378009 Collected: 02/03/21 10:30 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 20:13 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 20:13 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 20:13 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 20:13 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 20:13 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 20:13 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 20:13 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 20:13 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 20:13 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 20:13 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 20:13 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 20:13 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 20:13 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 20:13 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 20:13 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 20:13 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 20:13 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 20:13 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 20:13 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 20:13 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 20:13 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 20:13 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 20:13 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 20:13 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 20:13 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 20:13 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 20:13 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 20:13 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 20:13 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 20:13 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 20:13 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 20:13 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 20:13 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 20:13 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 20:13 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 20:13 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 20:13 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 20:13 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 20:13 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 20:13 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 20:13 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 20:13 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 20:13 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 20:13 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 20:13 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-9 Lab ID: 92520378009 Collected: 02/03/21 10:30 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 20:13 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 20:13 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 20:13 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 20:13 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 20:13 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 20:13 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 20:13 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 20:13 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 20:13 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 20:13 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 20:13 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 20:13 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 20:13 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 20:13 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 20:13 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/09/21 20:13 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %02/09/21 20:13 460-00-470-130 1
Toluene-d8 (S)102 %02/09/21 20:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-10 Lab ID: 92520378010 Collected: 02/03/21 10:45 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 42.7 ug/L 02/09/21 20:31 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 20:31 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 20:31 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 20:31 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 20:31 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 20:31 74-83-95.0 1.7 1
n-Butylbenzene 2.5 ug/L 02/09/21 20:31 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 20:31 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 20:31 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 20:31 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 20:31 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 20:31 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 20:31 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 20:31 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 20:31 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 20:31 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 20:31 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 20:31 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 20:31 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 20:31 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 20:31 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 20:31 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 20:31 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 20:31 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 20:31 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 20:31 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 20:31 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 20:31 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 20:31 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 20:31 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 20:31 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 20:31 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 20:31 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 20:31 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 20:31 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 20:31 108-20-30.50 0.33 1
Ethylbenzene 103 ug/L 02/09/21 20:31 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 20:31 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)26.3 ug/L 02/09/21 20:31 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 20:31 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 20:31 1634-04-40.50 0.44 1
Naphthalene 10.4 ug/L 02/09/21 20:31 91-20-32.0 0.66 1
n-Propylbenzene 10 ug/L 02/09/21 20:31 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 20:31 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 20:31 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: MW-10 Lab ID: 92520378010 Collected: 02/03/21 10:45 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 20:31 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 20:31 127-18-40.50 0.23 1
Toluene 1.7 ug/L 02/09/21 20:31 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 20:31 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 20:31 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 20:31 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 20:31 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 20:31 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 20:31 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 20:31 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene 34.8 ug/L 02/09/21 20:31 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene 19.2 ug/L 02/09/21 20:31 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 20:31 75-01-41.0 0.41 1
m&p-Xylene 52.9 ug/L 02/09/21 20:31 179601-23-11.0 0.44 1
o-Xylene 3.0 ug/L 02/09/21 20:31 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/09/21 20:31 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/09/21 20:31 460-00-470-130 1
Toluene-d8 (S)101 %02/09/21 20:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: DMW-1 Lab ID: 92520378011 Collected: 02/03/21 09:55 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 20:49 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 20:49 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 20:49 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 20:49 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 20:49 75-25-20.50 0.40 1
Bromomethane ND ug/L 02/09/21 20:49 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 20:49 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 20:49 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 20:49 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 20:49 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 20:49 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 20:49 75-00-31.0 0.58 1
Chloroform 0.82 ug/L 02/09/21 20:49 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 20:49 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 20:49 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 20:49 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 20:49 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 20:49 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 20:49 106-93-40.50 0.23 1
Dibromomethane ND ug/L 02/09/21 20:49 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 20:49 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 20:49 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 20:49 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 20:49 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 20:49 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 20:49 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 20:49 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 20:49 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 20:49 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 20:49 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 20:49 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 20:49 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 20:49 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 20:49 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 20:49 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 20:49 108-20-30.50 0.33 1
Ethylbenzene 0.36J ug/L 02/09/21 20:49 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 20:49 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 20:49 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 20:49 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 20:49 1634-04-40.50 0.44 1
Naphthalene 0.87J ug/L 02/09/21 20:49 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 20:49 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 20:49 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 20:49 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: DMW-1 Lab ID: 92520378011 Collected: 02/03/21 09:55 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 20:49 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 20:49 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 20:49 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 20:49 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 20:49 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 20:49 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 20:49 79-00-50.50 0.23 1
Trichloroethene ND ug/L 02/09/21 20:49 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 20:49 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 20:49 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene 0.50 ug/L 02/09/21 20:49 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 20:49 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 20:49 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 20:49 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 20:49 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %02/09/21 20:49 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %02/09/21 20:49 460-00-470-130 1
Toluene-d8 (S)99 %02/09/21 20:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: FB Lab ID: 92520378012 Collected: 02/03/21 09:00 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 22:55 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 22:55 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 22:55 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 22:55 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 22:55 75-25-2 L10.50 0.40 1
Bromomethane ND ug/L 02/09/21 22:55 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 22:55 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 22:55 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 22:55 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 22:55 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 22:55 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 22:55 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 22:55 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 22:55 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 22:55 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 22:55 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 22:55 96-12-8 L11.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 22:55 124-48-1 L10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 22:55 106-93-4 L10.50 0.23 1
Dibromomethane ND ug/L 02/09/21 22:55 74-95-3 L10.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 22:55 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 22:55 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 22:55 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 22:55 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 22:55 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 22:55 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 22:55 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 22:55 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 22:55 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 22:55 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 22:55 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 22:55 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 22:55 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 22:55 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 22:55 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 22:55 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 22:55 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 22:55 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 22:55 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 22:55 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 22:55 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 22:55 91-20-3 L12.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 22:55 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 22:55 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 22:55 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: FB Lab ID: 92520378012 Collected: 02/03/21 09:00 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 22:55 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 22:55 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 22:55 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 22:55 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 22:55 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 22:55 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 22:55 79-00-5 L10.50 0.23 1
Trichloroethene ND ug/L 02/09/21 22:55 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 22:55 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 22:55 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 22:55 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 22:55 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 22:55 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 22:55 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 22:55 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %02/09/21 22:55 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %02/09/21 22:55 460-00-470-130 1
Toluene-d8 (S)100 %02/09/21 22:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: WSW-10 Lab ID: 92520378013 Collected: 02/03/21 12:15 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/10/21 00:43 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/10/21 00:43 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/10/21 00:43 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/10/21 00:43 75-27-40.50 0.18 1
Bromoform ND ug/L 02/10/21 00:43 75-25-2 L10.50 0.40 1
Bromomethane ND ug/L 02/10/21 00:43 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/10/21 00:43 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/10/21 00:43 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/10/21 00:43 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/10/21 00:43 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/10/21 00:43 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/10/21 00:43 75-00-31.0 0.58 1
Chloroform ND ug/L 02/10/21 00:43 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/10/21 00:43 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/10/21 00:43 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/10/21 00:43 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/10/21 00:43 96-12-8 L11.0 0.38 1
Dibromochloromethane ND ug/L 02/10/21 00:43 124-48-1 L10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/10/21 00:43 106-93-4 L10.50 0.23 1
Dibromomethane ND ug/L 02/10/21 00:43 74-95-3 L10.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/10/21 00:43 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/10/21 00:43 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/10/21 00:43 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/10/21 00:43 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/10/21 00:43 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/10/21 00:43 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/10/21 00:43 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/10/21 00:43 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/10/21 00:43 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/10/21 00:43 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/10/21 00:43 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/10/21 00:43 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/10/21 00:43 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/10/21 00:43 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/10/21 00:43 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/10/21 00:43 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/10/21 00:43 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/10/21 00:43 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/10/21 00:43 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/10/21 00:43 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/10/21 00:43 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/10/21 00:43 91-20-3 L12.0 0.66 1
n-Propylbenzene ND ug/L 02/10/21 00:43 103-65-10.50 0.24 1
Styrene ND ug/L 02/10/21 00:43 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/10/21 00:43 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: WSW-10 Lab ID: 92520378013 Collected: 02/03/21 12:15 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/10/21 00:43 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/10/21 00:43 127-18-40.50 0.23 1
Toluene ND ug/L 02/10/21 00:43 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/10/21 00:43 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/10/21 00:43 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/10/21 00:43 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/10/21 00:43 79-00-5 L10.50 0.23 1
Trichloroethene ND ug/L 02/10/21 00:43 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/10/21 00:43 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/10/21 00:43 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/10/21 00:43 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/10/21 00:43 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/10/21 00:43 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/10/21 00:43 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/10/21 00:43 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %02/10/21 00:43 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %02/10/21 00:43 460-00-470-130 1
Toluene-d8 (S)99 %02/10/21 00:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: TB Lab ID: 92520378014 Collected: 02/04/21 00:00 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/09/21 23:13 71-43-20.50 0.24 1
Bromobenzene ND ug/L 02/09/21 23:13 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 02/09/21 23:13 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 02/09/21 23:13 75-27-40.50 0.18 1
Bromoform ND ug/L 02/09/21 23:13 75-25-2 L10.50 0.40 1
Bromomethane ND ug/L 02/09/21 23:13 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 02/09/21 23:13 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 02/09/21 23:13 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 02/09/21 23:13 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 02/09/21 23:13 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 02/09/21 23:13 108-90-70.50 0.22 1
Chloroethane ND ug/L 02/09/21 23:13 75-00-31.0 0.58 1
Chloroform ND ug/L 02/09/21 23:13 67-66-30.50 0.35 1
Chloromethane ND ug/L 02/09/21 23:13 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 02/09/21 23:13 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 02/09/21 23:13 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 02/09/21 23:13 96-12-8 L11.0 0.38 1
Dibromochloromethane ND ug/L 02/09/21 23:13 124-48-1 L10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 02/09/21 23:13 106-93-4 L10.50 0.23 1
Dibromomethane ND ug/L 02/09/21 23:13 74-95-3 L10.50 0.31 1
1,2-Dichlorobenzene ND ug/L 02/09/21 23:13 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 02/09/21 23:13 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 02/09/21 23:13 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 02/09/21 23:13 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 02/09/21 23:13 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 02/09/21 23:13 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 02/09/21 23:13 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 02/09/21 23:13 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 02/09/21 23:13 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 02/09/21 23:13 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 02/09/21 23:13 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 02/09/21 23:13 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 02/09/21 23:13 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 02/09/21 23:13 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 02/09/21 23:13 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 02/09/21 23:13 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 02/09/21 23:13 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 02/09/21 23:13 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 02/09/21 23:13 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 02/09/21 23:13 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 02/09/21 23:13 1634-04-40.50 0.44 1
Naphthalene ND ug/L 02/09/21 23:13 91-20-3 L12.0 0.66 1
n-Propylbenzene ND ug/L 02/09/21 23:13 103-65-10.50 0.24 1
Styrene ND ug/L 02/09/21 23:13 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/09/21 23:13 630-20-60.50 0.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92520378
HULL'S 66
Sample: TB Lab ID: 92520378014 Collected: 02/04/21 00:00 Received: 02/04/21 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/09/21 23:13 79-34-50.50 0.19 1
Tetrachloroethene ND ug/L 02/09/21 23:13 127-18-40.50 0.23 1
Toluene ND ug/L 02/09/21 23:13 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 02/09/21 23:13 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 02/09/21 23:13 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 02/09/21 23:13 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 02/09/21 23:13 79-00-5 L10.50 0.23 1
Trichloroethene ND ug/L 02/09/21 23:13 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 02/09/21 23:13 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 02/09/21 23:13 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 02/09/21 23:13 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 02/09/21 23:13 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 02/09/21 23:13 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 02/09/21 23:13 179601-23-11.0 0.44 1
o-Xylene ND ug/L 02/09/21 23:13 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %02/09/21 23:13 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %02/09/21 23:13 460-00-470-130 1
Toluene-d8 (S)99 %02/09/21 23:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
598656
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92520378001, 92520378002, 92520378004, 92520378005, 92520378006, 92520378007, 92520378008,
92520378009, 92520378010, 92520378011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3156159
Associated Lab Samples: 92520378001, 92520378002, 92520378004, 92520378005, 92520378006, 92520378007, 92520378008,
92520378009, 92520378010, 92520378011
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/09/21 12:250.42
1,1,1-Trichloroethane ug/L ND 0.50 02/09/21 12:250.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/09/21 12:250.19
1,1,2-Trichloroethane ug/L ND 0.50 02/09/21 12:250.23
1,1-Dichloroethane ug/L ND 0.50 02/09/21 12:250.24
1,1-Dichloroethene ug/L ND 0.50 02/09/21 12:250.22
1,1-Dichloropropene ug/L ND 0.50 02/09/21 12:250.35
1,2,3-Trichlorobenzene ug/L ND 2.0 02/09/21 12:250.78
1,2,3-Trichloropropane ug/L ND 0.50 02/09/21 12:250.27
1,2,4-Trichlorobenzene ug/L ND 2.0 02/09/21 12:250.44
1,2,4-Trimethylbenzene ug/L ND 0.50 02/09/21 12:250.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/09/21 12:250.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/09/21 12:250.23
1,2-Dichlorobenzene ug/L ND 0.50 02/09/21 12:250.24
1,2-Dichloroethane ug/L ND 0.50 02/09/21 12:250.26
1,2-Dichloropropane ug/L ND 0.50 02/09/21 12:250.18
1,3,5-Trimethylbenzene ug/L ND 0.50 02/09/21 12:250.23
1,3-Dichlorobenzene ug/L ND 0.50 02/09/21 12:250.25
1,3-Dichloropropane ug/L ND 0.50 02/09/21 12:250.34
1,4-Dichlorobenzene ug/L ND 0.50 02/09/21 12:250.25
2,2-Dichloropropane ug/L ND 0.50 02/09/21 12:250.28
2-Chlorotoluene ug/L ND 0.50 02/09/21 12:250.21
4-Chlorotoluene ug/L ND 0.50 02/09/21 12:250.21
Benzene ug/L ND 0.50 02/09/21 12:250.24
Bromobenzene ug/L ND 0.50 02/09/21 12:250.22
Bromochloromethane ug/L ND 0.50 02/09/21 12:250.26
Bromodichloromethane ug/L ND 0.50 02/09/21 12:250.18
Bromoform ug/L ND 0.50 02/09/21 12:250.40
Bromomethane ug/L ND 5.0 02/09/21 12:251.7
Carbon tetrachloride ug/L ND 0.50 02/09/21 12:250.23
Chlorobenzene ug/L ND 0.50 02/09/21 12:250.22
Chloroethane ug/L ND 1.0 02/09/21 12:250.58
Chloroform ug/L ND 0.50 02/09/21 12:250.35
Chloromethane ug/L ND 1.0 02/09/21 12:250.42
cis-1,2-Dichloroethene ug/L ND 0.50 02/09/21 12:250.21
cis-1,3-Dichloropropene ug/L ND 0.50 02/09/21 12:250.36
Dibromochloromethane ug/L ND 0.50 02/09/21 12:250.40
Dibromomethane ug/L ND 0.50 02/09/21 12:250.31
Dichlorodifluoromethane ug/L ND 0.50 02/09/21 12:250.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3156159
Associated Lab Samples: 92520378001, 92520378002, 92520378004, 92520378005, 92520378006, 92520378007, 92520378008,
92520378009, 92520378010, 92520378011
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 02/09/21 12:250.33
Ethylbenzene ug/L ND 0.50 02/09/21 12:250.24
Hexachloro-1,3-butadiene ug/L ND 2.0 02/09/21 12:251.2
Isopropylbenzene (Cumene)ug/L ND 0.50 02/09/21 12:250.24
m&p-Xylene ug/L ND 1.0 02/09/21 12:250.44
Methyl-tert-butyl ether ug/L ND 0.50 02/09/21 12:250.44
Methylene Chloride ug/L ND 2.0 02/09/21 12:251.5
n-Butylbenzene ug/L ND 0.50 02/09/21 12:250.35
n-Propylbenzene ug/L ND 0.50 02/09/21 12:250.24
Naphthalene ug/L ND 2.0 02/09/21 12:250.66
o-Xylene ug/L ND 0.50 02/09/21 12:250.24
sec-Butylbenzene ug/L ND 0.50 02/09/21 12:250.25
Styrene ug/L ND 0.50 02/09/21 12:250.26
tert-Butylbenzene ug/L ND 0.50 02/09/21 12:250.25
Tetrachloroethene ug/L ND 0.50 02/09/21 12:250.23
Toluene ug/L ND 0.50 02/09/21 12:250.23
trans-1,2-Dichloroethene ug/L ND 0.50 02/09/21 12:250.26
trans-1,3-Dichloropropene ug/L ND 0.50 02/09/21 12:250.39
Trichloroethene ug/L ND 0.50 02/09/21 12:250.23
Trichlorofluoromethane ug/L ND 1.0 02/09/21 12:250.34
Vinyl chloride ug/L ND 1.0 02/09/21 12:250.41
1,2-Dichloroethane-d4 (S)%94 70-130 02/09/21 12:25
4-Bromofluorobenzene (S)%94 70-130 02/09/21 12:25
Toluene-d8 (S)%100 70-130 02/09/21 12:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3156160LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.050 104 60-140
1,1,1-Trichloroethane ug/L 47.750 95 60-140
1,1,2,2-Tetrachloroethane ug/L 50.150 100 60-140
1,1,2-Trichloroethane ug/L 50.850 102 60-140
1,1-Dichloroethane ug/L 47.750 95 60-140
1,1-Dichloroethene ug/L 46.850 94 60-140
1,1-Dichloropropene ug/L 46.650 93 60-140
1,2,3-Trichlorobenzene ug/L 49.450 99 60-140
1,2,3-Trichloropropane ug/L 49.250 98 60-140
1,2,4-Trichlorobenzene ug/L 52.150 104 60-140
1,2,4-Trimethylbenzene ug/L 48.950 98 60-140
1,2-Dibromo-3-chloropropane ug/L 54.250 108 60-140
1,2-Dibromoethane (EDB)ug/L 52.850 106 60-140
1,2-Dichlorobenzene ug/L 50.250 100 60-140
1,2-Dichloroethane ug/L 44.350 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3156160LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 49.950 100 60-140
1,3,5-Trimethylbenzene ug/L 47.350 95 60-140
1,3-Dichlorobenzene ug/L 50.150 100 60-140
1,3-Dichloropropane ug/L 51.250 102 60-140
1,4-Dichlorobenzene ug/L 48.750 97 60-140
2,2-Dichloropropane ug/L 48.350 97 60-140
2-Chlorotoluene ug/L 48.850 98 60-140
4-Chlorotoluene ug/L 48.450 97 60-140
Benzene ug/L 48.050 96 60-140
Bromobenzene ug/L 49.850 100 60-140
Bromochloromethane ug/L 49.450 99 60-140
Bromodichloromethane ug/L 50.950 102 60-140
Bromoform ug/L 55.150 110 60-140
Bromomethane ug/L 49.450 99 60-140
Carbon tetrachloride ug/L 48.750 97 60-140
Chlorobenzene ug/L 49.850 100 60-140
Chloroethane ug/L 49.350 99 60-140
Chloroform ug/L 47.450 95 60-140
Chloromethane ug/L 45.450 91 60-140
cis-1,2-Dichloroethene ug/L 47.150 94 60-140
cis-1,3-Dichloropropene ug/L 52.350 105 60-140
Dibromochloromethane ug/L 54.550 109 60-140
Dibromomethane ug/L 51.550 103 60-140
Dichlorodifluoromethane ug/L 50.850 102 60-140
Diisopropyl ether ug/L 44.850 90 60-140
Ethylbenzene ug/L 48.850 98 60-140
Hexachloro-1,3-butadiene ug/L 50.250 100 60-140
Isopropylbenzene (Cumene)ug/L 49.350 99 60-140
m&p-Xylene ug/L 96.0100 96 60-140
Methyl-tert-butyl ether ug/L 47.450 95 60-140
Methylene Chloride ug/L 45.250 90 60-140
n-Butylbenzene ug/L 47.750 95 60-140
n-Propylbenzene ug/L 46.450 93 60-140
Naphthalene ug/L 53.150 106 60-140
o-Xylene ug/L 49.950 100 60-140
sec-Butylbenzene ug/L 47.750 95 60-140
Styrene ug/L 50.450 101 60-140
tert-Butylbenzene ug/L 40.650 81 60-140
Tetrachloroethene ug/L 49.150 98 60-140
Toluene ug/L 47.850 96 60-140
trans-1,2-Dichloroethene ug/L 48.050 96 60-140
trans-1,3-Dichloropropene ug/L 51.050 102 60-140
Trichloroethene ug/L 49.450 99 60-140
Trichlorofluoromethane ug/L 42.650 85 60-140
Vinyl chloride ug/L 46.650 93 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3156160LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3156161MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519777002
3156162
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 106 60-140112 5 302000ND2130 2240
1,1,1-Trichloroethane ug/L 2000 102 60-140108 6 302000ND2040 2160
1,1,2,2-Tetrachloroethane ug/L 2000 98 60-140108 10 302000ND1960 2160
1,1,2-Trichloroethane ug/L 2000 103 60-140105 2 302000ND2070 2110
1,1-Dichloroethane ug/L 2000 102 60-140106 4 302000ND2040 2120
1,1-Dichloroethene ug/L 2000 110 60-140112 2 302000ND2210 2240
1,1-Dichloropropene ug/L 2000 103 60-140110 7 302000ND2060 2200
1,2,3-Trichlorobenzene ug/L 2000 97 60-140103 6 302000ND1940 2060
1,2,3-Trichloropropane ug/L 2000 98 60-140108 10 302000ND1960 2160
1,2,4-Trichlorobenzene ug/L 2000 101 60-140107 6 302000ND2020 2140
1,2,4-Trimethylbenzene ug/L M1,R120009060-140200 32 30200040005810 8000
1,2-Dibromo-3-
chloropropane ug/L 2000 104 60-140118 12 302000ND2080 2360
1,2-Dibromoethane (EDB) ug/L 2000 107 60-140110 3 302000ND2160 2230
1,2-Dichlorobenzene ug/L 2000 103 60-140107 5 302000ND2050 2150
1,2-Dichloroethane ug/L 2000 94 60-14096 2 302000ND1880 1920
1,2-Dichloropropane ug/L 2000 105 60-140108 3 302000ND2100 2170
1,3,5-Trimethylbenzene ug/L 2000 98 60-140136 21 30200012703230 3990
1,3-Dichlorobenzene ug/L 2000 104 60-140107 3 302000ND2080 2140
1,3-Dichloropropane ug/L 2000 102 60-140107 4 302000ND2050 2140
1,4-Dichlorobenzene ug/L 2000 100 60-140103 4 302000ND2000 2070
2,2-Dichloropropane ug/L 2000 104 60-140106 2 302000ND2080 2130
2-Chlorotoluene ug/L 2000 111 60-140118 7 302000ND2210 2370
4-Chlorotoluene ug/L 2000 102 60-140105 3 302000ND2040 2110
Benzene ug/L M1200010660-140197 30 30200031105240 7050
Bromobenzene ug/L 2000 105 60-140107 2 302000ND2100 2130
Bromochloromethane ug/L 2000 104 60-140105 1 302000ND2080 2100
Bromodichloromethane ug/L 2000 103 60-140105 2 302000ND2060 2110
Bromoform ug/L 2000 104 60-140114 9 302000ND2090 2290
Bromomethane ug/L 2000 107 60-140109 1 302000ND2150 2170
Carbon tetrachloride ug/L 2000 107 60-140112 4 302000ND2150 2230
Chlorobenzene ug/L 2000 107 60-140110 3 302000ND2130 2210
Chloroethane ug/L 2000 114 60-140115 0 302000ND2280 2290
Chloroform ug/L 2000 101 60-140105 4 302000ND2010 2100
Chloromethane ug/L 2000 95 60-140107 11 302000ND1910 2140
cis-1,2-Dichloroethene ug/L 2000 101 60-140105 4 302000ND2020 2100
cis-1,3-Dichloropropene ug/L 2000 110 60-140111 1 302000ND2200 2220
Dibromochloromethane ug/L 2000 108 60-140111 2 302000ND2170 2210
Dibromomethane ug/L 2000 106 60-140108 2 302000ND2120 2160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3156161MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519777002
3156162
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 2000 113 60-140116 2 302000ND2270 2320
Diisopropyl ether ug/L 2000 92 60-14097 5 302000ND1840 1950
Ethylbenzene ug/L M1200010760-140156 24 30200014803620 4600
Hexachloro-1,3-butadiene ug/L 2000 97 60-140107 9 302000ND1950 2140
Isopropylbenzene(Cumene)ug/L 2000 107 60-140115 7 3020001132250 2420
m&p-Xylene ug/L M1,R1400010360-140198 31 304000635010500 14300
Methyl-tert-butyl ether ug/L 2000 95 60-140101 6 302000ND1910 2020
Methylene Chloride ug/L 2000 96 60-140102 7 302000ND1910 2050
n-Butylbenzene ug/L 2000 116 60-140129 11 302000ND2320 2580
n-Propylbenzene ug/L 2000 116 60-140129 10 302000ND2330 2580
Naphthalene ug/L M120009460-140145 29 30200011603030 4050
o-Xylene ug/L M1,R1200010860-140215 32 30200034005560 7700
sec-Butylbenzene ug/L 2000 105 60-140112 6 302000ND2110 2240
Styrene ug/L 2000 107 60-140111 4 302000ND2130 2220
tert-Butylbenzene ug/L 2000 88 60-14092 5 302000ND1750 1840
Tetrachloroethene ug/L 2000 109 60-140111 2 302000ND2170 2210
Toluene ug/L M1,R1200010060-140330 36 302000841010400 15000
trans-1,2-Dichloroethene ug/L 2000 105 60-140109 4 302000ND2100 2180
trans-1,3-Dichloropropene ug/L 2000 103 60-140109 6 302000ND2060 2180
Trichloroethene ug/L 2000 107 60-140111 4 302000ND2150 2230
Trichlorofluoromethane ug/L 2000 109 60-140112 2 302000ND2180 2230
Vinyl chloride ug/L 2000 105 60-140108 3 302000ND2110 2170
1,2-Dichloroethane-d4 (S) %103 70-130101
4-Bromofluorobenzene (S) %101 70-130101
Toluene-d8 (S)%101 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
598767
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92520378012, 92520378013, 92520378014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3156847
Associated Lab Samples:92520378012, 92520378013, 92520378014
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/09/21 22:370.42
1,1,1-Trichloroethane ug/L ND 0.50 02/09/21 22:370.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/09/21 22:370.19
1,1,2-Trichloroethane ug/L ND 0.50 02/09/21 22:370.23
1,1-Dichloroethane ug/L ND 0.50 02/09/21 22:370.24
1,1-Dichloroethene ug/L ND 0.50 02/09/21 22:370.22
1,1-Dichloropropene ug/L ND 0.50 02/09/21 22:370.35
1,2,3-Trichlorobenzene ug/L ND 2.0 02/09/21 22:370.78
1,2,3-Trichloropropane ug/L ND 0.50 02/09/21 22:370.27
1,2,4-Trichlorobenzene ug/L ND 2.0 02/09/21 22:370.44
1,2,4-Trimethylbenzene ug/L ND 0.50 02/09/21 22:370.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/09/21 22:370.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/09/21 22:370.23
1,2-Dichlorobenzene ug/L ND 0.50 02/09/21 22:370.24
1,2-Dichloroethane ug/L ND 0.50 02/09/21 22:370.26
1,2-Dichloropropane ug/L ND 0.50 02/09/21 22:370.18
1,3,5-Trimethylbenzene ug/L ND 0.50 02/09/21 22:370.23
1,3-Dichlorobenzene ug/L ND 0.50 02/09/21 22:370.25
1,3-Dichloropropane ug/L ND 0.50 02/09/21 22:370.34
1,4-Dichlorobenzene ug/L ND 0.50 02/09/21 22:370.25
2,2-Dichloropropane ug/L ND 0.50 02/09/21 22:370.28
2-Chlorotoluene ug/L ND 0.50 02/09/21 22:370.21
4-Chlorotoluene ug/L ND 0.50 02/09/21 22:370.21
Benzene ug/L ND 0.50 02/09/21 22:370.24
Bromobenzene ug/L ND 0.50 02/09/21 22:370.22
Bromochloromethane ug/L ND 0.50 02/09/21 22:370.26
Bromodichloromethane ug/L ND 0.50 02/09/21 22:370.18
Bromoform ug/L ND 0.50 02/09/21 22:370.40
Bromomethane ug/L ND 5.0 02/09/21 22:371.7
Carbon tetrachloride ug/L ND 0.50 02/09/21 22:370.23
Chlorobenzene ug/L ND 0.50 02/09/21 22:370.22
Chloroethane ug/L ND 1.0 02/09/21 22:370.58
Chloroform ug/L ND 0.50 02/09/21 22:370.35
Chloromethane ug/L ND 1.0 02/09/21 22:370.42
cis-1,2-Dichloroethene ug/L ND 0.50 02/09/21 22:370.21
cis-1,3-Dichloropropene ug/L ND 0.50 02/09/21 22:370.36
Dibromochloromethane ug/L ND 0.50 02/09/21 22:370.40
Dibromomethane ug/L ND 0.50 02/09/21 22:370.31
Dichlorodifluoromethane ug/L ND 0.50 02/09/21 22:370.28
Diisopropyl ether ug/L ND 0.50 02/09/21 22:370.33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3156847
Associated Lab Samples:92520378012, 92520378013, 92520378014
Matrix: Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 02/09/21 22:370.24
Hexachloro-1,3-butadiene ug/L ND 2.0 02/09/21 22:371.2
Isopropylbenzene (Cumene)ug/L ND 0.50 02/09/21 22:370.24
m&p-Xylene ug/L ND 1.0 02/09/21 22:370.44
Methyl-tert-butyl ether ug/L ND 0.50 02/09/21 22:370.44
Methylene Chloride ug/L ND 2.0 02/09/21 22:371.5
n-Butylbenzene ug/L ND 0.50 02/09/21 22:370.35
n-Propylbenzene ug/L ND 0.50 02/09/21 22:370.24
Naphthalene ug/L ND 2.0 02/09/21 22:370.66
o-Xylene ug/L ND 0.50 02/09/21 22:370.24
sec-Butylbenzene ug/L ND 0.50 02/09/21 22:370.25
Styrene ug/L ND 0.50 02/09/21 22:370.26
tert-Butylbenzene ug/L ND 0.50 02/09/21 22:370.25
Tetrachloroethene ug/L ND 0.50 02/09/21 22:370.23
Toluene ug/L ND 0.50 02/09/21 22:370.23
trans-1,2-Dichloroethene ug/L ND 0.50 02/09/21 22:370.26
trans-1,3-Dichloropropene ug/L ND 0.50 02/09/21 22:370.39
Trichloroethene ug/L ND 0.50 02/09/21 22:370.23
Trichlorofluoromethane ug/L ND 1.0 02/09/21 22:370.34
Vinyl chloride ug/L ND 1.0 02/09/21 22:370.41
1,2-Dichloroethane-d4 (S)%94 70-130 02/09/21 22:37
4-Bromofluorobenzene (S)%97 70-130 02/09/21 22:37
Toluene-d8 (S)%100 70-130 02/09/21 22:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3156848LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 68.050 136 60-140
1,1,1-Trichloroethane ug/L 61.850 124 60-140
1,1,2,2-Tetrachloroethane ug/L 69.950 140 60-140
1,1,2-Trichloroethane ug/L 71.5 L150143 60-140
1,1-Dichloroethane ug/L 61.950 124 60-140
1,1-Dichloroethene ug/L 58.850 118 60-140
1,1-Dichloropropene ug/L 60.450 121 60-140
1,2,3-Trichlorobenzene ug/L 65.550 131 60-140
1,2,3-Trichloropropane ug/L 67.450 135 60-140
1,2,4-Trichlorobenzene ug/L 68.050 136 60-140
1,2,4-Trimethylbenzene ug/L 62.550 125 60-140
1,2-Dibromo-3-chloropropane ug/L 78.3 L150157 60-140
1,2-Dibromoethane (EDB)ug/L 71.6 L150143 60-140
1,2-Dichlorobenzene ug/L 65.850 132 60-140
1,2-Dichloroethane ug/L 58.950 118 60-140
1,2-Dichloropropane ug/L 66.350 133 60-140
1,3,5-Trimethylbenzene ug/L 60.850 122 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3156848LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 65.750 131 60-140
1,3-Dichloropropane ug/L 67.650 135 60-140
1,4-Dichlorobenzene ug/L 63.450 127 60-140
2,2-Dichloropropane ug/L 61.550 123 60-140
2-Chlorotoluene ug/L 62.850 126 60-140
4-Chlorotoluene ug/L 62.450 125 60-140
Benzene ug/L 63.350 127 60-140
Bromobenzene ug/L 64.750 129 60-140
Bromochloromethane ug/L 67.850 136 60-140
Bromodichloromethane ug/L 67.850 136 60-140
Bromoform ug/L 76.9 L150154 60-140
Bromomethane ug/L 64.250 128 60-140
Carbon tetrachloride ug/L 64.450 129 60-140
Chlorobenzene ug/L 64.750 129 60-140
Chloroethane ug/L 66.750 133 60-140
Chloroform ug/L 60.050 120 60-140
Chloromethane ug/L 57.750 115 60-140
cis-1,2-Dichloroethene ug/L 61.150 122 60-140
cis-1,3-Dichloropropene ug/L 67.950 136 60-140
Dibromochloromethane ug/L 71.7 L150143 60-140
Dibromomethane ug/L 71.1 L150142 60-140
Dichlorodifluoromethane ug/L 65.250 130 60-140
Diisopropyl ether ug/L 60.750 121 60-140
Ethylbenzene ug/L 63.050 126 60-140
Hexachloro-1,3-butadiene ug/L 62.050 124 60-140
Isopropylbenzene (Cumene)ug/L 63.850 128 60-140
m&p-Xylene ug/L 123100 123 60-140
Methyl-tert-butyl ether ug/L 66.650 133 60-140
Methylene Chloride ug/L 59.250 118 60-140
n-Butylbenzene ug/L 60.450 121 60-140
n-Propylbenzene ug/L 58.350 117 60-140
Naphthalene ug/L 70.5 L150141 60-140
o-Xylene ug/L 65.250 130 60-140
sec-Butylbenzene ug/L 60.150 120 60-140
Styrene ug/L 65.550 131 60-140
tert-Butylbenzene ug/L 51.950 104 60-140
Tetrachloroethene ug/L 63.150 126 60-140
Toluene ug/L 62.950 126 60-140
trans-1,2-Dichloroethene ug/L 62.950 126 60-140
trans-1,3-Dichloropropene ug/L 69.850 140 60-140
Trichloroethene ug/L 65.150 130 60-140
Trichlorofluoromethane ug/L 48.950 98 60-140
Vinyl chloride ug/L 59.150 118 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3156849MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92520378013
3156850
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 94 60-140110 16 3020ND18.8 22.0
1,1,1-Trichloroethane ug/L 20 90 60-140105 15 3020ND18.0 20.9
1,1,2,2-Tetrachloroethane ug/L 20 87 60-140104 17 3020ND17.4 20.7
1,1,2-Trichloroethane ug/L 20 87 60-140106 19 3020ND17.5 21.2
1,1-Dichloroethane ug/L 20 88 60-140104 16 3020ND17.6 20.7
1,1-Dichloroethene ug/L 20 92 60-140110 18 3020ND18.5 22.0
1,1-Dichloropropene ug/L 20 89 60-140103 15 3020ND17.8 20.6
1,2,3-Trichlorobenzene ug/L 20 100 60-140106 6 3020ND20.0 21.2
1,2,3-Trichloropropane ug/L 20 87 60-140104 18 3020ND17.4 20.8
1,2,4-Trichlorobenzene ug/L 20 99 60-140111 12 3020ND19.7 22.2
1,2,4-Trimethylbenzene ug/L 20 88 60-140106 18 3020ND17.6 21.1
1,2-Dibromo-3-
chloropropane ug/L 20 99 60-140114 14 3020ND19.7 22.7
1,2-Dibromoethane (EDB) ug/L 20 90 60-140111 21 3020ND18.0 22.2
1,2-Dichlorobenzene ug/L 20 88 60-140103 16 3020ND17.6 20.6
1,2-Dichloroethane ug/L 20 77 60-14093 18 3020ND15.5 18.5
1,2-Dichloropropane ug/L 20 91 60-140104 14 3020ND18.1 20.9
1,3,5-Trimethylbenzene ug/L 20 90 60-140105 16 3020ND18.0 21.0
1,3-Dichlorobenzene ug/L 20 91 60-140106 15 3020ND18.1 21.1
1,3-Dichloropropane ug/L 20 87 60-140108 21 3020ND17.4 21.5
1,4-Dichlorobenzene ug/L 20 87 60-140103 17 3020ND17.4 20.6
2,2-Dichloropropane ug/L 20 94 60-140110 15 3020ND18.8 21.9
2-Chlorotoluene ug/L 20 89 60-140107 19 3020ND17.8 21.5
4-Chlorotoluene ug/L 20 89 60-140105 17 3020ND17.8 21.1
Benzene ug/L 20 88 60-140103 15 3020ND17.6 20.6
Bromobenzene ug/L 20 91 60-140107 16 3020ND18.2 21.4
Bromochloromethane ug/L 20 87 60-140100 14 3020ND17.3 20.0
Bromodichloromethane ug/L 20 88 60-140106 18 3020ND17.6 21.1
Bromoform ug/L 20 95 60-140114 18 3020ND19.0 22.8
Bromomethane ug/L 20 121 60-140129 7 3020ND24.2 25.9
Carbon tetrachloride ug/L 20 94 60-140110 16 3020ND18.8 22.0
Chlorobenzene ug/L 20 92 60-140108 16 3020ND18.5 21.7
Chloroethane ug/L 20 89 60-140106 17 3020ND17.8 21.1
Chloroform ug/L 20 84 60-140105 22 3020ND16.8 21.0
Chloromethane ug/L 20 86 60-14096 10 3020ND17.3 19.1
cis-1,2-Dichloroethene ug/L 20 85 60-140101 17 3020ND17.0 20.2
cis-1,3-Dichloropropene ug/L 20 93 60-140111 18 3020ND18.6 22.2
Dibromochloromethane ug/L 20 95 60-140109 15 3020ND18.9 21.9
Dibromomethane ug/L 20 96 60-140111 14 3020ND19.2 22.1
Dichlorodifluoromethane ug/L 20 81 60-14094 15 3020ND16.2 18.8
Diisopropyl ether ug/L 20 77 60-14093 18 3020ND15.4 18.5
Ethylbenzene ug/L 20 92 60-140109 17 3020ND18.3 21.7
Hexachloro-1,3-butadiene ug/L 20 108 60-140117 9 3020ND21.5 23.5
Isopropylbenzene(Cumene)ug/L 20 93 60-140109 16 3020ND18.6 21.8
m&p-Xylene ug/L 40 90 60-140107 17 3040ND36.0 42.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3156849MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92520378013
3156850
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 83 60-14097 15 3020ND16.7 19.4
Methylene Chloride ug/L 20 83 60-14097 16 3020ND16.5 19.3
n-Butylbenzene ug/L 20 93 60-140107 13 3020ND18.6 21.3
n-Propylbenzene ug/L 20 87 60-140103 17 3020ND17.5 20.7
Naphthalene ug/L 20 104 60-140107 3 3020ND20.7 21.4
o-Xylene ug/L 20 91 60-140108 17 3020ND18.3 21.7
sec-Butylbenzene ug/L 20 90 60-140106 16 3020ND18.0 21.3
Styrene ug/L 20 87 60-140104 18 3020ND17.4 20.9
tert-Butylbenzene ug/L 20 77 60-14092 18 3020ND15.5 18.5
Tetrachloroethene ug/L 20 92 60-140113 20 3020ND18.3 22.5
Toluene ug/L 20 92 60-140105 13 3020ND18.4 21.0
trans-1,2-Dichloroethene ug/L 20 92 60-140106 14 3020ND18.4 21.2
trans-1,3-Dichloropropene ug/L 20 92 60-140108 16 3020ND18.3 21.5
Trichloroethene ug/L 20 94 60-140111 17 3020ND18.9 22.3
Trichlorofluoromethane ug/L 20 92 60-140109 16 3020ND18.5 21.7
Vinyl chloride ug/L 20 85 60-14099 14 3020ND17.1 19.7
1,2-Dichloroethane-d4 (S) %98 70-13099
4-Bromofluorobenzene (S) %99 70-13098
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
598947
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92520378003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3157513
Associated Lab Samples:92520378003
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/10/21 23:150.42
1,1,1-Trichloroethane ug/L ND 0.50 02/10/21 23:150.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/10/21 23:150.19
1,1,2-Trichloroethane ug/L ND 0.50 02/10/21 23:150.23
1,1-Dichloroethane ug/L ND 0.50 02/10/21 23:150.24
1,1-Dichloroethene ug/L ND 0.50 02/10/21 23:150.22
1,1-Dichloropropene ug/L ND 0.50 02/10/21 23:150.35
1,2,3-Trichlorobenzene ug/L ND 2.0 02/10/21 23:150.78
1,2,3-Trichloropropane ug/L ND 0.50 02/10/21 23:150.27
1,2,4-Trichlorobenzene ug/L ND 2.0 02/10/21 23:150.44
1,2,4-Trimethylbenzene ug/L ND 0.50 02/10/21 23:150.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/10/21 23:150.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/10/21 23:150.23
1,2-Dichlorobenzene ug/L ND 0.50 02/10/21 23:150.24
1,2-Dichloroethane ug/L ND 0.50 02/10/21 23:150.26
1,2-Dichloropropane ug/L ND 0.50 02/10/21 23:150.18
1,3,5-Trimethylbenzene ug/L ND 0.50 02/10/21 23:150.23
1,3-Dichlorobenzene ug/L ND 0.50 02/10/21 23:150.25
1,3-Dichloropropane ug/L ND 0.50 02/10/21 23:150.34
1,4-Dichlorobenzene ug/L ND 0.50 02/10/21 23:150.25
2,2-Dichloropropane ug/L ND 0.50 02/10/21 23:150.28
2-Chlorotoluene ug/L ND 0.50 02/10/21 23:150.21
4-Chlorotoluene ug/L ND 0.50 02/10/21 23:150.21
Benzene ug/L ND 0.50 02/10/21 23:150.24
Bromobenzene ug/L ND 0.50 02/10/21 23:150.22
Bromochloromethane ug/L ND 0.50 02/10/21 23:150.26
Bromodichloromethane ug/L ND 0.50 02/10/21 23:150.18
Bromoform ug/L ND 0.50 02/10/21 23:150.40
Bromomethane ug/L ND 5.0 02/10/21 23:151.7
Carbon tetrachloride ug/L ND 0.50 02/10/21 23:150.23
Chlorobenzene ug/L ND 0.50 02/10/21 23:150.22
Chloroethane ug/L ND 1.0 02/10/21 23:150.58
Chloroform ug/L ND 0.50 02/10/21 23:150.35
Chloromethane ug/L ND 1.0 02/10/21 23:150.42
cis-1,2-Dichloroethene ug/L ND 0.50 02/10/21 23:150.21
cis-1,3-Dichloropropene ug/L ND 0.50 02/10/21 23:150.36
Dibromochloromethane ug/L ND 0.50 02/10/21 23:150.40
Dibromomethane ug/L ND 0.50 02/10/21 23:150.31
Dichlorodifluoromethane ug/L ND 0.50 02/10/21 23:150.28
Diisopropyl ether ug/L ND 0.50 02/10/21 23:150.33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3157513
Associated Lab Samples:92520378003
Matrix: Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 02/10/21 23:150.24
Hexachloro-1,3-butadiene ug/L ND 2.0 02/10/21 23:151.2
Isopropylbenzene (Cumene)ug/L ND 0.50 02/10/21 23:150.24
m&p-Xylene ug/L ND 1.0 02/10/21 23:150.44
Methyl-tert-butyl ether ug/L ND 0.50 02/10/21 23:150.44
Methylene Chloride ug/L ND 2.0 02/10/21 23:151.5
n-Butylbenzene ug/L ND 0.50 02/10/21 23:150.35
n-Propylbenzene ug/L ND 0.50 02/10/21 23:150.24
Naphthalene ug/L ND 2.0 02/10/21 23:150.66
o-Xylene ug/L ND 0.50 02/10/21 23:150.24
sec-Butylbenzene ug/L ND 0.50 02/10/21 23:150.25
Styrene ug/L ND 0.50 02/10/21 23:150.26
tert-Butylbenzene ug/L ND 0.50 02/10/21 23:150.25
Tetrachloroethene ug/L ND 0.50 02/10/21 23:150.23
Toluene ug/L ND 0.50 02/10/21 23:150.23
trans-1,2-Dichloroethene ug/L ND 0.50 02/10/21 23:150.26
trans-1,3-Dichloropropene ug/L ND 0.50 02/10/21 23:150.39
Trichloroethene ug/L ND 0.50 02/10/21 23:150.23
Trichlorofluoromethane ug/L ND 1.0 02/10/21 23:150.34
Vinyl chloride ug/L ND 1.0 02/10/21 23:150.41
1,2-Dichloroethane-d4 (S)%91 70-130 02/10/21 23:15
4-Bromofluorobenzene (S)%96 70-130 02/10/21 23:15
Toluene-d8 (S)%99 70-130 02/10/21 23:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3157514LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,1-Trichloroethane ug/L 45.150 90 60-140
1,1,2,2-Tetrachloroethane ug/L 48.150 96 60-140
1,1,2-Trichloroethane ug/L 48.750 97 60-140
1,1-Dichloroethane ug/L 43.350 87 60-140
1,1-Dichloroethene ug/L 43.750 87 60-140
1,1-Dichloropropene ug/L 44.050 88 60-140
1,2,3-Trichlorobenzene ug/L 49.150 98 60-140
1,2,3-Trichloropropane ug/L 48.450 97 60-140
1,2,4-Trichlorobenzene ug/L 50.950 102 60-140
1,2,4-Trimethylbenzene ug/L 45.750 91 60-140
1,2-Dibromo-3-chloropropane ug/L 57.150 114 60-140
1,2-Dibromoethane (EDB)ug/L 50.750 101 60-140
1,2-Dichlorobenzene ug/L 49.150 98 60-140
1,2-Dichloroethane ug/L 41.050 82 60-140
1,2-Dichloropropane ug/L 45.450 91 60-140
1,3,5-Trimethylbenzene ug/L 45.550 91 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
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[phone]
Page 48 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3157514LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.050 98 60-140
1,3-Dichloropropane ug/L 45.950 92 60-140
1,4-Dichlorobenzene ug/L 47.850 96 60-140
2,2-Dichloropropane ug/L 44.350 89 60-140
2-Chlorotoluene ug/L 47.150 94 60-140
4-Chlorotoluene ug/L 45.650 91 60-140
Benzene ug/L 44.650 89 60-140
Bromobenzene ug/L 48.350 97 60-140
Bromochloromethane ug/L 47.550 95 60-140
Bromodichloromethane ug/L 47.750 95 60-140
Bromoform ug/L 55.550 111 60-140
Bromomethane ug/L 51.250 102 60-140
Carbon tetrachloride ug/L 49.050 98 60-140
Chlorobenzene ug/L 48.250 96 60-140
Chloroethane ug/L 49.650 99 60-140
Chloroform ug/L 43.950 88 60-140
Chloromethane ug/L 40.550 81 60-140
cis-1,2-Dichloroethene ug/L 43.050 86 60-140
cis-1,3-Dichloropropene ug/L 49.250 98 60-140
Dibromochloromethane ug/L 54.850 110 60-140
Dibromomethane ug/L 52.350 105 60-140
Dichlorodifluoromethane ug/L 49.250 98 60-140
Diisopropyl ether ug/L 40.650 81 60-140
Ethylbenzene ug/L 47.350 95 60-140
Hexachloro-1,3-butadiene ug/L 49.350 99 60-140
Isopropylbenzene (Cumene)ug/L 48.250 96 60-140
m&p-Xylene ug/L 92.6100 93 60-140
Methyl-tert-butyl ether ug/L 44.750 89 60-140
Methylene Chloride ug/L 39.950 80 60-140
n-Butylbenzene ug/L 44.550 89 60-140
n-Propylbenzene ug/L 43.450 87 60-140
Naphthalene ug/L 52.850 106 60-140
o-Xylene ug/L 48.350 97 60-140
sec-Butylbenzene ug/L 45.550 91 60-140
Styrene ug/L 48.850 98 60-140
tert-Butylbenzene ug/L 39.550 79 60-140
Tetrachloroethene ug/L 48.750 97 60-140
Toluene ug/L 46.150 92 60-140
trans-1,2-Dichloroethene ug/L 43.850 88 60-140
trans-1,3-Dichloropropene ug/L 48.850 98 60-140
Trichloroethene ug/L 49.650 99 60-140
Trichlorofluoromethane ug/L 42.150 84 60-140
Vinyl chloride ug/L 43.050 86 60-140
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3159201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92520734001
3159202
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 1000 107 60-140108 1 301000<21.1 1070 1080
1,1,1-Trichloroethane ug/L 1000 97 60-14098 1 301000<13.9 969 980
1,1,2,2-Tetrachloroethane ug/L 1000 98 60-140100 2 301000<9.6 980 1000
1,1,2-Trichloroethane ug/L 1000 104 60-140103 1 301000<11.6 1040 1030
1,1-Dichloroethane ug/L 1000 92 60-14094 2 301000<12.2 919 938
1,1-Dichloroethene ug/L 1000 93 60-14097 4 301000<10.9 934 971
1,1-Dichloropropene ug/L 1000 95 60-14097 3 301000<17.4 945 971
1,2,3-Trichlorobenzene ug/L 1000 117 60-140114 3 301000<39.0 1170 1140
1,2,3-Trichloropropane ug/L 1000 97 60-14096 1 301000<13.6 972 958
1,2,4-Trichlorobenzene ug/L 1000 119 60-140114 4 301000<21.8 1190 1140
1,2,4-Trimethylbenzene ug/L 1000 91 60-140103 7 3010007941710 1830
1,2-Dibromo-3-
chloropropane ug/L 1000 117 60-140119 2 301000<19.2 1170 1190
1,2-Dibromoethane (EDB) ug/L 1000 103 60-140108 4 3010001151140 1190
1,2-Dichlorobenzene ug/L 1000 103 60-140103 0 301000<12.0 1030 1030
1,2-Dichloroethane ug/L 1000 84 60-14086 2 30100033.7 872 892
1,2-Dichloropropane ug/L 1000 96 60-14096 0 301000<9.2 957 961
1,3,5-Trimethylbenzene ug/L 1000 122 60-140126 3 301000<11.4 1220 1260
1,3-Dichlorobenzene ug/L 1000 106 60-140105 1 301000<12.5 1060 1050
1,3-Dichloropropane ug/L 1000 99 60-14098 0 301000<17.0 987 985
1,4-Dichlorobenzene ug/L 1000 102 60-140101 0 301000<12.4 1020 1010
2,2-Dichloropropane ug/L 1000 100 60-140103 3 301000<14.0 1000 1030
2-Chlorotoluene ug/L 1000 102 60-140103 1 301000<10.4 1020 1030
4-Chlorotoluene ug/L 1000 99 60-140102 3 301000<10.3 988 1020
Benzene ug/L 1000 64 60-14093 11 30100017702410 2700
Bromobenzene ug/L 1000 104 60-140107 3 301000<10.8 1040 1070
Bromochloromethane ug/L 1000 94 60-14096 2 301000<12.9 943 962
Bromodichloromethane ug/L 1000 100 60-140102 1 301000<9.2 1000 1020
Bromoform ug/L 1000 111 60-140110 1 301000<20.2 1110 1100
Bromomethane ug/L 1000 132 60-140132 0 301000<86.0 1320 1320
Carbon tetrachloride ug/L 1000 110 60-140110 0 301000<11.6 1100 1100
Chlorobenzene ug/L 1000 101 60-140102 1 301000<11.2 1010 1020
Chloroethane ug/L 1000 98 60-140107 9 301000<29.2 983 1070
Chloroform ug/L 1000 91 60-14097 6 301000<17.6 906 967
Chloromethane ug/L 1000 94 60-14096 1 301000<20.8 942 956
cis-1,2-Dichloroethene ug/L 1000 90 60-14091 2 301000<10.4 895 914
cis-1,3-Dichloropropene ug/L 1000 104 60-140105 1 301000<17.8 1040 1050
Dibromochloromethane ug/L 1000 109 60-140108 1 301000<20.1 1090 1080
Dibromomethane ug/L 1000 111 60-140107 4 301000<15.5 1110 1070
Dichlorodifluoromethane ug/L 1000 107 60-140110 3 301000<14.2 1070 1100
Diisopropyl ether ug/L 1000 82 60-14084 3 301000<16.7 817 840
Ethylbenzene ug/L 1000 95 60-140101 4 3010004371390 1450
Hexachloro-1,3-butadiene ug/L 1000 125 60-140121 3 301000<60.0 1250 1210
Isopropylbenzene(Cumene)ug/L 1000 106 60-140105 0 30100040.2 1100 1090
m&p-Xylene ug/L 2000 84 60-14097 7 30200018903580 3840
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92520378
HULL'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3159201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92520734001
3159202
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 1000 88 60-14090 2 301000<22.2 896 915
Methylene Chloride ug/L 1000 84 60-14085 1 301000<75.0 835 847
n-Butylbenzene ug/L 1000 106 60-140108 2 301000<17.6 1060 1080
n-Propylbenzene ug/L 1000 106 60-140110 4 301000<12.0 1060 1100
Naphthalene ug/L 1000 108 60-140106 1 3010002661340 1330
o-Xylene ug/L 1000 89 60-140100 5 30100011802070 2180
sec-Butylbenzene ug/L 1000 105 60-140105 1 301000<12.3 1050 1050
Styrene ug/L 1000 100 60-140101 0 301000<12.8 1000 1010
tert-Butylbenzene ug/L 1000 87 60-14089 3 301000<12.5 871 893
Tetrachloroethene ug/L 1000 106 60-140106 1 301000<11.6 1060 1060
Toluene ug/L M11000-25 60-14074 13 30100074607200 8200
trans-1,2-Dichloroethene ug/L 1000 92 60-14097 5 301000<12.8 924 973
trans-1,3-Dichloropropene ug/L 1000 100 60-140101 0 301000<19.7 1000 1010
Trichloroethene ug/L 1000 108 60-140106 2 301000<11.6 1080 1060
Trichlorofluoromethane ug/L 1000 107 60-140107 1 301000<16.8 1070 1070
Vinyl chloride ug/L 1000 93 60-14097 5 301000<20.4 929 972
1,2-Dichloroethane-d4 (S) %94 70-13092
4-Bromofluorobenzene (S) %100 70-13098
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 58
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92520378
HULL'S 66
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 58
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92520378
HULL'S 66
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92520378001 598656MW-1 SM 6200B
92520378002 598656MW-2 SM 6200B
92520378003 598947MW-3 SM 6200B
92520378004 598656MW-4 SM 6200B
92520378005 598656MW-5 SM 6200B
92520378006 598656MW-6 SM 6200B
92520378007 598656MW-7 SM 6200B
92520378008 598656MW-8 SM 6200B
92520378009 598656MW-9 SM 6200B
92520378010 598656MW-10 SM 6200B
92520378011 598656DMW-1 SM 6200B
92520378012 598767FBSM 6200B
92520378013 598767WSW-10 SM 6200B
92520378014 598767TBSM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/11/2021 12:33 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 58
Page 54 of 58
Page 55 of 58
Page 56 of 58
Page 57 of 58
Page 58 of 58

APPENDIX B
FIELD NOTES

APPENDIX C
PHOTOGRAPHS

Project No. 71179011A Date Photos Taken: February 3, 2021

Hull’s 66 (Incident No. 40162) – Monitoring Report
Photo 1: View of well MW-4.

Photo 2: View of wells DMW-1 (red arrow) and MW-2 (yellow arrow).
Project No. 71179011A Date Photos Taken: February 3, 2021

Hull’s 66 (Incident No. 40162) – Monitoring Report
Photo 3: View of well MW-6, at the front of the service bays for repair shop.

Photo 4: View of well MW-7.
Project No. 71179011A Date Photos Taken: February 3, 2021

Hull’s 66 (Incident No. 40162) – Monitoring Report
Photo 5: View of well MW-8.

Photo 6: View of well MW-3.

Project No. 71179011A Date Photos Taken: February 3, 2021

Hull’s 66 (Incident No. 40162) – Monitoring Report
Photo 7: View of well MW-2 (red arrow) and MW-1 (yellow arrow).

Photo 8: View of well MW-10 located northeast of site across NC Highway 27.

Project No. 71179011A Date Photos Taken: February 3, 2021

Hull’s 66 (Incident No. 40162) – Monitoring Report
Photo 9: View of well MW-9 to the north of the site across NC Highway 27.

Photo 10: View of water supply well WSW-10. (Taken March 2020)