MO-7074_40162_CA_LAB_20221018

10/26/22
Technical Report for
Terracon Consulting
Hulls 66; 6711 NC Hwy 27W, Vale, NC
71179011
SGS Job Number: FA99892
Sampling Date: 10/18/22
Report to:
Terracon
2701 Westport Rd
Charlotte, NC 28208
[e-mail]
ATTN: Ayla Honer
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Kelly Blanchard 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 10/26/22
e-Hardcopy 2.0
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Unauthorized modification of this report is strictly prohibited.
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FA99892
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................8
3.1: FA99892-1: MW-1 ........................................................................................................9
3.2: FA99892-2: MW-2 ........................................................................................................12
3.3: FA99892-3: MW-3 ........................................................................................................15
3.4: FA99892-4: MW-4 ........................................................................................................18
3.5: FA99892-5: MW-5 ........................................................................................................21
3.6: FA99892-6: MW-6 ........................................................................................................24
3.7: FA99892-7: MW-8 ........................................................................................................27
3.8: FA99892-8: MW-9 ........................................................................................................30
3.9: FA99892-9: MW-10 ......................................................................................................33
3.10: FA99892-10: DMW-1 .................................................................................................36
3.11: FA99892-11: WSW-10 ................................................................................................39
3.12: FA99892-12: WSW-16 ...............................................................................................43
3.13: FA99892-13: FB .........................................................................................................47
Section 4: Misc. Forms ............................................................................................................50
4.1: Chain of Custody ...........................................................................................................51
Section 5: MS Volatiles - QC Data Summaries .....................................................................54
5.1: Method Blank Summary ................................................................................................55
5.2: Blank Spike Summary ...................................................................................................58
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................61
Section 6: GC Volatiles - QC Data Summaries .....................................................................64
6.1: Method Blank Summary ................................................................................................65
6.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................66
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................67 1234562 of 67
FA99892
SGS North America Inc.
Sample Summary
Terracon Consulting
Job No:FA99892
Hulls 66; 6711 NC Hwy 27W, Vale, NC
Project No: 71179011
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA99892-1 10/18/22 10:20 THC 10/20/22 AQ Ground Water MW-1
FA99892-2 10/18/22 12:10 THC 10/20/22 AQ Ground Water MW-2
FA99892-3 10/18/22 13:50 THC 10/20/22 AQ Ground Water MW-3
FA99892-4 10/18/22 12:50 THC 10/20/22 AQ Ground Water MW-4
FA99892-5 10/18/22 12:30 THC 10/20/22 AQ Ground Water MW-5
FA99892-6 10/18/22 11:00 THC 10/20/22 AQ Ground Water MW-6
FA99892-7 10/18/22 11:55 THC 10/20/22 AQ Ground Water MW-8
FA99892-8 10/18/22 14:15 THC 10/20/22 AQ Ground Water MW-9
FA99892-9 10/18/22 13:30 THC 10/20/22 AQ Ground Water MW-10
FA99892-10 10/18/22 11:30 THC 10/20/22 AQ Ground Water DMW-1
FA99892-11 10/18/22 15:10 THC 10/20/22 AQ Ground Water WSW-10
FA99892-12 10/18/22 15:10 THC 10/20/22 AQ Ground Water WSW-16
3 of 67
FA998921
SGS North America Inc.
Sample Summary
(continued)
Terracon Consulting
Job No:FA99892
Hulls 66; 6711 NC Hwy 27W, Vale, NC
Project No: 71179011
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA99892-13 10/18/22 10:40 THC 10/20/22 AQ Field Blank Water FB
4 of 67
FA998921
Summary of Hits Page 1 of 3
Job Number:FA99892
Account:Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Collected:10/18/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA99892-1 MW-1
Chloroform 0.23 J 0.50 0.13 ug/l SM 6200B
FA99892-2 MW-2
n-Butylbenzene 4.3 J 10 2.5 ug/l SM 6200B
sec-Butylbenzene 3.2 J 10 2.5 ug/l SM 6200B
o-Chlorotoluene 22.8 10 2.5 ug/l SM 6200B
Ethylbenzene 189 10 2.5 ug/l SM 6200B
Isopropylbenzene 12.8 10 2.5 ug/l SM 6200B
Naphthalene 30.7 10 2.5 ug/l SM 6200B
n-Propylbenzene 29.1 10 2.5 ug/l SM 6200B
Toluene 24.4 10 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 426 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 187 10 2.5 ug/l SM 6200B
m,p-Xylene 1120 20 2.5 ug/l SM 6200B
o-Xylene 529 10 2.5 ug/l SM 6200B
Xylene (total)1640 30 5.0 ug/l SM 6200B
FA99892-3 MW-3
No hits reported in this sample.
FA99892-4 MW-4
Chloroform 0.53 0.50 0.13 ug/l SM 6200B
FA99892-5 MW-5
Acetone 2.6 J 10 2.0 ug/l SM 6200B
n-Butylbenzene 0.19 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.17 J 0.50 0.13 ug/l SM 6200B
Chloroform 1.7 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 0.53 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.27 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.69 0.50 0.13 ug/l SM 6200B
Naphthalene 0.22 J 0.50 0.13 ug/l SM 6200B
1,1,2,2-Tetrachloroethane 0.17 J 0.50 0.13 ug/l SM 6200B
FA99892-6 MW-6
Bromodichloromethane 1.0 0.50 0.13 ug/l SM 6200B
Chloroform 16.0 0.50 0.13 ug/l SM 6200B
5 of 67
FA998922
Summary of Hits Page 2 of 3
Job Number:FA99892
Account:Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Collected:10/18/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA99892-7 MW-8
Acetone 2.7 J 10 2.0 ug/l SM 6200B
Chloroform 0.78 0.50 0.13 ug/l SM 6200B
FA99892-8 MW-9
Chloroform 0.63 0.50 0.13 ug/l SM 6200B
FA99892-9 MW-10
Acetone 179 50 10 ug/l SM 6200B
Benzene 58.3 2.5 0.63 ug/l SM 6200B
n-Butylbenzene 2.8 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene 4.3 2.5 0.63 ug/l SM 6200B
tert-Butylbenzene 1.5 J 2.5 0.63 ug/l SM 6200B
Chloroethane 2.4 J 2.5 1.0 ug/l SM 6200B
Ethylbenzene 174 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 50.5 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene 2.4 J 2.5 0.63 ug/l SM 6200B
Methyl Chloride 1.7 J 2.5 1.0 ug/l SM 6200B
Methylene Chloride 5.4 J 10 5.0 ug/l SM 6200B
Naphthalene 28.4 2.5 0.63 ug/l SM 6200B
n-Propylbenzene 21.5 2.5 0.63 ug/l SM 6200B
Toluene 2.4 J 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene 56.3 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene 32.3 2.5 0.63 ug/l SM 6200B
Vinyl Acetate 26.6 25 5.0 ug/l SM 6200B
m,p-Xylene 62.1 5.0 0.63 ug/l SM 6200B
Xylene (total)62.1 7.5 1.3 ug/l SM 6200B
FA99892-10 DMW-1
Chloroform 0.88 0.50 0.13 ug/l SM 6200B
FA99892-11 WSW-10
No hits reported in this sample.
FA99892-12 WSW-16
No hits reported in this sample.
6 of 67
FA998922
Summary of Hits Page 3 of 3
Job Number:FA99892
Account:Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Collected:10/18/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA99892-13 FB
No hits reported in this sample.
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FA998922
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
8 of 67
FA998923
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA99892-1 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235122.D 1 10/25/22 12:56 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.23 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 67
FA9989233.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA99892-1 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 67
FA9989233.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA99892-1 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 67
FA9989233.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:FA99892-2 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235129.D 20 10/25/22 15:37 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 40 ug/l
71-43-2 Benzene ND 10 2.5 ug/l
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
78-93-3 2-Butanone (MEK)ND 50 25 ug/l
104-51-8 n-Butylbenzene 4.3 10 2.5 ug/l J
135-98-8 sec-Butylbenzene 3.2 10 2.5 ug/l J
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane ND 10 4.0 ug/l
67-66-3 Chloroform ND 10 2.5 ug/l
95-49-8 o-Chlorotoluene 22.8 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 67
FA9989233.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FA99892-2 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l
64-17-5 Ethyl Alcohol a ND 2000 1300 ug/l
100-41-4 Ethylbenzene 189 10 2.5 ug/l
591-78-6 2-Hexanone ND 100 20 ug/l
98-82-8 Isopropylbenzene 12.8 10 2.5 ug/l
99-87-6 p-Isopropyltoluene ND 10 2.5 ug/l
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride ND 10 4.0 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 2.5 ug/l
91-20-3 Naphthalene 30.7 10 2.5 ug/l
103-65-1 n-Propylbenzene 29.1 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 24.4 10 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene 426 10 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 187 10 2.5 ug/l
108-05-4 Vinyl Acetate ND 100 20 ug/l
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 1120 20 2.5 ug/l
95-47-6 o-Xylene 529 10 2.5 ug/l
1330-20-7 Xylene (total)1640 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 67
FA9989233.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FA99892-2 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 67
FA9989233.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA99892-3 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235123.D 1 10/25/22 13:18 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 67
FA9989233.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA99892-3 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 67
FA9989233.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA99892-3 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 67
FA9989233.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:FA99892-4 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235124.D 1 10/25/22 13:41 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.53 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 67
FA9989233.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:FA99892-4 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 67
FA9989233.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-4
Lab Sample ID:FA99892-4 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 67
FA9989233.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-5
Lab Sample ID:FA99892-5 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235125.D 1 10/25/22 14:06 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 2.6 10 2.0 ug/l J
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene 0.19 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 0.17 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 1.7 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.53 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 67
FA9989233.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-5
Lab Sample ID:FA99892-5 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene 0.27 0.50 0.13 ug/l J
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene 0.69 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.22 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.17 0.50 0.13 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 113%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 67
FA9989233.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-5
Lab Sample ID:FA99892-5 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 67
FA9989233.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-6
Lab Sample ID:FA99892-6 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235126.D 1 10/25/22 14:28 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane 1.0 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 16.0 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 67
FA9989233.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-6
Lab Sample ID:FA99892-6 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 67
FA9989233.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-6
Lab Sample ID:FA99892-6 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 67
FA9989233.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-8
Lab Sample ID:FA99892-7 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235127.D 1 10/25/22 14:51 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 2.7 10 2.0 ug/l J
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.78 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 67
FA9989233.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-8
Lab Sample ID:FA99892-7 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 105%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 67
FA9989233.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-8
Lab Sample ID:FA99892-7 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 67
FA9989233.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-9
Lab Sample ID:FA99892-8 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235133.D 1 10/25/22 17:09 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.63 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 67
FA9989233.8
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-9
Lab Sample ID:FA99892-8 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 67
FA9989233.8
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-9
Lab Sample ID:FA99892-8 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 67
FA9989233.8
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-10
Lab Sample ID:FA99892-9 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235128.D 5 10/25/22 15:14 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 179 50 10 ug/l
71-43-2 Benzene 58.3 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
78-93-3 2-Butanone (MEK)ND 13 6.3 ug/l
104-51-8 n-Butylbenzene 2.8 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene 4.3 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene 1.5 2.5 0.63 ug/l J
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane 2.4 2.5 1.0 ug/l J
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 67
FA9989233.9
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-10
Lab Sample ID:FA99892-9 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
108-20-3 Di-Isopropyl Ether ND 2.5 0.63 ug/l
64-17-5 Ethyl Alcohol a ND 500 330 ug/l
100-41-4 Ethylbenzene 174 2.5 0.63 ug/l
591-78-6 2-Hexanone ND 25 5.0 ug/l
98-82-8 Isopropylbenzene 50.5 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 2.4 2.5 0.63 ug/l J
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride 1.7 2.5 1.0 ug/l J
75-09-2 Methylene Chloride 5.4 10 5.0 ug/l J
108-10-1 4-Methyl-2-pentanone (MIBK)ND 13 6.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.63 ug/l
91-20-3 Naphthalene 28.4 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 21.5 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene 2.4 2.5 0.63 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 56.3 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 32.3 2.5 0.63 ug/l
108-05-4 Vinyl Acetate 26.6 25 5.0 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 62.1 5.0 0.63 ug/l
95-47-6 o-Xylene ND 2.5 0.63 ug/l
1330-20-7 Xylene (total)62.1 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 67
FA9989233.9
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-10
Lab Sample ID:FA99892-9 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 67
FA9989233.9
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:DMW-1
Lab Sample ID:FA99892-10 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235134.D 1 10/25/22 17:32 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.88 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 67
FA9989233.10
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:DMW-1
Lab Sample ID:FA99892-10 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 67
FA9989233.10
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:DMW-1
Lab Sample ID:FA99892-10 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 67
FA9989233.10
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:WSW-10
Lab Sample ID:FA99892-11 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235135.D 1 10/25/22 17:55 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 67
FA9989233.11
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:WSW-10
Lab Sample ID:FA99892-11 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 67
FA9989233.11
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:WSW-10
Lab Sample ID:FA99892-11 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 67
FA9989233.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-10
Lab Sample ID:FA99892-11 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:EPA 504.1 SW846 8011 Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CC085881.D 1 10/22/22 03:34 AF 10/21/22 08:45 OP93657 GCC2214
Run #2
Initial Volume Final Volume
Run #1 36.8 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.019 0.0095 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%63-137%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 67
FA9989233.11
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:WSW-16
Lab Sample ID:FA99892-12 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235136.D 1 10/25/22 18:17 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 67
FA9989233.12
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:WSW-16
Lab Sample ID:FA99892-12 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 67
FA9989233.12
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:WSW-16
Lab Sample ID:FA99892-12 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 67
FA9989233.12
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-16
Lab Sample ID:FA99892-12 Date Sampled:10/18/22
Matrix:AQ - Ground Water Date Received:10/20/22
Method:EPA 504.1 SW846 8011 Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CC085882.D 1 10/22/22 03:54 AF 10/21/22 08:45 OP93657 GCC2214
Run #2
Initial Volume Final Volume
Run #1 37.4 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.019 0.0094 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 82%63-137%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 67
FA9989233.12
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:FB
Lab Sample ID:FA99892-13 Date Sampled:10/18/22
Matrix:AQ - Field Blank Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0235121.D 1 10/25/22 12:33 SS n/a n/a VA3267
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 67
FA9989233.13
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:FB
Lab Sample ID:FA99892-13 Date Sampled:10/18/22
Matrix:AQ - Field Blank Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 67
FA9989233.13
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:FB
Lab Sample ID:FA99892-13 Date Sampled:10/18/22
Matrix:AQ - Field Blank Water Date Received:10/20/22
Method:SM 6200B Percent Solids:n/a
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV, ECC and BS outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 67
FA9989233.13
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
50 of 67
FA998924
FA99892: Chain of Custody
Page 1 of 3
51 of 67
FA9989244.1
FA99892: Chain of Custody
Page 2 of 3
52 of 67
FA9989244.1
Job Number:FA99892 Client:TERRACON
Date / Time Received:10/20/2022 9:00:00 AM Delivery Method:FEDEX
Project:HULLS 66
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.4);
Cooler 1: (2.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.6; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SAMUELM Date:Date:10/20/2022 9:00:00 A
FA99892: Chain of Custody
Page 3 of 3
53 of 67
FA9989244.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
54 of 67
FA998925
Method Blank Summary Page 1 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3267-MB A0235120.D 1 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
55 of 67
FA9989255.1.1
Method Blank Summary Page 2 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3267-MB A0235120.D 1 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 103%70-130%
56 of 67
FA9989255.1.1
Method Blank Summary Page 3 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3267-MB A0235120.D 1 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 105%70-130%
57 of 67
FA9989255.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3267-BS A0235118.D 1 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 34.6 69*70-130
71-43-2 Benzene 10 9.9 99 70-130
108-86-1 Bromobenzene 10 9.5 95 70-130
74-97-5 Bromochloromethane 10 9.8 98 70-130
75-27-4 Bromodichloromethane 10 9.9 99 70-130
75-25-2 Bromoform 10 10.1 101 70-130
78-93-3 2-Butanone (MEK)50 36.1 72 70-130
104-51-8 n-Butylbenzene 10 9.1 91 70-130
135-98-8 sec-Butylbenzene 10 9.8 98 70-130
98-06-6 tert-Butylbenzene 10 9.3 93 70-130
56-23-5 Carbon Tetrachloride 10 9.9 99 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 7.3 73 60-140
67-66-3 Chloroform 10 9.6 96 70-130
95-49-8 o-Chlorotoluene 10 9.2 92 70-130
106-43-4 p-Chlorotoluene 10 9.2 92 70-130
124-48-1 Dibromochloromethane 10 9.5 95 70-130
106-93-4 1,2-Dibromoethane 10 9.6 96 70-130
75-71-8 Dichlorodifluoromethane 10 7.7 77 60-140
95-50-1 1,2-Dichlorobenzene 10 10.2 102 70-130
541-73-1 1,3-Dichlorobenzene 10 10.4 104 70-130
106-46-7 1,4-Dichlorobenzene 10 9.7 97 70-130
75-34-3 1,1-Dichloroethane 10 10.2 102 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 10.0 100 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.9 99 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.4 94 70-130
142-28-9 1,3-Dichloropropane 10 8.9 89 70-130
594-20-7 2,2-Dichloropropane 10 10.8 108 70-130
563-58-6 1,1-Dichloropropene 10 9.8 98 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.2 92 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.6 96 70-130
108-20-3 Di-Isopropyl Ether 10 9.2 92 70-130
64-17-5 Ethyl Alcohol 500 347 69*70-130
100-41-4 Ethylbenzene 10 9.8 98 70-130
* = Outside of Control Limits.
58 of 67
FA9989255.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3267-BS A0235118.D 1 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 46.7 93 70-130
98-82-8 Isopropylbenzene 10 9.3 93 70-130
99-87-6 p-Isopropyltoluene 10 9.5 95 70-130
74-83-9 Methyl Bromide 10 7.2 72 60-140
74-87-3 Methyl Chloride 10 9.7 97 60-140
75-09-2 Methylene Chloride 10 7.1 71 70-130
108-10-1 4-Methyl-2-pentanone (MIBK)50 44.6 89 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.0 80 70-130
91-20-3 Naphthalene 10 9.9 99 70-130
103-65-1 n-Propylbenzene 10 9.3 93 70-130
100-42-5 Styrene 10 9.5 95 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.7 97 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.1 101 70-130
127-18-4 Tetrachloroethylene 10 10.1 101 70-130
108-88-3 Toluene 10 9.5 95 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.2 102 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.7 97 70-130
71-55-6 1,1,1-Trichloroethane 10 9.9 99 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10.0 100 70-130
75-69-4 Trichlorofluoromethane 10 8.3 83 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.3 93 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.9 89 70-130
108-05-4 Vinyl Acetate 50 55.9 112 70-130
75-01-4 Vinyl Chloride 10 8.0 80 60-140
m,p-Xylene 20 17.4 87 70-130
95-47-6 o-Xylene 10 8.9 89 70-130
1330-20-7 Xylene (total)30 26.3 88 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 94%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%70-130%
2037-26-5 Toluene-D8 99%70-130%
* = Outside of Control Limits.
59 of 67
FA9989255.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3267-BS A0235118.D 1 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
60 of 67
FA9989255.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA99898-2MS A0235130.D 200 10/25/22 SS n/a n/a VA3267
FA99898-2MSD A0235131.D 200 10/25/22 SS n/a n/a VA3267
FA99898-2 A0235143.D 200 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
FA99898-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 10000 11300 113 10000 8950 90 23*70-130/20
71-43-2 Benzene 61.9 J 2000 2070 100 2000 2160 105 4 70-130/20
108-86-1 Bromobenzene ND 2000 1850 93 2000 1970 99 6 70-130/20
74-97-5 Bromochloromethane ND 2000 1930 97 2000 2010 101 4 70-130/20
75-27-4 Bromodichloromethane ND 2000 2010 101 2000 2090 105 4 70-130/20
75-25-2 Bromoform ND 2000 1990 100 2000 2120 106 6 70-130/20
78-93-3 2-Butanone (MEK)ND 10000 8960 90 10000 8160 82 9 70-130/20
104-51-8 n-Butylbenzene 33.4 J 2000 1960 96 2000 2060 101 5 70-130/20
135-98-8 sec-Butylbenzene ND 2000 2020 101 2000 2120 106 5 70-130/20
98-06-6 tert-Butylbenzene ND 2000 1890 95 2000 2030 102 7 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 1990 100 2000 2080 104 4 70-130/20
108-90-7 Chlorobenzene ND 2000 1950 98 2000 2030 102 4 70-130/20
75-00-3 Chloroethane ND 2000 1560 78 2000 1740 87 11 60-140/20
67-66-3 Chloroform ND 2000 1950 98 2000 2030 102 4 70-130/20
95-49-8 o-Chlorotoluene ND 2000 2020 101 2000 2100 105 4 70-130/20
106-43-4 p-Chlorotoluene ND 2000 1790 90 2000 1930 97 8 70-130/20
124-48-1 Dibromochloromethane ND 2000 1850 93 2000 1970 99 6 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 1880 94 2000 2020 101 7 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 1560 78 2000 1880 94 19 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 2000 100 2000 2110 106 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 2020 101 2000 2160 108 7 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 1900 95 2000 2000 100 5 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2050 103 2000 2180 109 6 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 1860 93 2000 1940 97 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2030 102 2000 2140 107 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 1980 99 2000 2100 105 6 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2030 102 2000 2120 106 4 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 1890 95 2000 2010 101 6 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 1770 89 2000 1880 94 6 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 2120 106 2000 2270 114 7 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 1970 99 2000 2090 105 6 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 1860 93 2000 1970 99 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1860 93 2000 2000 100 7 70-130/20
108-20-3 Di-Isopropyl Ether ND 2000 1820 91 2000 1970 99 8 70-130/20
64-17-5 Ethyl Alcohol ND 100000 139000 139*100000 86000 86 47*70-130/20
100-41-4 Ethylbenzene 1660 2000 3620 98 2000 3660 100 1 70-130/20
* = Outside of Control Limits.
61 of 67
FA9989255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA99898-2MS A0235130.D 200 10/25/22 SS n/a n/a VA3267
FA99898-2MSD A0235131.D 200 10/25/22 SS n/a n/a VA3267
FA99898-2 A0235143.D 200 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
FA99898-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 10000 9040 90 10000 9500 95 5 70-130/20
98-82-8 Isopropylbenzene 78.7 J 2000 2010 97 2000 2120 102 5 70-130/20
99-87-6 p-Isopropyltoluene 33.6 J 2000 1930 95 2000 2060 101 7 70-130/20
74-83-9 Methyl Bromide ND 2000 1060 53*2000 1720 86 47*60-140/20
74-87-3 Methyl Chloride ND 2000 1970 99 2000 2280 114 15 60-140/20
75-09-2 Methylene Chloride 253 J 2000 1460 60*2000 1520 63*4 70-130/20
108-10-1 4-Methyl-2-pentanone (MIBK)ND 10000 8830 88 10000 9150 92 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 2000 1560 78 2000 1700 85 9 70-130/20
91-20-3 Naphthalene 541 2000 2790 112 2000 3150 130 12 70-130/20
103-65-1 n-Propylbenzene 254 2000 2210 98 2000 2320 103 5 70-130/20
100-42-5 Styrene ND 2000 1920 96 2000 2040 102 6 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 1940 97 2000 2030 102 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 2000 100 2000 2090 105 4 70-130/20
127-18-4 Tetrachloroethylene ND 2000 2020 101 2000 2150 108 6 70-130/20
108-88-3 Toluene 4360 2000 5600 62* a 2000 5560 60* a 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 2050 103 2000 2240 112 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 2060 103 2000 2240 112 8 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 1990 100 2000 2110 106 6 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 2000 100 2000 2070 104 3 70-130/20
79-01-6 Trichloroethylene ND 2000 2020 101 2000 2130 107 5 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 1700 85 2000 1990 100 16 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 1760 88 2000 1830 92 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 3940 2000 5760 91 2000 5720 89 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 968 2000 2880 96 2000 2930 98 2 70-130/20
108-05-4 Vinyl Acetate ND 10000 11500 115 10000 12200 122 6 70-130/20
75-01-4 Vinyl Chloride ND 2000 1610 81 2000 1950 98 19 60-140/20
m,p-Xylene 8470 4000 10500 51* a 4000 10400 48* a 1 70-130/20
95-47-6 o-Xylene 5250 2000 6310 53* a 2000 6240 50* a 1 70-130/20
1330-20-7 Xylene (total)13700 6000 16800 52* a 6000 16700 50* a 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA99898-2 Limits
1868-53-7 Dibromofluoromethane 93%93%109%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%97%119%70-130%
2037-26-5 Toluene-D8 98%98%100%70-130%
* = Outside of Control Limits.
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FA9989255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA99898-2MS A0235130.D 200 10/25/22 SS n/a n/a VA3267
FA99898-2MSD A0235131.D 200 10/25/22 SS n/a n/a VA3267
FA99898-2 A0235143.D 200 10/25/22 SS n/a n/a VA3267
The QC reported here applies to the following samples:Method: SM 6200B
FA99892-1, FA99892-2, FA99892-3, FA99892-4, FA99892-5, FA99892-6, FA99892-7, FA99892-8, FA99892-9,
FA99892-10, FA99892-11, FA99892-12, FA99892-13
CAS No.Surrogate Recoveries MS MSD FA99898-2 Limits
460-00-4 4-Bromofluorobenzene 100%102%95%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
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FA9989255.3.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
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FA998926
Method Blank Summary Page 1 of 1
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP93657-MB CC085857.D 1 10/21/22 AF 10/21/22 OP93657 GCC2214
The QC reported here applies to the following samples:Method: EPA 504.1
FA99892-11, FA99892-12
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.020 0.010 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 87%63-137%
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FA9989266.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP93657-BS CC085858.D 1 10/21/22 AF 10/21/22 OP93657 GCC2214
OP93657-BSD CC085859.D 1 10/21/22 AF 10/21/22 OP93657 GCC2214
The QC reported here applies to the following samples:Method: EPA 504.1
FA99892-11, FA99892-12
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
106-93-4 1,2-Dibromoethane 0.25 0.22 88 0.22 88 0 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 88%86%63-137%
* = Outside of Control Limits.
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FA9989266.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA99892
Account:TERCNCC Terracon Consulting
Project:Hulls 66; 6711 NC Hwy 27W, Vale, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP93657-MS CC085860.D 1 10/21/22 AF 10/21/22 OP93657 GCC2214
OP93657-MSD CC085861.D 1 10/21/22 AF 10/21/22 OP93657 GCC2214
FA99880-34 a CC085880.D 1 10/22/22 AF 10/21/22 OP93657 GCC2214
The QC reported here applies to the following samples:Method: EPA 504.1
FA99892-11, FA99892-12
FA99880-34 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
106-93-4 1,2-Dibromoethane 0.20 0.242 0.35 62*0.242 0.35 62*0 70-130/25
CAS No.Surrogate Recoveries MS MSD FA99880-34 Limits
460-00-4 4-Bromofluorobenzene 84%86%94%63-137%
(a) All hits confirmed by dual column analysis.
* = Outside of Control Limits.
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FA9989266.3.1