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HomeMy WebLinkAboutWS-6409_24177_CA_MRP_20230802 2725 E. Millbrook Road, Suite 121 Raleigh, NC 27604 Telephone 919-871-0999 www.atcgroupservices.com August 2, 2023 Ms. Linda Blalock North Carolina Department of Environmental Quality Division of Waste Management – Underground Storage Tank Section 1646 Mail Service Center Raleigh, North Carolina 27699-1646 Subject: Groundwater Monitoring Report Farrar’s Store 397 Farrar Store Road Stokesdale, Rockingham County, North Carolina NCDEQ Incident No. 24177 Dear Ms. Blalock: ATC Associates of North Carolina, P.C. (ATC) is submitting the enclosed Groundwater Monitoring Report for the Farrar’s Store site. The report presents investigative procedures, field activities, and laboratory analytical results for a groundwater sampling event conducted in June 2023. If you have any questions or require additional information, please contact our office at (919) 871-0999. Sincerely, ATC Associates of North Carolina, P.C. Nicholas Kramer Ashley M. W. Offer, P.G. Project Scientist Senior Project Manager Direct Line: 919-573-1198 Direct Line: 919-573-1206 Email: nicholas.kramer@oneatlas.com Email: ashley.offer@oneatlas.com Attachments: 1. Groundwater Monitoring Report Prepared for: North Carolina Department of Environmental Quality Division of Waste Management – Underground Storage Tank Section 1646 Mail Service Center Raleigh, North Carolina 27699-1646 GROUNDWATER MONITORING REPORT Farrar’s Store 397 Farrar Store Road Stokesdale, Rockingham County, North Carolina Incident #24177 ATC Project No. STL2417701 Prepared by: ATC Associates of North Carolina, P.C. 2725 E. Millbrook Road, Suite 121 Raleigh, North Carolina 27604 Telephone 919-871-0999 Nicholas Kramer Project Scientist Direct Line: 919-573-1198 Email: nicholas.kramer@oneatlas.com Ashley M. W. Offer, P.G. Senior Project Manager Direct Line: 919-573-1206 Email: ashley.offer@oneatlas.com August 2, 2023 Farrar’s Store August 2, 2023 Page i ATC Project No. STL2417701 NCDEQ State Lead Program Table of Contents 1.0 SITE IDENTIFICATION .......................................................................................................................... 1 2.0 EXECUTIVE SUMMARY ........................................................................................................................ 2 3.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................... 2 3.1 SITE CHARACTERIZATION .................................................................................................................................... 2 3.2 SITE HISTORY ................................................................................................................................................... 3 4.0 GROUNDWATER ASSESSMENT ACTIVITIES .................................................................................. 5 4.1 GROUNDWATER LEVELS ............................................................................................................................................. 5 4.2 GROUNDWATER ANALYTICAL RESULTS .................................................................................................................. 5 4.3 WATER SUPPLY WELL SAMPLING ......................................................................................................................... 6 5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................................... 6 TABLES: Table 1 – Water Supply Well Information Table 2 – Well Construction and Groundwater Elevation Data Table 3 – Field Parameters Table 4 – Groundwater Analytical Data Table 5 – Historical Groundwater Analytical Data Table 6 – Historical Water Supply Well Analytical Data FIGURES: Figure 1 – Topographic Map Figure 2 – Site Map Figure 3 – Potential Receptor Map Figure 4 – Groundwater Elevation Contour Map Figure 5 – Dissolved Benzene Isoconcentration Map Figure 6 – Dissolved 1,2-Dibromoethane Isoconcentration Map Figure 7 – Additional Chemicals of Concern in Groundwater APPENDICES: Appendix A – Conceptual Site Model Appendix B – Site Photographs Appendix C – Field Notes Appendix D – GSI Mann-Kendall Toolkit Appendix E – Laboratory Analytical Results Farrar’s Store August 2, 2023 Page 2 of 6 ATC Project No. STL2417701 NCDEQ State Lead Program 2.0 EXECUTIVE SUMMARY ATC Associates of North Carolina, P.C. (ATC) has completed a Groundwater Monitoring Report for the Farrar’s Store site. This report documents groundwater assessment activities conducted at the site in June 2023. The activities were performed based on the May 12, 2023, Task Authorization (TA-01) by the Trust Fund Branch of the Underground Storage Tank (UST) Section, Division of Waste Management (DWM), North Carolina Department of Environmental Quality (NCDEQ). The work is being performed as part of State Lead Contract #N70522-B between NCDEQ and ATC. The Farrar’s Store site is located at 397 Farrar Store Road in Stokesdale, Rockingham County, North Carolina. The site is currently developed with one single-story building that is currently vacant. Five monitoring wells (MW-1, MW-2, MW-3, MW-4, and MW-1D) are associated with the site. The UST system formerly located on the property consisted of two 575-gallon gasoline USTs (UST-1 and UST-2) and one 300-gallon gasoline UST (UST-3). The two 575-gallon gasoline USTs were installed in 1926 and removed on September 22, 2004 and the one 300-gallon gasoline UST was installed in 1926 and removed on April 7, 2015. There are twenty-one water supply wells within 1,000 feet of the site. Twenty water supply wells are active, and one well is inactive. Sixteen of the active water supply wells (WSW-2(new), WSW-3, WSW- 5, WSW-6, WSW-8 through WSW-18, and WSW-21) do not have an active municipal account and are assumed potable wells. On June 12, 2023, ATC mobilized to the site to collect groundwater samples from MW-1, MW-2, MW-3, MW-4, and MW-1D. Based on the data, groundwater flows to the east across the site. Light non-aqueous phase liquid (LNAPL) was not detected. 1,2-Dibromoethane was detected above the Gross Contaminant Level (GCL) in MW-3. Multiple petroleum constituents were detected above the 15A NCAC 02L. 0202 Groundwater Quality Standards (2L Standards) in monitoring wells MW-1, MW-2, MW-3, and MW-4. ATC also collected samples from WSW-2 and WSW-3 which are located within 500 feet of the site and are considered to be crossgradient of the site. WSW-2 and WSW-3 exhibited concentrations of 1,2- dichloroethane below the applicable 2L Standard. Tetrachloroethylene was also detected in WSW-3 at a concentration exceeding the 2L Standard which is comparable to historical data. Based on the groundwater analytical results, the extent of the petroleum groundwater impact is horizontally delineated to the south. Additionally, although well MW-1D did not indicate concentrations above 2L Standards, the well is located upgradient of the most impacted well on the property, MW-3. Therefore, the vertical plume is not adequately delineated. Additional groundwater monitoring is required to determine if the vertical extent of the groundwater impacts have been adequately delineated. ATC recommends conducting a comprehensive groundwater sampling event including the sampling of select potable wells within 500 feet of the site in December 2023 to confirm groundwater concentrations, particularly for MW-3 and MW-4. Following the December 2023 sampling event, ATC recommends installing additional monitoring wells in order to adequately delineate the groundwater contaminant plume. 3.0 SITE HISTORY AND CHARACTERIZATION 3.1 SITE CHARACTERIZATION The Farrar’s Store site is located at 397 Farrar Store Road in Stokesdale, North Carolina. The site is currently developed with a single-story building, which is vacant and utilized for storage. Five monitoring wells (MW-1 through MW-4 and MW-1D) are associated with the site. The UST system formerly located on the property consisted of two 575-gallon gasoline USTs and one 300-gallon gasoline UST. The two 575- gallon gasoline USTs were installed in 1926 and removed on September 22, 2004, and the one 300-gallon gasoline UST was installed in 1926 and removed on April 7, 2015. The site is bound to the north by NC Highway 65, to the southwest and southeast by Farrar Store Road. Municipal water is available to the site and vicinity. There are twenty-one water supply wells within 1,000 feet of the site. Twenty water supply wells are active, and one well is inactive. Sixteen of the active water supply wells (WSW-2(new), WSW-3, WSW-5, WSW-6, WSW-8 through WSW-18, and WSW-21) do not have an active municipal account and are assumed potable wells. Water supply well ownership information Farrar’s Store August 2, 2023 Page 3 of 6 ATC Project No. STL2417701 NCDEQ State Lead Program is included in Table 1. A site topographic map is included as Figure 1 and a site map depicting monitoring well locations and other pertinent site features is included as Figure 2. A map showing water supply well locations is included as Figure 3. A conceptual site model is included as Appendix A. Site photographs are included as Appendix B. 3.2 SITE HISTORY On April 3, 2002, the DWM UST section received a Health Risk Evaluation report and lab result of a water supply well sample, SW-1(old), collected by the Rockingham County Health Department. On the same day, bottled water service was requested for the Farrar’s residence. On November 18, 2002 the DWM UST section sent a Notice of Regulatory Requirements to responsible party. In May 2003, a carbon filter was installed at the Farrar residence on water supply well WSW-1(old). The UST Closure Report submitted by Pyramid Environmental & Engineering, P.C. (Pyramid) on October 29, 2004, documented the removal of two 575-gallon gasoline USTs (UST-1 and UST-2) in September 2004. Observations made during the UST removal suggested that there had been a release from the UST system. Based on these observations, 71.66 tons of petroleum contaminated soil was excavated and taken off-site for disposal. Results of the soil sampling, around UST-2, indicated exceedances to the Maximum Soil Contamination Concentrations (MSCCs) for multiple volatile organic compounds (VOCs), volatile petroleum hydrocarbons (VPHs), and extractable petroleum hydrocarbons (EPHs). On November 17, 2006, Pyramid performed a Limited Site Assessment (LSA) at the site property. A direct- push soil boring was installed in the suspected area of an underground anomaly identified with a metal detector during the UST closure activities in 2004. Approximately six inches below ground surface (bgs) a metal tank was discovered. Pyramid estimated that UST-3 has a capacity of 300-gallons. Pyramid also installed one Type II monitoring well (MW-1) in the source area. A soil sample was collected from the MW- 1 boring at 18-20 feet bgs. Results of the soil sampling indicated exceedances to the MSCCs for multiple VOCs and VPHs. On February 21 through 23, 2011, Pyramid supervised a geophysical survey utilizing electromagnetic resistivity and ground-penetrating radar to determine the exact location of UST-3. Pyramid also conducted an updated receptor survey, supervised the installation of 10 soil borings (B1 through B10), sampled monitoring well MW-1, and sampled water supply wells WSW-1(new), WSW-1(old), WSW-2(new), WSW- 2(old), WSW-3, WSW-5, WSW-6, and WSW-7. Results of the groundwater analytical data indicated exceedances to the 2L standards in MW-1 for benzene and 1,2-dibromoethane. The concentration of 1,2- dibromoethane also exceeded its representative GCL. Results of the soil sampling indicated contamination that exceeds the Residential MSCCs below the former 575-gallon USTs that extends to the groundwater table. Results of the water supply well sampling indicated exceedances to the 2L Standards in WSW-1(new) for benzene, 1,2-dichloroethane, 1,2-dichloropropane, and naphthalene. Water supply wells WSW-1(new) and WSW-3 also exceeded the 2L Standards for tetrachloroethylene. On October 28, 2011, Pyramid collected samples from the groundwater monitoring well MW-1 and water supply wells WSW-1(new), WSW-1(old), WSW-2(new), WSW-2(old), WSW-3, WSW-5, WSW-6, and WSW-7. Results of the groundwater analytical data indicated exceedances to the 2L Standards in MW-1 for benzene, toluene, total xylenes, 1,2-dibromethane, and1,2-dichloroethane. Results of the water supply well sampling indicated exceedances to the 2L Standards in WSW-1 (new) for benzene, 1,2-dichloroethane, 1,2-dichloropropane, and naphthalene. Water supply well WSW-3 also exceeded the 2L Standards for tetrachloroethylene. On April 7, 2015, ECS Carolinas, LLP (ECS) mobilized to the site and removed a 500-gallon UST (UST-3). ECS oversaw the removal contaminated soil underneath UST-3 and in the former UST-2 area. Soil was then backfilled on August 4, 2015 with 70.64 tons of clean imported soil. A report documenting closure Farrar’s Store August 2, 2023 Page 4 of 6 ATC Project No. STL2417701 NCDEQ State Lead Program activities was not available for ATC’s review; therefore, ATC cannot determine the exact amount of soil removed during the April 2015 activities. The dates for the UST removal and clean soil tonnage were derived from invoices from 2015. On May 2, 2018, ECS collected a groundwater sample from monitoring well MW-1 and from water supply wells WSW-1 (old), WSW-1 (new), and WSW-3. Results of the groundwater analytical data indicated exceedances to the 2L Standards for benzene, total xylenes, naphthalene, and 1,2-dibromoethane for MW- 1. Results of the water supply well samples indicated an exceedance to the 2L Standards in WSW-3 for tetrachloroethylene. On January 2, 2019, ECS installed Enviro-Bac in monitoring well MW-1. On January 31, 2019 and March 11, 2019, ECS mobilized to the site to collect a groundwater sample from MW-1. ECS also collected samples from water supply wells WSW-1 (old), WSW-1 (new), and WSW-3 on March 11, 2019. Monitoring well MW-1 indicated exceedances to the 2L Standards for 1,2-dibromoethane during both sampling events. Additional constituents were detected above the laboratory reporting limit, but below their representative 2L Standards. Results of the water supply well samples indicated an exceedance to the 2L Standards in WSW-3 for tetrachloroethylene. On November 14, 2019, ECS collected a groundwater sample from monitoring well MW-1. Results of the groundwater analytical data indicated exceedances of the 2L Standards for benzene, total xylenes, methyl butyl ketone, naphthalene, and 1,2-dibromoethane. On January 2, 2020, ECS collected a groundwater sample from monitoring well MW-1. Results of the groundwater analytical data indicated exceedances of the 2L Standards for benzene, total xylenes, methyl butyl ketone, naphthalene, 1,2-dibromoethane, and 1,1,2-trichloroethane. On March 29 and 31, 2021, SAEDACCO, Inc. mobilized to the site to abandon water supply wells WSW-1 (old) and WSW-1 (new), located approximately 240 feet from the site property. The property associated with both wells was connected to municipal water prior to the abandonment. On June 24, 2021, ATC conducted a groundwater sampling event on monitoring well MW-1. The laboratory analytical results indicated benzene, total xylenes, naphthalene, 1,2-dibromoethane, 1,2-dichloroethane, and 1,2,4-trimethylbenzene exceeded their respective 2L Standards. On November 12, 2021, ATC performed visual reconnaissance for an updated receptor survey. Based on ATC’s findings, there are twenty-one water supply wells located within 1,000 feet of the site. Sixteen of those wells appear to be used for drinking purposes, four are used for irrigation, and one is inactive. Public water is available within 1,000 feet of the site. On January 3, 2023, ATC submitted a Groundwater Monitoring Report documenting the installation of three Type II monitoring wells (MW-2, MW-3, and MW-4) and one Type III monitoring well (MW-1D) to delineate the groundwater impacts. On October 19, 2022, ATC mobilized to the site to collect groundwater samples from MW-1 through MW-4 and MW-1D. Based on the data, groundwater flows to the southeast across the site. LNAPL was not detected. 1,2-Dibromoethane was detected above the GCLs in MW-4. Multiple constituents were detected above 2L Standards in monitoring wells MW-1, MW-1D, MW-2, MW-3, and MW- 4. Based on the groundwater analytical results, it was determined that the extent of the petroleum groundwater impact was delineated to the southwest and the vertical extent of the groundwater impacts were not delineated. Farrar’s Store August 2, 2023 Page 5 of 6 ATC Project No. STL2417701 NCDEQ State Lead Program 4.0 GROUNDWATER ASSESSMENT ACTIVITIES 4.1 GROUNDWATER LEVELS On June 12, 2023, ATC mobilized to the site to collect groundwater samples from all existing monitoring wells (MW-1, MW-2, MW-3, MW-4, and MW-1D) and water supply wells WSW-2 and WSW-3. LNAPL was not detected during the event. Depth to water in the wells ranged from 36.11 feet bgs in MW-2 to 58.25 feet bgs in MW-1D. Based on the June 2023 groundwater gauging event, groundwater flows to the east across the site. Monitoring well construction details and groundwater elevation data are summarized in Table 2. Field parameter data, including temperature, dissolved oxygen, conductivity, pH, and oxygen reduction potential, were recorded during the sampling event and are included in Table 3. A groundwater elevation contour map is included as Figure 4. Photographs of the monitoring well locations are included in Appendix B. Field notes from the sampling event are included in Appendix C. 4.2 GROUNDWATER ANALYTICAL RESULTS The groundwater samples were placed in laboratory-supplied containers, entered into chain-of-custody control, placed on ice, and shipped to Pace Analytical in Mount Juliet, Tennessee for analysis by Standard Method 6200B. Field notes from the sampling event are included in Appendix C. The laboratory analytical results exhibited numerous compounds above 2L Standards:  Benzene: MW-1, MW-3  Total Xylenes: MW-1, MW-3  Naphthalene: MW-1, MW-3  Bromodichloromethane: MW-3  1,2-Dibromoethane: MW-1, MW-3, MW-4  1,2-Dichloroethane: MW-1  Tetrachloroethylene: MW-2  1,2,4-Trimethylbenzene: MW-3 1,2-Dibromoethane was detected at a concentration exceeding the applicable GCL. No additional compounds were detected above the respective GCLs. A summary of the laboratory analytical results from the June 2023 event are included in Table 4. Historical groundwater analytical results are included in Table 5. An isoconcentration contour map for dissolved benzene and 1,2-dibromoethane are included as Figure 5 and Figure 6, respectively. A map depicting additional chemicals of concern in groundwater is included as Figure 7. ATC reviewed groundwater concentrations trends for key compounds in wells MW-1 using a GSI Mann- Kendall Toolkit. Based on the results, naphthalene and 1,2,4-trimethylbenzene concentrations indicate an increasing trend. No statistical trends were identified for benzene, total xylenes, 1,2-dibromoethane, and 1,2-dichloroethane. The GSI Mann-Kendall Toolkit for MW-1 is included as Appendix D. It should be noted that based on the recent groundwater analytical data, it appears samples MW-3 and MW-4 were inadvertently switched during the October 2022 sampling event. Due to the downgradient location of MW-3 compared to the upgradient location of MW-4, and both well locations in respect to the former UST system location, ATC believes it is more probable for well MW-3 to be more highly impacted. As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of the laboratory report was conducted. During the review, it was concluded that samples were received by the laboratory in acceptable condition and properly preserved. The samples were analyzed within the correct holding times. A field blank sample was also analyzed for the site, which indicated detections of 2-butanone and methylene chloride at estimated concentrations. Methylene chloride is a common laboratory contaminant and is likely associated with the laboratory. 2-Butanone is commonly associated with petroleum sites and is potentially the result of cross-contamination during field sampling activities. However, the concentration was flagged with a “J” qualifier denoting that the concentration value is an estimate. The Farrar’s Store August 2, 2023 Page 6 of 6 ATC Project No. STL2417701 NCDEQ State Lead Program chain of custody was properly completed by all parties. The laboratory QC report shows an internal blank was analyzed for each method that was used for the original samples. The laboratory fortified blank and laboratory control sample data results were also provided for each analytical method. Refer to the laboratory report in Appendix E for details regarding QA results for the laboratory samples and any noted exceptions. Overall, ATC concludes that the laboratory results are usable and any exceptions do not significantly impact the conclusions presented in this report. 4.3 WATER SUPPLY WELL SAMPLING On June 12, 2023, ATC collected samples from WSW-2 and WSW-3 which are located within 500 feet of the site and are considered to be crossgradient of the site. Water supply well information is included in Table 1. Water supply well locations are shown on Figure 3. The samples were collected in laboratory- supplied containers and shipped to Pace Analytical in Mount Juliet, Tennessee for analysis of volatile organic compounds by Method 6200B. The water supply well analytical results were compared to the 2L Standards and GCLs. WSW-2 and WSW- 3 exhibited concentrations of 1,2-dichloroethane below the applicable 2L Standard. Tetrachloroethylene was also detected in WSW-3 at a concentration exceeding the 2L Standard which is comparable to historical data. No additional compounds were detected which exceeded the applicable laboratory detection limits. Water supply analytical results are included as Table 6. Field notes from the sampling event are included as Appendix B. 5.0 CONCLUSIONS AND RECOMMENDATIONS On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Groundwater Monitoring Report documenting the June 2023 groundwater sampling activities at the Farrar’s Store site located at 397 Farrar Store Road in Stokesdale, Rockingham County, North Carolina. On June 12, 2023, ATC mobilized to the site to collect groundwater samples from MW-1, MW-2, MW-3, MW-4, and MW-1D. Based on the data, groundwater flows to the east across the site. LNAPL was not detected. 1,2-Dibromoethane was detected above the GCL in MW-3. Multiple petroleum constituents were detected above 2L Standards in monitoring wells MW-1, MW-2, MW-3, and MW-4. Based on the groundwater analytical results, the extent of the petroleum groundwater impact is horizontally delineated to the south. Although well MW-1D did not indicate concentrations above 2L Standards, the well is located upgradient of the most impacted well on the property, MW-3. Therefore, the vertical plume is not adequately delineated. Additional groundwater monitoring is required to determine if the vertical extent of the groundwater impacts have adequately delineated. ATC recommends conducting a comprehensive groundwater sampling event including the sampling of select potable wells within 500 feet of the site in December 2023 to confirm groundwater concentrations, particularly for MW-3 and MW-4. Following the December 2023 sampling event, ATC recommends the installation of additional monitoring wells in order to adequately horizontally delineate the groundwater contaminant plume. Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program TABLES TABLE 1 WATER SUPPLY WELL INFORMATION FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 Water Supply Well Property Owner(s)Property Address Owner's Address Distance from Source (feet)Usage Additional Information WSW-1 (old)240 E Abandoned -- WSW-1 (new)200 SE Abandoned -- WSW-2 (old)200 SW Inactive -- WSW-2 (new)280 SW Potable Depth: 365 ft Year Installed: 1985 WSW-3 Susan Hyatt Barham (336) 420-0482 358 Farrar Store Road Stokesdale, NC 27357 358 Farrar Store Road Stokesdale, NC 27357 445 SW Potable Depth: 383 ft Year Installed: 2000 WSW-4 Glennie Goins 9120 NC Highway 65 Stokesdale, NC 27357 1285 Webb Loop Madison, NC 27025 300 E Irrigation -- WSW-5 Robert Yates, Sr.9157 NC Highway 65 Stokesdale, NC 27357 8885 Belews Creek Rd Belews Creek, NC 27009 180 N Potable -- WSW-6 Ross McSurdy 131 Classic Lane Stokesdale, NC 27357 131 Classic Lane Stokesdale, NC 27357 415 N Potable -- WSW-7 Tommy & Vanessa Barham 9123 NC Highway 65 Stokesdale, NC 27357 9123 NC Highway 65 Stokesdale, NC 27357 300 NE Irrigation -- WSW-8 Terry & Kathelene Shelton 110 Classic Lane Stokesdale, NC 27357 736 Lemons Road Stokesdale, NC 27357 390 NW Potable -- WSW-9 Rosemarie Berger 120 Classic Lane Stokesdale, NC 27357 701 Fairidge Drive Jamestown, NC 27282 440 NW Potable -- WSW-10 Albert & Barbara Hicks 140 Classic Lane Stokesdale, NC 27357 140 Classic Lane Stokesdale, NC 27357 560 NW Potable -- WSW-11 John & Mary Johnson 160 Classic Lane Stokesdale, NC 27357 160 Classic Lane Stokesdale, NC 27357 750 NW Potable -- WSW-12 Charles & Rhonda Ray (336) 580-3195 178 Classic Lane Stokesdale, NC 27357 178 Classic Lane Stokesdale, NC 27357 880 NW Potable Depth: Unknown Year Installed: 1991 Andrew & Julie Oakley 9136 NC Highway 65 Stokesdale, NC 27357 250 Harrison Crossroad Loop Reidsville, NC 27320 Bobbie R. Barham (336) 548-2986 378 Farrar Store Road Stokesdale, NC 27357 358 Farrar Store Road Stokesdale, NC 27357 Page 1 of 2 TABLE 1 WATER SUPPLY WELL INFORMATION FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 Water Supply Well Property Owner(s)Property Address Owner's Address Distance from Source (feet)Usage Additional Information WSW-13 Richard & Corinne Cunningham 175 Classic Lane Stokesdale, NC 27357 175 Classic Lane Stokesdale, NC 27357 900 N Potable -- WSW-14 William & Deborah Burgess 160 Red Oak Dr. Stokesdale, NC 27357 160 Red Oak Dr. Stokesdale, NC 27357 750 NW Potable -- WSW-15 Robert & Joanne Burgess 140 Red Oak Dr. Stokesdale, NC 27357 140 Red Oak Dr. Stokesdale, NC 27357 700 NW Potable -- WSW-16 James & Rebecca Wilson 9065 NC Highway 65 Stokesdale, NC 27357 9065 NC Highway 65 Stokesdale, NC 27357 815 E Potable -- WSW-17 G W Moore, Jr 9104 NC Highway 65 Stokesdale, NC 27357 9104 NC Highway 65 Stokesdale, NC 27357 600 E Potable -- WSW-18 Sample & Edna Anderson 345 Farrar Store Rd Stokesdale, NC 27357 345 Farrar Store Rd Stokesdale, NC 27357 530 S Potable -- WSW-19 Lea & Garrett Phillips 348 Farrar Store Rd Stokedale, NC 27357 348 Farrar Store Rd Stokesdale, NC 27357 600 S Irrigation -- WSW-20 Robert Yates, Sr.9220 NC Highway 65 Stokesdale, NC 27357 8885 Belews Creek Rd Belews Creek, NC 27009 890 SW Irrigation -- WSW-21 Lori and Bradford Vernon 9077 NC Highway 65 Stokesdale, NC 27357 9077 NC Highway 65 Stokesdale, NC 27357 650 E Potable -- Notes: 1. Property owner information obtained from Rockingham County GIS website (https://www.webgis.net/nc/Rockingham/). 2. Water supply well and municipal water information obtained Rockingham County Water Deparment, Town of Stokesdale Water Department, Aqua, and visual reconnaissance. Page 2 of 2 TABLE 2 WELL CONSTRUCTION AND GROUNDWATER ELEVATION DATA FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 Well ID Date Installed Well Diameter (inches) Total Depth (feet) Screen Interval (feet) TOC Elevation (Feet) Date Measured Depth to Groundwater (feet) Depth to LNAPL (feet) LNAPL Thickness (feet) Groundwater Elevation (feet) 11/14/2019 35.93 ----64.07 1/2/2020 36.31 ----63.69 6/24/2021 34.07 ----65.93 10/19/2022 37.21 ----62.79 6/12/2023 36.68 ----63.32 10/19/2022 36.82 ----62.53 6/12/2023 36.11 ----63.24 10/19/2022 37.25 ----62.55 6/12/2023 36.73 ----63.07 10/19/2022 37.16 ----62.85 6/12/2023 36.41 ----63.60 10/19/2022 79.55 ----20.28 6/12/2023 58.25 ----41.58 Notes: 1. TOC = Top of casing. 2. -- = LNAPL not detected. 3. Formula for determining groundwater elevation when LNAPL has been detected: TOC Elevation - Depth to Groundwater + [0.8581*LNAPL Thickness]. 4. Well construction information was obtained from previous consultants reports. 5. Top-of-casing elevation has not been surveyed. 6. LNAPL = Light non-aqueous phase liquid. 100.01 MW-1D 10/14/2022 2 80 70-80 99.83 MW-4 10/14/2022 2 45 30-45 99.35 MW-3 10/14/2022 2 45 30-45 99.80 MW-2 10/14/2022 2 44 29-44 100.00MW-1 11/17/2006 2 55 25-55 Page 1 of 1 TABLE 3 FIELD PARAMETERS FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 11/14/2019 17 5.12 NM 148 5.40 NM 1/20/2020 NM NM NM NM NM NM 6/24/2021 20.73 0.74 307 283 6.39 92.9 10/19/2022 15.7 2.62 941 773 5.99 172.8 6/12/2023 22.78 2.16 393 377 5.22 63.7 10/19/2022 16.3 4.74 276.3 230.3 5.99 181.2 6/12/2023 22.44 2.04 293 279 5.50 46.4 10/19/2022 15.8 2.00 102.9 84.7 5.77 167.9 6/12/2023 22.01 1.75 304 287 5.91 30.3 10/19/2022 15.1 4.65 281.6 227.8 6.14 164.0 6/12/2023 22.52 2.31 128 122 5.23 48.7 10/19/2022 6/12/2023 22.19 1.41 1,855 1,756 11.51 -136.9 Notes: 1. mg/L = Milligrams per Liter. 2. °C = Degrees Celcius. 3. µS/cm = MicroSiemens per Centimeter. 4. mV = Millivolts. 5. SU = Standard Units. 6. NM = Not measured. Conductivity (µS/cm) Oxygen Reduction Potential (mV) pH (SU)WELL I.D.DATE SAMPLED Temperature (°C) Dissolved Oxygen (µg/L) Specific Conductivity (µS/cm) MW-1 MW-2 MW-3 MW-4 MW-1D Not enough water for YSI reading. TABLE 4 GROUNDWATER ANALYTICAL DATA FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 Benzene Toluene Ethylbenzene Total Xylenes Naphthalene Acetone Bromodichloromethane sec-Butylbenzene Chloroethane Chloroform 1,2-Dibromoethane 1,2-Dichloroethane Isopropylbenzene p-Isopropyltoluene 2-Butanone (MEK) Methyl isobutyl ketone n-Propylbenzene Tetrachloroethylene 1,2,4-Trimethylbenzene 1,3,5-TrimethylbenzeneMW-1 06/12/2023 1.01 J 135 109 622 10.7 14.3 J <1.00 1.16 <5.00 <5.00 3.88 0.479 J 5.36 <1.00 <10.0 4.64 J 22.3 0.548 J 138 53.3 MW-2 06/12/2023 0.255 J <1.00 0.167 J 11.504 J <5.00 <50.0 <1.00 <1.00 <5.00 <5.00 <1.00 <1.00 0.141 J <1.00 <10.0 <10.0 0.115 J 3.16 0.635 J 2.59 MW-3 06/12/2023 413 <5.00 442 3,420 57.7 74.7 J 1.03 J <5.00 <25.0 <25.0 52.8 <5.00 12.7 5.15 55.5 74.8 53.7 <5.00 527 168 MW-4 06/12/2023 0.125 J 13.9 12.5 88.3 <5.00 <50.0 <1.00 <1.00 <5.00 <5.00 1.25 0.225 J 0.726 J 0.357 J <10.0 <10.0 2.23 0.385 J 11.2 8.90 MW-1D 06/12/2023 0.155 J <1.00 0.321 J 2.288 J <5.00 2,600 <1.00 <1.00 0.215 J 0.206 J <1.00 <1.00 0.125 J <1.00 7.66 J 0.872 J 0.193 J <1.00 0.663 J 1.24 1 600 600 500 6 6,000 0.6 70 NE 70 0.02 0.4 70 25 4,000 100 70 0.7 400 400 5,000 260,000 80,000 50,000 6,000 6,000,000 NE 8,800 NE 70,000 50 400 30,500 11,700 4,000,000 100,000 26,100 700 28,500 24,100 Notes: 1. "<" or ND = Not Detected at or above the reporting limit. 2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion (ppb). 5. GCL = Gross Contamination Level. 6. J = Reported value is an estimate. 7. NE = Not established. 4. Concentrations in Italics print equal or exceed the GCLs. GCL Method 6200B 3. Concentrations in BOLD print equal or exceed the NCDEQ 15A 2L NCAC Groundwater Standard (2L Standard). Monitoring Well Date 2L Standard Page 1 of 1 TABLE 5 HISTORICAL GROUNDWATER ANALYTICAL DATA FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 Benzene Toluene Ethylbenzene Total Xylenes Naphthalene Acrolein Bromodichloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dichloroethane 1,2-Dichloropropane 2-Hexanone Methyl Isobutly Ketone n-Propylbenzene Tetrachloroethylene 1,1,2-Trichloroethane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene5/2/2018 3.5 220 99 730 6.5 NR NR NR 7.4 0.70 NR 7.7 3.9 19 <0.5 <0.5 97 48 1/2/2019 1/31/2019 <0.5 17.3 10.7 114.8 2.9 NA <0.50 <1.0 1.3 <0.5 <0.50 NA NA <0.5 <0.5 <0.5 55 24.6 3/11/2019 <0.5 15.5 6.5 90.4 2.6 NA <0.50 <1.0 <0.2 <0.5 <0.50 NA NA <0.5 <0.5 <0.5 34.8 16.1 11/14/2019 2.8 72 90 520 30 NA <2.0 NA 16 <4.0 <2.0 98 48 10 <2.0 <2.0 110 62 1/2/2020 4.4 280 200 980 30 NA <1.0 NA 23 3.0 <1.0 100 68 29 0.64J 1.3 250 130 6/24/2021 7.25 J 356 333 3,080 59.5 J <2,500 <50.0 <250 44.0 J 7.30 J <50.0 NA 49.9 J 40.9 J <50.0 <50.0 548 205 10/19/2022 1.46 178 308 2,029 79.8 4.91 J <1.00 <5.00 12.6 1.74 0.590 J NA 31.9 51.2 0.633 J <1.00 510 222 6/12/2023 1.01 J 135 109 622 10.7 <50.0 <1.00 <5.00 3.88 0.479 J <1.00 NA 4.64 J 22.3 0.548 J <1.00 138 53.3 10/19/2022 0.190 J <1.00 0.256 J 6.901 J <5.00 <50.0 <1.00 0.946 J <1.00 0.135 J <1.00 NA <10.0 0.221 J 3.13 0.322 J 0.733 J 1.35 6/12/2023 0.255 J <1.00 0.167 J 11.504 J <5.00 <50.0 <1.00 <5.00 <1.00 <1.00 <1.00 NA <10.0 0.115 J 3.16 <1.00 0.635 J 2.59 10/19/2022 0.110 J 2.37 1.12 29.5 <5.00 <50.0 0.731 J <5.00 0.646 J 0.267 J <1.00 NA 1.30 J 0.312 J 0.420 J 0.521 J 3.36 4.69 6/12/2023 413 <5.00 442 3,420 57.7 <250 <5.00 <25.0 52.8 <5.00 <5.00 NA 74.8 53.7 <5.00 <5.00 527 168 10/19/2022 1,390 11,600 1,150 8,860 203 <50.0 <1.00 <5.00 164 <1.00 5.95 NA 239 121 0.635 J <1.00 1,450 502 6/12/2023 0.125 J 13.9 12.5 88.3 <5.00 <50.0 <1.00 <5.00 1.25 0.225 J <1.00 NA <10.0 2.23 0.385 J <1.00 11.2 8.90 10/19/2022 0.116J 7.72 0.631 J 6.42 1.41 J <50.0 <1.00 <5.00 0.312 J <1.00 <1.00 NA 5.79 J 0.564 J <1.00 0.282 J 4.39 1.56 6/12/2023 0.155 J <1.00 0.321 J 2.288 J <5.00 <50.0 <1.00 <5.00 <1.00 <1.00 <1.00 NA 0.872 J 0.193 J <1.00 <1.00 0.663 J 1.24 1 600 600 500 6 4 0.6 0.04 0.02 0.4 0.6 40 100 70 0.7 0.6 400 400 5,000 260,000 80,000 50,000 6,000 NE NE NE 50 400 600 40,000 100,000 26,100 700 600 28,500 24,100 Notes: 1. "<" or ND = Not Detected at or above the reporting limit. 2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion (ppb). 5. GCL = Gross Contamination Level. 6. J = Reported value is an estimate. 7. NE = Not established. 8. NA = Not analyzed. 9. NR = Not reported. GCL 3. Concentrations in BOLD print equal or exceed the NCDEQ 15A 2L NCAC Groundwater Standard (2L Standard). 4. Concentrations in Italics print equal or exceed the GCLs. Monitoring Well Date Method 6200B Enviro-Bac Installed 2L Standard MW-1 MW-2 MW-3 MW-4 MW-1D Page 1 of 1 TABLE 6 WATER SUPPLY WELL ANALYTICAL DATA FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT #24177 Benzene Toluene Ethylbenzene Total Xylenes Naphthalene 1,2-Dichloroethane Tetrachloroethylene5/2/2018 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3/11/2019 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5/2/2018 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3/11/2019 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 WSW-2 6/12/2023 <1.00 <1.00 <1.00 <2.00 <5.00 0.194 J <1.00 5/2/2018 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.6 3/11/2019 <0.5 <0.5 <0.5 <0.5 <0.5 0.37J 2.0 6/12/2023 <1.00 <1.00 <1.00 <2.00 <5.00 0.238 J 1.92 1 600 600 500 6 0.4 0.7 5,000 260,000 80,000 50,000 6,000 400 700 Notes: 1. "<" or ND = Not Detected at or above the reporting limit. 2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion (ppb). 5. GCL = Gross Contamination Level. 6. J = Reported value is an estimate. 7. NE = Not established. 8. NA = Not analyzed. 4. Concentrations in Italics print equal or exceed the GCLs. Monitoring Well Date Method 6200B WSW-1 (Old) WSW-1 (New) 2L Standard GCL 3. Concentrations in BOLD print equal or exceed the NCDEQ 15A 2L NCAC Groundwater Standard (2L Standard). WSW-3 Page 1 of 1 Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program FIGURES Project Number: Date:Scale: Drn. By: Ckd. By:H:\2021\OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAR'S STORE\SLC2417702-VIC.DWG, FIG107/14/2023 FARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701 DH JR 1 1:2,000TOPOGRAPHIC MAP N NC 65FARRAR STORE ROADLEGEND:SITE PROPERTY LINENOTE: ALL LOCATIONS ARE APPROXIMATEPARCEL LINESCALE: 1" = 20'05101520NF A R R A R S T O R E R O A D SITEBUILDINGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGUST-1UST-3PORCHUST-2GGGAS LINEAPPROXIMATE AREAOF EXCAVATIONMW-1MW-1SHALLOW MONITORING WELLWell IdentificationGG G G GGGGG G G G G GG EEEEE E E MW-4MW-3MW-2MW-1DEEUNDERGROUND ELECTRICMW-1DDEEP MONITORING WELLWell IdentificationFigure:Drawing File: Project Number: Ckd. By: Drn. By: App'd By: Ckd. Date:Scale:Date:H:\2023\1 OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAH'S STORE\STL2417701-SITE.DWG, FIG2 SITE MAP07/14/2023SEE LOWER LEFTFARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701AS SHOWNDH JR2NOTES: 1.Features shown are not an authoritative location, nor are they presented to a stated accuracy. COORDINATE SYSTEM: NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET 50SCALE: 1" = 200'0100150200NNC 65RED OAK DRIVECLASSIC LANEFARRAR STORE ROADINTERSTATE 220SPARKLE LANETHRUSH ROADWILDFLOWER DRIVESITELEGEND:SITE PROPERTY LINENOTE: ALL LOCATIONS ARE APPROXIMATEPARCEL LINEWSW-3POTABLE WATER SUPPLY WELLWell Identification500 FT.RADIUS1,000 FT.RADIUSWSW-12WSW-13WSW-11WSW-14WSW-15WSW-10WSW-9WSW-8WSW-6WSW-5WSW-7WSW-16WSW-2(OLD)WSW-2(NEW)WSW-1(NEW)WSW-1(OLD)WSW-4WSW-17WSW-18WSW-19WSW-20WSW-3WSW-1ABANDONED WATER SUPPLY WELLWell IdentificationWSW-17INACTIVE WATER SUPPLY WELLWell IdentificationFigure:Drawing File: Project Number: Ckd. By: Drn. By: App'd By: Ckd. Date:Scale:Date:H:\2021\OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAR'S STORE\SLC2417702-WSW.DWG, FIG3 POTENTIAL RECEPTOR MAP07/14/2023SEE LOWER LEFTFARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701AS SHOWNDH JR3NOTES: 1.Features shown are not an authoritative location, nor are they presented to a stated accuracy. COORDINATE SYSTEM: NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET NON-POTABLE WATER SUPPLY WELLWell IdentificationWSW-19WSW-21 NC 65FARRAR STORE ROADLEGEND:SITE PROPERTY LINEPARCEL LINESCALE: 1" = 20'05101520NF A R R A R S T O R E R O A D SITEBUILDINGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGUST-1UST-3PORCHUST-2GGGAS LINEAPPROXIMATE AREAOF EXCAVATIONMW-1GG G G GGGGG G G G G GG EEEEE E E MW-4MW-3MW-2MW-1DEEUNDERGROUND ELECTRICMW-1DDEEP MONITORING WELLWell IdentificationNOTE: ALL LOCATIONS ARE APPROXIMATE62.70GROUNDWATER ELEVATION CONTOUR(DASHED WHERE INFERRED) (ft)GROUNDWATER FLOW DIRECTIONMW-162.79SHALLOW MONITORING WELLWell IdentificationRelative Groundwater Elevation (ft)63.2463.0763.32*41.5863.6063.163.263.363.463.5Figure:Drawing File: Project Number: Ckd. By: Drn. By: App'd By: Ckd. Date:Scale:Date:H:\2023\1 OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAH'S STORE\STL2417701-POT.DWG, FIG3 GROUNDWATER ELEVATION CONTOUR MAP07/07/2023SEE LOWER LEFTFARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701AS SHOWNDH JR4NOTES: 1.Features shown are not an authoritative location, nor are they presented to a stated accuracy. 2.Groundwater elevations measured on June 12, 2023. 3.* MW-1D was not used to construct contours. COORDINATE SYSTEM: NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET NC 65FARRAR STORE ROADLEGEND:SITE PROPERTY LINEPARCEL LINESCALE: 1" = 20'05101520NF A R R A R S T O R E R O A D SITEBUILDINGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGUST-1UST-3PORCHUST-2GGGAS LINEAPPROXIMATE AREAOF EXCAVATIONMW-1GG G G GGGGG G G G G GG EEEEE E E MW-4MW-3MW-2MW-1DEEUNDERGROUND ELECTRICMW-1DDEEP MONITORING WELLWell IdentificationNOTE: ALL LOCATIONS ARE APPROXIMATE100BENZENE ISOCONCENTRATION CONTOUR(DASHED WHERE INFERRED) (µg/L)MW-11.01SHALLOW MONITORING WELLWell IdentificationBenzene Concentration (µg/L)0.255J4131.01 J*0.155J0.125J11 0 100Figure:Drawing File: Project Number: Ckd. By: Drn. By: App'd By: Ckd. Date:Scale:Date:H:\2023\1 OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAH'S STORE\STL2417701-BENZ.DWG, FIG4 DISSOLVED BENZENE ISOCONCENTRATION MAP07/07/2023SEE LOWER LEFTFARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701AS SHOWNDH JR5NOTES: 1.Features shown are not an authoritative location, nor are they presented to a stated accuracy. 2.Groundwater samples collected on June 12, 2023. 3.* MW-1D was not used to construct contours. 4.J = reported value is an estimate. COORDINATE SYSTEM: NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET NC 65FARRAR STORE ROADLEGEND:SITE PROPERTY LINEPARCEL LINESCALE: 1" = 20'05101520NF A R R A R S T O R E R O A D SITEBUILDINGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGUST-1UST-3PORCHUST-2GGGAS LINEAPPROXIMATE AREAOF EXCAVATIONMW-1GG G G GGGGG G G G G GG EEEEE E E MW-4MW-3MW-2MW-1DEEUNDERGROUND ELECTRICMW-1DDEEP MONITORING WELLWell IdentificationNOTE: ALL LOCATIONS ARE APPROXIMATE201,2-DIBROMOETHANE ISOCONCENTRATIONCONTOUR (DASHED WHERE INFERRED) (µg/L)MW-11.25SHALLOW MONITORING WELLWell Identification1,2-Dibromoethane Concentration (µg/L)<1.0052.83.88<1.001.25202.00.20.02Figure:Drawing File: Project Number: Ckd. By: Drn. By: App'd By: Ckd. Date:Scale:Date:H:\2023\1 OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAH'S STORE\STL2417701-12D.DWG, FIG5 DISSOLVED 1,2-DIBROMOETHANE ISOCONCENTRATION MAP07/07/2023SEE LOWER LEFTFARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701AS SHOWNDH JR6NOTES: 1.Features shown are not an authoritative location, nor are they presented to a stated accuracy. 2.Groundwater samples collected on June 12, 2023. 3.* MW-1D was not used to construct contours. 4.J = reported value is an estimate. COORDINATE SYSTEM: NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET NC 65FARRAR STORE ROADLEGEND:SITE PROPERTY LINENOTE: ALL LOCATIONS ARE APPROXIMATEPARCEL LINESCALE: 1" = 20'05101520NF A R R A R S T O R E R O A D SITEBUILDINGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGGUST-1UST-3PORCHUST-2GGGAS LINEAPPROXIMATE AREAOF EXCAVATIONMW-1MW-1SHALLOW MONITORING WELLWell IdentificationGG G G GGGGG G G G G GG EEEEE E E MW-4MW-3MW-2MW-1DEEUNDERGROUND ELECTRICMW-1DDEEP MONITORING WELLWell IdentificationFigure:Drawing File: Project Number: Ckd. By: Drn. By: App'd By: Ckd. Date:Scale:Date:H:\2023\1 OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\FARRAH'S STORE\STL2417701-GW.DWG, FIG6 ADDITIONAL CHEMICALS OF CONCERN IN GROUNDWATER07/07/2023SEE LOWER LEFTFARRAR'S STORE 397 FARRAR STORE ROAD STOKESDALE, ROCKINGHAM COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 24177 STL2417701AS SHOWNDH JR7NOTES: 1.Features shown are not an authoritative location, nor are they presented to a stated accuracy. 2.Groundwater samples collected on June 12, 2023. 3.Groundwater is measured in micrograms per liter (µg/L). 4.J = Reported value is an estimate. COORDINATE SYSTEM: NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program APPENDIX A CONCEPTUAL SITE MODEL Site Name: Farrars's Store Date: 07/14/2023 Property Owner: Greg Westmoreland Last Field Event Date:6/12/2023 Site Name:Farrar's Store Release Discovery Date:9/24/2004 NCDEQ UST Incident No.:24177 Source of Release:UST System Facility ID No.:Unregistered Estimated Volume of Release:Unknown Risk Classification:High Risk Rank:Unknown Gasoline (leaded)Unknown Site Address:397 Farrar Store Road Gasoline (unleaded)Unknown Site City, ST ZIP:Stokesdale, NC 27357 Gasoline (ethanol blend)Unknown Site County:Rockingham Diesel No NCDEQ Regional Office:Winston-Salem Kerosene No Active UST Facility:No Heating Oil (#2)No USTs Present:No Heating Oil (>#2)No Motor Oil No Hydraulic Oil No Major Soil Type:sand, clay, silt Used Oil No Surface Cover over impacted soil:No Utilities within plume (Y/N/U):Unknown >S-W MSCCs (Y/N/U):Yes >Residential MSCCs (Y/N/U):Yes Site (Current):Vacant >Comm/Ind MSCCs (Y/N/U):No Site (Future):Unknown North Adjacent:Residential East Adjacent:Residential Litho-Tectonic Zone Piemont South Adjacent:Residential Geologic Formation Charlotte and Milton Belts West Adjacent:Residential Rock Type Metamorphic Depth to Bedrock (ft bgs)44 Municipal Water (Y/N/U):Yes Active Potable Wells <1000 ft (#/U):Yes (16 total) Active Potable Wells <500 ft (#/U):Yes (6 total) Depth to water (ft-bgs) Type II Well Network: 34.07-37.25 ft bgs Type III Well Network: 58.25-79.55 ft bgs Impacted Wells (Y/N/U):Yes Gradient (ft/ft):0.00512 Any wells <250 ft (Y/N/U):Yes Direction (N E S W combo):East Hydraulic Conductivity (ft/day):Unknown <500 ft (Y/N):No Total Porosity (%):Unknown Type of Surface Water:N/A Effective Porosity (%):Unknown Name of Nearest Stream: Unnamed stream located approximately 900 feet south-southeast of the site which connects a freshwater pond to a wetland. Flow Rate (ft/year):Unknown Stream Classification:R4SBC (R - Riverine; 4 - intermittent; SB - streambed; C - seasonally flooded) COCs >2L (Y/N/U):Yes Impacted Surface Water (Y/N/U): - - COCs >2L Extent Defined (Y/N):No COCs >GCLs (Y/N/U):Yes COCs >GCLs (Wells):MW-3 >LEL in Structures:No COCs >GCLs Extent Defined (Y/N):No Vapors in Buildings:No COCs >2B Standards by 10X (Y/N/U):N/A Slab-on-grade or Crawlspace:No LNAPL (Y/N/U):N/A Dissolved VOCs <5 ft of Structures:No LNAPL (Max Thickness ft):N/A LNAPL <15 ft of Structures:No LNAPL (Wells):N/A Basement <30 ft of Dissolved COCs:No LNAPL Extent Defined (Y/N):N/A LNAPL (<5 ft beneath buildings/U):N/A Utilities within plume (Y/N/U):Unknown Alternative Water Source:Yes - connect at risk properties with water supply wells to municipal water NORP: - - Site Remediation: - - Soil Excavation: - - AFVR: - - MMPE: - - SVE/AS: - - Other:Need to delineate GCL impacts prior to determining a pathway to closure. Additional Support Documentation Available / Data Gaps: In Febraury 2011, ten soil borings were installed at the site which resulted in detections of contaminants of concern at concentrations which exceeded the applicable soil-to-groundwater and residential maximum soil contaminant concentrations. Source removal activities were completed in August 2015 which resulted in the removal of UST-3 and contaminated soils from within the former UST basins. Approximately 70.64 tons of imported fill was brought to the site following the UST and source removal. However, a report documenting UST closure and source removal activities was not available for review. Therefore, it is unknown whether or not soil impacts remain the the site and to what extent. Approach (general discussion): (1) Reduce risk classification by reducing receptors (abandoning water supply wells and connecting properties to municipal water). (2) Reduce impacted groundwater concentrations below GCLs. Surface Water Land Use / Zoning Site is currently vacant. CONCEPTUAL SITE MODEL Soil Information Possible Path(s) to Closure Site Information Release Information Petroleum Type Released Geologic Information Groundwater Information Comments: Receptor Information Water Supply Vapor Page 1 of 1 Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program APPENDIX B SITE PHOTOGRAPHS Photo 1: Site status Photo 2: View of MW-1. Site Photographs Farrar’s Store - Incident #24177 397 Farrar Store Road Stokesdale, Rockingham County, North Carolina 2725 E. Millbrook Road, Suite 121 Raleigh, North Carolina Tel: (919) 871-0999 Fax: (737) 207-8261 Photos Taken By: Justin Jones Site ID: Incident #24177 ATC Project No.: STL2417701 Photo 3: View of MW-2. Photo 4: View of MW-3. Site Photographs Farrar’s Store - Incident #24177 397 Farrar Store Road Stokesdale, Rockingham County, North Carolina 2725 E. Millbrook Road, Suite 121 Raleigh, North Carolina Tel: (919) 871-0999 Fax: (737) 207-8261 Photos Taken By: Justin Jones Site ID: Incident #24177 ATC Project No.: STL2417701 Photo 5: View of MW-4. Photo 6: View of MW-1D. Site Photographs Farrar’s Store - Incident #24177 397 Farrar Store Road Stokesdale, Rockingham County, North Carolina 2725 E. Millbrook Road, Suite 121 Raleigh, North Carolina Tel: (919) 871-0999 Fax: (737) 207-8261 Photos Taken By: Justin Jones Site ID: Incident #24177 ATC Project No.: STL2417701 Photo 7: View of WSW-2. Photo 8: View of WSW-3. Site Photographs Farrar’s Store - Incident #24177 397 Farrar Store Road Stokesdale, Rockingham County, North Carolina 2725 E. Millbrook Road, Suite 121 Raleigh, North Carolina Tel: (919) 871-0999 Fax: (737) 207-8261 Photos Taken By: Justin Jones Site ID: Incident #24177 ATC Project No.: STL2417701 Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program APPENDIX C FIELD NOTES Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program APPENDIX D GSI MANN-KENDALL TOOLKIT Evaluation Date:Job ID: Facility Name:Constituent: Conducted By:Concentration Units:µg/L Sampling Point ID:Benzene Total Xylenes Naphthalene EDB 1,2-DCE 1,2,4-TMB Sampling Sampling Event Date 1 05/02/18 3.5 730 6.5 7.4 0.7 97 2 01/31/19 0.25 114.8 2.9 1.3 0.25 55 3 03/11/19 0.25 90.4 2.6 0.1 0.25 34.8 4 11/14/19 2.8 520 30 16 0.2 110 5 01/02/20 4.4 980 30 23 3 250 6 06/24/21 7.25 3080 59.5 44 7.3 548 7 10/19/22 1.46 2029 79.8 12.6 1.74 510 8 06/12/23 1.01 622 10.7 3.88 0.479 138 9 10 11 12 13 14 15 16 17 18 19 20 Coefficient of Variation:0.92 1.01 1.03 1.08 1.41 0.93 Mann-Kendall Statistic (S):3 10 13 6 5 14 Confidence Factor:59.4%86.2%92.9%72.6%68.3%94.6% Concentration Trend:No Trend No Trend Prob. Increasing No Trend No Trend Prob. Increasing Notes: 1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples. 2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing; ≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable. 3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales, Ground Water, 41(3):355-367, 2003. DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein. GSI Environmental Inc., www.gsi-net.com MW-1 CONCENTRATION (µg/L) 7/14/2023 Farrar's Store MW-1 GSI MANN-KENDALL TOOLKIT for Constituent Trend Analysis ATC Associates of North Carolina, P.C. Incident #24177 0.1 1 10 100 1000 10000 09/17 02/19 06/20 10/21 03/23 07/24Concentration (µg/L)Sampling Date Benzene Total Xylenes Naphthalene EDB 1,2-DCE 1,2,4-TMB Farrar’s Store ATC Project No. STL2417701 NCDEQ State Lead Program APPENDIX E LABORATORY ANALYTICAL RESULTS ANALYTICAL REPORT June 22, 2023 ATC Group Services LLC Sample Delivery Group:L1625719 Samples Received:06/14/2023 Project Number: Description:Farrar's Store Report To:Nicholas Kramer 2725 E. Millbrook Road, Ste 121 Raleigh, NC 27604 Entire Report Reviewed By: June 22, 2023 [Preliminary Report] Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 1 of 36 June 23, 2023 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 1 of 36 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 MW-1 L1625719-01 5 MW-2 L1625719-02 7 MW-3 L1625719-03 9 MW-4 L1625719-04 11 MW-1D L1625719-05 13 FB-1 L1625719-06 15 WSW-2 L1625719-07 17 WSW-3 L1625719-08 19 Qc: Quality Control Summary 21 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 21 Gl: Glossary of Terms 34 Al: Accreditations & Locations 35 Sc: Sample Chain of Custody 36 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 2 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 2 of 36 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-1 L1625719-01 GW Justin Jones 06/12/23 11:25 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2079572 1 06/17/23 11:36 06/17/23 11:36 JAH Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2081057 10 06/21/23 12:45 06/21/23 12:45 TJJ Mt. Juliet, TN Collected by Collected date/time Received date/time MW-2 L1625719-02 GW Justin Jones 06/12/23 12:15 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2080288 1 06/19/23 12:15 06/19/23 12:15 JBE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2081917 1 06/21/23 16:22 06/21/23 16:22 JHH Mt. Juliet, TN Collected by Collected date/time Received date/time MW-3 L1625719-03 GW Justin Jones 06/12/23 12:25 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2080288 5 06/19/23 12:35 06/19/23 12:35 JBE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2081917 100 06/21/23 20:50 06/21/23 20:50 DYW Mt. Juliet, TN Collected by Collected date/time Received date/time MW-4 L1625719-04 GW Justin Jones 06/12/23 13:00 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2080288 1 06/19/23 12:56 06/19/23 12:56 JBE Mt. Juliet, TN Collected by Collected date/time Received date/time MW-1D L1625719-05 GW Justin Jones 06/12/23 11:00 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2080288 1 06/19/23 13:17 06/19/23 13:17 JBE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2081917 5 06/21/23 21:10 06/21/23 21:10 DYW Mt. Juliet, TN Collected by Collected date/time Received date/time FB-1 L1625719-06 GW Justin Jones 06/12/23 13:10 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2081917 1 06/21/23 17:03 06/21/23 17:03 DYW Mt. Juliet, TN Collected by Collected date/time Received date/time WSW-2 L1625719-07 GW Justin Jones 06/12/23 13:30 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2080288 1 06/19/23 13:37 06/19/23 13:37 JBE Mt. Juliet, TN Collected by Collected date/time Received date/time WSW-3 L1625719-08 GW Justin Jones 06/12/23 13:50 06/14/23 09:05 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2080288 1 06/19/23 13:58 06/19/23 13:58 JBE Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 3 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 3 of 36 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Heather J Wagner Project Manager 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 4 of 36 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 4 of 36 SAMPLE RESULTS - 01 L1625719 MW-1 Collected date/time: 06/12/23 11:25 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone 14.3 J 11.3 50.0 1 06/17/2023 11:36 WG2079572 Acrolein U 2.54 50.0 1 06/17/2023 11:36 WG2079572 Acrylonitrile U 0.671 10.0 1 06/17/2023 11:36 WG2079572 Benzene 1.01 J 0.941 10.0 10 06/21/2023 12:45 WG2081057 Bromobenzene U 0.118 1.00 1 06/17/2023 11:36 WG2079572 Bromodichloromethane U 0.136 1.00 1 06/17/2023 11:36 WG2079572 Bromoform U 0.129 1.00 1 06/17/2023 11:36 WG2079572 Bromomethane U 0.605 5.00 1 06/17/2023 11:36 WG2079572 n-Butylbenzene U 0.157 1.00 1 06/17/2023 11:36 WG2079572 sec-Butylbenzene 1.16 0.125 1.00 1 06/17/2023 11:36 WG2079572 tert-Butylbenzene U 0.127 1.00 1 06/17/2023 11:36 WG2079572 Carbon tetrachloride U 0.128 1.00 1 06/17/2023 11:36 WG2079572 Chlorobenzene U 0.116 1.00 1 06/17/2023 11:36 WG2079572 Chlorodibromomethane U 0.140 1.00 1 06/17/2023 11:36 WG2079572 Chloroethane U 0.192 5.00 1 06/17/2023 11:36 WG2079572 Chloroform U 0.111 5.00 1 06/17/2023 11:36 WG2079572 Chloromethane U 0.960 2.50 1 06/17/2023 11:36 WG2079572 2-Chlorotoluene U 0.106 1.00 1 06/17/2023 11:36 WG2079572 4-Chlorotoluene U 0.114 1.00 1 06/17/2023 11:36 WG2079572 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/17/2023 11:36 WG2079572 1,2-Dibromoethane 3.88 0.126 1.00 1 06/17/2023 11:36 WG2079572 Dibromomethane U 0.122 1.00 1 06/17/2023 11:36 WG2079572 1,2-Dichlorobenzene U 0.107 1.00 1 06/17/2023 11:36 WG2079572 1,3-Dichlorobenzene U 0.110 1.00 1 06/17/2023 11:36 WG2079572 1,4-Dichlorobenzene U 0.120 1.00 1 06/17/2023 11:36 WG2079572 Dichlorodifluoromethane U 0.374 5.00 1 06/17/2023 11:36 WG2079572 1,1-Dichloroethane U 0.100 1.00 1 06/17/2023 11:36 WG2079572 1,2-Dichloroethane 0.479 J 0.0819 1.00 1 06/17/2023 11:36 WG2079572 1,1-Dichloroethene U 0.188 1.00 1 06/17/2023 11:36 WG2079572 cis-1,2-Dichloroethene U 0.126 1.00 1 06/17/2023 11:36 WG2079572 trans-1,2-Dichloroethene U 0.149 1.00 1 06/17/2023 11:36 WG2079572 1,2-Dichloropropane U 0.149 1.00 1 06/17/2023 11:36 WG2079572 1,1-Dichloropropene U 0.142 1.00 1 06/17/2023 11:36 WG2079572 1,3-Dichloropropane U 0.110 1.00 1 06/17/2023 11:36 WG2079572 2,2-Dichloropropane U 0.161 1.00 1 06/17/2023 11:36 WG2079572 Di-isopropyl ether U 0.105 1.00 1 06/17/2023 11:36 WG2079572 Ethylbenzene 109 0.137 1.00 1 06/17/2023 11:36 WG2079572 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/17/2023 11:36 WG2079572 Isopropylbenzene 5.36 0.105 1.00 1 06/17/2023 11:36 WG2079572 p-Isopropyltoluene U 0.120 1.00 1 06/17/2023 11:36 WG2079572 2-Butanone (MEK)U 1.19 10.0 1 06/17/2023 11:36 WG2079572 Methylene Chloride U 0.430 5.00 1 06/17/2023 11:36 WG2079572 4-Methyl-2-pentanone (MIBK)4.64 J 0.478 10.0 1 06/17/2023 11:36 WG2079572 Methyl tert-butyl ether U 0.101 1.00 1 06/17/2023 11:36 WG2079572 Naphthalene 10.7 1.00 5.00 1 06/17/2023 11:36 WG2079572 n-Propylbenzene 22.3 0.0993 1.00 1 06/17/2023 11:36 WG2079572 Styrene U 0.118 1.00 1 06/17/2023 11:36 WG2079572 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/17/2023 11:36 WG2079572 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/17/2023 11:36 WG2079572 Tetrachloroethene 0.548 J 0.300 1.00 1 06/17/2023 11:36 WG2079572 Toluene 135 0.278 1.00 1 06/17/2023 11:36 WG2079572 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/17/2023 11:36 WG2079572 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/17/2023 11:36 WG2079572 1,1,1-Trichloroethane U 0.149 1.00 1 06/17/2023 11:36 WG2079572 1,1,2-Trichloroethane U 0.158 1.00 1 06/17/2023 11:36 WG2079572 Trichloroethene U 0.190 1.00 1 06/17/2023 11:36 WG2079572 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 5 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 5 of 36 SAMPLE RESULTS - 01 L1625719 MW-1 Collected date/time: 06/12/23 11:25 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/17/2023 11:36 WG2079572 1,2,3-Trichloropropane U 0.237 2.50 1 06/17/2023 11:36 WG2079572 1,2,4-Trimethylbenzene 138 0.322 1.00 1 06/17/2023 11:36 WG2079572 1,3,5-Trimethylbenzene 53.3 0.104 1.00 1 06/17/2023 11:36 WG2079572 Vinyl chloride U 0.234 1.00 1 06/17/2023 11:36 WG2079572 o-Xylene 198 1.74 10.0 10 06/21/2023 12:45 WG2081057 m&p-Xylenes 424 4.30 20.0 10 06/21/2023 12:45 WG2081057 (S) Toluene-d8 115 80.0-120 06/17/2023 11:36 WG2079572 (S) Toluene-d8 100 80.0-120 06/21/2023 12:45 WG2081057 (S) 4-Bromofluorobenzene 111 77.0-126 06/17/2023 11:36 WG2079572 (S) 4-Bromofluorobenzene 96.9 77.0-126 06/21/2023 12:45 WG2081057 (S) 1,2-Dichloroethane-d4 103 70.0-130 06/17/2023 11:36 WG2079572 (S) 1,2-Dichloroethane-d4 107 70.0-130 06/21/2023 12:45 WG2081057 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 6 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 6 of 36 SAMPLE RESULTS - 02 L1625719 MW-2 Collected date/time: 06/12/23 12:15 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 06/19/2023 12:15 WG2080288 Acrolein U 2.54 50.0 1 06/19/2023 12:15 WG2080288 Acrylonitrile U 0.671 10.0 1 06/19/2023 12:15 WG2080288 Benzene 0.255 J 0.0941 1.00 1 06/19/2023 12:15 WG2080288 Bromobenzene U 0.118 1.00 1 06/21/2023 16:22 WG2081917 Bromodichloromethane U 0.136 1.00 1 06/19/2023 12:15 WG2080288 Bromoform U 0.129 1.00 1 06/21/2023 16:22 WG2081917 Bromomethane U 0.605 5.00 1 06/19/2023 12:15 WG2080288 n-Butylbenzene U 0.157 1.00 1 06/21/2023 16:22 WG2081917 sec-Butylbenzene U 0.125 1.00 1 06/21/2023 16:22 WG2081917 tert-Butylbenzene U 0.127 1.00 1 06/21/2023 16:22 WG2081917 Carbon tetrachloride U 0.128 1.00 1 06/19/2023 12:15 WG2080288 Chlorobenzene U 0.116 1.00 1 06/21/2023 16:22 WG2081917 Chlorodibromomethane U 0.140 1.00 1 06/21/2023 16:22 WG2081917 Chloroethane U 0.192 5.00 1 06/19/2023 12:15 WG2080288 Chloroform U 0.111 5.00 1 06/19/2023 12:15 WG2080288 Chloromethane U 0.960 2.50 1 06/19/2023 12:15 WG2080288 2-Chlorotoluene U 0.106 1.00 1 06/21/2023 16:22 WG2081917 4-Chlorotoluene U 0.114 1.00 1 06/21/2023 16:22 WG2081917 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/21/2023 16:22 WG2081917 1,2-Dibromoethane U 0.126 1.00 1 06/21/2023 16:22 WG2081917 Dibromomethane U 0.122 1.00 1 06/19/2023 12:15 WG2080288 1,2-Dichlorobenzene U 0.107 1.00 1 06/21/2023 16:22 WG2081917 1,3-Dichlorobenzene U 0.110 1.00 1 06/21/2023 16:22 WG2081917 1,4-Dichlorobenzene U 0.120 1.00 1 06/21/2023 16:22 WG2081917 Dichlorodifluoromethane U 0.374 5.00 1 06/19/2023 12:15 WG2080288 1,1-Dichloroethane U 0.100 1.00 1 06/19/2023 12:15 WG2080288 1,2-Dichloroethane U 0.0819 1.00 1 06/19/2023 12:15 WG2080288 1,1-Dichloroethene U 0.188 1.00 1 06/19/2023 12:15 WG2080288 cis-1,2-Dichloroethene U 0.126 1.00 1 06/19/2023 12:15 WG2080288 trans-1,2-Dichloroethene U 0.149 1.00 1 06/19/2023 12:15 WG2080288 1,2-Dichloropropane U 0.149 1.00 1 06/19/2023 12:15 WG2080288 1,1-Dichloropropene U 0.142 1.00 1 06/19/2023 12:15 WG2080288 1,3-Dichloropropane U 0.110 1.00 1 06/21/2023 16:22 WG2081917 2,2-Dichloropropane U 0.161 1.00 1 06/19/2023 12:15 WG2080288 Di-isopropyl ether U 0.105 1.00 1 06/19/2023 12:15 WG2080288 Ethylbenzene 0.167 J 0.137 1.00 1 06/21/2023 16:22 WG2081917 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/21/2023 16:22 WG2081917 Isopropylbenzene 0.141 J 0.105 1.00 1 06/21/2023 16:22 WG2081917 p-Isopropyltoluene U 0.120 1.00 1 06/21/2023 16:22 WG2081917 2-Butanone (MEK)U 1.19 10.0 1 06/19/2023 12:15 WG2080288 Methylene Chloride U 0.430 5.00 1 06/19/2023 12:15 WG2080288 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 06/19/2023 12:15 WG2080288 Methyl tert-butyl ether U 0.101 1.00 1 06/19/2023 12:15 WG2080288 Naphthalene U 1.00 5.00 1 06/21/2023 16:22 WG2081917 n-Propylbenzene 0.115 J 0.0993 1.00 1 06/21/2023 16:22 WG2081917 Styrene U 0.118 1.00 1 06/21/2023 16:22 WG2081917 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/21/2023 16:22 WG2081917 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/21/2023 16:22 WG2081917 Tetrachloroethene 3.16 0.300 1.00 1 06/21/2023 16:22 WG2081917 Toluene U 0.278 1.00 1 06/21/2023 16:22 WG2081917 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/21/2023 16:22 WG2081917 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/21/2023 16:22 WG2081917 1,1,1-Trichloroethane U 0.149 1.00 1 06/19/2023 12:15 WG2080288 1,1,2-Trichloroethane U 0.158 1.00 1 06/21/2023 16:22 WG2081917 Trichloroethene U 0.190 1.00 1 06/19/2023 12:15 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 7 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 7 of 36 SAMPLE RESULTS - 02 L1625719 MW-2 Collected date/time: 06/12/23 12:15 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/19/2023 12:15 WG2080288 1,2,3-Trichloropropane U 0.237 2.50 1 06/21/2023 16:22 WG2081917 1,2,4-Trimethylbenzene 0.635 J 0.322 1.00 1 06/21/2023 16:22 WG2081917 1,3,5-Trimethylbenzene 2.59 0.104 1.00 1 06/21/2023 16:22 WG2081917 Vinyl chloride U 0.234 1.00 1 06/19/2023 12:15 WG2080288 o-Xylene 10.6 0.174 1.00 1 06/21/2023 16:22 WG2081917 m&p-Xylenes 0.904 J 0.430 2.00 1 06/21/2023 16:22 WG2081917 (S) Toluene-d8 107 80.0-120 06/19/2023 12:15 WG2080288 (S) Toluene-d8 115 80.0-120 06/21/2023 16:22 WG2081917 (S) 4-Bromofluorobenzene 103 77.0-126 06/19/2023 12:15 WG2080288 (S) 4-Bromofluorobenzene 96.0 77.0-126 06/21/2023 16:22 WG2081917 (S) 1,2-Dichloroethane-d4 88.9 70.0-130 06/19/2023 12:15 WG2080288 (S) 1,2-Dichloroethane-d4 120 70.0-130 06/21/2023 16:22 WG2081917 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 8 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 8 of 36 SAMPLE RESULTS - 03 L1625719 MW-3 Collected date/time: 06/12/23 12:25 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone 74.7 J 56.5 250 5 06/19/2023 12:35 WG2080288 Acrolein U 12.7 250 5 06/19/2023 12:35 WG2080288 Acrylonitrile U 3.36 50.0 5 06/19/2023 12:35 WG2080288 Benzene 413 0.471 5.00 5 06/19/2023 12:35 WG2080288 Bromobenzene U 0.590 5.00 5 06/19/2023 12:35 WG2080288 Bromodichloromethane 1.03 J 0.680 5.00 5 06/19/2023 12:35 WG2080288 Bromoform U 0.645 5.00 5 06/19/2023 12:35 WG2080288 Bromomethane U 3.03 25.0 5 06/19/2023 12:35 WG2080288 n-Butylbenzene U 0.785 5.00 5 06/19/2023 12:35 WG2080288 sec-Butylbenzene U 0.625 5.00 5 06/19/2023 12:35 WG2080288 tert-Butylbenzene U 0.635 5.00 5 06/19/2023 12:35 WG2080288 Carbon tetrachloride U 0.640 5.00 5 06/19/2023 12:35 WG2080288 Chlorobenzene U 0.580 5.00 5 06/19/2023 12:35 WG2080288 Chlorodibromomethane U 0.700 5.00 5 06/19/2023 12:35 WG2080288 Chloroethane U 0.960 25.0 5 06/19/2023 12:35 WG2080288 Chloroform U 0.555 25.0 5 06/19/2023 12:35 WG2080288 Chloromethane U 4.80 12.5 5 06/19/2023 12:35 WG2080288 2-Chlorotoluene U 0.530 5.00 5 06/19/2023 12:35 WG2080288 4-Chlorotoluene U 0.570 5.00 5 06/19/2023 12:35 WG2080288 1,2-Dibromo-3-Chloropropane U 1.38 25.0 5 06/19/2023 12:35 WG2080288 1,2-Dibromoethane 52.8 0.630 5.00 5 06/19/2023 12:35 WG2080288 Dibromomethane U 0.610 5.00 5 06/19/2023 12:35 WG2080288 1,2-Dichlorobenzene U 0.535 5.00 5 06/19/2023 12:35 WG2080288 1,3-Dichlorobenzene U 0.550 5.00 5 06/19/2023 12:35 WG2080288 1,4-Dichlorobenzene U 0.600 5.00 5 06/19/2023 12:35 WG2080288 Dichlorodifluoromethane U 1.87 25.0 5 06/19/2023 12:35 WG2080288 1,1-Dichloroethane U 0.500 5.00 5 06/19/2023 12:35 WG2080288 1,2-Dichloroethane U 0.409 5.00 5 06/19/2023 12:35 WG2080288 1,1-Dichloroethene U 0.940 5.00 5 06/19/2023 12:35 WG2080288 cis-1,2-Dichloroethene U 0.630 5.00 5 06/19/2023 12:35 WG2080288 trans-1,2-Dichloroethene U 0.745 5.00 5 06/19/2023 12:35 WG2080288 1,2-Dichloropropane U 0.745 5.00 5 06/19/2023 12:35 WG2080288 1,1-Dichloropropene U 0.710 5.00 5 06/19/2023 12:35 WG2080288 1,3-Dichloropropane U 0.550 5.00 5 06/19/2023 12:35 WG2080288 2,2-Dichloropropane U 0.805 5.00 5 06/19/2023 12:35 WG2080288 Di-isopropyl ether U 0.525 5.00 5 06/19/2023 12:35 WG2080288 Ethylbenzene 442 0.685 5.00 5 06/19/2023 12:35 WG2080288 Hexachloro-1,3-butadiene U 1.69 5.00 5 06/19/2023 12:35 WG2080288 Isopropylbenzene 12.7 0.525 5.00 5 06/19/2023 12:35 WG2080288 p-Isopropyltoluene 5.15 0.600 5.00 5 06/19/2023 12:35 WG2080288 2-Butanone (MEK)55.5 5.95 50.0 5 06/19/2023 12:35 WG2080288 Methylene Chloride U 2.15 25.0 5 06/19/2023 12:35 WG2080288 4-Methyl-2-pentanone (MIBK)74.8 2.39 50.0 5 06/19/2023 12:35 WG2080288 Methyl tert-butyl ether U 0.505 5.00 5 06/19/2023 12:35 WG2080288 Naphthalene 57.7 5.00 25.0 5 06/19/2023 12:35 WG2080288 n-Propylbenzene 53.7 0.497 5.00 5 06/19/2023 12:35 WG2080288 Styrene U 0.590 5.00 5 06/19/2023 12:35 WG2080288 1,1,1,2-Tetrachloroethane U 0.735 5.00 5 06/19/2023 12:35 WG2080288 1,1,2,2-Tetrachloroethane U 0.665 5.00 5 06/19/2023 12:35 WG2080288 Tetrachloroethene U 1.50 5.00 5 06/19/2023 12:35 WG2080288 Toluene U 1.39 5.00 5 06/19/2023 12:35 WG2080288 1,2,3-Trichlorobenzene U 1.15 5.00 5 06/19/2023 12:35 WG2080288 1,2,4-Trichlorobenzene U 2.41 5.00 5 06/19/2023 12:35 WG2080288 1,1,1-Trichloroethane U 0.745 5.00 5 06/19/2023 12:35 WG2080288 1,1,2-Trichloroethane U 0.790 5.00 5 06/19/2023 12:35 WG2080288 Trichloroethene U 0.950 5.00 5 06/19/2023 12:35 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 9 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 9 of 36 SAMPLE RESULTS - 03 L1625719 MW-3 Collected date/time: 06/12/23 12:25 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.800 25.0 5 06/19/2023 12:35 WG2080288 1,2,3-Trichloropropane U 1.19 12.5 5 06/19/2023 12:35 WG2080288 1,2,4-Trimethylbenzene 527 1.61 5.00 5 06/19/2023 12:35 WG2080288 1,3,5-Trimethylbenzene 168 0.520 5.00 5 06/19/2023 12:35 WG2080288 Vinyl chloride U 1.17 5.00 5 06/19/2023 12:35 WG2080288 o-Xylene 1120 17.4 100 100 06/21/2023 20:50 WG2081917 m&p-Xylenes 2300 43.0 200 100 06/21/2023 20:50 WG2081917 (S) Toluene-d8 89.7 80.0-120 06/19/2023 12:35 WG2080288 (S) Toluene-d8 113 80.0-120 06/21/2023 20:50 WG2081917 (S) 4-Bromofluorobenzene 103 77.0-126 06/19/2023 12:35 WG2080288 (S) 4-Bromofluorobenzene 94.4 77.0-126 06/21/2023 20:50 WG2081917 (S) 1,2-Dichloroethane-d4 92.4 70.0-130 06/19/2023 12:35 WG2080288 (S) 1,2-Dichloroethane-d4 122 70.0-130 06/21/2023 20:50 WG2081917 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 10 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 10 of 36 SAMPLE RESULTS - 04 L1625719 MW-4 Collected date/time: 06/12/23 13:00 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 06/19/2023 12:56 WG2080288 Acrolein U 2.54 50.0 1 06/19/2023 12:56 WG2080288 Acrylonitrile U 0.671 10.0 1 06/19/2023 12:56 WG2080288 Benzene 0.125 J 0.0941 1.00 1 06/19/2023 12:56 WG2080288 Bromobenzene U 0.118 1.00 1 06/19/2023 12:56 WG2080288 Bromodichloromethane U 0.136 1.00 1 06/19/2023 12:56 WG2080288 Bromoform U 0.129 1.00 1 06/19/2023 12:56 WG2080288 Bromomethane U 0.605 5.00 1 06/19/2023 12:56 WG2080288 n-Butylbenzene U 0.157 1.00 1 06/19/2023 12:56 WG2080288 sec-Butylbenzene U 0.125 1.00 1 06/19/2023 12:56 WG2080288 tert-Butylbenzene U 0.127 1.00 1 06/19/2023 12:56 WG2080288 Carbon tetrachloride U 0.128 1.00 1 06/19/2023 12:56 WG2080288 Chlorobenzene U 0.116 1.00 1 06/19/2023 12:56 WG2080288 Chlorodibromomethane U 0.140 1.00 1 06/19/2023 12:56 WG2080288 Chloroethane U 0.192 5.00 1 06/19/2023 12:56 WG2080288 Chloroform U 0.111 5.00 1 06/19/2023 12:56 WG2080288 Chloromethane U 0.960 2.50 1 06/19/2023 12:56 WG2080288 2-Chlorotoluene U 0.106 1.00 1 06/19/2023 12:56 WG2080288 4-Chlorotoluene U 0.114 1.00 1 06/19/2023 12:56 WG2080288 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/19/2023 12:56 WG2080288 1,2-Dibromoethane 1.25 0.126 1.00 1 06/19/2023 12:56 WG2080288 Dibromomethane U 0.122 1.00 1 06/19/2023 12:56 WG2080288 1,2-Dichlorobenzene U 0.107 1.00 1 06/19/2023 12:56 WG2080288 1,3-Dichlorobenzene U 0.110 1.00 1 06/19/2023 12:56 WG2080288 1,4-Dichlorobenzene U 0.120 1.00 1 06/19/2023 12:56 WG2080288 Dichlorodifluoromethane U 0.374 5.00 1 06/19/2023 12:56 WG2080288 1,1-Dichloroethane U 0.100 1.00 1 06/19/2023 12:56 WG2080288 1,2-Dichloroethane 0.225 J 0.0819 1.00 1 06/19/2023 12:56 WG2080288 1,1-Dichloroethene U 0.188 1.00 1 06/19/2023 12:56 WG2080288 cis-1,2-Dichloroethene U 0.126 1.00 1 06/19/2023 12:56 WG2080288 trans-1,2-Dichloroethene U 0.149 1.00 1 06/19/2023 12:56 WG2080288 1,2-Dichloropropane U 0.149 1.00 1 06/19/2023 12:56 WG2080288 1,1-Dichloropropene U 0.142 1.00 1 06/19/2023 12:56 WG2080288 1,3-Dichloropropane U 0.110 1.00 1 06/19/2023 12:56 WG2080288 2,2-Dichloropropane U 0.161 1.00 1 06/19/2023 12:56 WG2080288 Di-isopropyl ether U 0.105 1.00 1 06/19/2023 12:56 WG2080288 Ethylbenzene 12.5 0.137 1.00 1 06/19/2023 12:56 WG2080288 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/19/2023 12:56 WG2080288 Isopropylbenzene 0.726 J 0.105 1.00 1 06/19/2023 12:56 WG2080288 p-Isopropyltoluene 0.357 J 0.120 1.00 1 06/19/2023 12:56 WG2080288 2-Butanone (MEK)U 1.19 10.0 1 06/19/2023 12:56 WG2080288 Methylene Chloride U 0.430 5.00 1 06/19/2023 12:56 WG2080288 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 06/19/2023 12:56 WG2080288 Methyl tert-butyl ether U 0.101 1.00 1 06/19/2023 12:56 WG2080288 Naphthalene U 1.00 5.00 1 06/19/2023 12:56 WG2080288 n-Propylbenzene 2.23 0.0993 1.00 1 06/19/2023 12:56 WG2080288 Styrene U 0.118 1.00 1 06/19/2023 12:56 WG2080288 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/19/2023 12:56 WG2080288 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/19/2023 12:56 WG2080288 Tetrachloroethene 0.385 J 0.300 1.00 1 06/19/2023 12:56 WG2080288 Toluene 13.9 0.278 1.00 1 06/19/2023 12:56 WG2080288 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/19/2023 12:56 WG2080288 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/19/2023 12:56 WG2080288 1,1,1-Trichloroethane U 0.149 1.00 1 06/19/2023 12:56 WG2080288 1,1,2-Trichloroethane U 0.158 1.00 1 06/19/2023 12:56 WG2080288 Trichloroethene U 0.190 1.00 1 06/19/2023 12:56 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 11 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 11 of 36 SAMPLE RESULTS - 04 L1625719 MW-4 Collected date/time: 06/12/23 13:00 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/19/2023 12:56 WG2080288 1,2,3-Trichloropropane U 0.237 2.50 1 06/19/2023 12:56 WG2080288 1,2,4-Trimethylbenzene 11.2 0.322 1.00 1 06/19/2023 12:56 WG2080288 1,3,5-Trimethylbenzene 8.90 0.104 1.00 1 06/19/2023 12:56 WG2080288 Vinyl chloride U 0.234 1.00 1 06/19/2023 12:56 WG2080288 o-Xylene 32.4 0.174 1.00 1 06/19/2023 12:56 WG2080288 m&p-Xylenes 55.9 0.430 2.00 1 06/19/2023 12:56 WG2080288 (S) Toluene-d8 104 80.0-120 06/19/2023 12:56 WG2080288 (S) 4-Bromofluorobenzene 102 77.0-126 06/19/2023 12:56 WG2080288 (S) 1,2-Dichloroethane-d4 95.1 70.0-130 06/19/2023 12:56 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 12 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 12 of 36 SAMPLE RESULTS - 05 L1625719 MW-1D Collected date/time: 06/12/23 11:00 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone 2600 56.5 250 5 06/21/2023 21:10 WG2081917 Acrolein U 2.54 50.0 1 06/19/2023 13:17 WG2080288 Acrylonitrile U 0.671 10.0 1 06/19/2023 13:17 WG2080288 Benzene 0.155 J 0.0941 1.00 1 06/19/2023 13:17 WG2080288 Bromobenzene U 0.118 1.00 1 06/19/2023 13:17 WG2080288 Bromodichloromethane U 0.136 1.00 1 06/19/2023 13:17 WG2080288 Bromoform U 0.129 1.00 1 06/19/2023 13:17 WG2080288 Bromomethane U 0.605 5.00 1 06/19/2023 13:17 WG2080288 n-Butylbenzene U 0.157 1.00 1 06/19/2023 13:17 WG2080288 sec-Butylbenzene U 0.125 1.00 1 06/19/2023 13:17 WG2080288 tert-Butylbenzene U 0.127 1.00 1 06/19/2023 13:17 WG2080288 Carbon tetrachloride U 0.128 1.00 1 06/19/2023 13:17 WG2080288 Chlorobenzene U 0.116 1.00 1 06/19/2023 13:17 WG2080288 Chlorodibromomethane U 0.140 1.00 1 06/19/2023 13:17 WG2080288 Chloroethane 0.215 J 0.192 5.00 1 06/19/2023 13:17 WG2080288 Chloroform 0.206 J 0.111 5.00 1 06/19/2023 13:17 WG2080288 Chloromethane U 0.960 2.50 1 06/19/2023 13:17 WG2080288 2-Chlorotoluene U 0.106 1.00 1 06/19/2023 13:17 WG2080288 4-Chlorotoluene U 0.114 1.00 1 06/19/2023 13:17 WG2080288 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/19/2023 13:17 WG2080288 1,2-Dibromoethane U 0.126 1.00 1 06/19/2023 13:17 WG2080288 Dibromomethane U 0.122 1.00 1 06/19/2023 13:17 WG2080288 1,2-Dichlorobenzene U 0.107 1.00 1 06/19/2023 13:17 WG2080288 1,3-Dichlorobenzene U 0.110 1.00 1 06/19/2023 13:17 WG2080288 1,4-Dichlorobenzene U 0.120 1.00 1 06/19/2023 13:17 WG2080288 Dichlorodifluoromethane U 0.374 5.00 1 06/19/2023 13:17 WG2080288 1,1-Dichloroethane U 0.100 1.00 1 06/19/2023 13:17 WG2080288 1,2-Dichloroethane U 0.0819 1.00 1 06/19/2023 13:17 WG2080288 1,1-Dichloroethene U 0.188 1.00 1 06/19/2023 13:17 WG2080288 cis-1,2-Dichloroethene U 0.126 1.00 1 06/19/2023 13:17 WG2080288 trans-1,2-Dichloroethene U 0.149 1.00 1 06/19/2023 13:17 WG2080288 1,2-Dichloropropane U 0.149 1.00 1 06/19/2023 13:17 WG2080288 1,1-Dichloropropene U 0.142 1.00 1 06/19/2023 13:17 WG2080288 1,3-Dichloropropane U 0.110 1.00 1 06/19/2023 13:17 WG2080288 2,2-Dichloropropane U 0.161 1.00 1 06/19/2023 13:17 WG2080288 Di-isopropyl ether U 0.105 1.00 1 06/19/2023 13:17 WG2080288 Ethylbenzene 0.321 J 0.137 1.00 1 06/19/2023 13:17 WG2080288 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/19/2023 13:17 WG2080288 Isopropylbenzene 0.125 J 0.105 1.00 1 06/19/2023 13:17 WG2080288 p-Isopropyltoluene U 0.120 1.00 1 06/19/2023 13:17 WG2080288 2-Butanone (MEK)7.66 J 1.19 10.0 1 06/19/2023 13:17 WG2080288 Methylene Chloride U 0.430 5.00 1 06/19/2023 13:17 WG2080288 4-Methyl-2-pentanone (MIBK)0.872 J 0.478 10.0 1 06/19/2023 13:17 WG2080288 Methyl tert-butyl ether U 0.101 1.00 1 06/19/2023 13:17 WG2080288 Naphthalene U 1.00 5.00 1 06/19/2023 13:17 WG2080288 n-Propylbenzene 0.193 J 0.0993 1.00 1 06/19/2023 13:17 WG2080288 Styrene U 0.118 1.00 1 06/19/2023 13:17 WG2080288 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/19/2023 13:17 WG2080288 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/19/2023 13:17 WG2080288 Tetrachloroethene U 0.300 1.00 1 06/19/2023 13:17 WG2080288 Toluene U 0.278 1.00 1 06/19/2023 13:17 WG2080288 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/19/2023 13:17 WG2080288 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/19/2023 13:17 WG2080288 1,1,1-Trichloroethane U 0.149 1.00 1 06/19/2023 13:17 WG2080288 1,1,2-Trichloroethane U 0.158 1.00 1 06/19/2023 13:17 WG2080288 Trichloroethene U 0.190 1.00 1 06/19/2023 13:17 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 13 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 13 of 36 SAMPLE RESULTS - 05 L1625719 MW-1D Collected date/time: 06/12/23 11:00 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/19/2023 13:17 WG2080288 1,2,3-Trichloropropane U 0.237 2.50 1 06/19/2023 13:17 WG2080288 1,2,4-Trimethylbenzene 0.663 J 0.322 1.00 1 06/19/2023 13:17 WG2080288 1,3,5-Trimethylbenzene 1.24 0.104 1.00 1 06/19/2023 13:17 WG2080288 Vinyl chloride U 0.234 1.00 1 06/19/2023 13:17 WG2080288 o-Xylene 1.61 0.174 1.00 1 06/19/2023 13:17 WG2080288 m&p-Xylenes 0.678 J 0.430 2.00 1 06/19/2023 13:17 WG2080288 (S) Toluene-d8 104 80.0-120 06/19/2023 13:17 WG2080288 (S) Toluene-d8 116 80.0-120 06/21/2023 21:10 WG2081917 (S) 4-Bromofluorobenzene 104 77.0-126 06/19/2023 13:17 WG2080288 (S) 4-Bromofluorobenzene 92.4 77.0-126 06/21/2023 21:10 WG2081917 (S) 1,2-Dichloroethane-d4 94.5 70.0-130 06/19/2023 13:17 WG2080288 (S) 1,2-Dichloroethane-d4 118 70.0-130 06/21/2023 21:10 WG2081917 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 14 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 14 of 36 SAMPLE RESULTS - 06 L1625719 FB-1 Collected date/time: 06/12/23 13:10 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 06/21/2023 17:03 WG2081917 Acrolein U 2.54 50.0 1 06/21/2023 17:03 WG2081917 Acrylonitrile U 0.671 10.0 1 06/21/2023 17:03 WG2081917 Benzene U 0.0941 1.00 1 06/21/2023 17:03 WG2081917 Bromobenzene U 0.118 1.00 1 06/21/2023 17:03 WG2081917 Bromodichloromethane U 0.136 1.00 1 06/21/2023 17:03 WG2081917 Bromoform U 0.129 1.00 1 06/21/2023 17:03 WG2081917 Bromomethane U 0.605 5.00 1 06/21/2023 17:03 WG2081917 n-Butylbenzene U 0.157 1.00 1 06/21/2023 17:03 WG2081917 sec-Butylbenzene U 0.125 1.00 1 06/21/2023 17:03 WG2081917 tert-Butylbenzene U 0.127 1.00 1 06/21/2023 17:03 WG2081917 Carbon tetrachloride U 0.128 1.00 1 06/21/2023 17:03 WG2081917 Chlorobenzene U 0.116 1.00 1 06/21/2023 17:03 WG2081917 Chlorodibromomethane U 0.140 1.00 1 06/21/2023 17:03 WG2081917 Chloroethane U 0.192 5.00 1 06/21/2023 17:03 WG2081917 Chloroform U 0.111 5.00 1 06/21/2023 17:03 WG2081917 Chloromethane U 0.960 2.50 1 06/21/2023 17:03 WG2081917 2-Chlorotoluene U 0.106 1.00 1 06/21/2023 17:03 WG2081917 4-Chlorotoluene U 0.114 1.00 1 06/21/2023 17:03 WG2081917 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/21/2023 17:03 WG2081917 1,2-Dibromoethane U 0.126 1.00 1 06/21/2023 17:03 WG2081917 Dibromomethane U 0.122 1.00 1 06/21/2023 17:03 WG2081917 1,2-Dichlorobenzene U 0.107 1.00 1 06/21/2023 17:03 WG2081917 1,3-Dichlorobenzene U 0.110 1.00 1 06/21/2023 17:03 WG2081917 1,4-Dichlorobenzene U 0.120 1.00 1 06/21/2023 17:03 WG2081917 Dichlorodifluoromethane U 0.374 5.00 1 06/21/2023 17:03 WG2081917 1,1-Dichloroethane U J4 0.100 1.00 1 06/21/2023 17:03 WG2081917 1,2-Dichloroethane U 0.0819 1.00 1 06/21/2023 17:03 WG2081917 1,1-Dichloroethene U 0.188 1.00 1 06/21/2023 17:03 WG2081917 cis-1,2-Dichloroethene U 0.126 1.00 1 06/21/2023 17:03 WG2081917 trans-1,2-Dichloroethene U 0.149 1.00 1 06/21/2023 17:03 WG2081917 1,2-Dichloropropane U J4 0.149 1.00 1 06/21/2023 17:03 WG2081917 1,1-Dichloropropene U 0.142 1.00 1 06/21/2023 17:03 WG2081917 1,3-Dichloropropane U 0.110 1.00 1 06/21/2023 17:03 WG2081917 2,2-Dichloropropane U 0.161 1.00 1 06/21/2023 17:03 WG2081917 Di-isopropyl ether U 0.105 1.00 1 06/21/2023 17:03 WG2081917 Ethylbenzene U 0.137 1.00 1 06/21/2023 17:03 WG2081917 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/21/2023 17:03 WG2081917 Isopropylbenzene U 0.105 1.00 1 06/21/2023 17:03 WG2081917 p-Isopropyltoluene U 0.120 1.00 1 06/21/2023 17:03 WG2081917 2-Butanone (MEK)3.14 J 1.19 10.0 1 06/21/2023 17:03 WG2081917 Methylene Chloride 0.655 J 0.430 5.00 1 06/21/2023 17:03 WG2081917 4-Methyl-2-pentanone (MIBK)U J4 0.478 10.0 1 06/21/2023 17:03 WG2081917 Methyl tert-butyl ether U 0.101 1.00 1 06/21/2023 17:03 WG2081917 Naphthalene U 1.00 5.00 1 06/21/2023 17:03 WG2081917 n-Propylbenzene U 0.0993 1.00 1 06/21/2023 17:03 WG2081917 Styrene U 0.118 1.00 1 06/21/2023 17:03 WG2081917 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/21/2023 17:03 WG2081917 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/21/2023 17:03 WG2081917 Tetrachloroethene U 0.300 1.00 1 06/21/2023 17:03 WG2081917 Toluene U 0.278 1.00 1 06/21/2023 17:03 WG2081917 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/21/2023 17:03 WG2081917 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/21/2023 17:03 WG2081917 1,1,1-Trichloroethane U 0.149 1.00 1 06/21/2023 17:03 WG2081917 1,1,2-Trichloroethane U 0.158 1.00 1 06/21/2023 17:03 WG2081917 Trichloroethene U 0.190 1.00 1 06/21/2023 17:03 WG2081917 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 15 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 15 of 36 SAMPLE RESULTS - 06 L1625719 FB-1 Collected date/time: 06/12/23 13:10 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/21/2023 17:03 WG2081917 1,2,3-Trichloropropane U 0.237 2.50 1 06/21/2023 17:03 WG2081917 1,2,4-Trimethylbenzene U 0.322 1.00 1 06/21/2023 17:03 WG2081917 1,3,5-Trimethylbenzene U 0.104 1.00 1 06/21/2023 17:03 WG2081917 Vinyl chloride U 0.234 1.00 1 06/21/2023 17:03 WG2081917 o-Xylene U 0.174 1.00 1 06/21/2023 17:03 WG2081917 m&p-Xylenes U 0.430 2.00 1 06/21/2023 17:03 WG2081917 (S) Toluene-d8 118 80.0-120 06/21/2023 17:03 WG2081917 (S) 4-Bromofluorobenzene 91.4 77.0-126 06/21/2023 17:03 WG2081917 (S) 1,2-Dichloroethane-d4 125 70.0-130 06/21/2023 17:03 WG2081917 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 16 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 16 of 36 SAMPLE RESULTS - 07 L1625719 WSW-2 Collected date/time: 06/12/23 13:30 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 06/19/2023 13:37 WG2080288 Acrolein U 2.54 50.0 1 06/19/2023 13:37 WG2080288 Acrylonitrile U 0.671 10.0 1 06/19/2023 13:37 WG2080288 Benzene U 0.0941 1.00 1 06/19/2023 13:37 WG2080288 Bromobenzene U 0.118 1.00 1 06/19/2023 13:37 WG2080288 Bromodichloromethane U 0.136 1.00 1 06/19/2023 13:37 WG2080288 Bromoform U 0.129 1.00 1 06/19/2023 13:37 WG2080288 Bromomethane U 0.605 5.00 1 06/19/2023 13:37 WG2080288 n-Butylbenzene U 0.157 1.00 1 06/19/2023 13:37 WG2080288 sec-Butylbenzene U 0.125 1.00 1 06/19/2023 13:37 WG2080288 tert-Butylbenzene U 0.127 1.00 1 06/19/2023 13:37 WG2080288 Carbon tetrachloride U 0.128 1.00 1 06/19/2023 13:37 WG2080288 Chlorobenzene U 0.116 1.00 1 06/19/2023 13:37 WG2080288 Chlorodibromomethane U 0.140 1.00 1 06/19/2023 13:37 WG2080288 Chloroethane U 0.192 5.00 1 06/19/2023 13:37 WG2080288 Chloroform U 0.111 5.00 1 06/19/2023 13:37 WG2080288 Chloromethane U 0.960 2.50 1 06/19/2023 13:37 WG2080288 2-Chlorotoluene U 0.106 1.00 1 06/19/2023 13:37 WG2080288 4-Chlorotoluene U 0.114 1.00 1 06/19/2023 13:37 WG2080288 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/19/2023 13:37 WG2080288 1,2-Dibromoethane U 0.126 1.00 1 06/19/2023 13:37 WG2080288 Dibromomethane U 0.122 1.00 1 06/19/2023 13:37 WG2080288 1,2-Dichlorobenzene U 0.107 1.00 1 06/19/2023 13:37 WG2080288 1,3-Dichlorobenzene U 0.110 1.00 1 06/19/2023 13:37 WG2080288 1,4-Dichlorobenzene U 0.120 1.00 1 06/19/2023 13:37 WG2080288 Dichlorodifluoromethane U 0.374 5.00 1 06/19/2023 13:37 WG2080288 1,1-Dichloroethane U 0.100 1.00 1 06/19/2023 13:37 WG2080288 1,2-Dichloroethane 0.194 J 0.0819 1.00 1 06/19/2023 13:37 WG2080288 1,1-Dichloroethene U 0.188 1.00 1 06/19/2023 13:37 WG2080288 cis-1,2-Dichloroethene U 0.126 1.00 1 06/19/2023 13:37 WG2080288 trans-1,2-Dichloroethene U 0.149 1.00 1 06/19/2023 13:37 WG2080288 1,2-Dichloropropane U 0.149 1.00 1 06/19/2023 13:37 WG2080288 1,1-Dichloropropene U 0.142 1.00 1 06/19/2023 13:37 WG2080288 1,3-Dichloropropane U 0.110 1.00 1 06/19/2023 13:37 WG2080288 2,2-Dichloropropane U 0.161 1.00 1 06/19/2023 13:37 WG2080288 Di-isopropyl ether U 0.105 1.00 1 06/19/2023 13:37 WG2080288 Ethylbenzene U 0.137 1.00 1 06/19/2023 13:37 WG2080288 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/19/2023 13:37 WG2080288 Isopropylbenzene U 0.105 1.00 1 06/19/2023 13:37 WG2080288 p-Isopropyltoluene U 0.120 1.00 1 06/19/2023 13:37 WG2080288 2-Butanone (MEK)U 1.19 10.0 1 06/19/2023 13:37 WG2080288 Methylene Chloride U 0.430 5.00 1 06/19/2023 13:37 WG2080288 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 06/19/2023 13:37 WG2080288 Methyl tert-butyl ether U 0.101 1.00 1 06/19/2023 13:37 WG2080288 Naphthalene U 1.00 5.00 1 06/19/2023 13:37 WG2080288 n-Propylbenzene U 0.0993 1.00 1 06/19/2023 13:37 WG2080288 Styrene U 0.118 1.00 1 06/19/2023 13:37 WG2080288 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/19/2023 13:37 WG2080288 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/19/2023 13:37 WG2080288 Tetrachloroethene U 0.300 1.00 1 06/19/2023 13:37 WG2080288 Toluene U 0.278 1.00 1 06/19/2023 13:37 WG2080288 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/19/2023 13:37 WG2080288 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/19/2023 13:37 WG2080288 1,1,1-Trichloroethane U 0.149 1.00 1 06/19/2023 13:37 WG2080288 1,1,2-Trichloroethane U 0.158 1.00 1 06/19/2023 13:37 WG2080288 Trichloroethene U 0.190 1.00 1 06/19/2023 13:37 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 17 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 17 of 36 SAMPLE RESULTS - 07 L1625719 WSW-2 Collected date/time: 06/12/23 13:30 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/19/2023 13:37 WG2080288 1,2,3-Trichloropropane U 0.237 2.50 1 06/19/2023 13:37 WG2080288 1,2,4-Trimethylbenzene U 0.322 1.00 1 06/19/2023 13:37 WG2080288 1,3,5-Trimethylbenzene U 0.104 1.00 1 06/19/2023 13:37 WG2080288 Vinyl chloride U 0.234 1.00 1 06/19/2023 13:37 WG2080288 o-Xylene U 0.174 1.00 1 06/19/2023 13:37 WG2080288 m&p-Xylenes U 0.430 2.00 1 06/19/2023 13:37 WG2080288 (S) Toluene-d8 106 80.0-120 06/19/2023 13:37 WG2080288 (S) 4-Bromofluorobenzene 102 77.0-126 06/19/2023 13:37 WG2080288 (S) 1,2-Dichloroethane-d4 93.6 70.0-130 06/19/2023 13:37 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 18 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 18 of 36 SAMPLE RESULTS - 08 L1625719 WSW-3 Collected date/time: 06/12/23 13:50 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 06/19/2023 13:58 WG2080288 Acrolein U 2.54 50.0 1 06/19/2023 13:58 WG2080288 Acrylonitrile U 0.671 10.0 1 06/19/2023 13:58 WG2080288 Benzene U 0.0941 1.00 1 06/19/2023 13:58 WG2080288 Bromobenzene U 0.118 1.00 1 06/19/2023 13:58 WG2080288 Bromodichloromethane U 0.136 1.00 1 06/19/2023 13:58 WG2080288 Bromoform U 0.129 1.00 1 06/19/2023 13:58 WG2080288 Bromomethane U 0.605 5.00 1 06/19/2023 13:58 WG2080288 n-Butylbenzene U 0.157 1.00 1 06/19/2023 13:58 WG2080288 sec-Butylbenzene U 0.125 1.00 1 06/19/2023 13:58 WG2080288 tert-Butylbenzene U 0.127 1.00 1 06/19/2023 13:58 WG2080288 Carbon tetrachloride U 0.128 1.00 1 06/19/2023 13:58 WG2080288 Chlorobenzene U 0.116 1.00 1 06/19/2023 13:58 WG2080288 Chlorodibromomethane U 0.140 1.00 1 06/19/2023 13:58 WG2080288 Chloroethane U 0.192 5.00 1 06/19/2023 13:58 WG2080288 Chloroform U 0.111 5.00 1 06/19/2023 13:58 WG2080288 Chloromethane U 0.960 2.50 1 06/19/2023 13:58 WG2080288 2-Chlorotoluene U 0.106 1.00 1 06/19/2023 13:58 WG2080288 4-Chlorotoluene U 0.114 1.00 1 06/19/2023 13:58 WG2080288 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 06/19/2023 13:58 WG2080288 1,2-Dibromoethane U 0.126 1.00 1 06/19/2023 13:58 WG2080288 Dibromomethane U 0.122 1.00 1 06/19/2023 13:58 WG2080288 1,2-Dichlorobenzene U 0.107 1.00 1 06/19/2023 13:58 WG2080288 1,3-Dichlorobenzene U 0.110 1.00 1 06/19/2023 13:58 WG2080288 1,4-Dichlorobenzene U 0.120 1.00 1 06/19/2023 13:58 WG2080288 Dichlorodifluoromethane U 0.374 5.00 1 06/19/2023 13:58 WG2080288 1,1-Dichloroethane U 0.100 1.00 1 06/19/2023 13:58 WG2080288 1,2-Dichloroethane 0.238 J 0.0819 1.00 1 06/19/2023 13:58 WG2080288 1,1-Dichloroethene U 0.188 1.00 1 06/19/2023 13:58 WG2080288 cis-1,2-Dichloroethene U 0.126 1.00 1 06/19/2023 13:58 WG2080288 trans-1,2-Dichloroethene U 0.149 1.00 1 06/19/2023 13:58 WG2080288 1,2-Dichloropropane U 0.149 1.00 1 06/19/2023 13:58 WG2080288 1,1-Dichloropropene U 0.142 1.00 1 06/19/2023 13:58 WG2080288 1,3-Dichloropropane U 0.110 1.00 1 06/19/2023 13:58 WG2080288 2,2-Dichloropropane U 0.161 1.00 1 06/19/2023 13:58 WG2080288 Di-isopropyl ether U 0.105 1.00 1 06/19/2023 13:58 WG2080288 Ethylbenzene U 0.137 1.00 1 06/19/2023 13:58 WG2080288 Hexachloro-1,3-butadiene U 0.337 1.00 1 06/19/2023 13:58 WG2080288 Isopropylbenzene U 0.105 1.00 1 06/19/2023 13:58 WG2080288 p-Isopropyltoluene U 0.120 1.00 1 06/19/2023 13:58 WG2080288 2-Butanone (MEK)U 1.19 10.0 1 06/19/2023 13:58 WG2080288 Methylene Chloride U 0.430 5.00 1 06/19/2023 13:58 WG2080288 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 06/19/2023 13:58 WG2080288 Methyl tert-butyl ether U 0.101 1.00 1 06/19/2023 13:58 WG2080288 Naphthalene U 1.00 5.00 1 06/19/2023 13:58 WG2080288 n-Propylbenzene U 0.0993 1.00 1 06/19/2023 13:58 WG2080288 Styrene U 0.118 1.00 1 06/19/2023 13:58 WG2080288 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 06/19/2023 13:58 WG2080288 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/19/2023 13:58 WG2080288 Tetrachloroethene 1.92 0.300 1.00 1 06/19/2023 13:58 WG2080288 Toluene U 0.278 1.00 1 06/19/2023 13:58 WG2080288 1,2,3-Trichlorobenzene U 0.230 1.00 1 06/19/2023 13:58 WG2080288 1,2,4-Trichlorobenzene U 0.481 1.00 1 06/19/2023 13:58 WG2080288 1,1,1-Trichloroethane U 0.149 1.00 1 06/19/2023 13:58 WG2080288 1,1,2-Trichloroethane U 0.158 1.00 1 06/19/2023 13:58 WG2080288 Trichloroethene U 0.190 1.00 1 06/19/2023 13:58 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 19 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 19 of 36 SAMPLE RESULTS - 08 L1625719 WSW-3 Collected date/time: 06/12/23 13:50 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Trichlorofluoromethane U 0.160 5.00 1 06/19/2023 13:58 WG2080288 1,2,3-Trichloropropane U 0.237 2.50 1 06/19/2023 13:58 WG2080288 1,2,4-Trimethylbenzene U 0.322 1.00 1 06/19/2023 13:58 WG2080288 1,3,5-Trimethylbenzene U 0.104 1.00 1 06/19/2023 13:58 WG2080288 Vinyl chloride U 0.234 1.00 1 06/19/2023 13:58 WG2080288 o-Xylene U 0.174 1.00 1 06/19/2023 13:58 WG2080288 m&p-Xylenes U 0.430 2.00 1 06/19/2023 13:58 WG2080288 (S) Toluene-d8 107 80.0-120 06/19/2023 13:58 WG2080288 (S) 4-Bromofluorobenzene 101 77.0-126 06/19/2023 13:58 WG2080288 (S) 1,2-Dichloroethane-d4 88.4 70.0-130 06/19/2023 13:58 WG2080288 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 20 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 20 of 36 QUALITY CONTROL SUMMARYWG2079572 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-01 Method Blank (MB) (MB) R3938782-2 06/17/23 09:39 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acetone U 11.3 50.0 Acrolein U 2.54 50.0 Acrylonitrile U 0.671 10.0 Bromobenzene U 0.118 1.00 Bromodichloromethane U 0.136 1.00 Bromoform U 0.129 1.00 Bromomethane U 0.605 5.00 n-Butylbenzene U 0.157 1.00 sec-Butylbenzene U 0.125 1.00 tert-Butylbenzene U 0.127 1.00 Carbon tetrachloride U 0.128 1.00 Chlorobenzene U 0.116 1.00 Chlorodibromomethane U 0.140 1.00 Chloroethane U 0.192 5.00 Chloroform U 0.111 5.00 Chloromethane U 0.960 2.50 2-Chlorotoluene U 0.106 1.00 4-Chlorotoluene U 0.114 1.00 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1,2-Dibromoethane U 0.126 1.00 Dibromomethane U 0.122 1.00 1,2-Dichlorobenzene U 0.107 1.00 1,3-Dichlorobenzene U 0.110 1.00 1,4-Dichlorobenzene U 0.120 1.00 Dichlorodifluoromethane U 0.374 5.00 1,1-Dichloroethane U 0.100 1.00 1,2-Dichloroethane U 0.0819 1.00 1,1-Dichloroethene U 0.188 1.00 cis-1,2-Dichloroethene U 0.126 1.00 trans-1,2-Dichloroethene U 0.149 1.00 1,2-Dichloropropane U 0.149 1.00 1,1-Dichloropropene U 0.142 1.00 1,3-Dichloropropane U 0.110 1.00 2,2-Dichloropropane U 0.161 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 Hexachloro-1,3-butadiene U 0.337 1.00 Isopropylbenzene U 0.105 1.00 p-Isopropyltoluene U 0.120 1.00 2-Butanone (MEK)U 1.19 10.0 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 21 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 21 of 36 QUALITY CONTROL SUMMARYWG2079572 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-01 Method Blank (MB) (MB) R3938782-2 06/17/23 09:39 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Methylene Chloride U 0.430 5.00 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 Methyl tert-butyl ether U 0.101 1.00 Naphthalene U 1.00 5.00 n-Propylbenzene U 0.0993 1.00 Styrene U 0.118 1.00 1,1,1,2-Tetrachloroethane U 0.147 1.00 1,1,2,2-Tetrachloroethane U 0.133 1.00 Tetrachloroethene U 0.300 1.00 Toluene U 0.278 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 1,2,4-Trichlorobenzene U 0.481 1.00 1,1,1-Trichloroethane U 0.149 1.00 1,1,2-Trichloroethane U 0.158 1.00 Trichloroethene U 0.190 1.00 Trichlorofluoromethane U 0.160 5.00 1,2,3-Trichloropropane U 0.237 2.50 1,2,4-Trimethylbenzene U 0.322 1.00 1,3,5-Trimethylbenzene U 0.104 1.00 Vinyl chloride U 0.234 1.00 (S) Toluene-d8 110 80.0-120 (S) 4-Bromofluorobenzene 103 77.0-126 (S) 1,2-Dichloroethane-d4 102 70.0-130 Laboratory Control Sample (LCS) (LCS) R3938782-1 06/17/23 08:56 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acetone 25.0 29.4 118 19.0-160 Acrolein 25.0 24.1 96.4 10.0-160 Acrylonitrile 25.0 24.2 96.8 55.0-149 Bromobenzene 5.00 4.77 95.4 73.0-121 Bromodichloromethane 5.00 5.14 103 75.0-120 Bromoform 5.00 4.59 91.8 68.0-132 Bromomethane 5.00 3.79 75.8 10.0-160 n-Butylbenzene 5.00 4.71 94.2 73.0-125 sec-Butylbenzene 5.00 5.12 102 75.0-125 tert-Butylbenzene 5.00 5.22 104 76.0-124 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 22 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 22 of 36 QUALITY CONTROL SUMMARYWG2079572 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-01 Laboratory Control Sample (LCS) (LCS) R3938782-1 06/17/23 08:56 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Carbon tetrachloride 5.00 5.45 109 68.0-126 Chlorobenzene 5.00 5.03 101 80.0-121 Chlorodibromomethane 5.00 4.51 90.2 77.0-125 Chloroethane 5.00 5.17 103 47.0-150 Chloroform 5.00 5.02 100 73.0-120 Chloromethane 5.00 5.12 102 41.0-142 2-Chlorotoluene 5.00 4.79 95.8 76.0-123 4-Chlorotoluene 5.00 4.77 95.4 75.0-122 1,2-Dibromo-3-Chloropropane 5.00 4.43 88.6 58.0-134 1,2-Dibromoethane 5.00 4.96 99.2 80.0-122 Dibromomethane 5.00 5.15 103 80.0-120 1,2-Dichlorobenzene 5.00 4.92 98.4 79.0-121 1,3-Dichlorobenzene 5.00 4.68 93.6 79.0-120 1,4-Dichlorobenzene 5.00 4.58 91.6 79.0-120 Dichlorodifluoromethane 5.00 5.66 113 51.0-149 1,1-Dichloroethane 5.00 5.15 103 70.0-126 1,2-Dichloroethane 5.00 4.93 98.6 70.0-128 1,1-Dichloroethene 5.00 5.52 110 71.0-124 cis-1,2-Dichloroethene 5.00 4.95 99.0 73.0-120 trans-1,2-Dichloroethene 5.00 5.38 108 73.0-120 1,2-Dichloropropane 5.00 4.84 96.8 77.0-125 1,1-Dichloropropene 5.00 5.54 111 74.0-126 1,3-Dichloropropane 5.00 4.94 98.8 80.0-120 2,2-Dichloropropane 5.00 4.89 97.8 58.0-130 Di-isopropyl ether 5.00 5.39 108 58.0-138 Ethylbenzene 5.00 4.90 98.0 79.0-123 Hexachloro-1,3-butadiene 5.00 4.94 98.8 54.0-138 Isopropylbenzene 5.00 5.09 102 76.0-127 p-Isopropyltoluene 5.00 5.27 105 76.0-125 2-Butanone (MEK)25.0 28.3 113 44.0-160 Methylene Chloride 5.00 5.00 100 67.0-120 4-Methyl-2-pentanone (MIBK)25.0 26.5 106 68.0-142 Methyl tert-butyl ether 5.00 5.05 101 68.0-125 Naphthalene 5.00 3.60 72.0 54.0-135 n-Propylbenzene 5.00 5.15 103 77.0-124 Styrene 5.00 4.54 90.8 73.0-130 1,1,1,2-Tetrachloroethane 5.00 4.57 91.4 75.0-125 1,1,2,2-Tetrachloroethane 5.00 4.73 94.6 65.0-130 Tetrachloroethene 5.00 5.18 104 72.0-132 Toluene 5.00 5.04 101 79.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 23 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 23 of 36 QUALITY CONTROL SUMMARYWG2079572 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-01 Laboratory Control Sample (LCS) (LCS) R3938782-1 06/17/23 08:56 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 1,2,3-Trichlorobenzene 5.00 4.51 90.2 50.0-138 1,2,4-Trichlorobenzene 5.00 4.46 89.2 57.0-137 1,1,1-Trichloroethane 5.00 5.28 106 73.0-124 1,1,2-Trichloroethane 5.00 5.09 102 80.0-120 Trichloroethene 5.00 5.50 110 78.0-124 Trichlorofluoromethane 5.00 5.54 111 59.0-147 1,2,3-Trichloropropane 5.00 5.37 107 73.0-130 1,2,4-Trimethylbenzene 5.00 5.06 101 76.0-121 1,3,5-Trimethylbenzene 5.00 4.96 99.2 76.0-122 Vinyl chloride 5.00 5.45 109 67.0-131 (S) Toluene-d8 108 80.0-120 (S) 4-Bromofluorobenzene 104 77.0-126 (S) 1,2-Dichloroethane-d4 103 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 24 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 24 of 36 QUALITY CONTROL SUMMARYWG2080288 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,04,05,07,08 Method Blank (MB) (MB) R3939394-3 06/19/23 10:48 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acetone U 11.3 50.0 Acrolein U 2.54 50.0 Acrylonitrile U 0.671 10.0 Benzene U 0.0941 1.00 Bromobenzene U 0.118 1.00 Bromodichloromethane U 0.136 1.00 Bromoform U 0.129 1.00 Bromomethane U 0.605 5.00 n-Butylbenzene U 0.157 1.00 sec-Butylbenzene U 0.125 1.00 tert-Butylbenzene U 0.127 1.00 Carbon tetrachloride U 0.128 1.00 Chlorobenzene U 0.116 1.00 Chlorodibromomethane U 0.140 1.00 Chloroethane U 0.192 5.00 Chloroform U 0.111 5.00 Chloromethane U 0.960 2.50 2-Chlorotoluene U 0.106 1.00 4-Chlorotoluene U 0.114 1.00 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1,2-Dibromoethane U 0.126 1.00 Dibromomethane U 0.122 1.00 1,2-Dichlorobenzene U 0.107 1.00 1,3-Dichlorobenzene U 0.110 1.00 1,4-Dichlorobenzene U 0.120 1.00 Dichlorodifluoromethane U 0.374 5.00 1,1-Dichloroethane U 0.100 1.00 1,2-Dichloroethane U 0.0819 1.00 1,1-Dichloroethene U 0.188 1.00 cis-1,2-Dichloroethene U 0.126 1.00 trans-1,2-Dichloroethene U 0.149 1.00 1,2-Dichloropropane U 0.149 1.00 1,1-Dichloropropene U 0.142 1.00 1,3-Dichloropropane U 0.110 1.00 2,2-Dichloropropane U 0.161 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 Hexachloro-1,3-butadiene U 0.337 1.00 Isopropylbenzene U 0.105 1.00 p-Isopropyltoluene U 0.120 1.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 25 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 25 of 36 QUALITY CONTROL SUMMARYWG2080288 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,04,05,07,08 Method Blank (MB) (MB) R3939394-3 06/19/23 10:48 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l 2-Butanone (MEK)U 1.19 10.0 Methylene Chloride U 0.430 5.00 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 Methyl tert-butyl ether U 0.101 1.00 Naphthalene U 1.00 5.00 n-Propylbenzene U 0.0993 1.00 Styrene U 0.118 1.00 1,1,1,2-Tetrachloroethane U 0.147 1.00 1,1,2,2-Tetrachloroethane U 0.133 1.00 Tetrachloroethene U 0.300 1.00 Toluene U 0.278 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 1,2,4-Trichlorobenzene U 0.481 1.00 1,1,1-Trichloroethane U 0.149 1.00 1,1,2-Trichloroethane U 0.158 1.00 Trichloroethene U 0.190 1.00 Trichlorofluoromethane U 0.160 5.00 1,2,3-Trichloropropane U 0.237 2.50 1,2,4-Trimethylbenzene U 0.322 1.00 1,3,5-Trimethylbenzene U 0.104 1.00 Vinyl chloride U 0.234 1.00 o-Xylene U 0.174 1.00 m&p-Xylenes U 0.430 2.00 (S) Toluene-d8 106 80.0-120 (S) 4-Bromofluorobenzene 99.4 77.0-126 (S) 1,2-Dichloroethane-d4 91.6 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3939394-1 06/19/23 09:47 • (LCSD) R3939394-2 06/19/23 10:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Acetone 25.0 23.2 22.7 92.8 90.8 19.0-160 2.18 27 Acrolein 25.0 21.8 21.5 87.2 86.0 10.0-160 1.39 26 Acrylonitrile 25.0 23.3 22.6 93.2 90.4 55.0-149 3.05 20 Benzene 5.00 4.92 4.86 98.4 97.2 70.0-123 1.23 20 Bromobenzene 5.00 5.30 4.90 106 98.0 73.0-121 7.84 20 Bromodichloromethane 5.00 5.10 5.00 102 100 75.0-120 1.98 20 Bromoform 5.00 5.40 4.91 108 98.2 68.0-132 9.51 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 26 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 26 of 36 QUALITY CONTROL SUMMARYWG2080288 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,04,05,07,08 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3939394-1 06/19/23 09:47 • (LCSD) R3939394-2 06/19/23 10:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Bromomethane 5.00 5.08 4.92 102 98.4 10.0-160 3.20 25 n-Butylbenzene 5.00 5.50 5.27 110 105 73.0-125 4.27 20 sec-Butylbenzene 5.00 5.38 5.27 108 105 75.0-125 2.07 20 tert-Butylbenzene 5.00 5.40 5.36 108 107 76.0-124 0.744 20 Carbon tetrachloride 5.00 5.29 5.33 106 107 68.0-126 0.753 20 Chlorobenzene 5.00 5.32 5.29 106 106 80.0-121 0.566 20 Chlorodibromomethane 5.00 5.34 5.21 107 104 77.0-125 2.46 20 Chloroethane 5.00 6.35 6.06 127 121 47.0-150 4.67 20 Chloroform 5.00 4.94 5.07 98.8 101 73.0-120 2.60 20 Chloromethane 5.00 3.97 3.94 79.4 78.8 41.0-142 0.759 20 2-Chlorotoluene 5.00 5.03 5.04 101 101 76.0-123 0.199 20 4-Chlorotoluene 5.00 4.99 5.19 99.8 104 75.0-122 3.93 20 1,2-Dibromo-3-Chloropropane 5.00 5.39 5.07 108 101 58.0-134 6.12 20 1,2-Dibromoethane 5.00 5.39 5.37 108 107 80.0-122 0.372 20 Dibromomethane 5.00 5.23 4.99 105 99.8 80.0-120 4.70 20 1,2-Dichlorobenzene 5.00 5.58 5.51 112 110 79.0-121 1.26 20 1,3-Dichlorobenzene 5.00 5.33 5.27 107 105 79.0-120 1.13 20 1,4-Dichlorobenzene 5.00 5.07 4.94 101 98.8 79.0-120 2.60 20 Dichlorodifluoromethane 5.00 5.84 5.39 117 108 51.0-149 8.01 20 1,1-Dichloroethane 5.00 4.86 4.79 97.2 95.8 70.0-126 1.45 20 1,2-Dichloroethane 5.00 4.76 4.90 95.2 98.0 70.0-128 2.90 20 1,1-Dichloroethene 5.00 5.22 4.95 104 99.0 71.0-124 5.31 20 cis-1,2-Dichloroethene 5.00 5.21 4.89 104 97.8 73.0-120 6.34 20 trans-1,2-Dichloroethene 5.00 4.94 4.88 98.8 97.6 73.0-120 1.22 20 1,2-Dichloropropane 5.00 4.94 5.03 98.8 101 77.0-125 1.81 20 1,1-Dichloropropene 5.00 5.22 4.89 104 97.8 74.0-126 6.53 20 1,3-Dichloropropane 5.00 5.49 5.14 110 103 80.0-120 6.59 20 2,2-Dichloropropane 5.00 5.22 5.18 104 104 58.0-130 0.769 20 Di-isopropyl ether 5.00 4.24 4.27 84.8 85.4 58.0-138 0.705 20 Ethylbenzene 5.00 5.32 5.10 106 102 79.0-123 4.22 20 Hexachloro-1,3-butadiene 5.00 5.44 5.65 109 113 54.0-138 3.79 20 Isopropylbenzene 5.00 5.22 5.22 104 104 76.0-127 0.000 20 p-Isopropyltoluene 5.00 5.09 5.12 102 102 76.0-125 0.588 20 2-Butanone (MEK)25.0 23.8 23.3 95.2 93.2 44.0-160 2.12 20 Methylene Chloride 5.00 4.97 4.80 99.4 96.0 67.0-120 3.48 20 4-Methyl-2-pentanone (MIBK)25.0 25.1 24.2 100 96.8 68.0-142 3.65 20 Methyl tert-butyl ether 5.00 5.13 4.98 103 99.6 68.0-125 2.97 20 Naphthalene 5.00 5.19 5.05 104 101 54.0-135 2.73 20 n-Propylbenzene 5.00 5.35 5.18 107 104 77.0-124 3.23 20 Styrene 5.00 4.89 4.94 97.8 98.8 73.0-130 1.02 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 27 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 27 of 36 QUALITY CONTROL SUMMARYWG2080288 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,04,05,07,08 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3939394-1 06/19/23 09:47 • (LCSD) R3939394-2 06/19/23 10:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% 1,1,1,2-Tetrachloroethane 5.00 5.51 5.26 110 105 75.0-125 4.64 20 1,1,2,2-Tetrachloroethane 5.00 5.49 5.19 110 104 65.0-130 5.62 20 Tetrachloroethene 5.00 5.40 5.26 108 105 72.0-132 2.63 20 Toluene 5.00 5.02 5.09 100 102 79.0-120 1.38 20 1,2,3-Trichlorobenzene 5.00 5.62 5.03 112 101 50.0-138 11.1 20 1,2,4-Trichlorobenzene 5.00 5.99 5.54 120 111 57.0-137 7.81 20 1,1,1-Trichloroethane 5.00 5.05 5.12 101 102 73.0-124 1.38 20 1,1,2-Trichloroethane 5.00 5.52 5.09 110 102 80.0-120 8.11 20 Trichloroethene 5.00 5.15 5.01 103 100 78.0-124 2.76 20 Trichlorofluoromethane 5.00 6.35 6.32 127 126 59.0-147 0.474 20 1,2,3-Trichloropropane 5.00 5.37 5.29 107 106 73.0-130 1.50 20 1,2,4-Trimethylbenzene 5.00 5.06 5.16 101 103 76.0-121 1.96 20 1,3,5-Trimethylbenzene 5.00 5.07 4.93 101 98.6 76.0-122 2.80 20 Vinyl chloride 5.00 6.21 6.16 124 123 67.0-131 0.808 20 o-Xylene 5.00 5.15 4.92 103 98.4 80.0-122 4.57 20 m&p-Xylenes 10.0 10.3 10.0 103 100 80.0-122 2.96 20 (S) Toluene-d8 102 103 80.0-120 (S) 4-Bromofluorobenzene 100 97.6 77.0-126 (S) 1,2-Dichloroethane-d4 89.8 95.8 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 28 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 28 of 36 QUALITY CONTROL SUMMARYWG2081057 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-01 Method Blank (MB) (MB) R3940012-2 06/21/23 07:14 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Benzene U 0.0941 1.00 o-Xylene U 0.174 1.00 m&p-Xylenes U 0.430 2.00 (S) Toluene-d8 104 80.0-120 (S) 4-Bromofluorobenzene 92.8 77.0-126 (S) 1,2-Dichloroethane-d4 107 70.0-130 Laboratory Control Sample (LCS) (LCS) R3940012-1 06/21/23 06:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Benzene 5.00 5.36 107 70.0-123 o-Xylene 5.00 4.78 95.6 80.0-122 m&p-Xylenes 10.0 9.60 96.0 80.0-122 (S) Toluene-d8 103 80.0-120 (S) 4-Bromofluorobenzene 95.3 77.0-126 (S) 1,2-Dichloroethane-d4 109 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 29 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 29 of 36 QUALITY CONTROL SUMMARYWG2081917 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,05,06 Method Blank (MB) (MB) R3939676-2 06/21/23 14:52 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acetone U 11.3 50.0 Acrolein U 2.54 50.0 Acrylonitrile U 0.671 10.0 Benzene U 0.0941 1.00 Bromobenzene U 0.118 1.00 Bromodichloromethane U 0.136 1.00 Bromoform U 0.129 1.00 Bromomethane U 0.605 5.00 n-Butylbenzene U 0.157 1.00 sec-Butylbenzene U 0.125 1.00 tert-Butylbenzene U 0.127 1.00 Carbon tetrachloride U 0.128 1.00 Chlorobenzene U 0.116 1.00 Chlorodibromomethane U 0.140 1.00 Chloroethane U 0.192 5.00 Chloroform U 0.111 5.00 Chloromethane U 0.960 2.50 2-Chlorotoluene U 0.106 1.00 4-Chlorotoluene U 0.114 1.00 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1,2-Dibromoethane U 0.126 1.00 Dibromomethane U 0.122 1.00 1,2-Dichlorobenzene U 0.107 1.00 1,3-Dichlorobenzene U 0.110 1.00 1,4-Dichlorobenzene U 0.120 1.00 Dichlorodifluoromethane U 0.374 5.00 1,1-Dichloroethane U 0.100 1.00 1,2-Dichloroethane U 0.0819 1.00 1,1-Dichloroethene U 0.188 1.00 cis-1,2-Dichloroethene U 0.126 1.00 trans-1,2-Dichloroethene U 0.149 1.00 1,2-Dichloropropane U 0.149 1.00 1,1-Dichloropropene U 0.142 1.00 1,3-Dichloropropane U 0.110 1.00 2,2-Dichloropropane U 0.161 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 Hexachloro-1,3-butadiene U 0.337 1.00 Isopropylbenzene U 0.105 1.00 p-Isopropyltoluene U 0.120 1.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 30 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 30 of 36 QUALITY CONTROL SUMMARYWG2081917 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,05,06 Method Blank (MB) (MB) R3939676-2 06/21/23 14:52 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l 2-Butanone (MEK)U 1.19 10.0 Methylene Chloride U 0.430 5.00 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 Methyl tert-butyl ether U 0.101 1.00 Naphthalene U 1.00 5.00 n-Propylbenzene U 0.0993 1.00 Styrene U 0.118 1.00 1,1,1,2-Tetrachloroethane U 0.147 1.00 1,1,2,2-Tetrachloroethane U 0.133 1.00 Tetrachloroethene U 0.300 1.00 Toluene U 0.278 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 1,2,4-Trichlorobenzene U 0.481 1.00 1,1,1-Trichloroethane U 0.149 1.00 1,1,2-Trichloroethane U 0.158 1.00 Trichloroethene U 0.190 1.00 Trichlorofluoromethane U 0.160 5.00 1,2,3-Trichloropropane U 0.237 2.50 1,2,4-Trimethylbenzene U 0.322 1.00 1,3,5-Trimethylbenzene U 0.104 1.00 Vinyl chloride U 0.234 1.00 o-Xylene U 0.174 1.00 m&p-Xylenes U 0.430 2.00 (S) Toluene-d8 118 80.0-120 (S) 4-Bromofluorobenzene 93.8 77.0-126 (S) 1,2-Dichloroethane-d4 124 70.0-130 Laboratory Control Sample (LCS) (LCS) R3939676-1 06/21/23 13:50 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acetone 25.0 22.1 88.4 19.0-160 Acrolein 25.0 28.7 115 10.0-160 Acrylonitrile 25.0 34.9 140 55.0-149 Benzene 5.00 5.64 113 70.0-123 Bromobenzene 5.00 5.64 113 73.0-121 Bromodichloromethane 5.00 5.52 110 75.0-120 Bromoform 5.00 4.47 89.4 68.0-132 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 31 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 31 of 36 QUALITY CONTROL SUMMARYWG2081917 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,05,06 Laboratory Control Sample (LCS) (LCS) R3939676-1 06/21/23 13:50 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Bromomethane 5.00 3.11 62.2 10.0-160 n-Butylbenzene 5.00 5.41 108 73.0-125 sec-Butylbenzene 5.00 5.40 108 75.0-125 tert-Butylbenzene 5.00 5.42 108 76.0-124 Carbon tetrachloride 5.00 6.18 124 68.0-126 Chlorobenzene 5.00 5.37 107 80.0-121 Chlorodibromomethane 5.00 5.26 105 77.0-125 Chloroethane 5.00 4.40 88.0 47.0-150 Chloroform 5.00 5.60 112 73.0-120 Chloromethane 5.00 6.75 135 41.0-142 2-Chlorotoluene 5.00 5.61 112 76.0-123 4-Chlorotoluene 5.00 5.79 116 75.0-122 1,2-Dibromo-3-Chloropropane 5.00 5.55 111 58.0-134 1,2-Dibromoethane 5.00 4.92 98.4 80.0-122 Dibromomethane 5.00 5.18 104 80.0-120 1,2-Dichlorobenzene 5.00 5.43 109 79.0-121 1,3-Dichlorobenzene 5.00 5.32 106 79.0-120 1,4-Dichlorobenzene 5.00 5.21 104 79.0-120 Dichlorodifluoromethane 5.00 5.66 113 51.0-149 1,1-Dichloroethane 5.00 6.33 127 70.0-126 J4 1,2-Dichloroethane 5.00 6.08 122 70.0-128 1,1-Dichloroethene 5.00 5.45 109 71.0-124 cis-1,2-Dichloroethene 5.00 4.97 99.4 73.0-120 trans-1,2-Dichloroethene 5.00 5.70 114 73.0-120 1,2-Dichloropropane 5.00 6.36 127 77.0-125 J4 1,1-Dichloropropene 5.00 5.51 110 74.0-126 1,3-Dichloropropane 5.00 5.50 110 80.0-120 2,2-Dichloropropane 5.00 5.90 118 58.0-130 Di-isopropyl ether 5.00 6.84 137 58.0-138 Ethylbenzene 5.00 5.32 106 79.0-123 Hexachloro-1,3-butadiene 5.00 6.65 133 54.0-138 Isopropylbenzene 5.00 4.93 98.6 76.0-127 p-Isopropyltoluene 5.00 5.44 109 76.0-125 2-Butanone (MEK)25.0 28.8 115 44.0-160 Methylene Chloride 5.00 5.47 109 67.0-120 4-Methyl-2-pentanone (MIBK)25.0 35.8 143 68.0-142 J4 Methyl tert-butyl ether 5.00 5.56 111 68.0-125 Naphthalene 5.00 4.99 99.8 54.0-135 n-Propylbenzene 5.00 5.49 110 77.0-124 Styrene 5.00 4.93 98.6 73.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 32 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 32 of 36 QUALITY CONTROL SUMMARYWG2081917 Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1625719-02,03,05,06 Laboratory Control Sample (LCS) (LCS) R3939676-1 06/21/23 13:50 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 1,1,1,2-Tetrachloroethane 5.00 5.31 106 75.0-125 1,1,2,2-Tetrachloroethane 5.00 5.06 101 65.0-130 Tetrachloroethene 5.00 5.75 115 72.0-132 Toluene 5.00 5.66 113 79.0-120 1,2,3-Trichlorobenzene 5.00 5.53 111 50.0-138 1,2,4-Trichlorobenzene 5.00 5.89 118 57.0-137 1,1,1-Trichloroethane 5.00 5.67 113 73.0-124 1,1,2-Trichloroethane 5.00 5.19 104 80.0-120 Trichloroethene 5.00 5.58 112 78.0-124 Trichlorofluoromethane 5.00 5.51 110 59.0-147 1,2,3-Trichloropropane 5.00 5.26 105 73.0-130 1,2,4-Trimethylbenzene 5.00 5.44 109 76.0-121 1,3,5-Trimethylbenzene 5.00 5.54 111 76.0-122 Vinyl chloride 5.00 5.13 103 67.0-131 o-Xylene 5.00 5.28 106 80.0-122 m&p-Xylenes 10.0 10.2 102 80.0-122 (S) Toluene-d8 115 80.0-120 (S) 4-Bromofluorobenzene 94.9 77.0-126 (S) 1,2-Dichloroethane-d4 125 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 33 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 33 of 36 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. RDL Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J4 The associated batch QC was outside the established quality control range for accuracy. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 34 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 34 of 36 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/22/23 18:58 35 of 36 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: ATC Group Services LLC L1625719 06/23/23 09:07 35 of 36