WS-2669_6146_CA_LAB_20160308

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 8, 2016
Andrew Deppensmith
ATC Group Services LLC - Charlotte, NC
7606 Whitehall Executive Drive, Suite 800
Charlotte, NC 28273
Project Location: Glendale Springs, NC
Client Job Number:
Project Number: Moores Exxon
Laboratory Work Order Number: 16C0134
Enclosed are results of analyses for samples received by the laboratory on March 2, 2016. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 51
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 6
16C0134-01 6
16C0134-02 8
16C0134-03 10
16C0134-04 12
16C0134-05 14
16C0134-06 16
16C0134-07 18
16C0134-08 20
16C0134-09 22
16C0134-10 24
16C0134-11 26
16C0134-12 28
16C0134-13 30
Sample Preparation Information 32
QC Data 33
Volatile Organic Compounds by GC/MS 33
B143519 33
B143520 37
B143636 41
Flag/Qualifier Summary 45
Certifications 46
Chain of Custody/Sample Receipt 48
Page 2 of 51
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/8/2016
ATC Group Services LLC - Charlotte, NC
7606 Whitehall Executive Drive, Suite 800
Charlotte, NC 28273
ATTN: Andrew Deppensmith
Moores Exxon
16C0134
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Glendale Springs, NC
MW-1 16C0134-01 Ground Water SM21-22 6200B
MW-1R 16C0134-02 Ground Water SM21-22 6200B
MW-3R 16C0134-03 Ground Water SM21-22 6200B
MW-5 16C0134-04 Ground Water SM21-22 6200B
MW-10R 16C0134-05 Ground Water SM21-22 6200B
MW-11 16C0134-06 Ground Water SM21-22 6200B
MW-12 16C0134-07 Ground Water SM21-22 6200B
MW-13 16C0134-08 Ground Water SM21-22 6200B
WSW-26 16C0134-09 Ground Water SM21-22 6200B
WSW-121 16C0134-10 Ground Water SM21-22 6200B
WSW-7414 16C0134-11 Ground Water SM21-22 6200B
WSW-3 16C0134-12 Ground Water SM21-22 6200B
WSW-7471 16C0134-13 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 51
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Elevated reporting limits for all volatile compounds due to foaming sample matrix.
Analyte & Samples(s) Qualified:
DL-01
16C0134-08[MW-13]
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Bromomethane
B143520-BS1, B143520-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
2,2-Dichloropropane
16C0134-01[MW-1], 16C0134-02[MW-1R], 16C0134-04[MW-5], 16C0134-05[MW-10R], 16C0134-06[MW-11], 16C0134-07[MW-12], 16C0134-08[MW-13],
16C0134-09[WSW-26], 16C0134-10[WSW-121], 16C0134-11[WSW-7414], 16C0134-12[WSW-3], 16C0134-13[WSW-7471], B143519-BLK1, B143519-BS1,
B143519-BSD1, B143520-BLK1, B143520-BS1, B143520-BSD1
Ethanol
16C0134-11[WSW-7414], 16C0134-12[WSW-3], 16C0134-13[WSW-7471], B143520-BLK1, B143520-BS1, B143520-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Bromomethane
B143519-BS1
Vinyl Acetate
B143520-BS1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
16C0134-01[MW-1]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/1/2016 15:45
[TOC_2]16C0134-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 25000 3/5/16 12:46 MFFg/L2400 3/4/16SM21-22 6200B500Acetone
6000 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B500Benzene
ND 250 3/5/16 12:46 MFFg/L75 3/4/16SM21-22 6200B500Bromobenzene
ND 250 3/5/16 12:46 MFFg/L110 3/4/16SM21-22 6200B500Bromochloromethane
ND 500 3/5/16 12:46 MFFg/L44 3/4/16SM21-22 6200B500Bromodichloromethane
ND 250 3/5/16 12:46 MFFg/L100 3/4/16SM21-22 6200B500Bromoform
ND 1000 3/5/16 12:46 MFFg/L470 3/4/16SM21-22 6200B500Bromomethane
ND 2500 3/5/16 12:46 MFFg/L1200 3/4/16SM21-22 6200B5002-Butanone (MEK)
100 250 3/5/16 12:46 MFFg/L75 3/4/16SM21-22 6200B500Jn-Butylbenzene
ND 250 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B500sec-Butylbenzene
ND 250 3/5/16 12:46 MFFg/L55 3/4/16SM21-22 6200B500tert-Butylbenzene
ND 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B500Carbon Tetrachloride
ND 250 3/5/16 12:46 MFFg/L80 3/4/16SM21-22 6200B500Chlorobenzene
ND 25000 3/5/16 12:46 MFFg/L14000 3/4/16SM21-22 6200B500Ethanol
ND 250 3/5/16 12:46 MFFg/L50 3/4/16SM21-22 6200B500Chlorodibromomethane
ND 250 3/5/16 12:46 MFFg/L140 3/4/16SM21-22 6200B500Chloroethane
ND 500 3/5/16 12:46 MFFg/L110 3/4/16SM21-22 6200B500Chloroform
ND 500 3/5/16 12:46 MFFg/L160 3/4/16SM21-22 6200B500Chloromethane
ND 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B5002-Chlorotoluene
ND 250 3/5/16 12:46 MFFg/L70 3/4/16SM21-22 6200B5004-Chlorotoluene
ND 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B5001,2-Dibromoethane (EDB)
ND 250 3/5/16 12:46 MFFg/L85 3/4/16SM21-22 6200B5001,2-Dichlorobenzene
ND 250 3/5/16 12:46 MFFg/L85 3/4/16SM21-22 6200B5001,3-Dichlorobenzene
ND 250 3/5/16 12:46 MFFg/L75 3/4/16SM21-22 6200B5001,4-Dichlorobenzene
ND 250 3/5/16 12:46 MFFg/L90 3/4/16SM21-22 6200B500Dichlorodifluoromethane (Freon 12)
ND 500 3/5/16 12:46 MFFg/L79 3/4/16SM21-22 6200B5001,1-Dichloroethane
ND 250 3/5/16 12:46 MFFg/L97 3/4/16SM21-22 6200B5001,2-Dichloroethane
ND 500 3/5/16 12:46 MFFg/L100 3/4/16SM21-22 6200B5001,1-Dichloroethylene
ND 250 3/5/16 12:46 MFFg/L74 3/4/16SM21-22 6200B500cis-1,2-Dichloroethylene
ND 250 3/5/16 12:46 MFFg/L75 3/4/16SM21-22 6200B500trans-1,2-Dichloroethylene
ND 250 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B5001,2-Dichloropropane
ND 500 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B5001,3-Dichloropropane
ND 250 3/5/16 12:46 MFFg/L80 3/4/16SM21-22 6200B500L-042,2-Dichloropropane
ND 500 3/5/16 12:46 MFFg/L64 3/4/16SM21-22 6200B5001,1-Dichloropropene
ND 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B500cis-1,3-Dichloropropene
ND 250 3/5/16 12:46 MFFg/L55 3/4/16SM21-22 6200B500trans-1,3-Dichloropropene
1400 250 3/5/16 12:46 MFFg/L90 3/4/16SM21-22 6200B500Diisopropyl Ether (DIPE)
5900 250 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B500Ethylbenzene
ND 2500 3/5/16 12:46 MFFg/L760 3/4/16SM21-22 6200B5002-Hexanone (MBK)
160 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B500JIsopropylbenzene (Cumene)
ND 250 3/5/16 12:46 MFFg/L75 3/4/16SM21-22 6200B500p-Isopropyltoluene (p-Cymene)
ND 250 3/5/16 12:46 MFFg/L45 3/4/16SM21-22 6200B500Methyl tert-Butyl Ether (MTBE)
ND 2500 3/5/16 12:46 MFFg/L1600 3/4/16SM21-22 6200B500Methylene Chloride
ND 2500 3/5/16 12:46 MFFg/L730 3/4/16SM21-22 6200B5004-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/1/2016 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
700 250 3/5/16 12:46 MFFg/L60 3/4/16SM21-22 6200B500Naphthalene
420 250 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B500n-Propylbenzene
ND 250 3/5/16 12:46 MFFg/L75 3/4/16SM21-22 6200B500Styrene
ND 250 3/5/16 12:46 MFFg/L80 3/4/16SM21-22 6200B5001,1,2,2-Tetrachloroethane
ND 250 3/5/16 12:46 MFFg/L85 3/4/16SM21-22 6200B500Tetrachloroethylene
100000 2500 3/7/16 14:54 MFFg/L850 3/4/16SM21-22 6200B5000Toluene
ND 250 3/5/16 12:46 MFFg/L70 3/4/16SM21-22 6200B5001,2,3-Trichlorobenzene
ND 250 3/5/16 12:46 MFFg/L95 3/4/16SM21-22 6200B5001,2,4-Trichlorobenzene
ND 250 3/5/16 12:46 MFFg/L47 3/4/16SM21-22 6200B5001,1,1-Trichloroethane
ND 250 3/5/16 12:46 MFFg/L58 3/4/16SM21-22 6200B5001,1,2-Trichloroethane
ND 500 3/5/16 12:46 MFFg/L100 3/4/16SM21-22 6200B500Trichloroethylene
ND 250 3/5/16 12:46 MFFg/L74 3/4/16SM21-22 6200B500Trichlorofluoromethane (Freon 11)
ND 250 3/5/16 12:46 MFFg/L95 3/4/16SM21-22 6200B5001,2,3-Trichloropropane
4900 250 3/5/16 12:46 MFFg/L90 3/4/16SM21-22 6200B5001,2,4-Trimethylbenzene
1100 250 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B5001,3,5-Trimethylbenzene
ND 2500 3/5/16 12:46 MFFg/L720 3/4/16SM21-22 6200B500Vinyl Acetate
ND 250 3/5/16 12:46 MFFg/L66 3/4/16SM21-22 6200B500Vinyl Chloride
25000 500 3/5/16 12:46 MFFg/L120 3/4/16SM21-22 6200B500m+p Xylene
11000 500 3/5/16 12:46 MFFg/L65 3/4/16SM21-22 6200B500o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 118 3/5/16 12:4670-130
1,2-Dichloroethane-d4 116 3/7/16 14:5470-130
Toluene-d8 103 3/5/16 12:4670-130
Toluene-d8 98.3 3/7/16 14:5470-130
4-Bromofluorobenzene 87.8 3/5/16 12:4670-130
4-Bromofluorobenzene 87.4 3/7/16 14:5470-130
Page 7 of 51
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-02
Field Sample #: MW-1R
Sample Matrix: Ground Water
Sampled: 3/1/2016 15:20
[TOC_2]16C0134-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 8:51 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 8:51 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 8:51 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 8:51 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 8:51 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 8:51 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 8:51 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 8:51 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 8:51 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 8:51 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 8:51 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 8:51 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 8:51 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 8:51 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 8:51 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 8:51 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 8:51 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 8:51 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 8:51 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 8:51 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 8:51 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 8:51 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 8:51 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 8:51 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 8:51 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 8:51 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 8:51 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-02
Field Sample #: MW-1R
Sample Matrix: Ground Water
Sampled: 3/1/2016 15:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 8:51 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 8:51 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 8:51 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 8:51 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 8:51 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 8:51 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 8:51 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 8:51 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 8:51 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 8:51 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 8:51 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 8:51 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 8:51 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 8:51 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 120 3/5/16 8:5170-130
Toluene-d8 102 3/5/16 8:5170-130
4-Bromofluorobenzene 83.2 3/5/16 8:5170-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-03
Field Sample #: MW-3R
Sample Matrix: Ground Water
Sampled: 3/1/2016 14:50
[TOC_2]16C0134-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/7/16 13:36 MFFg/L4.9 3/7/16SM21-22 6200B1Acetone
0.55 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B1Benzene
ND 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1Bromobenzene
ND 0.50 3/7/16 13:36 MFFg/L0.22 3/7/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/7/16 13:36 MFFg/L0.088 3/7/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/7/16 13:36 MFFg/L0.21 3/7/16SM21-22 6200B1Bromoform
ND 2.0 3/7/16 13:36 MFFg/L0.94 3/7/16SM21-22 6200B1Bromomethane
ND 5.0 3/7/16 13:36 MFFg/L2.4 3/7/16SM21-22 6200B12-Butanone (MEK)
2.8 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1n-Butylbenzene
1.5 0.50 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B1sec-Butylbenzene
0.18 0.50 3/7/16 13:36 MFFg/L0.11 3/7/16SM21-22 6200B1Jtert-Butylbenzene
ND 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/7/16 13:36 MFFg/L0.16 3/7/16SM21-22 6200B1Chlorobenzene
ND 50 3/7/16 13:36 MFFg/L28 3/7/16SM21-22 6200B1Ethanol
ND 0.50 3/7/16 13:36 MFFg/L0.10 3/7/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/7/16 13:36 MFFg/L0.28 3/7/16SM21-22 6200B1Chloroethane
ND 1.0 3/7/16 13:36 MFFg/L0.22 3/7/16SM21-22 6200B1Chloroform
ND 1.0 3/7/16 13:36 MFFg/L0.32 3/7/16SM21-22 6200B1Chloromethane
ND 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/7/16 13:36 MFFg/L0.14 3/7/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/7/16 13:36 MFFg/L0.17 3/7/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/7/16 13:36 MFFg/L0.17 3/7/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/7/16 13:36 MFFg/L0.18 3/7/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/7/16 13:36 MFFg/L0.16 3/7/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/7/16 13:36 MFFg/L0.19 3/7/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/7/16 13:36 MFFg/L0.21 3/7/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/7/16 13:36 MFFg/L0.16 3/7/16SM21-22 6200B12,2-Dichloropropane
ND 1.0 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/7/16 13:36 MFFg/L0.11 3/7/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/7/16 13:36 MFFg/L0.18 3/7/16SM21-22 6200B1Diisopropyl Ether (DIPE)
1.1 0.50 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/7/16 13:36 MFFg/L1.5 3/7/16SM21-22 6200B12-Hexanone (MBK)
0.74 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B1Isopropylbenzene (Cumene)
1.0 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/7/16 13:36 MFFg/L0.090 3/7/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/7/16 13:36 MFFg/L3.2 3/7/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/7/16 13:36 MFFg/L1.5 3/7/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 10 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-03
Field Sample #: MW-3R
Sample Matrix: Ground Water
Sampled: 3/1/2016 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.88 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B1Naphthalene
3.4 0.50 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1Styrene
ND 0.50 3/7/16 13:36 MFFg/L0.16 3/7/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/7/16 13:36 MFFg/L0.17 3/7/16SM21-22 6200B1Tetrachloroethylene
0.28 0.50 3/7/16 13:36 MFFg/L0.17 3/7/16SM21-22 6200B1JToluene
ND 0.50 3/7/16 13:36 MFFg/L0.14 3/7/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/7/16 13:36 MFFg/L0.19 3/7/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/7/16 13:36 MFFg/L0.094 3/7/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/7/16 13:36 MFFg/L0.12 3/7/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/7/16 13:36 MFFg/L0.20 3/7/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/7/16 13:36 MFFg/L0.15 3/7/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/7/16 13:36 MFFg/L0.19 3/7/16SM21-22 6200B11,2,3-Trichloropropane
5.5 0.50 3/7/16 13:36 MFFg/L0.18 3/7/16SM21-22 6200B11,2,4-Trimethylbenzene
1.2 0.50 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/7/16 13:36 MFFg/L1.4 3/7/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B1Vinyl Chloride
0.46 1.0 3/7/16 13:36 MFFg/L0.25 3/7/16SM21-22 6200B1Jm+p Xylene
0.15 1.0 3/7/16 13:36 MFFg/L0.13 3/7/16SM21-22 6200B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 116 3/7/16 13:3670-130
Toluene-d8 101 3/7/16 13:3670-130
4-Bromofluorobenzene 88.0 3/7/16 13:3670-130
Page 11 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-04
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/1/2016 14:25
[TOC_2]16C0134-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 9:17 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 9:17 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 9:17 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 9:17 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 9:17 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 9:17 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 9:17 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 9:17 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 9:17 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 9:17 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 9:17 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 9:17 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 9:17 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 9:17 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 9:17 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 9:17 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 9:17 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 9:17 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 9:17 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 9:17 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 9:17 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 9:17 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 9:17 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 9:17 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 9:17 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 9:17 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 9:17 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 12 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-04
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/1/2016 14:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 9:17 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 9:17 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 9:17 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 9:17 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 9:17 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 9:17 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 9:17 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 9:17 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 9:17 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 9:17 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 9:17 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 9:17 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 9:17 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 9:17 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 117 3/5/16 9:1770-130
Toluene-d8 99.6 3/5/16 9:1770-130
4-Bromofluorobenzene 85.7 3/5/16 9:1770-130
Page 13 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-05
Field Sample #: MW-10R
Sample Matrix: Ground Water
Sampled: 3/1/2016 11:45
[TOC_2]16C0134-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 9:44 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 9:44 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 9:44 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 9:44 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 9:44 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 9:44 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 9:44 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 9:44 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 9:44 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 9:44 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 9:44 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 9:44 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 9:44 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 9:44 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 9:44 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 9:44 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 9:44 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 9:44 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 9:44 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 9:44 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 9:44 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 9:44 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 9:44 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 9:44 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 9:44 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 9:44 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 9:44 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 14 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-05
Field Sample #: MW-10R
Sample Matrix: Ground Water
Sampled: 3/1/2016 11:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 9:44 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 9:44 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 9:44 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 9:44 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 9:44 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 9:44 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 9:44 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 9:44 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 9:44 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 9:44 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 9:44 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 9:44 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 9:44 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 9:44 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 121 3/5/16 9:4470-130
Toluene-d8 100 3/5/16 9:4470-130
4-Bromofluorobenzene 86.3 3/5/16 9:4470-130
Page 15 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-06
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 3/1/2016 13:20
[TOC_2]16C0134-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 10:10 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 10:10 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 10:10 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 10:10 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 10:10 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 10:10 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 10:10 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 10:10 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 10:10 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 10:10 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 10:10 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 10:10 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 10:10 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 10:10 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 10:10 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 10:10 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 10:10 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 10:10 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 10:10 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 10:10 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 10:10 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 10:10 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 10:10 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 10:10 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 10:10 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 10:10 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 10:10 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 16 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-06
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 3/1/2016 13:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 10:10 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 10:10 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 10:10 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 10:10 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 10:10 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 10:10 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 10:10 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 10:10 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 10:10 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 10:10 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 10:10 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 10:10 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 10:10 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 10:10 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 118 3/5/16 10:1070-130
Toluene-d8 101 3/5/16 10:1070-130
4-Bromofluorobenzene 82.8 3/5/16 10:1070-130
Page 17 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-07
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 3/1/2016 13:50
[TOC_2]16C0134-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 10:36 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 10:36 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 10:36 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 10:36 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 10:36 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 10:36 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 10:36 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 10:36 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 10:36 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 10:36 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 10:36 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 10:36 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 10:36 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 10:36 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 10:36 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 10:36 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 10:36 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 10:36 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 10:36 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 10:36 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 10:36 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 10:36 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 10:36 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 10:36 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 10:36 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 10:36 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 10:36 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 18 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-07
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 3/1/2016 13:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 10:36 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 10:36 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 10:36 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 10:36 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 10:36 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 10:36 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 10:36 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 10:36 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 10:36 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 10:36 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 10:36 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 10:36 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 10:36 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 10:36 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 124 3/5/16 10:3670-130
Toluene-d8 102 3/5/16 10:3670-130
4-Bromofluorobenzene 83.0 3/5/16 10:3670-130
Page 19 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-08
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 3/1/2016 12:30
[TOC_2]16C0134-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: DL-01 Volatile Organic Compounds by GC/MS
ND 100 3/5/16 11:02 MFFg/L9.7 3/4/16SM21-22 6200B2Acetone
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B2Benzene
ND 1.0 3/5/16 11:02 MFFg/L0.30 3/4/16SM21-22 6200B2Bromobenzene
ND 1.0 3/5/16 11:02 MFFg/L0.45 3/4/16SM21-22 6200B2Bromochloromethane
ND 2.0 3/5/16 11:02 MFFg/L0.18 3/4/16SM21-22 6200B2Bromodichloromethane
ND 1.0 3/5/16 11:02 MFFg/L0.42 3/4/16SM21-22 6200B2Bromoform
ND 4.0 3/5/16 11:02 MFFg/L1.9 3/4/16SM21-22 6200B2Bromomethane
ND 10 3/5/16 11:02 MFFg/L4.7 3/4/16SM21-22 6200B22-Butanone (MEK)
ND 1.0 3/5/16 11:02 MFFg/L0.30 3/4/16SM21-22 6200B2n-Butylbenzene
ND 1.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B2sec-Butylbenzene
ND 1.0 3/5/16 11:02 MFFg/L0.22 3/4/16SM21-22 6200B2tert-Butylbenzene
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B2Carbon Tetrachloride
ND 1.0 3/5/16 11:02 MFFg/L0.32 3/4/16SM21-22 6200B2Chlorobenzene
ND 100 3/5/16 11:02 MFFg/L56 3/4/16SM21-22 6200B2Ethanol
ND 1.0 3/5/16 11:02 MFFg/L0.20 3/4/16SM21-22 6200B2Chlorodibromomethane
ND 1.0 3/5/16 11:02 MFFg/L0.56 3/4/16SM21-22 6200B2Chloroethane
ND 2.0 3/5/16 11:02 MFFg/L0.44 3/4/16SM21-22 6200B2Chloroform
ND 2.0 3/5/16 11:02 MFFg/L0.65 3/4/16SM21-22 6200B2Chloromethane
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B22-Chlorotoluene
ND 1.0 3/5/16 11:02 MFFg/L0.28 3/4/16SM21-22 6200B24-Chlorotoluene
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 3/5/16 11:02 MFFg/L0.34 3/4/16SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 3/5/16 11:02 MFFg/L0.34 3/4/16SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 3/5/16 11:02 MFFg/L0.30 3/4/16SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 3/5/16 11:02 MFFg/L0.36 3/4/16SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 2.0 3/5/16 11:02 MFFg/L0.32 3/4/16SM21-22 6200B21,1-Dichloroethane
ND 1.0 3/5/16 11:02 MFFg/L0.39 3/4/16SM21-22 6200B21,2-Dichloroethane
ND 2.0 3/5/16 11:02 MFFg/L0.42 3/4/16SM21-22 6200B21,1-Dichloroethylene
ND 1.0 3/5/16 11:02 MFFg/L0.29 3/4/16SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 3/5/16 11:02 MFFg/L0.30 3/4/16SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B21,2-Dichloropropane
ND 2.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B21,3-Dichloropropane
ND 1.0 3/5/16 11:02 MFFg/L0.32 3/4/16SM21-22 6200B2L-042,2-Dichloropropane
ND 2.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B21,1-Dichloropropene
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 3/5/16 11:02 MFFg/L0.22 3/4/16SM21-22 6200B2trans-1,3-Dichloropropene
ND 1.0 3/5/16 11:02 MFFg/L0.36 3/4/16SM21-22 6200B2Diisopropyl Ether (DIPE)
ND 1.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B2Ethylbenzene
ND 10 3/5/16 11:02 MFFg/L3.0 3/4/16SM21-22 6200B22-Hexanone (MBK)
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B2Isopropylbenzene (Cumene)
ND 1.0 3/5/16 11:02 MFFg/L0.30 3/4/16SM21-22 6200B2p-Isopropyltoluene (p-Cymene)
ND 1.0 3/5/16 11:02 MFFg/L0.18 3/4/16SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 3/5/16 11:02 MFFg/L6.4 3/4/16SM21-22 6200B2Methylene Chloride
ND 10 3/5/16 11:02 MFFg/L2.9 3/4/16SM21-22 6200B24-Methyl-2-pentanone (MIBK)
Page 20 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-08
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 3/1/2016 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: DL-01 Volatile Organic Compounds by GC/MS
ND 1.0 3/5/16 11:02 MFFg/L0.24 3/4/16SM21-22 6200B2Naphthalene
ND 1.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B2n-Propylbenzene
ND 1.0 3/5/16 11:02 MFFg/L0.30 3/4/16SM21-22 6200B2Styrene
ND 1.0 3/5/16 11:02 MFFg/L0.32 3/4/16SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 3/5/16 11:02 MFFg/L0.34 3/4/16SM21-22 6200B2Tetrachloroethylene
ND 1.0 3/5/16 11:02 MFFg/L0.34 3/4/16SM21-22 6200B2Toluene
ND 1.0 3/5/16 11:02 MFFg/L0.28 3/4/16SM21-22 6200B21,2,3-Trichlorobenzene
ND 1.0 3/5/16 11:02 MFFg/L0.38 3/4/16SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 3/5/16 11:02 MFFg/L0.19 3/4/16SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 3/5/16 11:02 MFFg/L0.23 3/4/16SM21-22 6200B21,1,2-Trichloroethane
ND 2.0 3/5/16 11:02 MFFg/L0.40 3/4/16SM21-22 6200B2Trichloroethylene
ND 1.0 3/5/16 11:02 MFFg/L0.29 3/4/16SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 3/5/16 11:02 MFFg/L0.38 3/4/16SM21-22 6200B21,2,3-Trichloropropane
ND 1.0 3/5/16 11:02 MFFg/L0.36 3/4/16SM21-22 6200B21,2,4-Trimethylbenzene
ND 1.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B21,3,5-Trimethylbenzene
ND 10 3/5/16 11:02 MFFg/L2.9 3/4/16SM21-22 6200B2Vinyl Acetate
ND 1.0 3/5/16 11:02 MFFg/L0.27 3/4/16SM21-22 6200B2Vinyl Chloride
ND 2.0 3/5/16 11:02 MFFg/L0.50 3/4/16SM21-22 6200B2m+p Xylene
ND 2.0 3/5/16 11:02 MFFg/L0.26 3/4/16SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 119 3/5/16 11:0270-130
Toluene-d8 101 3/5/16 11:0270-130
4-Bromofluorobenzene 86.2 3/5/16 11:0270-130
Page 21 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-09
Field Sample #: WSW-26
Sample Matrix: Ground Water
Sampled: 3/1/2016 11:50
[TOC_2]16C0134-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 4:57 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 4:57 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 4:57 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 4:57 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 4:57 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 4:57 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 4:57 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 4:57 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 4:57 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 4:57 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 4:57 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 4:57 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 4:57 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 4:57 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 4:57 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 4:57 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 4:57 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 4:57 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 4:57 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 4:57 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 4:57 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 4:57 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 4:57 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 4:57 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.53 0.50 3/5/16 4:57 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 4:57 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 4:57 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 22 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-09
Field Sample #: WSW-26
Sample Matrix: Ground Water
Sampled: 3/1/2016 11:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 4:57 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 4:57 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 4:57 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 4:57 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 4:57 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 4:57 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 4:57 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 4:57 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 4:57 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 4:57 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 4:57 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 4:57 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 4:57 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 4:57 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 118 3/5/16 4:5770-130
Toluene-d8 102 3/5/16 4:5770-130
4-Bromofluorobenzene 84.1 3/5/16 4:5770-130
Page 23 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-10
Field Sample #: WSW-121
Sample Matrix: Ground Water
Sampled: 3/1/2016 12:00
[TOC_2]16C0134-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 5:23 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 5:23 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 5:23 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 5:23 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 5:23 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 5:23 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 5:23 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 5:23 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 5:23 MFFg/L28 3/4/16SM21-22 6200B1Ethanol
ND 0.50 3/5/16 5:23 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 5:23 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 5:23 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 5:23 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 5:23 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 5:23 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 5:23 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 5:23 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 5:23 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 5:23 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 5:23 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 5:23 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 5:23 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 5:23 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 5:23 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 5:23 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 5:23 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 5:23 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-10
Field Sample #: WSW-121
Sample Matrix: Ground Water
Sampled: 3/1/2016 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 5:23 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 5:23 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 5:23 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 5:23 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 5:23 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 5:23 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 5:23 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 5:23 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 5:23 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 5:23 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 5:23 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 5:23 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 5:23 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 5:23 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 119 3/5/16 5:2370-130
Toluene-d8 101 3/5/16 5:2370-130
4-Bromofluorobenzene 82.6 3/5/16 5:2370-130
Page 25 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-11
Field Sample #: WSW-7414
Sample Matrix: Ground Water
Sampled: 3/1/2016 12:45
[TOC_2]16C0134-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
84 50 3/5/16 17:08 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 17:08 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 17:08 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 17:08 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 17:08 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
35 5.0 3/5/16 17:08 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 17:08 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 17:08 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 17:08 MFFg/L28 3/4/16SM21-22 6200B1L-04Ethanol
ND 0.50 3/5/16 17:08 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 17:08 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 17:08 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 17:08 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 17:08 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 17:08 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 17:08 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 17:08 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 17:08 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 17:08 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 17:08 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 17:08 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 17:08 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 17:08 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 17:08 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.55 0.50 3/5/16 17:08 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 17:08 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 17:08 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 26 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-11
Field Sample #: WSW-7414
Sample Matrix: Ground Water
Sampled: 3/1/2016 12:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 17:08 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 17:08 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 17:08 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 17:08 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 17:08 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 17:08 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 17:08 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 17:08 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 17:08 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 17:08 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 17:08 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 17:08 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 17:08 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 17:08 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 120 3/5/16 17:0870-130
Toluene-d8 100 3/5/16 17:0870-130
4-Bromofluorobenzene 85.2 3/5/16 17:0870-130
Page 27 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-12
Field Sample #: WSW-3
Sample Matrix: Ground Water
Sampled: 3/1/2016 16:00
[TOC_2]16C0134-12[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 17:34 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 17:34 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 17:34 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 17:34 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 17:34 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 17:34 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 17:34 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 17:34 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 17:34 MFFg/L28 3/4/16SM21-22 6200B1L-04Ethanol
ND 0.50 3/5/16 17:34 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 17:34 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 17:34 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 17:34 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 17:34 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 17:34 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 17:34 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 17:34 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 17:34 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 17:34 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 17:34 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 17:34 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 17:34 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 17:34 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 17:34 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 17:34 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 17:34 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 17:34 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-12
Field Sample #: WSW-3
Sample Matrix: Ground Water
Sampled: 3/1/2016 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 17:34 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 17:34 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 17:34 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 17:34 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 17:34 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 17:34 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 17:34 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 17:34 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 17:34 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 17:34 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 17:34 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 17:34 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 17:34 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 17:34 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 120 3/5/16 17:3470-130
Toluene-d8 101 3/5/16 17:3470-130
4-Bromofluorobenzene 85.1 3/5/16 17:3470-130
Page 29 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-13
Field Sample #: WSW-7471
Sample Matrix: Ground Water
Sampled: 3/1/2016 16:20
[TOC_2]16C0134-13[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/16 18:00 MFFg/L4.9 3/4/16SM21-22 6200B1Acetone
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B1Benzene
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1Bromobenzene
ND 0.50 3/5/16 18:00 MFFg/L0.22 3/4/16SM21-22 6200B1Bromochloromethane
ND 1.0 3/5/16 18:00 MFFg/L0.088 3/4/16SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/16 18:00 MFFg/L0.21 3/4/16SM21-22 6200B1Bromoform
ND 2.0 3/5/16 18:00 MFFg/L0.94 3/4/16SM21-22 6200B1Bromomethane
ND 5.0 3/5/16 18:00 MFFg/L2.4 3/4/16SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1n-Butylbenzene
ND 0.50 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/5/16 18:00 MFFg/L0.11 3/4/16SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/16 18:00 MFFg/L0.16 3/4/16SM21-22 6200B1Chlorobenzene
ND 50 3/5/16 18:00 MFFg/L28 3/4/16SM21-22 6200B1L-04Ethanol
ND 0.50 3/5/16 18:00 MFFg/L0.10 3/4/16SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/16 18:00 MFFg/L0.28 3/4/16SM21-22 6200B1Chloroethane
ND 1.0 3/5/16 18:00 MFFg/L0.22 3/4/16SM21-22 6200B1Chloroform
ND 1.0 3/5/16 18:00 MFFg/L0.32 3/4/16SM21-22 6200B1Chloromethane
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/16 18:00 MFFg/L0.14 3/4/16SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/16 18:00 MFFg/L0.17 3/4/16SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/16 18:00 MFFg/L0.17 3/4/16SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/16 18:00 MFFg/L0.18 3/4/16SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/5/16 18:00 MFFg/L0.16 3/4/16SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/5/16 18:00 MFFg/L0.19 3/4/16SM21-22 6200B11,2-Dichloroethane
ND 1.0 3/5/16 18:00 MFFg/L0.21 3/4/16SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B11,2-Dichloropropane
ND 1.0 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/16 18:00 MFFg/L0.16 3/4/16SM21-22 6200B1L-042,2-Dichloropropane
ND 1.0 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/16 18:00 MFFg/L0.11 3/4/16SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/5/16 18:00 MFFg/L0.18 3/4/16SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/16 18:00 MFFg/L1.5 3/4/16SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/5/16 18:00 MFFg/L0.090 3/4/16SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/16 18:00 MFFg/L3.2 3/4/16SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/16 18:00 MFFg/L1.5 3/4/16SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 30 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2016
Work Order: 16C0134Sample Description:Project Location: Glendale Springs, NC
Sample ID: 16C0134-13
Field Sample #: WSW-7471
Sample Matrix: Ground Water
Sampled: 3/1/2016 16:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B1Naphthalene
ND 0.50 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1Styrene
ND 0.50 3/5/16 18:00 MFFg/L0.16 3/4/16SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/16 18:00 MFFg/L0.17 3/4/16SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/5/16 18:00 MFFg/L0.17 3/4/16SM21-22 6200B1Toluene
ND 0.50 3/5/16 18:00 MFFg/L0.14 3/4/16SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/16 18:00 MFFg/L0.19 3/4/16SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/16 18:00 MFFg/L0.094 3/4/16SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/16 18:00 MFFg/L0.12 3/4/16SM21-22 6200B11,1,2-Trichloroethane
ND 1.0 3/5/16 18:00 MFFg/L0.20 3/4/16SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/16 18:00 MFFg/L0.15 3/4/16SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/16 18:00 MFFg/L0.19 3/4/16SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/5/16 18:00 MFFg/L0.18 3/4/16SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 3/5/16 18:00 MFFg/L1.4 3/4/16SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B1Vinyl Chloride
ND 1.0 3/5/16 18:00 MFFg/L0.25 3/4/16SM21-22 6200B1m+p Xylene
ND 1.0 3/5/16 18:00 MFFg/L0.13 3/4/16SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 120 3/5/16 18:0070-130
Toluene-d8 101 3/5/16 18:0070-130
4-Bromofluorobenzene 82.1 3/5/16 18:0070-130
Page 31 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B143519 03/04/160.01 5.0016C0134-01 [MW-1]
B143519 03/04/165 5.0016C0134-02 [MW-1R]
B143519 03/04/165 5.0016C0134-04 [MW-5]
B143519 03/04/165 5.0016C0134-05 [MW-10R]
B143519 03/04/165 5.0016C0134-06 [MW-11]
B143519 03/04/165 5.0016C0134-07 [MW-12]
B143519 03/04/162.5 5.0016C0134-08 [MW-13]
B143519 03/04/165 5.0016C0134-09 [WSW-26]
B143519 03/04/165 5.0016C0134-10 [WSW-121]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B143520 03/04/165 5.0016C0134-11 [WSW-7414]
B143520 03/04/165 5.0016C0134-12 [WSW-3]
B143520 03/04/165 5.0016C0134-13 [WSW-7471]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B143636 03/04/160.001 5.0016C0134-01RE1 [MW-1]
B143636 03/07/165 5.0016C0134-03 [MW-3R]
[TOC_1]Sample Preparation Information[TOC]
Page 32 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B143519 - SW-846 5030B
[TOC_3]B143519[TOC]
Blank (B143519-BLK1) Prepared: 03/04/16 Analyzed: 03/05/16
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L1.0ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L1.0ND
Chloromethane g/L1.0ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L1.0ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L1.0ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L1.0ND
2,2-Dichloropropane g/L0.50 L-04ND
1,1-Dichloropropene g/L1.0ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 33 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143519 - SW-846 5030B
Blank (B143519-BLK1) Prepared: 03/04/16 Analyzed: 03/05/16
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L1.0ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L1.0ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11929.7
g/L 25.0 70-130Surrogate: Toluene-d8 10025.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 82.520.6
LCS (B143519-BS1) Prepared: 03/04/16 Analyzed: 03/05/16
Acetone g/L50 100 70-13093.293.2
Benzene g/L0.50 10.0 70-13011111.1
Bromobenzene g/L0.50 10.0 70-13083.48.34
Bromochloromethane g/L0.50 10.0 70-13097.99.79
Bromodichloromethane g/L1.0 10.0 70-13010810.8
Bromoform g/L0.50 10.0 70-13010710.7
Bromomethane g/L2.0 10.0 L-0760-140161*16.1
2-Butanone (MEK)g/L5.0 100 70-13096.996.9
n-Butylbenzene g/L0.50 10.0 70-13094.09.40
sec-Butylbenzene g/L0.50 10.0 70-13094.19.41
tert-Butylbenzene g/L0.50 10.0 70-13092.59.25
Carbon Tetrachloride g/L0.50 10.0 70-13011311.3
Chlorobenzene g/L0.50 10.0 70-13087.98.79
Ethanol g/L50 100 70-13097.697.6
Chlorodibromomethane g/L0.50 10.0 70-13011211.2
Chloroethane g/L0.50 10.0 60-14013613.6
Chloroform g/L1.0 10.0 70-13011011.0
Chloromethane g/L1.0 10.0 60-14092.29.22
2-Chlorotoluene g/L0.50 10.0 70-13090.29.02
4-Chlorotoluene g/L0.50 10.0 70-13093.59.35
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13092.29.22
1,2-Dichlorobenzene g/L0.50 10.0 70-13089.78.97
1,3-Dichlorobenzene g/L0.50 10.0 70-13092.29.22
1,4-Dichlorobenzene g/L0.50 10.0 70-13089.18.91
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14094.19.41
1,1-Dichloroethane g/L1.0 10.0 70-13010310.3
1,2-Dichloroethane g/L0.50 10.0 70-13010110.1
1,1-Dichloroethylene g/L1.0 10.0 70-13012812.8
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13094.29.42
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010110.1
1,2-Dichloropropane g/L0.50 10.0 70-13094.69.46
1,3-Dichloropropane g/L1.0 10.0 70-13094.89.48
2,2-Dichloropropane g/L0.50 10.0 L-0470-13064.5 *6.45
1,1-Dichloropropene g/L1.0 10.0 70-13010310.3
cis-1,3-Dichloropropene g/L0.50 10.0 70-13088.18.81
trans-1,3-Dichloropropene g/L0.50 10.0 70-13088.58.85
Page 34 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143519 - SW-846 5030B
LCS (B143519-BS1) Prepared: 03/04/16 Analyzed: 03/05/16
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13090.09.00
Ethylbenzene g/L0.50 10.0 70-13091.89.18
2-Hexanone (MBK)g/L5.0 100 70-13089.889.8
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13085.08.50
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13094.39.43
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13096.79.67
Methylene Chloride g/L5.0 10.0 70-13010510.5
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13090.090.0
Naphthalene g/L0.50 10.0 70-13095.69.56
n-Propylbenzene g/L0.50 10.0 70-13086.98.69
Styrene g/L0.50 10.0 70-13082.78.27
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010510.5
Tetrachloroethylene g/L0.50 10.0 70-13086.08.60
Toluene g/L0.50 10.0 70-13099.29.92
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13089.48.94
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13082.68.26
1,1,1-Trichloroethane g/L0.50 10.0 70-13010310.3
1,1,2-Trichloroethane g/L0.50 10.0 70-13094.99.49
Trichloroethylene g/L1.0 10.0 70-13095.59.55
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13012812.8
1,2,3-Trichloropropane g/L0.50 10.0 70-13087.18.71
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13098.69.86
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13082.58.25
Vinyl Acetate g/L5.0 100 70-13084.184.1
Vinyl Chloride g/L0.50 10.0 60-14011411.4
m+p Xylene g/L1.0 20.0 70-13091.918.4
o-Xylene g/L1.0 10.0 70-13093.69.36
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11629.1
g/L 25.0 70-130Surrogate: Toluene-d8 10425.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 89.322.3
LCS Dup (B143519-BSD1) Prepared: 03/04/16 Analyzed: 03/05/16
Acetone g/L50 100 2570-13089.1 4.4189.1
Benzene g/L0.50 10.0 2570-130103 7.0210.3
Bromobenzene g/L0.50 10.0 2570-13080.4 3.668.04
Bromochloromethane g/L0.50 10.0 2570-13092.5 5.679.25
Bromodichloromethane g/L1.0 10.0 2570-130108 0.92610.8
Bromoform g/L0.50 10.0 2570-130100 6.6410.0
Bromomethane g/L2.0 10.0 2560-140138 15.313.8
2-Butanone (MEK)g/L5.0 100 2570-13094.6 2.3694.6
n-Butylbenzene g/L0.50 10.0 2570-13090.1 4.249.01
sec-Butylbenzene g/L0.50 10.0 2570-13090.4 4.019.04
tert-Butylbenzene g/L0.50 10.0 2570-13090.0 2.749.00
Carbon Tetrachloride g/L0.50 10.0 2570-130115 1.9311.5
Chlorobenzene g/L0.50 10.0 2570-13083.5 5.138.35
Ethanol g/L50 100 2570-13081.9 17.581.9
Chlorodibromomethane g/L0.50 10.0 2570-130116 2.6311.6
Chloroethane g/L0.50 10.0 2560-140124 9.2012.4
Chloroform g/L1.0 10.0 2570-130103 6.0210.3
Chloromethane g/L1.0 10.0 2560-14084.0 9.318.40
2-Chlorotoluene g/L0.50 10.0 2570-13084.1 7.008.41
4-Chlorotoluene g/L0.50 10.0 2570-13087.0 7.208.70
Page 35 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143519 - SW-846 5030B
LCS Dup (B143519-BSD1) Prepared: 03/04/16 Analyzed: 03/05/16
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13090.3 2.089.03
1,2-Dichlorobenzene g/L0.50 10.0 2570-13091.4 1.889.14
1,3-Dichlorobenzene g/L0.50 10.0 2570-13090.3 2.089.03
1,4-Dichlorobenzene g/L0.50 10.0 2570-13087.5 1.818.75
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14088.3 6.368.83
1,1-Dichloroethane g/L1.0 10.0 2570-13098.5 4.179.85
1,2-Dichloroethane g/L0.50 10.0 2570-13099.5 1.699.95
1,1-Dichloroethylene g/L1.0 10.0 2570-130113 12.911.3
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13093.3 0.9609.33
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13092.6 8.979.26
1,2-Dichloropropane g/L0.50 10.0 2570-13088.0 7.238.80
1,3-Dichloropropane g/L1.0 10.0 2570-13097.0 2.299.70
2,2-Dichloropropane g/L0.50 10.0 25 L-0470-13059.3 8.40*5.93
1,1-Dichloropropene g/L1.0 10.0 2570-130100 2.6610.0
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13089.3 1.358.93
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13087.6 1.028.76
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13086.6 3.858.66
Ethylbenzene g/L0.50 10.0 2570-13088.7 3.438.87
2-Hexanone (MBK)g/L5.0 100 2570-13089.3 0.53689.3
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13081.1 4.708.11
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13089.0 5.788.90
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13093.5 3.369.35
Methylene Chloride g/L5.0 10.0 2570-130101 4.0710.1
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13089.0 1.1889.0
Naphthalene g/L0.50 10.0 2570-13094.7 0.9469.47
n-Propylbenzene g/L0.50 10.0 2570-13082.4 5.328.24
Styrene g/L0.50 10.0 2570-13081.2 1.838.12
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130106 1.4210.6
Tetrachloroethylene g/L0.50 10.0 2570-13079.9 7.357.99
Toluene g/L0.50 10.0 2570-13096.8 2.459.68
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13083.8 6.478.38
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13081.6 1.228.16
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.0 6.299.70
1,1,2-Trichloroethane g/L0.50 10.0 2570-13090.4 4.869.04
Trichloroethylene g/L1.0 10.0 2570-13094.3 1.269.43
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130121 5.0612.1
1,2,3-Trichloropropane g/L0.50 10.0 2570-13087.7 0.6878.77
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13097.4 1.229.74
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13080.2 2.838.02
Vinyl Acetate g/L5.0 100 2570-13082.5 1.9282.5
Vinyl Chloride g/L0.50 10.0 2560-140103 10.110.3
m+p Xylene g/L1.0 20.0 2570-13088.2 4.1717.6
o-Xylene g/L1.0 10.0 2570-13087.2 7.088.72
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11629.0
g/L 25.0 70-130Surrogate: Toluene-d8 10526.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 89.922.5
Page 36 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143520 - SW-846 5030B
[TOC_3]B143520[TOC]
Blank (B143520-BLK1) Prepared: 03/04/16 Analyzed: 03/05/16
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L1.0ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50 L-04ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L1.0ND
Chloromethane g/L1.0ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L1.0ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L1.0ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L1.0ND
2,2-Dichloropropane g/L0.50 L-04ND
1,1-Dichloropropene g/L1.0ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 37 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143520 - SW-846 5030B
Blank (B143520-BLK1) Prepared: 03/04/16 Analyzed: 03/05/16
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L1.0ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L1.0ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11528.7
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 82.520.6
LCS (B143520-BS1) Prepared: 03/04/16 Analyzed: 03/05/16
Acetone g/L50 100 70-130118118
Benzene g/L0.50 10.0 70-13010510.5
Bromobenzene g/L0.50 10.0 70-13082.38.23
Bromochloromethane g/L0.50 10.0 70-13092.39.23
Bromodichloromethane g/L1.0 10.0 70-13011411.4
Bromoform g/L0.50 10.0 70-13010510.5
Bromomethane g/L2.0 10.0 L-0260-140169*16.9
2-Butanone (MEK)g/L5.0 100 70-13097.397.3
n-Butylbenzene g/L0.50 10.0 70-13087.68.76
sec-Butylbenzene g/L0.50 10.0 70-13092.59.25
tert-Butylbenzene g/L0.50 10.0 70-13091.99.19
Carbon Tetrachloride g/L0.50 10.0 70-13011311.3
Chlorobenzene g/L0.50 10.0 70-13085.08.50
Ethanol g/L50 100 L-04, J70-13034.2 *34.2
Chlorodibromomethane g/L0.50 10.0 70-13010910.9
Chloroethane g/L0.50 10.0 60-14011911.9
Chloroform g/L1.0 10.0 70-13011011.0
Chloromethane g/L1.0 10.0 60-14088.48.84
2-Chlorotoluene g/L0.50 10.0 70-13085.38.53
4-Chlorotoluene g/L0.50 10.0 70-13088.78.87
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13090.79.07
1,2-Dichlorobenzene g/L0.50 10.0 70-13086.78.67
1,3-Dichlorobenzene g/L0.50 10.0 70-13087.78.77
1,4-Dichlorobenzene g/L0.50 10.0 70-13087.38.73
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14083.28.32
1,1-Dichloroethane g/L1.0 10.0 70-13010110.1
1,2-Dichloroethane g/L0.50 10.0 70-13010310.3
1,1-Dichloroethylene g/L1.0 10.0 70-13011811.8
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13094.49.44
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13095.99.59
1,2-Dichloropropane g/L0.50 10.0 70-13088.48.84
1,3-Dichloropropane g/L1.0 10.0 70-13098.29.82
2,2-Dichloropropane g/L0.50 10.0 L-0470-13033.2 *3.32
1,1-Dichloropropene g/L1.0 10.0 70-13010310.3
cis-1,3-Dichloropropene g/L0.50 10.0 70-13078.07.80
trans-1,3-Dichloropropene g/L0.50 10.0 70-13079.07.90
Page 38 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143520 - SW-846 5030B
LCS (B143520-BS1) Prepared: 03/04/16 Analyzed: 03/05/16
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13089.38.93
Ethylbenzene g/L0.50 10.0 70-13087.38.73
2-Hexanone (MBK)g/L5.0 100 70-13091.291.2
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13083.68.36
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13089.18.91
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13095.79.57
Methylene Chloride g/L5.0 10.0 70-13010310.3
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13092.092.0
Naphthalene g/L0.50 10.0 70-13088.08.80
n-Propylbenzene g/L0.50 10.0 70-13082.88.28
Styrene g/L0.50 10.0 70-13083.58.35
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010210.2
Tetrachloroethylene g/L0.50 10.0 70-13083.28.32
Toluene g/L0.50 10.0 70-13096.59.65
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13081.68.16
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13078.27.82
1,1,1-Trichloroethane g/L0.50 10.0 70-13010110.1
1,1,2-Trichloroethane g/L0.50 10.0 70-13093.19.31
Trichloroethylene g/L1.0 10.0 70-13092.89.28
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13012212.2
1,2,3-Trichloropropane g/L0.50 10.0 70-13086.88.68
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13091.89.18
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13081.88.18
Vinyl Acetate g/L5.0 100 L-0770-13068.1 *68.1
Vinyl Chloride g/L0.50 10.0 60-14010910.9
m+p Xylene g/L1.0 20.0 70-13086.817.4
o-Xylene g/L1.0 10.0 70-13085.98.59
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11528.7
g/L 25.0 70-130Surrogate: Toluene-d8 10325.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 88.422.1
LCS Dup (B143520-BSD1) Prepared: 03/04/16 Analyzed: 03/05/16
Acetone g/L50 100 2570-130125 5.36125
Benzene g/L0.50 10.0 2570-130102 2.8010.2
Bromobenzene g/L0.50 10.0 2570-13082.9 0.7268.29
Bromochloromethane g/L0.50 10.0 2570-13092.8 0.5409.28
Bromodichloromethane g/L1.0 10.0 2570-130118 3.2811.8
Bromoform g/L0.50 10.0 2570-130113 6.6911.3
Bromomethane g/L2.0 10.0 25 L-0260-140165 2.16*16.5
2-Butanone (MEK)g/L5.0 100 2570-130100 2.96100
n-Butylbenzene g/L0.50 10.0 2570-13087.3 0.3438.73
sec-Butylbenzene g/L0.50 10.0 2570-13090.9 1.749.09
tert-Butylbenzene g/L0.50 10.0 2570-13089.7 2.428.97
Carbon Tetrachloride g/L0.50 10.0 2570-130108 4.5210.8
Chlorobenzene g/L0.50 10.0 2570-13085.3 0.3528.53
Ethanol g/L50 100 25 L-04, J70-13033.2 3.14*33.2
Chlorodibromomethane g/L0.50 10.0 2570-130115 5.6311.5
Chloroethane g/L0.50 10.0 2560-140128 7.3612.8
Chloroform g/L1.0 10.0 2570-130108 2.2010.8
Chloromethane g/L1.0 10.0 2560-14087.4 1.148.74
2-Chlorotoluene g/L0.50 10.0 2570-13084.3 1.188.43
4-Chlorotoluene g/L0.50 10.0 2570-13087.1 1.828.71
Page 39 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143520 - SW-846 5030B
LCS Dup (B143520-BSD1) Prepared: 03/04/16 Analyzed: 03/05/16
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13092.7 2.189.27
1,2-Dichlorobenzene g/L0.50 10.0 2570-13092.8 6.809.28
1,3-Dichlorobenzene g/L0.50 10.0 2570-13089.3 1.818.93
1,4-Dichlorobenzene g/L0.50 10.0 2570-13088.6 1.488.86
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14085.4 2.618.54
1,1-Dichloroethane g/L1.0 10.0 2570-13099.7 1.109.97
1,2-Dichloroethane g/L0.50 10.0 2570-130105 1.9210.5
1,1-Dichloroethylene g/L1.0 10.0 2570-130116 2.1311.6
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13090.8 3.899.08
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.4 0.5209.64
1,2-Dichloropropane g/L0.50 10.0 2570-13090.0 1.799.00
1,3-Dichloropropane g/L1.0 10.0 2570-13096.6 1.649.66
2,2-Dichloropropane g/L0.50 10.0 25 L-0470-13032.6 1.82*3.26
1,1-Dichloropropene g/L1.0 10.0 2570-13098.5 4.669.85
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13079.7 2.167.97
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13079.3 0.3797.93
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13086.8 2.848.68
Ethylbenzene g/L0.50 10.0 2570-13086.0 1.508.60
2-Hexanone (MBK)g/L5.0 100 2570-13095.6 4.6795.6
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13082.1 1.818.21
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13089.7 0.6718.97
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13097.9 2.279.79
Methylene Chloride g/L5.0 10.0 2570-13099.7 3.359.97
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13094.2 2.3694.2
Naphthalene g/L0.50 10.0 2570-13095.2 7.869.52
n-Propylbenzene g/L0.50 10.0 2570-13081.5 1.588.15
Styrene g/L0.50 10.0 2570-13080.9 3.168.09
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130104 1.9310.4
Tetrachloroethylene g/L0.50 10.0 2570-13083.2 0.008.32
Toluene g/L0.50 10.0 2570-13094.3 2.319.43
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13084.5 3.498.45
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13078.5 0.3837.85
1,1,1-Trichloroethane g/L0.50 10.0 2570-130100 0.79410.0
1,1,2-Trichloroethane g/L0.50 10.0 2570-13095.5 2.559.55
Trichloroethylene g/L1.0 10.0 2570-13094.9 2.249.49
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130118 2.7511.8
1,2,3-Trichloropropane g/L0.50 10.0 2570-13088.3 1.718.83
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13092.5 0.7609.25
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13081.1 0.8598.11
Vinyl Acetate g/L5.0 100 2570-13073.4 7.3973.4
Vinyl Chloride g/L0.50 10.0 2560-140101 7.6510.1
m+p Xylene g/L1.0 20.0 2570-13084.3 2.9816.9
o-Xylene g/L1.0 10.0 2570-13084.4 1.768.44
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11528.8
g/L 25.0 70-130Surrogate: Toluene-d8 10526.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 86.821.7
Page 40 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143636 - SW-846 5030B
[TOC_3]B143636[TOC]
Blank (B143636-BLK1) Prepared & Analyzed: 03/07/16
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L1.0ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L1.0ND
Chloromethane g/L1.0ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L1.0ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L1.0ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L1.0ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L1.0ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 41 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143636 - SW-846 5030B
Blank (B143636-BLK1) Prepared & Analyzed: 03/07/16
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L1.0ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L1.0ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11929.8
g/L 25.0 70-130Surrogate: Toluene-d8 99.624.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 86.121.5
LCS (B143636-BS1) Prepared & Analyzed: 03/07/16
Acetone g/L50 100 70-13097.297.2
Benzene g/L0.50 10.0 70-13010910.9
Bromobenzene g/L0.50 10.0 70-13087.18.71
Bromochloromethane g/L0.50 10.0 70-13085.48.54
Bromodichloromethane g/L1.0 10.0 70-13011611.6
Bromoform g/L0.50 10.0 70-13011711.7
Bromomethane g/L2.0 10.0 60-14012212.2
2-Butanone (MEK)g/L5.0 100 70-13089.489.4
n-Butylbenzene g/L0.50 10.0 70-13093.89.38
sec-Butylbenzene g/L0.50 10.0 70-13093.59.35
tert-Butylbenzene g/L0.50 10.0 70-13091.39.13
Carbon Tetrachloride g/L0.50 10.0 70-13011111.1
Chlorobenzene g/L0.50 10.0 70-13088.98.89
Ethanol g/L50 100 70-130119119
Chlorodibromomethane g/L0.50 10.0 70-13011811.8
Chloroethane g/L0.50 10.0 60-14011711.7
Chloroform g/L1.0 10.0 70-13010610.6
Chloromethane g/L1.0 10.0 60-14083.08.30
2-Chlorotoluene g/L0.50 10.0 70-13088.78.87
4-Chlorotoluene g/L0.50 10.0 70-13093.99.39
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13092.29.22
1,2-Dichlorobenzene g/L0.50 10.0 70-13089.38.93
1,3-Dichlorobenzene g/L0.50 10.0 70-13089.78.97
1,4-Dichlorobenzene g/L0.50 10.0 70-13090.19.01
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14083.38.33
1,1-Dichloroethane g/L1.0 10.0 70-13010110.1
1,2-Dichloroethane g/L0.50 10.0 70-13097.29.72
1,1-Dichloroethylene g/L1.0 10.0 70-13011311.3
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13097.19.71
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13092.69.26
1,2-Dichloropropane g/L0.50 10.0 70-13091.79.17
1,3-Dichloropropane g/L1.0 10.0 70-13093.89.38
2,2-Dichloropropane g/L0.50 10.0 70-13010810.8
1,1-Dichloropropene g/L1.0 10.0 70-13010110.1
cis-1,3-Dichloropropene g/L0.50 10.0 70-13097.49.74
trans-1,3-Dichloropropene g/L0.50 10.0 70-13099.29.92
Page 42 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143636 - SW-846 5030B
LCS (B143636-BS1) Prepared & Analyzed: 03/07/16
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13083.28.32
Ethylbenzene g/L0.50 10.0 70-13097.49.74
2-Hexanone (MBK)g/L5.0 100 70-13087.287.2
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13087.08.70
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13093.59.35
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13093.39.33
Methylene Chloride g/L5.0 10.0 70-13093.29.32
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13085.085.0
Naphthalene g/L0.50 10.0 70-13088.48.84
n-Propylbenzene g/L0.50 10.0 70-13088.28.82
Styrene g/L0.50 10.0 70-13086.08.60
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13099.89.98
Tetrachloroethylene g/L0.50 10.0 70-13090.79.07
Toluene g/L0.50 10.0 70-13010410.4
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13084.08.40
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13083.38.33
1,1,1-Trichloroethane g/L0.50 10.0 70-13010410.4
1,1,2-Trichloroethane g/L0.50 10.0 70-13092.39.23
Trichloroethylene g/L1.0 10.0 70-13094.39.43
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13012012.0
1,2,3-Trichloropropane g/L0.50 10.0 70-13090.09.00
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010210.2
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13085.88.58
Vinyl Acetate g/L5.0 100 70-13095.095.0
Vinyl Chloride g/L0.50 10.0 60-14097.79.77
m+p Xylene g/L1.0 20.0 70-13098.419.7
o-Xylene g/L1.0 10.0 70-13094.69.46
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11228.1
g/L 25.0 70-130Surrogate: Toluene-d8 10325.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 91.822.9
LCS Dup (B143636-BSD1) Prepared & Analyzed: 03/07/16
Acetone g/L50 100 2570-13095.1 2.1995.1
Benzene g/L0.50 10.0 2570-130112 2.3611.2
Bromobenzene g/L0.50 10.0 2570-13085.1 2.328.51
Bromochloromethane g/L0.50 10.0 2570-13091.2 6.579.12
Bromodichloromethane g/L1.0 10.0 2570-130113 2.7011.3
Bromoform g/L0.50 10.0 2570-130121 3.5412.1
Bromomethane g/L2.0 10.0 2560-140113 8.0111.3
2-Butanone (MEK)g/L5.0 100 2570-13090.2 0.90290.2
n-Butylbenzene g/L0.50 10.0 2570-13097.9 4.289.79
sec-Butylbenzene g/L0.50 10.0 2570-13093.9 0.4279.39
tert-Butylbenzene g/L0.50 10.0 2570-13093.2 2.069.32
Carbon Tetrachloride g/L0.50 10.0 2570-130118 6.1111.8
Chlorobenzene g/L0.50 10.0 2570-13089.2 0.3378.92
Ethanol g/L50 100 2570-130120 1.42120
Chlorodibromomethane g/L0.50 10.0 2570-130122 3.1712.2
Chloroethane g/L0.50 10.0 2560-140139 16.713.9
Chloroform g/L1.0 10.0 2570-130102 3.1710.2
Chloromethane g/L1.0 10.0 2560-14080.9 2.568.09
2-Chlorotoluene g/L0.50 10.0 2570-13089.1 0.4508.91
4-Chlorotoluene g/L0.50 10.0 2570-13093.5 0.4279.35
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B143636 - SW-846 5030B
LCS Dup (B143636-BSD1) Prepared & Analyzed: 03/07/16
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13094.2 2.159.42
1,2-Dichlorobenzene g/L0.50 10.0 2570-13094.1 5.239.41
1,3-Dichlorobenzene g/L0.50 10.0 2570-13094.1 4.799.41
1,4-Dichlorobenzene g/L0.50 10.0 2570-13093.0 3.179.30
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14086.7 4.008.67
1,1-Dichloroethane g/L1.0 10.0 2570-130102 1.2810.2
1,2-Dichloroethane g/L0.50 10.0 2570-13096.7 0.5169.67
1,1-Dichloroethylene g/L1.0 10.0 2570-130115 1.3211.5
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13093.0 4.319.30
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13091.9 0.7599.19
1,2-Dichloropropane g/L0.50 10.0 2570-13091.3 0.4379.13
1,3-Dichloropropane g/L1.0 10.0 2570-13092.7 1.189.27
2,2-Dichloropropane g/L0.50 10.0 2570-130112 2.8211.2
1,1-Dichloropropene g/L1.0 10.0 2570-13098.1 2.529.81
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13099.1 1.739.91
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13099.9 0.7039.99
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13087.0 4.478.70
Ethylbenzene g/L0.50 10.0 2570-13098.7 1.339.87
2-Hexanone (MBK)g/L5.0 100 2570-13083.6 4.1283.6
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13087.2 0.2308.72
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13096.6 3.269.66
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13098.0 4.919.80
Methylene Chloride g/L5.0 10.0 2570-13098.3 5.339.83
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13084.7 0.38984.7
Naphthalene g/L0.50 10.0 2570-13090.9 2.799.09
n-Propylbenzene g/L0.50 10.0 2570-13088.7 0.5658.87
Styrene g/L0.50 10.0 2570-13086.3 0.3488.63
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130101 1.5910.1
Tetrachloroethylene g/L0.50 10.0 2570-13082.8 9.118.28
Toluene g/L0.50 10.0 2570-130105 1.5310.5
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13089.1 5.898.91
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13087.2 4.578.72
1,1,1-Trichloroethane g/L0.50 10.0 2570-130103 0.87310.3
1,1,2-Trichloroethane g/L0.50 10.0 2570-13090.5 1.979.05
Trichloroethylene g/L1.0 10.0 2570-130101 6.5610.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130127 6.1512.7
1,2,3-Trichloropropane g/L0.50 10.0 2570-13089.6 0.4458.96
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130103 0.48810.3
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13084.8 1.178.48
Vinyl Acetate g/L5.0 100 2570-13094.3 0.70894.3
Vinyl Chloride g/L0.50 10.0 2560-140106 8.2410.6
m+p Xylene g/L1.0 20.0 2570-13098.2 0.20319.6
o-Xylene g/L1.0 10.0 2570-13096.6 2.099.66
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11127.7
g/L 25.0 70-130Surrogate: Toluene-d8 10225.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 89.622.4
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit
DL Method Detection Limit
MCL Maximum Contaminant Level
ND Not Detected
Elevated reporting limits for all volatile compounds due to foaming sample matrix.DL-01
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2018
M-MA100Massachusetts DEPMA 06/30/2016
PH-0567Connecticut Department of Publilc HealthCT 09/30/2017
10899 NELAPNew York State Department of HealthNY 04/1/2016
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2017
LAO00112Rhode Island Department of HealthRI 12/30/2016
652North Carolina Div. of Water QualityNC 12/31/2016
MA007 NELAPNew Jersey DEPNJ 06/30/2016
E871027 NELAPFlorida Department of HealthFL 06/30/2016
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2016
C2065State of Washington Department of EcologyWA 02/23/2016
2011028State of MaineME 06/9/2017
460217Commonwealth of VirginiaVA 12/14/2016
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2016
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Page 1 of 2
CLIENT NAME:RECEIVED BY:DATE:
1) Was the chain(s) of custody relinquished and signed?Yes x No
2) Does the chain agree with the samples?Yes x No
If not, explain:
3) Are all the samples in good condition?Yes x No
If not, explain:
4) How were the samples received:
On Ice x Direct from Sampling Ambient In Cooler(s)x
Were the samples received in Temperature Compliance of (2-6°C)?Yes x No N/A
Temperature °C by Temp blank 3 Temperature °C by Temp gun
5) Are there Dissolved samples for the lab to filter?Yes No x
Who was notified _____________Date ____________Time ___________
6) Are there any RUSH or SHORT HOLDING TIME samples?Yes No x
Who was notified _____________Date ____________Time ___________
Permission to subcontract samples? Yes No
7) Location where samples are stored:(Walk-in clients only) if not already approved
Client Signature: _______________________
8) Do all samples have the proper Acid pH: Yes No N/A x
9) Do all samples have the proper Base pH: Yes No N/A x
10) Was the PC notified of any discrepancies with the CoC vs the samples: Yes N/A x
40 mL vials:# HCl 39 # Methanol Time and Date Frozen:
# Bisulfate # DI Water
# Thiosulfate Unpreserved
Doc# 277
Rev. 4 August 2013
Encore Other
Colisure / bacteria bottle Flashpoint bottle
Dissolved Oxygen bottle Other glass jar
250 mL plastic SOC Kit
40 mL Vial - type listed below 39 Perchlorate Kit
1 Liter Plastic 2 oz amber/clear jar
500 mL Plastic Plastic Bag / Ziploc
500 mL Amber 8 oz amber/clear jar
250 mL Amber (8oz amber)4 oz amber/clear jar
Containers received at Con-Test
# of containers # of containers
1 Liter Amber 16 oz amber
39 Spruce St.
East Longmeadow, MA. 01028
P: 413-525-2332
F: 413-525-6405
www.contestlabs.com Sample Receipt Checklist
ATC Charlotte PB 3/3/2016
No COC Incl.
Login
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Page 2 of 2
Login Sample Receipt Checklist
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
Question Answer (True/False)Comment
T/F/NA
1) The cooler's custody seal, if present, is intact.
3) Samples were received on ice.
4) Cooler Temperature is acceptable.
5) Cooler Temperature is recorded.
6) COC is filled out in ink and legible.
7) COC is filled out with all pertinent information.
8) Field Sampler's name present on COC.
10) Samples are received within Holding Time.
11) Sample containers have legible labels.
12) Containers are not broken or leaking.
13) Air Cassettes are not broken/open.
14) Sample collection date/times are provided.
15) Appropriate sample containers are used.
16) Proper collection media used.
17) No headspace sample bottles are completely filled.
19) Trip blanks provided if applicable.
21) Samples do not require splitting or compositing.
Doc #277 Rev. 4 August 2013 Log-In Technician Initials: PB
Who notified of False statements? Date/Time:
T
18) There is sufficient volume for all requsted
analyses, including any requested MS/MSDs.
NA
Date/Time:3/3/16
T
20) VOA sample vials do not have head space or
bubble is <6mm (1/4") in diameter.
T
T
T
T
T
NA
T
T
9) There are no discrepancies between the
sample IDs on the container and the COC.
T
T
T
T
T
T
T
T
NA
T
2) The cooler or samples do not appear to have
been compromised or tampered with.
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