WS-2669_6146_CA_LAB_20150720

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
July 20, 2015
Andrew Deppensmith
Cardno ATC Associates - Charlotte, NC
7606 Whitehall Executive Drive, Suite 800
Charlotte, NC 28273
Project Location: Moore’s Exxon
Client Job Number:
Project Number: SL6146003
Laboratory Work Order Number: 15G0434
Enclosed are results of analyses for samples received by the laboratory on July 10, 2015. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 55
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 5
Sample Results 8
15G0434-01 8
15G0434-02 10
15G0434-03 12
15G0434-04 14
15G0434-05 16
15G0434-06 18
15G0434-07 20
15G0434-08 22
15G0434-09 24
15G0434-10 26
15G0434-11 28
15G0434-12 30
15G0434-13 32
Sample Preparation Information 34
QC Data 35
Volatile Organic Compounds by GC/MS 35
B126387 35
B126389 39
B126520 43
B126607 47
Flag/Qualifier Summary 48
Certifications 49
Chain of Custody/Sample Receipt 51
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Table of Contents (continued)
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
7/20/2015
Cardno ATC Associates - Charlotte, NC
7606 Whitehall Executive Drive, Suite 800
Charlotte, NC 28273
ATTN: Andrew Deppensmith
SL6146003
15G0434
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Moore’s Exxon
WSW-121 15G0434-01 Ground Water SM21-22 6200B
WSW-248 15G0434-02 Ground Water SM21-22 6200B
WSW-7385 15G0434-03 Ground Water SM21-22 6200B
WSW-7414 15G0434-04 Ground Water SM21-22 6200B
WSW-7471 15G0434-05 Ground Water SM21-22 6200B
MW-1 15G0434-06 Ground Water SM21-22 6200B
MW-1R 15G0434-07 Ground Water SM21-22 6200B
MW-3R 15G0434-08 Ground Water SM21-22 6200B
MW-5 15G0434-09 Ground Water SM21-22 6200B
MW-10R 15G0434-10 Ground Water SM21-22 6200B
MW-11 15G0434-11 Ground Water SM21-22 6200B
MW-12 15G0434-12 Ground Water SM21-22 6200B
MW-13 15G0434-13 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For 6200B method, Samples15G0434-06 was run at a dilution as concentration of target compounds exceeded calibration curve limits.
[TOC_1]Case Narrative[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SM21-22 6200B
Qualifications:
Analyte is found in the associated blank as well as in the sample.
Analyte & Samples(s) Qualified:
B
Acetone
15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-06[MW-1], 15G0434-07[MW-1R], 15G0434-09[MW-5], 15G0434-10[MW-10R],
15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13], B126387-BLK1, B126389-BLK1
Methylene chloride is a common laboratory contaminant.
Analyte & Samples(s) Qualified:
B-01
Acetone
15G0434-01[WSW-121], 15G0434-02[WSW-248]
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
2,2-Dichloropropane
15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-06[MW-1], 15G0434-07[MW-1R], 15G0434-09[MW-5], 15G0434-10[MW-10R],
15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13], B126389-BLK1, B126389-BS1, B126389-BSD1
Naphthalene
B126520-BLK1, B126520-BS1, B126520-BSD1
Vinyl Chloride
15G0434-01[WSW-121], 15G0434-02[WSW-248], B126387-BLK1, B126387-BS1, B126387-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.Analyte & Samples(s) Qualified:
L-07A
Vinyl Chloride
B126389-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Bromomethane
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-06[MW-1],
15G0434-07[MW-1R], 15G0434-08[MW-3R], 15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13],
B126387-BLK1, B126387-BS1, B126387-BSD1, B126389-BLK1, B126389-BS1, B126389-BSD1, B126520-BLK1, B126520-BS1, B126520-BSD1
Vinyl Chloride
15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-06[MW-1], 15G0434-07[MW-1R], 15G0434-09[MW-5], 15G0434-10[MW-10R],
15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13], B126389-BLK1, B126389-BS1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Elevated reporting limit based on lowest point in calibration.
Requested reporting limit not met.
Analyte & Samples(s) Qualified:
RL-03
1,2,3-Trichloropropane
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
1,2-Dichloroethane
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
2,2-Dichloropropane
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
2-Butanone (MEK)
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
Bromoform
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
Carbon Tetrachloride
15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R], 15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11],
15G0434-12[MW-12], 15G0434-13[MW-13]
n-Propylbenzene
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
Tetrachloroethylene
15G0434-01[WSW-121], 15G0434-02[WSW-248], 15G0434-03[WSW-7385], 15G0434-04[WSW-7414], 15G0434-05[WSW-7471], 15G0434-07[MW-1R],
15G0434-09[MW-5], 15G0434-10[MW-10R], 15G0434-11[MW-11], 15G0434-12[MW-12], 15G0434-13[MW-13]
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
15G0434-06[MW-1]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Laboratory Manager
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-01
Field Sample #: WSW-121
Sample Matrix: Ground Water
Sampled: 7/8/2015 15:15
[TOC_2]15G0434-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
7.2 50 7/18/15 11:04 CMRg/L4.7 7/16/15SM21-22 6200B1B-01, JAcetone
ND 0.50 7/18/15 11:04 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/18/15 11:04 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/18/15 11:04 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/18/15 11:04 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/18/15 11:04 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/18/15 11:04 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/18/15 11:04 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/18/15 11:04 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/18/15 11:04 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/18/15 11:04 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/18/15 11:04 CMRg/L0.10 7/16/15SM21-22 6200B1Carbon Tetrachloride
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/18/15 11:04 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/18/15 11:04 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/18/15 11:04 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/18/15 11:04 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/18/15 11:04 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/18/15 11:04 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/18/15 11:04 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/18/15 11:04 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/18/15 11:04 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/18/15 11:04 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/18/15 11:04 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/18/15 11:04 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/18/15 11:04 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/18/15 11:04 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/18/15 11:04 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/18/15 11:04 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/18/15 11:04 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/18/15 11:04 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/18/15 11:04 CMRg/L0.072 7/16/15SM21-22 6200B1RL-032,2-Dichloropropane
ND 0.50 7/18/15 11:04 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/18/15 11:04 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/18/15 11:04 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/18/15 11:04 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/18/15 11:04 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/18/15 11:04 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/18/15 11:04 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/18/15 11:04 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/18/15 11:04 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/18/15 11:04 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-01
Field Sample #: WSW-121
Sample Matrix: Ground Water
Sampled: 7/8/2015 15:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/18/15 11:04 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/18/15 11:04 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/18/15 11:04 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/18/15 11:04 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/18/15 11:04 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/18/15 11:04 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/18/15 11:04 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 2.0 7/18/15 11:04 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/18/15 11:04 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/18/15 11:04 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/18/15 11:04 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/18/15 11:04 CMRg/L0.13 7/16/15SM21-22 6200B1L-04Vinyl Chloride
ND 1.0 7/18/15 11:04 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/18/15 11:04 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.2 7/18/15 11:0470-130
Toluene-d8 98.2 7/18/15 11:0470-130
4-Bromofluorobenzene 94.6 7/18/15 11:0470-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-02
Field Sample #: WSW-248
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:30
[TOC_2]15G0434-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
7.0 50 7/18/15 11:30 CMRg/L4.7 7/16/15SM21-22 6200B1B-01, JAcetone
ND 0.50 7/18/15 11:30 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/18/15 11:30 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/18/15 11:30 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/18/15 11:30 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/18/15 11:30 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/18/15 11:30 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/18/15 11:30 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/18/15 11:30 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/18/15 11:30 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/18/15 11:30 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/18/15 11:30 CMRg/L0.10 7/16/15SM21-22 6200B1Carbon Tetrachloride
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/18/15 11:30 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/18/15 11:30 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/18/15 11:30 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/18/15 11:30 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/18/15 11:30 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/18/15 11:30 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/18/15 11:30 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/18/15 11:30 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/18/15 11:30 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/18/15 11:30 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/18/15 11:30 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/18/15 11:30 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/18/15 11:30 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/18/15 11:30 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/18/15 11:30 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/18/15 11:30 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/18/15 11:30 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/18/15 11:30 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/18/15 11:30 CMRg/L0.072 7/16/15SM21-22 6200B1RL-032,2-Dichloropropane
ND 0.50 7/18/15 11:30 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/18/15 11:30 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/18/15 11:30 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/18/15 11:30 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/18/15 11:30 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/18/15 11:30 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/18/15 11:30 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/18/15 11:30 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/18/15 11:30 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/18/15 11:30 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 10 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-02
Field Sample #: WSW-248
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/18/15 11:30 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/18/15 11:30 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/18/15 11:30 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/18/15 11:30 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/18/15 11:30 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/18/15 11:30 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/18/15 11:30 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 2.0 7/18/15 11:30 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/18/15 11:30 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/18/15 11:30 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/18/15 11:30 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/18/15 11:30 CMRg/L0.13 7/16/15SM21-22 6200B1L-04Vinyl Chloride
ND 1.0 7/18/15 11:30 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/18/15 11:30 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.3 7/18/15 11:3070-130
Toluene-d8 100 7/18/15 11:3070-130
4-Bromofluorobenzene 94.9 7/18/15 11:3070-130
Page 11 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-03
Field Sample #: WSW-7385
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:45
[TOC_2]15G0434-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
6.6 50 7/18/15 23:42 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/18/15 23:42 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/18/15 23:42 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/18/15 23:42 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/18/15 23:42 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/18/15 23:42 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/18/15 23:42 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/18/15 23:42 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/18/15 23:42 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/18/15 23:42 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/18/15 23:42 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/18/15 23:42 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/18/15 23:42 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/18/15 23:42 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/18/15 23:42 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/18/15 23:42 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/18/15 23:42 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/18/15 23:42 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/18/15 23:42 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/18/15 23:42 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/18/15 23:42 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/18/15 23:42 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/18/15 23:42 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/18/15 23:42 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/18/15 23:42 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/18/15 23:42 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/18/15 23:42 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/18/15 23:42 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/18/15 23:42 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/18/15 23:42 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/18/15 23:42 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/18/15 23:42 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/18/15 23:42 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/18/15 23:42 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/18/15 23:42 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/18/15 23:42 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/18/15 23:42 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/18/15 23:42 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.32 0.50 7/18/15 23:42 CMRg/L0.090 7/16/15SM21-22 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 7/18/15 23:42 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/18/15 23:42 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 12 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-03
Field Sample #: WSW-7385
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/18/15 23:42 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/18/15 23:42 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/18/15 23:42 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/18/15 23:42 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/18/15 23:42 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/18/15 23:42 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/18/15 23:42 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/18/15 23:42 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/18/15 23:42 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/18/15 23:42 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/18/15 23:42 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/18/15 23:42 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/18/15 23:42 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/18/15 23:42 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.9 7/18/15 23:4270-130
Toluene-d8 98.3 7/18/15 23:4270-130
4-Bromofluorobenzene 96.2 7/18/15 23:4270-130
Page 13 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-04
Field Sample #: WSW-7414
Sample Matrix: Ground Water
Sampled: 7/8/2015 15:00
[TOC_2]15G0434-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
7.2 50 7/19/15 0:12 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 0:12 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 0:12 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 0:12 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 0:12 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 0:12 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 0:12 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 0:12 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 0:12 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 0:12 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 0:12 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 0:12 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 0:12 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 0:12 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 0:12 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 0:12 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 0:12 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 0:12 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 0:12 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 0:12 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 0:12 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 0:12 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 0:12 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 0:12 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 0:12 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 0:12 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 0:12 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 0:12 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 0:12 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 0:12 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 0:12 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/19/15 0:12 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 0:12 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 0:12 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
0.40 0.50 7/19/15 0:12 CMRg/L0.18 7/16/15SM21-22 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 7/19/15 0:12 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 0:12 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 0:12 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.41 0.50 7/19/15 0:12 CMRg/L0.090 7/16/15SM21-22 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 0:12 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 0:12 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 14 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-04
Field Sample #: WSW-7414
Sample Matrix: Ground Water
Sampled: 7/8/2015 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 0:12 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 0:12 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 0:12 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 0:12 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 0:12 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 0:12 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 0:12 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 0:12 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 0:12 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 0:12 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 0:12 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 0:12 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 0:12 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 0:12 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.2 7/19/15 0:1270-130
Toluene-d8 100 7/19/15 0:1270-130
4-Bromofluorobenzene 95.0 7/19/15 0:1270-130
Page 15 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-05
Field Sample #: WSW-7471
Sample Matrix: Ground Water
Sampled: 7/8/2015 15:30
[TOC_2]15G0434-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
8.6 50 7/19/15 0:38 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 0:38 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 0:38 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 0:38 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 0:38 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 0:38 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 0:38 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 0:38 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 0:38 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 0:38 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 0:38 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 0:38 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 0:38 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 0:38 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 0:38 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 0:38 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 0:38 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 0:38 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 0:38 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 0:38 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 0:38 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 0:38 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 0:38 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 0:38 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 0:38 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 0:38 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 0:38 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 0:38 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 0:38 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 0:38 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 0:38 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/19/15 0:38 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 0:38 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 0:38 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/19/15 0:38 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/19/15 0:38 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 0:38 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 0:38 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/19/15 0:38 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 0:38 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 0:38 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 16 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-05
Field Sample #: WSW-7471
Sample Matrix: Ground Water
Sampled: 7/8/2015 15:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 0:38 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 0:38 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 0:38 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 0:38 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 0:38 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 0:38 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 0:38 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 0:38 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 0:38 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 0:38 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 0:38 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 0:38 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 0:38 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 0:38 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 100 7/19/15 0:3870-130
Toluene-d8 100 7/19/15 0:3870-130
4-Bromofluorobenzene 94.9 7/19/15 0:3870-130
Page 17 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-06
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 7/8/2015 12:45
[TOC_2]15G0434-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
6500 50000 7/19/15 8:40 CMRg/L4700 7/16/15SM21-22 6200B1000B, JAcetone
8400 500 7/19/15 8:40 CMRg/L79 7/16/15SM21-22 6200B1000Benzene
ND 500 7/19/15 8:40 CMRg/L44 7/16/15SM21-22 6200B1000Bromobenzene
ND 500 7/19/15 8:40 CMRg/L220 7/16/15SM21-22 6200B1000Bromochloromethane
ND 500 7/19/15 8:40 CMRg/L88 7/16/15SM21-22 6200B1000Bromodichloromethane
ND 1000 7/19/15 8:40 CMRg/L210 7/16/15SM21-22 6200B1000Bromoform
ND 1000 7/19/15 8:40 CMRg/L940 7/16/15SM21-22 6200B1000R-05Bromomethane
ND 10000 7/19/15 8:40 CMRg/L2400 7/16/15SM21-22 6200B10002-Butanone (MEK)
ND 500 7/19/15 8:40 CMRg/L54 7/16/15SM21-22 6200B1000n-Butylbenzene
ND 500 7/19/15 8:40 CMRg/L84 7/16/15SM21-22 6200B1000sec-Butylbenzene
ND 500 7/19/15 8:40 CMRg/L96 7/16/15SM21-22 6200B1000tert-Butylbenzene
ND 1000 7/19/15 8:40 CMRg/L100 7/16/15SM21-22 6200B1000Carbon Tetrachloride
ND 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B1000Chlorobenzene
ND 50000 7/19/15 8:40 CMRg/L28000 7/16/15SM21-22 6200B1000Ethanol
ND 500 7/19/15 8:40 CMRg/L54 7/16/15SM21-22 6200B1000Chlorodibromomethane
ND 500 7/19/15 8:40 CMRg/L160 7/16/15SM21-22 6200B1000Chloroethane
ND 500 7/19/15 8:40 CMRg/L140 7/16/15SM21-22 6200B1000Chloroform
ND 500 7/19/15 8:40 CMRg/L320 7/16/15SM21-22 6200B1000Chloromethane
ND 500 7/19/15 8:40 CMRg/L70 7/16/15SM21-22 6200B10002-Chlorotoluene
390 500 7/19/15 8:40 CMRg/L74 7/16/15SM21-22 6200B1000J4-Chlorotoluene
ND 500 7/19/15 8:40 CMRg/L89 7/16/15SM21-22 6200B10001,2-Dibromoethane (EDB)
ND 500 7/19/15 8:40 CMRg/L76 7/16/15SM21-22 6200B10001,2-Dichlorobenzene
ND 500 7/19/15 8:40 CMRg/L79 7/16/15SM21-22 6200B10001,3-Dichlorobenzene
ND 500 7/19/15 8:40 CMRg/L46 7/16/15SM21-22 6200B10001,4-Dichlorobenzene
ND 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B1000Dichlorodifluoromethane (Freon 12)
ND 500 7/19/15 8:40 CMRg/L160 7/16/15SM21-22 6200B10001,1-Dichloroethane
ND 1000 7/19/15 8:40 CMRg/L190 7/16/15SM21-22 6200B10001,2-Dichloroethane
ND 500 7/19/15 8:40 CMRg/L210 7/16/15SM21-22 6200B10001,1-Dichloroethylene
ND 500 7/19/15 8:40 CMRg/L150 7/16/15SM21-22 6200B1000cis-1,2-Dichloroethylene
ND 500 7/19/15 8:40 CMRg/L150 7/16/15SM21-22 6200B1000trans-1,2-Dichloroethylene
ND 500 7/19/15 8:40 CMRg/L110 7/16/15SM21-22 6200B10001,2-Dichloropropane
ND 500 7/19/15 8:40 CMRg/L99 7/16/15SM21-22 6200B10001,3-Dichloropropane
ND 1000 7/19/15 8:40 CMRg/L72 7/16/15SM21-22 6200B1000L-042,2-Dichloropropane
ND 500 7/19/15 8:40 CMRg/L130 7/16/15SM21-22 6200B10001,1-Dichloropropene
ND 500 7/19/15 8:40 CMRg/L62 7/16/15SM21-22 6200B1000cis-1,3-Dichloropropene
ND 500 7/19/15 8:40 CMRg/L56 7/16/15SM21-22 6200B1000trans-1,3-Dichloropropene
5000 500 7/19/15 8:40 CMRg/L180 7/16/15SM21-22 6200B1000Diisopropyl Ether (DIPE)
6700 500 7/19/15 8:40 CMRg/L92 7/16/15SM21-22 6200B1000Ethylbenzene
ND 5000 7/19/15 8:40 CMRg/L1500 7/16/15SM21-22 6200B10002-Hexanone (MBK)
210 500 7/19/15 8:40 CMRg/L110 7/16/15SM21-22 6200B1000JIsopropylbenzene (Cumene)
ND 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B1000p-Isopropyltoluene (p-Cymene)
280 500 7/19/15 8:40 CMRg/L90 7/16/15SM21-22 6200B1000JMethyl tert-Butyl Ether (MTBE)
ND 5000 7/19/15 8:40 CMRg/L3200 7/16/15SM21-22 6200B1000Methylene Chloride
ND 5000 7/19/15 8:40 CMRg/L1500 7/16/15SM21-22 6200B10004-Methyl-2-pentanone (MIBK)
Page 18 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-06
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 7/8/2015 12:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
2100 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B1000Naphthalene
470 1000 7/19/15 8:40 CMRg/L94 7/16/15SM21-22 6200B1000Jn-Propylbenzene
250 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B1000JStyrene
ND 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B10001,1,2,2-Tetrachloroethane
ND 1000 7/19/15 8:40 CMRg/L80 7/16/15SM21-22 6200B1000Tetrachloroethylene
110000 500 7/19/15 8:40 CMRg/L90 7/16/15SM21-22 6200B1000Toluene
ND 500 7/19/15 8:40 CMRg/L140 7/16/15SM21-22 6200B10001,2,3-Trichlorobenzene
ND 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B10001,2,4-Trichlorobenzene
ND 500 7/19/15 8:40 CMRg/L94 7/16/15SM21-22 6200B10001,1,1-Trichloroethane
ND 500 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B10001,1,2-Trichloroethane
ND 500 7/19/15 8:40 CMRg/L77 7/16/15SM21-22 6200B1000Trichloroethylene
ND 500 7/19/15 8:40 CMRg/L150 7/16/15SM21-22 6200B1000Trichlorofluoromethane (Freon 11)
ND 1000 7/19/15 8:40 CMRg/L120 7/16/15SM21-22 6200B10001,2,3-Trichloropropane
4500 500 7/19/15 8:40 CMRg/L180 7/16/15SM21-22 6200B10001,2,4-Trimethylbenzene
1100 500 7/19/15 8:40 CMRg/L100 7/16/15SM21-22 6200B10001,3,5-Trimethylbenzene
ND 5000 7/19/15 8:40 CMRg/L1300 7/16/15SM21-22 6200B1000Vinyl Acetate
ND 500 7/19/15 8:40 CMRg/L130 7/16/15SM21-22 6200B1000R-05Vinyl Chloride
26000 1000 7/19/15 8:40 CMRg/L180 7/16/15SM21-22 6200B1000m+p Xylene
12000 500 7/19/15 8:40 CMRg/L110 7/16/15SM21-22 6200B1000o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.0 7/19/15 8:4070-130
Toluene-d8 99.9 7/19/15 8:4070-130
4-Bromofluorobenzene 98.4 7/19/15 8:4070-130
Page 19 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-07
Field Sample #: MW-1R
Sample Matrix: Ground Water
Sampled: 7/8/2015 12:30
[TOC_2]15G0434-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
13 50 7/19/15 2:31 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
0.98 0.50 7/19/15 2:31 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 2:31 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 2:31 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 2:31 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 2:31 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 2:31 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 2:31 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 2:31 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 2:31 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 2:31 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 2:31 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 2:31 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 2:31 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 2:31 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 2:31 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 2:31 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 2:31 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 2:31 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 2:31 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 2:31 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 2:31 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 2:31 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 2:31 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 2:31 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 2:31 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 2:31 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 2:31 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 2:31 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 2:31 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 2:31 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/19/15 2:31 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 2:31 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 2:31 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
8.8 0.50 7/19/15 2:31 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
2.0 0.50 7/19/15 2:31 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 2:31 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
0.12 0.50 7/19/15 2:31 CMRg/L0.11 7/16/15SM21-22 6200B1JIsopropylbenzene (Cumene)
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
20 0.50 7/19/15 2:31 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 2:31 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 2:31 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 20 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-07
Field Sample #: MW-1R
Sample Matrix: Ground Water
Sampled: 7/8/2015 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
1.6 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
0.18 1.0 7/19/15 2:31 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03, Jn-Propylbenzene
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 2:31 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
2.2 0.50 7/19/15 2:31 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 2:31 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 2:31 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 2:31 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 2:31 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 2:31 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
5.2 0.50 7/19/15 2:31 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
0.69 0.50 7/19/15 2:31 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 2:31 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 2:31 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
9.6 1.0 7/19/15 2:31 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
3.1 0.50 7/19/15 2:31 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 95.9 7/19/15 2:3170-130
Toluene-d8 98.8 7/19/15 2:3170-130
4-Bromofluorobenzene 98.5 7/19/15 2:3170-130
Page 21 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-08
Field Sample #: MW-3R
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:00
[TOC_2]15G0434-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 7/20/15 11:34 MFFg/L4.7 7/16/15SM21-22 6200B1Acetone
25 0.50 7/20/15 11:34 MFFg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/20/15 11:34 MFFg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/20/15 11:34 MFFg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/20/15 11:34 MFFg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 0.50 7/20/15 11:34 MFFg/L0.21 7/16/15SM21-22 6200B1Bromoform
ND 1.0 7/20/15 11:34 MFFg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 5.0 7/20/15 11:34 MFFg/L2.4 7/16/15SM21-22 6200B12-Butanone (MEK)
24 0.50 7/20/15 11:34 MFFg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
12 1.0 7/20/15 11:34 MFFg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
2.0 0.50 7/20/15 11:34 MFFg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 0.50 7/20/15 11:34 MFFg/L0.10 7/16/15SM21-22 6200B1Carbon Tetrachloride
ND 0.50 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/20/15 11:34 MFFg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/20/15 11:34 MFFg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/20/15 11:34 MFFg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/20/15 11:34 MFFg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/20/15 11:34 MFFg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/20/15 11:34 MFFg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 1.0 7/20/15 11:34 MFFg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 1.0 7/20/15 11:34 MFFg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/20/15 11:34 MFFg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/20/15 11:34 MFFg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/20/15 11:34 MFFg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/20/15 11:34 MFFg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 0.50 7/20/15 11:34 MFFg/L0.19 7/16/15SM21-22 6200B11,2-Dichloroethane
ND 0.50 7/20/15 11:34 MFFg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/20/15 11:34 MFFg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/20/15 11:34 MFFg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/20/15 11:34 MFFg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/20/15 11:34 MFFg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/20/15 11:34 MFFg/L0.072 7/16/15SM21-22 6200B12,2-Dichloropropane
ND 0.50 7/20/15 11:34 MFFg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/20/15 11:34 MFFg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/20/15 11:34 MFFg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
3.8 0.50 7/20/15 11:34 MFFg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
110 0.50 7/20/15 11:34 MFFg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 20 7/20/15 11:34 MFFg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
51 0.50 7/20/15 11:34 MFFg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
12 0.50 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/20/15 11:34 MFFg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/20/15 11:34 MFFg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 10 7/20/15 11:34 MFFg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 22 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-08
Field Sample #: MW-3R
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
160 0.50 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B1Naphthalene
160 0.50 7/20/15 11:34 MFFg/L0.094 7/16/15SM21-22 6200B1n-Propylbenzene
ND 2.0 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 1.0 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 7/20/15 11:34 MFFg/L0.080 7/16/15SM21-22 6200B1Tetrachloroethylene
4.6 0.50 7/20/15 11:34 MFFg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/20/15 11:34 MFFg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/20/15 11:34 MFFg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/20/15 11:34 MFFg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/20/15 11:34 MFFg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/20/15 11:34 MFFg/L0.12 7/16/15SM21-22 6200B11,2,3-Trichloropropane
490 25 7/19/15 8:08 CMRg/L9.0 7/18/15SM21-22 6200B501,2,4-Trimethylbenzene
98 0.50 7/20/15 11:34 MFFg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 10 7/20/15 11:34 MFFg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/20/15 11:34 MFFg/L0.13 7/16/15SM21-22 6200B1Vinyl Chloride
50 1.0 7/20/15 11:34 MFFg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
5.3 0.50 7/20/15 11:34 MFFg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.4 7/20/15 11:3470-130
1,2-Dichloroethane-d4 101 7/19/15 8:0870-130
Toluene-d8 99.9 7/20/15 11:3470-130
Toluene-d8 101 7/19/15 8:0870-130
4-Bromofluorobenzene 101 7/20/15 11:3470-130
4-Bromofluorobenzene 96.4 7/19/15 8:0870-130
Page 23 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-09
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:15
[TOC_2]15G0434-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
5.5 50 7/19/15 3:02 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 3:02 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 3:02 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 3:02 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 3:02 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 3:02 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 3:02 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 3:02 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 3:02 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 3:02 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 3:02 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 3:02 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 3:02 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 3:02 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 3:02 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 3:02 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 3:02 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 3:02 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 3:02 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 3:02 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 3:02 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 3:02 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 3:02 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 3:02 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 3:02 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 3:02 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 3:02 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 3:02 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 3:02 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 3:02 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 3:02 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/19/15 3:02 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 3:02 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 3:02 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/19/15 3:02 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/19/15 3:02 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 3:02 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 3:02 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/19/15 3:02 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 3:02 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 3:02 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-09
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 3:02 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 3:02 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 3:02 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 3:02 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 3:02 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 3:02 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 3:02 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 3:02 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 3:02 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 3:02 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 3:02 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 3:02 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 3:02 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 3:02 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.3 7/19/15 3:0270-130
Toluene-d8 98.7 7/19/15 3:0270-130
4-Bromofluorobenzene 95.6 7/19/15 3:0270-130
Page 25 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-10
Field Sample #: MW-10R
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:15
[TOC_2]15G0434-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
8.9 50 7/19/15 3:28 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 3:28 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 3:28 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 3:28 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 3:28 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 3:28 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 3:28 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 3:28 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 3:28 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 3:28 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 3:28 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 3:28 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 3:28 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 3:28 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 3:28 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 3:28 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 3:28 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 3:28 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 3:28 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 3:28 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 3:28 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 3:28 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 3:28 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 3:28 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 3:28 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 3:28 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 3:28 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 3:28 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 3:28 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 3:28 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 3:28 CMRg/L0.072 7/16/15SM21-22 6200B1RL-03, L-042,2-Dichloropropane
ND 0.50 7/19/15 3:28 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 3:28 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 3:28 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/19/15 3:28 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/19/15 3:28 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 3:28 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 3:28 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/19/15 3:28 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 3:28 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 3:28 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 26 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-10
Field Sample #: MW-10R
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 3:28 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 3:28 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 3:28 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 3:28 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 3:28 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 3:28 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 3:28 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 3:28 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 3:28 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 3:28 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 3:28 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 3:28 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 3:28 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 3:28 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.2 7/19/15 3:2870-130
Toluene-d8 99.7 7/19/15 3:2870-130
4-Bromofluorobenzene 95.0 7/19/15 3:2870-130
Page 27 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-11
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:45
[TOC_2]15G0434-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
5.9 50 7/19/15 3:58 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 3:58 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 3:58 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 3:58 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 3:58 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 3:58 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 3:58 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 3:58 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 3:58 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 3:58 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 3:58 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 3:58 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 3:58 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 3:58 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 3:58 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 3:58 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 3:58 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 3:58 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 3:58 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 3:58 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 3:58 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 3:58 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 3:58 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 3:58 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 3:58 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 3:58 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 3:58 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 3:58 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 3:58 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 3:58 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 3:58 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/19/15 3:58 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 3:58 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 3:58 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/19/15 3:58 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/19/15 3:58 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 3:58 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 3:58 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/19/15 3:58 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 3:58 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 3:58 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-11
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 3:58 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 3:58 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 3:58 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 3:58 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 3:58 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 3:58 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 3:58 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 3:58 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 3:58 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 3:58 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 3:58 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 3:58 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 3:58 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 3:58 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.0 7/19/15 3:5870-130
Toluene-d8 98.4 7/19/15 3:5870-130
4-Bromofluorobenzene 95.4 7/19/15 3:5870-130
Page 29 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-12
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:30
[TOC_2]15G0434-12[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
6.0 50 7/19/15 4:24 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 4:24 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 4:24 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 4:24 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 4:24 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 4:24 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 4:24 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 4:24 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 4:24 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 4:24 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 4:24 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 4:24 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 4:24 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 4:24 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 4:24 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 4:24 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 4:24 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 4:24 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 4:24 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 4:24 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 4:24 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 4:24 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 4:24 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 4:24 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 4:24 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 4:24 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 4:24 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 4:24 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 4:24 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 4:24 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 4:24 CMRg/L0.072 7/16/15SM21-22 6200B1L-04, RL-032,2-Dichloropropane
ND 0.50 7/19/15 4:24 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 4:24 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 4:24 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/19/15 4:24 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/19/15 4:24 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 4:24 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 4:24 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/19/15 4:24 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 4:24 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 4:24 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 30 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-12
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 7/8/2015 13:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 4:24 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 4:24 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 4:24 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 4:24 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 4:24 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 4:24 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 4:24 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 4:24 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 4:24 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 4:24 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 4:24 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 4:24 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 4:24 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 4:24 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.0 7/19/15 4:2470-130
Toluene-d8 99.0 7/19/15 4:2470-130
4-Bromofluorobenzene 95.4 7/19/15 4:2470-130
Page 31 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-13
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:00
[TOC_2]15G0434-13[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
8.7 50 7/19/15 7:11 CMRg/L4.7 7/16/15SM21-22 6200B1B, JAcetone
ND 0.50 7/19/15 7:11 CMRg/L0.079 7/16/15SM21-22 6200B1Benzene
ND 0.50 7/19/15 7:11 CMRg/L0.044 7/16/15SM21-22 6200B1Bromobenzene
ND 0.50 7/19/15 7:11 CMRg/L0.22 7/16/15SM21-22 6200B1Bromochloromethane
ND 0.50 7/19/15 7:11 CMRg/L0.088 7/16/15SM21-22 6200B1Bromodichloromethane
ND 1.0 7/19/15 7:11 CMRg/L0.21 7/16/15SM21-22 6200B1RL-03Bromoform
ND 1.0 7/19/15 7:11 CMRg/L0.94 7/16/15SM21-22 6200B1R-05Bromomethane
ND 10 7/19/15 7:11 CMRg/L2.4 7/16/15SM21-22 6200B1RL-032-Butanone (MEK)
ND 0.50 7/19/15 7:11 CMRg/L0.054 7/16/15SM21-22 6200B1n-Butylbenzene
ND 0.50 7/19/15 7:11 CMRg/L0.084 7/16/15SM21-22 6200B1sec-Butylbenzene
ND 0.50 7/19/15 7:11 CMRg/L0.096 7/16/15SM21-22 6200B1tert-Butylbenzene
ND 1.0 7/19/15 7:11 CMRg/L0.10 7/16/15SM21-22 6200B1RL-03Carbon Tetrachloride
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B1Chlorobenzene
ND 50 7/19/15 7:11 CMRg/L28 7/16/15SM21-22 6200B1Ethanol
ND 0.50 7/19/15 7:11 CMRg/L0.054 7/16/15SM21-22 6200B1Chlorodibromomethane
ND 0.50 7/19/15 7:11 CMRg/L0.16 7/16/15SM21-22 6200B1Chloroethane
ND 0.50 7/19/15 7:11 CMRg/L0.14 7/16/15SM21-22 6200B1Chloroform
ND 0.50 7/19/15 7:11 CMRg/L0.32 7/16/15SM21-22 6200B1Chloromethane
ND 0.50 7/19/15 7:11 CMRg/L0.070 7/16/15SM21-22 6200B12-Chlorotoluene
ND 0.50 7/19/15 7:11 CMRg/L0.074 7/16/15SM21-22 6200B14-Chlorotoluene
ND 0.50 7/19/15 7:11 CMRg/L0.089 7/16/15SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 7/19/15 7:11 CMRg/L0.076 7/16/15SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 7/19/15 7:11 CMRg/L0.079 7/16/15SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 7/19/15 7:11 CMRg/L0.046 7/16/15SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 7/19/15 7:11 CMRg/L0.16 7/16/15SM21-22 6200B11,1-Dichloroethane
ND 1.0 7/19/15 7:11 CMRg/L0.19 7/16/15SM21-22 6200B1RL-031,2-Dichloroethane
ND 0.50 7/19/15 7:11 CMRg/L0.21 7/16/15SM21-22 6200B11,1-Dichloroethylene
ND 0.50 7/19/15 7:11 CMRg/L0.15 7/16/15SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 7/19/15 7:11 CMRg/L0.15 7/16/15SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 7/19/15 7:11 CMRg/L0.11 7/16/15SM21-22 6200B11,2-Dichloropropane
ND 0.50 7/19/15 7:11 CMRg/L0.099 7/16/15SM21-22 6200B11,3-Dichloropropane
ND 1.0 7/19/15 7:11 CMRg/L0.072 7/16/15SM21-22 6200B1RL-03, L-042,2-Dichloropropane
ND 0.50 7/19/15 7:11 CMRg/L0.13 7/16/15SM21-22 6200B11,1-Dichloropropene
ND 0.50 7/19/15 7:11 CMRg/L0.062 7/16/15SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 7/19/15 7:11 CMRg/L0.056 7/16/15SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 7/19/15 7:11 CMRg/L0.18 7/16/15SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 7/19/15 7:11 CMRg/L0.092 7/16/15SM21-22 6200B1Ethylbenzene
ND 5.0 7/19/15 7:11 CMRg/L1.5 7/16/15SM21-22 6200B12-Hexanone (MBK)
ND 0.50 7/19/15 7:11 CMRg/L0.11 7/16/15SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 7/19/15 7:11 CMRg/L0.090 7/16/15SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 7/19/15 7:11 CMRg/L3.2 7/16/15SM21-22 6200B1Methylene Chloride
ND 5.0 7/19/15 7:11 CMRg/L1.5 7/16/15SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 32 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/10/2015
Work Order: 15G0434Sample Description:Project Location: Moore’s Exxon
Sample ID: 15G0434-13
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 7/8/2015 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B1Naphthalene
ND 1.0 7/19/15 7:11 CMRg/L0.094 7/16/15SM21-22 6200B1RL-03n-Propylbenzene
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B1Styrene
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 1.0 7/19/15 7:11 CMRg/L0.080 7/16/15SM21-22 6200B1RL-03Tetrachloroethylene
ND 0.50 7/19/15 7:11 CMRg/L0.090 7/16/15SM21-22 6200B1Toluene
ND 0.50 7/19/15 7:11 CMRg/L0.14 7/16/15SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 7/19/15 7:11 CMRg/L0.094 7/16/15SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 7/19/15 7:11 CMRg/L0.077 7/16/15SM21-22 6200B1Trichloroethylene
ND 0.50 7/19/15 7:11 CMRg/L0.15 7/16/15SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 7/19/15 7:11 CMRg/L0.12 7/16/15SM21-22 6200B1RL-031,2,3-Trichloropropane
ND 0.50 7/19/15 7:11 CMRg/L0.18 7/16/15SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 7/19/15 7:11 CMRg/L0.10 7/16/15SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 7/19/15 7:11 CMRg/L1.3 7/16/15SM21-22 6200B1Vinyl Acetate
ND 0.50 7/19/15 7:11 CMRg/L0.13 7/16/15SM21-22 6200B1R-05Vinyl Chloride
ND 1.0 7/19/15 7:11 CMRg/L0.18 7/16/15SM21-22 6200B1m+p Xylene
ND 0.50 7/19/15 7:11 CMRg/L0.11 7/16/15SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.9 7/19/15 7:1170-130
Toluene-d8 100 7/19/15 7:1170-130
4-Bromofluorobenzene 95.4 7/19/15 7:1170-130
Page 33 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B126387 07/16/155 5.0015G0434-01 [WSW-121]
B126387 07/16/155 5.0015G0434-02 [WSW-248]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B126389 07/16/155 5.0015G0434-03 [WSW-7385]
B126389 07/16/155 5.0015G0434-04 [WSW-7414]
B126389 07/16/155 5.0015G0434-05 [WSW-7471]
B126389 07/16/150.005 5.0015G0434-06 [MW-1]
B126389 07/16/155 5.0015G0434-07 [MW-1R]
B126389 07/16/155 5.0015G0434-09 [MW-5]
B126389 07/16/155 5.0015G0434-10 [MW-10R]
B126389 07/16/155 5.0015G0434-11 [MW-11]
B126389 07/16/155 5.0015G0434-12 [MW-12]
B126389 07/16/155 5.0015G0434-13 [MW-13]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B126520 07/16/155 5.0015G0434-08 [MW-3R]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B126607 07/18/150.1 5.0015G0434-08RE1 [MW-3R]
[TOC_1]Sample Preparation Information[TOC]
Page 34 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B126387 - SW-846 5030B
[TOC_3]B126387[TOC]
Blank (B126387-BLK1) Prepared: 07/16/15 Analyzed: 07/18/15
Acetone g/L50 B, J5.7
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0 R-05ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.50ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 35 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126387 - SW-846 5030B
Blank (B126387-BLK1) Prepared: 07/16/15 Analyzed: 07/18/15
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50 L-04ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 98.624.6
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 92.923.2
LCS (B126387-BS1) Prepared: 07/16/15 Analyzed: 07/18/15
Acetone g/L50 100 70-13091.991.9
Benzene g/L0.50 10.0 70-13096.09.60
Bromobenzene g/L0.50 10.0 70-13096.69.66
Bromochloromethane g/L0.50 10.0 70-13010810.8
Bromodichloromethane g/L0.50 10.0 70-13099.59.95
Bromoform g/L0.50 10.0 70-13011111.1
Bromomethane g/L1.0 10.0 R-0560-14012812.8
2-Butanone (MEK)g/L5.0 100 70-130117117
n-Butylbenzene g/L0.50 10.0 70-13010310.3
sec-Butylbenzene g/L0.50 10.0 70-13010110.1
tert-Butylbenzene g/L0.50 10.0 70-13010210.2
Carbon Tetrachloride g/L0.50 10.0 70-13094.69.46
Chlorobenzene g/L0.50 10.0 70-13098.69.86
Ethanol g/L50 100 70-130127127
Chlorodibromomethane g/L0.50 10.0 70-13097.59.75
Chloroethane g/L0.50 10.0 60-14082.88.28
Chloroform g/L0.50 10.0 70-13089.98.99
Chloromethane g/L0.50 10.0 60-14095.19.51
2-Chlorotoluene g/L0.50 10.0 70-13099.89.98
4-Chlorotoluene g/L0.50 10.0 70-13096.49.64
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13096.19.61
1,2-Dichlorobenzene g/L0.50 10.0 70-13098.19.81
1,3-Dichlorobenzene g/L0.50 10.0 70-13097.99.79
1,4-Dichlorobenzene g/L0.50 10.0 70-13098.09.80
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14066.36.63
1,1-Dichloroethane g/L0.50 10.0 70-13099.39.93
1,2-Dichloroethane g/L0.50 10.0 70-13094.09.40
1,1-Dichloroethylene g/L0.50 10.0 70-13092.49.24
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13099.39.93
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010410.4
1,2-Dichloropropane g/L0.50 10.0 70-13099.79.97
1,3-Dichloropropane g/L0.50 10.0 70-13098.29.82
2,2-Dichloropropane g/L0.50 10.0 70-13010510.5
1,1-Dichloropropene g/L0.50 10.0 70-13097.69.76
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010610.6
trans-1,3-Dichloropropene g/L0.50 10.0 70-13012812.8
Page 36 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126387 - SW-846 5030B
LCS (B126387-BS1) Prepared: 07/16/15 Analyzed: 07/18/15
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13097.79.77
Ethylbenzene g/L0.50 10.0 70-13010010.0
2-Hexanone (MBK)g/L5.0 100 70-130107107
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13096.89.68
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010310.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13096.59.65
Methylene Chloride g/L5.0 10.0 70-13092.99.29
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130119119
Naphthalene g/L0.50 10.0 70-13092.99.29
n-Propylbenzene g/L0.50 10.0 70-13095.39.53
Styrene g/L0.50 10.0 70-13098.89.88
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13098.29.82
Tetrachloroethylene g/L0.50 10.0 70-13096.79.67
Toluene g/L0.50 10.0 70-13098.99.89
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13099.89.98
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13098.69.86
1,1,1-Trichloroethane g/L0.50 10.0 70-13095.89.58
1,1,2-Trichloroethane g/L0.50 10.0 70-13097.59.75
Trichloroethylene g/L0.50 10.0 70-13010210.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13084.38.43
1,2,3-Trichloropropane g/L0.50 10.0 70-13010010.0
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010410.4
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13097.39.73
Vinyl Acetate g/L5.0 100 70-130101101
Vinyl Chloride g/L0.50 10.0 L-0460-14048.2 *4.82
m+p Xylene g/L1.0 20.0 70-13099.019.8
o-Xylene g/L0.50 10.0 70-13097.99.79
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10125.3
g/L 25.0 70-130Surrogate: Toluene-d8 99.925.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.224.0
LCS Dup (B126387-BSD1) Prepared: 07/16/15 Analyzed: 07/18/15
Acetone g/L50 100 2570-13091.3 0.67791.3
Benzene g/L0.50 10.0 2570-13090.3 6.129.03
Bromobenzene g/L0.50 10.0 2570-13095.9 0.7279.59
Bromochloromethane g/L0.50 10.0 2570-130102 6.0010.2
Bromodichloromethane g/L0.50 10.0 2570-13097.0 2.549.70
Bromoform g/L0.50 10.0 2570-130113 1.6111.3
Bromomethane g/L1.0 10.0 25 R-0560-14085.4 40.2 *8.54
2-Butanone (MEK)g/L5.0 100 2570-130119 1.75119
n-Butylbenzene g/L0.50 10.0 2570-13099.4 3.179.94
sec-Butylbenzene g/L0.50 10.0 2570-13095.8 4.899.58
tert-Butylbenzene g/L0.50 10.0 2570-13097.5 4.229.75
Carbon Tetrachloride g/L0.50 10.0 2570-13088.2 7.008.82
Chlorobenzene g/L0.50 10.0 2570-13096.3 2.369.63
Ethanol g/L50 100 2570-130107 17.0107
Chlorodibromomethane g/L0.50 10.0 2570-13096.6 0.9279.66
Chloroethane g/L0.50 10.0 2560-14069.6 17.36.96
Chloroform g/L0.50 10.0 2570-13085.6 4.908.56
Chloromethane g/L0.50 10.0 2560-14096.0 0.9429.60
2-Chlorotoluene g/L0.50 10.0 2570-130100 0.40010.0
4-Chlorotoluene g/L0.50 10.0 2570-13092.7 3.919.27
Page 37 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126387 - SW-846 5030B
LCS Dup (B126387-BSD1) Prepared: 07/16/15 Analyzed: 07/18/15
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13099.3 3.289.93
1,2-Dichlorobenzene g/L0.50 10.0 2570-13096.9 1.239.69
1,3-Dichlorobenzene g/L0.50 10.0 2570-13095.4 2.599.54
1,4-Dichlorobenzene g/L0.50 10.0 2570-13094.4 3.749.44
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14062.5 5.906.25
1,1-Dichloroethane g/L0.50 10.0 2570-13093.8 5.709.38
1,2-Dichloroethane g/L0.50 10.0 2570-13092.8 1.289.28
1,1-Dichloroethylene g/L0.50 10.0 2570-13088.7 4.098.87
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13095.6 3.809.56
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13095.8 7.929.58
1,2-Dichloropropane g/L0.50 10.0 2570-13098.4 1.319.84
1,3-Dichloropropane g/L0.50 10.0 2570-13095.9 2.379.59
2,2-Dichloropropane g/L0.50 10.0 2570-13098.5 6.209.85
1,1-Dichloropropene g/L0.50 10.0 2570-13091.7 6.239.17
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130100 5.5410.0
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130125 2.3812.5
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13092.7 5.259.27
Ethylbenzene g/L0.50 10.0 2570-13097.4 2.739.74
2-Hexanone (MBK)g/L5.0 100 2570-130110 2.66110
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13094.0 2.949.40
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13098.5 4.669.85
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13092.8 3.919.28
Methylene Chloride g/L5.0 10.0 2570-13084.9 9.008.49
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130126 5.82126
Naphthalene g/L0.50 10.0 2570-13098.0 5.349.80
n-Propylbenzene g/L0.50 10.0 2570-13090.8 4.849.08
Styrene g/L0.50 10.0 2570-13096.1 2.779.61
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130100 1.8210.0
Tetrachloroethylene g/L0.50 10.0 2570-13091.3 5.749.13
Toluene g/L0.50 10.0 2570-13095.4 3.609.54
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-130106 6.2110.6
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130102 3.3910.2
1,1,1-Trichloroethane g/L0.50 10.0 2570-13089.6 6.698.96
1,1,2-Trichloroethane g/L0.50 10.0 2570-13098.9 1.439.89
Trichloroethylene g/L0.50 10.0 2570-130100 1.3810.0
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13080.2 4.988.02
1,2,3-Trichloropropane g/L0.50 10.0 2570-130102 1.9710.2
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13099.9 4.509.99
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13094.7 2.719.47
Vinyl Acetate g/L5.0 100 2570-130103 2.12103
Vinyl Chloride g/L0.50 10.0 25 L-0460-14044.0 9.11*4.40
m+p Xylene g/L1.0 20.0 2570-13094.7 4.3918.9
o-Xylene g/L0.50 10.0 2570-13096.2 1.759.62
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.4
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.024.0
Page 38 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126389 - SW-846 5030B
[TOC_3]B126389[TOC]
Blank (B126389-BLK1) Prepared: 07/16/15 Analyzed: 07/18/15
Acetone g/L50 B, J5.5
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0 R-05ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.50ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50 L-04ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 39 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126389 - SW-846 5030B
Blank (B126389-BLK1) Prepared: 07/16/15 Analyzed: 07/18/15
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50 R-05ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 99.124.8
g/L 25.0 70-130Surrogate: Toluene-d8 98.724.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.924.0
LCS (B126389-BS1) Prepared: 07/16/15 Analyzed: 07/18/15
Acetone g/L50 100 70-13088.888.8
Benzene g/L0.50 10.0 70-13092.99.29
Bromobenzene g/L0.50 10.0 70-13095.79.57
Bromochloromethane g/L0.50 10.0 70-13010410.4
Bromodichloromethane g/L0.50 10.0 70-13096.99.69
Bromoform g/L0.50 10.0 70-13011011.0
Bromomethane g/L1.0 10.0 R-0560-14010210.2
2-Butanone (MEK)g/L5.0 100 70-130106106
n-Butylbenzene g/L0.50 10.0 70-13092.49.24
sec-Butylbenzene g/L0.50 10.0 70-13094.79.47
tert-Butylbenzene g/L0.50 10.0 70-13097.79.77
Carbon Tetrachloride g/L0.50 10.0 70-13091.79.17
Chlorobenzene g/L0.50 10.0 70-13098.19.81
Ethanol g/L50 100 70-130103103
Chlorodibromomethane g/L0.50 10.0 70-13096.09.60
Chloroethane g/L0.50 10.0 60-14088.18.81
Chloroform g/L0.50 10.0 70-13086.38.63
Chloromethane g/L0.50 10.0 60-14094.39.43
2-Chlorotoluene g/L0.50 10.0 70-13098.89.88
4-Chlorotoluene g/L0.50 10.0 70-13094.29.42
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13097.09.70
1,2-Dichlorobenzene g/L0.50 10.0 70-13095.99.59
1,3-Dichlorobenzene g/L0.50 10.0 70-13094.19.41
1,4-Dichlorobenzene g/L0.50 10.0 70-13094.79.47
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14096.19.61
1,1-Dichloroethane g/L0.50 10.0 70-13096.19.61
1,2-Dichloroethane g/L0.50 10.0 70-13094.19.41
1,1-Dichloroethylene g/L0.50 10.0 70-13096.39.63
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13097.99.79
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13099.09.90
1,2-Dichloropropane g/L0.50 10.0 70-13099.59.95
1,3-Dichloropropane g/L0.50 10.0 70-13098.79.87
2,2-Dichloropropane g/L0.50 10.0 L-0470-13064.2 *6.42
1,1-Dichloropropene g/L0.50 10.0 70-13093.89.38
cis-1,3-Dichloropropene g/L0.50 10.0 70-13093.69.36
trans-1,3-Dichloropropene g/L0.50 10.0 70-13011311.3
Page 40 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126389 - SW-846 5030B
LCS (B126389-BS1) Prepared: 07/16/15 Analyzed: 07/18/15
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13094.99.49
Ethylbenzene g/L0.50 10.0 70-13099.49.94
2-Hexanone (MBK)g/L5.0 100 70-130100100
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13094.69.46
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13096.69.66
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13094.09.40
Methylene Chloride g/L5.0 10.0 70-13089.88.98
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130112112
Naphthalene g/L0.50 10.0 70-13088.78.87
n-Propylbenzene g/L0.50 10.0 70-13092.09.20
Styrene g/L0.50 10.0 70-13096.89.68
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13093.79.37
Tetrachloroethylene g/L0.50 10.0 70-13095.49.54
Toluene g/L0.50 10.0 70-13096.09.60
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13095.29.52
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13093.89.38
1,1,1-Trichloroethane g/L0.50 10.0 70-13093.49.34
1,1,2-Trichloroethane g/L0.50 10.0 70-13098.99.89
Trichloroethylene g/L0.50 10.0 70-13098.19.81
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13086.08.60
1,2,3-Trichloropropane g/L0.50 10.0 70-13095.89.58
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13098.49.84
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13095.39.53
Vinyl Acetate g/L5.0 100 70-13077.077.0
Vinyl Chloride g/L0.50 10.0 R-0560-14065.66.56
m+p Xylene g/L1.0 20.0 70-13096.719.3
o-Xylene g/L0.50 10.0 70-13097.69.76
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10125.2
g/L 25.0 70-130Surrogate: Toluene-d8 99.724.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.124.0
LCS Dup (B126389-BSD1) Prepared: 07/16/15 Analyzed: 07/18/15
Acetone g/L50 100 2570-13098.8 10.798.8
Benzene g/L0.50 10.0 2570-13091.6 1.419.16
Bromobenzene g/L0.50 10.0 2570-13095.9 0.2099.59
Bromochloromethane g/L0.50 10.0 2570-130100 3.8110.0
Bromodichloromethane g/L0.50 10.0 2570-13091.1 6.179.11
Bromoform g/L0.50 10.0 2570-130113 2.3411.3
Bromomethane g/L1.0 10.0 25 R-0560-14075.6 30.2 *7.56
2-Butanone (MEK)g/L5.0 100 2570-130122 14.0122
n-Butylbenzene g/L0.50 10.0 2570-13092.3 0.1089.23
sec-Butylbenzene g/L0.50 10.0 2570-13094.0 0.7429.40
tert-Butylbenzene g/L0.50 10.0 2570-13097.8 0.1029.78
Carbon Tetrachloride g/L0.50 10.0 2570-13090.5 1.329.05
Chlorobenzene g/L0.50 10.0 2570-13095.9 2.279.59
Ethanol g/L50 100 2570-130122 17.4122
Chlorodibromomethane g/L0.50 10.0 2570-13094.4 1.689.44
Chloroethane g/L0.50 10.0 2560-14082.1 7.058.21
Chloroform g/L0.50 10.0 2570-13085.3 1.178.53
Chloromethane g/L0.50 10.0 2560-14097.0 2.829.70
2-Chlorotoluene g/L0.50 10.0 2570-13097.7 1.129.77
4-Chlorotoluene g/L0.50 10.0 2570-13093.5 0.7469.35
Page 41 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126389 - SW-846 5030B
LCS Dup (B126389-BSD1) Prepared: 07/16/15 Analyzed: 07/18/15
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13097.3 0.3099.73
1,2-Dichlorobenzene g/L0.50 10.0 2570-13096.4 0.5209.64
1,3-Dichlorobenzene g/L0.50 10.0 2570-13095.4 1.379.54
1,4-Dichlorobenzene g/L0.50 10.0 2570-13092.9 1.929.29
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14086.0 11.18.60
1,1-Dichloroethane g/L0.50 10.0 2570-13092.3 4.039.23
1,2-Dichloroethane g/L0.50 10.0 2570-13094.2 0.1069.42
1,1-Dichloroethylene g/L0.50 10.0 2570-13092.0 4.579.20
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13097.3 0.6159.73
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13097.7 1.329.77
1,2-Dichloropropane g/L0.50 10.0 2570-13097.5 2.039.75
1,3-Dichloropropane g/L0.50 10.0 2570-13097.3 1.439.73
2,2-Dichloropropane g/L0.50 10.0 25 L-0470-13062.2 3.16*6.22
1,1-Dichloropropene g/L0.50 10.0 2570-13090.6 3.479.06
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13092.2 1.519.22
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130112 1.3311.2
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13096.7 1.889.67
Ethylbenzene g/L0.50 10.0 2570-13096.5 2.969.65
2-Hexanone (MBK)g/L5.0 100 2570-130111 10.3111
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13093.5 1.179.35
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13095.5 1.159.55
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13095.5 1.589.55
Methylene Chloride g/L5.0 10.0 2570-13090.7 0.9979.07
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130127 12.3127
Naphthalene g/L0.50 10.0 2570-130100 12.010.0
n-Propylbenzene g/L0.50 10.0 2570-13089.8 2.428.98
Styrene g/L0.50 10.0 2570-13096.0 0.8309.60
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13096.4 2.849.64
Tetrachloroethylene g/L0.50 10.0 2570-13089.5 6.388.95
Toluene g/L0.50 10.0 2570-13094.5 1.579.45
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-130107 11.310.7
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130101 7.4910.1
1,1,1-Trichloroethane g/L0.50 10.0 2570-13092.7 0.7529.27
1,1,2-Trichloroethane g/L0.50 10.0 2570-13098.2 0.7109.82
Trichloroethylene g/L0.50 10.0 2570-130105 6.7010.5
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13082.1 4.648.21
1,2,3-Trichloropropane g/L0.50 10.0 2570-130105 9.2610.5
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13099.2 0.8109.92
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13093.0 2.449.30
Vinyl Acetate g/L5.0 100 2570-13072.7 5.7672.7
Vinyl Chloride g/L0.50 10.0 25 L-07A60-14049.7 27.6**4.97
m+p Xylene g/L1.0 20.0 2570-13095.0 1.7219.0
o-Xylene g/L0.50 10.0 2570-13096.1 1.559.61
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10025.0
g/L 25.0 70-130Surrogate: Toluene-d8 98.224.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.424.1
Page 42 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126520 - SW-846 5030B
[TOC_3]B126520[TOC]
Blank (B126520-BLK1) Prepared: 07/19/15 Analyzed: 07/20/15
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0 R-05ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.50ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50 L-04ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 43 of 55
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126520 - SW-846 5030B
Blank (B126520-BLK1) Prepared: 07/19/15 Analyzed: 07/20/15
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10526.2
g/L 25.0 70-130Surrogate: Toluene-d8 97.224.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.7
LCS (B126520-BS1) Prepared: 07/19/15 Analyzed: 07/20/15
Acetone g/L50 100 70-13085.885.8
Benzene g/L0.50 10.0 70-13010510.5
Bromobenzene g/L0.50 10.0 70-13010510.5
Bromochloromethane g/L0.50 10.0 70-13011811.8
Bromodichloromethane g/L0.50 10.0 70-13094.59.45
Bromoform g/L0.50 10.0 70-13093.29.32
Bromomethane g/L1.0 10.0 R-0560-14013813.8
2-Butanone (MEK)g/L5.0 100 70-130113113
n-Butylbenzene g/L0.50 10.0 70-13088.18.81
sec-Butylbenzene g/L0.50 10.0 70-13010210.2
tert-Butylbenzene g/L0.50 10.0 70-13010210.2
Carbon Tetrachloride g/L0.50 10.0 70-13010110.1
Chlorobenzene g/L0.50 10.0 70-13010710.7
Ethanol g/L50 100 70-13091.091.0
Chlorodibromomethane g/L0.50 10.0 70-13095.39.53
Chloroethane g/L0.50 10.0 60-14093.79.37
Chloroform g/L0.50 10.0 70-13010910.9
Chloromethane g/L0.50 10.0 60-14090.79.07
2-Chlorotoluene g/L0.50 10.0 70-13011311.3
4-Chlorotoluene g/L0.50 10.0 70-13010910.9
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010410.4
1,2-Dichlorobenzene g/L0.50 10.0 70-13010110.1
1,3-Dichlorobenzene g/L0.50 10.0 70-13010410.4
1,4-Dichlorobenzene g/L0.50 10.0 70-13099.89.98
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14010410.4
1,1-Dichloroethane g/L0.50 10.0 70-13010610.6
1,2-Dichloroethane g/L0.50 10.0 70-13011011.0
1,1-Dichloroethylene g/L0.50 10.0 70-13097.79.77
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010610.6
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13011911.9
1,2-Dichloropropane g/L0.50 10.0 70-13010610.6
1,3-Dichloropropane g/L0.50 10.0 70-13010810.8
2,2-Dichloropropane g/L0.50 10.0 70-13011811.8
1,1-Dichloropropene g/L0.50 10.0 70-13010810.8
cis-1,3-Dichloropropene g/L0.50 10.0 70-13094.59.45
trans-1,3-Dichloropropene g/L0.50 10.0 70-13095.49.54
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126520 - SW-846 5030B
LCS (B126520-BS1) Prepared: 07/19/15 Analyzed: 07/20/15
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010610.6
Ethylbenzene g/L0.50 10.0 70-13011111.1
2-Hexanone (MBK)g/L5.0 100 70-130111111
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13094.59.45
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010610.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13012012.0
Methylene Chloride g/L5.0 10.0 70-13088.58.85
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130115115
Naphthalene g/L0.50 10.0 L-0470-13062.6 *6.26
n-Propylbenzene g/L0.50 10.0 70-13096.09.60
Styrene g/L0.50 10.0 70-13010210.2
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010410.4
Tetrachloroethylene g/L0.50 10.0 70-13011411.4
Toluene g/L0.50 10.0 70-13010910.9
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13078.57.85
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13078.17.81
1,1,1-Trichloroethane g/L0.50 10.0 70-13010210.2
1,1,2-Trichloroethane g/L0.50 10.0 70-13011211.2
Trichloroethylene g/L0.50 10.0 70-13010810.8
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13011411.4
1,2,3-Trichloropropane g/L0.50 10.0 70-13010910.9
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010410.4
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13096.49.64
Vinyl Acetate g/L5.0 100 70-130112112
Vinyl Chloride g/L0.50 10.0 60-14096.19.61
m+p Xylene g/L1.0 20.0 70-13011623.1
o-Xylene g/L0.50 10.0 70-13011011.0
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 99.424.8
g/L 25.0 70-130Surrogate: Toluene-d8 99.825.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.8
LCS Dup (B126520-BSD1) Prepared: 07/19/15 Analyzed: 07/20/15
Acetone g/L50 100 2570-13078.8 8.4578.8
Benzene g/L0.50 10.0 2570-130100 4.3810.0
Bromobenzene g/L0.50 10.0 2570-130103 1.8210.3
Bromochloromethane g/L0.50 10.0 2570-130114 3.5311.4
Bromodichloromethane g/L0.50 10.0 2570-13093.8 0.7439.38
Bromoform g/L0.50 10.0 2570-13091.1 2.289.11
Bromomethane g/L1.0 10.0 25 R-0560-14095.5 36.1 *9.55
2-Butanone (MEK)g/L5.0 100 2570-130115 1.40115
n-Butylbenzene g/L0.50 10.0 2570-13082.8 6.208.28
sec-Butylbenzene g/L0.50 10.0 2570-13096.9 4.649.69
tert-Butylbenzene g/L0.50 10.0 2570-13098.0 3.909.80
Carbon Tetrachloride g/L0.50 10.0 2570-13095.3 6.109.53
Chlorobenzene g/L0.50 10.0 2570-130104 2.9510.4
Ethanol g/L50 100 2570-130106 15.2106
Chlorodibromomethane g/L0.50 10.0 2570-13093.2 2.239.32
Chloroethane g/L0.50 10.0 2560-14088.4 5.828.84
Chloroform g/L0.50 10.0 2570-130103 5.4910.3
Chloromethane g/L0.50 10.0 2560-14085.2 6.258.52
2-Chlorotoluene g/L0.50 10.0 2570-130106 6.0310.6
4-Chlorotoluene g/L0.50 10.0 2570-130103 5.7710.3
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126520 - SW-846 5030B
LCS Dup (B126520-BSD1) Prepared: 07/19/15 Analyzed: 07/20/15
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130108 3.1210.8
1,2-Dichlorobenzene g/L0.50 10.0 2570-13099.6 1.309.96
1,3-Dichlorobenzene g/L0.50 10.0 2570-13099.7 4.329.97
1,4-Dichlorobenzene g/L0.50 10.0 2570-13098.4 1.419.84
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14096.7 7.379.67
1,1-Dichloroethane g/L0.50 10.0 2570-130102 3.8610.2
1,2-Dichloroethane g/L0.50 10.0 2570-130108 1.6510.8
1,1-Dichloroethylene g/L0.50 10.0 2570-13088.2 10.28.82
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130103 2.5810.3
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130104 13.410.4
1,2-Dichloropropane g/L0.50 10.0 2570-130102 4.6210.2
1,3-Dichloropropane g/L0.50 10.0 2570-130106 0.93510.6
2,2-Dichloropropane g/L0.50 10.0 2570-130109 8.4710.9
1,1-Dichloropropene g/L0.50 10.0 2570-130102 5.4310.2
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13093.3 1.289.33
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13093.7 1.809.37
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130102 3.8610.2
Ethylbenzene g/L0.50 10.0 2570-130106 5.3510.6
2-Hexanone (MBK)g/L5.0 100 2570-130114 2.32114
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13088.0 7.128.80
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130100 5.3510.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130113 6.1111.3
Methylene Chloride g/L5.0 10.0 2570-13072.0 20.67.20
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130117 2.13117
Naphthalene g/L0.50 10.0 25 L-0470-13066.1 5.44*6.61
n-Propylbenzene g/L0.50 10.0 2570-13090.4 6.019.04
Styrene g/L0.50 10.0 2570-13097.4 4.329.74
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130106 1.9010.6
Tetrachloroethylene g/L0.50 10.0 2570-130105 8.1410.5
Toluene g/L0.50 10.0 2570-130104 4.1210.4
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13079.6 1.397.96
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13079.4 1.657.94
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.0 5.129.70
1,1,2-Trichloroethane g/L0.50 10.0 2570-130111 0.35911.1
Trichloroethylene g/L0.50 10.0 2570-130104 3.6810.4
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130104 8.3510.4
1,2,3-Trichloropropane g/L0.50 10.0 2570-130110 1.2811.0
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13099.7 3.749.97
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13089.9 6.988.99
Vinyl Acetate g/L5.0 100 2570-130111 1.02111
Vinyl Chloride g/L0.50 10.0 2560-14090.2 6.339.02
m+p Xylene g/L1.0 20.0 2570-130109 6.1021.8
o-Xylene g/L0.50 10.0 2570-130104 6.0010.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.624.4
g/L 25.0 70-130Surrogate: Toluene-d8 99.824.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.5
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B126607 - SW-846 5030B
[TOC_3]B126607[TOC]
Blank (B126607-BLK1) Prepared & Analyzed: 07/18/15
1,2,4-Trimethylbenzene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 99.124.8
g/L 25.0 70-130Surrogate: Toluene-d8 98.724.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.924.0
LCS (B126607-BS1) Prepared & Analyzed: 07/18/15
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13012012.0
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10025.0
g/L 25.0 70-130Surrogate: Toluene-d8 99.024.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.624.1
LCS Dup (B126607-BSD1) Prepared & Analyzed: 07/18/15
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130116 3.2111.6
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10025.0
g/L 25.0 70-130Surrogate: Toluene-d8 99.825.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.924.5
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Analyte is found in the associated blank as well as in the sample.B
Methylene chloride is a common laboratory contaminant.B-01
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for
this compound.
L-07A
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Elevated reporting limit based on lowest point in calibration.
Requested reporting limit not met.
RL-03
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2016
M-MA100Massachusetts DEPMA 06/30/2016
PH-0567Connecticut Department of Publilc HealthCT 09/30/2015
10899 NELAPNew York State Department of HealthNY 04/1/2016
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2016
LAO00112Rhode Island Department of HealthRI 12/30/2015
652North Carolina Div. of Water QualityNC 12/31/2015
MA007 NELAPNew Jersey DEPNJ 09/30/2015
E871027 NELAPFlorida Department of HealthFL 06/30/2016
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2015
C2065State of Washington Department of EcologyWA 02/23/2016
2011028State of MaineME 06/9/2017
460217Commonwealth of VirginiaVA 12/14/2015
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2015
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