WI-304_32107_CA_MRP_20230816

SUBSEQUENT MONITORING REPORT
NORRIS LUV STATION (INCIDENT NO. 32107)
NC HIGHWAY 41 AND OAK STREET
CHINQUAPIN, DUPLIN COUNTY, NORTH CAROLINA
ESP PROJECT NO. 23-00200-094
Prepared For:
North Carolina Department of Environmental Quality
Division of Waste Management – UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Prepared By:
ESP Associates, Inc.
P. O. Box 7030
Charlotte, North Carolina 28241
August 16, 2023
ESP Associates, Inc.
P.O. Box 7030 • Charlotte, NC 28241
1.800.960.7317 • NC: 704.583.4949, fax [phone] • SC: 803.802.2440, fax [phone]
www.espassociates.com
August 16, 2023
Mr. Thomas Chapman
North Carolina Department of Environmental Quality
Division of Waste Management
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Email: [e-mail]
Reference:SUBSEQUENT MONITORING REPORT
Norris Luv Station
NC Highway 41 and Oak Street
Chinquapin, Duplin County, North Carolina
UST Incident No. 32107
ESP Project No. E6-23-00200-094
Dear Mr. Chapman:
ESP Associates, Inc. (ESP) is pleased to present this Subsequent Monitoring Report documenting
activities performed at the subject site, Norris Luv Station, in accordance with North Carolina
Department of Environmental Quality (NCDEQ), Task Authorization No. 1, approved on April 28,
2023. The subject site is located at the intersection of NC Highway 41 and Oak Street in Chinquapin,
Duplin County, North Carolina.
We appreciate the opportunity to provide environmental services on this project. If you should have
any questions, please do not hesitate to contact us at [phone].
Sincerely,
ESP Associates, Inc.
Matthew R. Craig Nora A. Zirps, PE, RSM
Project Manager Senior Project Engineer
Attachment – Subsequent Monitoring Report
TABLE OF CONTENTS
Section Page
SITE INFORMATION .....................................................................................................................i
EXECUTIVE SUMMARY..............................................................................................................iii
1.0 INTRODUCTION ...............................................................................................................1
1.1 SITE SETTING............................................................................................................1
1.2 SITE GEOLOGY AND HYDROGEOLOGY..................................................................1
1.3 SURFACE WATER .....................................................................................................2
1.4 WATER SUPPLY WELLS ...........................................................................................2
2.0 SITE HISTORY...................................................................................................................3
3.0 FIELD ACTIVITIES ...........................................................................................................4
3.1 WATER LEVEL GAUGING.........................................................................................4
3.2 FREE PRODUCTION EVALUATION ..........................................................................4
3.3 GROUNDWATER SAMPLING....................................................................................4
3.4 FIELD QUALITY CONTROL SAMPLING AND ANALYSIS ........................................5
4.0 GROUNDWATER ANALYTICAL RESULTS ....................................................................6
5.0 CONCLUSIONS AND RECOMMENDATIONS..................................................................7
6.0 REFERENCES ....................................................................................................................8
FIGURES
Figure 1 USGS Topographic Site Location Map
Figure 2 Site Map
Figure 3 Groundwater Elevation Map
Figure 4 Groundwater Results Map
Figure 5 Benzene Isoconcentration Map
TABLES
Table 1 Monitoring Well Construction and Groundwater Elevation Data
Table 2 Summary of Groundwater Analytical Results
APPENDICES
Appendix A Tables of Previous Groundwater Elevations and Analytical Results
Appendix B Field Documentation
Appendix C Laboratory Analytical Report
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
i
SITE INFORMATION
Date of Report:August 16, 2023
NCDEQ Incident No:32107
NCDEQ UST No.:WI-304
Site Name:Norris LUV Station
Site Location:NC Highway 41 and Oak Street
Chinquapin, Duplin County, North Carolina 28521
Latitude:N 34.832931
Longitude:W 77.822302
UST Owner/ Operator:N/A – USTs are not known to be currently located on-site; former
UST owner was reportedly Collier Gas and Fuel
Current Property
Owner:Ms. Patsy K. Lain Trustee
124 Kennedy Circle
Hubert, North Carolina 28539
(910)-336-1244
Current Property
Occupant:Unknown Tenant
Consultant:ESP Associates, Inc.
P.O. Box 7030
Charlotte, North Carolina 28241
[phone]
Laboratory:Pace Analytical Services, LLC
NCDEQ No. 5342
9800 Kincey Avenue
Huntersville, North Carolina 28028
[phone]
Release Information:Release Discovery Date: March 1993
Estimate Quantity: Unknown
Cause of Release: Underground Storage Tank (UST) system leak
Source of Release: Two 10,000-gallon gasoline USTs; two 1,000-
gallon gasoline USTs; one 500-gallon diesel UST; one 1,000-gallon
diesel UST; one 2,000-gallon diesel UST (all removed March1993)
Currently Active Tanks: None
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
ii
I, Nora A. Zirps, a Professional Engineer for ESP Associates, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.
ESP Associates, Inc. is licensed to practice both geology and engineering in North Carolina. ESP
Associates, Inc.’s certification numbers are: Geology: C-556 / Engineering: F-1407
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
iii
EXECUTIVE SUMMARY
This executive summary section provides an abbreviated reporting of our Site observations and
findings. Refer to the main text and appendices for a complete reporting of our observations and
findings.
ESP Associates, Inc. (ESP) has completed a Subsequent Monitoring Report documenting
assessment activity performed at the Norris Luv Station site (Incident No. 32107). The site is an
approximate 0.95-acre commercial property (Tax Parcel No. 335900364017) located at the corner of
NC Highway 41 and Oak Street in Chinquapin, Duplin County, North Carolina. This report was
completed to summarize the findings of assessment activities performed on May 31, 2023, in
accordance with North Carolina Department of Environmental Quality (NCDEQ), Task
Authorization No. 1, approved on April 28, 2023.
The work was performed as part of the State Lead Contract #N70522-D between NCDEQ and ESP
Associates, Inc. This report was prepared in general accordance with the 15A NCAC 2L .0115
regulations and the NCDEQ UST Section Guidelines for Assessment and Corrective Action for UST
Releases, January 2021, under the supervision of Nora A. Zirps, North Carolina registered
professional engineer (North Carolina License No. 023838).
On May 31, 2023, ESP performed the following field activities:
•Gauging static water levels in existing on-site monitoring wells.
•Gauging monitoring well MW-7 for the presence of free product.
•Collecting groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-8,
MW-9, MW-10 and MW-11. Although planned, ESP was unable to sample MW-4 because
it could not be located.
Collected groundwater samples were analyzed for volatile organic compounds (VOCs) for
comparison to both North Carolina Groundwater Quality Standards 15A NCAC 2L .0202 (2L
Standards) and Gross Contaminant Levels (GCLs).
Results of the assessment activities revealed the following:
•Static water levels ranged from 0.69 to 4.45 feet below top of casing.
•The general direction of groundwater flow beneath the site is toward the south-southeast
on the northern portion of the site and toward the east on the southern portion of the site.
•Free product is present in MW-7 with a thickness of 1.51 feet, which is greater than the
0.22 feet of free product measured in September 2021 following the August 2021 AFVR
event on MW-7.
•No VOCs in groundwater exceeded their respective GCLs.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
iv
•Benzene and naphthalene were the only two analytes detected about their 2L Standards in
May 2023. Benzene was detected at 312 µg/L in MW-9 which exceeds its 2L Standard of
1 µg/L, and naphthalene was detected at 20.9 µg/L in MW-8 and 53.3 µg/L in MW-9 above
its 2L Standard of 6 µg/L.
•VOC concentrations appear to have generally decreased in monitoring wells across the site
from September 2021 to May 2023.
•A groundwater sample was not collected from MW-4 (unable to locate).
Based on the above results, ESP offers the following recommendations:
•Permanently abandon damaged monitoring well MW-2. A replacement well for MW-2 is
not recommended at this time.
•Permanently abandon destroyed monitoring well MW-6R and install a replacement
monitoring well in the same general location since VOCs were historically detected above
2L Standards at this location.
•Prior to the next sampling event, implement a mobile multi-phase extraction (MMPE)
event on MW-7.
•Continue monitoring the groundwater quality on-site by conducting semi-annual
groundwater sampling events for on-site monitoring wells along with gauging of free
product in MW-7.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
1
1.0 INTRODUCTION
1.1 Site Setting
The Norris Luv Station site is an approximate 0.95-acre commercial site (Tax Parcel No.
335900364017) located at the corner of NC Highway 41 and Oak Street in Chinquapin, Duplin
County, North Carolina (see Figure 1 and Figure 2). The site includes an approximate 2,300-sqft
commercial building along with paved parking area. NC Highway 41 runs along the site’s
northeastern face, while Oak Street runs along the site’s northwestern face. The adjacent properties
to the north, west, and south consist of single-family residences and wooded areas, while the adjacent
property to the east is commercial but unoccupied.
1.2 Site Geology and Hydrogeology
Consideration of surface and subsurface drainage and geology are of interest since they provide
an indication of the direction that contamination, if present on-site or off-site, could be transported.
The site is in the Coastal Plain Region, or Inner Coastal Plains. This region is a higher, denser area
of sandy soil. The Coastal Plain Region was developed on loose, unconsolidated, and flat layers
of sediment, caused by sea level changes and erosion of the mountains. Most parts of the Coastal
Plain Region consist of well to moderately well-drained loamy soils.
The site is underlain by a sequence of marine sediments of the Cretaceous age known as the Black
Creek Formation (Kb). The Black Creek Formation consists of thin beds of fine grained,
micaceous sand and thick beds of coarse sand with fossiliferous clay in the upper layers. The soil
on the site was found to consist of Dragston fine sandy loan, 0 to 2 percent slopes (Da). Da soil
types are found in the uplands. They are developed from beds of sand that grade into and are
interbedded with light sandy clays. Da soil types are somewhat poorly drained, with slow runoff,
and depth to the water table is at or near the surface in lower areas.
Groundwater at the site is supplied by the Black Creek Aquifer. The aquifer’s characteristics are
lagoonal to marine consisting of thinly laminated clay interlayered with sand. Sediments in the
subsurface are highly organic and are from the Black Creek and Middendorf Formations. On
average, the Black Creek Aquifer consists of “nearly 60 percent sand”, and the hydraulic
conductivity ranges from 15 to 50 feet/day, averaging 28 feet/day. Recharge of the groundwater is
the result of downward percolation from the overlying aquifers. Discharge is typically into streams
where there are channels cut into it or its overlying confining unit.
The depth to the water table is not consistent and is dependent upon several factors that include
the amount of rainfall, permeability of the soil, and the influences of groundwater pumping. Based
on depth-to-water level measurements, the general groundwater flow direction beneath the site is
estimated to be toward the south-southeast on the northern portion and east on the southern portion.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
2
On May 31, 2023, the depth to groundwater in the on-site monitoring wells ranged from
approximately 0.69 to 4.45 feet below top of well casing (ft bTOC) in locations where free product
was not present.
1.3 Surface Water
The site is located within the drainage basin of the Oakie Branch-Northeast Cape Fear River, which,
at its closest point is located approximately 3,025 feet west of the site. No surface water features
were observed on or immediately adjacent to the site; however, an apparent unnamed tributary of
the Northeast Cape Fear River is located approximately 250 feet south of the source area (see
Figure 1).
1.4 Water Supply Wells
Public water is available to the site area. Previous receptor surveys have noted one municipal water
supply well adjacent to an elevated water tank located approximately 700 feet northwest and
upgradient of the source area. Reportedly, the municipal water supply well is 330 feet deep and is
screened at a depth of 295 feet below land surface. No other active drinking water supply wells
or municipal water supply wells were reportedly identified within 1,500 feet of the source area
during previous investigations (Terracon, 2021).
An irrigation well was previously identified on the western adjoining property, a parsonage for a
nearby church across Oak Street, approximately 100 feet west and upgradient of the source area.
This irrigation well reportedly is not connected to the parsonage and is not used for drinking
purposes. (Terracon, 2021).
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
3
2.0 SITE HISTORY
The following description of historical site activities was obtained from a report titled “Monitoring
Report - Former Norris Luv Station (Incident #32107)” dated November 10, 2021, by Terracon
Consultants, Inc. (Terracon, 2021). Tabulated historic groundwater elevations and laboratory
analytical results from this report are provided in Appendix A for reference. Locations of referenced
wells are depicted on Figure 2.
•The former on-site underground storage tank (UST) system consisted of: two 10,000-gallon
and two 1,000-gallon gasoline tanks; and one 500-gallon, one 1,000-gallon, and one 2,000-
gallon diesel tanks. The entire UST network was removed in March 1993, at which time a
petroleum leak was confirmed from the 10,000-gallon gasoline USTs.
•Free product has been consistently observed in MW-7. Free product in MW-7 had a
thickness of 2.28 feet in February 2020. The free product thickness in MW-7 was reduced
to 0.22 feet in September 2021 following a Multiple Aggressive Fluid Vapor Recovery
(AFVR) event on MW-7 on August 10, 2021. Historically, the free product thickness in
MW-7 also decreased significantly following the removal of contaminated soil in July 2015
and after an AFVR event performed in June 2016.
•The only reported exceedance of a Gross Contaminant Level (GCL) in groundwater at the
site was benzene in MW-6 in 2011 and 2013 (ranging from 5,800 to 8,000 micrograms per
liter [µg/L] compared to the GCL of 5,000 µg/L) before the well was destroyed and replaced
with MW-6R. Groundwater was only sampled from MW-6R one time (in 2016) before it
was also found to have been destroyed. The 2016 benzene concentration in MW-6R (13.1
µg/L) was well below the GCL.
•During recent sampling events (since 2019), benzene concentrations greater than its North
Carolina Groundwater Quality Standard 15A NCAC 2L .0202 (2L Standard) of 1 µg/L were
detected in wells MW-1, MW-4, MW-8, and MW-9, along with MW-6 and MW-6R before
they were destroyed.
•During recent sampling events (since 2019), the following additional volatile organic
compounds (VOCs) have been detected above their 2L Standards but below GCLs in one or
more monitoring well: diisopropyl ether (IPE); ethylbenzene; methyl tert-butyl ether
(MTBE); isopropylbenzene (cumene); naphthalene; n-propylbenzene; and xylene.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
4
3.0 FIELD ACTIVITIES
Field activities performed by ESP on May 31, 2023, included:
•Gauging static water levels in existing on-site monitoring wells.
•Gauging monitoring well MW-7 for the presence of free product.
•Collecting groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-8,
MW-9, MW-10 and MW-11. Although planned, ESP was unable to sample MW-4 because
it could not be located.
As provided in Appendix B, field logbook entries along with groundwater sampling and field
instrument calibration forms were completed in the field to document site activities. Details of
these activities are provided below.
3.1 Water Level Gauging
On May 31, 2023, prior to purging or collection of groundwater samples, depth to groundwater
from the top of casing (TOC) within each monitoring well was measured and recorded using a
decontaminated electronic water level meter. The water level measurements were collected by
first removing the plunger caps from all site monitoring wells and allowing water within the wells
to stabilize. The electronic water level meter probe was then lowered into the well and the depth
to water measured relative to the well’s TOC.
As shown on Table 1, static water level depths ranged from 0.69 to 4.45 ft bTOC (excluding
MW-7 which contained free product). As depicted on Figure 3, based on these static water level
depth measurements converted to relative groundwater elevations, groundwater flow beneath the
site is toward the south-southeast on the northern portion of the site and toward the east on the
southern portion of the site.
3.2 Free Product Evaluation
During the May 31, 2023, gauging event, free product thickness was measured in MW-7 with a
thickness of 1.51 ft (see water level survey form in Appendix B). Free product was not detected
in any of the other on-site monitoring wells.
3.3 Groundwater Sampling
On May 31, 2023, groundwater samples were collected from monitoring wells MW-1, MW-2,
MW-3, MW-8, MW-9, MW-10 and MW-11. Groundwater samples were collected using
dedicated and disposable polyvinyl chloride (PVC) bailers (1.5” x 3’) attached to braided nylon
rope. Prior to groundwater sample collection, each well was purged using the bailer. During
purging, water quality parameters including pH, conductivity, temperature, and turbidity were
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
5
measured using calibrated field water quality instruments. Readings were taken at the start of
purging and periodically until a minimum of three well volumes were removed from the well and
water quality parameters stabilized. Following purging, a groundwater sample for laboratory
analysis was collected from the well using the bailer. The water quality parameters were recorded
on groundwater sampling forms along with time, water level depth, and cumulative volume of
water purged (see groundwater sampling forms in Appendix B).
Groundwater samples were collected following Guidelines for Sampling by the Underground
Storage Tank Section, Division of Waste Management, North Carolina Department of
Environmental Quality (NCDEQ, 2022). Groundwater samples were placed in laboratory-
prepared vials preserved with hydrochloric acid (HCl), labeled, and stored on ice in a cooler for
subsequent delivery under standard chain-of-custody (COC) procedures to Pace Analytical (Pace),
a North Carolina-certified laboratory, located in Huntersville, North Carolina, for analysis. The
groundwater samples were analyzed for VOCs by EPA Method 6200B including MTBE, ethylene
dibromide (EDB), and IPE.
3.4 Field Quality Control Sampling and Analysis
One field duplicate sample was collected from MW-10 and analyzed for VOCs to assess variance.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
6
4.0 GROUNDWATER ANALYTICAL RESULTS
Results of the laboratory analysis of groundwater samples MW-1, MW-2, MW-3, MW-8, MW-9,
MW-10, and MW-11 from the May 31, 2023, sampling event (along with several of the recent
sampling events for comparison) are tabulated in Table 2. As noted in Table 2, the groundwater
analytical results are compared to both 2L Standards and GCLs. The Pace laboratory analytical
report is provided in Appendix C.
No analytes were detected at concentrations exceeding their respective GCLs during the May 31,
2023, sampling event. The only analytes exceeding their respective 2L Standards were benzene
and naphthalene in MW-9, and naphthalene in MW-8 (see Table 2 and Figure 4) detailed as
follows:
•Benzene was detected at 312 µg/L in MW-9 which exceeds its 2L Standard of 1 µg/L.
•Naphthalene was detected at 20.9 µg/L in MW-8 and 53.3 µg/L in MW-9 above its 2L
Standard of 6 µg/L.
Results of the groundwater sampling results relative to each well showing VOCs exceeding their
2L Standards are depicted on Figure 4. Figure 5 depicts the lateral extent of the dissolved benzene
groundwater plume.
As compared to the most recent sampling event performed in September 2021, VOC
concentrations in on-site monitoring wells across the site have generally decreased. For example,
benzene in MW-9 decreased significantly from 1,400 µg/L during the September 2021 sampling
event to 312 µg/L during the May 2023 sampling event as compared to its 2L Standard (1 µg/L).
Naphthalene exceeded its 2L Standard (6 µg/L) in MW-1, MW-8 (highest concentration of 98.3
µg/L), MW-9, and MW-10 during the September 2021 sampling event, but only exceeded its 2L
Standard in MW-8 and MW-9 (highest concentration of 53.3 µg/L) during the May 2023 sampling
event.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
7
5.0 CONCLUSIONS AND RECOMMENDATIONS
Based on results of the above sampling and assessment activities, ESP concludes the following:
•Static water levels ranged from 0.69 to 4.45 ft bTOC.
•The general direction of groundwater flow beneath the site is toward the south-southeast
on the northern portion of the site and toward the east on the southern portion of the site.
•Free product is present in MW-7 with a thickness of 1.51 feet, which is greater than the
0.22 feet of free product measured in September 2021 following the August 2021 AFVR
event on MW-7.
•No VOCs in groundwater exceeded their respective GCLs.
•Benzene and naphthalene were the only two analytes detected about their 2L Standards in
May 2023. Benzene was detected at 312 µg/L in MW-9 which exceeds its 2L Standard of
1 µg/L, and naphthalene was detected at 20.9 µg/L in MW-8 and 53.3 µg/L in MW-9 above
its 2L Standard of 6 µg/L.
•VOC concentrations appear to have generally decreased in monitoring wells across the site
from September 2021 to May 2023.
•A groundwater sample was not collected from MW-4 (unable to locate).
Based on the above results, ESP offers the following recommendations:
•Permanently abandon damaged monitoring well MW-2. A replacement well for MW-2 is
not recommended at this time.
•Permanently abandon destroyed monitoring well MW-6R and install a replacement
monitoring well in the same general location since VOCs were historically detected above
2L Standards at this location.
•Prior to the next sampling event, implement a mobile multi-phase extraction (MMPE)
event on MW-7.
•Continue monitoring the groundwater quality on-site by conducting semi-annual
groundwater sampling events for on-site monitoring wells along with gauging of free
product in MW-7.
Subsequent Monitoring Report ESP Project No. 23-00200-094
Norris Luv Station (Incident #32107)August 16, 2023
8
6.0 REFERENCES
Duplin County, North Carolina GIS website, http://gis.duplincountync.com/maps/default.htm.
1985 Geologic Map of North Carolina, The North Carolina Geological Survey, Phillip M. Brown,
1985.
Guideline for Sampling Underground Storage Tank Section, Division of Waste Management,
North Carolina Division of Environmental Quality, March 7, 2022, Change 4.
Terracon Consultants, Inc., November 10, 2021, Monitoring Report: Former Norris Luv Station
(Incident #32107), NC Highway 41 and Oak Street, Chinquapin, Duplin County, NC.

FIGURES
0 350 700Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
Phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
23-00200-094
ET
CWDATE06/28/2023
FIGURE 1USGS TOPOGRAPHIC SITE LOCATION MAPµAs Shown
CHINQUAPIN, NORTH CAROLINA
SITE BOUNDARY
All locations are approximate.
NORRIS LUV STATION
LEGEND:
NCDEQ Incident No. 32107Norris Luv StationNC Hwy 41 and Oak StreetChinquapin, North Carolina
SINGLE-FAMILY RESIDENCES SINGLE-FAMILY RESIDENCES
SINGLE-FAMILY RESIDENCES
VACANT COMMERCIAL BUSINESSES
NC-41
OAKSTREETNORRIS LUV STATION
FORMER DISPENSER ISLAND
FORMER UST BASIN
FORMER UST BASIN
FORMER UST BASIN
<
<<
<
<
FORMER AST CONCRETE PAD
<
<
<
<
<
FORMER PUMP ISLAND
MW-8
MW-10
MW-4
MW-11
MW-7
MW-9
MW-3
MW-6R MW-5MW-1MW-2<
0 20 40Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
Phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
23-00200-094
ET
CWDATE06/28/2023
FIGURE 2SITE MAPµAs Shown
CHINQUAPIN, NORTH CAROLINA
SITE BOUNDARY
MONITORING WELL
MONITORING WELL (DESTROYED)
MONITORING WELL (NOT LOCATED)
All locations are approximate.
NORRIS LUV STATION
LEGEND:
<
<
<
NCDEQ Incident No. 32107Norris Luv StationNC Hwy 41 and Oak StreetChinquapin, North Carolina
NC-41
OAK STREETNORRIS LUV STATION
<
<<
<
<
<
<
<
<
<
MW-8
MW-10
MW-4
MW-11
MW-7
MW-9
MW-3
MW-6R MW-5MW-1MW-2<
0 20 40Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
Phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
23-00200-094
ET
CWDATE06/28/2023
FIGURE 3GROUNDWATER ELEVATION MAPµAs Shown
CHINQUAPIN, NORTH CAROLINA
SITE BOUNDARYMONITORING WELLMONITORING WELL (DESTROYED)MONITORING WELL (NOT LOCATED)ESTIMATED GROUNDWATER ELEVATION
ESTIMATED GROUNDWATER DIRECTION
All locations are approximate.NM - not measured
FP - free product
NORRIS LUV STATION
LEGEND:
<
<
<
NCDEQ Incident No. 32107
Norris Luv StationNC Hwy 41 and Oak Street
Chinquapin, North Carolina
MW-2 (a deep well) and MW-7 (which containsfree product) were not used for groundwaterelevation contouring purposes.
Groundwater elevations are relative and calculatedusing top of casing elevations established in priorconsultants' reports.
(NM)
(DEEP WELL)
(96.28-ft)
(99.35-ft)
(96.33-ft)
(FP)
(NM)
(97.68-ft)
(95.69-ft)
(96.37-ft)
96
97
99
97
(NM)
NC-41
OAK STREETNORRIS LUV STATION
<
<<
<
<
<
<
<
<
<
MW-8
MW-10
MW-4
MW-11
MW-7
MW-9
MW-3
MW-6R MW-5MW-1MW-2<
0 20 40Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
Phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
23-00200-094
ET
CWDATE06/28/2023
FIGURE 4GROUNDWATER RESULTS MAPµAs Shown
CHINQUAPIN, NORTH CAROLINA
SITE BOUNDARYMONITORING WELL
MONITORING WELL (DESTROYED)MONITORING WELL (NOT LOCATED)
All locations are approximate.
NS - not sampled
NORRIS LUV STATION
LEGEND:
<
<
<
Only Analytes Greater Than 2L Standards Shown.
NCDEQ Incident No. 32107Norris Luv StationNC Hwy 41 and Oak StreetChinquapin, North Carolina
Samples Collected on 5/31/23 Bolded concentrations are greater than the 2LStandard.
Yellow highlighted values indicate constituentconcentrations greater than the GCL.
NS NS
NSNS
NC-41
OAKSTREET<
<
<<
<
<
<
<
<
<
<
MW-8
MW-10
MW-4
MW-11
MW-7
MW-9
MW-3
MW-6R MW-5MW-1MW-2
0 25 50Feet
ESP Associates, Inc.
P.O. Box 7030Charlotte, NC 28241
Phone [phone]
www.espassociates.com
SHEET TITLE
PROJECT
PROJECT NO.
SCALE
DRAWN BY
CHECKED BY
23-00200-094
ET
CWDATE06/28/2023
FIGURE 5BENZENE ISOCONCENTRATION MAPµAs Shown
CHINQUAPIN, NORTH CAROLINA
SITE BOUNDARYAPPROXIMATE CONCENTRATION CONTOURMONITORING WELL MONITORING WELL (DESTROYED)MONITORING WELL (NOT LOCATED)
All locations are approximate.Analytical Results Presented in Table 3.
NORRIS LUV STATION
LEGEND:
<
<
<
NCDEQ Incident No. 32107Norris Luv StationNC Hwy 41 and Oak StreetChinquapin, North Carolina
Samples Collected on 5/31/23
Benzene Comparison Criteria:2L Standard - 1 ug/LGCL - 5,000 ug/LND - not detectedNS - not sampled
FP - free product
NDND
ND
FPNS
ND NS
312
NDND NS 1 ug/L
500 ug/L
FP
TABLES
Table 1
Monitoring Well Construction and Groundwater Elevation Data
Norris Luv Station
Chinquapin, North Carolina
NCDEQ Incident No. 32107
Well ID Date
Intalled
Screened
Interval
(ft BGS) a
Top of Casing
Elevation
(ft) b
Date Water
Level & Well
BottomMeasured
Bottom of
Well from
Top of
Casing(ft bTOC)
Depth to Water
from Top of
Casing(ft bTOC)
Groundwater
Elevation
(ft)
Free Product
Thickness
(ft)
MW-1 4/5/2004
unknown
99.85 5/31/2023 12.80 3.52 96.33 --
MW-2 9/1/2004 99.91 5/31/2023 16.10 c 4.45 95.46 --
MW-3 8/25/2004 100.04 5/31/2023 10.54 0.69 99.35 --
MW-4 8/25/2004 Unable to Locate Well
MW-7 1/19/2011 99.67 5/31/2023 14.75 5.10 95.87 d 1.51
MW-8 1/19/2011 99.39 5/31/2023 15.10 3.70 95.69 --
MW-9 1/24/2018 100.14 5/31/2023 9.87 3.86 96.28 --
MW-10 1/24/2018 99.99 5/31/2023 9.92 3.62 96.37 --
MW-11 2/19/2020 99.88 5/31/2023 11.05 2.20 97.68 --
Notes:
a No previous report on file or in the laserfiche database contains screen interval data.
b Top of casing elevations are from previous consultants' monitoring reports (see Appendix A).
c Groundwater monitoring well MW-2 is reportedly a Type III deep aquifer well that potentially has been damaged as anobstruction was encountered at 16.10 ft bTOC on 5/31/2023. Previous reports reportedly indicate that MW-2 is 27 ft deep. Due
to MW-2 reportedly being a deep aquifer well, the groundwater elevation for MW-2 was not used for establishing the shallow
aquifer groundwater flow direction shown on Figure 3.
d Groundwater elevation adjusted for measureable free product by using the following calculation:
(TOC Elevation - Depth to water) + (FP thickness * 0.8581), where 0.8581 is used as the specific gravity of the free product for
consistency with previous consultants' reports. Due to the presence of free product in MW-7, the calculated groundwater
elevation for MW-7 was not used for establishing the shallow aquifer groundwater flow direction shown on Figure 3.
BGS - below ground surfaceft - feet
ft bTOC - feet below TOC
FP - free product
TOC - top of casing

Table 2Summary of Groundwater Analytical ResultsNorris Luv Station
Chinquapin, North CarolinaNCDEQ Incident No. 32107(Page 1 of 2)
Sample ID Collection Date
Benzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene1,2-Dibromoethane(EDB)Diisopropyl ether (IPE)EthylbenzeneIsopropylbenzene(cumene)p-IsopropyltolueneMethyl Tert-Butyl Ethyl(MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylene (Total)m&p-Xyleneo-Xylene2L Standard (µg/L)1 70 70 70 0.02 70 600 70 25 20 6 70 600 400 400 500 500 500
GCL (µg/L)5,000 5,900 8,800 14,750 50 70,000 80,000 30,500 11,700 20,000 6,000 26,100 260,000 28,500 24,100 50,000 50,000 50,000
MW-1
6/4/19 6.1 <0.5 <0.5 <0.5 <0.5 5.5 0.64 5.3 NR 2.3 4.5 4 0.55 1.8 <0.5 8.3 NR NR
2/27/20 MW-1 was found to be located in a large mud puddle on this date and could not be accessed for sampling.
9/15/21 3.7 <0.5 0.73 <0.5 <0.5 3.6 0.98 8.8 NR 1.9 9.4 1.7 <0.5 0.57 <0.5 6.19 NR NR
5/31/23 <0.34 <0.49 0.46J <0.32 <0.27 2.2 <0.30 4.2 NR 1.1 4.7 1.7 <0.24 <0.50 <0.33 NR 1.9 <0.34
MW-2
6/4/19 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 <0.5 NR 1.5 <2.0 <0.5 <0.5 <0.5 <0.5 <1 NR NR
2/27/20 <0.5 <0.5 <0.5 <0.5 <0.5 1.9 <0.5 <0.5 NR 1.6 <2 <0.5 <0.5 <0.5 <0.5 <1 NR NR
9/15/21 <0.5 <0.5 <0.5 <0.5 <0.5 0.84 <0.5 <0.5 NR 0.81 <2 <0.5 <0.5 <0.5 <0.5 <1 NR NR
5/31/23 <0.34 <0.49 <0.40 <0.32 <0.27 3.8 <0.30 <0.33 NR <0.42 <0.64 <0.34 <0.24 <0.50 <0.33 NR <0.71 <0.34
MW-3
6/4/19 A truck was parked over MW-3 on this date and no one was onsite to move the truck. MW-3 was not sampled on this date.
2/27/20 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NR <0.5 <2 <0.5 <0.5 <0.5 <0.5 <1 NR NR
9/15/21 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NR <0.5 <2 <0.5 <0.5 <0.5 <0.5 <1 NR NR
5/31/23 <0.34 <0.49 <0.40 <0.32 <0.27 <0.31 <0.30 <0.33 NR <0.42 <0.64 <0.34 <0.24 <0.50 <0.33 NR <0.71 <0.34
MW-4
6/4/19 <0.5 <0.5 <0.5 <0.5 <0.5 6.7 <0.5 3.3 NR 3.4 <2 2 <0.5 <0.5 <0.5 <1 NR NR
2/27/20 8.3 <0.5 <0.5 <0.5 <0.5 11.8 <0.5 4.6 NR 3.8 7.4 8.3 <0.5 <0.5 <0.5 1.3 NR NR
9/15/21 <0.5 <0.5 <0.5 <0.5 <0.5 0.76 <0.5 <0.5 NR <0.5 <2 <0.5 <0.5 <0.5 <0.5 <1 NR NR
5/31/23 MW-4 was not located and thus was not sampled on this date
MW-5 1/20/15 MW-5 was not located on January 20, 2015 and has reportedly been destroyed since at least 2008.
MW-6 1/31/11 8,000 <20 <20 <20 NR 80 2,500 130 <20 89 330 290 14,000 1,100 230 7,000 NR NR
5/3/13 5,800 940 230 <19 <18 48 6,200 690 130 92 2,000 2,300 14,000 11,000 3,400 27,300 NR NR
1/20/15 MW-6 was noted to be destroyed and was replaced with MW-6R on 2/9/16.
MW-6R 3/8/16 13.1 <1.2 3.1 <1.2 <1.2 <1.2 199 17.9 NR 0.86 J 56.1 51.5 437 346 105 750 NR NR
9/7/17 MW-6R was found to be destroyed on September 7, 2017.
MW-7
6/4/19 Not sampled, 1.99 feet of free product observed in this well.
2/27/20 Not sampled, 2.28 feet of free product observed in this well.
9/15/21 Not sampled, 0.22 feet of free product observed in this well. Note, an AFVR event was performed on this well on August 10, 2021.
5/31/23 Not sampled, 1.51 feet of free product observed in this well.
MW-8
6/4/19 2.5 <0.5 6.8 0.62 <0.5 2.9 <0.5 15.5 NR 3.5 98.1 24 <0.5 1.1 <0.5 2.6 NR NR
2/27/20 0.55 <0.5 2.9 <0.5 <0.5 1.2 <0.5 6.7 NR 2 31.7 8.9 <0.5 <0.5 <0.5 <1 NR NR
9/15/21 1.8 <0.5 6.7 0.58 <0.5 1.6 <0.5 15.6 NR 2.1 98.3 23.0 <0.5 <0.5 <0.5 <1 NR NR
5/31/23 <0.34 <0.49 4.4 0.49J <0.27 0.82 <0.30 8.8 NR 1.5 20.9 9.0 <0.24 <0.50 <0.33 NR <0.71 <0.34
MW-9
6/4/19 4,190 <20 <20 <20 <20 448 1,400 65.9 NR 60.1 187 152 543 257 42.2 981.7 NR NR
2/27/20 23.6 <0.5 <0.5 <0.5 <0.5 18.6 4.4 2.2 NR 2.4 <2 1.7 1.3 2 <0.5 6.5 NR NR
9/15/21 1,400 3.8 J 3.0 J <10 <10 130 160 41 NR 16 87 86 94 3.0 J <10 109 NR NR
5/31/23 312 2.7 1.9 <0.81 <0.68 35.0 66.6 16.7 NR 3.9 53.3 40.4 6.0 <1.2 <0.83 NR 33.2 2.0
Table 2Summary of Groundwater Analytical ResultsNorris Luv Station
Chinquapin, North CarolinaNCDEQ Incident No. 32107(Page 2 of 2)
MW-10
6/4/19 <0.5 0.88 3.7 <0.5 <0.5 <0.5 <0.5 8.8 NR 1.5 12.9 9.5 <0.5 <0.5 <0.5 <1 NR NR
2/27/20 <0.5 <0.5 0.95 <0.5 <0.5 <0.5 <0.5 2.3 NR <0.5 3.7 2.8 <0.5 <0.5 <0.5 <1 NR NR
9/15/21 <0.5 2.8 5.2 0.56 <0.5 0.62 0.13 J 13 NR 1.2 6.4 18 <0.5 <0.5 <0.5 <1 NR NR
5/31/23 <0.34 <0.49 1.7 <0.32 <0.27 <0.31 <0.30 3.5 NR <0.42 2.0 2.4 <0.24 <0.50 <0.33 NR <0.71 <0.34
MW-11 2/27/20 <0.5 <0.5 3.7 <0.5 <0.5 <0.5 1.1 4.7 NR <0.5 6.4 9.1 <0.5 <0.5 <0.5 <1 NR NR
9/15/21 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NR <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 NR NR
5/31/23 <0.34 <0.49 <0.40 <0.32 <0.27 <0.31 <0.30 <0.33 NR <0.42 <0.64 <0.34 <0.24 <0.50 <0.33 NR <0.71 <0.34
Field Duplicate
(MW-10)5/31/23 <0.34 <0.49 2.4 <0.32 <0.27 <0.31 <0.30 5.2 NR <0.42 2.7 3.7 <0.24 <0.50 <0.33 NR <0.71 <0.34
Notes:
Bold values indicate constituent concentrations were greater than the 2L Standard.
Yellow highlighted values indicate constituent concentrations were greater than the GCL.
Samples presented prior to the May 31, 2023 event were obtained from prevous consultants reports.
<## - less than the method detection limit
µg/L - micrograms per liter
2L Standard - North Carolina 02L standard for groundwater
GCL - Gross Contaminant Level
J - Estimated concentration above the method detection limit and below the reporting limit.
NR - not reported
Sample ID Collection Date
Benzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene1,2-Dibromoethane(EDB)Diisopropyl ether (IPE)EthylbenzeneIsopropylbenzene(cumene)p-IsopropyltolueneMethyl Tert-Butyl Ethyl(MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylene (Total)m&p-Xyleneo-Xylene2L Standard (µg/L)1 70 70 70 0.02 70 600 70 25 20 6 70 600 400 400 500 500 500
GCL (µg/L)5,000 5,900 8,800 14,750 50 70,000 80,000 30,500 11,700 20,000 6,000 26,100 260,000 28,500 24,100 50,000 50,000 50,000
APPENDIX A
APPENDIX B
APPENDIX C
#=CL#
July 06, 2023
LIMS USE: FR - CHRIS WARD
LIMS OBJECT ID: 92670120
92670120
Project:
Pace Project No.:
RE:
Chris Ward
ESP Associates
3475 Lakemont Boulevard
Fort Mill, SC 29708
FORMER NORRIS LUV STATION
Dear Chris Ward:
Enclosed are the analytical results for sample(s) received by the laboratory on June 01, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
Revision 1: J-flags set to <MDL.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
cc: Matt Craig, ESP Associates
Account Payable, ESP Associates
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 36
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Lab ID Sample ID Matrix Date Collected Date Received
92670120001 MW1 Water 05/31/23 15:25 06/01/23 11:36
92670120002 MW2 Water 05/31/23 14:45 06/01/23 11:36
92670120003 MW3 Water 05/31/23 14:00 06/01/23 11:36
92670120004 MW8 Water 05/31/23 17:15 06/01/23 11:36
92670120005 MW9 Water 05/31/23 15:55 06/01/23 11:36
92670120006 MW10 Water 05/31/23 17:35 06/01/23 11:36
92670120007 MW11 Water 05/31/23 16:30 06/01/23 11:36
92670120008 DUPLICATE Water 05/31/23 17:40 06/01/23 11:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92670120001 MW1 SM 6200B 63 PASI-CSAS
92670120002 MW2 SM 6200B 63 PASI-CSAS
92670120003 MW3 SM 6200B 63 PASI-CSAS
92670120004 MW8 SM 6200B 63 PASI-CSAS
92670120005 MW9 SM 6200B 63 PASI-CSAS
92670120006 MW10 SM 6200B 63 PASI-CSAS
92670120007 MW11 SM 6200B 63 PASI-CSAS
92670120008 DUPLICATE SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW1 Lab ID: 92670120001 Collected: 05/31/23 15:25 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/08/23 01:03 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 06/08/23 01:03 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/08/23 01:03 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/08/23 01:03 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 06/08/23 01:03 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 06/08/23 01:03 74-83-95.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/08/23 01:03 104-51-80.50 0.49 1
sec-Butylbenzene 0.46J ug/L 06/08/23 01:03 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 06/08/23 01:03 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/08/23 01:03 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 06/08/23 01:03 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 06/08/23 01:03 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 06/08/23 01:03 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 06/08/23 01:03 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/08/23 01:03 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/08/23 01:03 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/08/23 01:03 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 06/08/23 01:03 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/08/23 01:03 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 06/08/23 01:03 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/08/23 01:03 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/08/23 01:03 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/08/23 01:03 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/08/23 01:03 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/08/23 01:03 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/08/23 01:03 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/08/23 01:03 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/08/23 01:03 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/08/23 01:03 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/08/23 01:03 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/08/23 01:03 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/08/23 01:03 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 06/08/23 01:03 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 06/08/23 01:03 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/08/23 01:03 10061-02-60.50 0.36 1
Diisopropyl ether 2.2 ug/L 06/08/23 01:03 108-20-30.50 0.31 1
Ethylbenzene <0.30 ug/L 06/08/23 01:03 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/08/23 01:03 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)4.2 ug/L 06/08/23 01:03 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 06/08/23 01:03 75-09-22.0 2.0 1
Methyl-tert-butyl ether 1.1 ug/L 06/08/23 01:03 1634-04-40.50 0.42 1
Naphthalene 4.7 ug/L 06/08/23 01:03 91-20-32.0 0.64 1
n-Propylbenzene 1.7 ug/L 06/08/23 01:03 103-65-10.50 0.34 1
Styrene <0.29 ug/L 06/08/23 01:03 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/08/23 01:03 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW1 Lab ID: 92670120001 Collected: 05/31/23 15:25 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/08/23 01:03 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/08/23 01:03 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/08/23 01:03 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/08/23 01:03 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/08/23 01:03 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 06/08/23 01:03 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/08/23 01:03 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 06/08/23 01:03 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/08/23 01:03 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/08/23 01:03 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/08/23 01:03 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/08/23 01:03 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 06/08/23 01:03 75-01-41.0 0.39 1
m&p-Xylene 1.9 ug/L 06/08/23 01:03 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 06/08/23 01:03 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %06/08/23 01:03 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/08/23 01:03 460-00-470-130 1
Toluene-d8 (S)99 %06/08/23 01:03 2037-26-570-130 1
Sample: MW2 Lab ID: 92670120002 Collected: 05/31/23 14:45 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/07/23 07:15 71-43-2 M10.50 0.34 1
Bromobenzene <0.29 ug/L 06/07/23 07:15 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/07/23 07:15 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/07/23 07:15 75-27-4 M10.50 0.31 1
Bromoform <0.34 ug/L 06/07/23 07:15 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 06/07/23 07:15 74-83-95.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/07/23 07:15 104-51-8 M10.50 0.49 1
sec-Butylbenzene <0.40 ug/L 06/07/23 07:15 135-98-8 M10.50 0.40 1
tert-Butylbenzene <0.32 ug/L 06/07/23 07:15 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/07/23 07:15 56-23-5 M10.50 0.33 1
Chlorobenzene <0.28 ug/L 06/07/23 07:15 108-90-7 M10.50 0.28 1
Chloroethane <0.65 ug/L 06/07/23 07:15 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 06/07/23 07:15 67-66-3 M10.50 0.43 1
Chloromethane <0.54 ug/L 06/07/23 07:15 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/07/23 07:15 95-49-8 M10.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/07/23 07:15 106-43-4 M10.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/07/23 07:15 96-12-8 M11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW2 Lab ID: 92670120002 Collected: 05/31/23 14:45 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane <0.36 ug/L 06/07/23 07:15 124-48-1 M10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/07/23 07:15 106-93-4 M10.50 0.27 1
Dibromomethane <0.39 ug/L 06/07/23 07:15 74-95-3 M10.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/07/23 07:15 95-50-1 M10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/07/23 07:15 541-73-1 M10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/07/23 07:15 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/07/23 07:15 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/07/23 07:15 75-34-3 M10.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/07/23 07:15 107-06-2 M10.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/07/23 07:15 75-35-4 M10.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/07/23 07:15 156-59-2 M10.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/07/23 07:15 156-60-5 M10.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/07/23 07:15 78-87-5 M10.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/07/23 07:15 142-28-9 M10.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/07/23 07:15 594-20-7 M10.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 06/07/23 07:15 563-58-6 M10.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 06/07/23 07:15 10061-01-5 M10.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/07/23 07:15 10061-02-6 M10.50 0.36 1
Diisopropyl ether 3.8 ug/L 06/07/23 07:15 108-20-3 M10.50 0.31 1
Ethylbenzene <0.30 ug/L 06/07/23 07:15 100-41-4 M10.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/07/23 07:15 87-68-3 M12.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 06/07/23 07:15 98-82-8 M10.50 0.33 1
Methylene Chloride <2.0 ug/L 06/07/23 07:15 75-09-2 M12.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 06/07/23 07:15 1634-04-4 M10.50 0.42 1
Naphthalene <0.64 ug/L 06/07/23 07:15 91-20-3 M12.0 0.64 1
n-Propylbenzene <0.34 ug/L 06/07/23 07:15 103-65-1 M10.50 0.34 1
Styrene <0.29 ug/L 06/07/23 07:15 100-42-5 M10.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/07/23 07:15 630-20-6 M10.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/07/23 07:15 79-34-5 M10.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/07/23 07:15 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/07/23 07:15 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/07/23 07:15 87-61-6 M12.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/07/23 07:15 120-82-1 M12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 06/07/23 07:15 71-55-6 M10.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/07/23 07:15 79-00-5 M10.50 0.32 1
Trichloroethene <0.38 ug/L 06/07/23 07:15 79-01-6 M10.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/07/23 07:15 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/07/23 07:15 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/07/23 07:15 95-63-6 M10.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/07/23 07:15 108-67-8 M10.50 0.33 1
Vinyl chloride <0.39 ug/L 06/07/23 07:15 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 06/07/23 07:15 179601-23-1 M11.0 0.71 1
o-Xylene <0.34 ug/L 06/07/23 07:15 95-47-6 M10.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %06/07/23 07:15 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW2 Lab ID: 92670120002 Collected: 05/31/23 14:45 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)97 %06/07/23 07:15 460-00-470-130 1
Toluene-d8 (S)99 %06/07/23 07:15 2037-26-570-130 1
Sample: MW3 Lab ID: 92670120003 Collected: 05/31/23 14:00 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/07/23 07:33 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 06/07/23 07:33 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/07/23 07:33 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/07/23 07:33 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 06/07/23 07:33 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 06/07/23 07:33 74-83-95.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/07/23 07:33 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 06/07/23 07:33 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 06/07/23 07:33 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/07/23 07:33 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 06/07/23 07:33 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 06/07/23 07:33 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 06/07/23 07:33 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 06/07/23 07:33 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/07/23 07:33 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/07/23 07:33 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/07/23 07:33 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 06/07/23 07:33 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/07/23 07:33 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 06/07/23 07:33 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/07/23 07:33 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/07/23 07:33 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/07/23 07:33 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/07/23 07:33 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/07/23 07:33 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/07/23 07:33 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/07/23 07:33 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/07/23 07:33 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/07/23 07:33 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/07/23 07:33 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/07/23 07:33 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/07/23 07:33 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 06/07/23 07:33 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW3 Lab ID: 92670120003 Collected: 05/31/23 14:00 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene <0.36 ug/L 06/07/23 07:33 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/07/23 07:33 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 06/07/23 07:33 108-20-30.50 0.31 1
Ethylbenzene <0.30 ug/L 06/07/23 07:33 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/07/23 07:33 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 06/07/23 07:33 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 06/07/23 07:33 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 06/07/23 07:33 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 06/07/23 07:33 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 06/07/23 07:33 103-65-10.50 0.34 1
Styrene <0.29 ug/L 06/07/23 07:33 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/07/23 07:33 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/07/23 07:33 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/07/23 07:33 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/07/23 07:33 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/07/23 07:33 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/07/23 07:33 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 06/07/23 07:33 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/07/23 07:33 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 06/07/23 07:33 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/07/23 07:33 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/07/23 07:33 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/07/23 07:33 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/07/23 07:33 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 06/07/23 07:33 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 06/07/23 07:33 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 06/07/23 07:33 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)110 %06/07/23 07:33 17060-07-0 HS70-130 1
4-Bromofluorobenzene (S)97 %06/07/23 07:33 460-00-470-130 1
Toluene-d8 (S)99 %06/07/23 07:33 2037-26-570-130 1
Sample: MW8 Lab ID: 92670120004 Collected: 05/31/23 17:15 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/07/23 12:37 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 06/07/23 12:37 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/07/23 12:37 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/07/23 12:37 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 06/07/23 12:37 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW8 Lab ID: 92670120004 Collected: 05/31/23 17:15 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane <1.7 ug/L 06/07/23 12:37 74-83-95.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/07/23 12:37 104-51-80.50 0.49 1
sec-Butylbenzene 4.4 ug/L 06/07/23 12:37 135-98-80.50 0.40 1
tert-Butylbenzene 0.49J ug/L 06/07/23 12:37 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/07/23 12:37 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 06/07/23 12:37 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 06/07/23 12:37 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 06/07/23 12:37 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 06/07/23 12:37 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/07/23 12:37 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/07/23 12:37 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/07/23 12:37 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 06/07/23 12:37 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/07/23 12:37 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 06/07/23 12:37 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/07/23 12:37 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/07/23 12:37 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/07/23 12:37 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/07/23 12:37 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/07/23 12:37 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/07/23 12:37 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/07/23 12:37 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/07/23 12:37 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/07/23 12:37 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/07/23 12:37 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/07/23 12:37 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/07/23 12:37 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 06/07/23 12:37 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 06/07/23 12:37 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/07/23 12:37 10061-02-60.50 0.36 1
Diisopropyl ether 0.82 ug/L 06/07/23 12:37 108-20-30.50 0.31 1
Ethylbenzene <0.30 ug/L 06/07/23 12:37 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/07/23 12:37 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)8.8 ug/L 06/07/23 12:37 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 06/07/23 12:37 75-09-22.0 2.0 1
Methyl-tert-butyl ether 1.5 ug/L 06/07/23 12:37 1634-04-40.50 0.42 1
Naphthalene 20.9 ug/L 06/07/23 12:37 91-20-32.0 0.64 1
n-Propylbenzene 9.0 ug/L 06/07/23 12:37 103-65-10.50 0.34 1
Styrene <0.29 ug/L 06/07/23 12:37 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/07/23 12:37 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/07/23 12:37 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/07/23 12:37 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/07/23 12:37 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/07/23 12:37 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/07/23 12:37 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW8 Lab ID: 92670120004 Collected: 05/31/23 17:15 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane <0.33 ug/L 06/07/23 12:37 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/07/23 12:37 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 06/07/23 12:37 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/07/23 12:37 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/07/23 12:37 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/07/23 12:37 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/07/23 12:37 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 06/07/23 12:37 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 06/07/23 12:37 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 06/07/23 12:37 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)110 %06/07/23 12:37 17060-07-0 HS70-130 1
4-Bromofluorobenzene (S)99 %06/07/23 12:37 460-00-470-130 1
Toluene-d8 (S)99 %06/07/23 12:37 2037-26-570-130 1
Sample: MW9 Lab ID: 92670120005 Collected: 05/31/23 15:55 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 312 ug/L 06/08/23 09:05 71-43-21.2 0.86 2.5
Bromobenzene <0.72 ug/L 06/08/23 09:05 108-86-11.2 0.72 2.5
Bromochloromethane <1.2 ug/L 06/08/23 09:05 74-97-51.2 1.2 2.5
Bromodichloromethane <0.77 ug/L 06/08/23 09:05 75-27-41.2 0.77 2.5
Bromoform <0.85 ug/L 06/08/23 09:05 75-25-21.2 0.85 2.5
Bromomethane <4.2 ug/L 06/08/23 09:05 74-83-912.5 4.2 2.5
n-Butylbenzene 2.7 ug/L 06/08/23 09:05 104-51-81.2 1.2 2.5
sec-Butylbenzene 1.9 ug/L 06/08/23 09:05 135-98-81.2 1.0 2.5
tert-Butylbenzene <0.81 ug/L 06/08/23 09:05 98-06-61.2 0.81 2.5
Carbon tetrachloride <0.83 ug/L 06/08/23 09:05 56-23-51.2 0.83 2.5
Chlorobenzene <0.71 ug/L 06/08/23 09:05 108-90-71.2 0.71 2.5
Chloroethane <1.6 ug/L 06/08/23 09:05 75-00-32.5 1.6 2.5
Chloroform <1.1 ug/L 06/08/23 09:05 67-66-31.2 1.1 2.5
Chloromethane <1.4 ug/L 06/08/23 09:05 74-87-32.5 1.4 2.5
2-Chlorotoluene <0.80 ug/L 06/08/23 09:05 95-49-81.2 0.80 2.5
4-Chlorotoluene <0.81 ug/L 06/08/23 09:05 106-43-41.2 0.81 2.5
1,2-Dibromo-3-chloropropane <0.85 ug/L 06/08/23 09:05 96-12-82.5 0.85 2.5
Dibromochloromethane <0.90 ug/L 06/08/23 09:05 124-48-11.2 0.90 2.5
1,2-Dibromoethane (EDB)<0.68 ug/L 06/08/23 09:05 106-93-41.2 0.68 2.5
Dibromomethane <0.98 ug/L 06/08/23 09:05 74-95-31.2 0.98 2.5
1,2-Dichlorobenzene <0.85 ug/L 06/08/23 09:05 95-50-11.2 0.85 2.5
1,3-Dichlorobenzene <0.85 ug/L 06/08/23 09:05 541-73-11.2 0.85 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW9 Lab ID: 92670120005 Collected: 05/31/23 15:55 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene <0.83 ug/L 06/08/23 09:05 106-46-71.2 0.83 2.5
Dichlorodifluoromethane <0.86 ug/L 06/08/23 09:05 75-71-8 IH1.2 0.86 2.5
1,1-Dichloroethane <0.92 ug/L 06/08/23 09:05 75-34-31.2 0.92 2.5
1,2-Dichloroethane <0.80 ug/L 06/08/23 09:05 107-06-21.2 0.80 2.5
1,1-Dichloroethene <0.87 ug/L 06/08/23 09:05 75-35-41.2 0.87 2.5
cis-1,2-Dichloroethene <0.96 ug/L 06/08/23 09:05 156-59-21.2 0.96 2.5
trans-1,2-Dichloroethene <0.99 ug/L 06/08/23 09:05 156-60-51.2 0.99 2.5
1,2-Dichloropropane <0.89 ug/L 06/08/23 09:05 78-87-51.2 0.89 2.5
1,3-Dichloropropane <0.71 ug/L 06/08/23 09:05 142-28-91.2 0.71 2.5
2,2-Dichloropropane <0.97 ug/L 06/08/23 09:05 594-20-71.2 0.97 2.5
1,1-Dichloropropene <1.1 ug/L 06/08/23 09:05 563-58-61.2 1.1 2.5
cis-1,3-Dichloropropene <0.91 ug/L 06/08/23 09:05 10061-01-51.2 0.91 2.5
trans-1,3-Dichloropropene <0.91 ug/L 06/08/23 09:05 10061-02-61.2 0.91 2.5
Diisopropyl ether 35.0 ug/L 06/08/23 09:05 108-20-31.2 0.77 2.5
Ethylbenzene 66.6 ug/L 06/08/23 09:05 100-41-41.2 0.76 2.5
Hexachloro-1,3-butadiene <3.8 ug/L 06/08/23 09:05 87-68-35.0 3.8 2.5
Isopropylbenzene (Cumene)16.7 ug/L 06/08/23 09:05 98-82-81.2 0.83 2.5
Methylene Chloride <4.9 ug/L 06/08/23 09:05 75-09-25.0 4.9 2.5
Methyl-tert-butyl ether 3.9 ug/L 06/08/23 09:05 1634-04-41.2 1.1 2.5
Naphthalene 53.3 ug/L 06/08/23 09:05 91-20-35.0 1.6 2.5
n-Propylbenzene 40.4 ug/L 06/08/23 09:05 103-65-11.2 0.85 2.5
Styrene <0.73 ug/L 06/08/23 09:05 100-42-51.2 0.73 2.5
1,1,1,2-Tetrachloroethane <0.78 ug/L 06/08/23 09:05 630-20-61.2 0.78 2.5
1,1,2,2-Tetrachloroethane <0.56 ug/L 06/08/23 09:05 79-34-51.2 0.56 2.5
Tetrachloroethene <0.73 ug/L 06/08/23 09:05 127-18-41.2 0.73 2.5
Toluene 6.0 ug/L 06/08/23 09:05 108-88-31.2 0.60 2.5
1,2,3-Trichlorobenzene <2.0 ug/L 06/08/23 09:05 87-61-65.0 2.0 2.5
1,2,4-Trichlorobenzene <1.6 ug/L 06/08/23 09:05 120-82-15.0 1.6 2.5
1,1,1-Trichloroethane <0.83 ug/L 06/08/23 09:05 71-55-61.2 0.83 2.5
1,1,2-Trichloroethane <0.81 ug/L 06/08/23 09:05 79-00-51.2 0.81 2.5
Trichloroethene <0.96 ug/L 06/08/23 09:05 79-01-61.2 0.96 2.5
Trichlorofluoromethane <0.74 ug/L 06/08/23 09:05 75-69-42.5 0.74 2.5
1,2,3-Trichloropropane <0.65 ug/L 06/08/23 09:05 96-18-41.2 0.65 2.5
1,2,4-Trimethylbenzene <1.2 ug/L 06/08/23 09:05 95-63-61.2 1.2 2.5
1,3,5-Trimethylbenzene <0.83 ug/L 06/08/23 09:05 108-67-81.2 0.83 2.5
Vinyl chloride <0.96 ug/L 06/08/23 09:05 75-01-42.5 0.96 2.5
m&p-Xylene 33.2 ug/L 06/08/23 09:05 179601-23-12.5 1.8 2.5
o-Xylene 2.0 ug/L 06/08/23 09:05 95-47-61.2 0.84 2.5
Surrogates
1,2-Dichloroethane-d4 (S)107 %06/08/23 09:05 17060-07-070-130 2.5
4-Bromofluorobenzene (S)100 %06/08/23 09:05 460-00-470-130 2.5
Toluene-d8 (S)99 %06/08/23 09:05 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW10 Lab ID: 92670120006 Collected: 05/31/23 17:35 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/07/23 07:51 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 06/07/23 07:51 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/07/23 07:51 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/07/23 07:51 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 06/07/23 07:51 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 06/07/23 07:51 74-83-95.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/07/23 07:51 104-51-80.50 0.49 1
sec-Butylbenzene 1.7 ug/L 06/07/23 07:51 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 06/07/23 07:51 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/07/23 07:51 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 06/07/23 07:51 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 06/07/23 07:51 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 06/07/23 07:51 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 06/07/23 07:51 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/07/23 07:51 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/07/23 07:51 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/07/23 07:51 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 06/07/23 07:51 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/07/23 07:51 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 06/07/23 07:51 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/07/23 07:51 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/07/23 07:51 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/07/23 07:51 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/07/23 07:51 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/07/23 07:51 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/07/23 07:51 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/07/23 07:51 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/07/23 07:51 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/07/23 07:51 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/07/23 07:51 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/07/23 07:51 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/07/23 07:51 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 06/07/23 07:51 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 06/07/23 07:51 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/07/23 07:51 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 06/07/23 07:51 108-20-30.50 0.31 1
Ethylbenzene <0.30 ug/L 06/07/23 07:51 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/07/23 07:51 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)3.5 ug/L 06/07/23 07:51 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 06/07/23 07:51 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 06/07/23 07:51 1634-04-40.50 0.42 1
Naphthalene 2.0 ug/L 06/07/23 07:51 91-20-32.0 0.64 1
n-Propylbenzene 2.4 ug/L 06/07/23 07:51 103-65-10.50 0.34 1
Styrene <0.29 ug/L 06/07/23 07:51 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/07/23 07:51 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW10 Lab ID: 92670120006 Collected: 05/31/23 17:35 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/07/23 07:51 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/07/23 07:51 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/07/23 07:51 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/07/23 07:51 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/07/23 07:51 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 06/07/23 07:51 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/07/23 07:51 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 06/07/23 07:51 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/07/23 07:51 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/07/23 07:51 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/07/23 07:51 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/07/23 07:51 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 06/07/23 07:51 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 06/07/23 07:51 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 06/07/23 07:51 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %06/07/23 07:51 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/07/23 07:51 460-00-470-130 1
Toluene-d8 (S)99 %06/07/23 07:51 2037-26-570-130 1
Sample: MW11 Lab ID: 92670120007 Collected: 05/31/23 16:30 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/08/23 07:54 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 06/08/23 07:54 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/08/23 07:54 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/08/23 07:54 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 06/08/23 07:54 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 06/08/23 07:54 74-83-9 M1,R15.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/08/23 07:54 104-51-8 M10.50 0.49 1
sec-Butylbenzene <0.40 ug/L 06/08/23 07:54 135-98-8 M10.50 0.40 1
tert-Butylbenzene <0.32 ug/L 06/08/23 07:54 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/08/23 07:54 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 06/08/23 07:54 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 06/08/23 07:54 75-00-3 R11.0 0.65 1
Chloroform <0.43 ug/L 06/08/23 07:54 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 06/08/23 07:54 74-87-3 M1,R11.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/08/23 07:54 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/08/23 07:54 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/08/23 07:54 96-12-81.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW11 Lab ID: 92670120007 Collected: 05/31/23 16:30 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane <0.36 ug/L 06/08/23 07:54 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/08/23 07:54 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 06/08/23 07:54 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/08/23 07:54 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/08/23 07:54 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/08/23 07:54 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/08/23 07:54 75-71-8 IH,M1,
R10.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/08/23 07:54 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/08/23 07:54 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/08/23 07:54 75-35-4 M1,R10.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/08/23 07:54 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/08/23 07:54 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/08/23 07:54 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/08/23 07:54 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/08/23 07:54 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 06/08/23 07:54 563-58-6 M10.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 06/08/23 07:54 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/08/23 07:54 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 06/08/23 07:54 108-20-30.50 0.31 1
Ethylbenzene <0.30 ug/L 06/08/23 07:54 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/08/23 07:54 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 06/08/23 07:54 98-82-8 M10.50 0.33 1
Methylene Chloride <2.0 ug/L 06/08/23 07:54 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 06/08/23 07:54 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 06/08/23 07:54 91-20-3 M12.0 0.64 1
n-Propylbenzene <0.34 ug/L 06/08/23 07:54 103-65-10.50 0.34 1
Styrene <0.29 ug/L 06/08/23 07:54 100-42-5 M10.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/08/23 07:54 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/08/23 07:54 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/08/23 07:54 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/08/23 07:54 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/08/23 07:54 87-61-6 M12.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/08/23 07:54 120-82-1 M12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 06/08/23 07:54 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/08/23 07:54 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 06/08/23 07:54 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/08/23 07:54 75-69-4 R11.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/08/23 07:54 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/08/23 07:54 95-63-6 M10.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/08/23 07:54 108-67-8 M10.50 0.33 1
Vinyl chloride <0.39 ug/L 06/08/23 07:54 75-01-4 M1,R11.0 0.39 1
m&p-Xylene <0.71 ug/L 06/08/23 07:54 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 06/08/23 07:54 95-47-60.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: MW11 Lab ID: 92670120007 Collected: 05/31/23 16:30 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
1,2-Dichloroethane-d4 (S)112 %06/08/23 07:54 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %06/08/23 07:54 460-00-470-130 1
Toluene-d8 (S)99 %06/08/23 07:54 2037-26-570-130 1
Sample: DUPLICATE Lab ID: 92670120008 Collected: 05/31/23 17:40 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.34 ug/L 06/07/23 12:19 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 06/07/23 12:19 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 06/07/23 12:19 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 06/07/23 12:19 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 06/07/23 12:19 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 06/07/23 12:19 74-83-95.0 1.7 1
n-Butylbenzene <0.49 ug/L 06/07/23 12:19 104-51-80.50 0.49 1
sec-Butylbenzene 2.4 ug/L 06/07/23 12:19 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 06/07/23 12:19 98-06-60.50 0.32 1
Carbon tetrachloride <0.33 ug/L 06/07/23 12:19 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 06/07/23 12:19 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 06/07/23 12:19 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 06/07/23 12:19 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 06/07/23 12:19 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 06/07/23 12:19 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 06/07/23 12:19 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 06/07/23 12:19 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 06/07/23 12:19 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 06/07/23 12:19 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 06/07/23 12:19 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 06/07/23 12:19 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 06/07/23 12:19 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 06/07/23 12:19 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 06/07/23 12:19 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 06/07/23 12:19 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 06/07/23 12:19 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 06/07/23 12:19 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 06/07/23 12:19 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 06/07/23 12:19 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 06/07/23 12:19 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 06/07/23 12:19 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 06/07/23 12:19 594-20-70.50 0.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Sample: DUPLICATE Lab ID: 92670120008 Collected: 05/31/23 17:40 Received: 06/01/23 11:36 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloropropene <0.43 ug/L 06/07/23 12:19 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 06/07/23 12:19 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 06/07/23 12:19 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 06/07/23 12:19 108-20-30.50 0.31 1
Ethylbenzene <0.30 ug/L 06/07/23 12:19 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene <1.5 ug/L 06/07/23 12:19 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)5.2 ug/L 06/07/23 12:19 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 06/07/23 12:19 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 06/07/23 12:19 1634-04-40.50 0.42 1
Naphthalene 2.7 ug/L 06/07/23 12:19 91-20-32.0 0.64 1
n-Propylbenzene 3.7 ug/L 06/07/23 12:19 103-65-10.50 0.34 1
Styrene <0.29 ug/L 06/07/23 12:19 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 06/07/23 12:19 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 06/07/23 12:19 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 06/07/23 12:19 127-18-40.50 0.29 1
Toluene <0.24 ug/L 06/07/23 12:19 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 06/07/23 12:19 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 06/07/23 12:19 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 06/07/23 12:19 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 06/07/23 12:19 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 06/07/23 12:19 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 06/07/23 12:19 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 06/07/23 12:19 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 06/07/23 12:19 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 06/07/23 12:19 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 06/07/23 12:19 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 06/07/23 12:19 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 06/07/23 12:19 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)112 %06/07/23 12:19 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/07/23 12:19 460-00-470-130 1
Toluene-d8 (S)100 %06/07/23 12:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
778336
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92670120002, 92670120003, 92670120004, 92670120006, 92670120008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4037414
Associated Lab Samples:92670120002, 92670120003, 92670120004, 92670120006, 92670120008
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 06/07/23 06:030.31
1,1,1-Trichloroethane ug/L <0.33 0.50 06/07/23 06:030.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 06/07/23 06:030.22
1,1,2-Trichloroethane ug/L <0.32 0.50 06/07/23 06:030.32
1,1-Dichloroethane ug/L <0.37 0.50 06/07/23 06:030.37
1,1-Dichloroethene ug/L <0.35 0.50 06/07/23 06:030.35
1,1-Dichloropropene ug/L <0.43 0.50 06/07/23 06:030.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 06/07/23 06:030.81
1,2,3-Trichloropropane ug/L <0.26 0.50 06/07/23 06:030.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 06/07/23 06:030.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 06/07/23 06:030.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 06/07/23 06:030.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 06/07/23 06:030.27
1,2-Dichlorobenzene ug/L <0.34 0.50 06/07/23 06:030.34
1,2-Dichloroethane ug/L <0.32 0.50 06/07/23 06:030.32
1,2-Dichloropropane ug/L <0.36 0.50 06/07/23 06:030.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 06/07/23 06:030.33
1,3-Dichlorobenzene ug/L <0.34 0.50 06/07/23 06:030.34
1,3-Dichloropropane ug/L <0.28 0.50 06/07/23 06:030.28
1,4-Dichlorobenzene ug/L <0.33 0.50 06/07/23 06:030.33
2,2-Dichloropropane ug/L <0.39 0.50 06/07/23 06:030.39
2-Chlorotoluene ug/L <0.32 0.50 06/07/23 06:030.32
4-Chlorotoluene ug/L <0.32 0.50 06/07/23 06:030.32
Benzene ug/L <0.34 0.50 06/07/23 06:030.34
Bromobenzene ug/L <0.29 0.50 06/07/23 06:030.29
Bromochloromethane ug/L <0.47 0.50 06/07/23 06:030.47
Bromodichloromethane ug/L <0.31 0.50 06/07/23 06:030.31
Bromoform ug/L <0.34 0.50 06/07/23 06:030.34
Bromomethane ug/L <1.7 5.0 06/07/23 06:031.7
Carbon tetrachloride ug/L <0.33 0.50 06/07/23 06:030.33
Chlorobenzene ug/L <0.28 0.50 06/07/23 06:030.28
Chloroethane ug/L <0.65 1.0 06/07/23 06:030.65
Chloroform ug/L <0.43 0.50 06/07/23 06:030.43
Chloromethane ug/L <0.54 1.0 06/07/23 06:030.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 06/07/23 06:030.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 06/07/23 06:030.36
Dibromochloromethane ug/L <0.36 0.50 06/07/23 06:030.36
Dibromomethane ug/L <0.39 0.50 06/07/23 06:030.39
Dichlorodifluoromethane ug/L <0.35 0.50 IH06/07/23 06:030.35
Diisopropyl ether ug/L <0.31 0.50 06/07/23 06:030.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4037414
Associated Lab Samples:92670120002, 92670120003, 92670120004, 92670120006, 92670120008
Matrix: Water
AnalyzedMDL
Ethylbenzene ug/L <0.30 0.50 06/07/23 06:030.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 06/07/23 06:031.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 06/07/23 06:030.33
m&p-Xylene ug/L <0.71 1.0 06/07/23 06:030.71
Methyl-tert-butyl ether ug/L <0.42 0.50 06/07/23 06:030.42
Methylene Chloride ug/L <2.0 2.0 06/07/23 06:032.0
n-Butylbenzene ug/L <0.49 0.50 06/07/23 06:030.49
n-Propylbenzene ug/L <0.34 0.50 06/07/23 06:030.34
Naphthalene ug/L <0.64 2.0 06/07/23 06:030.64
o-Xylene ug/L <0.34 0.50 06/07/23 06:030.34
sec-Butylbenzene ug/L <0.40 0.50 06/07/23 06:030.40
Styrene ug/L <0.29 0.50 06/07/23 06:030.29
tert-Butylbenzene ug/L <0.32 0.50 06/07/23 06:030.32
Tetrachloroethene ug/L <0.29 0.50 06/07/23 06:030.29
Toluene ug/L <0.24 0.50 06/07/23 06:030.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 06/07/23 06:030.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 06/07/23 06:030.36
Trichloroethene ug/L <0.38 0.50 06/07/23 06:030.38
Trichlorofluoromethane ug/L <0.30 1.0 06/07/23 06:030.30
Vinyl chloride ug/L <0.39 1.0 06/07/23 06:030.39
1,2-Dichloroethane-d4 (S)%109 70-130 06/07/23 06:03
4-Bromofluorobenzene (S)%98 70-130 06/07/23 06:03
Toluene-d8 (S)%100 70-130 06/07/23 06:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4037415LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 17.820 89 60-140
1,1,1-Trichloroethane ug/L 18.620 93 60-140
1,1,2,2-Tetrachloroethane ug/L 18.720 94 60-140
1,1,2-Trichloroethane ug/L 18.820 94 60-140
1,1-Dichloroethane ug/L 19.220 96 60-140
1,1-Dichloroethene ug/L 20.320 102 60-140
1,1-Dichloropropene ug/L 19.620 98 60-140
1,2,3-Trichlorobenzene ug/L 18.320 91 60-140
1,2,3-Trichloropropane ug/L 18.420 92 60-140
1,2,4-Trichlorobenzene ug/L 17.620 88 60-140
1,2,4-Trimethylbenzene ug/L 18.720 93 60-140
1,2-Dibromo-3-chloropropane ug/L 17.620 88 60-140
1,2-Dibromoethane (EDB)ug/L 19.120 96 60-140
1,2-Dichlorobenzene ug/L 18.320 91 60-140
1,2-Dichloroethane ug/L 19.820 99 60-140
1,2-Dichloropropane ug/L 19.420 97 60-140
1,3,5-Trimethylbenzene ug/L 18.420 92 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4037415LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 17.620 88 60-140
1,3-Dichloropropane ug/L 18.520 92 60-140
1,4-Dichlorobenzene ug/L 17.520 88 60-140
2,2-Dichloropropane ug/L 16.520 83 60-140
2-Chlorotoluene ug/L 17.820 89 60-140
4-Chlorotoluene ug/L 18.620 93 60-140
Benzene ug/L 18.520 93 60-140
Bromobenzene ug/L 17.720 89 60-140
Bromochloromethane ug/L 18.620 93 60-140
Bromodichloromethane ug/L 18.020 90 60-140
Bromoform ug/L 16.520 83 60-140
Bromomethane ug/L 17.220 86 60-140
Carbon tetrachloride ug/L 17.420 87 60-140
Chlorobenzene ug/L 17.820 89 60-140
Chloroethane ug/L 18.720 94 60-140
Chloroform ug/L 18.820 94 60-140
Chloromethane ug/L 19.720 98 60-140
cis-1,2-Dichloroethene ug/L 19.720 98 60-140
cis-1,3-Dichloropropene ug/L 18.520 93 60-140
Dibromochloromethane ug/L 18.520 93 60-140
Dibromomethane ug/L 18.620 93 60-140
Dichlorodifluoromethane ug/L 24.5 IH20123 60-140
Diisopropyl ether ug/L 19.320 96 60-140
Ethylbenzene ug/L 17.520 88 60-140
Hexachloro-1,3-butadiene ug/L 16.320 82 60-140
Isopropylbenzene (Cumene)ug/L 18.020 90 60-140
m&p-Xylene ug/L 35.540 89 60-140
Methyl-tert-butyl ether ug/L 18.620 93 60-140
Methylene Chloride ug/L 19.020 95 60-140
n-Butylbenzene ug/L 17.320 87 60-140
n-Propylbenzene ug/L 17.420 87 60-140
Naphthalene ug/L 19.720 98 60-140
o-Xylene ug/L 17.820 89 60-140
sec-Butylbenzene ug/L 17.420 87 60-140
Styrene ug/L 19.020 95 60-140
tert-Butylbenzene ug/L 14.320 72 60-140
Tetrachloroethene ug/L 16.020 80 60-140
Toluene ug/L 17.320 86 60-140
trans-1,2-Dichloroethene ug/L 19.920 99 60-140
trans-1,3-Dichloropropene ug/L 18.320 91 60-140
Trichloroethene ug/L 17.720 88 60-140
Trichlorofluoromethane ug/L 18.220 91 60-140
Vinyl chloride ug/L 16.920 85 60-140
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4037416MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92670120002
4037417
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M12014860-140137 8 3020<0.31 29.5 27.3
1,1,1-Trichloroethane ug/L M12015460-140144 7 3020<0.33 30.8 28.8
1,1,2,2-Tetrachloroethane ug/L M12014560-140133 8 3020<0.22 28.9 26.7
1,1,2-Trichloroethane ug/L M12014360-140131 8 3020<0.32 28.5 26.2
1,1-Dichloroethane ug/L M12015160-140140 8 3020<0.37 30.3 28.1
1,1-Dichloroethene ug/L M12015860-140145 9 3020<0.35 31.7 29.0
1,1-Dichloropropene ug/L M12016560-140151 9 3020<0.43 33.1 30.3
1,2,3-Trichlorobenzene ug/L M12014560-140133 8 3020<0.81 29.0 26.6
1,2,3-Trichloropropane ug/L 20 136 60-140126 8 3020<0.26 27.3 25.2
1,2,4-Trichlorobenzene ug/L M12014360-140133 7 3020<0.64 28.6 26.6
1,2,4-Trimethylbenzene ug/L M12015660-140146 7 3020<0.50 31.2 29.1
1,2-Dibromo-3-
chloropropane ug/L M12014260-140130 9 3020<0.34 28.4 26.0
1,2-Dibromoethane (EDB) ug/L M12014960-140138 8 3020<0.27 29.8 27.6
1,2-Dichlorobenzene ug/L M12014360-140136 5 3020<0.34 28.6 27.3
1,2-Dichloroethane ug/L M12015160-140139 8 3020<0.32 30.2 27.8
1,2-Dichloropropane ug/L M12015460-140141 8 3020<0.36 30.7 28.3
1,3,5-Trimethylbenzene ug/L M12015360-140145 6 3020<0.33 30.6 28.9
1,3-Dichlorobenzene ug/L M12014260-140135 5 3020<0.34 28.4 27.0
1,3-Dichloropropane ug/L M12014460-140133 8 3020<0.28 28.8 26.6
1,4-Dichlorobenzene ug/L 20 138 60-140130 6 3020<0.33 27.6 26.1
2,2-Dichloropropane ug/L M12015160-140139 8 3020<0.39 30.1 27.8
2-Chlorotoluene ug/L M12014960-140138 8 3020<0.32 29.9 27.7
4-Chlorotoluene ug/L M12014960-140142 5 3020<0.32 29.7 28.4
Benzene ug/L M12014760-140135 8 3020<0.34 29.4 27.0
Bromobenzene ug/L 20 139 60-140131 6 3020<0.29 27.9 26.2
Bromochloromethane ug/L 20 139 60-140130 7 3020<0.47 27.9 26.0
Bromodichloromethane ug/L M12014460-140133 8 3020<0.31 28.7 26.6
Bromoform ug/L 20 124 60-140115 8 3020<0.34 24.8 22.9
Bromomethane ug/L 20 106 60-14099 7 3020<1.7 21.2 19.8
Carbon tetrachloride ug/L M12015260-140139 9 3020<0.33 30.4 27.7
Chlorobenzene ug/L M12014560-140134 8 3020<0.28 28.9 26.8
Chloroethane ug/L 20 129 60-140118 9 3020<0.65 25.9 23.6
Chloroform ug/L M12014660-140135 8 3020<0.43 29.2 27.0
Chloromethane ug/L 20 101 60-14093 8 3020<0.54 20.2 18.7
cis-1,2-Dichloroethene ug/L M12015260-140141 7 3020<0.38 30.3 28.2
cis-1,3-Dichloropropene ug/L M12014760-140135 9 3020<0.36 29.5 27.0
Dibromochloromethane ug/L M12014460-140134 7 3020<0.36 28.9 26.8
Dibromomethane ug/L M12014460-140135 7 3020<0.39 28.8 26.9
Dichlorodifluoromethane ug/L IH206960-14061 11 3020<0.35 13.7 12.3
Diisopropyl ether ug/L M12015460-140142 7 30203.8 34.6 32.1
Ethylbenzene ug/L M12014660-140135 8 3020<0.30 29.1 27.0
Hexachloro-1,3-butadiene ug/L M12015560-140143 8 3020<1.5 31.1 28.6
Isopropylbenzene(Cumene)ug/L M12015460-140144 7 3020<0.33 30.8 28.8
m&p-Xylene ug/L M14014860-140137 7 3040<0.71 59.0 54.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4037416MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92670120002
4037417
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L M12014460-140134 7 3020<0.42 28.8 26.8
Methylene Chloride ug/L M12014260-140131 8 3020<2.0 28.4 26.2
n-Butylbenzene ug/L M12015660-140147 6 3020<0.49 31.2 29.4
n-Propylbenzene ug/L M12014960-140140 6 3020<0.34 29.8 28.0
Naphthalene ug/L M12015960-140149 7 3020<0.64 31.9 29.8
o-Xylene ug/L M12014760-140137 7 3020<0.34 29.4 27.3
sec-Butylbenzene ug/L M12015560-140146 6 3020<0.40 30.9 29.1
Styrene ug/L M12015360-140143 7 3020<0.29 30.7 28.5
tert-Butylbenzene ug/L 20 125 60-140118 5 3020<0.32 25.0 23.7
Tetrachloroethene ug/L 20 138 60-140129 7 3020<0.29 27.7 25.7
Toluene ug/L 20 140 60-140129 8 3020<0.24 28.0 25.8
trans-1,2-Dichloroethene ug/L M12015660-140144 8 3020<0.40 31.3 28.7
trans-1,3-Dichloropropene ug/L M12014860-140135 9 3020<0.36 29.6 27.0
Trichloroethene ug/L M12014360-140132 8 3020<0.38 28.6 26.4
Trichlorofluoromethane ug/L 20 139 60-140127 9 3020<0.30 27.8 25.3
Vinyl chloride ug/L 20 102 60-14092 10 3020<0.39 20.4 18.4
1,2-Dichloroethane-d4 (S) %104 70-130105
4-Bromofluorobenzene (S) %101 70-130100
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
778650
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92670120001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4038977
Associated Lab Samples:92670120001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 06/07/23 23:520.31
1,1,1-Trichloroethane ug/L <0.33 0.50 06/07/23 23:520.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 06/07/23 23:520.22
1,1,2-Trichloroethane ug/L <0.32 0.50 06/07/23 23:520.32
1,1-Dichloroethane ug/L <0.37 0.50 06/07/23 23:520.37
1,1-Dichloroethene ug/L <0.35 0.50 06/07/23 23:520.35
1,1-Dichloropropene ug/L <0.43 0.50 06/07/23 23:520.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 06/07/23 23:520.81
1,2,3-Trichloropropane ug/L <0.26 0.50 06/07/23 23:520.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 06/07/23 23:520.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 06/07/23 23:520.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 06/07/23 23:520.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 06/07/23 23:520.27
1,2-Dichlorobenzene ug/L <0.34 0.50 06/07/23 23:520.34
1,2-Dichloroethane ug/L <0.32 0.50 06/07/23 23:520.32
1,2-Dichloropropane ug/L <0.36 0.50 06/07/23 23:520.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 06/07/23 23:520.33
1,3-Dichlorobenzene ug/L <0.34 0.50 06/07/23 23:520.34
1,3-Dichloropropane ug/L <0.28 0.50 06/07/23 23:520.28
1,4-Dichlorobenzene ug/L <0.33 0.50 06/07/23 23:520.33
2,2-Dichloropropane ug/L <0.39 0.50 06/07/23 23:520.39
2-Chlorotoluene ug/L <0.32 0.50 06/07/23 23:520.32
4-Chlorotoluene ug/L <0.32 0.50 06/07/23 23:520.32
Benzene ug/L <0.34 0.50 06/07/23 23:520.34
Bromobenzene ug/L <0.29 0.50 06/07/23 23:520.29
Bromochloromethane ug/L <0.47 0.50 06/07/23 23:520.47
Bromodichloromethane ug/L <0.31 0.50 06/07/23 23:520.31
Bromoform ug/L <0.34 0.50 06/07/23 23:520.34
Bromomethane ug/L <1.7 5.0 06/07/23 23:521.7
Carbon tetrachloride ug/L <0.33 0.50 06/07/23 23:520.33
Chlorobenzene ug/L <0.28 0.50 06/07/23 23:520.28
Chloroethane ug/L <0.65 1.0 06/07/23 23:520.65
Chloroform ug/L <0.43 0.50 06/07/23 23:520.43
Chloromethane ug/L <0.54 1.0 06/07/23 23:520.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 06/07/23 23:520.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 06/07/23 23:520.36
Dibromochloromethane ug/L <0.36 0.50 06/07/23 23:520.36
Dibromomethane ug/L <0.39 0.50 06/07/23 23:520.39
Dichlorodifluoromethane ug/L <0.35 0.50 IH06/07/23 23:520.35
Diisopropyl ether ug/L <0.31 0.50 06/07/23 23:520.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4038977
Associated Lab Samples:92670120001
Matrix: Water
AnalyzedMDL
Ethylbenzene ug/L <0.30 0.50 06/07/23 23:520.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 06/07/23 23:521.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 06/07/23 23:520.33
m&p-Xylene ug/L <0.71 1.0 06/07/23 23:520.71
Methyl-tert-butyl ether ug/L <0.42 0.50 06/07/23 23:520.42
Methylene Chloride ug/L <2.0 2.0 06/07/23 23:522.0
n-Butylbenzene ug/L <0.49 0.50 06/07/23 23:520.49
n-Propylbenzene ug/L <0.34 0.50 06/07/23 23:520.34
Naphthalene ug/L <0.64 2.0 06/07/23 23:520.64
o-Xylene ug/L <0.34 0.50 06/07/23 23:520.34
sec-Butylbenzene ug/L <0.40 0.50 06/07/23 23:520.40
Styrene ug/L <0.29 0.50 06/07/23 23:520.29
tert-Butylbenzene ug/L <0.32 0.50 06/07/23 23:520.32
Tetrachloroethene ug/L <0.29 0.50 06/07/23 23:520.29
Toluene ug/L <0.24 0.50 06/07/23 23:520.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 06/07/23 23:520.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 06/07/23 23:520.36
Trichloroethene ug/L <0.38 0.50 06/07/23 23:520.38
Trichlorofluoromethane ug/L <0.30 1.0 06/07/23 23:520.30
Vinyl chloride ug/L <0.39 1.0 06/07/23 23:520.39
1,2-Dichloroethane-d4 (S)%111 70-130 06/07/23 23:52
4-Bromofluorobenzene (S)%98 70-130 06/07/23 23:52
Toluene-d8 (S)%100 70-130 06/07/23 23:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4038978LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.020 95 60-140
1,1,1-Trichloroethane ug/L 19.620 98 60-140
1,1,2,2-Tetrachloroethane ug/L 20.120 101 60-140
1,1,2-Trichloroethane ug/L 20.020 100 60-140
1,1-Dichloroethane ug/L 20.720 103 60-140
1,1-Dichloroethene ug/L 21.420 107 60-140
1,1-Dichloropropene ug/L 20.820 104 60-140
1,2,3-Trichlorobenzene ug/L 18.920 95 60-140
1,2,3-Trichloropropane ug/L 19.020 95 60-140
1,2,4-Trichlorobenzene ug/L 18.420 92 60-140
1,2,4-Trimethylbenzene ug/L 20.120 101 60-140
1,2-Dibromo-3-chloropropane ug/L 19.520 98 60-140
1,2-Dibromoethane (EDB)ug/L 20.420 102 60-140
1,2-Dichlorobenzene ug/L 19.220 96 60-140
1,2-Dichloroethane ug/L 21.120 105 60-140
1,2-Dichloropropane ug/L 20.220 101 60-140
1,3,5-Trimethylbenzene ug/L 19.620 98 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4038978LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 18.920 95 60-140
1,3-Dichloropropane ug/L 19.520 97 60-140
1,4-Dichlorobenzene ug/L 18.420 92 60-140
2,2-Dichloropropane ug/L 17.720 89 60-140
2-Chlorotoluene ug/L 19.420 97 60-140
4-Chlorotoluene ug/L 19.720 98 60-140
Benzene ug/L 19.320 96 60-140
Bromobenzene ug/L 18.520 93 60-140
Bromochloromethane ug/L 19.620 98 60-140
Bromodichloromethane ug/L 19.120 96 60-140
Bromoform ug/L 17.620 88 60-140
Bromomethane ug/L 17.620 88 60-140
Carbon tetrachloride ug/L 18.720 94 60-140
Chlorobenzene ug/L 18.820 94 60-140
Chloroethane ug/L 19.820 99 60-140
Chloroform ug/L 19.320 97 60-140
Chloromethane ug/L 20.620 103 60-140
cis-1,2-Dichloroethene ug/L 20.720 104 60-140
cis-1,3-Dichloropropene ug/L 19.720 98 60-140
Dibromochloromethane ug/L 19.620 98 60-140
Dibromomethane ug/L 20.020 100 60-140
Dichlorodifluoromethane ug/L 24.5 IH20122 60-140
Diisopropyl ether ug/L 20.820 104 60-140
Ethylbenzene ug/L 18.620 93 60-140
Hexachloro-1,3-butadiene ug/L 17.120 85 60-140
Isopropylbenzene (Cumene)ug/L 19.020 95 60-140
m&p-Xylene ug/L 37.540 94 60-140
Methyl-tert-butyl ether ug/L 19.820 99 60-140
Methylene Chloride ug/L 20.220 101 60-140
n-Butylbenzene ug/L 18.920 95 60-140
n-Propylbenzene ug/L 18.720 94 60-140
Naphthalene ug/L 21.320 106 60-140
o-Xylene ug/L 18.820 94 60-140
sec-Butylbenzene ug/L 18.820 94 60-140
Styrene ug/L 20.020 100 60-140
tert-Butylbenzene ug/L 15.420 77 60-140
Tetrachloroethene ug/L 16.920 84 60-140
Toluene ug/L 18.220 91 60-140
trans-1,2-Dichloroethene ug/L 21.120 105 60-140
trans-1,3-Dichloropropene ug/L 19.620 98 60-140
Trichloroethene ug/L 18.420 92 60-140
Trichlorofluoromethane ug/L 19.220 96 60-140
Vinyl chloride ug/L 17.820 89 60-140
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4038979MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92669953001
4038980
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 126 60-140137 8 3020ND25.2 27.3
1,1,1-Trichloroethane ug/L 20 128 60-140140 9 3020ND25.6 28.0
1,1,2,2-Tetrachloroethane ug/L 20 129 60-140138 6 3020ND25.9 27.5
1,1,2-Trichloroethane ug/L 20 124 60-140133 7 3020ND24.8 26.6
1,1-Dichloroethane ug/L 20 125 60-140136 8 3020ND24.9 27.1
1,1-Dichloroethene ug/L 20 106 60-140113 7 3020ND21.2 22.6
1,1-Dichloropropene ug/L M12013760-140146 6 3020ND27.4 29.1
1,2,3-Trichlorobenzene ug/L M12014160-140151 7 3020ND28.2 30.3
1,2,3-Trichloropropane ug/L 20 121 60-140129 6 3020ND24.3 25.8
1,2,4-Trichlorobenzene ug/L M12013660-140149 9 3020ND27.3 29.8
1,2,4-Trimethylbenzene ug/L M12014360-140154 6 30204.5 33.2 35.3
1,2-Dibromo-3-
chloropropane ug/L M12014460-140154 7 3020ND28.9 30.9
1,2-Dibromoethane (EDB) ug/L 20 127 60-140136 7 3020ND25.3 27.2
1,2-Dichlorobenzene ug/L M12012960-140141 8 3020ND25.9 28.1
1,2-Dichloroethane ug/L 20 130 60-140137 5 3020ND26.0 27.4
1,2-Dichloropropane ug/L 20 130 60-140140 8 3020ND26.0 28.1
1,3,5-Trimethylbenzene ug/L M12013960-140150 7 30202.4 30.2 32.4
1,3-Dichlorobenzene ug/L 20 128 60-140139 8 3020ND25.6 27.8
1,3-Dichloropropane ug/L 20 123 60-140133 7 3020ND24.6 26.5
1,4-Dichlorobenzene ug/L 20 125 60-140135 8 3020ND25.0 27.0
2,2-Dichloropropane ug/L 20 129 60-140139 8 3020ND25.7 27.9
2-Chlorotoluene ug/L M12013360-140143 7 3020ND26.6 28.6
4-Chlorotoluene ug/L M12013260-140143 8 3020ND26.4 28.6
Benzene ug/L 20 122 60-140132 8 3020ND24.4 26.5
Bromobenzene ug/L 20 122 60-140134 10 3020ND24.4 26.8
Bromochloromethane ug/L 20 116 60-140127 8 3020ND23.3 25.3
Bromodichloromethane ug/L 20 123 60-140135 10 3020ND24.6 27.1
Bromoform ug/L 20 106 60-140115 8 3020ND21.3 23.1
Bromomethane ug/L M1204160-14041 1 3020ND8.2 8.1
Carbon tetrachloride ug/L 20 121 60-140135 11 3020ND24.2 27.0
Chlorobenzene ug/L 20 125 60-140134 7 3020ND25.0 26.7
Chloroethane ug/L 20 69 60-14070 1 3020ND13.8 13.9
Chloroform ug/L 20 126 60-140137 8 3020ND25.4 27.6
Chloromethane ug/L M1203260-14030 4 3020ND6.3 6.1
cis-1,2-Dichloroethene ug/L 20 131 60-140138 5 3020ND26.2 27.6
cis-1,3-Dichloropropene ug/L 20 126 60-140136 8 3020ND25.1 27.2
Dibromochloromethane ug/L 20 124 60-140134 8 3020ND24.8 26.8
Dibromomethane ug/L 20 119 60-140133 11 3020ND23.8 26.6
Dichlorodifluoromethane ug/L IH,M120760-1407 5 3020ND1.4 1.4
Diisopropyl ether ug/L 20 123 60-140131 7 3020ND24.6 26.2
Ethylbenzene ug/L 20 128 60-140137 7 30200.61 26.1 27.9
Hexachloro-1,3-butadiene ug/L M12014260-140157 10 3020ND28.4 31.3
Isopropylbenzene(Cumene)ug/L M12013660-140145 6 30201.1 28.2 30.1
m&p-Xylene ug/L 40 131 60-140139 6 30400.96J 53.4 56.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4038979MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92669953001
4038980
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 111 60-140117 6 3020ND22.2 23.4
Methylene Chloride ug/L 20 116 60-140121 4 3020ND23.1 24.1
n-Butylbenzene ug/L M12014660-140159 8 30201.3 30.5 33.1
n-Propylbenzene ug/L M12013260-140144 8 30200.86 27.3 29.6
Naphthalene ug/L M12016060-140172 5 302017.1 49.1 51.6
o-Xylene ug/L M12013160-140141 6 30203.1 29.4 31.2
sec-Butylbenzene ug/L M12014360-140155 8 3020ND28.5 30.9
Styrene ug/L M12013660-140143 5 3020ND27.2 28.6
tert-Butylbenzene ug/L 20 111 60-140120 8 3020ND22.2 24.0
Tetrachloroethene ug/L 20 120 60-140129 8 3020ND23.9 25.9
Toluene ug/L 20 120 60-140130 8 3020ND24.1 26.0
trans-1,2-Dichloroethene ug/L 20 125 60-140132 6 3020ND25.0 26.5
trans-1,3-Dichloropropene ug/L 20 126 60-140136 8 3020ND25.2 27.2
Trichloroethene ug/L 20 121 60-140132 9 3020ND24.3 26.5
Trichlorofluoromethane ug/L 20 76 60-14081 6 3020ND15.1 16.1
Vinyl chloride ug/L M1203460-14034 0 3020ND6.8 6.9
1,2-Dichloroethane-d4 (S) %107 70-130105
4-Bromofluorobenzene (S) %102 70-130101
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
779118
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92670120005, 92670120007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4041457
Associated Lab Samples:92670120005, 92670120007
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 06/08/23 07:180.31
1,1,1-Trichloroethane ug/L <0.33 0.50 06/08/23 07:180.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 06/08/23 07:180.22
1,1,2-Trichloroethane ug/L <0.32 0.50 06/08/23 07:180.32
1,1-Dichloroethane ug/L <0.37 0.50 06/08/23 07:180.37
1,1-Dichloroethene ug/L <0.35 0.50 06/08/23 07:180.35
1,1-Dichloropropene ug/L <0.43 0.50 06/08/23 07:180.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 06/08/23 07:180.81
1,2,3-Trichloropropane ug/L <0.26 0.50 06/08/23 07:180.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 06/08/23 07:180.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 06/08/23 07:180.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 06/08/23 07:180.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 06/08/23 07:180.27
1,2-Dichlorobenzene ug/L <0.34 0.50 06/08/23 07:180.34
1,2-Dichloroethane ug/L <0.32 0.50 06/08/23 07:180.32
1,2-Dichloropropane ug/L <0.36 0.50 06/08/23 07:180.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 06/08/23 07:180.33
1,3-Dichlorobenzene ug/L <0.34 0.50 06/08/23 07:180.34
1,3-Dichloropropane ug/L <0.28 0.50 06/08/23 07:180.28
1,4-Dichlorobenzene ug/L <0.33 0.50 06/08/23 07:180.33
2,2-Dichloropropane ug/L <0.39 0.50 06/08/23 07:180.39
2-Chlorotoluene ug/L <0.32 0.50 06/08/23 07:180.32
4-Chlorotoluene ug/L <0.32 0.50 06/08/23 07:180.32
Benzene ug/L <0.34 0.50 06/08/23 07:180.34
Bromobenzene ug/L <0.29 0.50 06/08/23 07:180.29
Bromochloromethane ug/L <0.47 0.50 06/08/23 07:180.47
Bromodichloromethane ug/L <0.31 0.50 06/08/23 07:180.31
Bromoform ug/L <0.34 0.50 06/08/23 07:180.34
Bromomethane ug/L <1.7 5.0 06/08/23 07:181.7
Carbon tetrachloride ug/L <0.33 0.50 06/08/23 07:180.33
Chlorobenzene ug/L <0.28 0.50 06/08/23 07:180.28
Chloroethane ug/L <0.65 1.0 06/08/23 07:180.65
Chloroform ug/L <0.43 0.50 06/08/23 07:180.43
Chloromethane ug/L <0.54 1.0 06/08/23 07:180.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 06/08/23 07:180.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 06/08/23 07:180.36
Dibromochloromethane ug/L <0.36 0.50 06/08/23 07:180.36
Dibromomethane ug/L <0.39 0.50 06/08/23 07:180.39
Dichlorodifluoromethane ug/L <0.35 0.50 IH06/08/23 07:180.35
Diisopropyl ether ug/L <0.31 0.50 06/08/23 07:180.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4041457
Associated Lab Samples:92670120005, 92670120007
Matrix: Water
AnalyzedMDL
Ethylbenzene ug/L <0.30 0.50 06/08/23 07:180.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 06/08/23 07:181.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 06/08/23 07:180.33
m&p-Xylene ug/L <0.71 1.0 06/08/23 07:180.71
Methyl-tert-butyl ether ug/L <0.42 0.50 06/08/23 07:180.42
Methylene Chloride ug/L <2.0 2.0 06/08/23 07:182.0
n-Butylbenzene ug/L <0.49 0.50 06/08/23 07:180.49
n-Propylbenzene ug/L <0.34 0.50 06/08/23 07:180.34
Naphthalene ug/L <0.64 2.0 06/08/23 07:180.64
o-Xylene ug/L <0.34 0.50 06/08/23 07:180.34
sec-Butylbenzene ug/L <0.40 0.50 06/08/23 07:180.40
Styrene ug/L <0.29 0.50 06/08/23 07:180.29
tert-Butylbenzene ug/L <0.32 0.50 06/08/23 07:180.32
Tetrachloroethene ug/L <0.29 0.50 06/08/23 07:180.29
Toluene ug/L <0.24 0.50 06/08/23 07:180.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 06/08/23 07:180.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 06/08/23 07:180.36
Trichloroethene ug/L <0.38 0.50 06/08/23 07:180.38
Trichlorofluoromethane ug/L <0.30 1.0 06/08/23 07:180.30
Vinyl chloride ug/L <0.39 1.0 06/08/23 07:180.39
1,2-Dichloroethane-d4 (S)%111 70-130 06/08/23 07:18
4-Bromofluorobenzene (S)%99 70-130 06/08/23 07:18
Toluene-d8 (S)%101 70-130 06/08/23 07:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4041458LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 17.720 88 60-140
1,1,1-Trichloroethane ug/L 18.520 93 60-140
1,1,2,2-Tetrachloroethane ug/L 18.720 94 60-140
1,1,2-Trichloroethane ug/L 18.320 91 60-140
1,1-Dichloroethane ug/L 19.120 96 60-140
1,1-Dichloroethene ug/L 20.420 102 60-140
1,1-Dichloropropene ug/L 20.020 100 60-140
1,2,3-Trichlorobenzene ug/L 17.820 89 60-140
1,2,3-Trichloropropane ug/L 18.420 92 60-140
1,2,4-Trichlorobenzene ug/L 16.920 84 60-140
1,2,4-Trimethylbenzene ug/L 18.420 92 60-140
1,2-Dibromo-3-chloropropane ug/L 17.320 86 60-140
1,2-Dibromoethane (EDB)ug/L 18.920 95 60-140
1,2-Dichlorobenzene ug/L 17.420 87 60-140
1,2-Dichloroethane ug/L 20.120 101 60-140
1,2-Dichloropropane ug/L 19.120 96 60-140
1,3,5-Trimethylbenzene ug/L 17.920 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4041458LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 17.120 86 60-140
1,3-Dichloropropane ug/L 18.320 91 60-140
1,4-Dichlorobenzene ug/L 16.920 85 60-140
2,2-Dichloropropane ug/L 16.020 80 60-140
2-Chlorotoluene ug/L 17.520 88 60-140
4-Chlorotoluene ug/L 18.120 90 60-140
Benzene ug/L 18.120 91 60-140
Bromobenzene ug/L 16.920 84 60-140
Bromochloromethane ug/L 17.720 89 60-140
Bromodichloromethane ug/L 17.520 88 60-140
Bromoform ug/L 15.920 80 60-140
Bromomethane ug/L 13.420 67 60-140
Carbon tetrachloride ug/L 17.620 88 60-140
Chlorobenzene ug/L 17.620 88 60-140
Chloroethane ug/L 18.920 95 60-140
Chloroform ug/L 18.420 92 60-140
Chloromethane ug/L 19.020 95 60-140
cis-1,2-Dichloroethene ug/L 19.320 97 60-140
cis-1,3-Dichloropropene ug/L 17.920 89 60-140
Dibromochloromethane ug/L 17.820 89 60-140
Dibromomethane ug/L 18.320 91 60-140
Dichlorodifluoromethane ug/L 24.5 IH20122 60-140
Diisopropyl ether ug/L 19.520 98 60-140
Ethylbenzene ug/L 17.620 88 60-140
Hexachloro-1,3-butadiene ug/L 15.320 76 60-140
Isopropylbenzene (Cumene)ug/L 18.020 90 60-140
m&p-Xylene ug/L 36.040 90 60-140
Methyl-tert-butyl ether ug/L 18.420 92 60-140
Methylene Chloride ug/L 19.620 98 60-140
n-Butylbenzene ug/L 17.320 87 60-140
n-Propylbenzene ug/L 17.320 87 60-140
Naphthalene ug/L 19.420 97 60-140
o-Xylene ug/L 18.020 90 60-140
sec-Butylbenzene ug/L 17.420 87 60-140
Styrene ug/L 18.620 93 60-140
tert-Butylbenzene ug/L 14.420 72 60-140
Tetrachloroethene ug/L 15.820 79 60-140
Toluene ug/L 17.320 86 60-140
trans-1,2-Dichloroethene ug/L 19.520 98 60-140
trans-1,3-Dichloropropene ug/L 17.520 88 60-140
Trichloroethene ug/L 17.120 86 60-140
Trichlorofluoromethane ug/L 18.520 92 60-140
Vinyl chloride ug/L 17.120 86 60-140
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4041459MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92670120007
4041460
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 136 60-140121 11 3020<0.31 27.2 24.2
1,1,1-Trichloroethane ug/L 20 131 60-140135 3 3020<0.33 26.1 26.9
1,1,2,2-Tetrachloroethane ug/L 20 136 60-140121 11 3020<0.22 27.1 24.3
1,1,2-Trichloroethane ug/L 20 137 60-140124 10 3020<0.32 27.4 24.7
1,1-Dichloroethane ug/L 20 123 60-140132 7 3020<0.37 24.6 26.5
1,1-Dichloroethene ug/L M1,R1209960-140145 37 3020<0.35 19.9 28.9
1,1-Dichloropropene ug/L M12013660-140144 6 3020<0.43 27.2 28.9
1,2,3-Trichlorobenzene ug/L M12014260-140123 14 3020<0.81 28.4 24.6
1,2,3-Trichloropropane ug/L 20 127 60-140113 11 3020<0.26 25.3 22.7
1,2,4-Trichlorobenzene ug/L M12014260-140121 16 3020<0.64 28.5 24.3
1,2,4-Trimethylbenzene ug/L M12014660-140129 13 3020<0.50 29.2 25.7
1,2-Dibromo-3-
chloropropane ug/L 20 139 60-140122 13 3020<0.34 27.9 24.5
1,2-Dibromoethane (EDB) ug/L 20 139 60-140127 9 3020<0.27 27.7 25.3
1,2-Dichlorobenzene ug/L 20 135 60-140120 12 3020<0.34 27.0 24.0
1,2-Dichloroethane ug/L 20 135 60-140131 3 3020<0.32 26.9 26.2
1,2-Dichloropropane ug/L 20 135 60-140130 4 3020<0.36 27.0 26.1
1,3,5-Trimethylbenzene ug/L M12014260-140127 11 3020<0.33 28.3 25.3
1,3-Dichlorobenzene ug/L 20 135 60-140120 12 3020<0.34 27.0 24.0
1,3-Dichloropropane ug/L 20 131 60-140121 8 3020<0.28 26.3 24.2
1,4-Dichlorobenzene ug/L 20 132 60-140117 12 3020<0.33 26.3 23.5
2,2-Dichloropropane ug/L 20 129 60-140137 5 3020<0.39 25.9 27.3
2-Chlorotoluene ug/L 20 138 60-140123 12 3020<0.32 27.6 24.6
4-Chlorotoluene ug/L 20 140 60-140125 12 3020<0.32 28.1 25.0
Benzene ug/L 20 125 60-140128 2 3020<0.34 24.9 25.5
Bromobenzene ug/L 20 133 60-140119 11 3020<0.29 26.5 23.8
Bromochloromethane ug/L 20 124 60-140124 1 3020<0.47 24.8 24.7
Bromodichloromethane ug/L 20 132 60-140123 7 3020<0.31 26.3 24.6
Bromoform ug/L 20 115 60-140106 8 3020<0.34 22.9 21.2
Bromomethane ug/L M1,R1203260-14062 64 3020<1.7 6.4 12.5
Carbon tetrachloride ug/L 20 121 60-140130 7 3020<0.33 24.3 26.0
Chlorobenzene ug/L 20 133 60-140121 9 3020<0.28 26.6 24.3
Chloroethane ug/L R1206060-140125 71 3020<0.65 12.0 25.0
Chloroform ug/L 20 130 60-140122 6 3020<0.43 26.1 24.5
Chloromethane ug/L M1,R1202760-140117 126 3020<0.54 5.3 23.3
cis-1,2-Dichloroethene ug/L 20 128 60-140134 4 3020<0.38 25.7 26.8
cis-1,3-Dichloropropene ug/L 20 134 60-140127 5 3020<0.36 26.8 25.5
Dibromochloromethane ug/L 20 135 60-140122 10 3020<0.36 26.9 24.5
Dibromomethane ug/L 20 133 60-140129 2 3020<0.39 26.5 25.9
Dichlorodifluoromethane ug/L IH,M1,
R120660-140171 187 3020<0.35 1.1 34.3
Diisopropyl ether ug/L 20 127 60-140128 1 3020<0.31 25.5 25.6
Ethylbenzene ug/L 20 132 60-140122 8 3020<0.30 26.4 24.5
Hexachloro-1,3-butadiene ug/L 20 137 60-140115 17 3020<1.5 27.4 23.1
Isopropylbenzene
(Cumene)ug/L M12014260-140128 10 3020<0.33 28.3 25.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4041459MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92670120007
4041460
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 136 60-140125 8 3040<0.71 54.3 50.0
Methyl-tert-butyl ether ug/L 20 118 60-140123 4 3020<0.42 23.6 24.5
Methylene Chloride ug/L 20 111 60-140121 8 3020<2.0 22.3 24.2
n-Butylbenzene ug/L M12014960-140129 14 3020<0.49 29.7 25.9
n-Propylbenzene ug/L 20 138 60-140123 12 3020<0.34 27.7 24.6
Naphthalene ug/L M12016960-140139 19 3020<0.64 33.8 27.9
o-Xylene ug/L 20 135 60-140123 9 3020<0.34 27.0 24.6
sec-Butylbenzene ug/L M12014260-140127 11 3020<0.40 28.5 25.4
Styrene ug/L M12014260-140128 10 3020<0.29 28.4 25.6
tert-Butylbenzene ug/L 20 115 60-140102 12 3020<0.32 23.1 20.4
Tetrachloroethene ug/L 20 125 60-140118 6 3020<0.29 25.1 23.6
Toluene ug/L 20 126 60-140120 5 3020<0.24 25.3 24.1
trans-1,2-Dichloroethene ug/L 20 121 60-140138 13 3020<0.40 24.3 27.6
trans-1,3-Dichloropropene ug/L 20 137 60-140128 7 3020<0.36 27.4 25.5
Trichloroethene ug/L 20 127 60-140126 1 3020<0.38 25.3 25.2
Trichlorofluoromethane ug/L R1207060-140133 62 3020<0.30 13.9 26.6
Vinyl chloride ug/L M1,R1202860-140118 123 3020<0.39 5.7 23.6
1,2-Dichloroethane-d4 (S) %107 70-130108
4-Bromofluorobenzene (S) %100 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92670120
FORMER NORRIS LUV STATION
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92670120001 778650MW1SM 6200B
92670120002 778336MW2SM 6200B
92670120003 778336MW3SM 6200B
92670120004 778336MW8SM 6200B
92670120005 779118MW9SM 6200B
92670120006 778336MW10SM 6200B
92670120007 779118MW11SM 6200B
92670120008 778336DUPLICATESM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/06/2023 09:29 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 36
Page 35 of 36
Page 36 of 36