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WithersRavenel
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115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. F‐1479
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MONITORING REPORT
Former Sam Puckett Property
UST # RA‐4570
Incident # 26305
10 Puckett Trail
Epsom, Franklin County, North Carolina
NCDEQ Contract # N70522‐C
WithersRavenel Project No. 23‐0307‐DY
Prepared for:
State of North Carolina
Department of Environmental Quality
Division of Waste Management
Underground Storage Tank Section
Federal & State Lead Program
1646 Mail Service Center
Raleigh, North Carolina 27699‐1646
Prepared by:
WithersRavenel
115 MacKenan Drive
Cary, North Carolina 27511
North Carolina Firm License No. C‐0832
August 11, 2023
WithersRavenel
Our People. Your Success.
Former Sam Puckett Property WR Project # 23‐0307‐CY
Monitoring Report August 2023
ii
August 11, 2023
State of North Carolina
Department of Environmental Quality
Federal & State Lead Program
Division of Waste Management‐Underground Storage Tank Section
1646 Mail Service Center
Raleigh, North Carolina 27699‐1646
Attn: Mr. Mark Petermann
Re: Monitoring Report
Former Sam Puckett Property
10 Puckett Trail
Epsom, Franklin County, North Carolina
Groundwater Incident Number: 26305
UST Number: RA‐4570
NCDEQ Contract # N70522‐C
WR Project Number: 23‐0307‐DY
Mr. Petermann:
WithersRavenel, Inc. (WR) has completed this Monitoring Report to document monitoring well
and supply well sampling activities completed at the site in association with our proposal,
numbered TA‐01, for the above referenced facility, approved by the Federal & State Lead Program
on May 17, 2023. The enclosed report summarizes results of the recently completed monitoring
activities.
WR appreciates the opportunity to be of service to the Federal & State Lead Program. Should you
have any questions regarding the attached, please contact Matthew James at (919) 469‐3340.
Cordially,
WithersRavenel
Kevin B. Buchanan G. Matthew James, PG
Staff Environmental Scientist III Senior Geologist
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Monitoring Report August 2023
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TABLE OF CONTENTS
SECTION A: SITE INFORMATION ..................................................................................................................... 1
SECTION B. EXECUTIVE SUMMARY ................................................................................................................ 3
SECTION C. SITE HISTORY AND CHARACTERIZATION ........................................................................... 6
SECTION D. MONITORING WELL SAMPLING –JUNE 2023 ................................................................ 14
SECTION E. SUPPLY WELL SAMPLING –JUNE 2023 .............................................................................. 16
SECTION F. CONCLUSIONS AND RECOMMENDATIONS .................................................................... 17
FIGURES
Figure 1 General Location Map
Figure 2 Site Map
Figure 3 Groundwater Hydraulic Gradient Map (ft) – June 2023
Figure 4 Groundwater Analytical Results (µg/L) – June 2023
Figure 5 Receptor Map
TABLES
Table B‐1 Site History: UST/AST System & Other Release Information
Table B‐4 Summary of Groundwater Analytical Results
Table B‐5A Public & Private Water Supply Well Information
Table B‐7 Monitoring & Remediation Well Construction Information
Table B‐9 Current & Historical Groundwater Elevations & Free Product Thickness’
APPENDICES
Appendix A Laboratory Analytical Report and Chain‐of‐Custody
Appendix B Field Notes and Photographic Record
Appendix C General Standard Operating Procedures
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Monitoring Report August 2023
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SECTION A: SITE INFORMATION
1. Site Identification
Date of Report: August 11, 2023
Facility I.D.: Unassigned
Incident No.: 26305
Site Risk: High
Site Rank: H655A
Land Use Category: Residential
Site Name: Former Sam Puckett Property
Site Location: 10 Puckett Trail
Nearest City/Town: Epsom
County: Franklin
Description of Geographical Data Point: Center of Former UST Area
Location Method: Google Earth
Latitude: 36.243643°
Longitude: ‐78.326044°
2. Contact Information
Responsible Party: Unknown (Orphan USTs)
Property Owner Roy Wayne Elks
Address: PO Box 2450
Henderson, NC 27537
Phone: 919‐210‐8752
Consultant/Contractor: WithersRavenel
Address: 115 MacKenan Drive, Cary, NC 27511
Phone: 919‐469‐3340
Analytical Laboratory: Waypoint Analytical, LLC
State Certification Number: ENV402
Address: 449 Springbrook Rd., Charlotte, NC 28217
Phone: 704‐529‐6364
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3.ReleaseInformation
DateDiscovered:March1993
EstimatedQuantityofRelease:Unknown
CauseofRelease:CompromisedUSTorDeliverySystem
SourceofRelease:USTorDeliverySystem
TypeofMaterialReleased:Gasoline
CriteriaUsedtoClassifyRisk:Groundwater2Lviolations,ProximitytoWater
SupplyWells,SupplyWellImpact(s)
Sizes&ContentsofUSTSystem(s)fromwhich
ReleaseOccurred:
One500Ŋgallonandone1,000Ŋgallonpetroleum
USTs
4.InformationaboutMonitoringReport
Date(s)ofAssessment/MonitoringEvent(s):June8,2023
5.Certification
I,G.MatthewJames,aLicensedGeologistfor
WithersRavenel,docertifythattheinformation
containedinthisreportiscorrectandaccurateto
thebestofmyknowledge.
WithersRavenel,islicensedtopractice
geology/engineeringinNorthCarolina.
ThecertificationnumbersareCŊ293(Geology)and
FŊ1479(Engineering).
08-11-2023
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Monitoring Report August 2023
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SECTION B. EXECUTIVE SUMMARY
1. Summary of Activities Associated with Current TA
WR completed a site‐wide groundwater monitoring event and obtained samples from select
supply wells. Activities associated with this TA were completed June 8 2023. While tasked with
collection of groundwater samples from monitoring wells MW‐1 and MW‐2, WR personnel were
unable to locate the wells. Therefore, MW‐1 and MW‐2 were not sampled. Monitoring well MW‐
6 has been destroyed, and was, therefore, not sampled.
2. Soil, Groundwater and LNAPL Assessment Information
Soils
No soil sampling was performed at the facility in association with this TA. Two USTs were
removed from the location on December 16, 2019, included one 1,000‐gallon UST and one 500‐
gallon UST, both assumed to have been used for the storage of petroleum fuels. These tanks were
wholly or in part located within the northern margin of the Right‐of‐Way (R/W) of NC Highway
39. Analytical results for soil samples submitted for laboratory analysis of TPH as gasoline range
organics (GRO) and diesel range organics (DRO) showed GRO and/or DRO at concentrations in
excess of the laboratory method detection limit (MDL) in each of the soil samples collected in
association with tank closures. Levels of TPH GRO and DRO in each sample exceeded the current
NCDEQ Action Levels for TPH. Soil samples obtained from the sidewalls of the excavation
analyzed by RBCA methods showed numerous volatile organic compounds (VOCs) and aliphatic
and/or aromatic hydrocarbons in each of the four samples submitted for testing by EPA Method
8260 and the MADEP‐VPH Method. Concentrations of numerous compounds and hydrocarbon
chains exceeded their respective Soil to Water MSCCs.
Groundwater
Laboratory results for groundwater samples obtained from site monitoring wells during June 2023
did not show impact by targeted petroleum compounds at concentrations exceeding the
laboratory method detection limit (MDL) for SM6200B in any well sampled excepting MW‐1. Data
for MW‐1 showed several compounds present, however only naphthalene was reported at a
concentration exceeding the 2L Standard.
Based on the June 2023 groundwater sampling event performed at the location, the extent of
surficial groundwater contamination has been nearly defined, with minor data gaps to the west
and southeast of the source area. Contaminants appear to extend hydraulically down‐gradient of
the source area to the northeast and appear stable. Based on groundwater elevation
measurements obtained during June 2023, groundwater flow was shown to divergent to the
southeast and northeast and averaged 2.1‐ft shallower than those measured in June 2022.
LNAPL/Free Product
No LNAPL/Free Product has been identified in association with the release at the site, to date.
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3. Receptor Information
WR performed a receptor survey update at the site on April 15, 2015, which included identification
of supply wells located within 1,000 feet of the release area as well as research into the availability
of municipal or county water supplies. Potable water is provided to the site and surrounding
properties exclusively through private supply wells, and no public water supply is available to the
site or surrounding properties through municipal or county facilities. WR identified seven supply
wells located within a 500‐foot radius of the site. Of these wells, two (WSW‐4 and WSW‐9) are
currently inactive. Supply well WSW‐1 was reported by previous consultants to have been
abandoned; however, the current property owner (Mr. Roy Elks) stated to WR personnel that the
well had never, to his knowledge, existed. An additional twelve supply wells were identified
between 500 and 1,000 feet of the source location on the site. Of these wells, eleven are believed
to be active potable supply wells, and the remaining well (WSW‐17A) is reported by the property
owner to be a “dry” well.
Supply wells WSW‐10 and WSW‐13, formerly having been identified as being located within
1,000 feet of the release area, were found to actually be located greater than 1,000 feet from the
source location. Previous consultants had based their search radius on the center of the site
property, rather than the center of the suspected source area, which would have these wells
located within the 1,000‐foot radius. As many as twenty‐two additional supply wells (including
WSW‐10 and WSW‐13) are located within 1,000 and 1,500 feet of the source area. WR oversaw
the installation of a replacement well for WSW‐3 during September 2020. Following the
replacement well installation (WSW‐3A), WR oversaw the abandonment of WSW‐3 on February
3, 2021. A point of entry (POE) system had been installed on supply well WSW‐4, but the POE
system on the well was reportedly disconnected by the owner several years ago. Research of the
site and vicinity through the NC Source Water Assessment Program (SWAP) indicates that the site
does not lie within a Wellhead Protection Area, and the site is not located within the Coastal Plain
Physiographic Province of North Carolina.
Analytical results for supply well samples obtained from WSW‐2, WSW‐6 and WSW‐8 in June
2023 did not show the presence of targeted compounds at levels above the MDLs for SM6200B
or EPA‐504.1. Data for the sample collected from WSW‐3A and WSW‐4 showed 1,2‐DCE and
EDB present at concentrations exceeding the 2L Standard but beneath the US EPA Maximum
Contaminant Level (MCL) for the compounds. WR does not believe the presence of these
chemicals in WSW‐3A and WSW‐4 to relate to the petroleum release at the Former Sam Puckett
Property, as these compounds have not historically been detected in monitoring wells MW‐2,
MW‐2D, MW‐3R MW‐4, MW‐4D, MW‐5 or MW‐9, each located between the source location
and the supply wells.
4. Remediation Activities
Two USTs were removed from the location on December 16, 2019, included one 1,000‐gallon
UST and one 500‐gallon UST, both assumed to have been used for the storage of petroleum fuels.
No remedial actions beyond UST closures have been completed at the location, to date.
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5. Recommendations
Based on the results of assessment and monitoring activities conducted at the site in association
with this TA and what appears as a decreasing trend in contaminants in MW‐1, WR recommends
the following:
Continued performance of routine groundwater and supply well monitoring at the site.
If adequate funding is available based on site risk, consider injection of chemical amendment
such as persulfate or BOS200 activated carbon to reduce contaminant concentrations in
groundwater.
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SECTION C. SITE HISTORY AND CHARACTERIZATION
WR has completed a groundwater monitoring well and supply well sampling event for the
referenced site in association with TA‐01 at the facility. The following information summarizes
the site history and characterization.
1. UST Information
1.1 Former USTs
The UST systems removed from the location on December 16, 2019, included one 1,000‐gallon
UST and one 500‐gallon UST, both assumed to have been used for the storage of petroleum fuels.
These tanks were wholly or in part located within the northern margin of the R/W of NC Highway
39. No information relating to the last uses of the tanks is available. The UST systems were orphan
tanks situated on property formerly owned by Mr. Sam Puckett, who obtained ownership of the
property in October 1992 and never operated the UST systems. The tanks were reportedly in
place when the property was owned by Mr. Wallace A. Duke (deceased) & Ms. Dorothy P. Duke,
pre‐dating Mr. Puckett’s ownership in 1992. Table B‐1 summarizes known information regarding
the former UST systems.
The location of the site imposed on the USGS Topographic Map for the vicinity is included as
Figure 1, while site improvements, including former USTs and monitoring well locations are
depicted on Figure 2.
2. Description of Release/General Assessment History
The following summary of the assessment history is based on WR’s review of historical files for
the subject incident:
Based on an internal memorandum at the North Carolina Department of Environmental Quality or
“NCDEQ” [formerly the Department of Environment and Natural Resources (NCDENR)] in
association with an application for State Lead Site acceptance, residents at the nearby Stephens
Rental Property (Incident# 9174) complained about the quality of water from an on‐site water
supply well. The groundwater monitoring wells at the site are apparently associated with the
Stephen’s Rental Property Site (TF‐9174). The Stephens Rental Property is located at 8105 NC
Highway 39 South, adjacent to the Sam Puckett Property site. The following summary of the
assessment history is based on WR’s review of historical files for the subject incident:
Stephens Rental Property (Incident # TF‐9174)
According to an Underground Storage Tank Closure Report prepared by ATEC Associates and
dated December 1, 1994, one 250‐gallon heating oil UST was removed from the Stephens
Rental Property on October 19, 1994. Free product was reportedly observed in the soils
immediately below the former UST. Approximately 25 tons of petroleum contaminated soils
were excavated and removed from the UST excavation. The laboratory analytical results for
confirmatory soil samples collected at the time of UST closure indicated that total petroleum
hydrocarbons (TPH) diesel range organics (DRO) were detected in concentrations between
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2,880 parts per million (ppm) and 23,400 ppm. Groundwater was reportedly not encountered
during the UST excavation.
In addition to removing the UST, ATEC also collected water samples from three nearby water
supply wells (two wells at the Puckett Residence, and one at the Fire Station). The laboratory
analytical results for these samples indicated that no petroleum‐related constituents were
detected above the laboratory MDLs. ATEC also sampled the well associated with the
Stephens Rental Property, which was equipped with a carbon adsorption system. Water
samples were collected from both influent and effluent sides of the system. The laboratory
analytical results for the water samples indicated that several VOCs were detected in
concentrations below the 2L Standards in the water entering the treatment system, and no
VOCs were detected in the effluent sample from the system
According to the Report of Environmental Services prepared by Mid‐Atlantic Associates and
dated December 3, 1996, groundwater monitoring wells MW‐1 through MW‐3 were installed
in October 1996. Monitoring well MW‐1 was installed on the property at 10 Puckett Trail to
the northwest and MW‐2 was installed at 20 Puckett Trail to the northwest of the site.
Monitoring well MW‐3 was installed at the site near the former UST excavation.
According to the Groundwater Monitoring Event Report prepared by Schnabel Engineering and
dated June 24, 2003, monitoring wells MW‐1 through MW‐3 were sampled on May 14, 2003.
The laboratory analytical results for the groundwater samples indicated that several VOCs
were detected in concentrations exceeding their respective 2L Standards at location MW‐1.
In addition, four soil borings were advanced near the former UST excavation on the Stephens
Rental Property. The laboratory analytical results for the soil samples indicated that no
petroleum‐related constituents were detected at concentrations above the MDLs.
Sam Puckett Property (Incident # TF‐26305)
In July 2003, Mr. Sam Puckett, who is the owner of the Sam Puckett Property at 10 Puckett
Trail, received a Notice of Regulatory Requirements (NORR) from the NCDENR due to the
detections of VOCs exceeding 2L Standards in monitoring well MW‐1, which was installed on
his property in association with the Stephens Rental site. In an Affidavit signed by Mr. Puckett
on January 20, 2004, Mr. Puckett indicated that he purchased the property in 1992 and did
not operate or even know about any USTs associated with the property. The remains of an old
service station are located on his property.
According to a Monitor Well Installation and Water Supply Well and Groundwater Sampling Report
prepared by Schnabel Engineering, eight soil borings were installed to depths of between 7
and 19 feet below ground surface at locations on the Sam Puckett Property and on adjacent
parcels. Soil samples collected from the soil borings were screened in the field for the presence
of VOCs. The soil borings that exhibited the highest VOC measurements (SB‐1 through SB‐3,
and SB‐8) were subsequently converted into monitoring wells (MW‐4 through MW‐7). Soil
samples from the borings were reportedly not collected for laboratory analysis. The entire
monitoring well network (MW‐1, MW‐2, and MW‐4 through MW‐7) was sampled on March
9, 2004. Monitoring well MW‐3 was not located during that sampling event. The laboratory
analytical results for the groundwater samples indicated that VOCs were detected in
concentrations exceeding their respective 2L Standards in the samples from monitoring wells
MW‐1 and MW‐6. The concentration of benzene exceeded the 2L Standard in the sample
monitoring well MW‐7. In addition, water samples were collected from water supply wells
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WSW‐1 through WSW‐6. The laboratory analytical results for the water supply well samples
indicated that 1,2‐dichloroethane was detected in concentrations exceeding the 2L Standard
in the samples from WSW‐3 and WSW‐4, and the benzene concentration in the sample from
WSW‐3 exceeded the 2L Standard.
The groundwater monitoring network (MW‐1, MW‐2, and MW‐3 through MW‐7) was
sampled sporadically between March 2004 and October 2012. Monitoring well MW‐3 had not
been located since prior to March 2004. The laboratory analytical results for groundwater
samples collected during this period indicated several VOCs present in the samples from MW‐
1 and MW‐6 in concentrations exceeding their respective 2L Standards. In addition, water
supply wells WSW‐1 through WSW‐6 were also sampled sporadically between March 2004
and May 2008. Water supply wells WSW‐3 and WSW‐4 reportedly have POE systems
connected to the wells. The laboratory results for the water supply well samples indicated the
presence of several VOCs in the influent samples for the POE systems installed on WSW‐3
and WSW‐4. The effluent samples from the POE systems did not have any detections of
petroleum‐related constituents exceeding the MDLs. In addition, no petroleum‐related
constituents were detected in the other water supply wells sampled.
A receptor survey was completed by Crawford Environmental Services as part of a
groundwater monitoring event in December 2012. According to the receptor survey, municipal
water is not available to the area. Nineteen water supply wells were identified within 1,000
feet of the site (WSW‐1 through WSW‐19). Water supply well WSW‐1 has been abandoned,
and supply wells WSW‐2 and WSW‐9 are both inactive wells. The remaining sixteen wells are
actively used as sources for drinking water and other domestic uses.
WR conducted a groundwater and supply well sampling event during June 2014. Analytical
results for groundwater samples were consistent with previous sampling events, and generally
showed a decreasing trend of compounds in affected wells. Several compounds were reported
at locations MW‐1 and MW‐6 at levels above their respective 2L Standards, and EDB was
reported in the sample from MW‐6 at a level exceeding the Gross Contaminant Level (GCL) for
the compound. Results of a GPR survey on the site identified the potential presence of two
previously unidentified USTs beneath the property. WR advanced four hand augured soil
borings over the location of one of the potential USTs, and encountered refusal at a depth of
approximately 22 inches in each boring at the location of a solid metal obstruction.
WR performed a receptor survey update, supervised performance of a GPR survey and air
knifed soil boring installations, gauged, purged and sampled site monitoring wells and purged
and sampled WSW‐2, WSW‐3 (Pre‐ and Post‐POE) and WSW‐8. Results of the receptor
survey verified a lack of available potable water from a private or municipal service, and
confirmed the presence of six active and one inactive (WSW‐9) supply wells within 500 feet
of the source area on the site, and an additional twelve active supply wells between 500 and
1,000 feet of the source area. Results of a GPR survey and subsequent air‐knifed soil borings
confirmed the presence of two steel USTs, located within the NCDOT R/W of NC Highway
39, approximately 10 feet northwest of monitoring well MW‐1. Analytical results for soil
samples retrieved from borings SB‐1 through SB‐4, indicated the presence of one or more
compounds in each of the samples at levels exceeding their respective Soil to Water MSCCs.
Aliphatic and aromatic hydrocarbons were reported in samples obtained from borings SB‐3
and SB‐4 at levels exceeding their respective Residential MSCCs. Based on the analytical
results for these four samples, the lateral extent of soil contamination surrounding these USTs
has not been defined to levels equivalent to the Soil to Water MSCCs.
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Analytical results for groundwater samples obtained from site monitoring wells indicated one
or more compounds present at levels exceeding their respective 2L Standards in samples
obtained from monitoring wells MW‐1 and MW‐6. In addition, 1,2‐dibromoethane (EDB) was
reported in the sample from MW‐6 at a level exceeding the GCL for the compound. Analytical
results for groundwater samples retrieved from wells MW‐2, MW‐4, MW‐5 and MW‐7 did
not indicate detectable concentrations of any petroleum‐related compounds by SM6200B or
EPA‐504.1 (EDB). Analytical results for supply well samples obtained on April 15, 2015
indicated the presence of EDB in the samples from WSW‐2, WSW‐3 (Pre‐POE), WSW‐3 (Post‐
POE) and WSW‐8. Levels of the compound reported in WSW‐3 (Pre‐POE) and WSW‐3 (Post‐
POE) were in excess of the 2L Standard for EDB. 1,2‐Dichloroethane was also detected in the
sample from WSW‐3 (Pre‐POE) at a level exceeding the 2L Standard for the compound.
In association with TA‐04 for the site under a previous contract, WR attempted to obtain an
access agreement for the Donald Wilby property to allow for the installation of additional
monitoring wells on his property and submitted a R/W Encroachment agreement to the NC
DOT to permit the installation of monitoring wells and removal of the USTs in the RW of NC
Highway 39. WR was further tasked with evaluating water supply wells located downgradient
of the site source area, to include wells WSW‐1, WSW‐2, WSW‐3, WSW‐4, WSW‐8 and
WSW‐9. Although WR submitted an access agreement to Mr. Wilby through Certified US
Mail, no response to the request for access has been received, to date. Following review,
NCDOT issued encroachment contract E53‐35‐15‐026 on July 28, 2015. This encroachment
includes provisions for installing two monitoring wells in the RW as well as the excavation and
removal of the USTs adjacent to MW‐1. WR was unable to locate supply well WSW‐1, which
was abandoned according to the Schnabel Engineering Monitoring Well Installation and Water
Supply Well and Groundwater Sampling Report dated April 2004. Despite having attempted to
contact the owner of WSW‐4 both through phone calls and a visit by WR personnel to the
location, WR was unable to gain access and obtain complete information about the
construction of WSW‐4. WR completed additional inquiry into the water supply well by
phoning the Franklin County Health Department‐Division of Environmental Health, who
informed WR that no records of wells, or well construction records, are available prior to 2008.
Supply wells WSW‐3 and WSW‐9 were found to have shallow screens, which likely intercept
shallow groundwater of the surficial aquifer.
In July 2016, WR gauged, purged and sampled monitoring wells MW‐1, MW‐2, and MW‐4
through MW‐7, and purged and sampled supply wells WSW‐2, WSW‐3 (Pre‐ and Post‐POE),
WSW‐6 and WSW‐8. Analytical results for groundwater samples obtained from site
monitoring wells on July 21, 2016 indicated one or more petroleum‐related compounds in
samples obtained from wells MW‐1 and MW‐6. Several compounds detected in each of the
samples were reported at concentrations exceeding their respective 2L Standards. EDB was
reported in the samples from MW‐1 and MW‐6 at levels above the 2L standard for the
compound. The concentration of EDB in MW‐6 was in excess of the GCL for the compound.
Analytical results for samples from the remaining wells did not indicate the presence of
compounds at concentrations exceeding the MDLs for SM6200B or EPA‐504.1. Analytical
results for the samples obtained from water supply wells on July 21, 2016 indicated the
presence of EDB in WSW‐3 (Pre‐POE) at a concentration in excess of the 2L Standard and the
US EPA MCL for drinking water. Analytical results for the Post‐POE sample from WSW‐3 and
samples from WSW‐2, WSW‐6 and WSW‐8 did not indicate the presence of petroleum‐
related compounds at concentrations above the MDLs for EPA Method SM6200B or EPA‐
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504.1. The analytical results for WSW‐3 (Post‐POE) confirm the continued efficiency of the
POE system in stripping contaminants from the water produced by the well.
In August 2017, WR supervised the installation of three Type II, 2‐inch diameter monitoring
wells (MW‐3R, MW‐8 and MW‐9), two additional “deep profile” Type II, 2‐inch diameter
monitoring wells (MW‐2D and MW‐4D), gauged, purged and sampled monitoring wells MW‐
1 through MW‐9, and purged and sampled supply wells WSW‐2, WSW‐3 (Pre‐ and Post‐POE),
WSW‐4, WSW‐6 and WSW‐8. Analytical results for groundwater samples obtained from site
monitoring wells on August 9, 2017 indicated the presence of one or more petroleum‐related
compounds in the samples obtained from MW‐1 and MW‐2D. One or more compounds in
the sample from MW‐1 were reported at concentrations in excess of their respective 2L
Standards. Historical data has shown the greatest levels of contaminants in samples
originating from MW‐6; however, this well could not be sampled during August 2017 as it was
“dry”. Analytical results for samples obtained from monitoring wells MW‐2, MW‐4, MW‐4D,
MW‐5, MW‐7, MW‐8 and MW‐9 did not show the presence of VOCs at levels exceeding the
laboratory MDL for SM6200B. Analytical results for supply well samples obtained from WSW‐
2, WSW‐6 and WSW‐8 did not show the presence of petroleum‐related compounds according
to SM6200B. Analytical results for the Pre‐POE sample from WSW‐3 showed EDB present
at a concentration exceeding the 2L Standard and US EPA MCL for the compound. Data for
this sample also showed t‐amyl alcohol (TAA) at an estimated concentration of 5.33 µg/L. WR
believes the reported presence of this compound to be suspect, and likely an artifact relating
to elevated reported detection limits for the sample. The two samples in which TAA was
reported, MW‐1 and WSW‐3 (pre‐POE), were also the only two wells in which benzene was
reported, both having elevated laboratory reported detection limits. Analytical results for the
Post‐POE sample for the well did not show any petroleum‐related compounds present above
the laboratory MDL. Results for the sample obtained from WSW‐4 showed EDB present at a
concentration above both the 2L Standard and US EPA MCL for the compound.
During November 2018, WR obtained a supply well sample from WSW‐3 in conjunction with
ProAct‐Carbonair’s scheduled POE system maintenance at the location. This sample was
collected to verify results for samples obtained from the well by WR and ProAct‐Carbonair.
Data for the sample showed concentrations of benzene and EDB in excess of their respective
2L Standards, while the level of EDB also exceeded the US EPA MCL for the compound.
Analytical results for groundwater samples obtained from site monitoring wells on January 17,
2019 indicated one or more petroleum‐related compounds in samples obtained from wells
MW‐1 and MW‐6. Several compounds detected in these samples were reported at
concentrations exceeding their respective 2L Standards. Analytical results for samples from
the remaining wells did not indicate the presence of compounds at concentrations exceeding
the MDLs for SM6200B or EPA‐504.1. Analytical results for the samples obtained from water
supply wells on January 17, 2019 indicated the presence of EDB in WSW‐3 (Pre‐POE) at a
concentration in excess of the 2L Standard and the US EPA MCL for drinking water. Results
for the Post‐POE sample from WSW‐3 showed the continued presence of EDB at a level above
the 2L Standard for the compound (but below the US EPA MCL).
WR completed the closure of two UST systems at the location during December 2019. The
UST systems removed from the location included one 1,000‐gallon UST and one 500‐gallon
UST, both assumed to have been used for the storage of petroleum fuels. Based upon the
concentrations of TPH as GRO and DRO detected in each of the soil samples obtained during
completion of closure activities, a release was verified in association with the UST systems.
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Soil samples obtained from the sidewalls of this excavation analyzed by Risk‐Based Corrective
Action (RBCA) methods showed several VOCs and aliphatic and/or aromatic hydrocarbons in
each of the four samples submitted for testing by EPA‐8260 and the MADEP‐VPH Method.
Levels of numerous compounds and hydrocarbon chains in each sample exceeded their
respective Soil to Water MSCCs.
WR completed a site‐wide groundwater sampling event at the location during January 2020.
Analytical results for groundwater samples obtained from site monitoring wells on January 28,
2020 indicated one or more petroleum‐related compounds in samples obtained from wells
MW‐1 and MW‐6. Several compounds detected in these samples were reported at
concentrations exceeding their respective 2L Standards. Data for EPA‐504.1 analysis showed
EDB in wells MW‐1 and MW‐6 at levels above the 2L Standard for the compound, while the
concentration detected in MW‐6 exceeded the GCL. Analytical results for samples from the
remaining wells did not indicate the presence of compounds at concentrations exceeding the
MDL for SM6200B or EPA‐504.1.
WR oversaw the installation of supply well WSW‐3A on the Cherie McBeth property located
to the east of the source area. This well was installed as a replacement for WSW‐3, which had
been contaminated by the release and was the location of an NCDEQ funded POE system.
WR verified the connection of WSW‐3A to the McBeth property on October 2, 2020.
WR Purged and sampled WSW‐3 on five occasions following connection to the property.
Samples were collected from the well on October 7, October 30, November 13, and December
14, 2020, as well as January 12, 2021. Results for samples from the well showed acetone in
the sample from October 7, 2020 at a level beneath the 2L Standard. Data for samples from
October 30, November 13, and December 14, 2020, as well as January 12, 2021 showed 1,2‐
DCE present at levels above the 2L Standard. Toluene was also reported at a level beneath
the 2L Standard in the sample collected on November 13, 2020.
WR oversaw the abandonment of supply well WSW‐3 located on the Cherie McBeth property
on February 3, 2021.
WR completed a site‐wide groundwater sampling event at the location during March 2021.
Analytical results for groundwater samples obtained from site monitoring wells on March 1‐2,
2021 analyzed by SM6200B indicated several petroleum‐related compounds in samples
obtained from well MW‐1 at concentrations exceeding their respective 2L Standards. Results
for the remaining wells, the field blank sample and laboratory trip blank did not show the
presence of targeted compounds at levels exceeding the laboratory MDL. Data for analysis by
EPA‐504.1 indicated EDB in samples obtained from well MW‐1 at a concentration exceeding
the 2L Standard for the compound. Results for the remaining wells did not show the presence
of EDB at levels exceeding the laboratory MDL. Analytical results for samples obtained from
supply wells on March 2, 2021 analyzed by SM6200B indicated 1,2‐DCE in samples obtained
from well WSW‐3A at a concentration exceeding the 2L Standard for the compound. Results
for the remaining wells (WSW‐2, WSW‐6 and WSW‐8) did not show the presence of targeted
compounds at levels exceeding the laboratory MDL. Analytical results for samples obtained
from supply wells on March 2, 2021 analyzed by EPA Method 504.1 indicated EDB in the
samples obtained from well WSW‐3A at a concentration exceeding the 2L Standard for the
compound. Results for the remaining wells (WSW‐2, WSW‐6 and WSW‐8) did not show the
presence of EDB at levels exceeding the laboratory MDL.
WR completed a site‐wide groundwater sampling event at the location during June 2022.
Analytical results for groundwater samples obtained from site monitoring wells on June 1,
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2022 analyzed by SM6200B indicated several petroleum‐related compounds in samples
obtained from well MW‐1 at concentrations exceeding their respective 2L Standards. Results
for the remaining wells, the field blank sample and laboratory trip blank did not show the
presence of targeted compounds at levels exceeding the laboratory MDL. Analytical results
for groundwater samples analyzed by EPA Method 504.1 indicated EDB in the sample
obtained from well MW‐1 at a concentration exceeding the 2L Standard for the compound.
Results for the remaining wells did not show the presence of EDB at levels exceeding the
laboratory MDL.
3. Brief Description of Site Characteristics
The property is located in Epsom, Franklin County, North Carolina (Figure 1). The facility address
is 10 Puckett Trail, and the location is currently vacant (Figure 2). The Franklin County Parcel ID
No. for the property is 036554. A one‐story building, which was reportedly a former gas
station/convenience store was located near the southwestern corner of the property. The
structure was razed sometime between May 2012 and April 2015. A single‐story residential home
is located to the northeast of the former structure on the parcel. This residence is serviced by
supply well WSW‐8. Two USTs were located within the NCDOT R/W of NC Highway 39, near
the southwestern wall of the former structure location. These tanks were permanently closed in
December 2019. Surface cover at the former UST locations include scattered areas of asphalt,
while surface cover on remaining portions of the site include grass and/or gravel.
4. Information on Receptors/Potential Receptors
WR performed a receptor survey update at the site on April 15, 2015, which included identification
of supply wells located within 1,000 feet of the release area as well as research into the availability
of municipal or county water supplies. Results of the update include the following:
Potable water is provided to the site and surrounding properties exclusively through private
supply wells.
No publicly available water supply is available to the site or surrounding properties through
municipal or county facilities.
WR identified seven supply wells located within a 500‐foot radius of the site. Of these wells,
two (WSW‐4 and WSW‐9) are currently inactive. Supply well WSW‐1 was reported by
previous consultants to have been abandoned; however, the current property owner Mr. Roy
Elks stated to WR personnel that the well had never, to his knowledge, existed. An additional
twelve supply wells were identified between 500 and 1,000 feet of the source location on the
site. Of these wells, eleven are believed to be active potable supply wells, and the remaining
well (WSW‐17A) is reported by the property owner to be a “dry” well.
Supply wells WSW‐10 and WSW‐13, formerly having been identified as being located within
1,000 feet of the release area, were found to actually be located greater than 1,000 feet from
the source location. Previous consultants had based their search radius on the center of the
site property, rather than the center of the suspected source area, which would have these
wells located within the 1,000‐foot radius.
As many as twenty‐two additional supply wells (including WSW‐10 and WSW‐13) are located
within 1,000 and 1,500 feet of the source area.
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A POE system had been in use at the former location of WSW‐3. This POE system was
decommissioned when the well was replaced with WSW‐3A and abandoned.
A POE system had been installed on supply well WSW‐4, but the POE system on the well was
reportedly disconnected by the owner several years ago. WR was granted access to sample
supply well WSW‐4 in August 2017 and did not observe a POE system installed on the well.
Research of the site and vicinity through the NC Source Water Assessment Program (SWAP)
indicates that the site does not lie within a Wellhead Protection Area.
The site is not located within the Coastal Plain Physiographic Province of North Carolina.
The nearest locations of public assembly are the John Mills Masonic Lodge located
approximately 350 feet northwest of the source area, and the New Beginnings Ministries
Church, located approximately 700 feet southeast of the source area. These properties are
the locations of supply wells WSW‐7 and WSW‐6, respectively.
The 1979 USGS 7.5 Minute Series Topographic Map for Ingleside, NC which includes the site
location shows an un‐named pond located approximately 500 feet southeast of the site. This
un‐named pond has been filled and the New Beginnings Ministries Church was built at the
former location of the pond.
Drainage north of the site moves towards Flatrock Creek, while drainage south of the site
moves towards Devil’s Cradle Creek. Both water bodies drain to the Tar‐Pamlico River Basin.
Supply well information is included on Table B‐5. Locations of supply wells within 1,000 feet of
the source area are depicted on Figure 5.
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SECTION D. MONITORING WELL SAMPLING –JUNE 2023
WR conducted a site‐wide groundwater monitoring event at the in association with TA‐01 under
NCDEQ Contract #N70522‐C. While tasked with collection of groundwater samples from
monitoring wells MW‐2, however, WR personnel were unable to locate the well. Therefore, MW‐
2 was not sampled. Monitoring well MW‐6 has been destroyed, and was, therefore, not sampled.
WR also purged and sampled supply wells WSW‐2, WSW‐3A, WSW‐4, WSW‐6 and WSW‐8 in
association with this TA. These activities are described below.
WR mobilized to the site on June 8, 2023 for the purposes of completing a site‐wide groundwater
sampling event. WR personnel were unable locate MW‐1 on June 8, 2023 and returned to the
location on June 29, 2023 to locate and sample the well.
1 Groundwater Elevations
Prior to the purging and sampling of site monitoring wells, WR personnel opened and gauged each
well with an electronic water level indicator to determine the depth to groundwater. In the
performance of these activities and eventual purging of the wells, free product was not measured
in any of the monitoring wells on the site. The depth to groundwater measurements as recorded
in the monitoring wells on June 8, 2023 ranged from 8.12 feet below the top of well casing (ft‐
BTOC) in monitoring well MW‐3R to 14.69‐ft‐BTOC in monitoring well MW‐8 Based on
groundwater elevation measurements obtained on June 8, 2023 groundwater averaged 2.1‐ft
shallower than those measured in June 2022. Based on groundwater elevation measurements
obtained in June 2023, groundwater flow currently appears to flow divergently to the southeast
and northeast as shown on Figure 3. As depicted on Figure 3, gradient at the location may be
affected by the removal of the USTs in December 2019 and emplacement of non‐native fill
materials in the excavated area. Groundwater elevation measurements for this event are
presented in Table B‐7. Historical groundwater elevations are included in Table B‐9.
2 Groundwater Sampling and Analytical Results
Monitoring Well Sampling
WR personnel obtained groundwater samples from MW‐1, MW‐2D, MW‐4, MW‐4D, MW‐5,
MW‐7, MW‐8 and MW‐9 following gauging and purging. As previously stated, MW‐1 could not
be located on June 8, 2023 but was later found and sampled on June 29, 2023. Each well was
purged and sampled with a separate polyethylene bailer, as described in the procedures outlined
in Appendix C. After completion of an appropriate purge, groundwater samples were obtained
with the bailer(s) and decanted directly into laboratory prepared sample containers holding
appropriate preservative(s) as required. Groundwater samples were submitted to Waypoint
Analytical, LLC (Waypoint) for analysis by SM6200B and EPA‐504.1 (EDB). Field notes associated
with the performance of assessment activities at the site are included in Appendix B.
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Laboratory Results
SM6200B
Analytical results for groundwater samples obtained from site monitoring wells on June 8 and 29,
2023 analyzed by SM6200B indicated several petroleum‐related compounds in samples obtained
from well MW‐1. Naphthalene was reported in the sample at a concentration exceeding the 2L
Standard. Results for the remaining wells did not show the presence of targeted compounds at
levels exceeding the laboratory MDL.
EPA‐504.1 (EDB)
Analytical results for groundwater samples obtained from site monitoring wells on June 8, 2023
analyzed by EPA Method 504.1 did not show the presence of EDB in any samples submitted for
analysis.
Groundwater analytical results are summarized in Table B‐4 and shown on Figure 4. The
laboratory analytical report and chain‐of‐custody record associated with groundwater samples
obtained from site monitoring wells during June 2023 are included in Appendix A.
Based solely on total BTEX concentrations for June 2023 compared to those from June 2022,
groundwater analytical results for samples showed a 48.5% decrease in MW‐1. WR believes
these continued reductions in groundwater contaminants within the well to relate to the removal
of the USTs from the location in December 2019, which included the removal of a small volume
of saturated source area soils. WR believes that the removal of severely contaminated soils and
emplacement of fill material has essentially created a more permeable pathway for groundwater
flow towards MW‐1, allowing for “washing” of contaminants through vadose zone soils. In
addition, based on groundwater elevation measurements obtained on June 8, 2023 groundwater
averaged 2.1‐ft shallower than those measured in June 2022.
The extent of surficial groundwater contamination has been nearly defined, with minor data gaps
to the west and southeast of the source area. No assessment of water quality conditions with the
underlying bedrock aquifer has been performed at the site to date; however, analytical data for
“deep” Type II wells MW‐2D and MW‐4D did not show impact by petroleum compounds, with
the exception of 1,2,4‐trimethylbenzene (reported in the sample obtained from MW‐2D in August
2017 at a concentration beneath the 2L Standard), inferring that contaminants do not appear to
be migrating to deeper water‐bearing zones to the northeast of the source area (towards WSW‐
8).
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SECTION E. SUPPLY WELL SAMPLING –JUNE 2023
1 Supply Well Sampling and Analytical Results
Supply Well Sampling
WR personnel obtained supply well samples from WSW‐2, WSW‐3A, WSW‐4, WSW‐6 and
WSW‐8 on June 8, 2023 following purging. Each well was purged by allowing the pump to run
continuously for a minimum of ten minutes, after which a sample was decanted directly from the
sample point into laboratory prepared sample containers holding appropriate preservative as
required. Supply well samples were submitted to Waypoint for analysis by SM6200B and EPA‐
504.1 (EDB).
Laboratory Results
SM6200B
Analytical results for groundwater samples obtained from supply wells on June 8, 2023 analyzed
by SM6200B indicated 1,2‐ Dichloroethane and EDB in samples obtained from wells WSW‐3A
and WSW‐4 at concentrations exceeding the 2L Standards for the compounds. Results for the
remaining wells (WSW‐2, WSW‐6 and WSW‐8) did not show the presence of targeted compounds
at levels exceeding the laboratory MDL.
EPA‐504.1 (EDB)
Analytical results for groundwater samples obtained from supply wells on June 8, 2023 analyzed
by EPA Method 504.1 indicated EDB in the samples obtained from wells WSW‐3A and WSW‐4
at concentrations exceeding the 2L Standard for the compound. Results for the remaining wells
(WSW‐2, WSW‐6 and WSW‐8) did not show the presence of EDB at levels exceeding the
laboratory MDL.
WR does not believe the presence of these chemicals in WSW‐3A and WSW‐4 to relate to the
petroleum release at the Former Sam Puckett Property, as these compounds have not historically been detected in monitoring wells MW‐2, MW‐2D, MW‐3R, MW‐4, MW‐4D, MW‐5
or MW‐9, each located between the source location and the supply wells.
The laboratory analytical report and chain‐of‐custody record associated with these samples are
included in Appendix A. Data are also shown on Figure 5.
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SECTION F. CONCLUSIONS AND RECOMMENDATIONS
This report documents the results of field activities conducted at the site for TA‐01, which included
the gauging, purging and sampling of monitoring wells MW‐1, MW‐2D, MW‐3R, MW‐4, MW‐4D,
MW‐5, MW‐5D, MW‐7, MW‐8 and MW‐9, and collection of supply well samples from WSW‐2,
WSW‐3A, WSW‐4, WSW‐6 and WSW‐8. Conclusions based on observations, analytical results
and research relating to the release at the site combined with historical information include the
following:
Seven supply wells are located within 500‐ft of the site. Of these wells, five are active and
two are inactive:
An additional twelve supply wells were identified between 500 and 1,000 feet of the source
location on the site. Of these wells, eleven are believed to be active potable supply wells, and
the remaining well (WSW‐17A) is reported by the property owner to be a dry well.
Two USTs were removed from the NCDOT R/W adjacent to the southwestern boundary of
the site in December 2019.
Analytical results for groundwater samples obtained from the site monitoring wells indicated
the presence of several petroleum‐related compounds in the samples from MW‐1.
Naphthalene was reported in the sample from MW‐1 at a concentration exceeding the 2L
Standard.
Based solely on total BTEX concentrations for June 2023 compared to those from June 2022,
groundwater analytical results for samples showed a decrease of 48.5% in MW‐1. WR believes
these continued reductions in groundwater contaminants within the well to relate to the
removal of the USTs from the location in December 2019, which included the removal of a
small volume of saturated source area soils. WR believes that the removal of severely
contaminated soils and emplacement of fill material has essentially created a more permeable
pathway for groundwater flow towards MW‐1, allowing for “washing” of contaminants
through vadose zone soils. In addition, based on groundwater elevation measurements
obtained on June 8, 2023, groundwater averaged 2.1‐ft shallower than those measured on
June 1, 2022.
Analytical results for groundwater samples obtained from the remaining monitoring wells in
June 2023 did not indicate the presence of targeted compounds at concentrations exceeding
the MDLs for SM6200B or EPA‐504.1.
The extent of surficial groundwater contamination has been nearly defined, with minor data
gaps to the west and southeast of the source area.
No free product was identified at the site during the June 2023 sampling event, nor has free
product been identified during previous monitoring events.
Based on groundwater elevation measurements obtained in June 2023, groundwater flow
currently appears to be divergent to the southeast and northeast. Gradient at the location may
be affected by the removal of the USTs in December 2019 and emplacement of non‐native fill
materials in the excavated area, in addition to groundwater averaging greater than 2.1‐ft
shallower than that measured in June 2022.
Analytical results for the samples obtained from water supply wells in June 2023 indicated the
presence of 1,2‐DCE and EDB in WSW‐3A and WSW‐4 at concentrations in excess of their
respective 2L Standards but beneath US EPA MCLs.
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Results for the remaining wells (WSW‐2, WSW‐6 and WSW‐8) did not show the presence of
targeted compounds at levels exceeding the laboratory MDL for SM6200B or EDB by EPA‐
504.1.
Based on the results of assessment and monitoring activities conducted at the site in association
with this TA and what appears as a decreasing trend in contaminants in MW‐1, WR recommends
the following:
Continued performance of routine groundwater and supply well monitoring at the site.
If adequate funding is available based on site risk, consider injection of chemical amendment
such as persulfate or BOS200 activated carbon to reduce contaminant concentrations in
groundwater.
WR appreciates the opportunity to be of service in the completion of these assessment activities.
Should you have questions, comments, or require additional information, please contact WR at
your earliest convenience.
Cordially,
WithersRavenel
Kevin B. Buchanan G. Matthew James, PG
Staff Environmental Scientist III Senior Geologist
FIGURES
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SUBJECT SITE
±1.46 ACRES
SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
FORMER SAM PUCKETT PROPERTYTF#26305
10 PUCKETT TRAILEPSOM, FRANKLIN, COUNTY, NC
GENERAL LOCATION MAP
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Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: F-1479 | www.withersravenel.com
1"=500 '
GRAPHIC SCALE
1 inch = 500 ft.
0 500250 1000
MW-5MW-4MW-2FORMER 1-STORYCONVENIENCE STORE(DEMOLISHED)MW-3MW-7MW-1FORMER USTLOCATIONSMW-6MW-3RMW-9MW-8MW-4DMW-2D(DESTROYED)(DESTROYED)KBB
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SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
FORMER SAM PUCKETT PROPERTY10 PUCKETT TRAIL
EPSOM, FRANKLIN, COUNTY, NC
SITE MAPWithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: F-1479 | www.withersravenel.com
1"=40 'GRAPHIC SCALE1 inch = 40 ft.0402080NOTE: 1.) 2021 AERIAL OBTAINED FROM NC ONE MAP.
MW-5MW-4MW-2FORMER 1-STORYCONVENIENCE STORE(DEMOLISHED)MW-3MW-7MW-1FORMER USTLOCATIONSMW-6MW-3RMW-9MW-8MW-4DMW-2D(DESTROYED)(DESTROYED)(92.71)(91.96)(NM)(92.63)(92.64)(91.94)(91.89)(NM)(93.71)(92.04)93929392KBB
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SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
FORMER SAM PUCKETT PROPERTY10 PUCKETT TRAIL
EPSOM, FRANKLIN, COUNTY, NC
GROUNDWATER HYDRAULIC
GRADIENT MAP (ft)JUNE 2022
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1"=30 '(92.71)GRAPHIC SCALE1 inch = 30 ft.030156093
MW-5MW-4MW-2FORMER 1-STORYCONVENIENCE STORE(DEMOLISHED)MW-3MW-7MW-1FORMER USTLOCATIONSMW-6MW-3RMW-9MW-8MW-4DMW-2D(DESTROYED)(DESTROYED)KBB
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SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
FORMER SAM PUCKETT PROPERTY10 PUCKETT TRAIL
EPSOM, FRANKLIN, COUNTY, NC
GROUNDWATER ANALYTICAL RESULTSJUNE 2022
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1"=40 'GRAPHIC SCALE1 inch = 40 ft.0402080
KBB
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SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
FORMER SAM PUCKETT PROPERTY10 PUCKETT TRAIL
EPSOM, FRANKLIN, COUNTY, NC
RECEPTOR MAPWITH JUNE 2022SUPPLY WELL ANALYTICALRESULTS SHOWN
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1"=300 'GRAPHIC SCALE1 inch = 300 ft.0300150600LEGENDWATER SUPPLY WELL (ACTIVE, POTABLE)WATER SUPPLY WELL (INACTIVE)WATER SUPPLY WELL (ABANDONED)"DRY" SUPPLY WELL
TABLES
UST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUSTWas release associated with UST System? (Y/N)1 Petroleum Unknown 1000Single‐Wall Steel4 X 10.5 Single‐Wall Steel Unknown REMOVED 12/16/19 YES2 Petroleum Unknown 550Single‐Wall Steel4 X 6 Single‐Wall Steel Unknown REMOVED 12/16/19 YESAST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofASTWas release associated with AST System? (Y/N)N/A N/A N/A N/A N/A N/A N/A N/A N/A N/AIncidentNumberMaterialReleasedDateofRelease26305 Petroleum UnknownNotes:1)Incident Number: 26305WR is unaware of any ASTs now or formerly associated with the subject site.Table B‐1Site History: UST/AST System & Other Release InformationFORMER SAM PUCKETT PROPERTYAdjacent property owners complained about the quality of water from an onsite water supply well. Upon removal of USTs on December 16, 2019, both tanks were found to be in poor condition, with numerous large diameter (up to 2‐inch) holes through tankwalls. A fiber optic cable trunk was found to have been installed through the lower sidewalls of the tanks. Penetration of the tanks during installation of the fiber optic trunk (reportedly in the 1990's) resulted in the creation of 2‐inch diameter holes in each of the USTs. 10 Puckett TrailEpsom, Franklin County, North CarolinaDescription of ReleasePage 1 of 1
CalculatedAcetoneBenzenen‐Butylbenzenesec‐Butylbenzenetert‐Butylbenzene1,2‐Dibromoethane(EDB)1,2‐Dichloroethane1,2‐Dichloropropane1,1‐DichloropropeneDi‐isopropyl etherEthylbenzeneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Naphthalenen‐PropylbenzeneStyreneToluene1,2,3‐Trimethylbenzene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal XyleneEthyl‐Tert‐Butyl‐EtherT‐Amyl AlcoholTert‐Butyl Formate1,2‐Dibromoethane(EDB)1,2‐Dibromo‐3‐Chloropropane67‐64‐171‐43‐2 104‐51‐8 135‐98‐898‐06‐6 106‐93‐4 107‐06‐278‐87‐5 563‐58‐6 108‐20‐3 100‐41‐498‐82‐899‐87‐678‐93‐3 108‐10‐191‐20‐3 103‐65‐1 100‐42‐5 108‐88‐3 526‐73‐895‐63‐6 108‐67‐8 NA 637‐92‐375‐85‐4 762‐75‐4 106‐93‐496‐12‐811/8/20075/14/2008NR2470ND NR NR84.914ND ND2100 108NR ND578 230NR20100NR1760 491 10960NR NR NR NA NA6/27/2014<500430 13<10 <10 <10 <10 <10 <10 <101000 60 22<100 <100300 160<101900NR1300 360 5500NR NR NR NA NA 04/16/2015<25077<5 <5 <5 <5 <5 <5 <5 <5180 9.9<5 <50 <5053 22<5250NR240 69 1050NR NR NR3.4<0.027/21/2016<501.63 1.67<1 <1 <1 <1 <1 <1 <143.93.911.22<10 <1026 11.3<18.34 30 125 38.6 300NR NR NR0.0666NR8/9/2017NR127 6.79 4.61NR <1 <1 <1 <1 <1395 33.1 8.02 4.93 145 82.3 991NR582 178 2196<19.26<201.53<0.021/17/2019<0.31 3.7 0.54<0.5 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 34 2.9<0.50 <0.24 <0.078 7.2 6.4<0.047 3.7NR57 18 220NANANA0.039NA1/28/202011 350 7 5.7 0.54 8.7<0.066 5.7<0.051 <0.050 1300 51 5.1<0.24 4.2 240 110 10 10000 870 280<0.060 7200NA NA NA7.5<0.0028 3/2/2021<100520<5.00 <5.00 <5.00 NR <5.006.62<5.00 <5.00962 46.1<5.00 <50.0 <10.0241 90.2 12.8 19300NR778 223 7600NR NR NR49.5NR6/1/202237.1 20.8<0.5000.845<2.00 <0.500 <0.500 <0.500 <0.500 <0.500129 7.88 1.5 5.98 10.6 36.1 13.9<0.500213 172 61.5<5.00813NA NA NA0.282NR6/29/2023<100 <5.005.31<5.00 <20.0 <5.00 <5.00 <5.00 <5.00 <5.00107 11.8<5.00 <50.0 <10.073.4 28.4<5.0043.1NR255 83.4 455NA NA NA NA NA11/8/2007NR ND ND NR NR ND ND NR ND ND ND ND NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA5/14/2008NR ND ND NR NR ND ND NR ND ND ND ND NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA12/15/2010NR ND ND NR NR ND ND NR ND ND ND ND NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA6/26/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR <1.0 <1.0 <2.0 NR NR NR NA NA 04/15/2015<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 NR <1 <1 <2 NR NR NR <0.01 <0.027/21/2016<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <1 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0025 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0209NR6/8/20238/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <10.422<1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <1 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0025 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0208NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0207NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0201 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0201 NA8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.5 J <0.054 <0.089 <0.24 <0.078 <1 <0.087 <0.047 <0.5 <0.054 <0.076 <0.060 <1.5 NA NA NA <0.0025 <0.0026 3/1/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0203 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0203 NA11/8/2007NR ND ND NR NR ND ND NR ND ND ND NR NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA5/14/2008NR ND ND NR NR ND ND NR ND ND ND NR NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA12/15/2010NR ND ND NR NR ND ND NR ND ND ND NR NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA10/11/20126/26/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR <1.0 <1.0 <2.0 NR NR NR NA NA 04/16/2015<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 NR <1 <1 <2 NR NR NR <0.01 <0.027/21/2016<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <1 <0.087 <0.047 <0.5 <0.054 <0.076 <0.060 <1.5 NA NA NA <0.0024 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0206NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0205 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0205 NA8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0025 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0208NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0203 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0203 NA6000 1 70 70 70 0.02 0.4 0.6 0.6 70 600 70 25 4000 100 6 70 70 600 NL 400 400 500 47 40 40 0.02 0.046,000,000 5,000 5,900 8,800 14,750 50 380 600 510 70,000 80,000 30,500 11,700 4,000,000 100,000 15,500 26,100 70,000 260,000 NL 28,500 24,100 50,000 47,000 40,000 40,000 50 NLNotes:1)2)3)4)NL= Not ListedND= Compound Not Detected Above Laboratory Detection Limits (Detection Limit Not Provided By Previous Consultant).ResultNR= Compound Not ReportedResultNA= Compound Not Analyzed for by Laboratory.Result Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L (Comprehensive Tables for Corrective Action Guidelines, September 2022). GCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for Groundwater (Comprehensive Tables for Corrective Action Guidelines, September 2022).= Result Exceeds Laboratory Detection Limits= Result Exceeds 2L Standard= Result Exceeds GCL ValueNC 2L Standard GCLs for Groundwater All results provided in ug/L (micrograms per liter) or parts per billionTABLE B‐4AEpsom, Franklin County, North CarolinaIncident Number: 26305SUMMARY OF GROUNDWATER ANALYTICAL RESULTS10 Puckett TrailMW‐4DMW‐4504.16200B ‐ Volatile Organic CompoundsFORMER SAM PUCKETT PROPERTYDateCollectedNot SampledAnalytical Method6200B ‐ Volatile Organic CompoundsMW‐1SampleIDNot Sampled ‐ Well DryMW‐3RMW‐2DMW‐2Not SampledPage 1 of 3
CalculatedAcetoneBenzenen‐Butylbenzenesec‐Butylbenzenetert‐Butylbenzene1,2‐Dibromoethane(EDB)1,2‐Dichloroethane1,2‐Dichloropropane1,1‐DichloropropeneDi‐isopropyl etherEthylbenzeneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Naphthalenen‐PropylbenzeneStyreneToluene1,2,3‐Trimethylbenzene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal XyleneEthyl‐Tert‐Butyl‐EtherT‐Amyl AlcoholTert‐Butyl Formate1,2‐Dibromoethane(EDB)1,2‐Dibromo‐3‐Chloropropane67‐64‐171‐43‐2 104‐51‐8 135‐98‐898‐06‐6 106‐93‐4 107‐06‐278‐87‐5 563‐58‐6 108‐20‐3 100‐41‐498‐82‐899‐87‐678‐93‐3 108‐10‐191‐20‐3 103‐65‐1 100‐42‐5 108‐88‐3 526‐73‐895‐63‐6 108‐67‐8 NA 637‐92‐375‐85‐4 762‐75‐4 106‐93‐496‐12‐8TABLE B‐4AEpsom, Franklin County, North CarolinaIncident Number: 26305SUMMARY OF GROUNDWATER ANALYTICAL RESULTS10 Puckett Trail504.16200B ‐ Volatile Organic CompoundsFORMER SAM PUCKETT PROPERTYDateCollectedAnalytical Method6200B ‐ Volatile Organic CompoundsSampleID11/8/2007NR ND ND NR NR ND ND NR ND ND ND ND NR NR NR ND ND NR ND NR ND ND ND NR NR NR NA NA5/14/2008NR ND ND NR NR ND ND NR ND ND ND ND NR NR NR ND ND NR ND NR ND ND ND NR NR NR NA NA12/15/2010NR ND ND NR NR ND ND NR ND ND ND ND NR NR NR ND ND NR ND NR ND ND ND NR NR NR NA NA10/11/2012NR ND ND NR NR ND ND NR ND ND ND ND NR NR NR ND ND NR1.5NR0.66ND2.35NR NR NR NA NA6/26/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR <1.0 <1.0 <2.0 NR NR NR NA NA 04/16/2015<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 NR <1 <1 <2 NR NR NR <0.01 <0.027/21/2016<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0025 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0211NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0210 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0210 NA11/8/2007NR2810 43.3NR NR16643.7ND19.2 1940 122NR ND364 314NR13500NR2800 785 14630NR NR NR NA NA5/14/2008NR601ND NR NR44.2 20.5ND ND444 58.3NR ND592 142NR2160NR2070 586 4750NR NR NR NA NA6/27/2014<5001200 18 10<106021<10 <10 <10410 32 34<100 <100270<10 <102100NR1400 410 4000NR NR NR NA NA 04/16/2015<50001600<100 <100 <100150<100 <100 <100 <100380<100 <100 <1000 <1000 <500 <100 <1003900NR1100 280 4300NR NR NR950.0727/21/2016<10001330<20 <20 <2010326.7<1 <20335 29.8<20 <200 <200382 76.2<202060 630 1900 586 4940NR NR NR89.8NR1/17/2019<3.1 1400<0.76 6.7<0.88 4010<1.1 <0.51 <5.0650 32<0.89 <2.4 <0.78 310 73 6.4 7400NR1700 530 6500NA NA NA31NA1/28/2020<1000360<7.6 <7.6 <8.8 <50 <6.6 <11 <5.1 <5.0 92<5.4 <8.9 <500 <7.8 <100 <8.7 <4.7 480 240 130<6.0 1300NA NA NA55<0.0026 6/1/202211/8/20075/14/2008NR ND ND NR NR ND ND ND ND ND ND NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA6/26/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR31.21.6NR NR NR NA NA 04/16/2015<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 NR <1 <1 <2 NR NR NR <0.01 <0.027/21/2016<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.5 <0.5 <0.076 <0.060 <1.5 NA NA NA <0.0025 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0204 NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0219 NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0204 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0204 NA8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0025 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0205 NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <<0.0211 NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0207 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0207 NA8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0024 <0.0025 3/1/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0207 NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0210 NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0204 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0204 NA6000 1 70 70 70 0.02 0.4 0.6 0.6 70 600 70 25 4000 100 6 70 70 600 NL 400 400 500 47 40 40 0.02 0.046,000,000 5,000 5,900 8,800 14,750 50 380 600 510 70,000 80,000 30,500 11,700 4,000,000 100,000 15,500 26,100 70,000 260,000 NL 28,500 24,100 50,000 47,000 40,000 40,000 50 NLNotes:1)2)3)4)NL= Not ListedND= Compound Not Detected Above Laboratory Detection Limits (Detection Limit Not Provided By Previous Consultant).ResultNR= Compound Not ReportedResultNA= Compound Not Analyzed for by Laboratory.ResultMW‐9MW‐8MW‐7NC 2L Standard Well DestroyedMW‐6GCLs for Groundwater All results provided in ug/L (micrograms per liter) or parts per billion NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L (Comprehensive Tables for Corrective Action Guidelines, September 2022). GCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for Groundwater (Comprehensive Tables for Corrective Action Guidelines, September 2022).= Result Exceeds Laboratory Detection LimitsMW‐5= Result Exceeds 2L Standard= Result Exceeds GCL ValueNot Sampled Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. Page 2 of 3
CalculatedAcetoneBenzenen‐Butylbenzenesec‐Butylbenzenetert‐Butylbenzene1,2‐Dibromoethane(EDB)1,2‐Dichloroethane1,2‐Dichloropropane1,1‐DichloropropeneDi‐isopropyl etherEthylbenzeneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Naphthalenen‐PropylbenzeneStyreneToluene1,2,3‐Trimethylbenzene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal XyleneEthyl‐Tert‐Butyl‐EtherT‐Amyl AlcoholTert‐Butyl Formate1,2‐Dibromoethane(EDB)1,2‐Dibromo‐3‐Chloropropane67‐64‐171‐43‐2 104‐51‐8 135‐98‐898‐06‐6 106‐93‐4 107‐06‐278‐87‐5 563‐58‐6 108‐20‐3 100‐41‐498‐82‐899‐87‐678‐93‐3 108‐10‐191‐20‐3 103‐65‐1 100‐42‐5 108‐88‐3 526‐73‐895‐63‐6 108‐67‐8 NA 637‐92‐375‐85‐4 762‐75‐4 106‐93‐496‐12‐8TABLE B‐4AEpsom, Franklin County, North CarolinaIncident Number: 26305SUMMARY OF GROUNDWATER ANALYTICAL RESULTS10 Puckett Trail504.16200B ‐ Volatile Organic CompoundsFORMER SAM PUCKETT PROPERTYDateCollectedAnalytical Method6200B ‐ Volatile Organic CompoundsSampleID12/15/2010NR ND ND NR NR ND ND ND ND ND NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA10/11/2012NR ND ND NR NR ND ND ND ND ND NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA6/27/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR <1.0 <1.0 <2.0 NR NR NR NA NA 04/15/2015<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 NR <1 <1 <2 NR NR NR0.012<0.027/21/2016<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0024 <0.0025 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0208NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0204 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0204 NA10/7/202057<0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 5.2<0.078 <0.19 <0.087 <0.047 <0.5 NR <0.054 <0.076 <1.5 NA NA NA NANA10/30/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 0.64<0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NR NR NR NRNR11/13/2020<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 0.65<0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 4<0.054 <0.076 <0.060 <0.15 NR NR NR NRNR12/14/2020<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 0.54<0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NR NR NR NRNR1/12/2021<10 <0.50 <0.50 <0.50 <0.50 <0.500.66<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <5.0 <1.0 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <5.0 <1.5 NR NR NR NRNR3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR0.756<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR0.0244NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.5000.903<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA0.0319NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.000.0262 0.737<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA0.0262NA11/8/2007NR ND ND NR NR ND2.3NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA5/14/2008NR ND ND NR NR ND1.2NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA10/11/2012NR ND ND NR NR ND2NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA7/21/201611/8/2007NR ND ND NR NR ND ND NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA5/14/2008NR ND ND NR NR ND1.2NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA12/15/2010NR ND ND NR NR ND2.8NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA6/1/2011NR ND ND NR NR ND2.4NR ND ND ND ND NR NR ND ND ND NR ND NR ND ND ND NR NR NR NA NA10/11/20128/12/2014<50 <1.0 <1.0 <1.0 <1.0 <1.01.5<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR <1.0 <1.0 <2.0 NR NR NR NA NA7/21/20168/9/2017NR <1 <1 <1 <1 <11.78<1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <200.0538NA6/8/2023<10.0 <0.500 <0.500 <0.500 <2.000.0455 1.67<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA0.0455NAWSW‐512/15/2010NR ND ND NR NR ND ND NR NR ND ND ND NR NR ND ND NR ND <1 ND ND ND NR NR NR NA NA7/21/2016<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206 NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0201 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0201 NA12/15/2010NR ND ND NR NR ND ND NR NR ND ND ND NR NR ND ND ND NR ND ND ND NR NR NR NA NA6/27/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <5.0 <1.0 <1.0 <5.0 NR <1.0 <1.0 <2.0 NR NR NR NA NA 04/15/2015<50 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 NR <1 <1 <2 NR NR NR0.015<0.027/21/2016<50 <1 <1 <1 <1 <1 <1 NR <1 <1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <3 NR NR NR <0.01 NR8/9/2017NR <1 <1 <1 <1 <1 <1 <10.43<1 <1 <1 <1 <10 <10 <5 <1 <1 <5 <1 <1 <1 <2 <1 <50 <20 <0.01 <0.021/17/2019<0.31 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.11 <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <0.19 <0.087 <0.047 <0.044 NR <0.054 <0.076 <0.15 NA NA NA <0.025 NA1/28/2020<10 <0.048 <0.076 <0.076 <0.088 <0.051 <0.066 <0.5 J <0.051 <0.050 <0.061 <0.054 <0.089 <0.24 <0.078 <1 <0.087 <0.047 <0.044 <0.054 <0.076 <0.060 <0.15 NA NA NA <0.0024 <0.0026 3/2/2021<10.0 <0.500 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NR NR NR <0.0206NR6/1/2022<10.0 <0.500 <0.500 <0.500 <2.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <0.500 NA NA NA <0.0207NR6/8/2023<10.0 <0.500 <0.500 <0.500 <2.00 <0.0205 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 <1.00 <1.00 <0.500 <0.500 <0.500 NR <0.500 <0.500 <0.500 NA NA NA <0.0205 NAWSW‐912/15/2010NR ND ND NR <1 <1 <1 <1 ND ND ND NR NR NR ND ND NR ND NR ND ND ND NR NR NR NA NA6000 1 70 70 70 0.02 0.4 0.6 0.6 70 600 70 25 4000 100 6 70 70 600 NL 400 400 500 47 40 40 0.02 0.046,000,000 5,000 5,900 8,800 14,750 50 380 600 510 70,000 80,000 30,500 11,700 4,000,000 100,000 15,500 26,100 70,000 260,000 NL 28,500 24,100 50,000 47,000 40,000 40,000 50 NLNL 5 NL NL 0.05 5 5 5 NL 700 NL NL NL NL NL NL 100 1000 NL NL NL NL NL NL NL 0.05 NLNotes:1)2)3)4)5)US EPA MCL = Maximum Contaminant Level for drinking water, established by the US EPA, Revion IV.6)POE System for WSW‐4 was removed at request of NCDEQ.NL= Not ListedND= Compound Not Detected Above Laboratory Detection Limits (Detection Limit Not Provided By Previous Consultant).ResultNR= Compound Not ReportedResultNA= Compound Not Analyzed for by Laboratory.ResultResultWSW‐4WSW‐3AWSW‐2= Result Exceeds 2L Standard and US EPA MCL (Applies to water supply well samples only)= Result Exceeds Laboratory Detection Limits= Result Exceeds 2L Standard= Result Exceeds GCL ValueWSW‐8WSW‐6WSW‐4(Post POE)WSW‐4(Pre POE)Not Sampled All results provided in ug/L (micrograms per liter) or parts per billionNC 2L Standard Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. GCLs for GroundwaterNot Sampled ‐ POE System Disconnected GCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for Groundwater (Comprehensive Tables for Corrective Action Guidelines, January 19, 2021). NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L (Comprehensive Tables for Corrective Action Guidelines, January 19, 2021).US EPA MCLNot SampledPage 3 of 3
Calculated 504.1Benzene1,2‐Dibromoethane(EDB)1,2‐DichloroethaneDi‐isopropyl etherEthylbenzeneNaphthaleneToluene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal Xylene1,2‐Dibromoethane(EDB)71‐43‐2 106‐93‐4 107‐06‐2 108‐20‐3 100‐41‐491‐20‐3 108‐88‐395‐63‐6 108‐67‐8 NA 106‐93‐4MW‐16/29/2023<5 <5 <5 <5107 73.4 43.1 255 83.4 455<2000MW‐26/8/2023MW‐2D6/8/2023<0.500 <0.0201 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0201MW‐3R6/8/2023<0.500 <0.0203 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0203MW‐46/8/2023<0.500 <0.0205 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0205MW‐4D6/8/2023<0.500 <0.0203 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0203MW‐56/8/2023<0.500 <0.0210 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0210MW‐76/8/2023<0.500 <0.0204 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0204MW‐86/8/2023<0.500 <0.0207 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0207MW‐96/8/2023<0.500 <0.0204 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0204WSW‐26/8/2023<0.500 <0.0204 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0204WSW‐3A6/8/2023<0.5000.0262 0.737<0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.5000.0262WSW‐46/8/2023<0.5000.0455 1.67<0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.5000.0455WSW‐66/8/2023<0.500 <0.0201 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.0201WSW‐86/8/2023<0.500 <0.0205 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <0.500 <0.500 <0.02051 0.02 0.4 70 600 6 600 400 400 500 0.025,000 50 380 70,000 80,000 15,500 260,000 28,500 24,100 50,000 505 0.05 5 NL 700 NL 1000 NL NL NL 0.05Notes:1)2)3)4)5)US EPA MCL = Maximum Contaminant Level for drinking water, established by the US EPA, Revion IV.Result= Result exceeds laboratory method detection limitResult= Result exceeds NC 2L StandardResult= Result exceeds NC GCLResult= Result exceeds EPA MCL All results provided in ug/L (micrograms per liter) or parts per billionCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L (Comprehensive Tables for Corrective Action Guidelines, September 2022). GCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for Groundwater (Comprehensive Tables for Corrective Action Guidelines, September 2022).NC 2L Standard GCLs for GroundwaterUS EPA MCLNOT SAMPLEDAnalytical MethodSampleIDDateCollectedTABLE B‐4BSUMMARY OF GROUNDWATER ANALYTICAL RESULTS (JUNE 2023)FORMER SAM PUCKETT PROPERTYIncident Number: 2630510 Puckett TrailEpsom, Franklin County, North CarolinaPage 1 of 1
Easting Northing10 Puckett Trail 10 Puckett TrailHenderson, NC 27537 Henderson, NC 2753720 Puckett Trail 20 Puckett TrailHenderson, NC 27537 Henderson, NC 275378105 NC HWY 39 8105 NC HWY 39Henderson, NC 27537 Henderson, NC 275378105 NC HWY 39 8105 NC HWY 39Henderson, NC 27537 Henderson, NC 275378125 NC HWY 39 8125 NC HWY 39Henderson, NC 27537 Henderson, NC 275378067 NC HWY 39 8067 NC HWY 39Henderson, NC 27537 Henderson, NC 275378139 NC HWY 39 P.O. Box 1084Henderson, NC 27537 Henderson, NC 275378057 NC HWY 39 8057 NC HWY 39Henderson, NC 27537 Henderson, NC 2753710 Puckett trail 10 Puckett trailHenderson, NC 27537 Henderson, NC 275378067 NC HWY 39 10 Puckett trailHenderson, NC 27537 Henderson, NC 2753740 Puckett Trail 40 Puckett TrailHenderson, NC 27537 Henderson, NC 27537NC HWY 39 P.O. Box 321Henderson, NC 27537 Saratoga, NC 278738008 NC HWY 39 8008 NC HWY 39Henderson, NC 27537 Henderson, NC 2753742 Dickie Drive 42 Dickie DriveHenderson, NC 27537 Henderson, NC 2753718 Epsom Rocky Ford Rd. 18 Epsom Rocky Ford Rd.Henderson, NC 27537 Henderson, NC 275378032 NC HWY 39 3418 Cape Forest DriveHenderson, NC 27537 Humble, TX 7734589 Epsom‐Rocky Ford Road 89 Epsom‐Rocky Ford RoadHenderson, NC 27537 Henderson, NC 2753792 Fletcher Fuller Road 92 Fletcher Fuller RoadHenderson, NC 27537 Henderson, NC 2753744 Fletcher Fuller Road 44 Fletcher Fuller RoadHenderson, NC 27537 Henderson, NC 275371217 Eaves Road 1217 Eaves RoadHenderson, NC 27537 Henderson, NC 275371216 Eaves Road 1216 Eaves RoadHenderson, NC 27537 Henderson, NC 275371)2)3)011009010998Parcel #025178011063010995010620011060010817027714010170036554010017037865010697036554010705010704010704033030395 Cross‐Gradient 2199177.84 908257.30Unknown Unknown 453 Cross‐Gradient 2199192.65WSW‐3A 1990‐98‐0119 Cherie McBeth‐Davis Potable 145 792199382.051990‐88‐7447Unknown Unknown 222 Down‐gradientPotableDonald WilibyAbandoned (Inactive)1990‐98‐3877Unknown20Unknown Unknown 702 Cross‐Gradient2198811.93Up‐Gradient527UnknownUnknown175 125‐175 218 Down‐gradient 2198935.502198670.37Cross‐Gradient344UnknownUnknownJohn Mills Masonic LodgeRoy Elks PotablePotablePotableNew Beginnings MinistriesPotable1990‐87‐98521990‐98‐11531990‐98‐0119Anna SmithEpsom Fire and RescuePotableCherie McBeth‐Davis Abandoned010032775 Cross‐Gradient 2198330.352198106.81Up‐Gradient82165 Cross‐Gradient 2198724.942199716.33Down‐gradient1109Potable Unknown UnknownUnknownUnknownPotable(Inactive)Potable Unknown UnknownUnknownUnknownPotable1990‐98‐68681990‐88‐7318 Roy ElksPhillip WilliamsCharles & Brenda HawkinsEdwards Grocery Inc0104672199235.08Down‐gradient1078UnknownUnknownPotablePotable Unknown Unknown 716 Up‐Gradient 2198170.352197892.742198335.20Up‐Gradient506Unknown901 Up‐GradientWalter BurgessBetty NewtonPotable UnknownPotablePotableUnknownUnknownPotableUnknownPotableUp‐GradientUp‐Gradient864UnknownUnknown 869908772.91909236.62W.J. Renn1990‐88‐26181990‐88‐24771990‐78‐8591908681.20908551.26908527.75Unknown908147.21907940.74907951.35908603.01908155.86907656.26908395.09908327.23908826.44908917.28908432.08908243.00Unknown Unknown 330 Down‐gradient 2199044.302198975.85Cross‐Gradient221WSW‐7WSW‐6WSW‐5WSW‐42198872.89 908459.35WSW‐3WSW‐2WSW‐1Roy Elks1990‐88‐74471990‐88‐56711990‐97‐3996WSW‐14WSW‐13WSW‐12WSW‐11WSW‐10WSW‐9WSW‐8Kevin Collier1990‐99‐12711990‐88‐17271990‐88‐3920WSW‐162198442.87Up‐Gradient759UnknownWSW‐15Nancy CollierKathryn WoodliefRonald RennUp‐Gradient 2198752.28 907343.93Unknown907578.942198141.222197900.56WSW‐19WSW‐18WSW‐17 1990‐78‐91561990‐87‐06911990‐87‐4581WSW‐20Betty R., Anthony R. & Donnie E. Newton, c/o Anthony R. NewtonPotable Unknown Unknown 926Well location addresses and property owner information obtained from the Franklin County GIS Department, current as of June 15, 2023.Supply wells WSW‐10 and WSW‐13 were identified by previous consultants as being located within 1,000 feet of the source area, however, the center of the 1,000 foot radius used by previous consultants was located at the middle of the former Sam Puckett property, rather than the middle of the UST area. Supply wells WSW‐10 and WSW‐13 are in actuality located 1,110 and 1,078 feet from the source area, respectively.With the exception of supply wells WSW‐10 and WSW‐13, as noted above, only those wells identified within 1,000 feet of the release location are shown hereon.Notes: Well Coordinates(NC State Plane NAD 83 Feet)Property Owner AddressProperty AddressWell ID Property OwnerPINWell UseWell Depth(feet)2808‐08‐6919Well Screen Interval(feet)TABLE B‐5PUBLIC & PRIVATE WATER SUPPLY WELL INFORMATIONFORMER SAM PUCKETT PROPERTY10 Puckett TrailEpsom, Franklin County, North CarolinaWell Distance from Source Area(feet)Location Relative to Groundwater FlowIncident Number: 26305Page 1 of 1
Easting NorthingMW‐1 Unknown 2 16.0 6.0 6 ‐ 16 105.86 6/1/2022 NM‐‐‐ ‐‐‐2198762.32 908265.80MW‐2 Unknown 2 16.0 6.0 6 ‐ 16 102.24 6/1/2022 NM‐‐‐ ‐‐‐2198914.82 908358.97MW‐2D 8/8/2017 2 30.0 25.0 25‐30 102.64 6/1/2022 10.75‐‐‐91.89 2198908.13 908365.32MW‐3R 8/8/2017 2 20.0 5.0 5 ‐ 20 100.06 6/1/2022 8.12‐‐‐91.94 2199080.28 908257.12MW‐4 3/9/2004 2 16.0 6.0 6 ‐ 16 103.58 6/1/2022 10.95‐‐‐92.63 2198866.28 908307.82MW‐4D 8/8/2017 2 30.0 25.0 25 ‐ 30 103.47 6/1/2022 10.83‐‐‐92.64 2198858.65 908316.88MW‐5 3/9/2004 2 16.0 6.0 6 ‐ 16 103.14 6/1/2022 10.43‐‐‐92.71 2198848.11 908234.63MW‐6 3/9/2004 2 16.0 6.0 6 ‐ 16 105.39‐‐‐DESTROYED‐‐‐ ‐‐‐2198789.74 908254.13MW‐7 3/9/2004 2 16.0 6.0 6 ‐ 16 106.50 6/1/2022 12.79‐‐‐93.71 2198734.17 908288.90MW‐8 8/8/2017 2 20.0 5.0 5 ‐ 20 106.73 6/1/2022 14.69‐‐‐92.04 2198735.65 908181.46MW‐9 8/8/2017 2 20.0 5.0 5 ‐ 20 102.16 6/1/2022 10.20‐‐‐91.96 2198925.20 908234.851)2)Epsom, Franklin County, North CarolinaTotal Depth (feet)FORMER SAM PUCKETT PROPERTYDate InstalledIncident Number: 26305TABLE B‐710 Puckett TrailMONITORING & REMEDIATION WELL CONSTRUCTION INFORMATIONWell Casing Diameter(inches)Free Product Thickness(feet)Well Casing Depth (feet)Well IDTop‐of‐Casing Elevation (feet)GroundwaterElevation (feet)Top‐of‐casing elevationsfor MW‐1, MW‐2, MW‐4, MW‐5, MW‐6 and MW‐7 were obtained from previous consultant's reports and are based on an arbitrary 100‐foot elevation benchmark. Previous consultants' reports have not identified the nature and location of the benchmark. Elevations for wells MW‐2D, MW‐3R, MW‐4D, MW‐8 and MW‐9 surveyed by WR utilizing the TOC elevation of a previously surveyed well as a reference point. Well Coordinates(NC State Plane NAD 83 Feet)Date Water Level MeasuredScreened Interval (feet)Notes: Well coordinates collected using a Trimble 2005 Series GeoXH GPS Unit.Depth‐to‐Water from Top‐of‐Casing(feet)Page 1 of 1
Well ID
Screened
Interval
(feet)
Top‐of‐Casing
Elevation
(feet)
Date Water Level
Measured
Depth‐to‐Product
(feet)
Depth‐to‐Water
Uncorrected
(feet)
Free Product
Thickness
(feet)
Depth‐to‐Water
Corrected
(feet)
Groundwater
Surface
Elevation
(feet)
5/14/08 ‐‐‐13.47 ‐‐‐13.47 92.39
12/15/10 ‐‐‐
10/11/12 ‐‐‐16.16 ‐‐‐16.16 89.70
6/26/14 ‐‐‐12.05 ‐‐‐12.05 93.81
4/16/15 ‐‐‐10.14 ‐‐‐10.14 95.72
7/21/16 ‐‐‐9.16 ‐‐‐9.16 96.70
8/9/17 ‐‐‐15.15 ‐‐‐15.15 90.71
1/17/19 ‐‐‐9.78 ‐‐‐9.78 96.08
1/28/20 ‐‐‐14.42 ‐‐‐14.42 91.44
3/1/21 ‐‐‐7.47 ‐‐‐7.47 98.39
6/1/22 ‐‐‐14.95 ‐‐‐14.95 90.91
6/8/23 ‐‐‐NM ‐‐‐NM ‐‐‐
5/14/08 ‐‐‐10.93 ‐‐‐. 91.31
12/15/10 ‐‐‐14.57 ‐‐‐14.57 87.67
10/11/12
6/26/14 ‐‐‐10.22 ‐‐‐10.22 92.02
4/16/15 ‐‐‐8.08 ‐‐‐8.08 94.16
7/21/16 ‐‐‐7.08 ‐‐‐7.08 95.16
8/9/17 ‐‐‐13.14 ‐‐‐13.14 89.10
1/17/19 ‐‐‐7.09 ‐‐‐7.09 95.15
1/28/20 ‐‐‐11.48 ‐‐‐11.48 90.76
3/1/21 ‐‐‐4.87 ‐‐‐4.87 97.37
6/1/22 ‐‐‐NM ‐‐‐NM ‐‐‐
6/8/23 ‐‐‐NM ‐‐‐NM ‐‐‐
8/9/17 ‐‐‐13.47 ‐‐‐13.47 89.17
1/17/19 ‐‐‐7.31 ‐‐‐7.31 95.33
1/28/20 ‐‐‐11.86 ‐‐‐11.86 90.78
3/1/21 ‐‐‐7.60 ‐‐‐7.60 95.04
6/1/22 ‐‐‐12.45 ‐‐‐12.45 90.19
6/8/23 10.75 10.75 91.89
8/9/17 ‐‐‐11.06 ‐‐‐11.06 89.00
1/17/19 ‐‐‐5.66 ‐‐‐5.66 94.40
1/28/20 ‐‐‐8.76 ‐‐‐8.76 91.30
3/1/21 2.80 2.80 97.26
6/1/22 ‐‐‐NM ‐‐‐NM ‐‐‐
6/8/23 8.12 8.12 91.94
5/14/08 ‐‐‐11.82 ‐‐‐11.82 91.76
12/15/10 ‐‐‐15.33 ‐‐‐15.33 88.25
10/11/12 ‐‐‐15.48 ‐‐‐15.48 88.10
6/26/14 ‐‐‐10.78 ‐‐‐10.78 92.80
4/16/15 ‐‐‐8.69 ‐‐‐8.69 94.89
7/21/16 ‐‐‐7.70 ‐‐‐7.70 95.88
8/9/17 ‐‐‐13.88 ‐‐‐13.88 89.70
1/17/19 ‐‐‐7.76 ‐‐‐7.76 95.82
1/28/20 ‐‐‐12.50 ‐‐‐12.50 91.08
3/1/21 ‐‐‐5.54 ‐‐‐5.54 98.04
6/1/22 ‐‐‐13.17 ‐‐‐13.17 90.41
6/8/23 10.95 10.95 92.63
8/9/17 ‐‐‐13.75 ‐‐‐13.75 89.72
1/17/19 ‐‐‐7.67 ‐‐‐7.67 95.80
1/28/20 ‐‐‐12.38 ‐‐‐12.38 91.09
3/1/21 ‐‐‐5.67 ‐‐‐5.67 97.80
6/1/22 ‐‐‐13.06 ‐‐‐13.06 90.41
6/8/23 10.83 10.83 92.64
102.246 ‐ 16
6 ‐ 16 105.86
25 ‐ 30
6 ‐ 16 103.58
100.065 ‐ 20
25 ‐ 30 102.64
MW‐4
MW‐4D 103.47
MW‐1
MW‐2
MW‐2D
MW‐3R
TABLE B‐9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
FORMER SAM PUCKETT PROPERTY
10 Puckett Trail
Epsom, Franklin County, North Carolina
Incident Number: 26305
Not Found
Dry
Page 1 of 2
Well ID
Screened
Interval
(feet)
Top‐of‐Casing
Elevation
(feet)
Date Water Level
Measured
Depth‐to‐Product
(feet)
Depth‐to‐Water
Uncorrected
(feet)
Free Product
Thickness
(feet)
Depth‐to‐Water
Corrected
(feet)
Groundwater
Surface
Elevation
(feet)
TABLE B‐9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
FORMER SAM PUCKETT PROPERTY
10 Puckett Trail
Epsom, Franklin County, North Carolina
Incident Number: 26305
5/14/08 ‐‐‐11.28 ‐‐‐11.28 91.86
12/15/10 ‐‐‐14.83 ‐‐‐14.83 88.31
10/11/12 ‐‐‐15.05 ‐‐‐15.05 88.09
6/26/14 ‐‐‐10.21 ‐‐‐10.21 92.93
4/16/15 ‐‐‐8.19 ‐‐‐8.19 94.95
7/21/16 ‐‐‐7.18 ‐‐‐7.18 95.96
8/9/17 ‐‐‐13.36 ‐‐‐13.36 89.78
1/17/19 ‐‐‐7.30 ‐‐‐7.30 95.84
1/28/20 ‐‐‐12.10 ‐‐‐12.10 91.04
3/1/21 ‐‐‐5.84 ‐‐‐5.84 97.30
6/1/22 ‐‐‐12.63 ‐‐‐12.63 90.51
6/8/23 10.43 10.43 92.71
5/14/08 ‐‐‐13.11 ‐‐‐13.11 92.28
12/15/10 ‐‐‐
10/11/12 ‐‐‐15.85 ‐‐‐15.85 89.54
6/26/14 ‐‐‐11.70 ‐‐‐11.70 93.69
4/16/15 ‐‐‐9.78 ‐‐‐9.78 95.61
7/21/16 ‐‐‐8.89 ‐‐‐8.89 96.50
8/9/17 ‐‐‐
1/17/19 ‐‐‐9.15 ‐‐‐9.15 96.24
1/28/20 ‐‐‐13.82 ‐‐‐13.82 91.57
3/1/21
5/14/08 ‐‐‐13.99 ‐‐‐13.99 92.51
12/15/10 ‐‐‐
10/11/12 ‐‐‐
6/26/14 ‐‐‐12.53 ‐‐‐12.53 93.97
4/16/15 ‐‐‐10.58 ‐‐‐10.58 95.92
7/21/16 ‐‐‐9.73 ‐‐‐9.73 96.77
8/9/17 ‐‐‐15.63 ‐‐‐15.63 90.87
1/17/19 ‐‐‐10.31 ‐‐‐10.31 96.19
1/28/20 ‐‐‐14.94 ‐‐‐14.94 91.56
3/1/21 ‐‐‐7.95 ‐‐‐7.95 98.55
6/1/22 ‐‐‐15.06 ‐‐‐15.06 91.44
6/8/23 12.79 12.79 93.71
8/9/17 ‐‐‐17.68 ‐‐‐17.68 89.05
1/17/19 ‐‐‐11.78 ‐‐‐11.78 94.95
1/28/20 ‐‐‐16.52 ‐‐‐16.52 90.21
3/1/21 ‐‐‐10.50 ‐‐‐10.50 96.23
6/1/22 ‐‐‐16.78 ‐‐‐16.78 89.95
6/8/23 14.69 14.69 92.04
8/9/17 ‐‐‐13.19 ‐‐‐13.19 88.97
1/17/19 ‐‐‐6.80 ‐‐‐6.80 95.36
1/28/20 ‐‐‐11.44 ‐‐‐11.44 90.72
3/1/21 ‐‐‐4.76 ‐‐‐4.76 97.40
6/1/22 ‐‐‐12.25 ‐‐‐12.25 89.91
6/8/23 10.20 10.20 91.96
1)
2)
5 ‐ 20 106.73
6 ‐ 16 106.50
105.396 ‐ 16
MW‐5
MW‐6
MW‐7
MW‐8
6 ‐ 16 103.14
MW‐95 ‐ 20 102.16
Notes:
Top‐of‐casing elevationsfor MW‐1, MW‐2, MW‐4, MW‐5, MW‐6 and MW‐7 were obtained from previous consultant's reports and are based on an
arbitrary 100‐foot elevation benchmark. Previous consultants' reports have not identified the nature and location of the benchmark. Elevations for wells
MW‐2D, MW‐3R, MW‐4D, MW‐8 and MW‐9 surveyed by WR utilizing the TOC elevation of a previously surveyed well as a reference point.
Dry
Dry
DRY
MW‐6 was found on March 1, 2021 to have been destroyed.
Dry
WELL DESTROYED
Page 2 of 2
APPENDIX A
LABORATORY ANALYTICAL REPORT & CHAIN OF CUSTODY
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
6/15/2023
Withers & Ravenel Kevin Buchanan
115 Mackenan Dr. BUILDING 117 Cary, NC, 27511
Ref: Analytical Testing
Lab Report Number: 23-160-0016 Client Project Description: Former Sam Puckett
23-0307-DY
Dear Kevin Buchanan:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/9/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 67
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-160-0016
Page 2 of 67
Report Number:
Sample Summary Table
Client Project Description:
23-160-0016
Former Sam Puckett
23-0307-DY
Lab No Client Sample ID Matrix Date Collected Date Received
06/08/2023 11:30Aqueous 97981 MW-2D 06/09/2023 12:35
06/08/2023 14:00Aqueous 97982 MW-3R 06/09/2023 12:35
06/08/2023 10:30Aqueous 97983 MW-4 06/09/2023 12:35
06/08/2023 11:00Aqueous 97984 MW-4D 06/09/2023 12:35
06/08/2023 13:00Aqueous 97985 MW-5 06/09/2023 12:35
06/08/2023 12:30Aqueous 97986 MW-7 06/09/2023 12:35
06/08/2023 12:00Aqueous 97987 MW-8 06/09/2023 12:35
06/08/2023 13:30Aqueous 97988 MW-9 06/09/2023 12:35
06/08/2023 15:20Aqueous 97989 WSW-2 06/09/2023 12:35
06/08/2023 15:40Aqueous 97990 WSW-3A 06/09/2023 12:35
06/08/2023 16:10Aqueous 97991 WSW-4 06/09/2023 12:35
06/08/2023 16:35Aqueous 97992 WSW-6 06/09/2023 12:35
06/08/2023 15:00Aqueous 97993 WSW-8 06/09/2023 12:35
Page 3 of 67
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-160-0016
Report Limit
Project:Former Sam Puckett
V 97990WSW-3A
0.737 06/14/2023 18:186200B1,2-Dichloroethane µg/L 0.500
0.0262 06/14/2023 11:03EPA-504.1 1,2-Dibromoethane µg/L 0.0202
V 97991WSW-4
1.67 06/14/2023 18:426200B1,2-Dichloroethane µg/L 0.500
0.0455 06/14/2023 11:04EPA-504.1 1,2-Dibromoethane µg/L 0.0207
Page 4 of 67
Client: Withers & Ravenel CASE NARRATIVE
Project: Former Sam Puckett Lab Report Number: 23-160-0016
Date: 6/15/2023
EDB and DBCP by Microextraction GC/ECD Method EPA-504.1 Sample 97990 (WSW-3A) Analyte: 1,2-Dibromoethane
QC Batch No: V34303/V34264 The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to
the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Volatile Organic Compounds - GC/MS Method 6200B Sample 97982 (MW-3R)
Analyte: 4-Bromofluorobenzene QC Batch No: V34362/V34358
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Page 5 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-2D
97981 Matrix:
6/8/2023 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 14:39 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 14:39 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 14:39 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 14:39 6200BMSA
<0.0201 µg/L 0.02011,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 14:39 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 6 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-2D
97981 Matrix:
6/8/2023 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 14:39 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 14:39 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 14:39 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 14:39 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 14:39 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 14:39 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 14:39 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 7 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-2D
97981 Matrix:
6/8/2023 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 14:39 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 14:39 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 14:39 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 14:39 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 8 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-2D
97981 Matrix:
6/8/2023 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 14:39 6200B
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%06/14/23 14:391 MSA V34362
Surrogate: Dibromofluoromethane 102 Limits: 70-130%06/14/23 14:391 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%06/14/23 14:391 MSA V34362
Surrogate: Toluene-d8 99.4 Limits: 70-130%06/14/23 14:391 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 9 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-3R
97982 Matrix:
6/8/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 15:03 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 15:03 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 15:03 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 15:03 6200BMSA
<0.0203 µg/L 0.02031,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 15:03 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 10 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-3R
97982 Matrix:
6/8/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 15:03 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 15:03 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 15:03 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 15:03 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 15:03 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 15:03 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 15:03 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 11 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-3R
97982 Matrix:
6/8/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 15:03 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 15:03 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 15:03 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 15:03 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 12 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-3R
97982 Matrix:
6/8/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 15:03 6200B
Surrogate: 4-Bromofluorobenzene 131 *Limits: 70-130%06/14/23 15:031 MSA V34362
Surrogate: Dibromofluoromethane 101 Limits: 70-130%06/14/23 15:031 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%06/14/23 15:031 MSA V34362
Surrogate: Toluene-d8 100 Limits: 70-130%06/14/23 15:031 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 13 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4
97983 Matrix:
6/8/2023 10:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 15:27 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 15:27 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 15:27 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 15:27 6200BMSA
<0.0205 µg/L 0.02051,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 15:27 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 14 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4
97983 Matrix:
6/8/2023 10:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 15:27 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 15:27 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 15:27 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 15:27 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 15:27 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 15:27 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 15:27 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 15 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4
97983 Matrix:
6/8/2023 10:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 15:27 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 15:27 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 15:27 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 15:27 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 16 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4
97983 Matrix:
6/8/2023 10:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 15:27 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%06/14/23 15:271 MSA V34362
Surrogate: Dibromofluoromethane 102 Limits: 70-130%06/14/23 15:271 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%06/14/23 15:271 MSA V34362
Surrogate: Toluene-d8 97.8 Limits: 70-130%06/14/23 15:271 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 17 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4D
97984 Matrix:
6/8/2023 11:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 15:52 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 15:52 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 15:52 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 15:52 6200BMSA
<0.0203 µg/L 0.02031,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 15:52 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 18 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4D
97984 Matrix:
6/8/2023 11:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 15:52 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 15:52 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 15:52 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 15:52 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 15:52 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 15:52 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 15:52 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 19 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4D
97984 Matrix:
6/8/2023 11:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 15:52 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 15:52 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 15:52 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 15:52 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 20 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-4D
97984 Matrix:
6/8/2023 11:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 15:52 6200B
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%06/14/23 15:521 MSA V34362
Surrogate: Dibromofluoromethane 100 Limits: 70-130%06/14/23 15:521 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%06/14/23 15:521 MSA V34362
Surrogate: Toluene-d8 98.6 Limits: 70-130%06/14/23 15:521 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 21 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-5
97985 Matrix:
6/8/2023 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 16:16 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 16:16 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 16:16 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 16:16 6200BMSA
<0.0210 µg/L 0.02101,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 16:16 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 22 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-5
97985 Matrix:
6/8/2023 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 16:16 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 16:16 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 16:16 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 16:16 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 16:16 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 16:16 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 16:16 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 23 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-5
97985 Matrix:
6/8/2023 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 16:16 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 16:16 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 16:16 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 16:16 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 24 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-5
97985 Matrix:
6/8/2023 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 16:16 6200B
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%06/14/23 16:161 MSA V34362
Surrogate: Dibromofluoromethane 102 Limits: 70-130%06/14/23 16:161 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%06/14/23 16:161 MSA V34362
Surrogate: Toluene-d8 98.6 Limits: 70-130%06/14/23 16:161 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 25 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-7
97986 Matrix:
6/8/2023 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 16:40 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 16:40 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 16:40 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 16:40 6200BMSA
<0.0204 µg/L 0.02041,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 16:40 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 26 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-7
97986 Matrix:
6/8/2023 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 16:40 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 16:40 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 16:40 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 16:40 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 16:40 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 16:40 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 16:40 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 27 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-7
97986 Matrix:
6/8/2023 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 16:40 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 16:40 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 16:40 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 16:40 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 28 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-7
97986 Matrix:
6/8/2023 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 16:40 6200B
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%06/14/23 16:401 MSA V34362
Surrogate: Dibromofluoromethane 101 Limits: 70-130%06/14/23 16:401 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%06/14/23 16:401 MSA V34362
Surrogate: Toluene-d8 100 Limits: 70-130%06/14/23 16:401 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 29 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-8
97987 Matrix:
6/8/2023 12:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 17:05 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 17:05 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 17:05 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 17:05 6200BMSA
<0.0207 µg/L 0.02071,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 17:05 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 30 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-8
97987 Matrix:
6/8/2023 12:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 17:05 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 17:05 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 17:05 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 17:05 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 17:05 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 17:05 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 17:05 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 31 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-8
97987 Matrix:
6/8/2023 12:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 17:05 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 17:05 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 17:05 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 17:05 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 32 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-8
97987 Matrix:
6/8/2023 12:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 17:05 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%06/14/23 17:051 MSA V34362
Surrogate: Dibromofluoromethane 101 Limits: 70-130%06/14/23 17:051 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%06/14/23 17:051 MSA V34362
Surrogate: Toluene-d8 98.2 Limits: 70-130%06/14/23 17:051 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 33 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-9
97988 Matrix:
6/8/2023 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 17:29 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 17:29 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 17:29 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 17:29 6200BMSA
<0.0204 µg/L 0.02041,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 17:29 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 34 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-9
97988 Matrix:
6/8/2023 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 17:29 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 17:29 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 17:29 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 17:29 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 17:29 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 17:29 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 17:29 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 35 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-9
97988 Matrix:
6/8/2023 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 17:29 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 17:29 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 17:29 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 17:29 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 36 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:MW-9
97988 Matrix:
6/8/2023 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 17:29 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%06/14/23 17:291 MSA V34362
Surrogate: Dibromofluoromethane 102 Limits: 70-130%06/14/23 17:291 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%06/14/23 17:291 MSA V34362
Surrogate: Toluene-d8 100 Limits: 70-130%06/14/23 17:291 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 37 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-2
97989 Matrix:
6/8/2023 15:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 17:53 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 17:53 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 17:53 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 17:53 6200BMSA
<0.0204 µg/L 0.02041,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 17:53 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 38 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-2
97989 Matrix:
6/8/2023 15:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 17:53 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 17:53 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 17:53 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 17:53 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 17:53 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 17:53 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 17:53 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 39 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-2
97989 Matrix:
6/8/2023 15:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 17:53 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 17:53 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 17:53 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 17:53 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 40 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-2
97989 Matrix:
6/8/2023 15:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 17:53 6200B
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%06/14/23 17:531 MSA V34362
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%06/14/23 17:531 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%06/14/23 17:531 MSA V34362
Surrogate: Toluene-d8 98.8 Limits: 70-130%06/14/23 17:531 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 41 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-3A
97990 Matrix:
6/8/2023 15:40
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 18:18 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 18:18 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 18:18 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 18:18 6200BMSA
0.0262 µg/L 0.02021,2-Dibromoethane 1 06/14/23 11:03 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 18:18 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 42 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-3A
97990 Matrix:
6/8/2023 15:40
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 18:18 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 18:18 6200BMSA
0.737 µg/L 0.5001,2-Dichloroethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 18:18 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 18:18 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 18:18 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 18:18 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 18:18 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 18:18 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 43 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-3A
97990 Matrix:
6/8/2023 15:40
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 18:18 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 18:18 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 18:18 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 18:18 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 44 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-3A
97990 Matrix:
6/8/2023 15:40
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 18:18 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%06/14/23 18:181 MSA V34362
Surrogate: Dibromofluoromethane 101 Limits: 70-130%06/14/23 18:181 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%06/14/23 18:181 MSA V34362
Surrogate: Toluene-d8 99.6 Limits: 70-130%06/14/23 18:181 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 45 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-4
97991 Matrix:
6/8/2023 16:10
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 18:42 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 18:42 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 18:42 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 18:42 6200BMSA
0.0455 µg/L 0.02071,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 18:42 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 46 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-4
97991 Matrix:
6/8/2023 16:10
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 18:42 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 18:42 6200BMSA
1.67 µg/L 0.5001,2-Dichloroethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 18:42 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 18:42 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 18:42 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 18:42 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 18:42 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 18:42 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 47 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-4
97991 Matrix:
6/8/2023 16:10
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 18:42 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 18:42 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 18:42 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 18:42 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 48 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-4
97991 Matrix:
6/8/2023 16:10
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 18:42 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%06/14/23 18:421 MSA V34362
Surrogate: Dibromofluoromethane 102 Limits: 70-130%06/14/23 18:421 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%06/14/23 18:421 MSA V34362
Surrogate: Toluene-d8 98.8 Limits: 70-130%06/14/23 18:421 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 49 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-6
97992 Matrix:
6/8/2023 16:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 19:06 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 19:06 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 19:06 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 19:06 6200BMSA
<0.0201 µg/L 0.02011,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 19:06 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 50 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-6
97992 Matrix:
6/8/2023 16:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 19:06 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 19:06 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 19:06 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 19:06 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 19:06 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 19:06 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 19:06 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 51 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-6
97992 Matrix:
6/8/2023 16:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 19:06 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 19:06 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 19:06 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 19:06 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 52 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-6
97992 Matrix:
6/8/2023 16:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 19:06 6200B
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%06/14/23 19:061 MSA V34362
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%06/14/23 19:061 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%06/14/23 19:061 MSA V34362
Surrogate: Toluene-d8 98.4 Limits: 70-130%06/14/23 19:061 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 53 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-8
97993 Matrix:
6/8/2023 15:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Benzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Bromobenzene 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.00Bromochloromethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Bromodichloromethane 1 06/14/23 19:31 6200BMSA
<5.00 µg/L 5.00Bromoform 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.00Bromomethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500n-Butylbenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500sec-Butyl benzene 1 06/14/23 19:31 6200BMSA
<2.00 µg/L 2.00tert-Butyl benzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Carbon Tetrachloride 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Chlorobenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Chlorodibromomethane 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.00Chloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Chloroform 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Chloromethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5002-Chlorotoluene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5004-Chlorotoluene 1 06/14/23 19:31 6200BMSA
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 06/14/23 19:31 6200BMSA
<0.0205 µg/L 0.02051,2-Dibromoethane 1 06/14/23 11:04 EPA-504.1TJW
<0.500 µg/L 0.500Dibromomethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 06/14/23 19:31 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 54 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-8
97993 Matrix:
6/8/2023 15:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 06/14/23 19:31 6200BMSA
<5.00 µg/L 5.00Dichlorodifluoromethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2-Dichloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1-Dichloroethene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2-Dichloropropane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,3-Dichloropropane 1 06/14/23 19:31 6200BMSA
<2.00 µg/L 2.002,2-Dichloropropane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1-Dichloropropene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 06/14/23 19:31 6200BMSA
<200 µg/L 200Ethanol 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Ethylbenzene 1 06/14/23 19:31 6200BMSA
<3.00 µg/L 3.00Hexachlorobutadiene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Isopropylbenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5004-Isopropyl toluene 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.002-Hexanone 1 06/14/23 19:31 6200BMSA
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 06/14/23 19:31 6200BMSA
<2.00 µg/L 2.00Methylene Chloride 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 06/14/23 19:31 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 55 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-8
97993 Matrix:
6/8/2023 15:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.00Naphthalene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500n-Propylbenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Styrene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Tetrachloroethene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Toluene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Trichloroethene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Trichlorofluoromethane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 06/14/23 19:31 6200BMSA
<5.00 µg/L 5.00Vinyl Acetate 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500Vinyl Chloride 1 06/14/23 19:31 6200BMSA
<1.00 µg/L 1.00m,p-Xylene 1 06/14/23 19:31 6200BMSA
<0.500 µg/L 0.500o-Xylene 1 06/14/23 19:31 6200BMSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 56 of 67
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-160-0016
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/09/2023
Former Sam Puckett
Report Date : 06/15/2023
Sample ID :
Lab No :
Sampled:WSW-8
97993 Matrix:
6/8/2023 15:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 06/14/23 19:31 6200B
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%06/14/23 19:311 MSA V34362
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%06/14/23 19:311 MSA V34362
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%06/14/23 19:311 MSA V34362
Surrogate: Toluene-d8 100 Limits: 70-130%06/14/23 19:311 MSA V34362
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 57 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V34362QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V34358
Associated Lab Samples: 97981, 97982, 97983, 97984, 97985, 97986, 97987, 97988, 97989, 97990, 97991, 97992, 97993
LRB-V34358 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
06/14/23 14:1510.0< 10.0µg/LAcetone
06/14/23 14:150.500< 0.500µg/LBenzene
06/14/23 14:150.500< 0.500µg/LBromobenzene
06/14/23 14:151.00< 1.00µg/LBromochloromethane
06/14/23 14:150.500< 0.500µg/LBromodichloromethane
06/14/23 14:155.00< 5.00µg/LBromoform
06/14/23 14:151.00< 1.00µg/LBromomethane
06/14/23 14:150.500< 0.500µg/Ln-Butylbenzene
06/14/23 14:150.500< 0.500µg/Lsec-Butyl benzene
06/14/23 14:152.00< 2.00µg/Ltert-Butyl benzene
06/14/23 14:150.500< 0.500µg/LCarbon Tetrachloride
06/14/23 14:150.500< 0.500µg/LChlorobenzene
06/14/23 14:150.500< 0.500µg/LChlorodibromomethane
06/14/23 14:151.00< 1.00µg/LChloroethane
06/14/23 14:150.500< 0.500µg/LChloroform
06/14/23 14:150.500< 0.500µg/LChloromethane
06/14/23 14:150.500< 0.500µg/L2-Chlorotoluene
06/14/23 14:150.500< 0.500µg/L4-Chlorotoluene
06/14/23 14:152.00< 2.00µg/L1,2-Dibromo-3-Chloropropane
06/14/23 14:150.500< 0.500µg/LDibromomethane
06/14/23 14:150.500< 0.500µg/L1,2-Dichlorobenzene
06/14/23 14:150.500< 0.500µg/L1,3-Dichlorobenzene
06/14/23 14:150.500< 0.500µg/L1,4-Dichlorobenzene
06/14/23 14:155.00< 5.00µg/LDichlorodifluoromethane
06/14/23 14:150.500< 0.500µg/L1,1-Dichloroethane
06/14/23 14:150.500< 0.500µg/L1,2-Dichloroethane
06/14/23 14:150.500< 0.500µg/L1,1-Dichloroethene
Page 1 of 7Date:06/15/2023 12:50 PM
Page 58 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V34362QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V34358
Associated Lab Samples: 97981, 97982, 97983, 97984, 97985, 97986, 97987, 97988, 97989, 97990, 97991, 97992, 97993
LRB-V34358 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
06/14/23 14:150.500< 0.500µg/Lcis-1,2-Dichloroethene
06/14/23 14:150.500< 0.500µg/Ltrans-1,2-Dichloroethene
06/14/23 14:150.500< 0.500µg/L1,2-Dichloropropane
06/14/23 14:150.500< 0.500µg/L1,3-Dichloropropane
06/14/23 14:152.00< 2.00µg/L2,2-Dichloropropane
06/14/23 14:150.500< 0.500µg/L1,1-Dichloropropene
06/14/23 14:150.500< 0.500µg/Lcis-1,3-Dichloropropene
06/14/23 14:150.500< 0.500µg/Ltrans-1,3-Dichloropropene
06/14/23 14:15200< 200µg/LEthanol
06/14/23 14:150.500< 0.500µg/LEthylbenzene
06/14/23 14:153.00< 3.00µg/LHexachlorobutadiene
06/14/23 14:150.500< 0.500µg/LDi-Isopropyl Ether (DIPE)
06/14/23 14:150.500< 0.500µg/LIsopropylbenzene
06/14/23 14:150.500< 0.500µg/L4-Isopropyl toluene
06/14/23 14:151.00< 1.00µg/L2-Hexanone
06/14/23 14:155.00< 5.00µg/LMethyl Ethyl Ketone (MEK)
06/14/23 14:152.00< 2.00µg/LMethylene Chloride
06/14/23 14:151.00< 1.00µg/LMethyl tert-butyl ether (MTBE)
06/14/23 14:151.00< 1.00µg/L4-Methyl-2-Pentanone
06/14/23 14:151.00< 1.00µg/LNaphthalene
06/14/23 14:150.500< 0.500µg/Ln-Propylbenzene
06/14/23 14:150.500< 0.500µg/LStyrene
06/14/23 14:150.500< 0.500µg/L1,1,1,2-Tetrachloroethane
06/14/23 14:150.500< 0.500µg/L1,1,2,2-Tetrachloroethane
06/14/23 14:150.500< 0.500µg/LTetrachloroethene
06/14/23 14:150.500< 0.500µg/LToluene
06/14/23 14:150.500< 0.500µg/L1,2,3-Trichlorobenzene
Page 2 of 7Date:06/15/2023 12:50 PM
Page 59 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V34362QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V34358
Associated Lab Samples: 97981, 97982, 97983, 97984, 97985, 97986, 97987, 97988, 97989, 97990, 97991, 97992, 97993
LRB-V34358 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
06/14/23 14:150.500< 0.500µg/L1,2,4-Trichlorobenzene
06/14/23 14:150.500< 0.500µg/L1,1,1-Trichloroethane
06/14/23 14:150.500< 0.500µg/L1,1,2-Trichloroethane
06/14/23 14:150.500< 0.500µg/LTrichloroethene
06/14/23 14:150.500< 0.500µg/LTrichlorofluoromethane
06/14/23 14:150.500< 0.500µg/L1,2,3-Trichloropropane
06/14/23 14:150.500< 0.500µg/L1,2,4-Trimethylbenzene
06/14/23 14:150.500< 0.500µg/L1,3,5-Trimethylbenzene
06/14/23 14:155.00< 5.00µg/LVinyl Acetate
06/14/23 14:150.500< 0.500µg/LVinyl Chloride
06/14/23 14:151.00< 1.00µg/Lm,p-Xylene
06/14/23 14:150.500< 0.500µg/Lo-Xylene
06/14/23 14:154-Bromofluorobenzene (S)102 70-130
06/14/23 14:15Dibromofluoromethane (S)100 70-130
06/14/23 14:151,2-Dichloroethane - d4 (S)103 70-130
06/14/23 14:15Toluene-d8 (S)99.4 70-130
LCS-V34358 LCSD-V34358Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.1 82.769.727.940.0µg/LAcetone 40-160 17.0 20.0
21.0 10510521.020.0µg/LBenzene 70-130 0.0 20.0
21.3 10710721.320.0µg/LBromobenzene 70-130 0.0 20.0
20.1 10110320.620.0µg/LBromochloromethane 70-130 2.4 20.0
21.2 10610721.420.0µg/LBromodichloromethane 70-130 0.9 20.0
21.2 10696.519.320.0µg/LBromoform 70-130 9.3 20.0
Page 3 of 7Date:06/15/2023 12:50 PM
Page 60 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V34362QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V34358
LCS-V34358 LCSD-V34358Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.5 92.590.018.020.0µg/LBromomethane 60-140 2.7 20.0
20.6 10310921.820.0µg/Ln-Butylbenzene 70-130 5.6 20.0
20.4 10210420.720.0µg/Lsec-Butyl benzene 70-130 1.4 20.0
19.8 99.010520.920.0µg/Ltert-Butyl benzene 70-130 5.4 20.0
20.8 10410520.920.0µg/LCarbon Tetrachloride 70-130 0.4 20.0
20.4 10210621.120.0µg/LChlorobenzene 70-130 3.3 20.0
20.6 10310320.520.0µg/LChlorodibromomethane 70-130 0.4 20.0
25.1 12612625.120.0µg/LChloroethane 60-140 0.0 20.0
20.7 10410621.220.0µg/LChloroform 70-130 2.3 20.0
22.2 11111021.920.0µg/LChloromethane 60-140 1.3 20.0
20.7 10410621.120.0µg/L2-Chlorotoluene 70-130 1.9 20.0
20.7 10410721.320.0µg/L4-Chlorotoluene 70-130 2.8 20.0
22.0 11090.518.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 19.4 20.0
21.0 10510120.220.0µg/LDibromomethane 70-130 3.8 20.0
21.2 10610621.220.0µg/L1,2-Dichlorobenzene 70-130 0.0 20.0
20.5 10310420.820.0µg/L1,3-Dichlorobenzene 70-130 1.4 20.0
20.6 10310520.920.0µg/L1,4-Dichlorobenzene 70-130 1.4 20.0
20.7 10410821.520.0µg/LDichlorodifluoromethane 60-140 3.7 20.0
21.5 10810821.520.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
21.5 10810320.620.0µg/L1,2-Dichloroethane 70-130 4.2 20.0
21.4 10710821.620.0µg/L1,1-Dichloroethene 70-130 0.9 20.0
20.9 10510320.620.0µg/Lcis-1,2-Dichloroethene 70-130 1.4 20.0
21.3 10710621.120.0µg/Ltrans-1,2-Dichloroethene 70-130 0.9 20.0
22.1 11110721.420.0µg/L1,2-Dichloropropane 70-130 3.2 20.0
21.8 10910420.820.0µg/L1,3-Dichloropropane 70-130 4.6 20.0
20.6 10310621.120.0µg/L2,2-Dichloropropane 70-130 2.3 20.0
Page 4 of 7Date:06/15/2023 12:50 PM
Page 61 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V34362QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V34358
LCS-V34358 LCSD-V34358Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.7 10911222.320.0µg/L1,1-Dichloropropene 70-130 2.7 20.0
21.9 11011021.920.0µg/Lcis-1,3-Dichloropropene 70-130 0.0 20.0
22.7 11410921.820.0µg/Ltrans-1,3-Dichloropropene 70-130 4.0 20.0
537 10796.4482500µg/LEthanol 60-140 10.7 20.0
20.1 10110420.720.0µg/LEthylbenzene 70-130 2.9 20.0
19.9 99.510520.920.0µg/LHexachlorobutadiene 70-130 4.9 20.0
22.9 11511122.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.1 20.0
20.6 10310821.520.0µg/LIsopropylbenzene 70-130 4.2 20.0
20.9 10511022.020.0µg/L4-Isopropyl toluene 70-130 5.1 20.0
19.9 99.586.017.220.0µg/L2-Hexanone 60-140 14.5 20.0
19.8 99.082.516.520.0µg/LMethyl Ethyl Ketone (MEK)60-140 18.1 20.0
21.4 10710821.620.0µg/LMethylene Chloride 70-130 0.9 20.0
22.9 11510520.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 9.1 20.0
22.0 11092.018.420.0µg/L4-Methyl-2-Pentanone 60-140 17.8 20.0
22.2 11110120.220.0µg/LNaphthalene 70-130 9.4 20.0
20.5 10310520.920.0µg/Ln-Propylbenzene 70-130 1.9 20.0
21.1 10610320.620.0µg/LStyrene 70-130 2.3 20.0
21.7 10910621.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.8 20.0
23.2 11610821.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 7.6 20.0
20.4 10210420.720.0µg/LTetrachloroethene 70-130 1.4 20.0
20.9 10510521.020.0µg/LToluene 70-130 0.4 20.0
24.2 12111222.420.0µg/L1,2,3-Trichlorobenzene 70-130 7.7 20.0
22.6 11311122.220.0µg/L1,2,4-Trichlorobenzene 70-130 1.7 20.0
20.3 10210320.520.0µg/L1,1,1-Trichloroethane 70-130 0.9 20.0
21.6 10810220.320.0µg/L1,1,2-Trichloroethane 70-130 6.2 20.0
20.1 10110420.720.0µg/LTrichloroethene 70-130 2.9 20.0
Page 5 of 7Date:06/15/2023 12:50 PM
Page 62 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V34362QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V34358
LCS-V34358 LCSD-V34358Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.7 11411422.820.0µg/LTrichlorofluoromethane 60-140 0.4 20.0
21.8 10999.519.920.0µg/L1,2,3-Trichloropropane 70-130 9.1 20.0
20.8 10410721.420.0µg/L1,2,4-Trimethylbenzene 70-130 2.8 20.0
20.7 10410721.320.0µg/L1,3,5-Trimethylbenzene 70-130 2.8 20.0
25.0 12511923.820.0µg/LVinyl Acetate 60-140 4.9 20.0
23.3 11711523.020.0µg/LVinyl Chloride 60-140 1.2 20.0
42.6 10710742.840.0µg/Lm,p-Xylene 70-130 0.4 20.0
20.2 10110320.620.0µg/Lo-Xylene 70-130 1.9 20.0
99.899.84-Bromofluorobenzene (S)70-130
99.898.2Dibromofluoromethane (S)70-130
1051011,2-Dichloroethane - d4 (S)70-130
10099.4Toluene-d8 (S)70-130
Page 6 of 7Date:06/15/2023 12:50 PM
Page 63 of 67
Quality Control Data
23-160-0016Report No:
Project Description:
Client ID:Withers & Ravenel
Former Sam Puckett
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V34303QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V34264
Associated Lab Samples: 97981, 97982, 97983, 97984, 97985, 97986, 97987, 97988, 97989, 97990, 97991, 97992, 97993
LRB-V34264 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
06/13/23 11:520.0200< 0.0200µg/L1,2-Dibromoethane
LCS-V34264 LCSD-V34264Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.319 1281120.2790.250µg/L1,2-Dibromoethane 70-130 13.3 20.0
V 97989-DUP-V34264Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 06/14/23 11:040.9< 0.0202< 0.0202µg/L1,2-Dibromoethane
V 97990-MS-V34264Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.291 1160.251< 0.0201µg/L1,2-Dibromoethane 70-130
Page 7 of 7Date:06/15/2023 12:50 PM
Page 64 of 67
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-160-0016
Withers & Ravenel
01221
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 0.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:06/09/2023 14:26:07
Special precautions or instructions included?
Comments:
Page 65 of 67
Page 66 of 67
Page 67 of 67
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
7/10/2023
Withers & Ravenel Kevin Buchanan
115 Mackenan Dr. BUILDING 117 Cary, NC, 27511
Ref: Analytical Testing
Lab Report Number: 23-181-0021 Client Project Description: Sam Puckett
23-0307-DY
Dear Kevin Buchanan:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/30/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 17
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-181-0021
Page 2 of 17
Report Number:
Sample Summary Table
Client Project Description:
23-181-0021
Sam Puckett
23-0307-DY
Lab No Client Sample ID Matrix Date Collected Date Received
06/29/2023 14:00Aqueous 99643 MW-1 06/30/2023 13:30
Page 3 of 17
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-181-0021
Report Limit
Project:Sam Puckett
V 99643MW-1
5.31 07/07/2023 09:226200Bn-Butylbenzene µg/L 5.00
107 07/07/2023 09:226200BEthylbenzeneµg/L 5.00
11.8 07/07/2023 09:226200BIsopropylbenzeneµg/L 5.00
73.4 07/07/2023 09:226200BNaphthaleneµg/L 10.0
28.4 07/07/2023 09:226200Bn-Propylbenzene µg/L 5.00
43.1 07/07/2023 09:226200BTolueneµg/L 5.00
255 07/07/2023 09:226200B1,2,4-Trimethylbenzene µg/L 5.00
83.4 07/07/2023 09:226200B1,3,5-Trimethylbenzene µg/L 5.00
142 07/07/2023 09:226200Bo-Xylene µg/L 5.00
313 07/07/2023 09:226200Bm,p-Xylene µg/L 10.0
455 07/07/2023 09:226200BXylene (Total)µg/L 5.00
Page 4 of 17
Client: Withers & Ravenel CASE NARRATIVE
Project: Sam Puckett Lab Report Number: 23-181-0021
Date: 7/7/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Ethanol QC Batch No: V35085/V35084
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 5 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-181-0021
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/30/2023
Sam Puckett
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1
99643 Matrix:
6/29/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100Acetone 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Benzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Bromobenzene 10 07/07/23 09:22 6200BMSA
<10.0 µg/L 10.0Bromochloromethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Bromodichloromethane 10 07/07/23 09:22 6200BMSA
<50.0 µg/L 50.0Bromoform 10 07/07/23 09:22 6200BMSA
<10.0 µg/L 10.0Bromomethane 10 07/07/23 09:22 6200BMSA
5.31 µg/L 5.00n-Butylbenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00sec-Butyl benzene 10 07/07/23 09:22 6200BMSA
<20.0 µg/L 20.0tert-Butyl benzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Carbon Tetrachloride 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Chlorobenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Chlorodibromomethane 10 07/07/23 09:22 6200BMSA
<10.0 µg/L 10.0Chloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Chloroform 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Chloromethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.002-Chlorotoluene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.004-Chlorotoluene 10 07/07/23 09:22 6200BMSA
<20.0 µg/L 20.01,2-Dibromo-3-Chloropropane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2-Dibromoethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Dibromomethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2-Dichlorobenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,3-Dichlorobenzene 10 07/07/23 09:22 6200BMSA
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 6 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-181-0021
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/30/2023
Sam Puckett
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1
99643 Matrix:
6/29/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<5.00 µg/L 5.001,4-Dichlorobenzene 10 07/07/23 09:22 6200BMSA
<50.0 µg/L 50.0Dichlorodifluoromethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1-Dichloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2-Dichloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1-Dichloroethene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00cis-1,2-Dichloroethene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00trans-1,2-Dichloroethene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2-Dichloropropane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,3-Dichloropropane 10 07/07/23 09:22 6200BMSA
<20.0 µg/L 20.02,2-Dichloropropane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1-Dichloropropene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00cis-1,3-Dichloropropene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00trans-1,3-Dichloropropene 10 07/07/23 09:22 6200BMSA
<2000 µg/L 2000Ethanol 10 07/07/23 09:22 6200BMSA
107 µg/L 5.00Ethylbenzene 10 07/07/23 09:22 6200BMSA
<30.0 µg/L 30.0Hexachlorobutadiene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Di-Isopropyl Ether (DIPE)10 07/07/23 09:22 6200BMSA
11.8 µg/L 5.00Isopropylbenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.004-Isopropyl toluene 10 07/07/23 09:22 6200BMSA
<10.0 µg/L 10.02-Hexanone 10 07/07/23 09:22 6200BMSA
<50.0 µg/L 50.0Methyl Ethyl Ketone (MEK)10 07/07/23 09:22 6200BMSA
<20.0 µg/L 20.0Methylene Chloride 10 07/07/23 09:22 6200BMSA
<10.0 µg/L 10.0Methyl tert-butyl ether (MTBE)10 07/07/23 09:22 6200BMSA
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 7 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-181-0021
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/30/2023
Sam Puckett
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1
99643 Matrix:
6/29/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.04-Methyl-2-Pentanone 10 07/07/23 09:22 6200BMSA
73.4 µg/L 10.0Naphthalene 10 07/07/23 09:22 6200BMSA
28.4 µg/L 5.00n-Propylbenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Styrene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1,1,2-Tetrachloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1,2,2-Tetrachloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Tetrachloroethene 10 07/07/23 09:22 6200BMSA
43.1 µg/L 5.00Toluene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2,3-Trichlorobenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2,4-Trichlorobenzene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1,1-Trichloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,1,2-Trichloroethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Trichloroethene 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Trichlorofluoromethane 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.001,2,3-Trichloropropane 10 07/07/23 09:22 6200BMSA
255 µg/L 5.001,2,4-Trimethylbenzene 10 07/07/23 09:22 6200BMSA
83.4 µg/L 5.001,3,5-Trimethylbenzene 10 07/07/23 09:22 6200BMSA
<50.0 µg/L 50.0Vinyl Acetate 10 07/07/23 09:22 6200BMSA
<5.00 µg/L 5.00Vinyl Chloride 10 07/07/23 09:22 6200BMSA
313 µg/L 10.0m,p-Xylene 10 07/07/23 09:22 6200BMSA
142 µg/L 5.00o-Xylene 10 07/07/23 09:22 6200BMSA
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 8 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
23-181-0021
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
23-0307-DY Received : 06/30/2023
Sam Puckett
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1
99643 Matrix:
6/29/2023 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
455 µg/L 5.00Xylene (Total)10 07/07/23 09:22 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/07/23 09:2210 MSA V35085
Surrogate: Dibromofluoromethane 94.8 Limits: 70-130%07/07/23 09:2210 MSA V35085
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%07/07/23 09:2210 MSA V35085
Surrogate: Toluene-d8 93.6 Limits: 70-130%07/07/23 09:2210 MSA V35085
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 9 of 17
Quality Control Data
23-181-0021Report No:
Project Description:
Client ID:Withers & Ravenel
Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35085QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35084
Associated Lab Samples: 99643
LRB-V35084 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/07/23 04:0010.0< 10.0µg/LAcetone
07/07/23 04:000.500< 0.500µg/LBenzene
07/07/23 04:000.500< 0.500µg/LBromobenzene
07/07/23 04:001.00< 1.00µg/LBromochloromethane
07/07/23 04:000.500< 0.500µg/LBromodichloromethane
07/07/23 04:005.00< 5.00µg/LBromoform
07/07/23 04:001.00< 1.00µg/LBromomethane
07/07/23 04:000.500< 0.500µg/Ln-Butylbenzene
07/07/23 04:000.500< 0.500µg/Lsec-Butyl benzene
07/07/23 04:002.00< 2.00µg/Ltert-Butyl benzene
07/07/23 04:000.500< 0.500µg/LCarbon Tetrachloride
07/07/23 04:000.500< 0.500µg/LChlorobenzene
07/07/23 04:000.500< 0.500µg/LChlorodibromomethane
07/07/23 04:001.00< 1.00µg/LChloroethane
07/07/23 04:000.500< 0.500µg/LChloroform
07/07/23 04:000.500< 0.500µg/LChloromethane
07/07/23 04:000.500< 0.500µg/L2-Chlorotoluene
07/07/23 04:000.500< 0.500µg/L4-Chlorotoluene
07/07/23 04:002.00< 2.00µg/L1,2-Dibromo-3-Chloropropane
07/07/23 04:000.500< 0.500µg/L1,2-Dibromoethane
07/07/23 04:000.500< 0.500µg/LDibromomethane
07/07/23 04:000.500< 0.500µg/L1,2-Dichlorobenzene
07/07/23 04:000.500< 0.500µg/L1,3-Dichlorobenzene
07/07/23 04:000.500< 0.500µg/L1,4-Dichlorobenzene
07/07/23 04:005.00< 5.00µg/LDichlorodifluoromethane
07/07/23 04:000.500< 0.500µg/L1,1-Dichloroethane
07/07/23 04:000.500< 0.500µg/L1,2-Dichloroethane
Page 1 of 6Date:07/10/2023 10:39 AM
Page 10 of 17
Quality Control Data
23-181-0021Report No:
Project Description:
Client ID:Withers & Ravenel
Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35085QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35084
Associated Lab Samples: 99643
LRB-V35084 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/07/23 04:000.500< 0.500µg/L1,1-Dichloroethene
07/07/23 04:000.500< 0.500µg/Lcis-1,2-Dichloroethene
07/07/23 04:000.500< 0.500µg/Ltrans-1,2-Dichloroethene
07/07/23 04:000.500< 0.500µg/L1,2-Dichloropropane
07/07/23 04:000.500< 0.500µg/L1,3-Dichloropropane
07/07/23 04:002.00< 2.00µg/L2,2-Dichloropropane
07/07/23 04:000.500< 0.500µg/L1,1-Dichloropropene
07/07/23 04:000.500< 0.500µg/Lcis-1,3-Dichloropropene
07/07/23 04:000.500< 0.500µg/Ltrans-1,3-Dichloropropene
07/07/23 04:00200< 200µg/LEthanol
07/07/23 04:000.500< 0.500µg/LEthylbenzene
07/07/23 04:003.00< 3.00µg/LHexachlorobutadiene
07/07/23 04:000.500< 0.500µg/LDi-Isopropyl Ether (DIPE)
07/07/23 04:000.500< 0.500µg/LIsopropylbenzene
07/07/23 04:000.500< 0.500µg/L4-Isopropyl toluene
07/07/23 04:001.00< 1.00µg/L2-Hexanone
07/07/23 04:005.00< 5.00µg/LMethyl Ethyl Ketone (MEK)
07/07/23 04:002.00< 2.00µg/LMethylene Chloride
07/07/23 04:001.00< 1.00µg/LMethyl tert-butyl ether (MTBE)
07/07/23 04:001.00< 1.00µg/L4-Methyl-2-Pentanone
07/07/23 04:001.00< 1.00µg/LNaphthalene
07/07/23 04:000.500< 0.500µg/Ln-Propylbenzene
07/07/23 04:000.500< 0.500µg/LStyrene
07/07/23 04:000.500< 0.500µg/L1,1,1,2-Tetrachloroethane
07/07/23 04:000.500< 0.500µg/L1,1,2,2-Tetrachloroethane
07/07/23 04:000.500< 0.500µg/LTetrachloroethene
07/07/23 04:000.500< 0.500µg/LToluene
Page 2 of 6Date:07/10/2023 10:39 AM
Page 11 of 17
Quality Control Data
23-181-0021Report No:
Project Description:
Client ID:Withers & Ravenel
Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35085QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35084
Associated Lab Samples: 99643
LRB-V35084 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/07/23 04:000.500< 0.500µg/L1,2,3-Trichlorobenzene
07/07/23 04:000.500< 0.500µg/L1,2,4-Trichlorobenzene
07/07/23 04:000.500< 0.500µg/L1,1,1-Trichloroethane
07/07/23 04:000.500< 0.500µg/L1,1,2-Trichloroethane
07/07/23 04:000.500< 0.500µg/LTrichloroethene
07/07/23 04:000.500< 0.500µg/LTrichlorofluoromethane
07/07/23 04:000.500< 0.500µg/L1,2,3-Trichloropropane
07/07/23 04:000.500< 0.500µg/L1,2,4-Trimethylbenzene
07/07/23 04:000.500< 0.500µg/L1,3,5-Trimethylbenzene
07/07/23 04:005.00< 5.00µg/LVinyl Acetate
07/07/23 04:000.500< 0.500µg/LVinyl Chloride
07/07/23 04:001.00< 1.00µg/Lm,p-Xylene
07/07/23 04:000.500< 0.500µg/Lo-Xylene
07/07/23 04:004-Bromofluorobenzene (S)99.0 70-130
07/07/23 04:00Dibromofluoromethane (S)95.6 70-130
07/07/23 04:001,2-Dichloroethane - d4 (S)96.8 70-130
07/07/23 04:00Toluene-d8 (S)94.4 70-130
LCS-V35084 LCSD-V35084Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
46.1 11512048.040.0µg/LAcetone 40-160 4.0 20.0
20.8 10410821.620.0µg/LBenzene 70-130 3.7 20.0
19.6 98.010320.520.0µg/LBromobenzene 70-130 4.4 20.0
22.2 11110821.620.0µg/LBromochloromethane 70-130 2.7 20.0
21.8 10911422.720.0µg/LBromodichloromethane 70-130 4.0 20.0
Page 3 of 6Date:07/10/2023 10:39 AM
Page 12 of 17
Quality Control Data
23-181-0021Report No:
Project Description:
Client ID:Withers & Ravenel
Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35085QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35084
LCS-V35084 LCSD-V35084Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.2 10611021.920.0µg/LBromoform 70-130 3.2 20.0
16.4 82.092.518.520.0µg/LBromomethane 60-140 12.0 20.0
19.6 98.010520.920.0µg/Ln-Butylbenzene 70-130 6.4 20.0
19.8 99.010621.120.0µg/Lsec-Butyl benzene 70-130 6.3 20.0
19.9 99.510420.820.0µg/Ltert-Butyl benzene 70-130 4.4 20.0
20.2 10110420.820.0µg/LCarbon Tetrachloride 70-130 2.9 20.0
20.8 10410721.420.0µg/LChlorobenzene 70-130 2.8 20.0
21.4 10710921.820.0µg/LChlorodibromomethane 70-130 1.8 20.0
19.4 97.011422.820.0µg/LChloroethane 60-140 16.1 20.0
21.0 10510921.820.0µg/LChloroform 70-130 3.7 20.0
17.7 88.510520.920.0µg/LChloromethane 60-140 16.5 20.0
20.4 10210721.420.0µg/L2-Chlorotoluene 70-130 4.7 20.0
20.0 10010420.720.0µg/L4-Chlorotoluene 70-130 3.4 20.0
20.2 10198.519.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.5 20.0
21.6 10810821.520.0µg/L1,2-Dibromoethane 70-130 0.4 20.0
22.6 11311523.020.0µg/LDibromomethane 70-130 1.7 20.0
19.9 99.510320.620.0µg/L1,2-Dichlorobenzene 70-130 3.4 20.0
19.7 98.510420.720.0µg/L1,3-Dichlorobenzene 70-130 4.9 20.0
19.5 97.510320.520.0µg/L1,4-Dichlorobenzene 70-130 5.0 20.0
20.0 10011723.320.0µg/LDichlorodifluoromethane 60-140 15.2 20.0
20.9 10510821.620.0µg/L1,1-Dichloroethane 70-130 3.2 20.0
21.9 11010921.820.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
19.9 99.510721.320.0µg/L1,1-Dichloroethene 70-130 6.7 20.0
21.2 10611122.120.0µg/Lcis-1,2-Dichloroethene 70-130 4.1 20.0
20.3 10210621.220.0µg/Ltrans-1,2-Dichloroethene 70-130 4.3 20.0
21.7 10911122.220.0µg/L1,2-Dichloropropane 70-130 2.2 20.0
Page 4 of 6Date:07/10/2023 10:39 AM
Page 13 of 17
Quality Control Data
23-181-0021Report No:
Project Description:
Client ID:Withers & Ravenel
Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35085QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35084
LCS-V35084 LCSD-V35084Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.1 10610721.320.0µg/L1,3-Dichloropropane 70-130 0.9 20.0
16.9 84.590.018.020.0µg/L2,2-Dichloropropane 70-130 6.3 20.0
20.8 10410821.620.0µg/L1,1-Dichloropropene 70-130 3.7 20.0
21.5 10811022.020.0µg/Lcis-1,3-Dichloropropene 70-130 2.2 20.0
22.0 11011122.220.0µg/Ltrans-1,3-Dichloropropene 70-130 0.9 20.0
489 97.8128640500µg/LEthanol 60-140 26.7*20.0
20.5 10310621.220.0µg/LEthylbenzene 70-130 3.3 20.0
18.9 94.510120.120.0µg/LHexachlorobutadiene 70-130 6.1 20.0
21.2 10610821.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.8 20.0
20.1 10110721.420.0µg/LIsopropylbenzene 70-130 6.2 20.0
19.9 99.510621.120.0µg/L4-Isopropyl toluene 70-130 5.8 20.0
20.6 10310521.020.0µg/L2-Hexanone 60-140 1.9 20.0
20.4 10210120.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.9 20.0
21.5 10811122.120.0µg/LMethylene Chloride 70-130 2.7 20.0
21.6 10810721.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.3 20.0
22.4 11211222.320.0µg/L4-Methyl-2-Pentanone 60-140 0.4 20.0
21.0 10599.519.920.0µg/LNaphthalene 70-130 5.3 20.0
20.2 10110721.420.0µg/Ln-Propylbenzene 70-130 5.7 20.0
21.1 10610921.720.0µg/LStyrene 70-130 2.8 20.0
20.5 10310821.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 4.7 20.0
19.8 99.098.519.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.5 20.0
20.2 10110420.820.0µg/LTetrachloroethene 70-130 2.9 20.0
21.3 10711122.220.0µg/LToluene 70-130 4.1 20.0
24.3 12210821.620.0µg/L1,2,3-Trichlorobenzene 70-130 11.7 20.0
20.2 10110220.320.0µg/L1,2,4-Trichlorobenzene 70-130 0.4 20.0
21.0 10510921.820.0µg/L1,1,1-Trichloroethane 70-130 3.7 20.0
Page 5 of 6* QC Fail Date:07/10/2023 10:39 AM
Page 14 of 17
Quality Control Data
23-181-0021Report No:
Project Description:
Client ID:Withers & Ravenel
Sam Puckett
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35085QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35084
LCS-V35084 LCSD-V35084Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.8 11411422.720.0µg/L1,1,2-Trichloroethane 70-130 0.4 20.0
21.0 10511122.220.0µg/LTrichloroethene 70-130 5.5 20.0
19.7 98.511522.920.0µg/LTrichlorofluoromethane 60-140 15.0 20.0
21.1 10610721.420.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0
20.0 10010521.020.0µg/L1,2,4-Trimethylbenzene 70-130 4.8 20.0
20.1 10110621.220.0µg/L1,3,5-Trimethylbenzene 70-130 5.3 20.0
20.4 10294.518.920.0µg/LVinyl Acetate 60-140 7.6 20.0
18.8 94.011122.220.0µg/LVinyl Chloride 60-140 16.5 20.0
44.1 11011546.040.0µg/Lm,p-Xylene 70-130 4.2 20.0
20.9 10510921.820.0µg/Lo-Xylene 70-130 4.2 20.0
99.41014-Bromofluorobenzene (S)70-130
95.494.8Dibromofluoromethane (S)70-130
1031011,2-Dichloroethane - d4 (S)70-130
95.294.6Toluene-d8 (S)70-130
Page 6 of 6Date:07/10/2023 10:39 AM
Page 15 of 17
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-181-0021
Withers & Ravenel
01221
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:06/30/2023 14:53:55
Special precautions or instructions included?
Comments:
Page 16 of 17
Page 17 of 17
APPENDIX B
FIELD NOTES & PHOTOGRAPHIC RECORD
PHOTO 1
MW‐2D
PHOTO 2
MW‐3R
PHOTO 3
MW‐4
PHOTO 4
MW‐4D
PHOTO 5
MW‐5
PHOTO 6
MW‐7
PHOTO 7
MW‐8
PHOTO 8
MW‐9
APPENDIX C
GENERAL STANDARD OPERATING PROCEDURES
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Soil Sampling, Soil Boring and Monitor Well Installation, Well Development
Soil borings are installed utilizing a stainless-steel hand auger, direct-push hydraulic drill or auger rotary
drill using either a macro core™ sampler, hollow stem augers, or air rotary roller cone bit. Soil borings are
typically sampled at discrete intervals from the bucket of a clean stainless steel hand auger, direct push
stainless steel sampler with acetate sleeve, or a split barrel sampler. When appropriate, soil samples may
be collected from drill cuttings associated with the boring or well installation.
Monitor wells are constructed within select soil borings of one, two, or four-inch inside diameter PVC
casing and machine slotted screen in accordance with NCAC Title 15A, Subchapter 02C (Well
Construction Standards, Criteria and Standards Applicable to Water Supply and Certain Other Wells).
Clean-washed “#2 Torpedo Sand” is typically utilized to fill the boring annulus surrounding the well
screen, extending to a minimum of 1-foot above the well screen. A minimum 1-foot thick bentonite clay
seal is emplaced above the sand pack and hydrated. Neat cement grout is placed in the remaining annulus
space from the upper portion of the bentonite seal to within 1-foot of surface grade. In coastal plain areas
where shallow groundwater is encountered, a variance to construction standards may be employed to
ensure the upper portion of the well screen intersects the upper aquifer surface. Wellheads may be
completed with either concrete-set flush mounted traffic-bearing steel skirted manholes with bolt down
covers or steel above-ground “stick-up” well protectors set in a concrete pad. The monitoring wells are
secured with locking caps. Temporary wells or piezometers may be completed with the PVC riser cut at
or above grade, and are abandoned within 24-hours of their installation.
Wells may be developed using a bailer, electric submersible pump, pneumatic pump, or peristaltic pump,
dependent upon site conditions. When wells are developed by the driller, they may be developed with
any of the methods outlined above, in addition to air or water injection. Soil boring logs and well
construction details are typically prepared for presentation in a report appendix. Borings completed in
bedrock may be drilled using air rotary, coring, or sonic drilling methods.
Groundwater Depth to Water Measurements
Groundwater level measurements are typically obtained using an electronic water level indicator which
registers a tone and/or illuminated light when the probe contacts groundwater. Depth to groundwater
measurements are obtained by lowering the probe attached to a cable usually marked in 0.01 foot
intervals into the well until the probe of the meter intersects the water surface. The measurement from
the top of the riser pipe or top of casing (TOC) to the water level is recorded to the nearest 0.01 foot. The
electronic water level indicator probe and exposed probe cable is decontaminated between measurement
locations.
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Free Product Level Measurements
Light Non-Aqueous Phase Liquid (LNAPL) or “free product” present on the water table is measured using
an electronic oil/water interface probe. The interface probe has both an audible and illuminating light
that indicate when a liquid level is encountered. The oil/water interface probe registers a solid tone and
solidly lit light when LNAPL petroleum product is encountered and a beeping tone flashing light when
groundwater is encountered. Depth to LNAPL measurements are obtained by lowering the probe
attached to a cable marked in 0.01 foot intervals into the well until the probe of the meter intersects the
product or groundwater. The measurements from the top of the riser pipe or TOC to the liquid level are
recorded to the nearest 0.01 foot. The thickness of LNAPL is calculated by subtracting the depth to
LNAPL measurement from the depth to groundwater measurement. The electronic interface probe is
decontaminated between measurement locations.
Soil Sampling and Field Screening
Soil sampling is performed in general accordance with ASTM: 1586-84 where applicable. Sampling
procedures are followed to protect the chemical integrity of the soil samples and minimize the potential
for cross contamination between sample locations, including discarding of the exterior of the sample
which contacts the auger bucket, acetate sleeve, or split barrel sampler, the use of stainless steel sampling
equipment, and the thorough decontamination of sampling apparatus prior to use and between sample
locations.
Soil samples retained as a part of excavation or other intrusive “digging” activities may be collected from
the bucket of excavation equipment or using a hand shovel, if appropriate. Care to collect soil samples
from excavation equipment includes retrieving native soil from material that has not made contact with
the excavating equipment. Samples are collected in sealable bags or by directly filling sample containers
as described above.
Sampling is performed using new, disposable nitrile gloves for each sample location to ensure sample
integrity and minimize the potential for cross contamination or field personnel exposure to contaminants.
Sampling equipment such as hand auger extensions and buckets, direct push samplers, split spoons or
shovels, are decontaminated prior to their use in the collection of samples.
Samples are placed within laboratory grade sample containers provided by the laboratory to which the
samples are submitted, labeled, sealed, and placed in an ice filled cooler. An aliquot of the sample is
typically placed in a clean sealable bag and allowed to reach ambient air temperature for future screening
of volatile vapor content with a photoionization detector (PID), flame-ionization detector (FID) or other
portable screening device.
Screening of samples with a PID, FID or other field screening device is performed in accordance with
device manufacturer specifications for screening, following calibration of the instrument based on
manufacturer recommended procedures.
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Groundwater Sampling
Groundwater samples are generally collected using one of three standard methods – through the use of a
dedicated, disposable bailer, a peristaltic pump or submersible electric pump.
When sampling with a bailer, a minimum of three well volumes of groundwater are extracted from the
well as a means of purging, unless the well is purged to a “dry” state prior to the removal of three volumes
of water. Prior to collection of the groundwater sample with the bailer, the water level is allowed to
recover to within 80% of the original level measured prior to purging.
When sampling with a peristaltic or submersible electric pump, polyethylene (PE) tubing (or equivalent) is
emplaced into the screened section of the monitoring well, and the pump is used to extract water through
the tubing. When using the either of these methods, general water quality measurements including but
not limited to pH, temperature, dissolved oxygen (DO), oxygen reductive potential (ORP), specific
conductivity and turbidity may be used as methods for determining when an adequate purge of the well
has been conducted. When water quality parameters are measured, the resulting data are included in
well purge forms or field notes specific to each site and sampling point.
Following the purging of three well volumes of groundwater (in the case of the bailed well) or stability of
monitored measurements (in the case of the peristaltic or submersible electric pump), the groundwater
sample(s) are introduced directly into sample containers provided by the laboratory to which samples are
ultimately submitted for analysis. Any samples requiring chemical preservation are contained in pre-
preserved container(s) provided by the laboratory.
Sampling is performed using new, disposable nitrile gloves for each sample location to ensure sample
integrity and minimize the potential for cross contamination of samples or field personnel exposure to
contaminants.
Water Supply Well Sampling
Sampling of water supply wells is accomplished through the collection of a representative sample from an
in-line water tap or other point accessible for sampling. Where possible, the sample is collected from a
point prior to any filtration or point of entry (POE) system which might be installed on a well. In some
cases, samples will be collected from both pre and post-POE locations. Prior to the collection of samples
through an in-place sampling point, the tap or sampling port is cleaned with an Alconox® and deionized
water solution, rinsed with deionized water, and again with an isopropyl alcohol (IPA) rinse.
In the case of active supply wells (e.g., a well with a useable well pump with an active power supply), the
well pump is energized and allowed to run for a minimum of ten (10) minutes time, after which a sample is
contained in laboratory grade sample containers as described in the previous section. Water quality
parameters may be (but are not necessarily) measured in association with the well purging.
Supply wells without active power supplies are not generally sampled, as the well seal cannot be
compromised by individuals not certified as a well contractor. However, in the case of a well with no
power supply or pump installed, samples could be obtained through the use of a bailer, peristaltic pump or
electric submersible pump.
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Decontamination Procedures
Decontamination procedures employed in the performance of field activities will vary dependent upon
the method(s) of sampling performed at any site, but will generally include the following:
• Remove excess soil/sludge from any sampling equipment as needed,
• Wash and scrub the equipment with a phosphate-free detergent such as Alconox® or Liquinox® in a
contaminant-free tap water solution. Use a brush to remove particulate matter and surface films as
necessary,
• Rinse thoroughly with tap water,
• Rinse thoroughly with analyte-free water (deionized water),
Rinse thoroughly with isopropyl alcohol,
• Allow the equipment to air dry,
• Prevent inadvertent contamination during storage and transport (accomplished through storage of
equipment in foil or plastic bags/sheeting).
In the case of disposable bailers and tubing utilized for the purging and sampling of wells, these items may
be decontaminated prior to their disposal. In general, no decontamination of these items is necessary
prior to their use in sampling.