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HomeMy WebLinkAboutRA-2743_17375_CA_HRE_20230710_Request_PearceClarkProp_WSW4Division of Waste Management UST Section MEMORANDUM To: From: Date: Subject: Dave Lilley Linda Blalock August 2, 2023 Health Risk Evaluation Request Related to UST Incident #17375/Country Crossroads Grocery Wendell/Wake County Please perform DHealth Risk Evaluation for the following water supply well. Recent lab report is attached. I'm requesting the HRE for :6:4. Well ID: :SW-4 (Results begin on page 4 of 54) Well Address: 1524 Eagle Rock Road, Wendell Owner's Name/Address: Pearce and Clark Properties, LLC 1532 Eagle Rock Rd. Wendell, NC 27591 Thank you for your assistance. If you need any additional information, please feel free to email me linda.blalock@deq.nc.gov . Attachment FF0DUN3HWHUPDQQ  39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 July 31, 2023 Sean O’Neil CATLIN Engineers & Scientists 1044 Washington Street Raleigh, NC 27605 Project Location: Wendell, NC Client Job Number: Project Number: 221074.01 Laboratory Work Order Number: 23G3086 Enclosed are results of analyses for samples as received by the laboratory on July 22, 2023. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kaitlyn A. Feliciano Project Manager Page 1 of 54 Table of Contents Table of Contents Sample Summary 4 Hits Only Report 5 Case Narrative 9 Sample Results 10 23G3086-01 10 23G3086-02 12 23G3086-03 14 23G3086-04 16 23G3086-05 18 23G3086-06 20 23G3086-07 22 23G3086-08 24 23G3086-09 26 23G3086-10 28 23G3086-11 30 23G3086-12 32 23G3086-13 34 23G3086-14 36 23G3086-15 38 23G3086-16 40 Sample Preparation Information 42 QC Data 43 Volatile Organic Compounds by GC/MS 43 B347066 43 Flag/Qualifier Summary 47 Page 2 of 54 Table of Contents Table of Contents (continued) Certifications 48 Chain of Custody/Sample Receipt 50 Page 3 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL SUMMARY 7/31/2023 CATLIN Engineers & Scientists 1044 Washington Street Raleigh, NC 27605 ATTN: Sean O’Neil 221074.01 23G3086 The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. PROJECT LOCATION: PURCHASE ORDER NUMBER: PROJECT NUMBER: REPORT DATE: WORK ORDER NUMBER: FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB Wendell, NC 210623-2 MW-1R 23G3086-01 Ground Water SM21-23 6200B MW-2 23G3086-02 Ground Water SM21-23 6200B MW-4 23G3086-03 Ground Water SM21-23 6200B MW-5R 23G3086-04 Ground Water SM21-23 6200B MW-6 23G3086-05 Ground Water SM21-23 6200B MW-7 23G3086-06 Ground Water SM21-23 6200B MW-8 23G3086-07 Ground Water SM21-23 6200B MW-9 23G3086-08 Ground Water SM21-23 6200B MW-10 23G3086-09 Ground Water SM21-23 6200B MW-11 23G3086-10 Ground Water SM21-23 6200B MW-12 23G3086-11 Ground Water SM21-23 6200B WSW-3 23G3086-12 Ground Water SM21-23 6200B WSW-4 23G3086-13 Ground Water SM21-23 6200B WSW-11 23G3086-14 Ground Water SM21-23 6200B FB 23G3086-15 Field Blank SM21-23 6200B TB 23G3086-16 Trip Blank Water SM21-23 6200B [TOC_1]Sample Summary[TOC] Page 4 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 [TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY Client ID:Lab ID:23G3086-02MW-2 No Results Detected Client ID:Lab ID:23G3086-04MW-5R No Results Detected Client ID:Lab ID:23G3086-05MW-6 No Results Detected Client ID:Lab ID:23G3086-12WSW-3 No Results Detected Client ID:Lab ID:23G3086-14WSW-11 No Results Detected Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary section of this report. Users must review this report in its entirety to determine data usability and assessment. Page 5 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 EXECUTIVE SUMMARY Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-01MW-1R DL 1,2,4-Trimethylbenzene 730 100 g/L SM21-23 6200B40 1,2-Dibromoethane (EDB)74 100 g/L SM21-23 6200BJ32 1,3,5-Trimethylbenzene 270 100 g/L SM21-23 6200B30 Benzene 5700 100 g/L SM21-23 6200B37 Ethylbenzene 1100 100 g/L SM21-23 6200B44 Isopropylbenzene (Cumene)80 100 g/L SM21-23 6200BJ30 m+p Xylene 3000 200 g/L SM21-23 6200B98 Naphthalene 340 100 g/L SM21-23 6200B76 n-Propylbenzene 74 100 g/L SM21-23 6200BJ25 o-Xylene 1500 100 g/L SM21-23 6200B49 Toluene 11000 100 g/L SM21-23 6200B45 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-03MW-4 DL 1,2,4-Trimethylbenzene 1100 20 g/L SM21-23 6200B8.0 1,3,5-Trimethylbenzene 380 20 g/L SM21-23 6200B6.0 2-Butanone (MEK)140 200 g/L SM21-23 6200BJ67 Acetone 130 2000 g/L SM21-23 6200BJ80 Benzene 350 20 g/L SM21-23 6200B7.4 Diisopropyl Ether (DIPE)16 20 g/L SM21-23 6200BJ8.1 Ethylbenzene 850 20 g/L SM21-23 6200B8.8 Isopropylbenzene (Cumene)130 20 g/L SM21-23 6200B6.0 m+p Xylene 4300 40 g/L SM21-23 6200B20 Methyl tert-Butyl Ether (MTBE)47 20 g/L SM21-23 6200B6.8 Naphthalene 210 20 g/L SM21-23 6200B15 n-Butylbenzene 44 20 g/L SM21-23 6200B6.0 n-Propylbenzene 110 20 g/L SM21-23 6200B5.0 o-Xylene 1900 20 g/L SM21-23 6200B9.7 p-Isopropyltoluene (p-Cymene)38 20 g/L SM21-23 6200B5.1 sec-Butylbenzene 17 20 g/L SM21-23 6200BJ5.1 Toluene 890 20 g/L SM21-23 6200B8.9 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-06MW-7 DL 1,2,4-Trimethylbenzene 1.2 0.50 g/L SM21-23 6200B0.20 1,3,5-Trimethylbenzene 1.8 0.50 g/L SM21-23 6200B0.15 Isopropylbenzene (Cumene)0.64 0.50 g/L SM21-23 6200B0.15 n-Butylbenzene 0.32 0.50 g/L SM21-23 6200BJ0.15 p-Isopropyltoluene (p-Cymene)0.40 0.50 g/L SM21-23 6200BJ0.13 sec-Butylbenzene 0.32 0.50 g/L SM21-23 6200BJ0.13 Page 6 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-07MW-8 DL 1,2,4-Trimethylbenzene 54 0.50 g/L SM21-23 6200B0.20 1,3,5-Trimethylbenzene 27 0.50 g/L SM21-23 6200B0.15 Acetone 5.7 50 g/L SM21-23 6200BJ2.0 Isopropylbenzene (Cumene)9.4 0.50 g/L SM21-23 6200B0.15 m+p Xylene 3.9 1.0 g/L SM21-23 6200B0.49 Naphthalene 4.5 0.50 g/L SM21-23 6200B0.38 n-Butylbenzene 1.5 0.50 g/L SM21-23 6200B0.15 n-Propylbenzene 0.17 0.50 g/L SM21-23 6200BJ0.12 o-Xylene 18 0.50 g/L SM21-23 6200B0.24 p-Isopropyltoluene (p-Cymene)44 0.50 g/L SM21-23 6200B0.13 sec-Butylbenzene 1.2 0.50 g/L SM21-23 6200B0.13 tert-Butylbenzene 0.33 0.50 g/L SM21-23 6200BJ0.14 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-08MW-9 DL 1,2,4-Trimethylbenzene 240 1.0 g/L SM21-23 6200B0.40 1,2-Dichloropropane 1.9 1.0 g/L SM21-23 6200B0.39 1,3,5-Trimethylbenzene 110 1.0 g/L SM21-23 6200B0.30 Acetone 5.9 100 g/L SM21-23 6200BJ4.0 Benzene 1.0 1.0 g/L SM21-23 6200B0.37 Ethylbenzene 5.0 1.0 g/L SM21-23 6200B0.44 Isopropylbenzene (Cumene)37 1.0 g/L SM21-23 6200B0.30 m+p Xylene 130 2.0 g/L SM21-23 6200B0.98 Naphthalene 26 1.0 g/L SM21-23 6200B0.76 n-Butylbenzene 5.5 1.0 g/L SM21-23 6200B0.30 n-Propylbenzene 3.3 1.0 g/L SM21-23 6200B0.25 o-Xylene 110 1.0 g/L SM21-23 6200B0.49 p-Isopropyltoluene (p-Cymene)14 1.0 g/L SM21-23 6200B0.25 sec-Butylbenzene 3.2 1.0 g/L SM21-23 6200B0.25 tert-Butylbenzene 1.1 1.0 g/L SM21-23 6200B0.28 Toluene 1.3 1.0 g/L SM21-23 6200B0.45 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-09MW-10 DL 1,2,4-Trimethylbenzene 430 2.5 g/L SM21-23 6200B0.99 1,2-Dichloropropane 3.5 2.5 g/L SM21-23 6200B0.97 1,3,5-Trimethylbenzene 85 2.5 g/L SM21-23 6200B0.75 Benzene 130 2.5 g/L SM21-23 6200B0.92 Diisopropyl Ether (DIPE)9.2 2.5 g/L SM21-23 6200B1.0 Ethylbenzene 330 2.5 g/L SM21-23 6200B1.1 Isopropylbenzene (Cumene)66 2.5 g/L SM21-23 6200B0.76 m+p Xylene 1000 5.0 g/L SM21-23 6200B2.5 Methyl tert-Butyl Ether (MTBE)44 2.5 g/L SM21-23 6200B0.85 Naphthalene 140 2.5 g/L SM21-23 6200B1.9 n-Butylbenzene 8.8 2.5 g/L SM21-23 6200B0.75 n-Propylbenzene 54 2.5 g/L SM21-23 6200B0.62 o-Xylene 230 2.5 g/L SM21-23 6200B1.2 p-Isopropyltoluene (p-Cymene)9.0 2.5 g/L SM21-23 6200B0.63 sec-Butylbenzene 5.3 2.5 g/L SM21-23 6200B0.63 tert-Butylbenzene 1.8 2.5 g/L SM21-23 6200BJ0.71 Toluene 58 2.5 g/L SM21-23 6200B1.1 Page 7 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-10MW-11 DL 1,2,4-Trimethylbenzene 63 0.50 g/L SM21-23 6200B0.20 1,3,5-Trimethylbenzene 31 0.50 g/L SM21-23 6200B0.15 Acetone 4.1 50 g/L SM21-23 6200BJ2.0 Isopropylbenzene (Cumene)9.4 0.50 g/L SM21-23 6200B0.15 m+p Xylene 1.9 1.0 g/L SM21-23 6200B0.49 Naphthalene 4.4 0.50 g/L SM21-23 6200B0.38 n-Butylbenzene 1.6 0.50 g/L SM21-23 6200B0.15 o-Xylene 13 0.50 g/L SM21-23 6200B0.24 p-Isopropyltoluene (p-Cymene)3.1 0.50 g/L SM21-23 6200B0.13 sec-Butylbenzene 1.2 0.50 g/L SM21-23 6200B0.13 tert-Butylbenzene 0.34 0.50 g/L SM21-23 6200BJ0.14 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-11MW-12 DL 1,2,4-Trimethylbenzene 30 0.50 g/L SM21-23 6200B0.20 1,3,5-Trimethylbenzene 15 0.50 g/L SM21-23 6200B0.15 Benzene 1.5 0.50 g/L SM21-23 6200B0.18 Isopropylbenzene (Cumene)5.8 0.50 g/L SM21-23 6200B0.15 m+p Xylene 0.71 1.0 g/L SM21-23 6200BJ0.49 Naphthalene 3.9 0.50 g/L SM21-23 6200B0.38 n-Butylbenzene 0.69 0.50 g/L SM21-23 6200B0.15 o-Xylene 22 0.50 g/L SM21-23 6200B0.24 p-Isopropyltoluene (p-Cymene)2.2 0.50 g/L SM21-23 6200B0.13 sec-Butylbenzene 0.68 0.50 g/L SM21-23 6200B0.13 Styrene 0.70 0.50 g/L SM21-23 6200B0.15 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-13WSW-4 DL Chloroform 0.25 0.50 g/L SM21-23 6200BJ0.14 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-15FB DL Acetone 4.0 50 g/L SM21-23 6200BJ2.0 Client ID:Lab ID: Analyte Results/Qual RL Units Method 23G3086-16TB DL Chloroform 0.18 0.50 g/L SM21-23 6200BJ0.14 Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary section of this report. Users must review this report in its entirety to determine data usability and assessment. Page 8 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method 6200B elevated reporting limits for samples 23G3086+01,03,08+09 due to high concentrations of target compounds. [TOC_1]Case Narrative[TOC] SM21-23 6200B Qualifications: Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. Analyte & Samples(s) Qualified: L-07A Vinyl Acetate B347066-BSD1 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: R-05 Vinyl Acetate 23G3086-01[MW-1R], 23G3086-02[MW-2], 23G3086-03[MW-4], 23G3086-04[MW-5R], 23G3086-05[MW-6], 23G3086-06[MW-7], 23G3086-07[MW-8], 23G3086-08[MW-9], 23G3086-09[MW-10], 23G3086-10[MW-11], 23G3086-11[MW-12], 23G3086-12[WSW-3], 23G3086-13[WSW-4], 23G3086-14[WSW-11], 23G3086-15[FB], 23G3086-16[TB], B347066-BLK1, B347066-BS1, B347066-BSD1 Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: RL-11 23G3086-01[MW-1R], 23G3086-03[MW-4], 23G3086-08[MW-9], 23G3086-09[MW-10] The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Tod E. Kopyscinski Laboratory Director Page 9 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-01 Field Sample #: MW-1R Sample Matrix: Ground Water Sampled: 7/20/2023 14:38 [TOC_2]23G3086-01[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS ND 10000 7/28/23 8:00 MFFg/L400 7/26/23SM21-23 6200B200Acetone 5700 100 7/28/23 8:00 MFFg/L37 7/26/23SM21-23 6200B200Benzene ND 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B200Bromobenzene ND 100 7/28/23 8:00 MFFg/L57 7/26/23SM21-23 6200B200Bromochloromethane ND 100 7/28/23 8:00 MFFg/L32 7/26/23SM21-23 6200B200Bromodichloromethane ND 100 7/28/23 8:00 MFFg/L82 7/26/23SM21-23 6200B200Bromoform ND 400 7/28/23 8:00 MFFg/L260 7/26/23SM21-23 6200B200Bromomethane ND 1000 7/28/23 8:00 MFFg/L340 7/26/23SM21-23 6200B2002-Butanone (MEK) ND 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B200n-Butylbenzene ND 100 7/28/23 8:00 MFFg/L25 7/26/23SM21-23 6200B200sec-Butylbenzene ND 100 7/28/23 8:00 MFFg/L28 7/26/23SM21-23 6200B200tert-Butylbenzene ND 100 7/28/23 8:00 MFFg/L33 7/26/23SM21-23 6200B200Carbon Tetrachloride ND 100 7/28/23 8:00 MFFg/L24 7/26/23SM21-23 6200B200Chlorobenzene ND 10000 7/28/23 8:00 MFFg/L4100 7/26/23SM21-23 6200B200Ethanol ND 100 7/28/23 8:00 MFFg/L40 7/26/23SM21-23 6200B200Chlorodibromomethane ND 100 7/28/23 8:00 MFFg/L68 7/26/23SM21-23 6200B200Chloroethane ND 100 7/28/23 8:00 MFFg/L28 7/26/23SM21-23 6200B200Chloroform ND 120 7/28/23 8:00 MFFg/L100 7/26/23SM21-23 6200B200Chloromethane ND 100 7/28/23 8:00 MFFg/L31 7/26/23SM21-23 6200B2002-Chlorotoluene ND 100 7/28/23 8:00 MFFg/L31 7/26/23SM21-23 6200B2004-Chlorotoluene 74 100 7/28/23 8:00 MFFg/L32 7/26/23SM21-23 6200B200J1,2-Dibromoethane (EDB) ND 100 7/28/23 8:00 MFFg/L26 7/26/23SM21-23 6200B2001,2-Dichlorobenzene ND 100 7/28/23 8:00 MFFg/L27 7/26/23SM21-23 6200B2001,3-Dichlorobenzene ND 100 7/28/23 8:00 MFFg/L26 7/26/23SM21-23 6200B2001,4-Dichlorobenzene ND 100 7/28/23 8:00 MFFg/L32 7/26/23SM21-23 6200B200Dichlorodifluoromethane (Freon 12) ND 100 7/28/23 8:00 MFFg/L27 7/26/23SM21-23 6200B2001,1-Dichloroethane ND 100 7/28/23 8:00 MFFg/L61 7/26/23SM21-23 6200B2001,2-Dichloroethane ND 100 7/28/23 8:00 MFFg/L28 7/26/23SM21-23 6200B2001,1-Dichloroethylene ND 100 7/28/23 8:00 MFFg/L28 7/26/23SM21-23 6200B200cis-1,2-Dichloroethylene ND 100 7/28/23 8:00 MFFg/L34 7/26/23SM21-23 6200B200trans-1,2-Dichloroethylene ND 100 7/28/23 8:00 MFFg/L39 7/26/23SM21-23 6200B2001,2-Dichloropropane ND 100 7/28/23 8:00 MFFg/L23 7/26/23SM21-23 6200B2001,3-Dichloropropane ND 100 7/28/23 8:00 MFFg/L70 7/26/23SM21-23 6200B2002,2-Dichloropropane ND 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B2001,1-Dichloropropene ND 100 7/28/23 8:00 MFFg/L33 7/26/23SM21-23 6200B200cis-1,3-Dichloropropene ND 100 7/28/23 8:00 MFFg/L28 7/26/23SM21-23 6200B200trans-1,3-Dichloropropene ND 100 7/28/23 8:00 MFFg/L40 7/26/23SM21-23 6200B200Diisopropyl Ether (DIPE) 1100 100 7/28/23 8:00 MFFg/L44 7/26/23SM21-23 6200B200Ethylbenzene ND 1000 7/28/23 8:00 MFFg/L240 7/26/23SM21-23 6200B2002-Hexanone (MBK) 80 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B200JIsopropylbenzene (Cumene) ND 100 7/28/23 8:00 MFFg/L25 7/26/23SM21-23 6200B200p-Isopropyltoluene (p-Cymene) ND 100 7/28/23 8:00 MFFg/L34 7/26/23SM21-23 6200B200Methyl tert-Butyl Ether (MTBE) ND 1000 7/28/23 8:00 MFFg/L35 7/26/23SM21-23 6200B200Methylene Chloride ND 1000 7/28/23 8:00 MFFg/L260 7/26/23SM21-23 6200B2004-Methyl-2-pentanone (MIBK) [TOC_1]Sample Results[TOC] Page 10 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-01 Field Sample #: MW-1R Sample Matrix: Ground Water Sampled: 7/20/2023 14:38 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 340 100 7/28/23 8:00 MFFg/L76 7/26/23SM21-23 6200B200Naphthalene 74 100 7/28/23 8:00 MFFg/L25 7/26/23SM21-23 6200B200Jn-Propylbenzene ND 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B200Styrene ND 100 7/28/23 8:00 MFFg/L27 7/26/23SM21-23 6200B2001,1,2,2-Tetrachloroethane ND 100 7/28/23 8:00 MFFg/L34 7/26/23SM21-23 6200B200Tetrachloroethylene 11000 100 7/28/23 8:00 MFFg/L45 7/26/23SM21-23 6200B200Toluene ND 200 7/28/23 8:00 MFFg/L68 7/26/23SM21-23 6200B2001,2,3-Trichlorobenzene ND 200 7/28/23 8:00 MFFg/L60 7/26/23SM21-23 6200B2001,2,4-Trichlorobenzene ND 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B2001,1,1-Trichloroethane ND 100 7/28/23 8:00 MFFg/L38 7/26/23SM21-23 6200B2001,1,2-Trichloroethane ND 100 7/28/23 8:00 MFFg/L35 7/26/23SM21-23 6200B200Trichloroethylene ND 100 7/28/23 8:00 MFFg/L31 7/26/23SM21-23 6200B200Trichlorofluoromethane (Freon 11) ND 100 7/28/23 8:00 MFFg/L55 7/26/23SM21-23 6200B2001,2,3-Trichloropropane 730 100 7/28/23 8:00 MFFg/L40 7/26/23SM21-23 6200B2001,2,4-Trimethylbenzene 270 100 7/28/23 8:00 MFFg/L30 7/26/23SM21-23 6200B2001,3,5-Trimethylbenzene ND 4000 7/28/23 8:00 MFFg/L330 7/26/23SM21-23 6200B200R-05Vinyl Acetate ND 100 7/28/23 8:00 MFFg/L47 7/26/23SM21-23 6200B200Vinyl Chloride 3000 200 7/28/23 8:00 MFFg/L98 7/26/23SM21-23 6200B200m+p Xylene 1500 100 7/28/23 8:00 MFFg/L49 7/26/23SM21-23 6200B200o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 94.6 7/28/23 8:0070-130 Toluene-d8 98.9 7/28/23 8:0070-130 4-Bromofluorobenzene 88.4 7/28/23 8:0070-130 Page 11 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-02 Field Sample #: MW-2 Sample Matrix: Ground Water Sampled: 7/20/2023 09:23 [TOC_2]23G3086-02[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 4:27 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 4:27 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 4:27 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 4:27 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 4:27 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 4:27 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 4:27 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 4:27 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 4:27 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 4:27 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 4:27 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 4:27 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 4:27 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 4:27 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 4:27 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 4:27 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 4:27 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 4:27 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 4:27 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 4:27 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 4:27 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 4:27 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 4:27 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 4:27 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 4:27 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 4:27 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 4:27 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 4:27 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 4:27 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 4:27 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 4:27 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 12 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-02 Field Sample #: MW-2 Sample Matrix: Ground Water Sampled: 7/20/2023 09:23 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 4:27 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 4:27 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 4:27 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 4:27 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 4:27 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 4:27 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 4:27 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 4:27 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 4:27 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 4:27 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 4:27 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 4:27 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 4:27 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 4:27 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 4:27 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 4:27 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.0 7/28/23 4:2770-130 Toluene-d8 99.0 7/28/23 4:2770-130 4-Bromofluorobenzene 87.8 7/28/23 4:2770-130 Page 13 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-03 Field Sample #: MW-4 Sample Matrix: Ground Water Sampled: 7/20/2023 14:24 [TOC_2]23G3086-03[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 130 2000 7/28/23 8:27 MFFg/L80 7/26/23SM21-23 6200B40JAcetone 350 20 7/28/23 8:27 MFFg/L7.4 7/26/23SM21-23 6200B40Benzene ND 20 7/28/23 8:27 MFFg/L5.9 7/26/23SM21-23 6200B40Bromobenzene ND 20 7/28/23 8:27 MFFg/L11 7/26/23SM21-23 6200B40Bromochloromethane ND 20 7/28/23 8:27 MFFg/L6.3 7/26/23SM21-23 6200B40Bromodichloromethane ND 20 7/28/23 8:27 MFFg/L16 7/26/23SM21-23 6200B40Bromoform ND 80 7/28/23 8:27 MFFg/L53 7/26/23SM21-23 6200B40Bromomethane 140 200 7/28/23 8:27 MFFg/L67 7/26/23SM21-23 6200B40J2-Butanone (MEK) 44 20 7/28/23 8:27 MFFg/L6.0 7/26/23SM21-23 6200B40n-Butylbenzene 17 20 7/28/23 8:27 MFFg/L5.1 7/26/23SM21-23 6200B40Jsec-Butylbenzene ND 20 7/28/23 8:27 MFFg/L5.7 7/26/23SM21-23 6200B40tert-Butylbenzene ND 20 7/28/23 8:27 MFFg/L6.5 7/26/23SM21-23 6200B40Carbon Tetrachloride ND 20 7/28/23 8:27 MFFg/L4.8 7/26/23SM21-23 6200B40Chlorobenzene ND 2000 7/28/23 8:27 MFFg/L810 7/26/23SM21-23 6200B40Ethanol ND 20 7/28/23 8:27 MFFg/L8.0 7/26/23SM21-23 6200B40Chlorodibromomethane ND 20 7/28/23 8:27 MFFg/L14 7/26/23SM21-23 6200B40Chloroethane ND 20 7/28/23 8:27 MFFg/L5.6 7/26/23SM21-23 6200B40Chloroform ND 24 7/28/23 8:27 MFFg/L20 7/26/23SM21-23 6200B40Chloromethane ND 20 7/28/23 8:27 MFFg/L6.2 7/26/23SM21-23 6200B402-Chlorotoluene ND 20 7/28/23 8:27 MFFg/L6.2 7/26/23SM21-23 6200B404-Chlorotoluene ND 20 7/28/23 8:27 MFFg/L6.4 7/26/23SM21-23 6200B401,2-Dibromoethane (EDB) ND 20 7/28/23 8:27 MFFg/L5.2 7/26/23SM21-23 6200B401,2-Dichlorobenzene ND 20 7/28/23 8:27 MFFg/L5.5 7/26/23SM21-23 6200B401,3-Dichlorobenzene ND 20 7/28/23 8:27 MFFg/L5.1 7/26/23SM21-23 6200B401,4-Dichlorobenzene ND 20 7/28/23 8:27 MFFg/L6.4 7/26/23SM21-23 6200B40Dichlorodifluoromethane (Freon 12) ND 20 7/28/23 8:27 MFFg/L5.5 7/26/23SM21-23 6200B401,1-Dichloroethane ND 20 7/28/23 8:27 MFFg/L12 7/26/23SM21-23 6200B401,2-Dichloroethane ND 20 7/28/23 8:27 MFFg/L5.6 7/26/23SM21-23 6200B401,1-Dichloroethylene ND 20 7/28/23 8:27 MFFg/L5.6 7/26/23SM21-23 6200B40cis-1,2-Dichloroethylene ND 20 7/28/23 8:27 MFFg/L6.9 7/26/23SM21-23 6200B40trans-1,2-Dichloroethylene ND 20 7/28/23 8:27 MFFg/L7.7 7/26/23SM21-23 6200B401,2-Dichloropropane ND 20 7/28/23 8:27 MFFg/L4.6 7/26/23SM21-23 6200B401,3-Dichloropropane ND 20 7/28/23 8:27 MFFg/L14 7/26/23SM21-23 6200B402,2-Dichloropropane ND 20 7/28/23 8:27 MFFg/L6.0 7/26/23SM21-23 6200B401,1-Dichloropropene ND 20 7/28/23 8:27 MFFg/L6.5 7/26/23SM21-23 6200B40cis-1,3-Dichloropropene ND 20 7/28/23 8:27 MFFg/L5.7 7/26/23SM21-23 6200B40trans-1,3-Dichloropropene 16 20 7/28/23 8:27 MFFg/L8.1 7/26/23SM21-23 6200B40JDiisopropyl Ether (DIPE) 850 20 7/28/23 8:27 MFFg/L8.8 7/26/23SM21-23 6200B40Ethylbenzene ND 200 7/28/23 8:27 MFFg/L48 7/26/23SM21-23 6200B402-Hexanone (MBK) 130 20 7/28/23 8:27 MFFg/L6.0 7/26/23SM21-23 6200B40Isopropylbenzene (Cumene) 38 20 7/28/23 8:27 MFFg/L5.1 7/26/23SM21-23 6200B40p-Isopropyltoluene (p-Cymene) 47 20 7/28/23 8:27 MFFg/L6.8 7/26/23SM21-23 6200B40Methyl tert-Butyl Ether (MTBE) ND 200 7/28/23 8:27 MFFg/L7.1 7/26/23SM21-23 6200B40Methylene Chloride ND 200 7/28/23 8:27 MFFg/L53 7/26/23SM21-23 6200B404-Methyl-2-pentanone (MIBK) Page 14 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-03 Field Sample #: MW-4 Sample Matrix: Ground Water Sampled: 7/20/2023 14:24 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 210 20 7/28/23 8:27 MFFg/L15 7/26/23SM21-23 6200B40Naphthalene 110 20 7/28/23 8:27 MFFg/L5.0 7/26/23SM21-23 6200B40n-Propylbenzene ND 20 7/28/23 8:27 MFFg/L6.0 7/26/23SM21-23 6200B40Styrene ND 20 7/28/23 8:27 MFFg/L5.5 7/26/23SM21-23 6200B401,1,2,2-Tetrachloroethane ND 20 7/28/23 8:27 MFFg/L6.7 7/26/23SM21-23 6200B40Tetrachloroethylene 890 20 7/28/23 8:27 MFFg/L8.9 7/26/23SM21-23 6200B40Toluene ND 40 7/28/23 8:27 MFFg/L14 7/26/23SM21-23 6200B401,2,3-Trichlorobenzene ND 40 7/28/23 8:27 MFFg/L12 7/26/23SM21-23 6200B401,2,4-Trichlorobenzene ND 20 7/28/23 8:27 MFFg/L6.0 7/26/23SM21-23 6200B401,1,1-Trichloroethane ND 20 7/28/23 8:27 MFFg/L7.6 7/26/23SM21-23 6200B401,1,2-Trichloroethane ND 20 7/28/23 8:27 MFFg/L7.0 7/26/23SM21-23 6200B40Trichloroethylene ND 20 7/28/23 8:27 MFFg/L6.2 7/26/23SM21-23 6200B40Trichlorofluoromethane (Freon 11) ND 20 7/28/23 8:27 MFFg/L11 7/26/23SM21-23 6200B401,2,3-Trichloropropane 1100 20 7/28/23 8:27 MFFg/L8.0 7/26/23SM21-23 6200B401,2,4-Trimethylbenzene 380 20 7/28/23 8:27 MFFg/L6.0 7/26/23SM21-23 6200B401,3,5-Trimethylbenzene ND 800 7/28/23 8:27 MFFg/L67 7/26/23SM21-23 6200B40R-05Vinyl Acetate ND 20 7/28/23 8:27 MFFg/L9.5 7/26/23SM21-23 6200B40Vinyl Chloride 4300 40 7/28/23 8:27 MFFg/L20 7/26/23SM21-23 6200B40m+p Xylene 1900 20 7/28/23 8:27 MFFg/L9.7 7/26/23SM21-23 6200B40o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 93.6 7/28/23 8:2770-130 Toluene-d8 99.2 7/28/23 8:2770-130 4-Bromofluorobenzene 89.8 7/28/23 8:2770-130 Page 15 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-04 Field Sample #: MW-5R Sample Matrix: Ground Water Sampled: 7/20/2023 09:55 [TOC_2]23G3086-04[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 4:54 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 4:54 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 4:54 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 4:54 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 4:54 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 4:54 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 4:54 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 4:54 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 4:54 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 4:54 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 4:54 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 4:54 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 4:54 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 4:54 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 4:54 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 4:54 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 4:54 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 4:54 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 4:54 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 4:54 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 4:54 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 4:54 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 4:54 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 4:54 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 4:54 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 4:54 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 4:54 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 4:54 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 4:54 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 4:54 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 4:54 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 16 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-04 Field Sample #: MW-5R Sample Matrix: Ground Water Sampled: 7/20/2023 09:55 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 4:54 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 4:54 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 4:54 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 4:54 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 4:54 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 4:54 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 4:54 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 4:54 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 4:54 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 4:54 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 4:54 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 4:54 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 4:54 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 4:54 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 4:54 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 4:54 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.9 7/28/23 4:5470-130 Toluene-d8 99.4 7/28/23 4:5470-130 4-Bromofluorobenzene 85.6 7/28/23 4:5470-130 Page 17 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-05 Field Sample #: MW-6 Sample Matrix: Ground Water Sampled: 7/20/2023 10:46 [TOC_2]23G3086-05[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 5:21 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 5:21 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 5:21 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 5:21 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 5:21 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 5:21 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 5:21 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 5:21 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 5:21 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 5:21 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 5:21 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 5:21 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 5:21 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 5:21 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 5:21 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 5:21 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 5:21 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 5:21 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 5:21 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 5:21 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 5:21 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 5:21 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 5:21 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 5:21 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 5:21 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 5:21 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 5:21 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 5:21 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 5:21 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 5:21 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 5:21 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 18 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-05 Field Sample #: MW-6 Sample Matrix: Ground Water Sampled: 7/20/2023 10:46 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 5:21 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 5:21 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 5:21 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 5:21 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 5:21 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 5:21 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 5:21 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 5:21 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 5:21 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 5:21 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 5:21 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 5:21 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 5:21 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 5:21 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 5:21 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 5:21 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 100 7/28/23 5:2170-130 Toluene-d8 98.9 7/28/23 5:2170-130 4-Bromofluorobenzene 86.9 7/28/23 5:2170-130 Page 19 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-06 Field Sample #: MW-7 Sample Matrix: Ground Water Sampled: 7/20/2023 09:01 [TOC_2]23G3086-06[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 5:47 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 5:47 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 5:47 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 5:47 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 5:47 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 5:47 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 5:47 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) 0.32 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B1Jn-Butylbenzene 0.32 0.50 7/28/23 5:47 MFFg/L0.13 7/26/23SM21-23 6200B1Jsec-Butylbenzene ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 5:47 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 5:47 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 5:47 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 5:47 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 5:47 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 5:47 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 5:47 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 5:47 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 5:47 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 5:47 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 5:47 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 5:47 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 5:47 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 5:47 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 5:47 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 5:47 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 5:47 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 5:47 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 5:47 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) 0.64 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) 0.40 0.50 7/28/23 5:47 MFFg/L0.13 7/26/23SM21-23 6200B1Jp-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 5:47 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 5:47 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 5:47 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 20 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-06 Field Sample #: MW-7 Sample Matrix: Ground Water Sampled: 7/20/2023 09:01 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 5:47 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 5:47 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 5:47 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 5:47 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 5:47 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 5:47 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 5:47 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 5:47 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 5:47 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 5:47 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane 1.2 0.50 7/28/23 5:47 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene 1.8 0.50 7/28/23 5:47 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 5:47 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 5:47 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 5:47 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 5:47 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.9 7/28/23 5:4770-130 Toluene-d8 98.8 7/28/23 5:4770-130 4-Bromofluorobenzene 86.8 7/28/23 5:4770-130 Page 21 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-07 Field Sample #: MW-8 Sample Matrix: Ground Water Sampled: 7/20/2023 12:30 [TOC_2]23G3086-07[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS 5.7 50 7/28/23 6:14 MFFg/L2.0 7/26/23SM21-23 6200B1JAcetone ND 0.50 7/28/23 6:14 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 6:14 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 6:14 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 6:14 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 6:14 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 6:14 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) 1.5 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene 1.2 0.50 7/28/23 6:14 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene 0.33 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B1Jtert-Butylbenzene ND 0.50 7/28/23 6:14 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 6:14 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 6:14 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 6:14 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 6:14 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 6:14 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 6:14 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 6:14 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 6:14 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 6:14 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 6:14 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 6:14 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 6:14 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 6:14 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 6:14 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 6:14 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 6:14 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 6:14 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 6:14 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) 9.4 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) 44 0.50 7/28/23 6:14 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 6:14 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 6:14 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 6:14 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 22 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-07 Field Sample #: MW-8 Sample Matrix: Ground Water Sampled: 7/20/2023 12:30 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS 4.5 0.50 7/28/23 6:14 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene 0.17 0.50 7/28/23 6:14 MFFg/L0.12 7/26/23SM21-23 6200B1Jn-Propylbenzene ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 6:14 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 6:14 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 6:14 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 6:14 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 6:14 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 6:14 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 6:14 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 6:14 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane 54 0.50 7/28/23 6:14 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene 27 0.50 7/28/23 6:14 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 6:14 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 6:14 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride 3.9 1.0 7/28/23 6:14 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene 18 0.50 7/28/23 6:14 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 95.3 7/28/23 6:1470-130 Toluene-d8 103 7/28/23 6:1470-130 4-Bromofluorobenzene 89.5 7/28/23 6:1470-130 Page 23 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-08 Field Sample #: MW-9 Sample Matrix: Ground Water Sampled: 7/20/2023 11:50 [TOC_2]23G3086-08[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 5.9 100 7/28/23 7:34 MFFg/L4.0 7/26/23SM21-23 6200B2JAcetone 1.0 1.0 7/28/23 7:34 MFFg/L0.37 7/26/23SM21-23 6200B2Benzene ND 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B2Bromobenzene ND 1.0 7/28/23 7:34 MFFg/L0.57 7/26/23SM21-23 6200B2Bromochloromethane ND 1.0 7/28/23 7:34 MFFg/L0.32 7/26/23SM21-23 6200B2Bromodichloromethane ND 1.0 7/28/23 7:34 MFFg/L0.82 7/26/23SM21-23 6200B2Bromoform ND 4.0 7/28/23 7:34 MFFg/L2.6 7/26/23SM21-23 6200B2Bromomethane ND 10 7/28/23 7:34 MFFg/L3.4 7/26/23SM21-23 6200B22-Butanone (MEK) 5.5 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B2n-Butylbenzene 3.2 1.0 7/28/23 7:34 MFFg/L0.25 7/26/23SM21-23 6200B2sec-Butylbenzene 1.1 1.0 7/28/23 7:34 MFFg/L0.28 7/26/23SM21-23 6200B2tert-Butylbenzene ND 1.0 7/28/23 7:34 MFFg/L0.33 7/26/23SM21-23 6200B2Carbon Tetrachloride ND 1.0 7/28/23 7:34 MFFg/L0.24 7/26/23SM21-23 6200B2Chlorobenzene ND 100 7/28/23 7:34 MFFg/L41 7/26/23SM21-23 6200B2Ethanol ND 1.0 7/28/23 7:34 MFFg/L0.40 7/26/23SM21-23 6200B2Chlorodibromomethane ND 1.0 7/28/23 7:34 MFFg/L0.68 7/26/23SM21-23 6200B2Chloroethane ND 1.0 7/28/23 7:34 MFFg/L0.28 7/26/23SM21-23 6200B2Chloroform ND 1.2 7/28/23 7:34 MFFg/L1.0 7/26/23SM21-23 6200B2Chloromethane ND 1.0 7/28/23 7:34 MFFg/L0.31 7/26/23SM21-23 6200B22-Chlorotoluene ND 1.0 7/28/23 7:34 MFFg/L0.31 7/26/23SM21-23 6200B24-Chlorotoluene ND 1.0 7/28/23 7:34 MFFg/L0.32 7/26/23SM21-23 6200B21,2-Dibromoethane (EDB) ND 1.0 7/28/23 7:34 MFFg/L0.26 7/26/23SM21-23 6200B21,2-Dichlorobenzene ND 1.0 7/28/23 7:34 MFFg/L0.27 7/26/23SM21-23 6200B21,3-Dichlorobenzene ND 1.0 7/28/23 7:34 MFFg/L0.26 7/26/23SM21-23 6200B21,4-Dichlorobenzene ND 1.0 7/28/23 7:34 MFFg/L0.32 7/26/23SM21-23 6200B2Dichlorodifluoromethane (Freon 12) ND 1.0 7/28/23 7:34 MFFg/L0.27 7/26/23SM21-23 6200B21,1-Dichloroethane ND 1.0 7/28/23 7:34 MFFg/L0.61 7/26/23SM21-23 6200B21,2-Dichloroethane ND 1.0 7/28/23 7:34 MFFg/L0.28 7/26/23SM21-23 6200B21,1-Dichloroethylene ND 1.0 7/28/23 7:34 MFFg/L0.28 7/26/23SM21-23 6200B2cis-1,2-Dichloroethylene ND 1.0 7/28/23 7:34 MFFg/L0.34 7/26/23SM21-23 6200B2trans-1,2-Dichloroethylene 1.9 1.0 7/28/23 7:34 MFFg/L0.39 7/26/23SM21-23 6200B21,2-Dichloropropane ND 1.0 7/28/23 7:34 MFFg/L0.23 7/26/23SM21-23 6200B21,3-Dichloropropane ND 1.0 7/28/23 7:34 MFFg/L0.70 7/26/23SM21-23 6200B22,2-Dichloropropane ND 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B21,1-Dichloropropene ND 1.0 7/28/23 7:34 MFFg/L0.33 7/26/23SM21-23 6200B2cis-1,3-Dichloropropene ND 1.0 7/28/23 7:34 MFFg/L0.28 7/26/23SM21-23 6200B2trans-1,3-Dichloropropene ND 1.0 7/28/23 7:34 MFFg/L0.40 7/26/23SM21-23 6200B2Diisopropyl Ether (DIPE) 5.0 1.0 7/28/23 7:34 MFFg/L0.44 7/26/23SM21-23 6200B2Ethylbenzene ND 10 7/28/23 7:34 MFFg/L2.4 7/26/23SM21-23 6200B22-Hexanone (MBK) 37 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B2Isopropylbenzene (Cumene) 14 1.0 7/28/23 7:34 MFFg/L0.25 7/26/23SM21-23 6200B2p-Isopropyltoluene (p-Cymene) ND 1.0 7/28/23 7:34 MFFg/L0.34 7/26/23SM21-23 6200B2Methyl tert-Butyl Ether (MTBE) ND 10 7/28/23 7:34 MFFg/L0.35 7/26/23SM21-23 6200B2Methylene Chloride ND 10 7/28/23 7:34 MFFg/L2.6 7/26/23SM21-23 6200B24-Methyl-2-pentanone (MIBK) Page 24 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-08 Field Sample #: MW-9 Sample Matrix: Ground Water Sampled: 7/20/2023 11:50 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 26 1.0 7/28/23 7:34 MFFg/L0.76 7/26/23SM21-23 6200B2Naphthalene 3.3 1.0 7/28/23 7:34 MFFg/L0.25 7/26/23SM21-23 6200B2n-Propylbenzene ND 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B2Styrene ND 1.0 7/28/23 7:34 MFFg/L0.27 7/26/23SM21-23 6200B21,1,2,2-Tetrachloroethane ND 1.0 7/28/23 7:34 MFFg/L0.34 7/26/23SM21-23 6200B2Tetrachloroethylene 1.3 1.0 7/28/23 7:34 MFFg/L0.45 7/26/23SM21-23 6200B2Toluene ND 2.0 7/28/23 7:34 MFFg/L0.68 7/26/23SM21-23 6200B21,2,3-Trichlorobenzene ND 2.0 7/28/23 7:34 MFFg/L0.60 7/26/23SM21-23 6200B21,2,4-Trichlorobenzene ND 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B21,1,1-Trichloroethane ND 1.0 7/28/23 7:34 MFFg/L0.38 7/26/23SM21-23 6200B21,1,2-Trichloroethane ND 1.0 7/28/23 7:34 MFFg/L0.35 7/26/23SM21-23 6200B2Trichloroethylene ND 1.0 7/28/23 7:34 MFFg/L0.31 7/26/23SM21-23 6200B2Trichlorofluoromethane (Freon 11) ND 1.0 7/28/23 7:34 MFFg/L0.55 7/26/23SM21-23 6200B21,2,3-Trichloropropane 240 1.0 7/28/23 7:34 MFFg/L0.40 7/26/23SM21-23 6200B21,2,4-Trimethylbenzene 110 1.0 7/28/23 7:34 MFFg/L0.30 7/26/23SM21-23 6200B21,3,5-Trimethylbenzene ND 40 7/28/23 7:34 MFFg/L3.3 7/26/23SM21-23 6200B2R-05Vinyl Acetate ND 1.0 7/28/23 7:34 MFFg/L0.47 7/26/23SM21-23 6200B2Vinyl Chloride 130 2.0 7/28/23 7:34 MFFg/L0.98 7/26/23SM21-23 6200B2m+p Xylene 110 1.0 7/28/23 7:34 MFFg/L0.49 7/26/23SM21-23 6200B2o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 97.0 7/28/23 7:3470-130 Toluene-d8 100 7/28/23 7:3470-130 4-Bromofluorobenzene 93.8 7/28/23 7:3470-130 Page 25 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-09 Field Sample #: MW-10 Sample Matrix: Ground Water Sampled: 7/20/2023 12:08 [TOC_2]23G3086-09[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS ND 250 7/28/23 8:54 MFFg/L10 7/26/23SM21-23 6200B5Acetone 130 2.5 7/28/23 8:54 MFFg/L0.92 7/26/23SM21-23 6200B5Benzene ND 2.5 7/28/23 8:54 MFFg/L0.74 7/26/23SM21-23 6200B5Bromobenzene ND 2.5 7/28/23 8:54 MFFg/L1.4 7/26/23SM21-23 6200B5Bromochloromethane ND 2.5 7/28/23 8:54 MFFg/L0.79 7/26/23SM21-23 6200B5Bromodichloromethane ND 2.5 7/28/23 8:54 MFFg/L2.0 7/26/23SM21-23 6200B5Bromoform ND 10 7/28/23 8:54 MFFg/L6.6 7/26/23SM21-23 6200B5Bromomethane ND 25 7/28/23 8:54 MFFg/L8.4 7/26/23SM21-23 6200B52-Butanone (MEK) 8.8 2.5 7/28/23 8:54 MFFg/L0.75 7/26/23SM21-23 6200B5n-Butylbenzene 5.3 2.5 7/28/23 8:54 MFFg/L0.63 7/26/23SM21-23 6200B5sec-Butylbenzene 1.8 2.5 7/28/23 8:54 MFFg/L0.71 7/26/23SM21-23 6200B5Jtert-Butylbenzene ND 2.5 7/28/23 8:54 MFFg/L0.82 7/26/23SM21-23 6200B5Carbon Tetrachloride ND 2.5 7/28/23 8:54 MFFg/L0.59 7/26/23SM21-23 6200B5Chlorobenzene ND 250 7/28/23 8:54 MFFg/L100 7/26/23SM21-23 6200B5Ethanol ND 2.5 7/28/23 8:54 MFFg/L1.0 7/26/23SM21-23 6200B5Chlorodibromomethane ND 2.5 7/28/23 8:54 MFFg/L1.7 7/26/23SM21-23 6200B5Chloroethane ND 2.5 7/28/23 8:54 MFFg/L0.70 7/26/23SM21-23 6200B5Chloroform ND 3.0 7/28/23 8:54 MFFg/L2.5 7/26/23SM21-23 6200B5Chloromethane ND 2.5 7/28/23 8:54 MFFg/L0.77 7/26/23SM21-23 6200B52-Chlorotoluene ND 2.5 7/28/23 8:54 MFFg/L0.77 7/26/23SM21-23 6200B54-Chlorotoluene ND 2.5 7/28/23 8:54 MFFg/L0.80 7/26/23SM21-23 6200B51,2-Dibromoethane (EDB) ND 2.5 7/28/23 8:54 MFFg/L0.65 7/26/23SM21-23 6200B51,2-Dichlorobenzene ND 2.5 7/28/23 8:54 MFFg/L0.68 7/26/23SM21-23 6200B51,3-Dichlorobenzene ND 2.5 7/28/23 8:54 MFFg/L0.64 7/26/23SM21-23 6200B51,4-Dichlorobenzene ND 2.5 7/28/23 8:54 MFFg/L0.80 7/26/23SM21-23 6200B5Dichlorodifluoromethane (Freon 12) ND 2.5 7/28/23 8:54 MFFg/L0.68 7/26/23SM21-23 6200B51,1-Dichloroethane ND 2.5 7/28/23 8:54 MFFg/L1.5 7/26/23SM21-23 6200B51,2-Dichloroethane ND 2.5 7/28/23 8:54 MFFg/L0.70 7/26/23SM21-23 6200B51,1-Dichloroethylene ND 2.5 7/28/23 8:54 MFFg/L0.70 7/26/23SM21-23 6200B5cis-1,2-Dichloroethylene ND 2.5 7/28/23 8:54 MFFg/L0.86 7/26/23SM21-23 6200B5trans-1,2-Dichloroethylene 3.5 2.5 7/28/23 8:54 MFFg/L0.97 7/26/23SM21-23 6200B51,2-Dichloropropane ND 2.5 7/28/23 8:54 MFFg/L0.58 7/26/23SM21-23 6200B51,3-Dichloropropane ND 2.5 7/28/23 8:54 MFFg/L1.7 7/26/23SM21-23 6200B52,2-Dichloropropane ND 2.5 7/28/23 8:54 MFFg/L0.75 7/26/23SM21-23 6200B51,1-Dichloropropene ND 2.5 7/28/23 8:54 MFFg/L0.82 7/26/23SM21-23 6200B5cis-1,3-Dichloropropene ND 2.5 7/28/23 8:54 MFFg/L0.71 7/26/23SM21-23 6200B5trans-1,3-Dichloropropene 9.2 2.5 7/28/23 8:54 MFFg/L1.0 7/26/23SM21-23 6200B5Diisopropyl Ether (DIPE) 330 2.5 7/28/23 8:54 MFFg/L1.1 7/26/23SM21-23 6200B5Ethylbenzene ND 25 7/28/23 8:54 MFFg/L6.0 7/26/23SM21-23 6200B52-Hexanone (MBK) 66 2.5 7/28/23 8:54 MFFg/L0.76 7/26/23SM21-23 6200B5Isopropylbenzene (Cumene) 9.0 2.5 7/28/23 8:54 MFFg/L0.63 7/26/23SM21-23 6200B5p-Isopropyltoluene (p-Cymene) 44 2.5 7/28/23 8:54 MFFg/L0.85 7/26/23SM21-23 6200B5Methyl tert-Butyl Ether (MTBE) ND 25 7/28/23 8:54 MFFg/L0.88 7/26/23SM21-23 6200B5Methylene Chloride ND 25 7/28/23 8:54 MFFg/L6.6 7/26/23SM21-23 6200B54-Methyl-2-pentanone (MIBK) Page 26 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-09 Field Sample #: MW-10 Sample Matrix: Ground Water Sampled: 7/20/2023 12:08 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Sample Flags: RL-11 Volatile Organic Compounds by GC/MS 140 2.5 7/28/23 8:54 MFFg/L1.9 7/26/23SM21-23 6200B5Naphthalene 54 2.5 7/28/23 8:54 MFFg/L0.62 7/26/23SM21-23 6200B5n-Propylbenzene ND 2.5 7/28/23 8:54 MFFg/L0.75 7/26/23SM21-23 6200B5Styrene ND 2.5 7/28/23 8:54 MFFg/L0.68 7/26/23SM21-23 6200B51,1,2,2-Tetrachloroethane ND 2.5 7/28/23 8:54 MFFg/L0.84 7/26/23SM21-23 6200B5Tetrachloroethylene 58 2.5 7/28/23 8:54 MFFg/L1.1 7/26/23SM21-23 6200B5Toluene ND 5.0 7/28/23 8:54 MFFg/L1.7 7/26/23SM21-23 6200B51,2,3-Trichlorobenzene ND 5.0 7/28/23 8:54 MFFg/L1.5 7/26/23SM21-23 6200B51,2,4-Trichlorobenzene ND 2.5 7/28/23 8:54 MFFg/L0.75 7/26/23SM21-23 6200B51,1,1-Trichloroethane ND 2.5 7/28/23 8:54 MFFg/L0.96 7/26/23SM21-23 6200B51,1,2-Trichloroethane ND 2.5 7/28/23 8:54 MFFg/L0.87 7/26/23SM21-23 6200B5Trichloroethylene ND 2.5 7/28/23 8:54 MFFg/L0.77 7/26/23SM21-23 6200B5Trichlorofluoromethane (Freon 11) ND 2.5 7/28/23 8:54 MFFg/L1.4 7/26/23SM21-23 6200B51,2,3-Trichloropropane 430 2.5 7/28/23 8:54 MFFg/L0.99 7/26/23SM21-23 6200B51,2,4-Trimethylbenzene 85 2.5 7/28/23 8:54 MFFg/L0.75 7/26/23SM21-23 6200B51,3,5-Trimethylbenzene ND 100 7/28/23 8:54 MFFg/L8.3 7/26/23SM21-23 6200B5R-05Vinyl Acetate ND 2.5 7/28/23 8:54 MFFg/L1.2 7/26/23SM21-23 6200B5Vinyl Chloride 1000 5.0 7/28/23 8:54 MFFg/L2.5 7/26/23SM21-23 6200B5m+p Xylene 230 2.5 7/28/23 8:54 MFFg/L1.2 7/26/23SM21-23 6200B5o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 94.2 7/28/23 8:5470-130 Toluene-d8 100 7/28/23 8:5470-130 4-Bromofluorobenzene 92.4 7/28/23 8:5470-130 Page 27 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-10 Field Sample #: MW-11 Sample Matrix: Ground Water Sampled: 7/20/2023 11:04 [TOC_2]23G3086-10[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS 4.1 50 7/28/23 6:41 MFFg/L2.0 7/26/23SM21-23 6200B1JAcetone ND 0.50 7/28/23 6:41 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 6:41 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 6:41 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 6:41 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 6:41 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 6:41 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) 1.6 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene 1.2 0.50 7/28/23 6:41 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene 0.34 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B1Jtert-Butylbenzene ND 0.50 7/28/23 6:41 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 6:41 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 6:41 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 6:41 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 6:41 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 6:41 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 6:41 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 6:41 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 6:41 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 6:41 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 6:41 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 6:41 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 6:41 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 6:41 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 6:41 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 6:41 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 6:41 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 6:41 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 6:41 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) 9.4 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) 3.1 0.50 7/28/23 6:41 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 6:41 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 6:41 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 6:41 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 28 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-10 Field Sample #: MW-11 Sample Matrix: Ground Water Sampled: 7/20/2023 11:04 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS 4.4 0.50 7/28/23 6:41 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 6:41 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 6:41 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 6:41 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 6:41 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 6:41 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 6:41 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 6:41 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 6:41 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 6:41 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane 63 0.50 7/28/23 6:41 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene 31 0.50 7/28/23 6:41 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 6:41 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 6:41 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride 1.9 1.0 7/28/23 6:41 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene 13 0.50 7/28/23 6:41 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 94.4 7/28/23 6:4170-130 Toluene-d8 101 7/28/23 6:4170-130 4-Bromofluorobenzene 90.0 7/28/23 6:4170-130 Page 29 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-11 Field Sample #: MW-12 Sample Matrix: Ground Water Sampled: 7/20/2023 11:26 [TOC_2]23G3086-11[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 7:07 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone 1.5 0.50 7/28/23 7:07 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 7:07 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 7:07 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 7:07 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 7:07 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 7:07 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) 0.69 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene 0.68 0.50 7/28/23 7:07 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 7:07 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 7:07 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 7:07 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 7:07 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 7:07 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 7:07 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 7:07 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 7:07 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 7:07 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 7:07 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 7:07 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 7:07 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 7:07 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 7:07 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 7:07 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 7:07 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 7:07 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 7:07 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 7:07 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) 5.8 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) 2.2 0.50 7/28/23 7:07 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 7:07 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 7:07 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 7:07 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 30 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-11 Field Sample #: MW-12 Sample Matrix: Ground Water Sampled: 7/20/2023 11:26 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS 3.9 0.50 7/28/23 7:07 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 7:07 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene 0.70 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 7:07 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 7:07 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 7:07 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 7:07 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 7:07 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 7:07 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 7:07 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 7:07 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane 30 0.50 7/28/23 7:07 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene 15 0.50 7/28/23 7:07 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 7:07 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 7:07 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride 0.71 1.0 7/28/23 7:07 MFFg/L0.49 7/26/23SM21-23 6200B1Jm+p Xylene 22 0.50 7/28/23 7:07 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 93.3 7/28/23 7:0770-130 Toluene-d8 97.4 7/28/23 7:0770-130 4-Bromofluorobenzene 93.5 7/28/23 7:0770-130 Page 31 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-12 Field Sample #: WSW-3 Sample Matrix: Ground Water Sampled: 7/20/2023 11:41 [TOC_2]23G3086-12[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 2:41 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 2:41 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 2:41 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 2:41 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 2:41 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 2:41 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 2:41 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 2:41 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 2:41 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 2:41 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 2:41 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 2:41 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 2:41 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 2:41 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 2:41 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 2:41 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 2:41 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 2:41 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 2:41 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 2:41 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 2:41 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 2:41 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 2:41 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 2:41 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 2:41 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 2:41 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 2:41 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 2:41 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 2:41 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 2:41 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 2:41 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 32 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-12 Field Sample #: WSW-3 Sample Matrix: Ground Water Sampled: 7/20/2023 11:41 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 2:41 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 2:41 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 2:41 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 2:41 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 2:41 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 2:41 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 2:41 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 2:41 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 2:41 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 2:41 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 2:41 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 2:41 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 2:41 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 2:41 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 2:41 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 2:41 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 96.6 7/28/23 2:4170-130 Toluene-d8 97.6 7/28/23 2:4170-130 4-Bromofluorobenzene 86.6 7/28/23 2:4170-130 Page 33 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-13 Field Sample #: WSW-4 Sample Matrix: Ground Water Sampled: 7/20/2023 12:06 [TOC_2]23G3086-13[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 3:08 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 3:08 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 3:08 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 3:08 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 3:08 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 3:08 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 3:08 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 3:08 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 3:08 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 3:08 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 3:08 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 3:08 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 3:08 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane 0.25 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B1JChloroform ND 0.60 7/28/23 3:08 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 3:08 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 3:08 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 3:08 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 3:08 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 3:08 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 3:08 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 3:08 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 3:08 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 3:08 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 3:08 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 3:08 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 3:08 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 3:08 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 3:08 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 3:08 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 3:08 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 3:08 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 34 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-13 Field Sample #: WSW-4 Sample Matrix: Ground Water Sampled: 7/20/2023 12:06 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 3:08 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 3:08 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 3:08 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 3:08 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 3:08 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 3:08 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 3:08 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 3:08 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 3:08 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 3:08 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 3:08 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 3:08 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 3:08 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 3:08 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 3:08 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 3:08 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.0 7/28/23 3:0870-130 Toluene-d8 101 7/28/23 3:0870-130 4-Bromofluorobenzene 85.6 7/28/23 3:0870-130 Page 35 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-14 Field Sample #: WSW-11 Sample Matrix: Ground Water Sampled: 7/20/2023 14:56 [TOC_2]23G3086-14[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 3:34 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 3:34 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 3:34 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 3:34 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 3:34 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 3:34 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 3:34 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 3:34 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 3:34 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 3:34 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 3:34 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 3:34 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 3:34 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 3:34 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 3:34 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 3:34 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 3:34 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 3:34 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 3:34 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 3:34 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 3:34 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 3:34 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 3:34 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 3:34 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 3:34 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 3:34 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 3:34 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 3:34 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 3:34 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 3:34 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 3:34 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 36 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-14 Field Sample #: WSW-11 Sample Matrix: Ground Water Sampled: 7/20/2023 14:56 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 3:34 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 3:34 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 3:34 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 3:34 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 3:34 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 3:34 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 3:34 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 3:34 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 3:34 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 3:34 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 3:34 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 3:34 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 3:34 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 3:34 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 3:34 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 3:34 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 97.9 7/28/23 3:3470-130 Toluene-d8 98.8 7/28/23 3:3470-130 4-Bromofluorobenzene 87.0 7/28/23 3:3470-130 Page 37 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-15 Field Sample #: FB Sample Matrix: Field Blank Sampled: 7/20/2023 15:00 [TOC_2]23G3086-15[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS 4.0 50 7/28/23 1:48 MFFg/L2.0 7/26/23SM21-23 6200B1JAcetone ND 0.50 7/28/23 1:48 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 1:48 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 1:48 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 1:48 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 1:48 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 1:48 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 1:48 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 1:48 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 1:48 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 1:48 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 1:48 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 1:48 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B1Chloroform ND 0.60 7/28/23 1:48 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 1:48 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 1:48 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 1:48 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 1:48 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 1:48 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 1:48 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 1:48 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 1:48 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 1:48 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 1:48 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 1:48 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 1:48 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 1:48 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 1:48 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 1:48 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 1:48 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 1:48 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 38 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-15 Field Sample #: FB Sample Matrix: Field Blank Sampled: 7/20/2023 15:00 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 1:48 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 1:48 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 1:48 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 1:48 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 1:48 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 1:48 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 1:48 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 1:48 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 1:48 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 1:48 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 1:48 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 1:48 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 1:48 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 1:48 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 1:48 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 1:48 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.3 7/28/23 1:4870-130 Toluene-d8 99.1 7/28/23 1:4870-130 4-Bromofluorobenzene 85.3 7/28/23 1:4870-130 Page 39 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-16 Field Sample #: TB Sample Matrix: Trip Blank Water Sampled: 7/20/2023 00:00 [TOC_2]23G3086-16[TOC] AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 50 7/28/23 2:14 MFFg/L2.0 7/26/23SM21-23 6200B1Acetone ND 0.50 7/28/23 2:14 MFFg/L0.18 7/26/23SM21-23 6200B1Benzene ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B1Bromobenzene ND 0.50 7/28/23 2:14 MFFg/L0.28 7/26/23SM21-23 6200B1Bromochloromethane ND 0.50 7/28/23 2:14 MFFg/L0.16 7/26/23SM21-23 6200B1Bromodichloromethane ND 0.50 7/28/23 2:14 MFFg/L0.41 7/26/23SM21-23 6200B1Bromoform ND 2.0 7/28/23 2:14 MFFg/L1.3 7/26/23SM21-23 6200B1Bromomethane ND 5.0 7/28/23 2:14 MFFg/L1.7 7/26/23SM21-23 6200B12-Butanone (MEK) ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B1n-Butylbenzene ND 0.50 7/28/23 2:14 MFFg/L0.13 7/26/23SM21-23 6200B1sec-Butylbenzene ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B1tert-Butylbenzene ND 0.50 7/28/23 2:14 MFFg/L0.16 7/26/23SM21-23 6200B1Carbon Tetrachloride ND 0.50 7/28/23 2:14 MFFg/L0.12 7/26/23SM21-23 6200B1Chlorobenzene ND 50 7/28/23 2:14 MFFg/L20 7/26/23SM21-23 6200B1Ethanol ND 0.50 7/28/23 2:14 MFFg/L0.20 7/26/23SM21-23 6200B1Chlorodibromomethane ND 0.50 7/28/23 2:14 MFFg/L0.34 7/26/23SM21-23 6200B1Chloroethane 0.18 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B1JChloroform ND 0.60 7/28/23 2:14 MFFg/L0.50 7/26/23SM21-23 6200B1Chloromethane ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B12-Chlorotoluene ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B14-Chlorotoluene ND 0.50 7/28/23 2:14 MFFg/L0.16 7/26/23SM21-23 6200B11,2-Dibromoethane (EDB) ND 0.50 7/28/23 2:14 MFFg/L0.13 7/26/23SM21-23 6200B11,2-Dichlorobenzene ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B11,3-Dichlorobenzene ND 0.50 7/28/23 2:14 MFFg/L0.13 7/26/23SM21-23 6200B11,4-Dichlorobenzene ND 0.50 7/28/23 2:14 MFFg/L0.16 7/26/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12) ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethane ND 0.50 7/28/23 2:14 MFFg/L0.30 7/26/23SM21-23 6200B11,2-Dichloroethane ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B11,1-Dichloroethylene ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B1cis-1,2-Dichloroethylene ND 0.50 7/28/23 2:14 MFFg/L0.17 7/26/23SM21-23 6200B1trans-1,2-Dichloroethylene ND 0.50 7/28/23 2:14 MFFg/L0.19 7/26/23SM21-23 6200B11,2-Dichloropropane ND 0.50 7/28/23 2:14 MFFg/L0.12 7/26/23SM21-23 6200B11,3-Dichloropropane ND 0.50 7/28/23 2:14 MFFg/L0.35 7/26/23SM21-23 6200B12,2-Dichloropropane ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B11,1-Dichloropropene ND 0.50 7/28/23 2:14 MFFg/L0.16 7/26/23SM21-23 6200B1cis-1,3-Dichloropropene ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B1trans-1,3-Dichloropropene ND 0.50 7/28/23 2:14 MFFg/L0.20 7/26/23SM21-23 6200B1Diisopropyl Ether (DIPE) ND 0.50 7/28/23 2:14 MFFg/L0.22 7/26/23SM21-23 6200B1Ethylbenzene ND 5.0 7/28/23 2:14 MFFg/L1.2 7/26/23SM21-23 6200B12-Hexanone (MBK) ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B1Isopropylbenzene (Cumene) ND 0.50 7/28/23 2:14 MFFg/L0.13 7/26/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene) ND 0.50 7/28/23 2:14 MFFg/L0.17 7/26/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE) ND 5.0 7/28/23 2:14 MFFg/L0.18 7/26/23SM21-23 6200B1Methylene Chloride ND 5.0 7/28/23 2:14 MFFg/L1.3 7/26/23SM21-23 6200B14-Methyl-2-pentanone (MIBK) Page 40 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 7/22/2023 Work Order: 23G3086Sample Description:Project Location: Wendell, NC Sample ID: 23G3086-16 Field Sample #: TB Sample Matrix: Trip Blank Water Sampled: 7/20/2023 00:00 AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time DL Units Date PreparedMethod Volatile Organic Compounds by GC/MS ND 0.50 7/28/23 2:14 MFFg/L0.38 7/26/23SM21-23 6200B1Naphthalene ND 0.50 7/28/23 2:14 MFFg/L0.12 7/26/23SM21-23 6200B1n-Propylbenzene ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B1Styrene ND 0.50 7/28/23 2:14 MFFg/L0.14 7/26/23SM21-23 6200B11,1,2,2-Tetrachloroethane ND 0.50 7/28/23 2:14 MFFg/L0.17 7/26/23SM21-23 6200B1Tetrachloroethylene ND 0.50 7/28/23 2:14 MFFg/L0.22 7/26/23SM21-23 6200B1Toluene ND 1.0 7/28/23 2:14 MFFg/L0.34 7/26/23SM21-23 6200B11,2,3-Trichlorobenzene ND 1.0 7/28/23 2:14 MFFg/L0.30 7/26/23SM21-23 6200B11,2,4-Trichlorobenzene ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B11,1,1-Trichloroethane ND 0.50 7/28/23 2:14 MFFg/L0.19 7/26/23SM21-23 6200B11,1,2-Trichloroethane ND 0.50 7/28/23 2:14 MFFg/L0.17 7/26/23SM21-23 6200B1Trichloroethylene ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B1Trichlorofluoromethane (Freon 11) ND 0.50 7/28/23 2:14 MFFg/L0.28 7/26/23SM21-23 6200B11,2,3-Trichloropropane ND 0.50 7/28/23 2:14 MFFg/L0.20 7/26/23SM21-23 6200B11,2,4-Trimethylbenzene ND 0.50 7/28/23 2:14 MFFg/L0.15 7/26/23SM21-23 6200B11,3,5-Trimethylbenzene ND 20 7/28/23 2:14 MFFg/L1.7 7/26/23SM21-23 6200B1R-05Vinyl Acetate ND 0.50 7/28/23 2:14 MFFg/L0.24 7/26/23SM21-23 6200B1Vinyl Chloride ND 1.0 7/28/23 2:14 MFFg/L0.49 7/26/23SM21-23 6200B1m+p Xylene ND 0.50 7/28/23 2:14 MFFg/L0.24 7/26/23SM21-23 6200B1o-Xylene Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.4 7/28/23 2:1470-130 Toluene-d8 98.8 7/28/23 2:1470-130 4-Bromofluorobenzene 86.4 7/28/23 2:1470-130 Page 41 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 5030B-SM21-23 6200B Lab Number [Field ID]Batch DateInitial [mL]Final [mL] B347066 07/26/230.025 5.0023G3086-01 [MW-1R] B347066 07/26/235 5.0023G3086-02 [MW-2] B347066 07/26/230.125 5.0023G3086-03 [MW-4] B347066 07/26/235 5.0023G3086-04 [MW-5R] B347066 07/26/235 5.0023G3086-05 [MW-6] B347066 07/26/235 5.0023G3086-06 [MW-7] B347066 07/26/235 5.0023G3086-07 [MW-8] B347066 07/26/232.5 5.0023G3086-08 [MW-9] B347066 07/26/231 5.0023G3086-09 [MW-10] B347066 07/26/235 5.0023G3086-10 [MW-11] B347066 07/26/235 5.0023G3086-11 [MW-12] B347066 07/26/235 5.0023G3086-12 [WSW-3] B347066 07/26/235 5.0023G3086-13 [WSW-4] B347066 07/26/235 5.0023G3086-14 [WSW-11] B347066 07/26/235 5.0023G3086-15 [FB] B347066 07/26/235 5.0023G3086-16 [TB] [TOC_1]Sample Preparation Information[TOC] Page 42 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Batch B347066 - SW-846 5030B [TOC_3]B347066[TOC] Blank (B347066-BLK1) Prepared: 07/26/23 Analyzed: 07/28/23 Acetone g/L50ND Benzene g/L0.50ND Bromobenzene g/L0.50ND Bromochloromethane g/L0.50ND Bromodichloromethane g/L0.50ND Bromoform g/L0.50ND Bromomethane g/L2.0ND 2-Butanone (MEK)g/L5.0ND n-Butylbenzene g/L0.50ND sec-Butylbenzene g/L0.50ND tert-Butylbenzene g/L0.50ND Carbon Tetrachloride g/L0.50ND Chlorobenzene g/L0.50ND Ethanol g/L50ND Chlorodibromomethane g/L0.50ND Chloroethane g/L0.50ND Chloroform g/L0.50ND Chloromethane g/L0.60ND 2-Chlorotoluene g/L0.50ND 4-Chlorotoluene g/L0.50ND 1,2-Dibromoethane (EDB)g/L0.50ND 1,2-Dichlorobenzene g/L0.50ND 1,3-Dichlorobenzene g/L0.50ND 1,4-Dichlorobenzene g/L0.50ND Dichlorodifluoromethane (Freon 12)g/L0.50ND 1,1-Dichloroethane g/L0.50ND 1,2-Dichloroethane g/L0.50ND 1,1-Dichloroethylene g/L0.50ND cis-1,2-Dichloroethylene g/L0.50ND trans-1,2-Dichloroethylene g/L0.50ND 1,2-Dichloropropane g/L0.50ND 1,3-Dichloropropane g/L0.50ND 2,2-Dichloropropane g/L0.50ND 1,1-Dichloropropene g/L0.50ND cis-1,3-Dichloropropene g/L0.50ND trans-1,3-Dichloropropene g/L0.50ND Diisopropyl Ether (DIPE)g/L0.50ND Ethylbenzene g/L0.50ND 2-Hexanone (MBK)g/L5.0ND Isopropylbenzene (Cumene)g/L0.50ND p-Isopropyltoluene (p-Cymene)g/L0.50ND Methyl tert-Butyl Ether (MTBE)g/L0.50ND Methylene Chloride g/L5.0ND 4-Methyl-2-pentanone (MIBK)g/L5.0ND Naphthalene g/L0.50ND n-Propylbenzene g/L0.50ND Styrene g/L0.50ND 1,1,2,2-Tetrachloroethane g/L0.50ND Tetrachloroethylene g/L0.50ND Toluene g/L0.50ND 1,2,3-Trichlorobenzene g/L1.0ND 1,2,4-Trichlorobenzene g/L0.50ND [TOC_1]QC Data[TOC] Page 43 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B347066 - SW-846 5030B Blank (B347066-BLK1) Prepared: 07/26/23 Analyzed: 07/28/23 1,1,1-Trichloroethane g/L0.50ND 1,1,2-Trichloroethane g/L0.50ND Trichloroethylene g/L0.50ND Trichlorofluoromethane (Freon 11)g/L0.50ND 1,2,3-Trichloropropane g/L0.50ND 1,2,4-Trimethylbenzene g/L0.50ND 1,3,5-Trimethylbenzene g/L0.50ND Vinyl Acetate g/L20 R-05ND Vinyl Chloride g/L0.50ND m+p Xylene g/L1.0ND o-Xylene g/L0.50ND g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.724.4 g/L 25.0 70-130Surrogate: Toluene-d8 98.724.7 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 86.421.6 LCS (B347066-BS1) Prepared: 07/26/23 Analyzed: 07/27/23 Acetone g/L50 100 70-13090.490.4 Benzene g/L0.50 10.0 70-13011211.2 Bromobenzene g/L0.50 10.0 70-13010310.3 Bromochloromethane g/L0.50 10.0 70-13012212.2 Bromodichloromethane g/L0.50 10.0 70-13010210.2 Bromoform g/L0.50 10.0 70-13084.08.40 Bromomethane g/L2.0 10.0 60-14013613.6 2-Butanone (MEK)g/L5.0 100 70-130103103 n-Butylbenzene g/L0.50 10.0 70-13098.89.88 sec-Butylbenzene g/L0.50 10.0 70-13094.69.46 tert-Butylbenzene g/L0.50 10.0 70-13090.29.02 Carbon Tetrachloride g/L0.50 10.0 70-13083.48.34 Chlorobenzene g/L0.50 10.0 70-13010710.7 Ethanol g/L50 100 70-13077.377.3 Chlorodibromomethane g/L0.50 10.0 70-13098.99.89 Chloroethane g/L0.50 10.0 60-14093.69.36 Chloroform g/L0.50 10.0 70-13010610.6 Chloromethane g/L0.60 10.0 60-14010710.7 2-Chlorotoluene g/L0.50 10.0 70-13099.29.92 4-Chlorotoluene g/L0.50 10.0 70-13010010.0 1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010710.7 1,2-Dichlorobenzene g/L0.50 10.0 70-13010510.5 1,3-Dichlorobenzene g/L0.50 10.0 70-13010810.8 1,4-Dichlorobenzene g/L0.50 10.0 70-13010710.7 Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14010410.4 1,1-Dichloroethane g/L0.50 10.0 70-13010410.4 1,2-Dichloroethane g/L0.50 10.0 70-13098.79.87 1,1-Dichloroethylene g/L0.50 10.0 70-13095.79.57 cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010210.2 trans-1,2-Dichloroethylene g/L0.50 10.0 70-13096.29.62 1,2-Dichloropropane g/L0.50 10.0 70-13011211.2 1,3-Dichloropropane g/L0.50 10.0 70-13010710.7 2,2-Dichloropropane g/L0.50 10.0 70-13085.58.55 1,1-Dichloropropene g/L0.50 10.0 70-13010510.5 cis-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3 trans-1,3-Dichloropropene g/L0.50 10.0 70-13099.69.96 Page 44 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B347066 - SW-846 5030B LCS (B347066-BS1) Prepared: 07/26/23 Analyzed: 07/27/23 Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010510.5 Ethylbenzene g/L0.50 10.0 70-13010310.3 2-Hexanone (MBK)g/L5.0 100 70-13093.693.6 Isopropylbenzene (Cumene)g/L0.50 10.0 70-13093.59.35 p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13095.49.54 Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13093.09.30 Methylene Chloride g/L5.0 10.0 70-13099.49.94 4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13092.392.3 Naphthalene g/L0.50 10.0 70-13070.47.04 n-Propylbenzene g/L0.50 10.0 70-13096.69.66 Styrene g/L0.50 10.0 70-13096.29.62 1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13095.69.56 Tetrachloroethylene g/L0.50 10.0 70-13010610.6 Toluene g/L0.50 10.0 70-13010810.8 1,2,3-Trichlorobenzene g/L1.0 10.0 70-13087.78.77 1,2,4-Trichlorobenzene g/L0.50 10.0 70-13085.28.52 1,1,1-Trichloroethane g/L0.50 10.0 70-13010510.5 1,1,2-Trichloroethane g/L0.50 10.0 70-13011211.2 Trichloroethylene g/L0.50 10.0 70-13010610.6 Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13097.19.71 1,2,3-Trichloropropane g/L0.50 10.0 70-13012112.1 1,2,4-Trimethylbenzene g/L0.50 10.0 70-13098.39.83 1,3,5-Trimethylbenzene g/L0.50 10.0 70-13098.79.87 Vinyl Acetate g/L20 100 R-0570-13087.987.9 Vinyl Chloride g/L0.50 10.0 60-14011611.6 m+p Xylene g/L1.0 20.0 70-13099.219.8 o-Xylene g/L0.50 10.0 70-13095.09.50 g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 94.823.7 g/L 25.0 70-130Surrogate: Toluene-d8 10225.6 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.023.5 LCS Dup (B347066-BSD1) Prepared: 07/26/23 Analyzed: 07/28/23 Acetone g/L50 100 2570-13095.4 5.4095.4 Benzene g/L0.50 10.0 2570-130116 3.4311.6 Bromobenzene g/L0.50 10.0 2570-130102 1.2710.2 Bromochloromethane g/L0.50 10.0 2570-130122 0.65612.2 Bromodichloromethane g/L0.50 10.0 2570-130104 1.1610.4 Bromoform g/L0.50 10.0 2570-13079.6 5.387.96 Bromomethane g/L2.0 10.0 2560-140133 2.0113.3 2-Butanone (MEK)g/L5.0 100 2570-130109 4.94109 n-Butylbenzene g/L0.50 10.0 2570-13099.5 0.7069.95 sec-Butylbenzene g/L0.50 10.0 2570-13096.4 1.889.64 tert-Butylbenzene g/L0.50 10.0 2570-13090.4 0.2219.04 Carbon Tetrachloride g/L0.50 10.0 2570-13082.8 0.7228.28 Chlorobenzene g/L0.50 10.0 2570-130106 1.1210.6 Ethanol g/L50 100 2570-13080.2 3.6780.2 Chlorodibromomethane g/L0.50 10.0 2570-13098.3 0.6099.83 Chloroethane g/L0.50 10.0 2560-140102 8.6910.2 Chloroform g/L0.50 10.0 2570-130107 0.94310.7 Chloromethane g/L0.60 10.0 2560-140104 3.1410.4 2-Chlorotoluene g/L0.50 10.0 2570-130101 1.7010.1 4-Chlorotoluene g/L0.50 10.0 2570-13098.7 1.819.87 Page 45 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control QUALITY CONTROL Batch B347066 - SW-846 5030B LCS Dup (B347066-BSD1) Prepared: 07/26/23 Analyzed: 07/28/23 1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130105 1.6010.5 1,2-Dichlorobenzene g/L0.50 10.0 2570-130105 0.19010.5 1,3-Dichlorobenzene g/L0.50 10.0 2570-130108 0.18610.8 1,4-Dichlorobenzene g/L0.50 10.0 2570-130106 1.3110.6 Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-140102 1.9510.2 1,1-Dichloroethane g/L0.50 10.0 2570-130103 0.67510.3 1,2-Dichloroethane g/L0.50 10.0 2570-13099.4 0.7079.94 1,1-Dichloroethylene g/L0.50 10.0 2570-13096.6 0.9369.66 cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130102 0.29510.2 trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13097.5 1.349.75 1,2-Dichloropropane g/L0.50 10.0 2570-130113 1.0711.3 1,3-Dichloropropane g/L0.50 10.0 2570-130108 1.6710.8 2,2-Dichloropropane g/L0.50 10.0 2570-13085.0 0.5878.50 1,1-Dichloropropene g/L0.50 10.0 2570-130105 0.28510.5 cis-1,3-Dichloropropene g/L0.50 10.0 2570-130105 1.4410.5 trans-1,3-Dichloropropene g/L0.50 10.0 2570-13099.2 0.4029.92 Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130106 1.1410.6 Ethylbenzene g/L0.50 10.0 2570-130100 2.6510.0 2-Hexanone (MBK)g/L5.0 100 2570-13096.4 2.9996.4 Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13092.8 0.7519.28 p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13094.2 1.279.42 Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13095.6 2.769.56 Methylene Chloride g/L5.0 10.0 2570-13098.7 0.7079.87 4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13095.0 2.8295.0 Naphthalene g/L0.50 10.0 2570-13072.1 2.397.21 n-Propylbenzene g/L0.50 10.0 2570-13096.1 0.5199.61 Styrene g/L0.50 10.0 2570-13095.3 0.9409.53 1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13089.8 6.268.98 Tetrachloroethylene g/L0.50 10.0 2570-130106 0.094310.6 Toluene g/L0.50 10.0 2570-130108 0.46210.8 1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13088.0 0.3418.80 1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13087.3 2.438.73 1,1,1-Trichloroethane g/L0.50 10.0 2570-130103 1.8310.3 1,1,2-Trichloroethane g/L0.50 10.0 2570-130109 2.8110.9 Trichloroethylene g/L0.50 10.0 2570-130110 4.1711.0 Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13096.4 0.7249.64 1,2,3-Trichloropropane g/L0.50 10.0 2570-130121 0.24812.1 1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13096.5 1.859.65 1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13099.2 0.5059.92 Vinyl Acetate g/L20 100 25 L-07A, R-0570-13063.0 33.0**63.0 Vinyl Chloride g/L0.50 10.0 2560-140111 3.7011.1 m+p Xylene g/L1.0 20.0 2570-13097.8 1.4719.6 o-Xylene g/L0.50 10.0 2570-13094.0 1.069.40 g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 98.624.6 g/L 25.0 70-130Surrogate: Toluene-d8 10325.7 g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 93.723.4 Page 46 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 *QC result is outside of established limits. Wide recovery limits established for difficult compound. Wide RPD limits established for difficult compound. #Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. FLAG/QUALIFIER SUMMARY Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). J Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. L-07A Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. R-05 Elevated reporting limit due to high concentration of target compounds.RL-11 [TOC_1]Flag/Qualifier Summary[TOC] Page 47 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report SM21-23 6200B in Water NCAcetone NCBenzene NCBromobenzene NCBromochloromethane NCBromodichloromethane NCBromoform NCBromomethane NC2-Butanone (MEK) NCn-Butylbenzene NCsec-Butylbenzene NCtert-Butylbenzene NCCarbon Tetrachloride NCChlorobenzene NCEthanol NCChlorodibromomethane NCChloroethane NCChloroform NCChloromethane NC2-Chlorotoluene NC4-Chlorotoluene NC1,2-Dibromoethane (EDB) NC1,2-Dichlorobenzene NC1,3-Dichlorobenzene NC1,4-Dichlorobenzene NCDichlorodifluoromethane (Freon 12) NC1,1-Dichloroethane NC1,2-Dichloroethane NC1,1-Dichloroethylene NCcis-1,2-Dichloroethylene NCtrans-1,2-Dichloroethylene NC1,2-Dichloropropane NC1,3-Dichloropropane NC2,2-Dichloropropane NC1,1-Dichloropropene NCcis-1,3-Dichloropropene NCtrans-1,3-Dichloropropene NCDiisopropyl Ether (DIPE) NCEthylbenzene NC2-Hexanone (MBK) NCIsopropylbenzene (Cumene) NCp-Isopropyltoluene (p-Cymene) NCMethyl tert-Butyl Ether (MTBE) NCMethylene Chloride NC4-Methyl-2-pentanone (MIBK) NCNaphthalene NCn-Propylbenzene NCStyrene [TOC_1]Certifications[TOC] Page 48 of 54 Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report SM21-23 6200B in Water NC1,1,2,2-Tetrachloroethane NCTetrachloroethylene NCToluene NC1,2,3-Trichlorobenzene NC1,2,4-Trichlorobenzene NC1,1,1-Trichloroethane NC1,1,2-Trichloroethane NCTrichloroethylene NCTrichlorofluoromethane (Freon 11) NC1,2,3-Trichloropropane NC1,2,4-Trimethylbenzene NC1,3,5-Trimethylbenzene NCVinyl Acetate NCVinyl Chloride NCm+p Xylene NCo-Xylene The CON-TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires 652North Carolina Div. of Water QualityNC 12/31/2023 Page 49 of 54 Table of Contents Page 50 of 54 Table of Contents Page 51 of 54 Table of Contents Page 52 of 54 Table of Contents Page 53 of 54 Table of Contents Page 54 of 54 Table of Contents