RA-1931_11828_CA_RS_20120402_GWMonRpt

Groundwater Monitoring and Receptor Survey Report S&ME Project No. 1354-12-055
TF-11828 Judy Faulkner-Smith Property April 2, 2012

i
TABLE OF CONTENTS
SITE IDENTIFICATION ........................................................................................................................ ii
1.0 SCOPE OF SERVICES ............................................................................................................... 1
2.0 SITE HISTORY ............................................................................................................................. 2
3.0 RECEPTOR INFORMATION .................................................................................................... 3
3.1 SITE RECONNAISSANCE .................................................................................................................. 3
3.2 WATER SUPPLY WELLS .................................................................................................................. 3
3.3 PUBLIC WATER SUPPLIES ............................................................................................................... 3
3.4 SURFACE WATER ............................................................................................................................ 3
4.0 GROUNDWATER MONITORING ........................................................................................... 4
4.1 WATER SUPPLY WELL SAMPLING................................................................................................... 4
4.2 WATER SUPPLY WELL SAMPLING RESULTS ................................................................................. 4
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................. 5

TABLES
TABLE 1: RECEPTOR INFORMATION AND ADJACENT PROPERTY OWNERS
TABLE 2: SUMMARY OF WATER SUPPLY WELL ANALYTICAL RESULTS

FIGURES
FIGURE 1: VICINITY MAP
FIGURE 2: SITE MAP
FIGURE 3: RECEPTOR SURVEY MAP WITH ADJACENT PROPERTY OWNERS AND WATER
SUPPLY WELLS
FIGURE 4: WATER SUPPLY WELL SAMPLING RESULTS

APPENDICES
APPENDIX I PHOTOGRAPHIC LOG
APPENDIX II LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY FORM
Receptor Survey and Groundwater Monitoring Report S&ME Project No. 1354-12-055
TF-11828 Judy Faulkner-Smith Property April 2, 2012

1
1.0 SCOPE OF SERVICES

The scope of services performed for this report were performed in general accordance
with S&ME’s Proposal No. P019-12V, dated February 2, 2012, and as authorized by
NCDENR’s Task Authorization No. 01, dated March 2, 2012 and within NCDENR’s
Contract No. 16-1713-3C for the Eastern Region.

S&ME’s approved Scope of Services for this Task Authorization included conducting the
initial project review and setup, preparing a health and safety plan, completing a site
reconnaissance and receptor survey update, collecting samples from three water supply
wells, and preparing this report.

The scope of services was completed as proposed.
Receptor Survey and Groundwater Monitoring Report S&ME Project No. 1354-12-055
TF-11828 Judy Faulkner-Smith Property April 2, 2012

2
2.0 SITE HISTORY

The subject site is located at 1300 Vicksboro Road in Henderson, Vance County, North
Carolina. The site is a single family residential home. The approximate central
coordinates of the subject site are 36º 19’ 01.85” north latitude and 78º 21’ 32.29” west
longitude. A vicinity map of the site is shown on Figure 1, and the site and pertinent
features are shown on Figure 2.

Based on a North Carolina Department of Environment and Natural Resources
(NCDENR) Pollution Incident/Leak Reporting Form dated July 7, 1993, concentrations
of several volatile organic compounds (VOCs) were detected in the water supply well at
the Faulkner-Smith residence. One of the VOCs (benzene) was detected in a
concentration exceeding the North Carolina 2L Groundwater Standard (2L Standard).
The source of the contamination was believed to be an old gasoline underground storage
tank (UST) located on an adjacent property. The UST was owned by Mr. William
Faulkner (deceased), and was reportedly taken out of service in 1958, but was never
properly abandoned.

According to a January 27, 2004 Receptor Survey and Site Reconnaissance Survey
Report by Groundwater Management Associates, Inc. (GMA), the water supply well at
the Faulkner-Smith residence was sampled again in November 1993. The laboratory
analytical results of the sample collected in November 1993 indicated that no
concentrations of VOCs were detected above the laboratory detection limits. The results
of the receptor survey indicated that there were at least three water supply wells located
within 500 feet and public water service was not available in the area. Twenty-three
water supply wells and two surface water features were identified within 1,500 feet of the
site.

On July 12, 2004, GMA submitted a Water Supply Well Monitoring Report. The report
indicated that three water supply wells located within 500 feet of the site (Faulkner-Smith
3-1, Faulkner-Smith 3-6, and Roberts B-29) were sampled on June 3, 2004. The
laboratory analytical results of the samples indicated that benzene was detected in a
concentration exceeding the 2L Standard in the Faulkner-Smith 3-1 supply well (site
well). Several other VOCs were also detected in the Faulkner-Smith 3-1 and one VOC
well below their respective 2L Standards. One VOC (methyl tert-butyl ether (MTBE))
was detected below the 2L Standard in the sample collected from Faulkner-Smith 3-6.

According to a February 3, 2006 Water Supply Well Sampling Report by GMA, the three
water supply wells were sampled in November 14, 2005. The laboratory analytical
results of the water samples indicated that benzene was present exceeding the 2L
Standard and several other VOCs below the 2L Standard in the Faulkner-Smith 3-1 water
supply well. No target contaminant constituents were detected in the other two water
supply wells sampled.

Receptor Survey and Groundwater Monitoring Report S&ME Project No. 1354-12-055
TF-11828 Judy Faulkner-Smith Property April 2, 2012

3

3.0 RECEPTOR INFORMATION

S&ME, Inc., (S&ME) performed an updated receptor survey. Information pertaining to
the receptors identified within 1,000 feet of the subject site is summarized below. The
vicinity and site are shown on Figure 1 and Figure 2. The locations of adjacent property
owners and potential receptors located within approximately 1,000 feet of the subject site
are shown on Figure 3.
3.1 Site Reconnaissance
S&ME personnel completed the site reconnaissance on March 8, 2012. The site is
located at 1300 Vicksboro Road in Henderson, Vance County, North Carolina and
currently consists of the Faulkner-Smith residence. The adjacent property to the east is
the location of a former store and gasoline station. The USTs presumably have not been
located or removed and are the likely source of the contamination in the Faulkner-Smith
residence water supply well. During the site reconnaissance, S&ME personnel observed
what appeared to be fill ports and vent pipes along the east side of the former store
structure. The ground surface is raised in the area in which the pipes were found, and are
possibly the location of the USTs. The surrounding property is primarily residential areas
and farmland. Photographs of the site and surrounding area are included in Appendix I.
3.2 Water Supply Wells
On March 8, 2012, S&ME performed a visual reconnaissance survey for public and
private water supply wells within 1,000 feet of the subject site. S&ME identified 19
possible private water supply wells within 1,000 feet of the site (Figure 3). The adjacent
property owner and water supply well information is included in Table 1.
3.3 Public Water Supplies
Public water is currently not available in the vicinity.
3.4 Surface Water
According to the 2010 Vicksboro USGS Quadrangle Map, an unnamed pond is located
approximately 1,500 feet to the southwest of the site. No other surface water bodies were
observed within 1,500 feet of the site during S&ME’s area reconnaissance.
Receptor Survey and Groundwater Monitoring Report S&ME Project No. 1354-12-055
TF-11828 Judy Faulkner-Smith Property April 2, 2012

4
4.0 WATER SUPPLY WELL SAMPLING

Site activities were performed in general accordance with a site-specific health and safety
plan (HASP) prepared by S&ME. The assessment was conducted in general accordance
with the procedures outlined in the NCDENR UST Section, Guidelines for the
Assessment and Corrective Action for UST Releases, July 2008 (Guidelines).
4.1 Water Supply Well Sampling

On March 8, 2012, S&ME sampled three water supply wells at and adjacent to the
Faulkner-Smith residence (3-6 Faulkner-Smith (site water supply well), 3-1 Faulkner-Smith,
and B-29 Roberts). Water supply wells were sampled at the outside spigot closest to the
water supply well. The spigot was opened and allowed to run for a minimum of 10 minutes
before sampling, after which S&ME reduced the flow and the water was placed directly into
laboratory-supplied containers.

The samples were stored in a cooler with ice, and shipped under chain-of-custody
procedures to Pace Analytical Laboratories (Pace) of Huntersville, North Carolina, a North
Carolina certified laboratory for analysis. The groundwater sample was analyzed for VOCs
by EPA Method 6200B.
4.2 Monitor Well Sampling Results

The laboratory analytical results of the water supply well samples collected on March 8,
2012 reported one VOC, MTBE, above the laboratory reporting limit but below the 2L
Standard in water supply well 3-6. No other constituents were detected at or above the
laboratory method detection limits in any of the wells sampled.

A summary of groundwater analytical results and a comparison to NCDENR’s regulatory
standards is included on Table 2. The groundwater constituent concentrations are
presented on Figure 4. A copy of the laboratory analytical results and chain-of-custody
form is included in Appendix II.

Receptor Survey and Groundwater Monitoring Report S&ME Project No. 1354-12-055
TF-11828 Judy Faulkner-Smith Property April 2, 2012

5
5.0 CONCLUSIONS AND RECOMMENDATIONS

A groundwater monitoring event and receptor survey update was conducted at the
Faulkner-Smith site located at 1300 Vicksboro Road, Henderson, North Carolina to
assess potential petroleum impact to water supply wells from a former UST system.

 On March 8, 2012, S&ME performed a receptor survey update to identify public and
private water supply wells, and other receptors within 1,000 feet of the subject site.
S&ME identified 19 private water supply wells within 1,000 feet of the site. No
surface water bodies were identified within 1,000 feet of the site. According to the
City of Henderson, municipal drinking water is not available to the site and properties
within 1,000 feet of the site.

 On March 8, 2012, S&ME personnel collected groundwater samples from three water
supply wells. One constituent, MTBE, was reported in water supply well 3-6 above
the laboratory method detection limit, but below the 2L Standard.

 During the site reconnaissance, S&ME observed possible UST fill ports and vent
pipes adjacent to the former store.

S&ME Recommends:

 Conducting a geophysical survey to verify the locations of the USTs observed
along the eastern side of the former store;

 Upon confirmation of the tank locations, S&ME recommends the removal of the
USTs and associated soil sampling; and,

 Until the source area is assessed and remediated, if needed, periodic sampling of
adjacent water supply wells is also recommended.

TABLES

Adjacent Property OwnersMap ID Parcel NumberLocation UsageDistance from source area of release(feet)Site 0532 030061300 Vicksboro Road, Henderson, NC 27537Residential Home100*1 0532 030020 Vicksboro Road, Henderson, NC 27537Undeveloped02 0532 01011356 Carey Chapel Road, Henderson, NC 27537Mobile HomesUnknownPublic and Private Water Supply WellsMap ID /Well IDParcel NumberLocation UsageDistance from source area of release(feet)Faulkner-Smith 3-60532 030061300 Vicksboro Road*Henderson, NC 27537Cooking, bathing; bottled water is being provided for drinkingSITEFaulkner-Smith 3-10532 030011300 Vicksboro Road*Henderson, NC 27537Drinking water3003-8 0532 03008180 Club Pond RoadHenderson, NC 27537Drinking water4506-46 0536 03046236 Club Pond RoadHenderson, NC 27537Drinking water8003-7 0532 0300725 Franklin RoadHenderson, NC 27537Drinking water7503-4 0532 030041148 Vicksboro RoadHenderson, NC 27537Drinking water4753-9 0532 030031204 Vicksboro RoadHenderson, NC 27537Drinking water5753-5 00532 030051250 Vicksboro RoadHenderson, NC 27537Drinking water8001-14 0532 010140 Willis Ferry LandHenderson, NC 27537Drinking water9001-28 0532 010281151 Vicksboro RoadHenderson, NC 27537Drinking water8001-12A 0532 01012238 Cary Chapel RoadHenderson, NC 27537Drinking water9701-12B 0532 01012238 Cary Chapel RoadHenderson, NC 27537Drinking water1,0001-11A 0532 01011356 Cary Chapel RoadHenderson, NC 27537Drinking water9501-11B 0532 01011356 Cary Chapel RoadHenderson, NC 27537Drinking water900Roberts B-29 0532B010300 G&G Meadows*Henderson, NC 27537Drinking water450B-28 0532B010280 G&G Meadows*Henderson, NC 27537Drinking water600B-27 0532B0102731 Gupton LaneHenderson, NC 27537Drinking water625B-26 0532B0102647 Gupton LaneHenderson, NC 27537Drinking water700B-6 0532B0100634 Gupton LaneHenderson, NC 27537Drinking water800Notes:Property owner information from the Vance County GIS Website*Properties listed with the same addressDescriptionContact/Telephone NumberResidential HomeCarl and Judy Smith / 252-915-3119Undeveloped LandRobert Faulkner / 919-365-9678Mobile HomesRussell Stevenson / 252-572-2133DescriptionContact / Telephone NumberResidential HomeCarl and Judy SmithResidential HomeCarl and Judy SmithResidential HomeSandra Kay ClarkResidential HomeJoshua A. NewmanResidential HomeStephen and Wanda FullerResidential HomeJohn and Linda HargroveResidential HomeElizabeth M. MedlinResidential HomeEugene and Joyce MatthewsResidential HomeJames A. FosterResidential HomeJerry and Reba SilvaLashonda DunstonResidential HomeWilliam M. and Rosa CarrollResidential HomeDenise and Wayne StevensonResidential HomeRussell W. StevensonResidential HomeRussell W. StevensonTABLE 1Receptor Information and Adjacent Property Owners - March 2012Judy Faulkner-Smith Residence1300 Vicksboro RoadHenderson, Vance County, North CarolinaNCDENR Incident No. 11828S&ME Project No. 1354-12-055Denise and Wayne StevensonResidential HomeResidential HomeRichard FainesResidential HomeCarlos and J. Hernandez SaldanaResidential HomePatricia A. RobertsResidential Home
Contaminant of ConcernBenzenesec-butylbenzeneDi-isopropyl etherEthylbenzeneIsoproplybenzeneMethyl-tert-butyl etherNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal xylenesDate6/3/20046.2BDL BDL2BDL3.5 3.3BDL <0.57.7 6.1 1511/14/20053.8BDL BDL BDL1 3.5 5.2BDL BDL13 12 213/8/2012BDL BDL BDL BDL BDL10.4BDL BDL BDL BDL BDL BDL6/3/2004BDL BDL BDL BDL BDL0.61BDL BDL BDL BDL BDL BDL11/14/2005BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL3/8/2012BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL6/3/2004BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL11/14/2005BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL3/8/2012BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL1 70 70 600 70 20 6 70 600 400 400 5005,000 8,500 70,000 84,500 25,000 20,000 6,000 30,000 260,000 28,500 25,000 85,500Notes:1. Analytes that are not shown were not detected for the method.2. All concentrations are reported in micrograms per liter (µg/L).3. NR: Anaylsis not Requested for sample4. All samples that exceed the 2L Standards are shown in Shaded and BOLD fields.5. Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.6. 2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202.7. BDL: Below Laboratory Detection LimitsTABLE 2Summary of Water Supply Well Analytical ResultsSample IDJudy Faulkner-Smith Property1300 Vicksboro RoadVolatile Organic Compounds by EPA 6200B or equivalentHenderson, Vance County, North CarolinaS&ME Project No. 1354-12-055NCDENR Incident No. 11828#3-6 Faulkner-Smith#3-1 Faulkner-SmithGross Contamination Levels2L Standards#B-29 Roberts

FIGURES

APPENDIX I

Photographic Log

Faulkner-Smith Property
Henderson, Vance County, North Carolina S&ME Project No. 1354-12-055
Taken by: CE Date Taken: 3/8/2012
1
1 Judy Faulkner Smith residence.2 Former Faulkner store.
3 Piping visible at northeast corner of the former store.4 Piping visible approximately 15 feet east of the former
store.
Faulkner-Smith Property
Henderson, Vance County, North Carolina S&ME Project No. 1354-12-055
Taken by: CE Date Taken: 3/8/2012
2
5 Partially uncovered piping.6 Northeast corner of the store where piping was
discovered.
7 View north across Vicksboro Road.8 Mobile home on road across from the Faulkner Smith
property, looking southwest.
Faulkner-Smith Property
Henderson, Vance County, North Carolina S&ME Project No. 1354-12-055
Taken by: CE Date Taken: 3/8/2012
3
9 View west on Vicksboro Road.10 Mobile home associated with water supply well 3-1.
11 View north along Gupton Lane.12 Water supply located at 1148 Vicksboro Road.

APPENDIX II

Laboratory Analytical Report and Chain of Custody Form
March 15, 2012
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 92113854
92113854
Project:
Pace Project No.:
RE:
Ms. Linda Blalock
NCDENR-UST Section
1637 Mail Service Center
Raleigh, NC 276991637
FAULKNER SMITH SITE TF#11828
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2012. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Erin Waters for
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92113854001 3-6 SM 6200B 64 PASI-CTLS
92113854002 B-29 SM 6200B 64 PASI-CTLS
92113854003 3-1 SM 6200B 64 PASI-CTLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92113854001 3-6
Methyl-tert-butyl ether 10.4 ug/L 03/12/12 23:500.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Method:
Client:S&ME_FTF_RDU
SM 6200B
Date:March 15, 2012
Description:6200B MSV
General Information:
3 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/18466
A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92113632032
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 734299)
• 1,1-Dichloroethane
• 1,1-Dichloropropene
• 2,2-Dichloropropane
• Bromochloromethane
• Bromomethane
• Chloroethane
• Chloromethane
• Diisopropyl ether
• cis-1,2-Dichloroethene
• trans-1,2-Dichloroethene
• MSD (Lab ID: 734300)
• 2,2-Dichloropropane
• Chloromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Method:
Client:S&ME_FTF_RDU
SM 6200B
Date:March 15, 2012
Description:6200B MSV
QC Batch: MSV/18466
A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92113632032
R1: RPD value was outside control limits.
• MSD (Lab ID: 734300)
• 2,2-Dichloropropane
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Sample:3-6 Lab ID:92113854001 Collected:03/08/12 10:15 Received:03/09/12 14:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene <0.50 ug/L 1 03/12/12 23:50 71-43-20.50
Bromobenzene <0.50 ug/L 1 03/12/12 23:50 108-86-10.50
Bromochloromethane <0.50 ug/L 1 03/12/12 23:50 74-97-50.50
Bromodichloromethane <0.50 ug/L 1 03/12/12 23:50 75-27-40.50
Bromoform <0.50 ug/L 1 03/12/12 23:50 75-25-20.50
Bromomethane <5.0 ug/L 1 03/12/12 23:50 74-83-95.0
n-Butylbenzene <0.50 ug/L 1 03/12/12 23:50 104-51-80.50
sec-Butylbenzene <0.50 ug/L 1 03/12/12 23:50 135-98-80.50
tert-Butylbenzene <0.50 ug/L 1 03/12/12 23:50 98-06-60.50
Carbon tetrachloride <0.50 ug/L 1 03/12/12 23:50 56-23-50.50
Chlorobenzene <0.50 ug/L 1 03/12/12 23:50 108-90-70.50
Chloroethane <1.0 ug/L 1 03/12/12 23:50 75-00-31.0
Chloroform <0.50 ug/L 1 03/12/12 23:50 67-66-30.50
Chloromethane <1.0 ug/L 1 03/12/12 23:50 74-87-31.0
2-Chlorotoluene <0.50 ug/L 1 03/12/12 23:50 95-49-80.50
4-Chlorotoluene <0.50 ug/L 1 03/12/12 23:50 106-43-40.50
1,2-Dibromo-3-chloropropane <1.0 ug/L 1 03/12/12 23:50 96-12-81.0
Dibromochloromethane <0.50 ug/L 1 03/12/12 23:50 124-48-10.50
1,2-Dibromoethane (EDB)<0.50 ug/L 1 03/12/12 23:50 106-93-40.50
Dibromomethane <0.50 ug/L 1 03/12/12 23:50 74-95-30.50
1,2-Dichlorobenzene <0.50 ug/L 1 03/12/12 23:50 95-50-10.50
1,3-Dichlorobenzene <0.50 ug/L 1 03/12/12 23:50 541-73-10.50
1,4-Dichlorobenzene <0.50 ug/L 1 03/12/12 23:50 106-46-70.50
Dichlorodifluoromethane <0.50 ug/L 1 03/12/12 23:50 75-71-80.50
1,1-Dichloroethane <0.50 ug/L 1 03/12/12 23:50 75-34-30.50
1,2-Dichloroethane <0.50 ug/L 1 03/12/12 23:50 107-06-20.50
1,1-Dichloroethene <0.50 ug/L 1 03/12/12 23:50 75-35-40.50
cis-1,2-Dichloroethene <0.50 ug/L 1 03/12/12 23:50 156-59-20.50
trans-1,2-Dichloroethene <0.50 ug/L 1 03/12/12 23:50 156-60-50.50
1,2-Dichloropropane <0.50 ug/L 1 03/12/12 23:50 78-87-50.50
1,3-Dichloropropane <0.50 ug/L 1 03/12/12 23:50 142-28-90.50
2,2-Dichloropropane <0.50 ug/L 1 03/12/12 23:50 594-20-70.50
1,1-Dichloropropene <0.50 ug/L 1 03/12/12 23:50 563-58-60.50
cis-1,3-Dichloropropene <0.50 ug/L 1 03/12/12 23:50 10061-01-50.50
trans-1,3-Dichloropropene <0.50 ug/L 1 03/12/12 23:50 10061-02-60.50
Diisopropyl ether <0.50 ug/L 1 03/12/12 23:50 108-20-30.50
Ethylbenzene <0.50 ug/L 1 03/12/12 23:50 100-41-40.50
Hexachloro-1,3-butadiene <2.0 ug/L 1 03/12/12 23:50 87-68-32.0
Isopropylbenzene (Cumene)<0.50 ug/L 1 03/12/12 23:50 98-82-80.50
Methylene Chloride <2.0 ug/L 1 03/12/12 23:50 75-09-22.0
Methyl-tert-butyl ether 10.4 ug/L 1 03/12/12 23:50 1634-04-40.50
Naphthalene <2.0 ug/L 1 03/12/12 23:50 91-20-32.0
n-Propylbenzene <0.50 ug/L 1 03/12/12 23:50 103-65-10.50
Styrene <0.50 ug/L 1 03/12/12 23:50 100-42-50.50
1,1,1,2-Tetrachloroethane <0.50 ug/L 1 03/12/12 23:50 630-20-60.50
1,1,2,2-Tetrachloroethane <0.50 ug/L 1 03/12/12 23:50 79-34-50.50
Tetrachloroethene <0.50 ug/L 1 03/12/12 23:50 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 7 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Sample:3-6 Lab ID:92113854001 Collected:03/08/12 10:15 Received:03/09/12 14:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene <0.50 ug/L 1 03/12/12 23:50 108-88-30.50
1,2,3-Trichlorobenzene <2.0 ug/L 1 03/12/12 23:50 87-61-62.0
1,2,4-Trichlorobenzene <2.0 ug/L 1 03/12/12 23:50 120-82-12.0
1,1,1-Trichloroethane <0.50 ug/L 1 03/12/12 23:50 71-55-60.50
1,1,2-Trichloroethane <0.50 ug/L 1 03/12/12 23:50 79-00-50.50
Trichloroethene <0.50 ug/L 1 03/12/12 23:50 79-01-60.50
Trichlorofluoromethane <1.0 ug/L 1 03/12/12 23:50 75-69-41.0
1,2,3-Trichloropropane <0.50 ug/L 1 03/12/12 23:50 96-18-40.50
1,2,4-Trimethylbenzene <0.50 ug/L 1 03/12/12 23:50 95-63-60.50
1,3,5-Trimethylbenzene <0.50 ug/L 1 03/12/12 23:50 108-67-80.50
Vinyl chloride <1.0 ug/L 1 03/12/12 23:50 75-01-41.0
m&p-Xylene <1.0 ug/L 1 03/12/12 23:50 179601-23-11.0
o-Xylene <0.50 ug/L 1 03/12/12 23:50 95-47-60.50
Surrogates
1,2-Dichloroethane-d4 (S)102 %1 03/12/12 23:50 17060-07-070-130
Dibromofluoromethane (S)97 %1 03/12/12 23:50 1868-53-770-130
4-Bromofluorobenzene (S)103 %1 03/12/12 23:50 460-00-470-130
Toluene-d8 (S)99 %1 03/12/12 23:50 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 8 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Sample:B-29 Lab ID:92113854002 Collected:03/08/12 11:15 Received:03/09/12 14:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene <0.50 ug/L 1 03/13/12 00:11 71-43-20.50
Bromobenzene <0.50 ug/L 1 03/13/12 00:11 108-86-10.50
Bromochloromethane <0.50 ug/L 1 03/13/12 00:11 74-97-50.50
Bromodichloromethane <0.50 ug/L 1 03/13/12 00:11 75-27-40.50
Bromoform <0.50 ug/L 1 03/13/12 00:11 75-25-20.50
Bromomethane <5.0 ug/L 1 03/13/12 00:11 74-83-95.0
n-Butylbenzene <0.50 ug/L 1 03/13/12 00:11 104-51-80.50
sec-Butylbenzene <0.50 ug/L 1 03/13/12 00:11 135-98-80.50
tert-Butylbenzene <0.50 ug/L 1 03/13/12 00:11 98-06-60.50
Carbon tetrachloride <0.50 ug/L 1 03/13/12 00:11 56-23-50.50
Chlorobenzene <0.50 ug/L 1 03/13/12 00:11 108-90-70.50
Chloroethane <1.0 ug/L 1 03/13/12 00:11 75-00-31.0
Chloroform <0.50 ug/L 1 03/13/12 00:11 67-66-30.50
Chloromethane <1.0 ug/L 1 03/13/12 00:11 74-87-31.0
2-Chlorotoluene <0.50 ug/L 1 03/13/12 00:11 95-49-80.50
4-Chlorotoluene <0.50 ug/L 1 03/13/12 00:11 106-43-40.50
1,2-Dibromo-3-chloropropane <1.0 ug/L 1 03/13/12 00:11 96-12-81.0
Dibromochloromethane <0.50 ug/L 1 03/13/12 00:11 124-48-10.50
1,2-Dibromoethane (EDB)<0.50 ug/L 1 03/13/12 00:11 106-93-40.50
Dibromomethane <0.50 ug/L 1 03/13/12 00:11 74-95-30.50
1,2-Dichlorobenzene <0.50 ug/L 1 03/13/12 00:11 95-50-10.50
1,3-Dichlorobenzene <0.50 ug/L 1 03/13/12 00:11 541-73-10.50
1,4-Dichlorobenzene <0.50 ug/L 1 03/13/12 00:11 106-46-70.50
Dichlorodifluoromethane <0.50 ug/L 1 03/13/12 00:11 75-71-80.50
1,1-Dichloroethane <0.50 ug/L 1 03/13/12 00:11 75-34-30.50
1,2-Dichloroethane <0.50 ug/L 1 03/13/12 00:11 107-06-20.50
1,1-Dichloroethene <0.50 ug/L 1 03/13/12 00:11 75-35-40.50
cis-1,2-Dichloroethene <0.50 ug/L 1 03/13/12 00:11 156-59-20.50
trans-1,2-Dichloroethene <0.50 ug/L 1 03/13/12 00:11 156-60-50.50
1,2-Dichloropropane <0.50 ug/L 1 03/13/12 00:11 78-87-50.50
1,3-Dichloropropane <0.50 ug/L 1 03/13/12 00:11 142-28-90.50
2,2-Dichloropropane <0.50 ug/L 1 03/13/12 00:11 594-20-70.50
1,1-Dichloropropene <0.50 ug/L 1 03/13/12 00:11 563-58-60.50
cis-1,3-Dichloropropene <0.50 ug/L 1 03/13/12 00:11 10061-01-50.50
trans-1,3-Dichloropropene <0.50 ug/L 1 03/13/12 00:11 10061-02-60.50
Diisopropyl ether <0.50 ug/L 1 03/13/12 00:11 108-20-30.50
Ethylbenzene <0.50 ug/L 1 03/13/12 00:11 100-41-40.50
Hexachloro-1,3-butadiene <2.0 ug/L 1 03/13/12 00:11 87-68-32.0
Isopropylbenzene (Cumene)<0.50 ug/L 1 03/13/12 00:11 98-82-80.50
Methylene Chloride <2.0 ug/L 1 03/13/12 00:11 75-09-22.0
Methyl-tert-butyl ether <0.50 ug/L 1 03/13/12 00:11 1634-04-40.50
Naphthalene <2.0 ug/L 1 03/13/12 00:11 91-20-32.0
n-Propylbenzene <0.50 ug/L 1 03/13/12 00:11 103-65-10.50
Styrene <0.50 ug/L 1 03/13/12 00:11 100-42-50.50
1,1,1,2-Tetrachloroethane <0.50 ug/L 1 03/13/12 00:11 630-20-60.50
1,1,2,2-Tetrachloroethane <0.50 ug/L 1 03/13/12 00:11 79-34-50.50
Tetrachloroethene <0.50 ug/L 1 03/13/12 00:11 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 9 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Sample:B-29 Lab ID:92113854002 Collected:03/08/12 11:15 Received:03/09/12 14:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene <0.50 ug/L 1 03/13/12 00:11 108-88-30.50
1,2,3-Trichlorobenzene <2.0 ug/L 1 03/13/12 00:11 87-61-62.0
1,2,4-Trichlorobenzene <2.0 ug/L 1 03/13/12 00:11 120-82-12.0
1,1,1-Trichloroethane <0.50 ug/L 1 03/13/12 00:11 71-55-60.50
1,1,2-Trichloroethane <0.50 ug/L 1 03/13/12 00:11 79-00-50.50
Trichloroethene <0.50 ug/L 1 03/13/12 00:11 79-01-60.50
Trichlorofluoromethane <1.0 ug/L 1 03/13/12 00:11 75-69-41.0
1,2,3-Trichloropropane <0.50 ug/L 1 03/13/12 00:11 96-18-40.50
1,2,4-Trimethylbenzene <0.50 ug/L 1 03/13/12 00:11 95-63-60.50
1,3,5-Trimethylbenzene <0.50 ug/L 1 03/13/12 00:11 108-67-80.50
Vinyl chloride <1.0 ug/L 1 03/13/12 00:11 75-01-41.0
m&p-Xylene <1.0 ug/L 1 03/13/12 00:11 179601-23-11.0
o-Xylene <0.50 ug/L 1 03/13/12 00:11 95-47-60.50
Surrogates
1,2-Dichloroethane-d4 (S)103 %1 03/13/12 00:11 17060-07-070-130
Dibromofluoromethane (S)99 %1 03/13/12 00:11 1868-53-770-130
4-Bromofluorobenzene (S)102 %1 03/13/12 00:11 460-00-470-130
Toluene-d8 (S)99 %1 03/13/12 00:11 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 10 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Sample:3-1 Lab ID:92113854003 Collected:03/08/12 11:50 Received:03/09/12 14:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene <0.50 ug/L 1 03/13/12 00:32 71-43-20.50
Bromobenzene <0.50 ug/L 1 03/13/12 00:32 108-86-10.50
Bromochloromethane <0.50 ug/L 1 03/13/12 00:32 74-97-50.50
Bromodichloromethane <0.50 ug/L 1 03/13/12 00:32 75-27-40.50
Bromoform <0.50 ug/L 1 03/13/12 00:32 75-25-20.50
Bromomethane <5.0 ug/L 1 03/13/12 00:32 74-83-95.0
n-Butylbenzene <0.50 ug/L 1 03/13/12 00:32 104-51-80.50
sec-Butylbenzene <0.50 ug/L 1 03/13/12 00:32 135-98-80.50
tert-Butylbenzene <0.50 ug/L 1 03/13/12 00:32 98-06-60.50
Carbon tetrachloride <0.50 ug/L 1 03/13/12 00:32 56-23-50.50
Chlorobenzene <0.50 ug/L 1 03/13/12 00:32 108-90-70.50
Chloroethane <1.0 ug/L 1 03/13/12 00:32 75-00-31.0
Chloroform <0.50 ug/L 1 03/13/12 00:32 67-66-30.50
Chloromethane <1.0 ug/L 1 03/13/12 00:32 74-87-31.0
2-Chlorotoluene <0.50 ug/L 1 03/13/12 00:32 95-49-80.50
4-Chlorotoluene <0.50 ug/L 1 03/13/12 00:32 106-43-40.50
1,2-Dibromo-3-chloropropane <1.0 ug/L 1 03/13/12 00:32 96-12-81.0
Dibromochloromethane <0.50 ug/L 1 03/13/12 00:32 124-48-10.50
1,2-Dibromoethane (EDB)<0.50 ug/L 1 03/13/12 00:32 106-93-40.50
Dibromomethane <0.50 ug/L 1 03/13/12 00:32 74-95-30.50
1,2-Dichlorobenzene <0.50 ug/L 1 03/13/12 00:32 95-50-10.50
1,3-Dichlorobenzene <0.50 ug/L 1 03/13/12 00:32 541-73-10.50
1,4-Dichlorobenzene <0.50 ug/L 1 03/13/12 00:32 106-46-70.50
Dichlorodifluoromethane <0.50 ug/L 1 03/13/12 00:32 75-71-80.50
1,1-Dichloroethane <0.50 ug/L 1 03/13/12 00:32 75-34-30.50
1,2-Dichloroethane <0.50 ug/L 1 03/13/12 00:32 107-06-20.50
1,1-Dichloroethene <0.50 ug/L 1 03/13/12 00:32 75-35-40.50
cis-1,2-Dichloroethene <0.50 ug/L 1 03/13/12 00:32 156-59-20.50
trans-1,2-Dichloroethene <0.50 ug/L 1 03/13/12 00:32 156-60-50.50
1,2-Dichloropropane <0.50 ug/L 1 03/13/12 00:32 78-87-50.50
1,3-Dichloropropane <0.50 ug/L 1 03/13/12 00:32 142-28-90.50
2,2-Dichloropropane <0.50 ug/L 1 03/13/12 00:32 594-20-70.50
1,1-Dichloropropene <0.50 ug/L 1 03/13/12 00:32 563-58-60.50
cis-1,3-Dichloropropene <0.50 ug/L 1 03/13/12 00:32 10061-01-50.50
trans-1,3-Dichloropropene <0.50 ug/L 1 03/13/12 00:32 10061-02-60.50
Diisopropyl ether <0.50 ug/L 1 03/13/12 00:32 108-20-30.50
Ethylbenzene <0.50 ug/L 1 03/13/12 00:32 100-41-40.50
Hexachloro-1,3-butadiene <2.0 ug/L 1 03/13/12 00:32 87-68-32.0
Isopropylbenzene (Cumene)<0.50 ug/L 1 03/13/12 00:32 98-82-80.50
Methylene Chloride <2.0 ug/L 1 03/13/12 00:32 75-09-22.0
Methyl-tert-butyl ether <0.50 ug/L 1 03/13/12 00:32 1634-04-40.50
Naphthalene <2.0 ug/L 1 03/13/12 00:32 91-20-32.0
n-Propylbenzene <0.50 ug/L 1 03/13/12 00:32 103-65-10.50
Styrene <0.50 ug/L 1 03/13/12 00:32 100-42-50.50
1,1,1,2-Tetrachloroethane <0.50 ug/L 1 03/13/12 00:32 630-20-60.50
1,1,2,2-Tetrachloroethane <0.50 ug/L 1 03/13/12 00:32 79-34-50.50
Tetrachloroethene <0.50 ug/L 1 03/13/12 00:32 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 11 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Sample:3-1 Lab ID:92113854003 Collected:03/08/12 11:50 Received:03/09/12 14:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene <0.50 ug/L 1 03/13/12 00:32 108-88-30.50
1,2,3-Trichlorobenzene <2.0 ug/L 1 03/13/12 00:32 87-61-62.0
1,2,4-Trichlorobenzene <2.0 ug/L 1 03/13/12 00:32 120-82-12.0
1,1,1-Trichloroethane <0.50 ug/L 1 03/13/12 00:32 71-55-60.50
1,1,2-Trichloroethane <0.50 ug/L 1 03/13/12 00:32 79-00-50.50
Trichloroethene <0.50 ug/L 1 03/13/12 00:32 79-01-60.50
Trichlorofluoromethane <1.0 ug/L 1 03/13/12 00:32 75-69-41.0
1,2,3-Trichloropropane <0.50 ug/L 1 03/13/12 00:32 96-18-40.50
1,2,4-Trimethylbenzene <0.50 ug/L 1 03/13/12 00:32 95-63-60.50
1,3,5-Trimethylbenzene <0.50 ug/L 1 03/13/12 00:32 108-67-80.50
Vinyl chloride <1.0 ug/L 1 03/13/12 00:32 75-01-41.0
m&p-Xylene <1.0 ug/L 1 03/13/12 00:32 179601-23-11.0
o-Xylene <0.50 ug/L 1 03/13/12 00:32 95-47-60.50
Surrogates
1,2-Dichloroethane-d4 (S)92 %1 03/13/12 00:32 17060-07-070-130
Dibromofluoromethane (S)92 %1 03/13/12 00:32 1868-53-770-130
4-Bromofluorobenzene (S)106 %1 03/13/12 00:32 460-00-470-130
Toluene-d8 (S)97 %1 03/13/12 00:32 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 12 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/18466
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92113854001, 92113854002, 92113854003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:733558
Associated Lab Samples:92113854001, 92113854002, 92113854003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 03/12/12 22:04
1,1,1-Trichloroethane ug/L <0.50 0.50 03/12/12 22:04
1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 03/12/12 22:04
1,1,2-Trichloroethane ug/L <0.50 0.50 03/12/12 22:04
1,1-Dichloroethane ug/L <0.50 0.50 03/12/12 22:04
1,1-Dichloroethene ug/L <0.50 0.50 03/12/12 22:04
1,1-Dichloropropene ug/L <0.50 0.50 03/12/12 22:04
1,2,3-Trichlorobenzene ug/L <2.0 2.0 03/12/12 22:04
1,2,3-Trichloropropane ug/L <0.50 0.50 03/12/12 22:04
1,2,4-Trichlorobenzene ug/L <2.0 2.0 03/12/12 22:04
1,2,4-Trimethylbenzene ug/L <0.50 0.50 03/12/12 22:04
1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 03/12/12 22:04
1,2-Dibromoethane (EDB)ug/L <0.50 0.50 03/12/12 22:04
1,2-Dichlorobenzene ug/L <0.50 0.50 03/12/12 22:04
1,2-Dichloroethane ug/L <0.50 0.50 03/12/12 22:04
1,2-Dichloropropane ug/L <0.50 0.50 03/12/12 22:04
1,3,5-Trimethylbenzene ug/L <0.50 0.50 03/12/12 22:04
1,3-Dichlorobenzene ug/L <0.50 0.50 03/12/12 22:04
1,3-Dichloropropane ug/L <0.50 0.50 03/12/12 22:04
1,4-Dichlorobenzene ug/L <0.50 0.50 03/12/12 22:04
2,2-Dichloropropane ug/L <0.50 0.50 03/12/12 22:04
2-Chlorotoluene ug/L <0.50 0.50 03/12/12 22:04
4-Chlorotoluene ug/L <0.50 0.50 03/12/12 22:04
Benzene ug/L <0.50 0.50 03/12/12 22:04
Bromobenzene ug/L <0.50 0.50 03/12/12 22:04
Bromochloromethane ug/L <0.50 0.50 03/12/12 22:04
Bromodichloromethane ug/L <0.50 0.50 03/12/12 22:04
Bromoform ug/L <0.50 0.50 03/12/12 22:04
Bromomethane ug/L <5.0 5.0 03/12/12 22:04
Carbon tetrachloride ug/L <0.50 0.50 03/12/12 22:04
Chlorobenzene ug/L <0.50 0.50 03/12/12 22:04
Chloroethane ug/L <1.0 1.0 03/12/12 22:04
Chloroform ug/L <0.50 0.50 03/12/12 22:04
Chloromethane ug/L <1.0 1.0 03/12/12 22:04
cis-1,2-Dichloroethene ug/L <0.50 0.50 03/12/12 22:04
cis-1,3-Dichloropropene ug/L <0.50 0.50 03/12/12 22:04
Dibromochloromethane ug/L <0.50 0.50 03/12/12 22:04
Dibromomethane ug/L <0.50 0.50 03/12/12 22:04
Dichlorodifluoromethane ug/L <0.50 0.50 03/12/12 22:04
Diisopropyl ether ug/L <0.50 0.50 03/12/12 22:04
Ethylbenzene ug/L <0.50 0.50 03/12/12 22:04
Hexachloro-1,3-butadiene ug/L <2.0 2.0 03/12/12 22:04
Isopropylbenzene (Cumene)ug/L <0.50 0.50 03/12/12 22:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 13 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:733558
Associated Lab Samples:92113854001, 92113854002, 92113854003
Matrix:Water
Analyzed
m&p-Xylene ug/L <1.0 1.0 03/12/12 22:04
Methyl-tert-butyl ether ug/L <0.50 0.50 03/12/12 22:04
Methylene Chloride ug/L <2.0 2.0 03/12/12 22:04
n-Butylbenzene ug/L <0.50 0.50 03/12/12 22:04
n-Propylbenzene ug/L <0.50 0.50 03/12/12 22:04
Naphthalene ug/L <2.0 2.0 03/12/12 22:04
o-Xylene ug/L <0.50 0.50 03/12/12 22:04
sec-Butylbenzene ug/L <0.50 0.50 03/12/12 22:04
Styrene ug/L <0.50 0.50 03/12/12 22:04
tert-Butylbenzene ug/L <0.50 0.50 03/12/12 22:04
Tetrachloroethene ug/L <0.50 0.50 03/12/12 22:04
Toluene ug/L <0.50 0.50 03/12/12 22:04
trans-1,2-Dichloroethene ug/L <0.50 0.50 03/12/12 22:04
trans-1,3-Dichloropropene ug/L <0.50 0.50 03/12/12 22:04
Trichloroethene ug/L <0.50 0.50 03/12/12 22:04
Trichlorofluoromethane ug/L <1.0 1.0 03/12/12 22:04
Vinyl chloride ug/L <1.0 1.0 03/12/12 22:04
1,2-Dichloroethane-d4 (S)%93 70-130 03/12/12 22:04
4-Bromofluorobenzene (S)%104 70-130 03/12/12 22:04
Dibromofluoromethane (S)%93 70-130 03/12/12 22:04
Toluene-d8 (S)%97 70-130 03/12/12 22:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
733559LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.650 111 60-140
1,1,1-Trichloroethane ug/L 54.950 110 60-140
1,1,2,2-Tetrachloroethane ug/L 52.650 105 60-140
1,1,2-Trichloroethane ug/L 52.250 104 60-140
1,1-Dichloroethane ug/L 50.850 102 60-140
1,1-Dichloroethene ug/L 54.350 109 60-140
1,1-Dichloropropene ug/L 52.950 106 60-140
1,2,3-Trichlorobenzene ug/L 54.850 110 60-140
1,2,3-Trichloropropane ug/L 54.750 109 60-140
1,2,4-Trichlorobenzene ug/L 55.350 111 60-140
1,2,4-Trimethylbenzene ug/L 53.850 108 60-140
1,2-Dibromo-3-chloropropane ug/L 57.350 115 60-140
1,2-Dibromoethane (EDB)ug/L 53.950 108 60-140
1,2-Dichlorobenzene ug/L 52.150 104 60-140
1,2-Dichloroethane ug/L 50.750 101 60-140
1,2-Dichloropropane ug/L 49.450 99 60-140
1,3,5-Trimethylbenzene ug/L 52.850 106 60-140
1,3-Dichlorobenzene ug/L 51.750 103 60-140
1,3-Dichloropropane ug/L 51.550 103 60-140
1,4-Dichlorobenzene ug/L 49.950 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 14 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
733559LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 52.450 105 60-140
2-Chlorotoluene ug/L 52.650 105 60-140
4-Chlorotoluene ug/L 52.450 105 60-140
Benzene ug/L 52.150 104 60-140
Bromobenzene ug/L 51.050 102 60-140
Bromochloromethane ug/L 42.650 85 60-140
Bromodichloromethane ug/L 53.250 106 60-140
Bromoform ug/L 60.550 121 60-140
Bromomethane ug/L 58.950 118 60-140
Carbon tetrachloride ug/L 50.250 100 60-140
Chlorobenzene ug/L 52.050 104 60-140
Chloroethane ug/L 49.550 99 60-140
Chloroform ug/L 50.850 102 60-140
Chloromethane ug/L 54.150 108 60-140
cis-1,2-Dichloroethene ug/L 48.250 96 60-140
cis-1,3-Dichloropropene ug/L 52.550 105 60-140
Dibromochloromethane ug/L 56.250 112 60-140
Dibromomethane ug/L 50.550 101 60-140
Dichlorodifluoromethane ug/L 64.950 130 60-140
Diisopropyl ether ug/L 48.650 97 60-140
Ethylbenzene ug/L 52.150 104 60-140
Hexachloro-1,3-butadiene ug/L 56.450 113 60-140
Isopropylbenzene (Cumene)ug/L 54.050 108 60-140
m&p-Xylene ug/L 107100 107 60-140
Methyl-tert-butyl ether ug/L 50.950 102 60-140
Methylene Chloride ug/L 45.050 90 60-140
n-Butylbenzene ug/L 53.850 108 60-140
n-Propylbenzene ug/L 52.350 105 60-140
Naphthalene ug/L 60.650 121 60-140
o-Xylene ug/L 51.750 103 60-140
sec-Butylbenzene ug/L 52.850 106 60-140
Styrene ug/L 54.150 108 60-140
tert-Butylbenzene ug/L 52.950 106 60-140
Tetrachloroethene ug/L 54.750 109 60-140
Toluene ug/L 50.150 100 60-140
trans-1,2-Dichloroethene ug/L 51.150 102 60-140
trans-1,3-Dichloropropene ug/L 53.650 107 60-140
Trichloroethene ug/L 53.150 106 60-140
Trichlorofluoromethane ug/L 54.750 109 60-140
Vinyl chloride ug/L 56.450 113 60-140
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%103 70-130
Dibromofluoromethane (S)%99 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 15 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
734299MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92113632032
734300
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 71 60-14090 2320ND14.2 17.9
1,1,1-Trichloroethane ug/L 20 63 60-14078 2120ND12.7 15.6
1,1,2,2-Tetrachloroethane ug/L 20 70 60-14087 2120ND14.1 17.3
1,1,2-Trichloroethane ug/L 20 73 60-14089 2020ND14.6 17.9
1,1-Dichloroethane ug/L M0205260-14068 2620ND10.4 13.5
1,1-Dichloroethene ug/L 20 63 60-14077 2020ND12.6 15.3
1,1-Dichloropropene ug/L M0205760-14073 2420ND11.5 14.5
1,2,3-Trichlorobenzene ug/L 20 75 60-14091 2020ND15.0 18.3
1,2,3-Trichloropropane ug/L 20 77 60-14092 1820ND15.3 18.4
1,2,4-Trichlorobenzene ug/L 20 74 60-14091 2120ND14.7 18.2
1,2,4-Trimethylbenzene ug/L 20 72 60-14088 2020ND14.5 17.6
1,2-Dibromo-3-chloropropane ug/L 20 78 60-14096 2120ND15.7 19.3
1,2-Dibromoethane (EDB)ug/L 20 71 60-14088 2120ND14.3 17.6
1,2-Dichlorobenzene ug/L 20 70 60-14086 2120ND14.0 17.3
1,2-Dichloroethane ug/L 20 65 60-14079 2020ND13.0 15.8
1,2-Dichloropropane ug/L 20 61 60-14074 1920ND12.1 14.8
1,3,5-Trimethylbenzene ug/L 20 69 60-14086 2120ND13.8 17.1
1,3-Dichlorobenzene ug/L 20 69 60-14086 2120ND13.9 17.1
1,3-Dichloropropane ug/L 20 65 60-14081 2220ND12.9 16.1
1,4-Dichlorobenzene ug/L 20 68 60-14083 1920ND13.7 16.5
2,2-Dichloropropane ug/L M0,R1204160-14058 3520ND8.2 11.7
2-Chlorotoluene ug/L 20 67 60-14084 2320ND13.5 16.9
4-Chlorotoluene ug/L 20 71 60-14086 2020ND14.2 17.3
Benzene ug/L 20 65 60-14081 2120ND13.1 16.2
Bromobenzene ug/L 20 66 60-14081 2020ND13.2 16.2
Bromochloromethane ug/L M0205760-14067 1620ND11.4 13.3
Bromodichloromethane ug/L 20 69 60-14083 1820ND13.9 16.6
Bromoform ug/L 20 81 60-14098 1920ND16.2 19.6
Bromomethane ug/L M0205860-14071 2020ND11.7 14.3
Carbon tetrachloride ug/L 20 63 60-14079 2220ND12.6 15.7
Chlorobenzene ug/L 20 70 60-14086 2020ND14.0 17.1
Chloroethane ug/L M0205460-14064 1720ND10.8 12.7
Chloroform ug/L 20 64 60-14081 2420ND12.7 16.1
Chloromethane ug/L M0204660-14058 2220ND9.3 11.6
cis-1,2-Dichloroethene ug/L M0205760-14071 2320ND11.4 14.3
cis-1,3-Dichloropropene ug/L 20 61 60-14076 2220ND12.2 15.2
Dibromochloromethane ug/L 20 73 60-14089 2120ND14.5 17.9
Dibromomethane ug/L 20 72 60-14088 1920ND14.4 17.5
Dichlorodifluoromethane ug/L 20 61 60-14076 2320ND12.1 15.2
Diisopropyl ether ug/L M0205760-14072 2220ND11.4 14.3
Ethylbenzene ug/L 20 69 60-14084 2020ND13.8 16.8
Hexachloro-1,3-butadiene ug/L 20 80 60-14098 2120ND16.0 19.7
Isopropylbenzene (Cumene)ug/L 20 69 60-14083 1920ND13.7 16.6
m&p-Xylene ug/L 40 69 60-14085 2040ND27.8 34.0
Methyl-tert-butyl ether ug/L 20 64 60-14080 2320ND12.7 16.1
Methylene Chloride ug/L 20 65 60-14082 2420ND13.0 16.5
n-Butylbenzene ug/L 20 68 60-14086 2320ND13.7 17.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 16 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
734299MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92113632032
734300
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 65 60-14079 1920ND13.1 15.9
Naphthalene ug/L 20 87 60-140109 2220ND17.5 21.8
o-Xylene ug/L 20 66 60-14080 1920ND13.1 15.9
sec-Butylbenzene ug/L 20 66 60-14082 2220ND13.3 16.5
Styrene ug/L 20 68 60-14086 2320ND13.7 17.3
tert-Butylbenzene ug/L 20 67 60-14082 2120ND13.3 16.4
Tetrachloroethene ug/L 20 68 60-14086 2320ND13.6 17.1
Toluene ug/L 20 66 60-14080 2020ND13.1 16.1
trans-1,2-Dichloroethene ug/L M0205760-14071 2220ND11.4 14.2
trans-1,3-Dichloropropene ug/L 20 65 60-14081 2220ND13.0 16.2
Trichloroethene ug/L 20 68 60-14084 2220ND13.6 16.9
Trichlorofluoromethane ug/L 20 65 60-14079 2020ND12.9 15.8
Vinyl chloride ug/L 20 63 60-14077 2120ND12.5 15.5
1,2-Dichloroethane-d4 (S)%103 70-130104
4-Bromofluorobenzene (S)%106 70-130103
Dibromofluoromethane (S)%99 70-130101
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 17 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 18 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92113854
FAULKNER SMITH SITE TF#11828
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92113854001 MSV/184663-6 SM 6200B
92113854002 MSV/18466B-29 SM 6200B
92113854003 MSV/184663-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/15/2012 03:43 PM Page 19 of 19
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]