HomeMy WebLinkAboutRA-494_2067_CA_FPR_202308302725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
Telephone 919-871-0999
www.atcgroupservices.com
ATC Project No. STL0206701 NCDEQ State Lead Program
August 30, 2023
Ms. Linda Blalock
North Carolina Department of Environmental Quality
Division of Waste Management
Underground Storage Tank Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Subject: Free Product Recovery and Groundwater Monitoring Letter Report
Faison’s Community
Intersection of Galatia Road and US Highway 158
Conway, Northampton County, North Carolina
NCDEQ Incident No. 2067
UST No. RA-494
Dear Ms. Blalock:
ATC Associates of North Carolina, P.C. (ATC) is pleased to submit the results of an aggressive fluid vapor
recovery (AFVR) event conducted on June 20, 2023, at the Faisons Community property located at the
intersection of Galatia Road and US Highway 158, Conway, North Carolina. The AFVR event was
performed based on an May 15, 2023, Task Authorization (TA-01) by the Trust Fund Branch of the
Underground Storage Tank (UST) Section, Division of Waste Management (DWM), North Carolina
Department of Environmental Quality (NCDEQ). The work is being performed as part of State Lead Contract
#N70522-B between NCDEQ and ATC.
The property is associated with one parcel that is developed with a residential building and the other that is
developed with a commercial building that appears to be used as a storage unit by the property owner. A
site topographic map is included as Figure 1. The site formerly utilized one 400-gallon UST, one 14,000-
gallon UST, and one 10,000-gallon UST, all of unknown contents and were removed in 2009. Eight Type II
monitoring wells (MW-1 through MW-8) are associated with the site. A site map depicting pertinent site
features is included as Figure 2. Based on ATC’s findings, it appears there are nine water supply wells
within 1,000 feet of the source area. Of the nine wells, six are inactive, one is used for drinking purposes,
and two are used for irrigation purposes, none of the water supply wells are within 250 feet of the source
area. Municipal water is available to all properties within the area. Water supply well ownership information
is included in Table 1 and the water supply well locations are depicted on the Potential Receptor Map
included as Figure 3.
On June 20, 2023, Eastern Environmental Management, LLC (Eastern) was subcontracted to perform an
eight-hour aggressive fluid vapor recovery (AFVR) event using MW-8 as an extraction point. Light non-
aqueous phase liquid (LNAPL) was previously detected in well MW-8 during the January 13, 2023 sampling
event. Prior to and following the event, ATC gauged MW-8 for liquid levels. LNAPL was detected at a
thickness of 0.26 feet prior to the AFVR event and was not detected following the event. Monitoring well
construction details and groundwater elevation data are included as Table 2 and 3, respectively. The AFVR
event began at 08:00 am and ended at 04:00 pm and generated approximately 675 gallons of petroleum
impacted groundwater from well MW-8. The AFVR calculations are included as Table 4. Field notes for the
field activities are included in Appendix A. The waste disposal manifest from the event is provided in
Appendix B. Based on calculated recovery volumes for the AFVR event, an estimated 3.39 gallons (0.54
pounds) of petroleum were recovered as vapors.
Faison’s Community
August 30, 2023
ATC Project No. STL0206701 NCDEQ State Lead Program
Attachments:
Table 1 – Water Supply Well Information
Table 2 – Well Construction Information
Table 3 – Groundwater Elevation Data
Table 4 – Field Data Measurements and Total Emissions Calculations
Table 5 – Groundwater Analytical Data
Table 6 – Historical Groundwater Analytical Data
Table 7 – Field Parameters
Figure 1 – Site Topographic Map
Figure 2 – Site Map
Figure 3 – Potential Receptor Map
Appendix A – Field Notes
Appendix B – Waste Disposal Manifest
Appendix C – Laboratory Analytical Report
Faison’s Community
ATC Project No. STL0206701 NCDEQ State Lead Program
TABLES
TABLE 1
WATER SUPPLY WELL INFORMATION
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
Well
Identification Property Owner and Address Property Address Well Use Approximate Distance
to Well (feet)
Registered for
Municipal Water
WSW-1
W.N. Jr. and Maggie Taylor
8457 US Highway 158
Seaboard, NC 27876
252-585-0553
8779 US 158 Highway Inactive 265 Yes
WSW-2
Beatrice Barnes
8923 US Highway 158
Conway, NC 27820
252-585-1748
8841 US Highway 158 Inactive 490 No
WSW-3
Lillie Ray
8742 US 158 Highway
Seaborad, NC 27876
252-585-9900
8742 US Highway 158 Inactive 495 Yes
WSW-4
Timothy and Shannon Byers
8754 US Highway 158
Seaboard, NC 27876
252-678-2421
8754 US Highway 158 Irrigation 410 Yes
WSW-5
Joyce Taylor
8727 US 158 Highway
Seaboard, NC 27876
252-585-0080
8727 US Highway 158 Irrigation 800 Yes
WSW-6
Ronnie and Maxine Hasty
8677 US 158 Highway
Seaboard, NC 27876
252-585-1855
8677 US Highway 158 Drinking 1,350 No
WSW-7
NC District of Council of Assembly of
God, Inc.
P.O. Box 250
Conway, NC 27820
252-585-1533
8852 US Highway 158 Inactive 744 Yes
WSW-8
Faisons Assembly of God
P.O. Box 250
Conway, NC 27820
252-585-1533
8842 US Highway 158 Inactive 500 Yes
WSW-9
Willie Norman
910 Greenhall Road
Edenton, NC 27932
252-564-4944
US Highway 158 Inactive 1,375 Yes
WSW-10
Beatrice Barnes
8923 US Highway 158
Conway, NC 27820
Phone Number Not Available
8849 US 158 Highway Inactive 590 No
WSW-11
Timothy and Crystal Stauffer
8678 US 158 Highway
Seaboard, NC 27876
Phone Number Not Available
8678 US 158 Highway Drinking
(assumed)1,370 No
WSW-12
Benjamin Wheeler
160 NCHS East Road
Conway, NC 27820
Phone Number Not Available
160 NCHS East Road Drinking
(assumed)707 No
Notes:
1. Water supply well information is based on well survey and interviews conducted during previous assessment activities.
2. Distances are based on the location of the water supply well in relation to the nearest former UST basin.
Page 1 of 1
TABLE 2
WELL CONSTRUCTION INFORMATION
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
Well ID Date of
Installation
Well Diameter
(inches)
Screen Slot
(inches)
Total Depth
(feet)
Screened Interval
(feet)
MW-1 4/7/2009 2.00 0.010 33 13-33
MW-2 4/7/2009 2.00 0.010 30 10-30
MW-3 6/2/2009 2.00 0.010 30 10-30
MW-4 6/2/2009 2.00 0.010 30 10-30
MW-5 6/3/2009 2.00 0.010 35 15-35
MW-6 7/27/2018 2.00 0.010 30 15-30
MW-7 7/27/2018 2.00 0.010 30 15-30
MW-8 2/24/2021 2.00 0.010 30 15-30
Page 1 of 1
TABLE 3
GROUNDWATER ELEVATION DATA
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
4/7/2009 ----21.96 75.10
7/24/2015 ----
10/6/2017 ----19.75 77.31
8/6/2018 ----19.30 77.76
6/24/2019 ----17.47 79.59
10/25/2019 ----NM NM
3/30/2020 ----NM NM
3/8/2021 ----16.94 80.12
6/17/2022 ----20.94 76.12
4/7/2009 ----26.10 73.47
7/24/2015 ----21.48 78.09
10/6/2017 ----24.04 75.53
8/6/2018 ----23.95 75.62
6/24/2019 ----21.86 77.71
10/25/2019 ----23.80 75.77
3/30/2020 ----24.15 75.42
3/8/2021 ----21.98 77.59
6/3/2009 ----19.68 75.64
7/24/2015 ----16.91 78.41
10/6/2017 ----17.65 77.67
8/6/2018 ----16.98 78.34
6/24/2019 ----15.36 79.96
10/25/2019 ----18.25 77.07
3/30/2020 ----17.10 78.22
3/8/2021 ----14.59 80.73
6/3/2009 ----24.08 74.63
7/24/2015 ----23.8 74.91
2/24/16 (Pre-AFVR)----20.93 77.78
2/24/16 (Post-AFVR)----21.79 76.92
3/25/2016 ----20.68 78.03
8/24/17 (Pre-AFVR)----21.89 76.82
8/24/17 (Post-AFVR)----25.55 73.16
10/6/2017 ----21.98 76.73
8/6/2018 ----21.68 77.03
5/24/2019 ----19.32 79.39
6/24/2019 ----19.71 79.00
10/25/2019 ----22.13 76.58
3/30/2020 ----21.45 77.26
3/8/2021 ----19.45 79.26
9/21/2021 ----20.8 77.91
6/17/2022 ----23.11 75.60
7/20/2023 ----23.68 75.03
6/3/2009 ----25.81 72.89
7/24/2015 ----23.7 75.00
10/6/2017 ----23.86 74.84
8/6/2018 ----23.80 74.90
6/24/2019 ----21.83 76.87
10/25/2019 ----23.61 75.09
3/30/2020 ----25.08 73.62
3/8/2021 ----22.02 76.68
8/6/2018 ----24.56 74.93
6/24/2019 ----22.97 76.52
10/25/2019 ----24.80 74.69
3/30/2020 ----25.18 74.31
3/8/2021 ----23.24 76.25
8/6/2018 ----26.35 76.34
6/24/2019 ----17.46 85.23
10/25/2019 ----18.85 83.84
3/30/2020 ----17.94 84.75
3/8/2021 ----16.49 86.20
3/8/2021 ----19.15 79.04
9/21/2021 20.18 1.14 21.32 77.85
5/17/2022 22.32 1.37 23.69 75.68
6/17/2022 ----22.76 75.43
11/15/2022 (Pre-AFVR)24.10 0.30 24.40 74.05
11/15/2022 (Post-AFVR)----24.47 73.72
1/13/2023 24.51 0.04 24.55 73.67
6/20/2023 (Pre-AFVR)23.18 0.26 23.44 74.97
6/20/2023 (Post-AFVR)----23.38 74.81
7/20/2023 23.30 0.02 23.32 74.89
Notes
1. LNAPL - Light non-aqueous phase liquid.
2. -- = LNAPL Not detected.
3. Formula for determing groundwater elevation when free product detected = TOC Elevation - Depth to Groundwater + [0.8581*LNAPL Thickeness].
4. TOC = Top of Casing.
5. NM = Not Measured.
MW-8 98.19
MW-4 98.71
LNAPL Thickness
(feet)
MW-5
MW-2
Groundwater
Elevation (feet)Well ID Sample Date
98.70
MW-3
MW-7 102.69
Depth to LNAPL
(feet)
Could Not Locate
99.49MW-6
99.57
95.32
Depth to Groundwater
(feet)
Top of Casing
Elevation (feet)
MW-1 97.06
TABLE 4
FIELD DATA MEASUREMENTS AND TOTAL EMISSIONS CALCULATIONS - June 20, 2023
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
Time Delta Time
(minute)
VOC
Concentration
(ppm)
Velocity
(feet/minute)
Temp
(˚F)
Relative
Humidity
(%)
Stack
Diameter
(inches)
Air Flow
(cfm)
Specific
Humidity
(lbW/lbDA)
Water
Vapor
(vol %)
Dry Basis
Air Flow
(dscfm)
Dry VOC
Concentration
(ppm)
Response
Factor
Corrected VOC
Concentration
(ppm)
Mass
Concentration
(mg/m3)
Mass
Concentration
(lb/ft3)
Mass
Removed
(lb)
8:00 0 349.8 109 79.1 100.0 6.0 21 0.022 0.033 20 362 1 362 1925 0.000120 0.00
8:15 15 266.1 106 82.7 100.0 6.0 21 0.024 0.037 20 276 1 276 1469 0.000092 0.03
8:30 15 364.1 110 91.2 100.0 6.0 22 0.032 0.049 20 383 1 383 2035 0.000127 0.04
8:45 15 396.2 117 115.9 100.0 6.0 22 0.071 0.102 18 441 1 441 2347 0.000146 0.04
9:00 15 1,695 109 129.3 100.0 6.0 21 0.109 0.149 16 1991 1 1991 10588 0.000661 0.16
9:15 15 1,431 103 135.9 100.0 6.0 21 0.134 0.177 15 1738 1 1738 9244 0.000577 0.13
9:30 15 1,425 123 142.2 100.0 6.0 21 0.164 0.208 15 1798 1 1798 9563 0.000597 0.13
9:45 15 1,434 112 147.0 100.0 6.0 21 0.191 0.234 14 1873 1 1873 9959 0.000622 0.13
10:15 15 1,526 143 152.9 100.0 6.0 21 0.232 0.271 13 2093 1 2093 11131 0.000695 0.14
10:45 30 1,326 120 160.3 100.0 6.0 20 0.300 0.325 11 1963 1 1963 10440 0.000652 0.22
11:15 30 1,325 161 163.1 100.0 6.0 20 0.331 0.347 11 2028 1 2028 10783 0.000673 0.22
11:45 30 1,517 181 162.1 100.0 6.0 20 0.320 0.339 11 2294 1 2294 12200 0.000762 0.26
12:45 30 1,472 127 165.7 100.0 6.0 20 0.365 0.369 11 2332 1 2332 12399 0.000774 0.25
13:45 60 1,240 182 165.5 100.0 6.0 20 0.362 0.367 11 1959 1 1959 10417 0.000650 0.42
14:45 60 1,273 119 162.6 100.0 6.0 20 0.326 0.343 11 1937 1 1937 10300 0.000643 0.43
15:45 60 1,212 168 167.1 100.0 6.0 20 0.384 0.381 10 1958 1 1958 10411 0.000650 0.41
16:00 60 1,148 164 163.2 100.0 6.0 20 0.333 0.348 11 1761 1 1761 9362 0.000584 0.39
3.39
Total Emissions in Gallons 0.54
Notes:
VOC = Volatile organic compounds measured using a photoionization detector (PID)
ppm = parts per million
cfm = cubic feet per minute
Air Flow= π*(Stack Diameter (in.)/12/2)2*Velocity
Specific Humidity = Data from psychrometric chart at measured temperature and relative humidity in pounds of water per pound of dry air (lbW/lbDA).
Water Vapor = % water vapor on a volume basis = (Specific Humidity / 18 lb-mole H2O) / [(1 / 28.84 lb-mole dry air) + (Specific Humidity / 18 lb-mole H2O)]
Dry Basis Air Flow = Flow volume on a dry basis at a standard temperature of 68˚F = (1-Water Vapor) (Air Flow) [528˚R / (Temperature+460)]
dscfm = dry standard cubic feet per minute
Dry VOC Concentration = [VOC Concentration / (1-Water Vapor)]
Response Factor = Response Factor of PID; 1 if response factor is unknown
Corrected VOC Concentration = Dry VOC Concentration x Response Factor
Mass Concentration (mg/m3) = Mass concentration VOC as gasoline dry basis at standard temperature = (Corrected VOC Concentration) (128 mg/mg-mole / 24.07 m3/mg-mole)
Mass Concentration (lb/ft3) = [Mass Concentration (mg/m3)] [(6.243 * 10-8)(lb/ft3)/(mg/m3)]
mg/m3 = milligrams per cubic meter
lb/ft3 = pounds per cubic foot
Mass Removed (lb) = [Mass Concentration (lb/ft3)] [Dry Basis Air Flow (dscfm)] [Time Interval (min)]
Total Emissions in Pounds
Page 1 of 1
TABLE 5
GROUNDWATER ANALYTICAL DATA
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
WELL ID SAMPLE
DATE
Benzene Toluene Ethylbenzene Total Xylenes Methyl Tert Butyl Ether 1,2-Dichloroethane n-Propylbenzene 1,2,4-Trimethylbenzene 1,3,5-TrimethylbenzeneMW-4 7/20/2023 1,680 Q 7,730 Q 928 Q 4480 Q 42.1 JQ 48.4 JQ 81.3 JQ 629 Q 177 JQ
MW-8 7/20/2023
1 600 600 500 20 0.4 70 400 400
5,000 260,000 80,000 50,000 20,000 400 26,100 28,500 24,100
Notes:
1. All measurements are in micrograms per liter (ug/L).
2. "<" or ND = None detected above method detection limit.
3. 2L Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
4. GCL = Gross Contaminant Level established by NCDEQ.
5. Concentrations in BOLD print equal or exceed the NCDEQ 2L Standard.
6. LNAPL = Light Non-Aqueous Phase Liquid.
7. J = Indicates and estimated value.
8. Q = Sample was prepared and/or analyzed past holding tim eas defined in the method. Concentations should be considered minimum values.
GCLs
ANALYTICAL METHOD EPA 6200B
Not Sampled - LNAPL Present (Thickness 0.02 feet)
2L Standards
Page 1 of 1
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL DATA
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
EPA
Method
6020
Benzene Toluene Ethylbenzene Total Xylenes Methyl Tert Butyl Ether Naphthalene 1,2-Dibromoethane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene 1,2-Dichloroethane Isopropylbenzene n-Butylbenzene n-Propylbenzene Tetrachloroethene 2-Methylnaphthalene Naphthalene Lead C5-C8 Aliphatics C9-C18 Aliphatics C19-C36 Aliphatics C9-C22 Aromatics1 600 600 500 20 6 0.02 400 400 0.4 70 70 70 0.7 30 6 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 50 28,500 24,100 400 30,500 5,900 26,100 700 12,000 6,000 15,000 NE NE NE NE
4/7/2009 890 620 370 1,760 <2 92 --1,900 590 33 --88 280 <2 NA 57 49 6,300 11,500 <200 7,930
7/24/2015
10/6/2017 150 270 73 402 9.9 20 <5.0 480 170 7.7 19 17 67 <5.0 NA NA NA NA NA NA NA
8/6/2018 519 986 144 799 14.7 12.8 5.2 613 208 140 19.4 22.6 86.2 <5.0 NA NA NA NA NA NA NA
6/24/2019
10/25/2019 78.0 <10 22.2 171 <10 11.7 <10 378 137 5.5 11.6 <10 56.5 <10 NA NA NA NA NA NA NA
3/30/2020 494 730 69.1 554 25.1 5.6 <5.0 213 84.7 20.9 7.7 <5.0 26.3 <5.0 NA NA NA NA NA NA NA
3/8/2021 267 769 163 907 <25.0 48.2 J 7.07 J 754 248 <25.0 31.3 <25.0 130 <25.0 NA NA NA NA NA NA NA
4/7/2009 480 11,000 1,100 6,300 <20 460 --1,100 280 <20 --37 120 --NA 360 172 23,000 17,000 <200 6,600
7/24/2015 120 1,100 210 1,310 <1.8 68 <1.8 450 130 <3.9 16 35J 53 <1.6 18 24 250 5,900 270 <100 2,300
10/6/2017 130 2,200 430 2,550 <12 190 <12 630 200 <12 24 33 72 <12 NA NA NA NA NA NA NA
8/6/2018 107 1,550 334 1,860 <10 155 <10 441 177 <4.0 14.5 <10 66.1 <10 NA NA NA NA NA NA NA
6/24/2019 113 1,930 400 2,180 <10 174 <10 610 179 <4.0 21.8 <10 76.4 <10 NA NA NA NA NA NA NA
10/25/2019 105 1,680 385 1,830 <10 164 <10 500 174 <10 19.5 11.3 69.2 <10 NA NA NA NA NA NA NA
3/30/2020 69.8 923 198 986 <10 103 <10 189 90.9 4.3 11.1 <10 30.2 <10 NA NA NA NA NA NA NA
3/8/2021 59.1 842 217 1,085 0.124 J 57.8 J <1.00 270 88.9 0.224 J 17.2 44.6 55.0 <1.00 NA NA NA NA NA NA NA
6/3/2009 2.6 18 2.9 12.4 <0.2 0.15 <0.1 1.4 <0.49 <0.1 <0.2 <0.1 0.27 0.53 45 96 <10 45 36 <200 <180
7/24/2015 <0.079 <0.09 <0.092 <0.18 <0.09 <0.12 <0.089 <0.18 <0.1 <0.19 <0.11 <0.054 <0.094 <0.08 <1.4 <1.4 73 <100 ND <100 ND
10/6/2017 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
8/6/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
6/24/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
10/25/2019 <0.50 <0.50 <0.50 0.74 <0.50 1.4 <0.50 0.58 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
3/30/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
3/8/2021 0.57 J <1.00 <1.00 <2.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA NA NA NA
6/3/2009 1,600 6,000 870 4,200 64 260 35 960 270 37 38 41 130 <10 77 310 11.2 23,000 13,500 <200 7,130
7/24/2015 7,200 33,000 2,800 12,600 520 490 84J 1,900 750 320 68J 24J 230 <16 72 370 72 86,000 2,100 <100 11,570
3/25/2016 3,400 12,000 1,500 6,900 280 420 <24 1,000 280 <39 42J 48J 130 <34 NA NA NA NA NA NA NA
10/6/2017 5,300 20,000 2,200 10,400 400 880 80J 1,400 410 230 56J <200 210 <200 NA NA NA NA NA NA NA
8/6/2018 5,630 24,100 3,130 15,700 335 607 114 1,940 578 161 <100 <100 251 <100 NA NA NA NA NA NA NA
5/24/2019 (30 days post-
injection)2,780 12,700 1,960 9,720 <100 374 <100 1,580 433 106 <100 <100 193 <100 NA NA NA NA NA NA NA
6/24/2019 (60 days post-
injection)2,720 11,400 1,580 8,140 <100 491 <100 1,420 363 98.6 <100 <100 146 <100 NA NA NA NA NA NA NA
10/25/2019 (6 months
post-injection)3,600 14,000 1,730 8,400 358 577 <100 1,390 350 225 <100 <100 147 <100 NA NA NA NA NA NA NA
3/30/2020 (12 months
post-injection)3,590 15,000 2,240 11,100 271 629 <100 1,710 488 240 <100 <100 190 <100 NA NA NA NA NA NA NA
3/8/2021 1,840 9,320 1,500 7,290 73.9 319 32.8 J 1,390 381 83.7 45.0 J <50.0 166 <50.0 NA NA NA NA NA NA NA
9/21/2021 2,540 12,700 1,880 8,920 125 556 <100 1,780 471 121 52.4 J 32.7 J 200 <100 NA NA NA NA NA NA NA
6/17/2022 1,300 7,230 990 4,190 132 454 <50 1,090 261 <20 32.3 J 42.4 J 125 <50 NA NA NA NA NA NA NA
7/20/2023 1,680 Q 7,730 Q 928 Q 4,480 Q 42.1 JQ <1,000 Q <200 Q 629 Q 177 JQ 48.4 JQ <200 Q <200 Q 81.3 JQ <200 Q NA NA NA NA NA NA NA
2L Standards
GCLs
MW-2
MW-3
MW-4
WELL I.D.SAMPLE DATE
EPA Method 6200B EPA Method 625 MADEP EPH and VPH
MW-1
Not Sampled/Could Not Locate
Damaged - Unable to Collect Sample
Page 1 of 2
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL DATA
FAISONS COMMUNITY
INTERSECTION OF US 158 HIGHWAY AND GALATIA ROAD
CONWAY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
EPA
Method
6020
Benzene Toluene Ethylbenzene Total Xylenes Methyl Tert Butyl Ether Naphthalene 1,2-Dibromoethane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene 1,2-Dichloroethane Isopropylbenzene n-Butylbenzene n-Propylbenzene Tetrachloroethene 2-Methylnaphthalene Naphthalene Lead C5-C8 Aliphatics C9-C18 Aliphatics C19-C36 Aliphatics C9-C22 Aromatics1 600 600 500 20 6 0.02 400 400 0.4 70 70 70 0.7 30 6 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 50 28,500 24,100 400 30,500 5,900 26,100 700 12,000 6,000 15,000 NE NE NE NE
2L Standards
GCLs
WELL I.D.SAMPLE DATE
EPA Method 6200B EPA Method 625 MADEP EPH and VPH
6/3/2009 280 1,600 740 4,600 <2 340 <1 980 250 <1 40 26 99 6 <5 <5 35 9,900 9,990 <200 5,780
7/24/2015 180 10,000 1,500 8,900 <4.5 500 <4.4 1,400 340 <9.7 53 26 150 <4 58 300 <0.11 32,000 690 <100 6,920
10/6/2017 140 6,900 1,100 6,500 <50 460 <50 1,000 250 <50 42J 22J 100 <50 NA NA NA NA NA NA NA
8/6/2018 141 6,490 1,380 8,410 <25 576 <25 1,520 423 <10 44.6 <25 161 <25 NA NA NA NA NA NA NA
6/24/2019 159 12,200 1,340 8,610 <25 535 <25 1,370 317 <10 48.0 <25 136 <25 NA NA NA NA NA NA NA
10/25/2019 117 8,010 1,160 6,440 <25 564 <25 1,190 290 <25 37.9 <25 109 <25 NA NA NA NA NA NA NA
3/30/2020 71.5 5,900 1,170 7,170 <50 530 <50 1,220 309 <20 <50 <50 104 <50 NA NA NA NA NA NA NA
3/8/2021 77.8 6,770 1,160 7,530 <50.0 501 <50.0 1,330 303 <50.0 49.6 J <50.0 126 <50.0 NA NA NA NA NA NA NA
8/6/2018 <0.50 <0.50 <0.50 1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
6/24/2019 <0.50 4.9 0.56 36.5 <0.50 5.1 <0.50 14.7 3.0 <0.20 0.87 <0.50 0.71 <0.50 NA NA NA NA NA NA NA
10/25/2019 2.5 84.4 8.1 259.0 <0.50 41.1 <0.50 68.1 24.7 <0.50 5.0 1.6 <0.50 <0.50 NA NA NA NA NA NA NA
3/30/2020 0.69 2.7 <0.50 30.8 <0.50 5.5 <0.50 8.7 <0.50 <0.20 0.89 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
3/8/2021 0.168 J 23.0 5.22 32.46 <1.00 13.1 <1.00 8.65 1.83 <1.00 0.216 J <1.00 1.09 <1.00 NA NA NA NA NA NA NA
8/6/2018 2.9 0.57 <0.50 0.95 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
6/24/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
10/25/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
3/30/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA
3/8/2021 0.440 J 6.15 1.78 8.06 <1.00 1.90 J <1.00 2.25 0.607 J <1.00 <1.00 <1.00 0.385 J <1.00 NA NA NA NA NA NA NA
3/8/2021 2,710 14,800 2,770 14,050 <200 1,090 27.6 J 3,260 903 47.8 J 118 J 267 465 <200 NA NA NA NA NA NA NA
9/21/2021
6/17/2022 1,810 16,600 5,910 33,500 <100 7,020 <100 30,600 E 5,500 <40 480 1,810 2,470 <100 NA NA NA NA NA NA NA
1/13/2023
7/20/2023
Notes:
1. All measurements are in micrograms per liter (ug/L).
2. "<" or ND = None detected above method detection limit or reporting limit.
3. 2L Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
4. GCL = Gross Contaminant Level established by NCDEQ.
5. NE = Not established.
6. J = Indicates and estimated value.
7. Values in Bold print indicate levels above 2L Groundwater Standards.
8. Concentrations in Bold Italics print equal or exceed the GCLs.
9. C9-C18 Aliphatics equals the sum of C9-C12 aliphatics and C9-C18 aliphatics as reported in the laboratory report.
10. C9-C22 Aromatics equals the sum of C9-10 aromatics and C11-C22 aromatics as reported in the laboratory report.
11. LNAPL = Light Non-Aqueous Phase Liquid.
12. Q = Sample was prepared and/or analyzed past holding tim eas defined in the method. Concentations should be considered minimum values.
Not Sampled - LNAPL Present (Thickness 0.04 feet)
Not Sampled - LNAPL Present (Thickness 0.02 feet)
MW-8
MW-5
MW-6
MW-7
Not Sampled - LNAPL Present (Thickness 1.14 feet)
Page 2 of 2
TABLE 7
FIELD PARAMETERS
FAISONS COMMUNITY
INTERSECTION OF US HWY 158 AND GALATIA
CONWAY, NORTHAMPTON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 2067
8/6/2018 21.96 1.17 0.224 5.84 64.9
6/24/2019
10/25/2019 19.9 1.30 0.0835 5.33 193.4
3/30/2020 22.26 1.17 0.107 5.35 -102.7
3/8/2021
8/6/2018 21.50 0.88 0.110 4.53 218.2
6/24/2019 26.1 2.02 0.182 4.80 111.1
10/25/2019 19.3 0.50 0.1152 5.09 -22.8
3/30/2020 23.14 1.00 0.119 4.96 -58.5
3/8/2021 18.5 0.73 0.091 5.42 115.8
8/6/2018 19.78 6.14 0.093 4.53 223.7
6/24/2019 22.3 5.35 0.1356 4.99 244.0
10/25/2019 19.5 5.06 0.0823 4.44 251.1
3/30/2020 25.61 4.10 0.201 4.25 155.3
3/8/2021 19.1 4.00 0.0864 4.97 164.3
8/6/2018 22.08 0.61 0.145 5.09 140.2
6/24/2019 25.0 1.62 0.578 5.34 48.9
10/25/2019 20.4 1.17 0.1457 5.13 100.6
3/30/2020
3/8/2021 19.5 0.91 0.2264 5.33 114.3
9/21/2021
6/17/2022 23.4 1.42 0.181 5.68 165.3
7/20/2023 21.10 1.67 0.136 7.31 35.7
8/6/2018 20.76 1.23 0.174 5.09 137.0
6/24/2019 23.0 2.80 0.1581 5.38 65.7
10/25/2019 19.9 0.81 0.1514 5.73 21.8
3/30/2020 22.59 1.26 0.141 4.53 93.1
3/8/2021 19.2 0.78 0.1364 5.83 78.7
8/6/2018 23.00 4.31 0.128 5.41 97.6
6/24/2019 24.2 3.96 0.1009 5.10 147.9
10/25/2019 20.0 3.79 0.0759 5.20 190.7
3/30/2020 22.28 2.64 0.061 4.49 159.9
3/8/2021 18.6 2.28 0.0541 5.63 126.6
8/6/2018 22.57 7.36 0.098 5.69 148.8
6/24/2019 23.1 7.12 0.1169 5.3 189.3
10/25/2019 18.9 4.55 0.0662 5.11 138.6
3/30/2020 20.09 5.52 0.087 3.97 192.8
3/8/2021 19.1 6.17 0.0769 5.38 176.3
3/8/2021
9/21/2021
6/17/2022
7/20/2023
Notes:
1. °C = degrees celsius.
2. mg/L = milligram per liter.
3. mS/cm = millisiemens per centimeter.
4. std unit = standard unit.
5. mV = millivolts.
6. LNAPL = Light non-aqueous phase liquid.Dissolved Oxygen (mg/L)Conductivity (ms/cm)Damaged - Unable to Sample
Not Collected - Strong Odor in Well
MW-7
MW-1
MW-5 Temperature (oC)Not Collected - Water Appeared to Have Sludge
MW-2 pHMW-3
Date
Collected
Not Collected - Sheen Present
MW-4
MW-8
Not Collected - LNAPL Present
Not Collected - Strong Odor in Well ORP (mV)MW-6
WELL ID
Not Collected - LNAPL Present
Not Collected - Strong Odor in Well
Page 1 of 1
Faison’s Community
ATC Project No. STL0206701 NCDEQ State Lead Program
FIGURES
2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
(919) 871-0999
FIGURE 1
SITE TOPOGRAPHIC MAP
PROJECT NO: SLC0206706
REVIEWED BY: AW SCALE: 1” = 775’DATE: 11/4/21
FAISONS COMMUNITY –INCIDENT #2067
INTERSECTION OF GALATIA ROAD AND
US HIGHWAY 158
CONWAY, NORTH CAROLINA
Source: My Free Topo
N
Site
CAD FILE PREP. BYDSCA #REV. BY SCALE PROJECT NO.
TITLE
DATE
NOTES:
Raleigh, North Carolina 27604 (919) 871-0999 FAX (919) 871-0335
2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
(919) 871-0999
FIGURE 3
POTENTIAL RECEPTOR MAP
PROJECT NO: SLC0206706
REVIEWED BY: EA SCALE: 1” = 400’DATE: 11/4/21
FAISONS COMMUNITY –INCIDENT #2067
INTERSECTION OF GALATIA ROAD AND
US HIGHWAY 158
CONWAY, NORTH CAROLINA
Source: Northampton County NC GIS
Drinking Water Supply Well
Irrigation Water Supply Well
Inactive Water Supply Well
500 Foot Radius
1,000 Foot Radius
Property Formerly
Containing Tank T-1
Property Formerly
Containing Tanks T-2, T-
3, and T-4 (Source Area)
WSW-1
WSW-2
WSW-3 WSW-4
N
WSW-5
WSW-6
WSW-7
WSW-8
WSW-9
WSW-10
WSW-11
WSW-12
Faison’s Community
ATC Project No. STL0206701 NCDEQ State Lead Program
APPENDIX A
FIELD NOTES
Faison’s Community
ATC Project No. STL0206701 NCDEQ State Lead Program
APPENDIX B
WASTE DISPOSAL MANIFEST
Faison’s Community
ATC Project No. STL0206701 NCDEQ State Lead Program
APPENDIX C
LABORATORY ANALYTICAL REPORT
ANALYTICAL REPORT
August 08, 2023
ATC Group Services LLC
Sample Delivery Group:L1638836
Samples Received:07/25/2023
Project Number:
Description:Faisons Community
Report To:Nicholas Kramer
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
Entire Report Reviewed By:
August 08, 2023
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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August 08, 2023
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-4 L1638836-01 5
FIELD BLANK L1638836-02 7
Qc: Quality Control Summary 9
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 9
Gl: Glossary of Terms 13
Al: Accreditations & Locations 14
Sc: Sample Chain of Custody 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-4 L1638836-01 GW Garrett Lewis 07/20/23 11:20 07/25/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2106395 200 08/04/23 00:40 08/04/23 00:40 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
FIELD BLANK L1638836-02 GW Garrett Lewis 07/20/23 11:30 07/25/23 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2106395 1 08/04/23 00:17 08/04/23 00:17 JHH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Project Narrative
Method 6200: Re-analysis performed out of hold due to failing QC in the initial in hold run.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1638836
MW-4
Collected date/time: 07/20/23 11:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U Q 2260 10000 200 08/04/2023 00:40 WG2106395
Acrolein U Q 508 10000 200 08/04/2023 00:40 WG2106395
Acrylonitrile U Q 134 2000 200 08/04/2023 00:40 WG2106395
Benzene 1680 Q 18.8 200 200 08/04/2023 00:40 WG2106395
Bromobenzene U Q 23.6 200 200 08/04/2023 00:40 WG2106395
Bromodichloromethane U Q 27.2 200 200 08/04/2023 00:40 WG2106395
Bromoform U Q 25.8 200 200 08/04/2023 00:40 WG2106395
Bromomethane U Q 121 1000 200 08/04/2023 00:40 WG2106395
n-Butylbenzene U Q 31.4 200 200 08/04/2023 00:40 WG2106395
sec-Butylbenzene U Q 25.0 200 200 08/04/2023 00:40 WG2106395
tert-Butylbenzene U Q 25.4 200 200 08/04/2023 00:40 WG2106395
Carbon tetrachloride U Q 25.6 200 200 08/04/2023 00:40 WG2106395
Chlorobenzene U Q 23.2 200 200 08/04/2023 00:40 WG2106395
Chlorodibromomethane U Q 28.0 200 200 08/04/2023 00:40 WG2106395
Chloroethane U Q 38.4 1000 200 08/04/2023 00:40 WG2106395
Chloroform U Q 22.2 1000 200 08/04/2023 00:40 WG2106395
Chloromethane U Q 192 500 200 08/04/2023 00:40 WG2106395
2-Chlorotoluene U Q 21.2 200 200 08/04/2023 00:40 WG2106395
4-Chlorotoluene U Q 22.8 200 200 08/04/2023 00:40 WG2106395
1,2-Dibromo-3-Chloropropane U Q 55.2 1000 200 08/04/2023 00:40 WG2106395
1,2-Dibromoethane U Q 25.2 200 200 08/04/2023 00:40 WG2106395
Dibromomethane U Q 24.4 200 200 08/04/2023 00:40 WG2106395
1,2-Dichlorobenzene U Q 21.4 200 200 08/04/2023 00:40 WG2106395
1,3-Dichlorobenzene U Q 22.0 200 200 08/04/2023 00:40 WG2106395
1,4-Dichlorobenzene U Q 24.0 200 200 08/04/2023 00:40 WG2106395
Dichlorodifluoromethane U Q 74.8 1000 200 08/04/2023 00:40 WG2106395
1,1-Dichloroethane U Q 20.0 200 200 08/04/2023 00:40 WG2106395
1,2-Dichloroethane 48.4 J Q 16.4 200 200 08/04/2023 00:40 WG2106395
1,1-Dichloroethene U Q 37.6 200 200 08/04/2023 00:40 WG2106395
cis-1,2-Dichloroethene U Q 25.2 200 200 08/04/2023 00:40 WG2106395
trans-1,2-Dichloroethene U Q 29.8 200 200 08/04/2023 00:40 WG2106395
1,2-Dichloropropane U Q 29.8 200 200 08/04/2023 00:40 WG2106395
1,1-Dichloropropene U Q 28.4 200 200 08/04/2023 00:40 WG2106395
1,3-Dichloropropane U Q 22.0 200 200 08/04/2023 00:40 WG2106395
2,2-Dichloropropane U Q 32.2 200 200 08/04/2023 00:40 WG2106395
Di-isopropyl ether U Q 21.0 200 200 08/04/2023 00:40 WG2106395
Ethylbenzene 928 Q 27.4 200 200 08/04/2023 00:40 WG2106395
Hexachloro-1,3-butadiene U Q 67.4 200 200 08/04/2023 00:40 WG2106395
Isopropylbenzene U Q 21.0 200 200 08/04/2023 00:40 WG2106395
p-Isopropyltoluene U Q 24.0 200 200 08/04/2023 00:40 WG2106395
2-Butanone (MEK)U Q 238 2000 200 08/04/2023 00:40 WG2106395
Methylene Chloride U Q 86.0 1000 200 08/04/2023 00:40 WG2106395
4-Methyl-2-pentanone (MIBK)U Q 95.6 2000 200 08/04/2023 00:40 WG2106395
Methyl tert-butyl ether 42.1 J Q 20.2 200 200 08/04/2023 00:40 WG2106395
Naphthalene U Q 200 1000 200 08/04/2023 00:40 WG2106395
n-Propylbenzene 81.3 J Q 19.9 200 200 08/04/2023 00:40 WG2106395
Styrene U Q 23.6 200 200 08/04/2023 00:40 WG2106395
1,1,1,2-Tetrachloroethane U Q 29.4 200 200 08/04/2023 00:40 WG2106395
1,1,2,2-Tetrachloroethane U Q 26.6 200 200 08/04/2023 00:40 WG2106395
Tetrachloroethene U Q 60.0 200 200 08/04/2023 00:40 WG2106395
Toluene 7730 Q 55.6 200 200 08/04/2023 00:40 WG2106395
1,2,3-Trichlorobenzene U Q 46.0 200 200 08/04/2023 00:40 WG2106395
1,2,4-Trichlorobenzene U Q 96.2 200 200 08/04/2023 00:40 WG2106395
1,1,1-Trichloroethane U Q 29.8 200 200 08/04/2023 00:40 WG2106395
1,1,2-Trichloroethane U Q 31.6 200 200 08/04/2023 00:40 WG2106395
Trichloroethene U Q 38.0 200 200 08/04/2023 00:40 WG2106395
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1638836
MW-4
Collected date/time: 07/20/23 11:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U Q 32.0 1000 200 08/04/2023 00:40 WG2106395
1,2,3-Trichloropropane U Q 47.4 500 200 08/04/2023 00:40 WG2106395
1,2,4-Trimethylbenzene 629 Q 64.4 200 200 08/04/2023 00:40 WG2106395
1,3,5-Trimethylbenzene 177 J Q 20.8 200 200 08/04/2023 00:40 WG2106395
Vinyl chloride U Q 46.8 200 200 08/04/2023 00:40 WG2106395
o-Xylene 1440 Q 34.8 200 200 08/04/2023 00:40 WG2106395
m&p-Xylenes 3040 Q 86.0 400 200 08/04/2023 00:40 WG2106395
(S) Toluene-d8 109 80.0-120 08/04/2023 00:40 WG2106395
(S) 4-Bromofluorobenzene 116 77.0-126 08/04/2023 00:40 WG2106395
(S) 1,2-Dichloroethane-d4 92.9 70.0-130 08/04/2023 00:40 WG2106395
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1638836
FIELD BLANK
Collected date/time: 07/20/23 11:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone 11.3 J Q 11.3 50.0 1 08/04/2023 00:17 WG2106395
Acrolein U Q 2.54 50.0 1 08/04/2023 00:17 WG2106395
Acrylonitrile U Q 0.671 10.0 1 08/04/2023 00:17 WG2106395
Benzene U Q 0.0941 1.00 1 08/04/2023 00:17 WG2106395
Bromobenzene U Q 0.118 1.00 1 08/04/2023 00:17 WG2106395
Bromodichloromethane U Q 0.136 1.00 1 08/04/2023 00:17 WG2106395
Bromoform U Q 0.129 1.00 1 08/04/2023 00:17 WG2106395
Bromomethane U Q 0.605 5.00 1 08/04/2023 00:17 WG2106395
n-Butylbenzene U Q 0.157 1.00 1 08/04/2023 00:17 WG2106395
sec-Butylbenzene U Q 0.125 1.00 1 08/04/2023 00:17 WG2106395
tert-Butylbenzene U Q 0.127 1.00 1 08/04/2023 00:17 WG2106395
Carbon tetrachloride U Q 0.128 1.00 1 08/04/2023 00:17 WG2106395
Chlorobenzene U Q 0.116 1.00 1 08/04/2023 00:17 WG2106395
Chlorodibromomethane U Q 0.140 1.00 1 08/04/2023 00:17 WG2106395
Chloroethane U Q 0.192 5.00 1 08/04/2023 00:17 WG2106395
Chloroform U Q 0.111 5.00 1 08/04/2023 00:17 WG2106395
Chloromethane U Q 0.960 2.50 1 08/04/2023 00:17 WG2106395
2-Chlorotoluene U Q 0.106 1.00 1 08/04/2023 00:17 WG2106395
4-Chlorotoluene U Q 0.114 1.00 1 08/04/2023 00:17 WG2106395
1,2-Dibromo-3-Chloropropane U Q 0.276 5.00 1 08/04/2023 00:17 WG2106395
1,2-Dibromoethane U Q 0.126 1.00 1 08/04/2023 00:17 WG2106395
Dibromomethane U Q 0.122 1.00 1 08/04/2023 00:17 WG2106395
1,2-Dichlorobenzene U Q 0.107 1.00 1 08/04/2023 00:17 WG2106395
1,3-Dichlorobenzene U Q 0.110 1.00 1 08/04/2023 00:17 WG2106395
1,4-Dichlorobenzene U Q 0.120 1.00 1 08/04/2023 00:17 WG2106395
Dichlorodifluoromethane U Q 0.374 5.00 1 08/04/2023 00:17 WG2106395
1,1-Dichloroethane U Q 0.100 1.00 1 08/04/2023 00:17 WG2106395
1,2-Dichloroethane U Q 0.0819 1.00 1 08/04/2023 00:17 WG2106395
1,1-Dichloroethene U Q 0.188 1.00 1 08/04/2023 00:17 WG2106395
cis-1,2-Dichloroethene U Q 0.126 1.00 1 08/04/2023 00:17 WG2106395
trans-1,2-Dichloroethene U Q 0.149 1.00 1 08/04/2023 00:17 WG2106395
1,2-Dichloropropane U Q 0.149 1.00 1 08/04/2023 00:17 WG2106395
1,1-Dichloropropene U Q 0.142 1.00 1 08/04/2023 00:17 WG2106395
1,3-Dichloropropane U Q 0.110 1.00 1 08/04/2023 00:17 WG2106395
2,2-Dichloropropane U Q 0.161 1.00 1 08/04/2023 00:17 WG2106395
Di-isopropyl ether U Q 0.105 1.00 1 08/04/2023 00:17 WG2106395
Ethylbenzene U Q 0.137 1.00 1 08/04/2023 00:17 WG2106395
Hexachloro-1,3-butadiene U Q 0.337 1.00 1 08/04/2023 00:17 WG2106395
Isopropylbenzene U Q 0.105 1.00 1 08/04/2023 00:17 WG2106395
p-Isopropyltoluene U Q 0.120 1.00 1 08/04/2023 00:17 WG2106395
2-Butanone (MEK)5.19 J Q 1.19 10.0 1 08/04/2023 00:17 WG2106395
Methylene Chloride U Q 0.430 5.00 1 08/04/2023 00:17 WG2106395
4-Methyl-2-pentanone (MIBK)U Q 0.478 10.0 1 08/04/2023 00:17 WG2106395
Methyl tert-butyl ether U Q 0.101 1.00 1 08/04/2023 00:17 WG2106395
Naphthalene U Q 1.00 5.00 1 08/04/2023 00:17 WG2106395
n-Propylbenzene U Q 0.0993 1.00 1 08/04/2023 00:17 WG2106395
Styrene U Q 0.118 1.00 1 08/04/2023 00:17 WG2106395
1,1,1,2-Tetrachloroethane U Q 0.147 1.00 1 08/04/2023 00:17 WG2106395
1,1,2,2-Tetrachloroethane U Q 0.133 1.00 1 08/04/2023 00:17 WG2106395
Tetrachloroethene U Q 0.300 1.00 1 08/04/2023 00:17 WG2106395
Toluene U Q 0.278 1.00 1 08/04/2023 00:17 WG2106395
1,2,3-Trichlorobenzene U Q 0.230 1.00 1 08/04/2023 00:17 WG2106395
1,2,4-Trichlorobenzene U Q 0.481 1.00 1 08/04/2023 00:17 WG2106395
1,1,1-Trichloroethane U Q 0.149 1.00 1 08/04/2023 00:17 WG2106395
1,1,2-Trichloroethane U Q 0.158 1.00 1 08/04/2023 00:17 WG2106395
Trichloroethene U Q 0.190 1.00 1 08/04/2023 00:17 WG2106395
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1638836
FIELD BLANK
Collected date/time: 07/20/23 11:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U Q 0.160 5.00 1 08/04/2023 00:17 WG2106395
1,2,3-Trichloropropane U Q 0.237 2.50 1 08/04/2023 00:17 WG2106395
1,2,4-Trimethylbenzene U Q 0.322 1.00 1 08/04/2023 00:17 WG2106395
1,3,5-Trimethylbenzene U Q 0.104 1.00 1 08/04/2023 00:17 WG2106395
Vinyl chloride U Q 0.234 1.00 1 08/04/2023 00:17 WG2106395
o-Xylene U Q 0.174 1.00 1 08/04/2023 00:17 WG2106395
m&p-Xylenes U Q 0.430 2.00 1 08/04/2023 00:17 WG2106395
(S) Toluene-d8 108 80.0-120 08/04/2023 00:17 WG2106395
(S) 4-Bromofluorobenzene 112 77.0-126 08/04/2023 00:17 WG2106395
(S) 1,2-Dichloroethane-d4 95.7 70.0-130 08/04/2023 00:17 WG2106395
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2106395
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1638836-01,02
Method Blank (MB)
(MB) R3957034-3 08/03/23 23:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2106395
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1638836-01,02
Method Blank (MB)
(MB) R3957034-3 08/03/23 23:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 115 77.0-126
(S) 1,2-Dichloroethane-d4 95.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957034-1 08/03/23 22:33 • (LCSD) R3957034-2 08/03/23 22:56
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 28.5 31.4 114 126 19.0-160 9.68 27
Acrolein 25.0 22.7 24.8 90.8 99.2 10.0-160 8.84 26
Acrylonitrile 25.0 23.8 25.5 95.2 102 55.0-149 6.90 20
Benzene 5.00 4.74 4.85 94.8 97.0 70.0-123 2.29 20
Bromobenzene 5.00 4.70 4.78 94.0 95.6 73.0-121 1.69 20
Bromodichloromethane 5.00 4.77 4.65 95.4 93.0 75.0-120 2.55 20
Bromoform 5.00 4.53 4.81 90.6 96.2 68.0-132 6.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2106395
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1638836-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957034-1 08/03/23 22:33 • (LCSD) R3957034-2 08/03/23 22:56
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 3.49 2.92 69.8 58.4 10.0-160 17.8 25
n-Butylbenzene 5.00 4.33 4.33 86.6 86.6 73.0-125 0.000 20
sec-Butylbenzene 5.00 4.69 4.81 93.8 96.2 75.0-125 2.53 20
tert-Butylbenzene 5.00 4.51 4.65 90.2 93.0 76.0-124 3.06 20
Carbon tetrachloride 5.00 4.95 4.74 99.0 94.8 68.0-126 4.33 20
Chlorobenzene 5.00 4.85 5.11 97.0 102 80.0-121 5.22 20
Chlorodibromomethane 5.00 4.33 4.66 86.6 93.2 77.0-125 7.34 20
Chloroethane 5.00 5.83 6.01 117 120 47.0-150 3.04 20
Chloroform 5.00 4.79 4.90 95.8 98.0 73.0-120 2.27 20
Chloromethane 5.00 4.81 4.78 96.2 95.6 41.0-142 0.626 20
2-Chlorotoluene 5.00 4.49 4.69 89.8 93.8 76.0-123 4.36 20
4-Chlorotoluene 5.00 4.54 4.62 90.8 92.4 75.0-122 1.75 20
1,2-Dibromo-3-Chloropropane 5.00 3.66 4.01 73.2 80.2 58.0-134 9.13 20
1,2-Dibromoethane 5.00 4.67 4.90 93.4 98.0 80.0-122 4.81 20
Dibromomethane 5.00 4.64 4.92 92.8 98.4 80.0-120 5.86 20
1,2-Dichlorobenzene 5.00 4.25 4.31 85.0 86.2 79.0-121 1.40 20
1,3-Dichlorobenzene 5.00 4.31 4.40 86.2 88.0 79.0-120 2.07 20
1,4-Dichlorobenzene 5.00 4.20 4.25 84.0 85.0 79.0-120 1.18 20
Dichlorodifluoromethane 5.00 6.16 6.27 123 125 51.0-149 1.77 20
1,1-Dichloroethane 5.00 4.71 4.84 94.2 96.8 70.0-126 2.72 20
1,2-Dichloroethane 5.00 4.77 4.78 95.4 95.6 70.0-128 0.209 20
1,1-Dichloroethene 5.00 4.90 5.18 98.0 104 71.0-124 5.56 20
cis-1,2-Dichloroethene 5.00 4.63 4.96 92.6 99.2 73.0-120 6.88 20
trans-1,2-Dichloroethene 5.00 4.82 5.20 96.4 104 73.0-120 7.58 20
1,2-Dichloropropane 5.00 4.52 4.74 90.4 94.8 77.0-125 4.75 20
1,1-Dichloropropene 5.00 4.81 5.16 96.2 103 74.0-126 7.02 20
1,3-Dichloropropane 5.00 4.43 4.69 88.6 93.8 80.0-120 5.70 20
2,2-Dichloropropane 5.00 4.68 4.91 93.6 98.2 58.0-130 4.80 20
Di-isopropyl ether 5.00 4.47 4.51 89.4 90.2 58.0-138 0.891 20
Ethylbenzene 5.00 5.08 5.17 102 103 79.0-123 1.76 20
Hexachloro-1,3-butadiene 5.00 4.51 4.53 90.2 90.6 54.0-138 0.442 20
Isopropylbenzene 5.00 5.00 5.28 100 106 76.0-127 5.45 20
p-Isopropyltoluene 5.00 4.54 4.66 90.8 93.2 76.0-125 2.61 20
2-Butanone (MEK)25.0 25.0 29.9 100 120 44.0-160 17.9 20
Methylene Chloride 5.00 4.54 4.44 90.8 88.8 67.0-120 2.23 20
4-Methyl-2-pentanone (MIBK)25.0 22.9 24.8 91.6 99.2 68.0-142 7.97 20
Methyl tert-butyl ether 5.00 4.71 4.93 94.2 98.6 68.0-125 4.56 20
Naphthalene 5.00 3.58 3.73 71.6 74.6 54.0-135 4.10 20
n-Propylbenzene 5.00 4.82 4.75 96.4 95.0 77.0-124 1.46 20
Styrene 5.00 5.00 5.15 100 103 73.0-130 2.96 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2106395
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1638836-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957034-1 08/03/23 22:33 • (LCSD) R3957034-2 08/03/23 22:56
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,1,1,2-Tetrachloroethane 5.00 4.60 5.00 92.0 100 75.0-125 8.33 20
1,1,2,2-Tetrachloroethane 5.00 4.54 4.39 90.8 87.8 65.0-130 3.36 20
Tetrachloroethene 5.00 5.18 5.35 104 107 72.0-132 3.23 20
Toluene 5.00 4.56 4.72 91.2 94.4 79.0-120 3.45 20
1,2,3-Trichlorobenzene 5.00 3.98 4.17 79.6 83.4 50.0-138 4.66 20
1,2,4-Trichlorobenzene 5.00 3.70 3.80 74.0 76.0 57.0-137 2.67 20
1,1,1-Trichloroethane 5.00 5.23 5.36 105 107 73.0-124 2.46 20
1,1,2-Trichloroethane 5.00 4.61 4.83 92.2 96.6 80.0-120 4.66 20
Trichloroethene 5.00 5.32 5.31 106 106 78.0-124 0.188 20
Trichlorofluoromethane 5.00 5.62 6.08 112 122 59.0-147 7.86 20
1,2,3-Trichloropropane 5.00 5.04 5.15 101 103 73.0-130 2.16 20
1,2,4-Trimethylbenzene 5.00 5.00 4.96 100 99.2 76.0-121 0.803 20
1,3,5-Trimethylbenzene 5.00 4.73 4.83 94.6 96.6 76.0-122 2.09 20
Vinyl chloride 5.00 5.59 5.90 112 118 67.0-131 5.40 20
o-Xylene 5.00 4.94 5.16 98.8 103 80.0-122 4.36 20
m&p-Xylenes 10.0 10.0 10.4 100 104 80.0-122 3.92 20
(S) Toluene-d8 107 108 80.0-120
(S) 4-Bromofluorobenzene 112 117 77.0-126
(S) 1,2-Dichloroethane-d4 92.8 92.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS
¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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