MO-88920_97031_CA_O_20230509_PhaseII

PHASE II LIMITED ENVIRONMENTAL SITE
ASSESSMENT
4357 Raleigh Street
4357 Raleigh Street
Charlotte,North Carolina 28213
BBG Project: 0523100027
Prepared For
Arris Holdings, LLC
2700 Apple Valley Road, Suite 50
Brookhaven, Georgia 30319
Report Date
March 28, 2023
Prepared By
BBG Assessments NC, Inc.
200 Providence Road
BBG Main Contact
Paul Stellato |[e-mail]
Copyright © 2023 BBG, Inc. All rights reserved.
March 28, 2023
Marshall Musser
Arris Holdings, LLC
2700 Apple Valley Road, Suite 50
Brookhaven,Georgia 30319
Re:Phase II Limited Environmental Site Assessment of
4357 Raleigh Street
4357 Raleigh Street
Charlotte, North Carolina 28213
BBG Project No.: 0523100027
Dear Mr. Musser:
BBG Assessments NC, Inc. (BBG) has completed a Phase II Limited Environmental Site Assessment of the above
referenced property.The work was conducted in accordance with BBG’s letter of engagement and generally
accepted industry standards.This report was prepared solely for the use of Arris Holdings, LLC (hereinafter
“Client”) and any party specifically referenced in Section 1.4 User Reliance.No other party shall use or rely on this
report or the findings herein, without the prior written consent of BBG.
Sincerely,
Matt Smelski Paul Stellato
Project Manager Managing Director
BBG Assessments NC, Inc.BBG Assessments NC, Inc.
Christopher R. Stang, PG
Senior Managing Director
BBG Assessments NC, Inc.
4357 Raleigh Street
BBG Project: 0523100027 Copyright © 2023 BBG, Inc. All rights reserved.
TABLE OF CONTENTS
1.0 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
1.1 Background and Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
1.2 Special Terms and Conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
1.3 Limitations and Exceptions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
1.4 Reliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
2.0 PHASE II ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
2.1 Preliminary Activities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
2.2 Assessment and Sampling Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
2.3 Analytical Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
3.0 FINDINGS, OPINIONS AND CONCLUSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
4.0 RECOMMENDATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
APPENDIX 1 Figures
APPENDIX 2 Tables
APPENDIX 3 Boring Logs
APPENDIX 4 Photographs
APPENDIX 5 Analytical Report
APPENDIX 6 Personnel Qualifications
4357 Raleigh Street
BBG Project: 0523100027 i
Copyright © 2023 BBG, Inc. All rights reserved.
1.0 INTRODUCTION
In accordance with our Proposal dated February 17, 2023, BBG is pleased to submit our Phase II Limited
Environmental Site Assessment (Phase II ESA) of the property located at 4357 Raleigh Street in Charlotte,
North Carolina 28213 herein referred to as the “Subject Property”.
1.1 Background and Purpose
BBGwasprovidedwithaPhaseIEnvironmentalSiteAssessment(ESA),preparedbyECSSoutheast,LP(ECS),
dated February 15, 2023 which identified the following Recognized Environmental Conditions (REC):
•“Staining and visible oil was observed on the gravel and pavement on the central southern portion of
the property. The staining appears to have originated from discarded motors on the property, and is
approximately 15 square feet in area. The observed staining is considered a REC.
•Stainingandvisibleoilwasobservedonthepavementontheeasternportionofthe property.Thestaining
appears to have originated from tractor trailers that were previously parked on the property, and is
approximately 75 square feet in area. The observed staining is considered a REC."
The purpose of this investigation was to assess the RECs identified in ECS’s Phase I ESA and determine
if subsurface soil and/or groundwater conditions onsite have been affected in the areas of observed soil
staining likely associated with former tractor trailers.A Topographic Location Map and a Boring Location
Map are included in Appendix 1.Photographs of the Subject Property are provided in Appendix 4.
1.2 Special Terms and Conditions
There are no special terms and conditions associated with this Phase II ESA.
1.3 Limitations and Exceptions
•The scope of work completed was designed solely to meet the needs of BBG’s Client.BBG shall not be
liable for any unintended use of this report by another party.
•No subsurface investigation can wholly eliminate uncertainty regarding the presence of contamination
on a property.This assessment was designed to reduce, but not eliminate the potential for RECs at
the property, within reasonable limits of time and cost.The ESA is not intended to be exhaustive or
all-inclusive and does not represent a guarantee of the identification of all possible environmental risk.
•Client is advised that if the ESA is obtained with the intent of qualifying the purchaser as an innocent
landowner, contiguous property owner, or bona fide prospective purchaser under CERCLA, there will be
continuing obligations of due care and responsiveness and additional legal requirements that likely apply
to such status.BBG accepts and undertakes no responsibility as to such requirements and advises that
counsel be separately consulted with respect to such requirements.
INTRODUCTION
4357 Raleigh Street
BBG Project: 0523100027 1
Copyright © 2023 BBG, Inc. All rights reserved.
1.4 Reliance
This investigation was conducted on behalf of and for the exclusive use of Arris Holdings, LLC (Client).This
report, and the findings contained herein, shall not, in whole or part, be disseminated or conveyed to or used
by any other party without the prior written consent of BBG.Any unauthorized party using or relying upon
the Report shall be liable to BBG for equitable compensation and appropriate punitive damages, and shall
be responsible to reimburse BBG for and indemnify, defend and hold BBG harmless from and against any
and all costs, claims, liabilities, expenses, lost profits and damages arising as a direct or indirect result of such
unauthorized use or reliance.
INTRODUCTION
4357 Raleigh Street
BBG Project: 0523100027 2
Copyright © 2023 BBG, Inc. All rights reserved.
2.0 PHASE II ACTIVITIES
2.1 Preliminary Activities
Utility Clearance and Geophysical Survey
A utility inspection was performed at the Subject Property at least 72 hours prior to the initiation of the
subsurface assessment.This inspection consisted of the marking the underground utility locations by
authorizedutilitylocatingpersonnel.Priortocommencementofthedrillingactivities,BBGretainedGround
Penetrating Radar Services, Inc. (GPRS) to conduct a private utility locating survey to verify utility locations
prior to boring advancement. The survey consisted of a combination of electromagnetic (EM) and
ground-penetrating (GPR) technologies.
2.2 Assessment and Sampling Methods
Soil Sampling Activities
On March 13, 2023, BBG conducted a limited subsurface investigation to assess subsurface conditions at
the Subject Property for potential impacts from the observed soil staining.During the investigation, four
soilborings,denotedasB-1through B-4,wereadvancedatthesitebyMidSouthEnvironmentalusing direct
pushtechnology(DPT)andhandauger methods.BoringsB-1and B-2 wereadvancedtomaximumdepthsof
approximately 4 to 8 feetbelow ground surface (bgs) and were located the in the soil stained area near the
eastern property line, while borings B-3 and B-4 were advanced to approximately 6 to 15 feet bgs in the soil
stained area near the center of the Subject Property.Groundwater was encountered in boring B-1 at about
5 feet bgs and in B-4 at about 12 feet bgs.As such, two unsaturated soil samples were collected from each
boring, one at a depth of 1 foot bgs and a second deeper sample at approximately 1-2 feet above the water
table.The boring locations are illustrated in Appendix 1, Figure 2.
Continuous soil cores were collected from borings B-1 through B-4 using a MacroCore® sampler lined with
an acetate sleeve to the terminal depths of each boring and inspected for evidence of volatile organic
compounds(VOC)contaminationusingaphotoionizationdetector(PID).Noolfactoryodors,staining,or PID
readingsabovebackgroundlevelswerenoted,exceptinboringB-1,whichdisplayedPIDreadingsofupto3.5
ppm and petroleum odors at around 4 feet bgs.Soils within each boring at the Subject Property appeared
to generally consist of moist, reddish-brown to light gray, gravellyclay in the upper 1 foot, overlying stiff,
reddish-brownandoliveclaythatbecomessaturatednearthewatertable.Basedonthescopeofwork,field
observations,andnatureofprevioussiteuses,soilsampleswerecollectedforchemicalanalysisfromborings
B-1 and B-2 at 1 foot bgs and 4 feet bgs, boring B-3 at 1 foot bgs and 5 feet bgs, and boring B-4 at 1 foot bgs
and 10 feet bgs .A copy of the boring logs is included in Appendix 3.
The soil samples were submitted to SGS North America, a North Carolina-certified laboratory.The soil
samples were submitted for analysis of VOCs per EPA Method 8260 and total petroleum hydrocarbons
(TPH) gasoline range organics (GRO) and diesel range organics (DRO) per EPA Method 8015.Dedicated
PHASE II ACTIVITIES
4357 Raleigh Street
BBG Project: 0523100027 3
Copyright © 2023 BBG, Inc. All rights reserved.
laboratory-supplied sample containers were used for sample collection. The samples were placed in an iced
cooler after collection.Chain-of-custody records were completed for the samples and included the sample
description,datecollected,timecollected,matrix,samplecontainerinformation,andanalysesrequired.The
chain-of-custody record was signed by BBG prior to delivery to the SGS laboratory.Following completion of
the sampling, all soil boring locations were properly abandoned and surface restoration was performed to
match the pre-existing surrounding material.
Groundwater Sampling Activities
In order to assess the groundwater at the Subject Property, two of theborings (B-1 and B-4) were converted
into temporary groundwater monitoring wells.The wells were constructed utilizing one-inch slotted screen
Schedule 40 PVC which was inserted approximately 3 feet into the water column.A peristaltic pump
attached to dedicated disposable tubing was utilized to extract groundwater samples at each boring
location.
The groundwater samples were submitted to SGS North America, a North Carolina-certified laboratory for
analysis of VOCs by 6200, and volatile petroleum hydrocarbons (VPH) and extractable petroleum
hydrocarbons (EPH)by MADEP Method EPA 625 Base/Neutrals and Acids.
Dedicatedlaboratory-suppliedsamplecontainerswereusedforsamplecollection.Thesampleswereplaced
in an iced cooler after collection.Chain-of-custody records were completed for the samples and included
the sample description, date collected, time collected, matrix, sample container information, and analyses
required.The chain-of-custody record was signed by BBG prior to delivery to the SGS laboratory.Following
completion of the sampling, all groundwater boring locations were abandoned in accordance with North
Carolina regulations and surface restoration was performed to match the pre-existing surrounding material.
2.3 Analytical Results
The soil analytical results were compared to the North Carolina Department of Environmental Quality
(NCDEQ) UST Guidance Screening Levels (June 2021).Specifically, preliminary soil remediation goals
(PSRGs) for industrial/commercial scenarios were utilized.The groundwater results were compared to the
North Carolina Department of Environmental Quality (NCDEQ) Groundwater Standards (April,
2022).Additionally, TPH results were compared to the action levels provided by the NCDEQ Division of
WasteManagement(DWM)USTSectionintheGuidelinesforSiteChecks,TankClosure,andinitialresponse
and abatement (May, 2021).The results are summarized in Appendix 2, Tables 1 and 2.A copy of the
laboratory analytical report is provided in Appendix 5.
Soil Results
Soil analytical results identified several VOCs and TPH GRO and DRO within select soil samples collected
from the Subject Property.None of the concentrations of the detected VOCs were reported to exceed
their respective PSRGs; however, the concentrations of TPH GRO and DRO were detected above the UST
GuidanceScreeningLevelswithinthesamplecollectedat4feetbgsfrom boringB-1attheSubjectProperty.
PHASE II ACTIVITIES
4357 Raleigh Street
BBG Project: 0523100027 4
Copyright © 2023 BBG, Inc. All rights reserved.
TPH GRO was detected at 57.4 milligrams per kilogram (mg/kg) and TPH DRO was detected at 2,380 mg/kg
in boring B-1, which exceeds their respective NCDEQ DWM action levels of 50 and 100 mg/kg for TPH GRO
and TPH DRO, respectively.
Groundwater Results
GroundwateranalyticalresultsidentifiedseveralVOCs,EPH,andVPHinthegroundwatersamplescollected
from the Subject Property.A concentration of naphthalene was detected at 8.0 micrograms per liter (µg/
l)as a VOC and 11.5 µg/l as a VPH within the groundwater sample from boring B-1, which exceeds its
respective NCDEQ Groundwater Standard of 6 µg/l for naphthalene.Additionally, EPH C11-C22 aromatics
range was detected at 556 and 267 µg/l in the groundwater samples from borings B-1 and B-4, respectively,
whichexceeds its respective NCDEQ Groundwater Standard of 200 µg/l for C11-C22 aromatics.
PHASE II ACTIVITIES
4357 Raleigh Street
BBG Project: 0523100027 5
Copyright © 2023 BBG, Inc. All rights reserved.
3.0 FINDINGS, OPINIONS AND CONCLUSIONS
BBG conducted a Phase II ESA located at 4357 Raleigh Street in Charlotte, North Carolina on March 13,
2023.The results of the Phase II ESA activities are summarized below:
•Prior to the investigation, a GPR survey was conducted to clear the boring locations for private utilities.
•During the investigation, four soil borings were advanced to investigate the subsurface conditions for
potential impacts indicated by onsite soil staining.Groundwater was encountered at a depth of
approximately 5 feet bgs within boring B-1, and 12 feet bgs within boring B-4.Two soil samples, one
near the upper 1 foot and one above the water table, were collected for chemical analysis from each of
the borings, and one groundwater sample was collected from boring B-1 and B-4.All soil samples were
analyzed for VOCs by EPA Method 8260 and TPH GRO/DRO by EPA Method 8015 and groundwater
samples were analyzed forVOCs by 6200 and VPH/EPH by MADEP Method EPA 625.
•Soilanalytical resultsidentifiedseveral VOCs andTPHGROandDROwithinselectsoil samplescollected
from the Subject Property.None of the concentrations of the detected VOCs were reported to exceed
their respective PSRGs; however, the concentrations of TPH GRO and DRO were detected above action
levels within the sample collected at 4 feet bgs from boring B-1 at the Subject Property.TPH GRO
was detected at 57.4 mg/kg and TPH DRO was detected at 2380 mg/kg in boring B-1, which exceeds
their respective NCDEQ DWM action levels of 50 and 100 mg/kg for TPH GRO and TPH DRO,
respectively.
•Groundwater analytical results identified several VOCs, EPH, and VPH in the groundwater samples
collected from the Subject Property.The concentration of naphthalene was detected at 8.0 µg/l as a
VOC and 11.5 µg/l as a VPH within the groundwater samplefrom boring B-1, which exceeds its
respective NCDEQ Groundwater Standard of 6 µg/l for naphthalene.Additionally, EPH C11-C22
aromatics range was detected at 556 and 267 µg/l in groundwater samples from borings B-1 and B-4,
respectively, which exceeds its respective NCDEQ Groundwater Standard of 200 µg/l for C11-C22
aromatics.
Based on the results of this LSI,it appears that the Subject Property has been impacted in the areas with
previously observed soil staining.Soil analytical results detected TPH GRO and DRO within the soil sample
collected from boring B-1 at concentrations exceeding their respective NCDEQ DWM UST Section's action
levels for TPH.Additionally, groundwater analytical results detected naphthalene in boring B-1, and EPH
C11-C22 aromatics in borings B-1 and B-4, in exceedance of their respective NCDEQ Groundwater
Standards.
BBG’s conclusions are based on the results of the Phase II Limited Site Assessment performed at 4357
Raleigh Street in Charlotte, North Carolina 28213.This investigation was intended to address the REC
previously identified as referenced above.It was not intended to satisfy the level of inquiry that may be
necessary to support remedial solutions or determine migration pathways related to a release from the REC.
FINDINGS, OPINIONS AND CONCLUSIONS
4357 Raleigh Street
BBG Project: 0523100027 6
Copyright © 2023 BBG, Inc. All rights reserved.
4.0 RECOMMENDATIONS
Based on the results of this LSI,it appears that the Subject Property has been impacted in the areas with
previously observed surficial soil staining.Soil analytical results detected TPH GRO and DRO within the soil
sample collected at 4 feet bgs from boring B-1 at concentrations exceeding their respective NCDEQ DWM
UST Section's action levels for TPH.Additionally, groundwater analytical results detected naphthalene in
boring B-1, and EPH C11-C22 aromatics in borings B-1 and B-4, in exceedance of their respective NCDEQ
Groundwater Standards.As such, the exceedances of TPH, EPH C11-C22, and naphthalene should be
reported to the NCDEQ.
RECOMMENDATIONS
4357 Raleigh Street
BBG Project: 0523100027 7
Copyright © 2023 BBG, Inc. All rights reserved.
Figures
Appendix 1
4357 Raleigh Street
BBG Project: 0523100027 8
Copyright © 2023 BBG, Inc. All rights reserved.
4357 Raleigh Street i BBG PROJECT NO.: 0523100027
4357 Raliegh Street
Charlotte, North Carolina 28213
FIGURE 2 – BORING LOCATION MAP
Base Map Source – Google Earth (2022)
- Soil/Groundwater Boring Location
- Areas of Observed Soil Staining
Approximate
Site Boundary
B-4
B-1
B-2
B-3
Tables
Appendix 2
4357 Raleigh Street
BBG Project: 0523100027 11
Copyright © 2023 BBG, Inc. All rights reserved.
TABLE 1
Summary of Soil Analytical Results
4357 Raleigh Street
Charlotte, North Carolina 28213
BBG Project #0523100027
Sample ID B-1 B-1 B-2 B-2 B-3 B-3 B-4 B-4
Sample Depth (feet bgs)1'4'1'4'1'5'1'10'
Sample Date 3/13/2023 3/13/2023 3/13/2023 3/13/2023 3/13/2023 3/13/2023 3/13/2023 3/13/2023
Volatile Organic Compounds (VOCs) by EPA Method 8260
n-Butylbenzene ND 0.285 ND ND ND ND ND ND 12,000 NA
sec-Butylbenzene ND 0.412 ND ND ND ND ND ND 23,000 NA
tert-Butylbenzene ND 0.0414 J ND ND ND ND ND ND 23,000 NA
Carbon Disulfide ND ND ND ND ND 0.0014 J ND ND 740 NA
o-Chlorotoluene ND 0.0747 J ND ND ND ND ND ND 4,700 NA
Ethylbenzene ND 0.186 J ND ND ND ND ND ND 27 NA
Isopropylbenzene ND 0.259 ND ND ND ND ND ND 2,100 NA
p-Isopropyltoluene ND 0.324 ND ND ND ND ND ND NE NA
Naphthalene ND 1.64 ND ND ND ND ND ND 8.8 NA
n-Propylbenzene ND 0.416 ND ND ND ND ND ND 5,100 NA
1,2,4-Trimethylbenzene ND 1.53 ND ND ND ND ND ND 370 NA
1,3,5-Trimethylbenzene ND 0.637 ND ND ND ND ND ND 320 NA
m,p-Xylene ND 0.194 J ND ND ND ND ND ND 500 NA
0-Xylene ND 1.282 ND ND ND ND ND ND 590 NA
Total Petroleum Hydrocarbons (TPH) by EPA Method 8015
TPH-GRO (C6-C10) ND 57.4 ND ND ND ND ND ND NA 50
TPH-DRO (C10-C28) 68.3 2380 9.99 32.9 79.9 70.8 78.0 47.1 NA 100
Notes:
Concentrations reported in milligrams per kilogram (mg/kg)
NCDEQ - North Carolina Department of Environmental Quality, UST Guidance, Soil Screening Levels
NCDEQ PSRG = Preliminary Soil Remediation Goals
NCDEQ UST = North Carolina Department of Environmental Quality, Division of Waste Management, UST Section, Guideline Action levels (May, 2021)
NCDEQ UST
ND = Not Detected, NE = Not Established, NA = Not Applicable
NCDEQ PSRG
Commercial
TABLE 2
Summary of Groundwater Analytical Results
4357 Raleigh Street
Charlotte, North Carolina 28213
Project #0523100027
Sample ID B-1 B-4
Sample Date 3/13/2022 3/13/2022
Volatile Organic Compounds (VOCs) by SM 6200
Acetone 8.9 J 11.8 6000
n-Butylbenzene 1.0 ND 70
sec-Butylbenzene 1.8 ND 70
tert-Butylbenzene 0.15 J ND 70
o-Chlorotoluene 0.24 J ND 100
Ethylbenzene 0.83 ND 600
Isopropylbenzene 1.2 ND 70
p-Isopropyltoluene 1.2 ND NE
Naphthalene 8.0 0.17 J 6
n-Propylbenzene 1.9 ND 70
Tetrachloroethene 0.51 ND 0.7
Toluene 0.42 J 0.49 J 600
1,2,4-Trimethylbenzene 7.9 0.17 J 400
1,3,5-Trimethylbenzene 2.1 ND 400
m,p-Xylene 0.83 J ND 500
o-Xylene 1.1 ND 500
Xylenes (total)1.9 ND 500
Volatile Petroleum Hydrocarbons (VPH) by MADEP Method 625
Benzene ND ND 1
Ethylbenzene 0.76 J ND 600
Methyl tert butyl ether ND ND 20
Naphthalene 11.5 ND 6
Toluene 0.43 J ND 600
Xylenes (total)2 J ND 500
C5-C8 Aliphatics ND ND 400
C9-C12 Aliphatics 216 ND 700
C9-C10 Aromatics 108 ND 200
Extractable Petroleum Hydrocarbons (EPH) by MADEP Method 625
Acenaphthene 4.6 ND 200
2-methylnaphthalene 13.4 ND 30
Naphthalene 4.1 ND 6
C11-C22 Aromatics 556 267 200
C9-C18 Aliphatics 183 J ND 700
C19-C36 Aliphatics 102 J ND 10,000
Notes:
Concentrations reported in micrograms per liter (µg/l)
J = Indicates an estimated value
Bold = Indicates reported concentration exceeds NCDEQ screening level
NCDEQ
NCDEQ - North Carolina Department of Environmental Quality, UST Guidance, Groundwater Standards
Boring Logs
Appendix 3
4357 Raleigh Street
BBG Project: 0523100027 14
Copyright © 2023 BBG, Inc. All rights reserved.
Depth (ft bgs)USCS SymbolPIDSample Interval
Selected for
Analysis GWLDepth (ft bgs)5 5
10 10
15 15
20 20
25 25
30 30
FIELD BORING LOG
Date and Time: 3/13/2023
Location of Boring: Southwest corner of eastern
stained area
Name of Driller: Don Warren Drilling Contractor: MidSouth Environmental
Project Name: 4357 Raleigh Street
Project No.: 0523100027
@ 3' ft : Clay, reddish brown, slighty moist, stiff
@ 4' ft : Encountered slight petroleum odor
@ 5' ft : Clay w/ trace Sand, olive, saturated, medium stiff
Make / Model of Drill Rig: Geoprobe 6712 DT
Static Depth to Groundwater (ft bgs): Encountered at 5'
Soil Classification / Description
(Color, Texture, Structures)
Depth GW First Encountered
Static GW Depth
Project Manager: Matt Smelski
Boring No.: B-1
Total Depth (ft bgs): 8'
Logged By: Matt Smelski
Type of Surface Completion: Soil Backfill
Notes:GWL Symbols:
1.7
3.5
CL
CL
CH
CH
Sample Collection Method: Direct Push Probe
@ 0' ft : Gravelly/Silty Clay at surface overlying stiff, reddish brown, Clay
@ 1' ft : Sandy Clay, light grey, moist, soft
Soil Sample @
1'
Soil Sample @
4'
CH
-Encountered groundwater @ 5'
@ 6.5' ft : Clay w/ trace Sand, yellowish-olive, saturated, soft
-Terminated boring @ 8'
Depth (ft bgs)USCS SymbolPIDSample Interval
Selected for
Analysis GWLDepth (ft bgs)5 5
10 10
15 15
20 20
25 25
30 30
Name of Driller: Don Warren Drilling Contractor: MidSouth Environmental
Sample Collection Method: Direct Push Probe Make / Model of Drill Rig: Geoprobe 6712 DT
Static Depth to Groundwater (ft bgs): Not encountered
Type of Surface Completion: Soil Backfill
FIELD BORING LOG
Location of Boring: Northeast corner of eastern stained
area
Project Name: 4357 Raleigh Street Boring No.: B-2
Total Depth (ft bgs): 4'
Project No.: 0523100027 Logged By: Matt Smelski
Project Manager: Matt Smelski
Date and Time: 3/13/2023
@ 1' ft : Clay w/ trace Sand, olive, moist, soft to medium stiff
CH 0.0
Soil Sample @
4' @ 3' ft : Clay, reddish brown, slighty moist, stiff
Notes:GWL Symbols:
Depth GW First Encountered
Static GW Depth
Soil Classification / Description
(Color, Texture, Structures)
CL
CH
@ 0' ft : Silty Clay, light gray, moist, gravels
0.0
Soil Sample @
1'
-Terminated boring @ 4'
Depth (ft bgs)USCS SymbolPIDSample Interval
Selected for
Analysis GWLDepth (ft bgs)5 5
10 10
15 15
20 20
25 25
30 30
Name of Driller: Don Warren Drilling Contractor: MidSouth Environmental
Sample Collection Method: Direct Push Probe Make / Model of Drill Rig: Geoprobe 6712 DT
Static Depth to Groundwater (ft bgs): Not encountered
Type of Surface Completion: Soil Backfill
FIELD BORING LOG
Location of Boring: North end of western stained area Project Name: 4357 Raleigh Street Boring No.: B-3
Total Depth (ft bgs): 6'
Project No.: 0523100027 Logged By: Matt Smelski
Project Manager: Matt Smelski
Date and Time: 3/13/2023
@ 1' ft: Clay w/ trace Sand, reddish/yellowish brown, slightly moist, med. stiff
0.0
Notes:GWL Symbols:
Depth GW First Encountered
Static GW Depth
Soil Classification / Description
(Color, Texture, Structures)
CL
CH
@ 0' ft : Gravelly Clay, olive brown, dry to slightly moist, soft
0.0
Soil Sample @
1'
-Terminated boring @ 6' as wet soils were encountered
0.0
Soil Sample @
5'
Depth (ft bgs)USCS SymbolPIDSample Interval
Selected for
Analysis GWLDepth (ft bgs)5 5
10 10
15 15
20 20
25 25
30 30
Name of Driller: Don Warren Drilling Contractor: MidSouth Environmental
Sample Collection Method: Direct Push Probe Make / Model of Drill Rig: Geoprobe 6712 DT
Static Depth to Groundwater (ft bgs): Encountered at 12'
Type of Surface Completion: Soil Backfill
FIELD BORING LOG
Location of Boring: South end of western stained area Project Name: 4357 Raleigh Street Boring No.: B-4
Total Depth (ft bgs): 15'
Project No.: 0523100027 Logged By: Matt Smelski
Project Manager: Matt Smelski
Date and Time: 3/13/2023
@ 1' ft : Clay, reddish brown, dry, stiff
CL 0.0 @ 3' ft : Silty Clay, olive, dry to slighty moist, soft
Notes:GWL Symbols:
Depth GW First Encountered
Static GW Depth
Soil Classification / Description
(Color, Texture, Structures)
SC
CH
@ 0' ft : Clayey Sand, yellowish brown, dry, soft
0.0
Soil Sample @
1'
CH 0.0 @ 7.5' ft : Clay, reddish-brown and gray-brown, dry to slightly moist, stiff
0.0
CH @ 10' ft : Clay, reddish-brown and gray-brown, moist to wet, stiff
0.0
0.0
Soil Sample @
10'
-Terminated boring @ 15'
-Encountered groundwater @ 12'
Photographs
Appendix 4
4357 Raleigh Street
BBG Project: 0523100027 16
Copyright © 2023 BBG, Inc. All rights reserved.
1.Gravel area of B-1/B-2 2.Gravel area of B-3/B-4
3.Soil staining near B-3 4.Soil staining near B-4
Appendix 4
4357 Raleigh Street
BBG Project: 0523100027 17
Copyright © 2023 BBG, Inc. All rights reserved.
Analytical Report
Appendix 5
4357 Raleigh Street
BBG Project: 0523100027 18
Copyright © 2023 BBG, Inc. All rights reserved.
03/24/23
Technical Report for
BBG Assessment
4357 Raleigh St, Charlotte, NC
0523100027
SGS Job Number: FC3398
Sampling Date: 03/13/23
Report to:
BBG Real Estate Services
3800 W Bay-to-Bay Blvd Unit 23
Tampa, FL 33629
[e-mail]
ATTN: Matt Smelski
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Kelly Blanchard 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 03/24/23
e-Hardcopy 2.0
Automated Report
101
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
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how we can serve you better at:
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1 of 101
FC3398
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FC3398-1: B-1 @ 4' ......................................................................................................8
3.2: FC3398-2: B-1 @ 1' ......................................................................................................13
3.3: FC3398-3: B-1 GW ......................................................................................................18
3.4: FC3398-4: B-2 @ 1' ......................................................................................................23
3.5: FC3398-5: B-2 @ 4' ......................................................................................................28
3.6: FC3398-6: B-3 @ 1' ......................................................................................................33
3.7: FC3398-7: B-3 @ 5' ......................................................................................................38
3.8: FC3398-8: B-4 @ 1' ......................................................................................................43
3.9: FC3398-9: B-4 @ 10' ....................................................................................................48
3.10: FC3398-10: B-4 GW ..................................................................................................53
Section 4: Misc. Forms ............................................................................................................58
4.1: Chain of Custody ...........................................................................................................59
Section 5: MS Volatiles - QC Data Summaries .....................................................................61
5.1: Method Blank Summary ................................................................................................62
5.2: Blank Spike Summary ...................................................................................................68
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................74
Section 6: GC Volatiles - QC Data Summaries .....................................................................80
6.1: Method Blank Summary ................................................................................................81
6.2: Blank Spike Summary ...................................................................................................82
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................83
Section 7: GC/LC Semi-volatiles - QC Data Summaries .....................................................84
7.1: Method Blank Summary ................................................................................................85
7.2: Blank Spike Summary ...................................................................................................87
7.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................88
7.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................89
Section 8: Misc. Forms (SGS Scott, LA) ................................................................................91
8.1: Chain of Custody ...........................................................................................................92
Section 9: GC Volatiles - QC Data (SGS Scott, LA) .............................................................96
9.1: Method Blank Summary ................................................................................................97
9.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................99
9.3: Duplicate Summary .......................................................................................................101 1234567892 of 101
FC3398
SGS North America Inc.
Sample Summary
BBG Assessment
Job No:FC3398
4357 Raleigh St, Charlotte, NC
Project No: 0523100027
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC3398-1 03/13/23 08:50 MS 03/14/23 SO Soil B-1 @ 4'
FC3398-2 03/13/23 09:00 MS 03/14/23 SO Soil B-1 @ 1'
FC3398-3 03/13/23 09:10 MS 03/14/23 AQ Ground Water B-1 GW
FC3398-4 03/13/23 10:00 MS 03/14/23 SO Soil B-2 @ 1'
FC3398-5 03/13/23 10:05 MS 03/14/23 SO Soil B-2 @ 4'
FC3398-6 03/13/23 10:45 MS 03/14/23 SO Soil B-3 @ 1'
FC3398-7 03/13/23 11:00 MS 03/14/23 SO Soil B-3 @ 5'
FC3398-8 03/13/23 11:50 MS 03/14/23 SO Soil B-4 @ 1'
FC3398-9 03/13/23 12:00 MS 03/14/23 SO Soil B-4 @ 10'
FC3398-10 03/13/23 12:15 MS 03/14/23 AQ Ground Water B-4 GW
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 101
FC33981
Summary of Hits Page 1 of 3
Job Number:FC3398
Account:BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Collected:03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC3398-1 B-1 @ 4'
n-Butylbenzene 285 200 39 ug/kg SW846 8260D
sec-Butylbenzene 412 200 39 ug/kg SW846 8260D
tert-Butylbenzene 41.4 J 200 39 ug/kg SW846 8260D
o-Chlorotoluene 74.7 J 200 39 ug/kg SW846 8260D
Ethylbenzene 186 J 200 39 ug/kg SW846 8260D
Isopropylbenzene 259 200 39 ug/kg SW846 8260D
p-Isopropyltoluene 324 200 39 ug/kg SW846 8260D
Naphthalene 1640 200 78 ug/kg SW846 8260D
n-Propylbenzene 416 200 39 ug/kg SW846 8260D
1,2,4-Trimethylbenzene 1530 200 39 ug/kg SW846 8260D
1,3,5-Trimethylbenzene 637 200 39 ug/kg SW846 8260D
m,p-Xylene 194 J 390 43 ug/kg SW846 8260D
o-Xylene 282 200 39 ug/kg SW846 8260D
TPH-GRO (C6-C10)57.4 44 17 mg/kg SW846 8015C
TPH (C10-C28)2380 610 300 mg/kg SW846 8015C
FC3398-2 B-1 @ 1'
TPH (C10-C28)68.3 58 29 mg/kg SW846 8015C
FC3398-3 B-1 GW
Acetone a 8.9 J 10 2.0 ug/l SM 6200B
n-Butylbenzene a 1.0 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene a 1.8 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene a 0.15 J 0.50 0.13 ug/l SM 6200B
o-Chlorotoluene a 0.24 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene a 0.83 0.50 0.13 ug/l SM 6200B
Isopropylbenzene a 1.2 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene a 1.2 0.50 0.13 ug/l SM 6200B
Naphthalene a 8.0 0.50 0.13 ug/l SM 6200B
n-Propylbenzene a 1.9 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene a 0.51 0.50 0.13 ug/l SM 6200B
Toluene a 0.42 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene a 7.9 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene a 2.1 0.50 0.13 ug/l SM 6200B
m,p-Xylene a 0.83 J 1.0 0.13 ug/l SM 6200B
o-Xylene a 1.1 0.50 0.13 ug/l SM 6200B
Xylene (total) a 1.9 1.5 0.25 ug/l SM 6200B
Ethylbenzene b 0.76 J 5.0 0.17 ug/l MADEP VPH REV 2.1
Naphthalene b 11.5 5.0 0.41 ug/l MADEP VPH REV 2.1
Toluene b 0.43 J 5.0 0.15 ug/l MADEP VPH REV 2.1
m,p-Xylene b 1.0 J 10 0.40 ug/l MADEP VPH REV 2.1
4 of 101
FC33982
Summary of Hits Page 2 of 3
Job Number:FC3398
Account:BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Collected:03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Xylene b 1.0 J 5.0 0.18 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.) b 216 100 50 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.) b 108 100 20 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics b 105 100 50 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics b 108 100 20 ug/l MADEP VPH REV 2.1
Acenaphthene 4.6 4.0 2.0 ug/l MADEP EPH REV 2.1
2-Methylnaphthalene 13.4 4.0 2.0 ug/l MADEP EPH REV 2.1
Naphthalene 4.1 4.0 2.0 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics (Unadj.)556 200 80 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics 534 200 80 ug/l MADEP EPH REV 2.1
C9-C18 Aliphatics 183 J 200 50 ug/l MADEP EPH REV 2.1
C19-C36 Aliphatics 102 J 200 50 ug/l MADEP EPH REV 2.1
FC3398-4 B-2 @ 1'
TPH (C10-C28)9.99 5.8 2.9 mg/kg SW846 8015C
FC3398-5 B-2 @ 4'
TPH (C10-C28)32.9 30 15 mg/kg SW846 8015C
FC3398-6 B-3 @ 1'
TPH (C10-C28)79.9 56 28 mg/kg SW846 8015C
FC3398-7 B-3 @ 5'
Carbon Disulfide 1.4 J 3.5 0.69 ug/kg SW846 8260D
TPH (C10-C28)70.8 31 16 mg/kg SW846 8015C
FC3398-8 B-4 @ 1'
TPH (C10-C28)78.0 58 29 mg/kg SW846 8015C
FC3398-9 B-4 @ 10'
TPH (C10-C28)47.1 30 15 mg/kg SW846 8015C
FC3398-10 B-4 GW
Acetone a 11.8 10 2.0 ug/l SM 6200B
Naphthalene a 0.17 J 0.50 0.13 ug/l SM 6200B
Toluene a 0.49 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene a 0.17 J 0.50 0.13 ug/l SM 6200B
C11-C22 Aromatics (Unadj.)267 200 80 ug/l MADEP EPH REV 2.1
5 of 101
FC33982
Summary of Hits Page 3 of 3
Job Number:FC3398
Account:BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Collected:03/13/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
C11-C22 Aromatics 267 200 80 ug/l MADEP EPH REV 2.1
(a) Sample was not preserved to a pH < 2.
(b) Analysis performed at SGS Scott, LA.
6 of 101
FC33982
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 101
FC33983
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-1 @ 4'
Lab Sample ID:FC3398-1 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:82.0
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185773.D 1 03/15/23 12:17 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 10.8 g 5.0 ml 100 ul
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 7800 3900 ug/kg
71-43-2 Benzene ND 200 48 ug/kg
108-86-1 Bromobenzene ND 200 39 ug/kg
74-97-5 Bromochloromethane ND 200 58 ug/kg
75-27-4 Bromodichloromethane ND 200 39 ug/kg
75-25-2 Bromoform ND 200 39 ug/kg
78-93-3 2-Butanone (MEK) a ND 980 290 ug/kg
104-51-8 n-Butylbenzene 285 200 39 ug/kg
135-98-8 sec-Butylbenzene 412 200 39 ug/kg
98-06-6 tert-Butylbenzene 41.4 200 39 ug/kg J
75-15-0 Carbon Disulfide ND 200 39 ug/kg
56-23-5 Carbon Tetrachloride ND 200 40 ug/kg
108-90-7 Chlorobenzene ND 200 39 ug/kg
75-00-3 Chloroethane a ND 200 78 ug/kg
67-66-3 Chloroform a ND 200 52 ug/kg
95-49-8 o-Chlorotoluene 74.7 200 39 ug/kg J
106-43-4 p-Chlorotoluene ND 200 39 ug/kg
124-48-1 Dibromochloromethane ND 200 39 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 200 75 ug/kg
106-93-4 1,2-Dibromoethane ND 200 39 ug/kg
75-71-8 Dichlorodifluoromethane a ND 200 78 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 39 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 39 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 45 ug/kg
75-34-3 1,1-Dichloroethane ND 200 69 ug/kg
107-06-2 1,2-Dichloroethane ND 200 39 ug/kg
75-35-4 1,1-Dichloroethylene ND 200 39 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 200 54 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 200 39 ug/kg
78-87-5 1,2-Dichloropropane ND 200 39 ug/kg
142-28-9 1,3-Dichloropropane ND 200 39 ug/kg
594-20-7 2,2-Dichloropropane ND 200 39 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 101
FC339833.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-1 @ 4'
Lab Sample ID:FC3398-1 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:82.0
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 200 40 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 200 39 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 200 39 ug/kg
100-41-4 Ethylbenzene 186 200 39 ug/kg J
87-68-3 Hexachlorobutadiene ND 200 51 ug/kg
591-78-6 2-Hexanone a ND 980 290 ug/kg
98-82-8 Isopropylbenzene 259 200 39 ug/kg
99-87-6 p-Isopropyltoluene 324 200 39 ug/kg
74-83-9 Methyl Bromide a ND 200 78 ug/kg
74-87-3 Methyl Chloride a ND 200 78 ug/kg
74-95-3 Methylene Bromide ND 200 39 ug/kg
75-09-2 Methylene Chloride ND 780 430 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 980 290 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 200 39 ug/kg
91-20-3 Naphthalene 1640 200 78 ug/kg
103-65-1 n-Propylbenzene 416 200 39 ug/kg
100-42-5 Styrene ND 200 39 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 200 40 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 200 39 ug/kg
127-18-4 Tetrachloroethylene ND 200 50 ug/kg
108-88-3 Toluene ND 780 390 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 200 55 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 39 ug/kg
71-55-6 1,1,1-Trichloroethane ND 200 39 ug/kg
79-00-5 1,1,2-Trichloroethane ND 200 39 ug/kg
79-01-6 Trichloroethylene ND 200 39 ug/kg
75-69-4 Trichlorofluoromethane a ND 200 78 ug/kg
96-18-4 1,2,3-Trichloropropane ND 200 49 ug/kg
95-63-6 1,2,4-Trimethylbenzene 1530 200 39 ug/kg
108-67-8 1,3,5-Trimethylbenzene 637 200 39 ug/kg
108-05-4 Vinyl Acetate a ND 980 640 ug/kg
75-01-4 Vinyl Chloride a ND 200 39 ug/kg
m,p-Xylene 194 390 43 ug/kg J
95-47-6 o-Xylene 282 200 39 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%72-135%
2037-26-5 Toluene-D8 96%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 101
FC339833.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-1 @ 4'
Lab Sample ID:FC3398-1 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:82.0
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 93%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 101
FC339833.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 @ 4'
Lab Sample ID:FC3398-1 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:82.0
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14394.D 1 03/15/23 13:00 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 9.35 g 5.0 ml 10.0 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)57.4 44 17 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 109%56-149%
98-08-8 aaa-Trifluorotoluene 92%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 101
FC339833.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 @ 4'
Lab Sample ID:FC3398-1 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:82.0
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38404.D 100 03/17/23 18:45 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)2380 610 300 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 0% a 56-122%
(a) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 101
FC339833.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-1 @ 1'
Lab Sample ID:FC3398-2 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:84.8
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185774.D 1 03/15/23 12:42 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 8.60 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 140 69 ug/kg
71-43-2 Benzene ND 3.4 0.84 ug/kg
108-86-1 Bromobenzene ND 3.4 0.69 ug/kg
74-97-5 Bromochloromethane ND 3.4 1.0 ug/kg
75-27-4 Bromodichloromethane ND 3.4 0.69 ug/kg
75-25-2 Bromoform ND 3.4 0.69 ug/kg
78-93-3 2-Butanone (MEK) a ND 17 5.0 ug/kg
104-51-8 n-Butylbenzene ND 3.4 0.69 ug/kg
135-98-8 sec-Butylbenzene ND 3.4 0.69 ug/kg
98-06-6 tert-Butylbenzene ND 3.4 0.69 ug/kg
75-15-0 Carbon Disulfide ND 3.4 0.69 ug/kg
56-23-5 Carbon Tetrachloride ND 3.4 0.70 ug/kg
108-90-7 Chlorobenzene ND 3.4 0.69 ug/kg
75-00-3 Chloroethane a ND 3.4 1.4 ug/kg
67-66-3 Chloroform a ND 3.4 0.91 ug/kg
95-49-8 o-Chlorotoluene ND 3.4 0.69 ug/kg
106-43-4 p-Chlorotoluene ND 3.4 0.69 ug/kg
124-48-1 Dibromochloromethane ND 3.4 0.69 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 3.4 1.3 ug/kg
106-93-4 1,2-Dibromoethane ND 3.4 0.69 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.4 1.4 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.4 0.69 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.4 0.69 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.4 0.79 ug/kg
75-34-3 1,1-Dichloroethane ND 3.4 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 3.4 0.69 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.4 0.69 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.4 0.95 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.4 0.69 ug/kg
78-87-5 1,2-Dichloropropane ND 3.4 0.69 ug/kg
142-28-9 1,3-Dichloropropane ND 3.4 0.69 ug/kg
594-20-7 2,2-Dichloropropane ND 3.4 0.69 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 101
FC339833.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-1 @ 1'
Lab Sample ID:FC3398-2 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:84.8
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 3.4 0.70 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.4 0.69 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 3.4 0.69 ug/kg
100-41-4 Ethylbenzene ND 3.4 0.69 ug/kg
87-68-3 Hexachlorobutadiene ND 3.4 0.88 ug/kg
591-78-6 2-Hexanone a ND 17 5.1 ug/kg
98-82-8 Isopropylbenzene ND 3.4 0.69 ug/kg
99-87-6 p-Isopropyltoluene ND 3.4 0.69 ug/kg
74-83-9 Methyl Bromide a ND 3.4 1.4 ug/kg
74-87-3 Methyl Chloride a ND 3.4 1.4 ug/kg
74-95-3 Methylene Bromide ND 3.4 0.69 ug/kg
75-09-2 Methylene Chloride ND 14 7.5 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 17 5.1 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.4 0.69 ug/kg
91-20-3 Naphthalene ND 3.4 1.4 ug/kg
103-65-1 n-Propylbenzene ND 3.4 0.69 ug/kg
100-42-5 Styrene ND 3.4 0.69 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.4 0.71 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.4 0.69 ug/kg
127-18-4 Tetrachloroethylene ND 3.4 0.88 ug/kg
108-88-3 Toluene ND 14 6.9 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.4 0.96 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.4 0.69 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.4 0.69 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.4 0.69 ug/kg
79-01-6 Trichloroethylene ND 3.4 0.69 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.4 1.4 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.4 0.86 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.4 0.69 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.4 0.69 ug/kg
108-05-4 Vinyl Acetate a ND 17 11 ug/kg
75-01-4 Vinyl Chloride a ND 3.4 0.69 ug/kg
m,p-Xylene ND 6.9 0.75 ug/kg
95-47-6 o-Xylene ND 3.4 0.69 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 118%72-135%
2037-26-5 Toluene-D8 94%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 101
FC339833.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-1 @ 1'
Lab Sample ID:FC3398-2 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:84.8
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 104%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 101
FC339833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 @ 1'
Lab Sample ID:FC3398-2 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:84.8
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14388.D 1 03/15/23 10:36 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.53 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.8 1.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 95%56-149%
98-08-8 aaa-Trifluorotoluene 89%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 101
FC339833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 @ 1'
Lab Sample ID:FC3398-2 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:84.8
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38386.D 10 03/17/23 09:53 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)68.3 58 29 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 83%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 101
FC339833.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-1 GW
Lab Sample ID:FC3398-3 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:SM 6200B Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3A272.D 1 03/20/23 15:52 TD n/a n/a V3A13
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 8.9 10 2.0 ug/l J
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK) b ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene 1.0 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.8 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.15 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene 0.24 0.50 0.13 ug/l J
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 101
FC339833.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-1 GW
Lab Sample ID:FC3398-3 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:SM 6200B Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene 0.83 0.50 0.13 ug/l
591-78-6 2-Hexanone c ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene 1.2 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 1.2 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIB b ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 8.0 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 1.9 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.51 0.50 0.13 ug/l
108-88-3 Toluene 0.42 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 7.9 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 2.1 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.83 1.0 0.13 ug/l J
95-47-6 o-Xylene 1.1 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.9 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 89%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 101
FC339833.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-1 GW
Lab Sample ID:FC3398-3 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:SM 6200B Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Sample was not preserved to a pH < 2.
(b) Associated CCV outside of control limits high, sample was ND.
(c) Associated CCV and BS outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 101
FC339833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 GW
Lab Sample ID:FC3398-3 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE040994.D 1 03/23/23 13:28 ALA n/a n/a L:GLE2401
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene 0.76 5.0 0.17 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 11.5 5.0 0.41 ug/l
108-88-3 Toluene 0.43 5.0 0.15 ug/l J
m,p-Xylene 1.0 10 0.40 ug/l J
95-47-6 o-Xylene 1.0 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)216 100 50 ug/l
C9- C10 Aromatics (Unadj.)108 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics 105 100 50 ug/l
C9- C10 Aromatics 108 100 20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 104%70-130%
615-59-8 2,5-Dibromotoluene 108%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 101
FC339833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 GW
Lab Sample ID:FC3398-3 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN041739.D 1 03/16/23 23:47 AF 03/15/23 08:00 OP95890 GNN1919
Run #2
Initial Volume Final Volume
Run #1 1000 ml 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene 4.6 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene 13.4 4.0 2.0 ug/l
91-20-3 Naphthalene 4.1 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)556 200 80 ug/l
C11-C22 Aromatics 534 200 80 ug/l
C9-C18 Aliphatics 183 200 50 ug/l J
C19-C36 Aliphatics 102 200 50 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 76%40-140%
580-13-2 2-Bromonaphthalene 113%40-140%
84-15-1 o-Terphenyl 91%40-140%
321-60-8 2-Fluorobiphenyl 111%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 101
FC339833.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-2 @ 1'
Lab Sample ID:FC3398-4 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:85.5
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185775.D 1 03/15/23 13:06 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 9.92 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 120 59 ug/kg
71-43-2 Benzene ND 2.9 0.72 ug/kg
108-86-1 Bromobenzene ND 2.9 0.59 ug/kg
74-97-5 Bromochloromethane ND 2.9 0.87 ug/kg
75-27-4 Bromodichloromethane ND 2.9 0.59 ug/kg
75-25-2 Bromoform ND 2.9 0.59 ug/kg
78-93-3 2-Butanone (MEK) a ND 15 4.3 ug/kg
104-51-8 n-Butylbenzene ND 2.9 0.59 ug/kg
135-98-8 sec-Butylbenzene ND 2.9 0.59 ug/kg
98-06-6 tert-Butylbenzene ND 2.9 0.59 ug/kg
75-15-0 Carbon Disulfide ND 2.9 0.59 ug/kg
56-23-5 Carbon Tetrachloride ND 2.9 0.60 ug/kg
108-90-7 Chlorobenzene ND 2.9 0.59 ug/kg
75-00-3 Chloroethane a ND 2.9 1.2 ug/kg
67-66-3 Chloroform a ND 2.9 0.78 ug/kg
95-49-8 o-Chlorotoluene ND 2.9 0.59 ug/kg
106-43-4 p-Chlorotoluene ND 2.9 0.59 ug/kg
124-48-1 Dibromochloromethane ND 2.9 0.59 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 2.9 1.1 ug/kg
106-93-4 1,2-Dibromoethane ND 2.9 0.59 ug/kg
75-71-8 Dichlorodifluoromethane a ND 2.9 1.2 ug/kg
95-50-1 1,2-Dichlorobenzene ND 2.9 0.59 ug/kg
541-73-1 1,3-Dichlorobenzene ND 2.9 0.59 ug/kg
106-46-7 1,4-Dichlorobenzene ND 2.9 0.68 ug/kg
75-34-3 1,1-Dichloroethane ND 2.9 1.0 ug/kg
107-06-2 1,2-Dichloroethane ND 2.9 0.59 ug/kg
75-35-4 1,1-Dichloroethylene ND 2.9 0.59 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 2.9 0.81 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 2.9 0.59 ug/kg
78-87-5 1,2-Dichloropropane ND 2.9 0.59 ug/kg
142-28-9 1,3-Dichloropropane ND 2.9 0.59 ug/kg
594-20-7 2,2-Dichloropropane ND 2.9 0.59 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 101
FC339833.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-2 @ 1'
Lab Sample ID:FC3398-4 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:85.5
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 2.9 0.60 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 2.9 0.59 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 2.9 0.59 ug/kg
100-41-4 Ethylbenzene ND 2.9 0.59 ug/kg
87-68-3 Hexachlorobutadiene ND 2.9 0.76 ug/kg
591-78-6 2-Hexanone a ND 15 4.4 ug/kg
98-82-8 Isopropylbenzene ND 2.9 0.59 ug/kg
99-87-6 p-Isopropyltoluene ND 2.9 0.59 ug/kg
74-83-9 Methyl Bromide a ND 2.9 1.2 ug/kg
74-87-3 Methyl Chloride a ND 2.9 1.2 ug/kg
74-95-3 Methylene Bromide ND 2.9 0.59 ug/kg
75-09-2 Methylene Chloride ND 12 6.5 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 15 4.4 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 2.9 0.59 ug/kg
91-20-3 Naphthalene ND 2.9 1.2 ug/kg
103-65-1 n-Propylbenzene ND 2.9 0.59 ug/kg
100-42-5 Styrene ND 2.9 0.59 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 2.9 0.61 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 2.9 0.59 ug/kg
127-18-4 Tetrachloroethylene ND 2.9 0.75 ug/kg
108-88-3 Toluene ND 12 5.9 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 2.9 0.83 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 2.9 0.59 ug/kg
71-55-6 1,1,1-Trichloroethane ND 2.9 0.59 ug/kg
79-00-5 1,1,2-Trichloroethane ND 2.9 0.59 ug/kg
79-01-6 Trichloroethylene ND 2.9 0.59 ug/kg
75-69-4 Trichlorofluoromethane a ND 2.9 1.2 ug/kg
96-18-4 1,2,3-Trichloropropane ND 2.9 0.74 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 2.9 0.59 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 2.9 0.59 ug/kg
108-05-4 Vinyl Acetate a ND 15 9.7 ug/kg
75-01-4 Vinyl Chloride a ND 2.9 0.59 ug/kg
m,p-Xylene ND 5.9 0.65 ug/kg
95-47-6 o-Xylene ND 2.9 0.59 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 117%72-135%
2037-26-5 Toluene-D8 96%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 101
FC339833.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-2 @ 1'
Lab Sample ID:FC3398-4 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:85.5
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 101
FC339833.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-2 @ 1'
Lab Sample ID:FC3398-4 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:85.5
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14391.D 1 03/15/23 11:48 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 9.30 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.0 1.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 95%56-149%
98-08-8 aaa-Trifluorotoluene 91%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 101
FC339833.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-2 @ 1'
Lab Sample ID:FC3398-4 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:85.5
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38387.D 1 03/17/23 10:22 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.3 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)9.99 5.8 2.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 86%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 101
FC339833.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-2 @ 4'
Lab Sample ID:FC3398-5 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:82.9
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185776.D 1 03/15/23 13:31 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 9.09 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 130 66 ug/kg
71-43-2 Benzene ND 3.3 0.81 ug/kg
108-86-1 Bromobenzene ND 3.3 0.66 ug/kg
74-97-5 Bromochloromethane ND 3.3 0.98 ug/kg
75-27-4 Bromodichloromethane ND 3.3 0.66 ug/kg
75-25-2 Bromoform ND 3.3 0.66 ug/kg
78-93-3 2-Butanone (MEK) a ND 17 4.8 ug/kg
104-51-8 n-Butylbenzene ND 3.3 0.66 ug/kg
135-98-8 sec-Butylbenzene ND 3.3 0.66 ug/kg
98-06-6 tert-Butylbenzene ND 3.3 0.66 ug/kg
75-15-0 Carbon Disulfide ND 3.3 0.66 ug/kg
56-23-5 Carbon Tetrachloride ND 3.3 0.68 ug/kg
108-90-7 Chlorobenzene ND 3.3 0.66 ug/kg
75-00-3 Chloroethane a ND 3.3 1.3 ug/kg
67-66-3 Chloroform a ND 3.3 0.88 ug/kg
95-49-8 o-Chlorotoluene ND 3.3 0.66 ug/kg
106-43-4 p-Chlorotoluene ND 3.3 0.66 ug/kg
124-48-1 Dibromochloromethane ND 3.3 0.66 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 3.3 1.3 ug/kg
106-93-4 1,2-Dibromoethane ND 3.3 0.66 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.3 1.3 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.3 0.66 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.3 0.66 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.3 0.76 ug/kg
75-34-3 1,1-Dichloroethane ND 3.3 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 3.3 0.66 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.3 0.66 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.3 0.92 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.3 0.66 ug/kg
78-87-5 1,2-Dichloropropane ND 3.3 0.66 ug/kg
142-28-9 1,3-Dichloropropane ND 3.3 0.66 ug/kg
594-20-7 2,2-Dichloropropane ND 3.3 0.66 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 101
FC339833.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-2 @ 4'
Lab Sample ID:FC3398-5 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:82.9
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 3.3 0.68 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.3 0.66 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 3.3 0.66 ug/kg
100-41-4 Ethylbenzene ND 3.3 0.66 ug/kg
87-68-3 Hexachlorobutadiene ND 3.3 0.86 ug/kg
591-78-6 2-Hexanone a ND 17 5.0 ug/kg
98-82-8 Isopropylbenzene ND 3.3 0.66 ug/kg
99-87-6 p-Isopropyltoluene ND 3.3 0.66 ug/kg
74-83-9 Methyl Bromide a ND 3.3 1.3 ug/kg
74-87-3 Methyl Chloride a ND 3.3 1.3 ug/kg
74-95-3 Methylene Bromide ND 3.3 0.66 ug/kg
75-09-2 Methylene Chloride ND 13 7.3 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 17 5.0 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.3 0.66 ug/kg
91-20-3 Naphthalene ND 3.3 1.3 ug/kg
103-65-1 n-Propylbenzene ND 3.3 0.66 ug/kg
100-42-5 Styrene ND 3.3 0.66 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.3 0.68 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.3 0.66 ug/kg
127-18-4 Tetrachloroethylene ND 3.3 0.85 ug/kg
108-88-3 Toluene ND 13 6.6 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.3 0.93 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.3 0.66 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.3 0.66 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.3 0.66 ug/kg
79-01-6 Trichloroethylene ND 3.3 0.66 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.3 1.3 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.3 0.83 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.3 0.66 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.3 0.66 ug/kg
108-05-4 Vinyl Acetate a ND 17 11 ug/kg
75-01-4 Vinyl Chloride a ND 3.3 0.66 ug/kg
m,p-Xylene ND 6.6 0.73 ug/kg
95-47-6 o-Xylene ND 3.3 0.66 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%75-124%
17060-07-0 1,2-Dichloroethane-D4 116%72-135%
2037-26-5 Toluene-D8 96%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 101
FC339833.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-2 @ 4'
Lab Sample ID:FC3398-5 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:82.9
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 99%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 101
FC339833.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-2 @ 4'
Lab Sample ID:FC3398-5 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:82.9
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14392.D 1 03/15/23 12:12 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.58 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.5 1.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 104%56-149%
98-08-8 aaa-Trifluorotoluene 96%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 101
FC339833.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-2 @ 4'
Lab Sample ID:FC3398-5 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:82.9
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38405.D 5 03/17/23 19:15 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)32.9 30 15 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 84%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 101
FC339833.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-3 @ 1'
Lab Sample ID:FC3398-6 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:89.8
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185777.D 1 03/15/23 13:56 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 7.26 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 150 77 ug/kg
71-43-2 Benzene ND 3.8 0.94 ug/kg
108-86-1 Bromobenzene ND 3.8 0.77 ug/kg
74-97-5 Bromochloromethane ND 3.8 1.1 ug/kg
75-27-4 Bromodichloromethane ND 3.8 0.77 ug/kg
75-25-2 Bromoform ND 3.8 0.77 ug/kg
78-93-3 2-Butanone (MEK) a ND 19 5.6 ug/kg
104-51-8 n-Butylbenzene ND 3.8 0.77 ug/kg
135-98-8 sec-Butylbenzene ND 3.8 0.77 ug/kg
98-06-6 tert-Butylbenzene ND 3.8 0.77 ug/kg
75-15-0 Carbon Disulfide ND 3.8 0.77 ug/kg
56-23-5 Carbon Tetrachloride ND 3.8 0.78 ug/kg
108-90-7 Chlorobenzene ND 3.8 0.77 ug/kg
75-00-3 Chloroethane a ND 3.8 1.5 ug/kg
67-66-3 Chloroform a ND 3.8 1.0 ug/kg
95-49-8 o-Chlorotoluene ND 3.8 0.77 ug/kg
106-43-4 p-Chlorotoluene ND 3.8 0.77 ug/kg
124-48-1 Dibromochloromethane ND 3.8 0.77 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 3.8 1.5 ug/kg
106-93-4 1,2-Dibromoethane ND 3.8 0.77 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.8 1.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.8 0.77 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.8 0.77 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.8 0.88 ug/kg
75-34-3 1,1-Dichloroethane ND 3.8 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 3.8 0.77 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.8 0.77 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.8 1.1 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.8 0.77 ug/kg
78-87-5 1,2-Dichloropropane ND 3.8 0.77 ug/kg
142-28-9 1,3-Dichloropropane ND 3.8 0.77 ug/kg
594-20-7 2,2-Dichloropropane ND 3.8 0.77 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 101
FC339833.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-3 @ 1'
Lab Sample ID:FC3398-6 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:89.8
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 3.8 0.78 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.8 0.77 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 3.8 0.77 ug/kg
100-41-4 Ethylbenzene ND 3.8 0.77 ug/kg
87-68-3 Hexachlorobutadiene ND 3.8 0.99 ug/kg
591-78-6 2-Hexanone a ND 19 5.8 ug/kg
98-82-8 Isopropylbenzene ND 3.8 0.77 ug/kg
99-87-6 p-Isopropyltoluene ND 3.8 0.77 ug/kg
74-83-9 Methyl Bromide a ND 3.8 1.5 ug/kg
74-87-3 Methyl Chloride a ND 3.8 1.5 ug/kg
74-95-3 Methylene Bromide ND 3.8 0.77 ug/kg
75-09-2 Methylene Chloride ND 15 8.4 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 19 5.8 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.8 0.77 ug/kg
91-20-3 Naphthalene ND 3.8 1.5 ug/kg
103-65-1 n-Propylbenzene ND 3.8 0.77 ug/kg
100-42-5 Styrene ND 3.8 0.77 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.8 0.79 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.8 0.77 ug/kg
127-18-4 Tetrachloroethylene ND 3.8 0.98 ug/kg
108-88-3 Toluene ND 15 7.7 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.8 1.1 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.8 0.77 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.8 0.77 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.8 0.77 ug/kg
79-01-6 Trichloroethylene ND 3.8 0.77 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.8 1.5 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.8 0.96 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.8 0.77 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.8 0.77 ug/kg
108-05-4 Vinyl Acetate a ND 19 13 ug/kg
75-01-4 Vinyl Chloride a ND 3.8 0.77 ug/kg
m,p-Xylene ND 7.7 0.84 ug/kg
95-47-6 o-Xylene ND 3.8 0.77 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 117%72-135%
2037-26-5 Toluene-D8 95%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 101
FC339833.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-3 @ 1'
Lab Sample ID:FC3398-6 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:89.8
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 101
FC339833.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-3 @ 1'
Lab Sample ID:FC3398-6 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:89.8
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14393.D 1 03/15/23 12:36 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.91 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 3.7 1.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 103%56-149%
98-08-8 aaa-Trifluorotoluene 95%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 101
FC339833.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-3 @ 1'
Lab Sample ID:FC3398-6 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:89.8
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38395.D 10 03/17/23 14:18 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)79.9 56 28 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 82%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 101
FC339833.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-3 @ 5'
Lab Sample ID:FC3398-7 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:79.1
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185778.D 1 03/15/23 14:21 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 9.14 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 140 69 ug/kg
71-43-2 Benzene ND 3.5 0.84 ug/kg
108-86-1 Bromobenzene ND 3.5 0.69 ug/kg
74-97-5 Bromochloromethane ND 3.5 1.0 ug/kg
75-27-4 Bromodichloromethane ND 3.5 0.69 ug/kg
75-25-2 Bromoform ND 3.5 0.69 ug/kg
78-93-3 2-Butanone (MEK) a ND 17 5.0 ug/kg
104-51-8 n-Butylbenzene ND 3.5 0.69 ug/kg
135-98-8 sec-Butylbenzene ND 3.5 0.69 ug/kg
98-06-6 tert-Butylbenzene ND 3.5 0.69 ug/kg
75-15-0 Carbon Disulfide 1.4 3.5 0.69 ug/kg J
56-23-5 Carbon Tetrachloride ND 3.5 0.71 ug/kg
108-90-7 Chlorobenzene ND 3.5 0.69 ug/kg
75-00-3 Chloroethane a ND 3.5 1.4 ug/kg
67-66-3 Chloroform a ND 3.5 0.92 ug/kg
95-49-8 o-Chlorotoluene ND 3.5 0.69 ug/kg
106-43-4 p-Chlorotoluene ND 3.5 0.69 ug/kg
124-48-1 Dibromochloromethane ND 3.5 0.69 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 3.5 1.3 ug/kg
106-93-4 1,2-Dibromoethane ND 3.5 0.69 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.5 1.4 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.5 0.69 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.5 0.69 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.5 0.80 ug/kg
75-34-3 1,1-Dichloroethane ND 3.5 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 3.5 0.69 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.5 0.69 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.5 0.95 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.5 0.69 ug/kg
78-87-5 1,2-Dichloropropane ND 3.5 0.69 ug/kg
142-28-9 1,3-Dichloropropane ND 3.5 0.69 ug/kg
594-20-7 2,2-Dichloropropane ND 3.5 0.69 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 101
FC339833.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-3 @ 5'
Lab Sample ID:FC3398-7 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:79.1
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 3.5 0.71 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.5 0.69 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 3.5 0.69 ug/kg
100-41-4 Ethylbenzene ND 3.5 0.69 ug/kg
87-68-3 Hexachlorobutadiene ND 3.5 0.89 ug/kg
591-78-6 2-Hexanone a ND 17 5.2 ug/kg
98-82-8 Isopropylbenzene ND 3.5 0.69 ug/kg
99-87-6 p-Isopropyltoluene ND 3.5 0.69 ug/kg
74-83-9 Methyl Bromide a ND 3.5 1.4 ug/kg
74-87-3 Methyl Chloride a ND 3.5 1.4 ug/kg
74-95-3 Methylene Bromide ND 3.5 0.69 ug/kg
75-09-2 Methylene Chloride ND 14 7.6 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 17 5.2 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.5 0.69 ug/kg
91-20-3 Naphthalene ND 3.5 1.4 ug/kg
103-65-1 n-Propylbenzene ND 3.5 0.69 ug/kg
100-42-5 Styrene ND 3.5 0.69 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.5 0.71 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.5 0.69 ug/kg
127-18-4 Tetrachloroethylene ND 3.5 0.89 ug/kg
108-88-3 Toluene ND 14 6.9 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.5 0.97 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.5 0.69 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.5 0.69 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.5 0.69 ug/kg
79-01-6 Trichloroethylene ND 3.5 0.69 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.5 1.4 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.5 0.86 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.5 0.69 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.5 0.69 ug/kg
108-05-4 Vinyl Acetate a ND 17 11 ug/kg
75-01-4 Vinyl Chloride a ND 3.5 0.69 ug/kg
m,p-Xylene ND 6.9 0.76 ug/kg
95-47-6 o-Xylene ND 3.5 0.69 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 121%72-135%
2037-26-5 Toluene-D8 95%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 101
FC339833.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-3 @ 5'
Lab Sample ID:FC3398-7 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:79.1
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 100%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 101
FC339833.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-3 @ 5'
Lab Sample ID:FC3398-7 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:79.1
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14398.D 1 03/15/23 15:28 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 9.32 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.7 1.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 102%56-149%
98-08-8 aaa-Trifluorotoluene 90%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 101
FC339833.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-3 @ 5'
Lab Sample ID:FC3398-7 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:79.1
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38396.D 5 03/17/23 14:48 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)70.8 31 16 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 90%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 101
FC339833.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-4 @ 1'
Lab Sample ID:FC3398-8 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:85.1
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185779.D 1 03/15/23 14:46 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 6.91 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 170 85 ug/kg
71-43-2 Benzene ND 4.3 1.0 ug/kg
108-86-1 Bromobenzene ND 4.3 0.85 ug/kg
74-97-5 Bromochloromethane ND 4.3 1.3 ug/kg
75-27-4 Bromodichloromethane ND 4.3 0.85 ug/kg
75-25-2 Bromoform ND 4.3 0.85 ug/kg
78-93-3 2-Butanone (MEK) a ND 21 6.2 ug/kg
104-51-8 n-Butylbenzene ND 4.3 0.85 ug/kg
135-98-8 sec-Butylbenzene ND 4.3 0.85 ug/kg
98-06-6 tert-Butylbenzene ND 4.3 0.85 ug/kg
75-15-0 Carbon Disulfide ND 4.3 0.85 ug/kg
56-23-5 Carbon Tetrachloride ND 4.3 0.87 ug/kg
108-90-7 Chlorobenzene ND 4.3 0.85 ug/kg
75-00-3 Chloroethane a ND 4.3 1.7 ug/kg
67-66-3 Chloroform a ND 4.3 1.1 ug/kg
95-49-8 o-Chlorotoluene ND 4.3 0.85 ug/kg
106-43-4 p-Chlorotoluene ND 4.3 0.85 ug/kg
124-48-1 Dibromochloromethane ND 4.3 0.85 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 4.3 1.6 ug/kg
106-93-4 1,2-Dibromoethane ND 4.3 0.85 ug/kg
75-71-8 Dichlorodifluoromethane a ND 4.3 1.7 ug/kg
95-50-1 1,2-Dichlorobenzene ND 4.3 0.85 ug/kg
541-73-1 1,3-Dichlorobenzene ND 4.3 0.85 ug/kg
106-46-7 1,4-Dichlorobenzene ND 4.3 0.98 ug/kg
75-34-3 1,1-Dichloroethane ND 4.3 1.5 ug/kg
107-06-2 1,2-Dichloroethane ND 4.3 0.85 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.3 0.85 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.3 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.3 0.85 ug/kg
78-87-5 1,2-Dichloropropane ND 4.3 0.85 ug/kg
142-28-9 1,3-Dichloropropane ND 4.3 0.85 ug/kg
594-20-7 2,2-Dichloropropane ND 4.3 0.85 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 101
FC339833.8
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-4 @ 1'
Lab Sample ID:FC3398-8 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:85.1
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 4.3 0.87 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.3 0.85 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.3 0.85 ug/kg
100-41-4 Ethylbenzene ND 4.3 0.85 ug/kg
87-68-3 Hexachlorobutadiene ND 4.3 1.1 ug/kg
591-78-6 2-Hexanone a ND 21 6.4 ug/kg
98-82-8 Isopropylbenzene ND 4.3 0.85 ug/kg
99-87-6 p-Isopropyltoluene ND 4.3 0.85 ug/kg
74-83-9 Methyl Bromide a ND 4.3 1.7 ug/kg
74-87-3 Methyl Chloride a ND 4.3 1.7 ug/kg
74-95-3 Methylene Bromide ND 4.3 0.85 ug/kg
75-09-2 Methylene Chloride ND 17 9.4 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 21 6.4 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 4.3 0.85 ug/kg
91-20-3 Naphthalene ND 4.3 1.7 ug/kg
103-65-1 n-Propylbenzene ND 4.3 0.85 ug/kg
100-42-5 Styrene ND 4.3 0.85 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.3 0.88 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.3 0.85 ug/kg
127-18-4 Tetrachloroethylene ND 4.3 1.1 ug/kg
108-88-3 Toluene ND 17 8.5 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.3 1.2 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.3 0.85 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.3 0.85 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.3 0.85 ug/kg
79-01-6 Trichloroethylene ND 4.3 0.85 ug/kg
75-69-4 Trichlorofluoromethane a ND 4.3 1.7 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.3 1.1 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.3 0.85 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.3 0.85 ug/kg
108-05-4 Vinyl Acetate a ND 21 14 ug/kg
75-01-4 Vinyl Chloride a ND 4.3 0.85 ug/kg
m,p-Xylene ND 8.5 0.94 ug/kg
95-47-6 o-Xylene ND 4.3 0.85 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 119%72-135%
2037-26-5 Toluene-D8 94%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 101
FC339833.8
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-4 @ 1'
Lab Sample ID:FC3398-8 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:85.1
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 101
FC339833.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 @ 1'
Lab Sample ID:FC3398-8 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:85.1
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14399.D 1 03/15/23 15:52 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.08 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.5 1.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 101%56-149%
98-08-8 aaa-Trifluorotoluene 91%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 101
FC339833.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 @ 1'
Lab Sample ID:FC3398-8 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:85.1
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38397.D 10 03/17/23 15:17 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)78.0 58 29 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 86%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 101
FC339833.8
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-4 @ 10'
Lab Sample ID:FC3398-9 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:84.2
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185780.D 1 03/15/23 15:10 AL n/a n/a V3C953
Run #2
Initial Weight Final Volume
Run #1 8.98 g 5.0 ml
Run #2
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 130 66 ug/kg
71-43-2 Benzene ND 3.3 0.81 ug/kg
108-86-1 Bromobenzene ND 3.3 0.66 ug/kg
74-97-5 Bromochloromethane ND 3.3 0.98 ug/kg
75-27-4 Bromodichloromethane ND 3.3 0.66 ug/kg
75-25-2 Bromoform ND 3.3 0.66 ug/kg
78-93-3 2-Butanone (MEK) a ND 17 4.8 ug/kg
104-51-8 n-Butylbenzene ND 3.3 0.66 ug/kg
135-98-8 sec-Butylbenzene ND 3.3 0.66 ug/kg
98-06-6 tert-Butylbenzene ND 3.3 0.66 ug/kg
75-15-0 Carbon Disulfide ND 3.3 0.66 ug/kg
56-23-5 Carbon Tetrachloride ND 3.3 0.67 ug/kg
108-90-7 Chlorobenzene ND 3.3 0.66 ug/kg
75-00-3 Chloroethane a ND 3.3 1.3 ug/kg
67-66-3 Chloroform a ND 3.3 0.88 ug/kg
95-49-8 o-Chlorotoluene ND 3.3 0.66 ug/kg
106-43-4 p-Chlorotoluene ND 3.3 0.66 ug/kg
124-48-1 Dibromochloromethane ND 3.3 0.66 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 3.3 1.3 ug/kg
106-93-4 1,2-Dibromoethane ND 3.3 0.66 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.3 1.3 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.3 0.66 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.3 0.66 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.3 0.76 ug/kg
75-34-3 1,1-Dichloroethane ND 3.3 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 3.3 0.66 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.3 0.66 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.3 0.91 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.3 0.66 ug/kg
78-87-5 1,2-Dichloropropane ND 3.3 0.66 ug/kg
142-28-9 1,3-Dichloropropane ND 3.3 0.66 ug/kg
594-20-7 2,2-Dichloropropane ND 3.3 0.66 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 101
FC339833.9
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-4 @ 10'
Lab Sample ID:FC3398-9 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:84.2
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 3.3 0.67 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.3 0.66 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 3.3 0.66 ug/kg
100-41-4 Ethylbenzene ND 3.3 0.66 ug/kg
87-68-3 Hexachlorobutadiene ND 3.3 0.85 ug/kg
591-78-6 2-Hexanone a ND 17 5.0 ug/kg
98-82-8 Isopropylbenzene ND 3.3 0.66 ug/kg
99-87-6 p-Isopropyltoluene ND 3.3 0.66 ug/kg
74-83-9 Methyl Bromide a ND 3.3 1.3 ug/kg
74-87-3 Methyl Chloride a ND 3.3 1.3 ug/kg
74-95-3 Methylene Bromide ND 3.3 0.66 ug/kg
75-09-2 Methylene Chloride ND 13 7.3 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 17 5.0 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.3 0.66 ug/kg
91-20-3 Naphthalene ND 3.3 1.3 ug/kg
103-65-1 n-Propylbenzene ND 3.3 0.66 ug/kg
100-42-5 Styrene ND 3.3 0.66 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.3 0.68 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.3 0.66 ug/kg
127-18-4 Tetrachloroethylene ND 3.3 0.85 ug/kg
108-88-3 Toluene ND 13 6.6 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.3 0.93 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.3 0.66 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.3 0.66 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.3 0.66 ug/kg
79-01-6 Trichloroethylene ND 3.3 0.66 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.3 1.3 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.3 0.83 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.3 0.66 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.3 0.66 ug/kg
108-05-4 Vinyl Acetate a ND 17 11 ug/kg
75-01-4 Vinyl Chloride a ND 3.3 0.66 ug/kg
m,p-Xylene ND 6.6 0.73 ug/kg
95-47-6 o-Xylene ND 3.3 0.66 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 120%72-135%
2037-26-5 Toluene-D8 97%75-126%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 101
FC339833.9
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-4 @ 10'
Lab Sample ID:FC3398-9 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8260D Percent Solids:84.2
Project:4357 Raleigh St, Charlotte, NC
VOA 8260 List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 102%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 101
FC339833.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 @ 10'
Lab Sample ID:FC3398-9 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C Percent Solids:84.2
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14400.D 1 03/15/23 16:16 JR n/a n/a G1U628
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.29 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.5 1.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 104%56-149%
98-08-8 aaa-Trifluorotoluene 94%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 101
FC339833.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 @ 10'
Lab Sample ID:FC3398-9 Date Sampled:03/13/23
Matrix:SO - Soil Date Received:03/14/23
Method:SW846 8015C SW846 3546 Percent Solids:84.2
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW38398.D 5 03/17/23 15:47 EG 03/16/23 10:00 OP95909 GWW1497
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)47.1 30 15 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 81%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 101
FC339833.9
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-4 GW
Lab Sample ID:FC3398-10 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:SM 6200B Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3A273.D 1 03/20/23 16:18 TD n/a n/a V3A13
Run #2 b E111722.D 1 03/21/23 16:49 TD n/a n/a VE2674
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 11.8 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND c 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
53 of 101
FC339833.10
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-4 GW
Lab Sample ID:FC3398-10 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:SM 6200B Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone d ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIB e ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.17 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.49 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.17 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%98%70-130%
2037-26-5 Toluene-D8 102%85%70-130%
460-00-4 4-Bromofluorobenzene 103%94%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 101
FC339833.10
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-4 GW
Lab Sample ID:FC3398-10 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:SM 6200B Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Sample was not preserved to a pH < 2.
(b) Sample vial(s) contained bubbles greater than 6mm.
(c) Result is from Run# 2
(d) Associated CCV and BS outside of control limits high, sample was ND.
(e) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
55 of 101
FC339833.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 GW
Lab Sample ID:FC3398-10 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LC856652.D 2 03/22/23 01:32 ALA n/a n/a L:GLC3518
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 10 0.28 ug/l
100-41-4 Ethylbenzene ND 10 0.35 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 0.27 ug/l
91-20-3 Naphthalene ND 10 0.82 ug/l
108-88-3 Toluene ND 10 0.30 ug/l
m,p-Xylene ND 20 0.80 ug/l
95-47-6 o-Xylene ND 10 0.37 ug/l
C5- C8 Aliphatics (Unadj.)ND 200 100 ug/l
C9- C12 Aliphatics (Unadj.)ND 200 100 ug/l
C9- C10 Aromatics (Unadj.)ND 200 40 ug/l
C5- C8 Aliphatics ND 200 100 ug/l
C9- C12 Aliphatics ND 200 100 ug/l
C9- C10 Aromatics ND 200 40 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 116%70-130%
615-59-8 2,5-Dibromotoluene 103%70-130%
(a) Dilution required due to high sediment. Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
56 of 101
FC339833.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 GW
Lab Sample ID:FC3398-10 Date Sampled:03/13/23
Matrix:AQ - Ground Water Date Received:03/14/23
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:4357 Raleigh St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN041740.D 1 03/17/23 00:16 AF 03/15/23 08:00 OP95890 GNN1919
Run #2
Initial Volume Final Volume
Run #1 1000 ml 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)267 200 80 ug/l
C11-C22 Aromatics 267 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 70%40-140%
580-13-2 2-Bromonaphthalene 108%40-140%
84-15-1 o-Terphenyl 87%40-140%
321-60-8 2-Fluorobiphenyl 107%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
57 of 101
FC339833.10
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
58 of 101
FC33984
FC3398: Chain of Custody
Page 1 of 2
59 of 101
FC339844.1
Job Number:FC3398 Client:BBG ASSESSMENTS
Date / Time Received:3/14/2023 9:40:00 AM Delivery Method:FEDEX
Project:4357 RALEIGH STREET
Airbill #'s:5707 9050 9638
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments FROZEN@ 3/14/2023 1125
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (5.2); Cooler 2: (4.2);
Cooler 1: (5.4); Cooler 2: (4.4);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:2
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:CARLSOD Date:Date:3/14/2023 9:40:00 AM
FC3398: Chain of Custody
Page 2 of 2
60 of 101
FC339844.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
61 of 101
FC33985
Method Blank Summary Page 1 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A13-MB 3A262.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
62 of 101
FC339855.1.1
Method Blank Summary Page 2 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A13-MB 3A262.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 92%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 101%70-130%
63 of 101
FC339855.1.1
Method Blank Summary Page 3 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A13-MB 3A262.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 104%70-130%
64 of 101
FC339855.1.1
Method Blank Summary Page 1 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C953-MB 3C185771.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.9 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
65 of 101
FC339855.1.2
Method Blank Summary Page 2 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C953-MB 3C185771.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Compound Result RL MDL Units Q
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/kg
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
74-95-3 Methylene Bromide ND 5.0 1.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%72-135%
66 of 101
FC339855.1.2
Method Blank Summary Page 3 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C953-MB 3C185771.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Surrogate Recoveries Limits
2037-26-5 Toluene-D8 97%75-126%
460-00-4 4-Bromofluorobenzene 93%71-133%
67 of 101
FC339855.1.2
Blank Spike Summary Page 1 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A13-BS 3A259.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 55.0 110 70-130
71-43-2 Benzene 10 10.7 107 70-130
108-86-1 Bromobenzene 10 10.6 106 70-130
74-97-5 Bromochloromethane 10 9.1 91 70-130
75-27-4 Bromodichloromethane 10 10 100 70-130
75-25-2 Bromoform 10 9.6 96 70-130
78-93-3 2-Butanone (MEK)50 56.9 114 70-130
104-51-8 n-Butylbenzene 10 11.4 114 70-130
135-98-8 sec-Butylbenzene 10 10.4 104 70-130
98-06-6 tert-Butylbenzene 10 11.0 110 70-130
56-23-5 Carbon Tetrachloride 10 10.4 104 70-130
108-90-7 Chlorobenzene 10 10.3 103 70-130
75-00-3 Chloroethane 10 10.5 105 60-140
67-66-3 Chloroform 10 10.2 102 70-130
95-49-8 o-Chlorotoluene 10 10.7 107 70-130
106-43-4 p-Chlorotoluene 10 10.9 109 70-130
124-48-1 Dibromochloromethane 10 8.6 86 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
75-71-8 Dichlorodifluoromethane 10 11.0 110 60-140
95-50-1 1,2-Dichlorobenzene 10 10.4 104 70-130
541-73-1 1,3-Dichlorobenzene 10 10.2 102 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 10.2 102 70-130
107-06-2 1,2-Dichloroethane 10 10.9 109 70-130
75-35-4 1,1-Dichloroethylene 10 10.4 104 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.4 104 70-130
78-87-5 1,2-Dichloropropane 10 11.7 117 70-130
142-28-9 1,3-Dichloropropane 10 11.9 119 70-130
594-20-7 2,2-Dichloropropane 10 11.2 112 70-130
563-58-6 1,1-Dichloropropene 10 11.1 111 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.2 112 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.0 90 70-130
108-20-3 Di-Isopropyl Ether 10 11.9 119 70-130
64-17-5 Ethyl Alcohol 500 491 98 70-130
100-41-4 Ethylbenzene 10 10.5 105 70-130
* = Outside of Control Limits.
68 of 101
FC339855.2.1
Blank Spike Summary Page 2 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A13-BS 3A259.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 68.0 136*70-130
98-82-8 Isopropylbenzene 10 10.5 105 70-130
99-87-6 p-Isopropyltoluene 10 10.6 106 70-130
74-83-9 Methyl Bromide 10 11.6 116 60-140
74-87-3 Methyl Chloride 10 12.5 125 60-140
75-09-2 Methylene Chloride 10 11.5 115 70-130
108-10-1 4-Methyl-2-pentanone (MIBK)50 64.0 128 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.7 117 70-130
91-20-3 Naphthalene 10 10.9 109 70-130
103-65-1 n-Propylbenzene 10 10.8 108 70-130
100-42-5 Styrene 10 10.2 102 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.8 88 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.5 115 70-130
127-18-4 Tetrachloroethylene 10 9.8 98 70-130
108-88-3 Toluene 10 10.6 106 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.1 101 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.3 103 70-130
71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130
79-00-5 1,1,2-Trichloroethane 10 11.2 112 70-130
79-01-6 Trichloroethylene 10 10.4 104 70-130
75-69-4 Trichlorofluoromethane 10 10.5 105 60-140
96-18-4 1,2,3-Trichloropropane 10 11.7 117 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.7 107 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.8 108 70-130
108-05-4 Vinyl Acetate 50 49.2 98 70-130
75-01-4 Vinyl Chloride 10 11.3 113 60-140
m,p-Xylene 20 21.5 108 70-130
95-47-6 o-Xylene 10 10.5 105 70-130
1330-20-7 Xylene (total)30 32.0 107 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 92%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 100%70-130%
* = Outside of Control Limits.
69 of 101
FC339855.2.1
Blank Spike Summary Page 3 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A13-BS 3A259.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 105%70-130%
* = Outside of Control Limits.
70 of 101
FC339855.2.1
Blank Spike Summary Page 1 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C953-BS 3C185769.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 298 119 61-152
71-43-2 Benzene 50 53.1 106 76-126
108-86-1 Bromobenzene 50 50.9 102 76-122
74-97-5 Bromochloromethane 50 55.5 111 77-120
75-27-4 Bromodichloromethane 50 54.7 109 74-130
75-25-2 Bromoform 50 49.0 98 76-127
78-93-3 2-Butanone (MEK)250 302 121 75-137
104-51-8 n-Butylbenzene 50 53.0 106 71-128
135-98-8 sec-Butylbenzene 50 48.4 97 79-135
98-06-6 tert-Butylbenzene 50 50.6 101 77-133
75-15-0 Carbon Disulfide 50 55.3 111 72-122
56-23-5 Carbon Tetrachloride 50 55.4 111 78-133
108-90-7 Chlorobenzene 50 50.7 101 81-129
75-00-3 Chloroethane 50 37.9 76 68-133
67-66-3 Chloroform 50 55.5 111 72-123
95-49-8 o-Chlorotoluene 50 50.5 101 77-129
106-43-4 p-Chlorotoluene 50 49.7 99 80-134
124-48-1 Dibromochloromethane 50 51.6 103 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 53.6 107 70-137
106-93-4 1,2-Dibromoethane 50 53.5 107 77-126
75-71-8 Dichlorodifluoromethane 50 52.1 104 68-168
95-50-1 1,2-Dichlorobenzene 50 49.5 99 80-129
541-73-1 1,3-Dichlorobenzene 50 49.0 98 81-129
106-46-7 1,4-Dichlorobenzene 50 49.9 100 76-130
75-34-3 1,1-Dichloroethane 50 52.2 104 73-125
107-06-2 1,2-Dichloroethane 50 56.9 114 74-128
75-35-4 1,1-Dichloroethylene 50 52.3 105 81-136
156-59-2 cis-1,2-Dichloroethylene 50 52.1 104 74-126
156-60-5 trans-1,2-Dichloroethylene 50 53.9 108 70-127
78-87-5 1,2-Dichloropropane 50 54.5 109 74-125
142-28-9 1,3-Dichloropropane 50 56.0 112 76-122
594-20-7 2,2-Dichloropropane 50 56.9 114 77-133
563-58-6 1,1-Dichloropropene 50 55.1 110 75-130
10061-01-5 cis-1,3-Dichloropropene 50 55.8 112 80-123
10061-02-6 trans-1,3-Dichloropropene 50 51.5 103 75-131
100-41-4 Ethylbenzene 50 50.5 101 77-123
* = Outside of Control Limits.
71 of 101
FC339855.2.2
Blank Spike Summary Page 2 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C953-BS 3C185769.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
87-68-3 Hexachlorobutadiene 50 51.3 103 74-136
591-78-6 2-Hexanone 250 301 120 72-133
98-82-8 Isopropylbenzene 50 50.6 101 80-136
99-87-6 p-Isopropyltoluene 50 49.3 99 77-131
74-83-9 Methyl Bromide 50 58.9 118 65-139
74-87-3 Methyl Chloride 50 55.6 111 71-144
74-95-3 Methylene Bromide 50 58.1 116 74-124
75-09-2 Methylene Chloride 50 51.5 103 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 289 116 76-132
1634-04-4 Methyl Tert Butyl Ether 50 58.7 117 77-120
91-20-3 Naphthalene 50 51.6 103 79-129
103-65-1 n-Propylbenzene 50 49.6 99 80-135
100-42-5 Styrene 50 51.4 103 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 52.6 105 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 51.7 103 71-126
127-18-4 Tetrachloroethylene 50 50.1 100 79-130
108-88-3 Toluene 50 51.3 103 76-124
87-61-6 1,2,3-Trichlorobenzene 50 52.1 104 77-128
120-82-1 1,2,4-Trichlorobenzene 50 52.1 104 78-130
71-55-6 1,1,1-Trichloroethane 50 54.7 109 70-129
79-00-5 1,1,2-Trichloroethane 50 52.3 105 74-124
79-01-6 Trichloroethylene 50 53.9 108 75-128
75-69-4 Trichlorofluoromethane 50 62.0 124 73-145
96-18-4 1,2,3-Trichloropropane 50 56.3 113 74-127
95-63-6 1,2,4-Trimethylbenzene 50 49.8 100 74-123
108-67-8 1,3,5-Trimethylbenzene 50 51.1 102 73-122
108-05-4 Vinyl Acetate 250 265 106 48-164
75-01-4 Vinyl Chloride 50 54.6 109 76-141
m,p-Xylene 100 102 102 80-128
95-47-6 o-Xylene 50 50.3 101 80-132
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%72-135%
* = Outside of Control Limits.
72 of 101
FC339855.2.2
Blank Spike Summary Page 3 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C953-BS 3C185769.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Surrogate Recoveries BSP Limits
2037-26-5 Toluene-D8 97%75-126%
460-00-4 4-Bromofluorobenzene 98%71-133%
* = Outside of Control Limits.
73 of 101
FC339855.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-3MS 3A275.D 5 03/20/23 TD n/a n/a V3A13
FC3398-3MSD 3A276.D 5 03/20/23 TD n/a n/a V3A13
FC3398-3 a 3A272.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
FC3398-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone 8.9 J 250 346 135*250 345 134*0 70-130/20
71-43-2 Benzene ND 50 56.7 113 50 59.1 118 4 70-130/20
108-86-1 Bromobenzene ND 50 53.3 107 50 55.4 111 4 70-130/20
74-97-5 Bromochloromethane ND 50 45.5 91 50 46.4 93 2 70-130/20
75-27-4 Bromodichloromethane ND 50 49.8 100 50 51.2 102 3 70-130/20
75-25-2 Bromoform ND 50 48.3 97 50 49.6 99 3 70-130/20
78-93-3 2-Butanone (MEK)ND 250 374 150*250 379 152*1 70-130/20
104-51-8 n-Butylbenzene 1.0 50 57.2 112 50 64.6 127 12 70-130/20
135-98-8 sec-Butylbenzene 1.8 50 51.8 100 50 58.4 113 12 70-130/20
98-06-6 tert-Butylbenzene 0.15 J 50 54.0 108 50 59.1 118 9 70-130/20
56-23-5 Carbon Tetrachloride ND 50 54.2 108 50 56.0 112 3 70-130/20
108-90-7 Chlorobenzene ND 50 52.0 104 50 54.8 110 5 70-130/20
75-00-3 Chloroethane ND 50 39.9 80 50 49.5 99 21*60-140/20
67-66-3 Chloroform ND 50 53.7 107 50 54.4 109 1 70-130/20
95-49-8 o-Chlorotoluene 0.24 J 50 54.2 108 50 57.6 115 6 70-130/20
106-43-4 p-Chlorotoluene ND 50 54.4 109 50 57.8 116 6 70-130/20
124-48-1 Dibromochloromethane ND 50 42.7 85 50 44.2 88 3 70-130/20
106-93-4 1,2-Dibromoethane ND 50 54.7 109 50 56.3 113 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 51.2 102 50 59.7 119 15 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 51.2 102 50 53.9 108 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 49.8 100 50 53.2 106 7 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 51.2 102 50 53.9 108 5 70-130/20
75-34-3 1,1-Dichloroethane ND 50 53.6 107 50 54.8 110 2 70-130/20
107-06-2 1,2-Dichloroethane ND 50 56.5 113 50 56.9 114 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 56.7 113 50 58.8 118 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 50.3 101 50 52.0 104 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 54.8 110 50 57.5 115 5 70-130/20
78-87-5 1,2-Dichloropropane ND 50 60.0 120 50 63.7 127 6 70-130/20
142-28-9 1,3-Dichloropropane ND 50 63.3 127 50 64.9 130 2 70-130/20
594-20-7 2,2-Dichloropropane ND 50 59.5 119 50 62.0 124 4 70-130/20
563-58-6 1,1-Dichloropropene ND 50 60.6 121 50 63.4 127 5 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 56.4 113 50 59.2 118 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 46.5 93 50 48.9 98 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 63.2 126 50 65.5 131*4 70-130/20
64-17-5 Ethyl Alcohol ND 2500 3280 131*2500 3150 126 4 70-130/20
100-41-4 Ethylbenzene 0.83 50 53.6 106 50 57.8 114 8 70-130/20
* = Outside of Control Limits.
74 of 101
FC339855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-3MS 3A275.D 5 03/20/23 TD n/a n/a V3A13
FC3398-3MSD 3A276.D 5 03/20/23 TD n/a n/a V3A13
FC3398-3 a 3A272.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
FC3398-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 250 436 174*250 451 180*3 70-130/20
98-82-8 Isopropylbenzene 1.2 50 54.0 106 50 58.7 115 8 70-130/20
99-87-6 p-Isopropyltoluene 1.2 50 51.7 101 50 58.3 114 12 70-130/20
74-83-9 Methyl Bromide ND 50 44.4 89 50 56.9 114 25*60-140/20
74-87-3 Methyl Chloride ND 50 56.5 113 50 65.9 132 15 60-140/20
75-09-2 Methylene Chloride ND 50 61.7 123 50 62.9 126 2 70-130/20
108-10-1 4-Methyl-2-pentanone (MIBK)ND 250 408 163*250 422 169*3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 63.3 127 50 64.9 130 2 70-130/20
91-20-3 Naphthalene 8.0 50 68.3 121 50 71.0 126 4 70-130/20
103-65-1 n-Propylbenzene 1.9 50 55.3 107 50 60.9 118 10 70-130/20
100-42-5 Styrene ND 50 51.7 103 50 54.5 109 5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 44.2 88 50 46.5 93 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 62.5 125 50 63.2 126 1 70-130/20
127-18-4 Tetrachloroethylene 0.51 50 53.5 106 50 55.2 109 3 70-130/20
108-88-3 Toluene 0.42 J 50 55.3 110 50 58.4 116 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 50.7 101 50 52.7 105 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 50.3 101 50 53.6 107 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 54.2 108 50 56.3 113 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 60.9 122 50 61.3 123 1 70-130/20
79-01-6 Trichloroethylene ND 50 55.5 111 50 58.3 117 5 70-130/20
75-69-4 Trichlorofluoromethane ND 50 46.4 93 50 54.2 108 16 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 65.9 132*50 66.6 133*1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 7.9 50 60.3 105 50 65.6 115 8 70-130/20
108-67-8 1,3,5-Trimethylbenzene 2.1 50 55.4 107 50 60.0 116 8 70-130/20
108-05-4 Vinyl Acetate ND 250 270 108 250 265 106 2 70-130/20
75-01-4 Vinyl Chloride ND 50 49.8 100 50 58.9 118 17 60-140/20
m,p-Xylene 0.83 J 100 110 109 100 117 116 6 70-130/20
95-47-6 o-Xylene 1.1 50 54.7 107 50 57.9 114 6 70-130/20
1330-20-7 Xylene (total)1.9 150 164 108 150 175 115 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FC3398-3 Limits
1868-53-7 Dibromofluoromethane 93%90%89%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%104%106%70-130%
2037-26-5 Toluene-D8 100%101%101%70-130%
* = Outside of Control Limits.
75 of 101
FC339855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-3MS 3A275.D 5 03/20/23 TD n/a n/a V3A13
FC3398-3MSD 3A276.D 5 03/20/23 TD n/a n/a V3A13
FC3398-3 a 3A272.D 1 03/20/23 TD n/a n/a V3A13
The QC reported here applies to the following samples:Method: SM 6200B
FC3398-3, FC3398-10
CAS No.Surrogate Recoveries MS MSD FC3398-3 Limits
460-00-4 4-Bromofluorobenzene 106%106%107%70-130%
(a) Sample was not preserved to a pH < 2.
* = Outside of Control Limits.
76 of 101
FC339855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-4MS 3C185790.D 1 03/15/23 AL n/a n/a V3C953
FC3398-4MSD 3C185791.D 1 03/15/23 AL n/a n/a V3C953
FC3398-4 3C185775.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
FC3398-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 294 313 106 282 297 105 5 61-152/27
71-43-2 Benzene ND 58.8 57.6 98 56.3 59.2 105 3 76-126/26
108-86-1 Bromobenzene ND 58.8 49.9 85 56.3 51.6 92 3 76-122/32
74-97-5 Bromochloromethane ND 58.8 57.4 98 56.3 59.0 105 3 77-120/24
75-27-4 Bromodichloromethane ND 58.8 56.1 95 56.3 58.5 104 4 74-130/25
75-25-2 Bromoform ND 58.8 46.7 79 56.3 48.3 86 3 76-127/26
78-93-3 2-Butanone (MEK)ND 294 309 105 282 301 107 3 75-137/25
104-51-8 n-Butylbenzene ND 58.8 47.6 81 56.3 49.0 87 3 71-128/35
135-98-8 sec-Butylbenzene ND 58.8 46.4 79 56.3 47.2 84 2 79-135/34
98-06-6 tert-Butylbenzene ND 58.8 49.3 84 56.3 50.0 89 1 77-133/34
75-15-0 Carbon Disulfide ND 58.8 59.1 100 56.3 60.7 108 3 72-122/29
56-23-5 Carbon Tetrachloride ND 58.8 57.3 97 56.3 59.1 105 3 78-133/29
108-90-7 Chlorobenzene ND 58.8 51.5 88 56.3 52.4 93 2 81-129/29
75-00-3 Chloroethane ND 58.8 33.8 57*56.3 43.9 78 26 68-133/29
67-66-3 Chloroform ND 58.8 59.5 101 56.3 59.8 106 1 72-123/26
95-49-8 o-Chlorotoluene ND 58.8 48.7 83 56.3 50.3 89 3 77-129/33
106-43-4 p-Chlorotoluene ND 58.8 47.4 81 56.3 48.6 86 3 80-134/33
124-48-1 Dibromochloromethane ND 58.8 50.5 86 56.3 52.1 92 3 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND 58.8 50.4 86 56.3 51.1 91 1 70-137/29
106-93-4 1,2-Dibromoethane ND 58.8 53.0 90 56.3 54.1 96 2 77-126/26
75-71-8 Dichlorodifluoromethane ND 58.8 58.1 99 56.3 54.8 97 6 68-168/29
95-50-1 1,2-Dichlorobenzene ND 58.8 45.0 76*56.3 46.0 82 2 80-129/32
541-73-1 1,3-Dichlorobenzene ND 58.8 43.9 75*56.3 45.8 81 4 81-129/33
106-46-7 1,4-Dichlorobenzene ND 58.8 45.1 77 56.3 47.2 84 5 76-130/32
75-34-3 1,1-Dichloroethane ND 58.8 57.1 97 56.3 57.4 102 1 73-125/27
107-06-2 1,2-Dichloroethane ND 58.8 59.0 100 56.3 59.7 106 1 74-128/23
75-35-4 1,1-Dichloroethylene ND 58.8 57.5 98 56.3 57.3 102 0 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 58.8 55.8 95 56.3 57.9 103 4 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 58.8 57.9 98 56.3 58.6 104 1 70-127/27
78-87-5 1,2-Dichloropropane ND 58.8 59.9 102 56.3 61.2 109 2 74-125/25
142-28-9 1,3-Dichloropropane ND 58.8 57.8 98 56.3 58.4 104 1 76-122/26
594-20-7 2,2-Dichloropropane ND 58.8 58.5 99 56.3 61.0 108 4 77-133/28
563-58-6 1,1-Dichloropropene ND 58.8 59.7 101 56.3 62.0 110 4 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 58.8 57.4 98 56.3 57.8 103 1 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 58.8 49.7 84 56.3 51.2 91 3 75-131/28
100-41-4 Ethylbenzene ND 58.8 52.4 89 56.3 53.2 94 2 77-123/31
* = Outside of Control Limits.
77 of 101
FC339855.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-4MS 3C185790.D 1 03/15/23 AL n/a n/a V3C953
FC3398-4MSD 3C185791.D 1 03/15/23 AL n/a n/a V3C953
FC3398-4 3C185775.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
FC3398-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
87-68-3 Hexachlorobutadiene ND 58.8 39.3 67*56.3 40.4 72*3 74-136/38
591-78-6 2-Hexanone ND 294 304 103 282 300 106 1 72-133/26
98-82-8 Isopropylbenzene ND 58.8 51.4 87 56.3 51.8 92 1 80-136/32
99-87-6 p-Isopropyltoluene ND 58.8 47.1 80 56.3 47.7 85 1 77-131/34
74-83-9 Methyl Bromide ND 58.8 61.7 105 56.3 64.3 114 4 65-139/31
74-87-3 Methyl Chloride ND 58.8 60.3 102 56.3 58.9 105 2 71-144/27
74-95-3 Methylene Bromide ND 58.8 59.8 102 56.3 60.8 108 2 74-124/24
75-09-2 Methylene Chloride ND 58.8 60.4 103 56.3 53.7 95 12 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 294 296 101 282 290 103 2 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 58.8 59.9 102 56.3 61.2 109 2 77-120/24
91-20-3 Naphthalene ND 58.8 42.7 73*56.3 45.0 80 5 79-129/33
103-65-1 n-Propylbenzene ND 58.8 48.9 83 56.3 49.8 88 2 80-135/33
100-42-5 Styrene ND 58.8 51.4 87 56.3 52.5 93 2 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 58.8 51.9 88 56.3 53.8 95 4 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 58.8 51.8 88 56.3 52.6 93 2 71-126/30
127-18-4 Tetrachloroethylene ND 58.8 55.9 95 56.3 54.3 96 3 79-130/31
108-88-3 Toluene ND 58.8 53.8 91 56.3 54.7 97 2 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 58.8 39.1 66*56.3 41.2 73*5 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 58.8 39.4 67*56.3 42.3 75*7 78-130/34
71-55-6 1,1,1-Trichloroethane ND 58.8 58.9 100 56.3 60.0 106 2 70-129/27
79-00-5 1,1,2-Trichloroethane ND 58.8 53.8 91 56.3 54.8 97 2 74-124/28
79-01-6 Trichloroethylene ND 58.8 58.4 99 56.3 59.2 105 1 75-128/27
75-69-4 Trichlorofluoromethane ND 58.8 70.3 119 56.3 69.0 122 2 73-145/31
96-18-4 1,2,3-Trichloropropane ND 58.8 54.7 93 56.3 54.8 97 0 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 58.8 47.9 81 56.3 49.5 88 3 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 58.8 49.8 85 56.3 51.4 91 3 73-122/33
108-05-4 Vinyl Acetate ND 294 134 46*282 136 48 1 48-164/37
75-01-4 Vinyl Chloride ND 58.8 62.2 106 56.3 61.8 110 1 76-141/27
m,p-Xylene ND 118 104 88 113 105 93 1 80-128/30
95-47-6 o-Xylene ND 58.8 50.9 87 56.3 51.8 92 2 80-132/30
CAS No.Surrogate Recoveries MS MSD FC3398-4 Limits
1868-53-7 Dibromofluoromethane 104%104%100%75-124%
17060-07-0 1,2-Dichloroethane-D4 104%106%117%72-135%
* = Outside of Control Limits.
78 of 101
FC339855.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-4MS 3C185790.D 1 03/15/23 AL n/a n/a V3C953
FC3398-4MSD 3C185791.D 1 03/15/23 AL n/a n/a V3C953
FC3398-4 3C185775.D 1 03/15/23 AL n/a n/a V3C953
The QC reported here applies to the following samples:Method: SW846 8260D
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Surrogate Recoveries MS MSD FC3398-4 Limits
2037-26-5 Toluene-D8 97%97%96%75-126%
460-00-4 4-Bromofluorobenzene 95%96%97%71-133%
* = Outside of Control Limits.
79 of 101
FC339855.3.2
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
80 of 101
FC33986
Method Blank Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U628-MB 1U14387.D 1 03/15/23 JR n/a n/a G1U628
The QC reported here applies to the following samples:Method: SW846 8015C
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.0 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 99%56-149%
98-08-8 aaa-Trifluorotoluene 92%66-132%
81 of 101
FC339866.1.1
Blank Spike Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U628-BS 1U14386.D 1 03/15/23 JR n/a n/a G1U628
The QC reported here applies to the following samples:Method: ADEC AK101
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
Spike BSP BSP
CAS No.Compound mg/l mg/l %Limits
TPH-GRO (C6-C10)0.4 0.343 86 60-120
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 104%60-120%
98-08-8 aaa-Trifluorotoluene 96%50-150%
* = Outside of Control Limits.
82 of 101
FC339866.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3398-2MS 1U14389.D 1 03/15/23 JR n/a n/a G1U628
FC3398-2MSD 1U14390.D 1 03/15/23 JR n/a n/a G1U628
FC3398-2 1U14388.D 1 03/15/23 JR n/a n/a G1U628
The QC reported here applies to the following samples:Method: SW846 8015C
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
FC3398-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)ND 19.2 16.2 84 19.2 15.0 78 8 74-128/17
CAS No.Surrogate Recoveries MS MSD FC3398-2 Limits
460-00-4 4-Bromofluorobenzene 97%94%95%56-149%
98-08-8 aaa-Trifluorotoluene 94%90%89%66-132%
* = Outside of Control Limits.
83 of 101
FC339866.3.1
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
84 of 101
FC33987
Method Blank Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95890-MB NN041724.D 1 03/16/23 AF 03/15/23 OP95890 GNN1919
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC3398-3, FC3398-10
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C11-C22 Aromatics ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 81%40-140%
580-13-2 2-Bromonaphthalene 128%40-140%
84-15-1 o-Terphenyl 104%40-140%
321-60-8 2-Fluorobiphenyl 127%40-140%
85 of 101
FC339877.1.1
Method Blank Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95909-MB WW38376.D 1 03/17/23 EG 03/16/23 OP95909 GWW1497
The QC reported here applies to the following samples:Method: SW846 8015C
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 5.0 2.5 mg/kg
CAS No.Surrogate Recoveries Limits
84-15-1 o-Terphenyl 81%56-122%
86 of 101
FC339877.1.2
Blank Spike Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95909-BS WW38377.D 1 03/17/23 EG 03/16/23 OP95909 GWW1497
The QC reported here applies to the following samples:Method: SW846 8015C
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH (C10-C28)50 46.8 94 62-116
CAS No.Surrogate Recoveries BSP Limits
84-15-1 o-Terphenyl 90%56-122%
* = Outside of Control Limits.
87 of 101
FC339877.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95890-BS NN041725.D 1 03/16/23 AF 03/15/23 OP95890 GNN1919
OP95890-BSD NN041726.D 1 03/16/23 AF 03/15/23 OP95890 GNN1919
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC3398-3, FC3398-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
83-32-9 Acenaphthene 100 109 109 110 110 1 40-140/30
208-96-8 Acenaphthylene 100 102 102 102 102 0 40-140/30
120-12-7 Anthracene 100 111 111 110 110 1 40-140/30
56-55-3 Benzo(a)anthracene 100 125 125 124 124 1 40-140/30
50-32-8 Benzo(a)pyrene 100 121 121 119 119 2 40-140/30
205-99-2 Benzo(b)fluoranthene 100 114 114 112 112 2 40-140/30
191-24-2 Benzo(g,h,i)perylene 100 108 108 106 106 2 40-140/30
207-08-9 Benzo(k)fluoranthene 100 109 109 108 108 1 40-140/30
218-01-9 Chrysene 100 117 117 116 116 1 40-140/30
53-70-3 Dibenzo(a,h)anthracene 100 116 116 114 114 2 40-140/30
206-44-0 Fluoranthene 100 112 112 111 111 1 40-140/30
86-73-7 Fluorene 100 109 109 109 109 0 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 100 109 109 107 107 2 40-140/30
91-57-6 2-Methylnaphthalene 100 96.9 97 96.6 97 0 40-140/30
91-20-3 Naphthalene 100 92.7 93 91.6 92 1 40-140/30
85-01-8 Phenanthrene 100 111 111 111 111 0 40-140/30
129-00-0 Pyrene 100 118 118 117 117 1 40-140/30
C11-C22 Aromatics (Unadj.)1700 1920 113 1910 112 1 40-140/30
C9-C18 Aliphatics 600 417 70 414 69 1 40-140/30
C19-C36 Aliphatics 800 745 93 750 94 1 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 83%82%40-140%
580-13-2 2-Bromonaphthalene 103%106%40-140%
84-15-1 o-Terphenyl 101%100%40-140%
321-60-8 2-Fluorobiphenyl 102%105%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP95890-BS 2-Methylnaphthalene 96.9 ND 0.0%5.0
OP95890-BS Naphthalene 92.7 ND 0.0%5.0
OP95890-BSD 2-Methylnaphthalene 96.6 ND 0.0%5.0
OP95890-BSD Naphthalene 91.6 ND 0.0%5.0
* = Outside of Control Limits.
88 of 101
FC339877.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95890-MS NN041727.D 1 03/16/23 AF 03/15/23 OP95890 GNN1919
OP95890-MSD NN041728.D 1 03/16/23 AF 03/15/23 OP95890 GNN1919
FC3332-2 NN041729.D 1 03/16/23 AF 03/15/23 OP95890 GNN1919
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC3398-3, FC3398-10
FC3332-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
83-32-9 Acenaphthene ND 200 178 89 200 228 114 25 40-140/50
208-96-8 Acenaphthylene ND 200 165 83 200 213 107 25 40-140/50
120-12-7 Anthracene ND 200 178 89 200 233 117 27 40-140/50
56-55-3 Benzo(a)anthracene ND 200 201 101 200 262 131 26 40-140/50
50-32-8 Benzo(a)pyrene ND 200 194 97 200 253 127 26 40-140/50
205-99-2 Benzo(b)fluoranthene ND 200 182 91 200 237 119 26 40-140/50
191-24-2 Benzo(g,h,i)perylene ND 200 173 87 200 225 113 26 40-140/50
207-08-9 Benzo(k)fluoranthene ND 200 175 88 200 229 115 27 40-140/50
218-01-9 Chrysene ND 200 188 94 200 244 122 26 40-140/50
53-70-3 Dibenzo(a,h)anthracene ND 200 186 93 200 242 121 26 40-140/50
206-44-0 Fluoranthene ND 200 179 90 200 233 117 26 40-140/50
86-73-7 Fluorene ND 200 176 88 200 227 114 25 40-140/50
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 175 88 200 228 114 26 40-140/50
91-57-6 2-Methylnaphthalene ND 200 156 78 200 201 101 25 40-140/50
91-20-3 Naphthalene ND 200 148 74 200 192 96 26 40-140/50
85-01-8 Phenanthrene ND 200 178 89 200 231 116 26 40-140/50
129-00-0 Pyrene ND 200 189 95 200 246 123 26 40-140/50
C11-C22 Aromatics (Unadj.)ND 3400 3100 91 3400 4010 118 26 40-140/50
C9-C18 Aliphatics ND 1200 717 60 1200 848 71 17 40-140/50
C19-C36 Aliphatics ND 1600 1450 91 1600 1520 95 5 40-140/50
CAS No.Surrogate Recoveries MS MSD FC3332-2 Limits
3386-33-2 1-Chlorooctadecane 71%83%78%40-140%
580-13-2 2-Bromonaphthalene 103%112%93%40-140%
84-15-1 o-Terphenyl 80%105%86%40-140%
321-60-8 2-Fluorobiphenyl 103%112%92%40-140%
* = Outside of Control Limits.
89 of 101
FC339877.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:BBGFLT BBG Assessment
Project:4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95909-MS WW38399.D 100 03/17/23 EG 03/16/23 OP95909 GWW1497
OP95909-MSD WW38400.D 100 03/17/23 EG 03/16/23 OP95909 GWW1497
FC3398-1 WW38404.D 100 03/17/23 EG 03/16/23 OP95909 GWW1497
The QC reported here applies to the following samples:Method: SW846 8015C
FC3398-1, FC3398-2, FC3398-4, FC3398-5, FC3398-6, FC3398-7, FC3398-8, FC3398-9
FC3398-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH (C10-C28)2380 60.7 2100 -461* a 61 2660 459* a 24 62-116/35
CAS No.Surrogate Recoveries MS MSD FC3398-1 Limits
84-15-1 o-Terphenyl 0% b 0% b 0% b 56-122%
(a) Outside control limits due to high level in sample relative to spike amount.
(b) Outside control limits due to dilution.
* = Outside of Control Limits.
90 of 101
FC339877.4.2
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
(SGS Scott, LA)
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 8
91 of 101
FC33988
FC3398: Chain of Custody
Page 1 of 4
SGS Scott, LA
92 of 101
FC339888.1
FC3398: Chain of Custody
Page 2 of 4
93 of 101
FC339888.1
Job Number:FC3398 Client:SGS-FL
Date / Time Received:3/21/2023 9:45:00 AM Delivery Method:FEDEX
Project:4357 RALEIGH ST
4. No. Coolers:1
Airbill #'s:6134 6606 8339
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR002;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments Coc states 3 vials per ID, rec'd 2 vials per ID.
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (2/1.8);
SGS Sample Receipt Summary
FC3398: Chain of Custody
Page 3 of 4
94 of 101
FC339888.1
Page 2 of 2
Problem Resolution
CSR:Response Date:
Response:
Job Number:FC3398
FC3398: Chain of Custody
Page 4 of 4
95 of 101
FC339888.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
(SGS Scott, LA)
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 9
96 of 101
FC33989
Method Blank Summary Page 1 of 1
Job Number:FC3398
Account:ALSE SGS Orlando, FL
Project:BBGFLT: 4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLC3518-MB1 LC856637.D 1 03/21/23 JB n/a n/a GLC3518
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC3398-10
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene ND 5.0 0.17 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 8.8 5.0 0.41 ug/l
108-88-3 Toluene ND 5.0 0.15 ug/l
m,p-Xylene ND 10 0.40 ug/l
95-47-6 o-Xylene ND 5.0 0.18 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 87%70-130%
615-59-8 2,5-Dibromotoluene 89%70-130%
97 of 101
FC339899.1.1
Method Blank Summary Page 1 of 1
Job Number:FC3398
Account:ALSE SGS Orlando, FL
Project:BBGFLT: 4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2401-MB1 LE040992.D 1 03/23/23 JB n/a n/a GLE2401
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC3398-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene 0.26 5.0 0.17 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 2.1 5.0 0.41 ug/l J
108-88-3 Toluene ND 5.0 0.15 ug/l
m,p-Xylene 0.80 10 0.40 ug/l J
95-47-6 o-Xylene 0.41 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 104%70-130%
615-59-8 2,5-Dibromotoluene 99%70-130%
98 of 101
FC339899.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:ALSE SGS Orlando, FL
Project:BBGFLT: 4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLC3518-BS1 LC856635.D 1 03/21/23 JB n/a n/a GLC3518
GLC3518-BSD1 LC856636.D 1 03/21/23 JB n/a n/a GLC3518
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC3398-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 40 39.4 99 40.3 101 2 70-130/25
100-41-4 Ethylbenzene 40 39.7 99 40.5 101 2 70-130/25
1634-04-4 Methyl Tert Butyl Ether 40 37.3 93 37.2 93 0 70-130/25
91-20-3 Naphthalene 40 53.9 135* a 47.8 120 12 70-130/25
108-88-3 Toluene 40 39.6 99 40.3 101 2 70-130/25
m,p-Xylene 80 78.9 99 79.9 100 1 70-130/25
95-47-6 o-Xylene 40 40.8 102 41.0 103 0 70-130/25
C5- C8 Aliphatics (Unadj.)120 128 106 128 107 0 70-130/25
C9- C12 Aliphatics (Unadj.)120 121 100 114 95 5 70-130/25
C9- C10 Aromatics (Unadj.)40 39.0 98 39.2 98 1 70-130/25
C5- C8 Aliphatics 177 177 0 70-130/25
C9- C12 Aliphatics 161 160 1 70-130/25
C9- C10 Aromatics 40 39.0 98 39.2 98 1 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 89%92%70-130%
615-59-8 2,5-Dibromotoluene 93%97%70-130%
(a) Outside control limits biased high.
* = Outside of Control Limits.
99 of 101
FC339899.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:ALSE SGS Orlando, FL
Project:BBGFLT: 4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2401-BS1 LE040990.D 1 03/23/23 JB n/a n/a GLE2401
GLE2401-BSD1 a LE040991.D 1 03/23/23 JB n/a n/a GLE2401
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC3398-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 40 38.2 96 39.1 98 2 70-130/25
100-41-4 Ethylbenzene 40 37.8 95 38.7 97 2 70-130/25
1634-04-4 Methyl Tert Butyl Ether 40 40.5 101 40.1 100 1 70-130/25
91-20-3 Naphthalene 40 42.4 106 42.0 105 1 70-130/25
108-88-3 Toluene 40 37.3 93 38.4 96 3 70-130/25
m,p-Xylene 80 73.7 92 75.4 94 2 70-130/25
95-47-6 o-Xylene 40 37.0 93 37.9 95 2 70-130/25
C5- C8 Aliphatics (Unadj.)120 131 109 133 111 2 70-130/25
C9- C12 Aliphatics (Unadj.)120 115 95 115 96 0 70-130/25
C9- C10 Aromatics (Unadj.)40 38.4 96 39.5 99 3 70-130/25
C5- C8 Aliphatics 240 244 2 70-130/25
C9- C12 Aliphatics 191 195 2 70-130/25
C9- C10 Aromatics 40 38.4 96 39.5 99 3 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 104%101%70-130%
615-59-8 2,5-Dibromotoluene 101%98%70-130%
(a) Insufficient sample available for MS/MSD.
* = Outside of Control Limits.
100 of 101
FC339899.2.2
Duplicate Summary Page 1 of 1
Job Number:FC3398
Account:ALSE SGS Orlando, FL
Project:BBGFLT: 4357 Raleigh St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3332-9DUP LC856642.D 5 03/21/23 JB n/a n/a GLC3518
FC3332-9 LC856641.D 5 03/21/23 JB n/a n/a GLC3518
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC3398-10
FC3332-9 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene 1.9 J 2.0 J 5 50
100-41-4 Ethylbenzene 2.6 J 2.8 J 7 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene 484 509 5 50
108-88-3 Toluene 1.6 J 1.9 J 17 50
m,p-Xylene 3.3 J 3.4 J 3 50
95-47-6 o-Xylene 2.5 J 3.0 J 18 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FC3332-9 Limits
615-59-8 2,5-Dibromotoluene 101%99%70-130%
615-59-8 2,5-Dibromotoluene 91%89%70-130%
* = Outside of Control Limits.
101 of 101
FC339899.3.1
Personnel Qualifications
Appendix 6
4357 Raleigh Street
BBG Project: 0523100027 20
Copyright © 2023 BBG, Inc. All rights reserved.
Paul Stellato
Senior Managing Director
Work: 914.218.1542
[e-mail]
March 2022
Education and Technical Training
B.A. Environmental Science, State University of New York at Plattsburgh
Experience
Mr. Paul Stellato brings more than 17 years of experience in the environmental and due diligence consulting industry.
He has conducted Environmental Site Assessments (ESAs) for a wide range of local and national clients, including
banks, agency lenders, investment banks, life companies, law firms, and property owners. The properties he has
evaluated have included multifamily residential, retail, office, industrial and hospitality facilities.
Mr. Stellato has conducted or reviewed hundreds of ESAs in accordance with ASTM E1527, the USEPA All Appropriate
Inquiry rules, and other client specific scopes of work. Based on his experience and education, he meets the
definition of an Environmental Professional as defined in §312.10 of 40 CFR 312. His environmental background
includes a detailed understanding of the risks associated with hazardous and regulated materials storage, use
generation and disposal, and above ground and underground storage tanks (USTs).
Mr. Stellato has also managed and provided technical support on a variety of environmental projects to ensure
regulatory compliance, and bring projects to completion, including UST removals, soil and groundwater remediation,
vapor intrusion mitigation, geophysical investigations, and third-party oversight and review, at sites across the
county with the government and private sectors.
Christopher Stang, PG
Senior Managing Director
Work: 843.478.8236
[e-mail]
January 2022
Education and Technical Training
B.S. Geology, College of Charleston
Licenses and Certifications
Professional Geologist, South Carolina
Experience
Mr. Christopher Stang brings more than 18 years of experience in the environmental and due diligence consulting
industry. He has conducted Environmental Site Assessments (ESAs) for a wide range of local and national clients,
including banks, agency lenders, investment banks, life companies, law firms and property owners. The properties
he has evaluated have included multifamily residential, retail, office, industrial and hospitality facilities.
Mr. Stang has conducted or reviewed hundreds of ESAs in accordance with ASTM E1527, the USEPA All Appropriate
Inquiry rules, Fannie Mae Delegated Underwriting Standards, Freddie Mac guidelines and other client specific scopes
of work. Based on his experience and education, he meets the definition of an Environmental Professional as defined
in §312.10 of 40 CFR 312. His environmental background includes a detailed understanding of the risks associated
with hazardous and regulated materials storage, use generation and disposal, above ground and underground
storage tanks and polychlorinated biphenyls (PCBs), as well as the ASTM non-scope considerations of asbestos, lead-
based paint, radon and microbial growth.
Mr. Stang has also managed and performed many remedial invitation (RI) site assessments at sites across the county
and has also conducted site remediation activities including implementing free product removal, groundwater pump
and treat, soil venting, bio-sparging technologies, in situ chemical oxidation (ISCO) via sub-surface injection or soil
blending, and air-sparge/soil vapor extraction.
Mr. Stang’s technical experience includes geologic and hydrogeologic aspects of subsurface investigations associated
with contaminant migration at petrochemical, chlorinated solvent and hazardous waste sites. He has performed
multiple vapor intrusion assessments and his experience also includes recovery and monitor well installation; aquifer
testing, including slug tests and pump tests, groundwater remediation and design; vapor, soil, water, industrial waste
stream sampling and geophysical surveys with the government and private sectors.