MO-88920_97031_CA_O_20230509_20230509_SSR

2701 Westport Road
Charlotte, NC 28208
P [phone]
F [phone]
Terracon.com
Facilities | Environmental | Geotechnical | Materials I
May 1, 2023
Arris NODA, LLC
2700 Apple Valley Road
Suite 50
Brookhaven, Georgia 20219
Attn: Mr. Marshall Musser
E-mail: [e-mail]
RE: Limited Soil Sampling Report
Arris NODA
4357 Raleigh Street
Charlotte, Mecklenburg County, North Carolina 28213
Terracon Project No. 71237184
Dear Mr. Musser:
Terracon Consultants, Inc. (Terracon) is pleased to submit this Limited Soil Sampling Report for the above-referenced property. The report presents data from recent soil sampling activities conducted on April 13, 2023. Terracon conducted the sampling activities in general accordance with Terracon
Proposal No. P71237184, dated April 10, 2023.
Terracon appreciates this opportunity to provide environmental consulting services to Arris
NODA, LLC. If you have any questions or require additional information, please do not hesitate
to contact our office at [phone].
Sincerely,
Terracon Consultants, Inc.
Ayla Homer, P.G. (NC) M. Neal McElveen, PE
Project Geologist Principal
Facilities | Environmental | Geotechnical | Materials I
haw
Limited Soil
Sampling Report
Arris NODA, LLC
4357 Raleigh Street
Charlotte, Mecklenburg County, North Carolina
May 1, 2023 | Project Number: 71237184
Facilities | Environmental | Geotechnical | Materials I
Limited Soil Sampling
Report
Arris NODA, LLC
4357 Raleigh Street
Charlotte, Mecklenburg County, North Carolina
May 1, 2023 | Project No: 71237184
Prepared for:
Arris NODA, LLC
2700 Apple Valley Road Suite 50
Brookhaven Georgia 20219
Prepared By:
Ayla Homer, P.G. (NC) M. Neal McElveen, PE
Project Geologist Principal
Terracon Consultants, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-367 and F-0869, respectively.

Facilities | Environmental | Geotechnical | Materials i
Table of Contents
1.0 Introduction ............................................................................... 1
1.1 Standard of Care ................................................................................................ 2
1.2 Additional Scope Limitations ................................................................................ 2
1.3 Reliance ............................................................................................................ 2
2.0 Field Investigation Methods .......................................................... 2
2.1 Soil Investigation ............................................................................................... 3
3.0 Field Investigation Results ............................................................ 3
3.1 Soil Analytical Results ......................................................................................... 3
4.0 Conclusions ................................................................................ 4
5.0 Recommendations ....................................................................... 4
List of Tables
Table 1 – Summary of Soil Analytical Results
List of Exhibits
Exhibit 1 – Topographic Vicinity Map
Exhibit 2 – Site Diagram
Exhibit 3 – Sample Location Map
List of Appendices
Appendix A – Site Photographs
Appendix B – Soil Disposal Manifests
Appendix C – Laboratory Analytical Report and Chain of Custody
Facilities | Environmental | Geotechnical | Materials 1
LIMITED SOIL SAMPLING REPORT
ARRIS NODA
4357 RALEIGH STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
TERRACON PROJECT NO. 71237184
May 1, 2023
1.0 Introduction
Terracon Consultants, Inc. (Terracon) completed limited soil sampling activities for Arris NODA, LLC.
The site is located at 4357 Raleigh Street in Charlotte, Mecklenburg County, North Carolina (site). The
site consists of an approximately 10-acre parcel and is identified on the Mecklenburg County
Geographic Information System (GIS) website as Parcel Number 091-051-12. The site location is
depicted on the Topographic Vicinity Map, included as Exhibit 1.
The site is comprised of concrete paved areas and vegetated areas surrounded by chain-link fencing. A
site map is included as Exhibit 2.
Engineering Consulting Services Southeast, LLP (ECS) completed a Phase I Environmental Site
Assessment (ESA), dated February 2023. The Phase I ESA identified the following recognized
environmental conditions (RECs):
Staining attributed to discarded motors in an approximately 15 square foot (ft2 ) area on the
central-southern portion of the site.
Staining attributed to previously parked tractor trailers in an approximately 75 ft2 area on the
eastern portion of the site.
Based on ECS’s recommendations in the Phase I ESA, BBG Consulting, Inc. (BBG) collected four soil
samples from four soil borings (B-1 through B-4), installed two temporary monitoring wells in B-1 and
B-4, collected two groundwater samples (B-1 GW and B-4 GW), and provided sampling activities and
analytical results in a Phase II Limited ESA: Soil and Groundwater Sampling Report dated March 2023.
According to BBG’s report, laboratory analytical results indicated Total Petroleum Hydrocarbon (TPH)-
Gasoline Range Organics (GRO) and TPH-Diesel Range Organics (DRO) were detected in the soil sample
B-1 at 4 feet below ground surface (ft-bgs) at concentrations of 57.4 milligram/kilogram (mg/kg) and
2,380 mg/kg, respectively, exceeding North Carolina Department of Environmental Quality (NCDEQ)
Action Levels of 50 mg/kg for TPH-GRO and 100 mg/kg for TPH-DRO. Analysis of Volatile Organic
Compounds (VOCs) was also requested, and VOC concentrations were detected above laboratory
detection limits, but below NCDEQ Residential-Health Based Preliminary Soil Remediation Goals
(PSRGs). Naphthalene was detected in the groundwater sample S-1 GW at 11.5 microgram/Liter (µg/L),
above the NCDEQ NCAC 2L Groundwater Standard (2L Standard) of 6.0 µg/L. In addition, petroleum
hydrocarbons in the C9-C18 Aliphatic range were detected in B-1 GW at 399 µg/L, below the 2L Standard
of 700 µg/L, but above the NCAC Surface Water Standards (2B Standard) of 180 µg/L. Petroleum
hydrocarbons in the C9-C32 aromatic range were detected in B-1 GW at 664 µg/L and B-4 GW at 267
µg/L, above the 2L Standard of 200 µg/L, but below the 2B Standard (830 µg/L).
Facilities | Environmental | Geotechnical | Materials 2
The purpose of Terracon’s investigation was to evaluate subsurface conditions in the area of boring B-
1, excavate petroleum impacted soils, and confirm the presumed source area (i.e., stained soil and
contamination) was adequately removed following excavation activities.
1.1 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of the
profession undertaken in similar studies in the same geographical area during the same time. Terracon
makes no warranties, expressed or implied, regarding the findings, conclusions, or recommendations.
Please note that Terracon does not warrant the work of laboratories, regulatory agencies, or other third
parties supplying information to prepare the report. The services were performed in accordance with
the scope of work authorized by our client, as reflected in our proposal and were not conducted in
accordance with ASTM E1903-19.
1.2 Additional Scope Limitations
Findings, conclusions, and recommendations resulting from these services are based upon information
derived from the on-site activities and other services performed under this scope of work; such
information is subject to change over time. Certain indicators of the presence of hazardous substances,
petroleum products, or other constituents may have been latent, inaccessible, unobservable, non-
detectable, or not present during these services. We cannot represent that the site is free of hazardous
substances, toxic materials, petroleum products, or other latent conditions beyond those identified
during this investigation. Subsurface conditions may vary from those encountered at specific borings or
wells or during other surveys, tests, assessments, investigations, or exploratory services. The data,
interpretations, findings, and recommendations are based solely upon data obtained at the time and
within the scope of these services.
1.3 Reliance
This report is for the exclusive use of Arris NODA, LLC, and any lenders who finance the acquisition,
development, and operation of the site. Any authorization for use or reliance by another party
(except a governmental entity having jurisdiction over the site) is prohibited without the expressed
written authorization of Arris NODA, LLC, and Terracon. Any unauthorized distribution or reuse is
at the sole risk of Arris NODA, LLC. Reliance by authorized parties will be subject to the terms,
conditions, and limitations stated in our proposal.
2.0 Field Investigation Methods
On April 13, 2023, Terracon mobilized to the site to identify the previously reported impacted area,
supervise the excavation activities, and collect post excavation confirmation soil samples. A Site Diagram
depicting location of the excavation, extent of the excavation, and sample locations are provided as
Exhibit 3.
Terracon conducted the fieldwork under the direction of a site-specific health and safety plan developed
for this project and scope of work. Work was performed using Occupational Safety and Health
Facilities | Environmental | Geotechnical | Materials 3
Administration Level D personal protective equipment (PPE), consisting of a hard hat, safety glasses,
safety vest, protective gloves, and protective boots.
2.1 Soil Investigation
Arris NODA, LLC, contracted with Dig Earthworks, LLC, to excavate stained soils in the vicinity of soil
boring B-1. During excavation activities, Terracon observed the excavated soils for evidence of
petroleum odors and visible staining, and field screened the soils for volatiles using a calibrated
photoionization detector (PID). A composite sample of stained soil was collected and screened with the
PID to establish initial soil conditions. The PID screening indicated an elevated reading of 403 parts per
million (ppm) from the composite soil sample. The contractor excavated an approximately 9-foot by 9-
foot area, to an approximate depth of 7 ft-bgs.
Following excavation activities, Terracon field screened soil samples from the sidewalls and bottom of
the excavation. PID readings indicated volatiles ranged from 0.8 to 2.6 ppm. Based on the reduced PID
screening results, and the absence of observed odor and soil staining in the excavation, Terracon
collected soil samples from each of the four sidewalls and the bottom of the excavation. The soil samples
were submitted for laboratory analysis of VOCs by Environmental Protection Agency (EPA) Method 8260,
semi-volatile organic compounds (SVOCs) by EPA Method 8270, volatile petroleum hydrocarbon (VPH)
by Massachusetts Department of Environmental Protection (MADEP) and extractable petroleum
hydrocarbon (EPH) by MADEP.
The soil sample locations are depicted in Exhibit 3 and photographs taken during the excavation
activities are included in Appendix A.
Three loads of soil were removed from the site associated with the excavation activities, resulting in the
excavation of approximately 28.22 tons of petroleum-impacted soils. Impacted soils were transported
to Zero Waste Recycling in Charlotte, North Carolina. Soil disposal manifests provided by Dig
Earthworks, are included in Appendix B. Following site activities, the excavation was backfilled using
stockpiled soil from the site.
3.0 Field Investigation Results
Soils encountered at the site during the investigation generally consisted of gray, tan, and reddish-
brown silts with varying amounts of clay and sand. Groundwater was not encountered during the
subsurface investigation.
3.1 Soil Analytical Results
Laboratory analytical results for the soil samples collected in April 2023 were compared to the NCDEQ
Health-Based PSRGs for the Protection of Groundwater, Residential, and Industrial/Commercial
standards, dated January 2023. The results of the laboratory report indicated the following:
VOCs and SVOCs
According to the laboratory analytical report, methylene chloride was detected in soil samples SS-1 at
0.44 mg/kg, SS-3 at 0.569 mg/kg, SS-4 at 0.265 mg/kg, and SS-5 at 0.227 mg/kg, above the Protection
of Groundwater PSRG of 0.025 mg/kg. Methylene chloride is noted in the laboratory report as a common
Facilities | Environmental | Geotechnical | Materials 4
laboratory contaminant, the detection of which is often biased high. The remaining VOCs detected above
laboratory detection limits (acetone, chloromethane, ethylbenzene, methylene chloride, naphthalene,
and p-isopropyltoluene) were not detected above PSRGs. SVOCs were not detected above laboratory
detection limits.
EPH and VPH
According to the laboratory report, soil sample SS-2 contained detectible concentrations of EPH
constituents including aliphatic C9-C18 (medium range) at 17 mg/kg, aliphatic C19-C36 (high range) at
22.1 mg/kg, and aromatic C11-C22 (medium range) at 19.9 mg/kg. None of the detected EPH
constituents exceeded Residential PSRGs, and VPH constituents were not detected above laboratory
detection limits.
The soil analytical results are summarized in Table 1. The laboratory analytical report is provided in
Appendix C.
4.0 Conclusions
On April 13, 2023, Terracon mobilized to the site to identify the stained soil and oversee soil excavation
activities in the general vicinity of B-1. The horizontal extents of the soil excavation were approximately
nine feet in each direction, and extended to a depth of approximately seven feet. Approximately 28.22
tons of impacted soil was removed from the site, and transported to Zero Waste Recycling in Charlotte,
North Carolina. Following excavation activities, four sidewall samples and one basin sample were
collected and analyzed for VOCs by EPA Method 8260, SVOCs by EPA Method 8270, VPH by MADEP, and
EPH by MADEP.
According to the laboratory analytical report, methylene chloride was detected in soil samples SS-1
(0.440 mg/kg), SS-3 (0.569 mg/kg), SS-4 (0.265 mg/kg), and SS-5 (0.227 mg/kg), above the
Protection of Groundwater PSRG of 0.025 mg/kg. Methylene chloride was identified by the laboratory
as a laboratory contaminant and is not considered to be indicative of on-site contamination. Additionally,
methylene chloride was not detected in the soil samples collected by BBG in March 2023, further
supporting the conclusion that the detection of methylene chloride in the soil samples collected in April
2023 is not indicative of on-site contamination. The detection of VPH constituents in sample SS-2 were
below residential PSRGs.
Based on field observations during the soil excavation, and the laboratory analytical results, the stained
soils associated with the source area of B-1 appear to have been adequately removed.
5.0 Recommendations
Additional assessment or excavation activities associated with the previously identified stained soils is
not warranted at this time.
Tables
Table 1Summary of Soil Analytical ResultsArris NODA4357 Raleigh StreetCharlotte, Mecklenburg County, North CarolinaTerracon Project: 71237184Sample IDSS-1 SS-2 SS-3 SS-4 SS-5Date Collected4/13/2023 4/13/2023 4/13/2023 4/13/2023 4/13/2023Sample Interval (ft bgs)6-73-53-53-53-5Acetone<0.0452<0.03670.0732 J<0.0393<0.04262514,000210,000Chloromethane<0.00590.0053 J<0.0064 <0.0051 <0.00560.0152399Ethylbenzene<0.0033<0.0027<0.0036<0.00290.005 J136.127Methylene Chloride0.440<0.01560.269 0.256 0.2270.02558650Naphthalene<0.0037<0.00300.0089<0.0032<0.00350.392.18.8p-Isopropyltoluene<0.0035<0.00280.0043 J<0.00300.0431NENENESVOCs (8270)BRLBRLBRLBRLBRL------Aliphatic C05-C08<14.0<12.0<13.0<14.0<16.08.644310Aliphatic C09-C12 (VPH)<14.0<12.0<13.0<14.0<16.0Aliphatic C09-C18 (EPH)<12.017.0<12.2 <12.5 <11.8Aliphatic C19-C36<12.022.1<12.2 <12.5 <11.8NE47,000700,000Aromatic C09-C10<14.0<12.0<13.0<14.0<16.0Aromatic C11-C22<12.019.9<12.2 <12.5 <11.8Notes:Units are presented in milligram/kilogram (mg/kg)Method number follows parameter in parenthesisConcentrations detected in at least one sample are presented in the table, refer to the laboratory report.1) North Carolina Department of Environmental Quality (NCDEQ) Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs) dated January 20232) NCDEQ Residential Health Based PSRGs dated January 20233) NCDEQ Industrial/Commercial Health Based PSRGs dated January 2023ft bgs = feet below ground surface< = below laboratory method detection limitBRL = Below Reporting LimitJ = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. NE = Not Established-- = Not ApplicableConcentrations in bold exceed Protection of Groundwater PSRGsConcentrations underlined exceed Residential PSRGs190 20 93NE 62 370Protection of Groundwater PSRGs (1)Residential PSRGs (2)Industrial/Commercial PSRGs (3)VPH/EPH (MADEP)VOCs (8260)N:\Projects\2023\71237184\Working Files\Tables\Soil Table4/28/2023Page 1 of 1

Exhibits

TOPOGRAPHIC MAP
Arris NODA Soil Sampling
4357 Raleigh Street Charlotte, NC
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY QUADRANGLES INCLUDE: DERITA, NC (1/1/1993) and CHARLOTTE EAST, NC (1/1/1988).
2701 Westport Rd
Charlotte, NC 28208-3608
71237184
Project Manager:
Drawn by:
Checked by:
Approved by:
CPM
AGH
MNM
1”=2,000’
Arris
April 2023
Project No.
Scale:
File Name:
Date: 1
Exhibit AGH
APPROXIMATE
SITE BOUNDARY

Appendix A
Site Photographs
Photograph 2: View of the excavation activities.
Photograph 1: View of the stained soil and previously reported subsurface contamination.
Arris NODA 4357 Raleigh Street Charlotte, North Carolina
Project No. 71237184 Photos taken: April 13, 2023
Photograph 2: View of the excavated soil.
Photograph 3: View of the soil samples prior to field screening.
Arris NODA 4357 Raleigh Street Charlotte, North Carolina
Project No. 71237184 Photos taken: April 13, 2023

Appendix B
Soil Disposal Manifests

Appendix C
Laboratory Analytical Report and Chain of Custody

#=CL#
April 20, 2023
LIMS USE: FR - ERIN GREENE
LIMS OBJECT ID: 92662174
92662174
Project:
Pace Project No.:
RE:
Erin Greene
Terracon
2701 Westport Road
Charlotte, NC 28208
ARRIS NODA 71237184
Dear Erin Greene:
Enclosed are the analytical results for sample(s) received by the laboratory on April 13, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 75
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 75
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Lab ID Sample ID Matrix Date Collected Date Received
92662174001 SS-1 Solid 04/13/23 12:10 04/13/23 15:15
92662174002 SS-2 Solid 04/13/23 12:25 04/13/23 15:15
92662174003 SS-3 Solid 04/13/23 12:35 04/13/23 15:15
92662174004 SS-4 Solid 04/13/23 12:40 04/13/23 15:15
92662174005 SS-5 Solid 04/13/23 12:50 04/13/23 15:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 75
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92662174001 SS-1 MADEP EPH 7 PASI-CBAJ, NND
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92662174002 SS-2 MADEP EPH 7 PASI-CBAJ, NND
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92662174003 SS-3 MADEP EPH 7 PASI-CBAJ, NND
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92662174004 SS-4 MADEP EPH 7 PASI-CBAJ, NND
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92662174005 SS-5 MADEP EPH 7 PASI-CBAJ, NND
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 75
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92662174001 SS-1
Methylene Chloride 440 ug/kg 04/13/23 22:15 C9,IK28.2EPA 8260D
Percent Moisture 16.8 %04/13/23 23:58 N20.10SW-846
92662174002 SS-2
Aliphatic (C09-C18)17.0 mg/kg 04/19/23 10:37 N211.5MADEP EPH
Aliphatic (C19-C36)22.1 mg/kg 04/19/23 10:37 N211.5MADEP EPH
Aromatic (C11-C22)19.9 mg/kg 04/19/23 10:37 N211.5MADEP EPH
Chloromethane 5.3J ug/kg 04/13/23 22:3311.4EPA 8260D
Percent Moisture 14.6 %04/13/23 23:58 N20.10SW-846
92662174003 SS-3
Acetone 73.2J ug/kg 04/13/23 23:08152EPA 8260D
p-Isopropyltoluene 4.3J ug/kg 04/13/23 23:087.6EPA 8260D
Methylene Chloride 269 ug/kg 04/13/23 23:08 C9,IK30.5EPA 8260D
Naphthalene 8.9 ug/kg 04/13/23 23:087.6EPA 8260D
Percent Moisture 16.9 %04/13/23 23:58 N20.10SW-846
92662174004 SS-4
Methylene Chloride 256 ug/kg 04/13/23 23:26 C9,IK24.5EPA 8260D
Percent Moisture 19.1 %04/13/23 23:58 N20.10SW-846
92662174005 SS-5
Ethylbenzene 5.0J ug/kg 04/13/23 23:446.6EPA 8260D
p-Isopropyltoluene 43.1 ug/kg 04/13/23 23:446.6EPA 8260D
Methylene Chloride 227 ug/kg 04/13/23 23:44 C9,IK26.5EPA 8260D
Percent Moisture 16.6 %04/13/23 23:58 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
MADEP EPH
Date:April 20, 2023
Description:MADEP EPH NC Soil
General Information:
5 samples were analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
EPA 8270E
Date:April 20, 2023
Description:8270E MSSV Microwave
General Information:
5 samples were analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 768315
L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samplesmay be biased low.
• LCS (Lab ID: 3989137)
• Benzoic Acid
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
EPA 8270E
Date:April 20, 2023
Description:8270E MSSV Microwave
Analyte Comments:
QC Batch: 768315
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• DUP (Lab ID: 3989140)
• Nitrobenzene-d5 (S)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
EPA 8260D
Date:April 20, 2023
Description:8260D/5035A/5030B Volatiles
General Information:
5 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
QC Batch: 767997
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should beconsidered an estimated value.
• BLANK (Lab ID: 3987668)
• Bromoform
• Methylene Chloride
• DUP (Lab ID: 3987671)
• Bromoform
• Methylene Chloride
• LCS (Lab ID: 3987669)
• Bromoform
• Methylene Chloride
• MS (Lab ID: 3987670)
• Bromoform
• Methylene Chloride
• SS-1 (Lab ID: 92662174001)
• Bromoform
• Methylene Chloride
• SS-2 (Lab ID: 92662174002)
• Bromoform
• Methylene Chloride
• SS-3 (Lab ID: 92662174003)
• Bromoform
• Methylene Chloride
• SS-4 (Lab ID: 92662174004)
• Bromoform
• Methylene Chloride
• SS-5 (Lab ID: 92662174005)
• Bromoform
• Methylene Chloride
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
EPA 8260D
Date:April 20, 2023
Description:8260D/5035A/5030B Volatiles
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 767997
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associatedsamples may have a high bias.
• BLANK (Lab ID: 3987668)
• Dichlorodifluoromethane
• DUP (Lab ID: 3987671)
• Dichlorodifluoromethane
• LCS (Lab ID: 3987669)
• Dichlorodifluoromethane
• MS (Lab ID: 3987670)
• Dichlorodifluoromethane
• SS-1 (Lab ID: 92662174001)
• Dichlorodifluoromethane
• SS-2 (Lab ID: 92662174002)
• Dichlorodifluoromethane
• SS-3 (Lab ID: 92662174003)
• Dichlorodifluoromethane
• SS-4 (Lab ID: 92662174004)
• Dichlorodifluoromethane
• SS-5 (Lab ID: 92662174005)
• Dichlorodifluoromethane
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• BLANK (Lab ID: 3987668)
• Bromomethane
• Vinyl chloride
• DUP (Lab ID: 3987671)
• Bromomethane
• Vinyl chloride
• SS-1 (Lab ID: 92662174001)
• Bromomethane
• Vinyl chloride
• SS-2 (Lab ID: 92662174002)
• Bromomethane
• Vinyl chloride
• SS-3 (Lab ID: 92662174003)
• Bromomethane
• Vinyl chloride
• SS-4 (Lab ID: 92662174004)
• Bromomethane
• Vinyl chloride
• SS-5 (Lab ID: 92662174005)
• Bromomethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
EPA 8260D
Date:April 20, 2023
Description:8260D/5035A/5030B Volatiles
QC Batch: 767997
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• Vinyl chloride
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• LCS (Lab ID: 3987669)
• Bromomethane
• Vinyl chloride
• MS (Lab ID: 3987670)
• Bromomethane
• Vinyl chloride
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 767997
C9: Common Laboratory Contaminant.
• SS-1 (Lab ID: 92662174001)
• Methylene Chloride
• SS-3 (Lab ID: 92662174003)
• Methylene Chloride
• SS-4 (Lab ID: 92662174004)
• Methylene Chloride
• SS-5 (Lab ID: 92662174005)
• Methylene Chloride
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 75
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Method:
Client:Terracon - Charlotte, NC
EPA 8260D
Date:April 20, 2023
Description:8260D/5035A/5030B Volatiles
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-1 Lab ID: 92662174001 Collected: 04/13/23 12:10 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 10:12 N204/18/23 08:2812.0 12.0 1
Aliphatic (C19-C36)ND mg/kg 04/19/23 10:12 N204/18/23 08:2812.0 12.0 1
Aromatic (C11-C22)ND mg/kg 04/19/23 10:12 N204/18/23 08:2812.0 12.0 1
Surrogates
1-Chlorooctadecane (S)68 %04/19/23 10:12 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)50 %04/19/23 10:12 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)83 %04/19/23 10:12 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)88 %04/19/23 10:12 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/16/23 11:59 83-32-904/15/23 15:46395 139 1
Acenaphthylene ND ug/kg 04/16/23 11:59 208-96-804/15/23 15:46395 139 1
Aniline ND ug/kg 04/16/23 11:59 62-53-304/15/23 15:46395 155 1
Anthracene ND ug/kg 04/16/23 11:59 120-12-704/15/23 15:46395 129 1
Benzo(a)anthracene ND ug/kg 04/16/23 11:59 56-55-304/15/23 15:46395 132 1
Benzo(a)pyrene ND ug/kg 04/16/23 11:59 50-32-804/15/23 15:46395 137 1
Benzo(b)fluoranthene ND ug/kg 04/16/23 11:59 205-99-204/15/23 15:46395 132 1
Benzo(g,h,i)perylene ND ug/kg 04/16/23 11:59 191-24-204/15/23 15:46395 153 1
Benzo(k)fluoranthene ND ug/kg 04/16/23 11:59 207-08-904/15/23 15:46395 139 1
Benzoic Acid ND ug/kg 04/16/23 11:59 65-85-0 L204/15/23 15:461980 850 1
Benzyl alcohol ND ug/kg 04/16/23 11:59 100-51-604/15/23 15:46791 300 1
4-Bromophenylphenyl ether ND ug/kg 04/16/23 11:59 101-55-304/15/23 15:46395 152 1
Butylbenzylphthalate ND ug/kg 04/16/23 11:59 85-68-704/15/23 15:46395 167 1
4-Chloro-3-methylphenol ND ug/kg 04/16/23 11:59 59-50-704/15/23 15:46791 278 1
4-Chloroaniline ND ug/kg 04/16/23 11:59 106-47-804/15/23 15:46791 310 1
bis(2-Chloroethoxy)methane ND ug/kg 04/16/23 11:59 111-91-104/15/23 15:46395 164 1
bis(2-Chloroethyl) ether ND ug/kg 04/16/23 11:59 111-44-404/15/23 15:46395 149 1
2-Chloronaphthalene ND ug/kg 04/16/23 11:59 91-58-704/15/23 15:46395 157 1
2-Chlorophenol ND ug/kg 04/16/23 11:59 95-57-804/15/23 15:46395 149 1
4-Chlorophenylphenyl ether ND ug/kg 04/16/23 11:59 7005-72-304/15/23 15:46395 147 1
Chrysene ND ug/kg 04/16/23 11:59 218-01-904/15/23 15:46395 144 1
Dibenz(a,h)anthracene ND ug/kg 04/16/23 11:59 53-70-304/15/23 15:46395 152 1
Dibenzofuran ND ug/kg 04/16/23 11:59 132-64-904/15/23 15:46395 143 1
1,2-Dichlorobenzene ND ug/kg 04/16/23 11:59 95-50-104/15/23 15:46395 143 1
1,3-Dichlorobenzene ND ug/kg 04/16/23 11:59 541-73-104/15/23 15:46395 140 1
1,4-Dichlorobenzene ND ug/kg 04/16/23 11:59 106-46-704/15/23 15:46395 151 1
3,3'-Dichlorobenzidine ND ug/kg 04/16/23 11:59 91-94-104/15/23 15:46791 267 1
2,4-Dichlorophenol ND ug/kg 04/16/23 11:59 120-83-204/15/23 15:46395 155 1
Diethylphthalate ND ug/kg 04/16/23 11:59 84-66-204/15/23 15:46395 145 1
2,4-Dimethylphenol ND ug/kg 04/16/23 11:59 105-67-904/15/23 15:46395 164 1
Dimethylphthalate ND ug/kg 04/16/23 11:59 131-11-304/15/23 15:46395 144 1
Di-n-butylphthalate ND ug/kg 04/16/23 11:59 84-74-204/15/23 15:46395 133 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/16/23 11:59 534-52-104/15/23 15:46791 369 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-1 Lab ID: 92662174001 Collected: 04/13/23 12:10 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 04/16/23 11:59 51-28-504/15/23 15:461980 1220 1
2,4-Dinitrotoluene ND ug/kg 04/16/23 11:59 121-14-204/15/23 15:46395 152 1
2,6-Dinitrotoluene ND ug/kg 04/16/23 11:59 606-20-204/15/23 15:46395 145 1
Di-n-octylphthalate ND ug/kg 04/16/23 11:59 117-84-004/15/23 15:46395 156 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/16/23 11:59 117-81-704/15/23 15:46395 153 1
Fluoranthene ND ug/kg 04/16/23 11:59 206-44-004/15/23 15:46395 135 1
Fluorene ND ug/kg 04/16/23 11:59 86-73-704/15/23 15:46395 139 1
Hexachloro-1,3-butadiene ND ug/kg 04/16/23 11:59 87-68-304/15/23 15:46395 171 1
Hexachlorobenzene ND ug/kg 04/16/23 11:59 118-74-104/15/23 15:46395 155 1
Hexachlorocyclopentadiene ND ug/kg 04/16/23 11:59 77-47-404/15/23 15:46395 226 1
Hexachloroethane ND ug/kg 04/16/23 11:59 67-72-104/15/23 15:46395 151 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/16/23 11:59 193-39-504/15/23 15:46395 156 1
Isophorone ND ug/kg 04/16/23 11:59 78-59-104/15/23 15:46395 176 1
1-Methylnaphthalene ND ug/kg 04/16/23 11:59 90-12-004/15/23 15:46395 139 1
2-Methylnaphthalene ND ug/kg 04/16/23 11:59 91-57-604/15/23 15:46395 158 1
2-Methylphenol(o-Cresol)ND ug/kg 04/16/23 11:59 95-48-704/15/23 15:46395 162 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/16/23 11:59 15831-10-404/15/23 15:46395 159 1
Naphthalene ND ug/kg 04/16/23 11:59 91-20-304/15/23 15:46395 134 1
2-Nitroaniline ND ug/kg 04/16/23 11:59 88-74-404/15/23 15:461980 324 1
3-Nitroaniline ND ug/kg 04/16/23 11:59 99-09-204/15/23 15:461980 310 1
4-Nitroaniline ND ug/kg 04/16/23 11:59 100-01-604/15/23 15:46791 301 1
Nitrobenzene ND ug/kg 04/16/23 11:59 98-95-304/15/23 15:46395 183 1
2-Nitrophenol ND ug/kg 04/16/23 11:59 88-75-504/15/23 15:46395 171 1
4-Nitrophenol ND ug/kg 04/16/23 11:59 100-02-704/15/23 15:461980 764 1
N-Nitrosodimethylamine ND ug/kg 04/16/23 11:59 62-75-904/15/23 15:46395 133 1
N-Nitroso-di-n-propylamine ND ug/kg 04/16/23 11:59 621-64-704/15/23 15:46395 149 1
N-Nitrosodiphenylamine ND ug/kg 04/16/23 11:59 86-30-604/15/23 15:46395 140 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/16/23 11:59 108-60-104/15/23 15:46395 188 1
Pentachlorophenol ND ug/kg 04/16/23 11:59 87-86-504/15/23 15:46791 387 1
Phenanthrene ND ug/kg 04/16/23 11:59 85-01-804/15/23 15:46395 129 1
Phenol ND ug/kg 04/16/23 11:59 108-95-204/15/23 15:46395 176 1
Pyrene ND ug/kg 04/16/23 11:59 129-00-004/15/23 15:46395 161 1
Pyridine ND ug/kg 04/16/23 11:59 110-86-104/15/23 15:46395 125 1
1,2,4-Trichlorobenzene ND ug/kg 04/16/23 11:59 120-82-104/15/23 15:46395 156 1
2,4,5-Trichlorophenol ND ug/kg 04/16/23 11:59 95-95-404/15/23 15:46395 181 1
2,4,6-Trichlorophenol ND ug/kg 04/16/23 11:59 88-06-204/15/23 15:46395 163 1
Surrogates
Nitrobenzene-d5 (S)11 %04/16/23 11:59 4165-60-004/15/23 15:4610-130 1
2-Fluorobiphenyl (S)21 %04/16/23 11:59 321-60-804/15/23 15:4610-130 1
Terphenyl-d14 (S)58 %04/16/23 11:59 1718-51-004/15/23 15:4610-130 1
Phenol-d6 (S)42 %04/16/23 11:59 13127-88-304/15/23 15:4610-130 1
2-Fluorophenol (S)40 %04/16/23 11:59 367-12-404/15/23 15:4610-130 1
2,4,6-Tribromophenol (S)37 %04/16/23 11:59 118-79-604/15/23 15:4610-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-1 Lab ID: 92662174001 Collected: 04/13/23 12:10 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/13/23 22:15 67-64-104/13/23 18:43141 45.2 1
Benzene ND ug/kg 04/13/23 22:15 71-43-204/13/23 18:437.0 2.8 1
Bromobenzene ND ug/kg 04/13/23 22:15 108-86-104/13/23 18:437.0 2.3 1
Bromochloromethane ND ug/kg 04/13/23 22:15 74-97-504/13/23 18:437.0 2.1 1
Bromodichloromethane ND ug/kg 04/13/23 22:15 75-27-404/13/23 18:437.0 2.7 1
Bromoform ND ug/kg 04/13/23 22:15 75-25-2 IK04/13/23 18:437.0 2.5 1
Bromomethane ND ug/kg 04/13/23 22:15 74-83-9 v204/13/23 18:4328.2 21.8 1
2-Butanone (MEK)ND ug/kg 04/13/23 22:15 78-93-304/13/23 18:43141 33.8 1
n-Butylbenzene ND ug/kg 04/13/23 22:15 104-51-804/13/23 18:437.0 4.4 1
sec-Butylbenzene ND ug/kg 04/13/23 22:15 135-98-804/13/23 18:437.0 3.1 1
tert-Butylbenzene ND ug/kg 04/13/23 22:15 98-06-604/13/23 18:437.0 2.5 1
Carbon tetrachloride ND ug/kg 04/13/23 22:15 56-23-504/13/23 18:437.0 2.6 1
Chlorobenzene ND ug/kg 04/13/23 22:15 108-90-704/13/23 18:437.0 4.0 1
Chloroethane ND ug/kg 04/13/23 22:15 75-00-304/13/23 18:4314.1 5.4 1
Chloroform ND ug/kg 04/13/23 22:15 67-66-304/13/23 18:437.0 5.9 1
Chloromethane ND ug/kg 04/13/23 22:15 74-87-304/13/23 18:4314.1 5.9 1
2-Chlorotoluene ND ug/kg 04/13/23 22:15 95-49-804/13/23 18:437.0 2.5 1
4-Chlorotoluene ND ug/kg 04/13/23 22:15 106-43-404/13/23 18:437.0 3.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/13/23 22:15 96-12-804/13/23 18:437.0 2.7 1
Dibromochloromethane ND ug/kg 04/13/23 22:15 124-48-104/13/23 18:437.0 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 04/13/23 22:15 106-93-404/13/23 18:437.0 3.1 1
Dibromomethane ND ug/kg 04/13/23 22:15 74-95-304/13/23 18:437.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 04/13/23 22:15 95-50-104/13/23 18:437.0 2.5 1
1,3-Dichlorobenzene ND ug/kg 04/13/23 22:15 541-73-104/13/23 18:437.0 2.2 1
1,4-Dichlorobenzene ND ug/kg 04/13/23 22:15 106-46-704/13/23 18:437.0 1.8 1
Dichlorodifluoromethane ND ug/kg 04/13/23 22:15 75-71-8 v104/13/23 18:4314.1 7.2 1
1,1-Dichloroethane ND ug/kg 04/13/23 22:15 75-34-304/13/23 18:437.0 2.9 1
1,2-Dichloroethane ND ug/kg 04/13/23 22:15 107-06-204/13/23 18:437.0 4.7 1
1,1-Dichloroethene ND ug/kg 04/13/23 22:15 75-35-404/13/23 18:437.0 2.9 1
cis-1,2-Dichloroethene ND ug/kg 04/13/23 22:15 156-59-204/13/23 18:437.0 2.4 1
trans-1,2-Dichloroethene ND ug/kg 04/13/23 22:15 156-60-504/13/23 18:437.0 6.0 1
1,2-Dichloropropane ND ug/kg 04/13/23 22:15 78-87-504/13/23 18:437.0 2.1 1
1,3-Dichloropropane ND ug/kg 04/13/23 22:15 142-28-904/13/23 18:437.0 2.2 1
2,2-Dichloropropane ND ug/kg 04/13/23 22:15 594-20-704/13/23 18:437.0 5.3 1
1,1-Dichloropropene ND ug/kg 04/13/23 22:15 563-58-604/13/23 18:437.0 3.4 1
cis-1,3-Dichloropropene ND ug/kg 04/13/23 22:15 10061-01-504/13/23 18:437.0 1.9 1
trans-1,3-Dichloropropene ND ug/kg 04/13/23 22:15 10061-02-604/13/23 18:437.0 2.4 1
Diisopropyl ether ND ug/kg 04/13/23 22:15 108-20-304/13/23 18:437.0 1.9 1
Ethylbenzene ND ug/kg 04/13/23 22:15 100-41-404/13/23 18:437.0 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/13/23 22:15 87-68-304/13/23 18:4314.1 11.5 1
2-Hexanone ND ug/kg 04/13/23 22:15 591-78-604/13/23 18:4370.5 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 04/13/23 22:15 98-82-804/13/23 18:437.0 2.4 1
p-Isopropyltoluene ND ug/kg 04/13/23 22:15 99-87-604/13/23 18:437.0 3.5 1
Methylene Chloride 440 ug/kg 04/13/23 22:15 75-09-2 C9,IK04/13/23 18:4328.2 19.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-1 Lab ID: 92662174001 Collected: 04/13/23 12:10 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/13/23 22:15 108-10-104/13/23 18:4370.5 6.8 1
Methyl-tert-butyl ether ND ug/kg 04/13/23 22:15 1634-04-404/13/23 18:437.0 2.6 1
Naphthalene ND ug/kg 04/13/23 22:15 91-20-304/13/23 18:437.0 3.7 1
n-Propylbenzene ND ug/kg 04/13/23 22:15 103-65-104/13/23 18:437.0 2.5 1
Styrene ND ug/kg 04/13/23 22:15 100-42-504/13/23 18:437.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/13/23 22:15 630-20-604/13/23 18:437.0 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/13/23 22:15 79-34-504/13/23 18:437.0 1.9 1
Tetrachloroethene ND ug/kg 04/13/23 22:15 127-18-404/13/23 18:437.0 2.2 1
Toluene ND ug/kg 04/13/23 22:15 108-88-304/13/23 18:437.0 4.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/13/23 22:15 87-61-604/13/23 18:437.0 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/13/23 22:15 120-82-104/13/23 18:437.0 5.9 1
1,1,1-Trichloroethane ND ug/kg 04/13/23 22:15 71-55-604/13/23 18:437.0 3.7 1
1,1,2-Trichloroethane ND ug/kg 04/13/23 22:15 79-00-504/13/23 18:437.0 2.3 1
Trichloroethene ND ug/kg 04/13/23 22:15 79-01-604/13/23 18:437.0 5.7 1
Trichlorofluoromethane ND ug/kg 04/13/23 22:15 75-69-404/13/23 18:437.0 3.9 1
1,2,3-Trichloropropane ND ug/kg 04/13/23 22:15 96-18-404/13/23 18:437.0 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 04/13/23 22:15 95-63-604/13/23 18:437.0 4.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/13/23 22:15 108-67-804/13/23 18:437.0 2.4 1
Vinyl acetate ND ug/kg 04/13/23 22:15 108-05-404/13/23 18:4370.5 14.5 1
Vinyl chloride ND ug/kg 04/13/23 22:15 75-01-4 v204/13/23 18:4314.1 3.6 1
Xylene (Total)ND ug/kg 04/13/23 22:15 1330-20-704/13/23 18:4314.1 4.0 1
m&p-Xylene ND ug/kg 04/13/23 22:15 179601-23-104/13/23 18:4314.1 4.8 1
o-Xylene ND ug/kg 04/13/23 22:15 95-47-604/13/23 18:437.0 3.1 1
Surrogates
Toluene-d8 (S)101 %04/13/23 22:15 2037-26-504/13/23 18:4370-130 1
4-Bromofluorobenzene (S)106 %04/13/23 22:15 460-00-404/13/23 18:4370-130 1
1,2-Dichloroethane-d4 (S)117 %04/13/23 22:15 17060-07-004/13/23 18:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.8 %04/13/23 23:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-2 Lab ID: 92662174002 Collected: 04/13/23 12:25 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)17.0 mg/kg 04/19/23 10:37 N204/18/23 08:2811.5 11.5 1
Aliphatic (C19-C36)22.1 mg/kg 04/19/23 10:37 N204/18/23 08:2811.5 11.5 1
Aromatic (C11-C22)19.9 mg/kg 04/19/23 10:37 N204/18/23 08:2811.5 11.5 1
Surrogates
1-Chlorooctadecane (S)90 %04/19/23 10:37 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)79 %04/19/23 10:37 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)109 %04/19/23 10:37 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)121 %04/19/23 10:37 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/23 13:11 83-32-904/15/23 15:46390 137 1
Acenaphthylene ND ug/kg 04/17/23 13:11 208-96-804/15/23 15:46390 137 1
Aniline ND ug/kg 04/17/23 13:11 62-53-304/15/23 15:46390 153 1
Anthracene ND ug/kg 04/17/23 13:11 120-12-704/15/23 15:46390 128 1
Benzo(a)anthracene ND ug/kg 04/17/23 13:11 56-55-304/15/23 15:46390 130 1
Benzo(a)pyrene ND ug/kg 04/17/23 13:11 50-32-804/15/23 15:46390 135 1
Benzo(b)fluoranthene ND ug/kg 04/17/23 13:11 205-99-204/15/23 15:46390 130 1
Benzo(g,h,i)perylene ND ug/kg 04/17/23 13:11 191-24-204/15/23 15:46390 151 1
Benzo(k)fluoranthene ND ug/kg 04/17/23 13:11 207-08-904/15/23 15:46390 137 1
Benzoic Acid ND ug/kg 04/17/23 13:11 65-85-0 L204/15/23 15:461950 839 1
Benzyl alcohol ND ug/kg 04/17/23 13:11 100-51-604/15/23 15:46781 296 1
4-Bromophenylphenyl ether ND ug/kg 04/17/23 13:11 101-55-304/15/23 15:46390 150 1
Butylbenzylphthalate ND ug/kg 04/17/23 13:11 85-68-704/15/23 15:46390 164 1
4-Chloro-3-methylphenol ND ug/kg 04/17/23 13:11 59-50-704/15/23 15:46781 274 1
4-Chloroaniline ND ug/kg 04/17/23 13:11 106-47-804/15/23 15:46781 306 1
bis(2-Chloroethoxy)methane ND ug/kg 04/17/23 13:11 111-91-104/15/23 15:46390 162 1
bis(2-Chloroethyl) ether ND ug/kg 04/17/23 13:11 111-44-404/15/23 15:46390 147 1
2-Chloronaphthalene ND ug/kg 04/17/23 13:11 91-58-704/15/23 15:46390 155 1
2-Chlorophenol ND ug/kg 04/17/23 13:11 95-57-804/15/23 15:46390 147 1
4-Chlorophenylphenyl ether ND ug/kg 04/17/23 13:11 7005-72-304/15/23 15:46390 145 1
Chrysene ND ug/kg 04/17/23 13:11 218-01-904/15/23 15:46390 142 1
Dibenz(a,h)anthracene ND ug/kg 04/17/23 13:11 53-70-304/15/23 15:46390 150 1
Dibenzofuran ND ug/kg 04/17/23 13:11 132-64-904/15/23 15:46390 141 1
1,2-Dichlorobenzene ND ug/kg 04/17/23 13:11 95-50-104/15/23 15:46390 141 1
1,3-Dichlorobenzene ND ug/kg 04/17/23 13:11 541-73-104/15/23 15:46390 138 1
1,4-Dichlorobenzene ND ug/kg 04/17/23 13:11 106-46-704/15/23 15:46390 149 1
3,3'-Dichlorobenzidine ND ug/kg 04/17/23 13:11 91-94-104/15/23 15:46781 264 1
2,4-Dichlorophenol ND ug/kg 04/17/23 13:11 120-83-204/15/23 15:46390 153 1
Diethylphthalate ND ug/kg 04/17/23 13:11 84-66-204/15/23 15:46390 143 1
2,4-Dimethylphenol ND ug/kg 04/17/23 13:11 105-67-904/15/23 15:46390 162 1
Dimethylphthalate ND ug/kg 04/17/23 13:11 131-11-304/15/23 15:46390 142 1
Di-n-butylphthalate ND ug/kg 04/17/23 13:11 84-74-204/15/23 15:46390 131 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/23 13:11 534-52-104/15/23 15:46781 364 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-2 Lab ID: 92662174002 Collected: 04/13/23 12:25 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 04/17/23 13:11 51-28-504/15/23 15:461950 1210 1
2,4-Dinitrotoluene ND ug/kg 04/17/23 13:11 121-14-204/15/23 15:46390 150 1
2,6-Dinitrotoluene ND ug/kg 04/17/23 13:11 606-20-204/15/23 15:46390 143 1
Di-n-octylphthalate ND ug/kg 04/17/23 13:11 117-84-004/15/23 15:46390 154 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/23 13:11 117-81-704/15/23 15:46390 151 1
Fluoranthene ND ug/kg 04/17/23 13:11 206-44-004/15/23 15:46390 134 1
Fluorene ND ug/kg 04/17/23 13:11 86-73-704/15/23 15:46390 137 1
Hexachloro-1,3-butadiene ND ug/kg 04/17/23 13:11 87-68-304/15/23 15:46390 169 1
Hexachlorobenzene ND ug/kg 04/17/23 13:11 118-74-104/15/23 15:46390 153 1
Hexachlorocyclopentadiene ND ug/kg 04/17/23 13:11 77-47-404/15/23 15:46390 224 1
Hexachloroethane ND ug/kg 04/17/23 13:11 67-72-104/15/23 15:46390 149 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/23 13:11 193-39-504/15/23 15:46390 154 1
Isophorone ND ug/kg 04/17/23 13:11 78-59-104/15/23 15:46390 174 1
1-Methylnaphthalene ND ug/kg 04/17/23 13:11 90-12-004/15/23 15:46390 137 1
2-Methylnaphthalene ND ug/kg 04/17/23 13:11 91-57-604/15/23 15:46390 156 1
2-Methylphenol(o-Cresol)ND ug/kg 04/17/23 13:11 95-48-704/15/23 15:46390 160 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/23 13:11 15831-10-404/15/23 15:46390 157 1
Naphthalene ND ug/kg 04/17/23 13:11 91-20-304/15/23 15:46390 132 1
2-Nitroaniline ND ug/kg 04/17/23 13:11 88-74-404/15/23 15:461950 319 1
3-Nitroaniline ND ug/kg 04/17/23 13:11 99-09-204/15/23 15:461950 306 1
4-Nitroaniline ND ug/kg 04/17/23 13:11 100-01-604/15/23 15:46781 297 1
Nitrobenzene ND ug/kg 04/17/23 13:11 98-95-304/15/23 15:46390 181 1
2-Nitrophenol ND ug/kg 04/17/23 13:11 88-75-504/15/23 15:46390 169 1
4-Nitrophenol ND ug/kg 04/17/23 13:11 100-02-704/15/23 15:461950 755 1
N-Nitrosodimethylamine ND ug/kg 04/17/23 13:11 62-75-904/15/23 15:46390 131 1
N-Nitroso-di-n-propylamine ND ug/kg 04/17/23 13:11 621-64-704/15/23 15:46390 147 1
N-Nitrosodiphenylamine ND ug/kg 04/17/23 13:11 86-30-604/15/23 15:46390 138 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/23 13:11 108-60-104/15/23 15:46390 186 1
Pentachlorophenol ND ug/kg 04/17/23 13:11 87-86-504/15/23 15:46781 382 1
Phenanthrene ND ug/kg 04/17/23 13:11 85-01-804/15/23 15:46390 128 1
Phenol ND ug/kg 04/17/23 13:11 108-95-204/15/23 15:46390 174 1
Pyrene ND ug/kg 04/17/23 13:11 129-00-004/15/23 15:46390 159 1
Pyridine ND ug/kg 04/17/23 13:11 110-86-104/15/23 15:46390 123 1
1,2,4-Trichlorobenzene ND ug/kg 04/17/23 13:11 120-82-104/15/23 15:46390 154 1
2,4,5-Trichlorophenol ND ug/kg 04/17/23 13:11 95-95-404/15/23 15:46390 179 1
2,4,6-Trichlorophenol ND ug/kg 04/17/23 13:11 88-06-204/15/23 15:46390 161 1
Surrogates
Nitrobenzene-d5 (S)31 %04/17/23 13:11 4165-60-004/15/23 15:4610-130 1
2-Fluorobiphenyl (S)23 %04/17/23 13:11 321-60-804/15/23 15:4610-130 1
Terphenyl-d14 (S)55 %04/17/23 13:11 1718-51-004/15/23 15:4610-130 1
Phenol-d6 (S)39 %04/17/23 13:11 13127-88-304/15/23 15:4610-130 1
2-Fluorophenol (S)34 %04/17/23 13:11 367-12-404/15/23 15:4610-130 1
2,4,6-Tribromophenol (S)38 %04/17/23 13:11 118-79-604/15/23 15:4610-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-2 Lab ID: 92662174002 Collected: 04/13/23 12:25 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/13/23 22:33 67-64-104/13/23 18:43114 36.7 1
Benzene ND ug/kg 04/13/23 22:33 71-43-204/13/23 18:435.7 2.3 1
Bromobenzene ND ug/kg 04/13/23 22:33 108-86-104/13/23 18:435.7 1.9 1
Bromochloromethane ND ug/kg 04/13/23 22:33 74-97-504/13/23 18:435.7 1.7 1
Bromodichloromethane ND ug/kg 04/13/23 22:33 75-27-404/13/23 18:435.7 2.2 1
Bromoform ND ug/kg 04/13/23 22:33 75-25-2 IK04/13/23 18:435.7 2.0 1
Bromomethane ND ug/kg 04/13/23 22:33 74-83-9 v204/13/23 18:4322.8 17.7 1
2-Butanone (MEK)ND ug/kg 04/13/23 22:33 78-93-304/13/23 18:43114 27.4 1
n-Butylbenzene ND ug/kg 04/13/23 22:33 104-51-804/13/23 18:435.7 3.6 1
sec-Butylbenzene ND ug/kg 04/13/23 22:33 135-98-804/13/23 18:435.7 2.5 1
tert-Butylbenzene ND ug/kg 04/13/23 22:33 98-06-604/13/23 18:435.7 2.0 1
Carbon tetrachloride ND ug/kg 04/13/23 22:33 56-23-504/13/23 18:435.7 2.1 1
Chlorobenzene ND ug/kg 04/13/23 22:33 108-90-704/13/23 18:435.7 3.3 1
Chloroethane ND ug/kg 04/13/23 22:33 75-00-304/13/23 18:4311.4 4.4 1
Chloroform ND ug/kg 04/13/23 22:33 67-66-304/13/23 18:435.7 4.8 1
Chloromethane 5.3J ug/kg 04/13/23 22:33 74-87-304/13/23 18:4311.4 4.8 1
2-Chlorotoluene ND ug/kg 04/13/23 22:33 95-49-804/13/23 18:435.7 2.0 1
4-Chlorotoluene ND ug/kg 04/13/23 22:33 106-43-404/13/23 18:435.7 3.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/13/23 22:33 96-12-804/13/23 18:435.7 2.2 1
Dibromochloromethane ND ug/kg 04/13/23 22:33 124-48-104/13/23 18:435.7 3.2 1
1,2-Dibromoethane (EDB)ND ug/kg 04/13/23 22:33 106-93-404/13/23 18:435.7 2.5 1
Dibromomethane ND ug/kg 04/13/23 22:33 74-95-304/13/23 18:435.7 1.2 1
1,2-Dichlorobenzene ND ug/kg 04/13/23 22:33 95-50-104/13/23 18:435.7 2.1 1
1,3-Dichlorobenzene ND ug/kg 04/13/23 22:33 541-73-104/13/23 18:435.7 1.8 1
1,4-Dichlorobenzene ND ug/kg 04/13/23 22:33 106-46-704/13/23 18:435.7 1.5 1
Dichlorodifluoromethane ND ug/kg 04/13/23 22:33 75-71-8 v104/13/23 18:4311.4 5.8 1
1,1-Dichloroethane ND ug/kg 04/13/23 22:33 75-34-304/13/23 18:435.7 2.4 1
1,2-Dichloroethane ND ug/kg 04/13/23 22:33 107-06-204/13/23 18:435.7 3.8 1
1,1-Dichloroethene ND ug/kg 04/13/23 22:33 75-35-404/13/23 18:435.7 2.4 1
cis-1,2-Dichloroethene ND ug/kg 04/13/23 22:33 156-59-204/13/23 18:435.7 2.0 1
trans-1,2-Dichloroethene ND ug/kg 04/13/23 22:33 156-60-504/13/23 18:435.7 4.9 1
1,2-Dichloropropane ND ug/kg 04/13/23 22:33 78-87-504/13/23 18:435.7 1.7 1
1,3-Dichloropropane ND ug/kg 04/13/23 22:33 142-28-904/13/23 18:435.7 1.8 1
2,2-Dichloropropane ND ug/kg 04/13/23 22:33 594-20-704/13/23 18:435.7 4.3 1
1,1-Dichloropropene ND ug/kg 04/13/23 22:33 563-58-604/13/23 18:435.7 2.7 1
cis-1,3-Dichloropropene ND ug/kg 04/13/23 22:33 10061-01-504/13/23 18:435.7 1.6 1
trans-1,3-Dichloropropene ND ug/kg 04/13/23 22:33 10061-02-604/13/23 18:435.7 2.0 1
Diisopropyl ether ND ug/kg 04/13/23 22:33 108-20-304/13/23 18:435.7 1.5 1
Ethylbenzene ND ug/kg 04/13/23 22:33 100-41-404/13/23 18:435.7 2.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/13/23 22:33 87-68-304/13/23 18:4311.4 9.3 1
2-Hexanone ND ug/kg 04/13/23 22:33 591-78-604/13/23 18:4357.1 5.5 1
Isopropylbenzene (Cumene)ND ug/kg 04/13/23 22:33 98-82-804/13/23 18:435.7 1.9 1
p-Isopropyltoluene ND ug/kg 04/13/23 22:33 99-87-604/13/23 18:435.7 2.8 1
Methylene Chloride ND ug/kg 04/13/23 22:33 75-09-2 IK04/13/23 18:4322.8 15.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-2 Lab ID: 92662174002 Collected: 04/13/23 12:25 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/13/23 22:33 108-10-104/13/23 18:4357.1 5.5 1
Methyl-tert-butyl ether ND ug/kg 04/13/23 22:33 1634-04-404/13/23 18:435.7 2.1 1
Naphthalene ND ug/kg 04/13/23 22:33 91-20-304/13/23 18:435.7 3.0 1
n-Propylbenzene ND ug/kg 04/13/23 22:33 103-65-104/13/23 18:435.7 2.0 1
Styrene ND ug/kg 04/13/23 22:33 100-42-504/13/23 18:435.7 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/13/23 22:33 630-20-604/13/23 18:435.7 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/13/23 22:33 79-34-504/13/23 18:435.7 1.5 1
Tetrachloroethene ND ug/kg 04/13/23 22:33 127-18-404/13/23 18:435.7 1.8 1
Toluene ND ug/kg 04/13/23 22:33 108-88-304/13/23 18:435.7 3.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/13/23 22:33 87-61-604/13/23 18:435.7 4.6 1
1,2,4-Trichlorobenzene ND ug/kg 04/13/23 22:33 120-82-104/13/23 18:435.7 4.8 1
1,1,1-Trichloroethane ND ug/kg 04/13/23 22:33 71-55-604/13/23 18:435.7 3.0 1
1,1,2-Trichloroethane ND ug/kg 04/13/23 22:33 79-00-504/13/23 18:435.7 1.9 1
Trichloroethene ND ug/kg 04/13/23 22:33 79-01-604/13/23 18:435.7 4.6 1
Trichlorofluoromethane ND ug/kg 04/13/23 22:33 75-69-404/13/23 18:435.7 3.1 1
1,2,3-Trichloropropane ND ug/kg 04/13/23 22:33 96-18-404/13/23 18:435.7 2.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/13/23 22:33 95-63-604/13/23 18:435.7 3.4 1
1,3,5-Trimethylbenzene ND ug/kg 04/13/23 22:33 108-67-804/13/23 18:435.7 1.9 1
Vinyl acetate ND ug/kg 04/13/23 22:33 108-05-404/13/23 18:4357.1 11.8 1
Vinyl chloride ND ug/kg 04/13/23 22:33 75-01-4 v204/13/23 18:4311.4 2.9 1
Xylene (Total)ND ug/kg 04/13/23 22:33 1330-20-704/13/23 18:4311.4 3.3 1
m&p-Xylene ND ug/kg 04/13/23 22:33 179601-23-104/13/23 18:4311.4 3.9 1
o-Xylene ND ug/kg 04/13/23 22:33 95-47-604/13/23 18:435.7 2.5 1
Surrogates
Toluene-d8 (S)99 %04/13/23 22:33 2037-26-504/13/23 18:4370-130 1
4-Bromofluorobenzene (S)105 %04/13/23 22:33 460-00-404/13/23 18:4370-130 1
1,2-Dichloroethane-d4 (S)116 %04/13/23 22:33 17060-07-004/13/23 18:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.6 %04/13/23 23:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-3 Lab ID: 92662174003 Collected: 04/13/23 12:35 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 11:03 N204/18/23 08:2812.2 12.2 1
Aliphatic (C19-C36)ND mg/kg 04/19/23 11:03 N204/18/23 08:2812.2 12.2 1
Aromatic (C11-C22)ND mg/kg 04/19/23 11:03 N204/18/23 08:2812.2 12.2 1
Surrogates
1-Chlorooctadecane (S)74 %04/19/23 11:03 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)80 %04/19/23 11:03 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)106 %04/19/23 11:03 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)111 %04/19/23 11:03 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/16/23 12:27 83-32-904/15/23 15:46393 138 1
Acenaphthylene ND ug/kg 04/16/23 12:27 208-96-804/15/23 15:46393 138 1
Aniline ND ug/kg 04/16/23 12:27 62-53-304/15/23 15:46393 154 1
Anthracene ND ug/kg 04/16/23 12:27 120-12-704/15/23 15:46393 129 1
Benzo(a)anthracene ND ug/kg 04/16/23 12:27 56-55-304/15/23 15:46393 131 1
Benzo(a)pyrene ND ug/kg 04/16/23 12:27 50-32-804/15/23 15:46393 136 1
Benzo(b)fluoranthene ND ug/kg 04/16/23 12:27 205-99-204/15/23 15:46393 131 1
Benzo(g,h,i)perylene ND ug/kg 04/16/23 12:27 191-24-204/15/23 15:46393 153 1
Benzo(k)fluoranthene ND ug/kg 04/16/23 12:27 207-08-904/15/23 15:46393 138 1
Benzoic Acid ND ug/kg 04/16/23 12:27 65-85-0 L204/15/23 15:461970 845 1
Benzyl alcohol ND ug/kg 04/16/23 12:27 100-51-604/15/23 15:46786 298 1
4-Bromophenylphenyl ether ND ug/kg 04/16/23 12:27 101-55-304/15/23 15:46393 151 1
Butylbenzylphthalate ND ug/kg 04/16/23 12:27 85-68-704/15/23 15:46393 166 1
4-Chloro-3-methylphenol ND ug/kg 04/16/23 12:27 59-50-704/15/23 15:46786 276 1
4-Chloroaniline ND ug/kg 04/16/23 12:27 106-47-804/15/23 15:46786 309 1
bis(2-Chloroethoxy)methane ND ug/kg 04/16/23 12:27 111-91-104/15/23 15:46393 163 1
bis(2-Chloroethyl) ether ND ug/kg 04/16/23 12:27 111-44-404/15/23 15:46393 148 1
2-Chloronaphthalene ND ug/kg 04/16/23 12:27 91-58-704/15/23 15:46393 156 1
2-Chlorophenol ND ug/kg 04/16/23 12:27 95-57-804/15/23 15:46393 148 1
4-Chlorophenylphenyl ether ND ug/kg 04/16/23 12:27 7005-72-304/15/23 15:46393 147 1
Chrysene ND ug/kg 04/16/23 12:27 218-01-904/15/23 15:46393 143 1
Dibenz(a,h)anthracene ND ug/kg 04/16/23 12:27 53-70-304/15/23 15:46393 151 1
Dibenzofuran ND ug/kg 04/16/23 12:27 132-64-904/15/23 15:46393 142 1
1,2-Dichlorobenzene ND ug/kg 04/16/23 12:27 95-50-104/15/23 15:46393 142 1
1,3-Dichlorobenzene ND ug/kg 04/16/23 12:27 541-73-104/15/23 15:46393 139 1
1,4-Dichlorobenzene ND ug/kg 04/16/23 12:27 106-46-704/15/23 15:46393 150 1
3,3'-Dichlorobenzidine ND ug/kg 04/16/23 12:27 91-94-104/15/23 15:46786 266 1
2,4-Dichlorophenol ND ug/kg 04/16/23 12:27 120-83-204/15/23 15:46393 154 1
Diethylphthalate ND ug/kg 04/16/23 12:27 84-66-204/15/23 15:46393 144 1
2,4-Dimethylphenol ND ug/kg 04/16/23 12:27 105-67-904/15/23 15:46393 163 1
Dimethylphthalate ND ug/kg 04/16/23 12:27 131-11-304/15/23 15:46393 143 1
Di-n-butylphthalate ND ug/kg 04/16/23 12:27 84-74-204/15/23 15:46393 132 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/16/23 12:27 534-52-104/15/23 15:46786 367 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-3 Lab ID: 92662174003 Collected: 04/13/23 12:35 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 04/16/23 12:27 51-28-504/15/23 15:461970 1220 1
2,4-Dinitrotoluene ND ug/kg 04/16/23 12:27 121-14-204/15/23 15:46393 151 1
2,6-Dinitrotoluene ND ug/kg 04/16/23 12:27 606-20-204/15/23 15:46393 144 1
Di-n-octylphthalate ND ug/kg 04/16/23 12:27 117-84-004/15/23 15:46393 155 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/16/23 12:27 117-81-704/15/23 15:46393 153 1
Fluoranthene ND ug/kg 04/16/23 12:27 206-44-004/15/23 15:46393 135 1
Fluorene ND ug/kg 04/16/23 12:27 86-73-704/15/23 15:46393 138 1
Hexachloro-1,3-butadiene ND ug/kg 04/16/23 12:27 87-68-304/15/23 15:46393 170 1
Hexachlorobenzene ND ug/kg 04/16/23 12:27 118-74-104/15/23 15:46393 154 1
Hexachlorocyclopentadiene ND ug/kg 04/16/23 12:27 77-47-404/15/23 15:46393 225 1
Hexachloroethane ND ug/kg 04/16/23 12:27 67-72-104/15/23 15:46393 150 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/16/23 12:27 193-39-504/15/23 15:46393 155 1
Isophorone ND ug/kg 04/16/23 12:27 78-59-104/15/23 15:46393 175 1
1-Methylnaphthalene ND ug/kg 04/16/23 12:27 90-12-004/15/23 15:46393 138 1
2-Methylnaphthalene ND ug/kg 04/16/23 12:27 91-57-604/15/23 15:46393 157 1
2-Methylphenol(o-Cresol)ND ug/kg 04/16/23 12:27 95-48-704/15/23 15:46393 161 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/16/23 12:27 15831-10-404/15/23 15:46393 158 1
Naphthalene ND ug/kg 04/16/23 12:27 91-20-304/15/23 15:46393 133 1
2-Nitroaniline ND ug/kg 04/16/23 12:27 88-74-404/15/23 15:461970 322 1
3-Nitroaniline ND ug/kg 04/16/23 12:27 99-09-204/15/23 15:461970 309 1
4-Nitroaniline ND ug/kg 04/16/23 12:27 100-01-604/15/23 15:46786 299 1
Nitrobenzene ND ug/kg 04/16/23 12:27 98-95-304/15/23 15:46393 182 1
2-Nitrophenol ND ug/kg 04/16/23 12:27 88-75-504/15/23 15:46393 170 1
4-Nitrophenol ND ug/kg 04/16/23 12:27 100-02-704/15/23 15:461970 760 1
N-Nitrosodimethylamine ND ug/kg 04/16/23 12:27 62-75-904/15/23 15:46393 132 1
N-Nitroso-di-n-propylamine ND ug/kg 04/16/23 12:27 621-64-704/15/23 15:46393 148 1
N-Nitrosodiphenylamine ND ug/kg 04/16/23 12:27 86-30-604/15/23 15:46393 139 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/16/23 12:27 108-60-104/15/23 15:46393 187 1
Pentachlorophenol ND ug/kg 04/16/23 12:27 87-86-504/15/23 15:46786 385 1
Phenanthrene ND ug/kg 04/16/23 12:27 85-01-804/15/23 15:46393 129 1
Phenol ND ug/kg 04/16/23 12:27 108-95-204/15/23 15:46393 175 1
Pyrene ND ug/kg 04/16/23 12:27 129-00-004/15/23 15:46393 160 1
Pyridine ND ug/kg 04/16/23 12:27 110-86-104/15/23 15:46393 124 1
1,2,4-Trichlorobenzene ND ug/kg 04/16/23 12:27 120-82-104/15/23 15:46393 155 1
2,4,5-Trichlorophenol ND ug/kg 04/16/23 12:27 95-95-404/15/23 15:46393 180 1
2,4,6-Trichlorophenol ND ug/kg 04/16/23 12:27 88-06-204/15/23 15:46393 162 1
Surrogates
Nitrobenzene-d5 (S)18 %04/16/23 12:27 4165-60-004/15/23 15:4610-130 1
2-Fluorobiphenyl (S)13 %04/16/23 12:27 321-60-804/15/23 15:4610-130 1
Terphenyl-d14 (S)47 %04/16/23 12:27 1718-51-004/15/23 15:4610-130 1
Phenol-d6 (S)31 %04/16/23 12:27 13127-88-304/15/23 15:4610-130 1
2-Fluorophenol (S)26 %04/16/23 12:27 367-12-404/15/23 15:4610-130 1
2,4,6-Tribromophenol (S)29 %04/16/23 12:27 118-79-604/15/23 15:4610-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-3 Lab ID: 92662174003 Collected: 04/13/23 12:35 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 73.2J ug/kg 04/13/23 23:08 67-64-104/13/23 18:43152 48.9 1
Benzene ND ug/kg 04/13/23 23:08 71-43-204/13/23 18:437.6 3.0 1
Bromobenzene ND ug/kg 04/13/23 23:08 108-86-104/13/23 18:437.6 2.5 1
Bromochloromethane ND ug/kg 04/13/23 23:08 74-97-504/13/23 18:437.6 2.3 1
Bromodichloromethane ND ug/kg 04/13/23 23:08 75-27-404/13/23 18:437.6 2.9 1
Bromoform ND ug/kg 04/13/23 23:08 75-25-2 IK04/13/23 18:437.6 2.7 1
Bromomethane ND ug/kg 04/13/23 23:08 74-83-9 v204/13/23 18:4330.5 23.6 1
2-Butanone (MEK)ND ug/kg 04/13/23 23:08 78-93-304/13/23 18:43152 36.6 1
n-Butylbenzene ND ug/kg 04/13/23 23:08 104-51-804/13/23 18:437.6 4.8 1
sec-Butylbenzene ND ug/kg 04/13/23 23:08 135-98-804/13/23 18:437.6 3.4 1
tert-Butylbenzene ND ug/kg 04/13/23 23:08 98-06-604/13/23 18:437.6 2.7 1
Carbon tetrachloride ND ug/kg 04/13/23 23:08 56-23-504/13/23 18:437.6 2.9 1
Chlorobenzene ND ug/kg 04/13/23 23:08 108-90-704/13/23 18:437.6 4.4 1
Chloroethane ND ug/kg 04/13/23 23:08 75-00-304/13/23 18:4315.2 5.9 1
Chloroform ND ug/kg 04/13/23 23:08 67-66-304/13/23 18:437.6 6.4 1
Chloromethane ND ug/kg 04/13/23 23:08 74-87-304/13/23 18:4315.2 6.4 1
2-Chlorotoluene ND ug/kg 04/13/23 23:08 95-49-804/13/23 18:437.6 2.7 1
4-Chlorotoluene ND ug/kg 04/13/23 23:08 106-43-404/13/23 18:437.6 4.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/13/23 23:08 96-12-804/13/23 18:437.6 3.0 1
Dibromochloromethane ND ug/kg 04/13/23 23:08 124-48-104/13/23 18:437.6 4.3 1
1,2-Dibromoethane (EDB)ND ug/kg 04/13/23 23:08 106-93-404/13/23 18:437.6 3.4 1
Dibromomethane ND ug/kg 04/13/23 23:08 74-95-304/13/23 18:437.6 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/13/23 23:08 95-50-104/13/23 18:437.6 2.7 1
1,3-Dichlorobenzene ND ug/kg 04/13/23 23:08 541-73-104/13/23 18:437.6 2.4 1
1,4-Dichlorobenzene ND ug/kg 04/13/23 23:08 106-46-704/13/23 18:437.6 2.0 1
Dichlorodifluoromethane ND ug/kg 04/13/23 23:08 75-71-8 v104/13/23 18:4315.2 7.8 1
1,1-Dichloroethane ND ug/kg 04/13/23 23:08 75-34-304/13/23 18:437.6 3.1 1
1,2-Dichloroethane ND ug/kg 04/13/23 23:08 107-06-204/13/23 18:437.6 5.0 1
1,1-Dichloroethene ND ug/kg 04/13/23 23:08 75-35-404/13/23 18:437.6 3.1 1
cis-1,2-Dichloroethene ND ug/kg 04/13/23 23:08 156-59-204/13/23 18:437.6 2.6 1
trans-1,2-Dichloroethene ND ug/kg 04/13/23 23:08 156-60-504/13/23 18:437.6 6.5 1
1,2-Dichloropropane ND ug/kg 04/13/23 23:08 78-87-504/13/23 18:437.6 2.3 1
1,3-Dichloropropane ND ug/kg 04/13/23 23:08 142-28-904/13/23 18:437.6 2.4 1
2,2-Dichloropropane ND ug/kg 04/13/23 23:08 594-20-704/13/23 18:437.6 5.8 1
1,1-Dichloropropene ND ug/kg 04/13/23 23:08 563-58-604/13/23 18:437.6 3.7 1
cis-1,3-Dichloropropene ND ug/kg 04/13/23 23:08 10061-01-504/13/23 18:437.6 2.1 1
trans-1,3-Dichloropropene ND ug/kg 04/13/23 23:08 10061-02-604/13/23 18:437.6 2.6 1
Diisopropyl ether ND ug/kg 04/13/23 23:08 108-20-304/13/23 18:437.6 2.1 1
Ethylbenzene ND ug/kg 04/13/23 23:08 100-41-404/13/23 18:437.6 3.6 1
Hexachloro-1,3-butadiene ND ug/kg 04/13/23 23:08 87-68-304/13/23 18:4315.2 12.5 1
2-Hexanone ND ug/kg 04/13/23 23:08 591-78-604/13/23 18:4376.2 7.3 1
Isopropylbenzene (Cumene)ND ug/kg 04/13/23 23:08 98-82-804/13/23 18:437.6 2.6 1
p-Isopropyltoluene 4.3J ug/kg 04/13/23 23:08 99-87-604/13/23 18:437.6 3.8 1
Methylene Chloride 269 ug/kg 04/13/23 23:08 75-09-2 C9,IK04/13/23 18:4330.5 20.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-3 Lab ID: 92662174003 Collected: 04/13/23 12:35 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/13/23 23:08 108-10-104/13/23 18:4376.2 7.3 1
Methyl-tert-butyl ether ND ug/kg 04/13/23 23:08 1634-04-404/13/23 18:437.6 2.9 1
Naphthalene 8.9 ug/kg 04/13/23 23:08 91-20-304/13/23 18:437.6 4.0 1
n-Propylbenzene ND ug/kg 04/13/23 23:08 103-65-104/13/23 18:437.6 2.7 1
Styrene ND ug/kg 04/13/23 23:08 100-42-504/13/23 18:437.6 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/13/23 23:08 630-20-604/13/23 18:437.6 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/13/23 23:08 79-34-504/13/23 18:437.6 2.0 1
Tetrachloroethene ND ug/kg 04/13/23 23:08 127-18-404/13/23 18:437.6 2.4 1
Toluene ND ug/kg 04/13/23 23:08 108-88-304/13/23 18:437.6 5.3 1
1,2,3-Trichlorobenzene ND ug/kg 04/13/23 23:08 87-61-604/13/23 18:437.6 6.2 1
1,2,4-Trichlorobenzene ND ug/kg 04/13/23 23:08 120-82-104/13/23 18:437.6 6.4 1
1,1,1-Trichloroethane ND ug/kg 04/13/23 23:08 71-55-604/13/23 18:437.6 4.0 1
1,1,2-Trichloroethane ND ug/kg 04/13/23 23:08 79-00-504/13/23 18:437.6 2.5 1
Trichloroethene ND ug/kg 04/13/23 23:08 79-01-604/13/23 18:437.6 6.1 1
Trichlorofluoromethane ND ug/kg 04/13/23 23:08 75-69-404/13/23 18:437.6 4.2 1
1,2,3-Trichloropropane ND ug/kg 04/13/23 23:08 96-18-404/13/23 18:437.6 3.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/13/23 23:08 95-63-604/13/23 18:437.6 4.5 1
1,3,5-Trimethylbenzene ND ug/kg 04/13/23 23:08 108-67-804/13/23 18:437.6 2.6 1
Vinyl acetate ND ug/kg 04/13/23 23:08 108-05-404/13/23 18:4376.2 15.7 1
Vinyl chloride ND ug/kg 04/13/23 23:08 75-01-4 v204/13/23 18:4315.2 3.9 1
Xylene (Total)ND ug/kg 04/13/23 23:08 1330-20-704/13/23 18:4315.2 4.3 1
m&p-Xylene ND ug/kg 04/13/23 23:08 179601-23-104/13/23 18:4315.2 5.2 1
o-Xylene ND ug/kg 04/13/23 23:08 95-47-604/13/23 18:437.6 3.4 1
Surrogates
Toluene-d8 (S)97 %04/13/23 23:08 2037-26-504/13/23 18:4370-130 1
4-Bromofluorobenzene (S)105 %04/13/23 23:08 460-00-404/13/23 18:4370-130 1
1,2-Dichloroethane-d4 (S)115 %04/13/23 23:08 17060-07-004/13/23 18:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.9 %04/13/23 23:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-4 Lab ID: 92662174004 Collected: 04/13/23 12:40 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 11:28 N204/18/23 08:2812.5 12.5 1
Aliphatic (C19-C36)ND mg/kg 04/19/23 11:28 N204/18/23 08:2812.5 12.5 1
Aromatic (C11-C22)ND mg/kg 04/19/23 11:28 N204/18/23 08:2812.5 12.5 1
Surrogates
1-Chlorooctadecane (S)86 %04/19/23 11:28 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)52 %04/19/23 11:28 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)89 %04/19/23 11:28 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)95 %04/19/23 11:28 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/16/23 12:55 83-32-904/15/23 15:46415 146 1
Acenaphthylene ND ug/kg 04/16/23 12:55 208-96-804/15/23 15:46415 146 1
Aniline ND ug/kg 04/16/23 12:55 62-53-304/15/23 15:46415 162 1
Anthracene ND ug/kg 04/16/23 12:55 120-12-704/15/23 15:46415 136 1
Benzo(a)anthracene ND ug/kg 04/16/23 12:55 56-55-304/15/23 15:46415 138 1
Benzo(a)pyrene ND ug/kg 04/16/23 12:55 50-32-804/15/23 15:46415 143 1
Benzo(b)fluoranthene ND ug/kg 04/16/23 12:55 205-99-204/15/23 15:46415 138 1
Benzo(g,h,i)perylene ND ug/kg 04/16/23 12:55 191-24-204/15/23 15:46415 161 1
Benzo(k)fluoranthene ND ug/kg 04/16/23 12:55 207-08-904/15/23 15:46415 146 1
Benzoic Acid ND ug/kg 04/16/23 12:55 65-85-0 L204/15/23 15:462070 891 1
Benzyl alcohol ND ug/kg 04/16/23 12:55 100-51-604/15/23 15:46829 314 1
4-Bromophenylphenyl ether ND ug/kg 04/16/23 12:55 101-55-304/15/23 15:46415 160 1
Butylbenzylphthalate ND ug/kg 04/16/23 12:55 85-68-704/15/23 15:46415 175 1
4-Chloro-3-methylphenol ND ug/kg 04/16/23 12:55 59-50-704/15/23 15:46829 292 1
4-Chloroaniline ND ug/kg 04/16/23 12:55 106-47-804/15/23 15:46829 325 1
bis(2-Chloroethoxy)methane ND ug/kg 04/16/23 12:55 111-91-104/15/23 15:46415 172 1
bis(2-Chloroethyl) ether ND ug/kg 04/16/23 12:55 111-44-404/15/23 15:46415 156 1
2-Chloronaphthalene ND ug/kg 04/16/23 12:55 91-58-704/15/23 15:46415 165 1
2-Chlorophenol ND ug/kg 04/16/23 12:55 95-57-804/15/23 15:46415 156 1
4-Chlorophenylphenyl ether ND ug/kg 04/16/23 12:55 7005-72-304/15/23 15:46415 155 1
Chrysene ND ug/kg 04/16/23 12:55 218-01-904/15/23 15:46415 151 1
Dibenz(a,h)anthracene ND ug/kg 04/16/23 12:55 53-70-304/15/23 15:46415 160 1
Dibenzofuran ND ug/kg 04/16/23 12:55 132-64-904/15/23 15:46415 150 1
1,2-Dichlorobenzene ND ug/kg 04/16/23 12:55 95-50-104/15/23 15:46415 150 1
1,3-Dichlorobenzene ND ug/kg 04/16/23 12:55 541-73-104/15/23 15:46415 147 1
1,4-Dichlorobenzene ND ug/kg 04/16/23 12:55 106-46-704/15/23 15:46415 158 1
3,3'-Dichlorobenzidine ND ug/kg 04/16/23 12:55 91-94-104/15/23 15:46829 280 1
2,4-Dichlorophenol ND ug/kg 04/16/23 12:55 120-83-204/15/23 15:46415 162 1
Diethylphthalate ND ug/kg 04/16/23 12:55 84-66-204/15/23 15:46415 152 1
2,4-Dimethylphenol ND ug/kg 04/16/23 12:55 105-67-904/15/23 15:46415 172 1
Dimethylphthalate ND ug/kg 04/16/23 12:55 131-11-304/15/23 15:46415 151 1
Di-n-butylphthalate ND ug/kg 04/16/23 12:55 84-74-204/15/23 15:46415 139 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/16/23 12:55 534-52-104/15/23 15:46829 387 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-4 Lab ID: 92662174004 Collected: 04/13/23 12:40 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 04/16/23 12:55 51-28-504/15/23 15:462070 1280 1
2,4-Dinitrotoluene ND ug/kg 04/16/23 12:55 121-14-204/15/23 15:46415 160 1
2,6-Dinitrotoluene ND ug/kg 04/16/23 12:55 606-20-204/15/23 15:46415 152 1
Di-n-octylphthalate ND ug/kg 04/16/23 12:55 117-84-004/15/23 15:46415 163 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/16/23 12:55 117-81-704/15/23 15:46415 161 1
Fluoranthene ND ug/kg 04/16/23 12:55 206-44-004/15/23 15:46415 142 1
Fluorene ND ug/kg 04/16/23 12:55 86-73-704/15/23 15:46415 146 1
Hexachloro-1,3-butadiene ND ug/kg 04/16/23 12:55 87-68-304/15/23 15:46415 180 1
Hexachlorobenzene ND ug/kg 04/16/23 12:55 118-74-104/15/23 15:46415 162 1
Hexachlorocyclopentadiene ND ug/kg 04/16/23 12:55 77-47-404/15/23 15:46415 237 1
Hexachloroethane ND ug/kg 04/16/23 12:55 67-72-104/15/23 15:46415 158 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/16/23 12:55 193-39-504/15/23 15:46415 163 1
Isophorone ND ug/kg 04/16/23 12:55 78-59-104/15/23 15:46415 185 1
1-Methylnaphthalene ND ug/kg 04/16/23 12:55 90-12-004/15/23 15:46415 146 1
2-Methylnaphthalene ND ug/kg 04/16/23 12:55 91-57-604/15/23 15:46415 166 1
2-Methylphenol(o-Cresol)ND ug/kg 04/16/23 12:55 95-48-704/15/23 15:46415 170 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/16/23 12:55 15831-10-404/15/23 15:46415 167 1
Naphthalene ND ug/kg 04/16/23 12:55 91-20-304/15/23 15:46415 141 1
2-Nitroaniline ND ug/kg 04/16/23 12:55 88-74-404/15/23 15:462070 339 1
3-Nitroaniline ND ug/kg 04/16/23 12:55 99-09-204/15/23 15:462070 325 1
4-Nitroaniline ND ug/kg 04/16/23 12:55 100-01-604/15/23 15:46829 315 1
Nitrobenzene ND ug/kg 04/16/23 12:55 98-95-304/15/23 15:46415 192 1
2-Nitrophenol ND ug/kg 04/16/23 12:55 88-75-504/15/23 15:46415 180 1
4-Nitrophenol ND ug/kg 04/16/23 12:55 100-02-704/15/23 15:462070 802 1
N-Nitrosodimethylamine ND ug/kg 04/16/23 12:55 62-75-904/15/23 15:46415 139 1
N-Nitroso-di-n-propylamine ND ug/kg 04/16/23 12:55 621-64-704/15/23 15:46415 156 1
N-Nitrosodiphenylamine ND ug/kg 04/16/23 12:55 86-30-604/15/23 15:46415 147 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/16/23 12:55 108-60-104/15/23 15:46415 197 1
Pentachlorophenol ND ug/kg 04/16/23 12:55 87-86-504/15/23 15:46829 406 1
Phenanthrene ND ug/kg 04/16/23 12:55 85-01-804/15/23 15:46415 136 1
Phenol ND ug/kg 04/16/23 12:55 108-95-204/15/23 15:46415 185 1
Pyrene ND ug/kg 04/16/23 12:55 129-00-004/15/23 15:46415 168 1
Pyridine ND ug/kg 04/16/23 12:55 110-86-104/15/23 15:46415 131 1
1,2,4-Trichlorobenzene ND ug/kg 04/16/23 12:55 120-82-104/15/23 15:46415 163 1
2,4,5-Trichlorophenol ND ug/kg 04/16/23 12:55 95-95-404/15/23 15:46415 190 1
2,4,6-Trichlorophenol ND ug/kg 04/16/23 12:55 88-06-204/15/23 15:46415 171 1
Surrogates
Nitrobenzene-d5 (S)20 %04/16/23 12:55 4165-60-004/15/23 15:4610-130 1
2-Fluorobiphenyl (S)17 %04/16/23 12:55 321-60-804/15/23 15:4610-130 1
Terphenyl-d14 (S)57 %04/16/23 12:55 1718-51-004/15/23 15:4610-130 1
Phenol-d6 (S)34 %04/16/23 12:55 13127-88-304/15/23 15:4610-130 1
2-Fluorophenol (S)32 %04/16/23 12:55 367-12-404/15/23 15:4610-130 1
2,4,6-Tribromophenol (S)30 %04/16/23 12:55 118-79-604/15/23 15:4610-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-4 Lab ID: 92662174004 Collected: 04/13/23 12:40 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/13/23 23:26 67-64-104/13/23 18:43123 39.3 1
Benzene ND ug/kg 04/13/23 23:26 71-43-204/13/23 18:436.1 2.4 1
Bromobenzene ND ug/kg 04/13/23 23:26 108-86-104/13/23 18:436.1 2.0 1
Bromochloromethane ND ug/kg 04/13/23 23:26 74-97-504/13/23 18:436.1 1.8 1
Bromodichloromethane ND ug/kg 04/13/23 23:26 75-27-404/13/23 18:436.1 2.4 1
Bromoform ND ug/kg 04/13/23 23:26 75-25-2 IK04/13/23 18:436.1 2.2 1
Bromomethane ND ug/kg 04/13/23 23:26 74-83-9 v204/13/23 18:4324.5 19.0 1
2-Butanone (MEK)ND ug/kg 04/13/23 23:26 78-93-304/13/23 18:43123 29.4 1
n-Butylbenzene ND ug/kg 04/13/23 23:26 104-51-804/13/23 18:436.1 3.9 1
sec-Butylbenzene ND ug/kg 04/13/23 23:26 135-98-804/13/23 18:436.1 2.7 1
tert-Butylbenzene ND ug/kg 04/13/23 23:26 98-06-604/13/23 18:436.1 2.2 1
Carbon tetrachloride ND ug/kg 04/13/23 23:26 56-23-504/13/23 18:436.1 2.3 1
Chlorobenzene ND ug/kg 04/13/23 23:26 108-90-704/13/23 18:436.1 3.5 1
Chloroethane ND ug/kg 04/13/23 23:26 75-00-304/13/23 18:4312.3 4.7 1
Chloroform ND ug/kg 04/13/23 23:26 67-66-304/13/23 18:436.1 5.1 1
Chloromethane ND ug/kg 04/13/23 23:26 74-87-304/13/23 18:4312.3 5.1 1
2-Chlorotoluene ND ug/kg 04/13/23 23:26 95-49-804/13/23 18:436.1 2.2 1
4-Chlorotoluene ND ug/kg 04/13/23 23:26 106-43-404/13/23 18:436.1 3.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/13/23 23:26 96-12-804/13/23 18:436.1 2.4 1
Dibromochloromethane ND ug/kg 04/13/23 23:26 124-48-104/13/23 18:436.1 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/13/23 23:26 106-93-404/13/23 18:436.1 2.7 1
Dibromomethane ND ug/kg 04/13/23 23:26 74-95-304/13/23 18:436.1 1.3 1
1,2-Dichlorobenzene ND ug/kg 04/13/23 23:26 95-50-104/13/23 18:436.1 2.2 1
1,3-Dichlorobenzene ND ug/kg 04/13/23 23:26 541-73-104/13/23 18:436.1 1.9 1
1,4-Dichlorobenzene ND ug/kg 04/13/23 23:26 106-46-704/13/23 18:436.1 1.6 1
Dichlorodifluoromethane ND ug/kg 04/13/23 23:26 75-71-8 v104/13/23 18:4312.3 6.2 1
1,1-Dichloroethane ND ug/kg 04/13/23 23:26 75-34-304/13/23 18:436.1 2.5 1
1,2-Dichloroethane ND ug/kg 04/13/23 23:26 107-06-204/13/23 18:436.1 4.1 1
1,1-Dichloroethene ND ug/kg 04/13/23 23:26 75-35-404/13/23 18:436.1 2.5 1
cis-1,2-Dichloroethene ND ug/kg 04/13/23 23:26 156-59-204/13/23 18:436.1 2.1 1
trans-1,2-Dichloroethene ND ug/kg 04/13/23 23:26 156-60-504/13/23 18:436.1 5.2 1
1,2-Dichloropropane ND ug/kg 04/13/23 23:26 78-87-504/13/23 18:436.1 1.8 1
1,3-Dichloropropane ND ug/kg 04/13/23 23:26 142-28-904/13/23 18:436.1 1.9 1
2,2-Dichloropropane ND ug/kg 04/13/23 23:26 594-20-704/13/23 18:436.1 4.6 1
1,1-Dichloropropene ND ug/kg 04/13/23 23:26 563-58-604/13/23 18:436.1 2.9 1
cis-1,3-Dichloropropene ND ug/kg 04/13/23 23:26 10061-01-504/13/23 18:436.1 1.7 1
trans-1,3-Dichloropropene ND ug/kg 04/13/23 23:26 10061-02-604/13/23 18:436.1 2.1 1
Diisopropyl ether ND ug/kg 04/13/23 23:26 108-20-304/13/23 18:436.1 1.7 1
Ethylbenzene ND ug/kg 04/13/23 23:26 100-41-404/13/23 18:436.1 2.9 1
Hexachloro-1,3-butadiene ND ug/kg 04/13/23 23:26 87-68-304/13/23 18:4312.3 10.0 1
2-Hexanone ND ug/kg 04/13/23 23:26 591-78-604/13/23 18:4361.3 5.9 1
Isopropylbenzene (Cumene)ND ug/kg 04/13/23 23:26 98-82-804/13/23 18:436.1 2.1 1
p-Isopropyltoluene ND ug/kg 04/13/23 23:26 99-87-604/13/23 18:436.1 3.0 1
Methylene Chloride 256 ug/kg 04/13/23 23:26 75-09-2 C9,IK04/13/23 18:4324.5 16.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-4 Lab ID: 92662174004 Collected: 04/13/23 12:40 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/13/23 23:26 108-10-104/13/23 18:4361.3 5.9 1
Methyl-tert-butyl ether ND ug/kg 04/13/23 23:26 1634-04-404/13/23 18:436.1 2.3 1
Naphthalene ND ug/kg 04/13/23 23:26 91-20-304/13/23 18:436.1 3.2 1
n-Propylbenzene ND ug/kg 04/13/23 23:26 103-65-104/13/23 18:436.1 2.2 1
Styrene ND ug/kg 04/13/23 23:26 100-42-504/13/23 18:436.1 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/13/23 23:26 630-20-604/13/23 18:436.1 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/13/23 23:26 79-34-504/13/23 18:436.1 1.6 1
Tetrachloroethene ND ug/kg 04/13/23 23:26 127-18-404/13/23 18:436.1 1.9 1
Toluene ND ug/kg 04/13/23 23:26 108-88-304/13/23 18:436.1 4.2 1
1,2,3-Trichlorobenzene ND ug/kg 04/13/23 23:26 87-61-604/13/23 18:436.1 5.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/13/23 23:26 120-82-104/13/23 18:436.1 5.1 1
1,1,1-Trichloroethane ND ug/kg 04/13/23 23:26 71-55-604/13/23 18:436.1 3.2 1
1,1,2-Trichloroethane ND ug/kg 04/13/23 23:26 79-00-504/13/23 18:436.1 2.0 1
Trichloroethene ND ug/kg 04/13/23 23:26 79-01-604/13/23 18:436.1 4.9 1
Trichlorofluoromethane ND ug/kg 04/13/23 23:26 75-69-404/13/23 18:436.1 3.4 1
1,2,3-Trichloropropane ND ug/kg 04/13/23 23:26 96-18-404/13/23 18:436.1 3.1 1
1,2,4-Trimethylbenzene ND ug/kg 04/13/23 23:26 95-63-604/13/23 18:436.1 3.6 1
1,3,5-Trimethylbenzene ND ug/kg 04/13/23 23:26 108-67-804/13/23 18:436.1 2.1 1
Vinyl acetate ND ug/kg 04/13/23 23:26 108-05-404/13/23 18:4361.3 12.6 1
Vinyl chloride ND ug/kg 04/13/23 23:26 75-01-4 v204/13/23 18:4312.3 3.1 1
Xylene (Total)ND ug/kg 04/13/23 23:26 1330-20-704/13/23 18:4312.3 3.5 1
m&p-Xylene ND ug/kg 04/13/23 23:26 179601-23-104/13/23 18:4312.3 4.2 1
o-Xylene ND ug/kg 04/13/23 23:26 95-47-604/13/23 18:436.1 2.7 1
Surrogates
Toluene-d8 (S)98 %04/13/23 23:26 2037-26-504/13/23 18:4370-130 1
4-Bromofluorobenzene (S)103 %04/13/23 23:26 460-00-404/13/23 18:4370-130 1
1,2-Dichloroethane-d4 (S)114 %04/13/23 23:26 17060-07-004/13/23 18:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.1 %04/13/23 23:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-5 Lab ID: 92662174005 Collected: 04/13/23 12:50 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 11:53 N204/18/23 08:2811.8 11.8 1
Aliphatic (C19-C36)ND mg/kg 04/19/23 11:53 N204/18/23 08:2811.8 11.8 1
Aromatic (C11-C22)ND mg/kg 04/19/23 11:53 N204/18/23 08:2811.8 11.8 1
Surrogates
1-Chlorooctadecane (S)70 %04/19/23 11:53 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)63 %04/19/23 11:53 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)102 %04/19/23 11:53 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)108 %04/19/23 11:53 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/16/23 13:23 83-32-904/15/23 15:46390 137 1
Acenaphthylene ND ug/kg 04/16/23 13:23 208-96-804/15/23 15:46390 137 1
Aniline ND ug/kg 04/16/23 13:23 62-53-304/15/23 15:46390 153 1
Anthracene ND ug/kg 04/16/23 13:23 120-12-704/15/23 15:46390 128 1
Benzo(a)anthracene ND ug/kg 04/16/23 13:23 56-55-304/15/23 15:46390 130 1
Benzo(a)pyrene ND ug/kg 04/16/23 13:23 50-32-804/15/23 15:46390 135 1
Benzo(b)fluoranthene ND ug/kg 04/16/23 13:23 205-99-204/15/23 15:46390 130 1
Benzo(g,h,i)perylene ND ug/kg 04/16/23 13:23 191-24-204/15/23 15:46390 151 1
Benzo(k)fluoranthene ND ug/kg 04/16/23 13:23 207-08-904/15/23 15:46390 137 1
Benzoic Acid ND ug/kg 04/16/23 13:23 65-85-0 L204/15/23 15:461950 839 1
Benzyl alcohol ND ug/kg 04/16/23 13:23 100-51-604/15/23 15:46781 296 1
4-Bromophenylphenyl ether ND ug/kg 04/16/23 13:23 101-55-304/15/23 15:46390 150 1
Butylbenzylphthalate ND ug/kg 04/16/23 13:23 85-68-704/15/23 15:46390 164 1
4-Chloro-3-methylphenol ND ug/kg 04/16/23 13:23 59-50-704/15/23 15:46781 275 1
4-Chloroaniline ND ug/kg 04/16/23 13:23 106-47-804/15/23 15:46781 306 1
bis(2-Chloroethoxy)methane ND ug/kg 04/16/23 13:23 111-91-104/15/23 15:46390 162 1
bis(2-Chloroethyl) ether ND ug/kg 04/16/23 13:23 111-44-404/15/23 15:46390 147 1
2-Chloronaphthalene ND ug/kg 04/16/23 13:23 91-58-704/15/23 15:46390 155 1
2-Chlorophenol ND ug/kg 04/16/23 13:23 95-57-804/15/23 15:46390 147 1
4-Chlorophenylphenyl ether ND ug/kg 04/16/23 13:23 7005-72-304/15/23 15:46390 146 1
Chrysene ND ug/kg 04/16/23 13:23 218-01-904/15/23 15:46390 142 1
Dibenz(a,h)anthracene ND ug/kg 04/16/23 13:23 53-70-304/15/23 15:46390 150 1
Dibenzofuran ND ug/kg 04/16/23 13:23 132-64-904/15/23 15:46390 141 1
1,2-Dichlorobenzene ND ug/kg 04/16/23 13:23 95-50-104/15/23 15:46390 141 1
1,3-Dichlorobenzene ND ug/kg 04/16/23 13:23 541-73-104/15/23 15:46390 138 1
1,4-Dichlorobenzene ND ug/kg 04/16/23 13:23 106-46-704/15/23 15:46390 149 1
3,3'-Dichlorobenzidine ND ug/kg 04/16/23 13:23 91-94-104/15/23 15:46781 264 1
2,4-Dichlorophenol ND ug/kg 04/16/23 13:23 120-83-204/15/23 15:46390 153 1
Diethylphthalate ND ug/kg 04/16/23 13:23 84-66-204/15/23 15:46390 143 1
2,4-Dimethylphenol ND ug/kg 04/16/23 13:23 105-67-904/15/23 15:46390 162 1
Dimethylphthalate ND ug/kg 04/16/23 13:23 131-11-304/15/23 15:46390 142 1
Di-n-butylphthalate ND ug/kg 04/16/23 13:23 84-74-204/15/23 15:46390 131 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/16/23 13:23 534-52-104/15/23 15:46781 364 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-5 Lab ID: 92662174005 Collected: 04/13/23 12:50 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 04/16/23 13:23 51-28-504/15/23 15:461950 1210 1
2,4-Dinitrotoluene ND ug/kg 04/16/23 13:23 121-14-204/15/23 15:46390 150 1
2,6-Dinitrotoluene ND ug/kg 04/16/23 13:23 606-20-204/15/23 15:46390 143 1
Di-n-octylphthalate ND ug/kg 04/16/23 13:23 117-84-004/15/23 15:46390 154 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/16/23 13:23 117-81-704/15/23 15:46390 151 1
Fluoranthene ND ug/kg 04/16/23 13:23 206-44-004/15/23 15:46390 134 1
Fluorene ND ug/kg 04/16/23 13:23 86-73-704/15/23 15:46390 137 1
Hexachloro-1,3-butadiene ND ug/kg 04/16/23 13:23 87-68-304/15/23 15:46390 169 1
Hexachlorobenzene ND ug/kg 04/16/23 13:23 118-74-104/15/23 15:46390 153 1
Hexachlorocyclopentadiene ND ug/kg 04/16/23 13:23 77-47-404/15/23 15:46390 224 1
Hexachloroethane ND ug/kg 04/16/23 13:23 67-72-104/15/23 15:46390 149 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/16/23 13:23 193-39-504/15/23 15:46390 154 1
Isophorone ND ug/kg 04/16/23 13:23 78-59-104/15/23 15:46390 174 1
1-Methylnaphthalene ND ug/kg 04/16/23 13:23 90-12-004/15/23 15:46390 137 1
2-Methylnaphthalene ND ug/kg 04/16/23 13:23 91-57-604/15/23 15:46390 156 1
2-Methylphenol(o-Cresol)ND ug/kg 04/16/23 13:23 95-48-704/15/23 15:46390 160 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/16/23 13:23 15831-10-404/15/23 15:46390 157 1
Naphthalene ND ug/kg 04/16/23 13:23 91-20-304/15/23 15:46390 133 1
2-Nitroaniline ND ug/kg 04/16/23 13:23 88-74-404/15/23 15:461950 319 1
3-Nitroaniline ND ug/kg 04/16/23 13:23 99-09-204/15/23 15:461950 306 1
4-Nitroaniline ND ug/kg 04/16/23 13:23 100-01-604/15/23 15:46781 297 1
Nitrobenzene ND ug/kg 04/16/23 13:23 98-95-304/15/23 15:46390 181 1
2-Nitrophenol ND ug/kg 04/16/23 13:23 88-75-504/15/23 15:46390 169 1
4-Nitrophenol ND ug/kg 04/16/23 13:23 100-02-704/15/23 15:461950 755 1
N-Nitrosodimethylamine ND ug/kg 04/16/23 13:23 62-75-904/15/23 15:46390 131 1
N-Nitroso-di-n-propylamine ND ug/kg 04/16/23 13:23 621-64-704/15/23 15:46390 147 1
N-Nitrosodiphenylamine ND ug/kg 04/16/23 13:23 86-30-604/15/23 15:46390 138 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/16/23 13:23 108-60-104/15/23 15:46390 186 1
Pentachlorophenol ND ug/kg 04/16/23 13:23 87-86-504/15/23 15:46781 382 1
Phenanthrene ND ug/kg 04/16/23 13:23 85-01-804/15/23 15:46390 128 1
Phenol ND ug/kg 04/16/23 13:23 108-95-204/15/23 15:46390 174 1
Pyrene ND ug/kg 04/16/23 13:23 129-00-004/15/23 15:46390 159 1
Pyridine ND ug/kg 04/16/23 13:23 110-86-104/15/23 15:46390 123 1
1,2,4-Trichlorobenzene ND ug/kg 04/16/23 13:23 120-82-104/15/23 15:46390 154 1
2,4,5-Trichlorophenol ND ug/kg 04/16/23 13:23 95-95-404/15/23 15:46390 179 1
2,4,6-Trichlorophenol ND ug/kg 04/16/23 13:23 88-06-204/15/23 15:46390 161 1
Surrogates
Nitrobenzene-d5 (S)29 %04/16/23 13:23 4165-60-004/15/23 15:4610-130 1
2-Fluorobiphenyl (S)19 %04/16/23 13:23 321-60-804/15/23 15:4610-130 1
Terphenyl-d14 (S)52 %04/16/23 13:23 1718-51-004/15/23 15:4610-130 1
Phenol-d6 (S)38 %04/16/23 13:23 13127-88-304/15/23 15:4610-130 1
2-Fluorophenol (S)31 %04/16/23 13:23 367-12-404/15/23 15:4610-130 1
2,4,6-Tribromophenol (S)37 %04/16/23 13:23 118-79-604/15/23 15:4610-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
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Page 30 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-5 Lab ID: 92662174005 Collected: 04/13/23 12:50 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/13/23 23:44 67-64-104/13/23 18:43133 42.6 1
Benzene ND ug/kg 04/13/23 23:44 71-43-204/13/23 18:436.6 2.6 1
Bromobenzene ND ug/kg 04/13/23 23:44 108-86-104/13/23 18:436.6 2.2 1
Bromochloromethane ND ug/kg 04/13/23 23:44 74-97-504/13/23 18:436.6 2.0 1
Bromodichloromethane ND ug/kg 04/13/23 23:44 75-27-404/13/23 18:436.6 2.6 1
Bromoform ND ug/kg 04/13/23 23:44 75-25-2 IK04/13/23 18:436.6 2.3 1
Bromomethane ND ug/kg 04/13/23 23:44 74-83-9 v204/13/23 18:4326.5 20.6 1
2-Butanone (MEK)ND ug/kg 04/13/23 23:44 78-93-304/13/23 18:43133 31.9 1
n-Butylbenzene ND ug/kg 04/13/23 23:44 104-51-804/13/23 18:436.6 4.2 1
sec-Butylbenzene ND ug/kg 04/13/23 23:44 135-98-804/13/23 18:436.6 2.9 1
tert-Butylbenzene ND ug/kg 04/13/23 23:44 98-06-604/13/23 18:436.6 2.4 1
Carbon tetrachloride ND ug/kg 04/13/23 23:44 56-23-504/13/23 18:436.6 2.5 1
Chlorobenzene ND ug/kg 04/13/23 23:44 108-90-704/13/23 18:436.6 3.8 1
Chloroethane ND ug/kg 04/13/23 23:44 75-00-304/13/23 18:4313.3 5.1 1
Chloroform ND ug/kg 04/13/23 23:44 67-66-304/13/23 18:436.6 5.5 1
Chloromethane ND ug/kg 04/13/23 23:44 74-87-304/13/23 18:4313.3 5.6 1
2-Chlorotoluene ND ug/kg 04/13/23 23:44 95-49-804/13/23 18:436.6 2.3 1
4-Chlorotoluene ND ug/kg 04/13/23 23:44 106-43-404/13/23 18:436.6 3.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/13/23 23:44 96-12-804/13/23 18:436.6 2.6 1
Dibromochloromethane ND ug/kg 04/13/23 23:44 124-48-104/13/23 18:436.6 3.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/13/23 23:44 106-93-404/13/23 18:436.6 2.9 1
Dibromomethane ND ug/kg 04/13/23 23:44 74-95-304/13/23 18:436.6 1.4 1
1,2-Dichlorobenzene ND ug/kg 04/13/23 23:44 95-50-104/13/23 18:436.6 2.4 1
1,3-Dichlorobenzene ND ug/kg 04/13/23 23:44 541-73-104/13/23 18:436.6 2.1 1
1,4-Dichlorobenzene ND ug/kg 04/13/23 23:44 106-46-704/13/23 18:436.6 1.7 1
Dichlorodifluoromethane ND ug/kg 04/13/23 23:44 75-71-8 v104/13/23 18:4313.3 6.8 1
1,1-Dichloroethane ND ug/kg 04/13/23 23:44 75-34-304/13/23 18:436.6 2.7 1
1,2-Dichloroethane ND ug/kg 04/13/23 23:44 107-06-204/13/23 18:436.6 4.4 1
1,1-Dichloroethene ND ug/kg 04/13/23 23:44 75-35-404/13/23 18:436.6 2.7 1
cis-1,2-Dichloroethene ND ug/kg 04/13/23 23:44 156-59-204/13/23 18:436.6 2.3 1
trans-1,2-Dichloroethene ND ug/kg 04/13/23 23:44 156-60-504/13/23 18:436.6 5.6 1
1,2-Dichloropropane ND ug/kg 04/13/23 23:44 78-87-504/13/23 18:436.6 2.0 1
1,3-Dichloropropane ND ug/kg 04/13/23 23:44 142-28-904/13/23 18:436.6 2.1 1
2,2-Dichloropropane ND ug/kg 04/13/23 23:44 594-20-704/13/23 18:436.6 5.0 1
1,1-Dichloropropene ND ug/kg 04/13/23 23:44 563-58-604/13/23 18:436.6 3.2 1
cis-1,3-Dichloropropene ND ug/kg 04/13/23 23:44 10061-01-504/13/23 18:436.6 1.8 1
trans-1,3-Dichloropropene ND ug/kg 04/13/23 23:44 10061-02-604/13/23 18:436.6 2.3 1
Diisopropyl ether ND ug/kg 04/13/23 23:44 108-20-304/13/23 18:436.6 1.8 1
Ethylbenzene 5.0J ug/kg 04/13/23 23:44 100-41-404/13/23 18:436.6 3.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/13/23 23:44 87-68-304/13/23 18:4313.3 10.9 1
2-Hexanone ND ug/kg 04/13/23 23:44 591-78-604/13/23 18:4366.4 6.4 1
Isopropylbenzene (Cumene)ND ug/kg 04/13/23 23:44 98-82-804/13/23 18:436.6 2.3 1
p-Isopropyltoluene 43.1 ug/kg 04/13/23 23:44 99-87-604/13/23 18:436.6 3.3 1
Methylene Chloride 227 ug/kg 04/13/23 23:44 75-09-2 C9,IK04/13/23 18:4326.5 18.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Sample: SS-5 Lab ID: 92662174005 Collected: 04/13/23 12:50 Received: 04/13/23 15:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/13/23 23:44 108-10-104/13/23 18:4366.4 6.4 1
Methyl-tert-butyl ether ND ug/kg 04/13/23 23:44 1634-04-404/13/23 18:436.6 2.5 1
Naphthalene ND ug/kg 04/13/23 23:44 91-20-304/13/23 18:436.6 3.5 1
n-Propylbenzene ND ug/kg 04/13/23 23:44 103-65-104/13/23 18:436.6 2.4 1
Styrene ND ug/kg 04/13/23 23:44 100-42-504/13/23 18:436.6 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/13/23 23:44 630-20-604/13/23 18:436.6 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/13/23 23:44 79-34-504/13/23 18:436.6 1.8 1
Tetrachloroethene ND ug/kg 04/13/23 23:44 127-18-404/13/23 18:436.6 2.1 1
Toluene ND ug/kg 04/13/23 23:44 108-88-304/13/23 18:436.6 4.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/13/23 23:44 87-61-604/13/23 18:436.6 5.4 1
1,2,4-Trichlorobenzene ND ug/kg 04/13/23 23:44 120-82-104/13/23 18:436.6 5.6 1
1,1,1-Trichloroethane ND ug/kg 04/13/23 23:44 71-55-604/13/23 18:436.6 3.5 1
1,1,2-Trichloroethane ND ug/kg 04/13/23 23:44 79-00-504/13/23 18:436.6 2.2 1
Trichloroethene ND ug/kg 04/13/23 23:44 79-01-604/13/23 18:436.6 5.3 1
Trichlorofluoromethane ND ug/kg 04/13/23 23:44 75-69-404/13/23 18:436.6 3.6 1
1,2,3-Trichloropropane ND ug/kg 04/13/23 23:44 96-18-404/13/23 18:436.6 3.4 1
1,2,4-Trimethylbenzene ND ug/kg 04/13/23 23:44 95-63-604/13/23 18:436.6 3.9 1
1,3,5-Trimethylbenzene ND ug/kg 04/13/23 23:44 108-67-804/13/23 18:436.6 2.2 1
Vinyl acetate ND ug/kg 04/13/23 23:44 108-05-404/13/23 18:4366.4 13.7 1
Vinyl chloride ND ug/kg 04/13/23 23:44 75-01-4 v204/13/23 18:4313.3 3.4 1
Xylene (Total)ND ug/kg 04/13/23 23:44 1330-20-704/13/23 18:4313.3 3.8 1
m&p-Xylene ND ug/kg 04/13/23 23:44 179601-23-104/13/23 18:4313.3 4.5 1
o-Xylene ND ug/kg 04/13/23 23:44 95-47-604/13/23 18:436.6 2.9 1
Surrogates
Toluene-d8 (S)97 %04/13/23 23:44 2037-26-504/13/23 18:4370-130 1
4-Bromofluorobenzene (S)110 %04/13/23 23:44 460-00-404/13/23 18:4370-130 1
1,2-Dichloroethane-d4 (S)116 %04/13/23 23:44 17060-07-004/13/23 18:4370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.6 %04/13/23 23:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
767997
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3987668
Associated Lab Samples:92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/13/23 17:331.9
1,1,1-Trichloroethane ug/kg ND 5.0 04/13/23 17:332.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/13/23 17:331.3
1,1,2-Trichloroethane ug/kg ND 5.0 04/13/23 17:331.7
1,1-Dichloroethane ug/kg ND 5.0 04/13/23 17:332.1
1,1-Dichloroethene ug/kg ND 5.0 04/13/23 17:332.1
1,1-Dichloropropene ug/kg ND 5.0 04/13/23 17:332.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/13/23 17:334.0
1,2,3-Trichloropropane ug/kg ND 5.0 04/13/23 17:332.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/13/23 17:334.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/13/23 17:333.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/13/23 17:331.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/13/23 17:332.2
1,2-Dichlorobenzene ug/kg ND 5.0 04/13/23 17:331.8
1,2-Dichloroethane ug/kg ND 5.0 04/13/23 17:333.3
1,2-Dichloropropane ug/kg ND 5.0 04/13/23 17:331.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/13/23 17:331.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/13/23 17:331.6
1,3-Dichloropropane ug/kg ND 5.0 04/13/23 17:331.6
1,4-Dichlorobenzene ug/kg ND 5.0 04/13/23 17:331.3
2,2-Dichloropropane ug/kg ND 5.0 04/13/23 17:333.8
2-Butanone (MEK)ug/kg ND 100 04/13/23 17:3324.0
2-Chlorotoluene ug/kg ND 5.0 04/13/23 17:331.8
2-Hexanone ug/kg ND 50.0 04/13/23 17:334.8
4-Chlorotoluene ug/kg ND 5.0 04/13/23 17:332.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/13/23 17:334.8
Acetone ug/kg ND 100 04/13/23 17:3332.1
Benzene ug/kg ND 5.0 04/13/23 17:332.0
Bromobenzene ug/kg ND 5.0 04/13/23 17:331.6
Bromochloromethane ug/kg ND 5.0 04/13/23 17:331.5
Bromodichloromethane ug/kg ND 5.0 04/13/23 17:331.9
Bromoform ug/kg ND 5.0 IK04/13/23 17:331.8
Bromomethane ug/kg ND 20.0 v204/13/23 17:3315.5
Carbon tetrachloride ug/kg ND 5.0 04/13/23 17:331.9
Chlorobenzene ug/kg ND 5.0 04/13/23 17:332.9
Chloroethane ug/kg ND 10.0 04/13/23 17:333.9
Chloroform ug/kg ND 5.0 04/13/23 17:334.2
Chloromethane ug/kg ND 10.0 04/13/23 17:334.2
cis-1,2-Dichloroethene ug/kg ND 5.0 04/13/23 17:331.7
cis-1,3-Dichloropropene ug/kg ND 5.0 04/13/23 17:331.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3987668
Associated Lab Samples:92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 04/13/23 17:332.8
Dibromomethane ug/kg ND 5.0 04/13/23 17:331.1
Dichlorodifluoromethane ug/kg ND 10.0 v104/13/23 17:335.1
Diisopropyl ether ug/kg ND 5.0 04/13/23 17:331.4
Ethylbenzene ug/kg ND 5.0 04/13/23 17:332.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 04/13/23 17:338.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/13/23 17:331.7
m&p-Xylene ug/kg ND 10.0 04/13/23 17:333.4
Methyl-tert-butyl ether ug/kg ND 5.0 04/13/23 17:331.9
Methylene Chloride ug/kg ND 20.0 IK04/13/23 17:3313.7
n-Butylbenzene ug/kg ND 5.0 04/13/23 17:333.2
n-Propylbenzene ug/kg ND 5.0 04/13/23 17:331.8
Naphthalene ug/kg ND 5.0 04/13/23 17:332.6
o-Xylene ug/kg ND 5.0 04/13/23 17:332.2
p-Isopropyltoluene ug/kg ND 5.0 04/13/23 17:332.5
sec-Butylbenzene ug/kg ND 5.0 04/13/23 17:332.2
Styrene ug/kg ND 5.0 04/13/23 17:331.3
tert-Butylbenzene ug/kg ND 5.0 04/13/23 17:331.8
Tetrachloroethene ug/kg ND 5.0 04/13/23 17:331.6
Toluene ug/kg ND 5.0 04/13/23 17:333.4
trans-1,2-Dichloroethene ug/kg ND 5.0 04/13/23 17:334.2
trans-1,3-Dichloropropene ug/kg ND 5.0 04/13/23 17:331.7
Trichloroethene ug/kg ND 5.0 04/13/23 17:334.0
Trichlorofluoromethane ug/kg ND 5.0 04/13/23 17:332.8
Vinyl acetate ug/kg ND 50.0 04/13/23 17:3310.3
Vinyl chloride ug/kg ND 10.0 v204/13/23 17:332.5
Xylene (Total)ug/kg ND 10.0 04/13/23 17:332.8
1,2-Dichloroethane-d4 (S)%114 70-130 04/13/23 17:33
4-Bromofluorobenzene (S)%101 70-130 04/13/23 17:33
Toluene-d8 (S)%98 70-130 04/13/23 17:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3987669LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 546500 109 70-130
1,1,1-Trichloroethane ug/kg 522500 104 70-130
1,1,2,2-Tetrachloroethane ug/kg 532500 106 70-130
1,1,2-Trichloroethane ug/kg 493500 99 70-130
1,1-Dichloroethane ug/kg 472500 94 70-130
1,1-Dichloroethene ug/kg 536500 107 70-130
1,1-Dichloropropene ug/kg 533500 107 70-130
1,2,3-Trichlorobenzene ug/kg 555500 111 70-130
1,2,3-Trichloropropane ug/kg 528500 106 70-130
1,2,4-Trichlorobenzene ug/kg 547500 109 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3987669LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 574500 115 70-130
1,2-Dibromo-3-chloropropane ug/kg 555500 111 67-130
1,2-Dibromoethane (EDB)ug/kg 535500 107 70-130
1,2-Dichlorobenzene ug/kg 541500 108 70-130
1,2-Dichloroethane ug/kg 524500 105 70-130
1,2-Dichloropropane ug/kg 450500 90 70-130
1,3,5-Trimethylbenzene ug/kg 562500 112 70-130
1,3-Dichlorobenzene ug/kg 562500 112 70-130
1,3-Dichloropropane ug/kg 518500 104 70-130
1,4-Dichlorobenzene ug/kg 514500 103 70-130
2,2-Dichloropropane ug/kg 512500 102 67-130
2-Butanone (MEK)ug/kg 9801000 98 66-130
2-Chlorotoluene ug/kg 566500 113 70-130
2-Hexanone ug/kg 11101000 111 70-130
4-Chlorotoluene ug/kg 535500 107 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 10201000 102 70-130
Acetone ug/kg 9781000 98 67-130
Benzene ug/kg 472500 94 70-130
Bromobenzene ug/kg 528500 106 70-130
Bromochloromethane ug/kg 499500 100 70-130
Bromodichloromethane ug/kg 519500 104 70-130
Bromoform ug/kg 445 IK50089 70-130
Bromomethane ug/kg 339 v350068 53-175
Carbon tetrachloride ug/kg 576500 115 70-130
Chlorobenzene ug/kg 513500 103 70-130
Chloroethane ug/kg 494500 99 70-135
Chloroform ug/kg 469500 94 70-130
Chloromethane ug/kg 493500 99 64-130
cis-1,2-Dichloroethene ug/kg 465500 93 70-130
cis-1,3-Dichloropropene ug/kg 508500 102 70-130
Dibromochloromethane ug/kg 534500 107 70-130
Dibromomethane ug/kg 484500 97 70-130
Dichlorodifluoromethane ug/kg 643 v1500129 63-145
Diisopropyl ether ug/kg 433500 87 68-130
Ethylbenzene ug/kg 490500 98 70-130
Hexachloro-1,3-butadiene ug/kg 566500 113 70-130
Isopropylbenzene (Cumene)ug/kg 560500 112 70-130
m&p-Xylene ug/kg 10901000 109 70-130
Methyl-tert-butyl ether ug/kg 463500 93 70-130
Methylene Chloride ug/kg 582 IK500116 67-130
n-Butylbenzene ug/kg 545500 109 70-130
n-Propylbenzene ug/kg 538500 108 70-130
Naphthalene ug/kg 564500 113 70-130
o-Xylene ug/kg 533500 107 70-130
p-Isopropyltoluene ug/kg 546500 109 70-130
sec-Butylbenzene ug/kg 539500 108 70-130
Styrene ug/kg 541500 108 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3987669LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 538500 108 64-130
Tetrachloroethene ug/kg 520500 104 70-130
Toluene ug/kg 478500 96 70-130
trans-1,2-Dichloroethene ug/kg 490500 98 70-130
trans-1,3-Dichloropropene ug/kg 498500 100 70-130
Trichloroethene ug/kg 484500 97 70-130
Trichlorofluoromethane ug/kg 562500 112 70-130
Vinyl acetate ug/kg 9991000 100 70-134
Vinyl chloride ug/kg 391 v350078 68-130
Xylene (Total)ug/kg 16301500 109 70-130
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3987670MATRIX SPIKE SAMPLE:
MSSpike
Result
92662174001
1,1,1,2-Tetrachloroethane ug/kg 635705 90 58-140ND
1,1,1-Trichloroethane ug/kg 606705 86 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 651705 92 52-139ND
1,1,2-Trichloroethane ug/kg 622705 88 56-140ND
1,1-Dichloroethane ug/kg 538705 76 58-145ND
1,1-Dichloroethene ug/kg 610705 87 57-158ND
1,1-Dichloropropene ug/kg 561705 80 58-151ND
1,2,3-Trichlorobenzene ug/kg 475705 67 48-149ND
1,2,3-Trichloropropane ug/kg 598705 85 54-132ND
1,2,4-Trichlorobenzene ug/kg 477705 68 51-151ND
1,2,4-Trimethylbenzene ug/kg 603705 86 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 612705 87 44-134ND
1,2-Dibromoethane (EDB)ug/kg 604705 86 60-138ND
1,2-Dichlorobenzene ug/kg 585705 83 59-147ND
1,2-Dichloroethane ug/kg 630705 89 57-139ND
1,2-Dichloropropane ug/kg 543705 77 62-145ND
1,3,5-Trimethylbenzene ug/kg 590705 84 47-159ND
1,3-Dichlorobenzene ug/kg 556705 79 58-144ND
1,3-Dichloropropane ug/kg 609705 86 60-142ND
1,4-Dichlorobenzene ug/kg 516705 73 57-143ND
2,2-Dichloropropane ug/kg 555705 79 37-144ND
2-Butanone (MEK)ug/kg 10301410 73 28-146ND
2-Chlorotoluene ug/kg 582705 83 55-158ND
2-Hexanone ug/kg 12501410 89 44-141ND
4-Chlorotoluene ug/kg 538705 76 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 11501410 82 50-138ND
Acetone ug/kg 10101410 72 20-136ND
Benzene ug/kg 562705 80 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3987670MATRIX SPIKE SAMPLE:
MSSpike
Result
92662174001
Bromobenzene ug/kg 570705 81 59-145ND
Bromochloromethane ug/kg 579705 82 57-143ND
Bromodichloromethane ug/kg 595705 84 53-133ND
Bromoform ug/kg 506 IK70572 48-133ND
Bromomethane ug/kg 329 v370547 10-167ND
Carbon tetrachloride ug/kg 525705 75 57-147ND
Chlorobenzene ug/kg 580705 82 61-144ND
Chloroethane ug/kg 415705 59 10-153ND
Chloroform ug/kg 549705 78 58-141ND
Chloromethane ug/kg 544705 77 54-165ND
cis-1,2-Dichloroethene ug/kg 545705 77 59-144ND
cis-1,3-Dichloropropene ug/kg 585705 83 56-137ND
Dibromochloromethane ug/kg 612705 87 53-139ND
Dibromomethane ug/kg 564705 80 60-136ND
Dichlorodifluoromethane ug/kg 623 v170588 49-177ND
Diisopropyl ether ug/kg 511705 72 53-136ND
Ethylbenzene ug/kg 535705 76 53-150ND
Hexachloro-1,3-butadiene ug/kg 522705 74 42-186ND
Isopropylbenzene (Cumene)ug/kg 629705 89 62-154ND
m&p-Xylene ug/kg 11501410 82 49-156ND
Methyl-tert-butyl ether ug/kg 554705 79 54-133ND
Methylene Chloride ug/kg 814 IK70553 50-153440
n-Butylbenzene ug/kg 485705 69 44-174ND
n-Propylbenzene ug/kg 524705 74 52-157ND
Naphthalene ug/kg 507705 72 37-150ND
o-Xylene ug/kg 601705 85 54-150ND
p-Isopropyltoluene ug/kg 541705 77 50-164ND
sec-Butylbenzene ug/kg 548705 78 58-161ND
Styrene ug/kg 595705 84 60-148ND
tert-Butylbenzene ug/kg 567705 80 44-151ND
Tetrachloroethene ug/kg 476705 68 53-151ND
Toluene ug/kg 542705 77 52-148ND
trans-1,2-Dichloroethene ug/kg 542705 77 60-148ND
trans-1,3-Dichloropropene ug/kg 577705 82 55-133ND
Trichloroethene ug/kg 534705 76 60-148ND
Trichlorofluoromethane ug/kg 340705 48 10-154ND
Vinyl acetate ug/kg 10801410 77 50-149ND
Vinyl chloride ug/kg 476 v370568 57-157ND
Xylene (Total)ug/kg 17502120 83 52-153ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%108 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662174002
3987671SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND IK30ND
Bromomethane ug/kg ND v230ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg 5.2J 305.3J
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662174002
3987671SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND IK30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 3.6J 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND v230ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%116116
4-Bromofluorobenzene (S)%107105
Toluene-d8 (S)%10099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768315
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3989138
Associated Lab Samples:92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 331 04/16/23 09:11130
1,2-Dichlorobenzene ug/kg ND 331 04/16/23 09:11119
1,3-Dichlorobenzene ug/kg ND 331 04/16/23 09:11117
1,4-Dichlorobenzene ug/kg ND 331 04/16/23 09:11126
1-Methylnaphthalene ug/kg ND 331 04/16/23 09:11116
2,2'-Oxybis(1-chloropropane)ug/kg ND 331 04/16/23 09:11158
2,4,5-Trichlorophenol ug/kg ND 331 04/16/23 09:11152
2,4,6-Trichlorophenol ug/kg ND 331 04/16/23 09:11136
2,4-Dichlorophenol ug/kg ND 331 04/16/23 09:11129
2,4-Dimethylphenol ug/kg ND 331 04/16/23 09:11137
2,4-Dinitrophenol ug/kg ND 1660 04/16/23 09:111020
2,4-Dinitrotoluene ug/kg ND 331 04/16/23 09:11127
2,6-Dinitrotoluene ug/kg ND 331 04/16/23 09:11121
2-Chloronaphthalene ug/kg ND 331 04/16/23 09:11131
2-Chlorophenol ug/kg ND 331 04/16/23 09:11124
2-Methylnaphthalene ug/kg ND 331 04/16/23 09:11132
2-Methylphenol(o-Cresol)ug/kg ND 331 04/16/23 09:11135
2-Nitroaniline ug/kg ND 1660 04/16/23 09:11271
2-Nitrophenol ug/kg ND 331 04/16/23 09:11143
3&4-Methylphenol(m&p Cresol)ug/kg ND 331 04/16/23 09:11133
3,3'-Dichlorobenzidine ug/kg ND 662 04/16/23 09:11224
3-Nitroaniline ug/kg ND 1660 04/16/23 09:11260
4,6-Dinitro-2-methylphenol ug/kg ND 662 04/16/23 09:11309
4-Bromophenylphenyl ether ug/kg ND 331 04/16/23 09:11127
4-Chloro-3-methylphenol ug/kg ND 662 04/16/23 09:11233
4-Chloroaniline ug/kg ND 662 04/16/23 09:11260
4-Chlorophenylphenyl ether ug/kg ND 331 04/16/23 09:11123
4-Nitroaniline ug/kg ND 662 04/16/23 09:11252
4-Nitrophenol ug/kg ND 1660 04/16/23 09:11640
Acenaphthene ug/kg ND 331 04/16/23 09:11116
Acenaphthylene ug/kg ND 331 04/16/23 09:11116
Aniline ug/kg ND 331 04/16/23 09:11129
Anthracene ug/kg ND 331 04/16/23 09:11108
Benzo(a)anthracene ug/kg ND 331 04/16/23 09:11110
Benzo(a)pyrene ug/kg ND 331 04/16/23 09:11114
Benzo(b)fluoranthene ug/kg ND 331 04/16/23 09:11110
Benzo(g,h,i)perylene ug/kg ND 331 04/16/23 09:11128
Benzo(k)fluoranthene ug/kg ND 331 04/16/23 09:11116
Benzoic Acid ug/kg ND 1660 04/16/23 09:11711
Benzyl alcohol ug/kg ND 662 04/16/23 09:11251
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3989138
Associated Lab Samples:92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 331 04/16/23 09:11137
bis(2-Chloroethyl) ether ug/kg ND 331 04/16/23 09:11124
bis(2-Ethylhexyl)phthalate ug/kg ND 331 04/16/23 09:11128
Butylbenzylphthalate ug/kg ND 331 04/16/23 09:11139
Chrysene ug/kg ND 331 04/16/23 09:11120
Di-n-butylphthalate ug/kg ND 331 04/16/23 09:11111
Di-n-octylphthalate ug/kg ND 331 04/16/23 09:11130
Dibenz(a,h)anthracene ug/kg ND 331 04/16/23 09:11127
Dibenzofuran ug/kg ND 331 04/16/23 09:11119
Diethylphthalate ug/kg ND 331 04/16/23 09:11121
Dimethylphthalate ug/kg ND 331 04/16/23 09:11120
Fluoranthene ug/kg ND 331 04/16/23 09:11113
Fluorene ug/kg ND 331 04/16/23 09:11116
Hexachloro-1,3-butadiene ug/kg ND 331 04/16/23 09:11143
Hexachlorobenzene ug/kg ND 331 04/16/23 09:11129
Hexachlorocyclopentadiene ug/kg ND 331 04/16/23 09:11190
Hexachloroethane ug/kg ND 331 04/16/23 09:11126
Indeno(1,2,3-cd)pyrene ug/kg ND 331 04/16/23 09:11130
Isophorone ug/kg ND 331 04/16/23 09:11147
N-Nitroso-di-n-propylamine ug/kg ND 331 04/16/23 09:11124
N-Nitrosodimethylamine ug/kg ND 331 04/16/23 09:11111
N-Nitrosodiphenylamine ug/kg ND 331 04/16/23 09:11117
Naphthalene ug/kg ND 331 04/16/23 09:11112
Nitrobenzene ug/kg ND 331 04/16/23 09:11154
Pentachlorophenol ug/kg ND 662 04/16/23 09:11324
Phenanthrene ug/kg ND 331 04/16/23 09:11108
Phenol ug/kg ND 331 04/16/23 09:11147
Pyrene ug/kg ND 331 04/16/23 09:11134
Pyridine ug/kg ND 331 04/16/23 09:11104
2,4,6-Tribromophenol (S)%59 10-131 04/16/23 09:11
2-Fluorobiphenyl (S)%60 10-130 04/16/23 09:11
2-Fluorophenol (S)%54 10-130 04/16/23 09:11
Nitrobenzene-d5 (S)%57 10-130 04/16/23 09:11
Phenol-d6 (S)%54 10-130 04/16/23 09:11
Terphenyl-d14 (S)%70 10-130 04/16/23 09:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989137LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11301670 68 43-130
1,2-Dichlorobenzene ug/kg 11101670 66 43-130
1,3-Dichlorobenzene ug/kg 10901670 65 43-130
1,4-Dichlorobenzene ug/kg 10901670 65 44-130
1-Methylnaphthalene ug/kg 12001670 72 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989137LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 9851670 59 29-130
2,4,5-Trichlorophenol ug/kg 12301670 73 47-130
2,4,6-Trichlorophenol ug/kg 12401670 74 47-130
2,4-Dichlorophenol ug/kg 12701670 76 45-130
2,4-Dimethylphenol ug/kg 17201670 103 45-130
2,4-Dinitrophenol ug/kg 38608360 46 27-140
2,4-Dinitrotoluene ug/kg 12101670 72 46-130
2,6-Dinitrotoluene ug/kg 12301670 73 48-130
2-Chloronaphthalene ug/kg 11401670 68 46-130
2-Chlorophenol ug/kg 11801670 71 43-130
2-Methylnaphthalene ug/kg 11301670 68 47-130
2-Methylphenol(o-Cresol)ug/kg 12201670 73 42-130
2-Nitroaniline ug/kg 22403340 67 41-130
2-Nitrophenol ug/kg 11601670 69 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 11801670 71 39-130
3,3'-Dichlorobenzidine ug/kg 20303340 61 41-130
3-Nitroaniline ug/kg 20003340 60 37-130
4,6-Dinitro-2-methylphenol ug/kg 22203340 66 38-141
4-Bromophenylphenyl ether ug/kg 11701670 70 47-130
4-Chloro-3-methylphenol ug/kg 24303340 73 44-130
4-Chloroaniline ug/kg 22003340 66 41-130
4-Chlorophenylphenyl ether ug/kg 11601670 69 45-130
4-Nitroaniline ug/kg 21703340 65 42-130
4-Nitrophenol ug/kg 59808360 72 39-131
Acenaphthene ug/kg 11701670 70 49-130
Acenaphthylene ug/kg 12001670 72 50-130
Aniline ug/kg 9761670 58 38-130
Anthracene ug/kg 11301670 67 49-130
Benzo(a)anthracene ug/kg 12201670 73 51-130
Benzo(a)pyrene ug/kg 13001670 78 51-130
Benzo(b)fluoranthene ug/kg 12901670 77 49-130
Benzo(g,h,i)perylene ug/kg 14001670 84 48-140
Benzo(k)fluoranthene ug/kg 13601670 81 51-130
Benzoic Acid ug/kg 834J L2836010 22-130
Benzyl alcohol ug/kg 21803340 65 43-130
bis(2-Chloroethoxy)methane ug/kg 10601670 64 43-130
bis(2-Chloroethyl) ether ug/kg 10501670 63 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12001670 72 43-130
Butylbenzylphthalate ug/kg 12201670 73 44-131
Chrysene ug/kg 12401670 74 51-130
Di-n-butylphthalate ug/kg 11501670 69 46-130
Di-n-octylphthalate ug/kg 11701670 70 45-130
Dibenz(a,h)anthracene ug/kg 13801670 82 48-130
Dibenzofuran ug/kg 11701670 70 10-130
Diethylphthalate ug/kg 11901670 71 48-130
Dimethylphthalate ug/kg 11801670 70 48-130
Fluoranthene ug/kg 11801670 71 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989137LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12001670 72 48-130
Hexachloro-1,3-butadiene ug/kg 11001670 66 39-130
Hexachlorobenzene ug/kg 11501670 69 47-130
Hexachlorocyclopentadiene ug/kg 12301670 74 17-130
Hexachloroethane ug/kg 11001670 66 40-130
Indeno(1,2,3-cd)pyrene ug/kg 14301670 85 50-130
Isophorone ug/kg 11301670 68 41-130
N-Nitroso-di-n-propylamine ug/kg 10801670 64 36-130
N-Nitrosodimethylamine ug/kg 10901670 65 34-130
N-Nitrosodiphenylamine ug/kg 11801670 70 48-130
Naphthalene ug/kg 11301670 68 46-130
Nitrobenzene ug/kg 10801670 65 39-130
Pentachlorophenol ug/kg 21803340 65 42-130
Phenanthrene ug/kg 12001670 72 50-130
Phenol ug/kg 12601670 76 42-130
Pyrene ug/kg 12701670 76 50-130
Pyridine ug/kg 8671670 52 26-130
2,4,6-Tribromophenol (S)%72 10-131
2-Fluorobiphenyl (S)%68 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%65 10-130
Phenol-d6 (S)%67 10-130
Terphenyl-d14 (S)%75 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3989139MATRIX SPIKE SAMPLE:
MSSpike
Result
92661774001
1,2,4-Trichlorobenzene ug/kg 10801830 59 16-130ND
1,2-Dichlorobenzene ug/kg 10001830 55 19-130ND
1,3-Dichlorobenzene ug/kg 9821830 53 19-130ND
1,4-Dichlorobenzene ug/kg 9951830 54 20-130ND
1-Methylnaphthalene ug/kg 10401830 57 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 8941830 49 10-130ND
2,4,5-Trichlorophenol ug/kg 10701830 58 19-130ND
2,4,6-Trichlorophenol ug/kg 11501830 63 18-130ND
2,4-Dichlorophenol ug/kg 11901830 65 16-130ND
2,4-Dimethylphenol ug/kg 17401830 95 10-130ND
2,4-Dinitrophenol ug/kg 52709190 57 10-143ND
2,4-Dinitrotoluene ug/kg 8131830 44 19-130ND
2,6-Dinitrotoluene ug/kg 11701830 64 22-130ND
2-Chloronaphthalene ug/kg 9271830 50 18-130ND
2-Chlorophenol ug/kg 10601830 58 20-130ND
2-Methylnaphthalene ug/kg 9751830 53 18-130ND
2-Methylphenol(o-Cresol)ug/kg 10601830 58 13-130ND
2-Nitroaniline ug/kg 19203670 52 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
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[phone]
Page 43 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3989139MATRIX SPIKE SAMPLE:
MSSpike
Result
92661774001
2-Nitrophenol ug/kg 12001830 65 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 10401830 57 13-130ND
3,3'-Dichlorobenzidine ug/kg 17003670 46 10-130ND
3-Nitroaniline ug/kg 1590J3670 43 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 22703670 62 10-144ND
4-Bromophenylphenyl ether ug/kg 11601830 63 18-130ND
4-Chloro-3-methylphenol ug/kg 20103670 55 16-130ND
4-Chloroaniline ug/kg 18503670 50 17-130ND
4-Chlorophenylphenyl ether ug/kg 10601830 58 17-130ND
4-Nitroaniline ug/kg 16903670 46 21-130ND
4-Nitrophenol ug/kg 50309190 55 13-131ND
Acenaphthene ug/kg 9621830 52 20-130ND
Acenaphthylene ug/kg 10101830 55 21-130ND
Aniline ug/kg 7721830 42 10-130ND
Anthracene ug/kg 9921830 54 19-130ND
Benzo(a)anthracene ug/kg 10801830 59 17-130ND
Benzo(a)pyrene ug/kg 11501830 63 14-130ND
Benzo(b)fluoranthene ug/kg 12101830 66 11-134ND
Benzo(g,h,i)perylene ug/kg 10001830 55 12-130ND
Benzo(k)fluoranthene ug/kg 12701830 69 15-130ND
Benzoic Acid ug/kg 48109190 52 10-130ND
Benzyl alcohol ug/kg 18603670 51 20-130ND
bis(2-Chloroethoxy)methane ug/kg 9801830 53 16-130ND
bis(2-Chloroethyl) ether ug/kg 9611830 52 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 10801830 59 11-130ND
Butylbenzylphthalate ug/kg 10201830 56 10-130ND
Chrysene ug/kg 11101830 61 17-130ND
Di-n-butylphthalate ug/kg 10101830 55 16-130ND
Di-n-octylphthalate ug/kg 10101830 55 16-130ND
Dibenz(a,h)anthracene ug/kg 10301830 56 13-130ND
Dibenzofuran ug/kg 10401830 57 19-130ND
Diethylphthalate ug/kg 9531830 52 22-130ND
Dimethylphthalate ug/kg 8161830 44 23-130ND
Fluoranthene ug/kg 11701830 64 14-130ND
Fluorene ug/kg 9611830 52 19-130ND
Hexachloro-1,3-butadiene ug/kg 11101830 61 12-130ND
Hexachlorobenzene ug/kg 12601830 68 17-130ND
Hexachlorocyclopentadiene ug/kg 11901830 65 10-130ND
Hexachloroethane ug/kg 10201830 55 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 10701830 58 13-130ND
Isophorone ug/kg 9761830 53 17-130ND
N-Nitroso-di-n-propylamine ug/kg 10001830 55 10-130ND
N-Nitrosodimethylamine ug/kg 9201830 50 16-130ND
N-Nitrosodiphenylamine ug/kg 15101830 82 19-130ND
Naphthalene ug/kg 10301830 56 18-130ND
Nitrobenzene ug/kg 10301830 56 15-130ND
Pentachlorophenol ug/kg 21903670 60 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3989139MATRIX SPIKE SAMPLE:
MSSpike
Result
92661774001
Phenanthrene ug/kg 10501830 57 17-130ND
Phenol ug/kg 11001830 60 15-130ND
Pyrene ug/kg 11101830 60 31-130ND
Pyridine ug/kg 6361830 35 10-130ND
2,4,6-Tribromophenol (S)%66 10-131
2-Fluorobiphenyl (S)%53 10-130
2-Fluorophenol (S)%52 10-130
Nitrobenzene-d5 (S)%56 10-130
Phenol-d6 (S)%51 10-130
Terphenyl-d14 (S)%63 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92661946008
3989140SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg 1290J 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92661946008
3989140SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg 2680 0 302.7 mg/kg
Benzo(a)anthracene ug/kg 8890 11 307.9 mg/kg
Benzo(a)pyrene ug/kg 7650 14 306.6 mg/kg
Benzo(b)fluoranthene ug/kg 11600 10 3010.5 mg/kg
Benzo(g,h,i)perylene ug/kg 5510 14 304.8 mg/kg
Benzo(k)fluoranthene ug/kg 4830 13 304.2 mg/kg
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg 9290 6 308.8 mg/kg
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg 1800J 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg 14900 4 3014.3 mg/kg
Fluorene ug/kg 1160J 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg 5180 16 304.4 mg/kg
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg 12600 6 3013.3 mg/kg
Phenol ug/kg ND 30ND
Pyrene ug/kg 16200 8 3015.0 mg/kg
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%3937
2-Fluorobiphenyl (S)%3834
2-Fluorophenol (S)%3729
Nitrobenzene-d5 (S)%49 D347
Phenol-d6 (S)%4840
Terphenyl-d14 (S)%6361
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768569
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3990298
Associated Lab Samples:92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Matrix: Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 10.1 N204/19/23 08:3110.1
Aliphatic (C19-C36)mg/kg ND 10.1 N204/19/23 08:3110.1
Aromatic (C11-C22)mg/kg ND 10.1 N204/19/23 08:3110.1
1-Chlorooctadecane (S)%114 40-140 04/19/23 08:31
2-Bromonaphthalene (S)%90 40-140 04/19/23 08:31
2-Fluorobiphenyl (S)%85 40-140 04/19/23 08:31
o-Terphenyl (S)%85 40-140 04/19/23 08:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3990299LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3990300
Aliphatic (C09-C18)mg/kg ND N210.1 77 40-14078ND 50
Aliphatic (C19-C36)mg/kg 17.7 N213.5 131 40-14013618.0 2 50
Aromatic (C11-C22)mg/kg 27.1 N228.7 94 40-1409426.5 2 50
1-Chlorooctadecane (S)%121 40-140124
2-Bromonaphthalene (S)%95 40-14095
2-Fluorobiphenyl (S)%90 40-14089
o-Terphenyl (S)%93 40-14090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
767976
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92662174001, 92662174002, 92662174003, 92662174004, 92662174005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662145004
3987544SAMPLE DUPLICATE:
Percent Moisture %14.8 N222515.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662174005
3987738SAMPLE DUPLICATE:
Percent Moisture %16.9 N222516.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 75
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result shouldbe considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 75
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92662174
ARRIS NODA 71237184
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92662174001 768569 768765SS-1 MADEP EPH MADEP EPH
92662174002 768569 768765SS-2 MADEP EPH MADEP EPH
92662174003 768569 768765SS-3 MADEP EPH MADEP EPH
92662174004 768569 768765SS-4 MADEP EPH MADEP EPH
92662174005 768569 768765SS-5 MADEP EPH MADEP EPH
92662174001 768315 768346SS-1 EPA 3546 EPA 8270E
92662174002 768315 768346SS-2 EPA 3546 EPA 8270E
92662174003 768315 768346SS-3 EPA 3546 EPA 8270E
92662174004 768315 768346SS-4 EPA 3546 EPA 8270E
92662174005 768315 768346SS-5 EPA 3546 EPA 8270E
92662174001 767997 768139SS-1 EPA 5035A/5030B EPA 8260D
92662174002 767997 768139SS-2 EPA 5035A/5030B EPA 8260D
92662174003 767997 768139SS-3 EPA 5035A/5030B EPA 8260D
92662174004 767997 768139SS-4 EPA 5035A/5030B EPA 8260D
92662174005 767997 768139SS-5 EPA 5035A/5030B EPA 8260D
92662174001 767976SS-1 SW-846
92662174002 767976SS-2 SW-846
92662174003 767976SS-3 SW-846
92662174004 767976SS-4 SW-846
92662174005 767976SS-5 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2023 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 75
Page 51 of 75
Page 52 of 75
Page 53 of 75
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 20, 2023
Taylor Cannon
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: ARRIS NODA 71237184
Client Job Number:
Project Number: 92662174
Laboratory Work Order Number: 23D1670
Enclosed are results of analyses for samples as received by the laboratory on April 14, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 22
Table of Contents
Page 54 of 75
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23D1670-01 5
23D1670-02 7
23D1670-03 9
23D1670-04 11
23D1670-05 13
Sample Preparation Information 15
QC Data 16
Petroleum Hydrocarbons Analyses - VPH 16
B337372 16
Flag/Qualifier Summary 18
Certifications 19
Chain of Custody/Sample Receipt 20
Page 2 of 22
Table of Contents
Page 55 of 75
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/20/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Taylor Cannon
92662174
23D1670
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
ARRIS NODA 71237184
SS-1 23D1670-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SS-2 23D1670-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SS-3 23D1670-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SS-4 23D1670-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SS-5 23D1670-05 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
Page 3 of 22
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 4 of 22
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 4/13/2023 12:10
[TOC_2]23D1670-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.03
Petroleum Hydrocarbons Analyses - VPH
ND 14 4/17/23 19:04 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 4/17/23 19:04 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 4/17/23 19:04 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 4/17/23 19:04 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 4/17/23 19:04 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)84.4 4/17/23 19:0470-130
2,5-Dibromotoluene (PID)83.6 4/17/23 19:0470-130
[TOC_1]Sample Results[TOC]
Page 5 of 22
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 4/13/2023 12:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.3 4/15/23 6:38 WDC% Wt 4/15/23SM 2540G1% Solids
Page 6 of 22
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 4/13/2023 12:25
[TOC_2]23D1670-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.25
Petroleum Hydrocarbons Analyses - VPH
ND 12 4/17/23 19:33 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 12 4/17/23 19:33 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 12 4/17/23 19:33 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 12 4/17/23 19:33 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 12 4/17/23 19:33 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)80.0 4/17/23 19:3370-130
2,5-Dibromotoluene (PID)82.3 4/17/23 19:3370-130
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-02
Field Sample #: SS-2
Sample Matrix: Soil
Sampled: 4/13/2023 12:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
83.5 4/15/23 6:38 WDC% Wt 4/15/23SM 2540G1% Solids
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-03
Field Sample #: SS-3
Sample Matrix: Soil
Sampled: 4/13/2023 12:35
[TOC_2]23D1670-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.04
Petroleum Hydrocarbons Analyses - VPH
ND 13 4/17/23 20:03 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 13 4/17/23 20:03 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 13 4/17/23 20:03 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 13 4/17/23 20:03 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 13 4/17/23 20:03 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)84.8 4/17/23 20:0370-130
2,5-Dibromotoluene (PID)84.1 4/17/23 20:0370-130
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-03
Field Sample #: SS-3
Sample Matrix: Soil
Sampled: 4/13/2023 12:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.1 4/15/23 6:38 WDC% Wt 4/15/23SM 2540G1% Solids
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-04
Field Sample #: SS-4
Sample Matrix: Soil
Sampled: 4/13/2023 12:40
[TOC_2]23D1670-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.11
Petroleum Hydrocarbons Analyses - VPH
ND 14 4/17/23 20:32 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 4/17/23 20:32 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 4/17/23 20:32 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 4/17/23 20:32 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 4/17/23 20:32 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)80.4 4/17/23 20:3270-130
2,5-Dibromotoluene (PID)85.0 4/17/23 20:3270-130
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-04
Field Sample #: SS-4
Sample Matrix: Soil
Sampled: 4/13/2023 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.7 4/15/23 6:38 WDC% Wt 4/15/23SM 2540G1% Solids
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-05
Field Sample #: SS-5
Sample Matrix: Soil
Sampled: 4/13/2023 12:50
[TOC_2]23D1670-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.81
Petroleum Hydrocarbons Analyses - VPH
ND 16 4/17/23 21:02 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 16 4/17/23 21:02 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 16 4/17/23 21:02 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 16 4/17/23 21:02 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 16 4/17/23 21:02 EEHmg/Kg dry 4/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)93.0 4/17/23 21:0270-130
2,5-Dibromotoluene (PID)94.0 4/17/23 21:0270-130
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Date Received: 4/14/2023
Work Order: 23D1670Sample Description:Project Location: ARRIS NODA 71237184
Sample ID: 23D1670-05
Field Sample #: SS-5
Sample Matrix: Soil
Sampled: 4/13/2023 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
84.7 4/15/23 6:38 WDC% Wt 4/15/23SM 2540G1% Solids
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Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B337372 04/17/2310.3 11.823D1670-01 [SS-1]
B337372 04/17/2312.5 12.123D1670-02 [SS-2]
B337372 04/17/2310.4 11.623D1670-03 [SS-3]
B337372 04/17/2311.1 12.123D1670-04 [SS-4]
B337372 04/17/238.06 11.223D1670-05 [SS-5]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B337296 04/15/2323D1670-01 [SS-1]
B337296 04/15/2323D1670-02 [SS-2]
B337296 04/15/2323D1670-03 [SS-3]
B337296 04/15/2323D1670-04 [SS-4]
B337296 04/15/2323D1670-05 [SS-5]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B337372 - MA VPH
[TOC_3]B337372[TOC]
Blank (B337372-BLK1) Prepared & Analyzed: 04/17/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)81.732.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)81.632.7
LCS (B337372-BS1) Prepared & Analyzed: 04/17/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-13098.57.39
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301047.79
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301102.74
Benzene mg/Kg wet0.050 2.50 70-1301112.77
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301112.78
Decane mg/Kg wet0.050 2.50 70-13087.42.18
Ethylbenzene mg/Kg wet0.050 2.50 70-1301122.80
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301102.75
2-Methylpentane mg/Kg wet0.050 2.50 70-1301052.62
Naphthalene mg/Kg wet0.50 2.50 70-13093.82.34
Nonane mg/Kg wet0.050 2.50 30-1301132.82
Pentane mg/Kg wet0.050 2.50 70-13094.12.35
Toluene mg/Kg wet0.050 2.50 70-1301112.77
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301102.74
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-13096.52.41
m+p Xylene mg/Kg wet0.10 5.00 70-1301125.60
o-Xylene mg/Kg wet0.050 2.50 70-1301142.84
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)98.639.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)99.239.7
[TOC_1]QC Data[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B337372 - MA VPH
LCS Dup (B337372-BSD1) Prepared & Analyzed: 04/17/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130102 3.277.63
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130106 2.357.97
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130112 2.422.81
Benzene mg/Kg wet0.050 2.50 2570-130113 1.902.82
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130114 2.622.86
Decane mg/Kg wet0.050 2.50 2570-13090.5 3.492.26
Ethylbenzene mg/Kg wet0.050 2.50 2570-130114 1.552.84
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130111 1.372.78
2-Methylpentane mg/Kg wet0.050 2.50 2570-130107 2.202.68
Naphthalene mg/Kg wet0.50 2.50 2570-130101 7.602.53
Nonane mg/Kg wet0.050 2.50 2530-130114 1.182.85
Pentane mg/Kg wet0.050 2.50 2570-13097.0 3.082.43
Toluene mg/Kg wet0.050 2.50 2570-130113 1.712.82
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-130112 2.422.81
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-130101 4.592.53
m+p Xylene mg/Kg wet0.10 5.00 2570-130114 1.805.70
o-Xylene mg/Kg wet0.050 2.50 2570-130115 1.592.88
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10040.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10341.1
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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