MO-28535_47783_CA_LSA_20211111

Limited Site Assessment Report
Former Snappy Food Mart (NCDEQ # 47783)
10100 Moores Chapel Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
PREPARED FOR:
LURE
10100 Moores Chapel Road
Charlotte, North Carolina 28214
PREPARED BY:
S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, North Carolina
November 9, 2021
S&ME, Inc. | 9751 Southern Pine Boulevard | Charlotte, NC 28273 | p 704.523.4726 | www.smeinc.com
November 9, 2021
LURE
10100 Moores Chapel Road
Charlotte, North Carolina 28214
Attention: Mr. Ehab Aziz
Reference: Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
S&ME, Inc. Geology License Certification No. C-145
Dear Mr. Aziz:
S&ME, Inc. (S&ME) is providing this report to summarize the receptor survey and limited soil and groundwater
assessment services performed at the above-referenced property. These services were performed in general
accordance with S&ME Proposal No. 211105A dated June 3, 2021. S&ME appreciates the opportunity to provide
environmental services for this project. Please contact us at your convenience if there are questions regarding the
information contained in this document.
Sincerely,
S&ME, Inc.
James Wellons, P.G. Tom Raymond, P.E.
Project Manager Senior Engineer/Senior Reviewer
[e-mail] [e-mail]
Attachment: Limited Site Assessment Report
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 i
Table of Contents
1.0 Site Identification and Contract Information.............................................................. 1
1.1 Site Identification Information...................................................................................................... 1
1.2 UST Contact Information .............................................................................................................. 1
1.3 Release Information ....................................................................................................................... 1
1.4 Certification ..................................................................................................................................... 2
2.0 Executive Summary .......................................................................................................... 3
3.0 Site History and Characterization ................................................................................. 4
3.1 Property Information ..................................................................................................................... 4
3.2 Project Background ........................................................................................................................ 4
3.3 UST Owner and Operator Information ....................................................................................... 5
3.4 Non-UST Information .................................................................................................................... 5
3.5 Site Characteristics ......................................................................................................................... 5
4.0 Risk Characterization ....................................................................................................... 6
5.0 Monitoring Well Installation .......................................................................................... 6
5.1 Monitoring Well Installation ......................................................................................................... 6
5.2 Soil Screening Activities ................................................................................................................ 7
6.0 Media Sampling Methodologies ................................................................................... 8
6.1 Soil Sampling .................................................................................................................................. 8
6.2 Groundwater Sampling ................................................................................................................. 8
7.0 Laboratory Analytical Results ........................................................................................ 8
7.1 Soil Analytical Results ................................................................................................................... 8
7.2 Groundwater Analytical Results .................................................................................................. 9
8.0 Free Product Investigation and Recovery Report ....................................................... 9
9.0 Receptor Information ....................................................................................................... 9
9.1 Water Supply Well Survey ............................................................................................................ 9
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 ii
9.2 Public Water Supplies .................................................................................................................... 9
9.3 Surface Water .................................................................................................................................. 9
9.4 Wellhead Protection Areas ............................................................................................................ 9
9.5 Property Use .................................................................................................................................... 9
9.6 Subsurface Structures .................................................................................................................. 10
9.7 Property Owners and Occupants ............................................................................................... 10
10.0 Site Geology and Hydrogeology .................................................................................. 10
10.1 Soil .................................................................................................................................................. 10
10.2 Groundwater ................................................................................................................................. 10
11.0 Conclusion ........................................................................................................................ 10
12.0 Sole Use Statement ......................................................................................................... 11
13.0 Limitations........................................................................................................................ 11
14.0 References ......................................................................................................................... 11
Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Receptor Survey Information
Appendix IV – Limited Site Assessment Risk Classification and Land Use Form
Appendix V – Site Photographs
Appendix VI – Monitoring Well Construction Information
Appendix VII – Laboratory Reports
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 1
1.0 Site Identification and Contract Information
The following information gives more detail as to the site; ownership, operator, and UST release information;
contacts; and report certification.
1.1 Site Identification Information
Date of Report:
Facility I.D. 31651 North Carolina Department of Environmental Quality (NCCDEQ) Incident No.: 47783
Site Risk: High Site Rank: TBD Land Use Category: Commercial
Site Name: Snappy Food Mart (former)
Site Address 10100 Moores Chapel Road
City/Town: Charlotte Zip Code: 28214 County: Mecklenburg
Description of Geographical Data: Location of former gasoline dispensers
Location Method: Google Earth
Latitude: 35.274753º N Longitude: -80.970128º W
1.2 UST Contact Information
UST Owner/Operator: Handy Dandy, Inc., a.k.a. Handy Dandy Food Stores, Inc. (no longer exists)
Property Owner: Costar, LLC
Address: 10100 Moores Chapel Road, Charlotte, NC 28214
Property Occupant: LURE, LLC
Address: 10100 Moores Chapel Road, Charlotte, NC 28214
1.3 Release Information
Date Discovered: March 31, 2021
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Unknown (likely gasoline lines)
Sizes and contents from which the release occurred: Unknown
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 3
2.0 Executive Summary
The subject property is addressed as 10100 Moores Chapel Road in Charlotte, Mecklenburg County, North
Carolina. The property is owned by Costar, LLC, and is occupied by LURE, LLC. Between March 30, 2021 and April
1, 2021, S&ME observed Contaminant Control, Inc. (CCI) during the removal of concrete, asphalt, and overburden
to expose the underground storage tanks (USTs) and product piping. S&ME observed staining and petroleum
odors following removal of the asphalt/concrete surfaces around the USTs and product piping. On March 31,
2021, CCI removed the USTs from the ground following UST vapor screening and Fire Marshal approval. Between
March 31, 2021 and April 1, 2021, 209.16 tons of petroleum-impacted soils were transported off site for disposal
at AES. Multiple target analytes were detected in sidewall soil samples and base samples associated with the
gasoline UST basin abatement actions at concentrations that exceed the Soil-to-Water Maximum Soil
Contaminant Concentrations (MSCCs). Multiple target analytes were detected in sidewall soil samples associated
with the gasoline UST basin abatement actions at concentrations that exceed the Residential MSCCs. The
concentration of naphthalene detected in sidewall samples SW-1A and SW-4A exceeded the
Industrial/Commercial MSCCs. On March 31, 2021, S&ME submitted a UST-61 form to the UST Section of the
NCDEQ, Mooresville Regional Office.
On May 26, 2021, LURE (Client) received a Notice of Regulatory Requirements (NORR) issued by the NCDEQ
requesting that a Phase I Limited Site Assessment (LSA) be performed.
On March 23, 2021, one monitoring well (identified as MW-1) was installed on the subject property to assess for
possible soil and groundwater contamination. Soil samples were collected from the 15-feet below ground surface
(ft bgs)., 25-ft bgs, and 35-ft bgs intervals and submitted for laboratory analysis. A groundwater sample was
collected and submitted for laboratory analyses.
Soil Sample Results: Several volatile organic compound (VOC) target analytes were detected at
concentrations that exceed the respective NCDEQs UST Soil-to-Water Maximum Soil Contaminant
Concentrations.
Groundwater Sample Results: Fifteen target petroleum constituents exceeded the respective NCDEQ 15A
NCAC 02L .0202 Standards (2L Standards). Four target constituents exceeded the respective NCDEQ UST
Gross Contaminant Levels (GCLs).
On June 23, 2021, S&ME conducted a receptor survey within 1,500 feet of the source area and mailed water
supply well information forms to select owners of properties within a 500-foot radius. S&ME identified water
supply wells within 1,500 feet of the subject property boundary. According to the City of Charlotte. Charlotte
Water Division, potable water is available to the properties within 1,500 feet of the subject property by Charlotte
Water. According to a review of the NCDEQ Division of Water Resources (DWR) Surface Waters Classification
website, no surface water bodies are located within 1,500 feet of the source area.
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 4
Table 2-1: Receptor Information Summary
Based on the collected information presented on the Limited Site Assessment Risk Classification and Land Use
Form, S&ME recommends a priority site ranking of “High Risk”. An “Industrial/Commercial” site land use
classification is recommended for the subject site.
3.0 Site History and Characterization
3.1 Property Information
The subject property is comprised of one parcel located west of the intersection of Moores Chapel Road and
Belmeade Drive in Charlotte, North Carolina. Based on a review of the Mecklenburg County Polaris 3G website,
the subject property totals 1.04 acres in size and the parcel is identified by parcel identification number (PIN)
05307120.
The approximate location of the subject site is indicated on Figure 1, Appendix I. A topographic map of the site
vicinity is provided as Figure 2, Appendix I. The site and approximate property lines are depicted in Figure 3,
Appendix I
3.2 Project Background
Between March 30, 2021 and April 1, 2021, S&ME observed Contaminant Control, Inc. (CCI) during the removal of
concrete, asphalt, and overburden to expose the USTs and product piping. S&ME observed staining and
petroleum odors following removal of the asphalt/concrete surfaces around the USTs and product piping. On
March 31, 2021, CCI removed the USTs from the ground following UST vapor screening and Fire Marshal approval.
S&ME did not observe holes in the USTs following removal. The concrete/asphalt, recovered liquids, USTs, and
product piping were removed from the site for disposal by CCI. Confirmatory soil samples were collected from
beneath the USTs, associated product lines, and dispensers. Total Petroleum Hydrocarbons (TPH) – Diesel Range
Organic (DRO) and/or TPH-Gasoline Range Organics (GRO) were reported at concentrations above their
respective action levels beneath UST-1 (diesel), the diesel product line and dispenser, and UST-2 and UST-3
(gasoline).
Between March 31, 2021 and April 1, 2021, S&ME observed over-excavation activities of petroleum-impacted soils
within the basin of the gasoline USTs. Due to elevated PID readings and since the initial abatement actions of
petroleum-impacted soil may not lead directly to closure of the subject incident, over-excavation of the
petroleum-impacted soils was discontinued. Risk-based samples were collected from the base and sidewalls of
Distance
from Source
(Feet)
Municipal
Water
Available
Active
Drinking Water
Wells
Unknown
Use Water
Wells
Inactive
Drinking
Water Wells
Irrigation
Wells
Surface
Water
Bodies
0 – 500 Yes 2 2 1 0 0
500 – 1,000 Yes 2 2 1 1 0
1,000 – 1,500 Yes 0 1 0 0 0
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 5
the excavation. Between March 31, 2021 and April 1, 2021, 209.16 tons of petroleum-impacted soils were
transported off site for disposal at Alternative Energy Solutions on NC, LLC (AES) in Thomasville, North Carolina.
Multiple target analytes were detected in sidewall soil samples and base samples associated with the gasoline UST
basin abatement actions at concentrations that exceed the Soil-to-Water Maximum Soil Contaminant
Concentrations (MSCCs). Multiple target analytes were detected in sidewall soil samples associated with the
gasoline UST basin abatement actions at concentrations that exceed the Residential MSCCs. The concentration of
naphthalene detected in sidewall samples SW-1A and SW-4A exceeded the Industrial/Commercial MSCCs. On
March 31, 2021, S&ME submitted a UST-61 form to the UST Section of the NCDEQ, MRO.
On May 26, 2021, LURE (Client) received a Notice of Regulatory Requirements (NORR) issued by the NCDEQ
requesting that a Phase I Limited Site Assessment (LSA) be performed. Upon receipt of the NORR, Mr. Aziz
contacted Mr. James Wellons of S&ME and requested a proposal to attempt closure of Incident# 47783 by
completing a Phase I LSA as requested by NCDEQ. LSAs involve gathering site specific information used to
determine the level of risk the incident poses to public and the environment. The risk information is used by
NCDEQ to determine if an incident may be eligible for no further action (NFA) required status, or if additional
measures are required to mitigate site risks, prior to eligibility for NFA status.
3.3 UST Owner and Operator Information
A January 26, 2021 email from Ms. Ruth Strauss of NCDEQ to Mr. Ehab Aziz (site owner) stated: “Based on our
records, the Permits & Inspection Branch of the UST Section finds that Costar, LLC is not a tank owner nor a tank
operator. Costar owns the property in which the UST systems are located. Because Costar is not a tank owner or
a tank operator, we have not invoiced it for tank fees nor enforced against it to bring the UST systems into
compliance. Handy Dandy, Inc. also known as Handy Dandy Food Stores Inc., was the last owner of the
tanks. Handy Dandy, Inc. did not own the property and no longer exists”.
3.4 Non-UST Information
Aboveground storage tanks were not present at the subject property at the time of the UST closure assessment
and Limited Site Assessment.
3.5 Site Characteristics
Land Use: The site is currently occupied by a convenience store with attached office and asphalt paved
parking lot and zoned as B-1; business (neighborhood business).
Land Use of Surrounding Area: The site is located in a mixed single-family dwelling and business
(neighborhood business-conditional zoning) area. The nearest residential dwelling is approximately 250
feet northwest of the source area.
Topography: Based upon the topographic map reviewed (Figure 2, Appendix I), the area of the subject
property generally slopes downward to the west. The subject property has a surface elevation of
approximately 760 feet above Mean Sea Level (MSL). Based on observations during the site visit, surface
drainage appears to drain to the west.
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 6
Surface Water: Based on a review of the Mecklenburg County Polaris 3G website
(https://polaris3g.mecklenburgcountync.gov/), the nearest downgradient surface water body is an
unnamed tributary to Long Creek Tributary 1 that is located approximately 2,045 feet west of the release
location.
Regional Geology: The site is within the Charlotte Belt Geologic Province of North Carolina and is
underlain by metamorphosed quartz diorite; foliated to massive.
Potential Receptors: Based on site observations, one unused water supply well is located on the subject
property. Eight water supply wells were identified within a 1,500-foot radius of the subject property. As
previously discussed, no downgradient surface water bodies are located within 1,500 feet of the subject
area.
4.0 Risk Characterization
Twelve water supply wells or other potential receptors were identified within 1,500 feet of the release area. The
surrounding area in which the receptor survey was performed is shown on Figure 4, Appendix I. A list of
identified parcels and property owners within 500 feet of the source area is included in Table 1, Appendix II.
Water supply well owner information is provided in Table 2, Appendix II. Receptor survey documents, including a
list of, certified mail receipts, delivery notifications and returned Water Supply Information forms are included in
Appendix III.
The subject site is located within Charlotte, North Carolina and is zoned Business (neighborhood business).
Properties within 1,500 feet of the subject property boundary are zoned as Single Family and Business
(neighborhood business, conditional zoning). The NCDEQ "Limited Site Assessment Risk Classification and Land
Use Form" is included in Appendix IV.
5.0 Monitoring Well Installation
S&ME contacted North Carolina One Call public utility locating service to identify public underground utilities that
were within the proposed work area. Additionally, S&ME contracted a private utility locator to identify private
underground utilities within the proposed work area. A Site-Specific Health and Safety Plan was prepared,
following the requirements of CFR 1910.120 Hazardous Waste Operations and Emergency Response Standard
(HAZWOPER) rule of the protection of workers who are exposed or potentially exposed to hazardous substances.
The scope of services was performed in general accordance with the NCDEQ Division of Waste Management
(DWM) – UST Section Assessment Guidelines: Petroleum and Hazardous Substance UST Releases, Petroleum Non-
UST Releases, January 18, 2021 Version, hereby referred to as the Guidelines.
5.1 Monitoring Well Installation
On June 23, 2021, one monitoring well (identified as MW-1) was installed on the subject property to assess for
possible petroleum groundwater contamination. S&ME was present on the subject property with a North Carolina
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 7
licensed well driller with Ransier Environmental Drilling, Inc. (REDI). An F3500 Foremost Mobile drill rig was used
with a 6-inch diameter, solid-flight augers for the installation of the monitoring well. Note that Subsurface
Investigation Permit (SIP) No. 70002895 was issued by Mecklenburg County Health Department, Groundwater and
Wastewater services prior to initiation of drilling. A copy of the SIP is included in Appendix VI.
The well was installed for the collection of shallow groundwater located above consolidated material at the site.
No drilling within rock/deep aquifer was performed at the monitoring well location. The monitoring well was
constructed of 2-inch diameter schedule 40, flush-thread, polyvinyl chloride (PVC) pipe installed in the 6-inch
diameter borehole. The lower portion of the well consisted of a 15-foot long manufactured well screen with
0.010-inch slots. Filter sand was placed to from 50 ft bgs to 33-ft bgs. A bentonite seal was placed from 33 ft bgs
to 31-ft bgs. Concrete grout was placed from 31-ft bgs to the existing ground surface. The well was completed
with a 2-foot by 2-foot concrete pad and 8-inch flush mount manhole. The approximate location of the
monitoring well is depicted in Figure 3,Appendix I. Site photographs of the monitoring well location is included
in Appendix V. The well construction data is summarized in Table 3, Appendix II and the well construction log is
included in Appendix VI.
5.2 Soil Screening Activities
Prior to well installation, a soil boring was advanced using a 2 ¼-inch outside diameter (OD) Macro-Core®
sampler and direct push techniques. During the advancement of the soil boring, soil profiles were contained in the
Macro-Core® sampler’s acetate sleeves and observed by S&ME personnel for soil lithology, the presence of
petroleum odors, staining, and evidence of groundwater.
Soil samples were collected from each acetate sleave at approximate 5-foot intervals. The soils collected were
placed in a sealable plastic bag and screened for the presence of volatile organic compounds (VOCs) utilizing a
calibrated MiniRAE 3000 Photoionization Detector (PID).
Volatile organic vapors were detected during field screening of the collected soil samples. The measured PID
results are included in Table 5-1 below.
Table 5-1: PID Screening Results
Soil Screening Results
Depth (ft-bgs) PID Readings (ppm)
5 No sample (backfill)
10 No sample (backfill)
15 11,221
25 11,777
35 11,066
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Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 8
6.0 Media Sampling Methodologies
6.1 Soil Sampling
On June 23, 2021, soil samples were collected at approximate 5-foot intervals from approximately 10 ft bgs to 40
ft bgs using a direct-push Macro-Core® sampler through hollow-stem augers. The samples were split and placed
in labeled zip top plastic bags. One aliquot from each sample was immediately placed in a cooler of ice, while the
other was allowed time to volatilize and field PID screenings were performed. Indication of groundwater were
observed in the 40 ft bgs Macro-Core® sample.
The collected soil samples from the 15-ft bgs, 25-ft bgs, and 35-ft bgs intervals were placed into laboratory-
supplied sample containers, placed in a cooler of ice, and delivered by S&ME personnel under chain of custody
procedures to TestAmerica Laboratories, Inc. dba Eurofins TestAmerica (Eurofins) in Pensacola, Florida to be
analyzed for VOCs by EPA Method 8260, Semi-VOCs (SVOCs) by EPA Method 8270, volatile petroleum
hydrocarbons (VPH) and extractable petroleum hydrocarbons by the Massachusetts Department of Environmental
Protection (MADEP) methods.
6.2 Groundwater Sampling
On June 24, 2021, prior to groundwater sampling activities, S&ME measured the depth to the water (DTW) within
monitor well MW-1 using an electronic water level probe at 36.60 feet below top of casing (BTOC). The depth to
groundwater measurements at the time of sampling is included in Table 3, Appendix II.
After measuring the DTW, S&ME purged MW-1 dry two times using a new disposable polyethylene bailer. After
purging, the well was allowed to recharge prior to sample collection. The groundwater sample was collected,
placed directly from the bailer into laboratory provided sample containers, and placed in a cooler of ice. The
groundwater sample was transported by S&ME personnel under chain of custody procedures to Eurofins. The
groundwater sample was analyzed for VOCs by Standard Method 6200B and SVOCs (base/neutrals and acids plus
10 largest non-target peaks) by EPA Method 625.1, VPH and EPH by the MADEP methods, and EDB by EPA
Method 504.1. The approximate location of MW-1 is depicted in Figure 3, Appendix I.
7.0 Laboratory Analytical Results
A qualitative review of the data was performed to verify that the detected concentrations in the laboratory report
were of known quality. A formal, quantitative data validation was not performed. Laboratory-assigned data
qualifiers were evaluated to verify that rejected or unsupportable data were not included in the dataset. Quality
control data provided in the laboratory reports were also reviewed. No rejected or otherwise unacceptable quality
data was reported from the laboratory.
7.1 Soil Analytical Results
Several VOC target analytes were detected at concentrations that exceed the respective NCDEQs UST Soil-to-
Water Maximum Soil Contaminant Concentrations.
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 9
A summary of the laboratory analytical results for the soil samples is presented in Table 4, Appendix II and
Figure 3, Appendix I. The laboratory report is included in Appendix VII.
7.2 Groundwater Analytical Results
Fifteen target petroleum constituents exceeded the respective NCDEQ 15A NCAC 02L .0202 Standards (2L
Standards). Four target constituents exceeded the respective NCDEQ UST Gross Contaminant Levels (GCLs). A
summary of the laboratory analytical results for the groundwater sample is presented in Table 5, Appendix II and
Figure 3, Appendix I. The laboratory reports are included in Appendix VII.
8.0 Free Product Investigation and Recovery Report
No free product was encountered during these assessment activities.
9.0 Receptor Information
9.1 Water Supply Well Survey
On June 24, 2021, S&ME conducted a visual water supply well survey. The survey included a visual reconnaissance
by vehicle to observe for the presence of suspected water meters and water well structures for properties within
1,500 feet of the subject property boundary. During the receptor survey, S&ME identified water supply wells
within 1,500 feet of the subject property boundary. Figure 4, Appendix I presents the receptor survey area.
9.2 Public Water Supplies
Based on visual observations of fire hydrants and water meters, in addition to data obtained from Mecklenburg
County GIS information, all properties within the within the 1,500-foot search radius surrounding the subject
property have access to drinking water from Charlotte Water.
9.3 Surface Water
Based on a review of the Mecklenburg County Polaris 3G website (https://polaris3g.mecklenburgcountync.gov/),
the nearest downgradient surface water body is an unnamed tributary to Long Creek Tributary 1 that is located
approximately 2,045 feet west of the release location.
9.4 Wellhead Protection Areas
According to a review of the NCDEQ DWR Wellhead Protection Areas website, no Wellhead Protection Areas were
identified on the website’s map within 1,500 feet of the release source area.
9.5 Property Use
The subject property is occupied with a convenience store with attached office and asphalt paved parking.
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 10
9.6 Subsurface Structures
Basements were not observed in off-site residential structured structures within 500 feet of the release source
area.
9.7 Property Owners and Occupants
The subject property is currently owned by Costar, LLC.
10.0 Site Geology and Hydrogeology
The site is located within the Charlotte Belt of the Piedmont Physiographic Province of North Carolina. Geologic
mapping by U.S. Geological Survey (USGS) indicates the underlying bedrock consists metamorphosed quartz
diorite; foliated to massive.
The Piedmont Province generally consists of well-rounded hills and ridges, which are dissected by a well-
developed system of draws and streams. The Piedmont Province is predominantly underlain by metamorphic rock
(formed by heat, pressure and/or chemical action) and igneous rock (formed directly from molten material), which
were initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks deposited in
the Piedmont Province during the Precambrian eras were the host for the metamorphism and were changed to
gneiss and schist. The more recent Paleozoic era had periods of igneous emplacement, with at least several
episodes of regional metamorphism resulting in the majority of the rock types seen today.
Groundwater is recharged by precipitation in the interstream areas. A part of the precipitation infiltrates through
the unsaturated zone to the water table, which normally occurs in saprolite. Groundwater is primarily stored in
void spaces in the saprolite with secondary storage in fractures within the bedrock. The groundwater flow
direction in the saprolite generally trends from topographic highs, or groundwater re-charge areas, toward
topographic lows where surface water bodies represent groundwater discharge points. Based on this general
trend, groundwater flow at the subject site is likely to the southwest.
10.1 Soil
During the drilling associated with the on-site monitoring well, the soil contained in the Macro-Core® sampler
consisted of tan/gray silty clay (weathered rock).
10.2 Groundwater
Based on the groundwater measurements collected by S&ME on June 24, 2021 in monitor well MW-1,
groundwater in the subject area is approximately 36-ft bgs.
11.0 Conclusion
Between March 30, 2021 and April 1, 2021, S&ME observed UST closure and over-excavation activities at the
subject site. Approximately 209 tons of petroleum-impacted soils were transported off site for disposal at AES in
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
November 9, 2021 11
Thomasville, North Carolina. Multiple target analytes were detected in sidewall soil samples and base samples
associated with the gasoline UST basin abatement actions at concentrations that exceed the Soil-to-Water MSCCs.
Multiple target analytes were detected in sidewall soil samples associated with the gasoline UST basin abatement
actions at concentrations that exceed the Residential MSCCs. The concentration of naphthalene detected in
sidewall samples SW-1A and SW-4A exceeded the Industrial/Commercial MSCCs. On March 31, 2021, S&ME
submitted a UST-61 form to the UST Section of the NCDEQ, MRO.
On May 26, 2021, LURE received a Notice of Regulatory Requirements (NORR) issued by the NCDEQ requesting
that a Phase I LSA be performed. Between June 23 and 24, 2021, soil and ground water samples were collected as
a part of Phase I LSA activities. Several VOC target analytes were detected at concentrations that exceed the
respective NCDEQs UST Soil-to-Water Maximum Soil Contaminant Concentrations. Fifteen target petroleum
constituents exceeded the respective NCDEQ 2L Standards. Four target constituents exceeded the respective
NCDEQ GCLs. Based on a June 24, 2021 visual water supply well survey and review of received water supply well
information forms, S&ME identified twelve water supply wells within 1,500 feet of the subject property boundary.
Based on the collected information presented on the Limited Site Assessment Risk Classification and Land Use
Form, S&ME recommends a priority site ranking of “High Risk”. An “Industrial/Commercial” site land use
classification is recommended for the subject site. Based on the data collected and reported herein, the site meets
the criteria for High-risk defined in 15A NCAC 02L .0406 and contaminant concentrations are in excess of
groundwater standards established under 15A NCAC 02L .0202 by a factor of 10 in the groundwater sample.
Therefore, additional monitoring wells are required. Off-property access may be required for additional well
installation.
12.0 Sole Use Statement
All materials and information used for this project were obtained by S&ME. This report is provided for the sole
use of LURE, LLC. for this project. Use of this report by any parties other than LURE, LLC. will be at such party's
sole risk. S&ME disclaims liability for any use of or reliance on this report by third parties.
13.0 Limitations
The assessment described herein represents the environmental conditions of the property at the locations
sampled and for the dates the soil and groundwater samples were collected for laboratory analysis. The
assessment data does not represent the future environmental conditions of the property and should not be
construed in this manner.
14.0 References
NCDEQ Division of Waste Management (DWM) – UST Section Assessment Guidelines: Petroleum and Hazardous
Substance UST Releases, Petroleum Non-UST Releases, January 18, 2021 Version.
Appendices
Appendix I – Figures
^_
^_Project Location
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 1.0 miles
4-27-21Drawing Path: T:\ENV\Projects\2021\211105 LURE_UST Removal_Moores Chapel Rd\GIS\1_vicinity.mxd plotted by DHomans 04-27-2021VICINITY MAP
³
REFERENCE: ESRI STREETMAP USA DATASETTHIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEYINFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: Sources: Esri, HERE, Garmin, USGS,Intermap, INCREMENT P, NRCan, Esri Japan, METI, EsriChina (Hong Kong), Esri Korea, Esri (Thailand), NGCC, (c)
0 1 2Miles
211105
FORMER SNAPPY FOOD MART10100 MOORES CHAPEL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
- NCDEQ No. 47783
^_
^_PROJECT LOCATION
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
21 " = 2,000 '
4-27-21Drawing Path: T:\ENV\Projects\2021\211105 LURE_UST Removal_Moores Chapel Rd\GIS\2_USGS TOPO.mxd plotted by DHomans 04-27-2021USGS TOPOGRAPHIC MAP
³
REFERENCE: USGS USA TOPO STREAMING DATASETGIS BASE LAYERS WERE OBTAINED FROM USGS NATIONAL MAP. THIS MAP IS FOR INFORMATIONALPURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASEDON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: USGS The National Map: NationalBoundaries Dataset, 3DEP Elevation Program, GeographicNames Information System, National Hydrography
0 2,000 4,000(FEET)
211105
FORMER SNAPPY FOOD MART10100 MOORES CHAPEL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
- NCDEQ No. 47783
USTs Removed in
March/April 2021
E
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ON RDN I-485 INNER HYS I-485 OUTER HYHUGUE W Y
M O O REBRO O K DR
I-485 RA1,500'1,500'1,000'500'
WSW-9
WSW-11 WSW-12
WSW-1(unused)
WSW-4 WSW-3
WSW-2
WSW-5
WSW-6
WSW-7
WSW-8
WSW-10
MeckCoGIS
Ð!G OBSERVED WATER SUPPLY WELLS●○W OBSERVED CITY WATER METERS
¬«OBSERVED FIRE HYDRANTS
E SOURCE
PROJECT PARCEL
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.4
1 " = 300 '
10-28-21
211105AFormer Snappy Food Mart10100 Moores Chapel RoadCharlotte, Mecklenburg County, North CarolinaDrawing Path: T:\ENV\Projects\2021\211105A LURE_Limited Site Assessment_Moores Chapel Rd\GIS\4_receptor.mxd plotted by DHomans 10-28-20210 300 600
(FEET)POTENTIAL RECEPTOR MAP³
REFERENCE: 2020 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM MECKLENBURG COUNTY. ALL FEATURELOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEYINFORMATION, UNLESS STATED OTHERWISE.- NCDEQ No. 47783
Appendix II – Tables
Parcel ID Owner Property Address Mailing Address
5307129 Patsy H Rorie & Richard E Rorie Belmeade Drive, Charlotte NC 28214 1400 Hawfield Road, Charlotte NC 28214
5549117 Dept of Transportation 10205 Moores Chapel Road, Charlotte NC 28214 PO Box 25201
5307120 C and D Franklin, Inc.10100 Moores Chapel Road, Charlotte NC 28214 235 River Loop Road
5307122 James Brown 10123 Amos Hoard Road, Charlotte NC 28214 10123 Amos Hoard Road, Charlotte NC 28214
5549115 JC Barefoot Properties of NC LLC 10109 Moores Chapel Road, Charlotte NC 28214 PO Box 19006, Charlotte NC 28214
5307119 Vu Hoang Cao & Thanh Loan Cao 10110 Moores Chapel Road, Charlotte NC 28214 2528 Bricker Drive, Charlotte NC 28214
5301305 Shelby Jean Cooper 3009 Belmeade Drive, Charlotte NC 28214 3009 Belmead Drive, Charlotte NC 28214
5301307 Edgar W Bullard & Trustees 3025 Belmeade Drive, Charlotte NC 28214 1600 Saint Francis Road C/O Betty Bullard Row, Greensboro, NC 27408
5307121 Charles & Judith Caldwell Irrevocable Family Trust & Leigh Ann Caldwell 3000 Belmeade Drive, Charlotte NC 28214 1801 Wildlife Club Road, Charlotte NC 28214
5307208 Shadybrook Baptist Church 2940 Belmeade Drive, Charlotte NC 28214 2940 Belmead Drive, Charlotte NC 28214
5301304 Camille T Jones & Arnold D Sr Jones 3001 Belmeade Drive, Charlotte NC 28214 3001 Belmead Drive, Charlotte NC 28214
5301306 Laura Bartels & Phillip M Hagood 3017 Belmeade Drive, Charlotte NC 28214 3017 Belmead Drive, Charlotte NC 28214
5301311 Stephen Lynn Brown & Lynette Elizbeth Brown Newton 1016 Moorebrook Drive, Charlotte NC 28214 901 Beechgrove Court, Charlotte NC 28212
5549112 David H Pippin & Marjorie J Pippin 1311 Rhyne Road, Charlotte NC 28214 1311 Rhyne Road, Charlotte NC 28214
5549113 JC Barefoot Properties of NC LLC 1319 Rhyne Road, Charlotte NC 28214 PO Box 19006, Charlotte NC 28219
5307117 Raymon L Auten 10200 Moores Chapel Road, Charlotte NC 28214 10200 Moores Chapel Road, Charlotte NC 28214
5549114 Jerry Barefoot 1407 Rhyne Road, Charlotte NC 28214 PO Box 19006, Charlotte NC 28219
5301310 Stephen Lynn Brown & Lynette Elizabeth Brown Newton 1022 Moorebrook Drive, Charlotte NC 28214 901 Beechgrove Court, Charlotte NC 28212
5301309 Cecil Oree Soles & Annie P Soles 1320 Rhyne Road, Charlotte NC 28214 1320 Rhyne Road, Charlotte NC 28214
5307472 Association Inc Belmeade Green Homeowners Tribune Drive, Charlotte NC 28214 PO Box 11906, Charlotte NC 28220
5307471 Antonio D Biggers & Tamira Biggers 410 Tribune Drive, Charlotte NC 28214 410 Tribune Drive, Charlotte NC 28214
5307128 Maribel Fonseca Penaloza & Jose Rigoberto Garcia Aguilar 10117 Belmeade Drive, Charlotte NC 28214 8642 Catfish Drive, Charlotte NC 28214
5549128 JC Barefoot Properties of NC, LLC Moores Chapel Road, Charlotte NC 28214 PO Box 19006, Charlotte NC 28219
5307118 Rachel Whitner Wingate 10132 Moores Chapel Road, Charlotte NC 28214 10132 Moores Chapel Road, Charlotte NC 28214
Table 1
Identified Properties Within 500' of Source Area
Snappy Food Mart (Former) - NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105A
Table 2
Water Supply Well Information
Well #Well Owner / User
(indicate which)Site Address Phone
Number
Latitude
(decimal)
Longitude
(decimal)Well Use
Well
Depth
(ft-BGS)
Type
of Well
Well
Casing
Depth
(ft-BGS)
Gradient
from
Source
(Up, Down, Cross)
WSW-1 Costar, LLC (owner)10100 Moores Chapel Road Not Provided 35.274617 -80.970481 Inactive Unknown Unknown Unknown 110 SW Down
WSW-2 Charles & Judith Caldwell
Irrevocable Family Trust (owner)3000 Belmead Drive 704.392.7176 35.275439 -80.970708 Active (drinking) Unknown Unknown Unknown 285 NW Cross
WSW-3 Rachel Wingate (owner/user) 10132 Moores Chapel Road Not Provided 35.273867 -80.971217 Unknown Unknown Unknown Unknown 465 SW Cross
WSW-4 Raymond Lauten (owner/user) 10200 Moores Chapel Road Not Provided 35.273794 -80.971279 Unknown Unknown Unknown Unknown 490 SW Cross
WSW-5 Cecil & Annie Soles (owner/user)1320 Rhyne Road Not Provided 35.275845 -80.969559 Unknown Unknown Unknown Unknown 415 NE Cross
WSW-6 Shelby Cooper
(owner/user)3009 Belmeade Drive Not Provided 35.276173 -80.970155 Active (irrigation) Unknown Unknown Unknown 505 N Cross
WSW-7 David & Marjorie Pippin
(owner/user)1311 Rhyne Road Not Provided 35.275045 -80.968236 Unknown Unknown Unknown Unknown 575 E Up
WSW-8 Stephen & Lynette Brown (owner) 1022 Moorebrook Drive Not Provided 35.276295 -80.969066 Inactive Unknown Unknown Unknown 625 NE Cross
WSW-9 Shadybrook Baptist Church
(owner/user)2940 Belmeade Drive Not Provided 35.27668 -80.97129 Unknown Unknown Unknown Unknown 760 NW Cross
WSW-10 Charles & Kenneth Dilling (owner) 1015 Moorebrook Drive Not Provided 35.277033 -80.968785 Unknown Unknown Unknown Unknown 900 NE Cross
WSW-11 James & Sherry Klutz (owner/user)2919 Belmeade Drive Not Provided 35.277265 -80.971389 Unknown Unknown Unknown Unknown 964 NW Cross
WSW-12 Charles & Kenneth Dilling (owner)1204 Rhyne Road Not Provided 35.277231 -80.96764 Unknown Unknown Unknown Unknown 1,150 NE Up
Notes:
Latitude and Longitude coordinates of water supply wells are estimated values
Only confirmed water supply wells are shown.
Water Supply well information obtained from responses of property owners as indicated on the letters received back from the well survey.
Groundwater flow direction has been estimated based on land elevations collected from Google Earth
Snappy Food Mart (Former) - NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105A
Distance (ft) /
Direction from
Source
Well ID Installation
Date
Well
Diameter
(inches)
Screened
Interval
(ft BGS)
Screen
Length
(feet)
Total Well
Depth
(ft BGS)
Top of
Casing
Elevation
Date
Measured
Depth to
Water
(ft-TOC)
MW-1 6/23/2021 2 35 - 50 15 50 NM 6/24/2021 36.60
Notes:
TOC = Top of Casing
BGS = Below Ground Surface
NM = Not Measured
Table 3
Monitoring Well Construction Information
Snappy Food Mart (Former) - NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105A
VOCs by 8260D
Depth
(ft-bgs)
Sample
Date
Sample
Time
n-ButylbenzeneAcenaphthyleneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenz(a,h)anthraceneFluorantheneFluorenePhenanthrenePyreneBenzo(a)anthracene1-Methylnaphthalene2-MethylnaphthaleneNaphthalene15 06/23/21 12:30 <0.92 14 3.4 J 18 5.6 J 2.2 J 48 18 7.2 130 47 43 73 120 <1.3 12 <1.6 5.9 J <11 0.09 0.066 0.0075 J 0.01 0.01 .0064 J 0.014 0.049 J 0.029 0.076 0.061 J 0.18 0.041 0.016 20 46 30 <740 260 3 1,530
25 06/23/21 12:55 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 2,800 2,740 <4 3,320
35 06/23/21 13:15 8.8 J 28 6.9 J 100 14 J 4.4 J 55 53 200 290 94 160 360 520 13 J 78 20 86 340 0.081 0.061 0.015 0.018 0.023 0.0092 0.024 0.0076 J 0.035 0.071 0.016 0.16 0.036 0.022 14 36 33 1,600 1430 12 1,990
NCDEQ UST Soil-to-Water MSCCs 0.0056 4.3 3.3 4.9 1.7 0.12 0.16 1.7 4.3 8.5 8.3 4.6 4.6 4.6 NSE NSE NSE NSE NSE 8.3 20 0.058 0.6 7,600 5.8 18 0.19 330 55 1.9 64 210 0.17 0.054 1.5 0.2 68 540 #31NCDEQ UST Residential MSCCs 18 626 626 1,560 1,564 100 313 626 1,200 782 782 3,129 3,129 3,129 NSE NSE NSE NSE NSE 930 930 0.66 6.6 469 66 663 0.66 625 625 6.63 469 469 6.6 22.8 62.5 5.5 625 1,560 31,200 469NCDEQ UST Industrial / Commercial MSCCs 164 16,350 16,350 40,000 40,880 4,000 8,176 16,350 32,000 20,440 20,440 81,760 81,760 81,760 NSE NSE NSE NSE NSE 14,000 14,000 3.2 32 7,000 327 3,270 3.27 9,340 9,340 32.7 7,000 7,000 32 112 934 27 9,340 23,300 467,000 7,000
Notes:
Value Concentration exceeds the Laboratory Reporting Limits
Value Concentration exceeds the NCDEQ UST Soil-to-Water MSCCs
Value Concentration exceeds the NCDEQ UST Residential MSCCs
Value Concentration exceeds the NCDEQ UST Industrial/Commercial MSCCs
Data presented in milligrams per kilogram (mg/kg)
NCDEQ = North Carolina Department of Environmental Quality
MSCC = Maximum Soil Contaminant Concentrations
VOC = Volatile Organic Compounds
SVOC = Semi-Volatile Organic Compounds
VPH/EPH = Volatile Petroleum Hydrocarbons / Extractable Petroleum Hydrocarbons by the MADEP Method
MADEP = Massachusetts Department of Environmental Protection
NSE = No Standard Established
# = Health based level >100%
NR = Not Requested
ft-bgs = Feet Below Ground Surface
<LRL = All reported analytes were detected at concentrations below the respective laboratory reporting limit
J = Analytes was detected at concentration between the method detection and laboratory reporting limits; the reported value is an estimate
B = The same analyte is found in the associated blank
Analytical Method VPH/EPH by MADEP Method
Table 4
Soil Analytical Results
Snappy Food Mart (Former) - NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
SVOCs by 8270E
C9-C22 AromaticsSample ID
MW-1 (15')
MW-1 (35')
Analytes of Potential Concern
BenzeneAcenaphthaleneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsMW-1 (25')sec-ButylbenzeneEthylbenzeneIsopropylbenzene4-IsopropyltolueneNaphthalenem-Xylene & p-XyleneTotal XylenesN-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzeneo-XylenesIndeno(1,2,3-cd)pyrene2-Methyl-2-propanolCyclohexaneMethylcyclohexaneHexanen-Heptane
Analytical Method EDB by
504.1
Date
Collected
Time
Collected
AcetoneBenzene2-Butanone (MEK)1,2-DichloroethaneDiisopropyl etherEthylbenzeneIsopropylbenzeneMethyl tert-butyl etherNaphthaleneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes, Total1,2-Dibromoethane (EDB)Benzo[a]pyreneBenzo[b]fluorantheneBenzo[k]fluorantheneButyl benzyl phthalateChrysene2,4-DimethylphenolFluoranthenePyreneNaphthaleneC19-C36 AliphaticsC9-C18 AliphaticsC11-C22 AromaticsC9-C10 AromaticsC5-C8 AliphaticsC9-C12 Aliphatics06/24/21 09:30 2,200 5,900 1,300 370 140 1,500 100 2,400 510 12,000 1,600 460 7,300 230 2 0.82 0.28 2.4 0.62 77 0.59 0.62 330 120 710 2,000 16,000 57,000 18,000
15A NCAC 02L .0202 (2L Standards)6,000 1 4,000 0.4 70 600 70 20 6 600 400 400 500 0.02 0.005 0.005 0.5 NSE 5 100 300 200 6 10,000 700 200 200 400 700
NCDEQ UST Gross Contamination Levels (GCLs)6,000,000 5,000 4,000,000 400 70,000 80,000 30,500 20,000 6,000 260,000 28,500 24,100 50,000 50 0.8 0.75 0.5 NSE 5 100,000 300 200 6,000 NSE NSE NSE NSE NSE NSE
Notes:
VOCs = Volatile Organic Compounds
SVOCs = Semi-Volatile Organic Compounds
Data presented in micrograms per liter (µg/L)
Value Concentration exceeds the Laboratory Reporting Limit
Value Concentration exceeds the 2L Standards
Value Concentration exceeds the NCDEQ UST GCLs
Analytes from the method suite that are not shown were not detected.
NSE = No Standard Established
NCDEQ = North Carolina Department of Environmental Quality
Sample ID
Analyte of Potential Concern
MW-1
Table 5
Groundwater Analytical Results
Snappy Food Mart (Former) - NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105A
VOCs by 6200 SVOCs by 625.1 VPH by MADEPEPH by MADEP
Appendix III – Receptor Survey Information
Appendix IV – Limited Site Assessment Risk Classification and
Land Use Form
Limited Site Assessment Report
Former Snappy Food Mart – NCDEQ No. 47783
10100 Moores Chapel Road, Charlotte, Mecklenburg County, NC
S&ME Project No. 211105
S&ME, Inc. | 44 Buck Shoals Road, Suite C-3 | Arden, NC 28704 | p 828.687.9080 | www.smeinc.com
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1.Has the release contaminated any water supply well including any well used for non-drinking purposes?
YES ☐ NO☒
2.Is a water supply well used for drinking water located within 1,000 feet of the source area of the release?
YES ☒ NO☐
3.Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water,
filling swimming pools) located within 250 feet of the source area of the release? YES ☒ NO☐
4.Does groundwater within 500 feet of the source area of the release have the potential for future use
(there is no other source of water supply other than the groundwater)? YES ☐ NO☒
5.Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the environment?
YES ☐ NO☒
If yes, describe.
6.Are there any other factors that would cause the release to pose an imminent danger to public health,
public safety, or the environment? YES ☐ NO☒
If yes, describe.
Intermediate Risk
7.Is a surface water body located within 500 feet of the source area of the release? YES ☐ NO☒
If YES, does the maximum groundwater contaminant concentration exceed the surface water quality
standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? YES ☐ NO☐
Limited Site Assessment Risk Classification and Land Use Form Page 2
S&ME, Inc.
8.Is the source area of the release located within an approved or planned wellhead protection area as
defined in 42 USC 300h-7(e)? YES ☐ NO☒
If yes, describe.
9.Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology
of North Carolina” published by the Department in 1985? YES ☐ NO☒
________________________________________________________________________________________________________
If YES, is the source area of the release located in an area in which there is recharge to an unconfined or
semi-confined deeper aquifer that is being used or may be used as a source of drinking water?
YES ☐ NO☐
If YES, describe.
________________________________________________________________________________________________________
10.Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels
(See Table 2.) established by the Department? YES ☒ NO☐
Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1.Does the property contain one or more primary or secondary residences (permanent or temporary)?
YES ☐ NO☒
Describe:
The property is occupied with a convenience store with attached office and asphalt paved parking.
2.Does the property contain a school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly? YES ☒ NO☐
Describe:
The property is occupied with a convenience store with attached office and asphalt paved parking.
3.Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.)
enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped?
YES ☒ NO☐
Describe:
The property is occupied with a convenience store with attached office and asphalt paved parking.
4.Do children visit the property? YES ☒ NO☐
Explain:
Children may visit the property to buy items at the convenience store.
Limited Site Assessment Risk Classification and Land Use Form Page 3
S&ME, Inc.
5.Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or
both)? YES ☐ NO☒
Explain.
Access to the property is not restricted due to operating as a convenience store.
6.Do pavement, buildings, or other structures cap the contaminated soil? YES ☒ NO☐
Describe:
A convenience store building and asphalt paved parking covers the majority of the subject site.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will
remain capped in the foreseeable future?
________________________________________________________________________________________________________________
7.What is the zoning status of the property?
Business (neighborhood business)
8.Is the use of the property likely to change in the next 20 years? YES ☐ NO☒
Explain.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property
containing source area of the release):
1.What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)?
A primary residence is located approximately 250 feet northwest of the source area.
2.What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly?
Shady Brook Baptist church is located approximately 365 feet to the northwest of the source location.
3.What is the zoning status of properties in the surrounding area?
Properties within 1,500 feet of the subject property boundary are zoned as mixed single-family dwelling
and business (neighborhood business-conditional zoning).
4.Briefly characterize the use and activities of the land in the surrounding area.
The surrounding land use is residential.
Appendix V – Site Photographs
Former Snappy Food Mart
10100 Moores Chapel Road
Charlotte, Mecklenburg County, NC
Project #: 211105A
Sheet 1 of 1
Photo 1 Date: June 23, 2021Photographer:M. BrundageLocation View of MW-1.
Remarks Facing north
Photo 2 Date: June 23, 2021Photographer:M. BrundageLocation View of MW-1.
Remarks Facing northeast
Appendix VI – Monitoring Well Construction Information
Well ID
MW-1
S&ME Staff
M Brundage
Drill Rig
Water Level at TOB (0.01 ft- bgs)Land Surface Elev. (0.01 ft)
Depth to Water (0.01 ft- BTOC)
Stickup Height - ft
TOC Relative to Ground 0.1 ft
0.1 to 35.0
35.0 to 50.0
Top of Seal - 31.0 0.1 ft-bgs
Top of Filter Pack - 33.0 0.1 ft-bgs
0.1 to 31.0
Top of Screen - 35.0 0.1 ft-bgs
31.0 to 33.0
Screened Interval -15.0 0.1 ft-bgs
33.0 to 50.0
Bottom of Screen - 50.0 0.1 ft-bgs
Bottom of Filter Pack - 50.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 50.0 0.1 ft-bgs
Form Revision Date:9/1/17 2:10 PM
TBD - To Be Determined
Notes: Soil boring performed utilizing Geoprobe® Macro-Core® direct-push methods prior to well installation.
Recovered soils were manually classified in the field and generally consisted of red tan clayey silty sand (Fill) to an
approximate depth of 9 ft-bgs underlain by dense residual soils generally consisting of brown tan fine sandy silt
with manganese staining.
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
Yes
BTOC - Below Top of Casing
Hollow Stem Auger
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
8-inch
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Project Name
Former Snappy Food Mart - Phase I LSA
Project Number
211105
WELL CONSTRUCTION DETAIL
50.0
44.40
Northing (0.1 ft)Date/Time
6/23/2021 / 1230
Total Well Depth (0.1 ft-bgs)
39.08 9/23/2021 / 1100
Ransier Environmental Drilling, Inc. (REDI)
Easting (0.1 ft)Date/Time
Installation Date
6/23/2021
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Mecklenburg Charlotte
License Number
3580-A
Well Permit Number
70002895
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Agent
6/14/2021
70002895
LURE
Ehab Aziz
704-506-6137
10100 Moores Chapel Road
Charlotte NC 28273
S&ME, Inc.
James Wellons
704-302-4399
9751 Southern Pine Blvd
Charlotte NC 28277
LURE
05307120
10100 MOORES CHAPEL RD
CHARLOTTE NC 28214
Appendix VII – Laboratory Report
ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-205219-1
Client Project/Site: LURE (Moores Chapel Rd.)
For:
S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, North Carolina 28273
Attn: James Wellons
Authorized for release by:
7/12/2021 12:01:02 PM
John Andros, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Laboratory Job ID: 400-205219-1
Page 2 of 69 Eurofins TestAmerica, Pensacola7/12/2021
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .69
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Case Narrative
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Job ID: 400-205219-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-205219-1
Comments
No additional comments.
Receipt
The samples were received on 6/26/2021 9:09 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 5.5º C.
GC/MS VOA
Method SM6200-B: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-1
(400-205219-4). Elevated reporting limits (RLs) are provided.
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-538241 recovered above the upper control limit for
1,1,1,2-Tetrachloroethane, 1,1,1-Trichloroethane, 1,1,2-Trichloro-1,2,2-trifluoroethane, 1,2-Dichloroethane, 2,2-Dichloropropane,
2-Butanone (MEK), 2-Hexanone, Acetone, Carbon tetrachloride, Hexachlorobutadiene, trans-1,4-Dichloro-2-butene and
Trichlorofluoromethane. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been
reported.
Method 8260D: The laboratory control sample (LCS) for preparation batch 400-538282 and analytical batch 400-538241 recovered outside
control limits for the following analytes: 2-Hexanone and Acetone. These analytes were biased high in the LCS and were not detected in
the associated samples; therefore, the data have been reported.
Method 8260D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-538282 and analytical batch
400-538241 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits.
Method 8260D: The following samples were diluted to bring the concentration of target analytes within the calibration range: MW-1 (15')
(400-205219-1) and MW-1 (35') (400-205219-3). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270E LL: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-537669 and analytical batch
400-537623 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits.
Method 8270E LL: Three surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside
acceptance criteria without performing re-extraction/re-analysis. The following sample contained an allowable number of surrogate
compounds outside limits: MW-1 (15') (400-205219-1). These results have been reported and qualified.
Methods 8270D LL, 8270E LL: The following samples were diluted to bring the concentration of target analytes within the calibration
range: MW-1 (15') (400-205219-1) and MW-1 (35') (400-205219-3). Elevated reporting limits (RLs) are provided.
Method 8270E LL: The method blank for preparation batch 400-537669 and 400-537669 and analytical batch 400-537935 contained
Naphthalene, 1-Methylnaphthalene and 2-Methylnaphthalene above the reporting limit (RL). Associated sample(s) were not re-extracted
and/or re-analyzed because results were greater than 10X the value found in the method blank.
Methods 8270D LL, 8270E LL: The method blank for preparation batch 400-537669 and analytical batch 400-537935 contained
Benzo[a]anthracene, Benzo[b]fluoranthene and Benzo[k]fluoranthene above the method detection limit. This target analyte concentration
was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.
Method 625.1: Surrogate recovery for the following sample was outside control limits: MW-1 (400-205219-4). Evidence of matrix
Eurofins TestAmerica, PensacolaPage 3 of 69 7/12/2021
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Case Narrative
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Job ID: 400-205219-1 (Continued)
Laboratory: Eurofins TestAmerica, Pensacola (Continued)
interference is present; therefore, re-extraction and/or re-analysis was not performed.
Methods 625, 625.1: The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for preparation batch
400-537819 and analytical batch 400-537932 recovered outside control limits for the following analyte(s): Benzidine. Benzidine has been
identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed.
Methods 625, 625.1: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation
batch 400-537819 and analytical batch 400-537932 recovered outside control limits for the following analytes: Benzidine.
Methods 625, 625.1: The continuing calibration verification (CCV) associated with batch 400-537932 recovered outside acceptance
criteria, low biased, for Benzidine and Hexachlorocyclopentadiene. A reporting limit (RL) standard was analyzed, and the target analyte
was detected. Since the associated samples were non-detect for this analyte, the data have been reported.
Method 625.1: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-1
(400-205219-4). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
Method MAVPH: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-1
(400-205219-4). Elevated reporting limits (RLs) are provided.
Method MAVPH: The following samples were diluted to bring the concentration of target analytes within the calibration range: MW-1 (15')
(400-205219-1), MW-1 (25') (400-205219-2) and MW-1 (35') (400-205219-3). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method MA-EPH: The method blank for preparation batch 400-537628 and analytical batch 400-537957 contained C11-C22 Aromatics
above the reporting limit (RL). Associated sample(s) were not re-extracted and/or re-analyzed because results were greater than 10X the
value found in the method blank.
Method MA-EPH: The method blank for preparation batch 400-537738 and analytical batch 400-538108 contained C19-C36 Aliphatics
above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or
re-analysis of samples was not performed.
Methods 504.1, 8011: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 400-538325.
Method 504.1: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-1
(400-205219-4). Elevated reporting limits (RLs) are provided.
Method 504.1: The following sample required a dilution due to the nature of the sample matrix: MW-1 (400-205219-4). Because of this
dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful
information.
Method MA-EPH: The following samples were diluted to bring the concentration of target analytes within the calibration range: MW-1 (15')
(400-205219-1), MW-1 (25') (400-205219-2) and MW-1 (35') (400-205219-3). Elevated reporting limits (RLs) are provided.
Method MA-EPH: The following sample was diluted due to the nature of the sample matrix: MW-1 (25') (400-205219-2). Elevated reporting
limits (RLs) are provided.
Method MA-EPH: The matrix spike (MS) recovery for preparation batch 400-538248 and analytical batch 400-538514 was outside control
limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS)
recovery was within acceptance limits.
Eurofins TestAmerica, PensacolaPage 4 of 69 7/12/2021
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Case Narrative
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Job ID: 400-205219-1 (Continued)
Laboratory: Eurofins TestAmerica, Pensacola (Continued)
Method MA-EPH: The following sample was diluted due to the nature of the sample matrix: MW-1 (25') (400-205219-2). Elevated reporting
limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, PensacolaPage 5 of 69 7/12/2021
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Detection Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1
☼n-Butylbenzene
RL
6800 ug/Kg
MDL
1300
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1000140008260D
☼sec-Butylbenzene 6800 ug/Kg1300 Total/NA10003400J8260D
☼Ethylbenzene 6800 ug/Kg830 Total/NA1000180008260D
☼Isopropylbenzene 6800 ug/Kg930 Total/NA10005600J8260D
☼4-Isopropyltoluene 6800 ug/Kg1400 Total/NA10002200J8260D
☼Naphthalene 6800 ug/Kg2700 Total/NA1000480008260D
☼N-Propylbenzene 6800 ug/Kg1200 Total/NA1000180008260D
☼Toluene 6800 ug/Kg1400 Total/NA100072008260D
☼1,2,4-Trimethylbenzene 6800 ug/Kg1400 Total/NA10001300008260D
☼1,3,5-Trimethylbenzene 6800 ug/Kg1100 Total/NA1000470008260D
☼o-Xylene 6800 ug/Kg1400 Total/NA1000430008260D
☼m-Xylene & p-Xylene 6800 ug/Kg1800 Total/NA1000730008260D
☼Xylenes, Total 14000 ug/Kg2600 Total/NA10001200008260D
☼Methylcyclohexane 6800 ug/Kg2100 Total/NA1000120008260D
☼n-Heptane 6800 ug/Kg3400 Total/NA10005900J8260D
☼Acenaphthene 8.4 ug/Kg1.3 Total/NA1908270E LL
☼Acenaphthylene 8.4 ug/Kg1.3 Total/NA1668270E LL
☼Benzo[a]pyrene 8.4 ug/Kg1.3 Total/NA17.5 J 8270E LL
☼Benzo[b]fluoranthene 8.4 ug/Kg1.3 Total/NA110B8270E LL
☼Benzo[g,h,i]perylene 8.4 ug/Kg2.6 Total/NA1108270E LL
☼Benzo[k]fluoranthene 8.4 ug/Kg1.3 Total/NA16.4 J B 8270E LL
☼Chrysene 8.4 ug/Kg1.3 Total/NA1148270E LL
☼Dibenz(a,h)anthracene 8.4 ug/Kg2.6 Total/NA14.9 J 8270E LL
☼Fluoranthene 8.4 ug/Kg1.3 Total/NA1298270E LL
☼Fluorene 8.4 ug/Kg1.3 Total/NA1768270E LL
☼Indeno[1,2,3-cd]pyrene 8.4 ug/Kg2.6 Total/NA16.1 J 8270E LL
☼Phenanthrene 8.4 ug/Kg1.3 Total/NA11808270E LL
☼Pyrene 8.4 ug/Kg1.3 Total/NA1418270E LL
☼Benzo[a]anthracene 8.4 ug/Kg1.3 Total/NA116B8270E LL
☼1-Methylnaphthalene - DL 420 ug/Kg64 Total/NA5020000B8270E LL
☼2-Methylnaphthalene - DL 420 ug/Kg64 Total/NA5046000B8270E LL
☼Naphthalene - DL 420 ug/Kg64 Total/NA5030000B8270E LL
☼C9-C12 Aliphatics 380 mg/Kg380 Total/NA10000610MAVPH
☼C9-C10 Aromatics 200 mg/Kg200 Total/NA100001300MAVPH
☼C19-C36 Aliphatics 2.0 mg/Kg2.0 Total/NA13.0 MA-EPH
☼C11-C22 Aromatics 3.7 mg/Kg3.7 Total/NA1230F1MA-EPH
☼C9-C18 Aliphatics - DL 4.0 mg/Kg4.0 Total/NA2260MA-EPH
Client Sample ID: MW-1 (25')Lab Sample ID: 400-205219-2
☼C5-C8 Aliphatics
RL
890 mg/Kg
MDL
890
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100002800MAVPH
☼C9-C12 Aliphatics 460 mg/Kg460 Total/NA100002000MAVPH
☼C9-C10 Aromatics 250 mg/Kg250 Total/NA100002800MAVPH
☼C11-C22 Aromatics 7.5 mg/Kg7.5 Total/NA2520MA-EPH
☼C9-C18 Aliphatics - DL 8.0 mg/Kg8.0 Total/NA4740MA-EPH
Client Sample ID: MW-1 (35')Lab Sample ID: 400-205219-3
☼Benzene
RL
20000 ug/Kg
MDL
2700
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2500J88008260D
☼n-Butylbenzene 20000 ug/Kg3800 Total/NA2500280008260D
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 (35') (Continued)Lab Sample ID: 400-205219-3
☼sec-Butylbenzene
RL
20000 ug/Kg
MDL
3800
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2500J69008260D
☼Ethylbenzene 20000 ug/Kg2400 Total/NA25001000008260D
☼Isopropylbenzene 20000 ug/Kg2700 Total/NA250014000J8260D
☼4-Isopropyltoluene 20000 ug/Kg4000 Total/NA25004400J8260D
☼Naphthalene 20000 ug/Kg7900 Total/NA2500550008260D
☼N-Propylbenzene 20000 ug/Kg3600 Total/NA2500530008260D
☼Toluene 20000 ug/Kg4000 Total/NA25002000008260D
☼1,2,4-Trimethylbenzene 20000 ug/Kg4000 Total/NA25002900008260D
☼1,3,5-Trimethylbenzene 20000 ug/Kg3300 Total/NA2500940008260D
☼o-Xylene 20000 ug/Kg4000 Total/NA25001600008260D
☼m-Xylene & p-Xylene 20000 ug/Kg5100 Total/NA25003600008260D
☼Xylenes, Total 40000 ug/Kg7500 Total/NA25005200008260D
☼Cyclohexane 20000 ug/Kg3700 Total/NA250013000J8260D
☼Methylcyclohexane 20000 ug/Kg5900 Total/NA2500780008260D
☼Hexane 20000 ug/Kg4800 Total/NA2500200008260D
☼n-Heptane 20000 ug/Kg9900 Total/NA2500860008260D
☼2-Methyl-2-propanol 40000 ug/Kg32000 Total/NA25003400008260D
☼Acenaphthene 8.7 ug/Kg1.3 Total/NA1818270E LL
☼Acenaphthylene 8.7 ug/Kg1.3 Total/NA1618270E LL
☼Benzo[a]pyrene 8.7 ug/Kg1.3 Total/NA1158270E LL
☼Benzo[b]fluoranthene 8.7 ug/Kg1.3 Total/NA118B8270E LL
☼Benzo[g,h,i]perylene 8.7 ug/Kg2.6 Total/NA1238270E LL
☼Benzo[k]fluoranthene 8.7 ug/Kg1.3 Total/NA19.2 B 8270E LL
☼Chrysene 8.7 ug/Kg1.3 Total/NA1248270E LL
☼Dibenz(a,h)anthracene 8.7 ug/Kg2.6 Total/NA17.6 J 8270E LL
☼Fluoranthene 8.7 ug/Kg1.3 Total/NA1358270E LL
☼Fluorene 8.7 ug/Kg1.3 Total/NA1718270E LL
☼Indeno[1,2,3-cd]pyrene 8.7 ug/Kg2.6 Total/NA1168270E LL
☼Phenanthrene 8.7 ug/Kg1.3 Total/NA11608270E LL
☼Pyrene 8.7 ug/Kg1.3 Total/NA1368270E LL
☼Benzo[a]anthracene 8.7 ug/Kg1.3 Total/NA122B8270E LL
☼1-Methylnaphthalene - DL 430 ug/Kg66 Total/NA5014000B8270E LL
☼2-Methylnaphthalene - DL 430 ug/Kg66 Total/NA5036000B8270E LL
☼Naphthalene - DL 430 ug/Kg66 Total/NA5033000B8270E LL
☼C5-C8 Aliphatics 860 mg/Kg860 Total/NA100001600MAVPH
☼C9-C12 Aliphatics 440 mg/Kg440 Total/NA100001000MAVPH
☼C9-C10 Aromatics 240 mg/Kg240 Total/NA100001700MAVPH
☼C19-C36 Aliphatics 2.1 mg/Kg2.1 Total/NA112MA-EPH
☼C11-C22 Aromatics 4.0 mg/Kg4.0 Total/NA1290MA-EPH
☼C9-C18 Aliphatics - DL 11 mg/Kg11 Total/NA5430MA-EPH
Client Sample ID: MW-1 Lab Sample ID: 400-205219-4
Acetone
RL
2500 ug/L
MDL
1000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100J2200SM6200-B
Benzene 100 ug/L38 Total/NA1005900SM6200-B
2-Butanone (MEK)2500 ug/L260 Total/NA1001300JSM6200-B
1,2-Dibromoethane (EDB)100 ug/L50 Total/NA100220SM6200-B
1,2-Dichloroethane 100 ug/L50 Total/NA100370SM6200-B
Diisopropyl ether 100 ug/L70 Total/NA100140SM6200-B
Ethylbenzene 100 ug/L50 Total/NA1001500SM6200-B
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 (Continued)Lab Sample ID: 400-205219-4
Isopropylbenzene
RL
100 ug/L
MDL
53
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100100SM6200-B
Methyl tert-butyl ether 100 ug/L74 Total/NA1002400SM6200-B
m-Xylene & p-Xylene 500 ug/L160 Total/NA1005000SM6200-B
Naphthalene 100 ug/L100 Total/NA100510SM6200-B
N-Propylbenzene 100 ug/L69 Total/NA100260SM6200-B
o-Xylene 500 ug/L60 Total/NA1002400SM6200-B
Toluene 100 ug/L41 Total/NA10012000SM6200-B
1,2,4-Trimethylbenzene 100 ug/L82 Total/NA1001600SM6200-B
1,3,5-Trimethylbenzene 100 ug/L56 Total/NA100460SM6200-B
Xylenes, Total 1000 ug/L160 Total/NA1007300SM6200-B
Benzo[a]pyrene 7.6 ug/L0.091 Total/NA12.0 J 625.1
Benzo[b]fluoranthene 7.6 ug/L0.11 Total/NA10.82 J 625.1
Benzo[k]fluoranthene 7.6 ug/L0.12 Total/NA10.28 J 625.1
Butyl benzyl phthalate 7.6 ug/L0.14 Total/NA12.4 J 625.1
Chrysene 7.6 ug/L0.14 Total/NA10.62 J 625.1
2,4-Dimethylphenol 7.6 ug/L1.5 Total/NA177625.1
Fluoranthene 7.6 ug/L0.14 Total/NA10.59 J 625.1
Pyrene 7.6 ug/L0.16 Total/NA10.62 J 625.1
Naphthalene - DL 38 ug/L0.65 Total/NA5330625.1
C5-C8 Aliphatics 13 mg/L13 Total/NA50057MAVPH
C9-C12 Aliphatics 5.5 mg/L5.5 Total/NA50018MAVPH
C9-C10 Aromatics 3.5 mg/L3.5 Total/NA50016MAVPH
1,2-Dibromoethane (EDB)4.1 ug/L3.1 Total/NA200230p504.1
C9-C18 Aliphatics 0.15 mg/L0.11 Total/NA10.71 MA-EPH
C19-C36 Aliphatics 0.15 mg/L0.099 Total/NA10.12 J B MA-EPH
C11-C22 Aromatics 0.30 mg/L0.11 Total/NA12.0 MA-EPH
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
400-205219-1 MW-1 (15')Soil 06/23/21 12:30 06/26/21 09:09
400-205219-2 MW-1 (25')Soil 06/23/21 12:55 06/26/21 09:09
400-205219-3 MW-1 (35')Soil 06/23/21 13:15 06/26/21 09:09
400-205219-4 MW-1 Ground Water 06/24/21 09:30 06/26/21 09:09
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-1Client Sample ID: MW-1 (15')
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 18000 U *[phone] ug/Kg ☼07/06/21 08:47 07/06/21 19:41 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6800 920 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Benzene 920 U
6800 1800 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Bromobenzene 1800 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Chlorobromomethane 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Dichlorobromomethane 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Bromoform 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Bromomethane 3400 U
34000 8200 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼2-Butanone (MEK)8200 U
6800 1300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼n-Butylbenzene 14000
6800 1300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼sec-Butylbenzene 3400 J
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼tert-Butylbenzene 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Carbon disulfide 3400 U
6800 2300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Carbon tetrachloride 2300 U
6800 710 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Chlorobenzene 710 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Chloroethane 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Chloroform 3400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Chloromethane 1400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼3-Chloro-1-propene 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼2-Chlorotoluene 3400 U
6800 1300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼4-Chlorotoluene 1300 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Chlorodibromomethane 3400 U
6800 4500 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2-Dibromo-3-Chloropropane 4500 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Ethylene Dibromide 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Dibromomethane 3400 U
6800 970 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2-Dichlorobenzene 970 U
6800 1300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,3-Dichlorobenzene 1300 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,4-Dichlorobenzene 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼trans-1,4-Dichloro-2-butene 3400 U
6800 1800 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Dichlorodifluoromethane 1800 U
6800 1100 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1-Dichloroethane 1100 U
6800 1100 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2-Dichloroethane 1100 U
6800 1000 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼cis-1,2-Dichloroethene 1000 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼trans-1,2-Dichloroethene 3400 U
6800 1900 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2-Dichloroethene, Total 1900 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1-Dichloroethene 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2-Dichloropropane 3400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,3-Dichloropropane 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼2,2-Dichloropropane 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1-Dichloropropene 3400 U
6800 1600 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼cis-1,3-Dichloropropene 1600 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼trans-1,3-Dichloropropene 3400 U
6800 830 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Ethylbenzene 18000
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Ethyl methacrylate 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Hexachlorobutadiene 3400 U
34000 6800 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼2-Hexanone 6800 U *+
6800 4600 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Iodomethane 4600 U
34000 14000 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Isobutyl alcohol 14000 U
6800 930 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Isopropylbenzene 5600 J
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼4-Isopropyltoluene 2200 J
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-1Client Sample ID: MW-1 (15')
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 14000 U 21000 14000 ug/Kg ☼07/06/21 08:47 07/06/21 19:41 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
34000 6800 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼4-Methyl-2-pentanone (MIBK)6800 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Methyl tert-butyl ether 1400 U
6800 2700 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Naphthalene 48000
6800 1200 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼N-Propylbenzene 18000
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Styrene 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1,1,2-Tetrachloroethane 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1,2,2-Tetrachloroethane 3400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Tetrachloroethene 3400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Toluene 7200
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2,3-Trichlorobenzene 3400 U
6800 2700 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2,4-Trichlorobenzene 2700 U
6800 1500 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1,1-Trichloroethane 1500 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1,2-Trichloroethane 3400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Trichloroethene 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Trichlorofluoromethane 3400 U
6800 4100 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2,3-Trichloropropane 4100 U
6800 2700 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,1,2-Trichloro-1,2,2-trifluoroethane 2700 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,2,4-Trimethylbenzene 130000
6800 1100 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,3,5-Trimethylbenzene 47000
34000 12000 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Vinyl acetate 12000 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Vinyl chloride 3400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼o-Xylene 43000
6800 1800 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼m-Xylene & p-Xylene 73000
14000 2600 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Xylenes, Total 120000
6800 1300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Cyclohexane 1300 U
6800 6300 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Methyl acetate 6300 U
6800 2100 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Methylcyclohexane 12000
14000 6800 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Tetrahydrofuran 6800 U
6800 1600 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Hexane 1600 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Ethyl ether 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼n-Heptane 5900 J
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,3-Dichloropropene, Total 3400 U
6800 1400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Butadiene 1400 U
6800 3400 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼Dichlorofluoromethane 3400 U
14000 11000 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼2-Methyl-2-propanol 11000 U
680000 68000 ug/Kg 07/06/21 08:47 07/06/21 19:41 1000☼1,4-Dioxane 68000 U
4-Bromofluorobenzene 105 67-130 07/06/21 08:47 07/06/21 19:41 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 97 07/06/21 08:47 07/06/21 19:41 100077-127
Toluene-d8 (Surr)101 07/06/21 08:47 07/06/21 19:41 100076-127
1,2-Dichloroethane-d4 (Surr)113 07/06/21 08:47 07/06/21 19:41 100078-146
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene 90 8.4 1.3 ug/Kg ☼06/30/21 10:37 06/30/21 18:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Acenaphthylene 66
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Anthracene 1.3 U
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Benzo[a]pyrene 7.5 J
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-1Client Sample ID: MW-1 (15')
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
RL MDL
Benzo[b]fluoranthene 10 B 8.4 1.3 ug/Kg ☼06/30/21 10:37 06/30/21 18:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.4 2.6 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Benzo[g,h,i]perylene 10
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Benzo[k]fluoranthene 6.4 J B
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Chrysene 14
8.4 2.6 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Dibenz(a,h)anthracene 4.9 J
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Fluoranthene 29
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Fluorene 76
8.4 2.6 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Indeno[1,2,3-cd]pyrene 6.1 J
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Phenanthrene 180
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Pyrene 41
8.4 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:43 1☼Benzo[a]anthracene 16 B
2-Fluorobiphenyl 65 27-127 06/30/21 10:37 06/30/21 18:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)230 S1+06/30/21 10:37 06/30/21 18:43 115-136
Terphenyl-d14 (Surr)111 06/30/21 10:37 06/30/21 18:43 124-146
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level - DL
RL MDL
1-Methylnaphthalene 20000 B 420 64 ug/Kg ☼06/30/21 10:37 07/01/21 18:13 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
420 64 ug/Kg 06/30/21 10:37 07/01/21 18:13 50☼2-Methylnaphthalene 46000 B
420 64 ug/Kg 06/30/21 10:37 07/01/21 18:13 50☼Naphthalene 30000 B
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 740 U 740 740 mg/Kg ☼06/28/21 12:30 07/01/21 16:04 10000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
380 380 mg/Kg 06/28/21 12:30 07/01/21 16:04 10000☼C9-C12 Aliphatics 610
200 200 mg/Kg 06/28/21 12:30 07/01/21 16:04 10000☼C9-C10 Aromatics 1300
a,a,a-Trifluorotoluene (fid)102 70-130 06/28/21 12:30 07/01/21 16:04 10000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)104 06/28/21 12:30 07/01/21 16:04 1000070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics 3.0 2.0 2.0 mg/Kg ☼07/06/21 08:31 07/07/21 19:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.7 3.7 mg/Kg 07/06/21 08:31 07/07/21 21:47 1☼C11-C22 Aromatics 230 F1
1-Chlorooctadecane 59 40-140 07/06/21 08:31 07/07/21 19:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 53 07/06/21 08:31 07/07/21 21:47 140-140
2-Fluorobiphenyl 68 07/06/21 08:31 07/07/21 21:47 140-140
2-Bromonaphthalene 63 07/06/21 08:31 07/07/21 21:47 140-140
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
RL MDL
C9-C18 Aliphatics 260 4.0 4.0 mg/Kg ☼07/06/21 08:31 07/08/21 13:34 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Solids 77.9 0.01 0.01 %06/29/21 13:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-1Client Sample ID: MW-1 (15')
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
General Chemistry (Continued)
RL MDL
Percent Moisture 22.1 0.01 0.01 %06/29/21 13:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-2Client Sample ID: MW-1 (25')
Matrix: SoilDate Collected: 06/23/21 12:55
Percent Solids: 77.9Date Received: 06/26/21 09:09
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 2800 890 890 mg/Kg ☼06/28/21 12:30 07/01/21 17:05 10000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
460 460 mg/Kg 06/28/21 12:30 07/01/21 17:05 10000☼C9-C12 Aliphatics 2000
250 250 mg/Kg 06/28/21 12:30 07/01/21 17:05 10000☼C9-C10 Aromatics 2800
a,a,a-Trifluorotoluene (fid)114 70-130 06/28/21 12:30 07/01/21 17:05 10000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)110 06/28/21 12:30 07/01/21 17:05 1000070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics 4.0 U 4.0 4.0 mg/Kg ☼07/06/21 08:31 07/08/21 13:47 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.5 7.5 mg/Kg 07/06/21 08:31 07/08/21 15:04 2☼C11-C22 Aromatics 520
1-Chlorooctadecane 52 40-140 07/06/21 08:31 07/08/21 13:47 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 47 07/06/21 08:31 07/08/21 15:04 240-140
2-Fluorobiphenyl 62 07/06/21 08:31 07/08/21 15:04 240-140
2-Bromonaphthalene 119 07/06/21 08:31 07/08/21 15:04 240-140
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
RL MDL
C9-C18 Aliphatics 740 8.0 8.0 mg/Kg ☼07/06/21 08:31 07/08/21 14:00 4
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Solids 77.9 0.01 0.01 %07/01/21 08:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %07/01/21 08:59 1Percent Moisture 22.1
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-3Client Sample ID: MW-1 (35')
Matrix: SoilDate Collected: 06/23/21 13:15
Percent Solids: 74.1Date Received: 06/26/21 09:09
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 51000 U *[phone] ug/Kg ☼07/06/21 08:47 07/06/21 20:06 2500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
20000 2700 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Benzene 8800 J
20000 5100 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Bromobenzene 5100 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Chlorobromomethane 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Dichlorobromomethane 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Bromoform 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Bromomethane 9900 U
99000 24000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼2-Butanone (MEK)24000 U
20000 3800 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼n-Butylbenzene 28000
20000 3800 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼sec-Butylbenzene 6900 J
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼tert-Butylbenzene 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Carbon disulfide 9900 U
20000 6700 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Carbon tetrachloride 6700 U
20000 2100 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Chlorobenzene 2100 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Chloroethane 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Chloroform 9900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Chloromethane 4000 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼3-Chloro-1-propene 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼2-Chlorotoluene 9900 U
20000 3900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼4-Chlorotoluene 3900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Chlorodibromomethane 9900 U
20000 13000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2-Dibromo-3-Chloropropane 13000 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Ethylene Dibromide 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Dibromomethane 9900 U
20000 2800 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2-Dichlorobenzene 2800 U
20000 3800 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,3-Dichlorobenzene 3800 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,4-Dichlorobenzene 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼trans-1,4-Dichloro-2-butene 9900 U
20000 5100 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Dichlorodifluoromethane 5100 U
20000 3300 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1-Dichloroethane 3300 U
20000 3200 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2-Dichloroethane 3200 U
20000 3000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼cis-1,2-Dichloroethene 3000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼trans-1,2-Dichloroethene 9900 U
20000 5500 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2-Dichloroethene, Total 5500 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1-Dichloroethene 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2-Dichloropropane 9900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,3-Dichloropropane 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼2,2-Dichloropropane 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1-Dichloropropene 9900 U
20000 4800 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼cis-1,3-Dichloropropene 4800 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼trans-1,3-Dichloropropene 9900 U
20000 2400 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Ethylbenzene 100000
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Ethyl methacrylate 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Hexachlorobutadiene 9900 U
99000 20000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼2-Hexanone 20000 U *+
20000 13000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Iodomethane 13000 U
99000 40000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Isobutyl alcohol 40000 U
20000 2700 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Isopropylbenzene 14000 J
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼4-Isopropyltoluene 4400 J
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-3Client Sample ID: MW-1 (35')
Matrix: SoilDate Collected: 06/23/21 13:15
Percent Solids: 74.1Date Received: 06/26/21 09:09
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 40000 U 59000 40000 ug/Kg ☼07/06/21 08:47 07/06/21 20:06 2500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
99000 20000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼4-Methyl-2-pentanone (MIBK)20000 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Methyl tert-butyl ether 4000 U
20000 7900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Naphthalene 55000
20000 3600 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼N-Propylbenzene 53000
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Styrene 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1,1,2-Tetrachloroethane 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1,2,2-Tetrachloroethane 9900 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Tetrachloroethene 9900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Toluene 200000
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2,3-Trichlorobenzene 9900 U
20000 7900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2,4-Trichlorobenzene 7900 U
20000 4400 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1,1-Trichloroethane 4400 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1,2-Trichloroethane 9900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Trichloroethene 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Trichlorofluoromethane 9900 U
20000 12000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2,3-Trichloropropane 12000 U
20000 7900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,1,2-Trichloro-1,2,2-trifluoroethane 7900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,2,4-Trimethylbenzene 290000
20000 3300 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,3,5-Trimethylbenzene 94000
99000 36000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Vinyl acetate 36000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Vinyl chloride 9900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼o-Xylene 160000
20000 5100 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼m-Xylene & p-Xylene 360000
40000 7500 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Xylenes, Total 520000
20000 3700 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Cyclohexane 13000 J
20000 18000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Methyl acetate 18000 U
20000 5900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Methylcyclohexane 78000
40000 20000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Tetrahydrofuran 20000 U
20000 4800 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Hexane 20000
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Ethyl ether 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼n-Heptane 86000
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,3-Dichloropropene, Total 9900 U
20000 4000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Butadiene 4000 U
20000 9900 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼Dichlorofluoromethane 9900 U
40000 32000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼2-Methyl-2-propanol 340000
2000000 200000 ug/Kg 07/06/21 08:47 07/06/21 20:06 2500☼1,4-Dioxane 200000 U
4-Bromofluorobenzene 99 67-130 07/06/21 08:47 07/06/21 20:06 2500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 97 07/06/21 08:47 07/06/21 20:06 250077-127
Toluene-d8 (Surr)103 07/06/21 08:47 07/06/21 20:06 250076-127
1,2-Dichloroethane-d4 (Surr)113 07/06/21 08:47 07/06/21 20:06 250078-146
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene 81 8.7 1.3 ug/Kg ☼06/30/21 10:37 06/30/21 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Acenaphthylene 61
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Anthracene 1.3 U
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Benzo[a]pyrene 15
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-3Client Sample ID: MW-1 (35')
Matrix: SoilDate Collected: 06/23/21 13:15
Percent Solids: 74.1Date Received: 06/26/21 09:09
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
RL MDL
Benzo[b]fluoranthene 18 B 8.7 1.3 ug/Kg ☼06/30/21 10:37 06/30/21 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.7 2.6 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Benzo[g,h,i]perylene 23
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Benzo[k]fluoranthene 9.2 B
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Chrysene 24
8.7 2.6 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Dibenz(a,h)anthracene 7.6 J
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Fluoranthene 35
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Fluorene 71
8.7 2.6 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Indeno[1,2,3-cd]pyrene 16
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Phenanthrene 160
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Pyrene 36
8.7 1.3 ug/Kg 06/30/21 10:37 06/30/21 18:58 1☼Benzo[a]anthracene 22 B
2-Fluorobiphenyl 98 27-127 06/30/21 10:37 06/30/21 18:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)122 06/30/21 10:37 06/30/21 18:58 115-136
Terphenyl-d14 (Surr)82 06/30/21 10:37 06/30/21 18:58 124-146
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level - DL
RL MDL
1-Methylnaphthalene 14000 B 430 66 ug/Kg ☼06/30/21 10:37 07/01/21 18:28 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
430 66 ug/Kg 06/30/21 10:37 07/01/21 18:28 50☼2-Methylnaphthalene 36000 B
430 66 ug/Kg 06/30/21 10:37 07/01/21 18:28 50☼Naphthalene 33000 B
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 1600 860 860 mg/Kg ☼06/28/21 12:30 07/01/21 18:05 10000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
440 440 mg/Kg 06/28/21 12:30 07/01/21 18:05 10000☼C9-C12 Aliphatics 1000
240 240 mg/Kg 06/28/21 12:30 07/01/21 18:05 10000☼C9-C10 Aromatics 1700
a,a,a-Trifluorotoluene (fid)110 70-130 06/28/21 12:30 07/01/21 18:05 10000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)107 06/28/21 12:30 07/01/21 18:05 1000070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics 12 2.1 2.1 mg/Kg ☼07/06/21 08:31 07/07/21 19:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.0 4.0 mg/Kg 07/06/21 08:31 07/07/21 22:13 1☼C11-C22 Aromatics 290
1-Chlorooctadecane 70 40-140 07/06/21 08:31 07/07/21 19:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 56 07/06/21 08:31 07/07/21 22:13 140-140
2-Fluorobiphenyl 67 07/06/21 08:31 07/07/21 22:13 140-140
2-Bromonaphthalene 60 07/06/21 08:31 07/07/21 22:13 140-140
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
RL MDL
C9-C18 Aliphatics 430 11 11 mg/Kg ☼07/06/21 08:31 07/08/21 14:12 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Solids 74.1 0.01 0.01 %06/29/21 13:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-3Client Sample ID: MW-1 (35')
Matrix: SoilDate Collected: 06/23/21 13:15
Percent Solids: 74.1Date Received: 06/26/21 09:09
General Chemistry (Continued)
RL MDL
Percent Moisture 25.9 0.01 0.01 %06/29/21 13:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-4Client Sample ID: MW-1
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Method: SM6200-B - Volatile Organic Compounds
RL MDL
Acetone 2200 J 2500 1000 ug/L 07/05/21 11:38 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
100 38 ug/L 07/05/21 11:38 100Benzene5900
100 54 ug/L 07/05/21 11:38 100Bromobenzene54U
100 52 ug/L 07/05/21 11:38 100Bromochloromethane52U
100 50 ug/L 07/05/21 11:38 100Bromodichloromethane50U
500 71 ug/L 07/05/21 11:38 100Bromoform71U
100 98 ug/L 07/05/21 11:38 100Bromomethane98U
2500 260 ug/L 07/05/21 11:38 1002-Butanone (MEK)1300 J
100 50 ug/L 07/05/21 11:38 100Carbon tetrachloride 50 U
100 50 ug/L 07/05/21 11:38 100Chlorobenzene50U
100 76 ug/L 07/05/21 11:38 100Chloroethane76U
100 60 ug/L 07/05/21 11:38 100Chloroform60U
100 83 ug/L 07/05/21 11:38 100Chloromethane83U
100 57 ug/L 07/05/21 11:38 1002-Chlorotoluene 57 U
100 56 ug/L 07/05/21 11:38 1004-Chlorotoluene 56 U
100 50 ug/L 07/05/21 11:38 100cis-1,2-Dichloroethene 50 U
500 50 ug/L 07/05/21 11:38 100cis-1,3-Dichloropropene 50 U
100 50 ug/L 07/05/21 11:38 100Dibromochloromethane50U
100 50 ug/L 07/05/21 11:38 1001,2-Dibromoethane (EDB)220
100 50 ug/L 07/05/21 11:38 1001,2-Dichlorobenzene 50 U
100 54 ug/L 07/05/21 11:38 1001,3-Dichlorobenzene 54 U
100 64 ug/L 07/05/21 11:38 1001,4-Dichlorobenzene 64 U
100 85 ug/L 07/05/21 11:38 100Dichlorodifluoromethane85U
100 50 ug/L 07/05/21 11:38 1001,1-Dichloroethane 50 U
100 50 ug/L 07/05/21 11:38 1001,2-Dichloroethane 370
100 50 ug/L 07/05/21 11:38 1001,1-Dichloroethene 50 U
100 50 ug/L 07/05/21 11:38 1001,2-Dichloropropane 50 U
100 50 ug/L 07/05/21 11:38 1001,3-Dichloropropane 50 U
100 50 ug/L 07/05/21 11:38 1002,2-Dichloropropane 50 U
100 50 ug/L 07/05/21 11:38 1001,1-Dichloropropene 50 U
100 70 ug/L 07/05/21 11:38 100Diisopropyl ether 140
10000 5200 ug/L 07/05/21 11:38 100Ethanol5200U
100 50 ug/L 07/05/21 11:38 100Ethylbenzene1500
2500 310 ug/L 07/05/21 11:38 1002-Hexanone 310 U
100 53 ug/L 07/05/21 11:38 100Isopropylbenzene100
500 300 ug/L 07/05/21 11:38 100Methylene Chloride 300 U
2500 180 ug/L 07/05/21 11:38 1004-Methyl-2-pentanone (MIBK)180 U
100 74 ug/L 07/05/21 11:38 100Methyl tert-butyl ether 2400
500 160 ug/L 07/05/21 11:38 100m-Xylene & p-Xylene 5000
100 100 ug/L 07/05/21 11:38 100Naphthalene510
100 76 ug/L 07/05/21 11:38 100n-Butylbenzene 76 U
100 69 ug/L 07/05/21 11:38 100N-Propylbenzene 260
500 60 ug/L 07/05/21 11:38 100o-Xylene 2400
100 71 ug/L 07/05/21 11:38 100p-Cymene (p-Isopropyltoluene)71 U
100 70 ug/L 07/05/21 11:38 100sec-Butylbenzene 70 U
100 100 ug/L 07/05/21 11:38 100Styrene100U
100 63 ug/L 07/05/21 11:38 100tert-Butylbenzene 63 U
100 52 ug/L 07/05/21 11:38 1001,1,1,2-Tetrachloroethane 52 U
100 50 ug/L 07/05/21 11:38 1001,1,2,2-Tetrachloroethane 50 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-4Client Sample ID: MW-1
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Tetrachloroethene 58 U 100 58 ug/L 07/05/21 11:38 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
100 41 ug/L 07/05/21 11:38 100Toluene12000
100 50 ug/L 07/05/21 11:38 100trans-1,2-Dichloroethene 50 U
500 50 ug/L 07/05/21 11:38 100trans-1,3-Dichloropropene 50 U
100 70 ug/L 07/05/21 11:38 1001,2,3-Trichlorobenzene 70 U
100 82 ug/L 07/05/21 11:38 1001,2,4-Trichlorobenzene 82 U
100 50 ug/L 07/05/21 11:38 1001,1,1-Trichloroethane 50 U
500 50 ug/L 07/05/21 11:38 1001,1,2-Trichloroethane 50 U
100 50 ug/L 07/05/21 11:38 100Trichloroethene50U
100 52 ug/L 07/05/21 11:38 100Trichlorofluoromethane52U
500 84 ug/L 07/05/21 11:38 1001,2,3-Trichloropropane 84 U
100 82 ug/L 07/05/21 11:38 1001,2,4-Trimethylbenzene 1600
100 56 ug/L 07/05/21 11:38 1001,3,5-Trimethylbenzene 460
2500 200 ug/L 07/05/21 11:38 100Vinyl acetate 200 U
100 50 ug/L 07/05/21 11:38 100Vinyl chloride 50 U
1000 160 ug/L 07/05/21 11:38 100Xylenes, Total 7300
4-Bromofluorobenzene 80 72-119 07/05/21 11:38 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 103 07/05/21 11:38 10075-126
Toluene-d8 (Surr)102 07/05/21 11:38 10064-132
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene 0.12 U 7.6 0.12 ug/L 07/01/21 08:08 07/02/21 01:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.6 0.13 ug/L 07/01/21 08:08 07/02/21 01:12 1Acenaphthylene0.13 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Anthracene0.14 U
7.6 0.76 ug/L 07/01/21 08:08 07/02/21 01:12 1Azobenzene0.76 U
19 15 ug/L 07/01/21 08:08 07/02/21 01:12 1Benzidine15U *- *1
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Benzo[a]anthracene 0.14 U
7.6 0.091 ug/L 07/01/21 08:08 07/02/21 01:12 1Benzo[a]pyrene 2.0 J
7.6 0.11 ug/L 07/01/21 08:08 07/02/21 01:12 1Benzo[b]fluoranthene 0.82 J
7.6 0.17 ug/L 07/01/21 08:08 07/02/21 01:12 1Benzo[g,h,i]perylene 0.17 U
7.6 0.12 ug/L 07/01/21 08:08 07/02/21 01:12 1Benzo[k]fluoranthene 0.28 J
7.6 0.12 ug/L 07/01/21 08:08 07/02/21 01:12 1Bis(2-chloroethoxy)methane 0.12 U
7.6 2.1 ug/L 07/01/21 08:08 07/02/21 01:12 1Bis(2-chloroethyl)ether 2.1 U
7.6 3.8 ug/L 07/01/21 08:08 07/02/21 01:12 1Bis(2-ethylhexyl) phthalate 3.8 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Butyl benzyl phthalate 2.4 J
7.6 2.9 ug/L 07/01/21 08:08 07/02/21 01:12 14-Chloro-3-methylphenol 2.9 U
7.6 0.11 ug/L 07/01/21 08:08 07/02/21 01:12 12-Chloronaphthalene 0.11 U
7.6 1.7 ug/L 07/01/21 08:08 07/02/21 01:12 12-Chlorophenol 1.7 U
7.6 1.5 ug/L 07/01/21 08:08 07/02/21 01:12 14-Chlorophenyl phenyl ether 1.5 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Chrysene0.62 J
7.6 0.18 ug/L 07/01/21 08:08 07/02/21 01:12 1Dibenz(a,h)anthracene 0.18 U
7.6 0.13 ug/L 07/01/21 08:08 07/02/21 01:12 11,2-Dichlorobenzene 0.13 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 11,3-Dichlorobenzene 0.14 U
7.6 0.12 ug/L 07/01/21 08:08 07/02/21 01:12 11,4-Dichlorobenzene 0.12 U
7.6 2.0 ug/L 07/01/21 08:08 07/02/21 01:12 13,3'-Dichlorobenzidine 2.0 U
7.6 1.5 ug/L 07/01/21 08:08 07/02/21 01:12 12,4-Dichlorophenol 1.5 U
7.6 0.18 ug/L 07/01/21 08:08 07/02/21 01:12 1Diethyl phthalate 0.18 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-4Client Sample ID: MW-1
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2,4-Dimethylphenol 77 7.6 1.5 ug/L 07/01/21 08:08 07/02/21 01:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.6 0.13 ug/L 07/01/21 08:08 07/02/21 01:12 1Dimethyl phthalate 0.13 U
7.6 1.1 ug/L 07/01/21 08:08 07/02/21 01:12 1Di-n-butyl phthalate 1.1 U
7.6 1.2 ug/L 07/01/21 08:08 07/02/21 01:12 14,6-Dinitro-2-methylphenol 1.2 U
23 2.6 ug/L 07/01/21 08:08 07/02/21 01:12 12,4-Dinitrophenol 2.6 U
7.6 1.4 ug/L 07/01/21 08:08 07/02/21 01:12 12,4-Dinitrotoluene 1.4 U
7.6 1.4 ug/L 07/01/21 08:08 07/02/21 01:12 12,6-Dinitrotoluene 1.4 U
7.6 0.13 ug/L 07/01/21 08:08 07/02/21 01:12 1Di-n-octyl phthalate 0.13 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Fluoranthene0.59 J
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Fluorene0.14 U
7.6 0.13 ug/L 07/01/21 08:08 07/02/21 01:12 1Hexachlorobenzene0.13 U
7.6 2.7 ug/L 07/01/21 08:08 07/02/21 01:12 1Hexachlorobutadiene2.7 U
15 2.0 ug/L 07/01/21 08:08 07/02/21 01:12 1Hexachlorocyclopentadiene2.0 U
7.6 3.2 ug/L 07/01/21 08:08 07/02/21 01:12 1Hexachloroethane3.2 U
7.6 0.17 ug/L 07/01/21 08:08 07/02/21 01:12 1Indeno[1,2,3-cd]pyrene 0.17 U
7.6 0.11 ug/L 07/01/21 08:08 07/02/21 01:12 1Isophorone0.11 U
7.6 0.099 ug/L 07/01/21 08:08 07/02/21 01:12 1Nitrobenzene0.099 U
7.6 1.8 ug/L 07/01/21 08:08 07/02/21 01:12 12-Nitrophenol 1.8 U
7.6 1.6 ug/L 07/01/21 08:08 07/02/21 01:12 14-Nitrophenol 1.6 U
7.6 2.7 ug/L 07/01/21 08:08 07/02/21 01:12 1N-Nitrosodimethylamine 2.7 U
7.6 2.5 ug/L 07/01/21 08:08 07/02/21 01:12 1N-Nitrosodi-n-propylamine 2.5 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1N-Nitrosodiphenylamine 0.14 U
7.6 0.12 ug/L 07/01/21 08:08 07/02/21 01:12 12,2'-oxybis(1-chloropropane)0.12 U
15 1.1 ug/L 07/01/21 08:08 07/02/21 01:12 1Pentachlorophenol1.1 U
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 1Phenanthrene0.14 U
7.6 0.84 ug/L 07/01/21 08:08 07/02/21 01:12 1Phenol0.84 U
7.6 0.16 ug/L 07/01/21 08:08 07/02/21 01:12 1Pyrene0.62 J
7.6 0.14 ug/L 07/01/21 08:08 07/02/21 01:12 11,2,4-Trichlorobenzene 0.14 U
7.6 2.0 ug/L 07/01/21 08:08 07/02/21 01:12 12,4,6-Trichlorophenol 2.0 U
Unknown 660 T J ug/L 3.70 07/01/21 08:08 07/02/21 01:12 1
Tentatively Identified Compound Dil FacAnalyzedPreparedUnitDQualifierEst. Result CAS No.RT
107/02/21 01:1207/01/21 08:08T J NToluene 108-88-34700ug/L 3.84
107/02/21 01:1207/01/21 08:08T J NEthylbenzene 100-41-41400ug/L 4.60
107/02/21 01:1207/01/21 08:08T J Np-Xylene 106-42-33000ug/L 4.67
107/02/21 01:1207/01/21 08:08T J Np-Xylene 106-42-31700ug/L 4.83
107/02/21 01:1207/01/21 08:08T J NBenzene, 1-ethyl-3-methyl-620-14-41200ug/L 5.23
107/02/21 01:1207/01/21 08:08T J NBenzene, 1,3,5-trimethyl-108-67-8840ug/L 5.28
107/02/21 01:1207/01/21 08:08T J NBenzene, 1,2,3-trimethyl-526-73-81900ug/L 5.43
107/02/21 01:1207/01/21 08:08T JUnknown470 ug/L 6.19
107/02/21 01:1207/01/21 08:08T J NEthanone, 1-(4-methylphenyl)-122-00-9470ug/L 6.27
2-Fluorobiphenyl 72 32-109 07/01/21 08:08 07/02/21 01:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 0 S1-07/01/21 08:08 07/02/21 01:12 110-104
Terphenyl-d14 89 07/01/21 08:08 07/02/21 01:12 130-129
2,4,6-Tribromophenol 105 07/01/21 08:08 07/02/21 01:12 115-135
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Lab Sample ID: 400-205219-4Client Sample ID: MW-1
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) - DL
RL MDL
Naphthalene 330 38 0.65 ug/L 07/01/21 08:08 07/02/21 19:20 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Unknown 380 T J ug/L 3.48 07/01/21 08:08 07/02/21 19:20 5
Tentatively Identified Compound Dil FacAnalyzedPreparedUnitDQualifierEst. Result CAS No.RT
507/02/21 19:2007/01/21 08:08T J NToluene 108-88-33800ug/L 3.82
507/02/21 19:2007/01/21 08:08T J NEthylbenzene 100-41-4880ug/L 4.59
507/02/21 19:2007/01/21 08:08T J Np-Xylene 106-42-32500ug/L 4.65
507/02/21 19:2007/01/21 08:08T J NBenzene, 1,3-dimethyl-108-38-31300ug/L 4.81
507/02/21 19:2007/01/21 08:08T J NBenzene, 1-ethyl-3-methyl-620-14-4810ug/L 5.22
507/02/21 19:2007/01/21 08:08T JUnknown500 ug/L 5.24
507/02/21 19:2007/01/21 08:08T J NBenzene, 1,3,5-trimethyl-108-67-8450ug/L 5.27
507/02/21 19:2007/01/21 08:08T J NBenzene, 1,2,4-trimethyl-95-63-6380ug/L 5.57
507/02/21 19:2007/01/21 08:08T J N7-Methylindan-1-one 39627-61-7390ug/L 7.25
Nitrobenzene-d5 65 31-111 07/01/21 08:08 07/02/21 19:20 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Phenol-d5 42 07/01/21 08:08 07/02/21 19:20 510-110
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 57 13 13 mg/L 07/01/21 15:10 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.5 5.5 mg/L 07/01/21 15:10 500C9-C12 Aliphatics 18
3.5 3.5 mg/L 07/01/21 15:10 500C9-C10 Aromatics 16
a,a,a-Trifluorotoluene (fid)105 70-130 07/01/21 15:10 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)106 07/01/21 15:10 50070-130
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
1,2-Dibromoethane (EDB)230 p 4.1 3.1 ug/L 07/06/21 12:40 07/07/21 12:06 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4-Bromofluorobenzene 0 S1-56-150 07/06/21 12:40 07/07/21 12:06 200
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C9-C18 Aliphatics 0.71 0.15 0.11 mg/L 06/30/21 13:53 07/03/21 01:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.15 0.099 mg/L 06/30/21 13:53 07/03/21 01:56 1C19-C36 Aliphatics 0.12 J B
0.30 0.11 mg/L 06/30/21 13:53 07/03/21 07:59 1C11-C22 Aromatics 2.0
1-Chlorooctadecane 82 40-140 06/30/21 13:53 07/03/21 01:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 67 06/30/21 13:53 07/03/21 07:59 140-140
2-Fluorobiphenyl 62 06/30/21 13:53 07/03/21 07:59 140-140
2-Bromonaphthalene 51 06/30/21 13:53 07/03/21 07:59 140-140
Eurofins TestAmerica, Pensacola
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Definitions/Glossary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
U Indicates the analyte was analyzed for but not detected.
GC/MS Semi VOA
Qualifier Description
*-LCS and/or LCSD is outside acceptance limits, low biased.
Qualifier
*1 LCS/LCSD RPD exceeds control limits.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
B Compound was found in the blank and sample.
E Result exceeded calibration range.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1-Surrogate recovery exceeds control limits, low biased.
S1+Surrogate recovery exceeds control limits, high biased.
U Indicates the analyte was analyzed for but not detected.
GC/MS Semi VOA TICs
Qualifier Description
J Indicates an Estimated Value for TICs
Qualifier
N This flag indicates the presumptive evidence of a compound.
T Result is a tentatively identified compound (TIC) and an estimated value.
GC VOA
Qualifier Description
U Indicates the analyte was analyzed for but not detected.
Qualifier
GC Semi VOA
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
B Compound was found in the blank and sample.
E Result exceeded calibration range.
F1 MS and/or MSD recovery exceeds control limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
S1-Surrogate recovery exceeds control limits, low biased.
U Indicates the analyte was analyzed for but not detected.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
Eurofins TestAmerica, Pensacola
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Definitions/Glossary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Glossary (Continued)
These commonly used abbreviations may or may not be present in this report.
MDA Minimum Detectable Activity (Radiochemistry)
Abbreviation
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8260D - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (67-130)(77-127)(76-127)(78-146)
BFB DBFM TOL DCA
105 97 101 113400-205219-1
Percent Surrogate Recovery (Acceptance Limits)
MW-1 (15')
99 97 103 113400-205219-3 MW-1 (35')
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (67-130)(77-127)(76-127)(78-146)
BFB DBFM TOL DCA
95 99 105 120400-205229-A-1-B MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
96 100 106 124400-205229-A-1-C MSD Matrix Spike Duplicate
95 98 103 126LCS 400-538282/1-A Lab Control Sample
93 99 101 126MB 400-538282/2-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
Method: SM6200-B - Volatile Organic Compounds
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (72-119)(75-126)(64-132)
BFB DBFM TOL
80 103 102400-205219-4
Percent Surrogate Recovery (Acceptance Limits)
MW-1
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Method: SM6200-B - Volatile Organic Compounds
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (72-119)(75-126)(64-132)
BFB DBFM TOL
81 99 100240-152187-A-1 MSD
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike Duplicate
82 96 101240-152187-N-1 MS Matrix Spike
80 100 103LCS 400-538220/1002 Lab Control Sample
79 101 101MB 400-538220/4 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
TOL = Toluene-d8 (Surr)
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (32-109)(10-104)(30-129)(15-135)
FBP 2FP TPHL TBP
72 0 S1-89 105400-205219-4
Percent Surrogate Recovery (Acceptance Limits)
MW-1
Surrogate Legend
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol
TPHL = Terphenyl-d14
TBP = 2,4,6-Tribromophenol
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (31-111)(10-110)
NBZ PHL
65 42400-205219-4 - DL
Percent Surrogate Recovery (Acceptance Limits)
MW-1
Surrogate Legend
NBZ = Nitrobenzene-d5
PHL = Phenol-d5
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (32-109)(10-104)(31-111)(10-110)(30-129)(15-135)
FBP 2FP NBZ PHL TPHL TBP
73 61 85 54 81 93LCS 400-537819/2-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
72 57 85 8348 92LCSD 400-537819/3-A Lab Control Sample Dup
83 64 72 9350 75MB 400-537819/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol
NBZ = Nitrobenzene-d5
PHL = Phenol-d5
TPHL = Terphenyl-d14
TBP = 2,4,6-Tribromophenol
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (27-127)(15-136)(24-146)
FBP NBZ TPHL
65 230 S1+111400-205219-1
Percent Surrogate Recovery (Acceptance Limits)
MW-1 (15')
79 50 59400-205219-1 MS MW-1 (15')
93 53 64400-205219-1 MSD MW-1 (15')
98 122 82400-205219-3 MW-1 (35')
Surrogate Legend
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5 (Surr)
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
TPHL = Terphenyl-d14 (Surr)
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (27-127)(15-136)(24-146)
FBP NBZ TPHL
79 71 87LCS 400-537669/2-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
72 41 74LCSD 400-537669/3-A Lab Control Sample Dup
95 111 139MB 400-537669/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
105 106400-205219-4
Percent Surrogate Recovery (Acceptance Limits)
MW-1
106 103400-205219-4 MS MW-1
107 105400-205219-4 MSD MW-1
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
102 104400-205219-1
Percent Surrogate Recovery (Acceptance Limits)
MW-1 (15')
114 110400-205219-2 MW-1 (25')
110 107400-205219-3 MW-1 (35')
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
104 104660-111548-E-23-C MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
102 102660-111548-E-23-D MSD Matrix Spike Duplicate
104 104LCS 400-537413/1-A Lab Control Sample
105 104LCSD 400-537413/2-A Lab Control Sample Dup
103 103MB 400-537413/3-A Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
106 104LCS 400-537862/3
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
105 105LCSD 400-537862/4 Lab Control Sample Dup
105 107MB 400-537862/2 Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (56-150)
BFB2
0 S1-400-205219-4
Percent Surrogate Recovery (Acceptance Limits)
MW-1
Surrogate Legend
BFB = 4-Bromofluorobenzene
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (56-150)
BFB2
102LCS 400-538325/2-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
91LCSD 400-538325/3-A Lab Control Sample Dup
80MB 400-538325/1-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (40-140)
1COD1
82400-205219-4
Percent Surrogate Recovery (Acceptance Limits)
MW-1
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Ground Water
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
OTPH1 FBP1 2BN1
67 62 51400-205219-4
Percent Surrogate Recovery (Acceptance Limits)
MW-1
Surrogate Legend
OTPH = o-Terphenyl
FBP = 2-Fluorobiphenyl
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
2BN = 2-Bromonaphthalene
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (40-140)
1COD1
59400-205219-1
Percent Surrogate Recovery (Acceptance Limits)
MW-1 (15')
58400-205219-1 MS MW-1 (15')
62400-205219-1 MSD MW-1 (15')
52400-205219-2 MW-1 (25')
70400-205219-3 MW-1 (35')
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
OTPH1 FBP1 2BN1
53 68 63400-205219-1
Percent Surrogate Recovery (Acceptance Limits)
MW-1 (15')
54 66 62400-205219-1 MS MW-1 (15')
53 62 52400-205219-1 MSD MW-1 (15')
47 62 119400-205219-2 MW-1 (25')
56 67 60400-205219-3 MW-1 (35')
Surrogate Legend
OTPH = o-Terphenyl
FBP = 2-Fluorobiphenyl
2BN = 2-Bromonaphthalene
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (40-140)
1COD1
65LCS 400-538248/2-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
70LCSD 400-538248/3-A Lab Control Sample Dup
78MB 400-538248/1-A Method Blank
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
OTPH1 FBP1 2BN1
62 71 69LCS 400-538248/2-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
55 63 62LCSD 400-538248/3-A Lab Control Sample Dup
63 70 70MB 400-538248/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl
FBP = 2-Fluorobiphenyl
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Surrogate Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
2BN = 2-Bromonaphthalene
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-140)
1COD1
90400-204853-B-4-B MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
88400-204853-B-4-C MSD Matrix Spike Duplicate
94LCS 400-537738/2-A Lab Control Sample
83LCSD 400-537738/3-A Lab Control Sample Dup
87MB 400-537738/1-A Method Blank
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
OTPH1 FBP1 2BN1
76 71 58400-204853-B-4-B MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
73 67 52400-204853-B-4-C MSD Matrix Spike Duplicate
77 71 54LCS 400-537738/2-A Lab Control Sample
72 66 51LCSD 400-537738/3-A Lab Control Sample Dup
66 61 54MB 400-537738/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl
FBP = 2-Fluorobiphenyl
2BN = 2-Bromonaphthalene
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
GC/MS VOA
Analysis Batch: 538220
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water SM6200-B400-205219-4 MW-1 Total/NA
Water SM6200-BMB 400-538220/4 Method Blank Total/NA
Water SM6200-BLCS 400-538220/1002 Lab Control Sample Total/NA
Analysis Batch: 538241
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 538282400-205219-1 MW-1 (15')Total/NA
Soil 8260D 538282400-205219-3 MW-1 (35')Total/NA
Solid 8260D 538282MB 400-538282/2-A Method Blank Total/NA
Solid 8260D 538282LCS 400-538282/1-A Lab Control Sample Total/NA
Prep Batch: 538282
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035400-205219-1 MW-1 (15')Total/NA
Soil 5035400-205219-3 MW-1 (35')Total/NA
Solid 5035MB 400-538282/2-A Method Blank Total/NA
Solid 5035LCS 400-538282/1-A Lab Control Sample Total/NA
GC/MS Semi VOA
Analysis Batch: 537623
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270E LL 537669400-205219-1 MW-1 (15')Total/NA
Soil 8270E LL 537669400-205219-3 MW-1 (35')Total/NA
Solid 8270E LL 537669LCS 400-537669/2-A Lab Control Sample Total/NA
Solid 8270E LL 537669LCSD 400-537669/3-A Lab Control Sample Dup Total/NA
Soil 8270E LL 537669400-205219-1 MS MW-1 (15')Total/NA
Soil 8270E LL 537669400-205219-1 MSD MW-1 (15')Total/NA
Prep Batch: 537669
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3546400-205219-1 MW-1 (15')Total/NA
Soil 3546400-205219-1 - DL MW-1 (15')Total/NA
Soil 3546400-205219-3 MW-1 (35')Total/NA
Soil 3546400-205219-3 - DL MW-1 (35')Total/NA
Solid 3546MB 400-537669/1-A Method Blank Total/NA
Solid 3546LCS 400-537669/2-A Lab Control Sample Total/NA
Solid 3546LCSD 400-537669/3-A Lab Control Sample Dup Total/NA
Soil 3546400-205219-1 MS MW-1 (15')Total/NA
Soil 3546400-205219-1 MSD MW-1 (15')Total/NA
Prep Batch: 537819
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 625400-205219-4 MW-1 Total/NA
Ground Water 625400-205219-4 - DL MW-1 Total/NA
Water 625MB 400-537819/1-A Method Blank Total/NA
Water 625LCS 400-537819/2-A Lab Control Sample Total/NA
Water 625LCSD 400-537819/3-A Lab Control Sample Dup Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
GC/MS Semi VOA
Analysis Batch: 537932
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 625.1 537819400-205219-4 MW-1 Total/NA
Water 625.1 537819MB 400-537819/1-A Method Blank Total/NA
Water 625.1 537819LCS 400-537819/2-A Lab Control Sample Total/NA
Water 625.1 537819LCSD 400-537819/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 537935
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270E LL 537669400-205219-1 - DL MW-1 (15')Total/NA
Soil 8270E LL 537669400-205219-3 - DL MW-1 (35')Total/NA
Solid 8270E LL 537669MB 400-537669/1-A Method Blank Total/NA
Analysis Batch: 538064
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 625.1 537819400-205219-4 - DL MW-1 Total/NA
GC VOA
Analysis Batch: 537324
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil MAVPH 537413400-205219-1 MW-1 (15')Total/NA
Soil MAVPH 537413400-205219-2 MW-1 (25')Total/NA
Soil MAVPH 537413400-205219-3 MW-1 (35')Total/NA
Solid MAVPH 537413MB 400-537413/3-A Method Blank Total/NA
Solid MAVPH 537413LCS 400-537413/1-A Lab Control Sample Total/NA
Solid MAVPH 537413LCSD 400-537413/2-A Lab Control Sample Dup Total/NA
Prep Batch: 537413
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035400-205219-1 MW-1 (15')Total/NA
Soil 5035400-205219-2 MW-1 (25')Total/NA
Soil 5035400-205219-3 MW-1 (35')Total/NA
Solid 5035MB 400-537413/3-A Method Blank Total/NA
Solid 5035LCS 400-537413/1-A Lab Control Sample Total/NA
Solid 5035LCSD 400-537413/2-A Lab Control Sample Dup Total/NA
Analysis Batch: 537862
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MAVPH400-205219-4 MW-1 Total/NA
Water MAVPHMB 400-537862/2 Method Blank Total/NA
Water MAVPHLCS 400-537862/3 Lab Control Sample Total/NA
Water MAVPHLCSD 400-537862/4 Lab Control Sample Dup Total/NA
Ground Water MAVPH400-205219-4 MS MW-1 Total/NA
Ground Water MAVPH400-205219-4 MSD MW-1 Total/NA
GC Semi VOA
Prep Batch: 537738
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 3511400-205219-4 MW-1 Total/NA
Water 3511MB 400-537738/1-A Method Blank Total/NA
Water 3511LCS 400-537738/2-A Lab Control Sample Total/NA
Water 3511LCSD 400-537738/3-A Lab Control Sample Dup Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
GC Semi VOA
Analysis Batch: 538108
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MA-EPH 537738400-205219-4 MW-1 Total/NA
Water MA-EPH 537738MB 400-537738/1-A Method Blank Total/NA
Water MA-EPH 537738LCS 400-537738/2-A Lab Control Sample Total/NA
Water MA-EPH 537738LCSD 400-537738/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 538109
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MA-EPH 537738400-205219-4 MW-1 Total/NA
Water MA-EPH 537738MB 400-537738/1-A Method Blank Total/NA
Water MA-EPH 537738LCS 400-537738/2-A Lab Control Sample Total/NA
Water MA-EPH 537738LCSD 400-537738/3-A Lab Control Sample Dup Total/NA
Prep Batch: 538248
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3546400-205219-1 MW-1 (15')Total/NA
Soil 3546400-205219-1 - DL MW-1 (15')Total/NA
Soil 3546400-205219-2 MW-1 (25')Total/NA
Soil 3546400-205219-2 - DL MW-1 (25')Total/NA
Soil 3546400-205219-3 MW-1 (35')Total/NA
Soil 3546400-205219-3 - DL MW-1 (35')Total/NA
Solid 3546MB 400-538248/1-A Method Blank Total/NA
Solid 3546LCS 400-538248/2-A Lab Control Sample Total/NA
Solid 3546LCSD 400-538248/3-A Lab Control Sample Dup Total/NA
Soil 3546400-205219-1 MS MW-1 (15')Total/NA
Soil 3546400-205219-1 MSD MW-1 (15')Total/NA
Prep Batch: 538325
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 504.1400-205219-4 MW-1 Total/NA
Water 504.1MB 400-538325/1-A Method Blank Total/NA
Water 504.1LCS 400-538325/2-A Lab Control Sample Total/NA
Water 504.1LCSD 400-538325/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 538346
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 504.1 538325MB 400-538325/1-A Method Blank Total/NA
Water 504.1 538325LCS 400-538325/2-A Lab Control Sample Total/NA
Water 504.1 538325LCSD 400-538325/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 538443
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 504.1 538325400-205219-4 MW-1 Total/NA
Analysis Batch: 538512
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil MA-EPH 538248400-205219-1 MW-1 (15')Total/NA
Soil MA-EPH 538248400-205219-3 MW-1 (35')Total/NA
Solid MA-EPH 538248MB 400-538248/1-A Method Blank Total/NA
Solid MA-EPH 538248LCS 400-538248/2-A Lab Control Sample Total/NA
Solid MA-EPH 538248LCSD 400-538248/3-A Lab Control Sample Dup Total/NA
Soil MA-EPH 538248400-205219-1 MS MW-1 (15')Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
GC Semi VOA (Continued)
Analysis Batch: 538512 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil MA-EPH 538248400-205219-1 MSD MW-1 (15')Total/NA
Analysis Batch: 538514
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil MA-EPH 538248400-205219-1 MW-1 (15')Total/NA
Soil MA-EPH 538248400-205219-3 MW-1 (35')Total/NA
Solid MA-EPH 538248MB 400-538248/1-A Method Blank Total/NA
Solid MA-EPH 538248LCS 400-538248/2-A Lab Control Sample Total/NA
Solid MA-EPH 538248LCSD 400-538248/3-A Lab Control Sample Dup Total/NA
Soil MA-EPH 538248400-205219-1 MS MW-1 (15')Total/NA
Soil MA-EPH 538248400-205219-1 MSD MW-1 (15')Total/NA
Analysis Batch: 538625
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil MA-EPH 538248400-205219-1 - DL MW-1 (15')Total/NA
Soil MA-EPH 538248400-205219-2 MW-1 (25')Total/NA
Soil MA-EPH 538248400-205219-2 - DL MW-1 (25')Total/NA
Soil MA-EPH 538248400-205219-3 - DL MW-1 (35')Total/NA
Analysis Batch: 538627
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil MA-EPH 538248400-205219-2 MW-1 (25')Total/NA
General Chemistry
Analysis Batch: 537541
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture400-205219-1 MW-1 (15')Total/NA
Soil Moisture400-205219-3 MW-1 (35')Total/NA
Analysis Batch: 537838
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture400-205219-2 MW-1 (25')Total/NA
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 400-538282/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538241 Prep Batch: 538282
RL MDL
Acetone 13 U 25 13 ug/Kg 07/06/21 08:47 07/06/21 10:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.67 U 0.675.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Benzene
1.3 U 1.35.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Bromobenzene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Chlorobromomethane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Dichlorobromomethane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Bromoform
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Bromomethane
6.0 U 6.025 ug/Kg 07/06/21 08:47 07/06/21 10:52 12-Butanone (MEK)
0.96 U 0.965.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1n-Butylbenzene
0.95 U 0.955.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1sec-Butylbenzene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1tert-Butylbenzene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Carbon disulfide
1.7 U 1.75.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Carbon tetrachloride
0.52 U 0.525.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Chlorobenzene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Chloroethane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Chloroform
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Chloromethane
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 13-Chloro-1-propene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 12-Chlorotoluene
0.98 U 0.985.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 14-Chlorotoluene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Chlorodibromomethane
3.3 U 3.35.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2-Dibromo-3-Chloropropane
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Ethylene Dibromide
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Dibromomethane
0.71 U 0.715.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2-Dichlorobenzene
0.95 U 0.955.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,3-Dichlorobenzene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,4-Dichlorobenzene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1trans-1,4-Dichloro-2-butene
1.3 U 1.35.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Dichlorodifluoromethane
0.83 U 0.835.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1-Dichloroethane
0.82 U 0.825.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2-Dichloroethane
0.76 U 0.765.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1cis-1,2-Dichloroethene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1trans-1,2-Dichloroethene
1.4 U 1.45.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2-Dichloroethene, Total
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1-Dichloroethene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2-Dichloropropane
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,3-Dichloropropane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 12,2-Dichloropropane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1-Dichloropropene
1.2 U 1.25.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1cis-1,3-Dichloropropene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1trans-1,3-Dichloropropene
0.61 U 0.615.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Ethylbenzene
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Ethyl methacrylate
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Hexachlorobutadiene
5.0 U 5.025 ug/Kg 07/06/21 08:47 07/06/21 10:52 12-Hexanone
3.4 U 3.45.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Iodomethane
10 U 1025 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Isobutyl alcohol
0.68 U 0.685.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Isopropylbenzene
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-538282/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538241 Prep Batch: 538282
RL MDL
4-Isopropyltoluene 1.0 U 5.0 1.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
10 U 1015 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Methylene Chloride
5.0 U 5.025 ug/Kg 07/06/21 08:47 07/06/21 10:52 14-Methyl-2-pentanone (MIBK)
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Methyl tert-butyl ether
2.0 U 2.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Naphthalene
0.90 U 0.905.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1N-Propylbenzene
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Styrene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1,1,2-Tetrachloroethane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1,2,2-Tetrachloroethane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Tetrachloroethene
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Toluene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2,3-Trichlorobenzene
2.0 U 2.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2,4-Trichlorobenzene
1.1 U 1.15.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1,1-Trichloroethane
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1,2-Trichloroethane
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Trichloroethene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Trichlorofluoromethane
3.0 U 3.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2,3-Trichloropropane
2.0 U 2.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,2,4-Trimethylbenzene
0.83 U 0.835.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,3,5-Trimethylbenzene
9.1 U 9.125 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Vinyl acetate
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Vinyl chloride
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1o-Xylene
1.3 U 1.35.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1m-Xylene & p-Xylene
1.9 U 1.910 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Xylenes, Total
0.94 U 0.945.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Cyclohexane
4.6 U 4.65.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Methyl acetate
1.5 U 1.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Methylcyclohexane
5.0 U 5.010 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Tetrahydrofuran
1.2 U 1.25.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Hexane
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Ethyl ether
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1n-Heptane
2.5 U 2.510 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,3-Dichloropropene, Total
1.0 U 1.05.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Butadiene
2.5 U 2.55.0 ug/Kg 07/06/21 08:47 07/06/21 10:52 1Dichlorofluoromethane
8.0 U 8.010 ug/Kg 07/06/21 08:47 07/06/21 10:52 12-Methyl-2-propanol
50 U 50500 ug/Kg 07/06/21 08:47 07/06/21 10:52 11,4-Dioxane
4-Bromofluorobenzene 93 67-130 07/06/21 10:52 1
MB MB
Surrogate
07/06/21 08:47
Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 07/06/21 08:47 07/06/21 10:52 1Dibromofluoromethane77-127
101 07/06/21 08:47 07/06/21 10:52 1Toluene-d8 (Surr)76-127
126 07/06/21 08:47 07/06/21 10:52 11,2-Dichloroethane-d4 (Surr)78-146
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538282/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538241 Prep Batch: 538282
Acetone 200 448 *+ug/Kg 224 48-160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 40.3 ug/Kg 81 65-130
Bromobenzene 50.0 49.4 ug/Kg 99 65-130
Chlorobromomethane 50.0 41.2 ug/Kg 82 65-130
Dichlorobromomethane 50.0 48.6 ug/Kg 97 61-130
Bromoform 50.0 52.2 ug/Kg 104 52-136
Bromomethane 50.0 51.1 ug/Kg 102 12-160
2-Butanone (MEK)200 257 ug/Kg 128 55-130
n-Butylbenzene 50.0 50.5 ug/Kg 101 66-130
sec-Butylbenzene 50.0 49.5 ug/Kg 99 67-130
tert-Butylbenzene 50.0 46.0 ug/Kg 92 67-130
Carbon disulfide 50.0 43.8 ug/Kg 88 46-141
Carbon tetrachloride 50.0 64.1 ug/Kg 128 60-130
Chlorobenzene 50.0 45.5 ug/Kg 91 70-130
Chloroethane 50.0 35.8 ug/Kg 72 55-134
Chloroform 50.0 44.5 ug/Kg 89 62-130
Chloromethane 50.0 47.8 ug/Kg 96 49-136
3-Chloro-1-propene 50.0 46.7 ug/Kg 93 57-130
2-Chlorotoluene 50.0 48.5 ug/Kg 97 67-130
4-Chlorotoluene 50.0 49.0 ug/Kg 98 66-130
Chlorodibromomethane 50.0 51.0 ug/Kg 102 58-132
1,2-Dibromo-3-Chloropropane 50.0 46.4 ug/Kg 93 49-130
Ethylene Dibromide 50.0 42.5 ug/Kg 85 67-130
Dibromomethane 50.0 40.5 ug/Kg 81 65-130
1,2-Dichlorobenzene 50.0 43.6 ug/Kg 87 64-130
1,3-Dichlorobenzene 50.0 46.5 ug/Kg 93 66-130
1,4-Dichlorobenzene 50.0 44.0 ug/Kg 88 65-130
trans-1,4-Dichloro-2-butene 50.0 53.2 ug/Kg 106 45-137
Dichlorodifluoromethane 50.0 45.4 ug/Kg 91 34-143
1,1-Dichloroethane 50.0 45.1 ug/Kg 90 59-130
1,2-Dichloroethane 50.0 53.5 ug/Kg 107 62-130
cis-1,2-Dichloroethene 50.0 46.7 ug/Kg 93 53-135
trans-1,2-Dichloroethene 50.0 41.0 ug/Kg 82 58-134
1,2-Dichloroethene, Total 100 87.7 ug/Kg 88 70-130
1,1-Dichloroethene 50.0 48.9 ug/Kg 98 55-137
1,2-Dichloropropane 50.0 42.0 ug/Kg 84 64-130
1,3-Dichloropropane 50.0 39.6 ug/Kg 79 67-130
2,2-Dichloropropane 50.0 63.0 ug/Kg 126 51-132
1,1-Dichloropropene 50.0 45.2 ug/Kg 90 65-130
cis-1,3-Dichloropropene 50.0 42.9 ug/Kg 86 61-130
trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 60-130
Ethylbenzene 50.0 48.2 ug/Kg 96 70-130
Ethyl methacrylate 50.0 40.0 ug/Kg 80 62-130
Hexachlorobutadiene 50.0 63.0 ug/Kg 126 62-133
2-Hexanone 200 278 *+ug/Kg 139 57-131
Iodomethane 50.0 49.8 ug/Kg 100 12-160
Isobutyl alcohol 1250 1130 ug/Kg 90 44-136
Isopropylbenzene 50.0 51.2 ug/Kg 102 70-130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538282/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538241 Prep Batch: 538282
4-Isopropyltoluene 50.0 50.6 ug/Kg 101 68-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Methylene Chloride 50.0 36.7 ug/Kg 73 57-132
4-Methyl-2-pentanone (MIBK)200 174 ug/Kg 87 58-130
Methyl tert-butyl ether 50.0 43.0 ug/Kg 86 63-130
Naphthalene 50.0 41.6 ug/Kg 83 45-144
N-Propylbenzene 50.0 50.2 ug/Kg 100 67-130
Styrene 50.0 45.7 ug/Kg 91 68-130
1,1,1,2-Tetrachloroethane 50.0 55.3 ug/Kg 111 65-130
1,1,2,2-Tetrachloroethane 50.0 37.1 ug/Kg 74 60-131
Tetrachloroethene 50.0 46.5 ug/Kg 93 67-130
Toluene 50.0 43.8 ug/Kg 88 70-130
1,2,3-Trichlorobenzene 50.0 46.5 ug/Kg 93 58-135
1,2,4-Trichlorobenzene 50.0 47.4 ug/Kg 95 56-138
1,1,1-Trichloroethane 50.0 54.7 ug/Kg 109 63-130
1,1,2-Trichloroethane 50.0 41.5 ug/Kg 83 65-130
Trichloroethene 50.0 46.5 ug/Kg 93 65-130
Trichlorofluoromethane 50.0 55.6 ug/Kg 111 61-136
1,2,3-Trichloropropane 50.0 39.7 ug/Kg 79 60-130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 56.4 ug/Kg 113 47-143
1,2,4-Trimethylbenzene 50.0 47.4 ug/Kg 95 66-130
1,3,5-Trimethylbenzene 50.0 49.8 ug/Kg 100 67-130
Vinyl acetate 100 84.5 ug/Kg 85 24-160
Vinyl chloride 50.0 50.6 ug/Kg 101 52-132
o-Xylene 50.0 49.4 ug/Kg 99 70-130
m-Xylene & p-Xylene 50.0 49.6 ug/Kg 99 70-130
Xylenes, Total 100 99.0 ug/Kg 99 70-130
Cyclohexane 50.0 43.2 ug/Kg 86 61-130
Methyl acetate 100 78.3 ug/Kg 78 49-139
Methylcyclohexane 50.0 42.5 ug/Kg 85 64-130
Tetrahydrofuran 100 72.9 ug/Kg 73 52-132
Hexane 50.0 48.0 ug/Kg 96 57-132
Ethyl ether 50.0 47.6 ug/Kg 95 58-130
n-Heptane 50.0 50.2 ug/Kg 100 61-130
1,3-Dichloropropene, Total 100 93.5 ug/Kg 94 60-140
Butadiene 50.0 49.5 ug/Kg 99 52-132
Dichlorofluoromethane 50.0 53.6 ug/Kg 107 57-134
2-Methyl-2-propanol 500 443 ug/Kg 89 33-130
1,4-Dioxane 1000 786 ug/Kg 79 41-148
4-Bromofluorobenzene 67 -130
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
98Dibromofluoromethane 77 -127
103Toluene-d8 (Surr)76 -127
1261,2-Dichloroethane-d4 (Surr)78 -146
Eurofins TestAmerica, Pensacola
Page 38 of 69 7/12/2021
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 400-538220/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538220
RL MDL
Acetone 10 U 25 10 ug/L 07/05/21 09:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.38 U 0.381.0 ug/L 07/05/21 09:18 1Benzene
0.54 U 0.541.0 ug/L 07/05/21 09:18 1Bromobenzene
0.52 U 0.521.0 ug/L 07/05/21 09:18 1Bromochloromethane
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Bromodichloromethane
0.71 U 0.715.0 ug/L 07/05/21 09:18 1Bromoform
0.98 U 0.981.0 ug/L 07/05/21 09:18 1Bromomethane
2.6 U 2.625 ug/L 07/05/21 09:18 12-Butanone (MEK)
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Carbon tetrachloride
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Chlorobenzene
0.76 U 0.761.0 ug/L 07/05/21 09:18 1Chloroethane
0.60 U 0.601.0 ug/L 07/05/21 09:18 1Chloroform
0.83 U 0.831.0 ug/L 07/05/21 09:18 1Chloromethane
0.57 U 0.571.0 ug/L 07/05/21 09:18 12-Chlorotoluene
0.56 U 0.561.0 ug/L 07/05/21 09:18 14-Chlorotoluene
0.50 U 0.501.0 ug/L 07/05/21 09:18 1cis-1,2-Dichloroethene
0.50 U 0.505.0 ug/L 07/05/21 09:18 1cis-1,3-Dichloropropene
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Dibromochloromethane
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,2-Dibromoethane (EDB)
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,2-Dichlorobenzene
0.54 U 0.541.0 ug/L 07/05/21 09:18 11,3-Dichlorobenzene
0.64 U 0.641.0 ug/L 07/05/21 09:18 11,4-Dichlorobenzene
0.85 U 0.851.0 ug/L 07/05/21 09:18 1Dichlorodifluoromethane
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,1-Dichloroethane
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,2-Dichloroethane
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,1-Dichloroethene
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,2-Dichloropropane
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,3-Dichloropropane
0.50 U 0.501.0 ug/L 07/05/21 09:18 12,2-Dichloropropane
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,1-Dichloropropene
0.70 U 0.701.0 ug/L 07/05/21 09:18 1Diisopropyl ether
52 U 52100 ug/L 07/05/21 09:18 1Ethanol
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Ethylbenzene
3.1 U 3.125 ug/L 07/05/21 09:18 12-Hexanone
0.53 U 0.531.0 ug/L 07/05/21 09:18 1Isopropylbenzene
3.0 U 3.05.0 ug/L 07/05/21 09:18 1Methylene Chloride
1.8 U 1.825 ug/L 07/05/21 09:18 14-Methyl-2-pentanone (MIBK)
0.74 U 0.741.0 ug/L 07/05/21 09:18 1Methyl tert-butyl ether
1.6 U 1.65.0 ug/L 07/05/21 09:18 1m-Xylene & p-Xylene
1.0 U 1.01.0 ug/L 07/05/21 09:18 1Naphthalene
0.76 U 0.761.0 ug/L 07/05/21 09:18 1n-Butylbenzene
0.69 U 0.691.0 ug/L 07/05/21 09:18 1N-Propylbenzene
0.60 U 0.605.0 ug/L 07/05/21 09:18 1o-Xylene
0.71 U 0.711.0 ug/L 07/05/21 09:18 1p-Cymene (p-Isopropyltoluene)
0.70 U 0.701.0 ug/L 07/05/21 09:18 1sec-Butylbenzene
1.0 U 1.01.0 ug/L 07/05/21 09:18 1Styrene
0.63 U 0.631.0 ug/L 07/05/21 09:18 1tert-Butylbenzene
0.52 U 0.521.0 ug/L 07/05/21 09:18 11,1,1,2-Tetrachloroethane
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-538220/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538220
RL MDL
1,1,2,2-Tetrachloroethane 0.50 U 1.0 0.50 ug/L 07/05/21 09:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.58 U 0.581.0 ug/L 07/05/21 09:18 1Tetrachloroethene
0.41 U 0.411.0 ug/L 07/05/21 09:18 1Toluene
0.50 U 0.501.0 ug/L 07/05/21 09:18 1trans-1,2-Dichloroethene
0.50 U 0.505.0 ug/L 07/05/21 09:18 1trans-1,3-Dichloropropene
0.70 U 0.701.0 ug/L 07/05/21 09:18 11,2,3-Trichlorobenzene
0.82 U 0.821.0 ug/L 07/05/21 09:18 11,2,4-Trichlorobenzene
0.50 U 0.501.0 ug/L 07/05/21 09:18 11,1,1-Trichloroethane
0.50 U 0.505.0 ug/L 07/05/21 09:18 11,1,2-Trichloroethane
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Trichloroethene
0.52 U 0.521.0 ug/L 07/05/21 09:18 1Trichlorofluoromethane
0.84 U 0.845.0 ug/L 07/05/21 09:18 11,2,3-Trichloropropane
0.82 U 0.821.0 ug/L 07/05/21 09:18 11,2,4-Trimethylbenzene
0.56 U 0.561.0 ug/L 07/05/21 09:18 11,3,5-Trimethylbenzene
2.0 U 2.025 ug/L 07/05/21 09:18 1Vinyl acetate
0.50 U 0.501.0 ug/L 07/05/21 09:18 1Vinyl chloride
1.6 U 1.610 ug/L 07/05/21 09:18 1Xylenes, Total
4-Bromofluorobenzene 79 72-119 07/05/21 09:18 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 07/05/21 09:18 1Dibromofluoromethane75-126
101 07/05/21 09:18 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538220/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538220
Acetone 200 187 ug/L 93 43-160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 51.6 ug/L 103 70-130
Bromobenzene 50.0 53.5 ug/L 107 70-132
Bromochloromethane 50.0 51.0 ug/L 102 70-130
Bromodichloromethane 50.0 45.0 ug/L 90 67-133
Bromoform 50.0 48.0 ug/L 96 57-140
Bromomethane 50.0 67.3 ug/L 135 10-160
2-Butanone (MEK)200 237 ug/L 119 61-145
Carbon tetrachloride 50.0 48.6 ug/L 97 61-137
Chlorobenzene 50.0 51.5 ug/L 103 70-130
Chloroethane 50.0 49.2 ug/L 98 55-141
Chloroform 50.0 47.9 ug/L 96 69-130
Chloromethane 50.0 37.1 ug/L 74 58-137
2-Chlorotoluene 50.0 46.3 ug/L 93 70-130
4-Chlorotoluene 50.0 45.6 ug/L 91 70-130
cis-1,2-Dichloroethene 50.0 50.6 ug/L 101 68-130
cis-1,3-Dichloropropene 50.0 50.2 ug/L 100 69-132
Dibromochloromethane 50.0 48.4 ug/L 97 67-135
1,2-Dibromoethane (EDB)50.0 46.2 ug/L 92 70-130
1,2-Dichlorobenzene 50.0 53.2 ug/L 106 67-130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538220/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538220
1,3-Dichlorobenzene 50.0 56.0 ug/L 112 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,4-Dichlorobenzene 50.0 56.6 ug/L 113 70-130
Dichlorodifluoromethane 50.0 45.9 ug/L 92 41-146
1,1-Dichloroethane 50.0 42.9 ug/L 86 70-130
1,2-Dichloroethane 50.0 41.9 ug/L 84 69-130
1,1-Dichloroethene 50.0 50.8 ug/L 102 63-134
1,2-Dichloropropane 50.0 45.9 ug/L 92 70-130
1,3-Dichloropropane 50.0 48.3 ug/L 97 70-130
2,2-Dichloropropane 50.0 47.2 ug/L 94 52-135
1,1-Dichloropropene 50.0 49.9 ug/L 100 70-130
Diisopropyl ether 50.0 41.2 ug/L 82 64-132
Ethanol 2000 1880 ug/L 94 20-160
Ethylbenzene 50.0 48.9 ug/L 98 70-130
2-Hexanone 200 199 ug/L 100 65-137
Isopropylbenzene 50.0 50.8 ug/L 102 70-130
Methylene Chloride 50.0 49.6 ug/L 99 66-135
4-Methyl-2-pentanone (MIBK)200 167 ug/L 84 69-138
Methyl tert-butyl ether 50.0 52.9 ug/L 106 66-130
m-Xylene & p-Xylene 50.0 48.6 ug/L 97 70-130
Naphthalene 50.0 48.2 ug/L 96 47-149
n-Butylbenzene 50.0 49.1 ug/L 98 67-130
N-Propylbenzene 50.0 50.1 ug/L 100 70-130
o-Xylene 50.0 48.3 ug/L 97 70-130
p-Cymene (p-Isopropyltoluene)50.0 51.0 ug/L 102 65-130
sec-Butylbenzene 50.0 47.9 ug/L 96 66-130
Styrene 50.0 48.2 ug/L 96 70-130
tert-Butylbenzene 50.0 45.0 ug/L 90 64-139
1,1,1,2-Tetrachloroethane 50.0 53.0 ug/L 106 67-131
1,1,2,2-Tetrachloroethane 50.0 46.4 ug/L 93 70-131
Tetrachloroethene 50.0 51.6 ug/L 103 65-130
Toluene 50.0 48.4 ug/L 97 70-130
trans-1,2-Dichloroethene 50.0 50.0 ug/L 100 70-130
trans-1,3-Dichloropropene 50.0 47.3 ug/L 95 63-130
1,2,3-Trichlorobenzene 50.0 62.9 ug/L 126 60-138
1,2,4-Trichlorobenzene 50.0 59.2 ug/L 118 60-140
1,1,1-Trichloroethane 50.0 44.2 ug/L 88 68-130
1,1,2-Trichloroethane 50.0 49.3 ug/L 99 70-130
Trichloroethene 50.0 55.3 ug/L 111 70-130
Trichlorofluoromethane 50.0 49.9 ug/L 100 65-138
1,2,3-Trichloropropane 50.0 43.7 ug/L 87 70-130
1,2,4-Trimethylbenzene 50.0 45.5 ug/L 91 70-130
1,3,5-Trimethylbenzene 50.0 45.6 ug/L 91 69-130
Vinyl acetate 100 133 ug/L 133 26-160
Vinyl chloride 50.0 49.7 ug/L 99 59-136
Xylenes, Total 100 96.9 ug/L 97 70-130
4-Bromofluorobenzene 72 -119
Surrogate
80
LCS LCS
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
Page 41 of 69 7/12/2021
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538220/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538220
Dibromofluoromethane 75 -126
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
103Toluene-d8 (Surr)64 -132
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 400-537819/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
RL MDL
Acenaphthene 0.16 U 10 0.16 ug/L 07/01/21 08:08 07/02/21 00:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.17 U 0.1710 ug/L 07/01/21 08:08 07/02/21 00:10 1Acenaphthylene
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 1Anthracene
1.0 U 1.010 ug/L 07/01/21 08:08 07/02/21 00:10 1Azobenzene
20 U 2025 ug/L 07/01/21 08:08 07/02/21 00:10 1Benzidine
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 1Benzo[a]anthracene
0.12 U 0.1210 ug/L 07/01/21 08:08 07/02/21 00:10 1Benzo[a]pyrene
0.15 U 0.1510 ug/L 07/01/21 08:08 07/02/21 00:10 1Benzo[b]fluoranthene
0.23 U 0.2310 ug/L 07/01/21 08:08 07/02/21 00:10 1Benzo[g,h,i]perylene
0.16 U 0.1610 ug/L 07/01/21 08:08 07/02/21 00:10 1Benzo[k]fluoranthene
0.16 U 0.1610 ug/L 07/01/21 08:08 07/02/21 00:10 1Bis(2-chloroethoxy)methane
2.7 U 2.710 ug/L 07/01/21 08:08 07/02/21 00:10 1Bis(2-chloroethyl)ether
5.0 U 5.010 ug/L 07/01/21 08:08 07/02/21 00:10 1Bis(2-ethylhexyl) phthalate
0.19 U 0.1910 ug/L 07/01/21 08:08 07/02/21 00:10 1Butyl benzyl phthalate
3.8 U 3.810 ug/L 07/01/21 08:08 07/02/21 00:10 14-Chloro-3-methylphenol
0.14 U 0.1410 ug/L 07/01/21 08:08 07/02/21 00:10 12-Chloronaphthalene
2.2 U 2.210 ug/L 07/01/21 08:08 07/02/21 00:10 12-Chlorophenol
2.0 U 2.010 ug/L 07/01/21 08:08 07/02/21 00:10 14-Chlorophenyl phenyl ether
0.19 U 0.1910 ug/L 07/01/21 08:08 07/02/21 00:10 1Chrysene
0.24 U 0.2410 ug/L 07/01/21 08:08 07/02/21 00:10 1Dibenz(a,h)anthracene
0.17 U 0.1710 ug/L 07/01/21 08:08 07/02/21 00:10 11,2-Dichlorobenzene
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 11,3-Dichlorobenzene
0.16 U 0.1610 ug/L 07/01/21 08:08 07/02/21 00:10 11,4-Dichlorobenzene
2.6 U 2.610 ug/L 07/01/21 08:08 07/02/21 00:10 13,3'-Dichlorobenzidine
2.0 U 2.010 ug/L 07/01/21 08:08 07/02/21 00:10 12,4-Dichlorophenol
0.24 U 0.2410 ug/L 07/01/21 08:08 07/02/21 00:10 1Diethyl phthalate
2.0 U 2.010 ug/L 07/01/21 08:08 07/02/21 00:10 12,4-Dimethylphenol
0.17 U 0.1710 ug/L 07/01/21 08:08 07/02/21 00:10 1Dimethyl phthalate
1.4 U 1.410 ug/L 07/01/21 08:08 07/02/21 00:10 1Di-n-butyl phthalate
1.6 U 1.610 ug/L 07/01/21 08:08 07/02/21 00:10 14,6-Dinitro-2-methylphenol
3.4 U 3.430 ug/L 07/01/21 08:08 07/02/21 00:10 12,4-Dinitrophenol
1.9 U 1.910 ug/L 07/01/21 08:08 07/02/21 00:10 12,4-Dinitrotoluene
1.9 U 1.910 ug/L 07/01/21 08:08 07/02/21 00:10 12,6-Dinitrotoluene
0.17 U 0.1710 ug/L 07/01/21 08:08 07/02/21 00:10 1Di-n-octyl phthalate
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 1Fluoranthene
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 1Fluorene
0.17 U 0.1710 ug/L 07/01/21 08:08 07/02/21 00:10 1Hexachlorobenzene
3.6 U 3.610 ug/L 07/01/21 08:08 07/02/21 00:10 1Hexachlorobutadiene
2.6 U 2.620 ug/L 07/01/21 08:08 07/02/21 00:10 1Hexachlorocyclopentadiene
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-537819/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
RL MDL
Hexachloroethane 4.2 U 10 4.2 ug/L 07/01/21 08:08 07/02/21 00:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.22 U 0.2210 ug/L 07/01/21 08:08 07/02/21 00:10 1Indeno[1,2,3-cd]pyrene
0.14 U 0.1410 ug/L 07/01/21 08:08 07/02/21 00:10 1Isophorone
0.17 U 0.1710 ug/L 07/01/21 08:08 07/02/21 00:10 1Naphthalene
0.13 U 0.1310 ug/L 07/01/21 08:08 07/02/21 00:10 1Nitrobenzene
2.4 U 2.410 ug/L 07/01/21 08:08 07/02/21 00:10 12-Nitrophenol
2.1 U 2.110 ug/L 07/01/21 08:08 07/02/21 00:10 14-Nitrophenol
3.5 U 3.510 ug/L 07/01/21 08:08 07/02/21 00:10 1N-Nitrosodimethylamine
3.3 U 3.310 ug/L 07/01/21 08:08 07/02/21 00:10 1N-Nitrosodi-n-propylamine
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 1N-Nitrosodiphenylamine
0.16 U 0.1610 ug/L 07/01/21 08:08 07/02/21 00:10 12,2'-oxybis(1-chloropropane)
1.4 U 1.420 ug/L 07/01/21 08:08 07/02/21 00:10 1Pentachlorophenol
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 1Phenanthrene
1.1 U 1.110 ug/L 07/01/21 08:08 07/02/21 00:10 1Phenol
0.21 U 0.2110 ug/L 07/01/21 08:08 07/02/21 00:10 1Pyrene
0.18 U 0.1810 ug/L 07/01/21 08:08 07/02/21 00:10 11,2,4-Trichlorobenzene
2.6 U 2.610 ug/L 07/01/21 08:08 07/02/21 00:10 12,4,6-Trichlorophenol
Tentatively Identified Compound None ug/L 07/01/21 08:08 07/02/21 00:10 1
MB MB
Tentatively Identified Compound Dil FacPreparedAnalyzedDUnitQualifierEst. Result RT CAS No.
2-Fluorobiphenyl 83 32-109 07/02/21 00:10 1
MB MB
Surrogate
07/01/21 08:08
Dil FacPreparedAnalyzedQualifierLimits%Recovery
64 07/01/21 08:08 07/02/21 00:10 12-Fluorophenol 10-104
72 07/01/21 08:08 07/02/21 00:10 1Nitrobenzene-d5 31-111
50 07/01/21 08:08 07/02/21 00:10 1Phenol-d5 10-110
93 07/01/21 08:08 07/02/21 00:10 1Terphenyl-d14 30-129
75 07/01/21 08:08 07/02/21 00:10 12,4,6-Tribromophenol 15-135
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537819/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
Acenaphthene 240 208 ug/L 86 60-132
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 240 196 ug/L 82 54-126
Anthracene 240 210 ug/L 88 43-120
Azobenzene 240 189 ug/L 79 40-130
Benzidine 480 20 U *-ug/L 4 5-130
Benzo[a]anthracene 240 228 ug/L 95 42-133
Benzo[a]pyrene 240 205 ug/L 85 32-148
Benzo[b]fluoranthene 240 212 ug/L 88 42-140
Benzo[g,h,i]perylene 240 257 ug/L 107 10-195
Benzo[k]fluoranthene 240 239 ug/L 100 25-146
Bis(2-chloroethoxy)methane 240 181 ug/L 75 49-165
Bis(2-chloroethyl)ether 240 167 ug/L 70 43-126
Bis(2-ethylhexyl) phthalate 240 227 ug/L 95 29-137
4-Bromophenyl phenyl ether 240 245 ug/L 102 65-120
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537819/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
Butyl benzyl phthalate 240 230 ug/L 96 10-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Chloro-3-methylphenol 240 235 ug/L 98 41-128
2-Chloronaphthalene 240 181 ug/L 76 65-120
2-Chlorophenol 240 195 ug/L 81 36-120
4-Chlorophenyl phenyl ether 240 219 ug/L 91 38-145
Chrysene 240 227 ug/L 94 44-140
Dibenz(a,h)anthracene 240 225 ug/L 94 10-200
1,2-Dichlorobenzene 240 161 ug/L 67 39-130
1,3-Dichlorobenzene 240 150 ug/L 63 36-130
1,4-Dichlorobenzene 240 155 ug/L 64 41-130
3,3'-Dichlorobenzidine 480 236 ug/L 49 10-213
2,4-Dichlorophenol 240 223 ug/L 93 53-122
Diethyl phthalate 240 207 ug/L 86 10-120
2,4-Dimethylphenol 240 188 ug/L 78 42-120
Dimethyl phthalate 240 217 ug/L 90 10-120
Di-n-butyl phthalate 240 231 ug/L 96 10-120
4,6-Dinitro-2-methylphenol 480 482 ug/L 100 53-130
2,4-Dinitrophenol 480 439 ug/L 91 10-173
2,4-Dinitrotoluene 240 221 ug/L 92 48-127
2,6-Dinitrotoluene 240 229 ug/L 95 68-137
Di-n-octyl phthalate 240 236 ug/L 98 19-132
Fluoranthene 240 220 ug/L 91 43-121
Fluorene 240 203 ug/L 85 70-120
Hexachlorobenzene 240 253 ug/L 106 10-142
Hexachlorobutadiene 240 166 ug/L 69 38-120
Hexachlorocyclopentadiene 240 115 ug/L 48 10-130
Hexachloroethane 240 148 ug/L 62 55-120
Indeno[1,2,3-cd]pyrene 240 217 ug/L 91 10-151
Isophorone 240 185 ug/L 77 47-180
Naphthalene 240 185 ug/L 77 36-120
Nitrobenzene 240 184 ug/L 77 54-158
2-Nitrophenol 240 198 ug/L 83 61-163
4-Nitrophenol 480 382 ug/L 79 13-129
N-Nitrosodimethylamine 240 166 ug/L 69 31-130
N-Nitrosodi-n-propylamine 240 183 ug/L 76 14-198
N-Nitrosodiphenylamine 238 211 ug/L 89 57-130
2,2'-oxybis(1-chloropropane)240 157 ug/L 65 63-139
Pentachlorophenol 480 467 ug/L 97 38-152
Phenanthrene 240 203 ug/L 85 65-120
Phenol 240 142 ug/L 59 17-120
Pyrene 240 220 ug/L 92 70-120
1,2,4-Trichlorobenzene 240 163 ug/L 68 57-130
2,4,6-Trichlorophenol 240 217 ug/L 90 52-129
2-Fluorobiphenyl 32 -109
Surrogate
73
LCS LCS
Qualifier Limits%Recovery
612-Fluorophenol 10 -104
85Nitrobenzene-d5 31 -111
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537819/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
Phenol-d5 10 -110
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
81Terphenyl-d14 30 -129
932,4,6-Tribromophenol 15 -135
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537819/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
Acenaphthene 240 219 ug/L 91 60-132 6 40
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 240 202 ug/L 84 54-126 3 40
Anthracene 240 220 ug/L 92 43-120 5 40
Azobenzene 240 198 ug/L 82 40-130 5 40
Benzidine 480 43.9 *1 ug/L 9 5-130 86 40
Benzo[a]anthracene 240 244 ug/L 102 42-133 7 40
Benzo[a]pyrene 240 226 ug/L 94 32-148 10 40
Benzo[b]fluoranthene 240 226 ug/L 94 42-140 7 40
Benzo[g,h,i]perylene 240 278 ug/L 116 10-195 8 40
Benzo[k]fluoranthene 240 264 ug/L 110 25-146 10 40
Bis(2-chloroethoxy)methane 240 185 ug/L 77 49-165 2 40
Bis(2-chloroethyl)ether 240 184 ug/L 77 43-126 10 40
Bis(2-ethylhexyl) phthalate 240 245 ug/L 102 29-137 8 40
4-Bromophenyl phenyl ether 240 252 ug/L 105 65-120 3 40
Butyl benzyl phthalate 240 248 ug/L 103 10-140 7 40
4-Chloro-3-methylphenol 240 233 ug/L 97 41-128 1 40
2-Chloronaphthalene 240 188 ug/L 78 65-120 4 24
2-Chlorophenol 240 201 ug/L 84 36-120 3 40
4-Chlorophenyl phenyl ether 240 224 ug/L 93 38-145 2 40
Chrysene 240 244 ug/L 102 44-140 7 40
Dibenz(a,h)anthracene 240 241 ug/L 100 10-200 7 40
1,2-Dichlorobenzene 240 167 ug/L 69 39-130 3 40
1,3-Dichlorobenzene 240 155 ug/L 65 36-130 3 40
1,4-Dichlorobenzene 240 162 ug/L 67 41-130 4 40
3,3'-Dichlorobenzidine 480 239 ug/L 50 10-213 1 40
2,4-Dichlorophenol 240 224 ug/L 93 53-122 1 40
Diethyl phthalate 240 217 ug/L 90 10-120 5 40
2,4-Dimethylphenol 240 193 ug/L 80 42-120 3 40
Dimethyl phthalate 240 222 ug/L 93 10-120 2 40
Di-n-butyl phthalate 240 249 ug/L 104 10-120 8 40
4,6-Dinitro-2-methylphenol 480 498 ug/L 104 53-130 3 40
2,4-Dinitrophenol 480 442 ug/L 92 10-173 1 40
2,4-Dinitrotoluene 240 229 ug/L 96 48-127 4 40
2,6-Dinitrotoluene 240 233 ug/L 97 68-137 2 40
Di-n-octyl phthalate 240 252 ug/L 105 19-132 7 40
Fluoranthene 240 235 ug/L 98 43-121 7 40
Fluorene 240 210 ug/L 88 70-120 3 38
Hexachlorobenzene 240 264 ug/L 110 10-142 4 40
Hexachlorobutadiene 240 170 ug/L 71 38-120 2 40
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537819/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537932 Prep Batch: 537819
Hexachlorocyclopentadiene 240 119 ug/L 50 10-130 3 40
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Hexachloroethane 240 153 ug/L 64 55-120 3 40
Indeno[1,2,3-cd]pyrene 240 232 ug/L 97 10-151 6 40
Isophorone 240 188 ug/L 78 47-180 2 40
Naphthalene 240 187 ug/L 78 36-120 1 40
Nitrobenzene 240 187 ug/L 78 54-158 2 40
2-Nitrophenol 240 206 ug/L 86 61-163 4 40
4-Nitrophenol 480 384 ug/L 80 13-129 1 40
N-Nitrosodimethylamine 240 160 ug/L 67 31-130 4 40
N-Nitrosodi-n-propylamine 240 192 ug/L 80 14-198 5 40
N-Nitrosodiphenylamine 238 218 ug/L 91 57-130 3 40
2,2'-oxybis(1-chloropropane)240 165 ug/L 69 63-139 5 40
Pentachlorophenol 480 478 ug/L 100 38-152 2 40
Phenanthrene 240 216 ug/L 90 65-120 6 39
Phenol 240 132 ug/L 55 17-120 7 40
Pyrene 240 235 ug/L 98 70-120 6 40
1,2,4-Trichlorobenzene 240 169 ug/L 70 57-130 4 40
2,4,6-Trichlorophenol 240 218 ug/L 91 52-129 0 40
2-Fluorobiphenyl 32 -109
Surrogate
72
LCSD LCSD
Qualifier Limits%Recovery
572-Fluorophenol 10 -104
85Nitrobenzene-d5 31 -111
48Phenol-d5 10 -110
83Terphenyl-d14 30 -129
922,4,6-Tribromophenol 15 -135
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level
Client Sample ID: Method BlankLab Sample ID: MB 400-537669/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537935 Prep Batch: 537669
RL MDL
Acenaphthene 1.0 U 6.6 1.0 ug/Kg 06/30/21 10:37 07/01/21 17:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Acenaphthylene
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Anthracene
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Benzo[a]pyrene
1.20 J 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Benzo[b]fluoranthene
2.0 U 2.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Benzo[g,h,i]perylene
1.32 J 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Benzo[k]fluoranthene
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Chrysene
2.0 U 2.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Dibenz(a,h)anthracene
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Fluoranthene
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Fluorene
2.0 U 2.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Indeno[1,2,3-cd]pyrene
8.04 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 11-Methylnaphthalene
15.3 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 12-Methylnaphthalene
16.1 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Naphthalene
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-537669/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537935 Prep Batch: 537669
RL MDL
Phenanthrene 1.0 U 6.6 1.0 ug/Kg 06/30/21 10:37 07/01/21 17:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.0 U 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Pyrene
1.26 J 1.06.6 ug/Kg 06/30/21 10:37 07/01/21 17:57 1Benzo[a]anthracene
2-Fluorobiphenyl 95 27-127 07/01/21 17:57 1
MB MB
Surrogate
06/30/21 10:37
Dil FacPreparedAnalyzedQualifierLimits%Recovery
111 06/30/21 10:37 07/01/21 17:57 1Nitrobenzene-d5 (Surr)15-136
139 06/30/21 10:37 07/01/21 17:57 1Terphenyl-d14 (Surr)24-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537669/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537623 Prep Batch: 537669
Acenaphthene 2000 1660 ug/Kg 83 50-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 2000 1770 ug/Kg 89 50-120
Anthracene 2000 1820 ug/Kg 91 52-120
Benzo[a]pyrene 2000 1770 ug/Kg 89 54-120
Benzo[b]fluoranthene 2000 1700 ug/Kg 85 55-120
Benzo[g,h,i]perylene 2000 1810 ug/Kg 90 45-120
Benzo[k]fluoranthene 2000 1650 ug/Kg 83 52-120
Chrysene 2000 1830 ug/Kg 91 54-120
Dibenz(a,h)anthracene 2000 1920 ug/Kg 96 49-120
Fluoranthene 2000 1710 ug/Kg 86 49-120
Fluorene 2000 1850 ug/Kg 92 47-120
Indeno[1,2,3-cd]pyrene 2000 1850 ug/Kg 92 47-120
1-Methylnaphthalene 2000 1660 ug/Kg 83 40-120
2-Methylnaphthalene 2000 1710 ug/Kg 85 40-120
Naphthalene 2000 1690 ug/Kg 85 41-120
Phenanthrene 2000 1740 ug/Kg 87 50-120
Pyrene 2000 1760 ug/Kg 88 54-120
Benzo[a]anthracene 2000 1790 ug/Kg 90 55-120
2-Fluorobiphenyl 27 -127
Surrogate
79
LCS LCS
Qualifier Limits%Recovery
71Nitrobenzene-d5 (Surr)15 -136
87Terphenyl-d14 (Surr)24 -146
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537669/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537623 Prep Batch: 537669
Acenaphthene 2000 1520 ug/Kg 76 50-120 9 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 2000 1580 ug/Kg 79 50-120 11 30
Anthracene 2000 1710 ug/Kg 86 52-120 6 30
Benzo[a]pyrene 2000 1620 ug/Kg 81 54-120 9 30
Benzo[b]fluoranthene 2000 1470 ug/Kg 74 55-120 14 30
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537669/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537623 Prep Batch: 537669
Benzo[g,h,i]perylene 2000 1690 ug/Kg 84 45-120 7 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzo[k]fluoranthene 2000 1570 ug/Kg 78 52-120 5 30
Chrysene 2000 1650 ug/Kg 82 54-120 10 30
Dibenz(a,h)anthracene 2000 1790 ug/Kg 90 49-120 7 30
Fluoranthene 2000 1660 ug/Kg 83 49-120 3 30
Fluorene 2000 1680 ug/Kg 84 47-120 9 30
Indeno[1,2,3-cd]pyrene 2000 1750 ug/Kg 88 47-120 5 30
1-Methylnaphthalene 2000 1570 ug/Kg 78 40-120 6 30
2-Methylnaphthalene 2000 1590 ug/Kg 80 40-120 7 30
Naphthalene 2000 1450 ug/Kg 73 41-120 15 30
Phenanthrene 2000 1640 ug/Kg 82 50-120 6 30
Pyrene 2000 1560 ug/Kg 78 54-120 12 30
Benzo[a]anthracene 2000 1640 ug/Kg 82 55-120 9 30
2-Fluorobiphenyl 27 -127
Surrogate
72
LCSD LCSD
Qualifier Limits%Recovery
41Nitrobenzene-d5 (Surr)15 -136
74Terphenyl-d14 (Surr)24 -146
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 537623 Prep Batch: 537669
Acenaphthene 64 U 2490 1650 ug/Kg 66 40-140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene 64 U 2490 1690 ug/Kg 68 40-140☼
Anthracene 64 U *3 2490 1800 ug/Kg 72 40-140☼
Benzo[a]pyrene 64 U 2490 1650 ug/Kg 66 40-140☼
Benzo[b]fluoranthene 64 U 2490 1490 ug/Kg 60 40-140☼
Benzo[g,h,i]perylene 130 U 2490 1750 ug/Kg 70 40-140☼
Benzo[k]fluoranthene 64 U 2490 1580 ug/Kg 63 40-140☼
Chrysene 64 U *3 2490 1720 ug/Kg 69 40-140☼
Dibenz(a,h)anthracene 130 U 2490 1920 ug/Kg 77 40-140☼
Fluoranthene 64 U *3 2490 1780 ug/Kg 72 40-140☼
Fluorene 64 U 2490 1750 ug/Kg 70 40-140☼
Indeno[1,2,3-cd]pyrene 130 U 2490 1840 ug/Kg 74 40-140☼
1-Methylnaphthalene 20000 B 2490 17800 E 4 ug/Kg -76 40-140☼
2-Methylnaphthalene 46000 B 2490 27800 E 4 ug/Kg -739 40-140☼
Naphthalene 30000 B 2490 21400 E 4 ug/Kg -335 40-140☼
Phenanthrene 210 J *3 2490 1820 ug/Kg 65 40-140☼
Pyrene 64 U *3 2490 1570 ug/Kg 63 40-140☼
Benzo[a]anthracene 64 U *3 2490 1710 ug/Kg 69 40-140☼
2-Fluorobiphenyl 27 -127
Surrogate
79
MS MS
Qualifier Limits%Recovery
50Nitrobenzene-d5 (Surr)15 -136
59Terphenyl-d14 (Surr)24 -146
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 8270E LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 537623 Prep Batch: 537669
Acenaphthene 64 U 2530 1940 ug/Kg 77 40-140 16 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 64 U 2530 2020 ug/Kg 80 40-140 18 30☼
Anthracene 64 U *3 2530 1970 ug/Kg 78 40-140 9 30☼
Benzo[a]pyrene 64 U 2530 1860 ug/Kg 73 40-140 12 30☼
Benzo[b]fluoranthene 64 U 2530 1670 ug/Kg 66 40-140 11 30☼
Benzo[g,h,i]perylene 130 U 2530 1960 ug/Kg 77 40-140 12 30☼
Benzo[k]fluoranthene 64 U 2530 1810 ug/Kg 71 40-140 14 30☼
Chrysene 64 U *3 2530 1880 ug/Kg 74 40-140 9 30☼
Dibenz(a,h)anthracene 130 U 2530 2120 ug/Kg 84 40-140 10 30☼
Fluoranthene 64 U *3 2530 1950 ug/Kg 77 40-140 9 30☼
Fluorene 64 U 2530 2030 ug/Kg 80 40-140 15 30☼
Indeno[1,2,3-cd]pyrene 130 U 2530 2040 ug/Kg 80 40-140 10 30☼
1-Methylnaphthalene 20000 B 2530 18500 E 4 ug/Kg -44 40-140 4 30☼
2-Methylnaphthalene 46000 B 2530 26500 E 4 ug/Kg -778 40-140 5 30☼
Naphthalene 30000 B 2530 20700 E 4 ug/Kg -357 40-140 3 30☼
Phenanthrene 210 J *3 2530 2050 ug/Kg 73 40-140 12 30☼
Pyrene 64 U *3 2530 1720 ug/Kg 68 40-140 9 30☼
Benzo[a]anthracene 64 U *3 2530 1880 ug/Kg 74 40-140 9 30☼
2-Fluorobiphenyl 27 -127
Surrogate
93
MSD MSD
Qualifier Limits%Recovery
53Nitrobenzene-d5 (Surr)15 -136
64Terphenyl-d14 (Surr)24 -146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-537413/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537324 Prep Batch: 537413
RL MDL
C5-C8 Aliphatics 2.7 U 2.7 2.7 mg/Kg 06/28/21 12:30 06/28/21 15:22 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.4 U 1.41.4 mg/Kg 06/28/21 12:30 06/28/21 15:22 50C9-C12 Aliphatics
0.75 U 0.750.75 mg/Kg 06/28/21 12:30 06/28/21 15:22 50C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)103 70-130 06/28/21 15:22 50
MB MB
Surrogate
06/28/21 12:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 06/28/21 12:30 06/28/21 15:22 50a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537413/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537324 Prep Batch: 537413
C5-C8 Aliphatics 15.0 14.5 mg/Kg 97 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C12 Aliphatics 17.5 17.3 mg/Kg 99 70-130
C9-C10 Aromatics 2.50 2.48 mg/Kg 99 70-130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537413/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537324 Prep Batch: 537413
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
104a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537413/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 537324 Prep Batch: 537413
C5-C8 Aliphatics 15.0 14.8 mg/Kg 99 70-130 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C12 Aliphatics 17.5 15.9 mg/Kg 91 70-130 8 25
C9-C10 Aromatics 2.50 2.45 mg/Kg 98 70-130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
104a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 400-537862/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537862
RL MDL
C5-C8 Aliphatics 0.026 U 0.026 0.026 mg/L 07/01/21 11:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.011 U 0.0110.011 mg/L 07/01/21 11:56 1C9-C12 Aliphatics
0.0070 U 0.00700.0070 mg/L 07/01/21 11:56 1C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)105 70-130 07/01/21 11:56 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 07/01/21 11:56 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537862/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537862
C5-C8 Aliphatics 0.300 0.293 mg/L 98 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C12 Aliphatics 0.350 0.380 mg/L 109 70-130
C9-C10 Aromatics 0.0500 0.0577 mg/L 115 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
106
LCS LCS
Qualifier Limits%Recovery
104a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537862/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537862
C5-C8 Aliphatics 0.300 0.289 mg/L 96 70-130 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537862/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 537862
C9-C12 Aliphatics 0.350 0.352 mg/L 101 70-130 8 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C10 Aromatics 0.0500 0.0564 mg/L 113 70-130 2 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
105
LCSD LCSD
Qualifier Limits%Recovery
105a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: MW-1Lab Sample ID: 400-205219-4 MS
Matrix: Ground Water Prep Type: Total/NA
Analysis Batch: 537862
C5-C8 Aliphatics 57 150 187 mg/L 87 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
C9-C12 Aliphatics 18 175 179 mg/L 92 70-130
C9-C10 Aromatics 16 25.0 44.5 mg/L 115 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
106
MS MS
Qualifier Limits%Recovery
103a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: MW-1Lab Sample ID: 400-205219-4 MSD
Matrix: Ground Water Prep Type: Total/NA
Analysis Batch: 537862
C5-C8 Aliphatics 57 150 197 mg/L 93 70-130 5 25
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
C9-C12 Aliphatics 18 175 176 mg/L 90 70-130 2 25
C9-C10 Aromatics 16 25.0 43.8 mg/L 112 70-130 2 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
107
MSD MSD
Qualifier Limits%Recovery
105a,a,a-Trifluorotoluene (pid)70 -130
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-538325/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538346 Prep Batch: 538325
RL MDL
1,2-Dibromoethane (EDB)0.015 U 0.020 0.015 ug/L 07/06/21 12:40 07/06/21 17:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
4-Bromofluorobenzene 80 56-150 07/06/21 17:05 1
MB MB
Surrogate
07/06/21 12:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538325/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538346 Prep Batch: 538325
1,2-Dibromoethane (EDB)0.101 0.0981 ug/L 97 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene 56 -150
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-538325/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538346 Prep Batch: 538325
1,2-Dibromoethane (EDB)0.101 0.0969 ug/L 96 70-130 1 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Bromofluorobenzene 56 -150
Surrogate
91
LCSD LCSD
Qualifier Limits%Recovery
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-537738/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538108 Prep Batch: 537738
RL MDL
C9-C18 Aliphatics 0.11 U 0.15 0.11 mg/L 06/30/21 13:53 07/02/21 20:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.124 J 0.100.15 mg/L 06/30/21 13:53 07/02/21 20:31 1C19-C36 Aliphatics
1-Chlorooctadecane 87 40-140 07/02/21 20:31 1
MB MB
Surrogate
06/30/21 13:53
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-537738/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538109 Prep Batch: 537738
RL MDL
C11-C22 Aromatics 0.11 U 0.31 0.11 mg/L 06/30/21 13:53 07/03/21 02:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 66 40-140 07/03/21 02:34 1
MB MB
Surrogate
06/30/21 13:53
Dil FacPreparedAnalyzedQualifierLimits%Recovery
61 06/30/21 13:53 07/03/21 02:34 12-Fluorobiphenyl 40-140
54 06/30/21 13:53 07/03/21 02:34 12-Bromonaphthalene 40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537738/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538108 Prep Batch: 537738
C9-C18 Aliphatics 1.36 1.22 mg/L 90 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C19-C36 Aliphatics 1.82 1.59 mg/L 87 40-140
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537738/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538108 Prep Batch: 537738
1-Chlorooctadecane 40 -140
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-537738/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538109 Prep Batch: 537738
C11-C22 Aromatics 3.86 3.32 mg/L 86 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
77
LCS LCS
Qualifier Limits%Recovery
712-Fluorobiphenyl 40 -140
542-Bromonaphthalene 40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537738/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538108 Prep Batch: 537738
C9-C18 Aliphatics 1.36 1.13 mg/L 83 40-140 8 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C19-C36 Aliphatics 1.82 1.40 mg/L 77 40-140 13 50
1-Chlorooctadecane 40 -140
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-537738/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 538109 Prep Batch: 537738
C11-C22 Aromatics 3.86 3.21 mg/L 83 40-140 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
72
LCSD LCSD
Qualifier Limits%Recovery
662-Fluorobiphenyl 40 -140
512-Bromonaphthalene 40 -140
Client Sample ID: Method BlankLab Sample ID: MB 400-538248/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538512 Prep Batch: 538248
RL MDL
C9-C18 Aliphatics 1.6 U 1.6 1.6 mg/Kg 07/06/21 08:30 07/07/21 18:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.6 U 1.61.6 mg/Kg 07/06/21 08:30 07/07/21 18:10 1C19-C36 Aliphatics
1-Chlorooctadecane 78 40-140 07/07/21 18:10 1
MB MB
Surrogate
07/06/21 08:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-538248/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
RL MDL
C11-C22 Aromatics 3.0 U 3.0 3.0 mg/Kg 07/06/21 08:30 07/07/21 20:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 63 40-140 07/07/21 20:43 1
MB MB
Surrogate
07/06/21 08:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
70 07/06/21 08:30 07/07/21 20:43 12-Fluorobiphenyl 40-140
70 07/06/21 08:30 07/07/21 20:43 12-Bromonaphthalene 40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538248/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538512 Prep Batch: 538248
C9-C18 Aliphatics 20.0 9.66 mg/Kg 48 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C19-C36 Aliphatics 26.7 16.0 mg/Kg 60 40-140
1-Chlorooctadecane 40 -140
Surrogate
65
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-538248/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
C11-C22 Aromatics 56.7 39.1 mg/Kg 69 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
62
LCS LCS
Qualifier Limits%Recovery
712-Fluorobiphenyl 40 -140
692-Bromonaphthalene 40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-538248/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538512 Prep Batch: 538248
C9-C18 Aliphatics 20.0 11.3 mg/Kg 57 40-140 16 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C19-C36 Aliphatics 26.7 18.4 mg/Kg 69 40-140 14 50
1-Chlorooctadecane 40 -140
Surrogate
70
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-538248/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
C11-C22 Aromatics 56.7 36.6 mg/Kg 65 40-140 7 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-538248/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
o-Terphenyl 40 -140
Surrogate
55
LCSD LCSD
Qualifier Limits%Recovery
632-Fluorobiphenyl 40 -140
622-Bromonaphthalene 40 -140
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 538512 Prep Batch: 538248
C9-C18 Aliphatics 250 E 25.4 324 E 4 mg/Kg 303 40-140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
C19-C36 Aliphatics 3.0 33.9 22.1 mg/Kg 56 40-140☼
1-Chlorooctadecane 40 -140
Surrogate
58
MS MS
Qualifier Limits%Recovery
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
C11-C22 Aromatics 230 F1 72.1 340 F1 mg/Kg 146 40-140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
54
MS MS
Qualifier Limits%Recovery
662-Fluorobiphenyl 40 -140
622-Bromonaphthalene 40 -140
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 538512 Prep Batch: 538248
C9-C18 Aliphatics 250 E 25.4 370 E 4 mg/Kg 486 40-140 13 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
C19-C36 Aliphatics 3.0 33.8 26.0 mg/Kg 68 40-140 16 50☼
1-Chlorooctadecane 40 -140
Surrogate
62
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
C11-C22 Aromatics 230 F1 71.9 315 mg/Kg 112 40-140 8 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
53
MSD MSD
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 538514 Prep Batch: 538248
2-Fluorobiphenyl 40 -140
Surrogate
62
MSD MSD
Qualifier Limits%Recovery
522-Bromonaphthalene 40 -140
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1
Matrix: SoilDate Collected: 06/23/21 12:30
Date Received: 06/26/21 09:09
Analysis Moisture BKW06/29/21 13:531 TAL PEN537541
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
Prep 5035 BEP07/06/21 08:47 TAL PEN538282
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 17.776 g 15 g
Analysis 8260D 1000 538241 07/06/21 19:41 BEP TAL PENTotal/NA 5 mL 5 mL
CurieInstrument ID:
Prep 3546 537669 06/30/21 10:37 BKL TAL PENTotal/NA 15.06 g 1 mL
Analysis 8270E LL 1 537623 06/30/21 18:43 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Prep 3546 DL 537669 06/30/21 10:37 BKL TAL PENTotal/NA 15.06 g 1 mL
Analysis 8270E LL DL 50 537935 07/01/21 18:13 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Prep 5035 537413 06/28/21 12:30 GRK TAL PENTotal/NA 17.786 g 15.0 g
Analysis MAVPH 10000 537324 07/01/21 16:04 GRK TAL PENTotal/NA 5 mL 5 mL
CH_TRACYInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.43 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 19:13 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.43 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 21:47 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 DL 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.43 g 2 mL
Analysis MA-EPH DL 2 538625 07/08/21 13:34 S1B TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: MW-1 (25')Lab Sample ID: 400-205219-2
Matrix: SoilDate Collected: 06/23/21 12:55
Date Received: 06/26/21 09:09
Analysis Moisture AW07/01/21 08:591 TAL PEN537838
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1 (25')Lab Sample ID: 400-205219-2
Matrix: SoilDate Collected: 06/23/21 12:55
Percent Solids: 77.9Date Received: 06/26/21 09:09
Prep 5035 GRK06/28/21 12:30 TAL PEN537413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 14.091 g 15.0 g
Analysis MAVPH 10000 537324 07/01/21 17:05 GRK TAL PENTotal/NA 5 mL 5 mL
CH_TRACYInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 (25')Lab Sample ID: 400-205219-2
Matrix: SoilDate Collected: 06/23/21 12:55
Percent Solids: 77.9Date Received: 06/26/21 09:09
Prep 3546 BKL07/06/21 08:31 TAL PEN538248
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.40 g 2 mL
Analysis MA-EPH 2 538625 07/08/21 13:47 S1B TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 DL 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.40 g 2 mL
Analysis MA-EPH DL 4 538625 07/08/21 14:00 S1B TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.40 g 2 mL
Analysis MA-EPH 2 538627 07/08/21 15:04 S1B TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: MW-1 (35')Lab Sample ID: 400-205219-3
Matrix: SoilDate Collected: 06/23/21 13:15
Date Received: 06/26/21 09:09
Analysis Moisture BKW06/29/21 13:531 TAL PEN537541
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1 (35')Lab Sample ID: 400-205219-3
Matrix: SoilDate Collected: 06/23/21 13:15
Percent Solids: 74.1Date Received: 06/26/21 09:09
Prep 5035 BEP07/06/21 08:47 TAL PEN538282
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 16.386 g 15 g
Analysis 8260D 2500 538241 07/06/21 20:06 BEP TAL PENTotal/NA 5 mL 5 mL
CurieInstrument ID:
Prep 3546 537669 06/30/21 10:37 BKL TAL PENTotal/NA 15.38 g 1 mL
Analysis 8270E LL 1 537623 06/30/21 18:58 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Prep 3546 DL 537669 06/30/21 10:37 BKL TAL PENTotal/NA 15.38 g 1 mL
Analysis 8270E LL DL 50 537935 07/01/21 18:28 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Prep 5035 537413 06/28/21 12:30 GRK TAL PENTotal/NA 16.386 g 15.0 g
Analysis MAVPH 10000 537324 07/01/21 18:05 GRK TAL PENTotal/NA 5 mL 5 mL
CH_TRACYInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.36 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 19:39 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.36 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 22:13 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 DL 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.36 g 2 mL
Analysis MA-EPH DL 5 538625 07/08/21 14:12 S1B TAL PENTotal/NA
WALLEInstrument ID:
Eurofins TestAmerica, Pensacola
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Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 Lab Sample ID: 400-205219-4
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Analysis SM6200-B WPD07/05/21 11:38100 TAL PEN538220
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:Rosalind
Prep 625 537819 07/01/21 08:08 HMW TAL PENTotal/NA 329.2 mL 1 mL
Analysis 625.1 1 537932 07/02/21 01:12 S1B TAL PENTotal/NA
MarianneInstrument ID:
Prep 625 DL 537819 07/01/21 08:08 HMW TAL PENTotal/NA 329.2 mL 1 mL
Analysis 625.1 DL 5 538064 07/02/21 19:20 S1B TAL PENTotal/NA
MarianneInstrument ID:
Analysis MAVPH 500 537862 07/01/21 15:10 GRK TAL PENTotal/NA 5 mL 5 mL
CH_CAROLInstrument ID:
Prep 504.1 538325 07/06/21 12:40 DS TAL PENTotal/NA 33.9 mL 35 mL
Analysis 504.1 200 538443 07/07/21 12:06 DS TAL PENTotal/NA
YetiInstrument ID:
Prep 3511 537738 06/30/21 13:53 KWS TAL PENTotal/NA 55.8 mL 2 mL
Analysis MA-EPH 1 538108 07/03/21 01:56 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3511 537738 06/30/21 13:53 KWS TAL PENTotal/NA 55.8 mL 2 mL
Analysis MA-EPH 1 538109 07/03/21 07:59 JAW TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: Method Blank Lab Sample ID: MB 400-537413/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 GRK06/28/21 12:30 TAL PEN537413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.0 g
Analysis MAVPH 50 537324 06/28/21 15:22 GRK TAL PENTotal/NA 5 mL 5 mL
CH_TRACYInstrument ID:
Client Sample ID: Method Blank Lab Sample ID: MB 400-537669/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL06/30/21 10:37 TAL PEN537669
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E LL 1 537935 07/01/21 17:57 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Client Sample ID: Method Blank Lab Sample ID: MB 400-537738/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3511 KWS06/30/21 13:53 TAL PEN537738
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 55 mL 2 mL
Analysis MA-EPH 1 538108 07/02/21 20:31 JAW TAL PENTotal/NA
WALLEInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: Method Blank Lab Sample ID: MB 400-537738/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3511 KWS06/30/21 13:53 TAL PEN537738
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 55 mL 2 mL
Analysis MA-EPH 1 538109 07/03/21 02:34 JAW TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: Method Blank Lab Sample ID: MB 400-537819/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 625 HMW07/01/21 08:08 TAL PEN537819
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 625.1 1 537932 07/02/21 00:10 S1B TAL PENTotal/NA
MarianneInstrument ID:
Client Sample ID: Method Blank Lab Sample ID: MB 400-537862/2
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis MAVPH GRK07/01/21 11:561 TAL PEN537862
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CH_CAROL
Client Sample ID: Method Blank Lab Sample ID: MB 400-538220/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD07/05/21 09:181 TAL PEN538220
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:Rosalind
Client Sample ID: Method Blank Lab Sample ID: MB 400-538248/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL07/06/21 08:30 TAL PEN538248
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 18:10 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:30 BKL TAL PENTotal/NA 15 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 20:43 JAW TAL PENTotal/NA
WALLEInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: Method Blank Lab Sample ID: MB 400-538282/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 BEP07/06/21 08:47 TAL PEN538282
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 538241 07/06/21 10:52 BEP TAL PENTotal/NA 5 mL 5 mL
CurieInstrument ID:
Client Sample ID: Method Blank Lab Sample ID: MB 400-538325/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 504.1 DS07/06/21 12:40 TAL PEN538325
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 35 mL 35 mL
Analysis 504.1 1 538346 07/06/21 17:05 DS TAL PENTotal/NA
YetiInstrument ID:
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-537413/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 GRK06/28/21 12:30 TAL PEN537413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.0 g
Analysis MAVPH 50 537324 06/28/21 13:22 GRK TAL PENTotal/NA 5 mL 5 mL
CH_TRACYInstrument ID:
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-537669/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL06/30/21 10:37 TAL PEN537669
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E LL 5 537623 06/30/21 17:41 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-537738/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3511 KWS06/30/21 13:53 TAL PEN537738
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 55 mL 2 mL
Analysis MA-EPH 1 538108 07/02/21 20:44 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3511 537738 06/30/21 13:53 KWS TAL PENTotal/NA 55 mL 2 mL
Analysis MA-EPH 1 538109 07/03/21 02:47 JAW TAL PENTotal/NA
WALLEInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-537819/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 625 HMW07/01/21 08:08 TAL PEN537819
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 625.1 1 537932 07/02/21 00:31 S1B TAL PENTotal/NA
MarianneInstrument ID:
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-537862/3
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis MAVPH GRK07/01/21 13:011 TAL PEN537862
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CH_CAROL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-538220/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD07/05/21 08:251 TAL PEN538220
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:Rosalind
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-538248/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL07/06/21 08:30 TAL PEN538248
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 18:23 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:30 BKL TAL PENTotal/NA 15 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 20:55 JAW TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-538282/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 BEP07/06/21 08:47 TAL PEN538282
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 538241 07/06/21 10:02 BEP TAL PENTotal/NA 5 mL 5 mL
CurieInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-538325/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 504.1 DS07/06/21 12:40 TAL PEN538325
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 35 mL 35 mL
Analysis 504.1 1 538346 07/06/21 16:25 DS TAL PENTotal/NA
YetiInstrument ID:
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-537413/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 GRK06/28/21 12:30 TAL PEN537413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.0 g
Analysis MAVPH 50 537324 06/28/21 14:22 GRK TAL PENTotal/NA 5 mL 5 mL
CH_TRACYInstrument ID:
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-537669/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL06/30/21 10:37 TAL PEN537669
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E LL 5 537623 06/30/21 17:56 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-537738/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3511 KWS06/30/21 13:53 TAL PEN537738
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 55 mL 2 mL
Analysis MA-EPH 1 538108 07/02/21 20:57 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3511 537738 06/30/21 13:53 KWS TAL PENTotal/NA 55 mL 2 mL
Analysis MA-EPH 1 538109 07/03/21 03:00 JAW TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-537819/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 625 HMW07/01/21 08:08 TAL PEN537819
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Analysis 625.1 1 537932 07/02/21 00:51 S1B TAL PENTotal/NA
MarianneInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-537862/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis MAVPH GRK07/01/21 14:051 TAL PEN537862
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CH_CAROL
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-538248/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL07/06/21 08:30 TAL PEN538248
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 18:35 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:30 BKL TAL PENTotal/NA 15 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 21:08 JAW TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-538325/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 504.1 DS07/06/21 12:40 TAL PEN538325
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 35 mL 35 mL
Analysis 504.1 1 538346 07/06/21 16:45 DS TAL PENTotal/NA
YetiInstrument ID:
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MS
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
Prep 3546 BKL06/30/21 10:37 TAL PEN537669
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.45 g 1 mL
Analysis 8270E LL 5 537623 06/30/21 18:12 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.14 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 18:48 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.14 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 21:21 JAW TAL PENTotal/NA
WALLEInstrument ID:
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Client Sample ID: MW-1 (15')Lab Sample ID: 400-205219-1 MSD
Matrix: SoilDate Collected: 06/23/21 12:30
Percent Solids: 77.9Date Received: 06/26/21 09:09
Prep 3546 BKL06/30/21 10:37 TAL PEN537669
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.20 g 1 mL
Analysis 8270E LL 5 537623 06/30/21 18:27 PP1 TAL PENTotal/NA
PeanutsInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.17 g 2 mL
Analysis MA-EPH 1 538512 07/07/21 19:01 JAW TAL PENTotal/NA
WALLEInstrument ID:
Prep 3546 538248 07/06/21 08:31 BKL TAL PENTotal/NA 15.17 g 2 mL
Analysis MA-EPH 1 538514 07/07/21 21:34 JAW TAL PENTotal/NA
WALLEInstrument ID:
Client Sample ID: MW-1 Lab Sample ID: 400-205219-4 MS
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Analysis MAVPH GRK07/01/21 17:19500 TAL PEN537862
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CH_CAROL
Client Sample ID: MW-1 Lab Sample ID: 400-205219-4 MSD
Matrix: Ground WaterDate Collected: 06/24/21 09:30
Date Received: 06/26/21 09:09
Analysis MAVPH GRK07/01/21 18:24500 TAL PEN537862
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CH_CAROL
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Method Summary
Job ID: 400-205219-1Client: S&ME, Inc.
Project/Site: LURE (Moores Chapel Rd.)
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL PEN
SMSM6200-B Volatile Organic Compounds TAL PEN
40CFR136A625.1 Semivolatile Organic Compounds (GC/MS)TAL PEN
SW8468270E LL Semivolatile Organic Compounds by GC/MS - Low Level TAL PEN
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)TAL PEN
EPA-DW504.1 EDB, DBCP and 1,2,3-TCP (GC)TAL PEN
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)TAL PEN
EPAMoisturePercent Moisture TAL PEN
SW8463511Microextraction of Organic Compounds TAL PEN
SW8463546Microwave Extraction TAL PEN
SW8465030BPurge and Trap TAL PEN
SW8465035Closed System Purge and Trap TAL PEN
EPA-DW504.1 Microextraction TAL PEN
40CFR136A625Liquid-Liquid Extraction TAL PEN
Protocol References:
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
EPA = US Environmental Protection Agency
EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements.
MA DEP = Massachusetts Department Of Environmental Protection
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 400-205219-1
Project/Site: LURE (Moores Chapel Rd.)
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)314State 12-31-21
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
8260D 5035 Soil 1,2-Dichloroethene, Total
8260D 5035 Soil 1,3-Dichloropropene, Total
8260D 5035 Soil Butadiene
8260D 5035 Soil Hexane
8260D 5035 Soil n-Heptane
8260D 5035 Soil Tetrahydrofuran
Moisture Soil Percent Moisture
Moisture Soil Percent Solids
SM6200-B Ground Water 2-Butanone (MEK)
SM6200-B Ground Water 2-Hexanone
SM6200-B Ground Water 4-Methyl-2-pentanone (MIBK)
SM6200-B Ground Water Acetone
SM6200-B Ground Water Vinyl acetate
Eurofins TestAmerica, Pensacola
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 400-205219-1
Login Number: 205219
Question Answer Comment
Creator: Whitley, Adrian
List Source: Eurofins TestAmerica, Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.5.5°C IR9
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Pensacola
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