MO-28535_47783_CA_IAR_20210504

UST Closure Report
Former Snappy Food Mart
10100 Moores Chapel Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
PREPARED FOR:
LURE
10100 Moores Chapel Road
Charlotte, North Carolina 28273
PREPARED BY:
S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, North Carolina 28273
May 4, 2021
S&ME, Inc. | 9751 Southern Pine Boulevard | Charlotte, NC 28273 | p 704.523.4726 | www.smeinc.com
May 4, 2021
LURE
10100 Moores Chapel Road
Charlotte, North Carolina 28273
Attention: Mr. Ehab Aziz via email: [e-mail]
Reference: UST Closure Report
Former Snappy Food Mart
10100 Moores Chapel Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
S&ME, Inc. Engineering License Certification No. F-0176
Dear Mr. Aziz:
S&ME, Inc. (S&ME) is submitting this Underground Storage Tank (UST) Closure Report for the above-referenced
property. S&ME’s services were conducted in general accordance with S&ME Proposal No. 211105 dated
February 3, 2021. S&ME appreciates the opportunity to provide environmental services for this project. Please
contact us at your convenience if there are questions regarding the information contained in this document.
Sincerely,
S&ME, Inc.
James Wellons, P.G. Thomas P. Raymond, P.E., P.M.P.
Senior Project Manager Senior Engineer
[e-mail] [e-mail]
cc: Mr. Dan Bowser
North Carolina Department of Environmental Quality
Division of Waste Management, UST Section
Mooresville Regional Office
610 East Center Avenue
Mooresville, North Carolina 28115
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 ii
Table of Contents
1.0 Site Information ................................................................................................................ 1
1.1 Site Identification ............................................................................................................................ 1
1.2 Information about Contacts Associated with the Leaking UST System ................................. 1
1.3 Information about the Release ...................................................................................................... 1
1.4 Certification ..................................................................................................................................... 1
2.0 Scope of Services ............................................................................................................... 2
3.0 Background ........................................................................................................................ 2
3.1 Property Information ..................................................................................................................... 2
3.2 Project Background ........................................................................................................................ 2
4.0 Site History and Characterization ................................................................................. 2
4.1 UST Information ............................................................................................................................. 2
4.2 Non-UST Information .................................................................................................................... 3
4.3 UST Owner and Operator Information ....................................................................................... 3
4.4 Site Characteristics ......................................................................................................................... 3
5.0 UST Closure Services ....................................................................................................... 4
5.1 Pre-UST Closure Activities ........................................................................................................... 4
5.2 UST Closure Activities ................................................................................................................... 4
5.3 UST Closure Soil Analytical Results ............................................................................................ 5
5.4 Description of Release .................................................................................................................... 5
6.0 Site Check Report ............................................................................................................. 5
7.0 Free Product ........................................................................................................................ 5
8.0 Initial Response and Abatement Action ...................................................................... 6
8.1 Excavation of Contaminated Soil ................................................................................................. 6
8.2 NCDEQ Correspondence During the Initial Abatement Actions ........................................... 6
8.3 Post-Excavation Confirmation Sampling Methodology ........................................................... 6
8.4 Soil Analytical Results ................................................................................................................... 7
9.0 Sole Use Statement ........................................................................................................... 7
10.0 Limitations.......................................................................................................................... 7
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 iii
11.0 Conclusions and Recommendations ............................................................................. 7
Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – NCDEQ UST-3 Form
Appendix IV – Liquid, Concrete/Asphalt, and USTs Disposal Manifests
Appendix V – Site Photographs
Appendix VI – Soil Laboratory Report
Appendix VII – NCDEQ UST-61 Form
Appendix VIII – Soil Disposal Manifests
Appendix IX – Backfill Manifests
Appendix X – NCDEQ UST-2 Form
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 2
2.0 Scope of Services
The scope of services for this project included the removal of four USTs and associated piping by CCI, collection of
closure soil samples, collection of confirmation soil samples from the excavation limits, and the reporting herein.
The removal date of the dispensers is unknown.
3.0 Background
3.1 Property Information
According to the Mecklenburg County GIS website, the subject property consists of one 1.04-acre parcel owned
by Costar, LLC. The parcel is listed on the Mecklenburg County GIS with a parcel identification number (PIN)
05307120. The subject property is developed with a convenience store operated by LURE; LURE did not own or
operate the USTs. A Vicinity Map (Figure 1), USGS Topographic Map (Figure 2), and Site Map (Figure 3) are
included in Appendix I. The vicinity of the subject property is comprised of vacant and residential properties.
3.2 Project Background
On January 28, 2021, Mr. Ehab Aziz, LURE owner/operator, contacted Mr. James Wellons with S&ME, via
telephone, requesting a proposal for the closure of four USTs at the Former Snappy Food Mart property
addressed as 10100 Moores Chapel Road in Charlotte, Mecklenburg County, North Carolina. The removal of the
USTs was to prepare the site for development of a new petroleum retail station/convenience store.
Mr. Aziz provided S&ME with email correspondence between LURE and North Carolina Department of
Environmental Quality (NCDEQ). Included in the correspondence was an April 26, 2018, Phase I Environmental
Site Assessment (ESA) - Franklin’s Fast Stop & Jones Hardware, prepared by Enviro Probe, Inc. Based on the
review of a NCDEQ UST-10B form provided in the ESA:
the facility identification number is 00-0-0000031651,
the UST system consists of one 1,000 diesel UST, two 4,000-gallon gasoline USTs, and one 10,000-gallon
gasoline UST,
two 4,000-gallon gasoline USTs were installed in March 1975, one 10,000-gallon gasoline UST was
installed in March 1978, and one 1,000-gallon diesel UST was installed in March 1982,
and the USTs are constructed from single-wall steel.
S&ME’s services herein were conducted in general accordance with S&ME Proposal No. 211105 dated February 3,
2021.
4.0 Site History and Characterization
4.1 UST Information
Information regarding the former USTs is presented in Table 4-1.
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 3
Table 4-1: UST System Information
UST ID
Number
Capacity
(gallons)Contents Construction
Details
Tank
Dimensions
(Length x
Diameter)
Use Date Tank
Installed
Status of
UST
Release
Observed?
1 1,000 Diesel Single-wall steel /
fiberglass lined 6 x 5.33 feet Retail 3/30/1982 Removed
(3/31/2021) Yes
2 4,000 Gasoline Single-wall steel /
fiberglass lined 24 x 5.5 feet Retail 3/30/1975 Removed
(3/31/2021) Yes
3 4,000 Gasoline Single-wall steel /
fiberglass lined 24 x 5.5 feet Retail 3/30/1975 Removed
(3/31/2021) Yes
4 10,000 Gasoline Single-wall steel /
fiberglass lined 26 x 8 feet Retail 3/30/1978 Removed
(3/31/2021) Yes
4.2 Non-UST Information
Above ground storage tanks were not present at the subject property at the time of the UST closure assessment.
4.3 UST Owner and Operator Information
A January 26, 2021 email from Ms. Ruth Strauss of NCDEQ to Mr. Aziz states: “Based on our records, the Permits &
Inspection Branch of the UST Section finds that Costar, LLC is not a tank owner nor a tank operator. Costar owns
the property in which the UST systems are located. Because Costar is not a tank owner or a tank operator, we
have not invoiced it for tank fees nor enforced against it to bring the UST systems into compliance. Handy Dandy,
Inc. also known as Handy Dandy Food Stores Inc., was the last owner of the tanks. Handy Dandy, Inc. did not own
the property and no longer exists”.
4.4 Site Characteristics
Land Use: The site is currently developed as a convenience store that is operated by LURE. The property
is zoned as B-1; Business (neighborhood business).
Land Use of Surrounding Area: The site is located in a residential area of Charlotte, North Carolina. The
nearest single-family residence is located approximately 224 feet northwest of the release. Two adjacent
undeveloped properties are zoned B-1 (Business).
Topography: Based upon the topographic map reviewed (Figure 2, Appendix I), the area of the subject
property slopes downward to the west.
Surface Water: Based on a review of the Mecklenburg County Polaris 3G website
(https://polaris3g.mecklenburgcountync.gov/), the nearest downgradient surface water body is an
unnamed tributary to Long Creek Tributary 1 that is located approximately 2,045 feet west of the release
location.
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 4
Regional Geology: The property lies within the Charlotte Belt Geologic Province of North Carolina and is
underlain by metamorphosed quartz diorite; foliated to massive.
Potential Receptors: Based on-site observations and discussions with the property owner, no water
supply wells were observed in the vicinity of the subject property. Charlotte Mecklenburg Utility provides
water to the site and is available to surrounding properties.
5.0 UST Closure Services
S&ME conducted the closure activities in general accordance with the NCDEQ Guidelines for Site Checks, Tank
Closure, and Initial Response and Abatement, Petroleum and Hazardous Substance UST Releases, Petroleum Non-
UST Releases, Change 10, dated January 19, 2021 (hereinafter referred to as the UST Guidelines).
5.1 Pre-UST Closure Activities
A Notification of Intent:UST Permanent Closure or Change-in-Service form (UST-3) was submitted to the NCDEQ
Mooresville Regional Office (MRO) on March 2, 2021. The completed UST-3 Form is included in Appendix III.
Prior to the removal of the USTs, S&ME subcontracted GPRS to locate underground utilities, the USTs, and
associated product lines. S&ME subcontracted CCI to remove the UST system. Prior to the removal of the UST
system, CCI contacted North Carolina 811 to locate underground utilities and notified the Charlotte Fire
Department for a Fire Permit.
5.2 UST Closure Activities
Between March 30, 2021 and April 1, 2021, S&ME observed CCI during the removal of concrete, asphalt, and
overburden to expose the USTs and product piping. S&ME observed staining and petroleum odors following
removal of the asphalt/concrete surfaces around the USTs and product piping. S&ME periodically screened
overburden soils for volatile organic compounds (VOCs) with a calibrated MiniRAE 3000 photoionization detector
(PID). The PID readings for the excavated soils ranged from 89.4 to 10,056 parts per million (ppm); see Table 1 for
soil field screening results). No excavated soils were used as backfill due to elevated PID readings. CCI utilized a
vacuum truck to recover approximately 617 gallons of residual liquid and rinseate from UST-1 (diesel) and UST-2
through UST-4 (gasoline).
On March 31, 2021, CCI removed the USTs from the ground following UST vapor screening and Fire Marshal
approval. S&ME did not observe holes in the USTs following removal. The concrete/asphalt, recovered liquids,
USTs, and product piping were removed from the site for disposal by CCI (Appendix IV). Site photographs during
UST closure services are included in Appendix V.
Between March 30, 2021 and April 1, 2021, confirmation soil samples were collected within two feet below the
centerline of the USTs, the product lines, and former dispensers. S&ME screened confirmation soil samples for
VOCs with a PID. The PID readings for the confirmation soil samples ranged from 2.9 to 8,240 parts per million
(ppm; see Table 1 for soil field screening results). Groundwater was not observed in the base of the excavation.
The depth of the excavations ranged from five feet below the ground surface (ft-bgs) (diesel UST) to
approximately seven to eleven ft-bgs (gasoline USTs) The soil samples were placed in laboratory-supplied
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 5
containers, placed in ice-filled coolers, and shipped under chain of custody procedures to Eurofins for analysis of
Total Petroleum Hydrocarbons (TPH) Gasoline Range Organics (GRO) and TPH Diesel Range Organics (DRO) by
EPA Method 8015.
5.3 UST Closure Soil Analytical Results
TPH GRO or DRO was detected in the following soil samples at concentrations that exceed the respective State
Action Levels of 50 mg/kg for GRO and 100 mg/kg for DRO, respectively.
T-1/S-1: North end of UST-1 (TPH DRO – 620 mg/kg)
D-3: Diesel dispenser (TPH DRO – 200 mg/kg)
PL-1: Diesel product line (TPH GRO – 66 mg/kg)
T2/S3: South end of UST-2 (TPH GRO – 74 mg/kg)
T3/S1: North end of UST-3 (TPH GRO – 76 mg/kg)
T3/S3: South end of UST-3 (TPH GRO – 94 mg/kg)
A summary of the analytical results is included in Table 1, Appendix II and Figure 4, Appendix I.The laboratory
report is included in Appendix VI.
5.4 Description of Release
The closure soil sampling results indicate a release occurred in the vicinity of the diesel product dispenser and
piping, UST-1 (diesel) and UST-2 and UST-3 (gasoline). However, due to the tanks being lined and the lack of
holes observed in the USTs upon removal, it is believed that the release could be related to the product lines with
lateral flow of petroleum through backfill sands that were placed when the UST system was installed. A rainfall
event occurred on March 31, 2021 while the USTs were exposed prior to Fire Marshal approval for removal;
rainwater may have caused some petroleum migration.
On behalf of LURE, on March 31, 2021, submitted UST-61 24-Hour Release and UST Leak Reporting Form via email
to Mr. Dan Bowser and Mr. Ron Taraban of UST Section of the NCDEQ MRO. The UST-61 Form is included in
Appendix VII.
6.0 Site Check Report
A site check was not conducted as part of the authorized services provided by S&ME.
7.0 Free Product
No free product was encountered during these activities.
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 6
8.0 Initial Response and Abatement Action
8.1 Excavation of Contaminated Soil
On April 1, 2021, S&ME observed CCI’s over-excavation activities of petroleum-impacted soils that were in the
vicinity UST-2 through UST-4. During the soil excavation activities, S&ME monitored the excavated soils for
evidence of petroleum impacts by field screening, including observing for staining and odors and measuring
volatile organic vapors via a calibrated MiniRAE 3000 PID. Over-excavation was not performed in the vicinity of
UST-1 (diesel) and associated product line and dispenser due to low PID readings ranging from 2.9 to 38.8 ppm
and the close proximity of the site structure.
Abatement activities were attempted by excavating approximately two feet into the sidewalls of the excavation
that was conducted to remove the gasoline USTs and approximately five feet into the floor of the excavation or to
a depth of approximately 16 ft-bgs. When excavating into the floor of the excavation, groundwater was not
encountered. The USTs were removed and soil samples were collected between March 30, 2021 and April 1, 2021.
The approximate limits of the over-excavation for the basin of the gasoline USTs are shown on Figure 4,
Appendix I.
Between March 31, 2021 and April 1, 2021, CCI removed 209.16 tons of petroleum-impacted soils from the subject
property for disposal at Alternative Energy Solutions on NC, LLC (AES) in Thomasville, North Carolina. S&ME
collected one soil sample per truckload (L-1 through L-13) for analysis of TPH GRO. The PID readings for the
truckload soil samples ranged from 89.4 to 10,056 ppm; see Table 1 for soil field screening results. A summary of
the analytical results is included in Table 1,Appendix II and the laboratory report is included in Appendix VI. A
decision was made to discontinue over-excavation activities due to elevated PID readings and the concern that
the initial abatement actions of petroleum-impacted soil may not lead directly to closure of the subject incident.
The soil disposal manifests are included in Appendix VIII.
8.2 NCDEQ Correspondence During the Initial Abatement Actions
During the UST removal services on April 1, 2021, Mr. James Wellons with S&ME contacted Mr. Dan Bowser, the
Incident Manger with the NCDEQ, UST Section, Corrective Action Branch, by telephone to discuss the removal of
the petroleum-impacted soils and quantities of which may be removed. Mr. Bowser stated that up to 800 tons of
petroleum impacted soil could be removed from the property and another 400 tons could be approved if needed.
Mr. Bowser stated that one TPH DRO and/or TPH GRO soil sample would be needed for each truckload of
petroleum impacted soil.
8.3 Post-Excavation Confirmation Sampling Methodology
On April 1, 2021, S&ME collected confirmation soil samples from the sidewalls and floor of the final excavation
limits. The soil samples were collected from the bucket of the excavator. The PID readings for the over-
excavation soil samples ranged from 68.8 to 2,189 parts per million (ppm; see Table 1 for soil field screening
results). The collected soil samples were placed in laboratory-supplied containers, placed in ice-filled coolers, and
shipped under chain of custody procedures to Eurofins for analysis by VOCs using EPA Method 8260 and MADEP
VPH. The approximate locations of the confirmation soil samples are depicted on Figure 4,Appendix I. CCI
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 7
backfilled the excavation with clean fill obtained from C&M Recycling, Inc. Six inches of crushed aggregate base
coarse stone was placed to make the backfill flush with the existing asphalt parking lot. Backfill and based coarse
stone manifests are included in Appendix IX.
8.4 Soil Analytical Results
Multiple target analytes were detected in sidewall soil samples (SW-1A, SW-1B, SW-2B, SW-3A, SW-4A, and SW-
4B) and base samples (B-1 and B-2) associated with the gasoline UST basin abatement actions at concentrations
that exceed the Soil-to-Water Maximum Soil Contaminant Concentrations (MSCCs). Multiple target analytes were
detected in sidewall soil samples (SW-1A, SW-1B, SW-4A) associated with the gasoline UST basin abatement
actions at concentrations that exceed the Residential MSCCs. The concentration of naphthalene detected in
sidewall samples SW-1A and SW-4A exceeded the Industrial/Commercial MSCCs. A summary of the analytical
results is included in Table 1,Appendix II and the laboratory report is included in Appendix VI.
9.0 Sole Use Statement
All materials and information used for this project were obtained by S&ME. This report is provided for the sole
use of LURE. Use of this report by any parties other than LURE will be at such party's sole risk. S&ME disclaims
liability for any use of or reliance on this report by third parties.
10.0 Limitations
The assessment described herein represents the environmental conditions of the property at the date the samples
were collected for laboratory analysis. The assessment data does not represent the future environmental
conditions of the property and should not be construed in this manner.
11.0 Conclusions and Recommendations
The following summarizes the documented release and initial abatement actions:
Four fiberglass-lined single-walled steel USTs (one 1,000-gallon diesel, two 4,000-gallon gasoline, and
one 10,000-gallon gasoline) were removed from the site on March 31, 2021.
Petroleum odors and elevated PID readings were noted during excavation activities, and during the
collection of confirmation soil samples.
Confirmatory soil samples were collected from beneath the USTs, associated product lines, and
dispensers. TPH DRO and/or TPH-GRO were reported at concentrations above their respective action
levels beneath UST-1 (diesel), the diesel product line and dispenser, and UST-2 and UST-3 (gasoline).
Between March 31, 2021 and April 1, 2021, S&ME observed over-excavation activities of petroleum-
impacted soils within the basin of the gasoline USTs. Due to elevated PID readings and since the
initial abatement actions of petroleum-impacted soil may not lead directly to closure of the subject
incident, over-excavation of the petroleum-impacted soils was discontinued. Risk-based samples
were collected from the base and sidewalls of the excavation.
UST Closure Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
NCDEQ Incident No. TBD
May 4, 2021 8
Between March 31, 2021 and April 1, 2021, 209.16 tons of petroleum-impacted soils were transported
off site for disposal at AES.
Multiple target analytes were detected in sidewall soil samples (SW-1A, SW-1B, SW-2B, SW-3A, SW-
4A, and SW-4B) and base samples (B-1 and B-2) associated with the gasoline UST basin abatement
actions at concentrations that exceed the Soil-to-Water MSCCs.
Multiple target analytes were detected in sidewall soil samples (SW-1A, SW-1B, SW-4A) associated
with the gasoline UST basin abatement actions at concentrations that exceed the Residential MSCCs.
The concentration of naphthalene detected in sidewall samples SW-1A and SW-4A exceeded the
Industrial/Commercial MSCCs.
On March 31, 2021, S&ME submitted a UST-61 form to the UST Section of the NCDEQ, MRO.
A Site Investigation Report for Permanent Closure of Change-in-Service of Registered UST form (UST-
2A) is included as Appendix X.
LURE and Costar, LLC are not the Responsible Party and never owned or operated the UST system. The previous
owner of the UST system was Handy Dandy, Inc., also known as Handy Dandy Food Stores, Inc. Handy Dandy did
not own the property and no longer exists.
Appendices
Appendix I – Figures
^_
^_Project Location
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 1.0 miles
4-27-21Drawing Path: T:\ENV\Projects\2021\211105 LURE_UST Removal_Moores Chapel Rd\GIS\1_vicinity.mxd plotted by DHomans 04-27-2021VICINITY MAP
³
REFERENCE: ESRI STREETMAP USA DATASETTHIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEYINFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: Sources: Esri, HERE, Garmin, USGS,Intermap, INCREMENT P, NRCan, Esri Japan, METI, EsriChina (Hong Kong), Esri Korea, Esri (Thailand), NGCC, (c)
0 1 2Miles
211105
FORMER SNAPPY FOOD MART10100 MOORES CHAPEL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
^_
^_PROJECT LOCATION
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
21 " = 2,000 '
4-27-21Drawing Path: T:\ENV\Projects\2021\211105 LURE_UST Removal_Moores Chapel Rd\GIS\2_USGS TOPO.mxd plotted by DHomans 04-27-2021USGS TOPOGRAPHIC MAP
³
REFERENCE: USGS USA TOPO STREAMING DATASETGIS BASE LAYERS WERE OBTAINED FROM USGS NATIONAL MAP. THIS MAP IS FOR INFORMATIONALPURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASEDON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: USGS The National Map: NationalBoundaries Dataset, 3DEP Elevation Program, GeographicNames Information System, National Hydrography
0 2,000 4,000(FEET)
211105
FORMER SNAPPY FOOD MART10100 MOORES CHAPEL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
¦Former Dispenser
¦Approx. FormerDispenser Locations
UST 1
UST 2
UST 3
UST 4
¦Approx. FormerDispenser Locations
BELMEADEDR
UNDERGROUND STORAGE TANKS (REMOVED)
APPROXIMATE EXCAVATION AREAS
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
31 " = 30 '
4-28-21
211105
FORMER SNAPPY FOOD MART10100 MOORES CHAPEL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINADrawing Path: T:\ENV\Projects\2021\211105 LURE_UST Removal_Moores Chapel Rd\GIS\3_SiteMap.mxd plotted by DHomans 04-28-2021SITE MAP
³
REFERENCE: 2020 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM MECKLENBURG COUNTY. ALL FEATURELOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVILSURVEY INFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: MeckCoGIS
0 30 60(FEET)
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D-3 (@2.5' BGS)TPH DRO: 200
T1/S1 (@5' BGS)TPH DRO: 620
T1/S2 (@5' BGS)All < State Action Levels
PL-1 (@1.67' BGS)TPH GRO: 66
T2/S1 (@7.5' BGS)All < State Action Levels
T2/S2 (@7.5' BGS)All < State Action Levels T2/S3 (@7.5' BGS)TPH GRO: 74
D-1 (@2.5' BGS)All < State Action Levels
D-2 (@2.5' BGS)All < State Action Levels
PL-2 (@1.67' BGS)All < State Action Levels
SW-1B (@12' BGS)2-Hexanone: 2.3 J4-Isopropyltoluene: 0.450 JNaphthalene: 16n-Propylbenzene: 3.41,2,4-Trimethylbenzene: 371,3,5-Trimethylbenzene: 13Total Xylenes: 16C5 - C8 Aliphatics: 140C9 - C22 Aromatics: 340
B-1 (@16' BGS)Ethylene Dibromide: 0.0025 J1,2-Dichloroethane: 0.0048 J2-Hexanone: 0.18Methyl tert-butyl ether: 0.13
T3/S2 (@7.5' BGS)All < State Action Levels
T3/S1 (@7.5' BGS)TPH GRO: 76
SW-2A (@12' BGS)All < MSCCs
SW-2B (@12' BGS)Benzene: 0.049 J2-Hexanone: 0.910 J4-Isopropyltoluene: 0.160 JNaphthalene: 2.61,2,4-Trimethylbenzene: 9.9C9 - C22 Aromatics: 130
SW-4B (@12' BGS)Ethylene Dibromide: 0.0015 J
T4/S2 (@11' BGS)All < State Action Levels
T4/S1 (@11' BGS)All < State Action Levels
T4/S3 (@11' BGS)All < State Action Levels
SW-3B (@12' BGS)All < MSCCs
SW-3A (@12' BGS)Ethylene Dibromide: 0.0013 J
B-2 (@16' BGS)Ethylene Dibromide: 0.0017 J1,2-Dichloroethane: 0.0032 J2-Hexanone: 0.18
SW-4A (@12' BGS)Benzene: 3.2 Jsec-Butylbenzene: 25Ethylbenzene: 1402-Hexanone: 180Isopropylbenzene: 424-Methyl-2-pentanone (MIBK): 28 JNaphthalene: 200n-Propylbenzene: 150Toluene: 1201,2,4-Trimethylbenzene: 4501,3,5-Trimethylbenzene: 140Total Xylenes: 600C5 - C8 Aliphatics: 2,500C9 - C18 Aliphatics : 3,700C9 - C22 Aromatics: 4,900
T3/S3 (@7.5' BGS)TPH GRO: 94
SW-1A (@12' BGS)sec-Butylbenzene: 7.52-Hexanone: 16 JIsopropylbenzene: 8.34-Methyl-2-pentanone (MIBK): 5.0 JNaphthalene: 67n-Propylbenzene: 34Toluene: 151,2,4-Trimethylbenzene: 1101,3,5-Trimethylbenzene: 110Total Xylenes: 240C5 - C8 Aliphatics: 720C9 - C22 Aromatics: 1,500
UST (REMOVED)
APPROXIMATE EXCAVATION AREAS
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
41 " = 13 '
4-28-21
211105
FORMER SNAPPY FOOD MART10100 MOORES CHAPEL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINADrawing Path: T:\ENV\Projects\2021\211105 LURE_UST Removal_Moores Chapel Rd\GIS\4_soilquality.mxd plotted by DHomans 04-28-2021SOIL QUALITY MAP
³
Service Layer Credits: MeckCoGIS
0 10 20(FEET)
NOTES:J = Estimated concentration between method detection limit and practical quantitation limit
BGS= Below Ground Surface
Closure samples were assessed for total petroleum hydrocarbons (TPH) diesel range organics(DRO) and gasoline range organics (GRO). Concentrations exceeding the North CarolinaUnderground Storage Tank (UST) Action Level are shown above in milligrams per kilogram(mg/kg).
Over-excavation samples were assessed for volatile organic compounds (VOCs) and volatilepetroleum hydrocarbons (VPH). Concentrations exceeding the North Carolina Soil-to-Groundwater Maximum Soil Contaminant Concentration Levels (MSCCs) are shown above inmg/kg.Concentrations exceeding the Residential MSCCs are shown in BoldConcentrations exceeding the Industrial/Commercial MSCCs are shown in Red
Appendix II – Tables
Sample
Category Sample ID Location
Date
Collected
Sample
Depth
(ft-bgs)
PID
Reading
(PPM)BenzeneBromomethane2-Butanone (MEK)2-ChlorotolueneCyclohexaneEthylene Dibromide1,2-DichloroethaneEthyl ethern-HeptaneHexane2-HexanoneIodomethane4-IsopropyltolueneMethyl acetateMethylcyclohexane2-Methyl-2-propanol Tolueneo-Xylenem-Xylene & p-XyleneT-1/S-1 North end of UST-1 3/30/2021 5 2.9 620 2.8
T-1/S-2 South end of UST-1 3/30/2021 5 22.9 7.3 2.9
PL-1 Diesel product line 4/1/2021 1.67 31.7 58 66
D-3 Diesel dispenser 4/1/2021 2.5 28.3 200 2.7 J
T2/S1 North end of UST-2 3/31/2021 7.5 8,204 NR 5.1
T2/S2 Center of UST-2 3/31/2021 7.5 385.7 NR 16
T2/S3 South end of UST-2 3/31/2021 7.5 2,840.70 NR 74
T3/S1 North end of UST-3 3/31/2021 7.5 347.6 NR 76
T3/S2 Center of UST-3 3/31/2021 7.5 194.5 NR 5.1 J
T3/S3 South end of UST-3 3/31/2021 7.5 137.4 NR 94
T4/S1 North end of UST-4 3/31/2021 11 183.4 NR 3.2
T4/S2 Center of UST-4 3/31/2021 11 182.3 NR 4.5
T4/S3 South end of UST-4 3/31/2021 11 210.2 NR 3.5
PL-2 Gasoline product line 4/1/2021 1.67 37.5 NR 3.6 J
D-1 Gasoline dispener 1 4/1/2021 2.5 28.8 NR 3.1 J
D-2 Gasoline dispener 2 4/1/2021 2.5 36.5 NR 18
L-1 Sample from truck 1 3/31/2021 --89.4 NR 770
L-2 Sample from truck 2 3/31/2021 --130.3 NR 400
L-3 Sample from truck 3 4/1/2021 --4,656 NR 3,400
L-4 Sample from truck 4 4/1/2021 --674.7 NR 470
L-5 Sample from truck 5 4/1/2021 --759.4 NR 140
L-6 Sample from truck 6 4/1/2021 --234.6 NR 97
L-7 Sample from truck 7 4/1/2021 --4,186 NR 1,700
L-8 Sample from truck 8 4/1/2021 --10,056 NR 1,900
L-9 Sample from truck 9 4/1/2021 --359.6 NR 90
L-10 Sample from truck 10 4/1/2021 --958.7 NR 1,800
L-11 Sample from truck 11 4/1/2021 --589.5 NR 680
L-12 Sample from truck 12 4/1/2021 --1,193 NR 66
L-13 Sample from truck 13 4/1/2021 --3,647 NR 8.8
SW-1A Base of W sidewall 1 4/1/2021 12 1,919 <8.7 <0.45 <0.87 7.5 <4.0 31 <0.63 <0.67 <0.55 25 <0.67 3.6 <0.8 16 J <2.3 8.3 NR 5.0 J <3.1 4.8 <5.3 <0.67 67 34 15 110 110 87 150 240 720 520 1,500
SW-1B Base of W sidewall 2 4/1/2021 12 2,189 <1.6 <0.084 <0.31 1.0 <0.75 <0.13 <0.12 <0.13 <0.1 1.9 <0.13 <0.31 <0.15 2.3 J <0.43 0.770 0.450 J <0.63 <0.58 0.380 J 1.2 J <0.13 16 3.4 0.82 37 13 7.4 8.6 16 140 170 340
SW-2A Base of N sidewall 1 4/1/2021 12 84.5 0.18 <0.0085 <0.0032 <0.0012 0.025 J <0.0032 <0.0012 <0.0013 <0.001 <0.00078 <0.0013 <0.0032 <0.0015 0.0077 J <0.0043 <0.00087 <0.0013 <0.0064 <0.0059 <0.0019 0.16 0.0042 J 0.0099 <0.0011 <0.0013 0.0039 J 0.0016 J <0.0013 <0.0017 <0.0024 4.1 2.1 3.6
SW-2B Base of N sidewall 2 4/1/2021 12 384.9 <0.65 0.049 J <0.13 0.140 J <0.3 <0.13 <0.047 <0.05 <0.041 0.56 <0.05 0.5 0.27 0.910 J 0.4 0.160 J 0.160 J <0.25 0.27 0.210 J <0.4 <0.05 2.6 0.63 0.56 9.9 3.3 1.9 3.2 5 54 63 130
SW-3A Base of E sidewall 1 4/1/2021 12 301.6 0.2 0.0012 J <0.0017 <0.0013 0.073 <0.0033 <0.0013 0.0013 J 0.0017 J 0.0025 J <0.0013 <0.0033 <0.0016 0.021 J <0.0045 <0.00091 <0.0013 0.0072 J <0.0061 <0.002 0.21 0.04 0.0056 J 0.0013 J 0.007 0.011 0.0047 J 0.011 0.013 0.024 4.2 2.2 1.2
SW-3B Base of E sidewall 2 4/1/2021 12 201.7 0.28 <0.00081 0.013 <0.0012 0.13 <0.003 <0.0011 <0.0012 0.0014 J <0.00074 <0.0012 <0.003 <0.0015 0.045 0.43 <0.00083 <0.0012 0.012 J <0.0056 <0.0018 1.1 0.04 0.0062 <0.0011 <0.0012 0.0028 J 0.0016 J <0.0012 <0.0016 0.0024 J 4.1 2.1 1.1
SW-4A Base of S sidewall 1 4/1/2021 12 1,882 <16 3.2 J <1.6 25 <7.3 140 8.2 <1.2 <1.0 140 <1.2 57 7.3 180 <4.1 42 NR 28 J <5.6 66 <9.8 <1.2 200 150 120 450 140 220 380 600 2,500 3,700 4,900
SW-4B Base of S sidewall 2 4/1/2021 12 68.8 0.077 <0.00085 <0.0032 <0.0012 0.022 J <0.0032 <0.0012 0.0015 J 0.0015 J 0.0014 J <0.0013 <0.0032 <0.0015 0.027 J <0.0043 0.00091 J <0.0013 0.0089 J <0.0058 <0.0019 0.66 0.024 0.022 0.0013 J 0.0025 J 0.019 0.0073 0.0086 0.006 J 0.015 4.1 2.1 2.2
B-1 Base of UST basin 1 4/1/2021 16 731.3 1.2 0.0012 J <0.003 0.0047 J 0.59 <0.003 <0.0011 0.0025 J 0.0048 J 0.0012 J 0.0022 J <0.003 <0.0014 0.18 0.0058 J 0.0016 J 0.0019 J 0.042 <0.0055 <0.0018 0.32 0.13 0.037 0.0031 J 0.0028 J 0.038 0.018 0.0084 0.0055 J 0.014 4.3 3.3 4.9
B-2 Base of UST basin 2 4/1/2021 16 384.2 1.2 <0.00095 <0.0036 <0.0014 0.65 <0.0036 <0.0013 0.0017 J 0.0032 J 0.0011 J 0.0015 J <0.0036 <0.0017 0.18 <0.0048 <0.00097 0.0014 J 0.029 J <0.0066 <0.0021 2.7 0.083 0.0061 J <0.0013 0.0027 J 0.0042 J 0.004 J 0.0054 J 0.0047 J 0.010 J 5.4 2.8 1.6
100 50 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 24 0.0072 0.047 2.2 16 NE NE 0.000096 0.0019 8 NE NE NE 0.17 NE 1.3 0.12 0.42 NE NE NE 0.085 0.2 1.4 5.4 6.6 6.6 NE NE 6.0 68 540 31
NE NE 14,000 12 21 1,560 9,380 NE NE 0.33 7.29 60.3 NE NE NE 78.2 NE 1,560 1,560 1,250 NE NE NE 156 5.5 1,560 1,250 156 156 NE NE 3,120 939 1,500 469
NE NE 360,000 59.4 327 23,300 140,000 NE NE 1.63 35.9 297 NE NE NE 1,160 NE 23,300 23,300 18,600 NE NE NE 1,810 27 23,300 18,600 2,330 2,330 NE NE 46,700 24,528 40,000 12,264
Notes:
Concentrations are reported in milligrams per kilograms (mg/Kg)NE = not established
ft-bgs = feet below ground surface NR = not reported
Only constituents detected above the laboratory detection limit are shown MADEP - VPH = Massachusetts Department of Environmental Protection - Voliatile Petroleum Hydrocarbons
Concentrations exceeding the North Carolina Underground Storage Tank (UST) Action Level or Soil-to-Water are shown in Bold fields EPH = Extractable Petroleum Hydrocarbons
Concentrations exceeding the Soil to Groundwater Maximum Soil Contaminant Concentration Levels (MSCCs) are shown in Bold Italicized fields J = Concentration is an estimated value
Concentrations exceeding the Industrial/Commercial Maximum Soil Contaminant Concentration Levels (MSCCs) are shown in Bold Italicized and shaded fields TPH = Total Petroleum Hydrocarbons
MDL = Laboratory Method Detection Limit
PPM = Parts per million
North Carolina UST Section Action Level
Soil to Groundwater MSCC
Residential MSCC
Industrial/Commercial MSCC
Gasoline
UST System
Truckload
Samples
Not Analyzedn-PropylbenzeneNot AnalyzedEthylbenzeneIsopropylbenzenesec-Butylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesC5 - C8 AliphaticsC9 - C18 Aliphatics C9 - C22 Aromatics4-Methyl-2-pentanone (MIBK)Methyl tert-butyl etherNaphthaleneNot AnalyzedOver-
Excavation
Samples
Diesel UST System AcetoneDiesel Range OrganicsGasoline Range OrganicsContaminant of Concern
TABLE 1
Summary of Soil Sampling Results
Former Snappy Food Mart10100 Moores Chapel RoadCharlotte, Mecklenburg County, North CarolinaS&ME Project No. 211105
TPH by EPA
Method 8015
VPH by MADEP Method
(mg/kg)Volatile Organic Compounds by EPA Method 8260D (mg/kg)Analytical Method
Appendix III – NCDEQ UST-3 Form
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY
I.D. #_____________________
Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities. If a Professional Engineer (P.E.) or a Licensed
Geologist (L.G.) provides supervision for closure or change-in-service site assessment activities and signs and seals all closure reports then at least a five
(5) working days’ notice is acceptable.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted to the
appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be
submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out.
Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank Closure
and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust. Note: To close tanks in place you must
obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
’,6.= %,6.=# (6-$ !0785/8 +)* 7;6/8 67 4761/8 /<29:9"
Facility Name or Company
Former Snappy Food Mart
Street Address Facility ID # (If known)
00-0-0000031651
City County Street Address
10100 Moores Chapel Road
State Zip Code City
Charlotte
County
Mecklenburg
Zip Code
28214
Phone Number
704-506-6137
Email
[e-mail] Phone Number
5066137
III. CONTACT PERSONNEL
Name:
Ehab Aziz
Company Name:
LURE
Job Title:
Owner/Operator
Phone Number:
5066137
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1. Contact local fire marshal.
2. Plan entire closure event.
3. Conduct Site Soil Assessment.
4. If removing tanks or closing in place, refer to
API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5. Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7. If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G.
is not required.
8. Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name: Contractor Company Name:
CCI Environmental Services
Address:
281 Lane Parkway, Salisbury
State:
NC
Zip Code:
28146
Phone No:
704-273-1500
Primary Consultant Name:
James Wellons
Primary Consultant Company Name:
S&ME, Inc.
Consultant Phone No:
704-302-4399
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE
Tank ID No.Size in Gallons Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place *New Contents Stored
1 4000 Gasoline, Gas Mix
2 4000 Gasoline, Gas Mix
3 10000 Gasoline, Gas Mix
4 1000 Dielsel, Dielsel Mix
*Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER’S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title: James Wellons, Senior Project Geologist
Signature Date Signed
2/25/2021
SCHEDULED REMOVAL DATE
3/"!/2021
Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 3/2020
LURE wants to remove the USTs but never owned/operated
Appendix IV – Liquid, Concrete/Asphalt, and USTs Disposal
Manifests
/ Former Snappy Food MartCCI Environmental Services, Inc.281 Lane ParkwaySalisbury, NC 28146
/ Former Snappy Food MartCCI Environmental Services, Inc.281 Lane ParkwaySalisbury, NC 28146
CCI Environmental Services, Inc.281 Lane ParkwaySalisbury, NC 28146/Former Snappy Food Mart
/ Former Snappy Food MartCCI Environmental Services, Inc.281 Lane ParkwaySalisbury, NC 28146
Appendix V – Site Photographs
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 i Date:3/30/2021Photographer: J. WellonsLocation / Orientation Northeast side of site structure / Facing north
Remarks View of AST-1 (diesel) Date: 3/30/2021Photographer: M. BrundageLocation / Orientation Southeast side of site structure / Facing north
Remarks Removal of aphalt/concrete over UST-2 through
UST-4 (gasoline)
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 ii Date: 3/30/2021Photographer: M. BrundageLocation / Orientation Southeast side of site structure / Facing north
Remarks Removal of piping over gasoline USTs Date: 3/30/2021Photographer: M. BrundageLocation / Orientation Southeast side of site structure / Facing east
Remarks View of gasoline USTs
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 iii Date: 3/30/2021Photographer: M. BrundageLocation / Orientation Southeast side of site structure / Facing north
Remarks View of UST-2 through UST-4 (gasoline) Date: 4/1/2021Photographer: M. Brundage6 Location / Orientation Adjacent to northeast of site structure
Remarks Former location of diesel dispenser
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 iv Date: 4/1/2021Photographer: M. Brundage7 Location / Orientation Gasoline UST basin
Remarks Soil below UST-4 (10,000-gallon gasoline) Date: 4/1/2021Photographer: M. Brundage8 Location / Orientation Northeast side of site structure / Facing west
Remarks View of former location of UST-1 (diesel)
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 v Date: 4/1/2021Photographer: M. Brundage9 Location / Orientation Southeast side of site structure
Remarks Former gasoline dispenser area with backfill. Date: 4/1/2021Photographer: M. Brundage10 Location / Orientation Southeast side of site structure / Facing north
Remarks Backfill of gasoline UST basin
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 vi Date: 4/1/2021Photographer: M. Brundage 11 Location / Orientation Southeast side of site structure / Facing north
Remarks Back fill of gasoline UST basin Date: 4/2/2021Photographer: J. Wellons 12
Location / Orientation Northeast side of site structure/ facing west
Remarks Former location of UST-1 (diesel) and dispenser
Underground Storage Tank Closure and Initial Abatement Report
Former Snappy Food Mart
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211105
April 22, 2021 vii Date: 4/2/2021Photographer: J. Wellons 13 Location / Orientation Southeast side of site structure / Facing southwest
Remarks Former location of UST-2 through UST-4
(gasoline) and dispensers. Date: 4/2/2021Photographer: J. Wellons 14 Location / Orientation Southeast side of site structure / Facing west
Remarks Former location of UST-1 through UST-4
Appendix VI – Soil Laboratory Report
ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-201537-1
Laboratory Sample Delivery Group: Lure Moores Chapel
Client Project/Site: LURE
For:
S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, North Carolina 28273
Attn: James Wellons
Authorized for release by:
4/15/2021 7:54:30 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: S&ME, Inc.
Project/Site: LURE
Laboratory Job ID: 400-201537-1
SDG: Lure Moores Chapel
Page 2 of 116 Eurofins TestAmerica, Pensacola4/15/2021
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .72
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .73
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .76
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .92
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .111
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .112
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .116
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Case Narrative
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Job ID: 400-201537-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-201537-1
Comments
No additional comments.
Receipt
The samples were received on 4/3/2021 9:40 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 0.0º C, 0.0º C, 0.4º C and 1.1º C.
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-527343 recovered above the upper control limit for
1,2,4-Trichlorobenzene, 4-Isopropyltoluene, Hexachlorobutadiene, Iodomethane and n-Butylbenzene. The samples associated with this
CCV were below the reporting limit or not reported for the affected analytes; therefore, the data have been reported.
Method 8260D: The laboratory control sample (LCS) for preparation batch 400-527442 and analytical batch 400-527343 recovered outside
control limits for the following analytes: n-Butylbenzene. These analytes were biased high in the LCS and were not detected in the
associated samples; therefore, the data have been reported.
Method 8260D: The following samples were diluted to bring the concentration of target analytes within the calibration range: SW-1A
(400-201537-25), SW-1B (400-201537-26), SW-2B (400-201537-28) and SW-4A (400-201537-31). Elevated reporting limits (RLs) are
provided.
Method 8260D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-527442 and analytical batch
400-527343 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
Method 8015C: The following samples were diluted because the base dilution for methanol preserved is 1:50: T-1/S-1 (400-201537-1),
T-1/S-2 (400-201537-2), T2/S1 (400-201537-3), T2/S2 (400-201537-4), T2/S3 (400-201537-5), T3/S1 (400-201537-6), T3/S2
(400-201537-7), T3/S3 (400-201537-8), T4/S1 (400-201537-9), T4/S2 (400-201537-10), T4/S3 (400-201537-11), L-13 (400-201537-12),
L-5 (400-201537-17), L-6 (400-201537-18),L-9 (400-201537-21), L-12 (400-201537-24), PL-1 (400-201537-35), PL-2 (400-201537-36),
D-1 (400-201537-37), D-2 (400-201537-38) and D-3 (400-201537-39)
Method 8015C: The following samples were diluted to bring the concentration of target analytes within the calibration range: L-1
(400-201537-13), L-2 (400-201537-14), L-3 (400-201537-15), L-4 (400-201537-16), L-7 (400-201537-19), L-8 (400-201537-20), L-10
(400-201537-22) and L-11 (400-201537-23). Elevated reporting limits (RLs) are provided.
Method MAVPH: The following samples were diluted because the base dilution for VPH soil analysis is 1:50.SW-2A (400-201537-27),
SW-3A (400-201537-29), SW-3B (400-201537-30), SW-4B (400-201537-32), B-1 (400-201537-33) and B-2 (400-201537-34)
Method MAVPH: The following samples were diluted to bring the concentration of target analytes within the calibration range: SW-1A
(400-201537-25), SW-1B (400-201537-26), SW-2B (400-201537-28) and SW-4A (400-201537-31). Elevated reporting limits (RLs) are
provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method 8015C: The following samples were diluted due to color and odor: T-1/S-1 (400-201537-1) and D-3 (400-201537-39). Elevated
reporting limits (RL) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
Eurofins TestAmerica, PensacolaPage 3 of 116 4/15/2021
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Case Narrative
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Job ID: 400-201537-1 (Continued)
Laboratory: Eurofins TestAmerica, Pensacola (Continued)
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: T-1/S-1 Lab Sample ID: 400-201537-1
☼C10-C28
RL
27 mg/Kg
MDL
11
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA56208015C
Client Sample ID: T-1/S-2 Lab Sample ID: 400-201537-2
☼C10-C28
RL
6.3 mg/Kg
MDL
2.5
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA17.3 8015C
Client Sample ID: T2/S1 Lab Sample ID: 400-201537-3
No Detections.
Client Sample ID: T2/S2 Lab Sample ID: 400-201537-4
☼C6-C10
RL
7700 ug/Kg
MDL
3800
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50160008015C
Client Sample ID: T2/S3 Lab Sample ID: 400-201537-5
☼C6-C10
RL
7900 ug/Kg
MDL
3900
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50740008015C
Client Sample ID: T3/S1 Lab Sample ID: 400-201537-6
☼C6-C10
RL
7200 ug/Kg
MDL
3600
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50760008015C
Client Sample ID: T3/S2 Lab Sample ID: 400-201537-7
☼C6-C10
RL
7700 ug/Kg
MDL
3900
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50J51008015C
Client Sample ID: T3/S3 Lab Sample ID: 400-201537-8
☼C6-C10
RL
6200 ug/Kg
MDL
3100
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50940008015C
Client Sample ID: T4/S1 Lab Sample ID: 400-201537-9
No Detections.
Client Sample ID: T4/S2 Lab Sample ID: 400-201537-10
No Detections.
Client Sample ID: T4/S3 Lab Sample ID: 400-201537-11
No Detections.
Client Sample ID: L-13 Lab Sample ID: 400-201537-12
☼C6-C10
RL
7700 ug/Kg
MDL
3800
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5088008015C
Client Sample ID: L-1 Lab Sample ID: 400-201537-13
☼C6-C10
RL
39000 ug/Kg
MDL
20000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2507700008015C
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
Page 5 of 116 4/15/2021
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: L-2 Lab Sample ID: 400-201537-14
☼C6-C10
RL
30000 ug/Kg
MDL
15000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2004000008015C
Client Sample ID: L-3 Lab Sample ID: 400-201537-15
☼C6-C10
RL
90000 ug/Kg
MDL
45000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50034000008015C
Client Sample ID: L-4 Lab Sample ID: 400-201537-16
☼C6-C10
RL
23000 ug/Kg
MDL
11000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2004700008015C
Client Sample ID: L-5 Lab Sample ID: 400-201537-17
☼C6-C10
RL
9500 ug/Kg
MDL
4800
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA501400008015C
Client Sample ID: L-6 Lab Sample ID: 400-201537-18
☼C6-C10
RL
9200 ug/Kg
MDL
4600
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50970008015C
Client Sample ID: L-7 Lab Sample ID: 400-201537-19
☼C6-C10
RL
80000 ug/Kg
MDL
40000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50017000008015C
Client Sample ID: L-8 Lab Sample ID: 400-201537-20
☼C6-C10
RL
98000 ug/Kg
MDL
49000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50019000008015C
Client Sample ID: L-9 Lab Sample ID: 400-201537-21
☼C6-C10
RL
6600 ug/Kg
MDL
3300
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50900008015C
Client Sample ID: L-10 Lab Sample ID: 400-201537-22
☼C6-C10
RL
140000 ug/Kg
MDL
68000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100018000008015C
Client Sample ID: L-11 Lab Sample ID: 400-201537-23
☼C6-C10
RL
140000 ug/Kg
MDL
70000
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10006800008015C
Client Sample ID: L-12 Lab Sample ID: 400-201537-24
☼C6-C10
RL
5800 ug/Kg
MDL
2900
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50660008015C
Client Sample ID: SW-1A Lab Sample ID: 400-201537-25
☼sec-Butylbenzene
RL
3300 ug/Kg
MDL
630
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50075008260D
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
Page 6 of 116 4/15/2021
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: SW-1A (Continued)Lab Sample ID: 400-201537-25
☼2-Chlorotoluene
RL
3300 ug/Kg
MDL
1700
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA500310008260D
☼Ethylbenzene 3300 ug/Kg410 Total/NA500250008260D
☼2-Hexanone 17000 ug/Kg3300 Total/NA50016000J8260D
☼Isopropylbenzene 3300 ug/Kg450 Total/NA50083008260D
☼4-Methyl-2-pentanone (MIBK)17000 ug/Kg3300 Total/NA5005000J8260D
☼Naphthalene 3300 ug/Kg1300 Total/NA500670008260D
☼N-Propylbenzene 3300 ug/Kg600 Total/NA500340008260D
☼Toluene 3300 ug/Kg670 Total/NA500150008260D
☼1,3,5-Trimethylbenzene 3300 ug/Kg550 Total/NA5001100008260D
☼o-Xylene 3300 ug/Kg670 Total/NA500870008260D
☼m-Xylene & p-Xylene 3300 ug/Kg870 Total/NA5001500008260D
☼Xylenes, Total 6700 ug/Kg1300 Total/NA5002400008260D
☼Methylcyclohexane 3300 ug/Kg1000 Total/NA50048008260D
☼n-Heptane 3300 ug/Kg1700 Total/NA50036008260D
☼1,2,4-Trimethylbenzene - DL 6700 ug/Kg1300 Total/NA10001100008260D
☼C9-C12 Aliphatics 370 mg/Kg370 Total/NA10000520MAVPH
☼C9-C10 Aromatics 200 mg/Kg200 Total/NA100001500MAVPH
Client Sample ID: SW-1B Lab Sample ID: 400-201537-26
☼sec-Butylbenzene
RL
630 ug/Kg
MDL
120
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10010008260D
☼Ethylbenzene 630 ug/Kg76 Total/NA10019008260D
☼2-Hexanone 3100 ug/Kg630 Total/NA1002300J8260D
☼Isopropylbenzene 630 ug/Kg85 Total/NA1007708260D
☼4-Isopropyltoluene 630 ug/Kg130 Total/NA100450J8260D
☼Naphthalene 630 ug/Kg250 Total/NA100160008260D
☼N-Propylbenzene 630 ug/Kg110 Total/NA10034008260D
☼Toluene 630 ug/Kg130 Total/NA1008208260D
☼1,2,4-Trimethylbenzene 630 ug/Kg130 Total/NA100370008260D
☼1,3,5-Trimethylbenzene 630 ug/Kg100 Total/NA100130008260D
☼o-Xylene 630 ug/Kg130 Total/NA10074008260D
☼m-Xylene & p-Xylene 630 ug/Kg160 Total/NA10086008260D
☼Xylenes, Total 1300 ug/Kg240 Total/NA100160008260D
☼Methylcyclohexane 630 ug/Kg190 Total/NA100380J8260D
☼2-Methyl-2-propanol 1300 ug/Kg1000 Total/NA1001200J8260D
☼C9-C12 Aliphatics 70 mg/Kg70 Total/NA2000170MAVPH
☼C9-C10 Aromatics 38 mg/Kg38 Total/NA2000340MAVPH
Client Sample ID: SW-2A Lab Sample ID: 400-201537-27
☼Acetone
RL
32 ug/Kg
MDL
17
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11808260D
☼2-Butanone (MEK)32 ug/Kg7.7 Total/NA125J8260D
☼2-Hexanone 32 ug/Kg6.4 Total/NA17.7 J 8260D
☼Methyl tert-butyl ether 6.4 ug/Kg1.3 Total/NA14.2 J 8260D
☼Naphthalene 6.4 ug/Kg2.6 Total/NA19.9 8260D
☼1,2,4-Trimethylbenzene 6.4 ug/Kg1.3 Total/NA13.9 J 8260D
☼1,3,5-Trimethylbenzene 6.4 ug/Kg1.1 Total/NA11.6 J 8260D
☼2-Methyl-2-propanol 13 ug/Kg10 Total/NA11608260D
☼C9-C10 Aromatics 1.1 mg/Kg1.1 Total/NA503.6 MAVPH
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: SW-2B Lab Sample ID: 400-201537-28
☼Benzene
RL
250 ug/Kg
MDL
34
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50J498260D
☼sec-Butylbenzene 250 ug/Kg48 Total/NA50140J8260D
☼Ethylbenzene 250 ug/Kg31 Total/NA505608260D
☼2-Hexanone 1300 ug/Kg250 Total/NA50910J8260D
☼Iodomethane 250 ug/Kg170 Total/NA504008260D
☼Isopropylbenzene 250 ug/Kg34 Total/NA50160J8260D
☼4-Isopropyltoluene 250 ug/Kg50 Total/NA50160J8260D
☼Naphthalene 250 ug/Kg100 Total/NA5026008260D
☼N-Propylbenzene 250 ug/Kg45 Total/NA506308260D
☼Toluene 250 ug/Kg50 Total/NA505608260D
☼1,2,4-Trimethylbenzene 250 ug/Kg50 Total/NA5099008260D
☼1,3,5-Trimethylbenzene 250 ug/Kg42 Total/NA5033008260D
☼o-Xylene 250 ug/Kg50 Total/NA5019008260D
☼m-Xylene & p-Xylene 250 ug/Kg65 Total/NA5032008260D
☼Xylenes, Total 500 ug/Kg96 Total/NA5050008260D
☼Methyl acetate 250 ug/Kg230 Total/NA502708260D
☼Methylcyclohexane 250 ug/Kg75 Total/NA50210J8260D
☼Hexane 250 ug/Kg60 Total/NA502708260D
☼n-Heptane 250 ug/Kg130 Total/NA505008260D
☼C9-C12 Aliphatics 28 mg/Kg28 Total/NA100063MAVPH
☼C9-C10 Aromatics 15 mg/Kg15 Total/NA1000130MAVPH
Client Sample ID: SW-3A Lab Sample ID: 400-201537-29
☼Acetone
RL
33 ug/Kg
MDL
17
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12008260D
☼Benzene 6.7 ug/Kg0.89 Total/NA11.2 J 8260D
☼2-Butanone (MEK)33 ug/Kg8.0 Total/NA1738260D
☼Ethylene Dibromide 6.7 ug/Kg1.3 Total/NA11.3 J 8260D
☼1,2-Dichloroethane 6.7 ug/Kg1.1 Total/NA11.7 J 8260D
☼Ethylbenzene 6.7 ug/Kg0.81 Total/NA12.5 J 8260D
☼2-Hexanone 33 ug/Kg6.7 Total/NA121J8260D
☼4-Methyl-2-pentanone (MIBK)33 ug/Kg6.7 Total/NA17.2 J 8260D
☼Methyl tert-butyl ether 6.7 ug/Kg1.3 Total/NA1408260D
☼Naphthalene 6.7 ug/Kg2.7 Total/NA15.6 J 8260D
☼N-Propylbenzene 6.7 ug/Kg1.2 Total/NA11.3 J 8260D
☼Toluene 6.7 ug/Kg1.3 Total/NA17.0 8260D
☼1,2,4-Trimethylbenzene 6.7 ug/Kg1.3 Total/NA1118260D
☼1,3,5-Trimethylbenzene 6.7 ug/Kg1.1 Total/NA14.7 J 8260D
☼o-Xylene 6.7 ug/Kg1.3 Total/NA1118260D
☼m-Xylene & p-Xylene 6.7 ug/Kg1.7 Total/NA1138260D
☼Xylenes, Total 13 ug/Kg2.5 Total/NA1248260D
☼2-Methyl-2-propanol 13 ug/Kg11 Total/NA12108260D
Client Sample ID: SW-3B Lab Sample ID: 400-201537-30
☼Acetone
RL
30 ug/Kg
MDL
16
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12808260D
☼Bromomethane 6.1 ug/Kg3.0 Total/NA1138260D
☼2-Butanone (MEK)30 ug/Kg7.3 Total/NA11308260D
☼1,2-Dichloroethane 6.1 ug/Kg1.0 Total/NA11.4 J 8260D
☼2-Hexanone 30 ug/Kg6.1 Total/NA1458260D
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: SW-3B (Continued)Lab Sample ID: 400-201537-30
☼4-Methyl-2-pentanone (MIBK)
RL
30 ug/Kg
MDL
6.1
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J128260D
☼Methyl tert-butyl ether 6.1 ug/Kg1.2 Total/NA1408260D
☼Naphthalene 6.1 ug/Kg2.4 Total/NA16.2 8260D
☼1,2,4-Trimethylbenzene 6.1 ug/Kg1.2 Total/NA12.8 J 8260D
☼1,3,5-Trimethylbenzene 6.1 ug/Kg1.0 Total/NA11.6 J 8260D
☼Xylenes, Total 12 ug/Kg2.3 Total/NA12.4 J 8260D
☼Iodomethane - DL 380 ug/Kg260 Total/NA504308260D
☼2-Methyl-2-propanol - DL 760 ug/Kg610 Total/NA5011008260D
Client Sample ID: SW-4A Lab Sample ID: 400-201537-31
☼Benzene
RL
6100 ug/Kg
MDL
820
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA250J32008260D
☼sec-Butylbenzene 6100 ug/Kg1200 Total/NA250250008260D
☼2-Chlorotoluene 6100 ug/Kg3000 Total/NA2501400008260D
☼Ethylbenzene 6100 ug/Kg740 Total/NA2501400008260D
☼2-Hexanone 30000 ug/Kg6100 Total/NA2501800008260D
☼Isopropylbenzene 6100 ug/Kg830 Total/NA250420008260D
☼4-Methyl-2-pentanone (MIBK)30000 ug/Kg6100 Total/NA25028000J8260D
☼Naphthalene 6100 ug/Kg2400 Total/NA2502000008260D
☼N-Propylbenzene 6100 ug/Kg1100 Total/NA2501500008260D
☼Toluene 6100 ug/Kg1200 Total/NA2501200008260D
☼Cyclohexane 6100 ug/Kg1100 Total/NA25082008260D
☼Methylcyclohexane 6100 ug/Kg1800 Total/NA250660008260D
☼Hexane 6100 ug/Kg1500 Total/NA25073008260D
☼n-Heptane 6100 ug/Kg3000 Total/NA250570008260D
☼1,2,4-Trimethylbenzene - DL 24000 ug/Kg4900 Total/NA10004500008260D
☼1,3,5-Trimethylbenzene - DL 24000 ug/Kg4000 Total/NA10001400008260D
☼o-Xylene - DL 24000 ug/Kg4900 Total/NA10002200008260D
☼m-Xylene & p-Xylene - DL 24000 ug/Kg6300 Total/NA10003800008260D
☼Xylenes, Total - DL 49000 ug/Kg9300 Total/NA10006000008260D
☼C5-C8 Aliphatics 1300 mg/Kg1300 Total/NA50002500MAVPH
☼C9-C12 Aliphatics 680 mg/Kg680 Total/NA50003700MAVPH
☼C9-C10 Aromatics 370 mg/Kg370 Total/NA50004900MAVPH
Client Sample ID: SW-4B Lab Sample ID: 400-201537-32
☼Acetone
RL
32 ug/Kg
MDL
16
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1778260D
☼2-Butanone (MEK)32 ug/Kg7.6 Total/NA122J8260D
☼Ethylene Dibromide 6.3 ug/Kg1.3 Total/NA11.5 J 8260D
☼1,2-Dichloroethane 6.3 ug/Kg1.0 Total/NA11.5 J 8260D
☼Ethylbenzene 6.3 ug/Kg0.77 Total/NA11.4 J 8260D
☼2-Hexanone 32 ug/Kg6.3 Total/NA127J8260D
☼Isopropylbenzene 6.3 ug/Kg0.86 Total/NA10.91 J 8260D
☼4-Methyl-2-pentanone (MIBK)32 ug/Kg6.3 Total/NA18.9 J 8260D
☼Methyl tert-butyl ether 6.3 ug/Kg1.3 Total/NA1248260D
☼Naphthalene 6.3 ug/Kg2.5 Total/NA1228260D
☼N-Propylbenzene 6.3 ug/Kg1.1 Total/NA11.3 J 8260D
☼Toluene 6.3 ug/Kg1.3 Total/NA12.5 J 8260D
☼1,2,4-Trimethylbenzene 6.3 ug/Kg1.3 Total/NA1198260D
☼1,3,5-Trimethylbenzene 6.3 ug/Kg1.1 Total/NA17.3 8260D
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
Page 9 of 116 4/15/2021
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: SW-4B (Continued)Lab Sample ID: 400-201537-32
☼o-Xylene
RL
6.3 ug/Kg
MDL
1.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA18.6 8260D
☼m-Xylene & p-Xylene 6.3 ug/Kg1.6 Total/NA16.0 J 8260D
☼Xylenes, Total 13 ug/Kg2.4 Total/NA1158260D
☼2-Methyl-2-propanol 13 ug/Kg10 Total/NA16608260D
☼C9-C10 Aromatics 1.2 mg/Kg1.2 Total/NA502.2 MAVPH
Client Sample ID: B-1 Lab Sample ID: 400-201537-33
☼Acetone
RL
30 ug/Kg
MDL
16
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA112008260D
☼Benzene 6.0 ug/Kg0.81 Total/NA11.2 J 8260D
☼2-Butanone (MEK)30 ug/Kg7.2 Total/NA15908260D
☼sec-Butylbenzene 6.0 ug/Kg1.1 Total/NA14.7 J 8260D
☼Ethylene Dibromide 6.0 ug/Kg1.2 Total/NA12.5 J 8260D
☼1,2-Dichloroethane 6.0 ug/Kg0.99 Total/NA14.8 J 8260D
☼Ethylbenzene 6.0 ug/Kg0.73 Total/NA11.2 J 8260D
☼2-Hexanone 30 ug/Kg6.0 Total/NA11808260D
☼Iodomethane 6.0 ug/Kg4.1 Total/NA15.8 J 8260D
☼Isopropylbenzene 6.0 ug/Kg0.82 Total/NA11.6 J 8260D
☼4-Isopropyltoluene 6.0 ug/Kg1.2 Total/NA11.9 J 8260D
☼4-Methyl-2-pentanone (MIBK)30 ug/Kg6.0 Total/NA1428260D
☼Methyl tert-butyl ether 6.0 ug/Kg1.2 Total/NA11308260D
☼Naphthalene 6.0 ug/Kg2.4 Total/NA1378260D
☼N-Propylbenzene 6.0 ug/Kg1.1 Total/NA13.1 J 8260D
☼Toluene 6.0 ug/Kg1.2 Total/NA12.8 J 8260D
☼1,2,4-Trimethylbenzene 6.0 ug/Kg1.2 Total/NA1388260D
☼1,3,5-Trimethylbenzene 6.0 ug/Kg1.0 Total/NA1188260D
☼o-Xylene 6.0 ug/Kg1.2 Total/NA18.4 8260D
☼m-Xylene & p-Xylene 6.0 ug/Kg1.6 Total/NA15.5 J 8260D
☼Xylenes, Total 12 ug/Kg2.3 Total/NA1148260D
☼Ethyl ether 6.0 ug/Kg1.2 Total/NA12.2 J 8260D
☼2-Methyl-2-propanol 12 ug/Kg9.6 Total/NA13208260D
☼C9-C12 Aliphatics 2.2 mg/Kg2.2 Total/NA503.3 MAVPH
☼C9-C10 Aromatics 1.2 mg/Kg1.2 Total/NA504.9 MAVPH
Client Sample ID: B-2 Lab Sample ID: 400-201537-34
☼Acetone
RL
36 ug/Kg
MDL
19
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA112008260D
☼2-Butanone (MEK)36 ug/Kg8.5 Total/NA16508260D
☼Ethylene Dibromide 7.1 ug/Kg1.4 Total/NA11.7 J 8260D
☼1,2-Dichloroethane 7.1 ug/Kg1.2 Total/NA13.2 J 8260D
☼Ethylbenzene 7.1 ug/Kg0.87 Total/NA11.1 J 8260D
☼2-Hexanone 36 ug/Kg7.1 Total/NA11808260D
☼4-Isopropyltoluene 7.1 ug/Kg1.4 Total/NA11.4 J 8260D
☼4-Methyl-2-pentanone (MIBK)36 ug/Kg7.1 Total/NA129J8260D
☼Methyl tert-butyl ether 7.1 ug/Kg1.4 Total/NA1838260D
☼Naphthalene 7.1 ug/Kg2.8 Total/NA16.1 J 8260D
☼Toluene 7.1 ug/Kg1.4 Total/NA12.7 J 8260D
☼1,2,4-Trimethylbenzene 7.1 ug/Kg1.4 Total/NA14.2 J 8260D
☼1,3,5-Trimethylbenzene 7.1 ug/Kg1.2 Total/NA14.0 J 8260D
☼o-Xylene 7.1 ug/Kg1.4 Total/NA15.4 J 8260D
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
Page 10 of 116 4/15/2021
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Detection Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Client Sample ID: B-2 (Continued)Lab Sample ID: 400-201537-34
☼m-Xylene & p-Xylene
RL
7.1 ug/Kg
MDL
1.9
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J4.7 8260D
☼Xylenes, Total 14 ug/Kg2.7 Total/NA110J8260D
☼Ethyl ether 7.1 ug/Kg1.4 Total/NA11.5 J 8260D
☼2-Methyl-2-propanol 14 ug/Kg11 Total/NA127008260D
☼C9-C10 Aromatics 1.5 mg/Kg1.5 Total/NA501.6 MAVPH
Client Sample ID: PL-1 Lab Sample ID: 400-201537-35
☼C6-C10
RL
5200 ug/Kg
MDL
2600
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50660008015C
☼C10-C28 5.7 mg/Kg2.3 Total/NA1588015C
Client Sample ID: PL-2 Lab Sample ID: 400-201537-36
☼C6-C10
RL
5200 ug/Kg
MDL
2600
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50J36008015C
Client Sample ID: D-1 Lab Sample ID: 400-201537-37
☼C6-C10
RL
5900 ug/Kg
MDL
2900
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50J31008015C
Client Sample ID: D-2 Lab Sample ID: 400-201537-38
☼C6-C10
RL
6800 ug/Kg
MDL
3400
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50180008015C
Client Sample ID: D-3 Lab Sample ID: 400-201537-39
☼C6-C10
RL
5000 ug/Kg
MDL
2500
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50J27008015C
☼C10-C28 29 mg/Kg11 Total/NA52008015C
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
400-201537-1 T-1/S-1 Solid 03/30/21 10:55 04/03/21 09:40
400-201537-2 T-1/S-2 Solid 03/30/21 11:00 04/03/21 09:40
400-201537-3 T2/S1 Solid 03/31/21 11:00 04/03/21 09:40
400-201537-4 T2/S2 Solid 03/31/21 11:05 04/03/21 09:40
400-201537-5 T2/S3 Solid 03/31/21 11:10 04/03/21 09:40
400-201537-6 T3/S1 Solid 03/31/21 10:45 04/03/21 09:40
400-201537-7 T3/S2 Solid 03/31/21 10:50 04/03/21 09:40
400-201537-8 T3/S3 Solid 03/31/21 10:55 04/03/21 09:40
400-201537-9 T4/S1 Solid 03/31/21 10:30 04/03/21 09:40
400-201537-10 T4/S2 Solid 03/31/21 10:35 04/03/21 09:40
400-201537-11 T4/S3 Solid 03/31/21 10:40 04/03/21 09:40
400-201537-12 L-13 Solid 04/01/21 10:30 04/03/21 09:40
400-201537-13 L-1 Solid 03/31/21 14:00 04/03/21 09:40
400-201537-14 L-2 Solid 03/31/21 14:30 04/03/21 09:40
400-201537-15 L-3 Solid 04/01/21 08:00 04/03/21 09:40
400-201537-16 L-4 Solid 04/01/21 08:10 04/03/21 09:40
400-201537-17 L-5 Solid 04/01/21 08:20 04/03/21 09:40
400-201537-18 L-6 Solid 04/01/21 08:30 04/03/21 09:40
400-201537-19 L-7 Solid 04/01/21 08:40 04/03/21 09:40
400-201537-20 L-8 Solid 04/01/21 09:00 04/03/21 09:40
400-201537-21 L-9 Solid 04/01/21 09:10 04/03/21 09:40
400-201537-22 L-10 Solid 04/01/21 09:20 04/03/21 09:40
400-201537-23 L-11 Solid 04/01/21 09:30 04/03/21 09:40
400-201537-24 L-12 Solid 04/01/21 10:00 04/03/21 09:40
400-201537-25 SW-1A Solid 04/01/21 11:10 04/03/21 09:40
400-201537-26 SW-1B Solid 04/01/21 11:45 04/03/21 09:40
400-201537-27 SW-2A Solid 04/01/21 11:15 04/03/21 09:40
400-201537-28 SW-2B Solid 04/01/21 11:20 04/03/21 09:40
400-201537-29 SW-3A Solid 04/01/21 11:25 04/03/21 09:40
400-201537-30 SW-3B Solid 04/01/21 11:30 04/03/21 09:40
400-201537-31 SW-4A Solid 04/01/21 11:35 04/03/21 09:40
400-201537-32 SW-4B Solid 04/01/21 11:40 04/03/21 09:40
400-201537-33 B-1 Solid 04/01/21 11:00 04/03/21 09:40
400-201537-34 B-2 Solid 04/01/21 11:05 04/03/21 09:40
400-201537-35 PL-1 Solid 04/01/21 15:00 04/03/21 09:40
400-201537-36 PL-2 Solid 04/01/21 15:45 04/03/21 09:40
400-201537-37 D-1 Solid 04/01/21 15:25 04/03/21 09:40
400-201537-38 D-2 Solid 04/01/21 15:30 04/03/21 09:40
400-201537-39 D-3 Solid 04/01/21 15:15 04/03/21 09:40
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-1Client Sample ID: T-1/S-1
Matrix: SolidDate Collected: 03/30/21 10:55
Percent Solids: 92.2Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 2800 U 5500 2800 ug/Kg ☼04/07/21 21:00 04/08/21 02:10 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)107 65-125 04/07/21 21:00 04/08/21 02:10 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 620 27 11 mg/Kg ☼04/06/21 12:56 04/07/21 17:23 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)83 27-150 04/06/21 12:56 04/07/21 17:23 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 92.3 0.01 0.01 %04/08/21 12:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/08/21 12:01 1Percent Moisture 7.7
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-2Client Sample ID: T-1/S-2
Matrix: SolidDate Collected: 03/30/21 11:00
Percent Solids: 78.7Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 2900 U 5700 2900 ug/Kg ☼04/07/21 21:00 04/08/21 03:27 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)106 65-125 04/07/21 21:00 04/08/21 03:27 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 7.3 6.3 2.5 mg/Kg ☼04/06/21 12:56 04/07/21 17:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)101 27-150 04/06/21 12:56 04/07/21 17:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 78.7 0.01 0.01 %04/08/21 12:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/08/21 12:01 1Percent Moisture 21.3
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-3Client Sample ID: T2/S1
Matrix: SolidDate Collected: 03/31/21 11:00
Percent Solids: 73.4Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 5100 U 10000 5100 ug/Kg ☼04/07/21 21:00 04/08/21 04:19 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)102 65-125 04/07/21 21:00 04/08/21 04:19 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 73.4 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 26.6
Eurofins TestAmerica, Pensacola
Page 15 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-4Client Sample ID: T2/S2
Matrix: SolidDate Collected: 03/31/21 11:05
Percent Solids: 82.2Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 16000 7700 3800 ug/Kg ☼04/07/21 21:00 04/08/21 04:45 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)107 65-125 04/07/21 21:00 04/08/21 04:45 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 82.2 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 17.8
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-5Client Sample ID: T2/S3
Matrix: SolidDate Collected: 03/31/21 11:10
Percent Solids: 80.0Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 74000 7900 3900 ug/Kg ☼04/07/21 21:00 04/08/21 05:12 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)104 65-125 04/07/21 21:00 04/08/21 05:12 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 80.0 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 20.0
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-6Client Sample ID: T3/S1
Matrix: SolidDate Collected: 03/31/21 10:45
Percent Solids: 74.3Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 76000 7200 3600 ug/Kg ☼04/07/21 21:00 04/08/21 05:38 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)110 65-125 04/07/21 21:00 04/08/21 05:38 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 74.3 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 25.7
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-7Client Sample ID: T3/S2
Matrix: SolidDate Collected: 03/31/21 10:50
Percent Solids: 78.8Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 5100 J 7700 3900 ug/Kg ☼04/07/21 21:00 04/08/21 06:04 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)105 65-125 04/07/21 21:00 04/08/21 06:04 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 78.8 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 21.2
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-8Client Sample ID: T3/S3
Matrix: SolidDate Collected: 03/31/21 10:55
Percent Solids: 80.6Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 94000 6200 3100 ug/Kg ☼04/07/21 21:00 04/08/21 06:30 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)103 65-125 04/07/21 21:00 04/08/21 06:30 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 80.6 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 19.4
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-9Client Sample ID: T4/S1
Matrix: SolidDate Collected: 03/31/21 10:30
Percent Solids: 80.7Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 3200 U 6400 3200 ug/Kg ☼04/07/21 21:00 04/08/21 06:57 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)105 65-125 04/07/21 21:00 04/08/21 06:57 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 80.7 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 19.3
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-10Client Sample ID: T4/S2
Matrix: SolidDate Collected: 03/31/21 10:35
Percent Solids: 77.1Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 4500 U 9000 4500 ug/Kg ☼04/07/21 21:00 04/08/21 07:23 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)102 65-125 04/07/21 21:00 04/08/21 07:23 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 77.1 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 22.9
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-11Client Sample ID: T4/S3
Matrix: SolidDate Collected: 03/31/21 10:40
Percent Solids: 81.2Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 3500 U 6900 3500 ug/Kg ☼04/07/21 21:00 04/08/21 07:50 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)103 65-125 04/07/21 21:00 04/08/21 07:50 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 81.2 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 18.8
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-12Client Sample ID: L-13
Matrix: SolidDate Collected: 04/01/21 10:30
Percent Solids: 78.3Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 8800 7700 3800 ug/Kg ☼04/07/21 21:00 04/08/21 08:16 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)107 65-125 04/07/21 21:00 04/08/21 08:16 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 78.3 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 21.7
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-13Client Sample ID: L-1
Matrix: SolidDate Collected: 03/31/21 14:00
Percent Solids: 80.5Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 770000 39000 20000 ug/Kg ☼04/08/21 16:00 04/08/21 23:05 250
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)102 65-125 04/08/21 16:00 04/08/21 23:05 250
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 80.5 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 19.5
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-14Client Sample ID: L-2
Matrix: SolidDate Collected: 03/31/21 14:30
Percent Solids: 81.3Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 400000 30000 15000 ug/Kg ☼04/08/21 16:00 04/08/21 23:32 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)106 65-125 04/08/21 16:00 04/08/21 23:32 200
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 81.3 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 18.7
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-15Client Sample ID: L-3
Matrix: SolidDate Collected: 04/01/21 08:00
Percent Solids: 73.9Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 3400000 90000 45000 ug/Kg ☼04/08/21 16:00 04/08/21 23:58 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)94 65-125 04/08/21 16:00 04/08/21 23:58 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 73.9 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 26.1
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-16Client Sample ID: L-4
Matrix: SolidDate Collected: 04/01/21 08:10
Percent Solids: 85.8Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 470000 23000 11000 ug/Kg ☼04/08/21 16:00 04/09/21 00:24 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)104 65-125 04/08/21 16:00 04/09/21 00:24 200
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 85.8 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 14.2
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-17Client Sample ID: L-5
Matrix: SolidDate Collected: 04/01/21 08:20
Percent Solids: 71.1Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 140000 9500 4800 ug/Kg ☼04/07/21 21:00 04/08/21 10:55 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)102 65-125 04/07/21 21:00 04/08/21 10:55 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 71.1 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 28.9
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-18Client Sample ID: L-6
Matrix: SolidDate Collected: 04/01/21 08:30
Percent Solids: 75.2Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 97000 9200 4600 ug/Kg ☼04/07/21 21:00 04/08/21 11:22 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)104 65-125 04/07/21 21:00 04/08/21 11:22 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 75.2 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 24.8
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-19Client Sample ID: L-7
Matrix: SolidDate Collected: 04/01/21 08:40
Percent Solids: 74.4Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 1700000 80000 40000 ug/Kg ☼04/08/21 16:00 04/09/21 00:51 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)112 65-125 04/08/21 16:00 04/09/21 00:51 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 74.4 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 25.6
Eurofins TestAmerica, Pensacola
Page 31 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-20Client Sample ID: L-8
Matrix: SolidDate Collected: 04/01/21 09:00
Percent Solids: 75.3Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 1900000 98000 49000 ug/Kg ☼04/08/21 16:00 04/09/21 01:18 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)110 65-125 04/08/21 16:00 04/09/21 01:18 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 75.3 0.01 0.01 %04/10/21 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:09 1Percent Moisture 24.7
Eurofins TestAmerica, Pensacola
Page 32 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-21Client Sample ID: L-9
Matrix: SolidDate Collected: 04/01/21 09:10
Percent Solids: 82.0Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 90000 6600 3300 ug/Kg ☼04/08/21 16:00 04/08/21 17:48 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)100 65-125 04/08/21 16:00 04/08/21 17:48 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 82.0 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 18.0
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-22Client Sample ID: L-10
Matrix: SolidDate Collected: 04/01/21 09:20
Percent Solids: 79.4Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 1800000 140000 68000 ug/Kg ☼04/09/21 12:00 04/09/21 14:58 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)111 65-125 04/09/21 12:00 04/09/21 14:58 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 79.4 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 20.6
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-23Client Sample ID: L-11
Matrix: SolidDate Collected: 04/01/21 09:30
Percent Solids: 80.0Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 680000 140000 70000 ug/Kg ☼04/09/21 12:00 04/09/21 16:15 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)108 65-125 04/09/21 12:00 04/09/21 16:15 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 80.0 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 20.0
Eurofins TestAmerica, Pensacola
Page 35 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-24Client Sample ID: L-12
Matrix: SolidDate Collected: 04/01/21 10:00
Percent Solids: 83.5Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 66000 5800 2900 ug/Kg ☼04/08/21 16:00 04/08/21 20:00 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)102 65-125 04/08/21 16:00 04/08/21 20:00 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 83.5 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 16.5
Eurofins TestAmerica, Pensacola
Page 36 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-25Client Sample ID: SW-1A
Matrix: SolidDate Collected: 04/01/21 11:10
Percent Solids: 86.7Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 8700 U 17000 8700 ug/Kg ☼04/13/21 12:34 04/13/21 23:01 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3300 450 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Benzene 450 U
3300 870 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Bromobenzene 870 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Chlorobromomethane 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Dichlorobromomethane 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Bromoform 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Bromomethane 1700 U
17000 4000 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼2-Butanone (MEK)4000 U
3300 640 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼n-Butylbenzene 640 U *+
3300 630 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼sec-Butylbenzene 7500
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼tert-Butylbenzene 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Carbon disulfide 1700 U
3300 1100 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Carbon tetrachloride 1100 U
3300 350 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Chlorobenzene 350 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Chloroethane 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Chloroform 1700 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Chloromethane 670 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼3-Chloro-1-propene 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼2-Chlorotoluene 31000
3300 650 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼4-Chlorotoluene 650 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Chlorodibromomethane 1700 U
3300 2200 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2-Dibromo-3-Chloropropane 2200 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Ethylene Dibromide 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Dibromomethane 1700 U
3300 470 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2-Dichlorobenzene 470 U
3300 630 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,3-Dichlorobenzene 630 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,4-Dichlorobenzene 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼trans-1,4-Dichloro-2-butene 1700 U
3300 870 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Dichlorodifluoromethane 870 U
3300 550 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1-Dichloroethane 550 U
3300 550 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2-Dichloroethane 550 U
3300 510 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼cis-1,2-Dichloroethene 510 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼trans-1,2-Dichloroethene 1700 U
3300 930 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2-Dichloroethene, Total 930 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1-Dichloroethene 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2-Dichloropropane 1700 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,3-Dichloropropane 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼2,2-Dichloropropane 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1-Dichloropropene 1700 U
3300 800 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼cis-1,3-Dichloropropene 800 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼trans-1,3-Dichloropropene 1700 U
3300 410 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Ethylbenzene 25000
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Ethyl methacrylate 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Hexachlorobutadiene 1700 U
17000 3300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼2-Hexanone 16000 J
3300 2300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Iodomethane 2300 U
17000 6700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Isobutyl alcohol 6700 U
3300 450 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Isopropylbenzene 8300
10000 6700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Methylene Chloride 6700 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-25Client Sample ID: SW-1A
Matrix: SolidDate Collected: 04/01/21 11:10
Percent Solids: 86.7Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
4-Methyl-2-pentanone (MIBK)5000 J 17000 3300 ug/Kg ☼04/13/21 12:34 04/13/21 23:01 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Methyl tert-butyl ether 670 U
3300 1300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Naphthalene 67000
3300 600 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼N-Propylbenzene 34000
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Styrene 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1,1,2-Tetrachloroethane 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1,2,2-Tetrachloroethane 1700 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Tetrachloroethene 1700 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Toluene 15000
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2,3-Trichlorobenzene 1700 U
3300 1300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2,4-Trichlorobenzene 1300 U
3300 730 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1,1-Trichloroethane 730 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1,2-Trichloroethane 1700 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Trichloroethene 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Trichlorofluoromethane 1700 U
3300 2000 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,2,3-Trichloropropane 2000 U
3300 1300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,1,2-Trichloro-1,2,2-trifluoroethane 1300 U
3300 550 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,3,5-Trimethylbenzene 110000
17000 6100 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Vinyl acetate 6100 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Vinyl chloride 1700 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼o-Xylene 87000
3300 870 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼m-Xylene & p-Xylene 150000
6700 1300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Xylenes, Total 240000
3300 630 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Cyclohexane 630 U
3300 3100 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Methyl acetate 3100 U
3300 1000 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Methylcyclohexane 4800
6700 3300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Tetrahydrofuran 3300 U
3300 800 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Hexane 800 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Ethyl ether 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼n-Heptane 3600
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,3-Dichloropropene, Total 1700 U
3300 670 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Butadiene 670 U
3300 1700 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼Dichlorofluoromethane 1700 U
6700 5300 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼2-Methyl-2-propanol 5300 U
330000 33000 ug/Kg 04/13/21 12:34 04/13/21 23:01 500☼1,4-Dioxane 33000 U
4-Bromofluorobenzene 91 67-130 04/13/21 12:34 04/13/21 23:01 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 104 04/13/21 12:34 04/13/21 23:01 50077-127
Toluene-d8 (Surr)105 04/13/21 12:34 04/13/21 23:01 50076-127
1,2-Dichloroethane-d4 (Surr)98 04/13/21 12:34 04/13/21 23:01 50078-146
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
4-Isopropyltoluene 1300 U 6700 1300 ug/Kg ☼04/14/21 17:34 04/15/21 04:20 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6700 1300 ug/Kg 04/14/21 17:34 04/15/21 04:20 1000☼1,2,4-Trimethylbenzene 110000
4-Bromofluorobenzene 91 67-130 04/14/21 17:34 04/15/21 04:20 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 93 04/14/21 17:34 04/15/21 04:20 100077-127
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-25Client Sample ID: SW-1A
Matrix: SolidDate Collected: 04/01/21 11:10
Percent Solids: 86.7Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS - DL (Continued)
Toluene-d8 (Surr)105 76-127 04/14/21 17:34 04/15/21 04:20 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)101 04/14/21 17:34 04/15/21 04:20 100078-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 720 U 720 720 mg/Kg ☼04/09/21 09:45 04/10/21 04:47 10000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
370 370 mg/Kg 04/09/21 09:45 04/10/21 04:47 10000☼C9-C12 Aliphatics 520
200 200 mg/Kg 04/09/21 09:45 04/10/21 04:47 10000☼C9-C10 Aromatics 1500
a,a,a-Trifluorotoluene (fid)99 70-130 04/09/21 09:45 04/10/21 04:47 10000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)100 04/09/21 09:45 04/10/21 04:47 1000070-130
General Chemistry
RL MDL
Percent Solids 86.7 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 13.3
Eurofins TestAmerica, Pensacola
Page 39 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-26Client Sample ID: SW-1B
Matrix: SolidDate Collected: 04/01/21 11:45
Percent Solids: 89.2Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 1600 U 3100 1600 ug/Kg ☼04/13/21 12:34 04/13/21 22:08 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
630 84 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Benzene 84 U
630 160 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Bromobenzene 160 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Chlorobromomethane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Dichlorobromomethane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Bromoform 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Bromomethane 310 U
3100 750 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼2-Butanone (MEK)750 U
630 120 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼n-Butylbenzene 120 U *+
630 120 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼sec-Butylbenzene 1000
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼tert-Butylbenzene 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Carbon disulfide 310 U
630 210 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Carbon tetrachloride 210 U
630 65 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Chlorobenzene 65 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Chloroethane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Chloroform 310 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Chloromethane 130 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼3-Chloro-1-propene 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼2-Chlorotoluene 310 U
630 120 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼4-Chlorotoluene 120 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Chlorodibromomethane 310 U
630 410 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2-Dibromo-3-Chloropropane 410 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Ethylene Dibromide 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Dibromomethane 310 U
630 89 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2-Dichlorobenzene 89 U
630 120 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,3-Dichlorobenzene 120 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,4-Dichlorobenzene 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼trans-1,4-Dichloro-2-butene 310 U
630 160 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Dichlorodifluoromethane 160 U
630 100 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1-Dichloroethane 100 U
630 100 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2-Dichloroethane 100 U
630 95 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼cis-1,2-Dichloroethene 95 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼trans-1,2-Dichloroethene 310 U
630 180 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2-Dichloroethene, Total 180 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1-Dichloroethene 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2-Dichloropropane 310 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,3-Dichloropropane 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼2,2-Dichloropropane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1-Dichloropropene 310 U
630 150 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼cis-1,3-Dichloropropene 150 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼trans-1,3-Dichloropropene 310 U
630 76 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Ethylbenzene 1900
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Ethyl methacrylate 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Hexachlorobutadiene 310 U
3100 630 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼2-Hexanone 2300 J
630 430 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Iodomethane 430 U
3100 1300 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Isobutyl alcohol 1300 U
630 85 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Isopropylbenzene 770
630 130 ug/Kg 04/14/21 17:34 04/15/21 03:53 100☼4-Isopropyltoluene 450 J
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-26Client Sample ID: SW-1B
Matrix: SolidDate Collected: 04/01/21 11:45
Percent Solids: 89.2Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 1300 U 1900 1300 ug/Kg ☼04/13/21 12:34 04/13/21 22:08 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3100 630 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼4-Methyl-2-pentanone (MIBK)630 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Methyl tert-butyl ether 130 U
630 250 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Naphthalene 16000
630 110 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼N-Propylbenzene 3400
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Styrene 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1,1,2-Tetrachloroethane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1,2,2-Tetrachloroethane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Tetrachloroethene 310 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Toluene 820
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2,3-Trichlorobenzene 310 U
630 250 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2,4-Trichlorobenzene 250 U
630 140 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1,1-Trichloroethane 140 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1,2-Trichloroethane 310 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Trichloroethene 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Trichlorofluoromethane 310 U
630 380 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2,3-Trichloropropane 380 U
630 250 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,1,2-Trichloro-1,2,2-trifluoroethane 250 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,2,4-Trimethylbenzene 37000
630 100 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,3,5-Trimethylbenzene 13000
3100 1100 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Vinyl acetate 1100 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Vinyl chloride 310 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼o-Xylene 7400
630 160 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼m-Xylene & p-Xylene 8600
1300 240 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Xylenes, Total 16000
630 120 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Cyclohexane 120 U
630 580 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Methyl acetate 580 U
630 190 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Methylcyclohexane 380 J
1300 630 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Tetrahydrofuran 630 U
630 150 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Hexane 150 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Ethyl ether 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼n-Heptane 310 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,3-Dichloropropene, Total 310 U
630 130 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Butadiene 130 U
630 310 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼Dichlorofluoromethane 310 U
1300 1000 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼2-Methyl-2-propanol 1200 J
63000 6300 ug/Kg 04/13/21 12:34 04/13/21 22:08 100☼1,4-Dioxane 6300 U
4-Bromofluorobenzene 90 67-130 04/13/21 12:34 04/13/21 22:08 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene 88 04/14/21 17:34 04/15/21 03:53 10067-130
Dibromofluoromethane 101 04/13/21 12:34 04/13/21 22:08 10077-127
Dibromofluoromethane 101 04/14/21 17:34 04/15/21 03:53 10077-127
Toluene-d8 (Surr)103 04/13/21 12:34 04/13/21 22:08 10076-127
Toluene-d8 (Surr)103 04/14/21 17:34 04/15/21 03:53 10076-127
1,2-Dichloroethane-d4 (Surr)98 04/13/21 12:34 04/13/21 22:08 10078-146
1,2-Dichloroethane-d4 (Surr)97 04/14/21 17:34 04/15/21 03:53 10078-146
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-26Client Sample ID: SW-1B
Matrix: SolidDate Collected: 04/01/21 11:45
Percent Solids: 89.2Date Received: 04/03/21 09:40
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 140 U 140 140 mg/Kg ☼04/09/21 09:45 04/10/21 05:48 2000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
70 70 mg/Kg 04/09/21 09:45 04/10/21 05:48 2000☼C9-C12 Aliphatics 170
38 38 mg/Kg 04/09/21 09:45 04/10/21 05:48 2000☼C9-C10 Aromatics 340
a,a,a-Trifluorotoluene (fid)100 70-130 04/09/21 09:45 04/10/21 05:48 2000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)99 04/09/21 09:45 04/10/21 05:48 200070-130
General Chemistry
RL MDL
Percent Solids 89.2 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 10.8
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-27Client Sample ID: SW-2A
Matrix: SolidDate Collected: 04/01/21 11:15
Percent Solids: 77.9Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 180 32 17 ug/Kg ☼04/13/21 12:34 04/13/21 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.4 0.85 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Benzene 0.85 U
6.4 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Bromobenzene 1.7 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Chlorobromomethane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Dichlorobromomethane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Bromoform 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Bromomethane 3.2 U
32 7.7 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼2-Butanone (MEK)25 J
6.4 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼n-Butylbenzene 1.2 U *+
6.4 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼sec-Butylbenzene 1.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼tert-Butylbenzene 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Carbon disulfide 3.2 U
6.4 2.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Carbon tetrachloride 2.2 U
6.4 0.66 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Chlorobenzene 0.66 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Chloroethane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Chloroform 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Chloromethane 1.3 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼3-Chloro-1-propene 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼2-Chlorotoluene 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼4-Chlorotoluene 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Chlorodibromomethane 3.2 U
6.4 4.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2-Dibromo-3-Chloropropane 4.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Ethylene Dibromide 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Dibromomethane 3.2 U
6.4 0.91 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2-Dichlorobenzene 0.91 U
6.4 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,3-Dichlorobenzene 1.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,4-Dichlorobenzene 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼trans-1,4-Dichloro-2-butene 3.2 U
6.4 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Dichlorodifluoromethane 1.7 U
6.4 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1-Dichloroethane 1.1 U
6.4 1.0 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2-Dichloroethane 1.0 U
6.4 0.97 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼cis-1,2-Dichloroethene 0.97 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼trans-1,2-Dichloroethene 3.2 U
6.4 1.8 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2-Dichloroethene, Total 1.8 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1-Dichloroethene 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2-Dichloropropane 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,3-Dichloropropane 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼2,2-Dichloropropane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1-Dichloropropene 3.2 U
6.4 1.5 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼cis-1,3-Dichloropropene 1.5 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼trans-1,3-Dichloropropene 3.2 U
6.4 0.78 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Ethylbenzene 0.78 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Ethyl methacrylate 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Hexachlorobutadiene 3.2 U
32 6.4 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼2-Hexanone 7.7 J
6.4 4.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Iodomethane 4.3 U
32 13 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Isobutyl alcohol 13 U
6.4 0.87 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Isopropylbenzene 0.87 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼4-Isopropyltoluene 1.3 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-27Client Sample ID: SW-2A
Matrix: SolidDate Collected: 04/01/21 11:15
Percent Solids: 77.9Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 13 U 19 13 ug/Kg ☼04/13/21 12:34 04/13/21 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
32 6.4 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼4-Methyl-2-pentanone (MIBK)6.4 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Methyl tert-butyl ether 4.2 J
6.4 2.6 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Naphthalene 9.9
6.4 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼N-Propylbenzene 1.1 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Styrene 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1,1,2-Tetrachloroethane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1,2,2-Tetrachloroethane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Tetrachloroethene 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Toluene 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2,3-Trichlorobenzene 3.2 U
6.4 2.6 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2,4-Trichlorobenzene 2.6 U
6.4 1.4 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1,1-Trichloroethane 1.4 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1,2-Trichloroethane 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Trichloroethene 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Trichlorofluoromethane 3.2 U
6.4 3.8 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2,3-Trichloropropane 3.8 U
6.4 2.6 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 2.6 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,2,4-Trimethylbenzene 3.9 J
6.4 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,3,5-Trimethylbenzene 1.6 J
32 12 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Vinyl acetate 12 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Vinyl chloride 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼o-Xylene 1.3 U
6.4 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼m-Xylene & p-Xylene 1.7 U
13 2.4 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Xylenes, Total 2.4 U
6.4 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Cyclohexane 1.2 U
6.4 5.9 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Methyl acetate 5.9 U
6.4 1.9 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Methylcyclohexane 1.9 U
13 6.4 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Tetrahydrofuran 6.4 U
6.4 1.5 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Hexane 1.5 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Ethyl ether 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼n-Heptane 3.2 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,3-Dichloropropene, Total 3.2 U
6.4 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Butadiene 1.3 U
6.4 3.2 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼Dichlorofluoromethane 3.2 U
13 10 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼2-Methyl-2-propanol 160
640 64 ug/Kg 04/13/21 12:34 04/13/21 19:03 1☼1,4-Dioxane 64 U
4-Bromofluorobenzene 93 67-130 04/13/21 12:34 04/13/21 19:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 108 04/13/21 12:34 04/13/21 19:03 177-127
Toluene-d8 (Surr)100 04/13/21 12:34 04/13/21 19:03 176-127
1,2-Dichloroethane-d4 (Surr)116 04/13/21 12:34 04/13/21 19:03 178-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 4.1 U 4.1 4.1 mg/Kg ☼04/09/21 09:45 04/09/21 14:43 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.1 2.1 mg/Kg 04/09/21 09:45 04/09/21 14:43 50☼C9-C12 Aliphatics 2.1 U
1.1 1.1 mg/Kg 04/09/21 09:45 04/09/21 14:43 50☼C9-C10 Aromatics 3.6
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-27Client Sample ID: SW-2A
Matrix: SolidDate Collected: 04/01/21 11:15
Percent Solids: 77.9Date Received: 04/03/21 09:40
a,a,a-Trifluorotoluene (fid)99 70-130 04/09/21 09:45 04/09/21 14:43 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 04/09/21 09:45 04/09/21 14:43 5070-130
General Chemistry
RL MDL
Percent Solids 77.9 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 22.1
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-28Client Sample ID: SW-2B
Matrix: SolidDate Collected: 04/01/21 11:20
Percent Solids: 89.8Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 650 U 1300 650 ug/Kg ☼04/13/21 12:34 04/13/21 21:42 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
250 34 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Benzene 49 J
250 65 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Bromobenzene 65 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Chlorobromomethane 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Dichlorobromomethane 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Bromoform 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Bromomethane 130 U
1300 300 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼2-Butanone (MEK)300 U
250 48 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼n-Butylbenzene 48 U *+
250 48 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼sec-Butylbenzene 140 J
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼tert-Butylbenzene 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Carbon disulfide 130 U
250 85 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Carbon tetrachloride 85 U
250 26 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Chlorobenzene 26 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Chloroethane 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Chloroform 130 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Chloromethane 50 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼3-Chloro-1-propene 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼2-Chlorotoluene 130 U
250 49 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼4-Chlorotoluene 49 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Chlorodibromomethane 130 U
250 170 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2-Dibromo-3-Chloropropane 170 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Ethylene Dibromide 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Dibromomethane 130 U
250 36 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2-Dichlorobenzene 36 U
250 48 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,3-Dichlorobenzene 48 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,4-Dichlorobenzene 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼trans-1,4-Dichloro-2-butene 130 U
250 65 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Dichlorodifluoromethane 65 U
250 42 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1-Dichloroethane 42 U
250 41 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2-Dichloroethane 41 U
250 38 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼cis-1,2-Dichloroethene 38 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼trans-1,2-Dichloroethene 130 U
250 70 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2-Dichloroethene, Total 70 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1-Dichloroethene 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2-Dichloropropane 130 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,3-Dichloropropane 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼2,2-Dichloropropane 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1-Dichloropropene 130 U
250 60 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼cis-1,3-Dichloropropene 60 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼trans-1,3-Dichloropropene 130 U
250 31 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Ethylbenzene 560
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Ethyl methacrylate 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Hexachlorobutadiene 130 U
1300 250 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼2-Hexanone 910 J
250 170 ug/Kg 04/14/21 17:34 04/15/21 01:12 50☼Iodomethane 400
1300 500 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Isobutyl alcohol 500 U
250 34 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Isopropylbenzene 160 J
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼4-Isopropyltoluene 160 J
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-28Client Sample ID: SW-2B
Matrix: SolidDate Collected: 04/01/21 11:20
Percent Solids: 89.8Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 500 U 750 500 ug/Kg ☼04/13/21 12:34 04/13/21 21:42 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1300 250 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼4-Methyl-2-pentanone (MIBK)250 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Methyl tert-butyl ether 50 U
250 100 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Naphthalene 2600
250 45 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼N-Propylbenzene 630
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Styrene 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1,1,2-Tetrachloroethane 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1,2,2-Tetrachloroethane 130 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Tetrachloroethene 130 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Toluene 560
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2,3-Trichlorobenzene 130 U
250 100 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2,4-Trichlorobenzene 100 U
250 55 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1,1-Trichloroethane 55 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1,2-Trichloroethane 130 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Trichloroethene 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Trichlorofluoromethane 130 U
250 150 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2,3-Trichloropropane 150 U
250 100 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,1,2-Trichloro-1,2,2-trifluoroethane 100 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,2,4-Trimethylbenzene 9900
250 42 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,3,5-Trimethylbenzene 3300
1300 460 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Vinyl acetate 460 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Vinyl chloride 130 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼o-Xylene 1900
250 65 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼m-Xylene & p-Xylene 3200
500 96 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Xylenes, Total 5000
250 47 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Cyclohexane 47 U
250 230 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Methyl acetate 270
250 75 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Methylcyclohexane 210 J
500 250 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Tetrahydrofuran 250 U
250 60 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Hexane 270
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Ethyl ether 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼n-Heptane 500
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,3-Dichloropropene, Total 130 U
250 50 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Butadiene 50 U
250 130 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼Dichlorofluoromethane 130 U
500 400 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼2-Methyl-2-propanol 400 U
25000 2500 ug/Kg 04/13/21 12:34 04/13/21 21:42 50☼1,4-Dioxane 2500 U
4-Bromofluorobenzene 94 67-130 04/13/21 12:34 04/13/21 21:42 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene 89 04/14/21 17:34 04/15/21 01:12 5067-130
Dibromofluoromethane 105 04/13/21 12:34 04/13/21 21:42 5077-127
Dibromofluoromethane 104 04/14/21 17:34 04/15/21 01:12 5077-127
Toluene-d8 (Surr)104 04/13/21 12:34 04/13/21 21:42 5076-127
Toluene-d8 (Surr)103 04/14/21 17:34 04/15/21 01:12 5076-127
1,2-Dichloroethane-d4 (Surr)104 04/13/21 12:34 04/13/21 21:42 5078-146
1,2-Dichloroethane-d4 (Surr)106 04/14/21 17:34 04/15/21 01:12 5078-146
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-28Client Sample ID: SW-2B
Matrix: SolidDate Collected: 04/01/21 11:20
Percent Solids: 89.8Date Received: 04/03/21 09:40
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 54 U 54 54 mg/Kg ☼04/09/21 09:45 04/10/21 06:48 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
28 28 mg/Kg 04/09/21 09:45 04/10/21 06:48 1000☼C9-C12 Aliphatics 63
15 15 mg/Kg 04/09/21 09:45 04/10/21 06:48 1000☼C9-C10 Aromatics 130
a,a,a-Trifluorotoluene (fid)98 70-130 04/09/21 09:45 04/10/21 06:48 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)99 04/09/21 09:45 04/10/21 06:48 100070-130
General Chemistry
RL MDL
Percent Solids 89.8 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 10.2
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-29Client Sample ID: SW-3A
Matrix: SolidDate Collected: 04/01/21 11:25
Percent Solids: 80.2Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 200 33 17 ug/Kg ☼04/13/21 12:34 04/13/21 19:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.7 0.89 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Benzene 1.2 J
6.7 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Bromobenzene 1.7 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Chlorobromomethane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Dichlorobromomethane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Bromoform 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Bromomethane 3.3 U
33 8.0 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼2-Butanone (MEK)73
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼n-Butylbenzene 1.3 U *+
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼sec-Butylbenzene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼tert-Butylbenzene 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Carbon disulfide 3.3 U
6.7 2.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Carbon tetrachloride 2.3 U
6.7 0.69 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Chlorobenzene 0.69 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Chloroethane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Chloroform 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Chloromethane 1.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼3-Chloro-1-propene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼2-Chlorotoluene 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼4-Chlorotoluene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Chlorodibromomethane 3.3 U
6.7 4.4 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2-Dibromo-3-Chloropropane 4.4 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Ethylene Dibromide 1.3 J
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Dibromomethane 3.3 U
6.7 0.95 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2-Dichlorobenzene 0.95 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,3-Dichlorobenzene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,4-Dichlorobenzene 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼trans-1,4-Dichloro-2-butene 3.3 U
6.7 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Dichlorodifluoromethane 1.7 U
6.7 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1-Dichloroethane 1.1 U
6.7 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2-Dichloroethane 1.7 J
6.7 1.0 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼cis-1,2-Dichloroethene 1.0 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼trans-1,2-Dichloroethene 3.3 U
6.7 1.9 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2-Dichloroethene, Total 1.9 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1-Dichloroethene 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2-Dichloropropane 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,3-Dichloropropane 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼2,2-Dichloropropane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1-Dichloropropene 3.3 U
6.7 1.6 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼cis-1,3-Dichloropropene 1.6 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼trans-1,3-Dichloropropene 3.3 U
6.7 0.81 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Ethylbenzene 2.5 J
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Ethyl methacrylate 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Hexachlorobutadiene 3.3 U
33 6.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼2-Hexanone 21 J
6.7 4.5 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Iodomethane 4.5 U
33 13 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Isobutyl alcohol 13 U
6.7 0.91 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Isopropylbenzene 0.91 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼4-Isopropyltoluene 1.3 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-29Client Sample ID: SW-3A
Matrix: SolidDate Collected: 04/01/21 11:25
Percent Solids: 80.2Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 13 U 20 13 ug/Kg ☼04/13/21 12:34 04/13/21 19:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
33 6.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼4-Methyl-2-pentanone (MIBK)7.2 J
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Methyl tert-butyl ether 40
6.7 2.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Naphthalene 5.6 J
6.7 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼N-Propylbenzene 1.3 J
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Styrene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1,1,2-Tetrachloroethane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1,2,2-Tetrachloroethane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Tetrachloroethene 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Toluene 7.0
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2,3-Trichlorobenzene 3.3 U
6.7 2.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2,4-Trichlorobenzene 2.7 U
6.7 1.5 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1,1-Trichloroethane 1.5 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1,2-Trichloroethane 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Trichloroethene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Trichlorofluoromethane 3.3 U
6.7 4.0 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2,3-Trichloropropane 4.0 U
6.7 2.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 2.7 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,2,4-Trimethylbenzene 11
6.7 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,3,5-Trimethylbenzene 4.7 J
33 12 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Vinyl acetate 12 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Vinyl chloride 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼o-Xylene 11
6.7 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼m-Xylene & p-Xylene 13
13 2.5 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Xylenes, Total 24
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Cyclohexane 1.3 U
6.7 6.1 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Methyl acetate 6.1 U
6.7 2.0 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Methylcyclohexane 2.0 U
13 6.7 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Tetrahydrofuran 6.7 U
6.7 1.6 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Hexane 1.6 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Ethyl ether 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼n-Heptane 3.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,3-Dichloropropene, Total 3.3 U
6.7 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Butadiene 1.3 U
6.7 3.3 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼Dichlorofluoromethane 3.3 U
13 11 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼2-Methyl-2-propanol 210
670 67 ug/Kg 04/13/21 12:34 04/13/21 19:29 1☼1,4-Dioxane 67 U
4-Bromofluorobenzene 92 67-130 04/13/21 12:34 04/13/21 19:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 113 04/13/21 12:34 04/13/21 19:29 177-127
Toluene-d8 (Surr)99 04/13/21 12:34 04/13/21 19:29 176-127
1,2-Dichloroethane-d4 (Surr)118 04/13/21 12:34 04/13/21 19:29 178-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 4.2 U 4.2 4.2 mg/Kg ☼04/09/21 09:45 04/10/21 03:47 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.2 2.2 mg/Kg 04/09/21 09:45 04/10/21 03:47 50☼C9-C12 Aliphatics 2.2 U
1.2 1.2 mg/Kg 04/09/21 09:45 04/10/21 03:47 50☼C9-C10 Aromatics 1.2 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-29Client Sample ID: SW-3A
Matrix: SolidDate Collected: 04/01/21 11:25
Percent Solids: 80.2Date Received: 04/03/21 09:40
a,a,a-Trifluorotoluene (fid)97 70-130 04/09/21 09:45 04/10/21 03:47 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 04/09/21 09:45 04/10/21 03:47 5070-130
General Chemistry
RL MDL
Percent Solids 80.2 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 19.8
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-30Client Sample ID: SW-3B
Matrix: SolidDate Collected: 04/01/21 11:30
Percent Solids: 78.7Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 280 30 16 ug/Kg ☼04/13/21 12:34 04/13/21 19:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.1 0.81 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Benzene 0.81 U
6.1 1.6 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Bromobenzene 1.6 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Chlorobromomethane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Dichlorobromomethane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Bromoform 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Bromomethane 13
30 7.3 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼2-Butanone (MEK)130
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼n-Butylbenzene 1.2 U *+
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼sec-Butylbenzene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼tert-Butylbenzene 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Carbon disulfide 3.0 U
6.1 2.1 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Carbon tetrachloride 2.1 U
6.1 0.63 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Chlorobenzene 0.63 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Chloroethane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Chloroform 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Chloromethane 1.2 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼3-Chloro-1-propene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼2-Chlorotoluene 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼4-Chlorotoluene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Chlorodibromomethane 3.0 U
6.1 4.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2-Dibromo-3-Chloropropane 4.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Ethylene Dibromide 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Dibromomethane 3.0 U
6.1 0.86 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2-Dichlorobenzene 0.86 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,3-Dichlorobenzene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,4-Dichlorobenzene 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼trans-1,4-Dichloro-2-butene 3.0 U
6.1 1.6 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Dichlorodifluoromethane 1.6 U
6.1 1.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1-Dichloroethane 1.0 U
6.1 1.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2-Dichloroethane 1.4 J
6.1 0.92 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼cis-1,2-Dichloroethene 0.92 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼trans-1,2-Dichloroethene 3.0 U
6.1 1.7 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2-Dichloroethene, Total 1.7 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1-Dichloroethene 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2-Dichloropropane 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,3-Dichloropropane 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼2,2-Dichloropropane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1-Dichloropropene 3.0 U
6.1 1.5 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼cis-1,3-Dichloropropene 1.5 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼trans-1,3-Dichloropropene 3.0 U
6.1 0.74 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Ethylbenzene 0.74 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Ethyl methacrylate 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Hexachlorobutadiene 3.0 U
30 6.1 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼2-Hexanone 45
30 12 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Isobutyl alcohol 12 U
6.1 0.83 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Isopropylbenzene 0.83 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼4-Isopropyltoluene 1.2 U
18 12 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Methylene Chloride 12 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-30Client Sample ID: SW-3B
Matrix: SolidDate Collected: 04/01/21 11:30
Percent Solids: 78.7Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
4-Methyl-2-pentanone (MIBK)12 J 30 6.1 ug/Kg ☼04/13/21 12:34 04/13/21 19:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Methyl tert-butyl ether 40
6.1 2.4 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Naphthalene 6.2
6.1 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼N-Propylbenzene 1.1 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Styrene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1,1,2-Tetrachloroethane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1,2,2-Tetrachloroethane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Tetrachloroethene 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Toluene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2,3-Trichlorobenzene 3.0 U
6.1 2.4 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2,4-Trichlorobenzene 2.4 U
6.1 1.3 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1,1-Trichloroethane 1.3 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1,2-Trichloroethane 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Trichloroethene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Trichlorofluoromethane 3.0 U
6.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2,3-Trichloropropane 3.6 U
6.1 2.4 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 2.4 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,2,4-Trimethylbenzene 2.8 J
6.1 1.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,3,5-Trimethylbenzene 1.6 J
30 11 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Vinyl acetate 11 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Vinyl chloride 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼o-Xylene 1.2 U
6.1 1.6 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼m-Xylene & p-Xylene 1.6 U
12 2.3 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Xylenes, Total 2.4 J
6.1 1.1 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Cyclohexane 1.1 U
6.1 5.6 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Methyl acetate 5.6 U
6.1 1.8 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Methylcyclohexane 1.8 U
12 6.1 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Tetrahydrofuran 6.1 U
6.1 1.5 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Hexane 1.5 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Ethyl ether 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼n-Heptane 3.0 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,3-Dichloropropene, Total 3.0 U
6.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Butadiene 1.2 U
6.1 3.0 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼Dichlorofluoromethane 3.0 U
610 61 ug/Kg 04/13/21 12:34 04/13/21 19:56 1☼1,4-Dioxane 61 U
4-Bromofluorobenzene 93 67-130 04/13/21 12:34 04/13/21 19:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 111 04/13/21 12:34 04/13/21 19:56 177-127
Toluene-d8 (Surr)99 04/13/21 12:34 04/13/21 19:56 176-127
1,2-Dichloroethane-d4 (Surr)121 04/13/21 12:34 04/13/21 19:56 178-146
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
Iodomethane 430 380 260 ug/Kg ☼04/14/21 17:34 04/15/21 01:38 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
760 610 ug/Kg 04/14/21 17:34 04/15/21 01:38 50☼2-Methyl-2-propanol 1100
4-Bromofluorobenzene 99 67-130 04/14/21 17:34 04/15/21 01:38 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 102 04/14/21 17:34 04/15/21 01:38 5077-127
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-30Client Sample ID: SW-3B
Matrix: SolidDate Collected: 04/01/21 11:30
Percent Solids: 78.7Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS - DL (Continued)
Toluene-d8 (Surr)106 76-127 04/14/21 17:34 04/15/21 01:38 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)100 04/14/21 17:34 04/15/21 01:38 5078-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 4.1 U 4.1 4.1 mg/Kg ☼04/09/21 09:45 04/10/21 02:47 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.1 2.1 mg/Kg 04/09/21 09:45 04/10/21 02:47 50☼C9-C12 Aliphatics 2.1 U
1.1 1.1 mg/Kg 04/09/21 09:45 04/10/21 02:47 50☼C9-C10 Aromatics 1.1 U
a,a,a-Trifluorotoluene (fid)98 70-130 04/09/21 09:45 04/10/21 02:47 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 04/09/21 09:45 04/10/21 02:47 5070-130
General Chemistry
RL MDL
Percent Solids 78.7 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 21.3
Eurofins TestAmerica, Pensacola
Page 54 of 116 4/15/2021
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-31Client Sample ID: SW-4A
Matrix: SolidDate Collected: 04/01/21 11:35
Percent Solids: 76.5Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 16000 U 30000 16000 ug/Kg ☼04/13/21 12:34 04/13/21 22:35 250
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6100 820 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Benzene 3200 J
6100 1600 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Bromobenzene 1600 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Chlorobromomethane 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Dichlorobromomethane 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Bromoform 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Bromomethane 3000 U
30000 7300 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼2-Butanone (MEK)7300 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼n-Butylbenzene 1200 U *+
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼sec-Butylbenzene 25000
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼tert-Butylbenzene 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Carbon disulfide 3000 U
6100 2100 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Carbon tetrachloride 2100 U
6100 630 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Chlorobenzene 630 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Chloroethane 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Chloroform 3000 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Chloromethane 1200 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼3-Chloro-1-propene 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼2-Chlorotoluene 140000
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼4-Chlorotoluene 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Chlorodibromomethane 3000 U
6100 4000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2-Dibromo-3-Chloropropane 4000 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Ethylene Dibromide 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Dibromomethane 3000 U
6100 870 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2-Dichlorobenzene 870 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,3-Dichlorobenzene 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,4-Dichlorobenzene 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼trans-1,4-Dichloro-2-butene 3000 U
6100 1600 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Dichlorodifluoromethane 1600 U
6100 1000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1-Dichloroethane 1000 U
6100 1000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2-Dichloroethane 1000 U
6100 930 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼cis-1,2-Dichloroethene 930 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼trans-1,2-Dichloroethene 3000 U
6100 1700 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2-Dichloroethene, Total 1700 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1-Dichloroethene 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2-Dichloropropane 3000 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,3-Dichloropropane 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼2,2-Dichloropropane 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1-Dichloropropene 3000 U
6100 1500 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼cis-1,3-Dichloropropene 1500 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼trans-1,3-Dichloropropene 3000 U
6100 740 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Ethylbenzene 140000
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Ethyl methacrylate 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Hexachlorobutadiene 3000 U
30000 6100 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼2-Hexanone 180000
6100 4100 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Iodomethane 4100 U
30000 12000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Isobutyl alcohol 12000 U
6100 830 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Isopropylbenzene 42000
18000 12000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Methylene Chloride 12000 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-31Client Sample ID: SW-4A
Matrix: SolidDate Collected: 04/01/21 11:35
Percent Solids: 76.5Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
4-Methyl-2-pentanone (MIBK)28000 J 30000 6100 ug/Kg ☼04/13/21 12:34 04/13/21 22:35 250
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Methyl tert-butyl ether 1200 U
6100 2400 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Naphthalene 200000
6100 1100 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼N-Propylbenzene 150000
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Styrene 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1,1,2-Tetrachloroethane 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1,2,2-Tetrachloroethane 3000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Tetrachloroethene 3000 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Toluene 120000
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2,3-Trichlorobenzene 3000 U
6100 2400 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2,4-Trichlorobenzene 2400 U
6100 1300 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1,1-Trichloroethane 1300 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1,2-Trichloroethane 3000 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Trichloroethene 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Trichlorofluoromethane 3000 U
6100 3700 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,2,3-Trichloropropane 3700 U
6100 2400 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,1,2-Trichloro-1,2,2-trifluoroethane 2400 U
30000 11000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Vinyl acetate 11000 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Vinyl chloride 3000 U
6100 1100 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Cyclohexane 8200
6100 5600 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Methyl acetate 5600 U
6100 1800 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Methylcyclohexane 66000
12000 6100 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Tetrahydrofuran 6100 U
6100 1500 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Hexane 7300
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Ethyl ether 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼n-Heptane 57000
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,3-Dichloropropene, Total 3000 U
6100 1200 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Butadiene 1200 U
6100 3000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼Dichlorofluoromethane 3000 U
12000 9800 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼2-Methyl-2-propanol 9800 U
610000 61000 ug/Kg 04/13/21 12:34 04/13/21 22:35 250☼1,4-Dioxane 61000 U
4-Bromofluorobenzene 108 67-130 04/13/21 12:34 04/13/21 22:35 250
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 97 04/13/21 12:34 04/13/21 22:35 25077-127
Toluene-d8 (Surr)109 04/13/21 12:34 04/13/21 22:35 25076-127
1,2-Dichloroethane-d4 (Surr)94 04/13/21 12:34 04/13/21 22:35 25078-146
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
4-Isopropyltoluene 4900 U 24000 4900 ug/Kg ☼04/14/21 17:34 04/15/21 04:46 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
24000 4900 ug/Kg 04/14/21 17:34 04/15/21 04:46 1000☼1,2,4-Trimethylbenzene 450000
24000 4000 ug/Kg 04/14/21 17:34 04/15/21 04:46 1000☼1,3,5-Trimethylbenzene 140000
24000 4900 ug/Kg 04/14/21 17:34 04/15/21 04:46 1000☼o-Xylene 220000
24000 6300 ug/Kg 04/14/21 17:34 04/15/21 04:46 1000☼m-Xylene & p-Xylene 380000
49000 9300 ug/Kg 04/14/21 17:34 04/15/21 04:46 1000☼Xylenes, Total 600000
4-Bromofluorobenzene 84 67-130 04/14/21 17:34 04/15/21 04:46 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 92 04/14/21 17:34 04/15/21 04:46 100077-127
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-31Client Sample ID: SW-4A
Matrix: SolidDate Collected: 04/01/21 11:35
Percent Solids: 76.5Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS - DL (Continued)
Toluene-d8 (Surr)103 76-127 04/14/21 17:34 04/15/21 04:46 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)94 04/14/21 17:34 04/15/21 04:46 100078-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 2500 1300 1300 mg/Kg ☼04/09/21 09:45 04/10/21 09:53 5000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
680 680 mg/Kg 04/09/21 09:45 04/10/21 09:53 5000☼C9-C12 Aliphatics 3700
370 370 mg/Kg 04/09/21 09:45 04/10/21 09:53 5000☼C9-C10 Aromatics 4900
a,a,a-Trifluorotoluene (fid)104 70-130 04/09/21 09:45 04/10/21 09:53 5000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)104 04/09/21 09:45 04/10/21 09:53 500070-130
General Chemistry
RL MDL
Percent Solids 76.5 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 23.5
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-32Client Sample ID: SW-4B
Matrix: SolidDate Collected: 04/01/21 11:40
Percent Solids: 78.1Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 77 32 16 ug/Kg ☼04/13/21 12:34 04/13/21 20:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.3 0.85 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Benzene 0.85 U
6.3 1.6 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Bromobenzene 1.6 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Chlorobromomethane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Dichlorobromomethane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Bromoform 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Bromomethane 3.2 U
32 7.6 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼2-Butanone (MEK)22 J
6.3 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼n-Butylbenzene 1.2 U *+
6.3 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼sec-Butylbenzene 1.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼tert-Butylbenzene 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Carbon disulfide 3.2 U
6.3 2.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Carbon tetrachloride 2.2 U
6.3 0.66 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Chlorobenzene 0.66 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Chloroethane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Chloroform 3.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Chloromethane 1.3 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼3-Chloro-1-propene 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼2-Chlorotoluene 3.2 U
6.3 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼4-Chlorotoluene 1.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Chlorodibromomethane 3.2 U
6.3 4.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2-Dibromo-3-Chloropropane 4.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Ethylene Dibromide 1.5 J
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Dibromomethane 3.2 U
6.3 0.90 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2-Dichlorobenzene 0.90 U
6.3 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,3-Dichlorobenzene 1.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,4-Dichlorobenzene 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼trans-1,4-Dichloro-2-butene 3.2 U
6.3 1.6 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Dichlorodifluoromethane 1.6 U
6.3 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1-Dichloroethane 1.1 U
6.3 1.0 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2-Dichloroethane 1.5 J
6.3 0.96 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼cis-1,2-Dichloroethene 0.96 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼trans-1,2-Dichloroethene 3.2 U
6.3 1.8 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2-Dichloroethene, Total 1.8 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1-Dichloroethene 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2-Dichloropropane 3.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,3-Dichloropropane 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼2,2-Dichloropropane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1-Dichloropropene 3.2 U
6.3 1.5 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼cis-1,3-Dichloropropene 1.5 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼trans-1,3-Dichloropropene 3.2 U
6.3 0.77 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Ethylbenzene 1.4 J
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Ethyl methacrylate 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Hexachlorobutadiene 3.2 U
32 6.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼2-Hexanone 27 J
6.3 4.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Iodomethane 4.3 U
32 13 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Isobutyl alcohol 13 U
6.3 0.86 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Isopropylbenzene 0.91 J
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼4-Isopropyltoluene 1.3 U
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-32Client Sample ID: SW-4B
Matrix: SolidDate Collected: 04/01/21 11:40
Percent Solids: 78.1Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 13 U 19 13 ug/Kg ☼04/13/21 12:34 04/13/21 20:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
32 6.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼4-Methyl-2-pentanone (MIBK)8.9 J
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Methyl tert-butyl ether 24
6.3 2.5 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Naphthalene 22
6.3 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼N-Propylbenzene 1.3 J
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Styrene 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1,1,2-Tetrachloroethane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1,2,2-Tetrachloroethane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Tetrachloroethene 3.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Toluene 2.5 J
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2,3-Trichlorobenzene 3.2 U
6.3 2.5 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2,4-Trichlorobenzene 2.5 U
6.3 1.4 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1,1-Trichloroethane 1.4 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1,2-Trichloroethane 3.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Trichloroethene 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Trichlorofluoromethane 3.2 U
6.3 3.8 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2,3-Trichloropropane 3.8 U
6.3 2.5 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 2.5 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,2,4-Trimethylbenzene 19
6.3 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,3,5-Trimethylbenzene 7.3
32 12 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Vinyl acetate 12 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Vinyl chloride 3.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼o-Xylene 8.6
6.3 1.6 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼m-Xylene & p-Xylene 6.0 J
13 2.4 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Xylenes, Total 15
6.3 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Cyclohexane 1.2 U
6.3 5.8 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Methyl acetate 5.8 U
6.3 1.9 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Methylcyclohexane 1.9 U
13 6.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Tetrahydrofuran 6.3 U
6.3 1.5 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Hexane 1.5 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Ethyl ether 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼n-Heptane 3.2 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,3-Dichloropropene, Total 3.2 U
6.3 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Butadiene 1.3 U
6.3 3.2 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼Dichlorofluoromethane 3.2 U
13 10 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼2-Methyl-2-propanol 660
630 63 ug/Kg 04/13/21 12:34 04/13/21 20:22 1☼1,4-Dioxane 63 U
4-Bromofluorobenzene 91 67-130 04/13/21 12:34 04/13/21 20:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 112 04/13/21 12:34 04/13/21 20:22 177-127
Toluene-d8 (Surr)101 04/13/21 12:34 04/13/21 20:22 176-127
1,2-Dichloroethane-d4 (Surr)120 04/13/21 12:34 04/13/21 20:22 178-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 4.1 U 4.1 4.1 mg/Kg ☼04/09/21 09:45 04/09/21 21:45 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.1 2.1 mg/Kg 04/09/21 09:45 04/09/21 21:45 50☼C9-C12 Aliphatics 2.1 U
1.2 1.2 mg/Kg 04/09/21 09:45 04/09/21 21:45 50☼C9-C10 Aromatics 2.2
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-32Client Sample ID: SW-4B
Matrix: SolidDate Collected: 04/01/21 11:40
Percent Solids: 78.1Date Received: 04/03/21 09:40
a,a,a-Trifluorotoluene (fid)95 70-130 04/09/21 09:45 04/09/21 21:45 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 04/09/21 09:45 04/09/21 21:45 5070-130
General Chemistry
RL MDL
Percent Solids 78.1 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 21.9
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-33Client Sample ID: B-1
Matrix: SolidDate Collected: 04/01/21 11:00
Percent Solids: 78.0Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 1200 30 16 ug/Kg ☼04/13/21 12:34 04/13/21 20:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.0 0.81 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Benzene 1.2 J
6.0 1.6 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Bromobenzene 1.6 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Chlorobromomethane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Dichlorobromomethane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Bromoform 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Bromomethane 3.0 U
30 7.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼2-Butanone (MEK)590
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼n-Butylbenzene 1.2 U *+
6.0 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼sec-Butylbenzene 4.7 J
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼tert-Butylbenzene 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Carbon disulfide 3.0 U
6.0 2.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Carbon tetrachloride 2.0 U
6.0 0.63 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Chlorobenzene 0.63 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Chloroethane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Chloroform 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Chloromethane 1.2 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼3-Chloro-1-propene 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼2-Chlorotoluene 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼4-Chlorotoluene 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Chlorodibromomethane 3.0 U
6.0 4.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2-Dibromo-3-Chloropropane 4.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Ethylene Dibromide 2.5 J
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Dibromomethane 3.0 U
6.0 0.85 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2-Dichlorobenzene 0.85 U
6.0 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,3-Dichlorobenzene 1.1 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,4-Dichlorobenzene 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼trans-1,4-Dichloro-2-butene 3.0 U
6.0 1.6 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Dichlorodifluoromethane 1.6 U
6.0 1.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1-Dichloroethane 1.0 U
6.0 0.99 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2-Dichloroethane 4.8 J
6.0 0.91 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼cis-1,2-Dichloroethene 0.91 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼trans-1,2-Dichloroethene 3.0 U
6.0 1.7 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2-Dichloroethene, Total 1.7 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1-Dichloroethene 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2-Dichloropropane 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,3-Dichloropropane 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼2,2-Dichloropropane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1-Dichloropropene 3.0 U
6.0 1.4 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼cis-1,3-Dichloropropene 1.4 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼trans-1,3-Dichloropropene 3.0 U
6.0 0.73 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Ethylbenzene 1.2 J
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Ethyl methacrylate 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Hexachlorobutadiene 3.0 U
30 6.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼2-Hexanone 180
6.0 4.1 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Iodomethane 5.8 J
30 12 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Isobutyl alcohol 12 U
6.0 0.82 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Isopropylbenzene 1.6 J
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼4-Isopropyltoluene 1.9 J
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-33Client Sample ID: B-1
Matrix: SolidDate Collected: 04/01/21 11:00
Percent Solids: 78.0Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 12 U 18 12 ug/Kg ☼04/13/21 12:34 04/13/21 20:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
30 6.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼4-Methyl-2-pentanone (MIBK)42
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Methyl tert-butyl ether 130
6.0 2.4 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Naphthalene 37
6.0 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼N-Propylbenzene 3.1 J
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Styrene 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1,1,2-Tetrachloroethane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1,2,2-Tetrachloroethane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Tetrachloroethene 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Toluene 2.8 J
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2,3-Trichlorobenzene 3.0 U
6.0 2.4 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2,4-Trichlorobenzene 2.4 U
6.0 1.3 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1,1-Trichloroethane 1.3 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1,2-Trichloroethane 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Trichloroethene 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Trichlorofluoromethane 3.0 U
6.0 3.6 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2,3-Trichloropropane 3.6 U
6.0 2.4 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 2.4 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,2,4-Trimethylbenzene 38
6.0 1.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,3,5-Trimethylbenzene 18
30 11 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Vinyl acetate 11 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Vinyl chloride 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼o-Xylene 8.4
6.0 1.6 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼m-Xylene & p-Xylene 5.5 J
12 2.3 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Xylenes, Total 14
6.0 1.1 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Cyclohexane 1.1 U
6.0 5.5 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Methyl acetate 5.5 U
6.0 1.8 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Methylcyclohexane 1.8 U
12 6.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Tetrahydrofuran 6.0 U
6.0 1.4 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Hexane 1.4 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Ethyl ether 2.2 J
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼n-Heptane 3.0 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,3-Dichloropropene, Total 3.0 U
6.0 1.2 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Butadiene 1.2 U
6.0 3.0 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼Dichlorofluoromethane 3.0 U
12 9.6 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼2-Methyl-2-propanol 320
600 60 ug/Kg 04/13/21 12:34 04/13/21 20:49 1☼1,4-Dioxane 60 U
4-Bromofluorobenzene 95 67-130 04/13/21 12:34 04/13/21 20:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 108 04/13/21 12:34 04/13/21 20:49 177-127
Toluene-d8 (Surr)101 04/13/21 12:34 04/13/21 20:49 176-127
1,2-Dichloroethane-d4 (Surr)115 04/13/21 12:34 04/13/21 20:49 178-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 4.3 U 4.3 4.3 mg/Kg ☼04/09/21 09:45 04/09/21 22:45 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.2 2.2 mg/Kg 04/09/21 09:45 04/09/21 22:45 50☼C9-C12 Aliphatics 3.3
1.2 1.2 mg/Kg 04/09/21 09:45 04/09/21 22:45 50☼C9-C10 Aromatics 4.9
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-33Client Sample ID: B-1
Matrix: SolidDate Collected: 04/01/21 11:00
Percent Solids: 78.0Date Received: 04/03/21 09:40
a,a,a-Trifluorotoluene (fid)96 70-130 04/09/21 09:45 04/09/21 22:45 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)96 04/09/21 09:45 04/09/21 22:45 5070-130
General Chemistry
RL MDL
Percent Solids 78.0 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 22.0
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-34Client Sample ID: B-2
Matrix: SolidDate Collected: 04/01/21 11:05
Percent Solids: 79.6Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
Acetone 1200 36 19 ug/Kg ☼04/13/21 12:34 04/13/21 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.1 0.95 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Benzene 0.95 U
7.1 1.9 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Bromobenzene 1.9 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Chlorobromomethane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Dichlorobromomethane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Bromoform 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Bromomethane 3.6 U
36 8.5 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼2-Butanone (MEK)650
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼n-Butylbenzene 1.4 U *+
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼sec-Butylbenzene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼tert-Butylbenzene 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Carbon disulfide 3.6 U
7.1 2.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Carbon tetrachloride 2.4 U
7.1 0.74 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Chlorobenzene 0.74 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Chloroethane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Chloroform 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Chloromethane 1.4 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼3-Chloro-1-propene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼2-Chlorotoluene 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼4-Chlorotoluene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Chlorodibromomethane 3.6 U
7.1 4.7 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2-Dibromo-3-Chloropropane 4.7 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Ethylene Dibromide 1.7 J
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Dibromomethane 3.6 U
7.1 1.0 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2-Dichlorobenzene 1.0 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,3-Dichlorobenzene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,4-Dichlorobenzene 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼trans-1,4-Dichloro-2-butene 3.6 U
7.1 1.9 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Dichlorodifluoromethane 1.9 U
7.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1-Dichloroethane 1.2 U
7.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2-Dichloroethane 3.2 J
7.1 1.1 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼cis-1,2-Dichloroethene 1.1 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼trans-1,2-Dichloroethene 3.6 U
7.1 2.0 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2-Dichloroethene, Total 2.0 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1-Dichloroethene 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2-Dichloropropane 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,3-Dichloropropane 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼2,2-Dichloropropane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1-Dichloropropene 3.6 U
7.1 1.7 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼cis-1,3-Dichloropropene 1.7 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼trans-1,3-Dichloropropene 3.6 U
7.1 0.87 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Ethylbenzene 1.1 J
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Ethyl methacrylate 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Hexachlorobutadiene 3.6 U
36 7.1 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼2-Hexanone 180
7.1 4.8 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Iodomethane 4.8 U
36 14 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Isobutyl alcohol 14 U
7.1 0.97 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Isopropylbenzene 0.97 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼4-Isopropyltoluene 1.4 J
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-34Client Sample ID: B-2
Matrix: SolidDate Collected: 04/01/21 11:05
Percent Solids: 79.6Date Received: 04/03/21 09:40
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride 14 U 21 14 ug/Kg ☼04/13/21 12:34 04/13/21 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
36 7.1 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼4-Methyl-2-pentanone (MIBK)29 J
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Methyl tert-butyl ether 83
7.1 2.8 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Naphthalene 6.1 J
7.1 1.3 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼N-Propylbenzene 1.3 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Styrene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1,1,2-Tetrachloroethane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1,2,2-Tetrachloroethane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Tetrachloroethene 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Toluene 2.7 J
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2,3-Trichlorobenzene 3.6 U
7.1 2.8 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2,4-Trichlorobenzene 2.8 U
7.1 1.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1,1-Trichloroethane 1.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1,2-Trichloroethane 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Trichloroethene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Trichlorofluoromethane 3.6 U
7.1 4.3 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2,3-Trichloropropane 4.3 U
7.1 2.8 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 2.8 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,2,4-Trimethylbenzene 4.2 J
7.1 1.2 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,3,5-Trimethylbenzene 4.0 J
36 13 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Vinyl acetate 13 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Vinyl chloride 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼o-Xylene 5.4 J
7.1 1.9 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼m-Xylene & p-Xylene 4.7 J
14 2.7 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Xylenes, Total 10 J
7.1 1.3 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Cyclohexane 1.3 U
7.1 6.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Methyl acetate 6.6 U
7.1 2.1 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Methylcyclohexane 2.1 U
14 7.1 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Tetrahydrofuran 7.1 U
7.1 1.7 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Hexane 1.7 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Ethyl ether 1.5 J
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼n-Heptane 3.6 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,3-Dichloropropene, Total 3.6 U
7.1 1.4 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Butadiene 1.4 U
7.1 3.6 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼Dichlorofluoromethane 3.6 U
14 11 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼2-Methyl-2-propanol 2700
710 71 ug/Kg 04/13/21 12:34 04/13/21 21:15 1☼1,4-Dioxane 71 U
4-Bromofluorobenzene 94 67-130 04/13/21 12:34 04/13/21 21:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 104 04/13/21 12:34 04/13/21 21:15 177-127
Toluene-d8 (Surr)103 04/13/21 12:34 04/13/21 21:15 176-127
1,2-Dichloroethane-d4 (Surr)110 04/13/21 12:34 04/13/21 21:15 178-146
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 5.4 U 5.4 5.4 mg/Kg ☼04/09/21 09:45 04/09/21 23:46 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.8 2.8 mg/Kg 04/09/21 09:45 04/09/21 23:46 50☼C9-C12 Aliphatics 2.8 U
1.5 1.5 mg/Kg 04/09/21 09:45 04/09/21 23:46 50☼C9-C10 Aromatics 1.6
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-34Client Sample ID: B-2
Matrix: SolidDate Collected: 04/01/21 11:05
Percent Solids: 79.6Date Received: 04/03/21 09:40
a,a,a-Trifluorotoluene (fid)96 70-130 04/09/21 09:45 04/09/21 23:46 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 04/09/21 09:45 04/09/21 23:46 5070-130
General Chemistry
RL MDL
Percent Solids 79.6 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 20.4
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-35Client Sample ID: PL-1
Matrix: SolidDate Collected: 04/01/21 15:00
Percent Solids: 86.1Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 66000 5200 2600 ug/Kg ☼04/08/21 16:00 04/08/21 20:27 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)110 65-125 04/08/21 16:00 04/08/21 20:27 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 58 5.7 2.3 mg/Kg ☼04/06/21 12:56 04/08/21 12:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)93 27-150 04/06/21 12:56 04/08/21 12:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 86.1 0.01 0.01 %04/08/21 12:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/08/21 12:01 1Percent Moisture 13.9
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-36Client Sample ID: PL-2
Matrix: SolidDate Collected: 04/01/21 15:45
Percent Solids: 90.5Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 3600 J 5200 2600 ug/Kg ☼04/08/21 16:00 04/08/21 20:53 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)106 65-125 04/08/21 16:00 04/08/21 20:53 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 90.5 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 9.5
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-37Client Sample ID: D-1
Matrix: SolidDate Collected: 04/01/21 15:25
Percent Solids: 82.9Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 3100 J 5900 2900 ug/Kg ☼04/08/21 16:00 04/08/21 21:46 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)105 65-125 04/08/21 16:00 04/08/21 21:46 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 82.9 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 17.1
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-38Client Sample ID: D-2
Matrix: SolidDate Collected: 04/01/21 15:30
Percent Solids: 75.5Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 18000 6800 3400 ug/Kg ☼04/08/21 16:00 04/08/21 22:13 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)102 65-125 04/08/21 16:00 04/08/21 22:13 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 75.5 0.01 0.01 %04/10/21 10:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/10/21 10:40 1Percent Moisture 24.5
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Lab Sample ID: 400-201537-39Client Sample ID: D-3
Matrix: SolidDate Collected: 04/01/21 15:15
Percent Solids: 86.7Date Received: 04/03/21 09:40
Method: 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
C6-C10 2700 J 5000 2500 ug/Kg ☼04/08/21 16:00 04/08/21 22:39 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene (fid)106 65-125 04/08/21 16:00 04/08/21 22:39 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8015C - Diesel Range Organics (DRO) (GC)
RL MDL
C10-C28 200 29 11 mg/Kg ☼04/06/21 12:56 04/07/21 18:06 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Terphenyl (Surr)95 27-150 04/06/21 12:56 04/07/21 18:06 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Solids 86.7 0.01 0.01 %04/08/21 12:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %04/08/21 12:01 1Percent Moisture 13.3
Eurofins TestAmerica, Pensacola
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Definitions/Glossary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
U Indicates the analyte was analyzed for but not detected.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
U Indicates the analyte was analyzed for but not detected.
GC Semi VOA
Qualifier Description
U Indicates the analyte was analyzed for but not detected.
Qualifier
General Chemistry
Qualifier Description
F3 Duplicate RPD exceeds the control limit
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8260D - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (67-130)(77-127)(76-127)(78-146)
BFB DBFM TOL DCA
82 108 100 116400-201481-B-10-E MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
85 106 98 115400-201481-B-10-F MSD Matrix Spike Duplicate
87 107 101 111400-201521-B-8-E MS Matrix Spike
88 106 103 111400-201521-B-8-F MSD Matrix Spike Duplicate
91 104 105 98400-201537-25 SW-1A
91 93 105 101400-201537-25 - DL SW-1A
90 101 103 98400-201537-26 SW-1B
88 101 103 97400-201537-26 SW-1B
93 108 100 116400-201537-27 SW-2A
94 105 104 104400-201537-28 SW-2B
89 104 103 106400-201537-28 SW-2B
92 113 99 118400-201537-29 SW-3A
93 111 99 121400-201537-30 SW-3B
99 102 106 100400-201537-30 - DL SW-3B
108 97 109 94400-201537-31 SW-4A
84 92 103 94400-201537-31 - DL SW-4A
91 112 101 120400-201537-32 SW-4B
95 108 101 115400-201537-33 B-1
94 104 103 110400-201537-34 B-2
84 107 101 104LCS 400-527442/1-A Lab Control Sample
84 108 101 103LCS 400-527637/1-A Lab Control Sample
97 110 103 110MB 400-527442/2-A Method Blank
100 112 102 108MB 400-527637/2-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
Method: 8015C - Gasoline Range Organics (GRO) (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (65-125)
TFT-F2
107400-201537-1
Percent Surrogate Recovery (Acceptance Limits)
T-1/S-1
99400-201537-1 MS T-1/S-1
103400-201537-1 MSD T-1/S-1
106400-201537-2 T-1/S-2
102400-201537-3 T2/S1
107400-201537-4 T2/S2
104400-201537-5 T2/S3
110400-201537-6 T3/S1
105400-201537-7 T3/S2
103400-201537-8 T3/S3
105400-201537-9 T4/S1
102400-201537-10 T4/S2
103400-201537-11 T4/S3
107400-201537-12 L-13
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8015C - Gasoline Range Organics (GRO) (GC) (Continued)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (65-125)
TFT-F2
102400-201537-13
Percent Surrogate Recovery (Acceptance Limits)
L-1
106400-201537-14 L-2
94400-201537-15 L-3
104400-201537-16 L-4
102400-201537-17 L-5
104400-201537-18 L-6
112400-201537-19 L-7
110400-201537-20 L-8
100400-201537-21 L-9
97400-201537-21 MS L-9
95400-201537-21 MSD L-9
111400-201537-22 L-10
101400-201537-22 MS L-10
103400-201537-22 MSD L-10
108400-201537-23 L-11
102400-201537-24 L-12
110400-201537-35 PL-1
106400-201537-36 PL-2
105400-201537-37 D-1
102400-201537-38 D-2
106400-201537-39 D-3
101LCS 400-526785/2-A Lab Control Sample
101LCS 400-526959/1-A Lab Control Sample
101LCS 400-527015/1-A Lab Control Sample
105MB 400-526785/1-A Method Blank
103MB 400-526959/2-A Method Blank
103MB 400-527015/2-A Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
99 100400-201537-25
Percent Surrogate Recovery (Acceptance Limits)
SW-1A
100 99400-201537-26 SW-1B
99 98400-201537-27 SW-2A
97 98400-201537-27 MS SW-2A
98 98400-201537-27 MSD SW-2A
98 99400-201537-28 SW-2B
97 97400-201537-29 SW-3A
98 98400-201537-30 SW-3B
104 104400-201537-31 SW-4A
95 97400-201537-32 SW-4B
96 96400-201537-33 B-1
96 97400-201537-34 B-2
98 98LCS 400-526975/2-A Lab Control Sample
99 97LCSD 400-526975/3-A Lab Control Sample Dup
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
98 98MB 400-526975/1-A
Percent Surrogate Recovery (Acceptance Limits)
Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Method: 8015C - Diesel Range Organics (DRO) (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (27-150)
OTPH1
89400-201494-B-1-B MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
86400-201494-B-1-C MSD Matrix Spike Duplicate
83400-201537-1 T-1/S-1
101400-201537-2 T-1/S-2
93400-201537-35 PL-1
95400-201537-39 D-3
107LCS 400-526533/2-A Lab Control Sample
97LCSD 400-526533/3-A Lab Control Sample Dup
87MB 400-526533/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
GC/MS VOA
Analysis Batch: 527343
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 527442400-201537-25 SW-1A Total/NA
Solid 8260D 527442400-201537-26 SW-1B Total/NA
Solid 8260D 527442400-201537-27 SW-2A Total/NA
Solid 8260D 527442400-201537-28 SW-2B Total/NA
Solid 8260D 527442400-201537-29 SW-3A Total/NA
Solid 8260D 527442400-201537-30 SW-3B Total/NA
Solid 8260D 527442400-201537-31 SW-4A Total/NA
Solid 8260D 527442400-201537-32 SW-4B Total/NA
Solid 8260D 527442400-201537-33 B-1 Total/NA
Solid 8260D 527442400-201537-34 B-2 Total/NA
Solid 8260D 527442MB 400-527442/2-A Method Blank Total/NA
Solid 8260D 527442LCS 400-527442/1-A Lab Control Sample Total/NA
Prep Batch: 527442
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-201537-25 SW-1A Total/NA
Solid 5035400-201537-26 SW-1B Total/NA
Solid 5035400-201537-27 SW-2A Total/NA
Solid 5035400-201537-28 SW-2B Total/NA
Solid 5035400-201537-29 SW-3A Total/NA
Solid 5035400-201537-30 SW-3B Total/NA
Solid 5035400-201537-31 SW-4A Total/NA
Solid 5035400-201537-32 SW-4B Total/NA
Solid 5035400-201537-33 B-1 Total/NA
Solid 5035400-201537-34 B-2 Total/NA
Solid 5035MB 400-527442/2-A Method Blank Total/NA
Solid 5035LCS 400-527442/1-A Lab Control Sample Total/NA
Analysis Batch: 527629
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 527637400-201537-25 - DL SW-1A Total/NA
Solid 8260D 527637400-201537-26 SW-1B Total/NA
Solid 8260D 527637400-201537-28 SW-2B Total/NA
Solid 8260D 527637400-201537-30 - DL SW-3B Total/NA
Solid 8260D 527637400-201537-31 - DL SW-4A Total/NA
Solid 8260D 527637MB 400-527637/2-A Method Blank Total/NA
Solid 8260D 527637LCS 400-527637/1-A Lab Control Sample Total/NA
Prep Batch: 527637
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-201537-25 - DL SW-1A Total/NA
Solid 5035400-201537-26 SW-1B Total/NA
Solid 5035400-201537-28 SW-2B Total/NA
Solid 5035400-201537-30 - DL SW-3B Total/NA
Solid 5035400-201537-31 - DL SW-4A Total/NA
Solid 5035MB 400-527637/2-A Method Blank Total/NA
Solid 5035LCS 400-527637/1-A Lab Control Sample Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
GC VOA
Prep Batch: 526785
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-201537-1 T-1/S-1 Total/NA
Solid 5035400-201537-2 T-1/S-2 Total/NA
Solid 5035400-201537-3 T2/S1 Total/NA
Solid 5035400-201537-4 T2/S2 Total/NA
Solid 5035400-201537-5 T2/S3 Total/NA
Solid 5035400-201537-6 T3/S1 Total/NA
Solid 5035400-201537-7 T3/S2 Total/NA
Solid 5035400-201537-8 T3/S3 Total/NA
Solid 5035400-201537-9 T4/S1 Total/NA
Solid 5035400-201537-10 T4/S2 Total/NA
Solid 5035400-201537-11 T4/S3 Total/NA
Solid 5035400-201537-12 L-13 Total/NA
Solid 5035400-201537-17 L-5 Total/NA
Solid 5035400-201537-18 L-6 Total/NA
Solid 5035MB 400-526785/1-A Method Blank Total/NA
Solid 5035LCS 400-526785/2-A Lab Control Sample Total/NA
Solid 5035400-201537-1 MS T-1/S-1 Total/NA
Solid 5035400-201537-1 MSD T-1/S-1 Total/NA
Analysis Batch: 526810
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 526785400-201537-1 T-1/S-1 Total/NA
Solid 8015C 526785400-201537-2 T-1/S-2 Total/NA
Solid 8015C 526785400-201537-3 T2/S1 Total/NA
Solid 8015C 526785400-201537-4 T2/S2 Total/NA
Solid 8015C 526785400-201537-5 T2/S3 Total/NA
Solid 8015C 526785400-201537-6 T3/S1 Total/NA
Solid 8015C 526785400-201537-7 T3/S2 Total/NA
Solid 8015C 526785400-201537-8 T3/S3 Total/NA
Solid 8015C 526785400-201537-9 T4/S1 Total/NA
Solid 8015C 526785400-201537-10 T4/S2 Total/NA
Solid 8015C 526785400-201537-11 T4/S3 Total/NA
Solid 8015C 526785400-201537-12 L-13 Total/NA
Solid 8015C 526785400-201537-17 L-5 Total/NA
Solid 8015C 526785400-201537-18 L-6 Total/NA
Solid 8015C 526785MB 400-526785/1-A Method Blank Total/NA
Solid 8015C 526785LCS 400-526785/2-A Lab Control Sample Total/NA
Solid 8015C 526785400-201537-1 MS T-1/S-1 Total/NA
Solid 8015C 526785400-201537-1 MSD T-1/S-1 Total/NA
Analysis Batch: 526866
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 526959400-201537-13 L-1 Total/NA
Solid 8015C 526959400-201537-14 L-2 Total/NA
Solid 8015C 526959400-201537-15 L-3 Total/NA
Solid 8015C 526959400-201537-16 L-4 Total/NA
Solid 8015C 526959400-201537-19 L-7 Total/NA
Solid 8015C 526959400-201537-20 L-8 Total/NA
Solid 8015C 526959400-201537-21 L-9 Total/NA
Solid 8015C 526959400-201537-24 L-12 Total/NA
Solid 8015C 526959400-201537-35 PL-1 Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
GC VOA (Continued)
Analysis Batch: 526866 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 526959400-201537-36 PL-2 Total/NA
Solid 8015C 526959400-201537-37 D-1 Total/NA
Solid 8015C 526959400-201537-38 D-2 Total/NA
Solid 8015C 526959400-201537-39 D-3 Total/NA
Solid 8015C 526959MB 400-526959/2-A Method Blank Total/NA
Solid 8015C 526959LCS 400-526959/1-A Lab Control Sample Total/NA
Solid 8015C 526959400-201537-21 MS L-9 Total/NA
Solid 8015C 526959400-201537-21 MSD L-9 Total/NA
Prep Batch: 526959
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-201537-13 L-1 Total/NA
Solid 5035400-201537-14 L-2 Total/NA
Solid 5035400-201537-15 L-3 Total/NA
Solid 5035400-201537-16 L-4 Total/NA
Solid 5035400-201537-19 L-7 Total/NA
Solid 5035400-201537-20 L-8 Total/NA
Solid 5035400-201537-21 L-9 Total/NA
Solid 5035400-201537-24 L-12 Total/NA
Solid 5035400-201537-35 PL-1 Total/NA
Solid 5035400-201537-36 PL-2 Total/NA
Solid 5035400-201537-37 D-1 Total/NA
Solid 5035400-201537-38 D-2 Total/NA
Solid 5035400-201537-39 D-3 Total/NA
Solid 5035MB 400-526959/2-A Method Blank Total/NA
Solid 5035LCS 400-526959/1-A Lab Control Sample Total/NA
Solid 5035400-201537-21 MS L-9 Total/NA
Solid 5035400-201537-21 MSD L-9 Total/NA
Prep Batch: 526975
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-201537-25 SW-1A Total/NA
Solid 5035400-201537-26 SW-1B Total/NA
Solid 5035400-201537-27 SW-2A Total/NA
Solid 5035400-201537-28 SW-2B Total/NA
Solid 5035400-201537-29 SW-3A Total/NA
Solid 5035400-201537-30 SW-3B Total/NA
Solid 5035400-201537-31 SW-4A Total/NA
Solid 5035400-201537-32 SW-4B Total/NA
Solid 5035400-201537-33 B-1 Total/NA
Solid 5035400-201537-34 B-2 Total/NA
Solid 5035MB 400-526975/1-A Method Blank Total/NA
Solid 5035LCS 400-526975/2-A Lab Control Sample Total/NA
Solid 5035LCSD 400-526975/3-A Lab Control Sample Dup Total/NA
Solid 5035400-201537-27 MS SW-2A Total/NA
Solid 5035400-201537-27 MSD SW-2A Total/NA
Analysis Batch: 526980
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 526975400-201537-25 SW-1A Total/NA
Solid MAVPH 526975400-201537-26 SW-1B Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
GC VOA (Continued)
Analysis Batch: 526980 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 526975400-201537-27 SW-2A Total/NA
Solid MAVPH 526975400-201537-28 SW-2B Total/NA
Solid MAVPH 526975400-201537-29 SW-3A Total/NA
Solid MAVPH 526975400-201537-30 SW-3B Total/NA
Solid MAVPH 526975400-201537-31 SW-4A Total/NA
Solid MAVPH 526975400-201537-32 SW-4B Total/NA
Solid MAVPH 526975400-201537-33 B-1 Total/NA
Solid MAVPH 526975400-201537-34 B-2 Total/NA
Solid MAVPH 526975MB 400-526975/1-A Method Blank Total/NA
Solid MAVPH 526975LCS 400-526975/2-A Lab Control Sample Total/NA
Solid MAVPH 526975LCSD 400-526975/3-A Lab Control Sample Dup Total/NA
Solid MAVPH 526975400-201537-27 MS SW-2A Total/NA
Solid MAVPH 526975400-201537-27 MSD SW-2A Total/NA
Analysis Batch: 527014
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 527015400-201537-22 L-10 Total/NA
Solid 8015C 527015400-201537-23 L-11 Total/NA
Solid 8015C 527015MB 400-527015/2-A Method Blank Total/NA
Solid 8015C 527015LCS 400-527015/1-A Lab Control Sample Total/NA
Solid 8015C 527015400-201537-22 MS L-10 Total/NA
Solid 8015C 527015400-201537-22 MSD L-10 Total/NA
Prep Batch: 527015
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-201537-22 L-10 Total/NA
Solid 5035400-201537-23 L-11 Total/NA
Solid 5035MB 400-527015/2-A Method Blank Total/NA
Solid 5035LCS 400-527015/1-A Lab Control Sample Total/NA
Solid 5035400-201537-22 MS L-10 Total/NA
Solid 5035400-201537-22 MSD L-10 Total/NA
GC Semi VOA
Prep Batch: 526533
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546400-201537-1 T-1/S-1 Total/NA
Solid 3546400-201537-2 T-1/S-2 Total/NA
Solid 3546400-201537-35 PL-1 Total/NA
Solid 3546400-201537-39 D-3 Total/NA
Solid 3546MB 400-526533/1-A Method Blank Total/NA
Solid 3546LCS 400-526533/2-A Lab Control Sample Total/NA
Solid 3546LCSD 400-526533/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 526686
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 526533400-201537-1 T-1/S-1 Total/NA
Solid 8015C 526533400-201537-2 T-1/S-2 Total/NA
Solid 8015C 526533400-201537-39 D-3 Total/NA
Solid 8015C 526533MB 400-526533/1-A Method Blank Total/NA
Solid 8015C 526533LCS 400-526533/2-A Lab Control Sample Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
GC Semi VOA (Continued)
Analysis Batch: 526686 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 526533LCSD 400-526533/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 526835
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 526533400-201537-35 PL-1 Total/NA
General Chemistry
Analysis Batch: 526832
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture400-201537-1 T-1/S-1 Total/NA
Solid Moisture400-201537-2 T-1/S-2 Total/NA
Solid Moisture400-201537-35 PL-1 Total/NA
Solid Moisture400-201537-39 D-3 Total/NA
Analysis Batch: 527101
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture400-201537-3 T2/S1 Total/NA
Solid Moisture400-201537-4 T2/S2 Total/NA
Solid Moisture400-201537-5 T2/S3 Total/NA
Solid Moisture400-201537-6 T3/S1 Total/NA
Solid Moisture400-201537-7 T3/S2 Total/NA
Solid Moisture400-201537-8 T3/S3 Total/NA
Solid Moisture400-201537-9 T4/S1 Total/NA
Solid Moisture400-201537-10 T4/S2 Total/NA
Solid Moisture400-201537-11 T4/S3 Total/NA
Solid Moisture400-201537-12 L-13 Total/NA
Solid Moisture400-201537-13 L-1 Total/NA
Solid Moisture400-201537-14 L-2 Total/NA
Solid Moisture400-201537-15 L-3 Total/NA
Solid Moisture400-201537-16 L-4 Total/NA
Solid Moisture400-201537-17 L-5 Total/NA
Solid Moisture400-201537-18 L-6 Total/NA
Solid Moisture400-201537-19 L-7 Total/NA
Solid Moisture400-201537-20 L-8 Total/NA
Solid Moisture400-201537-21 L-9 Total/NA
Solid Moisture400-201537-22 L-10 Total/NA
Solid Moisture400-201537-23 L-11 Total/NA
Solid Moisture400-201537-24 L-12 Total/NA
Solid Moisture400-201537-25 SW-1A Total/NA
Solid Moisture400-201537-26 SW-1B Total/NA
Solid Moisture400-201537-27 SW-2A Total/NA
Solid Moisture400-201537-28 SW-2B Total/NA
Solid Moisture400-201537-29 SW-3A Total/NA
Solid Moisture400-201537-30 SW-3B Total/NA
Solid Moisture400-201537-31 SW-4A Total/NA
Solid Moisture400-201537-32 SW-4B Total/NA
Solid Moisture400-201537-33 B-1 Total/NA
Solid Moisture400-201537-34 B-2 Total/NA
Solid Moisture400-201537-36 PL-2 Total/NA
Solid Moisture400-201537-37 D-1 Total/NA
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
General Chemistry (Continued)
Analysis Batch: 527101 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture400-201537-38 D-2 Total/NA
Solid Moisture400-201537-21 DU L-9 Total/NA
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 400-527442/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527343 Prep Batch: 527442
RL MDL
Acetone 13 U 25 13 ug/Kg 04/13/21 12:34 04/13/21 14:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.67 U 0.675.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Benzene
1.3 U 1.35.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Bromobenzene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Chlorobromomethane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Dichlorobromomethane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Bromoform
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Bromomethane
6.0 U 6.025 ug/Kg 04/13/21 12:34 04/13/21 14:10 12-Butanone (MEK)
0.96 U 0.965.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1n-Butylbenzene
0.95 U 0.955.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1sec-Butylbenzene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1tert-Butylbenzene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Carbon disulfide
1.7 U 1.75.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Carbon tetrachloride
0.52 U 0.525.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Chlorobenzene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Chloroethane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Chloroform
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Chloromethane
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 13-Chloro-1-propene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 12-Chlorotoluene
0.98 U 0.985.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 14-Chlorotoluene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Chlorodibromomethane
3.3 U 3.35.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2-Dibromo-3-Chloropropane
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Ethylene Dibromide
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Dibromomethane
0.71 U 0.715.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2-Dichlorobenzene
0.95 U 0.955.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,3-Dichlorobenzene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,4-Dichlorobenzene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1trans-1,4-Dichloro-2-butene
1.3 U 1.35.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Dichlorodifluoromethane
0.83 U 0.835.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1-Dichloroethane
0.82 U 0.825.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2-Dichloroethane
0.76 U 0.765.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1cis-1,2-Dichloroethene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1trans-1,2-Dichloroethene
1.4 U 1.45.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2-Dichloroethene, Total
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1-Dichloroethene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2-Dichloropropane
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,3-Dichloropropane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 12,2-Dichloropropane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1-Dichloropropene
1.2 U 1.25.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1cis-1,3-Dichloropropene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1trans-1,3-Dichloropropene
0.61 U 0.615.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Ethylbenzene
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Ethyl methacrylate
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Hexachlorobutadiene
5.0 U 5.025 ug/Kg 04/13/21 12:34 04/13/21 14:10 12-Hexanone
3.4 U 3.45.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Iodomethane
10 U 1025 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Isobutyl alcohol
0.68 U 0.685.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Isopropylbenzene
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-527442/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527343 Prep Batch: 527442
RL MDL
4-Isopropyltoluene 1.0 U 5.0 1.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
10 U 1015 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Methylene Chloride
5.0 U 5.025 ug/Kg 04/13/21 12:34 04/13/21 14:10 14-Methyl-2-pentanone (MIBK)
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Methyl tert-butyl ether
2.0 U 2.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Naphthalene
0.90 U 0.905.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1N-Propylbenzene
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Styrene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1,1,2-Tetrachloroethane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1,2,2-Tetrachloroethane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Tetrachloroethene
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Toluene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2,3-Trichlorobenzene
2.0 U 2.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2,4-Trichlorobenzene
1.1 U 1.15.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1,1-Trichloroethane
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1,2-Trichloroethane
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Trichloroethene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Trichlorofluoromethane
3.0 U 3.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2,3-Trichloropropane
2.0 U 2.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,2,4-Trimethylbenzene
0.83 U 0.835.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,3,5-Trimethylbenzene
9.1 U 9.125 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Vinyl acetate
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Vinyl chloride
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1o-Xylene
1.3 U 1.35.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1m-Xylene & p-Xylene
1.9 U 1.910 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Xylenes, Total
0.94 U 0.945.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Cyclohexane
4.6 U 4.65.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Methyl acetate
1.5 U 1.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Methylcyclohexane
5.0 U 5.010 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Tetrahydrofuran
1.2 U 1.25.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Hexane
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Ethyl ether
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1n-Heptane
2.5 U 2.510 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,3-Dichloropropene, Total
1.0 U 1.05.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Butadiene
2.5 U 2.55.0 ug/Kg 04/13/21 12:34 04/13/21 14:10 1Dichlorofluoromethane
8.0 U 8.010 ug/Kg 04/13/21 12:34 04/13/21 14:10 12-Methyl-2-propanol
50 U 50500 ug/Kg 04/13/21 12:34 04/13/21 14:10 11,4-Dioxane
4-Bromofluorobenzene 97 67-130 04/13/21 14:10 1
MB MB
Surrogate
04/13/21 12:34
Dil FacPreparedAnalyzedQualifierLimits%Recovery
110 04/13/21 12:34 04/13/21 14:10 1Dibromofluoromethane77-127
103 04/13/21 12:34 04/13/21 14:10 1Toluene-d8 (Surr)76-127
110 04/13/21 12:34 04/13/21 14:10 11,2-Dichloroethane-d4 (Surr)78-146
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-527442/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527343 Prep Batch: 527442
Acetone 200 210 ug/Kg 105 48-160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 51.9 ug/Kg 104 65-130
Bromobenzene 50.0 55.4 ug/Kg 111 65-130
Chlorobromomethane 50.0 58.6 ug/Kg 117 65-130
Dichlorobromomethane 50.0 50.3 ug/Kg 101 61-130
Bromoform 50.0 56.8 ug/Kg 114 52-136
Bromomethane 50.0 57.5 ug/Kg 115 12-160
2-Butanone (MEK)200 209 ug/Kg 105 55-130
n-Butylbenzene 50.0 65.9 *+ug/Kg 132 66-130
sec-Butylbenzene 50.0 57.0 ug/Kg 114 67-130
tert-Butylbenzene 50.0 45.9 ug/Kg 92 67-130
Carbon disulfide 50.0 53.6 ug/Kg 107 46-141
Carbon tetrachloride 50.0 56.5 ug/Kg 113 60-130
Chlorobenzene 50.0 54.8 ug/Kg 110 70-130
Chloroethane 50.0 57.6 ug/Kg 115 55-134
Chloroform 50.0 51.7 ug/Kg 103 62-130
Chloromethane 50.0 57.1 ug/Kg 114 49-136
3-Chloro-1-propene 50.0 55.2 ug/Kg 110 57-130
2-Chlorotoluene 50.0 54.9 ug/Kg 110 67-130
4-Chlorotoluene 50.0 54.8 ug/Kg 110 66-130
Chlorodibromomethane 50.0 55.7 ug/Kg 111 58-132
1,2-Dibromo-3-Chloropropane 50.0 52.7 ug/Kg 105 49-130
Ethylene Dibromide 50.0 53.2 ug/Kg 106 67-130
Dibromomethane 50.0 51.8 ug/Kg 104 65-130
1,2-Dichlorobenzene 50.0 57.5 ug/Kg 115 64-130
1,3-Dichlorobenzene 50.0 59.5 ug/Kg 119 66-130
1,4-Dichlorobenzene 50.0 57.6 ug/Kg 115 65-130
trans-1,4-Dichloro-2-butene 50.0 48.0 ug/Kg 96 45-137
Dichlorodifluoromethane 50.0 55.4 ug/Kg 111 34-143
1,1-Dichloroethane 50.0 51.5 ug/Kg 103 59-130
1,2-Dichloroethane 50.0 50.9 ug/Kg 102 62-130
cis-1,2-Dichloroethene 50.0 53.7 ug/Kg 107 53-135
trans-1,2-Dichloroethene 50.0 52.5 ug/Kg 105 58-134
1,2-Dichloroethene, Total 100 106 ug/Kg 106 70-130
1,1-Dichloroethene 50.0 49.3 ug/Kg 99 55-137
1,2-Dichloropropane 50.0 51.4 ug/Kg 103 64-130
1,3-Dichloropropane 50.0 50.3 ug/Kg 101 67-130
2,2-Dichloropropane 50.0 50.9 ug/Kg 102 51-132
1,1-Dichloropropene 50.0 51.6 ug/Kg 103 65-130
cis-1,3-Dichloropropene 50.0 48.0 ug/Kg 96 61-130
trans-1,3-Dichloropropene 50.0 51.3 ug/Kg 103 60-130
Ethylbenzene 50.0 54.3 ug/Kg 109 70-130
Ethyl methacrylate 50.0 47.7 ug/Kg 95 62-130
Hexachlorobutadiene 50.0 64.7 ug/Kg 129 62-133
2-Hexanone 200 229 ug/Kg 114 57-131
Iodomethane 50.0 60.3 ug/Kg 121 12-160
Isobutyl alcohol 1250 1390 ug/Kg 111 44-136
Isopropylbenzene 50.0 55.8 ug/Kg 112 70-130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-527442/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527343 Prep Batch: 527442
4-Isopropyltoluene 50.0 61.9 ug/Kg 124 68-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Methylene Chloride 50.0 51.2 ug/Kg 102 57-132
4-Methyl-2-pentanone (MIBK)200 222 ug/Kg 111 58-130
Methyl tert-butyl ether 50.0 47.4 ug/Kg 95 63-130
Naphthalene 50.0 41.9 ug/Kg 84 45-144
N-Propylbenzene 50.0 57.1 ug/Kg 114 67-130
Styrene 50.0 52.3 ug/Kg 105 68-130
1,1,1,2-Tetrachloroethane 50.0 58.2 ug/Kg 116 65-130
1,1,2,2-Tetrachloroethane 50.0 51.0 ug/Kg 102 60-131
Tetrachloroethene 50.0 59.1 ug/Kg 118 67-130
Toluene 50.0 52.9 ug/Kg 106 70-130
1,2,3-Trichlorobenzene 50.0 55.7 ug/Kg 111 58-135
1,2,4-Trichlorobenzene 50.0 60.8 ug/Kg 122 56-138
1,1,1-Trichloroethane 50.0 53.2 ug/Kg 106 63-130
1,1,2-Trichloroethane 50.0 53.0 ug/Kg 106 65-130
Trichloroethene 50.0 55.9 ug/Kg 112 65-130
Trichlorofluoromethane 50.0 51.8 ug/Kg 104 61-136
1,2,3-Trichloropropane 50.0 50.3 ug/Kg 101 60-130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 55.6 ug/Kg 111 47-143
1,2,4-Trimethylbenzene 50.0 59.4 ug/Kg 119 66-130
1,3,5-Trimethylbenzene 50.0 54.8 ug/Kg 110 67-130
Vinyl acetate 100 101 ug/Kg 101 24-160
Vinyl chloride 50.0 56.3 ug/Kg 113 52-132
o-Xylene 50.0 54.1 ug/Kg 108 70-130
m-Xylene & p-Xylene 50.0 53.6 ug/Kg 107 70-130
Xylenes, Total 100 108 ug/Kg 108 70-130
Cyclohexane 50.0 51.3 ug/Kg 103 61-130
Methyl acetate 100 115 ug/Kg 115 49-139
Methylcyclohexane 50.0 50.7 ug/Kg 101 64-130
Tetrahydrofuran 100 100 ug/Kg 100 52-132
Hexane 50.0 53.6 ug/Kg 107 57-132
Ethyl ether 50.0 52.0 ug/Kg 104 58-130
n-Heptane 50.0 56.6 ug/Kg 113 61-130
1,3-Dichloropropene, Total 100 99.3 ug/Kg 99 60-140
Butadiene 50.0 60.0 ug/Kg 120 52-132
Dichlorofluoromethane 50.0 52.6 ug/Kg 105 57-134
2-Methyl-2-propanol 500 521 ug/Kg 104 33-130
1,4-Dioxane 1000 957 ug/Kg 96 41-148
4-Bromofluorobenzene 67 -130
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
107Dibromofluoromethane 77 -127
101Toluene-d8 (Surr)76 -127
1041,2-Dichloroethane-d4 (Surr)78 -146
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-527637/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527629 Prep Batch: 527637
RL MDL
Iodomethane 3.4 U 5.0 3.4 ug/Kg 04/14/21 17:34 04/14/21 19:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.0 U 1.05.0 ug/Kg 04/14/21 17:34 04/14/21 19:54 14-Isopropyltoluene
1.0 U 1.05.0 ug/Kg 04/14/21 17:34 04/14/21 19:54 11,2,4-Trimethylbenzene
0.83 U 0.835.0 ug/Kg 04/14/21 17:34 04/14/21 19:54 11,3,5-Trimethylbenzene
1.0 U 1.05.0 ug/Kg 04/14/21 17:34 04/14/21 19:54 1o-Xylene
1.3 U 1.35.0 ug/Kg 04/14/21 17:34 04/14/21 19:54 1m-Xylene & p-Xylene
1.9 U 1.910 ug/Kg 04/14/21 17:34 04/14/21 19:54 1Xylenes, Total
8.0 U 8.010 ug/Kg 04/14/21 17:34 04/14/21 19:54 12-Methyl-2-propanol
4-Bromofluorobenzene 100 67-130 04/14/21 19:54 1
MB MB
Surrogate
04/14/21 17:34
Dil FacPreparedAnalyzedQualifierLimits%Recovery
112 04/14/21 17:34 04/14/21 19:54 1Dibromofluoromethane77-127
102 04/14/21 17:34 04/14/21 19:54 1Toluene-d8 (Surr)76-127
108 04/14/21 17:34 04/14/21 19:54 11,2-Dichloroethane-d4 (Surr)78-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-527637/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527629 Prep Batch: 527637
Iodomethane 50.0 52.2 ug/Kg 104 12-160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Isopropyltoluene 50.0 58.7 ug/Kg 117 68-130
1,2,4-Trimethylbenzene 50.0 56.5 ug/Kg 113 66-130
1,3,5-Trimethylbenzene 50.0 52.7 ug/Kg 105 67-130
o-Xylene 50.0 52.0 ug/Kg 104 70-130
m-Xylene & p-Xylene 50.0 51.5 ug/Kg 103 70-130
Xylenes, Total 100 104 ug/Kg 104 70-130
2-Methyl-2-propanol 500 409 ug/Kg 82 33-130
4-Bromofluorobenzene 67 -130
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
108Dibromofluoromethane 77 -127
101Toluene-d8 (Surr)76 -127
1031,2-Dichloroethane-d4 (Surr)78 -146
Method: 8015C - Gasoline Range Organics (GRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-526785/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526810 Prep Batch: 526785
RL MDL
C6-C10 50 U 100 50 ug/Kg 04/07/21 21:00 04/08/21 01:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)105 65-125 04/08/21 01:13 1
MB MB
Surrogate
04/07/21 21:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8015C - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-526785/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526810 Prep Batch: 526785
C6-C10 1000 1030 ug/Kg 103 62-141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: T-1/S-1Lab Sample ID: 400-201537-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526810 Prep Batch: 526785
C6-C10 2800 U 55200 60600 ug/Kg 110 10-150☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
99
MS MS
Qualifier Limits%Recovery
Client Sample ID: T-1/S-1Lab Sample ID: 400-201537-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526810 Prep Batch: 526785
C6-C10 2800 U 55200 64500 ug/Kg 117 10-150 6 32☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-526959/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526866 Prep Batch: 526959
RL MDL
C6-C10 50 U 100 50 ug/Kg 04/08/21 16:00 04/09/21 11:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)103 65-125 04/09/21 11:20 1
MB MB
Surrogate
04/08/21 16:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-526959/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526866 Prep Batch: 526959
C6-C10 1000 1050 ug/Kg 105 62-141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8015C - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: L-9Lab Sample ID: 400-201537-21 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526866 Prep Batch: 526959
C6-C10 90000 65900 158000 ug/Kg 104 10-150☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
97
MS MS
Qualifier Limits%Recovery
Client Sample ID: L-9Lab Sample ID: 400-201537-21 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526866 Prep Batch: 526959
C6-C10 90000 65900 158000 ug/Kg 104 10-150 0 32☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
95
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-527015/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527014 Prep Batch: 527015
RL MDL
C6-C10 50 U 100 50 ug/Kg 04/09/21 12:00 04/09/21 14:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)103 65-125 04/09/21 14:28 1
MB MB
Surrogate
04/09/21 12:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-527015/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527014 Prep Batch: 527015
C6-C10 1000 1060 ug/Kg 106 62-141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: L-10Lab Sample ID: 400-201537-22 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527014 Prep Batch: 527015
C6-C10 1800000 1350000 3420000 ug/Kg 121 10-150☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
101
MS MS
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8015C - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: L-10Lab Sample ID: 400-201537-22 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527014 Prep Batch: 527015
C6-C10 1800000 1350000 3180000 ug/Kg 104 10-150 7 32☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-526975/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526980 Prep Batch: 526975
RL MDL
C5-C8 Aliphatics 2.7 U 2.7 2.7 mg/Kg 04/09/21 09:45 04/09/21 11:43 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.4 U 1.41.4 mg/Kg 04/09/21 09:45 04/09/21 11:43 50C9-C12 Aliphatics
0.75 U 0.750.75 mg/Kg 04/09/21 09:45 04/09/21 11:43 50C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)98 70-130 04/09/21 11:43 50
MB MB
Surrogate
04/09/21 09:45
Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 04/09/21 09:45 04/09/21 11:43 50a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-526975/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526980 Prep Batch: 526975
C5-C8 Aliphatics 15.0 14.3 mg/Kg 96 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C12 Aliphatics 17.5 16.8 mg/Kg 96 70-130
C9-C10 Aromatics 2.50 2.51 mg/Kg 100 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-526975/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526980 Prep Batch: 526975
C5-C8 Aliphatics 15.0 15.0 mg/Kg 100 70-130 4 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C12 Aliphatics 17.5 17.5 mg/Kg 100 70-130 4 25
C9-C10 Aromatics 2.50 2.57 mg/Kg 103 70-130 2 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: SW-2ALab Sample ID: 400-201537-27 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526980 Prep Batch: 526975
C5-C8 Aliphatics 4.1 U 22.6 23.5 mg/Kg 104 70-130☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
C9-C12 Aliphatics 2.1 U 26.4 26.0 mg/Kg 99 70-130☼
C9-C10 Aromatics 3.6 3.77 7.18 mg/Kg 96 70-130☼
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
97
MS MS
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: SW-2ALab Sample ID: 400-201537-27 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526980 Prep Batch: 526975
C5-C8 Aliphatics 4.1 U 22.6 23.7 mg/Kg 105 70-130 1 25☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
C9-C12 Aliphatics 2.1 U 26.4 26.2 mg/Kg 99 70-130 1 25☼
C9-C10 Aromatics 3.6 3.77 6.92 mg/Kg 89 70-130 4 25☼
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
98
MSD MSD
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Method: 8015C - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-526533/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526686 Prep Batch: 526533
RL MDL
C10-C28 2.0 U 5.0 2.0 mg/Kg 04/06/21 12:45 04/07/21 16:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl (Surr)87 27-150 04/07/21 16:41 1
MB MB
Surrogate
04/06/21 12:45
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-526533/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526686 Prep Batch: 526533
C10-C28 277 243 mg/Kg 88 38-138
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr)27 -150
Surrogate
107
LCS LCS
Qualifier Limits%Recovery
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method: 8015C - Diesel Range Organics (DRO) (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-526533/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 526686 Prep Batch: 526533
C10-C28 277 230 mg/Kg 83 38-138 5 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
o-Terphenyl (Surr)27 -150
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
Method: Moisture - Percent Moisture
Client Sample ID: L-9Lab Sample ID: 400-201537-21 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 527101
Percent Solids 82.0 92.0 F3 %11 4
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Moisture 18.0 8.0 F3 %77 4
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: T-1/S-1 Lab Sample ID: 400-201537-1
Matrix: SolidDate Collected: 03/30/21 10:55
Date Received: 04/03/21 09:40
Analysis Moisture TMP04/08/21 12:011 TAL PEN526832
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T-1/S-1 Lab Sample ID: 400-201537-1
Matrix: SolidDate Collected: 03/30/21 10:55
Percent Solids: 92.2Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.311 g 5.00 g
Analysis 8015C 50 526810 04/08/21 02:10 NTH TAL PENTotal/NA 5 mL 5 mL
Prep 3546 526533 04/06/21 12:56 BKL TAL PENTotal/NA 15.20 g 1 mL
Analysis 8015C 5 526686 04/07/21 17:23 LHB TAL PENTotal/NA
Client Sample ID: T-1/S-2 Lab Sample ID: 400-201537-2
Matrix: SolidDate Collected: 03/30/21 11:00
Date Received: 04/03/21 09:40
Analysis Moisture TMP04/08/21 12:011 TAL PEN526832
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T-1/S-2 Lab Sample ID: 400-201537-2
Matrix: SolidDate Collected: 03/30/21 11:00
Percent Solids: 78.7Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 7.269 g 5.00 g
Analysis 8015C 50 526810 04/08/21 03:27 NTH TAL PENTotal/NA 5 mL 5 mL
Prep 3546 526533 04/06/21 12:56 BKL TAL PENTotal/NA 15.07 g 1 mL
Analysis 8015C 1 526686 04/07/21 17:37 LHB TAL PENTotal/NA
Client Sample ID: T2/S1 Lab Sample ID: 400-201537-3
Matrix: SolidDate Collected: 03/31/21 11:00
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T2/S1 Lab Sample ID: 400-201537-3
Matrix: SolidDate Collected: 03/31/21 11:00
Percent Solids: 73.4Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.065 g 5.00 g
Analysis 8015C 50 526810 04/08/21 04:19 NTH TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: T2/S2 Lab Sample ID: 400-201537-4
Matrix: SolidDate Collected: 03/31/21 11:05
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T2/S2 Lab Sample ID: 400-201537-4
Matrix: SolidDate Collected: 03/31/21 11:05
Percent Solids: 82.2Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.601 g 5.00 g
Analysis 8015C 50 526810 04/08/21 04:45 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T2/S3 Lab Sample ID: 400-201537-5
Matrix: SolidDate Collected: 03/31/21 11:10
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T2/S3 Lab Sample ID: 400-201537-5
Matrix: SolidDate Collected: 03/31/21 11:10
Percent Solids: 80.0Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.712 g 5.00 g
Analysis 8015C 50 526810 04/08/21 05:12 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T3/S1 Lab Sample ID: 400-201537-6
Matrix: SolidDate Collected: 03/31/21 10:45
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T3/S1 Lab Sample ID: 400-201537-6
Matrix: SolidDate Collected: 03/31/21 10:45
Percent Solids: 74.3Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.135 g 5.00 g
Analysis 8015C 50 526810 04/08/21 05:38 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T3/S2 Lab Sample ID: 400-201537-7
Matrix: SolidDate Collected: 03/31/21 10:50
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: T3/S2 Lab Sample ID: 400-201537-7
Matrix: SolidDate Collected: 03/31/21 10:50
Percent Solids: 78.8Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.994 g 5.00 g
Analysis 8015C 50 526810 04/08/21 06:04 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T3/S3 Lab Sample ID: 400-201537-8
Matrix: SolidDate Collected: 03/31/21 10:55
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T3/S3 Lab Sample ID: 400-201537-8
Matrix: SolidDate Collected: 03/31/21 10:55
Percent Solids: 80.6Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.2 g 5.00 g
Analysis 8015C 50 526810 04/08/21 06:30 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T4/S1 Lab Sample ID: 400-201537-9
Matrix: SolidDate Collected: 03/31/21 10:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T4/S1 Lab Sample ID: 400-201537-9
Matrix: SolidDate Collected: 03/31/21 10:30
Percent Solids: 80.7Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.981 g 5.00 g
Analysis 8015C 50 526810 04/08/21 06:57 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T4/S2 Lab Sample ID: 400-201537-10
Matrix: SolidDate Collected: 03/31/21 10:35
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: T4/S2 Lab Sample ID: 400-201537-10
Matrix: SolidDate Collected: 03/31/21 10:35
Percent Solids: 77.1Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.292 g 5.00 g
Analysis 8015C 50 526810 04/08/21 07:23 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T4/S3 Lab Sample ID: 400-201537-11
Matrix: SolidDate Collected: 03/31/21 10:40
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: T4/S3 Lab Sample ID: 400-201537-11
Matrix: SolidDate Collected: 03/31/21 10:40
Percent Solids: 81.2Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.339 g 5.00 g
Analysis 8015C 50 526810 04/08/21 07:50 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-13 Lab Sample ID: 400-201537-12
Matrix: SolidDate Collected: 04/01/21 10:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-13 Lab Sample ID: 400-201537-12
Matrix: SolidDate Collected: 04/01/21 10:30
Percent Solids: 78.3Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1 g 5.00 g
Analysis 8015C 50 526810 04/08/21 08:16 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-1 Lab Sample ID: 400-201537-13
Matrix: SolidDate Collected: 03/31/21 14:00
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: L-1 Lab Sample ID: 400-201537-13
Matrix: SolidDate Collected: 03/31/21 14:00
Percent Solids: 80.5Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.718 g 5.00 g
Analysis 8015C 250 526866 04/08/21 23:05 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-2 Lab Sample ID: 400-201537-14
Matrix: SolidDate Collected: 03/31/21 14:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-2 Lab Sample ID: 400-201537-14
Matrix: SolidDate Collected: 03/31/21 14:30
Percent Solids: 81.3Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.88 g 5.00 g
Analysis 8015C 200 526866 04/08/21 23:32 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-3 Lab Sample ID: 400-201537-15
Matrix: SolidDate Collected: 04/01/21 08:00
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-3 Lab Sample ID: 400-201537-15
Matrix: SolidDate Collected: 04/01/21 08:00
Percent Solids: 73.9Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.655 g 5.00 g
Analysis 8015C 500 526866 04/08/21 23:58 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-4 Lab Sample ID: 400-201537-16
Matrix: SolidDate Collected: 04/01/21 08:10
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: L-4 Lab Sample ID: 400-201537-16
Matrix: SolidDate Collected: 04/01/21 08:10
Percent Solids: 85.8Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.985 g 5.00 g
Analysis 8015C 200 526866 04/09/21 00:24 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-5 Lab Sample ID: 400-201537-17
Matrix: SolidDate Collected: 04/01/21 08:20
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-5 Lab Sample ID: 400-201537-17
Matrix: SolidDate Collected: 04/01/21 08:20
Percent Solids: 71.1Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.703 g 5.00 g
Analysis 8015C 50 526810 04/08/21 10:55 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-6 Lab Sample ID: 400-201537-18
Matrix: SolidDate Collected: 04/01/21 08:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-6 Lab Sample ID: 400-201537-18
Matrix: SolidDate Collected: 04/01/21 08:30
Percent Solids: 75.2Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.409 g 5.00 g
Analysis 8015C 50 526810 04/08/21 11:22 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-7 Lab Sample ID: 400-201537-19
Matrix: SolidDate Collected: 04/01/21 08:40
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: L-7 Lab Sample ID: 400-201537-19
Matrix: SolidDate Collected: 04/01/21 08:40
Percent Solids: 74.4Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.321 g 5.00 g
Analysis 8015C 500 526866 04/09/21 00:51 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-8 Lab Sample ID: 400-201537-20
Matrix: SolidDate Collected: 04/01/21 09:00
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:091 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-8 Lab Sample ID: 400-201537-20
Matrix: SolidDate Collected: 04/01/21 09:00
Percent Solids: 75.3Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.082 g 5.00 g
Analysis 8015C 500 526866 04/09/21 01:18 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-9 Lab Sample ID: 400-201537-21
Matrix: SolidDate Collected: 04/01/21 09:10
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-9 Lab Sample ID: 400-201537-21
Matrix: SolidDate Collected: 04/01/21 09:10
Percent Solids: 82.0Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.554 g 5.00 g
Analysis 8015C 50 526866 04/08/21 17:48 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-10 Lab Sample ID: 400-201537-22
Matrix: SolidDate Collected: 04/01/21 09:20
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: L-10 Lab Sample ID: 400-201537-22
Matrix: SolidDate Collected: 04/01/21 09:20
Percent Solids: 79.4Date Received: 04/03/21 09:40
Prep 5035 NTH04/09/21 12:00 TAL PEN527015
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.744 g 5.00 g
Analysis 8015C 1000 527014 04/09/21 14:58 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-11 Lab Sample ID: 400-201537-23
Matrix: SolidDate Collected: 04/01/21 09:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-11 Lab Sample ID: 400-201537-23
Matrix: SolidDate Collected: 04/01/21 09:30
Percent Solids: 80.0Date Received: 04/03/21 09:40
Prep 5035 NTH04/09/21 12:00 TAL PEN527015
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.389 g 5.00 g
Analysis 8015C 1000 527014 04/09/21 16:15 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-12 Lab Sample ID: 400-201537-24
Matrix: SolidDate Collected: 04/01/21 10:00
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: L-12 Lab Sample ID: 400-201537-24
Matrix: SolidDate Collected: 04/01/21 10:00
Percent Solids: 83.5Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.247 g 5.00 g
Analysis 8015C 50 526866 04/08/21 20:00 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-1A Lab Sample ID: 400-201537-25
Matrix: SolidDate Collected: 04/01/21 11:10
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: SW-1A Lab Sample ID: 400-201537-25
Matrix: SolidDate Collected: 04/01/21 11:10
Percent Solids: 86.7Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 14.644 g 15.00 g
Analysis 8260D 500 527343 04/13/21 23:01 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 DL 527637 04/14/21 17:34 EEH TAL PENTotal/NA 14.644 g 15.00 g
Analysis 8260D DL 1000 527629 04/15/21 04:20 EEH TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 14.644 g 15.00 g
Analysis MAVPH 10000 526980 04/10/21 04:47 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-1B Lab Sample ID: 400-201537-26
Matrix: SolidDate Collected: 04/01/21 11:45
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-1B Lab Sample ID: 400-201537-26
Matrix: SolidDate Collected: 04/01/21 11:45
Percent Solids: 89.2Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 14.834 g 15.00 g
Analysis 8260D 100 527343 04/13/21 22:08 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 527637 04/14/21 17:34 EEH TAL PENTotal/NA 14.834 g 15.00 g
Analysis 8260D 100 527629 04/15/21 03:53 EEH TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 14.834 g 15.00 g
Analysis MAVPH 2000 526980 04/10/21 05:48 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-2A Lab Sample ID: 400-201537-27
Matrix: SolidDate Collected: 04/01/21 11:15
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-2A Lab Sample ID: 400-201537-27
Matrix: SolidDate Collected: 04/01/21 11:15
Percent Solids: 77.9Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.032 g 5.00 g
Analysis 8260D 1 527343 04/13/21 19:03 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 15.74 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 14:43 GRK TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: SW-2B Lab Sample ID: 400-201537-28
Matrix: SolidDate Collected: 04/01/21 11:20
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-2B Lab Sample ID: 400-201537-28
Matrix: SolidDate Collected: 04/01/21 11:20
Percent Solids: 89.8Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 18.743 g 15.00 g
Analysis 8260D 50 527343 04/13/21 21:42 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 527637 04/14/21 17:34 EEH TAL PENTotal/NA 18.743 g 15.00 g
Analysis 8260D 50 527629 04/15/21 01:12 EEH TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 18.743 g 15.00 g
Analysis MAVPH 1000 526980 04/10/21 06:48 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-3A Lab Sample ID: 400-201537-29
Matrix: SolidDate Collected: 04/01/21 11:25
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-3A Lab Sample ID: 400-201537-29
Matrix: SolidDate Collected: 04/01/21 11:25
Percent Solids: 80.2Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.671 g 5.00 g
Analysis 8260D 1 527343 04/13/21 19:29 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 14.149 g 15.00 g
Analysis MAVPH 50 526980 04/10/21 03:47 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-3B Lab Sample ID: 400-201537-30
Matrix: SolidDate Collected: 04/01/21 11:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-3B Lab Sample ID: 400-201537-30
Matrix: SolidDate Collected: 04/01/21 11:30
Percent Solids: 78.7Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.231 g 5.00 g
Analysis 8260D 1 527343 04/13/21 19:56 SAB TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: SW-3B Lab Sample ID: 400-201537-30
Matrix: SolidDate Collected: 04/01/21 11:30
Percent Solids: 78.7Date Received: 04/03/21 09:40
Prep 5035 EEH04/14/21 17:34DL TAL PEN527637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.25 g 15.00 g
Analysis 8260D DL 50 527629 04/15/21 01:38 EEH TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 15.25 g 15.00 g
Analysis MAVPH 50 526980 04/10/21 02:47 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-4A Lab Sample ID: 400-201537-31
Matrix: SolidDate Collected: 04/01/21 11:35
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-4A Lab Sample ID: 400-201537-31
Matrix: SolidDate Collected: 04/01/21 11:35
Percent Solids: 76.5Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.29 g 15.00 g
Analysis 8260D 250 527343 04/13/21 22:35 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 DL 527637 04/14/21 17:34 EEH TAL PENTotal/NA 4.29 g 15.00 g
Analysis 8260D DL 1000 527629 04/15/21 04:46 EEH TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 4.29 g 15.00 g
Analysis MAVPH 5000 526980 04/10/21 09:53 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-4B Lab Sample ID: 400-201537-32
Matrix: SolidDate Collected: 04/01/21 11:40
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SW-4B Lab Sample ID: 400-201537-32
Matrix: SolidDate Collected: 04/01/21 11:40
Percent Solids: 78.1Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.052 g 5.00 g
Analysis 8260D 1 527343 04/13/21 20:22 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 15.298 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 21:45 GRK TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: B-1 Lab Sample ID: 400-201537-33
Matrix: SolidDate Collected: 04/01/21 11:00
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: B-1 Lab Sample ID: 400-201537-33
Matrix: SolidDate Collected: 04/01/21 11:00
Percent Solids: 78.0Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.324 g 5.00 g
Analysis 8260D 1 527343 04/13/21 20:49 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 14.573 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 22:45 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: B-2 Lab Sample ID: 400-201537-34
Matrix: SolidDate Collected: 04/01/21 11:05
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: B-2 Lab Sample ID: 400-201537-34
Matrix: SolidDate Collected: 04/01/21 11:05
Percent Solids: 79.6Date Received: 04/03/21 09:40
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.41 g 5.00 g
Analysis 8260D 1 527343 04/13/21 21:15 SAB TAL PENTotal/NA 5 mL 5 mL
Prep 5035 526975 04/09/21 09:45 SAB TAL PENTotal/NA 10.881 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 23:46 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: PL-1 Lab Sample ID: 400-201537-35
Matrix: SolidDate Collected: 04/01/21 15:00
Date Received: 04/03/21 09:40
Analysis Moisture TMP04/08/21 12:011 TAL PEN526832
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: PL-1 Lab Sample ID: 400-201537-35
Matrix: SolidDate Collected: 04/01/21 15:00
Percent Solids: 86.1Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.563 g 5.00 g
Analysis 8015C 50 526866 04/08/21 20:27 NTH TAL PENTotal/NA 5 mL 5 mL
Prep 3546 526533 04/06/21 12:56 BKL TAL PENTotal/NA 15.36 g 1 mL
Analysis 8015C 1 526835 04/08/21 12:57 JAW TAL PENTotal/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: PL-2 Lab Sample ID: 400-201537-36
Matrix: SolidDate Collected: 04/01/21 15:45
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: PL-2 Lab Sample ID: 400-201537-36
Matrix: SolidDate Collected: 04/01/21 15:45
Percent Solids: 90.5Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.923 g 5.00 g
Analysis 8015C 50 526866 04/08/21 20:53 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: D-1 Lab Sample ID: 400-201537-37
Matrix: SolidDate Collected: 04/01/21 15:25
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: D-1 Lab Sample ID: 400-201537-37
Matrix: SolidDate Collected: 04/01/21 15:25
Percent Solids: 82.9Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.218 g 5.00 g
Analysis 8015C 50 526866 04/08/21 21:46 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: D-2 Lab Sample ID: 400-201537-38
Matrix: SolidDate Collected: 04/01/21 15:30
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: D-2 Lab Sample ID: 400-201537-38
Matrix: SolidDate Collected: 04/01/21 15:30
Percent Solids: 75.5Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.36 g 5.00 g
Analysis 8015C 50 526866 04/08/21 22:13 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: D-3 Lab Sample ID: 400-201537-39
Matrix: SolidDate Collected: 04/01/21 15:15
Date Received: 04/03/21 09:40
Analysis Moisture TMP04/08/21 12:011 TAL PEN526832
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: D-3 Lab Sample ID: 400-201537-39
Matrix: SolidDate Collected: 04/01/21 15:15
Percent Solids: 86.7Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.804 g 5.00 g
Analysis 8015C 50 526866 04/08/21 22:39 NTH TAL PENTotal/NA 5 mL 5 mL
Prep 3546 526533 04/06/21 12:56 BKL TAL PENTotal/NA 15.07 g 1 mL
Analysis 8015C 5 526686 04/07/21 18:06 LHB TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-526533/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL04/06/21 12:45 TAL PEN526533
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8015C 1 526686 04/07/21 16:41 LHB TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-526785/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8015C 1 526810 04/08/21 01:13 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-526959/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8015C 1 526866 04/09/21 11:20 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-526975/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 SAB04/09/21 09:45 TAL PEN526975
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 11:43 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-527015/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 NTH04/09/21 12:00 TAL PEN527015
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8015C 1 527014 04/09/21 14:28 NTH TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: Method Blank Lab Sample ID: MB 400-527442/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 527343 04/13/21 14:10 SAB TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-527637/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 EEH04/14/21 17:34 TAL PEN527637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 527629 04/14/21 19:54 EEH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-526533/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL04/06/21 12:45 TAL PEN526533
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8015C 1 526686 04/07/21 16:55 LHB TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-526785/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8015C 1 526810 04/08/21 01:39 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-526959/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8015C 1 526866 04/09/21 11:37 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-526975/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 SAB04/09/21 09:45 TAL PEN526975
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 12:43 GRK TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-527015/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 NTH04/09/21 12:00 TAL PEN527015
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8015C 1 527014 04/09/21 14:11 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-527442/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 SAB04/13/21 12:34 TAL PEN527442
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 527343 04/13/21 13:10 SAB TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-527637/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 EEH04/14/21 17:34 TAL PEN527637
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.00 g 5.00 g
Analysis 8260D 1 527629 04/14/21 18:57 EEH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-526533/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL04/06/21 12:45 TAL PEN526533
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8015C 1 526686 04/07/21 17:09 LHB TAL PENTotal/NA
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-526975/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 5035 SAB04/09/21 09:45 TAL PEN526975
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 15.00 g
Analysis MAVPH 50 526980 04/09/21 13:43 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: T-1/S-1 Lab Sample ID: 400-201537-1 MS
Matrix: SolidDate Collected: 03/30/21 10:55
Percent Solids: 92.2Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.311 g 5.00 g
Analysis 8015C 50 526810 04/08/21 02:34 NTH TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: T-1/S-1 Lab Sample ID: 400-201537-1 MSD
Matrix: SolidDate Collected: 03/30/21 10:55
Percent Solids: 92.2Date Received: 04/03/21 09:40
Prep 5035 NTH04/07/21 21:00 TAL PEN526785
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.311 g 5.00 g
Analysis 8015C 50 526810 04/08/21 03:00 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-9 Lab Sample ID: 400-201537-21 MS
Matrix: SolidDate Collected: 04/01/21 09:10
Percent Solids: 82.0Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.554 g 5.00 g
Analysis 8015C 50 526866 04/08/21 18:14 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-9 Lab Sample ID: 400-201537-21 MSD
Matrix: SolidDate Collected: 04/01/21 09:10
Percent Solids: 82.0Date Received: 04/03/21 09:40
Prep 5035 NTH04/08/21 16:00 TAL PEN526959
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.554 g 5.00 g
Analysis 8015C 50 526866 04/08/21 18:41 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-10 Lab Sample ID: 400-201537-22 MS
Matrix: SolidDate Collected: 04/01/21 09:20
Percent Solids: 79.4Date Received: 04/03/21 09:40
Prep 5035 NTH04/09/21 12:00 TAL PEN527015
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.744 g 5.00 g
Analysis 8015C 1000 527014 04/09/21 15:22 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-10 Lab Sample ID: 400-201537-22 MSD
Matrix: SolidDate Collected: 04/01/21 09:20
Percent Solids: 79.4Date Received: 04/03/21 09:40
Prep 5035 NTH04/09/21 12:00 TAL PEN527015
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.744 g 5.00 g
Analysis 8015C 1000 527014 04/09/21 15:49 NTH TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: SW-2A Lab Sample ID: 400-201537-27 MS
Matrix: SolidDate Collected: 04/01/21 11:15
Percent Solids: 77.9Date Received: 04/03/21 09:40
Prep 5035 SAB04/09/21 09:45 TAL PEN526975
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.74 g 15.00 g
Analysis MAVPH 50 526980 04/10/21 00:46 GRK TAL PENTotal/NA 5 mL 5 mL
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Client Sample ID: SW-2A Lab Sample ID: 400-201537-27 MSD
Matrix: SolidDate Collected: 04/01/21 11:15
Percent Solids: 77.9Date Received: 04/03/21 09:40
Prep 5035 SAB04/09/21 09:45 TAL PEN526975
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.74 g 15.00 g
Analysis MAVPH 50 526980 04/10/21 01:46 GRK TAL PENTotal/NA 5 mL 5 mL
Client Sample ID: L-9 Lab Sample ID: 400-201537-21 DU
Matrix: SolidDate Collected: 04/01/21 09:10
Date Received: 04/03/21 09:40
Analysis Moisture AW04/10/21 10:401 TAL PEN527101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Method Summary
Job ID: 400-201537-1Client: S&ME, Inc.
SDG: Lure Moores ChapelProject/Site: LURE
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL PEN
SW8468015CGasoline Range Organics (GRO) (GC)TAL PEN
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)TAL PEN
EPA8015CDiesel Range Organics (DRO) (GC)TAL PEN
EPAMoisturePercent Moisture TAL PEN
SW8463546Microwave Extraction TAL PEN
SW8465035Closed System Purge and Trap TAL PEN
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 400-201537-1
Project/Site: LURE SDG: Lure Moores Chapel
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)314State 12-31-21
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
8260D 5035 Solid 1,2-Dichloroethene, Total
8260D 5035 Solid 1,3-Dichloropropene, Total
8260D 5035 Solid Butadiene
8260D 5035 Solid Hexane
8260D 5035 Solid n-Heptane
8260D 5035 Solid Tetrahydrofuran
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
Eurofins TestAmerica, Pensacola
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 400-201537-1
SDG Number: Lure Moores Chapel
Login Number: 201537
Question Answer Comment
Creator: Conrady, Hank W
List Source: Eurofins TestAmerica, Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.4°C 0.0°C 0.0°C 1.1°C IR-7
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Pensacola
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Appendix VII – NCDEQ UST-61 Form
Appendix IX – Backfill Manifests

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report Region _______
Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________
Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
 GIS Address matching
 Other
 Unknown
Describe location:

HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
 Release Detection Equipment or Methods
 During UST Closure/Removal
 Property Transfer
 Visual/Odor
 Water in Tank
 Water Supply Well Contamination
 Groundwater Contamination
 Surface Water Contamination
 Other (specify) _______________

SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)

 Tank
 Piping
 Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
 Unknown
Definitions presented on reverse

 Spill
 Overfill
 Corrosion
 Physical/Mechanical
Damage
 Install Problem
 Other
 Unknown
Definitions presented on reverse

 Petroleum
 Non-Petroleum
 Both
Location
(Check one)
 Facility
 Residence
 Other

 Gasoline/ Diesel/
Kerosene
 Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics

 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2

Y
Y YN
N
316513/31/21CommReg
10100 Moores Chapel Road
Charlotte
Mecklenburg
28214
35.274753 -80.970128
x
Center of former dispenserisland
On March 31, 2021, field screening of soil beneath 10,000-gal gasoline UST indicated a release. However,
release is suspected to have been from lines and/or dispensers and flowed laterally to back-filled sands
that were used during the UST system installation. Field screening of native soils at a few feet below the
10,000-gallon gasoline UST were at levels that may indicate limited vertical contaminant migration.
X
XX
X X
X
Former Snappy Food Mart (previously operated by Handy Dandy; they no longer exist)

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3.
UST SYSTEM OWNER UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined
A January 26, 2021 email from Ruth Strauss (NCDEQ) references Handy Dandy as last owner of the USTs. Handy Dandy no longer exists.
A January 26, 2021 email from Ruth Strauss (NCDEQ) references Handy Dandy as last owner of USTs but did not list the last operator of the USTs. Handy Dandy no longer exists.
Charlotte NC 28214
10100 Moores Chapel Road
[phone]
Costar, LLC
James Wellons
Senior Project Manager
S&ME, Inc.
3/31/21
[phone]
9751 Southern Pine Boulevard
Appendix VIII – Soil Disposal Manifests
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
aka Former Snappy Food Mart
Appendix X – NCDEQ UST-2A Form
UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST

Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING

phone [phone] fax [phone] http://www.wastenotnc.org/

STATE USE ONLY: Facility ID #

Date Received

INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II, III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City County Street Address
State

Zip Code

City

County

Zip Code

Phone Number
Phone Number

III. CONTACT PERSONNEL
Contact for Facility:

Job Title:

Phone #:

Closure Contractor Name:

Closure Contractor Company:

Address:

Phone #

Primary Consultant Name:

Primary Consultant Company:

Address:

Phone #

IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/ concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete.
Print name and official title of owner or owner’s authorized representative

Signature Date Signed

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016