MO-28112_47377_CA_CLO_20201028

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
Excel Civil & Environmental Associates, PLLC
6 2 5 H u n t s m a n C o u r t
G a s t o n i a , N o r t h C a r o l i n a 2 8 0 5 4
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F a c s i m i l e : ( 7 0 4 ) 8 5 3 - 3 9 4 9
I n t e r n e t : www.excelengr.com
October 28, 2020

Mr. Dan Bowser
NCDEQ / DWM / UST Section
Mooresville Regional Office
610 East Center Ave, Suite 301
Mooresville, North Carolina 28115

Re: UST Closure Report
Sam’s Mart 80
8325 Old Statesville Road
Charlotte, North Carolina
Land Use: COMMERCIAL
NCDEQ Facility ID No. 00-0-0000035683
EXCEL Project No. 2020102

Dear Mr. Bowser:

Excel Civil & Environmental Associates, PLLC (Excel) respectfully submits for your review
and approval this UST Closure Report for the above-referenced facility. This report details
the underground storage tank closure activities conducted at the facility by Excel during
October 2020.

If you have any questions, please contact the undersigned.

Sincerely yours,
EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
M. T. Stanforth, P.E., DEE
Principal Engineer

UST Closure Report Page No. i
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
TABLE OF CONTENTS

SECTION NO. PAGE NO.
1.0 GENERAL INFORMATION .................................................................................................... 1
2.0 CLOSURE PROCEDURES .................................................................................................... 2
3.0 SITE INVESTIGATION .......................................................................................................... 4
4.0 CONCLUSIONS & RECOMMENDATIONS ............................................................................... 6
5.0 LIMITATIONS ..................................................................................................................... 6
6.0 REFERENECES .................................................................................................................. 7
7.0 SIGNATURE OF PROFESSIONAL ENGINEER ......................................................................... 7

LIST OF TABLES
TABLE 1 – PROJECT CONTACTS
TABLE 2 – UST INFORMATION
TABLE 3 – SOIL SUMMARY DATA
TABLE 4 – GROUNDWATER SUMMARY DATA

LIST OF FIGURES
FIGURE 1 – SITE VICINITY MAP
FIGURE 2 – SITE PLAN
FIGURE 3 – SOIL CONSTITUENTS MAP

APPENDICES
APPENDIX A – LABORATORY REPORT & COC FORM
APPENDIX B – SITE PHOTOGRAPHS
APPENDIX C – DISPOSAL MANIFEST

UST Closure Report Page No. 1
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
UST CLOSURE REPORT

(The closure report should contain, at a minimum, the following information. Any other information
that is pertinent to the site should be included.)

1.0 General Information

A. Ownership of USTs

1. Name of UST owner;
Sam’s Mart, Inc.

2. Owner address and telephone number;

7935 Council Place
Charlotte, North Carolina 28105
Telephone: [phone]

B. Facility Information

1. Facility name;
Sam’s Mart 103

2. Facility ID #;

00-0-0000035683

3. Facility address, telephone number and county;

8325 Old Statesville Road
Charlotte, Mecklenburg County, North Carolina 28269
Telephone: [phone]

C. Contacts

1. Name, address, telephone number and job title of primary contact person

Mr. Adnan Jazairi
Sam’s Mart, Incorporated
7935 Council Place, Suite 200
Matthews, North Carolina 28105
[phone]

2. Name, address, and telephone number of closure contractor;
Diversified Demolition
1431 Springwood Lane
Charlotte, North Carolina 28210
Telephone: [phone]
UST Closure Report Page No. 2
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
3. Name, address, and telephone number of primary consultant;
Excel Civil & Environmental Associates, PLLC (ECEA)
625 Huntsman Court
Gastonia, North Carolina 28054
Telephone: [phone]
Attn: Mike Stanforth

4. Name, address, telephone number, and State certification number of
laboratory;
PACE Analytical
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Telephone: [phone]
NC Certification No: 5342

D. UST Information - not applicable, line closure only

E. Site Characteristics

1. Describe any past releases at this site;

No release has been reported in association with this UST system.

2. Is the facility active or inactive at this time? If the facility is inactive note the
last time the USTs were in operation;
The facility is currently active.

3. Describe surrounding property use (for example, residential, commercial,
farming, etc.);
The area is generally commercial in nature. Surrounding properties consist of a paint store
to the north, Old Statesville Road and a gas station, WT Harris Boulevard and vacant land
beyond and auto repair to the west.

4. Describe site geology/hydrogeology;

The subject site is located in the Piedmont Physiographic Province. Rocks are, for the
most part, metamorphosed and deeply weathered. The 1985 USGS Geologic Map of
North Carolina indicates underlying formations in this area of the Piedmont Physiographic
Province consisting of a biotite gneiss and schists. No bedrock was encountered during
line closure activities. The soils were identified as silts and clays encountered to a depth
of approximately eleven feet below grade level.

2.0 Closure Procedures

A. Describe preparations for closure including the steps taken to notify authorities,
permits obtained and the steps taken to cleanup and purge the tanks;

UST Closure Report Page No. 3
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
The “Notice of Intent: UST Permanent Closure or Change-In-Service” form (GW/UST-3) was
submitted by ECEA to the NCDEQ, Division of Waste Management (DWM), Mooresville Regional
Office (MRO).

B. Note the amount of residual material pumped from the tank(s);
The product lines were drained prior to removal; the product was returned to the USTs and
approximately 200 gallons was pumped out prior to closure operations.

C. Describe the storage, sampling and disposal of the residual material;
Storage, sampling, and disposal of residual materials were conducted by Diversified Demolition,
Charlotte, North Carolina.

D. Excavation;

Note: Refer to the "Groundwater Section Guidelines for the Investigation and Remediation
of Soils and Groundwater" on limiting excavations. The Trust Fund will not pay for
excessive excavation unless it is justified and verified by laboratory results.

1. Describe excavation procedures noting the conditions of the soils and the
dimensions of the excavation in relation to the tanks, piping, and/or pumps;

UST system closure activities were conducted at the site in October 2020. The product
lines and UST were removed on October 13, 2020. The UST measured approximately five
feet in diameter and 12 feet long. The excavation was measured at approximately 15 feet
by 10 feet by 11 feet in depth. Soil samples were collected underneath the product lines,
sidewalls of the excavation and a groundwater sample was collected due to the depth of
the water table. Refer to Figure 2 for soil sampling locations.

The guidelines were followed as detailed in the NCDEQ’s “Underground Storage Tank
Section Guidelines for Site Checks, Tank Closure and Initial Response and Abatement”,
dated March 1, 2007 with subsequent revisions.

2. Note the depth of tank burial(s) (from land surface to top of tank);
The product lines and UST were observed to be located approximately three feet below
grade level (bgl).

3. Quantity of soil removed;
None.

4. Describe soil type(s);
Native or residual soils encountered during soil sampling activities were observed to be
red to reddish brown in color consisting of a silt-clay mixture. No bedrock was encountered
during closure activities.

UST Closure Report Page No. 4
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

5. Type and source of backfill used;
The excavation was replaced with pea rock.

E. CONTAMINATED SOIL

1. Describe how it was determined to what extent to excavate the soil;
No over excavation was not conducted as part of the UST closure operations.

2. Describe method of temporary storage, sampling and treatment/disposal of
soil;
Not applicable

3.0 Site Investigation

A. Provide information on field screening and observations, include methods used to
calibrate field-screening instrument(s);

Soil samples were screened during assessment activities as part of ECEA standard operating
procedures for UST Closures.

B. Describe soil sampling points and sampling procedures used;
A total of eight soil samples were collected from the sidewalls of the excavation and product line
with one additional groundwater sample collected from the base of the excavation due to
encountering groundwater (refer to Figure 2 for sample locations).
Soil and groundwater samples for laboratory analysis were preserved and packed into approved
sample containers, stored in a chilled cooler, and submitted to a North Carolina certified
laboratory. Soil samples were collected directly beneath the associated piping and dispensing
systems. The soil samples were analyzed for Total Petroleum Hydrocarbons, gasoline range and
diesel range organics by Method 8015, volatile organics and semi volatile organics by Methods
8260 and 8270 (refer to Table 3). Groundwater samples were collected for volatile organics by
Method 6200B, semi volatile organics by Method 625, MADEP VPH and EPH (refer to Table 4).

C. Describe groundwater or surface water sampling procedures used:

Note: Refer to the "Groundwater Section Guidelines for the Investigation and
Remediation of Soils and Groundwater" for information about sampling
requirements.
Temporary well screen was installed in the excavation, samples collected and removed
after sampling.

UST Closure Report Page No. 5
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
D. Quality Control Measures
Describe sample-handling procedures including sample preservation and
transportation:

After collection, samples were placed in laboratory-supplied containers and labeled. The
samples were then placed in an ice filled cooler for preservation and transported to the
laboratory for applicable analysis.

Describe decontamination procedures used;

To reduce the risk of cross contamination, new disposable latex gloves were worn during
each sample collection. The decontamination procedures outlined below are used for field
equipment (e.g., hand augers, split spoon sampling device, trowels) that come into direct
contact with the material being sampled and that is used more than once at a particular
site. All sampling equipment was decontaminated between each sample by using alconox
and distilled water.

Describe time and date samples were collected and date submitted to lab;
Samples were collected at the site between 1520 and 1630 on October 13, 2020. The
samples were logged into the laboratory October 16, 2020 (see laboratory reports and
associated Chain-of-Custody Forms in Appendix C).

Describe samples collected for quality control purposes (e.g. duplicates, field
blanks, trip blanks, etc.). Include methods used to obtain these samples and
analytical parameters;
No quality control samples were utilized for this assessment.

Describe how results of quality control samples may have affected your
interpretation of soil, groundwater or surface water sample results;
No quality control samples were utilized for this assessment.

E. Investigation Results

Describe results of Site Sensitivity Evaluation (SSE), (if SSE was not conducted,
explain why not);

A surface water body is located approximately 1,800 feet to the northeast of the subject
property and a water well located approximately 1,500 feet to the west.
In addition, underground utilities such as storm sewer, sanitary sewer, water lines, etc.,
are typically considered potential vapor collection points and conduits for
vapor/contamination travel, which are located near Old Statesville Road and WT Harris
Boulevard.

UST Closure Report Page No. 6
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
Describe methods of analyses used (include U.S. EPA method number);

Soil samples were collected directly beneath the associated piping and dispensing
systems. The soil samples were analyzed for Total Petroleum Hydrocarbons, gasoline
range and diesel range organics by Method 8015, volatile organics and semi volatile
organics by Methods 8260 and 8270. Groundwater samples were collected for volatile
organics by Method 6200B, semi volatile organics by Method 625, MADEP VPH and EPH.

Describe analytical results for samples; discuss in relation to site-specific cleanup
level or action level, as appropriate;

Soil samples were collected directly beneath the associated piping and dispensing
systems. The soil samples were analyzed for Total Petroleum Hydrocarbons, gasoline
range and diesel range organics by Method 8015, volatile organics and semi volatile
organics by Methods 8260 and 8270. Groundwater samples were collected for volatile
organics by Method 6200B, semi volatile organics by Method 625, MADEP VPH and EPH.

Soil sample results for all soil sample except for S-2 exceeded the soil to water action limit
for benzene and the S-5 soil sample exceeded the TPH- DRO Action Limit. Groundwater
sample results were below regulatory standards for all analyzed constituents.

Laboratory analytical results for the soil samples are presented in Table 3, groundwater
sample results presented in Table 4, with the analytical laboratory reports presented in
Appendix C.

4.0 Conclusions & Recommendations

Based upon the information in this report, it appears that the soils at the Sam’s Mart 80 UST
system at 8325 Old Statesville Road, Charlotte, North Carolina, have been impacted by petroleum
hydrocarbons from the former UST system.

5.0 Limitations

This report is based on a limited number of soil samples and chemical analyses. The conclusions
presented in this report are based only on the observation made during this investigation and on
data provided by others. The report presents a description of the subsurface conditions observed
at each excavation location during this investigation. Subsurface conditions may vary significantly
with time, particularly with respect to groundwater elevations and quality. Conclusions and
recommendations set forth herein are applicable only to the facts and conditions described at the
time of this report.

In performing its professional services, Excel uses that degree of care and skill exercised under
similar circumstances by members of the environmental profession practicing at the same or
similar locality under similar conditions. The standard of care shall be judged exclusively as of the
time these services are rendered and not according to later standards. Excel makes no express
or implied warranty beyond its conformance to this standard. Excel shall not be responsible for
conditions or consequences arising from the relevant facts that were concealed, withheld or not
fully disclosed for this report. Excel believes that all information contained in this report is factual,
but no guarantee is made or implied.

UST Closure Report Page No. 7
Sam’s Mart 80
Charlotte, North Carolina Excel No. 2020102

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

6.0 References

EPA Region III, 1997. Risk-based Concentration Tables (RBC Tables). Office of RCRA, Technical
and Program Branch, (http://www.epa.gov/reg3hwmd/index.html).

“Underground Storage Tank Section Guidelines for Site Checks, Tank Closure and Initial
Response and Abatement for UST Releases” completed by the UST Section of the NCDEQ,
Division of Waste Management dated March 1, 2007 with subsequent revisions.

“Guidelines for Assessment and Corrective Action for UST Releases” completed by the UST
Section of the NCDEQ, Division of Waste Management dated December 1, 2008 with subsequent
revisions.

7.0 Signature of Professional Engineer

_________________________
Michael T. Stanforth, P.E., DEE
Principal Engineer
UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST
Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
phone [phone] fax [phone] http://www.wastenotnc.org/
STATE USE ONLY:Facility ID #
Date Received
INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II,III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company
Street Address Facility ID # (If known)
City County Street Address
State Zip Code City County Zip Code
Phone Number Phone Number
III. CONTACT PERSONNEL
Contact for Facility: Job Title: Phone #:
Closure Contractor Name: Closure Contractor Company: Address: Phone #
Primary Consultant Name: Primary Consultant Company: Address: Phone #
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/
concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No
VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete.
Signature Date Signed
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY
I.D. #_____________________
Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities. If a Professional Engineer (P.E.) or a Licensed
Geologist (L.G.) provides supervision for closure or change-in-service site assessment activities and signs and seals all closure reports then at least a five
(5) working days is acceptable.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted to the
appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be
submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out.
Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank Closure
and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust. Note: To close tanks in place you must
obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company
Street Address Facility ID # (If known)
City County Street Address
State

Zip Code City County
Zip Code
Phone Number Email Phone Number
III. CONTACT PERSONNEL
Name: Company Name: Job Title: Phone Number:
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1. Contact local fire marshal.
2. Plan entire closure event.
3. Conduct Site Soil Assessment.
4.If removing tanks or closing in place, refer toAPI Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5. Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7.If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G. is not required.
8. Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name: Contractor Company Name:
Address: State:

Zip Code: Phone No:
Primary Consultant Name: Primary Consultant Company Name: Consultant Phone No:
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE
Tank ID No. Size in Gallons Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place * New Contents Stored
*Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title:
Signature Date Signed SCHEDULED REMOVAL DATE Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 3/2020
NC Mecklenburg
NC

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

TABLES

Table 1 – Project Contacts

Table 2 – UST Information

Table 3 –Soil Summary Data

Table 4 –Groundwater Summary Data

Table 1 - Project Contacts
SM 80
8325 Old Statesville Road
Charlotte, North Carolina
Excel Project No. 2020102

OWNERSHIP OF TANKS
Owner Name: Sam’s Mart, Inc.
PROPERTY OWNER
Owner Name: Sam’s Mart, Inc.
Address: 7935 Council Place Charlotte, North Carolina 28105
Telephone Number: [phone]
PROPERTY CONTACT PERSON
Name: Mr. Adnan Jazairi
Job Title: Chief Operating Officer
Telephone Number: [phone]
CLOSURE CONTRACTOR
Name: Diversified Demolition
Address: P.O. Box 519, Cornelius, North Carolina 28031
Telephone Number: [phone]
PRIMARY CONSULTANT
Name: Excel Civil & Environmental Associates, PLLC
Address: 625 Huntsman Court, Gastonia NC 28056
Telephone Number: [phone]
LABORATORY
Name: Pace Analytical
Address: 12065 Lebanon Road, Mt. Juliet, Tennessee 37122
Telephone Number: [phone]
Certification Number: 5342
Table 2 - UST Information
SM 80
8325 Old Statesville Road
Charlotte, North Carolina
Excel Project No. 2020102

Tank No. Size in Gallons Dimensions (ft) Last Contents Noticeable Impact
4 2,000 5 ft dia x 12 ft Kerosene No

Table 3 - Soil Summary Data
Sam's Mart 80
8325 Old Statesville Road, Charlotte, North Carolina
Excel Project No. 2020102
S-1 S-2 S-3 S-4 S-5 S-6 S-7 S-8
10 ft 10 ft 10 ft 10 ft 10 ft 10 ft 3 ft 3 ft
DATE SAMPLED
PID READING 0.0 0.1 0.1 0.0 11.2 0.2 6.0 3.9 ------
BENZENE 0.00627 0.0049 0.00763 0.00795 0.00813 0.00744 0.00757 0.00788 0.0056 18 164
TOLUENE 0.055 0.0418 0.0685 0.0558 0.0727 0.0587 0.0582 0.0607 4.3 1,200 32,000
ETHYLBENZENE 0.00741 0.006 0.0105 0.0115 0.0104 0.00981 0.00813 0.00885 4.9 1,560 40,000
XYLENES 0.0397 0.0334 0.0554 0.0611 0.0584 0.0558 0.0443 0.471 4.6 3,129 81,760
MTBE < 0.000655 < 0.000565 < 0.000666 < 0.00062 < 0.000715 < 0.000651 < 0.000633 < 0.000589 0.091 350 3,100
ACETONE < 0.0683 < 0.0589 < 0.0694 < 0.0646 < 0.0746 < 0.0679 0.0931 0.135 24 14,000 360,000
n-BUTYLBENZENE < 0.00983 < 0.00847 < 0.00999 < 0.00929 < 0.0107 < 0.00976 < 0.00949 0.0113 J 4.3 626 16,350
sec-BUTYLBENZENE < 0.00539 < 0.00465 < 0.00548 < 0.0051 0.0164 J < 0.00536 0.00786 J 0.0254 3.3 626 16,350
NAPHTHALENE < 0.00913 J0 J3 < 0.00787 J0 J3 < 0.00929 J0 J3 < 0.00864 J0 J3 < 0.00997 J0 J3 < 0.00908 0.0123 J 0.0202 J 0.16 313 8,176
ISOPROPYLBENZENE < 0.000795 < 0.000686 0.00142 J 0.00114 J 0.00172 J 0.00107 J 0.00154 J 0.00232 J 1.7 1,564 40,880
TRICHLOROETHENE < 0.00109 < 0.000942 < 0.00111 < 0.00103 < 0.00119 < 0.00109 0.00124 J < 0.000985 0.019 4.6 120
n-PROPYLBENZENE 0.00296 J 0.00226 J 0.00323 J 0.00297 J 0.00343 J 0.00252 J 0.00483 J 0.00501 J 1.7 626 16,350
STYRENE 0.000842 J 0.000632 J 0.00384 J 0.00121 J 0.00135 J 0.0013 J 0.000732 J 0.000928 J 1.5 3,128 81,760
1,2,4-TRIMETHYLBENZENE 0.0119 0.00973 0.0143 0.0164 0.0142 0.0217 0.013 0.0150 8.5 782 20,440
1,3,5-TRIMETHYLBENZENE < 0.00374 < 0.00323 0.00434 J 0.0048 J 0.0046 J 0.00378 J 0.00365 J 0.00484 J 8.5 782 20,440
FLUORENE < 0.00766 < 0.00706 < 0.00782 < 0.00725 0.0185 J < 0.00768 < 0.00738 < 0.00724 47 620 16,400
2-METHYLNAPHTHALENE < 0.0061 < 0.00563 < 0.00623 < 0.00578 0.029 J < 0.00918 0.00753 J 0.0264 J 3.6 63 1,635
NCDEQ Action
Levels
TPH GRO < 1.02 J3 < 0.923 < 1.3 < 0.969 12.3 < 1.01 1.9 J 2.32 B J J3 50
TPH DRO < 1.09 1.3 J < 1.11 1.35 J 141 1.28 J 24.8 11.1 100
NOTES:
Data in mg/kg
VOC - Volatile Organic Compound
SVOC - Semi-Volatile Organic Compound
Bold data represents constituents above Soil-to-Water MSCCs (Maximum Soil Contaminant Concentrations)
Highlighted data represent constituents above Residential Soil Cleanup Levels or NCDEQ Action Levels
Italicized data represent constituents above Industrial / Commercial Soil Cleanup Levels
J - Reported value is an estimate
B - The same analyte was found in the associated blank
J3 - Associated batch QC was outside the established quality control range for precision
Residential
Soil Cleanup
Levels
Industrial /
Commercial
Soil Cleanup
Levels13-Oct-20
SVOCsVOCsSAMPLE LOCATION Soil-to-Water
MSCCs
Table 4 - Groundwater Summary Data
Sam's Mart 80
8325 Old Statesville Road, Charlotte, North Carolina
Excel Project No. 2020102
SAMPLE LOCATION GW-1
DATE SAMPLED 13-Oct-20
EPH C9 - C18 Aliphatics 178 -- --
EPH C19 - C36 Aliphatics < 33.3 10,000 --
EPH C11 - C22 Aromatics 79 J J3 -- --
VPH C5 - C8 Aliphatics < 33.3 400 --
VPH C9 - C12 Aliphatics 85.9 J -- --
VPH C9 - C10 Aromatics 38.1 J -- --
TOTAL C9 - C18 Aliphatics 263.9 J 700 --
TOTAL C9 - C22 Aromatics 117.1 J J3 200 --
BENZENE < 0.0941 1 5,000
TOLUENE < 0.278 600 260,000
ETHYLBENZENE < 0.137 600 84,500
TOTAL XYLENES < 0.604 500 85,500
MTBE < 0.101 20 20,000
NAPHTHALENE < 1 6 6,000
N-PROPYLBENZENE 0.13 J 70 30,000
STYRENE 0.18 J 70 70,000
1,2,4-TRIMETHYLBENZENE 2.92 400 28,500
1,3,5-TRIMETHYLBENZENE 0.991 J 400 25,000
CHLOROFORM 0.31 J 70 70,000
sec-BUTYLBENZENE 0.459 J 70 8,500
ISOPROPYLBENZENE 0.125 J 70 25,000
p-ISOPROPYLTOLUENE 1.92 25 11,700
2-BUTANONE (MEK)2.3 J 4,000 4,000,000
NAPHTHALENE 0.272 J 6 6,000
FLUORANTHENE 0.107 J 300 300
DIMETHYL PHTHALATE 1.6 J ----
PYRENE 0.119 J 200 200
NOTES:
Data in ug/l
MADEP - Massachusetts Dept. of Environmental Protection
EPH - Extractable Petroleum Hydrocarbons
VPH - Volatile Petroleum Hydrocarbons
VOC - Volatile Organic Compound
SVOC - Semi-Volatile Organic Compound
MTBE - Methyl Tert Butyl Ether
J - Reported value is an estimate
J3 - Associated batch QC was outside the established quality control range for precision
NA - Not Analyzed
Bold data represents constituents above NCAC 2L Standards
Highlighted data represent constituents above GCL Standards MADEPSVOCsNCAC 2L GCL
VOCs

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

FIGURES

Figure 1 – Site Vicinity Map

Figure 2 – Site Plan

Figure 3 – Soils Constituent Map

EXCEL CIVIL & ENVIRONMENTAL
ASSOCIATES, PLLC
625 HUNTSMAN COURT
GASTONIA, NC 28054
(704) 853-08000
TOPOGRAPHIC MAP
Excel Project No. 2020102

Source: USGS, 2016 N

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDICES

Appendix A – Laboratory Reports & COC Forms

Appendix B – Site Photographs

Appendix C – Waste Disposal Manifest

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX A

Laboratory Reports & COC Forms

ANALYTICAL REPORT
October 27, 2020
Excel Civil & Environmental Associates
Sample Delivery Group:L1274449
Samples Received:10/16/2020
Project Number:2020102
Description:Sam's Mart 80
Report To:Mr. Mike Stanforth
625 Huntsman Court
Gastonia, NC 28054
Entire Report Reviewed By:
October 27, 2020
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Project Manager
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ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
S-1 L1274449-01 6
S-2 L1274449-02 9
S-3 L1274449-03 12
S-4 L1274449-04 15
S-5 L1274449-05 18
S-6 L1274449-06 21
S-7 L1274449-07 24
S-8 L1274449-08 27
GW-1 L1274449-09 30
Qc: Quality Control Summary 33
Total Solids by Method 2540 G-2011 33
Volatile Petroleum Hydrocarbons by Method MADEPV 35
Volatile Organic Compounds (GC) by Method 8015C 36
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 38
Volatile Organic Compounds (GC/MS) by Method 8260D 43
Semi-Volatile Organic Compounds (GC) by Method 8015C 57
TPH by Method MADEPE 58
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 59
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 64
Gl: Glossary of Terms 70
Al: Accreditations & Locations 72
Sc: Sample Chain of Custody 73
1 Cp
2Tc
3Ss
4Cn
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6Qc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-1 L1274449-01 Solid C DeVane 10/13/20 15:20 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563415 1 10/22/20 15:34 10/22/20 15:48 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563287 25.8 10/13/20 15:20 10/22/20 19:55 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1563529 1 10/13/20 15:20 10/22/20 19:17 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 00:06 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 05:06 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-2 L1274449-02 Solid C DeVane 10/13/20 15:25 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563415 1 10/22/20 15:34 10/22/20 15:48 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563292 26.8 10/13/20 15:25 10/22/20 06:27 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1563529 1 10/13/20 15:25 10/22/20 19:36 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/22/20 23:26 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 02:04 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-3 L1274449-03 Solid C DeVane 10/13/20 15:30 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563415 1 10/22/20 15:34 10/22/20 15:48 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563292 34 10/13/20 15:30 10/22/20 06:49 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1563529 1 10/13/20 15:30 10/22/20 19:55 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 00:19 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 02:45 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-4 L1274449-04 Solid C DeVane 10/13/20 15:35 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563415 1 10/22/20 15:34 10/22/20 15:48 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563292 25 10/13/20 15:35 10/22/20 07:12 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1563529 1 10/13/20 15:35 10/22/20 20:14 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 00:32 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 03:45 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-5 L1274449-05 Solid C DeVane 10/13/20 15:40 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563415 1 10/22/20 15:34 10/22/20 15:48 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563292 25 10/13/20 15:40 10/22/20 07:35 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1563529 1 10/13/20 15:40 10/22/20 20:33 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 03:57 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 04:26 JNJ Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-6 L1274449-06 Solid C DeVane 10/13/20 15:45 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563415 1 10/22/20 15:34 10/22/20 15:48 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563292 25.5 10/13/20 15:45 10/22/20 07:57 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1564404 1.02 10/13/20 15:45 10/23/20 20:36 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1565803 1.07 10/13/20 15:45 10/27/20 01:58 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 04:10 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 02:24 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-7 L1274449-07 Solid C DeVane 10/13/20 16:05 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563417 1 10/22/20 12:33 10/22/20 12:43 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563292 25 10/13/20 16:05 10/22/20 08:19 AV Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1565803 1 10/13/20 16:05 10/27/20 02:36 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 04:23 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 04:46 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-8 L1274449-08 Solid C DeVane 10/13/20 16:25 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1563417 1 10/22/20 12:33 10/22/20 12:43 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015C WG1563287 25.3 10/13/20 16:25 10/22/20 20:16 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1565803 1.01 10/13/20 16:25 10/27/20 02:17 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1563260 1 10/22/20 10:19 10/23/20 04:50 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1563259 1 10/22/20 18:18 10/23/20 06:07 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
GW-1 L1274449-09 GW C DeVane 10/13/20 16:30 10/16/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1563655 1 10/22/20 17:56 10/22/20 17:56 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1565201 1 10/26/20 03:00 10/26/20 03:00 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1565707 1 10/27/20 11:27 10/27/20 11:27 ADM Mt. Juliet, TN
TPH by Method MADEPE WG1563445 1 10/21/20 13:03 10/24/20 08:29 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1563445 1 10/21/20 13:03 10/24/20 10:41 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1561307 1 10/19/20 20:46 10/20/20 03:55 JNJ Mt. Juliet, TN
1 Cp
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3Ss
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5Sr
6Qc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1274449
S-1
Collected date/time: 10/13/20 15:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 70.8 1 10/22/2020 15:48 WG1563415
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction U J3 1020 4680 25.8 10/22/2020 19:55 WG1563287
(S)
a,a,a-Trifluorotoluene(FID)108 77.0-120 10/22/2020 19:55 WG1563287
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 68.3 93.6 1 10/22/2020 19:17 WG1563529
Acrylonitrile U 6.76 23.4 1 10/22/2020 19:17 WG1563529
Benzene 6.27 0.874 1.87 1 10/22/2020 19:17 WG1563529
Bromobenzene U 1.68 23.4 1 10/22/2020 19:17 WG1563529
Bromodichloromethane U 1.36 4.68 1 10/22/2020 19:17 WG1563529
Bromoform U 2.19 46.8 1 10/22/2020 19:17 WG1563529
Bromomethane U J0 J3 3.69 23.4 1 10/22/2020 19:17 WG1563529
n-Butylbenzene U 9.83 23.4 1 10/22/2020 19:17 WG1563529
sec-Butylbenzene U 5.39 23.4 1 10/22/2020 19:17 WG1563529
tert-Butylbenzene U 3.65 9.36 1 10/22/2020 19:17 WG1563529
Carbon tetrachloride U 1.68 9.36 1 10/22/2020 19:17 WG1563529
Chlorobenzene U 0.393 4.68 1 10/22/2020 19:17 WG1563529
Chlorodibromomethane U 1.15 4.68 1 10/22/2020 19:17 WG1563529
Chloroethane U 3.18 9.36 1 10/22/2020 19:17 WG1563529
Chloroform U 1.93 4.68 1 10/22/2020 19:17 WG1563529
Chloromethane U J0 8.14 23.4 1 10/22/2020 19:17 WG1563529
2-Chlorotoluene U 1.62 4.68 1 10/22/2020 19:17 WG1563529
4-Chlorotoluene U 0.842 9.36 1 10/22/2020 19:17 WG1563529
1,2-Dibromo-3-Chloropropane U 7.30 46.8 1 10/22/2020 19:17 WG1563529
1,2-Dibromoethane U 1.21 4.68 1 10/22/2020 19:17 WG1563529
Dibromomethane U 1.40 9.36 1 10/22/2020 19:17 WG1563529
1,2-Dichlorobenzene U J3 0.795 9.36 1 10/22/2020 19:17 WG1563529
1,3-Dichlorobenzene U 1.12 9.36 1 10/22/2020 19:17 WG1563529
1,4-Dichlorobenzene U 1.31 9.36 1 10/22/2020 19:17 WG1563529
Dichlorodifluoromethane U 3.01 4.68 1 10/22/2020 19:17 WG1563529
1,1-Dichloroethane U 0.919 4.68 1 10/22/2020 19:17 WG1563529
1,2-Dichloroethane U 1.21 4.68 1 10/22/2020 19:17 WG1563529
1,1-Dichloroethene U 1.13 4.68 1 10/22/2020 19:17 WG1563529
cis-1,2-Dichloroethene U 1.37 4.68 1 10/22/2020 19:17 WG1563529
trans-1,2-Dichloroethene U 1.95 9.36 1 10/22/2020 19:17 WG1563529
1,2-Dichloropropane U 2.66 9.36 1 10/22/2020 19:17 WG1563529
1,1-Dichloropropene U 1.51 4.68 1 10/22/2020 19:17 WG1563529
1,3-Dichloropropane U 0.938 9.36 1 10/22/2020 19:17 WG1563529
cis-1,3-Dichloropropene U 1.42 4.68 1 10/22/2020 19:17 WG1563529
trans-1,3-Dichloropropene U 2.13 9.36 1 10/22/2020 19:17 WG1563529
2,2-Dichloropropane U 2.58 4.68 1 10/22/2020 19:17 WG1563529
Di-isopropyl ether U 0.767 1.87 1 10/22/2020 19:17 WG1563529
Ethylbenzene 7.41 1.38 4.68 1 10/22/2020 19:17 WG1563529
Hexachloro-1,3-butadiene U 11.2 46.8 1 10/22/2020 19:17 WG1563529
Isopropylbenzene U 0.795 4.68 1 10/22/2020 19:17 WG1563529
p-Isopropyltoluene U 4.77 9.36 1 10/22/2020 19:17 WG1563529
2-Butanone (MEK)U 119 187 1 10/22/2020 19:17 WG1563529
Methylene Chloride U 12.4 46.8 1 10/22/2020 19:17 WG1563529
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1274449
S-1
Collected date/time: 10/13/20 15:20
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 4.27 46.8 1 10/22/2020 19:17 WG1563529
Methyl tert-butyl ether U 0.655 1.87 1 10/22/2020 19:17 WG1563529
Naphthalene U J0 J3 9.13 23.4 1 10/22/2020 19:17 WG1563529
n-Propylbenzene 2.96 J 1.78 9.36 1 10/22/2020 19:17 WG1563529
Styrene 0.842 J 0.429 23.4 1 10/22/2020 19:17 WG1563529
1,1,1,2-Tetrachloroethane U 1.77 4.68 1 10/22/2020 19:17 WG1563529
1,1,2,2-Tetrachloroethane U 1.30 4.68 1 10/22/2020 19:17 WG1563529
Tetrachloroethene U 1.68 4.68 1 10/22/2020 19:17 WG1563529
Toluene 55.0 2.43 9.36 1 10/22/2020 19:17 WG1563529
1,2,3-Trichlorobenzene U C4 13.7 23.4 1 10/22/2020 19:17 WG1563529
1,2,4-Trichlorobenzene U 8.24 23.4 1 10/22/2020 19:17 WG1563529
1,1,1-Trichloroethane U 1.73 4.68 1 10/22/2020 19:17 WG1563529
1,1,2-Trichloroethane U 1.12 4.68 1 10/22/2020 19:17 WG1563529
Trichloroethene U 1.09 1.87 1 10/22/2020 19:17 WG1563529
Trichlorofluoromethane U 1.55 4.68 1 10/22/2020 19:17 WG1563529
1,2,3-Trichloropropane U 3.03 23.4 1 10/22/2020 19:17 WG1563529
1,2,4-Trimethylbenzene 11.9 2.96 9.36 1 10/22/2020 19:17 WG1563529
1,3,5-Trimethylbenzene U 3.74 9.36 1 10/22/2020 19:17 WG1563529
Vinyl chloride U J0 J4 2.17 4.68 1 10/22/2020 19:17 WG1563529
Xylenes, Total 39.7 1.65 12.2 1 10/22/2020 19:17 WG1563529
(S) Toluene-d8 110 75.0-131 10/22/2020 19:17 WG1563529
(S) 4-Bromofluorobenzene 86.4 67.0-138 10/22/2020 19:17 WG1563529
(S) 1,2-Dichloroethane-d4 90.4 70.0-130 10/22/2020 19:17 WG1563529
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction U 1090 5650 1 10/23/2020 00:06 WG1563260
(S) o-Terphenyl 80.3 18.0-148 10/23/2020 00:06 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.62 47.1 1 10/23/2020 05:06 WG1563259
Acenaphthylene U 6.63 47.1 1 10/23/2020 05:06 WG1563259
Anthracene U 8.38 47.1 1 10/23/2020 05:06 WG1563259
Atrazine U 16.3 471 1 10/23/2020 05:06 WG1563259
Benzaldehyde U 25.0 471 1 10/23/2020 05:06 WG1563259
Benzo(a)anthracene U 8.29 47.1 1 10/23/2020 05:06 WG1563259
Benzo(b)fluoranthene U 8.78 47.1 1 10/23/2020 05:06 WG1563259
Benzo(k)fluoranthene U 8.37 47.1 1 10/23/2020 05:06 WG1563259
Benzo(g,h,i)perylene U 8.61 47.1 1 10/23/2020 05:06 WG1563259
Benzo(a)pyrene U 8.75 47.1 1 10/23/2020 05:06 WG1563259
Biphenyl U 15.0 471 1 10/23/2020 05:06 WG1563259
Bis(2-chlorethoxy)methane U 14.1 471 1 10/23/2020 05:06 WG1563259
Bis(2-chloroethyl)ether U 15.5 471 1 10/23/2020 05:06 WG1563259
2,2-Oxybis(1-Chloropropane)U 20.3 471 1 10/23/2020 05:06 WG1563259
4-Bromophenyl-phenylether U 16.5 471 1 10/23/2020 05:06 WG1563259
Caprolactam U 23.3 471 1 10/23/2020 05:06 WG1563259
Carbazole U 14.6 471 1 10/23/2020 05:06 WG1563259
2-Chloronaphthalene U 8.27 47.1 1 10/23/2020 05:06 WG1563259
4-Chlorophenyl-phenylether U 16.4 471 1 10/23/2020 05:06 WG1563259
Chrysene U 9.35 47.1 1 10/23/2020 05:06 WG1563259
Dibenz(a,h)anthracene U 13.0 47.1 1 10/23/2020 05:06 WG1563259
3,3-Dichlorobenzidine U J3 17.4 471 1 10/23/2020 05:06 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1274449
S-1
Collected date/time: 10/13/20 15:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 13.5 471 1 10/23/2020 05:06 WG1563259
2,6-Dinitrotoluene U 15.4 471 1 10/23/2020 05:06 WG1563259
Fluoranthene U 8.49 47.1 1 10/23/2020 05:06 WG1563259
Fluorene U 7.66 47.1 1 10/23/2020 05:06 WG1563259
Hexachlorobenzene U 16.7 471 1 10/23/2020 05:06 WG1563259
Hexachloro-1,3-butadiene U 15.8 471 1 10/23/2020 05:06 WG1563259
Hexachlorocyclopentadiene U 24.7 471 1 10/23/2020 05:06 WG1563259
Hexachloroethane U 18.5 471 1 10/23/2020 05:06 WG1563259
Indeno(1,2,3-cd)pyrene U 13.3 47.1 1 10/23/2020 05:06 WG1563259
Isophorone U 14.4 471 1 10/23/2020 05:06 WG1563259
Naphthalene U 11.8 47.1 1 10/23/2020 05:06 WG1563259
Nitrobenzene U 16.4 471 1 10/23/2020 05:06 WG1563259
n-Nitrosodiphenylamine U 35.6 471 1 10/23/2020 05:06 WG1563259
n-Nitrosodi-n-propylamine U 15.7 471 1 10/23/2020 05:06 WG1563259
Phenanthrene U 9.34 47.1 1 10/23/2020 05:06 WG1563259
Benzylbutyl phthalate U 14.7 471 1 10/23/2020 05:06 WG1563259
Bis(2-ethylhexyl)phthalate U 59.6 471 1 10/23/2020 05:06 WG1563259
Di-n-butyl phthalate U 16.1 471 1 10/23/2020 05:06 WG1563259
Diethyl phthalate U 15.5 471 1 10/23/2020 05:06 WG1563259
Dimethyl phthalate U 99.8 471 1 10/23/2020 05:06 WG1563259
Di-n-octyl phthalate U 31.8 471 1 10/23/2020 05:06 WG1563259
Pyrene U 9.16 47.1 1 10/23/2020 05:06 WG1563259
4-Chloroaniline U 17.0 471 1 10/23/2020 05:06 WG1563259
4-Chloro-3-methylphenol U 15.3 471 1 10/23/2020 05:06 WG1563259
2-Chlorophenol U 15.5 471 1 10/23/2020 05:06 WG1563259
Dibenzofuran U 15.4 471 1 10/23/2020 05:06 WG1563259
2,4-Dichlorophenol U 13.7 471 1 10/23/2020 05:06 WG1563259
2,4-Dimethylphenol U 12.3 471 1 10/23/2020 05:06 WG1563259
4,6-Dinitro-2-methylphenol U 107 471 1 10/23/2020 05:06 WG1563259
2,4-Dinitrophenol U 110 471 1 10/23/2020 05:06 WG1563259
2-Methylnaphthalene U 6.10 47.1 1 10/23/2020 05:06 WG1563259
2-Methylphenol U 14.1 471 1 10/23/2020 05:06 WG1563259
3&4-Methyl Phenol U 14.7 471 1 10/23/2020 05:06 WG1563259
2-Nitroaniline U 15.1 471 1 10/23/2020 05:06 WG1563259
3-Nitroaniline U 15.0 471 1 10/23/2020 05:06 WG1563259
4-Nitroaniline U 13.7 471 1 10/23/2020 05:06 WG1563259
2-Nitrophenol U 16.8 471 1 10/23/2020 05:06 WG1563259
4-Nitrophenol U 14.7 471 1 10/23/2020 05:06 WG1563259
Pentachlorophenol U 12.7 471 1 10/23/2020 05:06 WG1563259
Phenol U 18.9 471 1 10/23/2020 05:06 WG1563259
2,4,6-Trichlorophenol U 15.1 471 1 10/23/2020 05:06 WG1563259
Acetophenone U 14.7 471 1 10/23/2020 05:06 WG1563259
1,2,4,5-Tetrachlorobenzene U 22.5 471 1 10/23/2020 05:06 WG1563259
2,4,5-Trichlorophenol U 16.0 471 1 10/23/2020 05:06 WG1563259
2,3,4,6-Tetrachlorophenol U 17.8 471 1 10/23/2020 05:06 WG1563259
(S) 2-Fluorophenol 47.7 12.0-120 10/23/2020 05:06 WG1563259
(S) Phenol-d5 45.0 10.0-120 10/23/2020 05:06 WG1563259
(S) Nitrobenzene-d5 39.1 10.0-122 10/23/2020 05:06 WG1563259
(S) 2-Fluorobiphenyl 45.9 15.0-120 10/23/2020 05:06 WG1563259
(S) 2,4,6-Tribromophenol 60.9 10.0-127 10/23/2020 05:06 WG1563259
(S) p-Terphenyl-d14 48.3 10.0-120 10/23/2020 05:06 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1274449
S-2
Collected date/time: 10/13/20 15:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.8 1 10/22/2020 15:48 WG1563415
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction U 923 4250 26.8 10/22/2020 06:27 WG1563292
(S)
a,a,a-Trifluorotoluene(FID)99.3 77.0-120 10/22/2020 06:27 WG1563292
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 58.9 80.6 1 10/22/2020 19:36 WG1563529
Acrylonitrile U 5.82 20.2 1 10/22/2020 19:36 WG1563529
Benzene 4.90 0.753 1.61 1 10/22/2020 19:36 WG1563529
Bromobenzene U 1.45 20.2 1 10/22/2020 19:36 WG1563529
Bromodichloromethane U 1.17 4.03 1 10/22/2020 19:36 WG1563529
Bromoform U 1.89 40.3 1 10/22/2020 19:36 WG1563529
Bromomethane U J0 J3 3.18 20.2 1 10/22/2020 19:36 WG1563529
n-Butylbenzene U 8.47 20.2 1 10/22/2020 19:36 WG1563529
sec-Butylbenzene U 4.65 20.2 1 10/22/2020 19:36 WG1563529
tert-Butylbenzene U 3.15 8.06 1 10/22/2020 19:36 WG1563529
Carbon tetrachloride U 1.45 8.06 1 10/22/2020 19:36 WG1563529
Chlorobenzene U 0.339 4.03 1 10/22/2020 19:36 WG1563529
Chlorodibromomethane U 0.987 4.03 1 10/22/2020 19:36 WG1563529
Chloroethane U 2.74 8.06 1 10/22/2020 19:36 WG1563529
Chloroform U 1.66 4.03 1 10/22/2020 19:36 WG1563529
Chloromethane U J0 7.02 20.2 1 10/22/2020 19:36 WG1563529
2-Chlorotoluene U 1.40 4.03 1 10/22/2020 19:36 WG1563529
4-Chlorotoluene U 0.726 8.06 1 10/22/2020 19:36 WG1563529
1,2-Dibromo-3-Chloropropane U 6.29 40.3 1 10/22/2020 19:36 WG1563529
1,2-Dibromoethane U 1.05 4.03 1 10/22/2020 19:36 WG1563529
Dibromomethane U 1.21 8.06 1 10/22/2020 19:36 WG1563529
1,2-Dichlorobenzene U J3 0.686 8.06 1 10/22/2020 19:36 WG1563529
1,3-Dichlorobenzene U 0.968 8.06 1 10/22/2020 19:36 WG1563529
1,4-Dichlorobenzene U 1.13 8.06 1 10/22/2020 19:36 WG1563529
Dichlorodifluoromethane U 2.60 4.03 1 10/22/2020 19:36 WG1563529
1,1-Dichloroethane U 0.792 4.03 1 10/22/2020 19:36 WG1563529
1,2-Dichloroethane U 1.05 4.03 1 10/22/2020 19:36 WG1563529
1,1-Dichloroethene U 0.977 4.03 1 10/22/2020 19:36 WG1563529
cis-1,2-Dichloroethene U 1.18 4.03 1 10/22/2020 19:36 WG1563529
trans-1,2-Dichloroethene U 1.68 8.06 1 10/22/2020 19:36 WG1563529
1,2-Dichloropropane U 2.29 8.06 1 10/22/2020 19:36 WG1563529
1,1-Dichloropropene U 1.30 4.03 1 10/22/2020 19:36 WG1563529
1,3-Dichloropropane U 0.808 8.06 1 10/22/2020 19:36 WG1563529
cis-1,3-Dichloropropene U 1.22 4.03 1 10/22/2020 19:36 WG1563529
trans-1,3-Dichloropropene U 1.84 8.06 1 10/22/2020 19:36 WG1563529
2,2-Dichloropropane U 2.23 4.03 1 10/22/2020 19:36 WG1563529
Di-isopropyl ether U 0.661 1.61 1 10/22/2020 19:36 WG1563529
Ethylbenzene 6.00 1.19 4.03 1 10/22/2020 19:36 WG1563529
Hexachloro-1,3-butadiene U 9.68 40.3 1 10/22/2020 19:36 WG1563529
Isopropylbenzene U 0.686 4.03 1 10/22/2020 19:36 WG1563529
p-Isopropyltoluene U 4.11 8.06 1 10/22/2020 19:36 WG1563529
2-Butanone (MEK)U 102 161 1 10/22/2020 19:36 WG1563529
Methylene Chloride U 10.7 40.3 1 10/22/2020 19:36 WG1563529
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1274449
S-2
Collected date/time: 10/13/20 15:25
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 3.68 40.3 1 10/22/2020 19:36 WG1563529
Methyl tert-butyl ether U 0.565 1.61 1 10/22/2020 19:36 WG1563529
Naphthalene U J0 J3 7.87 20.2 1 10/22/2020 19:36 WG1563529
n-Propylbenzene 2.26 J 1.53 8.06 1 10/22/2020 19:36 WG1563529
Styrene 0.632 J 0.369 20.2 1 10/22/2020 19:36 WG1563529
1,1,1,2-Tetrachloroethane U 1.53 4.03 1 10/22/2020 19:36 WG1563529
1,1,2,2-Tetrachloroethane U 1.12 4.03 1 10/22/2020 19:36 WG1563529
Tetrachloroethene U 1.45 4.03 1 10/22/2020 19:36 WG1563529
Toluene 41.8 2.10 8.06 1 10/22/2020 19:36 WG1563529
1,2,3-Trichlorobenzene U C4 11.8 20.2 1 10/22/2020 19:36 WG1563529
1,2,4-Trichlorobenzene U 7.10 20.2 1 10/22/2020 19:36 WG1563529
1,1,1-Trichloroethane U 1.49 4.03 1 10/22/2020 19:36 WG1563529
1,1,2-Trichloroethane U 0.963 4.03 1 10/22/2020 19:36 WG1563529
Trichloroethene U 0.942 1.61 1 10/22/2020 19:36 WG1563529
Trichlorofluoromethane U 1.33 4.03 1 10/22/2020 19:36 WG1563529
1,2,3-Trichloropropane U 2.61 20.2 1 10/22/2020 19:36 WG1563529
1,2,4-Trimethylbenzene 9.73 2.55 8.06 1 10/22/2020 19:36 WG1563529
1,3,5-Trimethylbenzene U 3.23 8.06 1 10/22/2020 19:36 WG1563529
Vinyl chloride U J0 J4 1.87 4.03 1 10/22/2020 19:36 WG1563529
Xylenes, Total 33.4 1.42 10.5 1 10/22/2020 19:36 WG1563529
(S) Toluene-d8 108 75.0-131 10/22/2020 19:36 WG1563529
(S) 4-Bromofluorobenzene 101 67.0-138 10/22/2020 19:36 WG1563529
(S) 1,2-Dichloroethane-d4 92.4 70.0-130 10/22/2020 19:36 WG1563529
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction 1300 J 1000 5210 1 10/22/2020 23:26 WG1563260
(S) o-Terphenyl 82.6 18.0-148 10/22/2020 23:26 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.02 43.4 1 10/23/2020 02:04 WG1563259
Acenaphthylene U 6.11 43.4 1 10/23/2020 02:04 WG1563259
Anthracene U 7.73 43.4 1 10/23/2020 02:04 WG1563259
Atrazine U 15.0 434 1 10/23/2020 02:04 WG1563259
Benzaldehyde U 23.1 434 1 10/23/2020 02:04 WG1563259
Benzo(a)anthracene U 7.65 43.4 1 10/23/2020 02:04 WG1563259
Benzo(b)fluoranthene U 8.09 43.4 1 10/23/2020 02:04 WG1563259
Benzo(k)fluoranthene U 7.71 43.4 1 10/23/2020 02:04 WG1563259
Benzo(g,h,i)perylene U 7.93 43.4 1 10/23/2020 02:04 WG1563259
Benzo(a)pyrene U 8.06 43.4 1 10/23/2020 02:04 WG1563259
Biphenyl U 13.8 434 1 10/23/2020 02:04 WG1563259
Bis(2-chlorethoxy)methane U 13.0 434 1 10/23/2020 02:04 WG1563259
Bis(2-chloroethyl)ether U 14.3 434 1 10/23/2020 02:04 WG1563259
2,2-Oxybis(1-Chloropropane)U 18.8 434 1 10/23/2020 02:04 WG1563259
4-Bromophenyl-phenylether U 15.2 434 1 10/23/2020 02:04 WG1563259
Caprolactam U 21.5 434 1 10/23/2020 02:04 WG1563259
Carbazole U 13.4 434 1 10/23/2020 02:04 WG1563259
2-Chloronaphthalene U 7.62 43.4 1 10/23/2020 02:04 WG1563259
4-Chlorophenyl-phenylether U 15.1 434 1 10/23/2020 02:04 WG1563259
Chrysene U 8.62 43.4 1 10/23/2020 02:04 WG1563259
Dibenz(a,h)anthracene U 12.0 43.4 1 10/23/2020 02:04 WG1563259
3,3-Dichlorobenzidine U 16.0 434 1 10/23/2020 02:04 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1274449
S-2
Collected date/time: 10/13/20 15:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 12.4 434 1 10/23/2020 02:04 WG1563259
2,6-Dinitrotoluene U 14.2 434 1 10/23/2020 02:04 WG1563259
Fluoranthene U 7.83 43.4 1 10/23/2020 02:04 WG1563259
Fluorene U 7.06 43.4 1 10/23/2020 02:04 WG1563259
Hexachlorobenzene U 15.4 434 1 10/23/2020 02:04 WG1563259
Hexachloro-1,3-butadiene U 14.6 434 1 10/23/2020 02:04 WG1563259
Hexachlorocyclopentadiene U 22.8 434 1 10/23/2020 02:04 WG1563259
Hexachloroethane U 17.1 434 1 10/23/2020 02:04 WG1563259
Indeno(1,2,3-cd)pyrene U 12.3 43.4 1 10/23/2020 02:04 WG1563259
Isophorone U 13.3 434 1 10/23/2020 02:04 WG1563259
Naphthalene U 10.9 43.4 1 10/23/2020 02:04 WG1563259
Nitrobenzene U 15.1 434 1 10/23/2020 02:04 WG1563259
n-Nitrosodiphenylamine U 32.8 434 1 10/23/2020 02:04 WG1563259
n-Nitrosodi-n-propylamine U 14.5 434 1 10/23/2020 02:04 WG1563259
Phenanthrene U 8.61 43.4 1 10/23/2020 02:04 WG1563259
Benzylbutyl phthalate U 13.5 434 1 10/23/2020 02:04 WG1563259
Bis(2-ethylhexyl)phthalate U 55.0 434 1 10/23/2020 02:04 WG1563259
Di-n-butyl phthalate U 14.9 434 1 10/23/2020 02:04 WG1563259
Diethyl phthalate U 14.3 434 1 10/23/2020 02:04 WG1563259
Dimethyl phthalate U 92.0 434 1 10/23/2020 02:04 WG1563259
Di-n-octyl phthalate U 29.3 434 1 10/23/2020 02:04 WG1563259
Pyrene U 8.44 43.4 1 10/23/2020 02:04 WG1563259
4-Chloroaniline U 15.6 434 1 10/23/2020 02:04 WG1563259
4-Chloro-3-methylphenol U 14.1 434 1 10/23/2020 02:04 WG1563259
2-Chlorophenol U 14.3 434 1 10/23/2020 02:04 WG1563259
Dibenzofuran U 14.2 434 1 10/23/2020 02:04 WG1563259
2,4-Dichlorophenol U 12.6 434 1 10/23/2020 02:04 WG1563259
2,4-Dimethylphenol U 11.3 434 1 10/23/2020 02:04 WG1563259
4,6-Dinitro-2-methylphenol U 98.4 434 1 10/23/2020 02:04 WG1563259
2,4-Dinitrophenol U 101 434 1 10/23/2020 02:04 WG1563259
2-Methylnaphthalene U 5.63 43.4 1 10/23/2020 02:04 WG1563259
2-Methylphenol U 13.0 434 1 10/23/2020 02:04 WG1563259
3&4-Methyl Phenol U 13.5 434 1 10/23/2020 02:04 WG1563259
2-Nitroaniline U 13.9 434 1 10/23/2020 02:04 WG1563259
3-Nitroaniline U 13.8 434 1 10/23/2020 02:04 WG1563259
4-Nitroaniline U 12.7 434 1 10/23/2020 02:04 WG1563259
2-Nitrophenol U 15.5 434 1 10/23/2020 02:04 WG1563259
4-Nitrophenol U 13.5 434 1 10/23/2020 02:04 WG1563259
Pentachlorophenol U 11.7 434 1 10/23/2020 02:04 WG1563259
Phenol U 17.5 434 1 10/23/2020 02:04 WG1563259
2,4,6-Trichlorophenol U 13.9 434 1 10/23/2020 02:04 WG1563259
Acetophenone U 13.5 434 1 10/23/2020 02:04 WG1563259
1,2,4,5-Tetrachlorobenzene U 20.7 434 1 10/23/2020 02:04 WG1563259
2,4,5-Trichlorophenol U 14.7 434 1 10/23/2020 02:04 WG1563259
2,3,4,6-Tetrachlorophenol U 16.4 434 1 10/23/2020 02:04 WG1563259
(S) 2-Fluorophenol 53.2 12.0-120 10/23/2020 02:04 WG1563259
(S) Phenol-d5 48.3 10.0-120 10/23/2020 02:04 WG1563259
(S) Nitrobenzene-d5 42.6 10.0-122 10/23/2020 02:04 WG1563259
(S) 2-Fluorobiphenyl 51.2 15.0-120 10/23/2020 02:04 WG1563259
(S) 2,4,6-Tribromophenol 56.4 10.0-127 10/23/2020 02:04 WG1563259
(S) p-Terphenyl-d14 49.4 10.0-120 10/23/2020 02:04 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 14:56 11 of 74
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1274449
S-3
Collected date/time: 10/13/20 15:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 69.3 1 10/22/2020 15:48 WG1563415
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction U 1300 6010 34 10/22/2020 06:49 WG1563292
(S)
a,a,a-Trifluorotoluene(FID)99.4 77.0-120 10/22/2020 06:49 WG1563292
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 69.4 95.1 1 10/22/2020 19:55 WG1563529
Acrylonitrile U 6.87 23.8 1 10/22/2020 19:55 WG1563529
Benzene 7.63 0.889 1.90 1 10/22/2020 19:55 WG1563529
Bromobenzene U 1.71 23.8 1 10/22/2020 19:55 WG1563529
Bromodichloromethane U 1.38 4.76 1 10/22/2020 19:55 WG1563529
Bromoform U 2.23 47.6 1 10/22/2020 19:55 WG1563529
Bromomethane U J0 J3 3.75 23.8 1 10/22/2020 19:55 WG1563529
n-Butylbenzene U 9.99 23.8 1 10/22/2020 19:55 WG1563529
sec-Butylbenzene U 5.48 23.8 1 10/22/2020 19:55 WG1563529
tert-Butylbenzene U 3.71 9.51 1 10/22/2020 19:55 WG1563529
Carbon tetrachloride U 1.71 9.51 1 10/22/2020 19:55 WG1563529
Chlorobenzene U 0.400 4.76 1 10/22/2020 19:55 WG1563529
Chlorodibromomethane U 1.16 4.76 1 10/22/2020 19:55 WG1563529
Chloroethane U 3.23 9.51 1 10/22/2020 19:55 WG1563529
Chloroform U 1.96 4.76 1 10/22/2020 19:55 WG1563529
Chloromethane U J0 8.28 23.8 1 10/22/2020 19:55 WG1563529
2-Chlorotoluene U 1.65 4.76 1 10/22/2020 19:55 WG1563529
4-Chlorotoluene U 0.856 9.51 1 10/22/2020 19:55 WG1563529
1,2-Dibromo-3-Chloropropane U 7.42 47.6 1 10/22/2020 19:55 WG1563529
1,2-Dibromoethane U 1.23 4.76 1 10/22/2020 19:55 WG1563529
Dibromomethane U 1.43 9.51 1 10/22/2020 19:55 WG1563529
1,2-Dichlorobenzene U J3 0.809 9.51 1 10/22/2020 19:55 WG1563529
1,3-Dichlorobenzene U 1.14 9.51 1 10/22/2020 19:55 WG1563529
1,4-Dichlorobenzene U 1.33 9.51 1 10/22/2020 19:55 WG1563529
Dichlorodifluoromethane U 3.06 4.76 1 10/22/2020 19:55 WG1563529
1,1-Dichloroethane U 0.934 4.76 1 10/22/2020 19:55 WG1563529
1,2-Dichloroethane U 1.23 4.76 1 10/22/2020 19:55 WG1563529
1,1-Dichloroethene U 1.15 4.76 1 10/22/2020 19:55 WG1563529
cis-1,2-Dichloroethene U 1.40 4.76 1 10/22/2020 19:55 WG1563529
trans-1,2-Dichloroethene U 1.98 9.51 1 10/22/2020 19:55 WG1563529
1,2-Dichloropropane U 2.70 9.51 1 10/22/2020 19:55 WG1563529
1,1-Dichloropropene U 1.54 4.76 1 10/22/2020 19:55 WG1563529
1,3-Dichloropropane U 0.953 9.51 1 10/22/2020 19:55 WG1563529
cis-1,3-Dichloropropene U 1.44 4.76 1 10/22/2020 19:55 WG1563529
trans-1,3-Dichloropropene U 2.17 9.51 1 10/22/2020 19:55 WG1563529
2,2-Dichloropropane U 2.63 4.76 1 10/22/2020 19:55 WG1563529
Di-isopropyl ether U 0.780 1.90 1 10/22/2020 19:55 WG1563529
Ethylbenzene 10.5 1.40 4.76 1 10/22/2020 19:55 WG1563529
Hexachloro-1,3-butadiene U 11.4 47.6 1 10/22/2020 19:55 WG1563529
Isopropylbenzene 1.42 J 0.809 4.76 1 10/22/2020 19:55 WG1563529
p-Isopropyltoluene U 4.85 9.51 1 10/22/2020 19:55 WG1563529
2-Butanone (MEK)U 121 190 1 10/22/2020 19:55 WG1563529
Methylene Chloride U 12.6 47.6 1 10/22/2020 19:55 WG1563529
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1274449
S-3
Collected date/time: 10/13/20 15:30
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 4.34 47.6 1 10/22/2020 19:55 WG1563529
Methyl tert-butyl ether U 0.666 1.90 1 10/22/2020 19:55 WG1563529
Naphthalene U J0 J3 9.29 23.8 1 10/22/2020 19:55 WG1563529
n-Propylbenzene 3.23 J 1.81 9.51 1 10/22/2020 19:55 WG1563529
Styrene 3.84 J 0.436 23.8 1 10/22/2020 19:55 WG1563529
1,1,1,2-Tetrachloroethane U 1.80 4.76 1 10/22/2020 19:55 WG1563529
1,1,2,2-Tetrachloroethane U 1.32 4.76 1 10/22/2020 19:55 WG1563529
Tetrachloroethene U 1.70 4.76 1 10/22/2020 19:55 WG1563529
Toluene 68.5 2.47 9.51 1 10/22/2020 19:55 WG1563529
1,2,3-Trichlorobenzene U C4 13.9 23.8 1 10/22/2020 19:55 WG1563529
1,2,4-Trichlorobenzene U 8.37 23.8 1 10/22/2020 19:55 WG1563529
1,1,1-Trichloroethane U 1.76 4.76 1 10/22/2020 19:55 WG1563529
1,1,2-Trichloroethane U 1.14 4.76 1 10/22/2020 19:55 WG1563529
Trichloroethene U 1.11 1.90 1 10/22/2020 19:55 WG1563529
Trichlorofluoromethane U 1.57 4.76 1 10/22/2020 19:55 WG1563529
1,2,3-Trichloropropane U 3.08 23.8 1 10/22/2020 19:55 WG1563529
1,2,4-Trimethylbenzene 14.3 3.01 9.51 1 10/22/2020 19:55 WG1563529
1,3,5-Trimethylbenzene 4.34 J 3.81 9.51 1 10/22/2020 19:55 WG1563529
Vinyl chloride U J0 J4 2.21 4.76 1 10/22/2020 19:55 WG1563529
Xylenes, Total 55.4 1.67 12.4 1 10/22/2020 19:55 WG1563529
(S) Toluene-d8 108 75.0-131 10/22/2020 19:55 WG1563529
(S) 4-Bromofluorobenzene 95.1 67.0-138 10/22/2020 19:55 WG1563529
(S) 1,2-Dichloroethane-d4 89.9 70.0-130 10/22/2020 19:55 WG1563529
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction U 1110 5770 1 10/23/2020 00:19 WG1563260
(S) o-Terphenyl 77.4 18.0-148 10/23/2020 00:19 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.77 48.0 1 10/23/2020 02:45 WG1563259
Acenaphthylene U 6.76 48.0 1 10/23/2020 02:45 WG1563259
Anthracene U 8.55 48.0 1 10/23/2020 02:45 WG1563259
Atrazine U 16.6 480 1 10/23/2020 02:45 WG1563259
Benzaldehyde U 25.5 480 1 10/23/2020 02:45 WG1563259
Benzo(a)anthracene U 8.46 48.0 1 10/23/2020 02:45 WG1563259
Benzo(b)fluoranthene U 8.96 48.0 1 10/23/2020 02:45 WG1563259
Benzo(k)fluoranthene U 8.54 48.0 1 10/23/2020 02:45 WG1563259
Benzo(g,h,i)perylene U 8.78 48.0 1 10/23/2020 02:45 WG1563259
Benzo(a)pyrene U 8.93 48.0 1 10/23/2020 02:45 WG1563259
Biphenyl U 15.3 480 1 10/23/2020 02:45 WG1563259
Bis(2-chlorethoxy)methane U 14.4 480 1 10/23/2020 02:45 WG1563259
Bis(2-chloroethyl)ether U 15.9 480 1 10/23/2020 02:45 WG1563259
2,2-Oxybis(1-Chloropropane)U 20.8 480 1 10/23/2020 02:45 WG1563259
4-Bromophenyl-phenylether U 16.9 480 1 10/23/2020 02:45 WG1563259
Caprolactam U 23.8 480 1 10/23/2020 02:45 WG1563259
Carbazole U 14.9 480 1 10/23/2020 02:45 WG1563259
2-Chloronaphthalene U 8.44 48.0 1 10/23/2020 02:45 WG1563259
4-Chlorophenyl-phenylether U 16.7 480 1 10/23/2020 02:45 WG1563259
Chrysene U 9.55 48.0 1 10/23/2020 02:45 WG1563259
Dibenz(a,h)anthracene U 13.3 48.0 1 10/23/2020 02:45 WG1563259
3,3-Dichlorobenzidine U 17.7 480 1 10/23/2020 02:45 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1274449
S-3
Collected date/time: 10/13/20 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 13.8 480 1 10/23/2020 02:45 WG1563259
2,6-Dinitrotoluene U 15.7 480 1 10/23/2020 02:45 WG1563259
Fluoranthene U 8.67 48.0 1 10/23/2020 02:45 WG1563259
Fluorene U 7.82 48.0 1 10/23/2020 02:45 WG1563259
Hexachlorobenzene U 17.0 480 1 10/23/2020 02:45 WG1563259
Hexachloro-1,3-butadiene U 16.2 480 1 10/23/2020 02:45 WG1563259
Hexachlorocyclopentadiene U 25.2 480 1 10/23/2020 02:45 WG1563259
Hexachloroethane U 18.9 480 1 10/23/2020 02:45 WG1563259
Indeno(1,2,3-cd)pyrene U 13.6 48.0 1 10/23/2020 02:45 WG1563259
Isophorone U 14.7 480 1 10/23/2020 02:45 WG1563259
Naphthalene U 12.1 48.0 1 10/23/2020 02:45 WG1563259
Nitrobenzene U 16.7 480 1 10/23/2020 02:45 WG1563259
n-Nitrosodiphenylamine U 36.3 480 1 10/23/2020 02:45 WG1563259
n-Nitrosodi-n-propylamine U 16.0 480 1 10/23/2020 02:45 WG1563259
Phenanthrene U 9.53 48.0 1 10/23/2020 02:45 WG1563259
Benzylbutyl phthalate U 15.0 480 1 10/23/2020 02:45 WG1563259
Bis(2-ethylhexyl)phthalate U 60.9 480 1 10/23/2020 02:45 WG1563259
Di-n-butyl phthalate U 16.4 480 1 10/23/2020 02:45 WG1563259
Diethyl phthalate U 15.9 480 1 10/23/2020 02:45 WG1563259
Dimethyl phthalate U 102 480 1 10/23/2020 02:45 WG1563259
Di-n-octyl phthalate U 32.4 480 1 10/23/2020 02:45 WG1563259
Pyrene U 9.34 48.0 1 10/23/2020 02:45 WG1563259
4-Chloroaniline U 17.3 480 1 10/23/2020 02:45 WG1563259
4-Chloro-3-methylphenol U 15.6 480 1 10/23/2020 02:45 WG1563259
2-Chlorophenol U 15.9 480 1 10/23/2020 02:45 WG1563259
Dibenzofuran U 15.7 480 1 10/23/2020 02:45 WG1563259
2,4-Dichlorophenol U 14.0 480 1 10/23/2020 02:45 WG1563259
2,4-Dimethylphenol U 12.5 480 1 10/23/2020 02:45 WG1563259
4,6-Dinitro-2-methylphenol U 109 480 1 10/23/2020 02:45 WG1563259
2,4-Dinitrophenol U 112 480 1 10/23/2020 02:45 WG1563259
2-Methylnaphthalene U 6.23 48.0 1 10/23/2020 02:45 WG1563259
2-Methylphenol U 14.4 480 1 10/23/2020 02:45 WG1563259
3&4-Methyl Phenol U 15.0 480 1 10/23/2020 02:45 WG1563259
2-Nitroaniline U 15.4 480 1 10/23/2020 02:45 WG1563259
3-Nitroaniline U 15.3 480 1 10/23/2020 02:45 WG1563259
4-Nitroaniline U 14.0 480 1 10/23/2020 02:45 WG1563259
2-Nitrophenol U 17.2 480 1 10/23/2020 02:45 WG1563259
4-Nitrophenol U 15.0 480 1 10/23/2020 02:45 WG1563259
Pentachlorophenol U 12.9 480 1 10/23/2020 02:45 WG1563259
Phenol U 19.3 480 1 10/23/2020 02:45 WG1563259
2,4,6-Trichlorophenol U 15.4 480 1 10/23/2020 02:45 WG1563259
Acetophenone U 15.0 480 1 10/23/2020 02:45 WG1563259
1,2,4,5-Tetrachlorobenzene U 22.9 480 1 10/23/2020 02:45 WG1563259
2,4,5-Trichlorophenol U 16.3 480 1 10/23/2020 02:45 WG1563259
2,3,4,6-Tetrachlorophenol U 18.2 480 1 10/23/2020 02:45 WG1563259
(S) 2-Fluorophenol 63.6 12.0-120 10/23/2020 02:45 WG1563259
(S) Phenol-d5 57.3 10.0-120 10/23/2020 02:45 WG1563259
(S) Nitrobenzene-d5 47.1 10.0-122 10/23/2020 02:45 WG1563259
(S) 2-Fluorobiphenyl 56.9 15.0-120 10/23/2020 02:45 WG1563259
(S) 2,4,6-Tribromophenol 72.3 10.0-127 10/23/2020 02:45 WG1563259
(S) p-Terphenyl-d14 60.2 10.0-120 10/23/2020 02:45 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1274449
S-4
Collected date/time: 10/13/20 15:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.7 1 10/22/2020 15:48 WG1563415
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction U 969 4460 25 10/22/2020 07:12 WG1563292
(S)
a,a,a-Trifluorotoluene(FID)100 77.0-120 10/22/2020 07:12 WG1563292
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 64.6 88.5 1 10/22/2020 20:14 WG1563529
Acrylonitrile U 6.39 22.1 1 10/22/2020 20:14 WG1563529
Benzene 7.95 0.827 1.77 1 10/22/2020 20:14 WG1563529
Bromobenzene U 1.59 22.1 1 10/22/2020 20:14 WG1563529
Bromodichloromethane U 1.28 4.43 1 10/22/2020 20:14 WG1563529
Bromoform U 2.07 44.3 1 10/22/2020 20:14 WG1563529
Bromomethane U J0 J3 3.49 22.1 1 10/22/2020 20:14 WG1563529
n-Butylbenzene U 9.29 22.1 1 10/22/2020 20:14 WG1563529
sec-Butylbenzene U 5.10 22.1 1 10/22/2020 20:14 WG1563529
tert-Butylbenzene U 3.45 8.85 1 10/22/2020 20:14 WG1563529
Carbon tetrachloride U 1.59 8.85 1 10/22/2020 20:14 WG1563529
Chlorobenzene U 0.372 4.43 1 10/22/2020 20:14 WG1563529
Chlorodibromomethane U 1.08 4.43 1 10/22/2020 20:14 WG1563529
Chloroethane U 3.01 8.85 1 10/22/2020 20:14 WG1563529
Chloroform U 1.82 4.43 1 10/22/2020 20:14 WG1563529
Chloromethane U J0 7.70 22.1 1 10/22/2020 20:14 WG1563529
2-Chlorotoluene U 1.53 4.43 1 10/22/2020 20:14 WG1563529
4-Chlorotoluene U 0.797 8.85 1 10/22/2020 20:14 WG1563529
1,2-Dibromo-3-Chloropropane U 6.90 44.3 1 10/22/2020 20:14 WG1563529
1,2-Dibromoethane U 1.15 4.43 1 10/22/2020 20:14 WG1563529
Dibromomethane U 1.33 8.85 1 10/22/2020 20:14 WG1563529
1,2-Dichlorobenzene U J3 0.752 8.85 1 10/22/2020 20:14 WG1563529
1,3-Dichlorobenzene U 1.06 8.85 1 10/22/2020 20:14 WG1563529
1,4-Dichlorobenzene U 1.24 8.85 1 10/22/2020 20:14 WG1563529
Dichlorodifluoromethane U 2.85 4.43 1 10/22/2020 20:14 WG1563529
1,1-Dichloroethane U 0.869 4.43 1 10/22/2020 20:14 WG1563529
1,2-Dichloroethane U 1.15 4.43 1 10/22/2020 20:14 WG1563529
1,1-Dichloroethene U 1.07 4.43 1 10/22/2020 20:14 WG1563529
cis-1,2-Dichloroethene U 1.30 4.43 1 10/22/2020 20:14 WG1563529
trans-1,2-Dichloroethene U 1.84 8.85 1 10/22/2020 20:14 WG1563529
1,2-Dichloropropane U 2.51 8.85 1 10/22/2020 20:14 WG1563529
1,1-Dichloropropene U 1.43 4.43 1 10/22/2020 20:14 WG1563529
1,3-Dichloropropane U 0.887 8.85 1 10/22/2020 20:14 WG1563529
cis-1,3-Dichloropropene U 1.34 4.43 1 10/22/2020 20:14 WG1563529
trans-1,3-Dichloropropene U 2.02 8.85 1 10/22/2020 20:14 WG1563529
2,2-Dichloropropane U 2.44 4.43 1 10/22/2020 20:14 WG1563529
Di-isopropyl ether U 0.726 1.77 1 10/22/2020 20:14 WG1563529
Ethylbenzene 11.5 1.30 4.43 1 10/22/2020 20:14 WG1563529
Hexachloro-1,3-butadiene U 10.6 44.3 1 10/22/2020 20:14 WG1563529
Isopropylbenzene 1.14 J 0.752 4.43 1 10/22/2020 20:14 WG1563529
p-Isopropyltoluene U 4.51 8.85 1 10/22/2020 20:14 WG1563529
2-Butanone (MEK)U 112 177 1 10/22/2020 20:14 WG1563529
Methylene Chloride U 11.8 44.3 1 10/22/2020 20:14 WG1563529
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1274449
S-4
Collected date/time: 10/13/20 15:35
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 4.04 44.3 1 10/22/2020 20:14 WG1563529
Methyl tert-butyl ether U 0.620 1.77 1 10/22/2020 20:14 WG1563529
Naphthalene U J0 J3 8.64 22.1 1 10/22/2020 20:14 WG1563529
n-Propylbenzene 2.97 J 1.68 8.85 1 10/22/2020 20:14 WG1563529
Styrene 1.21 J 0.405 22.1 1 10/22/2020 20:14 WG1563529
1,1,1,2-Tetrachloroethane U 1.68 4.43 1 10/22/2020 20:14 WG1563529
1,1,2,2-Tetrachloroethane U 1.23 4.43 1 10/22/2020 20:14 WG1563529
Tetrachloroethene U 1.59 4.43 1 10/22/2020 20:14 WG1563529
Toluene 55.8 2.30 8.85 1 10/22/2020 20:14 WG1563529
1,2,3-Trichlorobenzene U C4 13.0 22.1 1 10/22/2020 20:14 WG1563529
1,2,4-Trichlorobenzene U 7.79 22.1 1 10/22/2020 20:14 WG1563529
1,1,1-Trichloroethane U 1.63 4.43 1 10/22/2020 20:14 WG1563529
1,1,2-Trichloroethane U 1.06 4.43 1 10/22/2020 20:14 WG1563529
Trichloroethene U 1.03 1.77 1 10/22/2020 20:14 WG1563529
Trichlorofluoromethane U 1.46 4.43 1 10/22/2020 20:14 WG1563529
1,2,3-Trichloropropane U 2.87 22.1 1 10/22/2020 20:14 WG1563529
1,2,4-Trimethylbenzene 16.4 2.80 8.85 1 10/22/2020 20:14 WG1563529
1,3,5-Trimethylbenzene 4.80 J 3.54 8.85 1 10/22/2020 20:14 WG1563529
Vinyl chloride U J0 J4 2.05 4.43 1 10/22/2020 20:14 WG1563529
Xylenes, Total 61.1 1.56 11.5 1 10/22/2020 20:14 WG1563529
(S) Toluene-d8 92.1 75.0-131 10/22/2020 20:14 WG1563529
(S) 4-Bromofluorobenzene 97.1 67.0-138 10/22/2020 20:14 WG1563529
(S) 1,2-Dichloroethane-d4 88.9 70.0-130 10/22/2020 20:14 WG1563529
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction 1350 J 1030 5350 1 10/23/2020 00:32 WG1563260
(S) o-Terphenyl 82.3 18.0-148 10/23/2020 00:32 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.21 44.6 1 10/23/2020 03:45 WG1563259
Acenaphthylene U 6.28 44.6 1 10/23/2020 03:45 WG1563259
Anthracene U 7.94 44.6 1 10/23/2020 03:45 WG1563259
Atrazine U 15.4 446 1 10/23/2020 03:45 WG1563259
Benzaldehyde U 23.7 446 1 10/23/2020 03:45 WG1563259
Benzo(a)anthracene U 7.85 44.6 1 10/23/2020 03:45 WG1563259
Benzo(b)fluoranthene U 8.31 44.6 1 10/23/2020 03:45 WG1563259
Benzo(k)fluoranthene U 7.92 44.6 1 10/23/2020 03:45 WG1563259
Benzo(g,h,i)perylene U 8.15 44.6 1 10/23/2020 03:45 WG1563259
Benzo(a)pyrene U 8.28 44.6 1 10/23/2020 03:45 WG1563259
Biphenyl U 14.2 446 1 10/23/2020 03:45 WG1563259
Bis(2-chlorethoxy)methane U 13.4 446 1 10/23/2020 03:45 WG1563259
Bis(2-chloroethyl)ether U 14.7 446 1 10/23/2020 03:45 WG1563259
2,2-Oxybis(1-Chloropropane)U 19.3 446 1 10/23/2020 03:45 WG1563259
4-Bromophenyl-phenylether U 15.7 446 1 10/23/2020 03:45 WG1563259
Caprolactam U 22.1 446 1 10/23/2020 03:45 WG1563259
Carbazole U 13.8 446 1 10/23/2020 03:45 WG1563259
2-Chloronaphthalene U 7.83 44.6 1 10/23/2020 03:45 WG1563259
4-Chlorophenyl-phenylether U 15.5 446 1 10/23/2020 03:45 WG1563259
Chrysene U 8.86 44.6 1 10/23/2020 03:45 WG1563259
Dibenz(a,h)anthracene U 12.4 44.6 1 10/23/2020 03:45 WG1563259
3,3-Dichlorobenzidine U 16.5 446 1 10/23/2020 03:45 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 14:56 16 of 74
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 17:45 16 of 74
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1274449
S-4
Collected date/time: 10/13/20 15:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 12.8 446 1 10/23/2020 03:45 WG1563259
2,6-Dinitrotoluene U 14.6 446 1 10/23/2020 03:45 WG1563259
Fluoranthene U 8.04 44.6 1 10/23/2020 03:45 WG1563259
Fluorene U 7.25 44.6 1 10/23/2020 03:45 WG1563259
Hexachlorobenzene U 15.8 446 1 10/23/2020 03:45 WG1563259
Hexachloro-1,3-butadiene U 15.0 446 1 10/23/2020 03:45 WG1563259
Hexachlorocyclopentadiene U 23.4 446 1 10/23/2020 03:45 WG1563259
Hexachloroethane U 17.5 446 1 10/23/2020 03:45 WG1563259
Indeno(1,2,3-cd)pyrene U 12.6 44.6 1 10/23/2020 03:45 WG1563259
Isophorone U 13.6 446 1 10/23/2020 03:45 WG1563259
Naphthalene U 11.2 44.6 1 10/23/2020 03:45 WG1563259
Nitrobenzene U 15.5 446 1 10/23/2020 03:45 WG1563259
n-Nitrosodiphenylamine U 33.7 446 1 10/23/2020 03:45 WG1563259
n-Nitrosodi-n-propylamine U 14.9 446 1 10/23/2020 03:45 WG1563259
Phenanthrene U 8.85 44.6 1 10/23/2020 03:45 WG1563259
Benzylbutyl phthalate U 13.9 446 1 10/23/2020 03:45 WG1563259
Bis(2-ethylhexyl)phthalate U 56.5 446 1 10/23/2020 03:45 WG1563259
Di-n-butyl phthalate U 15.3 446 1 10/23/2020 03:45 WG1563259
Diethyl phthalate U 14.7 446 1 10/23/2020 03:45 WG1563259
Dimethyl phthalate U 94.5 446 1 10/23/2020 03:45 WG1563259
Di-n-octyl phthalate U 30.1 446 1 10/23/2020 03:45 WG1563259
Pyrene U 8.67 44.6 1 10/23/2020 03:45 WG1563259
4-Chloroaniline U 16.1 446 1 10/23/2020 03:45 WG1563259
4-Chloro-3-methylphenol U 14.5 446 1 10/23/2020 03:45 WG1563259
2-Chlorophenol U 14.7 446 1 10/23/2020 03:45 WG1563259
Dibenzofuran U 14.6 446 1 10/23/2020 03:45 WG1563259
2,4-Dichlorophenol U 13.0 446 1 10/23/2020 03:45 WG1563259
2,4-Dimethylphenol U 11.6 446 1 10/23/2020 03:45 WG1563259
4,6-Dinitro-2-methylphenol U 101 446 1 10/23/2020 03:45 WG1563259
2,4-Dinitrophenol U 104 446 1 10/23/2020 03:45 WG1563259
2-Methylnaphthalene U 5.78 44.6 1 10/23/2020 03:45 WG1563259
2-Methylphenol U 13.4 446 1 10/23/2020 03:45 WG1563259
3&4-Methyl Phenol U 13.9 446 1 10/23/2020 03:45 WG1563259
2-Nitroaniline U 14.3 446 1 10/23/2020 03:45 WG1563259
3-Nitroaniline U 14.2 446 1 10/23/2020 03:45 WG1563259
4-Nitroaniline U 13.0 446 1 10/23/2020 03:45 WG1563259
2-Nitrophenol U 15.9 446 1 10/23/2020 03:45 WG1563259
4-Nitrophenol U 13.9 446 1 10/23/2020 03:45 WG1563259
Pentachlorophenol U 12.0 446 1 10/23/2020 03:45 WG1563259
Phenol U 17.9 446 1 10/23/2020 03:45 WG1563259
2,4,6-Trichlorophenol U 14.3 446 1 10/23/2020 03:45 WG1563259
Acetophenone U 13.9 446 1 10/23/2020 03:45 WG1563259
1,2,4,5-Tetrachlorobenzene U 21.3 446 1 10/23/2020 03:45 WG1563259
2,4,5-Trichlorophenol U 15.1 446 1 10/23/2020 03:45 WG1563259
2,3,4,6-Tetrachlorophenol U 16.9 446 1 10/23/2020 03:45 WG1563259
(S) 2-Fluorophenol 74.7 12.0-120 10/23/2020 03:45 WG1563259
(S) Phenol-d5 69.4 10.0-120 10/23/2020 03:45 WG1563259
(S) Nitrobenzene-d5 60.6 10.0-122 10/23/2020 03:45 WG1563259
(S) 2-Fluorobiphenyl 68.1 15.0-120 10/23/2020 03:45 WG1563259
(S) 2,4,6-Tribromophenol 85.2 10.0-127 10/23/2020 03:45 WG1563259
(S) p-Terphenyl-d14 72.5 10.0-120 10/23/2020 03:45 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1274449
S-5
Collected date/time: 10/13/20 15:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 66.9 1 10/22/2020 15:48 WG1563415
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction 12300 1240 5700 25 10/22/2020 07:35 WG1563292
(S)
a,a,a-Trifluorotoluene(FID)100 77.0-120 10/22/2020 07:35 WG1563292
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 74.6 102 1 10/22/2020 20:33 WG1563529
Acrylonitrile U 7.37 25.5 1 10/22/2020 20:33 WG1563529
Benzene 8.13 0.954 2.04 1 10/22/2020 20:33 WG1563529
Bromobenzene U 1.84 25.5 1 10/22/2020 20:33 WG1563529
Bromodichloromethane U 1.48 5.11 1 10/22/2020 20:33 WG1563529
Bromoform U 2.39 51.1 1 10/22/2020 20:33 WG1563529
Bromomethane U J0 J3 4.02 25.5 1 10/22/2020 20:33 WG1563529
n-Butylbenzene U 10.7 25.5 1 10/22/2020 20:33 WG1563529
sec-Butylbenzene 16.4 J 5.88 25.5 1 10/22/2020 20:33 WG1563529
tert-Butylbenzene U 3.98 10.2 1 10/22/2020 20:33 WG1563529
Carbon tetrachloride U 1.83 10.2 1 10/22/2020 20:33 WG1563529
Chlorobenzene U 0.429 5.11 1 10/22/2020 20:33 WG1563529
Chlorodibromomethane U 1.25 5.11 1 10/22/2020 20:33 WG1563529
Chloroethane U 3.47 10.2 1 10/22/2020 20:33 WG1563529
Chloroform U 2.10 5.11 1 10/22/2020 20:33 WG1563529
Chloromethane U J0 8.89 25.5 1 10/22/2020 20:33 WG1563529
2-Chlorotoluene U 1.77 5.11 1 10/22/2020 20:33 WG1563529
4-Chlorotoluene U 0.919 10.2 1 10/22/2020 20:33 WG1563529
1,2-Dibromo-3-Chloropropane U 7.97 51.1 1 10/22/2020 20:33 WG1563529
1,2-Dibromoethane U 1.32 5.11 1 10/22/2020 20:33 WG1563529
Dibromomethane U 1.53 10.2 1 10/22/2020 20:33 WG1563529
1,2-Dichlorobenzene U J3 0.868 10.2 1 10/22/2020 20:33 WG1563529
1,3-Dichlorobenzene U 1.23 10.2 1 10/22/2020 20:33 WG1563529
1,4-Dichlorobenzene U 1.43 10.2 1 10/22/2020 20:33 WG1563529
Dichlorodifluoromethane U 3.29 5.11 1 10/22/2020 20:33 WG1563529
1,1-Dichloroethane U 1.00 5.11 1 10/22/2020 20:33 WG1563529
1,2-Dichloroethane U 1.33 5.11 1 10/22/2020 20:33 WG1563529
1,1-Dichloroethene U 1.24 5.11 1 10/22/2020 20:33 WG1563529
cis-1,2-Dichloroethene U 1.50 5.11 1 10/22/2020 20:33 WG1563529
trans-1,2-Dichloroethene U 2.12 10.2 1 10/22/2020 20:33 WG1563529
1,2-Dichloropropane U 2.90 10.2 1 10/22/2020 20:33 WG1563529
1,1-Dichloropropene U 1.65 5.11 1 10/22/2020 20:33 WG1563529
1,3-Dichloropropane U 1.02 10.2 1 10/22/2020 20:33 WG1563529
cis-1,3-Dichloropropene U 1.55 5.11 1 10/22/2020 20:33 WG1563529
trans-1,3-Dichloropropene U 2.33 10.2 1 10/22/2020 20:33 WG1563529
2,2-Dichloropropane U 2.82 5.11 1 10/22/2020 20:33 WG1563529
Di-isopropyl ether U 0.837 2.04 1 10/22/2020 20:33 WG1563529
Ethylbenzene 10.4 1.51 5.11 1 10/22/2020 20:33 WG1563529
Hexachloro-1,3-butadiene U 12.3 51.1 1 10/22/2020 20:33 WG1563529
Isopropylbenzene 1.72 J 0.868 5.11 1 10/22/2020 20:33 WG1563529
p-Isopropyltoluene U 5.21 10.2 1 10/22/2020 20:33 WG1563529
2-Butanone (MEK)U 130 204 1 10/22/2020 20:33 WG1563529
Methylene Chloride U 13.6 51.1 1 10/22/2020 20:33 WG1563529
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1274449
S-5
Collected date/time: 10/13/20 15:40
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 4.66 51.1 1 10/22/2020 20:33 WG1563529
Methyl tert-butyl ether U 0.715 2.04 1 10/22/2020 20:33 WG1563529
Naphthalene U J0 J3 9.97 25.5 1 10/22/2020 20:33 WG1563529
n-Propylbenzene 3.43 J 1.94 10.2 1 10/22/2020 20:33 WG1563529
Styrene 1.35 J 0.468 25.5 1 10/22/2020 20:33 WG1563529
1,1,1,2-Tetrachloroethane U 1.94 5.11 1 10/22/2020 20:33 WG1563529
1,1,2,2-Tetrachloroethane U 1.42 5.11 1 10/22/2020 20:33 WG1563529
Tetrachloroethene U 1.83 5.11 1 10/22/2020 20:33 WG1563529
Toluene 72.7 2.66 10.2 1 10/22/2020 20:33 WG1563529
1,2,3-Trichlorobenzene U C4 15.0 25.5 1 10/22/2020 20:33 WG1563529
1,2,4-Trichlorobenzene U 8.99 25.5 1 10/22/2020 20:33 WG1563529
1,1,1-Trichloroethane U 1.89 5.11 1 10/22/2020 20:33 WG1563529
1,1,2-Trichloroethane U 1.22 5.11 1 10/22/2020 20:33 WG1563529
Trichloroethene U 1.19 2.04 1 10/22/2020 20:33 WG1563529
Trichlorofluoromethane U 1.69 5.11 1 10/22/2020 20:33 WG1563529
1,2,3-Trichloropropane U 3.31 25.5 1 10/22/2020 20:33 WG1563529
1,2,4-Trimethylbenzene 14.2 3.23 10.2 1 10/22/2020 20:33 WG1563529
1,3,5-Trimethylbenzene 4.60 J 4.09 10.2 1 10/22/2020 20:33 WG1563529
Vinyl chloride U J0 J4 2.37 5.11 1 10/22/2020 20:33 WG1563529
Xylenes, Total 58.4 1.80 13.3 1 10/22/2020 20:33 WG1563529
(S) Toluene-d8 111 75.0-131 10/22/2020 20:33 WG1563529
(S) 4-Bromofluorobenzene 96.5 67.0-138 10/22/2020 20:33 WG1563529
(S) 1,2-Dichloroethane-d4 92.5 70.0-130 10/22/2020 20:33 WG1563529
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction 141000 1150 5980 1 10/23/2020 03:57 WG1563260
(S) o-Terphenyl 90.8 18.0-148 10/23/2020 03:57 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 8.06 49.8 1 10/23/2020 04:26 WG1563259
Acenaphthylene U 7.01 49.8 1 10/23/2020 04:26 WG1563259
Anthracene U 8.87 49.8 1 10/23/2020 04:26 WG1563259
Atrazine U 17.2 498 1 10/23/2020 04:26 WG1563259
Benzaldehyde U 26.5 498 1 10/23/2020 04:26 WG1563259
Benzo(a)anthracene U 8.78 49.8 1 10/23/2020 04:26 WG1563259
Benzo(b)fluoranthene U 9.29 49.8 1 10/23/2020 04:26 WG1563259
Benzo(k)fluoranthene U 8.85 49.8 1 10/23/2020 04:26 WG1563259
Benzo(g,h,i)perylene U 9.11 49.8 1 10/23/2020 04:26 WG1563259
Benzo(a)pyrene U 9.26 49.8 1 10/23/2020 04:26 WG1563259
Biphenyl U 15.9 498 1 10/23/2020 04:26 WG1563259
Bis(2-chlorethoxy)methane U 15.0 498 1 10/23/2020 04:26 WG1563259
Bis(2-chloroethyl)ether U 16.5 498 1 10/23/2020 04:26 WG1563259
2,2-Oxybis(1-Chloropropane)U 21.5 498 1 10/23/2020 04:26 WG1563259
4-Bromophenyl-phenylether U 17.5 498 1 10/23/2020 04:26 WG1563259
Caprolactam U 24.7 498 1 10/23/2020 04:26 WG1563259
Carbazole U 15.4 498 1 10/23/2020 04:26 WG1563259
2-Chloronaphthalene U 8.75 49.8 1 10/23/2020 04:26 WG1563259
4-Chlorophenyl-phenylether U 17.3 498 1 10/23/2020 04:26 WG1563259
Chrysene U 9.90 49.8 1 10/23/2020 04:26 WG1563259
Dibenz(a,h)anthracene U 13.8 49.8 1 10/23/2020 04:26 WG1563259
3,3-Dichlorobenzidine U 18.4 498 1 10/23/2020 04:26 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1274449
S-5
Collected date/time: 10/13/20 15:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 14.3 498 1 10/23/2020 04:26 WG1563259
2,6-Dinitrotoluene U 16.3 498 1 10/23/2020 04:26 WG1563259
Fluoranthene U 8.99 49.8 1 10/23/2020 04:26 WG1563259
Fluorene 18.5 J 8.11 49.8 1 10/23/2020 04:26 WG1563259
Hexachlorobenzene U 17.6 498 1 10/23/2020 04:26 WG1563259
Hexachloro-1,3-butadiene U 16.7 498 1 10/23/2020 04:26 WG1563259
Hexachlorocyclopentadiene U 26.2 498 1 10/23/2020 04:26 WG1563259
Hexachloroethane U 19.6 498 1 10/23/2020 04:26 WG1563259
Indeno(1,2,3-cd)pyrene U 14.1 49.8 1 10/23/2020 04:26 WG1563259
Isophorone U 15.3 498 1 10/23/2020 04:26 WG1563259
Naphthalene U 12.5 49.8 1 10/23/2020 04:26 WG1563259
Nitrobenzene U 17.3 498 1 10/23/2020 04:26 WG1563259
n-Nitrosodiphenylamine U 37.7 498 1 10/23/2020 04:26 WG1563259
n-Nitrosodi-n-propylamine U 16.6 498 1 10/23/2020 04:26 WG1563259
Phenanthrene U 9.89 49.8 1 10/23/2020 04:26 WG1563259
Benzylbutyl phthalate U 15.6 498 1 10/23/2020 04:26 WG1563259
Bis(2-ethylhexyl)phthalate U 63.1 498 1 10/23/2020 04:26 WG1563259
Di-n-butyl phthalate U 17.0 498 1 10/23/2020 04:26 WG1563259
Diethyl phthalate U 16.5 498 1 10/23/2020 04:26 WG1563259
Dimethyl phthalate U 106 498 1 10/23/2020 04:26 WG1563259
Di-n-octyl phthalate U 33.6 498 1 10/23/2020 04:26 WG1563259
Pyrene U 9.69 49.8 1 10/23/2020 04:26 WG1563259
4-Chloroaniline U 17.9 498 1 10/23/2020 04:26 WG1563259
4-Chloro-3-methylphenol U 16.2 498 1 10/23/2020 04:26 WG1563259
2-Chlorophenol U 16.5 498 1 10/23/2020 04:26 WG1563259
Dibenzofuran U 16.3 498 1 10/23/2020 04:26 WG1563259
2,4-Dichlorophenol U 14.5 498 1 10/23/2020 04:26 WG1563259
2,4-Dimethylphenol U 13.0 498 1 10/23/2020 04:26 WG1563259
4,6-Dinitro-2-methylphenol U 113 498 1 10/23/2020 04:26 WG1563259
2,4-Dinitrophenol U 117 498 1 10/23/2020 04:26 WG1563259
2-Methylnaphthalene 29.0 J 6.46 49.8 1 10/23/2020 04:26 WG1563259
2-Methylphenol U 15.0 498 1 10/23/2020 04:26 WG1563259
3&4-Methyl Phenol U 15.6 498 1 10/23/2020 04:26 WG1563259
2-Nitroaniline U 16.0 498 1 10/23/2020 04:26 WG1563259
3-Nitroaniline U 15.9 498 1 10/23/2020 04:26 WG1563259
4-Nitroaniline U 14.5 498 1 10/23/2020 04:26 WG1563259
2-Nitrophenol U 17.8 498 1 10/23/2020 04:26 WG1563259
4-Nitrophenol U 15.6 498 1 10/23/2020 04:26 WG1563259
Pentachlorophenol U 13.4 498 1 10/23/2020 04:26 WG1563259
Phenol U 20.0 498 1 10/23/2020 04:26 WG1563259
2,4,6-Trichlorophenol U 16.0 498 1 10/23/2020 04:26 WG1563259
Acetophenone U 15.6 498 1 10/23/2020 04:26 WG1563259
1,2,4,5-Tetrachlorobenzene U 23.8 498 1 10/23/2020 04:26 WG1563259
2,4,5-Trichlorophenol U 16.9 498 1 10/23/2020 04:26 WG1563259
2,3,4,6-Tetrachlorophenol U 18.8 498 1 10/23/2020 04:26 WG1563259
(S) 2-Fluorophenol 67.8 12.0-120 10/23/2020 04:26 WG1563259
(S) Phenol-d5 61.9 10.0-120 10/23/2020 04:26 WG1563259
(S) Nitrobenzene-d5 50.9 10.0-122 10/23/2020 04:26 WG1563259
(S) 2-Fluorobiphenyl 63.4 15.0-120 10/23/2020 04:26 WG1563259
(S) 2,4,6-Tribromophenol 77.7 10.0-127 10/23/2020 04:26 WG1563259
(S) p-Terphenyl-d14 64.7 10.0-120 10/23/2020 04:26 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 17:45 20 of 74
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1274449
S-6
Collected date/time: 10/13/20 15:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 70.6 1 10/22/2020 15:48 WG1563415
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction U 1010 4650 25.5 10/22/2020 07:57 WG1563292
(S)
a,a,a-Trifluorotoluene(FID)99.8 77.0-120 10/22/2020 07:57 WG1563292
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 67.9 93.0 1.02 10/23/2020 20:36 WG1564404
Acrylonitrile U 6.71 23.3 1.02 10/23/2020 20:36 WG1564404
Benzene 7.44 0.868 1.86 1.02 10/23/2020 20:36 WG1564404
Bromobenzene U J4 1.67 23.3 1.02 10/23/2020 20:36 WG1564404
Bromodichloromethane U 1.35 4.65 1.02 10/23/2020 20:36 WG1564404
Bromoform U 2.17 46.5 1.02 10/23/2020 20:36 WG1564404
Bromomethane U 3.81 24.2 1.07 10/27/2020 01:58 WG1565803
n-Butylbenzene U 9.76 23.3 1.02 10/23/2020 20:36 WG1564404
sec-Butylbenzene U 5.36 23.3 1.02 10/23/2020 20:36 WG1564404
tert-Butylbenzene U 3.63 9.30 1.02 10/23/2020 20:36 WG1564404
Carbon tetrachloride U 1.67 9.30 1.02 10/23/2020 20:36 WG1564404
Chlorobenzene U 0.390 4.65 1.02 10/23/2020 20:36 WG1564404
Chlorodibromomethane U 1.14 4.65 1.02 10/23/2020 20:36 WG1564404
Chloroethane U 3.29 9.66 1.07 10/27/2020 01:58 WG1565803
Chloroform U 1.92 4.65 1.02 10/23/2020 20:36 WG1564404
Chloromethane U 8.40 24.2 1.07 10/27/2020 01:58 WG1565803
2-Chlorotoluene U 1.61 4.65 1.02 10/23/2020 20:36 WG1564404
4-Chlorotoluene U 0.837 9.30 1.02 10/23/2020 20:36 WG1564404
1,2-Dibromo-3-Chloropropane U 7.26 46.5 1.02 10/23/2020 20:36 WG1564404
1,2-Dibromoethane U 1.21 4.65 1.02 10/23/2020 20:36 WG1564404
Dibromomethane U 1.40 9.30 1.02 10/23/2020 20:36 WG1564404
1,2-Dichlorobenzene U 0.790 9.30 1.02 10/23/2020 20:36 WG1564404
1,3-Dichlorobenzene U 1.12 9.30 1.02 10/23/2020 20:36 WG1564404
1,4-Dichlorobenzene U 1.30 9.30 1.02 10/23/2020 20:36 WG1564404
Dichlorodifluoromethane U 2.99 4.65 1.02 10/23/2020 20:36 WG1564404
1,1-Dichloroethane U 0.914 4.65 1.02 10/23/2020 20:36 WG1564404
1,2-Dichloroethane U 1.21 4.65 1.02 10/23/2020 20:36 WG1564404
1,1-Dichloroethene U 1.13 4.65 1.02 10/23/2020 20:36 WG1564404
cis-1,2-Dichloroethene U 1.37 4.65 1.02 10/23/2020 20:36 WG1564404
trans-1,2-Dichloroethene U 1.93 9.30 1.02 10/23/2020 20:36 WG1564404
1,2-Dichloropropane U 2.64 9.30 1.02 10/23/2020 20:36 WG1564404
1,1-Dichloropropene U 1.50 4.65 1.02 10/23/2020 20:36 WG1564404
1,3-Dichloropropane U 0.932 9.30 1.02 10/23/2020 20:36 WG1564404
cis-1,3-Dichloropropene U 1.41 4.65 1.02 10/23/2020 20:36 WG1564404
trans-1,3-Dichloropropene U 2.12 9.30 1.02 10/23/2020 20:36 WG1564404
2,2-Dichloropropane U 2.57 4.65 1.02 10/23/2020 20:36 WG1564404
Di-isopropyl ether U 0.762 1.86 1.02 10/23/2020 20:36 WG1564404
Ethylbenzene 9.81 1.37 4.65 1.02 10/23/2020 20:36 WG1564404
Hexachloro-1,3-butadiene U J4 11.2 46.5 1.02 10/23/2020 20:36 WG1564404
Isopropylbenzene 1.07 J 0.790 4.65 1.02 10/23/2020 20:36 WG1564404
p-Isopropyltoluene U 4.74 9.30 1.02 10/23/2020 20:36 WG1564404
2-Butanone (MEK)U 118 186 1.02 10/23/2020 20:36 WG1564404
Methylene Chloride U 12.3 46.5 1.02 10/23/2020 20:36 WG1564404
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1274449
S-6
Collected date/time: 10/13/20 15:45
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 4.25 46.5 1.02 10/23/2020 20:36 WG1564404
Methyl tert-butyl ether U 0.651 1.86 1.02 10/23/2020 20:36 WG1564404
Naphthalene U 9.08 23.3 1.02 10/23/2020 20:36 WG1564404
n-Propylbenzene 2.52 J 1.77 9.30 1.02 10/23/2020 20:36 WG1564404
Styrene 1.30 J 0.427 23.3 1.02 10/23/2020 20:36 WG1564404
1,1,1,2-Tetrachloroethane U 1.76 4.65 1.02 10/23/2020 20:36 WG1564404
1,1,2,2-Tetrachloroethane U 1.29 4.65 1.02 10/23/2020 20:36 WG1564404
Tetrachloroethene U 1.67 4.65 1.02 10/23/2020 20:36 WG1564404
Toluene 58.7 2.43 9.30 1.02 10/23/2020 20:36 WG1564404
1,2,3-Trichlorobenzene U J4 13.6 23.3 1.02 10/23/2020 20:36 WG1564404
1,2,4-Trichlorobenzene U J4 8.19 23.3 1.02 10/23/2020 20:36 WG1564404
1,1,1-Trichloroethane U 1.72 4.65 1.02 10/23/2020 20:36 WG1564404
1,1,2-Trichloroethane U 1.11 4.65 1.02 10/23/2020 20:36 WG1564404
Trichloroethene U 1.09 1.86 1.02 10/23/2020 20:36 WG1564404
Trichlorofluoromethane U 1.60 4.84 1.07 10/27/2020 01:58 WG1565803
1,2,3-Trichloropropane U 3.01 23.3 1.02 10/23/2020 20:36 WG1564404
1,2,4-Trimethylbenzene 21.7 3.05 9.66 1.07 10/27/2020 01:58 WG1565803
1,3,5-Trimethylbenzene 3.78 J 3.72 9.30 1.02 10/23/2020 20:36 WG1564404
Vinyl chloride U 2.24 4.84 1.07 10/27/2020 01:58 WG1565803
Xylenes, Total 55.8 1.64 12.1 1.02 10/23/2020 20:36 WG1564404
(S) Toluene-d8 119 75.0-131 10/23/2020 20:36 WG1564404
(S) Toluene-d8 114 75.0-131 10/27/2020 01:58 WG1565803
(S) 4-Bromofluorobenzene 106 67.0-138 10/23/2020 20:36 WG1564404
(S) 4-Bromofluorobenzene 93.9 67.0-138 10/27/2020 01:58 WG1565803
(S) 1,2-Dichloroethane-d4 95.0 70.0-130 10/23/2020 20:36 WG1564404
(S) 1,2-Dichloroethane-d4 90.8 70.0-130 10/27/2020 01:58 WG1565803
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction 1280 J 1090 5670 1 10/23/2020 04:10 WG1563260
(S) o-Terphenyl 87.6 18.0-148 10/23/2020 04:10 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.64 47.2 1 10/23/2020 02:24 WG1563259
Acenaphthylene U 6.64 47.2 1 10/23/2020 02:24 WG1563259
Anthracene U 8.40 47.2 1 10/23/2020 02:24 WG1563259
Atrazine U 16.3 472 1 10/23/2020 02:24 WG1563259
Benzaldehyde U 25.1 472 1 10/23/2020 02:24 WG1563259
Benzo(a)anthracene U 8.32 47.2 1 10/23/2020 02:24 WG1563259
Benzo(b)fluoranthene U 8.80 47.2 1 10/23/2020 02:24 WG1563259
Benzo(k)fluoranthene U 8.39 47.2 1 10/23/2020 02:24 WG1563259
Benzo(g,h,i)perylene U 8.63 47.2 1 10/23/2020 02:24 WG1563259
Benzo(a)pyrene U 8.77 47.2 1 10/23/2020 02:24 WG1563259
Biphenyl U 15.0 472 1 10/23/2020 02:24 WG1563259
Bis(2-chlorethoxy)methane U 14.2 472 1 10/23/2020 02:24 WG1563259
Bis(2-chloroethyl)ether U 15.6 472 1 10/23/2020 02:24 WG1563259
2,2-Oxybis(1-Chloropropane)U 20.4 472 1 10/23/2020 02:24 WG1563259
4-Bromophenyl-phenylether U 16.6 472 1 10/23/2020 02:24 WG1563259
Caprolactam U 23.4 472 1 10/23/2020 02:24 WG1563259
Carbazole U 14.6 472 1 10/23/2020 02:24 WG1563259
2-Chloronaphthalene U 8.29 47.2 1 10/23/2020 02:24 WG1563259
4-Chlorophenyl-phenylether U 16.4 472 1 10/23/2020 02:24 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1274449
S-6
Collected date/time: 10/13/20 15:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Chrysene U 9.38 47.2 1 10/23/2020 02:24 WG1563259
Dibenz(a,h)anthracene U 13.1 47.2 1 10/23/2020 02:24 WG1563259
3,3-Dichlorobenzidine U 17.4 472 1 10/23/2020 02:24 WG1563259
2,4-Dinitrotoluene U 13.5 472 1 10/23/2020 02:24 WG1563259
2,6-Dinitrotoluene U 15.4 472 1 10/23/2020 02:24 WG1563259
Fluoranthene U 8.51 47.2 1 10/23/2020 02:24 WG1563259
Fluorene U 7.68 47.2 1 10/23/2020 02:24 WG1563259
Hexachlorobenzene U 16.7 472 1 10/23/2020 02:24 WG1563259
Hexachloro-1,3-butadiene U 15.9 472 1 10/23/2020 02:24 WG1563259
Hexachlorocyclopentadiene U 24.8 472 1 10/23/2020 02:24 WG1563259
Hexachloroethane U 18.6 472 1 10/23/2020 02:24 WG1563259
Indeno(1,2,3-cd)pyrene U 13.3 47.2 1 10/23/2020 02:24 WG1563259
Isophorone U 14.4 472 1 10/23/2020 02:24 WG1563259
Naphthalene U 11.8 47.2 1 10/23/2020 02:24 WG1563259
Nitrobenzene U 16.4 472 1 10/23/2020 02:24 WG1563259
n-Nitrosodiphenylamine U 35.7 472 1 10/23/2020 02:24 WG1563259
n-Nitrosodi-n-propylamine U 15.7 472 1 10/23/2020 02:24 WG1563259
Phenanthrene U 9.36 47.2 1 10/23/2020 02:24 WG1563259
Benzylbutyl phthalate U 14.7 472 1 10/23/2020 02:24 WG1563259
Bis(2-ethylhexyl)phthalate U 59.8 472 1 10/23/2020 02:24 WG1563259
Di-n-butyl phthalate U 16.1 472 1 10/23/2020 02:24 WG1563259
Diethyl phthalate U 15.6 472 1 10/23/2020 02:24 WG1563259
Dimethyl phthalate U 100 472 1 10/23/2020 02:24 WG1563259
Di-n-octyl phthalate U 31.9 472 1 10/23/2020 02:24 WG1563259
Pyrene U 9.18 47.2 1 10/23/2020 02:24 WG1563259
4-Chloroaniline U 17.0 472 1 10/23/2020 02:24 WG1563259
4-Chloro-3-methylphenol U 15.3 472 1 10/23/2020 02:24 WG1563259
2-Chlorophenol U 15.6 472 1 10/23/2020 02:24 WG1563259
Dibenzofuran U 15.4 472 1 10/23/2020 02:24 WG1563259
2,4-Dichlorophenol U 13.7 472 1 10/23/2020 02:24 WG1563259
2,4-Dimethylphenol U 12.3 472 1 10/23/2020 02:24 WG1563259
4,6-Dinitro-2-methylphenol U 107 472 1 10/23/2020 02:24 WG1563259
2,4-Dinitrophenol U 110 472 1 10/23/2020 02:24 WG1563259
2-Methylnaphthalene U 6.12 47.2 1 10/23/2020 02:24 WG1563259
2-Methylphenol U 14.2 472 1 10/23/2020 02:24 WG1563259
3&4-Methyl Phenol U 14.7 472 1 10/23/2020 02:24 WG1563259
2-Nitroaniline U 15.2 472 1 10/23/2020 02:24 WG1563259
3-Nitroaniline U 15.0 472 1 10/23/2020 02:24 WG1563259
4-Nitroaniline U 13.8 472 1 10/23/2020 02:24 WG1563259
2-Nitrophenol U 16.9 472 1 10/23/2020 02:24 WG1563259
4-Nitrophenol U 14.7 472 1 10/23/2020 02:24 WG1563259
Pentachlorophenol U 12.7 472 1 10/23/2020 02:24 WG1563259
Phenol U 19.0 472 1 10/23/2020 02:24 WG1563259
2,4,6-Trichlorophenol U 15.2 472 1 10/23/2020 02:24 WG1563259
Acetophenone U 14.7 472 1 10/23/2020 02:24 WG1563259
1,2,4,5-Tetrachlorobenzene U 22.5 472 1 10/23/2020 02:24 WG1563259
2,4,5-Trichlorophenol U 16.0 472 1 10/23/2020 02:24 WG1563259
2,3,4,6-Tetrachlorophenol U 17.8 472 1 10/23/2020 02:24 WG1563259
(S) 2-Fluorophenol 68.0 12.0-120 10/23/2020 02:24 WG1563259
(S) Phenol-d5 61.8 10.0-120 10/23/2020 02:24 WG1563259
(S) Nitrobenzene-d5 54.3 10.0-122 10/23/2020 02:24 WG1563259
(S) 2-Fluorobiphenyl 62.4 15.0-120 10/23/2020 02:24 WG1563259
(S) 2,4,6-Tribromophenol 76.9 10.0-127 10/23/2020 02:24 WG1563259
(S) p-Terphenyl-d14 66.8 10.0-120 10/23/2020 02:24 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1274449
S-7
Collected date/time: 10/13/20 16:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.4 1 10/22/2020 12:43 WG1563417
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction 1900 J 981 4520 25 10/22/2020 08:19 WG1563292
(S)
a,a,a-Trifluorotoluene(FID)99.8 77.0-120 10/22/2020 08:19 WG1563292
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone 93.1 66.0 90.4 1 10/27/2020 02:36 WG1565803
Acrylonitrile U 6.52 22.6 1 10/27/2020 02:36 WG1565803
Benzene 7.57 0.844 1.81 1 10/27/2020 02:36 WG1565803
Bromobenzene U 1.63 22.6 1 10/27/2020 02:36 WG1565803
Bromodichloromethane U 1.31 4.52 1 10/27/2020 02:36 WG1565803
Bromoform U 2.11 45.2 1 10/27/2020 02:36 WG1565803
Bromomethane U 3.56 22.6 1 10/27/2020 02:36 WG1565803
n-Butylbenzene U 9.49 22.6 1 10/27/2020 02:36 WG1565803
sec-Butylbenzene 7.86 J 5.21 22.6 1 10/27/2020 02:36 WG1565803
tert-Butylbenzene U 3.52 9.04 1 10/27/2020 02:36 WG1565803
Carbon tetrachloride U 1.62 9.04 1 10/27/2020 02:36 WG1565803
Chlorobenzene U 0.380 4.52 1 10/27/2020 02:36 WG1565803
Chlorodibromomethane U 1.11 4.52 1 10/27/2020 02:36 WG1565803
Chloroethane U 3.07 9.04 1 10/27/2020 02:36 WG1565803
Chloroform U 1.86 4.52 1 10/27/2020 02:36 WG1565803
Chloromethane U 7.86 22.6 1 10/27/2020 02:36 WG1565803
2-Chlorotoluene U 1.56 4.52 1 10/27/2020 02:36 WG1565803
4-Chlorotoluene U 0.813 9.04 1 10/27/2020 02:36 WG1565803
1,2-Dibromo-3-Chloropropane U 7.05 45.2 1 10/27/2020 02:36 WG1565803
1,2-Dibromoethane U 1.17 4.52 1 10/27/2020 02:36 WG1565803
Dibromomethane U 1.36 9.04 1 10/27/2020 02:36 WG1565803
1,2-Dichlorobenzene U 0.768 9.04 1 10/27/2020 02:36 WG1565803
1,3-Dichlorobenzene U 1.08 9.04 1 10/27/2020 02:36 WG1565803
1,4-Dichlorobenzene U 1.27 9.04 1 10/27/2020 02:36 WG1565803
Dichlorodifluoromethane U 2.91 4.52 1 10/27/2020 02:36 WG1565803
1,1-Dichloroethane U 0.887 4.52 1 10/27/2020 02:36 WG1565803
1,2-Dichloroethane U 1.17 4.52 1 10/27/2020 02:36 WG1565803
1,1-Dichloroethene U 1.10 4.52 1 10/27/2020 02:36 WG1565803
cis-1,2-Dichloroethene U 1.33 4.52 1 10/27/2020 02:36 WG1565803
trans-1,2-Dichloroethene U 1.88 9.04 1 10/27/2020 02:36 WG1565803
1,2-Dichloropropane U 2.57 9.04 1 10/27/2020 02:36 WG1565803
1,1-Dichloropropene U 1.46 4.52 1 10/27/2020 02:36 WG1565803
1,3-Dichloropropane U 0.905 9.04 1 10/27/2020 02:36 WG1565803
cis-1,3-Dichloropropene U 1.37 4.52 1 10/27/2020 02:36 WG1565803
trans-1,3-Dichloropropene U 2.06 9.04 1 10/27/2020 02:36 WG1565803
2,2-Dichloropropane U 2.49 4.52 1 10/27/2020 02:36 WG1565803
Di-isopropyl ether U 0.741 1.81 1 10/27/2020 02:36 WG1565803
Ethylbenzene 8.13 1.33 4.52 1 10/27/2020 02:36 WG1565803
Hexachloro-1,3-butadiene U 10.8 45.2 1 10/27/2020 02:36 WG1565803
Isopropylbenzene 1.54 J 0.768 4.52 1 10/27/2020 02:36 WG1565803
p-Isopropyltoluene U 4.61 9.04 1 10/27/2020 02:36 WG1565803
2-Butanone (MEK)U 115 181 1 10/27/2020 02:36 WG1565803
Methylene Chloride U 12.0 45.2 1 10/27/2020 02:36 WG1565803
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1274449
S-7
Collected date/time: 10/13/20 16:05
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 4.12 45.2 1 10/27/2020 02:36 WG1565803
Methyl tert-butyl ether U 0.633 1.81 1 10/27/2020 02:36 WG1565803
Naphthalene 12.3 J 8.82 22.6 1 10/27/2020 02:36 WG1565803
n-Propylbenzene 4.83 J 1.72 9.04 1 10/27/2020 02:36 WG1565803
Styrene 0.732 J 0.414 22.6 1 10/27/2020 02:36 WG1565803
1,1,1,2-Tetrachloroethane U 1.71 4.52 1 10/27/2020 02:36 WG1565803
1,1,2,2-Tetrachloroethane U 1.26 4.52 1 10/27/2020 02:36 WG1565803
Tetrachloroethene U 1.62 4.52 1 10/27/2020 02:36 WG1565803
Toluene 58.2 2.35 9.04 1 10/27/2020 02:36 WG1565803
1,2,3-Trichlorobenzene U C4 13.2 22.6 1 10/27/2020 02:36 WG1565803
1,2,4-Trichlorobenzene U 7.95 22.6 1 10/27/2020 02:36 WG1565803
1,1,1-Trichloroethane U 1.67 4.52 1 10/27/2020 02:36 WG1565803
1,1,2-Trichloroethane U 1.08 4.52 1 10/27/2020 02:36 WG1565803
Trichloroethene 1.24 J 1.06 1.81 1 10/27/2020 02:36 WG1565803
Trichlorofluoromethane U 1.49 4.52 1 10/27/2020 02:36 WG1565803
1,2,3-Trichloropropane U 2.93 22.6 1 10/27/2020 02:36 WG1565803
1,2,4-Trimethylbenzene 13.0 2.86 9.04 1 10/27/2020 02:36 WG1565803
1,3,5-Trimethylbenzene 3.65 J 3.61 9.04 1 10/27/2020 02:36 WG1565803
Vinyl chloride U 2.10 4.52 1 10/27/2020 02:36 WG1565803
Xylenes, Total 44.3 1.59 11.7 1 10/27/2020 02:36 WG1565803
(S) Toluene-d8 113 75.0-131 10/27/2020 02:36 WG1565803
(S) 4-Bromofluorobenzene 98.6 67.0-138 10/27/2020 02:36 WG1565803
(S) 1,2-Dichloroethane-d4 93.1 70.0-130 10/27/2020 02:36 WG1565803
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction 24800 1050 5450 1 10/23/2020 04:23 WG1563260
(S) o-Terphenyl 89.8 18.0-148 10/23/2020 04:23 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.34 45.3 1 10/23/2020 04:46 WG1563259
Acenaphthylene U 6.39 45.3 1 10/23/2020 04:46 WG1563259
Anthracene U 8.08 45.3 1 10/23/2020 04:46 WG1563259
Atrazine U 15.7 453 1 10/23/2020 04:46 WG1563259
Benzaldehyde U 24.1 453 1 10/23/2020 04:46 WG1563259
Benzo(a)anthracene U 7.99 45.3 1 10/23/2020 04:46 WG1563259
Benzo(b)fluoranthene U 8.46 45.3 1 10/23/2020 04:46 WG1563259
Benzo(k)fluoranthene U 8.06 45.3 1 10/23/2020 04:46 WG1563259
Benzo(g,h,i)perylene U 8.29 45.3 1 10/23/2020 04:46 WG1563259
Benzo(a)pyrene U 8.43 45.3 1 10/23/2020 04:46 WG1563259
Biphenyl U 14.4 453 1 10/23/2020 04:46 WG1563259
Bis(2-chlorethoxy)methane U 13.6 453 1 10/23/2020 04:46 WG1563259
Bis(2-chloroethyl)ether U 15.0 453 1 10/23/2020 04:46 WG1563259
2,2-Oxybis(1-Chloropropane)U 19.6 453 1 10/23/2020 04:46 WG1563259
4-Bromophenyl-phenylether U 15.9 453 1 10/23/2020 04:46 WG1563259
Caprolactam U 22.5 453 1 10/23/2020 04:46 WG1563259
Carbazole U 14.0 453 1 10/23/2020 04:46 WG1563259
2-Chloronaphthalene U 7.97 45.3 1 10/23/2020 04:46 WG1563259
4-Chlorophenyl-phenylether U 15.8 453 1 10/23/2020 04:46 WG1563259
Chrysene U 9.01 45.3 1 10/23/2020 04:46 WG1563259
Dibenz(a,h)anthracene U 12.6 45.3 1 10/23/2020 04:46 WG1563259
3,3-Dichlorobenzidine U 16.7 453 1 10/23/2020 04:46 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 14:56 25 of 74
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 17:45 25 of 74
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1274449
S-7
Collected date/time: 10/13/20 16:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 13.0 453 1 10/23/2020 04:46 WG1563259
2,6-Dinitrotoluene U 14.8 453 1 10/23/2020 04:46 WG1563259
Fluoranthene U 8.18 45.3 1 10/23/2020 04:46 WG1563259
Fluorene U 7.38 45.3 1 10/23/2020 04:46 WG1563259
Hexachlorobenzene U 16.1 453 1 10/23/2020 04:46 WG1563259
Hexachloro-1,3-butadiene U 15.3 453 1 10/23/2020 04:46 WG1563259
Hexachlorocyclopentadiene U 23.8 453 1 10/23/2020 04:46 WG1563259
Hexachloroethane U 17.8 453 1 10/23/2020 04:46 WG1563259
Indeno(1,2,3-cd)pyrene U 12.8 45.3 1 10/23/2020 04:46 WG1563259
Isophorone U 13.9 453 1 10/23/2020 04:46 WG1563259
Naphthalene U 11.4 45.3 1 10/23/2020 04:46 WG1563259
Nitrobenzene U 15.8 453 1 10/23/2020 04:46 WG1563259
n-Nitrosodiphenylamine U 34.3 453 1 10/23/2020 04:46 WG1563259
n-Nitrosodi-n-propylamine U 15.1 453 1 10/23/2020 04:46 WG1563259
Phenanthrene U 9.00 45.3 1 10/23/2020 04:46 WG1563259
Benzylbutyl phthalate U 14.2 453 1 10/23/2020 04:46 WG1563259
Bis(2-ethylhexyl)phthalate U 57.5 453 1 10/23/2020 04:46 WG1563259
Di-n-butyl phthalate U 15.5 453 1 10/23/2020 04:46 WG1563259
Diethyl phthalate U 15.0 453 1 10/23/2020 04:46 WG1563259
Dimethyl phthalate U 96.1 453 1 10/23/2020 04:46 WG1563259
Di-n-octyl phthalate U 30.6 453 1 10/23/2020 04:46 WG1563259
Pyrene U 8.82 45.3 1 10/23/2020 04:46 WG1563259
4-Chloroaniline U 16.3 453 1 10/23/2020 04:46 WG1563259
4-Chloro-3-methylphenol U 14.7 453 1 10/23/2020 04:46 WG1563259
2-Chlorophenol U 15.0 453 1 10/23/2020 04:46 WG1563259
Dibenzofuran U 14.8 453 1 10/23/2020 04:46 WG1563259
2,4-Dichlorophenol U 13.2 453 1 10/23/2020 04:46 WG1563259
2,4-Dimethylphenol U 11.8 453 1 10/23/2020 04:46 WG1563259
4,6-Dinitro-2-methylphenol U 103 453 1 10/23/2020 04:46 WG1563259
2,4-Dinitrophenol U 106 453 1 10/23/2020 04:46 WG1563259
2-Methylnaphthalene 7.53 J 5.88 45.3 1 10/23/2020 04:46 WG1563259
2-Methylphenol U 13.6 453 1 10/23/2020 04:46 WG1563259
3&4-Methyl Phenol U 14.2 453 1 10/23/2020 04:46 WG1563259
2-Nitroaniline U 14.6 453 1 10/23/2020 04:46 WG1563259
3-Nitroaniline U 14.4 453 1 10/23/2020 04:46 WG1563259
4-Nitroaniline U 13.2 453 1 10/23/2020 04:46 WG1563259
2-Nitrophenol U 16.2 453 1 10/23/2020 04:46 WG1563259
4-Nitrophenol U 14.2 453 1 10/23/2020 04:46 WG1563259
Pentachlorophenol U 12.2 453 1 10/23/2020 04:46 WG1563259
Phenol U 18.2 453 1 10/23/2020 04:46 WG1563259
2,4,6-Trichlorophenol U 14.6 453 1 10/23/2020 04:46 WG1563259
Acetophenone U 14.2 453 1 10/23/2020 04:46 WG1563259
1,2,4,5-Tetrachlorobenzene U 21.7 453 1 10/23/2020 04:46 WG1563259
2,4,5-Trichlorophenol U 15.4 453 1 10/23/2020 04:46 WG1563259
2,3,4,6-Tetrachlorophenol U 17.2 453 1 10/23/2020 04:46 WG1563259
(S) 2-Fluorophenol 73.0 12.0-120 10/23/2020 04:46 WG1563259
(S) Phenol-d5 68.3 10.0-120 10/23/2020 04:46 WG1563259
(S) Nitrobenzene-d5 54.3 10.0-122 10/23/2020 04:46 WG1563259
(S) 2-Fluorobiphenyl 67.8 15.0-120 10/23/2020 04:46 WG1563259
(S) 2,4,6-Tribromophenol 93.9 10.0-127 10/23/2020 04:46 WG1563259
(S) p-Terphenyl-d14 71.2 10.0-120 10/23/2020 04:46 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1274449
S-8
Collected date/time: 10/13/20 16:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.9 1 10/22/2020 12:43 WG1563417
Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) Low Fraction 2320 B J J3 916 4220 25.3 10/22/2020 20:16 WG1563287
(S)
a,a,a-Trifluorotoluene(FID)111 77.0-120 10/22/2020 20:16 WG1563287
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone 135 61.6 84.3 1.01 10/27/2020 02:17 WG1565803
Acrylonitrile U 6.09 21.0 1.01 10/27/2020 02:17 WG1565803
Benzene 7.88 0.788 1.69 1.01 10/27/2020 02:17 WG1565803
Bromobenzene U 1.52 21.0 1.01 10/27/2020 02:17 WG1565803
Bromodichloromethane U 1.22 4.22 1.01 10/27/2020 02:17 WG1565803
Bromoform U 1.97 42.2 1.01 10/27/2020 02:17 WG1565803
Bromomethane U 3.32 21.0 1.01 10/27/2020 02:17 WG1565803
n-Butylbenzene 11.3 J 8.85 21.0 1.01 10/27/2020 02:17 WG1565803
sec-Butylbenzene 25.4 4.86 21.0 1.01 10/27/2020 02:17 WG1565803
tert-Butylbenzene U 3.29 8.43 1.01 10/27/2020 02:17 WG1565803
Carbon tetrachloride U 1.51 8.43 1.01 10/27/2020 02:17 WG1565803
Chlorobenzene U 0.354 4.22 1.01 10/27/2020 02:17 WG1565803
Chlorodibromomethane U 1.03 4.22 1.01 10/27/2020 02:17 WG1565803
Chloroethane U 2.87 8.43 1.01 10/27/2020 02:17 WG1565803
Chloroform U 1.74 4.22 1.01 10/27/2020 02:17 WG1565803
Chloromethane U 7.33 21.0 1.01 10/27/2020 02:17 WG1565803
2-Chlorotoluene U 1.46 4.22 1.01 10/27/2020 02:17 WG1565803
4-Chlorotoluene U 0.759 8.43 1.01 10/27/2020 02:17 WG1565803
1,2-Dibromo-3-Chloropropane U 6.58 42.2 1.01 10/27/2020 02:17 WG1565803
1,2-Dibromoethane U 1.09 4.22 1.01 10/27/2020 02:17 WG1565803
Dibromomethane U 1.26 8.43 1.01 10/27/2020 02:17 WG1565803
1,2-Dichlorobenzene U 0.716 8.43 1.01 10/27/2020 02:17 WG1565803
1,3-Dichlorobenzene U 1.01 8.43 1.01 10/27/2020 02:17 WG1565803
1,4-Dichlorobenzene U 1.18 8.43 1.01 10/27/2020 02:17 WG1565803
Dichlorodifluoromethane U 2.72 4.22 1.01 10/27/2020 02:17 WG1565803
1,1-Dichloroethane U 0.828 4.22 1.01 10/27/2020 02:17 WG1565803
1,2-Dichloroethane U 1.09 4.22 1.01 10/27/2020 02:17 WG1565803
1,1-Dichloroethene U 1.02 4.22 1.01 10/27/2020 02:17 WG1565803
cis-1,2-Dichloroethene U 1.24 4.22 1.01 10/27/2020 02:17 WG1565803
trans-1,2-Dichloroethene U 1.75 8.43 1.01 10/27/2020 02:17 WG1565803
1,2-Dichloropropane U 2.39 8.43 1.01 10/27/2020 02:17 WG1565803
1,1-Dichloropropene U 1.36 4.22 1.01 10/27/2020 02:17 WG1565803
1,3-Dichloropropane U 0.844 8.43 1.01 10/27/2020 02:17 WG1565803
cis-1,3-Dichloropropene U 1.28 4.22 1.01 10/27/2020 02:17 WG1565803
trans-1,3-Dichloropropene U 1.92 8.43 1.01 10/27/2020 02:17 WG1565803
2,2-Dichloropropane U 2.32 4.22 1.01 10/27/2020 02:17 WG1565803
Di-isopropyl ether U 0.691 1.69 1.01 10/27/2020 02:17 WG1565803
Ethylbenzene 8.85 1.24 4.22 1.01 10/27/2020 02:17 WG1565803
Hexachloro-1,3-butadiene U 10.1 42.2 1.01 10/27/2020 02:17 WG1565803
Isopropylbenzene 2.32 J 0.716 4.22 1.01 10/27/2020 02:17 WG1565803
p-Isopropyltoluene U 4.31 8.43 1.01 10/27/2020 02:17 WG1565803
2-Butanone (MEK)U 107 169 1.01 10/27/2020 02:17 WG1565803
Methylene Chloride U 11.2 42.2 1.01 10/27/2020 02:17 WG1565803
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1274449
S-8
Collected date/time: 10/13/20 16:25
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
4-Methyl-2-pentanone (MIBK)U 3.84 42.2 1.01 10/27/2020 02:17 WG1565803
Methyl tert-butyl ether U 0.589 1.69 1.01 10/27/2020 02:17 WG1565803
Naphthalene 20.2 J 8.23 21.0 1.01 10/27/2020 02:17 WG1565803
n-Propylbenzene 5.01 J 1.60 8.43 1.01 10/27/2020 02:17 WG1565803
Styrene 0.928 J 0.386 21.0 1.01 10/27/2020 02:17 WG1565803
1,1,1,2-Tetrachloroethane U 1.60 4.22 1.01 10/27/2020 02:17 WG1565803
1,1,2,2-Tetrachloroethane U 1.17 4.22 1.01 10/27/2020 02:17 WG1565803
Tetrachloroethene U 1.51 4.22 1.01 10/27/2020 02:17 WG1565803
Toluene 60.7 2.19 8.43 1.01 10/27/2020 02:17 WG1565803
1,2,3-Trichlorobenzene U C4 12.3 21.0 1.01 10/27/2020 02:17 WG1565803
1,2,4-Trichlorobenzene U 7.41 21.0 1.01 10/27/2020 02:17 WG1565803
1,1,1-Trichloroethane U 1.56 4.22 1.01 10/27/2020 02:17 WG1565803
1,1,2-Trichloroethane U 1.01 4.22 1.01 10/27/2020 02:17 WG1565803
Trichloroethene U 0.985 1.69 1.01 10/27/2020 02:17 WG1565803
Trichlorofluoromethane U 1.39 4.22 1.01 10/27/2020 02:17 WG1565803
1,2,3-Trichloropropane U 2.74 21.0 1.01 10/27/2020 02:17 WG1565803
1,2,4-Trimethylbenzene 15.0 2.67 8.43 1.01 10/27/2020 02:17 WG1565803
1,3,5-Trimethylbenzene 4.84 J 3.37 8.43 1.01 10/27/2020 02:17 WG1565803
Vinyl chloride U 1.95 4.22 1.01 10/27/2020 02:17 WG1565803
Xylenes, Total 47.1 1.48 10.9 1.01 10/27/2020 02:17 WG1565803
(S) Toluene-d8 113 75.0-131 10/27/2020 02:17 WG1565803
(S) 4-Bromofluorobenzene 96.9 67.0-138 10/27/2020 02:17 WG1565803
(S) 1,2-Dichloroethane-d4 90.4 70.0-130 10/27/2020 02:17 WG1565803
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
TPH (GC/FID) High Fraction 11100 1030 5340 1 10/23/2020 04:50 WG1563260
(S) o-Terphenyl 86.7 18.0-148 10/23/2020 04:50 WG1563260
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acenaphthene U 7.20 44.5 1 10/23/2020 06:07 WG1563259
Acenaphthylene U 6.26 44.5 1 10/23/2020 06:07 WG1563259
Anthracene U 7.92 44.5 1 10/23/2020 06:07 WG1563259
Atrazine U 15.4 445 1 10/23/2020 06:07 WG1563259
Benzaldehyde U 23.6 445 1 10/23/2020 06:07 WG1563259
Benzo(a)anthracene U 7.84 44.5 1 10/23/2020 06:07 WG1563259
Benzo(b)fluoranthene U 8.29 44.5 1 10/23/2020 06:07 WG1563259
Benzo(k)fluoranthene U 7.91 44.5 1 10/23/2020 06:07 WG1563259
Benzo(g,h,i)perylene U 8.13 44.5 1 10/23/2020 06:07 WG1563259
Benzo(a)pyrene U 8.27 44.5 1 10/23/2020 06:07 WG1563259
Biphenyl U 14.2 445 1 10/23/2020 06:07 WG1563259
Bis(2-chlorethoxy)methane U 13.4 445 1 10/23/2020 06:07 WG1563259
Bis(2-chloroethyl)ether U 14.7 445 1 10/23/2020 06:07 WG1563259
2,2-Oxybis(1-Chloropropane)U 19.2 445 1 10/23/2020 06:07 WG1563259
4-Bromophenyl-phenylether U 15.6 445 1 10/23/2020 06:07 WG1563259
Caprolactam U 22.0 445 1 10/23/2020 06:07 WG1563259
Carbazole U 13.8 445 1 10/23/2020 06:07 WG1563259
2-Chloronaphthalene U 7.81 44.5 1 10/23/2020 06:07 WG1563259
4-Chlorophenyl-phenylether U 15.5 445 1 10/23/2020 06:07 WG1563259
Chrysene U 8.84 44.5 1 10/23/2020 06:07 WG1563259
Dibenz(a,h)anthracene U 12.3 44.5 1 10/23/2020 06:07 WG1563259
3,3-Dichlorobenzidine U 16.4 445 1 10/23/2020 06:07 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1274449
S-8
Collected date/time: 10/13/20 16:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
2,4-Dinitrotoluene U 12.8 445 1 10/23/2020 06:07 WG1563259
2,6-Dinitrotoluene U 14.6 445 1 10/23/2020 06:07 WG1563259
Fluoranthene U 8.03 44.5 1 10/23/2020 06:07 WG1563259
Fluorene U 7.24 44.5 1 10/23/2020 06:07 WG1563259
Hexachlorobenzene U 15.8 445 1 10/23/2020 06:07 WG1563259
Hexachloro-1,3-butadiene U 15.0 445 1 10/23/2020 06:07 WG1563259
Hexachlorocyclopentadiene U 23.4 445 1 10/23/2020 06:07 WG1563259
Hexachloroethane U 17.5 445 1 10/23/2020 06:07 WG1563259
Indeno(1,2,3-cd)pyrene U 12.6 44.5 1 10/23/2020 06:07 WG1563259
Isophorone U 13.6 445 1 10/23/2020 06:07 WG1563259
Naphthalene U 11.2 44.5 1 10/23/2020 06:07 WG1563259
Nitrobenzene U 15.5 445 1 10/23/2020 06:07 WG1563259
n-Nitrosodiphenylamine U 33.7 445 1 10/23/2020 06:07 WG1563259
n-Nitrosodi-n-propylamine U 14.8 445 1 10/23/2020 06:07 WG1563259
Phenanthrene U 8.83 44.5 1 10/23/2020 06:07 WG1563259
Benzylbutyl phthalate U 13.9 445 1 10/23/2020 06:07 WG1563259
Bis(2-ethylhexyl)phthalate U 56.4 445 1 10/23/2020 06:07 WG1563259
Di-n-butyl phthalate U 15.2 445 1 10/23/2020 06:07 WG1563259
Diethyl phthalate U 14.7 445 1 10/23/2020 06:07 WG1563259
Dimethyl phthalate U 94.3 445 1 10/23/2020 06:07 WG1563259
Di-n-octyl phthalate U 30.0 445 1 10/23/2020 06:07 WG1563259
Pyrene U 8.65 44.5 1 10/23/2020 06:07 WG1563259
4-Chloroaniline U 16.0 445 1 10/23/2020 06:07 WG1563259
4-Chloro-3-methylphenol U 14.4 445 1 10/23/2020 06:07 WG1563259
2-Chlorophenol U 14.7 445 1 10/23/2020 06:07 WG1563259
Dibenzofuran U 14.6 445 1 10/23/2020 06:07 WG1563259
2,4-Dichlorophenol U 13.0 445 1 10/23/2020 06:07 WG1563259
2,4-Dimethylphenol U 11.6 445 1 10/23/2020 06:07 WG1563259
4,6-Dinitro-2-methylphenol U 101 445 1 10/23/2020 06:07 WG1563259
2,4-Dinitrophenol U 104 445 1 10/23/2020 06:07 WG1563259
2-Methylnaphthalene 26.4 J 5.77 44.5 1 10/23/2020 06:07 WG1563259
2-Methylphenol U 13.4 445 1 10/23/2020 06:07 WG1563259
3&4-Methyl Phenol U 13.9 445 1 10/23/2020 06:07 WG1563259
2-Nitroaniline U 14.3 445 1 10/23/2020 06:07 WG1563259
3-Nitroaniline U 14.2 445 1 10/23/2020 06:07 WG1563259
4-Nitroaniline U 13.0 445 1 10/23/2020 06:07 WG1563259
2-Nitrophenol U 15.9 445 1 10/23/2020 06:07 WG1563259
4-Nitrophenol U 13.9 445 1 10/23/2020 06:07 WG1563259
Pentachlorophenol U 12.0 445 1 10/23/2020 06:07 WG1563259
Phenol U 17.9 445 1 10/23/2020 06:07 WG1563259
2,4,6-Trichlorophenol U 14.3 445 1 10/23/2020 06:07 WG1563259
Acetophenone U 13.9 445 1 10/23/2020 06:07 WG1563259
1,2,4,5-Tetrachlorobenzene U 21.2 445 1 10/23/2020 06:07 WG1563259
2,4,5-Trichlorophenol U 15.1 445 1 10/23/2020 06:07 WG1563259
2,3,4,6-Tetrachlorophenol U 16.8 445 1 10/23/2020 06:07 WG1563259
(S) 2-Fluorophenol 70.8 12.0-120 10/23/2020 06:07 WG1563259
(S) Phenol-d5 66.8 10.0-120 10/23/2020 06:07 WG1563259
(S) Nitrobenzene-d5 56.4 10.0-122 10/23/2020 06:07 WG1563259
(S) 2-Fluorobiphenyl 64.9 15.0-120 10/23/2020 06:07 WG1563259
(S) 2,4,6-Tribromophenol 94.5 10.0-127 10/23/2020 06:07 WG1563259
(S) p-Terphenyl-d14 68.7 10.0-120 10/23/2020 06:07 WG1563259
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1274449
GW-1
Collected date/time: 10/13/20 16:30
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 10/22/2020 17:56 WG1563655
Unadjusted C9-C12 Aliphatics 85.9 J 33.3 100 1 10/22/2020 17:56 WG1563655
Unadjusted C9-C10 Aromatics 38.1 J 33.3 100 1 10/22/2020 17:56 WG1563655
Total VPH 124 33.3 100 1 10/22/2020 17:56 WG1563655
(S) 2,5-Dibromotoluene(FID)90.3 70.0-130 10/22/2020 17:56 WG1563655
(S) 2,5-Dibromotoluene(PID)95.7 70.0-130 10/22/2020 17:56 WG1563655
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U J4 11.3 50.0 1 10/26/2020 03:00 WG1565201
Acrolein U 2.54 50.0 1 10/26/2020 03:00 WG1565201
Acrylonitrile U 0.671 10.0 1 10/26/2020 03:00 WG1565201
Benzene U 0.0941 1.00 1 10/26/2020 03:00 WG1565201
Bromobenzene U 0.118 1.00 1 10/26/2020 03:00 WG1565201
Bromodichloromethane U 0.136 1.00 1 10/26/2020 03:00 WG1565201
Bromoform U 0.129 1.00 1 10/26/2020 03:00 WG1565201
Bromomethane U 0.605 5.00 1 10/26/2020 03:00 WG1565201
n-Butylbenzene U 0.157 1.00 1 10/26/2020 03:00 WG1565201
sec-Butylbenzene 0.459 J 0.125 1.00 1 10/26/2020 03:00 WG1565201
tert-Butylbenzene U 0.127 1.00 1 10/26/2020 03:00 WG1565201
Carbon tetrachloride U 0.128 1.00 1 10/26/2020 03:00 WG1565201
Chlorobenzene U 0.116 1.00 1 10/26/2020 03:00 WG1565201
Chlorodibromomethane U 0.140 1.00 1 10/26/2020 03:00 WG1565201
Chloroethane U 0.192 5.00 1 10/26/2020 03:00 WG1565201
Chloroform 0.310 J 0.111 5.00 1 10/26/2020 03:00 WG1565201
Chloromethane U 0.960 2.50 1 10/26/2020 03:00 WG1565201
2-Chlorotoluene U 0.106 1.00 1 10/26/2020 03:00 WG1565201
4-Chlorotoluene U 0.114 1.00 1 10/26/2020 03:00 WG1565201
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 10/26/2020 03:00 WG1565201
1,2-Dibromoethane U 0.126 1.00 1 10/26/2020 03:00 WG1565201
Dibromomethane U 0.122 1.00 1 10/26/2020 03:00 WG1565201
1,2-Dichlorobenzene U 0.107 1.00 1 10/26/2020 03:00 WG1565201
1,3-Dichlorobenzene U 0.110 1.00 1 10/26/2020 03:00 WG1565201
1,4-Dichlorobenzene U 0.120 1.00 1 10/26/2020 03:00 WG1565201
Dichlorodifluoromethane U 0.374 5.00 1 10/26/2020 03:00 WG1565201
1,1-Dichloroethane U 0.100 1.00 1 10/26/2020 03:00 WG1565201
1,2-Dichloroethane U 0.0819 1.00 1 10/26/2020 03:00 WG1565201
1,1-Dichloroethene U 0.188 1.00 1 10/26/2020 03:00 WG1565201
cis-1,2-Dichloroethene U 0.126 1.00 1 10/26/2020 03:00 WG1565201
trans-1,2-Dichloroethene U 0.149 1.00 1 10/26/2020 03:00 WG1565201
1,2-Dichloropropane U 0.149 1.00 1 10/26/2020 03:00 WG1565201
1,1-Dichloropropene U 0.142 1.00 1 10/26/2020 03:00 WG1565201
1,3-Dichloropropane U 0.110 1.00 1 10/26/2020 03:00 WG1565201
2,2-Dichloropropane U 0.161 1.00 1 10/27/2020 11:27 WG1565707
Di-isopropyl ether U 0.105 1.00 1 10/26/2020 03:00 WG1565201
Ethylbenzene U 0.137 1.00 1 10/26/2020 03:00 WG1565201
Hexachloro-1,3-butadiene U 0.337 1.00 1 10/26/2020 03:00 WG1565201
Isopropylbenzene 0.125 J 0.105 1.00 1 10/26/2020 03:00 WG1565201
p-Isopropyltoluene 1.92 0.120 1.00 1 10/26/2020 03:00 WG1565201
2-Butanone (MEK)2.30 J 1.19 10.0 1 10/27/2020 11:27 WG1565707
Methylene Chloride U 0.430 5.00 1 10/26/2020 03:00 WG1565201
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 10/26/2020 03:00 WG1565201
Methyl tert-butyl ether U 0.101 1.00 1 10/26/2020 03:00 WG1565201
Naphthalene U 1.00 5.00 1 10/26/2020 03:00 WG1565201
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1274449
GW-1
Collected date/time: 10/13/20 16:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
n-Propylbenzene 0.130 J 0.0993 1.00 1 10/26/2020 03:00 WG1565201
Styrene 0.180 J 0.118 1.00 1 10/26/2020 03:00 WG1565201
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 10/26/2020 03:00 WG1565201
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 10/26/2020 03:00 WG1565201
Tetrachloroethene U 0.300 1.00 1 10/26/2020 03:00 WG1565201
Toluene U 0.278 1.00 1 10/26/2020 03:00 WG1565201
1,2,3-Trichlorobenzene U 0.230 1.00 1 10/26/2020 03:00 WG1565201
1,2,4-Trichlorobenzene U 0.481 1.00 1 10/26/2020 03:00 WG1565201
1,1,1-Trichloroethane U 0.149 1.00 1 10/26/2020 03:00 WG1565201
1,1,2-Trichloroethane U 0.158 1.00 1 10/26/2020 03:00 WG1565201
Trichloroethene U 0.190 1.00 1 10/26/2020 03:00 WG1565201
Trichlorofluoromethane U 0.160 5.00 1 10/26/2020 03:00 WG1565201
1,2,3-Trichloropropane U 0.237 2.50 1 10/26/2020 03:00 WG1565201
1,2,4-Trimethylbenzene 2.92 0.322 1.00 1 10/26/2020 03:00 WG1565201
1,3,5-Trimethylbenzene 0.991 J 0.104 1.00 1 10/26/2020 03:00 WG1565201
Vinyl chloride U 0.234 1.00 1 10/26/2020 03:00 WG1565201
o-Xylene U 0.174 1.00 1 10/26/2020 03:00 WG1565201
m&p-Xylenes U 0.430 2.00 1 10/26/2020 03:00 WG1565201
(S) Toluene-d8 106 80.0-120 10/26/2020 03:00 WG1565201
(S) Toluene-d8 103 80.0-120 10/27/2020 11:27 WG1565707
(S) 4-Bromofluorobenzene 94.4 77.0-126 10/26/2020 03:00 WG1565201
(S) 4-Bromofluorobenzene 99.2 77.0-126 10/27/2020 11:27 WG1565707
(S) 1,2-Dichloroethane-d4 96.9 70.0-130 10/26/2020 03:00 WG1565201
(S) 1,2-Dichloroethane-d4 115 70.0-130 10/27/2020 11:27 WG1565707
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 178 33.3 100 1 10/24/2020 08:29 WG1563445
Unadjusted C19-C36 Aliphatics U 33.3 100 1 10/24/2020 08:29 WG1563445
Unadjusted C11-C22 Aromatics 79.0 J J3 33.3 100 1 10/24/2020 10:41 WG1563445
Unadjusted Total Petroleum
Hydrocarbons 257 33.3 100 1 10/24/2020 10:41 WG1563445
(S) o-Terphenyl 69.4 40.0-140 10/24/2020 10:41 WG1563445
(S) 1-Chloro-octadecane 58.5 40.0-140 10/24/2020 08:29 WG1563445
(S) 2-Fluorobiphenyl 82.5 40.0-140 10/24/2020 10:41 WG1563445
(S) 2-Bromonaphthalene 78.0 40.0-140 10/24/2020 10:41 WG1563445
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 10/20/2020 03:55 WG1561307
Acenaphthylene U 0.0921 1.00 1 10/20/2020 03:55 WG1561307
Anthracene U 0.0804 1.00 1 10/20/2020 03:55 WG1561307
Benzidine U 3.74 10.0 1 10/20/2020 03:55 WG1561307
Benzo(a)anthracene U 0.199 1.00 1 10/20/2020 03:55 WG1561307
Benzo(b)fluoranthene U 0.130 1.00 1 10/20/2020 03:55 WG1561307
Benzo(k)fluoranthene U 0.120 1.00 1 10/20/2020 03:55 WG1561307
Benzo(g,h,i)perylene U 0.121 1.00 1 10/20/2020 03:55 WG1561307
Benzo(a)pyrene U 0.0381 1.00 1 10/20/2020 03:55 WG1561307
Bis(2-chlorethoxy)methane U 0.116 10.0 1 10/20/2020 03:55 WG1561307
Bis(2-chloroethyl)ether U 0.137 10.0 1 10/20/2020 03:55 WG1561307
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 10/20/2020 03:55 WG1561307
4-Bromophenyl-phenylether U 0.0877 10.0 1 10/20/2020 03:55 WG1561307
2-Chloronaphthalene U 0.0648 1.00 1 10/20/2020 03:55 WG1561307
4-Chlorophenyl-phenylether U 0.0926 10.0 1 10/20/2020 03:55 WG1561307
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1274449
GW-1
Collected date/time: 10/13/20 16:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Chrysene U 0.130 1.00 1 10/20/2020 03:55 WG1561307
Dibenz(a,h)anthracene U 0.0644 1.00 1 10/20/2020 03:55 WG1561307
3,3-Dichlorobenzidine U 0.212 10.0 1 10/20/2020 03:55 WG1561307
2,4-Dinitrotoluene U 0.0983 10.0 1 10/20/2020 03:55 WG1561307
2,6-Dinitrotoluene U 0.250 10.0 1 10/20/2020 03:55 WG1561307
Fluoranthene 0.107 J 0.102 1.00 1 10/20/2020 03:55 WG1561307
Fluorene U 0.0844 1.00 1 10/20/2020 03:55 WG1561307
Hexachlorobenzene U 0.0755 1.00 1 10/20/2020 03:55 WG1561307
Hexachloro-1,3-butadiene U 0.0968 10.0 1 10/20/2020 03:55 WG1561307
Hexachlorocyclopentadiene U 0.0598 10.0 1 10/20/2020 03:55 WG1561307
Hexachloroethane U 0.127 10.0 1 10/20/2020 03:55 WG1561307
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 10/20/2020 03:55 WG1561307
Isophorone U 0.143 10.0 1 10/20/2020 03:55 WG1561307
Naphthalene 0.272 J 0.159 1.00 1 10/20/2020 03:55 WG1561307
Nitrobenzene U 0.297 10.0 1 10/20/2020 03:55 WG1561307
n-Nitrosodimethylamine U 0.998 10.0 1 10/20/2020 03:55 WG1561307
n-Nitrosodiphenylamine U 2.37 10.0 1 10/20/2020 03:55 WG1561307
n-Nitrosodi-n-propylamine U 0.261 10.0 1 10/20/2020 03:55 WG1561307
Phenanthrene U 0.112 1.00 1 10/20/2020 03:55 WG1561307
Benzylbutyl phthalate U 0.765 3.00 1 10/20/2020 03:55 WG1561307
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 10/20/2020 03:55 WG1561307
Di-n-butyl phthalate U 0.453 3.00 1 10/20/2020 03:55 WG1561307
Diethyl phthalate U 0.287 3.00 1 10/20/2020 03:55 WG1561307
Dimethyl phthalate 1.60 J 0.260 3.00 1 10/20/2020 03:55 WG1561307
Di-n-octyl phthalate U 0.932 3.00 1 10/20/2020 03:55 WG1561307
Pyrene 0.119 J 0.107 1.00 1 10/20/2020 03:55 WG1561307
1,2,4-Trichlorobenzene U 0.0698 10.0 1 10/20/2020 03:55 WG1561307
4-Chloro-3-methylphenol U 0.131 10.0 1 10/20/2020 03:55 WG1561307
2-Chlorophenol U 0.133 10.0 1 10/20/2020 03:55 WG1561307
2,4-Dichlorophenol U 0.102 10.0 1 10/20/2020 03:55 WG1561307
2,4-Dimethylphenol U 0.0636 10.0 1 10/20/2020 03:55 WG1561307
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 10/20/2020 03:55 WG1561307
2,4-Dinitrophenol U 5.93 10.0 1 10/20/2020 03:55 WG1561307
2-Nitrophenol U 0.117 10.0 1 10/20/2020 03:55 WG1561307
4-Nitrophenol U 0.143 10.0 1 10/20/2020 03:55 WG1561307
Pentachlorophenol U 0.313 10.0 1 10/20/2020 03:55 WG1561307
Phenol U 4.33 10.0 1 10/20/2020 03:55 WG1561307
2,4,6-Trichlorophenol U 0.100 10.0 1 10/20/2020 03:55 WG1561307
(S) 2-Fluorophenol 36.8 10.0-120 10/20/2020 03:55 WG1561307
(S) Phenol-d5 24.6 8.00-424 10/20/2020 03:55 WG1561307
(S) Nitrobenzene-d5 76.9 15.0-314 10/20/2020 03:55 WG1561307
(S) 2-Fluorobiphenyl 65.8 22.0-127 10/20/2020 03:55 WG1561307
(S) 2,4,6-Tribromophenol 46.9 10.0-153 10/20/2020 03:55 WG1561307
(S) p-Terphenyl-d14 62.3 29.0-141 10/20/2020 03:55 WG1561307
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier MDL RDL Dilution Analysis Batch CAS #RT
Analyte ug/l ug/l ug/l date / time
1H-Indene, 2,3-Dihydro-4-Methyl-5.89 J N 0.000 0.000 1 10/20/2020 03:55 WG1561307 000824-22-6 3.65
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICs are identified and quantitated using individual standards. TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation isaccomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is 10% or more of that of the nearest internal standard.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563415
Total Solids by Method 2540 G-2011 L1274449-01,02,03,04,05,06
Method Blank (MB)
(MB) R3584795-1 10/22/20 15:48
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1274442-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1274442-01 10/22/20 15:48 • (DUP) R3584795-3 10/22/20 15:48
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 81.4 79.0 1 3.05 10
Laboratory Control Sample (LCS)
(LCS) R3584795-2 10/22/20 15:48
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563417
Total Solids by Method 2540 G-2011 L1274449-07,08
Method Blank (MB)
(MB) R3584789-1 10/22/20 12:43
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1274451-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1274451-02 10/22/20 12:43 • (DUP) R3584789-3 10/22/20 12:43
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 86.0 85.5 1 0.572 10
Laboratory Control Sample (LCS)
(LCS) R3584789-2 10/22/20 12:43
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563655
Volatile Petroleum Hydrocarbons by Method MADEPV L1274449-09
Method Blank (MB)
(MB) R3584911-3 10/22/20 12:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID)84.4 70.0-130
(S) 2,5-Dibromotoluene(PID)89.2 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3584911-1 10/22/20 10:13 • (LCSD) R3584911-2 10/22/20 11:11
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 993 982 82.7 81.8 70.0-130 1.11 25
Unadjusted C9-C12 Aliphatics 1400 1550 1580 111 113 70.0-130 1.92 25
Unadjusted C9-C10 Aromatics 200 236 204 118 102 70.0-130 14.5 25
Total VPH 2800 2780 2770 99.3 98.9 70.0-130 0.360 25
(S) 2,5-Dibromotoluene(FID) 96.4 93.8 70.0-130
(S) 2,5-Dibromotoluene(PID) 99.4 99.2 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563287
Volatile Organic Compounds (GC) by Method 8015C L1274449-01,08
Method Blank (MB)
(MB) R3584543-3 10/22/20 10:53
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
TPH (GC/FID) Low Fraction 43.0 J 21.7 100
(S)
a,a,a-Trifluorotoluene(FID)111 77.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3584543-2 10/22/20 10:32 • (LCSD) R3584543-4 10/22/20 15:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
TPH (GC/FID) Low Fraction 5500 5140 6510 93.5 118 72.0-127 J3 23.5 20
(S)
a,a,a-Trifluorotoluene(FID) 102 107 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563292
Volatile Organic Compounds (GC) by Method 8015C L1274449-02,03,04,05,06,07
Method Blank (MB)
(MB) R3584537-2 10/22/20 05:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
TPH (GC/FID) Low Fraction U 21.7 100
(S)
a,a,a-Trifluorotoluene(FID)101 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3584537-1 10/22/20 04:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
TPH (GC/FID) Low Fraction 5500 6300 115 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 99.6 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565201
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1274449-09
Method Blank (MB)
(MB) R3585673-2 10/25/20 23:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
Methylene Chloride U 0.430 5.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565201
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1274449-09
Method Blank (MB)
(MB) R3585673-2 10/25/20 23:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 92.5 77.0-126
(S) 1,2-Dichloroethane-d4 99.1 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3585673-1 10/25/20 21:55
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acetone 25.0 47.7 191 19.0-160 J4
Acrolein 25.0 24.1 96.4 10.0-160
Acrylonitrile 25.0 34.5 138 55.0-149
Benzene 5.00 5.00 100 70.0-123
Bromobenzene 5.00 5.35 107 73.0-121
Bromodichloromethane 5.00 4.31 86.2 75.0-120
Bromoform 5.00 5.33 107 68.0-132
Bromomethane 5.00 4.66 93.2 10.0-160
n-Butylbenzene 5.00 4.04 80.8 73.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565201
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1274449-09
Laboratory Control Sample (LCS)
(LCS) R3585673-1 10/25/20 21:55
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
sec-Butylbenzene 5.00 5.19 104 75.0-125
tert-Butylbenzene 5.00 5.07 101 76.0-124
Carbon tetrachloride 5.00 4.23 84.6 68.0-126
Chlorobenzene 5.00 5.24 105 80.0-121
Chlorodibromomethane 5.00 4.83 96.6 77.0-125
Chloroethane 5.00 4.56 91.2 47.0-150
Chloroform 5.00 4.71 94.2 73.0-120
Chloromethane 5.00 4.65 93.0 41.0-142
2-Chlorotoluene 5.00 5.27 105 76.0-123
4-Chlorotoluene 5.00 4.97 99.4 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.66 93.2 58.0-134
1,2-Dibromoethane 5.00 5.60 112 80.0-122
Dibromomethane 5.00 5.26 105 80.0-120
1,2-Dichlorobenzene 5.00 4.86 97.2 79.0-121
1,3-Dichlorobenzene 5.00 5.08 102 79.0-120
1,4-Dichlorobenzene 5.00 5.14 103 79.0-120
Dichlorodifluoromethane 5.00 3.34 66.8 51.0-149
1,1-Dichloroethane 5.00 5.40 108 70.0-126
1,2-Dichloroethane 5.00 4.62 92.4 70.0-128
1,1-Dichloroethene 5.00 4.54 90.8 71.0-124
cis-1,2-Dichloroethene 5.00 4.93 98.6 73.0-120
trans-1,2-Dichloroethene 5.00 4.76 95.2 73.0-120
1,2-Dichloropropane 5.00 5.54 111 77.0-125
1,1-Dichloropropene 5.00 4.56 91.2 74.0-126
1,3-Dichloropropane 5.00 5.35 107 80.0-120
Di-isopropyl ether 5.00 5.05 101 58.0-138
Ethylbenzene 5.00 5.53 111 79.0-123
Hexachloro-1,3-butadiene 5.00 4.69 93.8 54.0-138
Isopropylbenzene 5.00 4.81 96.2 76.0-127
p-Isopropyltoluene 5.00 4.76 95.2 76.0-125
Methylene Chloride 5.00 4.91 98.2 67.0-120
4-Methyl-2-pentanone (MIBK)25.0 31.5 126 68.0-142
Methyl tert-butyl ether 5.00 4.26 85.2 68.0-125
Naphthalene 5.00 3.79 75.8 54.0-135
n-Propylbenzene 5.00 5.24 105 77.0-124
Styrene 5.00 4.98 99.6 73.0-130
1,1,1,2-Tetrachloroethane 5.00 4.99 99.8 75.0-125
1,1,2,2-Tetrachloroethane 5.00 4.88 97.6 65.0-130
Tetrachloroethene 5.00 5.59 112 72.0-132
Toluene 5.00 5.19 104 79.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565201
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1274449-09
Laboratory Control Sample (LCS)
(LCS) R3585673-1 10/25/20 21:55
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,2,3-Trichlorobenzene 5.00 4.39 87.8 50.0-138
1,2,4-Trichlorobenzene 5.00 4.11 82.2 57.0-137
1,1,1-Trichloroethane 5.00 4.15 83.0 73.0-124
1,1,2-Trichloroethane 5.00 5.33 107 80.0-120
Trichloroethene 5.00 5.87 117 78.0-124
Trichlorofluoromethane 5.00 4.41 88.2 59.0-147
1,2,3-Trichloropropane 5.00 5.82 116 73.0-130
1,2,4-Trimethylbenzene 5.00 4.98 99.6 76.0-121
1,3,5-Trimethylbenzene 5.00 5.09 102 76.0-122
Vinyl chloride 5.00 4.57 91.4 67.0-131
o-Xylene 5.00 5.10 102 80.0-122
m&p-Xylenes 10.0 9.97 99.7 80.0-122
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 94.4 77.0-126
(S) 1,2-Dichloroethane-d4 95.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565707
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1274449-09
Method Blank (MB)
(MB) R3586094-3 10/27/20 09:47
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
2,2-Dichloropropane U 0.161 1.00
2-Butanone (MEK)U 1.19 10.0
(S) Toluene-d8 100 80.0-120
(S) 4-Bromofluorobenzene 94.1 77.0-126
(S) 1,2-Dichloroethane-d4 114 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3586094-1 10/27/20 08:42
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
2,2-Dichloropropane 5.00 4.75 95.0 58.0-130
2-Butanone (MEK)25.0 27.9 112 44.0-160
(S) Toluene-d8 100 80.0-120
(S) 4-Bromofluorobenzene 97.6 77.0-126
(S) 1,2-Dichloroethane-d4 118 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563529
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-01,02,03,04,05
Method Blank (MB)
(MB) R3584553-3 10/22/20 11:15
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Acetone U 36.5 50.0
Acrylonitrile U 3.61 12.5
Benzene U 0.467 1.00
Bromobenzene U 0.900 12.5
Bromodichloromethane U 0.725 2.50
Bromoform U 1.17 25.0
Bromomethane U 1.97 12.5
n-Butylbenzene U 5.25 12.5
sec-Butylbenzene U 2.88 12.5
tert-Butylbenzene U 1.95 5.00
Carbon tetrachloride U 0.898 5.00
Chlorobenzene U 0.210 2.50
Chlorodibromomethane U 0.612 2.50
Chloroethane U 1.70 5.00
Chloroform U 1.03 2.50
Chloromethane U 4.35 12.5
2-Chlorotoluene U 0.865 2.50
4-Chlorotoluene U 0.450 5.00
1,2-Dibromo-3-Chloropropane U 3.90 25.0
1,2-Dibromoethane U 0.648 2.50
Dibromomethane U 0.750 5.00
1,2-Dichlorobenzene U 0.425 5.00
1,3-Dichlorobenzene U 0.600 5.00
1,4-Dichlorobenzene U 0.700 5.00
Dichlorodifluoromethane U 1.61 2.50
1,1-Dichloroethane U 0.491 2.50
1,2-Dichloroethane U 0.649 2.50
1,1-Dichloroethene U 0.606 2.50
cis-1,2-Dichloroethene U 0.734 2.50
trans-1,2-Dichloroethene U 1.04 5.00
1,2-Dichloropropane U 1.42 5.00
1,1-Dichloropropene U 0.809 2.50
1,3-Dichloropropane U 0.501 5.00
cis-1,3-Dichloropropene U 0.757 2.50
trans-1,3-Dichloropropene U 1.14 5.00
2,2-Dichloropropane U 1.38 2.50
Di-isopropyl ether U 0.410 1.00
Ethylbenzene U 0.737 2.50
Hexachloro-1,3-butadiene U 6.00 25.0
Isopropylbenzene U 0.425 2.50
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563529
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-01,02,03,04,05
Method Blank (MB)
(MB) R3584553-3 10/22/20 11:15
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
p-Isopropyltoluene U 2.55 5.00
2-Butanone (MEK)U 63.5 100
Methylene Chloride U 6.64 25.0
4-Methyl-2-pentanone (MIBK)U 2.28 25.0
Methyl tert-butyl ether U 0.350 1.00
Naphthalene U 4.88 12.5
n-Propylbenzene U 0.950 5.00
Styrene U 0.229 12.5
1,1,1,2-Tetrachloroethane U 0.948 2.50
1,1,2,2-Tetrachloroethane U 0.695 2.50
Tetrachloroethene U 0.896 2.50
Toluene U 1.30 5.00
1,2,3-Trichlorobenzene U 7.33 12.5
1,2,4-Trichlorobenzene U 4.40 12.5
1,1,1-Trichloroethane U 0.923 2.50
1,1,2-Trichloroethane U 0.597 2.50
Trichloroethene U 0.584 1.00
Trichlorofluoromethane U 0.827 2.50
1,2,3-Trichloropropane U 1.62 12.5
1,2,4-Trimethylbenzene U 1.58 5.00
1,3,5-Trimethylbenzene U 2.00 5.00
Vinyl chloride U 1.16 2.50
Xylenes, Total U 0.880 6.50
(S) Toluene-d8 108 75.0-131
(S) 4-Bromofluorobenzene 100 67.0-138
(S) 1,2-Dichloroethane-d4 93.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3584553-1 10/22/20 09:59 • (LCSD) R3584553-2 10/22/20 10:18
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Acetone 625 756 789 121 126 10.0-160 4.27 31
Acrylonitrile 625 781 754 125 121 45.0-153 3.52 22
Benzene 125 117 125 93.6 100 70.0-123 6.61 20
Bromobenzene 125 116 127 92.8 102 73.0-121 9.05 20
Bromodichloromethane 125 110 115 88.0 92.0 73.0-121 4.44 20
Bromoform 125 119 125 95.2 100 64.0-132 4.92 20
Bromomethane 125 91.4 112 73.1 89.6 56.0-147 J3 20.3 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563529
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3584553-1 10/22/20 09:59 • (LCSD) R3584553-2 10/22/20 10:18
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
n-Butylbenzene 125 139 161 111 129 68.0-135 14.7 20
sec-Butylbenzene 125 126 145 101 116 74.0-130 14.0 20
tert-Butylbenzene 125 117 134 93.6 107 75.0-127 13.5 20
Carbon tetrachloride 125 102 111 81.6 88.8 66.0-128 8.45 20
Chlorobenzene 125 121 130 96.8 104 76.0-128 7.17 20
Chlorodibromomethane 125 120 124 96.0 99.2 74.0-127 3.28 20
Chloroethane 125 101 113 80.8 90.4 61.0-134 11.2 20
Chloroform 125 107 114 85.6 91.2 72.0-123 6.33 20
Chloromethane 125 86.3 81.6 69.0 65.3 51.0-138 5.60 20
2-Chlorotoluene 125 120 142 96.0 114 75.0-124 16.8 20
4-Chlorotoluene 125 116 128 92.8 102 75.0-124 9.84 20
1,2-Dibromo-3-Chloropropane 125 106 117 84.8 93.6 59.0-130 9.87 20
1,2-Dibromoethane 125 125 129 100 103 74.0-128 3.15 20
Dibromomethane 125 121 128 96.8 102 75.0-122 5.62 20
1,2-Dichlorobenzene 125 113 141 90.4 113 76.0-124 J3 22.0 20
1,3-Dichlorobenzene 125 126 141 101 113 76.0-125 11.2 20
1,4-Dichlorobenzene 125 122 131 97.6 105 77.0-121 7.11 20
Dichlorodifluoromethane 125 104 94.6 83.2 75.7 43.0-156 9.47 20
1,1-Dichloroethane 125 109 119 87.2 95.2 70.0-127 8.77 20
1,2-Dichloroethane 125 102 106 81.6 84.8 65.0-131 3.85 20
1,1-Dichloroethene 125 110 119 88.0 95.2 65.0-131 7.86 20
cis-1,2-Dichloroethene 125 118 124 94.4 99.2 73.0-125 4.96 20
trans-1,2-Dichloroethene 125 111 120 88.8 96.0 71.0-125 7.79 20
1,2-Dichloropropane 125 115 125 92.0 100 74.0-125 8.33 20
1,1-Dichloropropene 125 103 113 82.4 90.4 73.0-125 9.26 20
1,3-Dichloropropane 125 120 129 96.0 103 80.0-125 7.23 20
cis-1,3-Dichloropropene 125 101 112 80.8 89.6 76.0-127 10.3 20
trans-1,3-Dichloropropene 125 118 121 94.4 96.8 73.0-127 2.51 20
2,2-Dichloropropane 125 106 121 84.8 96.8 59.0-135 13.2 20
Di-isopropyl ether 125 116 121 92.8 96.8 60.0-136 4.22 20
Ethylbenzene 125 122 136 97.6 109 74.0-126 10.9 20
Hexachloro-1,3-butadiene 125 109 131 87.2 105 57.0-150 18.3 20
Isopropylbenzene 125 127 138 102 110 72.0-127 8.30 20
p-Isopropyltoluene 125 126 148 101 118 72.0-133 16.1 20
2-Butanone (MEK)625 701 614 112 98.2 30.0-160 13.2 24
Methylene Chloride 125 117 122 93.6 97.6 68.0-123 4.18 20
4-Methyl-2-pentanone (MIBK)625 673 702 108 112 56.0-143 4.22 20
Methyl tert-butyl ether 125 116 120 92.8 96.0 66.0-132 3.39 20
Naphthalene 125 96.3 122 77.0 97.6 59.0-130 J3 23.5 20
n-Propylbenzene 125 118 136 94.4 109 74.0-126 14.2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563529
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3584553-1 10/22/20 09:59 • (LCSD) R3584553-2 10/22/20 10:18
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Styrene 125 124 137 99.2 110 72.0-127 9.96 20
1,1,1,2-Tetrachloroethane 125 112 119 89.6 95.2 74.0-129 6.06 20
1,1,2,2-Tetrachloroethane 125 135 142 108 114 68.0-128 5.05 20
Tetrachloroethene 125 115 127 92.0 102 70.0-136 9.92 20
Toluene 125 115 124 92.0 99.2 75.0-121 7.53 20
1,2,3-Trichlorobenzene 125 114 138 91.2 110 59.0-139 19.0 20
1,2,4-Trichlorobenzene 125 119 143 95.2 114 62.0-137 18.3 20
1,1,1-Trichloroethane 125 101 113 80.8 90.4 69.0-126 11.2 20
1,1,2-Trichloroethane 125 127 132 102 106 78.0-123 3.86 20
Trichloroethene 125 111 120 88.8 96.0 76.0-126 7.79 20
Trichlorofluoromethane 125 103 107 82.4 85.6 61.0-142 3.81 20
1,2,3-Trichloropropane 125 114 126 91.2 101 67.0-129 10.0 20
1,2,4-Trimethylbenzene 125 121 137 96.8 110 70.0-126 12.4 20
1,3,5-Trimethylbenzene 125 120 137 96.0 110 73.0-127 13.2 20
Vinyl chloride 125 72.3 66.4 57.8 53.1 63.0-134 J4 J4 8.51 20
Xylenes, Total 375 348 413 92.8 110 72.0-127 17.1 20
(S) Toluene-d8 106 107 75.0-131
(S) 4-Bromofluorobenzene 102 99.4 67.0-138
(S) 1,2-Dichloroethane-d4 98.9 98.8 70.0-130
L1274114-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274114-05 10/22/20 15:09 • (MS) R3584553-4 10/22/20 20:52 • (MSD) R3584553-5 10/22/20 21:11
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
Acetone 620 U 351 323 56.6 52.1 1 10.0-160 8.31 40
Acrylonitrile 620 U 625 584 101 94.2 1 10.0-160 6.78 40
Benzene 124 U 99.6 120 80.3 96.8 1 10.0-149 18.6 37
Bromobenzene 124 U 106 127 85.5 102 1 10.0-156 18.0 38
Bromodichloromethane 124 U 93.5 108 75.4 87.1 1 10.0-143 14.4 37
Bromoform 124 U 106 114 85.5 91.9 1 10.0-146 7.27 36
Bromomethane 124 U 48.3 64.0 39.0 51.6 1 10.0-149 28.0 38
n-Butylbenzene 124 U 122 150 98.4 121 1 10.0-160 20.6 40
sec-Butylbenzene 124 U 117 143 94.4 115 1 10.0-159 20.0 39
tert-Butylbenzene 124 U 110 135 88.7 109 1 10.0-156 20.4 39
Carbon tetrachloride 124 U 91.0 104 73.4 83.9 1 10.0-145 13.3 37
Chlorobenzene 124 U 108 127 87.1 102 1 10.0-152 16.2 39
Chlorodibromomethane 124 U 108 121 87.1 97.6 1 10.0-146 11.4 37
Chloroethane 124 U 39.5 45.4 31.9 36.6 1 10.0-146 13.9 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563529
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-01,02,03,04,05
L1274114-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274114-05 10/22/20 15:09 • (MS) R3584553-4 10/22/20 20:52 • (MSD) R3584553-5 10/22/20 21:11
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
Chloroform 124 U 93.3 108 75.2 87.1 1 10.0-146 14.6 37
Chloromethane 124 U 75.9 84.4 61.2 68.1 1 10.0-159 10.6 37
2-Chlorotoluene 124 U 112 133 90.3 107 1 10.0-159 17.1 38
4-Chlorotoluene 124 U 105 130 84.7 105 1 10.0-155 21.3 39
1,2-Dibromo-3-Chloropropane 124 U 84.1 85.3 67.8 68.8 1 10.0-151 1.42 39
1,2-Dibromoethane 124 U 111 123 89.5 99.2 1 10.0-148 10.3 34
Dibromomethane 124 U 109 115 87.9 92.7 1 10.0-147 5.36 35
1,2-Dichlorobenzene 124 U 114 130 91.9 105 1 10.0-155 13.1 37
1,3-Dichlorobenzene 124 U 112 130 90.3 105 1 10.0-153 14.9 38
1,4-Dichlorobenzene 124 U 107 123 86.3 99.2 1 10.0-151 13.9 38
Dichlorodifluoromethane 124 U 82.8 115 66.8 92.7 1 10.0-160 32.6 35
1,1-Dichloroethane 124 U 91.8 110 74.0 88.7 1 10.0-147 18.0 37
1,2-Dichloroethane 124 U 90.1 98.1 72.7 79.1 1 10.0-148 8.50 35
1,1-Dichloroethene 124 U 65.9 78.1 53.1 63.0 1 10.0-155 16.9 37
cis-1,2-Dichloroethene 124 U 96.6 117 77.9 94.4 1 10.0-149 19.1 37
trans-1,2-Dichloroethene 124 U 92.0 111 74.2 89.5 1 10.0-150 18.7 37
1,2-Dichloropropane 124 U 99.3 118 80.1 95.2 1 10.0-148 17.2 37
1,1-Dichloropropene 124 U 89.6 110 72.3 88.7 1 10.0-153 20.4 35
1,3-Dichloropropane 124 U 114 126 91.9 102 1 10.0-154 10.0 35
cis-1,3-Dichloropropene 124 U 91.1 103 73.5 83.1 1 10.0-151 12.3 37
trans-1,3-Dichloropropene 124 U 102 118 82.3 95.2 1 10.0-148 14.5 37
2,2-Dichloropropane 124 U 76.7 82.8 61.9 66.8 1 10.0-138 7.65 36
Di-isopropyl ether 124 U 100 113 80.6 91.1 1 10.0-147 12.2 36
Ethylbenzene 124 U 109 132 87.9 106 1 10.0-160 19.1 38
Hexachloro-1,3-butadiene 124 U 102 111 82.3 89.5 1 10.0-160 8.45 40
Isopropylbenzene 124 U 113 135 91.1 109 1 10.0-155 17.7 38
p-Isopropyltoluene 124 U 117 140 94.4 113 1 10.0-160 17.9 40
2-Butanone (MEK)620 U 399 343 64.4 55.3 1 10.0-160 15.1 40
Methylene Chloride 124 U 72.3 77.1 58.3 62.2 1 10.0-141 6.43 37
4-Methyl-2-pentanone (MIBK)620 U 540 564 87.1 91.0 1 10.0-160 4.35 35
Methyl tert-butyl ether 124 U 102 101 82.3 81.5 1 11.0-147 0.985 35
Naphthalene 124 U 71.2 76.7 57.4 61.9 1 10.0-160 7.44 36
n-Propylbenzene 124 U 106 132 85.5 106 1 10.0-158 21.8 38
Styrene 124 U 110 133 88.7 107 1 10.0-160 18.9 40
1,1,1,2-Tetrachloroethane 124 U 98.5 114 79.4 91.9 1 10.0-149 14.6 39
1,1,2,2-Tetrachloroethane 124 U 89.6 98.2 72.3 79.2 1 10.0-160 9.16 35
Tetrachloroethene 124 U 104 130 83.9 105 1 10.0-156 22.2 39
Toluene 124 U 101 125 81.5 101 1 10.0-156 21.2 38
1,2,3-Trichlorobenzene 124 U 109 103 87.9 83.1 1 10.0-160 5.66 40
1,2,4-Trichlorobenzene 124 U 101 103 81.5 83.1 1 10.0-160 1.96 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 14:56 47 of 74
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 2020102 L1274449 10/27/20 17:45 47 of 74
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563529
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-01,02,03,04,05
L1274114-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274114-05 10/22/20 15:09 • (MS) R3584553-4 10/22/20 20:52 • (MSD) R3584553-5 10/22/20 21:11
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
1,1,1-Trichloroethane 124 U 93.5 112 75.4 90.3 1 10.0-144 18.0 35
1,1,2-Trichloroethane 124 U 114 126 91.9 102 1 10.0-160 10.0 35
Trichloroethene 124 U 114 135 91.9 109 1 10.0-156 16.9 38
Trichlorofluoromethane 124 U 46.1 55.9 37.2 45.1 1 10.0-160 19.2 40
1,2,3-Trichloropropane 124 U 101 112 81.5 90.3 1 10.0-156 10.3 35
1,2,4-Trimethylbenzene 124 U 108 127 87.1 102 1 10.0-160 16.2 36
1,3,5-Trimethylbenzene 124 U 109 131 87.9 106 1 10.0-160 18.3 38
Vinyl chloride 124 U 60.6 75.4 48.9 60.8 1 10.0-160 21.8 37
Xylenes, Total 372 U 331 400 89.0 108 1 10.0-160 18.9 38
(S) Toluene-d8 106 109 75.0-131
(S) 4-Bromofluorobenzene 101 99.4 67.0-138
(S) 1,2-Dichloroethane-d4 94.6 92.9 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1564404
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06
Method Blank (MB)
(MB) R3585781-2 10/23/20 18:41
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Acetone U 36.5 50.0
Acrylonitrile U 3.61 12.5
Benzene U 0.467 1.00
Bromobenzene U 0.900 12.5
Bromodichloromethane U 0.725 2.50
Bromoform U 1.17 25.0
n-Butylbenzene U 5.25 12.5
sec-Butylbenzene U 2.88 12.5
tert-Butylbenzene U 1.95 5.00
Carbon tetrachloride U 0.898 5.00
Chlorobenzene U 0.210 2.50
Chlorodibromomethane U 0.612 2.50
Chloroform U 1.03 2.50
2-Chlorotoluene U 0.865 2.50
4-Chlorotoluene U 0.450 5.00
1,2-Dibromo-3-Chloropropane U 3.90 25.0
1,2-Dibromoethane U 0.648 2.50
Dibromomethane U 0.750 5.00
1,2-Dichlorobenzene U 0.425 5.00
1,3-Dichlorobenzene U 0.600 5.00
1,4-Dichlorobenzene U 0.700 5.00
Dichlorodifluoromethane U 1.61 2.50
1,1-Dichloroethane U 0.491 2.50
1,2-Dichloroethane U 0.649 2.50
1,1-Dichloroethene U 0.606 2.50
cis-1,2-Dichloroethene U 0.734 2.50
trans-1,2-Dichloroethene U 1.04 5.00
1,2-Dichloropropane U 1.42 5.00
1,1-Dichloropropene U 0.809 2.50
1,3-Dichloropropane U 0.501 5.00
cis-1,3-Dichloropropene U 0.757 2.50
trans-1,3-Dichloropropene U 1.14 5.00
2,2-Dichloropropane U 1.38 2.50
Di-isopropyl ether U 0.410 1.00
Ethylbenzene U 0.737 2.50
Hexachloro-1,3-butadiene U 6.00 25.0
Isopropylbenzene U 0.425 2.50
p-Isopropyltoluene U 2.55 5.00
2-Butanone (MEK)U 63.5 100
Methylene Chloride U 6.64 25.0
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1564404
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06
Method Blank (MB)
(MB) R3585781-2 10/23/20 18:41
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
4-Methyl-2-pentanone (MIBK)U 2.28 25.0
Methyl tert-butyl ether U 0.350 1.00
Naphthalene U 4.88 12.5
n-Propylbenzene U 0.950 5.00
Styrene U 0.229 12.5
1,1,1,2-Tetrachloroethane U 0.948 2.50
1,1,2,2-Tetrachloroethane U 0.695 2.50
Tetrachloroethene U 0.896 2.50
Toluene U 1.30 5.00
1,2,3-Trichlorobenzene U 7.33 12.5
1,2,4-Trichlorobenzene U 4.40 12.5
1,1,1-Trichloroethane U 0.923 2.50
1,1,2-Trichloroethane U 0.597 2.50
Trichloroethene U 0.584 1.00
1,2,3-Trichloropropane U 1.62 12.5
1,3,5-Trimethylbenzene U 2.00 5.00
Xylenes, Total U 0.880 6.50
(S) Toluene-d8 109 75.0-131
(S) 4-Bromofluorobenzene 70.8 67.0-138
(S) 1,2-Dichloroethane-d4 95.4 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3585781-1 10/23/20 17:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
Acetone 625 698 112 10.0-160
Acrylonitrile 625 684 109 45.0-153
Benzene 125 117 93.6 70.0-123
Bromobenzene 125 164 131 73.0-121 J4
Bromodichloromethane 125 116 92.8 73.0-121
Bromoform 125 133 106 64.0-132
n-Butylbenzene 125 138 110 68.0-135
sec-Butylbenzene 125 144 115 74.0-130
tert-Butylbenzene 125 145 116 75.0-127
Carbon tetrachloride 125 106 84.8 66.0-128
Chlorobenzene 125 122 97.6 76.0-128
Chlorodibromomethane 125 144 115 74.0-127
Chloroform 125 111 88.8 72.0-123
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1564404
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06
Laboratory Control Sample (LCS)
(LCS) R3585781-1 10/23/20 17:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
2-Chlorotoluene 125 133 106 75.0-124
4-Chlorotoluene 125 149 119 75.0-124
1,2-Dibromo-3-Chloropropane 125 123 98.4 59.0-130
1,2-Dibromoethane 125 143 114 74.0-128
Dibromomethane 125 124 99.2 75.0-122
1,2-Dichlorobenzene 125 134 107 76.0-124
1,3-Dichlorobenzene 125 129 103 76.0-125
1,4-Dichlorobenzene 125 123 98.4 77.0-121
Dichlorodifluoromethane 125 112 89.6 43.0-156
1,1-Dichloroethane 125 111 88.8 70.0-127
1,2-Dichloroethane 125 104 83.2 65.0-131
1,1-Dichloroethene 125 109 87.2 65.0-131
cis-1,2-Dichloroethene 125 121 96.8 73.0-125
trans-1,2-Dichloroethene 125 113 90.4 71.0-125
1,2-Dichloropropane 125 113 90.4 74.0-125
1,1-Dichloropropene 125 109 87.2 73.0-125
1,3-Dichloropropane 125 148 118 80.0-125
cis-1,3-Dichloropropene 125 105 84.0 76.0-127
trans-1,3-Dichloropropene 125 136 109 73.0-127
2,2-Dichloropropane 125 123 98.4 59.0-135
Di-isopropyl ether 125 111 88.8 60.0-136
Ethylbenzene 125 125 100 74.0-126
Hexachloro-1,3-butadiene 125 196 157 57.0-150 J4
Isopropylbenzene 125 122 97.6 72.0-127
p-Isopropyltoluene 125 131 105 72.0-133
2-Butanone (MEK)625 601 96.2 30.0-160
Methylene Chloride 125 113 90.4 68.0-123
4-Methyl-2-pentanone (MIBK)625 744 119 56.0-143
Methyl tert-butyl ether 125 117 93.6 66.0-132
Naphthalene 125 147 118 59.0-130
n-Propylbenzene 125 157 126 74.0-126
Styrene 125 130 104 72.0-127
1,1,1,2-Tetrachloroethane 125 112 89.6 74.0-129
1,1,2,2-Tetrachloroethane 125 153 122 68.0-128
Tetrachloroethene 125 141 113 70.0-136
Toluene 125 130 104 75.0-121
1,2,3-Trichlorobenzene 125 192 154 59.0-139 J4
1,2,4-Trichlorobenzene 125 181 145 62.0-137 J4
1,1,1-Trichloroethane 125 109 87.2 69.0-126
1,1,2-Trichloroethane 125 152 122 78.0-123
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1564404
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06
Laboratory Control Sample (LCS)
(LCS) R3585781-1 10/23/20 17:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
Trichloroethene 125 116 92.8 76.0-126
1,2,3-Trichloropropane 125 139 111 67.0-129
1,3,5-Trimethylbenzene 125 133 106 73.0-127
Xylenes, Total 375 342 91.2 72.0-127
(S) Toluene-d8 118 75.0-131
(S) 4-Bromofluorobenzene 101 67.0-138
(S) 1,2-Dichloroethane-d4 101 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565803
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06,07,08
Method Blank (MB)
(MB) R3586063-3 10/27/20 01:20
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Acetone U 36.5 50.0
Acrylonitrile U 3.61 12.5
Benzene U 0.467 1.00
Bromobenzene U 0.900 12.5
Bromodichloromethane U 0.725 2.50
Bromoform U 1.17 25.0
Bromomethane U 1.97 12.5
n-Butylbenzene U 5.25 12.5
sec-Butylbenzene U 2.88 12.5
tert-Butylbenzene U 1.95 5.00
Carbon tetrachloride U 0.898 5.00
Chlorobenzene U 0.210 2.50
Chlorodibromomethane U 0.612 2.50
Chloroethane U 1.70 5.00
Chloroform U 1.03 2.50
Chloromethane U 4.35 12.5
2-Chlorotoluene U 0.865 2.50
4-Chlorotoluene U 0.450 5.00
1,2-Dibromo-3-Chloropropane U 3.90 25.0
1,2-Dibromoethane U 0.648 2.50
Dibromomethane U 0.750 5.00
1,2-Dichlorobenzene U 0.425 5.00
1,3-Dichlorobenzene U 0.600 5.00
1,4-Dichlorobenzene U 0.700 5.00
Dichlorodifluoromethane U 1.61 2.50
1,1-Dichloroethane U 0.491 2.50
1,2-Dichloroethane U 0.649 2.50
1,1-Dichloroethene U 0.606 2.50
cis-1,2-Dichloroethene U 0.734 2.50
trans-1,2-Dichloroethene U 1.04 5.00
1,2-Dichloropropane U 1.42 5.00
1,1-Dichloropropene U 0.809 2.50
1,3-Dichloropropane U 0.501 5.00
cis-1,3-Dichloropropene U 0.757 2.50
trans-1,3-Dichloropropene U 1.14 5.00
2,2-Dichloropropane U 1.38 2.50
Di-isopropyl ether U 0.410 1.00
Ethylbenzene U 0.737 2.50
Hexachloro-1,3-butadiene U 6.00 25.0
Isopropylbenzene U 0.425 2.50
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565803
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06,07,08
Method Blank (MB)
(MB) R3586063-3 10/27/20 01:20
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
p-Isopropyltoluene U 2.55 5.00
2-Butanone (MEK)U 63.5 100
Methylene Chloride U 6.64 25.0
4-Methyl-2-pentanone (MIBK)U 2.28 25.0
Methyl tert-butyl ether U 0.350 1.00
Naphthalene U 4.88 12.5
n-Propylbenzene U 0.950 5.00
Styrene U 0.229 12.5
1,1,1,2-Tetrachloroethane U 0.948 2.50
1,1,2,2-Tetrachloroethane U 0.695 2.50
Tetrachloroethene U 0.896 2.50
Toluene U 1.30 5.00
1,2,3-Trichlorobenzene U 7.33 12.5
1,2,4-Trichlorobenzene U 4.40 12.5
1,1,1-Trichloroethane U 0.923 2.50
1,1,2-Trichloroethane U 0.597 2.50
Trichloroethene U 0.584 1.00
Trichlorofluoromethane U 0.827 2.50
1,2,3-Trichloropropane U 1.62 12.5
1,2,4-Trimethylbenzene U 1.58 5.00
1,3,5-Trimethylbenzene U 2.00 5.00
Vinyl chloride U 1.16 2.50
Xylenes, Total U 0.880 6.50
(S) Toluene-d8 113 75.0-131
(S) 4-Bromofluorobenzene 96.5 67.0-138
(S) 1,2-Dichloroethane-d4 96.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3586063-1 10/26/20 22:51 • (LCSD) R3586063-2 10/26/20 23:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Acetone 625 711 714 114 114 10.0-160 0.421 31
Acrylonitrile 625 659 707 105 113 45.0-153 7.03 22
Benzene 125 125 129 100 103 70.0-123 3.15 20
Bromobenzene 125 136 132 109 106 73.0-121 2.99 20
Bromodichloromethane 125 127 135 102 108 73.0-121 6.11 20
Bromoform 125 131 132 105 106 64.0-132 0.760 20
Bromomethane 125 136 140 109 112 56.0-147 2.90 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565803
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3586063-1 10/26/20 22:51 • (LCSD) R3586063-2 10/26/20 23:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
n-Butylbenzene 125 128 132 102 106 68.0-135 3.08 20
sec-Butylbenzene 125 137 134 110 107 74.0-130 2.21 20
tert-Butylbenzene 125 134 134 107 107 75.0-127 0.000 20
Carbon tetrachloride 125 137 134 110 107 66.0-128 2.21 20
Chlorobenzene 125 132 132 106 106 76.0-128 0.000 20
Chlorodibromomethane 125 124 122 99.2 97.6 74.0-127 1.63 20
Chloroethane 125 134 142 107 114 61.0-134 5.80 20
Chloroform 125 129 130 103 104 72.0-123 0.772 20
Chloromethane 125 131 130 105 104 51.0-138 0.766 20
2-Chlorotoluene 125 140 144 112 115 75.0-124 2.82 20
4-Chlorotoluene 125 138 134 110 107 75.0-124 2.94 20
1,2-Dibromo-3-Chloropropane 125 117 126 93.6 101 59.0-130 7.41 20
1,2-Dibromoethane 125 130 129 104 103 74.0-128 0.772 20
Dibromomethane 125 125 126 100 101 75.0-122 0.797 20
1,2-Dichlorobenzene 125 130 131 104 105 76.0-124 0.766 20
1,3-Dichlorobenzene 125 131 133 105 106 76.0-125 1.52 20
1,4-Dichlorobenzene 125 128 129 102 103 77.0-121 0.778 20
Dichlorodifluoromethane 125 113 123 90.4 98.4 43.0-156 8.47 20
1,1-Dichloroethane 125 133 131 106 105 70.0-127 1.52 20
1,2-Dichloroethane 125 121 121 96.8 96.8 65.0-131 0.000 20
1,1-Dichloroethene 125 138 130 110 104 65.0-131 5.97 20
cis-1,2-Dichloroethene 125 135 138 108 110 73.0-125 2.20 20
trans-1,2-Dichloroethene 125 127 130 102 104 71.0-125 2.33 20
1,2-Dichloropropane 125 123 132 98.4 106 74.0-125 7.06 20
1,1-Dichloropropene 125 128 130 102 104 73.0-125 1.55 20
1,3-Dichloropropane 125 132 132 106 106 80.0-125 0.000 20
cis-1,3-Dichloropropene 125 124 133 99.2 106 76.0-127 7.00 20
trans-1,3-Dichloropropene 125 130 134 104 107 73.0-127 3.03 20
2,2-Dichloropropane 125 123 123 98.4 98.4 59.0-135 0.000 20
Di-isopropyl ether 125 134 132 107 106 60.0-136 1.50 20
Ethylbenzene 125 132 133 106 106 74.0-126 0.755 20
Hexachloro-1,3-butadiene 125 119 137 95.2 110 57.0-150 14.1 20
Isopropylbenzene 125 135 138 108 110 72.0-127 2.20 20
p-Isopropyltoluene 125 131 134 105 107 72.0-133 2.26 20
2-Butanone (MEK)625 688 815 110 130 30.0-160 16.9 24
Methylene Chloride 125 134 123 107 98.4 68.0-123 8.56 20
4-Methyl-2-pentanone (MIBK)625 685 685 110 110 56.0-143 0.000 20
Methyl tert-butyl ether 125 130 133 104 106 66.0-132 2.28 20
Naphthalene 125 122 139 97.6 111 59.0-130 13.0 20
n-Propylbenzene 125 143 142 114 114 74.0-126 0.702 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1565803
Volatile Organic Compounds (GC/MS) by Method 8260D L1274449-06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3586063-1 10/26/20 22:51 • (LCSD) R3586063-2 10/26/20 23:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Styrene 125 133 131 106 105 72.0-127 1.52 20
1,1,1,2-Tetrachloroethane 125 128 131 102 105 74.0-129 2.32 20
1,1,2,2-Tetrachloroethane 125 126 123 101 98.4 68.0-128 2.41 20
Tetrachloroethene 125 139 143 111 114 70.0-136 2.84 20
Toluene 125 126 128 101 102 75.0-121 1.57 20
1,2,3-Trichlorobenzene 125 127 142 102 114 59.0-139 11.2 20
1,2,4-Trichlorobenzene 125 119 137 95.2 110 62.0-137 14.1 20
1,1,1-Trichloroethane 125 125 127 100 102 69.0-126 1.59 20
1,1,2-Trichloroethane 125 129 128 103 102 78.0-123 0.778 20
Trichloroethene 125 128 137 102 110 76.0-126 6.79 20
Trichlorofluoromethane 125 126 129 101 103 61.0-142 2.35 20
1,2,3-Trichloropropane 125 135 126 108 101 67.0-129 6.90 20
1,2,4-Trimethylbenzene 125 132 131 106 105 70.0-126 0.760 20
1,3,5-Trimethylbenzene 125 137 138 110 110 73.0-127 0.727 20
Vinyl chloride 125 128 134 102 107 63.0-134 4.58 20
Xylenes, Total 375 389 397 104 106 72.0-127 2.04 20
(S) Toluene-d8 105 107 75.0-131
(S) 4-Bromofluorobenzene 99.2 98.4 67.0-138
(S) 1,2-Dichloroethane-d4 105 103 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563260
Semi-Volatile Organic Compounds (GC) by Method 8015C L1274449-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3584675-1 10/22/20 22:20
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
TPH (GC/FID) High Fraction U 769 4000
(S) o-Terphenyl 86.5 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3584675-2 10/22/20 22:33
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
TPH (GC/FID) High Fraction 50000 48400 96.8 50.0-150
(S) o-Terphenyl 113 18.0-148
L1274449-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274449-02 10/22/20 23:26 • (MS) R3584675-3 10/22/20 23:40 • (MSD) R3584675-4 10/22/20 23:53
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
TPH (GC/FID) High Fraction 64800 1300 60600 61800 93.6 95.4 1 50.0-150 1.92 20
(S) o-Terphenyl 105 108 18.0-148
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563445
TPH by Method MADEPE L1274449-09
Method Blank (MB)
(MB) R3585477-1 10/24/20 03:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 83.5 40.0-140
Method Blank (MB)
(MB) R3585477-4 10/24/20 04:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 78.6 40.0-140
(S) 2-Fluorobiphenyl 82.6 40.0-140
(S) 2-Bromonaphthalene 67.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3585477-2 10/24/20 04:06 • (LCSD) R3585477-3 10/24/20 04:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 367 323 61.2 53.8 40.0-140 12.8 25
Unadjusted C19-C36 Aliphatics 800 593 511 74.1 63.9 40.0-140 14.9 25
(S) 1-Chloro-octadecane 87.1 75.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3585477-5 10/24/20 05:11 • (LCSD) R3585477-6 10/24/20 05:33
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1340 1010 78.8 59.4 40.0-140 J3 28.1 25
(S) o-Terphenyl 81.9 61.6 40.0-140
(S) 2-Fluorobiphenyl 85.6 75.4 40.0-140
(S) 2-Bromonaphthalene 77.3 56.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1561307
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1274449-09
Method Blank (MB)
(MB) R3583474-2 10/20/20 02:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzidine U 3.74 10.0
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-oxybis(1-chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1561307
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1274449-09
Method Blank (MB)
(MB) R3583474-2 10/20/20 02:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Pyrene U 0.107 1.00
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
(S) Nitrobenzene-d5 54.8 15.0-314
(S) 2-Fluorobiphenyl 65.6 22.0-127
(S) p-Terphenyl-d14 72.7 29.0-141
(S) Phenol-d5 21.1 8.00-424
(S) 2-Fluorophenol 35.9 10.0-120
(S) 2,4,6-Tribromophenol 62.5 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3583474-1 10/20/20 02:24
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 31.3 62.6 47.0-145
Acenaphthylene 50.0 35.3 70.6 33.0-145
Anthracene 50.0 30.9 61.8 27.0-133
Benzidine 100 35.9 35.9 1.00-120
Benzo(a)anthracene 50.0 36.9 73.8 33.0-143
Benzo(b)fluoranthene 50.0 33.0 66.0 24.0-159
Benzo(k)fluoranthene 50.0 32.2 64.4 11.0-162
Benzo(g,h,i)perylene 50.0 28.2 56.4 1.00-219
Benzo(a)pyrene 50.0 35.3 70.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 29.8 59.6 1.00-219
Bis(2-chloroethyl)ether 50.0 32.6 65.2 33.0-185
2,2-oxybis(1-chloropropane)50.0 28.9 57.8 36.0-166
4-Bromophenyl-phenylether 50.0 33.2 66.4 53.0-127
2-Chloronaphthalene 50.0 32.8 65.6 60.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1561307
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1274449-09
Laboratory Control Sample (LCS)
(LCS) R3583474-1 10/20/20 02:24
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
4-Chlorophenyl-phenylether 50.0 34.1 68.2 25.0-158
Chrysene 50.0 31.7 63.4 17.0-168
Dibenz(a,h)anthracene 50.0 30.2 60.4 1.00-227
3,3-Dichlorobenzidine 100 74.9 74.9 1.00-262
2,4-Dinitrotoluene 50.0 36.5 73.0 39.0-139
2,6-Dinitrotoluene 50.0 35.3 70.6 50.0-158
Fluoranthene 50.0 31.5 63.0 26.0-137
Fluorene 50.0 33.0 66.0 59.0-121
Hexachlorobenzene 50.0 32.8 65.6 1.00-152
Hexachloro-1,3-butadiene 50.0 28.4 56.8 24.0-120
Hexachlorocyclopentadiene 50.0 19.7 39.4 10.0-120
Hexachloroethane 50.0 29.3 58.6 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 29.9 59.8 1.00-171
Isophorone 50.0 29.6 59.2 21.0-196
Naphthalene 50.0 27.6 55.2 21.0-133
Nitrobenzene 50.0 28.9 57.8 35.0-180
n-Nitrosodimethylamine 50.0 15.5 31.0 10.0-120
n-Nitrosodiphenylamine 50.0 32.3 64.6 44.0-120
n-Nitrosodi-n-propylamine 50.0 32.5 65.0 1.00-230
Phenanthrene 50.0 33.1 66.2 54.0-120
Benzylbutyl phthalate 50.0 41.1 82.2 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 36.3 72.6 8.00-158
Di-n-butyl phthalate 50.0 34.6 69.2 1.00-120
Diethyl phthalate 50.0 34.3 68.6 1.00-120
Dimethyl phthalate 50.0 34.0 68.0 1.00-120
Di-n-octyl phthalate 50.0 33.9 67.8 4.00-146
Pyrene 50.0 35.8 71.6 52.0-120
1,2,4-Trichlorobenzene 50.0 28.7 57.4 44.0-142
4-Chloro-3-methylphenol 50.0 28.9 57.8 22.0-147
2-Chlorophenol 50.0 28.7 57.4 23.0-134
2,4-Dichlorophenol 50.0 30.3 60.6 39.0-135
2,4-Dimethylphenol 50.0 29.4 58.8 32.0-120
4,6-Dinitro-2-methylphenol 50.0 35.7 71.4 1.00-181
2,4-Dinitrophenol 50.0 35.1 70.2 1.00-191
2-Nitrophenol 50.0 32.0 64.0 29.0-182
4-Nitrophenol 50.0 12.8 25.6 1.00-132
Pentachlorophenol 50.0 30.8 61.6 14.0-176
Phenol 50.0 11.7 23.4 5.00-120
2,4,6-Trichlorophenol 50.0 34.2 68.4 37.0-144
(S) Nitrobenzene-d5 50.2 15.0-314
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1561307
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1274449-09
Laboratory Control Sample (LCS)
(LCS) R3583474-1 10/20/20 02:24
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) 2-Fluorobiphenyl 65.3 22.0-127
(S) p-Terphenyl-d14 69.7 29.0-141
(S) Phenol-d5 22.2 8.00-424
(S) 2-Fluorophenol 35.7 10.0-120
(S) 2,4,6-Tribromophenol 67.0 10.0-153
L1274446-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274446-01 10/20/20 09:16 • (MS) R3583474-3 10/20/20 09:36 • (MSD) R3583474-4 10/20/20 09:57
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 U 31.4 29.4 62.8 58.8 1 47.0-145 6.58 48
Acenaphthylene 50.0 U 34.6 32.1 69.2 64.2 1 33.0-145 7.50 74
Anthracene 50.0 U 30.5 28.2 61.0 56.4 1 27.0-133 7.84 66
Benzidine 100 U 22.6 3.97 22.6 3.97 1 1.00-120 J3 140 40
Benzo(a)anthracene 50.0 U 35.0 32.5 70.0 65.0 1 33.0-143 7.41 53
Benzo(b)fluoranthene 50.0 U 31.9 29.4 63.8 58.8 1 24.0-159 8.16 71
Benzo(k)fluoranthene 50.0 U 30.2 29.0 60.4 58.0 1 11.0-162 4.05 63
Benzo(g,h,i)perylene 50.0 U 26.0 25.4 52.0 50.8 1 1.00-219 2.33 97
Benzo(a)pyrene 50.0 U 33.2 31.4 66.4 62.8 1 17.0-163 5.57 72
Bis(2-chlorethoxy)methane 50.0 U 30.4 29.1 60.8 58.2 1 33.0-184 4.37 54
Bis(2-chloroethyl)ether 50.0 U 32.6 29.9 65.2 59.8 1 12.0-158 8.64 108
2,2-oxybis(1-chloropropane)50.0 U 29.3 26.8 58.6 53.6 1 36.0-166 8.91 76
4-Bromophenyl-phenylether 50.0 U 32.7 30.2 65.4 60.4 1 53.0-127 7.95 43
2-Chloronaphthalene 50.0 U 32.0 30.9 64.0 61.8 1 60.0-120 3.50 24
4-Chlorophenyl-phenylether 50.0 U 32.4 29.9 64.8 59.8 1 25.0-158 8.03 61
Chrysene 50.0 U 30.7 29.5 61.4 59.0 1 17.0-168 3.99 87
Dibenz(a,h)anthracene 50.0 U 27.6 26.5 55.2 53.0 1 1.00-227 4.07 126
3,3-Dichlorobenzidine 100 U 66.8 60.9 66.8 60.9 1 1.00-262 9.24 108
2,4-Dinitrotoluene 50.0 U 34.0 31.2 68.0 62.4 1 39.0-139 8.59 42
2,6-Dinitrotoluene 50.0 U 33.3 30.5 66.6 61.0 1 50.0-158 8.78 48
Fluoranthene 50.0 U 29.1 27.1 58.2 54.2 1 26.0-137 7.12 66
Fluorene 50.0 U 32.1 29.7 64.2 59.4 1 59.0-121 7.77 38
Hexachlorobenzene 50.0 U 31.5 28.8 63.0 57.6 1 1.00-152 8.96 55
Hexachloro-1,3-butadiene 50.0 U 28.2 28.4 56.4 56.8 1 24.0-120 0.707 62
Hexachlorocyclopentadiene 50.0 U 20.2 19.4 40.4 38.8 1 10.0-146 4.04 34
Hexachloroethane 50.0 U 29.3 28.1 58.6 56.2 1 40.0-120 4.18 52
Indeno(1,2,3-cd)pyrene 50.0 U 27.5 26.3 55.0 52.6 1 1.00-171 4.46 99
Isophorone 50.0 U 29.4 27.4 58.8 54.8 1 21.0-196 7.04 93
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1561307
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1274449-09
L1274446-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274446-01 10/20/20 09:16 • (MS) R3583474-3 10/20/20 09:36 • (MSD) R3583474-4 10/20/20 09:57
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Naphthalene 50.0 U 27.4 26.5 54.8 53.0 1 21.0-133 3.34 65
Nitrobenzene 50.0 U 29.0 27.7 58.0 55.4 1 35.0-180 4.59 62
n-Nitrosodimethylamine 50.0 U 17.2 16.4 34.4 32.8 1 10.0-120 4.76 40
n-Nitrosodiphenylamine 50.0 U 32.6 29.8 65.2 59.6 1 16.0-160 8.97 28
n-Nitrosodi-n-propylamine 50.0 U 33.0 28.7 66.0 57.4 1 1.00-230 13.9 87
Phenanthrene 50.0 U 32.4 30.5 64.8 61.0 1 54.0-120 6.04 39
Benzylbutyl phthalate 50.0 U 40.6 36.9 81.2 73.8 1 1.00-152 9.55 60
Bis(2-ethylhexyl)phthalate 50.0 U 35.1 32.3 70.2 64.6 1 8.00-158 8.31 82
Di-n-butyl phthalate 50.0 U 32.5 30.1 65.0 60.2 1 1.00-120 7.67 47
Diethyl phthalate 50.0 U 32.4 29.8 64.8 59.6 1 1.00-120 8.36 100
Dimethyl phthalate 50.0 U 32.7 30.1 65.4 60.2 1 1.00-120 8.28 183
Di-n-octyl phthalate 50.0 U 31.5 29.7 63.0 59.4 1 4.00-146 5.88 69
Pyrene 50.0 U 35.5 33.1 71.0 66.2 1 52.0-120 7.00 49
1,2,4-Trichlorobenzene 50.0 U 28.1 27.7 56.2 55.4 1 44.0-142 1.43 50
4-Chloro-3-methylphenol 50.0 U 28.4 25.6 56.8 51.2 1 22.0-147 10.4 73
2-Chlorophenol 50.0 U 29.2 27.7 58.4 55.4 1 23.0-134 5.27 61
2,4-Dichlorophenol 50.0 U 29.6 28.4 59.2 56.8 1 39.0-135 4.14 50
2,4-Dimethylphenol 50.0 U 30.3 28.3 60.6 56.6 1 32.0-120 6.83 58
4,6-Dinitro-2-methylphenol 50.0 U 34.3 30.7 68.6 61.4 1 1.00-181 11.1 203
2,4-Dinitrophenol 50.0 U 32.9 27.4 65.8 54.8 1 1.00-191 18.2 132
2-Nitrophenol 50.0 U 31.5 30.1 63.0 60.2 1 29.0-182 4.55 55
4-Nitrophenol 50.0 U 12.8 12.4 25.6 24.8 1 1.00-132 3.17 131
Pentachlorophenol 50.0 U 28.5 25.0 57.0 50.0 1 14.0-176 13.1 86
Phenol 50.0 U 12.5 12.7 25.0 25.4 1 5.00-120 1.59 64
2,4,6-Trichlorophenol 50.0 U 33.7 30.8 67.4 61.6 1 37.0-144 8.99 58
(S) Nitrobenzene-d5 50.2 47.5 15.0-314
(S) 2-Fluorobiphenyl 64.4 59.7 22.0-127
(S) p-Terphenyl-d14 68.3 62.0 29.0-141
(S) Phenol-d5 24.6 24.9 8.00-424
(S) 2-Fluorophenol 37.4 38.5 10.0-120
(S) 2,4,6-Tribromophenol 64.5 57.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563259
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1274449-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3584772-2 10/23/20 01:03
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Acenaphthene U 5.39 33.3
Acenaphthylene U 4.69 33.3
Acetophenone U 10.4 333
Anthracene U 5.93 33.3
Atrazine U 11.5 333
Benzaldehyde U 17.7 333
Benzo(a)anthracene U 5.87 33.3
Benzo(b)fluoranthene U 6.21 33.3
Benzo(k)fluoranthene U 5.92 33.3
Benzo(g,h,i)perylene U 6.09 33.3
Benzo(a)pyrene U 6.19 33.3
Biphenyl U 10.6 333
Bis(2-chlorethoxy)methane U 10.0 333
Bis(2-chloroethyl)ether U 11.0 333
2,2-Oxybis(1-Chloropropane)U 14.4 333
4-Bromophenyl-phenylether U 11.7 333
Caprolactam U 16.5 333
Carbazole U 10.3 333
4-Chloroaniline U 12.0 333
2-Chloronaphthalene U 5.85 33.3
4-Chlorophenyl-phenylether U 11.6 333
Chrysene U 6.62 33.3
Dibenz(a,h)anthracene U 9.23 33.3
Dibenzofuran U 10.9 333
3,3-Dichlorobenzidine U 12.3 333
2,4-Dinitrotoluene U 9.55 333
2,6-Dinitrotoluene U 10.9 333
Fluoranthene U 6.01 33.3
Fluorene U 5.42 33.3
Hexachlorobenzene U 11.8 333
Hexachloro-1,3-butadiene U 11.2 333
Hexachlorocyclopentadiene U 17.5 333
Hexachloroethane U 13.1 333
Indeno(1,2,3-cd)pyrene U 9.41 33.3
Isophorone U 10.2 333
2-Methylnaphthalene U 4.32 33.3
Naphthalene U 8.36 33.3
2-Nitroaniline U 10.7 333
3-Nitroaniline U 10.6 333
4-Nitroaniline U 9.71 333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563259
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1274449-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3584772-2 10/23/20 01:03
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Nitrobenzene U 11.6 333
n-Nitrosodiphenylamine U 25.2 333
n-Nitrosodi-n-propylamine U 11.1 333
Phenanthrene U 6.61 33.3
Benzylbutyl phthalate U 10.4 333
Bis(2-ethylhexyl)phthalate U 42.2 333
Di-n-butyl phthalate U 11.4 333
Diethyl phthalate U 11.0 333
Dimethyl phthalate U 70.6 333
Di-n-octyl phthalate U 22.5 333
Pyrene U 6.48 33.3
4-Chloro-3-methylphenol U 10.8 333
2-Chlorophenol U 11.0 333
2-Methylphenol U 10.0 333
3&4-Methyl Phenol U 10.4 333
2,4-Dichlorophenol U 9.70 333
2,4-Dimethylphenol U 8.70 333
4,6-Dinitro-2-methylphenol U 75.5 333
2,4-Dinitrophenol U 77.9 333
2-Nitrophenol U 11.9 333
4-Nitrophenol U 10.4 333
Pentachlorophenol U 8.96 333
Phenol U 13.4 333
1,2,4,5-Tetrachlorobenzene U 15.9 333
2,4,5-Trichlorophenol U 11.3 333
2,4,6-Trichlorophenol U 10.7 333
2,3,4,6-Tetrachlorophenol U 12.6 333
(S) Nitrobenzene-d5 62.2 10.0-122
(S) 2-Fluorobiphenyl 70.9 15.0-120
(S) p-Terphenyl-d14 76.0 10.0-120
(S) Phenol-d5 71.8 10.0-120
(S) 2-Fluorophenol 78.2 12.0-120
(S) 2,4,6-Tribromophenol 84.4 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563259
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1274449-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS)
(LCS) R3584772-1 10/23/20 00:43
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
Acenaphthene 666 457 68.6 38.0-120
Acenaphthylene 666 492 73.9 40.0-120
Acetophenone 666 517 77.6 29.0-120
Anthracene 666 489 73.4 42.0-120
Atrazine 666 532 79.9 43.0-120
Benzaldehyde 666 273 41.0 10.0-160
Benzo(a)anthracene 666 538 80.8 44.0-120
Benzo(b)fluoranthene 666 514 77.2 43.0-120
Benzo(k)fluoranthene 666 548 82.3 44.0-120
Benzo(g,h,i)perylene 666 470 70.6 43.0-120
Benzo(a)pyrene 666 564 84.7 45.0-120
Biphenyl 666 472 70.9 39.0-120
Bis(2-chlorethoxy)methane 666 387 58.1 20.0-120
Bis(2-chloroethyl)ether 666 526 79.0 16.0-120
2,2-Oxybis(1-Chloropropane)666 450 67.6 23.0-120
4-Bromophenyl-phenylether 666 514 77.2 40.0-120
Caprolactam 666 660 99.1 38.0-120
Carbazole 666 494 74.2 48.0-120
4-Chloroaniline 666 317 47.6 18.0-120
2-Chloronaphthalene 666 478 71.8 35.0-120
4-Chlorophenyl-phenylether 666 502 75.4 40.0-120
Chrysene 666 504 75.7 43.0-120
Dibenz(a,h)anthracene 666 488 73.3 44.0-120
Dibenzofuran 666 491 73.7 44.0-120
3,3-Dichlorobenzidine 1330 888 66.8 28.0-120
2,4-Dinitrotoluene 666 532 79.9 45.0-120
2,6-Dinitrotoluene 666 509 76.4 42.0-120
Fluoranthene 666 509 76.4 44.0-120
Fluorene 666 495 74.3 41.0-120
Hexachlorobenzene 666 525 78.8 39.0-120
Hexachloro-1,3-butadiene 666 384 57.7 15.0-120
Hexachlorocyclopentadiene 666 443 66.5 15.0-120
Hexachloroethane 666 431 64.7 17.0-120
Indeno(1,2,3-cd)pyrene 666 487 73.1 45.0-120
Isophorone 666 378 56.8 23.0-120
2-Methylnaphthalene 666 385 57.8 34.0-120
Naphthalene 666 386 58.0 18.0-120
2-Nitroaniline 666 558 83.8 46.0-120
3-Nitroaniline 666 491 73.7 36.0-120
4-Nitroaniline 666 650 97.6 36.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563259
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1274449-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS)
(LCS) R3584772-1 10/23/20 00:43
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/kg ug/kg %%
Nitrobenzene 666 387 58.1 17.0-120
n-Nitrosodiphenylamine 666 478 71.8 40.0-120
n-Nitrosodi-n-propylamine 666 441 66.2 26.0-120
Phenanthrene 666 476 71.5 42.0-120
Benzylbutyl phthalate 666 535 80.3 40.0-120
Bis(2-ethylhexyl)phthalate 666 534 80.2 41.0-120
Di-n-butyl phthalate 666 497 74.6 43.0-120
Diethyl phthalate 666 494 74.2 43.0-120
Dimethyl phthalate 666 502 75.4 43.0-120
Di-n-octyl phthalate 666 530 79.6 40.0-120
Pyrene 666 498 74.8 41.0-120
4-Chloro-3-methylphenol 666 401 60.2 28.0-120
2-Chlorophenol 666 473 71.0 28.0-120
2-Methylphenol 666 472 70.9 35.0-120
3&4-Methyl Phenol 666 524 78.7 42.0-120
2,4-Dichlorophenol 666 403 60.5 25.0-120
2,4-Dimethylphenol 666 391 58.7 15.0-120
4,6-Dinitro-2-methylphenol 666 523 78.5 16.0-120
2,4-Dinitrophenol 666 421 63.2 10.0-120
2-Nitrophenol 666 457 68.6 20.0-120
4-Nitrophenol 666 535 80.3 27.0-120
Pentachlorophenol 666 531 79.7 29.0-120
Phenol 666 452 67.9 28.0-120
1,2,4,5-Tetrachlorobenzene 666 460 69.1 30.0-120
2,4,5-Trichlorophenol 666 477 71.6 38.0-120
2,4,6-Trichlorophenol 666 495 74.3 37.0-120
2,3,4,6-Tetrachlorophenol 666 540 81.1 39.0-120
(S) Nitrobenzene-d5 60.4 10.0-122
(S) 2-Fluorobiphenyl 71.8 15.0-120
(S) p-Terphenyl-d14 73.3 10.0-120
(S) Phenol-d5 71.2 10.0-120
(S) 2-Fluorophenol 76.1 12.0-120
(S) 2,4,6-Tribromophenol 90.8 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563259
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1274449-01,02,03,04,05,06,07,08
L1274449-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274449-01 10/23/20 05:06 • (MS) R3584772-3 10/23/20 05:27 • (MSD) R3584772-4 10/23/20 05:47
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
Acenaphthene 930 U 480 547 51.7 59.7 1 18.0-120 12.9 32
Acenaphthylene 930 U 514 589 55.3 64.4 1 25.0-120 13.6 32
Acetophenone 930 U 541 589 58.2 64.4 1 10.0-120 8.50 37
Anthracene 930 U 524 620 56.4 67.7 1 22.0-120 16.8 29
Atrazine 930 U 598 707 64.3 77.2 1 20.0-131 16.7 28
Benzaldehyde 930 U 766 817 82.4 89.2 1 10.0-160 6.43 40
Benzo(a)anthracene 930 U 550 658 59.1 71.9 1 25.0-120 18.0 29
Benzo(b)fluoranthene 930 U 543 640 58.4 69.9 1 19.0-122 16.5 31
Benzo(k)fluoranthene 930 U 555 658 59.7 71.9 1 23.0-120 17.0 30
Benzo(g,h,i)perylene 930 U 500 593 53.8 64.8 1 10.0-120 17.1 33
Benzo(a)pyrene 930 U 584 691 62.8 75.5 1 24.0-120 16.9 30
Biphenyl 930 U 495 562 53.2 61.4 1 15.0-120 12.8 33
Bis(2-chlorethoxy)methane 930 U 432 463 46.5 50.6 1 10.0-120 6.94 34
Bis(2-chloroethyl)ether 930 U 527 612 56.7 66.8 1 10.0-120 14.9 40
2,2-Oxybis(1-Chloropropane)930 U 458 499 49.2 54.5 1 10.0-120 8.57 40
4-Bromophenyl-phenylether 930 U 554 670 59.6 73.1 1 27.0-120 18.9 30
Caprolactam 930 U 675 837 72.6 91.4 1 11.0-141 21.3 31
Carbazole 930 U 514 627 55.3 68.5 1 31.0-120 19.8 24
4-Chloroaniline 930 U 326 387 35.1 42.3 1 10.0-120 17.0 36
2-Chloronaphthalene 930 U 512 564 55.0 61.6 1 20.0-120 9.72 32
4-Chlorophenyl-phenylether 930 U 544 623 58.5 68.1 1 24.0-120 13.6 29
Chrysene 930 U 514 612 55.3 66.8 1 21.0-120 17.3 29
Dibenz(a,h)anthracene 930 U 507 595 54.6 65.0 1 10.0-120 15.9 32
Dibenzofuran 930 U 520 599 55.9 65.4 1 24.0-120 14.1 30
3,3-Dichlorobenzidine 1870 U 762 1090 40.8 59.5 1 10.0-120 J3 35.8 34
2,4-Dinitrotoluene 930 U 569 673 61.2 73.5 1 30.0-120 16.6 31
2,6-Dinitrotoluene 930 U 544 654 58.5 71.5 1 25.0-120 18.4 31
Fluoranthene 930 U 550 663 59.1 72.4 1 18.0-126 18.6 32
Fluorene 930 U 527 615 56.7 67.1 1 25.0-120 15.3 30
Hexachlorobenzene 930 U 579 683 62.3 74.5 1 27.0-120 16.3 28
Hexachloro-1,3-butadiene 930 U 423 452 45.4 49.4 1 10.0-120 6.79 38
Hexachlorocyclopentadiene 930 U 418 462 45.0 50.5 1 10.0-120 9.95 40
Hexachloroethane 930 U 432 456 46.5 49.8 1 10.0-120 5.41 40
Indeno(1,2,3-cd)pyrene 930 U 517 616 55.6 67.3 1 10.0-120 17.5 32
Isophorone 930 U 423 452 45.4 49.4 1 13.0-120 6.79 34
2-Methylnaphthalene 930 U 424 462 45.6 50.5 1 10.0-120 8.61 37
Naphthalene 930 U 424 459 45.6 50.2 1 10.0-120 8.00 35
2-Nitroaniline 930 U 602 711 64.7 77.6 1 24.0-120 16.6 30
3-Nitroaniline 930 U 471 579 50.6 63.3 1 11.0-120 20.7 32
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1563259
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1274449-01,02,03,04,05,06,07,08
L1274449-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1274449-01 10/23/20 05:06 • (MS) R3584772-3 10/23/20 05:27 • (MSD) R3584772-4 10/23/20 05:47
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
4-Nitroaniline 930 U 579 729 62.3 79.6 1 15.0-120 22.9 31
Nitrobenzene 930 U 435 463 46.8 50.6 1 10.0-120 6.29 36
n-Nitrosodiphenylamine 930 U 478 589 51.4 64.4 1 17.0-120 20.9 29
n-Nitrosodi-n-propylamine 930 U 469 513 50.5 56.0 1 10.0-120 8.92 37
Phenanthrene 930 U 507 609 54.6 66.5 1 17.0-120 18.2 31
Benzylbutyl phthalate 930 U 561 657 60.3 71.8 1 23.0-120 15.8 30
Bis(2-ethylhexyl)phthalate 930 U 536 637 57.6 69.6 1 17.0-126 17.3 30
Di-n-butyl phthalate 930 U 519 625 55.8 68.2 1 30.0-120 18.5 29
Diethyl phthalate 930 U 513 608 55.2 66.4 1 26.0-120 16.9 28
Dimethyl phthalate 930 U 536 637 57.6 69.6 1 25.0-120 17.3 29
Di-n-octyl phthalate 930 U 550 657 59.1 71.8 1 21.0-123 17.8 29
Pyrene 930 U 506 610 54.4 66.7 1 16.0-121 18.7 32
4-Chloro-3-methylphenol 930 U 430 514 46.2 56.2 1 15.0-120 18.0 30
2-Chlorophenol 930 U 479 534 51.5 58.3 1 15.0-120 10.9 37
2-Methylphenol 930 U 476 561 51.2 61.3 1 11.0-120 16.3 40
3&4-Methyl Phenol 930 U 519 613 55.8 67.0 1 12.0-123 16.7 38
2,4-Dichlorophenol 930 U 444 497 47.7 54.3 1 20.0-120 11.4 31
2,4-Dimethylphenol 930 U 373 454 40.1 49.5 1 10.0-120 19.5 33
4,6-Dinitro-2-methylphenol 930 U 626 776 67.3 84.7 1 10.0-120 21.4 39
2,4-Dinitrophenol 930 U 586 746 63.1 81.5 1 10.0-121 24.0 40
2-Nitrophenol 930 U 519 564 55.8 61.6 1 12.0-120 8.36 39
4-Nitrophenol 930 U 591 732 63.5 79.9 1 10.0-137 21.4 32
Pentachlorophenol 930 U 568 733 61.1 80.1 1 10.0-160 25.4 31
Phenol 930 U 465 526 50.0 57.4 1 12.0-120 12.3 38
1,2,4,5-Tetrachlorobenzene 930 U 526 564 56.5 61.6 1 14.0-120 7.00 36
2,4,5-Trichlorophenol 930 U 503 623 54.1 68.1 1 20.0-120 21.3 30
2,4,6-Trichlorophenol 930 U 499 596 53.6 65.1 1 19.0-120 17.8 32
(S) Nitrobenzene-d5 48.3 42.3 10.0-122
(S) 2-Fluorobiphenyl 54.7 63.6 15.0-120
(S) p-Terphenyl-d14 53.8 67.0 10.0-120
(S) Phenol-d5 53.2 61.1 10.0-120
(S) 2-Fluorophenol 56.7 64.8 12.0-120
(S) 2,4,6-Tribromophenol 72.3 91.8 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RT Retention Time.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Data is likely to show a low bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J0 J0: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met method criteria.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Qualifier Description
N The analyte is tentatively identified and the associated numerical value may not be consistent with the actual
concentration present in the sample.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX B

Site Photographs

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
Excel Project No. 2020102

PHOTOGRAPH LOG
PHOTOGRAPH
NUMBER PHOTOGRAPH REVIEW AND COMMENTS
1 View looking at removed UST.
2 View looking at removed UST
3 View at UST excavation – note groundwater.

Excel Project No. 2020102

Photograph Number 1

Photograph Number 2

Excel Project No. 2020102

Photograph Number 3

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
APPENDIX C
Waste Disposal Manifest