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HomeMy WebLinkAboutMO-27965_47256_CA_LSA_20201030_Phase I LSA PHASE I LIMITED SITE ASSESSMENT REPORT KWICK MART-MINT HILL 10308 ALBEMARLE ROAD CHARLOTTE, MECKLENBURG COUNTY NORTH CAROLINA INCIDENT NUMBER 47256 FACILITY ID NUMBER 00-0-034068 Prepared for: Mr. John Hendley Brewer-Hendley Oil Company, Inc. Post Office Box 769 Marshville, North Carolina 28103 Prepared by: Resolve Environmental Services, PLLC 500 Devonport Drive Matthews, North Carolina 28104 October 30, 2020 Laura Minor Project Manager i EXECUTIVE SUMMARY The Kwick Mart-Mint Hill is an underground storage tank (UST) site located at 10308 Albemarle Road in Charlotte, Mecklenburg County, North Carolina. A total of three (3) USTs (one 12,000-gallon gasoline UST, one 8,000-gallon gasoline UST and one (1) 4,000-gallon kerosene UST) have existed at the property since June 1994 to the present. The adjoining properties are commercial and residential. During a routine compliance inspection conducted by the North Carolina Department of Environmental Quality (NCDEQ) on August 27, 2019, the spill bucket at the 12,000-gallon regular gasoline UST was noted to need repair/replacement. A NCDEQ Notice of Violation dated August 28, 2019 requesting a Site Check was sent to Mr. John N. Hendley, Registered Agent, of Brewer-Hendley Oil Company, Inc. (BHOC) of Marshville, North Carolina. A soil sample was collected adjacent to the regular gasoline spill bucket on September 18, 2019. The sample was submitted for analyses for gasoline-range organics (GRO) by Method 8015C. TPH-GRO was not detected in the soil sample. Therefore, no further assessment was required. In May 2020, Resolve was contracted to perform a Phase II Environmental Site Assessment (ESA) at the site by BHOC. Four (4) temporary monitoring wells were installed at the site. Soil and ground water samples were collected from each sampling point. No detectable concentrations of TPH-GRO or diesel- range organics (DRO) were reported in the soil samples. A concentration of benzene that exceeded the maximum allowable concentration (MAC) was reported in one of the ground water samples (TMW-4). Based on the ground water quality violation, a UST-61 form dated September 10, 2020 was submitted to the NCDEQ. A Notice of Regulatory Requirements (NORR) dated September 15, 2020 was prepared by the NCDEQ which requested Limited Site Assessment (LSA) activities. Resolve supervised the installation of one (1) Type II monitoring well (MW-1) on September 16, 2020 in the former location of Phase II ESA sampling point TMW-4. The well was completed to a depth of 35 feet on September 18, 2020. With the exception of an estimated concentration of acetone in soil sample MW-1-5’, no other requested method constituents were reported in the collected soil samples. ii Concentrations of benzene, MTBE, EDB and lead that exceeded the MACs were reported in the ground water sample collected from MW-1. None of the concentrations exceeded the gross contamination levels (GCLs) nor 10 times the 2L ground water quality standards. In addition, detectable and/or estimated concentrations of other requested method constituents were reported in the ground water sample collected from MW-1; however, none of the concentrations exceeded the MACs. During the September 2020 receptor survey, a total of thirteen water supply wells (WSW-1 through WSW- 13) were identified within 1,500-feet of the source area. Four (4) potable wells (WSW-1, WSW-2, WSW- 5 and WSW-10) are located with 1,000 feet of the sources area. An additional potable well, WSW-13 is located approximately 1,200 feet from the source area. The remaining identified ells are presumed to be used for irrigation purposes only, since all of the corresponding properties are connected to municipal water. County water is available to all properties in the surrounding area of the site. No surface water body was identified with a 500-foot radius of the site. Azusa Grotto Lake is located approximately 1,300 feet to the southwest of the site and an unnamed tributary of Clear Creek is located approximately 1,300 feet east of the site. County water is available to all properties in the surrounding area of the site. Based on the receptor survey information and ground water quality data collected to date, the site meets the criteria for a high-risk classification. It should be noted that the detectable concentrations of identified compounds exceeding 2L and the distance to the nearest receptor (480 feet) make the potential for affecting the receptor at or above the EPA’s MCL extremely low. In addition, the presence of MTBE indicates that the release occurred prior to 2009. iii SITE INFORMATION 1. Site Identification: Date of Report: October 30, 2020 Facility ID No. 00-0-034068 Incident Number: 42756 Site Name: Kwick Mart-Mint Hill Site Street Address: 10308 Albemarle Road City: Charlotte Zip Code: 28227 County: Mecklenburg Description of Geographic Data Point: Calculated from top of the gasoline (regular) spill bucket Location Method: Online lat/long finder Latitude: 35.204020° N Longitude: 80.751270° W 2. Contacts Associated with Leaking UST System: UST Owner: Brewer-Hendley Oil Company, Inc. (Table 1) P.O. Box 769 Marshville, North Carolina 28103 (704) 233-2600 UST Operator: Kwick Mart Yohannes Inc. (Table 1) 10308 Albemarle Road Charlotte, North Carolina 28227 (704) 573-2615 Property Owner: Hendley Family LLC P.O. Box 769 Marshville, North Carolina 28103 Drilling Contractor: Geological Resources, Inc. 3502 Hayes Road Monroe, North Carolina 28110 (704) 6845-4010 Primary Consultant: Resolve Environmental Services, PLLC 500 Devonport Drive Matthews, North Carolina 28104 (704) 289-5881 Laboratory: SGS North America, Inc. 4405 Vineland Road, Suite C-15 Orlando, Florida 32811 (407) 425-6700 North Carolina Certification No. 573 3. Release Information Date Discovered: The release was discovered during Phase II ESA activities conducted on August 20, 2020 Estimated Quantity of Release: Undetermined Cause of Release: Damaged spill bucket Source of Release: 12,000-gallon gasoline UST iv UST Size and contents: (1) 12,000-gallon gasoline UST (1) 8,000-gallon gasoline UST (1) 4,000-gallon kerosene UST (Table 2) Certification: I, Terry D. Kennedy, a Licensed Geologist for Resolve Environmental Services, PLLC, do certify that the information contained in this report is correct and accurate to the best of my knowledge. Resolve Environmental Services, PLLC, is licensed to practice geology in North Carolina. The certification number of the corporation is C-416. v TABLE OF CONTENTS 1. RISK CHARACTERIZATION ....................................................................................... 1 2. RECEPTOR INFORMATION ........................................................................................ 3 3. SITE GEOLOGY AND HYDROGEOLOGY ................................................................ 5 4. SITE INVESTIGATION .................................................................................................. 5 5. CONCLUSIONS AND RECOMMENDATIONS .......................................................... 7 6. LIMITATIONS ................................................................................................................. 7 FIGURES Figure 1: Site Location Map Figure 2: Site Vicinity Map Figure 3: Site Map Figure 4: Soil Sample Location Map Figure 5: Ground Water Quality Map TABLES Table 1: UST Owner/Operator Information Table 2: UST System Information Table 3: Water Supply Well Owner Information Table 4: Adjacent Property Owner Information Table 5: Well Construction and Gauging Information Table 6: Summary of Ground Water Sample Analytical Results APPENDICES Appendix A: Well Construction Record and Subsurface Log Appendix B: Laboratory Analytical Report 1 1. RISK CHARACTERIZATION Limited Site Assessment Risk Classification and Land Use Form Part I – Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the release contaminated any water supply well including any well used for non-drinking purposes? NO 2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release? YES 3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of the release? NO 4. Does ground water within 500 feet of the source area of the release have the potential for future use (there is no other source of water supply other than the groundwater)? NO Potable wells are located within 100 feet of the source area. However, public water is available to the site and surrounding properties. 5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment? NO 6. Are there any other factors that would cause the release to pose an imminent danger to public health, public safety, or the environment? NO If YES, explain: Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the release? NO No surface water bodies were identified within a 500-foot radius of the site. If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? NA 8. Is the source area of the release located within an approved or planned wellhead protection area as defined in 42 USC 300h-7(e)? NO 9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology of North Carolina” published by the Department in 1985? NO If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of 2 drinking water? 10. Do the levels of ground water contamination for any contaminant exceed the gross contamination levels established by the Department? NO Part II - Land Use Property Containing Source Area of Release The questions below pertain to the property containing the source area of the release. 1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO Explain: The subject property contains a petroleum retail facility/convenience store. 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? NO Explain: The subject property contains a petroleum retail facility. 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? YES Explain: The subject property contains a petroleum retail facility/convenience store. 4. Do children visit the property? YES Explain: The subject property contains a petroleum retail facility and children visit the property. 6. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? NO Explain: The property is easily accessible to pedestrian and vehicular traffic. 7. Do pavement, buildings, or other structures cap the contaminated soil? YES Explain: The UST basin and dispenser areas are capped with asphalt or concrete. If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future? The site use is expected to remain the same for the foreseeable future. 7. What is the zoning status of the property? According to the City of Charlotte, the property is zoned General Business. 3 8. Is the use of the property likely to change in the next 20 years? NO Explain: Property Surrounding Source Area of Release The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing source area of the release): 9. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)? A mobile home park is located on the adjacent property to the east with the closest trailer being approximately 325’ east/southeast from the source area. 11. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? Wilson Grove Baptist Church is located approximately 960 feet south of the source area. 12. What is the zoning status of properties in the surrounding area? According to the City of Charlotte, the area surrounding the site to the east, west and south is zoned Business and the area to the north is zoned Industrial. 13. Briefly characterize the use and activities of the land in the surrounding area. Used auto lots are located across Wilgrove Mint Hill Road to the west and across Albemarle Road, north of the site. A medical office and mobile home park is located to the south and west of the site, respectively. 2. RECEPTOR INFORMATION 1. Water Supply Wells: Thirteen (13) water supply wells (WSW-1 through WSW-13) were identified within a 1,500-foot radius of the subject site. Four potable water supply wells (WSW-1, WSW-2, WSW-5 and WSW- 4 10) were identified within 1,000 feet of the source area. Potable well, WSW-13, was identified within 1,200 feet of the source area. The remaining identified wells are presumed to be used for irrigation purposes only, since the corresponding properties are connected to municipal water. A site location map is provided as Figure 1 and a Site Vicinity Map showing property boundaries for the site and surrounding properties have been included as Figure 2. Water supply well owner information is summarized in Table 3. Water supply well usage questionnaires dated October 22, 2020 were mailed to all property owners located within 500-feet of the source area. The questionnaires will be forwarded to the NCDEQ incident manager upon receipt. Please note that addresses tied to each parcel that a water supply well was identified to be present were verified of either having active water accounts with the City of Charlotte or alternatively, not possessing active water accounts with the City of Charlotte by Resolve personnel on October 27, 2020. 2. Public Water Supplies: Are public water supplies available within 1,500 feet of the source area of the release? YES If yes, where is the location of the nearest public water lines and the source(s) of the public water supply. Explain: Municipal water is available to the site and the surrounding properties. Water lines run parallel to Albemarle Road and Wilgrove Mint Hill Road, north and west of the onsite structure, respectively. 3. Surface Water: Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the source area of the release. This information must be shown on the USGS topographic map. Azusa Grotto Lake is located approximately 1,300 feet southwest of the source area. An unnamed tributary of Clear Creek is located approximately 1,300 feet east of the source area. 4. Wellhead Protection Areas: Identify all planned or approved wellhead protection areas in the vicinity of the source area. This information must be shown on the USGS topographic map. Wellhead protection areas are defined in 42 USC 300h-7(e). On October 24, 2020, Resolve personnel accessed the North Carolina Department of Environmental Quality (NCDEQ) Source Water Assessment and Protection (SWAP) Program’s website to identify wellhead protection areas in the vicinity of the subject site. There were no designated wellhead protection areas near the subject site. 5 5. Deep Aquifers in the Coastal Plain Physiographic Region: The site is not located in the Coastal Plan Physiographic Region. 6. Subsurface Structures: No structures with basements were observed in the vicinity of the source area. Utilities in the area do not appear to intersect the seasonal high water table. 7. Property Owners and Occupants: The names and addresses of the owners of properties adjacent to the site are presented in Table 4. Property boundaries are shown on Figure 2. 3. SITE GEOLOGY AND HYDROGEOLOGY According to the 1985 Geologic Map of North Carolina, the site is located in the Charlotte Belt of metamorphic rocks. The underlying rock consists of interbedded felsic to mafic tuffs and flowrock. Ground water in the area moves through fractures and cleavage planes within the metamorphic rock. Red clayey silt was encountered during the borehole drilling for MW-1. Water was encountered during the installation of MW-1 at a depth of approximately 21 feet and the well was set to a total depth of 35 feet BGS with a 20-foot section of screen. Copies of the well construction record and subsurface log have been included as Appendix A. A Site Map is included as Figure 3. Well construction and gauging information is presented in Table 5. 4. SITE INVESTIGATION Following the identification of a faulty spill bucket at the 12,000-gallon gasoline tank during a routine compliance inspection conducted by NCDEQ on August 27, 2019, Resolve conducted site check activities in September 2019. A soil sample was collected near the 12,000-gallon gasoline spill bucket on September 18, 2019. TPH-GRO was not detected in the soil sample. Per BHOC’s request, Resolve conducted a Phase II ESA at the site in May 2020. Four (4) temporary monitoring wells (TMW-1 through TMW-4) were installed at the site on August 20, 2020. Soil and ground water samples were collected from each sampling point. No detectable concentrations of TPH-GRO or TPH-DRO were reported in the soil samples. A concentration of benzene that exceeded the MAC was reported in one of the ground water samples (TMW- 4). Based on the ground water quality violation, a UST-61 form dated September 10, 2020 was submitted to the NCDEQ. 6 A Notice of Regulatory Requirements (NORR) dated September 15, 2020 was prepared by the NCDEQ which requested Limited Site Assessment (LSA) activities. Resolve supervised the installation of one (1) Type II monitoring well (MW-1) beginning on September 16, 2020. MW-1 was initially installed to a total depth of 25 feet and completed with a 10-foot screened interval set to bracket the water table at the time of installation. However, due to lack of water, MW-1 was re-installed on September 18, 2020 to a total depth of 35 feet and completed with a 20-foot screened interval set to bracket the water table. MW-1 was installed in the former location of the Phase II ESA sampling point, TMW-4. 1. Soil Sampling: On September 16, 2020, three (3) soil samples (MW-1-5’, MW-1-10’ and MW-1-15’) were collected during the initial installation of monitoring well MW-1 on September 16, 2020. The soil samples were submitted for laboratory analyses of volatile organic compounds (VOCs) by SW846 Method 8260B and for volatile petroleum hydrocarbons (VPH) using the MADEP Method. With the exception of an estimated concentration of acetone in MW-1-5’, no other detectable concentrations of requested method constituents were reported in the soil samples. The concentration of acetone did not exceed the soil-to-ground water maximum contaminant concentration (MCC). A Soil Sample Location Map has been included as Figure 4. 2. Ground Water Sampling: On September 22, 2020, a ground water sample was collected from MW-1 and submitted for laboratory analyses of VOCs by EPA Method 6200B, VPH by the MADEP Method, EDB by Method 504.1 and lead. Concentrations of benzene, MTBE, EDB and lead that exceeded the MACs were reported in the ground water sample collected from MW-1. None of the concentrations exceeded the GCLs. In addition, detectable and/or estimated concentrations of other requested method constituents were reported in the ground water sample collected from MW-1; however, none of the concentrations exceeded the MACs nor 10 times the 2L ground water quality standards. A summary of ground water sample analytical results is presented in Table 6. A Ground Water Quality Map is included as Figure 5. A copy of the laboratory analytical report is presented as Appendix B. 3. Quality Control: The soil and ground water samples were immediately placed in laboratory-supplied containers, which were then placed in iced coolers. New disposable bailers were used to sample the monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples were logged using 7 proper chain-of-custody procedures. The samples were transported to a North Carolina certified laboratory for analysis. 5. CONCLUSIONS AND RECOMMENDATIONS  The site contains a petroleum retail facility/convenience store. Land use in the area primarily consists of commercial properties mixed with residential properties.  During the September 2020 receptor survey, a total of thirteen (13) water supply wells (WSW-1 through WSW-13) were identified within 1,500-feet of the source area. One (1) potable well (WSW-1) is located approximately 480 feet of the release. Four (4) additional potable wells (WSW-2, WSW-5, WSW-10 and WSW-13) were identified between 700 feet and 1,200 feet from the source area. The remaining wells are presumed to be used for irrigation purposes only. County water is available to all properties in the surrounding area of the site.  Azusa Grotto Lake is located approximately 1,300 feet southwest of the source area. A stream is located approximately 1,300 feet east of the source area. Underground utilities in the source areas are not likely to intersect the water table.  An estimated concentration of acetone was reported in soil sample MW-1-5’ collected at the site; however, the concentration did not exceed the MCC. Concentrations of benzene, MTBE, EDB and lead that exceeded the MAC were reported in the ground water sample collected from MW-1. None of the concentrations exceeded the GCLs.  Based on this information, the site risk should be classified as high risk. It should be noted that the detectable concentrations of identified compounds exceeding 2L and the distance to the nearest receptor (480 feet) make the potential for affecting the receptor at or above the EPA’s MCL extremely low. In addition, the presence of MTBE indicates that the release occurred prior to 2009. 6. LIMITATIONS This report has been prepared for the exclusive use of Mr. John Hendley and Brewer-Hendley Oil Company, Inc. for specific application to the referenced site in Mecklenburg County, North Carolina. The assessment was conducted based on the scope of work and level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of geology and hydrogeology practices in the State of North Carolina, available information and our professional judgment. No other warranty is expressed or implied. 8 The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. FIGURES SITE LOCATIONFigure 1 Site LocationKwick Mart- Mint Hill10308 Albemarle Road Mint Hill, Mecklenburg County, NC Incident No. 47256Resolve Project No. 5209500 M2000 FTDate: 09/12/2020Location: 35.208904° N -80.669633 ° W Dad "J "J "J"J"J "J "J "J "J "J "J "J "J SITE 11116211 11116406 11116421 13707604 11116207 1111621010940215 10940209 13707613 10940210 10940208 1094020111116407 1 0 94 0 1 03 13707612 1370763713707605 10 94 01 06 1 0 94 01 04 WSW-9 WSW-8 WSW-7 WSW-6 WSW-5 WSW-4 WSW-3 WSW-2 WSW-1 WSW-13 WSW-12 WSW-11 WSW-10 Parkton RdAlbemarle Rd Hu n tle y Rd Wilgrove-Mint Hill RdPine Grove AvPleasant View Ln W ilson G rove R dCe d ar br oo k DrGrandview Ri dge DrAvery CtSilver Valley Dr Cedar Grove RdSpring Laurel DrOne Woodlake Ct Burkandt RdLake Leslie LnSpring Ridge LnPiney Creek Ct Sunway Dr Guice Crossing LnDoblinway DrFIGURE 2: SITE VICINITY MAPKWICK MART-MINT HILL10308 ALBEMARLE ROADCHARLOTTE, MECKLENBURG COUNTYNORTH CAROLINAINCIDENT NO. 42756 PREPARED BY:RESOLVE ENVIRONMENTAL SERVICES, PLLCSEPTEMBER 11, 2020 ³ 0 300150Feet1 inch = 300 feet 1,500-FOOT RADIUS 1,000-FOOT RADIUS 500-FOOT RADIUS 250-FOOT RADIUS LEGEND "J Water Supply Well Streets Creeks_Streams Lakes_Ponds Well Owners and Adjacent Properties Mecklenburg County, NC Parcels UnnamedTributaryofClearC reekAZUSAGROTTO LAKE RESOLVEENVIRONMENTALSERVICES, PLLCKWICK MART - MINT HILL10308 ALBERMARLE ROADMINT HILL, MECKLENBURG COUNTY, NCINCIDENT NO: 47256RESOLVE PROJECT NO. 5209FIGURE 3SITE MAP RESOLVEENVIRONMENTALSERVICES, PLLCKWICK MART - MINT HILL10308 ALBERMARLE ROADMINT HILL, MECKLENBURG COUNTY, NCINCIDENT NO: 47256RESOLVE PROJECT NO. 5209FIGURE 4SOIL SAMPLE LOCATION MAP RESOLVEENVIRONMENTALSERVICES, PLLCKWICK MART - MINT HILL10308 ALBERMARLE ROADMINT HILL, MECKLENBURG COUNTY, NCINCIDENT NO: 47256RESOLVE PROJECT NO. 5209FIGURE 5GROUND WATER QUALITY MAP TABLES UST ID Number 1 - 3 Facility ID Number Owner or Operator? Owner/Operator NA NA Name of Owner or Operator Dates of Ownership / Operation TABLE 1 UST OWNER/OPERATOR INFORMATION KWICK MART - MINT HILL 00-0-00000034068 Brewer Hendley Oil Company 6/1/1994 Address Telephone Number P.O. Box 769, Marshville, NC 28103 704.233.2600 INCIDENT NO. 47256 Page 1 of 1 Was Release Associated with UST System? (Yes / No) 1 Gasoline Gasoline 8,000 06/01/94 Single wall FRP 8' x 21' 4"Single wall FRP Current No 2 Gasoline Gasoline 12,000 06/01/94 Single wall FRP 8' x 32'Single wall FRP Current Yes 4 Kerosene Kerosene 4,000 06/01/94 Single wall FRP 64" x 24'Single wall FRP Current No Notes: • Data obtained from the NCDEQ registered tank database. • FRP: Fiberglass Reinforced Plastic. Construction Details Tank Dimensions Description of Associated Product Piping and Pumps Status of UST TABLE 2 UST SYSTEM INFORMATION KWICK MART - MINT HILL Date: 9/28/2020 Facility ID 0-00-0000034068 UST ID No. Current or Most Recent Contents Previous Contents Capacity (gallons) Date Installed INCIDENT NO. 47256 Page 1 of 1 Date 9/28/2020 Facility ID 00-0-0000034068 Well #Parcel ID Number Well Owner Well Location (Addresses Tied to Parcel)Phone Number Well Use Well Depth (ft BGS) Well Casing Depth (ft BGS) Well Screen Interval (x to y ft BGS) Distance from source area of release (ft.) and direction WSW-1 11116407 Terry J Wilson 10417 Albemarle Road Unknown Potable (No active City of CLT water account) Unknown Unknown Unknown 480 NE WSW-2 11116421 Steve R & Evelyn S Berrier 10522 Parkton Rd & 10510 Parkton Rd Unknown Potable (10522: no active City of CLT water account; 10510: active City of CLT water account) Unknown Unknown Unknown 700 NE WSW-3 11116211 Yohannes Tzeggai & Teclemariam Letehawariat 10335 Parkton Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 600 N/NE WSW-4 11116210 Maria M & Ioannis Fourtounis 10311 Parkton Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 575 N WSW-5 11116208 Joanne A & TR Craft 10303 Parkton Rd Unknown Potable (No active City of CLT water account) Unknown Unknown Unknown 680 NW WSW-6 10940208 Gene Eric Privette 6719 Huntley Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 650 SW WSW-7 10940209 Meldona T Gladden 6725 Huntley Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 635 SW 9820 Thornridge Dr Indian Trail NC 28079 TABLE 3 WATER SUPPLY WELL OWNER INFORMATION KWICK MART - MINT HILL INCIDENT NO. 47256 Mailing Address 8513 Rolling Fields Rd Charlotte NC 28227 Wells Within 500' Wells Within 1,000' 2022 Tanfield Dr Matthews NC 28104 4716 Dawnwood Dr Charlotte NC 28212 6023 Wilgrove Mint Hill Rd Charlotte NC 28227 7017 Indian Trail Fairview Rd Indian Trail NC 28079 6416 Oak Hill Rd Charlotte NC 28227 Date 9/28/2020 Facility ID 00-0-0000034068 Well #Parcel ID Number Well Owner Well Location (Addresses Tied to Parcel)Phone Number Well Use Well Depth (ft BGS) Well Casing Depth (ft BGS) Well Screen Interval (x to y ft BGS) Distance from source area of release (ft.) and direction TABLE 3 WATER SUPPLY WELL OWNER INFORMATION KWICK MART - MINT HILL INCIDENT NO. 47256 Mailing Address WSW-8 10940210 Joyce M & William Lee Gladden 6811 Huntley Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 775 S/SW WSW-9 10940106 William Lee Gladden 6814 Huntley Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 900 SW WSW-10 13707612 Ted Douglas Harkey & Marcia Mauney 6708 Wilgrove Mint Hill Rd Unknown Potable (No active City of CLT water account) Unknown Unknown Unknown 750 S WSW-11 13707613 Wilson Grove Baptist Church 6700 Wilgrove Mint Hill Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 875 S/SE WSW-12 10940104 Joyce M & William Lee Gladden 6822 Huntley Rd Unknown Irrigation (active City of CLT water account) Unknown Unknown Unknown 1,080 SW WSW-13 10940103 Joyce M & William Lee Gladden 7731 Wilgrove Mint Hill Rd Unknown Potable: No active City of CLT water account) Unknown Unknown Unknown 1,200 SW Notes: 1. Owner information current as of 9/28/2020 and obtained via Mecklenburg County NC GIS website: http://polaris3g.mecklenburgcountync.gov/. 2. City of Charlotte water department information current as of October 27, 2020. 6811 Huntley Rd Charlotte NC 28227 6811 Huntley Rd Charlotte NC 28227 Wells Within 1,500' 6811 Huntley Rd Charlotte NC 28227 6811 Huntley Rd Charlotte NC 28227 11055 Flowes Store Rd Midland NC 28107 6624 Wilgrove Mint Hill Rd Charlotte NC 28227 Date: 9/28/2020 Facility ID 00-0-0000034068 13707605 (Site) & 13707637 Hendley Family LLC P.O. Box 769 Marshville NC 28103 10940201 Letha Joanne Craft & Billy Edward Arant 6023 Wilgrove Mint Hill Rd. Charlotte NC 28227 11116406A Robert S Furr Jr.P.O. Box 5647 Charlotte NC 28299 137070604 L&K Leasing LLC 6824 Wilgrove Mint Hill Rd. Charlotte NC 28227 Note: • Property information current as of September 28, 2020. Information obtained from Mecklenburg County NC GIS website: https://polaris3g.mecklenburgcountync.gov/. TABLE 4 ADJACENT PROPERTY OWNER INFORMATION KWICK MART - MINT HILL INCIDENT NO. 47256 Parcel ID Number Property Owner Property Owner Address Date:9/28/2020 Facility ID #: 00-0-0000034068 MW-1 9/18/2020 9/18/2020 15 15-35 35 NM 21.05 NA NM Notes: • ft BGS : feet below ground surface. • NA: Not available. • NM: Not measured. TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION KWICK MART - MINT HILL INCIDENT NO. 47256 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Comments Date: 10/05/20 EPA 504.1 SW846 6010D Well ID Date Collected (mm/dd/yy) 1 20 0.02 15 5,000 20,000 50 15,000 MW-1 09/22/20 8.8 41.5 0.10 137 Notes: • Results reported in micrograms per liter (µg/l). • < : Less than the method detection limit specified in the laboratory report. • 2L Standard specified in T15A NCAC 2L.0202. • GCL: Gross contamination level. • NE: Not Established. • Concentrations in bold face type exceeded the 2L standards. • Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established. GCL (µg/l) Contaminant of Concern BenzeneMethyl-tert-butyl ether(MTBE)1,2-Dibromoethane(EDB)Lead2L Standard (µg/l) TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS KWICK MART INCIDENT NO. 47256 Facility ID: 00-0-0000034068 Analytical Method SM 6200B Page 1 of 1 APPENDICES APPENDIX A Well Construction Record and Subsurface Log Resolve Environmental Services, PLLC Phone:(704) 289-5881 500 Devonport Drive Matthews, NC 28104 SUBSURFACE LOG Project Kwick Mart - Mint Hill Address 10308 Albemarle Road, Charlotte Boring Number MW-1 Date Drilled Sample Method Grab Drilling Method Auger Completion Details Well completed with 15 feet of dscreen set to bracket the water table. Driller S. Bowers Log By TDK Lab Sample OVA Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS 0 0-3" Asphalt 3"-35'Red clayey SILT 2 4 MW-1-5'4.5'-5'N/A 6 8 10 MW-1-10'9.5'-10'N/A 12 14 MW-1-15'14.5-15'N/A 16 18 20 22 24 26 28 30 32 34 TD 35' 36 38 40 9/16/20 & 9/18/20 APPENDIX B Laboratory Analytical Report 10/05/20 Technical Report for Resolve Environmental Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC SGS Job Number: FA79064 Sampling Dates: 09/16/20 - 09/22/20 Report to: Resolve Environmental 500 Devonport Dr Matthews, NC 28104 resolve@carolina.rr.com ATTN: Laura Minor Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 10/05/20 e-Hardcopy 2.0 Automated Report 91 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 91 FA79064 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................5 3.1: FA79064-1: MW-1-5' ....................................................................................................6 3.2: FA79064-2: MW-1-10' ..................................................................................................14 3.3: FA79064-3: MW-1-15' ..................................................................................................16 3.4: FA79064-4: MW-1 ........................................................................................................24 Section 4: Misc. Forms ............................................................................................................33 4.1: Chain of Custody ...........................................................................................................34 Section 5: MS Volatiles - QC Data Summaries .....................................................................36 5.1: Method Blank Summary ................................................................................................37 5.2: Blank Spike Summary ...................................................................................................42 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................47 Section 6: MS Semi-volatiles - QC Data Summaries ............................................................52 6.1: Method Blank Summary ................................................................................................53 6.2: Blank Spike Summary ...................................................................................................58 6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................63 Section 7: GC Volatiles - QC Data Summaries .....................................................................65 7.1: Method Blank Summary ................................................................................................66 7.2: Blank Spike Summary ...................................................................................................69 7.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................70 7.4: Matrix Spike Summary ..................................................................................................72 7.5: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................74 7.6: Duplicate Summary .......................................................................................................75 Section 8: GC/LC Semi-volatiles - QC Data Summaries .....................................................77 8.1: Method Blank Summary ................................................................................................78 8.2: Blank Spike Summary ...................................................................................................80 8.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................82 8.4: Duplicate Summary .......................................................................................................84 Section 9: Metals Analysis - QC Data Summaries ................................................................85 9.1: Prep QC MP37857: Pb ..................................................................................................86 1234567892 of 91 FA79064 SGS North America Inc. Sample Summary Resolve Environmental Job No:FA79064 Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA79064-1 09/16/20 14:50 TK 09/23/20 SO Soil MW-1-5' FA79064-2 09/16/20 14:59 TK 09/23/20 SO Soil MW-1-10' FA79064-3 09/16/20 15:13 TK 09/23/20 SO Soil MW-1-15' FA79064-4 09/22/20 16:00 TK 09/23/20 AQ Ground Water MW-1 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 3 of 91 FA790641 Summary of Hits Page 1 of 1 Job Number:FA79064 Account:Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Collected:09/16/20 thru 09/22/20 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA79064-1 MW-1-5' Acetone a 0.172 J 0.26 0.13 mg/kg SW846 8260D FA79064-2 MW-1-10' No hits reported in this sample. FA79064-3 MW-1-15' No hits reported in this sample. FA79064-4 MW-1 Benzene 8.8 0.50 0.13 ug/l SM 6200B Di-Isopropyl Ether 0.33 J 0.50 0.13 ug/l SM 6200B Isopropylbenzene 0.23 J 0.50 0.13 ug/l SM 6200B Methyl Chloride 0.27 J 0.50 0.20 ug/l SM 6200B Methyl Tert Butyl Ether 41.5 0.50 0.13 ug/l SM 6200B Naphthalene 1.8 0.50 0.13 ug/l SM 6200B 1,2,4-Trimethylbenzene 1.3 0.50 0.13 ug/l SM 6200B o-Xylene 0.91 0.50 0.13 ug/l SM 6200B Naphthalene 0.94 J 4.8 0.48 ug/l EPA 625.1 Total TIC, Semi-Volatile 80.5 J ug/l 1,2-Dibromoethane b 0.10 0.019 0.0094 ug/l EPA 504.1 Benzene 7.6 1.0 1.0 ug/l MADEP VPH REV 2.1 Methyl Tert Butyl Ether 35.3 2.0 1.0 ug/l MADEP VPH REV 2.1 o-Xylene 1.0 J 2.0 1.0 ug/l MADEP VPH REV 2.1 C11-C22 Aromatics (Unadj.)84.7 J 190 77 ug/l MADEP EPH REV 2.1 C11-C22 Aromatics 84.7 J 190 77 ug/l MADEP EPH REV 2.1 Lead 137 5.0 ug/l SW846 6010D (a) Results reported from bisulfate-preserved sample. Internal standard response(s) outside method criteria due to sample matrix interference; associated analyte(s) ND. (b) All hits confirmed by dual column analysis. 4 of 91 FA790642 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 5 of 91 FA790643 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8260D Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a 2B14726.D 1 09/23/20 17:47 SP n/a n/a V2B585 Run #2 Initial Weight Final Volume Run #1 4.84 g 5.0 ml Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.172 0.26 0.13 mg/kg J 71-43-2 Benzene ND 0.0066 0.0016 mg/kg 108-86-1 Bromobenzene ND 0.0066 0.0013 mg/kg 74-97-5 Bromochloromethane ND 0.0066 0.0019 mg/kg 75-27-4 Bromodichloromethane b ND 0.0066 0.0013 mg/kg 75-25-2 Bromoform ND 0.0066 0.0013 mg/kg 78-93-3 2-Butanone (MEK)ND 0.033 0.0096 mg/kg 104-51-8 n-Butylbenzene ND 0.0066 0.0013 mg/kg 135-98-8 sec-Butylbenzene ND 0.0066 0.0013 mg/kg 98-06-6 tert-Butylbenzene ND 0.0066 0.0013 mg/kg 56-23-5 Carbon Tetrachloride ND 0.0066 0.0013 mg/kg 108-90-7 Chlorobenzene ND 0.0066 0.0013 mg/kg 75-00-3 Chloroethane c ND 0.0066 0.0026 mg/kg 67-66-3 Chloroform ND 0.0066 0.0018 mg/kg 95-49-8 o-Chlorotoluene ND 0.0066 0.0013 mg/kg 106-43-4 p-Chlorotoluene ND 0.0066 0.0013 mg/kg 124-48-1 Dibromochloromethane ND 0.0066 0.0013 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0066 0.0013 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0066 0.0026 mg/kg 95-50-1 1,2-Dichlorobenzene ND 0.0066 0.0013 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.0066 0.0013 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.0066 0.0015 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0066 0.0023 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0066 0.0013 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0066 0.0013 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0066 0.0018 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0066 0.0013 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0066 0.0013 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0066 0.0013 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0066 0.0013 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0066 0.0013 mg/kg 10061-01-5 cis-1,3-Dichloropropene b ND 0.0066 0.0013 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8260D Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0066 0.0013 mg/kg 108-20-3 Di-Isopropyl Ether ND 0.0066 0.0031 mg/kg 64-17-5 Ethyl Alcohol d ND 0.53 0.099 mg/kg 100-41-4 Ethylbenzene ND 0.0066 0.0013 mg/kg 591-78-6 2-Hexanone ND 0.033 0.0099 mg/kg 98-82-8 Isopropylbenzene ND 0.0066 0.0013 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0066 0.0013 mg/kg 74-83-9 Methyl Bromide ND 0.0066 0.0026 mg/kg 74-87-3 Methyl Chloride ND 0.0066 0.0026 mg/kg 75-09-2 Methylene Chloride b ND 0.026 0.014 mg/kg 108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.033 0.0099 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0066 0.0013 mg/kg 91-20-3 Naphthalene ND 0.0066 0.0026 mg/kg 103-65-1 n-Propylbenzene ND 0.0066 0.0013 mg/kg 100-42-5 Styrene ND 0.0066 0.0013 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0066 0.0014 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0066 0.0013 mg/kg 127-18-4 Tetrachloroethylene ND 0.0066 0.0017 mg/kg 108-88-3 Toluene ND 0.026 0.013 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0066 0.0018 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0066 0.0013 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0066 0.0013 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0066 0.0013 mg/kg 79-01-6 Trichloroethylene ND 0.0066 0.0013 mg/kg 75-69-4 Trichlorofluoromethane b ND 0.0066 0.0026 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0066 0.0016 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0066 0.0013 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0066 0.0013 mg/kg 108-05-4 Vinyl Acetate ND 0.033 0.022 mg/kg 75-01-4 Vinyl Chloride ND 0.0066 0.0013 mg/kg m,p-Xylene ND 0.013 0.0014 mg/kg 95-47-6 o-Xylene ND 0.0066 0.0013 mg/kg 1330-20-7 Xylene (total)ND 0.020 0.0028 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 105%75-124% 17060-07-0 1,2-Dichloroethane-D4 113%72-135% 2037-26-5 Toluene-D8 94%75-126% 460-00-4 4-Bromofluorobenzene 96%71-133% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8260D Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Results reported from bisulfate-preserved sample. Internal standard response(s) outside method criteria due to sample matrix interference; associated analyte(s) ND. (b) Associated CCV outside of control limits high, sample was ND. (c) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits high, sample was ND. (d) Associated internal standard response outside method criteria due to sample matrix interference; however, analyte is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8270D SW846 3550C Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 9I009877.D 1 09/25/20 18:59 MV 09/24/20 08:10 OP82150 S9I359 Run #2 Initial Weight Final Volume Run #1 30.2 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 1.1 0.21 mg/kg 59-50-7 4-Chloro-3-methyl Phenol ND 0.21 0.024 mg/kg 95-57-8 2-Chlorophenol ND 0.21 0.026 mg/kg 120-83-2 2,4-Dichlorophenol ND 0.21 0.024 mg/kg 105-67-9 2,4-Dimethylphenol ND 0.21 0.056 mg/kg 51-28-5 2,4-Dinitrophenol ND 1.1 0.21 mg/kg 534-52-1 4,6-Dinitro-o-cresol ND 0.42 0.084 mg/kg 95-48-7 2-Methylphenol ND 0.21 0.025 mg/kg 3&4-Methylphenol ND 0.21 0.035 mg/kg 88-75-5 2-Nitrophenol ND 0.21 0.023 mg/kg 100-02-7 4-Nitrophenol ND 1.1 0.21 mg/kg 87-86-5 Pentachlorophenol ND 1.1 0.21 mg/kg 108-95-2 Phenol ND 0.21 0.021 mg/kg 88-06-2 2,4,6-Trichlorophenol ND 0.21 0.024 mg/kg 83-32-9 Acenaphthene ND 0.21 0.022 mg/kg 208-96-8 Acenaphthylene ND 0.21 0.021 mg/kg 120-12-7 Anthracene ND 0.21 0.024 mg/kg 56-55-3 Benzo(a)anthracene ND 0.21 0.021 mg/kg 50-32-8 Benzo(a)pyrene ND 0.21 0.025 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.21 0.023 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.21 0.022 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.21 0.028 mg/kg 100-51-6 Benzyl Alcohol ND 0.21 0.021 mg/kg 101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.022 mg/kg 85-68-7 Butyl benzyl phthalate ND 0.21 0.042 mg/kg 106-47-8 4-Chloroaniline ND 0.21 0.053 mg/kg 111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg 111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.024 mg/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.21 0.027 mg/kg 91-58-7 2-Chloronaphthalene ND 0.21 0.021 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.021 mg/kg 218-01-9 Chrysene ND 0.21 0.022 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8270D SW846 3550C Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 53-70-3 Dibenzo(a,h)anthracene a ND 0.21 0.026 mg/kg 132-64-9 Dibenzofuran ND 0.21 0.021 mg/kg 95-50-1 1,2-Dichlorobenzene ND 0.21 0.021 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.21 0.023 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.21 0.028 mg/kg 91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.050 mg/kg 84-66-2 Diethyl Phthalate ND 0.42 0.042 mg/kg 131-11-3 Dimethyl Phthalate ND 0.21 0.042 mg/kg 117-84-0 Di-n-octyl Phthalate ND 0.21 0.042 mg/kg 84-74-2 Di-n-butyl Phthalate ND 0.42 0.084 mg/kg 122-66-7 1,2-Diphenylhydrazine ND 0.21 0.021 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 0.42 0.042 mg/kg 206-44-0 Fluoranthene ND 0.21 0.021 mg/kg 86-73-7 Fluorene ND 0.21 0.023 mg/kg 118-74-1 Hexachlorobenzene ND 0.21 0.021 mg/kg 87-68-3 Hexachlorobutadiene ND 0.21 0.021 mg/kg 77-47-4 Hexachlorocyclopentadiene ND 0.21 0.042 mg/kg 67-72-1 Hexachloroethane ND 0.21 0.025 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene a ND 0.21 0.026 mg/kg 78-59-1 Isophorone ND 0.21 0.021 mg/kg 90-12-0 1-Methylnaphthalene ND 0.21 0.021 mg/kg 91-57-6 2-Methylnaphthalene b ND 0.21 0.021 mg/kg 91-20-3 Naphthalene ND 0.21 0.021 mg/kg 98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg 621-64-7 N-Nitrosodi-n-propylamine ND 0.21 0.021 mg/kg 86-30-6 N-Nitrosodiphenylamine a ND 0.21 0.023 mg/kg 85-01-8 Phenanthrene ND 0.21 0.021 mg/kg 129-00-0 Pyrene ND 0.21 0.024 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.21 0.025 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 54%40-102% 4165-62-2 Phenol-d5 62%41-100% 118-79-6 2,4,6-Tribromophenol 73%42-108% 4165-60-0 Nitrobenzene-d5 61%40-105% 321-60-8 2-Fluorobiphenyl 65%43-107% 1718-51-0 Terphenyl-d14 74%45-119% (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8270D SW846 3550C Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:MADEP VPH REV 2.1 Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1S3762.D 1 09/30/20 14:41 EG n/a n/a G1S87 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.99 g 5.0 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.067 0.067 mg/kg 100-41-4 Ethylbenzene ND 0.13 0.067 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.13 0.067 mg/kg 91-20-3 Naphthalene ND 0.33 0.20 mg/kg 108-88-3 Toluene ND 0.13 0.067 mg/kg m,p-Xylene ND 0.27 0.13 mg/kg 95-47-6 o-Xylene ND 0.13 0.067 mg/kg C5- C8 Aliphatics (Unadj.)ND 6.7 2.3 mg/kg C9- C12 Aliphatics (Unadj.)ND 6.7 2.3 mg/kg C9- C10 Aromatics (Unadj.)ND 6.7 2.3 mg/kg C5- C8 Aliphatics ND 6.7 2.3 mg/kg C9- C12 Aliphatics ND 6.7 2.3 mg/kg C9- C10 Aromatics ND 6.7 2.3 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 88%70-130% 460-00-4 BFB 92%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1-5' Lab Sample ID:FA79064-1 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:78.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN029976.D 1 09/30/20 14:24 JA 09/25/20 08:15 OP82169 GNN1466 Run #2 Initial Weight Final Volume Run #1 19.7 g 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 0.26 0.13 mg/kg 208-96-8 Acenaphthylene ND 0.26 0.13 mg/kg 120-12-7 Anthracene ND 0.26 0.13 mg/kg 56-55-3 Benzo(a)anthracene ND 0.26 0.13 mg/kg 50-32-8 Benzo(a)pyrene ND 0.26 0.13 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.26 0.13 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.26 0.13 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.26 0.13 mg/kg 218-01-9 Chrysene ND 0.26 0.13 mg/kg 53-70-3 Dibenzo(a,h)anthracene a ND 0.26 0.13 mg/kg 206-44-0 Fluoranthene ND 0.26 0.13 mg/kg 86-73-7 Fluorene ND 0.26 0.13 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.26 0.13 mg/kg 91-57-6 2-Methylnaphthalene ND 0.26 0.13 mg/kg 91-20-3 Naphthalene ND 0.26 0.13 mg/kg 85-01-8 Phenanthrene ND 0.26 0.13 mg/kg 129-00-0 Pyrene ND 0.26 0.13 mg/kg C11-C22 Aromatics (Unadj.)ND 13 5.2 mg/kg C11-C22 Aromatics ND 13 5.2 mg/kg C9-C18 Aliphatics ND 13 3.2 mg/kg C19-C36 Aliphatics ND 13 3.2 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 66%40-140% 580-13-2 2-Bromonaphthalene 61%40-140% 84-15-1 o-Terphenyl 54%40-140% 321-60-8 2-Fluorobiphenyl 58%40-140% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 91 FA7906433.1 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1-10' Lab Sample ID:FA79064-2 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:MADEP VPH REV 2.1 Percent Solids:74.4 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1S3747.D 1 09/30/20 07:27 EG n/a n/a G1S87 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.02 g 5.0 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.10 0.10 mg/kg 100-41-4 Ethylbenzene ND 0.20 0.10 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.10 mg/kg 91-20-3 Naphthalene ND 0.50 0.30 mg/kg 108-88-3 Toluene ND 0.20 0.10 mg/kg m,p-Xylene ND 0.40 0.20 mg/kg 95-47-6 o-Xylene ND 0.20 0.10 mg/kg C5- C8 Aliphatics (Unadj.)ND 10 3.5 mg/kg C9- C12 Aliphatics (Unadj.)ND 10 3.5 mg/kg C9- C10 Aromatics (Unadj.)ND 10 3.5 mg/kg C5- C8 Aliphatics ND 10 3.5 mg/kg C9- C12 Aliphatics ND 10 3.5 mg/kg C9- C10 Aromatics ND 10 3.5 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 90%70-130% 460-00-4 BFB 92%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 14 of 91 FA7906433.2 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1-10' Lab Sample ID:FA79064-2 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:74.4 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN029977.D 1 09/30/20 14:53 JA 09/25/20 08:15 OP82169 GNN1466 Run #2 Initial Weight Final Volume Run #1 19.9 g 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 0.27 0.14 mg/kg 208-96-8 Acenaphthylene ND 0.27 0.14 mg/kg 120-12-7 Anthracene ND 0.27 0.14 mg/kg 56-55-3 Benzo(a)anthracene ND 0.27 0.14 mg/kg 50-32-8 Benzo(a)pyrene ND 0.27 0.14 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.27 0.14 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.27 0.14 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.27 0.14 mg/kg 218-01-9 Chrysene ND 0.27 0.14 mg/kg 53-70-3 Dibenzo(a,h)anthracene a ND 0.27 0.14 mg/kg 206-44-0 Fluoranthene ND 0.27 0.14 mg/kg 86-73-7 Fluorene ND 0.27 0.14 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.27 0.14 mg/kg 91-57-6 2-Methylnaphthalene ND 0.27 0.14 mg/kg 91-20-3 Naphthalene ND 0.27 0.14 mg/kg 85-01-8 Phenanthrene ND 0.27 0.14 mg/kg 129-00-0 Pyrene ND 0.27 0.14 mg/kg C11-C22 Aromatics (Unadj.)ND 14 5.4 mg/kg C11-C22 Aromatics ND 14 5.4 mg/kg C9-C18 Aliphatics ND 14 3.4 mg/kg C19-C36 Aliphatics ND 14 3.4 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 54%40-140% 580-13-2 2-Bromonaphthalene 72%40-140% 84-15-1 o-Terphenyl 53%40-140% 321-60-8 2-Fluorobiphenyl 67%40-140% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 91 FA7906433.2 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8260D Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a 2B14727.D 1 09/23/20 18:13 SP n/a n/a V2B585 Run #2 Initial Weight Final Volume Run #1 3.91 g 5.0 ml Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 0.34 0.17 mg/kg 71-43-2 Benzene ND 0.0085 0.0021 mg/kg 108-86-1 Bromobenzene ND 0.0085 0.0017 mg/kg 74-97-5 Bromochloromethane ND 0.0085 0.0025 mg/kg 75-27-4 Bromodichloromethane b ND 0.0085 0.0017 mg/kg 75-25-2 Bromoform ND 0.0085 0.0017 mg/kg 78-93-3 2-Butanone (MEK)ND 0.042 0.012 mg/kg 104-51-8 n-Butylbenzene ND 0.0085 0.0017 mg/kg 135-98-8 sec-Butylbenzene ND 0.0085 0.0017 mg/kg 98-06-6 tert-Butylbenzene ND 0.0085 0.0017 mg/kg 56-23-5 Carbon Tetrachloride ND 0.0085 0.0017 mg/kg 108-90-7 Chlorobenzene ND 0.0085 0.0017 mg/kg 75-00-3 Chloroethane c ND 0.0085 0.0034 mg/kg 67-66-3 Chloroform ND 0.0085 0.0023 mg/kg 95-49-8 o-Chlorotoluene ND 0.0085 0.0017 mg/kg 106-43-4 p-Chlorotoluene ND 0.0085 0.0017 mg/kg 124-48-1 Dibromochloromethane ND 0.0085 0.0017 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0085 0.0017 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0085 0.0034 mg/kg 95-50-1 1,2-Dichlorobenzene ND 0.0085 0.0017 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.0085 0.0017 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.0085 0.0019 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0085 0.0030 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0085 0.0017 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0085 0.0017 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0085 0.0023 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0085 0.0017 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0085 0.0017 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0085 0.0017 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0085 0.0017 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0085 0.0017 mg/kg 10061-01-5 cis-1,3-Dichloropropene b ND 0.0085 0.0017 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8260D Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0085 0.0017 mg/kg 108-20-3 Di-Isopropyl Ether ND 0.0085 0.0039 mg/kg 64-17-5 Ethyl Alcohol d ND 0.68 0.13 mg/kg 100-41-4 Ethylbenzene ND 0.0085 0.0017 mg/kg 591-78-6 2-Hexanone ND 0.042 0.013 mg/kg 98-82-8 Isopropylbenzene ND 0.0085 0.0017 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0085 0.0017 mg/kg 74-83-9 Methyl Bromide ND 0.0085 0.0034 mg/kg 74-87-3 Methyl Chloride ND 0.0085 0.0034 mg/kg 75-09-2 Methylene Chloride b ND 0.034 0.019 mg/kg 108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.042 0.013 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0085 0.0017 mg/kg 91-20-3 Naphthalene ND 0.0085 0.0034 mg/kg 103-65-1 n-Propylbenzene ND 0.0085 0.0017 mg/kg 100-42-5 Styrene ND 0.0085 0.0017 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0085 0.0017 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0085 0.0017 mg/kg 127-18-4 Tetrachloroethylene ND 0.0085 0.0022 mg/kg 108-88-3 Toluene ND 0.034 0.017 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0085 0.0024 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0085 0.0017 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0085 0.0017 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0085 0.0017 mg/kg 79-01-6 Trichloroethylene ND 0.0085 0.0017 mg/kg 75-69-4 Trichlorofluoromethane b ND 0.0085 0.0034 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0085 0.0021 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0085 0.0017 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0085 0.0017 mg/kg 108-05-4 Vinyl Acetate ND 0.042 0.028 mg/kg 75-01-4 Vinyl Chloride ND 0.0085 0.0017 mg/kg m,p-Xylene ND 0.017 0.0019 mg/kg 95-47-6 o-Xylene ND 0.0085 0.0017 mg/kg 1330-20-7 Xylene (total)ND 0.025 0.0036 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 105%75-124% 17060-07-0 1,2-Dichloroethane-D4 113%72-135% 2037-26-5 Toluene-D8 94%75-126% 460-00-4 4-Bromofluorobenzene 96%71-133% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8260D Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Results reported from bisulfate-preserved sample. Internal standard response(s) outside method criteria due to sample matrix interference; associated analyte(s) ND. (b) Associated CCV outside of control limits high, sample was ND. (c) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits high, sample was ND. (d) Associated internal standard response outside method criteria due to sample matrix interference; however, analyte is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8270D SW846 3550C Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 9I009878.D 1 09/25/20 19:25 MV 09/24/20 08:10 OP82150 S9I359 Run #2 Initial Weight Final Volume Run #1 29.9 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 1.1 0.22 mg/kg 59-50-7 4-Chloro-3-methyl Phenol ND 0.22 0.025 mg/kg 95-57-8 2-Chlorophenol ND 0.22 0.027 mg/kg 120-83-2 2,4-Dichlorophenol ND 0.22 0.025 mg/kg 105-67-9 2,4-Dimethylphenol ND 0.22 0.059 mg/kg 51-28-5 2,4-Dinitrophenol ND 1.1 0.22 mg/kg 534-52-1 4,6-Dinitro-o-cresol ND 0.44 0.089 mg/kg 95-48-7 2-Methylphenol ND 0.22 0.027 mg/kg 3&4-Methylphenol ND 0.22 0.036 mg/kg 88-75-5 2-Nitrophenol ND 0.22 0.024 mg/kg 100-02-7 4-Nitrophenol ND 1.1 0.22 mg/kg 87-86-5 Pentachlorophenol ND 1.1 0.22 mg/kg 108-95-2 Phenol ND 0.22 0.022 mg/kg 88-06-2 2,4,6-Trichlorophenol ND 0.22 0.026 mg/kg 83-32-9 Acenaphthene ND 0.22 0.024 mg/kg 208-96-8 Acenaphthylene ND 0.22 0.022 mg/kg 120-12-7 Anthracene ND 0.22 0.025 mg/kg 56-55-3 Benzo(a)anthracene ND 0.22 0.022 mg/kg 50-32-8 Benzo(a)pyrene ND 0.22 0.026 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.22 0.024 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.22 0.023 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.22 0.029 mg/kg 100-51-6 Benzyl Alcohol ND 0.22 0.022 mg/kg 101-55-3 4-Bromophenyl phenyl ether ND 0.22 0.023 mg/kg 85-68-7 Butyl benzyl phthalate ND 0.22 0.044 mg/kg 106-47-8 4-Chloroaniline ND 0.22 0.056 mg/kg 111-91-1 bis(2-Chloroethoxy)methane ND 0.22 0.022 mg/kg 111-44-4 bis(2-Chloroethyl)ether ND 0.22 0.026 mg/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.22 0.028 mg/kg 91-58-7 2-Chloronaphthalene ND 0.22 0.022 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 0.22 0.022 mg/kg 218-01-9 Chrysene ND 0.22 0.023 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8270D SW846 3550C Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 53-70-3 Dibenzo(a,h)anthracene a ND 0.22 0.028 mg/kg 132-64-9 Dibenzofuran ND 0.22 0.022 mg/kg 95-50-1 1,2-Dichlorobenzene ND 0.22 0.022 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.22 0.024 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.22 0.030 mg/kg 91-94-1 3,3'-Dichlorobenzidine ND 0.22 0.053 mg/kg 84-66-2 Diethyl Phthalate ND 0.44 0.044 mg/kg 131-11-3 Dimethyl Phthalate ND 0.22 0.044 mg/kg 117-84-0 Di-n-octyl Phthalate ND 0.22 0.044 mg/kg 84-74-2 Di-n-butyl Phthalate ND 0.44 0.089 mg/kg 122-66-7 1,2-Diphenylhydrazine ND 0.22 0.022 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 0.44 0.044 mg/kg 206-44-0 Fluoranthene ND 0.22 0.022 mg/kg 86-73-7 Fluorene ND 0.22 0.024 mg/kg 118-74-1 Hexachlorobenzene ND 0.22 0.023 mg/kg 87-68-3 Hexachlorobutadiene ND 0.22 0.022 mg/kg 77-47-4 Hexachlorocyclopentadiene ND 0.22 0.044 mg/kg 67-72-1 Hexachloroethane ND 0.22 0.026 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene a ND 0.22 0.027 mg/kg 78-59-1 Isophorone ND 0.22 0.022 mg/kg 90-12-0 1-Methylnaphthalene ND 0.22 0.022 mg/kg 91-57-6 2-Methylnaphthalene b ND 0.22 0.022 mg/kg 91-20-3 Naphthalene ND 0.22 0.022 mg/kg 98-95-3 Nitrobenzene ND 0.22 0.022 mg/kg 621-64-7 N-Nitrosodi-n-propylamine ND 0.22 0.022 mg/kg 86-30-6 N-Nitrosodiphenylamine a ND 0.22 0.024 mg/kg 85-01-8 Phenanthrene ND 0.22 0.022 mg/kg 129-00-0 Pyrene ND 0.22 0.026 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.22 0.026 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 52%40-102% 4165-62-2 Phenol-d5 60%41-100% 118-79-6 2,4,6-Tribromophenol 73%42-108% 4165-60-0 Nitrobenzene-d5 58%40-105% 321-60-8 2-Fluorobiphenyl 63%43-107% 1718-51-0 Terphenyl-d14 71%45-119% (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:SW846 8270D SW846 3550C Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:MADEP VPH REV 2.1 Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1S3748.D 1 09/30/20 07:55 EG n/a n/a G1S87 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.66 g 5.0 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.087 0.087 mg/kg 100-41-4 Ethylbenzene ND 0.17 0.087 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.17 0.087 mg/kg 91-20-3 Naphthalene ND 0.44 0.26 mg/kg 108-88-3 Toluene ND 0.17 0.087 mg/kg m,p-Xylene ND 0.35 0.17 mg/kg 95-47-6 o-Xylene ND 0.17 0.087 mg/kg C5- C8 Aliphatics (Unadj.)ND 8.7 3.1 mg/kg C9- C12 Aliphatics (Unadj.)ND 8.7 3.1 mg/kg C9- C10 Aromatics (Unadj.)ND 8.7 3.1 mg/kg C5- C8 Aliphatics ND 8.7 3.1 mg/kg C9- C12 Aliphatics ND 8.7 3.1 mg/kg C9- C10 Aromatics ND 8.7 3.1 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 87%70-130% 460-00-4 BFB 87%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1-15' Lab Sample ID:FA79064-3 Date Sampled:09/16/20 Matrix:SO - Soil Date Received:09/23/20 Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:75.5 Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN029974.D 1 09/30/20 13:25 JA 09/25/20 08:15 OP82169 GNN1466 Run #2 Initial Weight Final Volume Run #1 20.2 g 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 0.26 0.13 mg/kg 208-96-8 Acenaphthylene ND 0.26 0.13 mg/kg 120-12-7 Anthracene ND 0.26 0.13 mg/kg 56-55-3 Benzo(a)anthracene ND 0.26 0.13 mg/kg 50-32-8 Benzo(a)pyrene ND 0.26 0.13 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.26 0.13 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.26 0.13 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.26 0.13 mg/kg 218-01-9 Chrysene ND 0.26 0.13 mg/kg 53-70-3 Dibenzo(a,h)anthracene a ND 0.26 0.13 mg/kg 206-44-0 Fluoranthene ND 0.26 0.13 mg/kg 86-73-7 Fluorene ND 0.26 0.13 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.26 0.13 mg/kg 91-57-6 2-Methylnaphthalene ND 0.26 0.13 mg/kg 91-20-3 Naphthalene ND 0.26 0.13 mg/kg 85-01-8 Phenanthrene ND 0.26 0.13 mg/kg 129-00-0 Pyrene ND 0.26 0.13 mg/kg C11-C22 Aromatics (Unadj.)ND 13 5.2 mg/kg C11-C22 Aromatics ND 13 5.2 mg/kg C9-C18 Aliphatics ND 13 3.3 mg/kg C19-C36 Aliphatics ND 13 3.3 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 60%40-140% 580-13-2 2-Bromonaphthalene 67%40-140% 84-15-1 o-Terphenyl 56%40-140% 321-60-8 2-Fluorobiphenyl 64%40-140% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 91 FA7906433.3 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:SM 6200B Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0223730.D 1 09/28/20 15:07 LR n/a n/a VA2791 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 8.8 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:SM 6200B Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 0.33 0.50 0.13 ug/l J 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 0.23 0.50 0.13 ug/l J 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride 0.27 0.50 0.20 ug/l J 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 41.5 0.50 0.13 ug/l 91-20-3 Naphthalene 1.8 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 1.3 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene 0.91 0.50 0.13 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 111%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 96%70-130% (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:EPA 625.1 SW846 3510C Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 9I009853.D 1 09/24/20 22:25 MV 09/24/20 08:15 OP82157 S9I358 Run #2 Initial Volume Final Volume Run #1 1050 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.5 ug/l 59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l 95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l 120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l 105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l 51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l 534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/l 95-48-7 2-Methylphenol ND 4.8 0.53 ug/l 3&4-Methylphenol ND 4.8 0.93 ug/l 88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l 100-02-7 4-Nitrophenol ND 24 4.8 ug/l 87-86-5 Pentachlorophenol ND 24 4.8 ug/l 108-95-2 Phenol ND 4.8 0.48 ug/l 88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l 83-32-9 Acenaphthene ND 4.8 0.60 ug/l 208-96-8 Acenaphthylene ND 4.8 0.61 ug/l 120-12-7 Anthracene ND 4.8 0.76 ug/l 56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l 50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l 205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l 207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l 100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l 101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l 85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l 106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l 111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l 108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l 91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l 7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l 218-01-9 Chrysene ND 4.8 0.81 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:EPA 625.1 SW846 3510C Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l 132-64-9 Dibenzofuran ND 4.8 0.57 ug/l 95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l 541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l 106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l 84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l 131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l 84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l 117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l 117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l 206-44-0 Fluoranthene ND 4.8 0.53 ug/l 86-73-7 Fluorene ND 4.8 0.67 ug/l 118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l 87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l 77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l 67-72-1 Hexachloroethane ND 4.8 1.6 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l 78-59-1 Isophorone ND 4.8 0.74 ug/l 90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l 91-57-6 2-Methylnaphthalene a ND 4.8 0.57 ug/l 91-20-3 Naphthalene 0.94 4.8 0.48 ug/l J 98-95-3 Nitrobenzene ND 4.8 0.89 ug/l 621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l 85-01-8 Phenanthrene ND 4.8 0.82 ug/l 129-00-0 Pyrene ND 4.8 0.65 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 26%14-67% 4165-62-2 Phenol-d5 19%10-50% 118-79-6 2,4,6-Tribromophenol 84%33-118% 4165-60-0 Nitrobenzene-d5 76%42-108% 321-60-8 2-Fluorobiphenyl 76%40-106% 1718-51-0 Terphenyl-d14 78%39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:EPA 625.1 SW846 3510C Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC ABN List for NC, May 2012 CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q 611-14-3 Benzene, 1-ethyl-2-methyl-5.08 4.5 ug/l JN 56554-54-2 Butanoic acid, 2-ethyl-, 1,2,3-pro 5.85 8.3 ug/l JN 52856-07-2 Ethyl 3-methyl-3-nitrobutanoate 6.20 10 ug/l JN 3937-30-2 Allyldimethylsilane 6.24 9.2 ug/l JN 36712-20-6 Furan, 3-butyltetrahydro-2-methyl-6.37 4.3 ug/l JN 80-46-6 Phenol, 4-(1,1-dimethylpropyl)-8.32 6.3 ug/l JN 96-76-4 Phenol, 2,4-bis(1,1-dimethylethyl)8.99 9 ug/l JN 1000132-40-9N-Ethyl-O-toluenesulfonamide 9.87 13 ug/l JN 80-39-7 Benzenesulfonamide, N-ethyl-4-meth 10.22 8.1 ug/l JN 100-23-2 Benzenamine, N,N-dimethyl-4-nitro-10.32 7.8 ug/l JN Total TIC, Semi-Volatile 80.5 ug/l J (a) Associated CCV and BS outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:EPA 504.1 EPA 504.1 Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a DD113542.D 1 09/29/20 14:32 CV 09/24/20 14:10 OP82165 GDD3276 Run #2 Initial Volume Final Volume Run #1 37.4 ml 2.0 ml Run #2 CAS No.Compound Result RL MDL Units Q 106-93-4 1,2-Dibromoethane 0.10 0.019 0.0094 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 113%63-137% (a) All hits confirmed by dual column analysis. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:MADEP VPH REV 2.1 Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1S3776.D 1 09/30/20 21:31 EG n/a n/a G1S88 Run #2 Purge Volume Run #1 5.0 ml Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 7.6 1.0 1.0 ug/l 100-41-4 Ethylbenzene ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 35.3 2.0 1.0 ug/l 91-20-3 Naphthalene ND 5.0 3.0 ug/l 108-88-3 Toluene ND 2.0 1.0 ug/l m,p-Xylene ND 4.0 2.0 ug/l 95-47-6 o-Xylene 1.0 2.0 1.0 ug/l J C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l C9- C10 Aromatics (Unadj.)ND 100 35 ug/l C5- C8 Aliphatics ND 100 35 ug/l C9- C12 Aliphatics ND 100 35 ug/l C9- C10 Aromatics ND 100 35 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 98%70-130% 460-00-4 BFB 100%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN029965.D 1 09/29/20 16:03 JA 09/25/20 07:53 OP82174 GNN1465 Run #2 a NN030015.D 1 10/05/20 11:38 JA 09/25/20 07:53 OP82174 GNN1469 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 1040 ml 2.0 ml MAEPH List CAS No.Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 3.8 1.9 ug/l 208-96-8 Acenaphthylene ND 3.8 1.9 ug/l 120-12-7 Anthracene ND 3.8 1.9 ug/l 56-55-3 Benzo(a)anthracene ND 3.8 1.9 ug/l 50-32-8 Benzo(a)pyrene ND 3.8 1.9 ug/l 205-99-2 Benzo(b)fluoranthene ND 3.8 1.9 ug/l 191-24-2 Benzo(g,h,i)perylene ND 3.8 1.9 ug/l 207-08-9 Benzo(k)fluoranthene ND 3.8 1.9 ug/l 218-01-9 Chrysene ND 3.8 1.9 ug/l 53-70-3 Dibenzo(a,h)anthracene ND 3.8 1.9 ug/l 206-44-0 Fluoranthene ND 3.8 1.9 ug/l 86-73-7 Fluorene ND 3.8 1.9 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 3.8 1.9 ug/l 91-57-6 2-Methylnaphthalene ND 3.8 1.9 ug/l 91-20-3 Naphthalene ND 3.8 1.9 ug/l 85-01-8 Phenanthrene ND 3.8 1.9 ug/l 129-00-0 Pyrene ND 3.8 1.9 ug/l C11-C22 Aromatics (Unadj.)84.7 190 77 ug/l J C11-C22 Aromatics 84.7 190 77 ug/l J C9-C18 Aliphatics ND 190 48 ug/l C19-C36 Aliphatics ND 190 48 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 32% b 28%40-140% 580-13-2 2-Bromonaphthalene 101%79%40-140% 84-15-1 o-Terphenyl 80%60%40-140% 321-60-8 2-Fluorobiphenyl 95%70%40-140% (a) Confirmation run for surrogate recoveries. (b) Outside control limits. Confirmed by refractionation and reanalysis. Insufficient sample for re-extraction. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 31 of 91 FA7906433.4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-1 Lab Sample ID:FA79064-4 Date Sampled:09/22/20 Matrix:AQ - Ground Water Date Received:09/23/20 Percent Solids:n/a Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Total Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 137 5.0 ug/l 1 09/25/20 09/25/20 LM SW846 6010D 1 SW846 3010A 2 (1) Instrument QC Batch: MA17078 (2) Prep QC Batch: MP37857 RL = Reporting Limit 32 of 91 FA7906433.4 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 33 of 91 FA790644 FA79064: Chain of Custody Page 1 of 2 34 of 91 FA7906444.1 Job Number:FA79064 Client:RESOLVE ENVIRONMENTAL SERVICES Date / Time Received:9/23/2020 10:10:00 AM Delivery Method:FEDEX Project:KWICK MART Airbill #'s:100963783692 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments "MW-1-5"- VIAL (NAHSO4) ARRIVED BROKEN "MW-1-10" VPH VIAL ARRIVED BROKEN "MW-1"- METAL BOTTLE AND 2 EXT 1L AMBERS BOTTLES LABEL STATES DATED 9/16/20 BUT COC DATES 9/22/20 SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (2.8); Cooler 1: (2.6); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:-0.2; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:MAGALEAK Date:Date: 9/23/2020 10:10:00 A FA79064: Chain of Custody Page 2 of 2 35 of 91 FA7906444.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 36 of 91 FA790645 Method Blank Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2791-MB A0223727.D 1 09/28/20 LR n/a n/a VA2791 The QC reported here applies to the following samples:Method: SM 6200B FA79064-4 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 37 of 91 FA7906455.1.1 Method Blank Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2791-MB A0223727.D 1 09/28/20 LR n/a n/a VA2791 The QC reported here applies to the following samples:Method: SM 6200B FA79064-4 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 111%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 102%70-130% 38 of 91 FA7906455.1.1 Method Blank Summary Page 1 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2B585-MB 2B14716.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 200 100 ug/kg 71-43-2 Benzene ND 5.0 1.2 ug/kg 108-86-1 Bromobenzene ND 5.0 1.0 ug/kg 74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg 75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg 75-25-2 Bromoform ND 5.0 1.0 ug/kg 78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg 104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg 135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg 98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg 56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg 108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg 75-00-3 Chloroethane ND 5.0 2.0 ug/kg 67-66-3 Chloroform ND 5.0 1.3 ug/kg 95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg 106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg 124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg 106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg 95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg 541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg 106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg 75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg 108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg 64-17-5 Ethyl Alcohol ND 400 75 ug/kg 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 39 of 91 FA7906455.1.2 Method Blank Summary Page 2 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2B585-MB 2B14716.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 CAS No.Compound Result RL MDL Units Q 591-78-6 2-Hexanone ND 25 7.5 ug/kg 98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg 99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg 74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg 74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg 75-09-2 Methylene Chloride ND 20 11 ug/kg 108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg 108-88-3 Toluene ND 20 10 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg 71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg 79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 108-05-4 Vinyl Acetate ND 25 16 ug/kg 75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg m,p-Xylene ND 10 1.1 ug/kg 95-47-6 o-Xylene ND 5.0 1.0 ug/kg 1330-20-7 Xylene (total)ND 15 2.1 ug/kg CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 99%75-124% 17060-07-0 1,2-Dichloroethane-D4 107%72-135% 2037-26-5 Toluene-D8 94%75-126% 40 of 91 FA7906455.1.2 Method Blank Summary Page 3 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2B585-MB 2B14716.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 97%71-133% 41 of 91 FA7906455.1.2 Blank Spike Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2791-BS A0223725.D 1 09/28/20 LR n/a n/a VA2791 The QC reported here applies to the following samples:Method: SM 6200B FA79064-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.0 100 70-130 108-86-1 Bromobenzene 10 10.3 103 70-130 74-97-5 Bromochloromethane 10 9.6 96 70-130 75-27-4 Bromodichloromethane 10 9.6 96 70-130 75-25-2 Bromoform 10 9.6 96 70-130 104-51-8 n-Butylbenzene 10 10.8 108 70-130 135-98-8 sec-Butylbenzene 10 10.7 107 70-130 98-06-6 tert-Butylbenzene 10 10.1 101 70-130 56-23-5 Carbon Tetrachloride 10 10.0 100 70-130 108-90-7 Chlorobenzene 10 10.2 102 70-130 75-00-3 Chloroethane 10 7.9 79 60-140 67-66-3 Chloroform 10 9.6 96 70-130 95-49-8 o-Chlorotoluene 10 10.1 101 70-130 106-43-4 p-Chlorotoluene 10 10.1 101 70-130 124-48-1 Dibromochloromethane 10 9.9 99 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 9.7 97 70-130 106-93-4 1,2-Dibromoethane 10 10.6 106 70-130 75-71-8 Dichlorodifluoromethane 10 5.9 59* a 60-140 95-50-1 1,2-Dichlorobenzene 10 10 100 70-130 541-73-1 1,3-Dichlorobenzene 10 10.3 103 70-130 106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130 75-34-3 1,1-Dichloroethane 10 9.6 96 70-130 107-06-2 1,2-Dichloroethane 10 10.5 105 70-130 75-35-4 1,1-Dichloroethylene 10 9.9 99 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.4 94 70-130 156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130 78-87-5 1,2-Dichloropropane 10 10.1 101 70-130 142-28-9 1,3-Dichloropropane 10 10.4 104 70-130 594-20-7 2,2-Dichloropropane 10 9.3 93 70-130 563-58-6 1,1-Dichloropropene 10 10.5 105 70-130 10061-01-5 cis-1,3-Dichloropropene 10 10.4 104 70-130 10061-02-6 trans-1,3-Dichloropropene 10 11.0 110 70-130 108-20-3 Di-Isopropyl Ether 10 9.3 93 70-130 100-41-4 Ethylbenzene 10 10.3 103 70-130 87-68-3 Hexachlorobutadiene 10 10 100 70-130 98-82-8 Isopropylbenzene 10 10 100 70-130 * = Outside of Control Limits. 42 of 91 FA7906455.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2791-BS A0223725.D 1 09/28/20 LR n/a n/a VA2791 The QC reported here applies to the following samples:Method: SM 6200B FA79064-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.4 104 70-130 74-83-9 Methyl Bromide 10 8.8 88 60-140 74-87-3 Methyl Chloride 10 8.8 88 60-140 74-95-3 Methylene Bromide 10 9.9 99 70-130 75-09-2 Methylene Chloride 10 9.4 94 70-130 1634-04-4 Methyl Tert Butyl Ether 10 10.0 100 70-130 91-20-3 Naphthalene 10 9.5 95 70-130 103-65-1 n-Propylbenzene 10 10.4 104 70-130 100-42-5 Styrene 10 9.5 95 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 10.0 100 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 11.0 110 70-130 127-18-4 Tetrachloroethylene 10 10.2 102 70-130 108-88-3 Toluene 10 10.1 101 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.4 94 70-130 71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130 79-00-5 1,1,2-Trichloroethane 10 10.8 108 70-130 79-01-6 Trichloroethylene 10 10.2 102 70-130 75-69-4 Trichlorofluoromethane 10 9.0 90 60-140 96-18-4 1,2,3-Trichloropropane 10 10.8 108 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.8 98 70-130 108-67-8 1,3,5-Trimethylbenzene 10 10.2 102 70-130 75-01-4 Vinyl Chloride 10 8.7 87 60-140 m,p-Xylene 20 20.3 102 70-130 95-47-6 o-Xylene 10 9.5 95 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 109%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% (a) Sporadic marginal failure. * = Outside of Control Limits. 43 of 91 FA7906455.2.1 Blank Spike Summary Page 1 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2B585-BS 2B14715.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 67-64-1 Acetone 250 293 117 61-152 71-43-2 Benzene 50 56.3 113 76-126 108-86-1 Bromobenzene 50 49.3 99 76-122 74-97-5 Bromochloromethane 50 57.4 115 77-120 75-27-4 Bromodichloromethane 50 60.4 121 74-130 75-25-2 Bromoform 50 51.6 103 76-127 78-93-3 2-Butanone (MEK)250 292 117 75-137 104-51-8 n-Butylbenzene 50 50.6 101 71-128 135-98-8 sec-Butylbenzene 50 50.8 102 79-135 98-06-6 tert-Butylbenzene 50 48.7 97 77-133 56-23-5 Carbon Tetrachloride 50 57.0 114 78-133 108-90-7 Chlorobenzene 50 51.4 103 81-129 75-00-3 Chloroethane 50 85.6 171*68-133 67-66-3 Chloroform 50 56.7 113 72-123 95-49-8 o-Chlorotoluene 50 49.1 98 77-129 106-43-4 p-Chlorotoluene 50 48.2 96 80-134 124-48-1 Dibromochloromethane 50 50.6 101 76-127 106-93-4 1,2-Dibromoethane 50 52.0 104 77-126 75-71-8 Dichlorodifluoromethane 50 39.7 79 68-168 95-50-1 1,2-Dichlorobenzene 50 48.9 98 80-129 541-73-1 1,3-Dichlorobenzene 50 48.7 97 81-129 106-46-7 1,4-Dichlorobenzene 50 48.3 97 76-130 75-34-3 1,1-Dichloroethane 50 56.8 114 73-125 107-06-2 1,2-Dichloroethane 50 57.7 115 74-128 75-35-4 1,1-Dichloroethylene 50 57.0 114 81-136 156-59-2 cis-1,2-Dichloroethylene 50 57.0 114 74-126 156-60-5 trans-1,2-Dichloroethylene 50 56.1 112 70-127 78-87-5 1,2-Dichloropropane 50 57.8 116 74-125 142-28-9 1,3-Dichloropropane 50 50.1 100 76-122 594-20-7 2,2-Dichloropropane 50 56.5 113 77-133 563-58-6 1,1-Dichloropropene 50 55.6 111 75-130 10061-01-5 cis-1,3-Dichloropropene 50 59.6 119 80-123 10061-02-6 trans-1,3-Dichloropropene 50 53.9 108 75-131 108-20-3 Di-Isopropyl Ether 50 59.5 119 75-122 64-17-5 Ethyl Alcohol 1000 1040 104 53-154 100-41-4 Ethylbenzene 50 51.2 102 77-123 * = Outside of Control Limits. 44 of 91 FA7906455.2.2 Blank Spike Summary Page 2 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2B585-BS 2B14715.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 591-78-6 2-Hexanone 250 274 110 72-133 98-82-8 Isopropylbenzene 50 51.4 103 80-136 99-87-6 p-Isopropyltoluene 50 50.3 101 77-131 74-83-9 Methyl Bromide 50 58.3 117 65-139 74-87-3 Methyl Chloride 50 50.8 102 71-144 75-09-2 Methylene Chloride 50 68.0 136 74-137 108-10-1 4-Methyl-2-pentanone (MIBK)250 273 109 76-132 1634-04-4 Methyl Tert Butyl Ether 50 50.1 100 77-120 91-20-3 Naphthalene 50 49.7 99 79-129 103-65-1 n-Propylbenzene 50 48.7 97 80-135 100-42-5 Styrene 50 52.6 105 78-125 630-20-6 1,1,1,2-Tetrachloroethane 50 54.3 109 78-126 79-34-5 1,1,2,2-Tetrachloroethane 50 53.0 106 71-126 127-18-4 Tetrachloroethylene 50 47.7 95 79-130 108-88-3 Toluene 50 48.6 97 76-124 87-61-6 1,2,3-Trichlorobenzene 50 49.4 99 77-128 120-82-1 1,2,4-Trichlorobenzene 50 48.3 97 78-130 71-55-6 1,1,1-Trichloroethane 50 55.3 111 70-129 79-00-5 1,1,2-Trichloroethane 50 51.0 102 74-124 79-01-6 Trichloroethylene 50 56.1 112 75-128 75-69-4 Trichlorofluoromethane 50 63.8 128 73-145 96-18-4 1,2,3-Trichloropropane 50 49.5 99 74-127 95-63-6 1,2,4-Trimethylbenzene 50 49.0 98 74-123 108-67-8 1,3,5-Trimethylbenzene 50 50.0 100 73-122 108-05-4 Vinyl Acetate 250 263 105 48-164 75-01-4 Vinyl Chloride 50 53.6 107 76-141 m,p-Xylene 100 103 103 80-128 95-47-6 o-Xylene 50 51.7 103 80-132 1330-20-7 Xylene (total)150 155 103 80-129 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 106%75-124% 17060-07-0 1,2-Dichloroethane-D4 104%72-135% 2037-26-5 Toluene-D8 92%75-126% * = Outside of Control Limits. 45 of 91 FA7906455.2.2 Blank Spike Summary Page 3 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2B585-BS 2B14715.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 CAS No.Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 97%71-133% * = Outside of Control Limits. 46 of 91 FA7906455.2.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79192-2MS A0223738.D 1 09/28/20 LR n/a n/a VA2791 FA79192-2MSD A0223739.D 1 09/28/20 LR n/a n/a VA2791 FA79192-2 a A0223733.D 1 09/28/20 LR n/a n/a VA2791 The QC reported here applies to the following samples:Method: SM 6200B FA79064-4 FA79192-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene ND 10 9.2 92 10 9.2 92 0 70-130/20 108-86-1 Bromobenzene ND 10 9.3 93 10 9.2 92 1 70-130/20 74-97-5 Bromochloromethane ND 10 8.7 87 10 8.7 87 0 70-130/20 75-27-4 Bromodichloromethane ND 10 7.9 79 10 7.8 78 1 70-130/20 75-25-2 Bromoform ND 10 5.7 57*10 5.7 57*0 70-130/20 104-51-8 n-Butylbenzene ND 10 10.0 100 10 10 100 0 70-130/20 135-98-8 sec-Butylbenzene 0.25 J 10 9.7 95 10 9.6 94 1 70-130/20 98-06-6 tert-Butylbenzene 0.15 J 10 9.2 91 10 9.1 90 1 70-130/20 56-23-5 Carbon Tetrachloride ND 10 8.5 85 10 8.5 85 0 70-130/20 108-90-7 Chlorobenzene ND 10 9.3 93 10 9.3 93 0 70-130/20 75-00-3 Chloroethane ND 10 7.5 75 10 8.8 88 16 60-140/20 67-66-3 Chloroform ND 10 8.8 88 10 8.8 88 0 70-130/20 95-49-8 o-Chlorotoluene ND 10 9.2 92 10 9.2 92 0 70-130/20 106-43-4 p-Chlorotoluene ND 10 9.1 91 10 9.1 91 0 70-130/20 124-48-1 Dibromochloromethane ND 10 6.9 69*10 6.9 69*0 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.7 87 10 8.6 86 1 70-130/20 106-93-4 1,2-Dibromoethane ND 10 9.1 91 10 9.1 91 0 70-130/20 75-71-8 Dichlorodifluoromethane ND 10 5.5 55*10 6.7 67 20 60-140/20 95-50-1 1,2-Dichlorobenzene ND 10 9.2 92 10 9.1 91 1 70-130/20 541-73-1 1,3-Dichlorobenzene ND 10 9.4 94 10 9.3 93 1 70-130/20 106-46-7 1,4-Dichlorobenzene ND 10 9.3 93 10 9.2 92 1 70-130/20 75-34-3 1,1-Dichloroethane ND 10 8.9 89 10 9.0 90 1 70-130/20 107-06-2 1,2-Dichloroethane ND 10 9.5 95 10 9.6 96 1 70-130/20 75-35-4 1,1-Dichloroethylene ND 10 9.1 91 10 9.1 91 0 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 10 8.5 85 10 8.5 85 0 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 10 8.7 87 10 8.8 88 1 70-130/20 78-87-5 1,2-Dichloropropane ND 10 9.2 92 10 9.2 92 0 70-130/20 142-28-9 1,3-Dichloropropane ND 10 9.3 93 10 9.2 92 1 70-130/20 594-20-7 2,2-Dichloropropane ND 10 8.1 81 10 8.1 81 0 70-130/20 563-58-6 1,1-Dichloropropene ND 10 9.5 95 10 9.5 95 0 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 10 7.7 77 10 7.8 78 1 70-130/20 10061-02-6 trans-1,3-Dichloropropene 2.4 10 8.7 63*10 8.9 65*2 70-130/20 108-20-3 Di-Isopropyl Ether 0.26 J 10 8.4 81 10 8.4 81 0 70-130/20 100-41-4 Ethylbenzene ND 10 9.3 93 10 9.3 93 0 70-130/20 87-68-3 Hexachlorobutadiene ND 10 9.0 90 10 9.1 91 1 70-130/20 98-82-8 Isopropylbenzene 1.2 10 9.1 79 10 9.2 80 1 70-130/20 * = Outside of Control Limits. 47 of 91 FA7906455.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79192-2MS A0223738.D 1 09/28/20 LR n/a n/a VA2791 FA79192-2MSD A0223739.D 1 09/28/20 LR n/a n/a VA2791 FA79192-2 a A0223733.D 1 09/28/20 LR n/a n/a VA2791 The QC reported here applies to the following samples:Method: SM 6200B FA79064-4 FA79192-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 10 9.3 93 10 9.2 92 1 70-130/20 74-83-9 Methyl Bromide ND 10 8.5 85 10 10.1 101 17 60-140/20 74-87-3 Methyl Chloride ND 10 8.4 84 10 9.7 97 14 60-140/20 74-95-3 Methylene Bromide ND 10 9.0 90 10 8.9 89 1 70-130/20 75-09-2 Methylene Chloride ND 10 9.3 93 10 9.3 93 0 70-130/20 1634-04-4 Methyl Tert Butyl Ether 0.48 J 10 8.8 83 10 8.9 84 1 70-130/20 91-20-3 Naphthalene ND 10 8.5 85 10 8.7 87 2 70-130/20 103-65-1 n-Propylbenzene ND 10 9.3 93 10 9.3 93 0 70-130/20 100-42-5 Styrene ND 10 8.1 81 10 8.1 81 0 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.0 90 10 8.9 89 1 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.1 101 10 10.1 101 0 70-130/20 127-18-4 Tetrachloroethylene ND 10 9.1 91 10 9.2 92 1 70-130/20 108-88-3 Toluene ND 10 9.1 91 10 9.2 92 1 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 10 8.7 87 10 8.7 87 0 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 10 8.7 87 10 8.7 87 0 70-130/20 71-55-6 1,1,1-Trichloroethane ND 10 8.7 87 10 8.9 89 2 70-130/20 79-00-5 1,1,2-Trichloroethane ND 10 9.8 98 10 9.7 97 1 70-130/20 79-01-6 Trichloroethylene ND 10 9.0 90 10 9.2 92 2 70-130/20 75-69-4 Trichlorofluoromethane ND 10 8.5 85 10 10.1 101 17 60-140/20 96-18-4 1,2,3-Trichloropropane ND 10 9.6 96 10 9.5 95 1 70-130/20 95-63-6 1,2,4-Trimethylbenzene ND 10 8.8 88 10 8.8 88 0 70-130/20 108-67-8 1,3,5-Trimethylbenzene ND 10 9.1 91 10 9.0 90 1 70-130/20 75-01-4 Vinyl Chloride ND 10 8.0 80 10 9.8 98 20 60-140/20 m,p-Xylene ND 20 18.2 91 20 18.3 92 1 70-130/20 95-47-6 o-Xylene 0.19 J 10 8.4 82 10 8.6 84 2 70-130/20 CAS No.Surrogate Recoveries MS MSD FA79192-2 Limits 1868-53-7 Dibromofluoromethane 102%102%97%70-130% 17060-07-0 1,2-Dichloroethane-D4 110%110%112%70-130% 2037-26-5 Toluene-D8 99%100%99%70-130% 460-00-4 4-Bromofluorobenzene 96%96%99%70-130% (a) Confirmation run. * = Outside of Control Limits. 48 of 91 FA7906455.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79038-2MS 2B14728.D 1 09/23/20 SP n/a n/a V2B585 FA79038-2MSD 2B14729.D 1 09/23/20 SP n/a n/a V2B585 FA79038-2 a 2B14724.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 FA79038-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 67-64-1 Acetone 220 U 264 367 139 264 196 74 61*61-152/27 71-43-2 Benzene 5.5 U 52.8 51.1 97 52.8 51.1 97 0 76-126/26 108-86-1 Bromobenzene 5.5 U 52.8 27.6 52*52.8 31.9 60*14 76-122/32 74-97-5 Bromochloromethane 5.5 U 52.8 38.4 73*52.8 35.9 68*7 77-120/24 75-27-4 Bromodichloromethane 5.5 U 52.8 42.8 81 52.8 42.0 80 2 74-130/25 75-25-2 Bromoform 5.5 U 52.8 23.6 45*52.8 22.0 42*7 76-127/26 78-93-3 2-Butanone (MEK)27 U 264 279 106 264 144 55*64*75-137/25 104-51-8 n-Butylbenzene 5.5 U 52.8 44.5 84 52.8 47.0 89 5 71-128/35 135-98-8 sec-Butylbenzene 5.5 U 52.8 48.5 92 52.8 50.0 95 3 79-135/34 98-06-6 tert-Butylbenzene 5.5 U 52.8 46.0 87 52.8 47.5 90 3 77-133/34 56-23-5 Carbon Tetrachloride 5.5 U 52.8 57.8 110 52.8 57.5 109 1 78-133/29 108-90-7 Chlorobenzene 5.5 U 52.8 37.9 72*52.8 41.1 78*8 81-129/29 75-00-3 Chloroethane 5.5 U 52.8 63.8 121 52.8 64.3 122 1 68-133/29 67-66-3 Chloroform 5.5 U 52.8 48.3 92 52.8 47.4 90 2 72-123/26 95-49-8 o-Chlorotoluene 5.5 U 52.8 37.6 71*52.8 41.1 78 9 77-129/33 106-43-4 p-Chlorotoluene 5.5 U 52.8 34.2 65*52.8 38.1 72*11 80-134/33 124-48-1 Dibromochloromethane 5.5 U 52.8 29.3 56*52.8 28.1 53*4 76-127/27 106-93-4 1,2-Dibromoethane 5.5 U 52.8 28.0 53*52.8 25.8 49*8 77-126/26 75-71-8 Dichlorodifluoromethane 5.5 U 52.8 43.2 82 52.8 42.1 80 3 68-168/29 95-50-1 1,2-Dichlorobenzene 5.5 U 52.8 23.0 44*52.8 27.9 53*19 80-129/32 541-73-1 1,3-Dichlorobenzene 5.5 U 52.8 27.5 52*52.8 32.6 62*17 81-129/33 106-46-7 1,4-Dichlorobenzene 5.5 U 52.8 25.5 48*52.8 30.5 58*18 76-130/32 75-34-3 1,1-Dichloroethane 5.5 U 52.8 51.9 98 52.8 51.1 97 2 73-125/27 107-06-2 1,2-Dichloroethane 5.5 U 52.8 40.6 77 52.8 36.7 70*10 74-128/23 75-35-4 1,1-Dichloroethylene 5.5 U 52.8 58.6 111 52.8 58.8 111 0 81-136/28 156-59-2 cis-1,2-Dichloroethylene 5.5 U 52.8 45.7 87 52.8 46.2 88 1 74-126/26 156-60-5 trans-1,2-Dichloroethylene 5.5 U 52.8 52.7 100 52.8 53.2 101 1 70-127/27 78-87-5 1,2-Dichloropropane 5.5 U 52.8 45.7 87 52.8 44.1 84 4 74-125/25 142-28-9 1,3-Dichloropropane 5.5 U 52.8 30.8 58*52.8 28.2 53*9 76-122/26 594-20-7 2,2-Dichloropropane 5.5 U 52.8 54.2 103 52.8 54.0 102 0 77-133/28 563-58-6 1,1-Dichloropropene 5.5 U 52.8 59.7 113 52.8 59.6 113 0 75-130/28 10061-01-5 cis-1,3-Dichloropropene 5.5 U 52.8 38.8 74*52.8 37.9 72*2 80-123/26 10061-02-6 trans-1,3-Dichloropropene 5.5 U 52.8 30.9 59*52.8 30.1 57*3 75-131/28 108-20-3 Di-Isopropyl Ether 5.5 U 52.8 44.3 84 52.8 41.7 79 6 75-122/25 64-17-5 Ethyl Alcohol 440 U 1060 4010 380*1060 1630 154 84*53-154/42 100-41-4 Ethylbenzene 5.5 U 52.8 47.3 90 52.8 49.0 93 4 77-123/31 * = Outside of Control Limits. 49 of 91 FA7906455.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79038-2MS 2B14728.D 1 09/23/20 SP n/a n/a V2B585 FA79038-2MSD 2B14729.D 1 09/23/20 SP n/a n/a V2B585 FA79038-2 a 2B14724.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 FA79038-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 591-78-6 2-Hexanone 27 U 264 134 51*264 80.4 30*50*72-133/26 98-82-8 Isopropylbenzene 5.5 U 52.8 48.3 92 52.8 50.3 95 4 80-136/32 99-87-6 p-Isopropyltoluene 5.5 U 52.8 46.9 89 52.8 48.8 92 4 77-131/34 74-83-9 Methyl Bromide 5.5 U 52.8 50.8 96 52.8 49.1 93 3 65-139/31 74-87-3 Methyl Chloride 5.5 U 52.8 50.8 96 52.8 48.6 92 4 71-144/27 75-09-2 Methylene Chloride 22 U 52.8 48.2 91 52.8 45.6 86 6 74-137/28 108-10-1 4-Methyl-2-pentanone (MIBK)27 U 264 160 61*264 102 39*44*76-132/26 1634-04-4 Methyl Tert Butyl Ether 5.5 U 52.8 30.6 58*52.8 25.1 48*20 77-120/24 91-20-3 Naphthalene 5.5 U 52.8 10 19*52.8 13.7 26*31 79-129/33 103-65-1 n-Propylbenzene 5.5 U 52.8 45.2 86 52.8 46.8 89 3 80-135/33 100-42-5 Styrene 5.5 U 52.8 30.9 59*52.8 36.1 68*16 78-125/30 630-20-6 1,1,1,2-Tetrachloroethane 5.5 U 52.8 38.6 73*52.8 40.1 76*4 78-126/27 79-34-5 1,1,2,2-Tetrachloroethane 5.5 U 52.8 25.8 49*52.8 23.4 44*10 71-126/30 127-18-4 Tetrachloroethylene 5.5 U 52.8 49.3 93 52.8 49.4 94 0 79-130/31 108-88-3 Toluene 22 U 52.8 43.4 82 52.8 44.4 84 2 76-124/30 87-61-6 1,2,3-Trichlorobenzene 5.5 U 52.8 14.4 27*52.8 19.5 37*30 77-128/35 120-82-1 1,2,4-Trichlorobenzene 5.5 U 52.8 16.8 32*52.8 22.0 42*27 78-130/34 71-55-6 1,1,1-Trichloroethane 5.5 U 52.8 54.7 104 52.8 54.6 103 0 70-129/27 79-00-5 1,1,2-Trichloroethane 5.5 U 52.8 31.5 60*52.8 29.2 55*8 74-124/28 79-01-6 Trichloroethylene 5.5 U 52.8 54.6 103 52.8 54.6 103 0 75-128/27 75-69-4 Trichlorofluoromethane 5.5 U 52.8 72.1 137 52.8 70.0 133 3 73-145/31 96-18-4 1,2,3-Trichloropropane 5.5 U 52.8 24.5 46*52.8 20.2 38*19 74-127/27 95-63-6 1,2,4-Trimethylbenzene 5.5 U 52.8 38.1 72*52.8 41.6 79 9 74-123/34 108-67-8 1,3,5-Trimethylbenzene 5.5 U 52.8 42.8 81 52.8 45.5 86 6 73-122/33 108-05-4 Vinyl Acetate 27 U 264 159 60 264 133 50 18 48-164/37 75-01-4 Vinyl Chloride 5.5 U 52.8 53.6 102 52.8 52.8 100 2 76-141/27 m,p-Xylene 11 U 106 93.2 88 106 98.1 93 5 80-128/30 95-47-6 o-Xylene 5.5 U 52.8 41.5 79*52.8 44.1 84 6 80-132/30 1330-20-7 Xylene (total)16 U 158 135 85 158 142 90 5 80-129/30 CAS No.Surrogate Recoveries MS MSD FA79038-2 Limits 1868-53-7 Dibromofluoromethane 107%109%106%75-124% 17060-07-0 1,2-Dichloroethane-D4 116%117%120%72-135% 2037-26-5 Toluene-D8 91%91%94%75-126% * = Outside of Control Limits. 50 of 91 FA7906455.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79038-2MS 2B14728.D 1 09/23/20 SP n/a n/a V2B585 FA79038-2MSD 2B14729.D 1 09/23/20 SP n/a n/a V2B585 FA79038-2 a 2B14724.D 1 09/23/20 SP n/a n/a V2B585 The QC reported here applies to the following samples:Method: SW846 8260D FA79064-1, FA79064-3 CAS No.Surrogate Recoveries MS MSD FA79038-2 Limits 460-00-4 4-Bromofluorobenzene 96%94%97%71-133% (a) Results reported from bisulfate-preserved sample. Sample was received in a bulk container and preserved within 48 hours of sampling. * = Outside of Control Limits. 51 of 91 FA7906455.3.2 SGS North America Inc. MS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 6 52 of 91 FA790646 Method Blank Summary Page 1 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82157-MB 9I009851.D 1 09/24/20 MV 09/24/20 OP82157 S9I358 The QC reported here applies to the following samples:Method: EPA 625.1 FA79064-4 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 50 10 ug/l 59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l 95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l 120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l 105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l 51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l 534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l 95-48-7 2-Methylphenol ND 5.0 0.56 ug/l 3&4-Methylphenol ND 5.0 0.98 ug/l 88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l 100-02-7 4-Nitrophenol ND 25 5.0 ug/l 87-86-5 Pentachlorophenol ND 25 5.0 ug/l 108-95-2 Phenol ND 5.0 0.50 ug/l 88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l 83-32-9 Acenaphthene ND 5.0 0.63 ug/l 208-96-8 Acenaphthylene ND 5.0 0.64 ug/l 120-12-7 Anthracene ND 5.0 0.80 ug/l 56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l 50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l 205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l 191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l 207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l 100-51-6 Benzyl Alcohol ND 5.0 0.61 ug/l 101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l 85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l 106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l 111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l 108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l 91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l 7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l 218-01-9 Chrysene ND 5.0 0.85 ug/l 53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l 132-64-9 Dibenzofuran ND 5.0 0.60 ug/l 95-50-1 1,2-Dichlorobenzene ND 5.0 0.50 ug/l 541-73-1 1,3-Dichlorobenzene ND 5.0 0.50 ug/l 53 of 91 FA7906466.1.1 Method Blank Summary Page 2 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82157-MB 9I009851.D 1 09/24/20 MV 09/24/20 OP82157 S9I358 The QC reported here applies to the following samples:Method: EPA 625.1 FA79064-4 CAS No.Compound Result RL MDL Units Q 106-46-7 1,4-Dichlorobenzene ND 5.0 0.50 ug/l 91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l 84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l 131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l 84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l 117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l 122-66-7 1,2-Diphenylhydrazine ND 5.0 0.76 ug/l 117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l 206-44-0 Fluoranthene ND 5.0 0.55 ug/l 86-73-7 Fluorene ND 5.0 0.70 ug/l 118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l 87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l 77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l 67-72-1 Hexachloroethane ND 5.0 1.6 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l 78-59-1 Isophorone ND 5.0 0.78 ug/l 90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l 91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l 91-20-3 Naphthalene ND 5.0 0.50 ug/l 98-95-3 Nitrobenzene ND 5.0 0.93 ug/l 621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l 86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l 85-01-8 Phenanthrene ND 5.0 0.86 ug/l 129-00-0 Pyrene ND 5.0 0.68 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.1 ug/l CAS No.Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 28%14-67% 4165-62-2 Phenol-d5 19%10-50% 118-79-6 2,4,6-Tribromophenol 72%33-118% 4165-60-0 Nitrobenzene-d5 55%42-108% 321-60-8 2-Fluorobiphenyl 70%40-106% 1718-51-0 Terphenyl-d14 74%39-121% 54 of 91 FA7906466.1.1 Method Blank Summary Page 3 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82157-MB 9I009851.D 1 09/24/20 MV 09/24/20 OP82157 S9I358 The QC reported here applies to the following samples:Method: FA79064-4 CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q Total TIC, Semi-Volatile 0 ug/l 55 of 91 FA7906466.1.1 Method Blank Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82150-MB 9I009861.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 The QC reported here applies to the following samples:Method: SW846 8270D FA79064-1, FA79064-3 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 830 170 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg 95-57-8 2-Chlorophenol ND 170 20 ug/kg 120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg 105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg 51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg 95-48-7 2-Methylphenol ND 170 20 ug/kg 3&4-Methylphenol ND 170 27 ug/kg 88-75-5 2-Nitrophenol ND 170 18 ug/kg 100-02-7 4-Nitrophenol ND 830 170 ug/kg 87-86-5 Pentachlorophenol ND 830 170 ug/kg 108-95-2 Phenol ND 170 17 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg 83-32-9 Acenaphthene ND 170 18 ug/kg 208-96-8 Acenaphthylene ND 170 17 ug/kg 120-12-7 Anthracene ND 170 19 ug/kg 56-55-3 Benzo(a)anthracene ND 170 17 ug/kg 50-32-8 Benzo(a)pyrene ND 170 20 ug/kg 205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg 207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg 100-51-6 Benzyl Alcohol ND 170 17 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg 85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg 106-47-8 4-Chloroaniline ND 170 42 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg 91-58-7 2-Chloronaphthalene ND 170 17 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg 218-01-9 Chrysene ND 170 17 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg 132-64-9 Dibenzofuran ND 170 17 ug/kg 95-50-1 1,2-Dichlorobenzene ND 170 17 ug/kg 541-73-1 1,3-Dichlorobenzene ND 170 18 ug/kg 56 of 91 FA7906466.1.2 Method Blank Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82150-MB 9I009861.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 The QC reported here applies to the following samples:Method: SW846 8270D FA79064-1, FA79064-3 CAS No.Compound Result RL MDL Units Q 106-46-7 1,4-Dichlorobenzene ND 170 22 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg 84-66-2 Diethyl Phthalate ND 330 33 ug/kg 131-11-3 Dimethyl Phthalate ND 170 33 ug/kg 117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg 84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 170 17 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg 206-44-0 Fluoranthene ND 170 17 ug/kg 86-73-7 Fluorene ND 170 18 ug/kg 118-74-1 Hexachlorobenzene ND 170 17 ug/kg 87-68-3 Hexachlorobutadiene ND 170 17 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg 67-72-1 Hexachloroethane ND 170 20 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg 78-59-1 Isophorone ND 170 17 ug/kg 90-12-0 1-Methylnaphthalene ND 170 17 ug/kg 91-57-6 2-Methylnaphthalene ND 170 17 ug/kg 91-20-3 Naphthalene ND 170 17 ug/kg 98-95-3 Nitrobenzene ND 170 17 ug/kg 621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg 85-01-8 Phenanthrene ND 170 17 ug/kg 129-00-0 Pyrene ND 170 19 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 170 20 ug/kg CAS No.Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 56%40-102% 4165-62-2 Phenol-d5 63%41-100% 118-79-6 2,4,6-Tribromophenol 78%42-108% 4165-60-0 Nitrobenzene-d5 66%40-105% 321-60-8 2-Fluorobiphenyl 67%43-107% 1718-51-0 Terphenyl-d14 72%45-119% 57 of 91 FA7906466.1.2 Blank Spike Summary Page 1 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82157-BS a 9I009850.D 1 09/24/20 MV 09/24/20 OP82157 S9I358 The QC reported here applies to the following samples:Method: EPA 625.1 FA79064-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 65-85-0 Benzoic Acid 100 20.7 21 10-69 59-50-7 4-Chloro-3-methyl Phenol 50 32.1 64 54-103 95-57-8 2-Chlorophenol 50 34.6 69 52-98 120-83-2 2,4-Dichlorophenol 50 35.5 71 53-103 105-67-9 2,4-Dimethylphenol 50 32.9 66 43-90 51-28-5 2,4-Dinitrophenol 100 63.8 64 44-112 534-52-1 4,6-Dinitro-o-cresol 100 75.8 76 66-121 95-48-7 2-Methylphenol 50 25.1 50 43-90 3&4-Methylphenol 100 44.3 44 36-88 88-75-5 2-Nitrophenol 50 36.7 73 53-102 100-02-7 4-Nitrophenol 100 24.5 25 18-62 87-86-5 Pentachlorophenol 100 71.1 71 61-115 108-95-2 Phenol 50 15.5 31 19-56 88-06-2 2,4,6-Trichlorophenol 50 37.9 76 59-107 83-32-9 Acenaphthene 50 39.8 80 61-107 208-96-8 Acenaphthylene 50 45.1 90 60-104 120-12-7 Anthracene 50 39.3 79 65-108 56-55-3 Benzo(a)anthracene 50 41.8 84 66-111 50-32-8 Benzo(a)pyrene 50 40.5 81 62-107 205-99-2 Benzo(b)fluoranthene 50 44.7 89 65-114 191-24-2 Benzo(g,h,i)perylene 50 42.4 85 66-116 207-08-9 Benzo(k)fluoranthene 50 41.6 83 65-114 100-51-6 Benzyl Alcohol 50 31.2 62 46-94 101-55-3 4-Bromophenyl Phenyl Ether 50 40.6 81 65-109 85-68-7 Butyl Benzyl Phthalate 50 42.3 85 65-112 106-47-8 4-Chloroaniline 50 31.3 63 49-105 111-91-1 bis(2-Chloroethoxy)methane 50 32.4 65 51-102 111-44-4 bis(2-Chloroethyl)ether 50 39.1 78 53-100 108-60-1 2,2'-Oxybis(1-chloropropane)50 30.1 60 45-106 91-58-7 2-Chloronaphthalene 50 36.9 74 57-103 7005-72-3 4-Chlorophenyl Phenyl Ether 50 37.3 75 62-105 218-01-9 Chrysene 50 40.9 82 66-111 53-70-3 Dibenzo(a,h)anthracene 50 38.1 76 66-119 132-64-9 Dibenzofuran 50 42.4 85 61-106 95-50-1 1,2-Dichlorobenzene 50 35.9 72 48-97 541-73-1 1,3-Dichlorobenzene 50 39.1 78 45-95 * = Outside of Control Limits. 58 of 91 FA7906466.2.1 Blank Spike Summary Page 2 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82157-BS a 9I009850.D 1 09/24/20 MV 09/24/20 OP82157 S9I358 The QC reported here applies to the following samples:Method: EPA 625.1 FA79064-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 106-46-7 1,4-Dichlorobenzene 50 34.3 69 45-98 91-94-1 3,3'-Dichlorobenzidine 50 43.4 87 46-117 84-66-2 Diethyl Phthalate 50 39.9 80 64-108 131-11-3 Dimethyl Phthalate 50 40.7 81 63-106 84-74-2 Di-n-butyl Phthalate 50 41.2 82 65-107 117-84-0 Di-n-octyl Phthalate 50 44.8 90 62-118 122-66-7 1,2-Diphenylhydrazine 50 36.6 73 61-110 117-81-7 bis(2-Ethylhexyl)phthalate 50 39.3 79 61-117 206-44-0 Fluoranthene 50 40.7 81 63-106 86-73-7 Fluorene 50 39.0 78 62-108 118-74-1 Hexachlorobenzene 50 41.6 83 63-108 87-68-3 Hexachlorobutadiene 50 41.5 83 42-102 77-47-4 Hexachlorocyclopentadiene 50 44.5 89 39-102 67-72-1 Hexachloroethane 50 34.7 69 42-100 193-39-5 Indeno(1,2,3-cd)pyrene 50 40.2 80 64-119 78-59-1 Isophorone 50 34.4 69 43-87 90-12-0 1-Methylnaphthalene 50 35.8 72 53-102 91-57-6 2-Methylnaphthalene 50 54.5 109*51-102 91-20-3 Naphthalene 50 36.6 73 47-100 98-95-3 Nitrobenzene 50 33.4 67 50-104 621-64-7 N-Nitrosodi-n-propylamine 50 33.6 67 52-104 86-30-6 N-Nitrosodiphenylamine 50 38.3 77 64-108 85-01-8 Phenanthrene 50 40.6 81 66-110 129-00-0 Pyrene 50 42.5 85 64-113 120-82-1 1,2,4-Trichlorobenzene 50 36.7 73 45-97 CAS No.Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 39%14-67% 4165-62-2 Phenol-d5 32%10-50% 118-79-6 2,4,6-Tribromophenol 83%33-118% 4165-60-0 Nitrobenzene-d5 65%42-108% 321-60-8 2-Fluorobiphenyl 73%40-106% 1718-51-0 Terphenyl-d14 81%39-121% * = Outside of Control Limits. 59 of 91 FA7906466.2.1 Blank Spike Summary Page 3 of 3 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82157-BS a 9I009850.D 1 09/24/20 MV 09/24/20 OP82157 S9I358 The QC reported here applies to the following samples:Method: EPA 625.1 FA79064-4 (a) Insufficient sample for MS/MSD. * = Outside of Control Limits. 60 of 91 FA7906466.2.1 Blank Spike Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82150-BS 9I009860.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 The QC reported here applies to the following samples:Method: SW846 8270D FA79064-1, FA79064-3 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 65-85-0 Benzoic Acid 3330 2040 61 36-118 59-50-7 4-Chloro-3-methyl Phenol 1670 1060 64 52-108 95-57-8 2-Chlorophenol 1670 972 58 48-104 120-83-2 2,4-Dichlorophenol 1670 1080 65 51-105 105-67-9 2,4-Dimethylphenol 1670 1000 60 43-96 51-28-5 2,4-Dinitrophenol 3330 2080 62 40-119 534-52-1 4,6-Dinitro-o-cresol 3330 2220 67 64-121 95-48-7 2-Methylphenol 1670 956 57 46-107 3&4-Methylphenol 3330 1850 56 44-111 88-75-5 2-Nitrophenol 1670 1090 65 49-104 100-02-7 4-Nitrophenol 3330 2020 61 56-116 87-86-5 Pentachlorophenol 3330 2140 64 61-114 108-95-2 Phenol 1670 999 60 45-110 88-06-2 2,4,6-Trichlorophenol 1670 1150 69 56-109 83-32-9 Acenaphthene 1670 1050 63 56-109 208-96-8 Acenaphthylene 1670 1180 71 56-106 120-12-7 Anthracene 1670 1020 61 61-110 56-55-3 Benzo(a)anthracene 1670 1150 69 66-111 50-32-8 Benzo(a)pyrene 1670 1100 66 59-104 205-99-2 Benzo(b)fluoranthene 1670 1240 74 67-113 191-24-2 Benzo(g,h,i)perylene 1670 1130 68 67-113 207-08-9 Benzo(k)fluoranthene 1670 1160 70 67-114 100-51-6 Benzyl Alcohol 1670 1170 70 53-108 101-55-3 4-Bromophenyl phenyl ether 1670 1090 65 62-110 85-68-7 Butyl benzyl phthalate 1670 1180 71 65-113 106-47-8 4-Chloroaniline 1670 870 52 30-115 111-91-1 bis(2-Chloroethoxy)methane 1670 976 59 48-105 111-44-4 bis(2-Chloroethyl)ether 1670 937 56 46-103 108-60-1 2,2'-Oxybis(1-chloropropane)1670 927 56 40-110 91-58-7 2-Chloronaphthalene 1670 1020 61 53-106 7005-72-3 4-Chlorophenyl phenyl ether 1670 1090 65 58-106 218-01-9 Chrysene 1670 1120 67 65-112 53-70-3 Dibenzo(a,h)anthracene 1670 1040 62*68-115 132-64-9 Dibenzofuran 1670 1110 67 57-108 95-50-1 1,2-Dichlorobenzene 1670 942 57 44-102 541-73-1 1,3-Dichlorobenzene 1670 960 58 42-100 * = Outside of Control Limits. 61 of 91 FA7906466.2.2 Blank Spike Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82150-BS 9I009860.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 The QC reported here applies to the following samples:Method: SW846 8270D FA79064-1, FA79064-3 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 106-46-7 1,4-Dichlorobenzene 1670 886 53 40-106 91-94-1 3,3'-Dichlorobenzidine 1670 1050 63 36-114 84-66-2 Diethyl Phthalate 1670 1170 70 61-109 131-11-3 Dimethyl Phthalate 1670 1100 66 59-108 117-84-0 Di-n-octyl Phthalate 1670 1220 73 64-119 84-74-2 Di-n-butyl Phthalate 1670 1100 66 63-108 122-66-7 1,2-Diphenylhydrazine 1670 1050 63 58-112 117-81-7 bis(2-Ethylhexyl)phthalate 1670 1080 65 64-115 206-44-0 Fluoranthene 1670 1070 64 60-108 86-73-7 Fluorene 1670 1100 66 58-109 118-74-1 Hexachlorobenzene 1670 1090 65 59-111 87-68-3 Hexachlorobutadiene 1670 1090 65 41-108 77-47-4 Hexachlorocyclopentadiene 1670 1280 77 49-110 67-72-1 Hexachloroethane 1670 926 56 40-105 193-39-5 Indeno(1,2,3-cd)pyrene 1670 1070 64*66-116 78-59-1 Isophorone 1670 1020 61 42-89 90-12-0 1-Methylnaphthalene 1670 967 58 49-106 91-57-6 2-Methylnaphthalene 1670 1520 91 47-106 91-20-3 Naphthalene 1670 963 58 44-104 98-95-3 Nitrobenzene 1670 1020 61 43-108 621-64-7 N-Nitrosodi-n-propylamine 1670 979 59 48-108 86-30-6 N-Nitrosodiphenylamine 1670 1020 61*62-110 85-01-8 Phenanthrene 1670 1060 64 63-111 129-00-0 Pyrene 1670 1130 68 65-115 120-82-1 1,2,4-Trichlorobenzene 1670 989 59 45-100 CAS No.Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 51%40-102% 4165-62-2 Phenol-d5 60%41-100% 118-79-6 2,4,6-Tribromophenol 67%42-108% 4165-60-0 Nitrobenzene-d5 57%40-105% 321-60-8 2-Fluorobiphenyl 61%43-107% 1718-51-0 Terphenyl-d14 67%45-119% * = Outside of Control Limits. 62 of 91 FA7906466.2.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82150-MS 9I009864.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 OP82150-MSD 9I009865.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 FA79038-2 9I009863.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 The QC reported here applies to the following samples:Method: SW846 8270D FA79064-1, FA79064-3 FA79038-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 65-85-0 Benzoic Acid 900 U 3600 977 27*109 23.7 22*191*36-118/41 59-50-7 4-Chloro-3-methyl Phenol 180 U 1800 1240 69 54.5 33.7 62 189*52-108/21 95-57-8 2-Chlorophenol 180 U 1800 1150 64 54.5 31.6 58 189*48-104/26 120-83-2 2,4-Dichlorophenol 180 U 1800 1250 70 54.5 33.7 62 189*51-105/27 105-67-9 2,4-Dimethylphenol 180 U 1800 1180 66 54.5 33.2 61 189*43-96/23 51-28-5 2,4-Dinitrophenol 900 U 3600 1390 39*109 31.6 29*191*40-119/32 534-52-1 4,6-Dinitro-o-cresol 360 U 3600 2280 63*109 59.2 54*190*64-121/29 95-48-7 2-Methylphenol 180 U 1800 1130 63 54.5 31.0 57 189*46-107/24 3&4-Methylphenol 180 U 3600 2160 60 109 60.2 55 189*44-111/24 88-75-5 2-Nitrophenol 180 U 1800 1240 69 54.5 34.7 64 189*49-104/27 100-02-7 4-Nitrophenol 900 U 3600 2400 67 109 63.8 59 190*56-116/23 87-86-5 Pentachlorophenol 900 U 3600 2160 60*109 58.3 54*189*61-114/23 108-95-2 Phenol 180 U 1800 1150 64 54.5 32.3 59 189*45-110/24 88-06-2 2,4,6-Trichlorophenol 180 U 1800 1400 78 54.5 37.4 69 190*56-109/25 83-32-9 Acenaphthene 180 U 1800 1260 70 54.5 34.1 63 189*56-109/23 208-96-8 Acenaphthylene 180 U 1800 1410 78 54.5 38.3 70 189*56-106/23 120-12-7 Anthracene 180 U 1800 1260 70 54.5 34.4 63 189*61-110/21 56-55-3 Benzo(a)anthracene 180 U 1800 1390 77 54.5 38.4 71 189*66-111/23 50-32-8 Benzo(a)pyrene 180 U 1800 1310 73 54.5 35.4 65 189*59-104/23 205-99-2 Benzo(b)fluoranthene 24.9 J 1800 1470 80 54.5 38.8 26*190*67-113/24 191-24-2 Benzo(g,h,i)perylene 180 U 1800 1280 71 54.5 34.7 64*189*67-113/21 207-08-9 Benzo(k)fluoranthene 180 U 1800 1400 78 54.5 38.5 71 189*67-114/22 100-51-6 Benzyl Alcohol 180 U 1800 1370 76 54.5 37.4 69 189*53-108/24 101-55-3 4-Bromophenyl phenyl ether 180 U 1800 1350 75 54.5 36.2 66 190*62-110/21 85-68-7 Butyl benzyl phthalate 180 U 1800 1440 80 54.5 39.5 73 189*65-113/20 106-47-8 4-Chloroaniline 180 U 1800 1020 57 54.5 28.4 52 189*30-115/30 111-91-1 bis(2-Chloroethoxy)methane 180 U 1800 1110 62 54.5 30.7 56 189*48-105/24 111-44-4 bis(2-Chloroethyl)ether 180 U 1800 1080 60 54.5 30.0 55 189*46-103/27 108-60-1 2,2'-Oxybis(1-chloropropane)180 U 1800 1080 60 54.5 30.5 56 189*40-110/25 91-58-7 2-Chloronaphthalene 180 U 1800 1210 67 54.5 32.8 60 189*53-106/23 7005-72-3 4-Chlorophenyl phenyl ether 180 U 1800 1300 72 54.5 35.0 64 190*58-106/21 218-01-9 Chrysene 180 U 1800 1350 75 54.5 37.0 68 189*65-112/25 53-70-3 Dibenzo(a,h)anthracene 180 U 1800 1190 66*54.5 31.5 58*190*68-115/23 132-64-9 Dibenzofuran 180 U 1800 1350 75 54.5 36.0 66 190*57-108/22 95-50-1 1,2-Dichlorobenzene 180 U 1800 1100 61 54.5 30.2 55 189*44-102/28 541-73-1 1,3-Dichlorobenzene 180 U 1800 1090 61 54.5 30.9 57 189*42-100/30 * = Outside of Control Limits. 63 of 91 FA7906466.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82150-MS 9I009864.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 OP82150-MSD 9I009865.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 FA79038-2 9I009863.D 1 09/25/20 MV 09/24/20 OP82150 S9I359 The QC reported here applies to the following samples:Method: SW846 8270D FA79064-1, FA79064-3 FA79038-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 106-46-7 1,4-Dichlorobenzene 180 U 1800 1010 56 54.5 28.1 52 189*40-106/29 91-94-1 3,3'-Dichlorobenzidine 180 U 1800 1430 80 54.5 39.5 73 189*36-114/28 84-66-2 Diethyl Phthalate 360 U 1800 1390 77 54.5 37.6 69 189*61-109/20 131-11-3 Dimethyl Phthalate 180 U 1800 1350 75 54.5 35.6 65 190*59-108/20 117-84-0 Di-n-octyl Phthalate 180 U 1800 1470 82 54.5 41.3 76 189*64-119/21 84-74-2 Di-n-butyl Phthalate 360 U 1800 1350 75 54.5 37.0 68 189*63-108/19 122-66-7 1,2-Diphenylhydrazine 180 U 1800 1300 72 54.5 34.9 64 190*58-112/22 117-81-7 bis(2-Ethylhexyl)phthalate 360 U 1800 1330 74 54.5 36.2 66 189*64-115/23 206-44-0 Fluoranthene 180 U 1800 1340 75 54.5 36.9 68 189*60-108/25 86-73-7 Fluorene 180 U 1800 1330 74 54.5 36.1 66 189*58-109/21 118-74-1 Hexachlorobenzene 180 U 1800 1320 73 54.5 35.7 66 189*59-111/21 87-68-3 Hexachlorobutadiene 180 U 1800 1220 68 54.5 34.2 63 189*41-108/27 77-47-4 Hexachlorocyclopentadiene 180 U 1800 1500 83 54.5 40.6 75 189*49-110/31 67-72-1 Hexachloroethane 180 U 1800 1060 59 54.5 29.8 55 189*40-105/32 193-39-5 Indeno(1,2,3-cd)pyrene 180 U 1800 1220 68 54.5 32.8 60*190*66-116/22 78-59-1 Isophorone 180 U 1800 1160 65 54.5 32.3 59 189*42-89/22 90-12-0 1-Methylnaphthalene 180 U 1800 1110 62 54.5 30.1 55 189*49-106/26 91-57-6 2-Methylnaphthalene 180 U 1800 1750 97 54.5 47.2 87 189*47-106/27 91-20-3 Naphthalene 180 U 1800 1100 61 54.5 30.5 56 189*44-104/27 98-95-3 Nitrobenzene 180 U 1800 1130 63 54.5 31.5 58 189*43-108/25 621-64-7 N-Nitrosodi-n-propylamine 180 U 1800 1140 63 54.5 31.5 58 189*48-108/27 86-30-6 N-Nitrosodiphenylamine 180 U 1800 1290 72 54.5 34.9 64 189*62-110/21 85-01-8 Phenanthrene 180 U 1800 1310 73 54.5 35.6 65 189*63-111/22 129-00-0 Pyrene 180 U 1800 1400 78 54.5 38.4 71 189*65-115/25 120-82-1 1,2,4-Trichlorobenzene 180 U 1800 1120 62 54.5 31.1 57 189*45-100/26 CAS No.Surrogate Recoveries MS MSD FA79038-2 Limits 367-12-4 2-Fluorophenol 56%52%48%40-102% 4165-62-2 Phenol-d5 66%60%55%41-100% 118-79-6 2,4,6-Tribromophenol 77%68%61%42-108% 4165-60-0 Nitrobenzene-d5 60%56%55%40-105% 321-60-8 2-Fluorobiphenyl 69%61%57%43-107% 1718-51-0 Terphenyl-d14 75%69%63%45-119% * = Outside of Control Limits. 64 of 91 FA7906466.3.1 SGS North America Inc. GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 7 65 of 91 FA790647 Method Blank Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch G1S87-MB 1S3737.D 1 09/29/20 EG n/a n/a G1S87 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 50 50 ug/kg 100-41-4 Ethylbenzene ND 100 50 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 100 50 ug/kg 91-20-3 Naphthalene ND 250 150 ug/kg 108-88-3 Toluene ND 100 50 ug/kg m,p-Xylene ND 200 100 ug/kg 95-47-6 o-Xylene ND 100 50 ug/kg C5- C8 Aliphatics (Unadj.)ND 5000 1800 ug/kg C9- C12 Aliphatics (Unadj.)ND 5000 1800 ug/kg C9- C10 Aromatics (Unadj.)ND 5000 1800 ug/kg C5- C8 Aliphatics ND 5000 1800 ug/kg C9- C12 Aliphatics ND 5000 1800 ug/kg C9- C10 Aromatics ND 5000 1800 ug/kg CAS No.Surrogate Recoveries Limits 460-00-4 BFB 92%70-130% 460-00-4 BFB 94%70-130% 66 of 91 FA7906477.1.1 Method Blank Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch G1S88-MB 1S3772.D 1 09/30/20 EG n/a n/a G1S88 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-4 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 1.0 ug/l 100-41-4 Ethylbenzene ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l 91-20-3 Naphthalene ND 5.0 3.0 ug/l 108-88-3 Toluene ND 2.0 1.0 ug/l m,p-Xylene ND 4.0 2.0 ug/l 95-47-6 o-Xylene ND 2.0 1.0 ug/l C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l C9- C10 Aromatics (Unadj.)ND 100 35 ug/l C5- C8 Aliphatics ND 100 35 ug/l C9- C12 Aliphatics ND 100 35 ug/l C9- C10 Aromatics ND 100 35 ug/l CAS No.Surrogate Recoveries Limits 460-00-4 BFB 94%70-130% 460-00-4 BFB 99%70-130% 67 of 91 FA7906477.1.2 Method Blank Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82165-MB DD113541.D 1 09/29/20 CV 09/24/20 OP82165 GDD3276 The QC reported here applies to the following samples:Method: EPA 504.1 FA79064-4 CAS No.Compound Result RL MDL Units Q 106-93-4 1,2-Dibromoethane ND 0.020 0.010 ug/l CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 98%63-137% 68 of 91 FA7906477.1.3 Blank Spike Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82165-BS DD113540.D 1 09/29/20 CV 09/24/20 OP82165 GDD3276 The QC reported here applies to the following samples:Method: EPA 504.1 FA79064-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 106-93-4 1,2-Dibromoethane 0.25 0.25 100 70-130 CAS No.Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 100%63-137% * = Outside of Control Limits. 69 of 91 FA7906477.2.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch G1S87-BS 1S3735.D 1 09/29/20 EG n/a n/a G1S87 G1S87-BSD 1S3736.D 1 09/29/20 EG n/a n/a G1S87 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD 71-43-2 Benzene 4080 4160 102 4130 101 1 70-130/25 100-41-4 Ethylbenzene 4080 4100 100 4070 100 1 70-130/25 1634-04-4 Methyl Tert Butyl Ether 4080 4010 98 3950 97 2 70-130/25 91-20-3 Naphthalene 4080 3790 93 3750 92 1 70-130/25 108-88-3 Toluene 4080 4070 100 4040 99 1 70-130/25 m,p-Xylene 8160 8120 100 8080 99 0 70-130/25 95-47-6 o-Xylene 4080 4060 100 4020 99 1 70-130/25 C5- C8 Aliphatics (Unadj.)12200 13400 109 13400 109 0 70-130/25 C9- C12 Aliphatics (Unadj.)8160 6050 74 5930 73 2 70-130/25 C9- C10 Aromatics (Unadj.)4080 4590 113 4550 112 1 70-130/25 C9- C10 Aromatics 4080 4590 113 4550 112 1 70-130/25 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 93%91%70-130% 460-00-4 BFB 94%92%70-130% * = Outside of Control Limits. 70 of 91 FA7906477.3.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch G1S88-BS 1S3770.D 1 09/30/20 EG n/a n/a G1S88 G1S88-BSD 1S3771.D 1 09/30/20 EG n/a n/a G1S88 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-4 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD 71-43-2 Benzene 80 83.1 104 86.1 108 4 70-130/25 100-41-4 Ethylbenzene 80 82.1 103 86.0 108 5 70-130/25 1634-04-4 Methyl Tert Butyl Ether 80 78.3 98 81.9 102 4 70-130/25 91-20-3 Naphthalene 80 74.2 93 77.8 97 5 70-130/25 108-88-3 Toluene 80 81.3 102 85.1 106 5 70-130/25 m,p-Xylene 160 163 102 170 106 4 70-130/25 95-47-6 o-Xylene 80 81.5 102 84.9 106 4 70-130/25 C5- C8 Aliphatics (Unadj.)240 240 100 259 108 8 70-130/25 C9- C12 Aliphatics (Unadj.)160 117 73 118 74 1 70-130/25 C9- C10 Aromatics (Unadj.)80 89.0 111 92.3 115 4 70-130/25 C9- C10 Aromatics 80 89.0 111 92.3 115 4 70-130/25 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 92%94%70-130% 460-00-4 BFB 97%99%70-130% * = Outside of Control Limits. 71 of 91 FA7906477.3.2 Matrix Spike Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79164-4MS 1S3765.D 1 09/30/20 EG n/a n/a G1S87 FA79164-4 1S3759.D 1 09/30/20 EG n/a n/a G1S87 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 FA79164-4 Spike MS MS CAS No.Compound ug/kg Q ug/kg ug/kg %Limits 71-43-2 Benzene ND 8530 8850 104 70-130 100-41-4 Ethylbenzene ND 8530 8750 103 70-130 1634-04-4 Methyl Tert Butyl Ether ND 8530 7790 91 70-130 91-20-3 Naphthalene ND 8530 7320 86 70-130 108-88-3 Toluene ND 8530 8670 102 70-130 m,p-Xylene ND 17100 17300 101 70-130 95-47-6 o-Xylene ND 8530 8650 101 70-130 C5- C8 Aliphatics (Unadj.)ND 51200 54400 106 70-130 C9- C12 Aliphatics (Unadj.)ND 42600 49100 115 70-130 C9- C10 Aromatics (Unadj.)ND 25600 9360 37*70-130 C9- C10 Aromatics ND 25600 9360 37*70-130 CAS No.Surrogate Recoveries MS FA79164-4 Limits 460-00-4 BFB 93%95%70-130% 460-00-4 BFB 97%99%70-130% * = Outside of Control Limits. 72 of 91 FA7906477.4.1 Matrix Spike Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79007-1MS 1S3779.D 1 09/30/20 EG n/a n/a G1S88 FA79007-1 1S3773.D 1 09/30/20 EG n/a n/a G1S88 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-4 FA79007-1 Spike MS MS CAS No.Compound ug/l Q ug/l ug/l %Limits 71-43-2 Benzene ND 80 86.7 108 70-130 100-41-4 Ethylbenzene ND 80 86.5 108 70-130 1634-04-4 Methyl Tert Butyl Ether ND 80 74.9 94 70-130 91-20-3 Naphthalene ND 80 69.6 87 70-130 108-88-3 Toluene ND 80 93.9 117 70-130 m,p-Xylene ND 160 171 107 70-130 95-47-6 o-Xylene ND 80 84.7 106 70-130 C5- C8 Aliphatics (Unadj.)ND 480 526 110 70-130 C9- C12 Aliphatics (Unadj.)ND 400 480 120 70-130 C9- C10 Aromatics (Unadj.)ND 240 94.1 39*70-130 C9- C10 Aromatics ND 240 94.1 39*70-130 CAS No.Surrogate Recoveries MS FA79007-1 Limits 460-00-4 BFB 90%91%70-130% 460-00-4 BFB 95%95%70-130% * = Outside of Control Limits. 73 of 91 FA7906477.4.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82165-MS DD113547.D 1 09/29/20 CV 09/24/20 OP82165 GDD3276 OP82165-MSD DD113548.D 1 09/29/20 CV 09/24/20 OP82165 GDD3276 FA79086-1 DD113544.D 1 09/29/20 CV 09/24/20 OP82165 GDD3276 The QC reported here applies to the following samples:Method: EPA 504.1 FA79064-4 FA79086-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 106-93-4 1,2-Dibromoethane 0.019 U 0.238 0.24 101 0.242 0.25 103 4 70-130/25 CAS No.Surrogate Recoveries MS MSD FA79086-1 Limits 460-00-4 4-Bromofluorobenzene 105%104%98%63-137% * = Outside of Control Limits. 74 of 91 FA7906477.5.1 Duplicate Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79164-4DUP 1S3760.D 1 09/30/20 EG n/a n/a G1S87 FA79164-4 1S3759.D 1 09/30/20 EG n/a n/a G1S87 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 FA79164-4 DUP CAS No.Compound ug/kg Q ug/kg Q RPD Limits 71-43-2 Benzene ND ND nc 50 100-41-4 Ethylbenzene ND ND nc 50 1634-04-4 Methyl Tert Butyl Ether ND ND nc 50 91-20-3 Naphthalene ND ND nc 50 108-88-3 Toluene ND ND nc 50 m,p-Xylene ND ND nc 50 95-47-6 o-Xylene ND ND nc 50 C5- C8 Aliphatics (Unadj.)ND ND nc 50 C9- C12 Aliphatics (Unadj.)ND ND nc 50 C9- C10 Aromatics (Unadj.)ND ND nc 50 C5- C8 Aliphatics ND ND nc 50 C9- C12 Aliphatics ND ND nc 50 C9- C10 Aromatics ND ND nc 50 CAS No.Surrogate Recoveries DUP FA79164-4 Limits 460-00-4 BFB 94%95%70-130% 460-00-4 BFB 98%99%70-130% * = Outside of Control Limits. 75 of 91 FA7906477.6.1 Duplicate Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA79007-1DUP 1S3774.D 1 09/30/20 EG n/a n/a G1S88 FA79007-1 1S3773.D 1 09/30/20 EG n/a n/a G1S88 The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1 FA79064-4 FA79007-1 DUP CAS No.Compound ug/l Q ug/l Q RPD Limits 71-43-2 Benzene ND ND nc 50 100-41-4 Ethylbenzene ND ND nc 50 1634-04-4 Methyl Tert Butyl Ether ND ND nc 50 91-20-3 Naphthalene ND ND nc 50 108-88-3 Toluene ND ND nc 50 m,p-Xylene ND ND nc 50 95-47-6 o-Xylene ND ND nc 50 C5- C8 Aliphatics (Unadj.)ND ND nc 50 C9- C12 Aliphatics (Unadj.)ND ND nc 50 C9- C10 Aromatics (Unadj.)ND ND nc 50 C5- C8 Aliphatics ND ND nc 50 C9- C12 Aliphatics ND ND nc 50 C9- C10 Aromatics ND ND nc 50 CAS No.Surrogate Recoveries DUP FA79007-1 Limits 460-00-4 BFB 92%91%70-130% 460-00-4 BFB 97%95%70-130% * = Outside of Control Limits. 76 of 91 FA7906477.6.2 SGS North America Inc. GC/LC Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 8 77 of 91 FA790648 Method Blank Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82174-MB NN029960.D 1 09/29/20 JA 09/25/20 OP82174 GNN1465 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-4 CAS No.Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 4.0 2.0 ug/l 208-96-8 Acenaphthylene ND 4.0 2.0 ug/l 120-12-7 Anthracene ND 4.0 2.0 ug/l 56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l 50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l 205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l 191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l 207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l 218-01-9 Chrysene ND 4.0 2.0 ug/l 53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l 206-44-0 Fluoranthene ND 4.0 2.0 ug/l 86-73-7 Fluorene ND 4.0 2.0 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l 91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l 91-20-3 Naphthalene ND 4.0 2.0 ug/l 85-01-8 Phenanthrene ND 4.0 2.0 ug/l 129-00-0 Pyrene ND 4.0 2.0 ug/l C11-C22 Aromatics (Unadj.)ND 200 80 ug/l C11-C22 Aromatics ND 200 80 ug/l C9-C18 Aliphatics ND 200 50 ug/l C19-C36 Aliphatics ND 200 50 ug/l CAS No.Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane 83%40-140% 580-13-2 2-Bromonaphthalene 69%40-140% 84-15-1 o-Terphenyl 72%40-140% 321-60-8 2-Fluorobiphenyl 67%40-140% 78 of 91 FA7906488.1.1 Method Blank Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82169-MB NN029971.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 CAS No.Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 200 100 ug/kg 208-96-8 Acenaphthylene ND 200 100 ug/kg 120-12-7 Anthracene ND 200 100 ug/kg 56-55-3 Benzo(a)anthracene ND 200 100 ug/kg 50-32-8 Benzo(a)pyrene ND 200 100 ug/kg 205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg 207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg 218-01-9 Chrysene ND 200 100 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg 206-44-0 Fluoranthene ND 200 100 ug/kg 86-73-7 Fluorene ND 200 100 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg 91-57-6 2-Methylnaphthalene ND 200 100 ug/kg 91-20-3 Naphthalene ND 200 100 ug/kg 85-01-8 Phenanthrene ND 200 100 ug/kg 129-00-0 Pyrene ND 200 100 ug/kg C11-C22 Aromatics (Unadj.)ND 10000 4000 ug/kg C11-C22 Aromatics ND 10000 4000 ug/kg C9-C18 Aliphatics ND 10000 2500 ug/kg C19-C36 Aliphatics ND 10000 2500 ug/kg CAS No.Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane 65%40-140% 580-13-2 2-Bromonaphthalene 65%40-140% 84-15-1 o-Terphenyl 55%40-140% 321-60-8 2-Fluorobiphenyl 62%40-140% 79 of 91 FA7906488.1.2 Blank Spike Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82174-BS a NN029961.D 1 09/29/20 JA 09/25/20 OP82174 GNN1465 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 83-32-9 Acenaphthene 100 84.2 84 40-140 208-96-8 Acenaphthylene 100 84.2 84 40-140 120-12-7 Anthracene 100 95.6 96 40-140 56-55-3 Benzo(a)anthracene 100 101 101 40-140 50-32-8 Benzo(a)pyrene 100 102 102 40-140 205-99-2 Benzo(b)fluoranthene 100 102 102 40-140 191-24-2 Benzo(g,h,i)perylene 100 101 101 40-140 207-08-9 Benzo(k)fluoranthene 100 105 105 40-140 218-01-9 Chrysene 100 105 105 40-140 53-70-3 Dibenzo(a,h)anthracene 100 111 111 40-140 206-44-0 Fluoranthene 100 99.7 100 40-140 86-73-7 Fluorene 100 89.1 89 40-140 193-39-5 Indeno(1,2,3-cd)pyrene 100 107 107 40-140 91-57-6 2-Methylnaphthalene 100 76.1 76 40-140 91-20-3 Naphthalene 100 70.4 70 40-140 85-01-8 Phenanthrene 100 91.9 92 40-140 129-00-0 Pyrene 100 102 102 40-140 C11-C22 Aromatics (Unadj.)1700 1660 98 40-140 C11-C22 Aromatics 1700 ND 0*50-150 b C9-C18 Aliphatics 600 467 78 40-140 C19-C36 Aliphatics 800 771 96 40-140 CAS No.Surrogate Recoveries BSP Limits 3386-33-2 1-Chlorooctadecane 80%40-140% 580-13-2 2-Bromonaphthalene 84%40-140% 84-15-1 o-Terphenyl 82%40-140% 321-60-8 2-Fluorobiphenyl 80%40-140% Sample Compound Col #1 Col #2 Breakthrough Limit OP82174-BS 2-Methylnaphthalene 76.1 ND 0.0%5.0 OP82174-BS Naphthalene 70.4 ND 0.0%5.0 (a) BSD unavailable due to loss during sample fractionation. * = Outside of Control Limits. 80 of 91 FA7906488.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82174-BS a NN029961.D 1 09/29/20 JA 09/25/20 OP82174 GNN1465 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-4 (b) Advisory control limits. * = Outside of Control Limits. 81 of 91 FA7906488.2.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82169-BS NN029972.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 OP82169-BSD NN029973.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD 83-32-9 Acenaphthene 5000 3120 62 3350 67 7 40-140/30 208-96-8 Acenaphthylene 5000 3140 63 3380 68 7 40-140/30 120-12-7 Anthracene 5000 3370 67 3610 72 7 40-140/30 56-55-3 Benzo(a)anthracene 5000 3480 70 3760 75 8 40-140/30 50-32-8 Benzo(a)pyrene 5000 3510 70 3780 76 7 40-140/30 205-99-2 Benzo(b)fluoranthene 5000 3430 69 3710 74 8 40-140/30 191-24-2 Benzo(g,h,i)perylene 5000 3510 70 3790 76 8 40-140/30 207-08-9 Benzo(k)fluoranthene 5000 3600 72 3900 78 8 40-140/30 218-01-9 Chrysene 5000 3600 72 3890 78 8 40-140/30 53-70-3 Dibenzo(a,h)anthracene 5000 3900 78 4240 85 8 40-140/30 206-44-0 Fluoranthene 5000 3460 69 3690 74 6 40-140/30 86-73-7 Fluorene 5000 3300 66 3510 70 6 40-140/30 193-39-5 Indeno(1,2,3-cd)pyrene 5000 3670 73 3950 79 7 40-140/30 91-57-6 2-Methylnaphthalene 5000 2800 56 3030 61 8 40-140/30 91-20-3 Naphthalene 5000 2590 52 2790 56 7 40-140/30 85-01-8 Phenanthrene 5000 3270 65 3470 69 6 40-140/30 129-00-0 Pyrene 5000 3540 71 3790 76 7 40-140/30 C11-C22 Aromatics (Unadj.)85000 59800 70 64100 75 7 40-140/30 C11-C22 Aromatics 85000 ND 0*ND 0*nc 50-150/30 a C9-C18 Aliphatics 30000 18400 61 16200 54 13 40-140/30 C19-C36 Aliphatics 40000 27300 68 24700 62 10 40-140/30 CAS No.Surrogate Recoveries BSP BSD Limits 3386-33-2 1-Chlorooctadecane 70%63%40-140% 580-13-2 2-Bromonaphthalene 67%72%40-140% 84-15-1 o-Terphenyl 57%62%40-140% 321-60-8 2-Fluorobiphenyl 63%69%40-140% Sample Compound Col #1 Col #2 Breakthrough Limit OP82169-BS 2-Methylnaphthalene 2800 ND 0.0%5.0 OP82169-BS Naphthalene 2590 ND 0.0%5.0 OP82169-BSD 2-Methylnaphthalene 3030 ND 0.0%5.0 OP82169-BSD Naphthalene 2790 ND 0.0%5.0 * = Outside of Control Limits. 82 of 91 FA7906488.3.1 Blank Spike/Blank Spike Duplicate Summary Page 2 of 2 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82169-BS NN029972.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 OP82169-BSD NN029973.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 (a) Advisory control limits. * = Outside of Control Limits. 83 of 91 FA7906488.3.1 Duplicate Summary Page 1 of 1 Job Number:FA79064 Account:RENCM Resolve Environmental Project:Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP82169-DUP NN029975.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 FA79064-3 NN029974.D 1 09/30/20 JA 09/25/20 OP82169 GNN1466 The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1 FA79064-1, FA79064-2, FA79064-3 FA79064-3 DUP CAS No.Compound ug/kg Q ug/kg Q RPD Limits 83-32-9 Acenaphthene ND ND nc 30 a 208-96-8 Acenaphthylene ND ND nc 30 a 120-12-7 Anthracene ND ND nc 30 a 56-55-3 Benzo(a)anthracene ND ND nc 30 a 50-32-8 Benzo(a)pyrene ND ND nc 30 a 205-99-2 Benzo(b)fluoranthene ND ND nc 30 a 191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a 207-08-9 Benzo(k)fluoranthene ND ND nc 30 a 218-01-9 Chrysene ND ND nc 30 a 53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 a 206-44-0 Fluoranthene ND ND nc 30 a 86-73-7 Fluorene ND ND nc 30 a 193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 a 91-57-6 2-Methylnaphthalene ND ND nc 30 a 91-20-3 Naphthalene ND ND nc 30 a 85-01-8 Phenanthrene ND ND nc 30 a 129-00-0 Pyrene ND ND nc 30 a C11-C22 Aromatics (Unadj.)ND ND nc 30 a C11-C22 Aromatics ND ND nc 30 a C9-C18 Aliphatics ND ND nc 30 a C19-C36 Aliphatics ND ND nc 30 a CAS No.Surrogate Recoveries DUP FA79064-3 Limits 3386-33-2 1-Chlorooctadecane 55%60%40-140% 580-13-2 2-Bromonaphthalene 68%67%40-140% 84-15-1 o-Terphenyl 49%56%40-140% 321-60-8 2-Fluorobiphenyl 65%64%40-140% (a) Advisory control limits. * = Outside of Control Limits. 84 of 91 FA7906488.4.1 SGS North America Inc. Metals Analysis QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries Orlando, FL Section 9 85 of 91 FA790649 BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: FA79064 Account: RENCM - Resolve Environmental Project: Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC QC Batch ID: MP37857 Methods: SW846 6010D Matrix Type: AQUEOUS Units: ug/l Prep Date: 09/25/20 MB Metal RL IDL MDL raw final Aluminum 200 14 14 Antimony 6.0 1 1 Arsenic 10 1.3 1.3 Barium 200 1 1 Beryllium 4.0 .2 .2 Cadmium 5.0 .2 .2 Calcium 1000 50 50 Chromium 10 1 1 Cobalt 50 .2 .2 Copper 25 1 1 Iron 300 17 17 Lead 5.0 1 1.1 -1.2 <5.0 Magnesium 5000 35 35 Manganese 15 .5 1 Molybdenum 50 .3 .3 Nickel 40 .4 .4 Potassium 10000 200 200 Selenium 10 2.4 2.9 Silver 10 .7 .7 Sodium 10000 500 500 Strontium 10 .5 .5 Thallium 10 1.1 1.4 Tin 50 .9 1 Titanium 10 .5 1 Vanadium 50 .5 .6 Zinc 20 3 4.4 Associated samples MP37857: FA79064-4 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested _________________________________________________________________________________________________________ Page 1 86 of 91 FA7906499.1.1 MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: FA79064 Account: RENCM - Resolve Environmental Project: Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC QC Batch ID: MP37857 Methods: SW846 6010D Matrix Type: AQUEOUS Units: ug/l Prep Date: 09/25/20 09/25/20 FA79042-1 QC FA79042-1 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium anr Chromium Cobalt Copper anr Iron anr Lead 342 351 2.6 0-20 342 797 500 91.0 80-120 Magnesium anr Manganese Molybdenum anr Nickel anr Potassium Selenium anr Silver Sodium Strontium Thallium anr Tin Titanium Vanadium Zinc anr Associated samples MP37857: FA79064-4 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested _________________________________________________________________________________________________________ Page 1 87 of 91 FA7906499.1.2 MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: FA79064 Account: RENCM - Resolve Environmental Project: Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC QC Batch ID: MP37857 Methods: SW846 6010D Matrix Type: AQUEOUS Units: ug/l Prep Date: 09/25/20 FA79042-1 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium anr Chromium Cobalt Copper anr Iron anr Lead 342 825 500 96.6 3.5 20 Magnesium anr Manganese Molybdenum anr Nickel anr Potassium Selenium anr Silver Sodium Strontium Thallium anr Tin Titanium Vanadium Zinc anr Associated samples MP37857: FA79064-4 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested _________________________________________________________________________________________________________ Page 2 88 of 91 FA7906499.1.2 SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: FA79064 Account: RENCM - Resolve Environmental Project: Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC QC Batch ID: MP37857 Methods: SW846 6010D Matrix Type: AQUEOUS Units: ug/l Prep Date: 09/25/20 BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium anr Chromium Cobalt Copper anr Iron anr Lead 488 500 97.6 80-120 Magnesium anr Manganese Molybdenum anr Nickel anr Potassium Selenium anr Silver Sodium Strontium Thallium anr Tin Titanium Vanadium Zinc anr Associated samples MP37857: FA79064-4 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested _________________________________________________________________________________________________________ Page 1 89 of 91 FA7906499.1.3 SERIAL DILUTION RESULTS SUMMARY Login Number: FA79064 Account: RENCM - Resolve Environmental Project: Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC QC Batch ID: MP37857 Methods: SW846 6010D Matrix Type: AQUEOUS Units: ug/l Prep Date: 09/25/20 FA79042-1 QC Metal Original SDL 1:5 %DIF Limits Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium anr Chromium Cobalt Copper anr Iron anr Lead 342 345 1.0 0-10 Magnesium anr Manganese Molybdenum anr Nickel anr Potassium Selenium anr Silver Sodium Strontium Thallium anr Tin Titanium Vanadium Zinc anr Associated samples MP37857: FA79064-4 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested _________________________________________________________________________________________________________ Page 1 90 of 91 FA7906499.1.4 POST DIGESTATE SPIKE SUMMARY Login Number: FA79064 Account: RENCM - Resolve Environmental Project: Kwick Mart; 10308 Albemarle Rd, Mint Hill, NC QC Batch ID: MP37857 Methods: SW846 6010D Matrix Type: AQUEOUS Units: ug/l Prep Date: 09/25/20 Sample Final FA79042-1 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead 9.8 10 341.5 334.67 388.6 0.2 2.5 50 107.9 80-120 Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Associated samples MP37857: FA79064-4 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (**) Corr. sample result = Raw * (sample volume / final volume) (anr) Analyte not requested _________________________________________________________________________________________________________ Page 1 91 of 91 FA7906499.1.5