MO-27965_47256_CA_LAB_20220720

 
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/19/2022
Resolve Environmental Laura Minor
500 Devonport Dr. Matthews, NC, 28104
Ref: Analytical Testing
Lab Report Number: 22-192-0008 Client Project Description: Kwik Mart
Dear Laura Minor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/11/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Danyale Love Project Manager
Page 1 of 34
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-192-0008
Page 2 of 34
Report Number:
Sample Summary Table
Client Project Description:
22-192-0008
Kwik Mart
Lab No Client Sample ID Matrix Date Collected Date Received
07/08/2022 15:50Aqueous 93996 WSW-1 07/11/2022 12:04
07/08/2022 16:12Aqueous 93997 WSW-2 07/11/2022 12:04
07/08/2022 16:22Aqueous 93998 WSW-5 07/11/2022 12:04
07/08/2022 16:48Aqueous 93999 WSW-10 07/11/2022 12:04
Page 3 of 34
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-192-0008
Report Limit
Project:Kwik Mart
V 93996WSW-1
2.66 07/16/2022 12:326200BTrichloroetheneµg/L 0.500
V 93997WSW-2
1.80 07/16/2022 12:566200BMethyl tert-butyl ether (MTBE)µg/L 1.00
1.01 07/16/2022 12:566200BTrichloroetheneµg/L 0.500
V 93998WSW-5
13.6 07/16/2022 13:206200BBromodichloromethaneµg/L 0.500
3.83 07/16/2022 13:206200BChlorodibromomethaneµg/L 0.500
46.5 07/16/2022 13:206200BChloroformµg/L 0.500
Page 4 of 34

Client: Resolve Environmental CASE NARRATIVE
Project: Kwik Mart Lab Report Number: 22-192-0008
Date: 7/19/2022
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V21442/V21441
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.

Page 5 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-1
93996 Matrix:
7/8/2022 15:50
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.03,3-Dimethyl-1-butanol 1 07/16/22 12:32 6200BJLB
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/16/22 12:321 JLB V21442
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%07/16/22 12:321 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 95.2 Limits: 70-130%07/16/22 12:321 JLB V21442
Surrogate: Toluene-d8 92.2 Limits: 70-130%07/16/22 12:321 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-1
93996 Matrix:
7/8/2022 15:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<10.0 µg/L 10.0Acetone 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Benzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Bromobenzene 1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.00Bromochloromethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/16/22 12:32 V21442JLB
<5.00 µg/L 5.00Bromoform 1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.00Bromomethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/16/22 12:32 V21442JLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Chlorobenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.00Chloroethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Chloroform 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Chloromethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/16/22 12:32 V21442JLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Dibromomethane 1 07/16/22 12:32 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-1
93996 Matrix:
7/8/2022 15:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/16/22 12:32 V21442JLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/16/22 12:32 V21442JLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/16/22 12:32 V21442JLB
<200 µg/L 200Ethanol 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Ethylbenzene 1 07/16/22 12:32 V21442JLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.002-Hexanone 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/16/22 12:32 V21442JLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/16/22 12:32 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-1
93996 Matrix:
7/8/2022 15:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/16/22 12:32 V21442JLB
<2.00 µg/L 2.00Methylene Chloride 1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.00Naphthalene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Styrene 1 07/16/22 12:32 V21442JLB
<10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 07/16/22 12:32 V21442JLB
<10.0 µg/L 10.0tert-Butyl formate (TBF)1 07/16/22 12:32 V21442JLB
<10.0 µg/L 10.0tert-Amyl Alcohol (TAA)1 07/16/22 12:32 V21442JLB
<10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Toluene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/16/22 12:32 V21442JLB
2.66 µg/L 0.500Trichloroethene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 07/16/22 12:32 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-1
93996 Matrix:
7/8/2022 15:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/16/22 12:32 V21442JLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500o-Xylene 1 07/16/22 12:32 V21442JLB
<1.00 µg/L 1.00m,p-Xylene 1 07/16/22 12:32 V21442JLB
<0.500 µg/L 0.500Xylene (Total)1 07/16/22 12:32 V21442
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/16/22 12:321 JLB V21442
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%07/16/22 12:321 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 95.2 Limits: 70-130%07/16/22 12:321 JLB V21442
Surrogate: Toluene-d8 92.2 Limits: 70-130%07/16/22 12:321 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-2
93997 Matrix:
7/8/2022 16:12
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.03,3-Dimethyl-1-butanol 1 07/16/22 12:56 6200BJLB
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/16/22 12:561 JLB V21442
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%07/16/22 12:561 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%07/16/22 12:561 JLB V21442
Surrogate: Toluene-d8 93.2 Limits: 70-130%07/16/22 12:561 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-2
93997 Matrix:
7/8/2022 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<10.0 µg/L 10.0Acetone 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Benzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Bromobenzene 1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.00Bromochloromethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/16/22 12:56 V21442JLB
<5.00 µg/L 5.00Bromoform 1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.00Bromomethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/16/22 12:56 V21442JLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Chlorobenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.00Chloroethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Chloroform 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Chloromethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/16/22 12:56 V21442JLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Dibromomethane 1 07/16/22 12:56 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-2
93997 Matrix:
7/8/2022 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/16/22 12:56 V21442JLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/16/22 12:56 V21442JLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/16/22 12:56 V21442JLB
<200 µg/L 200Ethanol 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Ethylbenzene 1 07/16/22 12:56 V21442JLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.002-Hexanone 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/16/22 12:56 V21442JLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/16/22 12:56 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-2
93997 Matrix:
7/8/2022 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
1.80 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/16/22 12:56 V21442JLB
<2.00 µg/L 2.00Methylene Chloride 1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.00Naphthalene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Styrene 1 07/16/22 12:56 V21442JLB
<10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 07/16/22 12:56 V21442JLB
<10.0 µg/L 10.0tert-Butyl formate (TBF)1 07/16/22 12:56 V21442JLB
<10.0 µg/L 10.0tert-Amyl Alcohol (TAA)1 07/16/22 12:56 V21442JLB
<10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Toluene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/16/22 12:56 V21442JLB
1.01 µg/L 0.500Trichloroethene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 07/16/22 12:56 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-2
93997 Matrix:
7/8/2022 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/16/22 12:56 V21442JLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500o-Xylene 1 07/16/22 12:56 V21442JLB
<1.00 µg/L 1.00m,p-Xylene 1 07/16/22 12:56 V21442JLB
<0.500 µg/L 0.500Xylene (Total)1 07/16/22 12:56 V21442
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/16/22 12:561 JLB V21442
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%07/16/22 12:561 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%07/16/22 12:561 JLB V21442
Surrogate: Toluene-d8 93.2 Limits: 70-130%07/16/22 12:561 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-5
93998 Matrix:
7/8/2022 16:22
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.03,3-Dimethyl-1-butanol 1 07/16/22 13:20 6200BJLB
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/16/22 13:201 JLB V21442
Surrogate: Dibromofluoromethane 104 Limits: 70-130%07/16/22 13:201 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%07/16/22 13:201 JLB V21442
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/16/22 13:201 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-5
93998 Matrix:
7/8/2022 16:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<10.0 µg/L 10.0Acetone 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Benzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Bromobenzene 1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.00Bromochloromethane 1 07/16/22 13:20 V21442JLB
13.6 µg/L 0.500Bromodichloromethane 1 07/16/22 13:20 V21442JLB
<5.00 µg/L 5.00Bromoform 1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.00Bromomethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/16/22 13:20 V21442JLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Chlorobenzene 1 07/16/22 13:20 V21442JLB
3.83 µg/L 0.500Chlorodibromomethane 1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.00Chloroethane 1 07/16/22 13:20 V21442JLB
46.5 µg/L 0.500Chloroform 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Chloromethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/16/22 13:20 V21442JLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Dibromomethane 1 07/16/22 13:20 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-5
93998 Matrix:
7/8/2022 16:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/16/22 13:20 V21442JLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/16/22 13:20 V21442JLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/16/22 13:20 V21442JLB
<200 µg/L 200Ethanol 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Ethylbenzene 1 07/16/22 13:20 V21442JLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.002-Hexanone 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/16/22 13:20 V21442JLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/16/22 13:20 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-5
93998 Matrix:
7/8/2022 16:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/16/22 13:20 V21442JLB
<2.00 µg/L 2.00Methylene Chloride 1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.00Naphthalene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Styrene 1 07/16/22 13:20 V21442JLB
<10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 07/16/22 13:20 V21442JLB
<10.0 µg/L 10.0tert-Butyl formate (TBF)1 07/16/22 13:20 V21442JLB
<10.0 µg/L 10.0tert-Amyl Alcohol (TAA)1 07/16/22 13:20 V21442JLB
<10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Toluene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Trichloroethene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 07/16/22 13:20 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-5
93998 Matrix:
7/8/2022 16:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/16/22 13:20 V21442JLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500o-Xylene 1 07/16/22 13:20 V21442JLB
<1.00 µg/L 1.00m,p-Xylene 1 07/16/22 13:20 V21442JLB
<0.500 µg/L 0.500Xylene (Total)1 07/16/22 13:20 V21442
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/16/22 13:201 JLB V21442
Surrogate: Dibromofluoromethane 104 Limits: 70-130%07/16/22 13:201 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%07/16/22 13:201 JLB V21442
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/16/22 13:201 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-10
93999 Matrix:
7/8/2022 16:48
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.03,3-Dimethyl-1-butanol 1 07/16/22 13:44 6200BJLB
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%07/16/22 13:441 JLB V21442
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%07/16/22 13:441 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%07/16/22 13:441 JLB V21442
Surrogate: Toluene-d8 91.8 Limits: 70-130%07/16/22 13:441 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-10
93999 Matrix:
7/8/2022 16:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<10.0 µg/L 10.0Acetone 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Benzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Bromobenzene 1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.00Bromochloromethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/16/22 13:44 V21442JLB
<5.00 µg/L 5.00Bromoform 1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.00Bromomethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/16/22 13:44 V21442JLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Chlorobenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.00Chloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Chloroform 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Chloromethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/16/22 13:44 V21442JLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Dibromomethane 1 07/16/22 13:44 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-10
93999 Matrix:
7/8/2022 16:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/16/22 13:44 V21442JLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/16/22 13:44 V21442JLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/16/22 13:44 V21442JLB
<200 µg/L 200Ethanol 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Ethylbenzene 1 07/16/22 13:44 V21442JLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.002-Hexanone 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/16/22 13:44 V21442JLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/16/22 13:44 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-10
93999 Matrix:
7/8/2022 16:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/16/22 13:44 V21442JLB
<2.00 µg/L 2.00Methylene Chloride 1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.00Naphthalene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Styrene 1 07/16/22 13:44 V21442JLB
<10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 07/16/22 13:44 V21442JLB
<10.0 µg/L 10.0tert-Butyl formate (TBF)1 07/16/22 13:44 V21442JLB
<10.0 µg/L 10.0tert-Amyl Alcohol (TAA)1 07/16/22 13:44 V21442JLB
<10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Toluene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Trichloroethene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 07/16/22 13:44 V21442JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
22-192-0008
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 07/11/2022
Kwik Mart
Report Date : 07/19/2022
Sample ID :
Lab No :
Sampled:WSW-10
93999 Matrix:
7/8/2022 16:48
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21441 07/15/22 20:00
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/16/22 13:44 V21442JLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500o-Xylene 1 07/16/22 13:44 V21442JLB
<1.00 µg/L 1.00m,p-Xylene 1 07/16/22 13:44 V21442JLB
<0.500 µg/L 0.500Xylene (Total)1 07/16/22 13:44 V21442
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%07/16/22 13:441 JLB V21442
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%07/16/22 13:441 JLB V21442
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%07/16/22 13:441 JLB V21442
Surrogate: Toluene-d8 91.8 Limits: 70-130%07/16/22 13:441 JLB V21442
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
Associated Lab Samples: 93996, 93997, 93998, 93999
LRB-V21441 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/16/22 12:0810.0< 10.0µg/LAcetone
07/16/22 12:080.500< 0.500µg/LBenzene
07/16/22 12:080.500< 0.500µg/LBromobenzene
07/16/22 12:081.00< 1.00µg/LBromochloromethane
07/16/22 12:080.500< 0.500µg/LBromodichloromethane
07/16/22 12:085.00< 5.00µg/LBromoform
07/16/22 12:081.00< 1.00µg/LBromomethane
07/16/22 12:080.500< 0.500µg/Ln-Butylbenzene
07/16/22 12:080.500< 0.500µg/Lsec-Butyl benzene
07/16/22 12:082.00< 2.00µg/Ltert-Butyl benzene
07/16/22 12:080.500< 0.500µg/LCarbon Tetrachloride
07/16/22 12:080.500< 0.500µg/LChlorobenzene
07/16/22 12:080.500< 0.500µg/LChlorodibromomethane
07/16/22 12:081.00< 1.00µg/LChloroethane
07/16/22 12:080.500< 0.500µg/LChloroform
07/16/22 12:080.500< 0.500µg/LChloromethane
07/16/22 12:080.500< 0.500µg/L2-Chlorotoluene
07/16/22 12:080.500< 0.500µg/L4-Chlorotoluene
07/16/22 12:080.500< 0.500µg/LDi-Isopropyl Ether (DIPE)
07/16/22 12:082.00< 2.00µg/L1,2-Dibromo-3-Chloropropane
07/16/22 12:080.500< 0.500µg/L1,2-Dibromoethane
07/16/22 12:080.500< 0.500µg/LDibromomethane
07/16/22 12:080.500< 0.500µg/L1,2-Dichlorobenzene
07/16/22 12:080.500< 0.500µg/L1,3-Dichlorobenzene
07/16/22 12:080.500< 0.500µg/L1,4-Dichlorobenzene
07/16/22 12:085.00< 5.00µg/LDichlorodifluoromethane
07/16/22 12:080.500< 0.500µg/L1,1-Dichloroethane
Page 1 of 7Date:07/19/2022 05:05 PM
Page 26 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
Associated Lab Samples: 93996, 93997, 93998, 93999
LRB-V21441 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/16/22 12:080.500< 0.500µg/L1,2-Dichloroethane
07/16/22 12:080.500< 0.500µg/L1,1-Dichloroethene
07/16/22 12:080.500< 0.500µg/Lcis-1,2-Dichloroethene
07/16/22 12:080.500< 0.500µg/Ltrans-1,2-Dichloroethene
07/16/22 12:080.500< 0.500µg/L1,2-Dichloropropane
07/16/22 12:080.500< 0.500µg/L1,3-Dichloropropane
07/16/22 12:082.00< 2.00µg/L2,2-Dichloropropane
07/16/22 12:080.500< 0.500µg/L1,1-Dichloropropene
07/16/22 12:080.500< 0.500µg/Lcis-1,3-Dichloropropene
07/16/22 12:080.500< 0.500µg/Ltrans-1,3-Dichloropropene
07/16/22 12:08200< 200µg/LEthanol
07/16/22 12:080.500< 0.500µg/LEthylbenzene
07/16/22 12:083.00< 3.00µg/LHexachlorobutadiene
07/16/22 12:081.00< 1.00µg/L2-Hexanone
07/16/22 12:080.500< 0.500µg/LIsopropylbenzene
07/16/22 12:080.500< 0.500µg/L4-Isopropyl toluene
07/16/22 12:085.00< 5.00µg/LMethyl Ethyl Ketone (MEK)
07/16/22 12:081.00< 1.00µg/LMethyl tert-butyl ether (MTBE)
07/16/22 12:081.00< 1.00µg/L4-Methyl-2-Pentanone
07/16/22 12:082.00< 2.00µg/LMethylene Chloride
07/16/22 12:081.00< 1.00µg/LNaphthalene
07/16/22 12:080.500< 0.500µg/Ln-Propylbenzene
07/16/22 12:080.500< 0.500µg/LStyrene
07/16/22 12:0810.0< 10.0µg/Ltert-Butyl Alcohol (TBA)
07/16/22 12:0810.0< 10.0µg/Ltert-Butyl formate (TBF)
07/16/22 12:0810.0< 10.0µg/Ltert-Amyl Alcohol (TAA)
07/16/22 12:0810.0< 10.0µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 7Date:07/19/2022 05:05 PM
Page 27 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
Associated Lab Samples: 93996, 93997, 93998, 93999
LRB-V21441 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/16/22 12:080.500< 0.500µg/L1,1,1,2-Tetrachloroethane
07/16/22 12:080.500< 0.500µg/L1,1,2,2-Tetrachloroethane
07/16/22 12:080.500< 0.500µg/LTetrachloroethene
07/16/22 12:080.500< 0.500µg/LToluene
07/16/22 12:080.500< 0.500µg/L1,2,3-Trichlorobenzene
07/16/22 12:080.500< 0.500µg/L1,2,4-Trichlorobenzene
07/16/22 12:080.500< 0.500µg/L1,1,1-Trichloroethane
07/16/22 12:080.500< 0.500µg/L1,1,2-Trichloroethane
07/16/22 12:080.500< 0.500µg/LTrichloroethene
07/16/22 12:080.500< 0.500µg/LTrichlorofluoromethane
07/16/22 12:080.500< 0.500µg/L1,2,3-Trichloropropane
07/16/22 12:080.500< 0.500µg/L1,2,4-Trimethylbenzene
07/16/22 12:080.500< 0.500µg/L1,3,5-Trimethylbenzene
07/16/22 12:085.00< 5.00µg/LVinyl Acetate
07/16/22 12:080.500< 0.500µg/LVinyl Chloride
07/16/22 12:080.500< 0.500µg/Lo-Xylene
07/16/22 12:081.00< 1.00µg/Lm,p-Xylene
07/16/22 12:0810.0< 10.0µg/L3,3-Dimethyl-1-butanol
07/16/22 12:084-Bromofluorobenzene (S)100 70-130
07/16/22 12:08Dibromofluoromethane (S)105 70-130
07/16/22 12:081,2-Dichloroethane - d4 (S)102 70-130
07/16/22 12:08Toluene-d8 (S)93.4 70-130
Page 3 of 7Date:07/19/2022 05:05 PM
Page 28 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
LCS-V21441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11723.320.0µg/L3,3-Dimethyl-1-butanol 70-130
LCS-V21441 LCSD-V21441Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
44.5 11111144.540.0µg/LAcetone 40-160 0.0 20.0
22.3 11211923.720.0µg/LBenzene 70-130 6.0 20.0
19.5 97.510120.120.0µg/LBromobenzene 70-130 3.0 20.0
22.9 11512023.920.0µg/LBromochloromethane 70-130 4.2 20.0
22.7 11411723.420.0µg/LBromodichloromethane 70-130 3.0 20.0
21.4 10711322.520.0µg/LBromoform 70-130 5.0 20.0
21.2 10611422.820.0µg/LBromomethane 60-140 7.2 20.0
18.4 92.010020.020.0µg/Ln-Butylbenzene 70-130 8.3 20.0
18.7 93.510220.420.0µg/Lsec-Butyl benzene 70-130 8.6 20.0
18.4 92.010220.420.0µg/Ltert-Butyl benzene 70-130 10.3 20.0
23.7 11912825.620.0µg/LCarbon Tetrachloride 70-130 7.7 20.0
20.1 10110621.120.0µg/LChlorobenzene 70-130 4.8 20.0
21.2 10611322.620.0µg/LChlorodibromomethane 70-130 6.3 20.0
20.6 10310921.820.0µg/LChloroethane 60-140 5.6 20.0
21.7 10911523.020.0µg/LChloroform 70-130 5.8 20.0
19.7 98.510521.020.0µg/LChloromethane 60-140 6.3 20.0
19.4 97.010320.520.0µg/L2-Chlorotoluene 70-130 5.5 20.0
18.4 92.010220.420.0µg/L4-Chlorotoluene 70-130 10.3 20.0
21.7 10911222.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.7 20.0
23.1 11610821.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 6.7 20.0
22.0 11011623.220.0µg/L1,2-Dibromoethane 70-130 5.3 20.0
Page 4 of 7Date:07/19/2022 05:05 PM
Page 29 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
LCS-V21441 LCSD-V21441Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.4 11712224.420.0µg/LDibromomethane 70-130 4.1 20.0
19.7 98.510521.020.0µg/L1,2-Dichlorobenzene 70-130 6.3 20.0
19.1 95.510320.620.0µg/L1,3-Dichlorobenzene 70-130 7.5 20.0
19.2 96.010220.320.0µg/L1,4-Dichlorobenzene 70-130 5.5 20.0
19.8 99.010520.920.0µg/LDichlorodifluoromethane 60-140 5.4 20.0
21.7 10911222.420.0µg/L1,1-Dichloroethane 70-130 3.1 20.0
22.7 11411623.120.0µg/L1,2-Dichloroethane 70-130 1.7 20.0
20.8 10411222.420.0µg/L1,1-Dichloroethene 70-130 7.4 20.0
22.0 11011623.120.0µg/Lcis-1,2-Dichloroethene 70-130 4.8 20.0
21.2 10611322.520.0µg/Ltrans-1,2-Dichloroethene 70-130 5.9 20.0
21.7 10911623.220.0µg/L1,2-Dichloropropane 70-130 6.6 20.0
21.5 10811322.620.0µg/L1,3-Dichloropropane 70-130 4.9 20.0
20.6 10311422.720.0µg/L2,2-Dichloropropane 70-130 9.6 20.0
22.0 11011623.120.0µg/L1,1-Dichloropropene 70-130 4.8 20.0
23.9 12012625.220.0µg/Lcis-1,3-Dichloropropene 70-130 5.2 20.0
23.9 12012625.220.0µg/Ltrans-1,3-Dichloropropene 70-130 5.2 20.0
567 113114569500µg/LEthanol 60-140 0.3 20.0
19.7 98.510621.220.0µg/LEthylbenzene 70-130 7.3 20.0
17.0 85.096.519.320.0µg/LHexachlorobutadiene 70-130 12.6 20.0
23.4 11711522.920.0µg/L2-Hexanone 60-140 2.1 20.0
19.0 95.010220.320.0µg/LIsopropylbenzene 70-130 6.6 20.0
19.0 95.010220.420.0µg/L4-Isopropyl toluene 70-130 7.1 20.0
25.5 12811823.520.0µg/LMethyl Ethyl Ketone (MEK)60-140 8.1 20.0
24.8 12412524.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.4 20.0
23.5 11811923.720.0µg/L4-Methyl-2-Pentanone 60-140 0.8 20.0
20.4 10210721.320.0µg/LMethylene Chloride 70-130 4.3 20.0
Page 5 of 7Date:07/19/2022 05:05 PM
Page 30 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
LCS-V21441 LCSD-V21441Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.1 11111623.220.0µg/LNaphthalene 70-130 4.8 20.0
18.9 94.510220.420.0µg/Ln-Propylbenzene 70-130 7.6 20.0
20.3 10211122.220.0µg/LStyrene 70-130 8.9 20.0
45.3 11311746.740.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.0 20.0
50.5 12612851.140.0µg/Ltert-Butyl formate (TBF)40-140 1.1 20.0
24.4 12211723.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 4.6 20.0
50.8 12712750.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.0 20.0
20.3 10210821.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.7 20.0
21.2 10610721.420.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.9 20.0
18.9 94.510120.220.0µg/LTetrachloroethene 70-130 6.6 20.0
22.3 11211723.420.0µg/LToluene 70-130 4.8 20.0
22.5 11313025.920.0µg/L1,2,3-Trichlorobenzene 70-130 14.0 20.0
20.8 10410621.120.0µg/L1,2,4-Trichlorobenzene 70-130 1.4 20.0
21.3 10711523.020.0µg/L1,1,1-Trichloroethane 70-130 7.6 20.0
24.1 12112825.520.0µg/L1,1,2-Trichloroethane 70-130 5.6 20.0
21.2 10611523.020.0µg/LTrichloroethene 70-130 8.1 20.0
20.0 10010921.720.0µg/LTrichlorofluoromethane 60-140 8.1 20.0
20.1 10110220.320.0µg/L1,2,3-Trichloropropane 70-130 0.9 20.0
19.0 95.010120.220.0µg/L1,2,4-Trimethylbenzene 70-130 6.1 20.0
19.1 95.510120.220.0µg/L1,3,5-Trimethylbenzene 70-130 5.5 20.0
22.5 11312023.920.0µg/LVinyl Acetate 60-140 6.0 20.0
20.5 10310521.020.0µg/LVinyl Chloride 60-140 2.4 20.0
20.5 10310921.720.0µg/Lo-Xylene 70-130 5.6 20.0
42.4 10611244.640.0µg/Lm,p-Xylene 70-130 5.0 20.0
99.81024-Bromofluorobenzene (S)70-130
10199.6Dibromofluoromethane (S)70-130
Page 6 of 7Date:07/19/2022 05:05 PM
Page 31 of 34
Quality Control Data
22-192-0008Report No:
Project Description:
Client ID:Resolve Environmental
Kwik Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21442QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21441
LCS-V21441 LCSD-V21441Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
97.21031,2-Dichloroethane - d4 (S)70-130
94.894.6Toluene-d8 (S)70-130
Page 7 of 7Date:07/19/2022 05:05 PM
Page 32 of 34
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-192-0008
Resolve Environmental
00238
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 4.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:07/11/2022 12:22:10
Special precautions or instructions included?
Comments:
Page 33 of 34
Page 34 of 34