MO-3214_8097_CA_MRP_20210521

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 
www.excelengr.com 

Excel Civil & Environmental Associates, PLLC
625 Huntsman Court
Gastonia, North Carolina 28054
NC License No. P-0129
Telephone: [phone]
Facsimile: [phone]
Internet: www.excelengr.com

May 21, 2021

Mr. Dan Bowser
NCDEQ / DWM / UST Section
Mooresville Regional Office
610 East Center Avenue
Mooresville, North Carolina 28115

Re: Letter Report
Former SERVCO No. 01612
120 South Graham Street
Charlotte, North Carolina
MO-3214_8097_CA_RPTS_20210521
NCDEQ No. 8097
EXCEL No. 22117

Dear Mr. Bowser:

Excel Civil & Environmental Associates, PLLC is pleased to submit a copy of this Letter
Report for the above referenced site on behalf of Service Distributing Company,
Incorporated (Servco) the former UST Owner.

If you have any questions after review of this report, please feel free to contact me.

Sincerely yours,

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
Aaron C. Long, P.E.
Project Engineer

p.c. Robert Gresham – Servco, Albemarle, NC
Misc. Letter Report May 21, 2021
(Former) SERVCO No. 01612 Incident No. 8097
Charlotte, North Carolina Excel No. 22117

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 
www.excelengr.com 

PROJECT SUMMARY

 Groundwater quality samples were collected from monitoring wells MW-1 through
MW-5 on December 3rd and 4th, 2020. The samples were analyzed for volatile
organic compounds (VOCs) by EPA Method 6200B, ethylene dibromide (EDB) by
EPA Method 504.1, and Lead by EPA Method 3030C. During the site visit,
monitoring well MW-102 was found to be dry and MW-6 was not located.

 No free product was observed during the sampling event, therefore samples were
collected accordingly. It is Excel’s standard operating procedure not to gauge
monitoring wells with an oil-water interface probe prior to sampling if said well has
not historically shown free product. Static water levels were collected with a
decontaminated water level indicator at the locations of all other monitoring wells
which were sampled.

 The results of the laboratory analysis from the December 2020 sampling event
indicate that none of the samples exceeded Gross Contamination Levels (GCLs) for
all constituents analyzed.

 Review of current liquid level data indicates that groundwater is flowing from south to
north.

 To evaluate current soil conditions Excel mobilized a drill rig to the site on April 21,
2021 to collect a soil sample at a suspect residual hot spot area. The soil sample
was collected at approximately twelve feet below grade level. Benzene and
Naphthalene were above Soil-to-Water MSCCs, but all results were below
Residential Soil Cleanup Levels.

CONCLUSIONS / RECOMMENDATIONS

 The results from the December 2020 groundwater sampling event indicated that
results were below Gross Contamination Levels.

 The results from the April 2021 soil assessment indicated that results were below
Residential Soil Cleanup Levels.

 At this time, we recommend that this incident be closed out and no further action
(NFA) be issued with land use restriction (LUR).
Misc. Letter Report May 21, 2021
(Former) SERVCO No. 01612 Incident No. 8097
Charlotte, North Carolina Excel No. 22117
EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 
www.excelengr.com 

TABLE 1 – December 2020 LIQUID LEVEL DATA

Well ID
Number
Top of
Casing (ft)
Depth to
Product (ft)
Depth to
Water (ft)
Product
Thickness (ft)
Water Table
Elevation (ft)
MW-1 90.00 -- 26.10 -- 63.90
MW-2R 87.55 -- 24.90 -- 62.65
MW-3 83.38 -- 20.27 -- 63.11
MW-4 83.83 -- 21.22 -- 62.61
MW-5 81.20 -- 19.05 -- 62.65
MW-6 83.05 Not Located
MW-102 -- Dry
NOTES: All data provided in feet / TOC – Top of Casing Elevation / DTW – Depth to Water
WTE – Water Table Elevation

May 21, 2021 Incident No. 8097 Misc. Letter Report(Former) SERVCO No. 01612 Charlotte, North Carolina Excel No. 22117 EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC www.excelengr.com TABLE 2 - SUMMARY OF HISTORICAL GROUNDWATER ANALYTICAL DATA Well ID No. Sample Date Benzene Toluene Ethylbenzene Xylenes MTBE IPE PCE TCE cis-1,2,DCE GCLs - 5,000 260,000 84,500 85,500 20,000 70,000 700 3,000 70,000 MW-1 7/27/12 < 1 < 5 < 1 < 3 < 1 < 1 < 1 < 1 < 1 12/3/20 < 0.0941 < 0.278 < 0.137 < 0.604 < 0.101 < 0.105 2.0 < 0.190 < 0.126 MW-2 11/8/04 19,000 18,000 < 2,500 12,700 < 12,000 < 12,000 < 2,500 < 2,500 < 2,500 12/1/06 5,300 2,000738,4002,40081 NANA NA 1/23/08 16,000 < 50,000 < 5,000 < 15,000 < 10,000 < 10,000 NA NA NA 7/27/12 10,000 2,600 2,900 11,600 < 500 < 500 < 500 < 500 < 500 MW-2R 5/14/20 6,420 5,660 4,450 19,270 239 J < 52.5 < 150 < 95 < 63 12/4/205923962772,950< 2.02 < 2.10 < 6 < 3.8 < 2.52 MW-3 7/27/12 9 < 5 8.9 < 3 130 120 < 1 < 1 < 1 5/15/20 0.113 J < 0.278 < 0.137 < 0.664 0.615 J 1.77 < 0.300 < 0.190 < 0.126 12/3/20 1.18 0.422 J 0.692 J 3.8 1.92 6.22 < 0.3 < 0.190 < 0.126 MW-4 7/27/12 < 1 < 5 < 1 < 3 63 12 < 1 < 1 < 1 5/15/20 < 0.0941 < 0.278 < 0.137 < 0.604 0.365 J < 0.105 14.6 0.546 J2.2812/3/20 < 0.0941 < 0.278 0.276 J 1.516 J < 0.101 < 0.105 8.38 0.233 J 0.809 J MW-5 7/27/12 < 1 < 5 < 1 < 3 < 1 < 1 24 2.2 1.8 5/14/20 0.120 J < 0.278 0.257 J 1.345 J 0.260 J < 0.105 9.49 0.711 J 0.699 J 12/3/20 < 0.0941 < 0.278 0.195 J < 0.604 0.296 J < 0.105 9.82 0.633 J 0.766 J MW-6 11/8/04 < 1 < 5 < 1 < 2 7.7 < 5 1.5 1 < 1 7/27/12 < 1 < 5 < 1 < 3 2.7 < 1 74 3.8 9.3 NOTES: Data provided in ug/l (ppb – parts per billion) / NA – Not Analyzed / MTBE – Methyl Tert Butyl Ether / IPE – Di-Isopropyl Ether / Data in BOLD and Highlighted indicates levels above GCLs / PCE – Tetrachloroethene / TCE – Trichloroethene / cis-1,2,DCE – cis-1,2,Dichloroethene
May 21, 2021 Incident No. 8097 Misc. Letter Report (Former) SERVCO No. 01612 Charlotte, North Carolina Excel No. 22117 EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC www.excelengr.com ADDITIONAL CONSTITUENTS DETECTED DURING 5/20 SAMPLING EVENT: MW-2R: n-Butylbenzene = 86.4 J ug/l; Isopropylbenzene = 181 J ug/l; Napthalene = 818 J ug/l; n-propylbenzene = 613 ug/l; 1,2,4-Trimethylbenzene = 3,850ug/l; 1,3,5-Trimethylbenzene = 1,080 ug/l; Lead = 58.2 ug/l MW-3: n-Butylbenzene = 0.166 J ug/l; sec-Butylbenzene = 2.38 ug/l; tert-Butylbenzene = 1.33 ug/l; Isopropylbenzene = 0.448 J; n-propylbenzene = 0.234 Jug/l; Lead = 8.21 ug/lMW-4: Chloroform = 2.90 J ug/l; Lead = 25.9 ug/lMW-5: Bromodichloromethane = 0.163 J ug/l; Chloroform = 6.90 J ug/l; 1,2-Dichloroethane = 0.192 J ug/l; n-propylbenzene = 0.148 J ug/l; 1,2,4-Trimethylbenzene = 0.799 J ug/l; 1,3,5-Trimethylbenzene = 0.233 J ug/l; Lead = 4.17 J ug/lADDITIONAL CONSTITUENTS DETECTED DURING 12/20 SAMPLING EVENT: MW-1: Bromobenzene = 0.164 BJ ug/l; Chloroform = 6.32 ug/l; 1,2-Dichlorobenzene = 0.117 BJ ug/l; 1,3-Dichlorobenzene = 0.111 BJ ug/l; 1,4-Dichlorobenzene = 0.178 BJ ug/l; 1,2,3-Trichlorobenzene = 0.411 BJJ4 ug/l; Lead = 3.33 J ug/l MW-2R: sec-Butylbenzene = 6.77 J ug/l; Isopropylbenzene = 16.5 J ug/l; p-Isopropyltoluene = 7.31 J ug/l; Napthalene = 168 ug/l; n-propylbenzene = 40.2 ug/l; 1,2,4-Trimethylbenzene = 753 ug/l; 1,3,5-Trimethylbenzene = 481 ug/l; Lead = 35.1 ug/l MW-3: n-Butylbenzene = 4.82 ug/l; sec-Butylbenzene = 6.41 ug/l; tert-Butylbenzene = 3.02 ug/l; 1,2-Dichlorobenzene = 0.177 BJ ug/l; 1,3-Dichlorobenzene= 0.134 BJ ug/l; 1,4-Dichlorobenzene = 0.181 BJ ug/l; Isopropylbenzene = 0.877 J ug/l; Naphthalene 3.99 JJ4 ug/l; n-propylbenzene = 0.767 BJ ug/l;1,2,3-Trichlorobenzene = 0.63 BJJ4 ug/l; 1,2,4-Trimethylbenzene = 4.05 ug/l; 1,3,5-Trimethylbenzene = 1.14 ug/l; Lead = 40.6 ug/lMW-4: sec-Butylbenzene = 0.141 J ug/l; Chloroform = 1.44 J ug/l; 1,2-Dichlorobenzene = 0.117 BJ ug/l; 1,4-Dichlorobenzene = 0.136 BJ ug/l; n-propylbenzene = 0.206 BJ ug/l; 1,2,3-Trichlorobenzene = 0.331 BJJ4 ug/l; 1,2,4-Trimethylbenzene = 1.35 ug/l; 1,3,5-Trimethylbenzene = 0.495 BJug/l; Lead = 156 ug/lMW-5: n-Butylbenzene = 0.26 J ug/l; Chloroform = 7.72 ug/l; 1,2-Dichlorobenzene = 0.111 BJ ug/l; 1,4-Dichlorobenzene = 0.214 BJ ug/l; n-propylbenzene =0.113 BJ ug/l; 1,2,3-Trichlorobenzene = 0.315 BJJ4 ug/l; 1,2,4-Trimethylbenzene = 0.491 J ug/l; 1,3,5-Trimethylbenzene = 0.266 BJ ug/l
Table 3 - Soil Summary DataFormer Servco 01612120 South Graham Street, Charlotte, North CarolinaNCDEQ Incident 8097Excel Project No. 22117S7.212 ftDATE SAMPLED 21-Apr-21PID READING58.0 -- -- --VPH C5 - C8 Aliphatics18.268 93924,528VPH C9 - C12 Aliphatics32.5 -- -- --VPH C9 - C10 Aromatics24.4 -- -- --BENZENE 0.0127 0.0056 18164TOLUENE0.00428 J4.3 1,20032,000ETHYLBENZENE0.2624.9 1,56040,000XYLENES0.0714.63,12981,760MTBE0.02130.0913503,100n-BUTYLBENZENE0.1844.362616,350sec-BUTYLBENZENE0.08953.362616,350tert-BUTYLBENZENE0.00708 J3.462616,350NAPHTHALENE1.08 C30.163138,176ISOPROPYLBENZENE0.07861.71,56440,880p-ISOPROPYLTOLUENE0.02130.121004,000n-PROPYLBENZENE0.2561.762616,3501,2,4-TRIMETHYLBENZENE0.3328.578220,4401,3,5-TRIMETHYLBENZENE0.03958.578220,440NOTES:Data in mg/kgFBGL - Feet Below Grade LevelVPH - Volatile Petroleum HydrocarbonsBold data represents constituents above Soil-to-Water MSCCs (Maximum Soil Contaminant Concentrations)Highlighted data represent constituents above Residential Soil Cleanup Levels Italicized data represent constituents above Industrial / Commercial Soil Cleanup LevelsJ - Reported value is an estimateC3 - Reported concentration is an estimateResidential Soil Cleanup LevelsIndustrial / Commercial Soil Cleanup LevelsSAMPLE LOCATIONSoil-to-Water MSCCs

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 
www.excelengr.com 

APPENDICES

APPENDIX A – FIGURES

APPENDIX B – LABORATORY ANALYSES & CHAIN OF CUSTODY FORMS

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 
www.excelengr.com 

APPENDIX A - FIGURES

Figure 1 – Site Vicinity

Figure 2 – Site Plan

Figure 3 – Water Table Contour Map

Figure 4 – Groundwater Constituents Map

Figure 5 – Soil Constituents Map

EXCEL CIVIL & ENVIRONMENTAL
ASSOCIATES, PLLC
625 HUNTSMAN COURT
GASTONIA, NC 28054
[phone]

FIGURE 1 –
SITE VICINITY MAP

Source: U.S.G.S. 7.5 Minute Topographic Map
Charlotte East, NC, Quadrangle, 1991 N

GROUNDWATER MONITORING REPORT120 SOUTH GRAHAM STREET, CHARLOTTE, NC625 HUNTSMANCOURT., GASTONIA, NCFORMER SERVCO FACILITY NO. 01612SERVICE DISTRIBUTING CO., INC.FIGURE 2 - SITE PLANDRAWN BY :22117PROJECT NO. :MAP TITLE :PREPARED FOR :SCALE :JDM1" = 30'8/8/12DATE :PHONE : [phone]W. FOURTH STREETMonitoring Well LocationLEGENDUST - Underground Storage TankMecklenburg County Tax Map.Map adapted from Aerial Photograph &NOTESASPHALTFORMER SERVCONO.
01612SEWNS. GRAHAM STREETPARKING LOTUST AREAFORMERPARKING LOTASPHALTASPHALTPARKING LOTPARKING LOTGRAVELPARKING LOTASPHALTASPHALTPARKING LOTMW-1MW-2MW-6MW-3MW-4MW-5RETAIN
ING WALLMW-102
NOTESMap adapted from Aerial Photograph &Mecklenburg County Tax Map.UST - Underground Storage TankLEGENDASPHALTPARKING LOTS. GRAHAM STREETMW-4PARKING LOTASPHALTMW-5GRAVELPARKING LOTW. FOURTH STREETMW-3ASPHALTPARKING LOTMW-6FIGURE 5 - SOIL CONSTITUENTS MAPSERVICE DISTRIBUTING CO., INC.FORMER SERVCO FACILITY NO. 01612120 SOUTH GRAHAM STREET, CHARLOTTE, NCGROUNDWATER MONITORING REPORTSoil Boring Location22117PREPARED FOR :MAP TITLE :PROJECT NO. :625 HUNTSMAN COURT., GASTONIA, NCPARKING LOTASPHALTPHONE : (704) 853-08005.21.20211" = 30'SCALE :DATE :FORMER SERVCOMW-2RSPARKING LOTASPHALTNO.
01612WENMW-1Data is provided in mg/kgData from liquid levels collected in April 2021BenzeneTolueneEthylbenzeneXylenesMTBEData BoxLegendMTBE - Methyl Tert-Butyl Ether0.01270.00428 J0.2620.0710.0213RETAIN
ING WALLMW-102ACLDRAWN BY :NaphthaleneS7.21.08

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 
www.excelengr.com 

APPENDIX B - LABORATORY ANALYSES & CHAIN OF CUSTODY FORMS

ANALYTICAL REPORT
April 30, 2021
Excel Civil & Environmental Associates
Sample Delivery Group:L1342835
Samples Received:04/23/2021
Project Number:22117
Description:Servco 01612
Report To:Aaron Long
625 Huntsman Court
Gastonia, NC 28054
Entire Report Reviewed By:
April 30, 2021
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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April 30, 2021
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
S7.2 L1342835-01 5
Qc: Quality Control Summary 7
Total Solids by Method 2540 G-2011 7
Volatile Petroleum Hydrocarbons by Method MADEPV 8
Volatile Organic Compounds (GC/MS) by Method 8260D 9
Gl: Glossary of Terms 14
Al: Accreditations & Locations 15
Sc: Sample Chain of Custody 16
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S7.2 L1342835-01 Solid Aaron Long 04/21/21 13:50 04/23/21 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1659534 1 04/29/21 11:27 04/29/21 11:35 KDW Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1660200 1 04/21/21 13:50 04/28/21 14:09 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1659007 1 04/21/21 13:50 04/26/21 18:36 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1660321 1 04/21/21 13:50 04/29/21 10:09 JAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1342835
S7.2
Collected date/time: 04/21/21 13:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 66.4 1 04/29/2021 11:35 WG1659534
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Unadjusted C5-C8 Aliphatics 18200 3420 10200 1 04/28/2021 14:09 WG1660200
Unadjusted C9-C12 Aliphatics 32500 3420 10200 1 04/28/2021 14:09 WG1660200
Unadjusted C9-C10 Aromatics 24400 3420 10200 1 04/28/2021 14:09 WG1660200
Total VPH 75100 3420 10200 1 04/28/2021 14:09 WG1660200
(S) 2,5-Dibromotoluene(FID) 100 70.0-130 04/28/2021 14:09 WG1660200
(S) 2,5-Dibromotoluene(PID) 86.8 70.0-130 04/28/2021 14:09 WG1660200
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
Acetone U 74.7 102 1 04/26/2021 18:36 WG1659007
Acrylonitrile U 7.39 25.6 1 04/26/2021 18:36 WG1659007
Benzene 12.7 0.956 2.05 1 04/26/2021 18:36 WG1659007
Bromobenzene U J4 1.84 25.6 1 04/26/2021 18:36 WG1659007
Bromodichloromethane U 1.48 5.12 1 04/26/2021 18:36 WG1659007
Bromoform U 2.40 51.2 1 04/26/2021 18:36 WG1659007
Bromomethane U 4.03 25.6 1 04/26/2021 18:36 WG1659007
n-Butylbenzene 184 10.7 25.6 1 04/26/2021 18:36 WG1659007
sec-Butylbenzene 89.5 5.90 25.6 1 04/26/2021 18:36 WG1659007
tert-Butylbenzene 7.08 J 3.99 10.2 1 04/26/2021 18:36 WG1659007
Carbon tetrachloride U 1.84 10.2 1 04/26/2021 18:36 WG1659007
Chlorobenzene 6.33 0.430 5.12 1 04/26/2021 18:36 WG1659007
Chlorodibromomethane U 1.25 5.12 1 04/26/2021 18:36 WG1659007
Chloroethane U 3.48 10.2 1 04/26/2021 18:36 WG1659007
Chloroform U 2.11 5.12 1 04/26/2021 18:36 WG1659007
Chloromethane U 8.90 25.6 1 04/26/2021 18:36 WG1659007
2-Chlorotoluene U 1.77 5.12 1 04/26/2021 18:36 WG1659007
4-Chlorotoluene U 0.921 10.2 1 04/26/2021 18:36 WG1659007
1,2-Dibromo-3-Chloropropane U 7.98 51.2 1 04/26/2021 18:36 WG1659007
1,2-Dibromoethane U 1.33 5.12 1 04/26/2021 18:36 WG1659007
Dibromomethane U 1.54 10.2 1 04/26/2021 18:36 WG1659007
1,2-Dichlorobenzene U 0.870 10.2 1 04/26/2021 18:36 WG1659007
1,3-Dichlorobenzene U 1.23 10.2 1 04/26/2021 18:36 WG1659007
1,4-Dichlorobenzene U 1.43 10.2 1 04/26/2021 18:36 WG1659007
Dichlorodifluoromethane U 3.30 5.12 1 04/26/2021 18:36 WG1659007
1,1-Dichloroethane U 1.01 5.12 1 04/26/2021 18:36 WG1659007
1,2-Dichloroethane U 1.33 5.12 1 04/26/2021 18:36 WG1659007
1,1-Dichloroethene U 1.24 5.12 1 04/26/2021 18:36 WG1659007
cis-1,2-Dichloroethene U 1.50 5.12 1 04/26/2021 18:36 WG1659007
trans-1,2-Dichloroethene U 2.13 10.2 1 04/26/2021 18:36 WG1659007
1,2-Dichloropropane U 2.91 10.2 1 04/26/2021 18:36 WG1659007
1,1-Dichloropropene U 1.66 5.12 1 04/26/2021 18:36 WG1659007
1,3-Dichloropropane U 1.03 10.2 1 04/26/2021 18:36 WG1659007
cis-1,3-Dichloropropene U 1.55 5.12 1 04/26/2021 18:36 WG1659007
trans-1,3-Dichloropropene U 2.33 10.2 1 04/26/2021 18:36 WG1659007
2,2-Dichloropropane U 2.82 5.12 1 04/26/2021 18:36 WG1659007
Di-isopropyl ether U 0.839 2.05 1 04/26/2021 18:36 WG1659007
Ethylbenzene 262 1.51 5.12 1 04/26/2021 18:36 WG1659007
Hexachloro-1,3-butadiene U 12.3 51.2 1 04/26/2021 18:36 WG1659007
Isopropylbenzene 78.6 0.870 5.12 1 04/26/2021 18:36 WG1659007
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1342835
S7.2
Collected date/time: 04/21/21 13:50
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte ug/kg ug/kg ug/kg date / time
p-Isopropyltoluene 21.3 5.22 10.2 1 04/26/2021 18:36 WG1659007
2-Butanone (MEK)307 130 205 1 04/26/2021 18:36 WG1659007
Methylene Chloride U 13.6 51.2 1 04/26/2021 18:36 WG1659007
4-Methyl-2-pentanone (MIBK) U 4.67 51.2 1 04/26/2021 18:36 WG1659007
Methyl tert-butyl ether 21.3 0.716 2.05 1 04/26/2021 18:36 WG1659007
Naphthalene 1080 C3 9.99 25.6 1 04/26/2021 18:36 WG1659007
n-Propylbenzene 256 1.94 10.2 1 04/26/2021 18:36 WG1659007
Styrene U 0.469 25.6 1 04/26/2021 18:36 WG1659007
1,1,1,2-Tetrachloroethane U 1.94 5.12 1 04/26/2021 18:36 WG1659007
1,1,2,2-Tetrachloroethane U 1.42 5.12 1 04/26/2021 18:36 WG1659007
Tetrachloroethene U 1.83 5.12 1 04/29/2021 10:09 WG1660321
Toluene 4.28 J 2.66 10.2 1 04/26/2021 18:36 WG1659007
1,2,3-Trichlorobenzene U C3 15.0 25.6 1 04/26/2021 18:36 WG1659007
1,2,4-Trichlorobenzene U C3 9.01 25.6 1 04/26/2021 18:36 WG1659007
1,1,1-Trichloroethane U 1.89 5.12 1 04/26/2021 18:36 WG1659007
1,1,2-Trichloroethane U 1.22 5.12 1 04/26/2021 18:36 WG1659007
Trichloroethene U 1.20 2.05 1 04/26/2021 18:36 WG1659007
Trichlorofluoromethane U 1.69 5.12 1 04/26/2021 18:36 WG1659007
1,2,3-Trichloropropane U 3.32 25.6 1 04/26/2021 18:36 WG1659007
1,2,4-Trimethylbenzene 332 3.23 10.2 1 04/26/2021 18:36 WG1659007
1,3,5-Trimethylbenzene 39.5 4.09 10.2 1 04/26/2021 18:36 WG1659007
Vinyl chloride U 2.37 5.12 1 04/26/2021 18:36 WG1659007
Xylenes, Total 71.0 1.80 13.3 1 04/26/2021 18:36 WG1659007
(S) Toluene-d8 108 75.0-131 04/26/2021 18:36 WG1659007
(S) Toluene-d8 111 75.0-131 04/29/2021 10:09 WG1660321
(S) 4-Bromofluorobenzene 105 67.0-138 04/26/2021 18:36 WG1659007
(S) 4-Bromofluorobenzene 110 67.0-138 04/29/2021 10:09 WG1660321
(S) 1,2-Dichloroethane-d4 112 70.0-130 04/26/2021 18:36 WG1659007
(S) 1,2-Dichloroethane-d4 115 70.0-130 04/29/2021 10:09 WG1660321
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1659534
Total Solids by Method 2540 G-2011 L1342835-01
Method Blank (MB)
(MB) R3648520-1 04/29/21 11:35
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1342809-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1342809-03 04/29/21 11:35 • (DUP) R3648520-3 04/29/21 11:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 88.3 90.4 1 2.34 10
Laboratory Control Sample (LCS)
(LCS) R3648520-2 04/29/21 11:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1660200
Volatile Petroleum Hydrocarbons by Method MADEPV L1342835-01
Method Blank (MB)
(MB) R3648656-3 04/28/21 10:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Unadjusted C5-C8 Aliphatics U 1670 5000
Unadjusted C9-C12 Aliphatics U 1670 5000
Unadjusted C9-C10 Aromatics U 1670 5000
Total VPH U 1670 5000
(S) 2,5-Dibromotoluene(FID) 95.0 70.0-130
(S) 2,5-Dibromotoluene(PID) 84.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3648656-1 04/28/21 07:11 • (LCSD) R3648656-2 04/28/21 07:45
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Unadjusted C5-C8 Aliphatics 60000 59500 58100 99.2 96.8 70.0-130 2.38 25
Unadjusted C9-C12 Aliphatics 70000 82100 80900 117 116 70.0-130 1.47 25
Unadjusted C9-C10 Aromatics 10000 12100 12200 121 122 70.0-130 0.823 25
Total VPH 140000 154000 151000 110 108 70.0-130 1.97 25
(S) 2,5-Dibromotoluene(FID) 97.8 99.4 70.0-130
(S) 2,5-Dibromotoluene(PID) 86.8 88.5 70.0-130
L1343628-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1343628-01 04/28/21 22:24 • (MS) R3648656-4 04/28/21 23:30 • (MSD) R3648656-5 04/29/21 00:03
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg ug/kg %%%%%
Unadjusted C5-C8 Aliphatics 55200 U 54700 50900 99.1 92.2 1 70.0-130 7.20 25
Unadjusted C9-C12 Aliphatics 64400 U 76400 70300 119 109 1 70.0-130 8.32 25
Unadjusted C9-C10 Aromatics 9200 U 11400 10900 124 118 1 70.0-130 4.48 25
Total VPH 129000 U 143000 132000 111 102 1 70.0-130 8.00 25
(S) 2,5-Dibromotoluene(FID) 97.3 98.4 70.0-130
(S) 2,5-Dibromotoluene(PID) 84.7 85.9 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1659007
Volatile Organic Compounds (GC/MS) by Method 8260D L1342835-01
Method Blank (MB)
(MB) R3647493-3 04/26/21 13:09
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Acetone U 36.5 50.0
Acrylonitrile U 3.61 12.5
Benzene U 0.467 1.00
Bromobenzene U 0.900 12.5
Bromodichloromethane U 0.725 2.50
Bromoform U 1.17 25.0
Bromomethane U 1.97 12.5
n-Butylbenzene U 5.25 12.5
sec-Butylbenzene U 2.88 12.5
tert-Butylbenzene U 1.95 5.00
Carbon tetrachloride U 0.898 5.00
Chlorobenzene U 0.210 2.50
Chlorodibromomethane U 0.612 2.50
Chloroethane U 1.70 5.00
Chloroform U 1.03 2.50
Chloromethane U 4.35 12.5
2-Chlorotoluene U 0.865 2.50
4-Chlorotoluene U 0.450 5.00
1,2-Dibromo-3-Chloropropane U 3.90 25.0
1,2-Dibromoethane U 0.648 2.50
Dibromomethane U 0.750 5.00
1,2-Dichlorobenzene U 0.425 5.00
1,3-Dichlorobenzene U 0.600 5.00
1,4-Dichlorobenzene U 0.700 5.00
Dichlorodifluoromethane U 1.61 2.50
1,1-Dichloroethane U 0.491 2.50
1,2-Dichloroethane U 0.649 2.50
1,1-Dichloroethene U 0.606 2.50
cis-1,2-Dichloroethene U 0.734 2.50
trans-1,2-Dichloroethene U 1.04 5.00
1,2-Dichloropropane U 1.42 5.00
1,1-Dichloropropene U 0.809 2.50
1,3-Dichloropropane U 0.501 5.00
cis-1,3-Dichloropropene U 0.757 2.50
trans-1,3-Dichloropropene U 1.14 5.00
2,2-Dichloropropane U 1.38 2.50
Di-isopropyl ether U 0.410 1.00
Ethylbenzene U 0.737 2.50
Hexachloro-1,3-butadiene U 6.00 25.0
Isopropylbenzene U 0.425 2.50
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1659007
Volatile Organic Compounds (GC/MS) by Method 8260D L1342835-01
Method Blank (MB)
(MB) R3647493-3 04/26/21 13:09
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
p-Isopropyltoluene U 2.55 5.00
2-Butanone (MEK)U 63.5 100
Methylene Chloride U 6.64 25.0
4-Methyl-2-pentanone (MIBK) U 2.28 25.0
Methyl tert-butyl ether U 0.350 1.00
Naphthalene U 4.88 12.5
n-Propylbenzene U 0.950 5.00
Styrene U 0.229 12.5
1,1,1,2-Tetrachloroethane U 0.948 2.50
1,1,2,2-Tetrachloroethane U 0.695 2.50
Toluene U 1.30 5.00
1,2,3-Trichlorobenzene U 7.33 12.5
1,2,4-Trichlorobenzene U 4.40 12.5
1,1,1-Trichloroethane U 0.923 2.50
1,1,2-Trichloroethane U 0.597 2.50
Trichloroethene U 0.584 1.00
Trichlorofluoromethane U 0.827 2.50
1,2,3-Trichloropropane U 1.62 12.5
1,2,4-Trimethylbenzene U 1.58 5.00
1,3,5-Trimethylbenzene U 2.00 5.00
Vinyl chloride U 1.16 2.50
Xylenes, Total U 0.880 6.50
(S) Toluene-d8 112 75.0-131
(S) 4-Bromofluorobenzene 93.6 67.0-138
(S) 1,2-Dichloroethane-d4 105 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3647493-1 04/26/21 11:53 • (LCSD) R3647493-2 04/26/21 12:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Acetone 625 871 976 139 156 10.0-160 11.4 31
Acrylonitrile 625 676 715 108 114 45.0-153 5.61 22
Benzene 125 121 124 96.8 99.2 70.0-123 2.45 20
Bromobenzene 125 155 144 124 115 73.0-121 J4 7.36 20
Bromodichloromethane 125 125 127 100 102 73.0-121 1.59 20
Bromoform 125 157 162 126 130 64.0-132 3.13 20
Bromomethane 125 128 127 102 102 56.0-147 0.784 20
n-Butylbenzene 125 111 112 88.8 89.6 68.0-135 0.897 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1659007
Volatile Organic Compounds (GC/MS) by Method 8260D L1342835-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3647493-1 04/26/21 11:53 • (LCSD) R3647493-2 04/26/21 12:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
sec-Butylbenzene 125 133 120 106 96.0 74.0-130 10.3 20
tert-Butylbenzene 125 132 120 106 96.0 75.0-127 9.52 20
Carbon tetrachloride 125 132 134 106 107 66.0-128 1.50 20
Chlorobenzene 125 134 133 107 106 76.0-128 0.749 20
Chlorodibromomethane 125 128 123 102 98.4 74.0-127 3.98 20
Chloroethane 125 127 117 102 93.6 61.0-134 8.20 20
Chloroform 125 136 135 109 108 72.0-123 0.738 20
Chloromethane 125 127 119 102 95.2 51.0-138 6.50 20
2-Chlorotoluene 125 136 127 109 102 75.0-124 6.84 20
4-Chlorotoluene 125 126 117 101 93.6 75.0-124 7.41 20
1,2-Dibromo-3-Chloropropane 125 113 117 90.4 93.6 59.0-130 3.48 20
1,2-Dibromoethane 125 126 123 101 98.4 74.0-128 2.41 20
Dibromomethane 125 128 136 102 109 75.0-122 6.06 20
1,2-Dichlorobenzene 125 139 142 111 114 76.0-124 2.14 20
1,3-Dichlorobenzene 125 143 151 114 121 76.0-125 5.44 20
1,4-Dichlorobenzene 125 124 134 99.2 107 77.0-121 7.75 20
Dichlorodifluoromethane 125 120 125 96.0 100 43.0-156 4.08 20
1,1-Dichloroethane 125 126 131 101 105 70.0-127 3.89 20
1,2-Dichloroethane 125 138 141 110 113 65.0-131 2.15 20
1,1-Dichloroethene 125 117 120 93.6 96.0 65.0-131 2.53 20
cis-1,2-Dichloroethene 125 136 129 109 103 73.0-125 5.28 20
trans-1,2-Dichloroethene 125 129 129 103 103 71.0-125 0.000 20
1,2-Dichloropropane 125 120 117 96.0 93.6 74.0-125 2.53 20
1,1-Dichloropropene 125 117 123 93.6 98.4 73.0-125 5.00 20
1,3-Dichloropropane 125 128 120 102 96.0 80.0-125 6.45 20
cis-1,3-Dichloropropene 125 128 122 102 97.6 76.0-127 4.80 20
trans-1,3-Dichloropropene 125 133 126 106 101 73.0-127 5.41 20
2,2-Dichloropropane 125 140 139 112 111 59.0-135 0.717 20
Di-isopropyl ether 125 112 114 89.6 91.2 60.0-136 1.77 20
Ethylbenzene 125 134 137 107 110 74.0-126 2.21 20
Hexachloro-1,3-butadiene 125 134 132 107 106 57.0-150 1.50 20
Isopropylbenzene 125 134 141 107 113 72.0-127 5.09 20
p-Isopropyltoluene 125 126 121 101 96.8 72.0-133 4.05 20
2-Butanone (MEK)625 652 684 104 109 30.0-160 4.79 24
Methylene Chloride 125 115 122 92.0 97.6 68.0-123 5.91 20
4-Methyl-2-pentanone (MIBK) 625 701 679 112 109 56.0-143 3.19 20
Methyl tert-butyl ether 125 134 136 107 109 66.0-132 1.48 20
Naphthalene 125 98.6 104 78.9 83.2 59.0-130 5.33 20
n-Propylbenzene 125 131 115 105 92.0 74.0-126 13.0 20
Styrene 125 124 128 99.2 102 72.0-127 3.17 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1659007
Volatile Organic Compounds (GC/MS) by Method 8260D L1342835-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3647493-1 04/26/21 11:53 • (LCSD) R3647493-2 04/26/21 12:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
1,1,1,2-Tetrachloroethane 125 137 145 110 116 74.0-129 5.67 20
1,1,2,2-Tetrachloroethane 125 112 103 89.6 82.4 68.0-128 8.37 20
Toluene 125 127 125 102 100 75.0-121 1.59 20
1,2,3-Trichlorobenzene 125 86.1 91.0 68.9 72.8 59.0-139 5.53 20
1,2,4-Trichlorobenzene 125 94.7 101 75.8 80.8 62.0-137 6.44 20
1,1,1-Trichloroethane 125 148 157 118 126 69.0-126 5.90 20
1,1,2-Trichloroethane 125 130 124 104 99.2 78.0-123 4.72 20
Trichloroethene 125 155 157 124 126 76.0-126 1.28 20
Trichlorofluoromethane 125 123 127 98.4 102 61.0-142 3.20 20
1,2,3-Trichloropropane 125 157 139 126 111 67.0-129 12.2 20
1,2,4-Trimethylbenzene 125 129 123 103 98.4 70.0-126 4.76 20
1,3,5-Trimethylbenzene 125 123 116 98.4 92.8 73.0-127 5.86 20
Vinyl chloride 125 109 112 87.2 89.6 63.0-134 2.71 20
Xylenes, Total 375 365 373 97.3 99.5 72.0-127 2.17 20
(S) Toluene-d8 105 100 75.0-131
(S) 4-Bromofluorobenzene 95.0 101 67.0-138
(S) 1,2-Dichloroethane-d4 115 114 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1660321
Volatile Organic Compounds (GC/MS) by Method 8260D L1342835-01
Method Blank (MB)
(MB) R3647992-3 04/29/21 02:48
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/kg ug/kg ug/kg
Tetrachloroethene U 0.896 2.50
(S) Toluene-d8 108 75.0-131
(S) 4-Bromofluorobenzene 103 67.0-138
(S) 1,2-Dichloroethane-d4 104 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3647992-1 04/29/21 01:32 • (LCSD) R3647992-2 04/29/21 01:51
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/kg ug/kg ug/kg %%%%%
Tetrachloroethene 125 106 106 84.8 84.8 70.0-136 0.000 20
(S) Toluene-d8 102 106 75.0-131
(S) 4-Bromofluorobenzene 107 109 67.0-138
(S) 1,2-Dichloroethane-d4 116 119 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Canada 1461.01 USDA P330-15-00234
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ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 22117 L1342835 04/30/21 15:39 15 of 16
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 22117 L1342835 04/30/21 15:50 15 of 16