MO-7402_36069_CA_MRP_20231006

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
October 9, 2023

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Ground Water Monitoring Report
September 2023
Handy Stop #7
1500 Rock Barn Road
Conover, Catawba County
North Carolina
Facility ID Number: 00-0-0000031674
Incident Number: 36069
GRI Project Number: 3067

Dear Mr. Newton,

Please find enclosed the referenced report for the above-mentioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Gail Williams; Shell brothers Distributors, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
September 2023
Handy Stop #7
1500 Rock Barn Road
Conover, Catawba County
North Carolina 28314
Facility ID Number: 00-0-0000031674
Incident Number: 36069
GRI Project Number: 3067

Prepared for:

Shell Brothers Distributors, Inc.
Ms. Gail Shell Williams
1-C Fountain Manor Drive, Unit. C
Greensboro, North Carolina 27401

October 6, 2023

Joanna Alley, P.E.
Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
ii
EXECUTIVE SUMMARY
Handy Stop #7 is located at 1500 Rock Barn Road in Conover, Catawba County, North Carolina. The site is
currently owned and operated by C.C Royal Enterprises, LLC as a petroleum retail facility and convenience
store. According to the North Carolina Registered Tank database, three 10,000-gallon gasoline USTs, one
5,200-gallon diesel UST and one 5,200-gallon kerosene UST are in use at the site. According to historical
information from the previous consultants, a release was discovered in March 2006 during a Phase II ESA.
The site and surrounding area are primarily commercial and residential. According to the 2013 update to
the receptor survey, a total of fourteen water supply wells were identified within 1,500 feet of the subject
site. There are five non-potable water supply wells located within 1,000 feet of the site. Please note that
on July 22, 2021, the property of water supply well WSW-3 was connected to municipal water. Public
water is available to the site and surrounding properties within 1,500 feet of the site.

In accordance with the 2009 CAP and 2016 system redesign, an AS and SVE system was installed at the
site and activated on February 20, 2018. The system installation included the installation and connection
of a total of five AS wells and six SVE wells throughout the contaminant plume. No projected milestones
were established in the CAP. The remediation system was shut down and winterized during the January
2022 site visit.

On September 20, 2023, ten monitoring wells, three telescoping wells and two observation wells were
gauged, purged and/or sampled. No free product was observed in any of the wells. The concentrations
of BTEX constituents, MTBE, naphthalene, TAA, TAME, TBA, isopropylbenzene, IPE, MIBK, n-
propylbenzene, styrene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene reported in the ground
water samples collected from MW-1R, MW-3, MW-4, DW-2, DW-3 and OW-2 exceeded the MACs. The
concentration of benzene reported in the ground water sample collected from DW-2 exceeded the GCL.

Calculations based on the September 2023 ground water sampling event indicate that contaminant mass
has been reduced by 18.4%, 14.7%, 97.2 and 96.1% in Areas 1 through 4, respectively, when compared to
the baseline sampling event. The total contaminant mass for the site has decreased by 41.1%.

Based on this information the risk ranking should remain intermediate risk. GRI recommends conducting
the formerly discussed feasibility study to determine the best remedial strategy for addressing the
contamination remaining in telescoping well DW-2.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
iii
SITE INFORMATION
1. Site Identification
 Handy Stop #7 (Facility ID 00-0-0000031674)
 Incident Number 36069 – Intermediate Risk (I210A)
 Location of Source Area: 1500 Rock Barn Road
Conover, NC 28314
Catawba County
35.7222431°N, 81.1843913°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Royal Enterprises, Inc.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
704-633-2434

UST/AST Operator
Royal Enterprises, Inc.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
704-633-2434

Property Owner
C.C. Royal Enterprises, LLC.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
Phone No. Unknown

Property Occupant
C.C. Royal Enterprises, LLC.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
Phone No. Unknown

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Certification No. 37735, 402
704-529-6364
3. Information about Release
 Release was discovered on March 14, 2006
 An unknown amount of product was released from the leaking UST System
 Three 10,000-gallon gasoline USTs, one 5,200-gallon diesel UST, and one 5,200-gallon kerosene
UST and associated pumps and product piping are active at the site

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... ii
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
3.0 FREE PRODUCT REMOVAL ........................................................................................................5
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................6
5.0 CONCLUSIONS .........................................................................................................................6
6.0 LIMITATIONS ...........................................................................................................................6
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................6

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Reports
Appendix D: Historical Soil Quality Information
Appendix E: Laboratory Analytical Report
Appendix F: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the September 2023 ground water sampling event at the Handy Stop #7 site;
located at 1500 Rock Barn Road in Conover, Catawba County, North Carolina. A topographic map showing
the general site location and the surrounding area is included as Figure 1. These activities were conducted
in accordance with GRI Proposal No. 23-372, which was submitted to the NCDEQ on June 28, 2023, and
was approved as Task Authorization No. 36069-65 on June 29, 2023. State correspondence is included as
Appendix A.

The site is currently owned and operated by C.C. Royal, Enterprises, LLC as a petroleum retail facility and
convenience store. According to historical information from the previous consultants, a release was
discovered in March 2006 during a Phase II ESA. Currently, three 10,000-gallon gasoline USTs, one 5,200-
gallon diesel UST, and one 5,200-gallon kerosene UST are active at the site. UST owner/operator
information and UST system information are included as Table 1 and Table 2, respectively. The Registered
Tank Report is shown below:

The site and surrounding area consists of primarily commercial and residential properties. A copy of the
Land Use table is included as Appendix B. The site contains three buildings (the store, car wash and
remediation system building) and is primarily capped with concrete and asphalt. The overall topography
at the site is relatively flat with a fairly steep elevation drop to the northeast and east of the site. Ten
Type II monitoring wells (MW-1 through MW-10), three Type III monitoring wells (DW-1 through DW-3),
two observation wells (OW-1 and OW-2), five air sparging wells (AS-1 through AS-5) and six vapor
extraction wells (SVE-1 through SVE-6) were installed at the site during previous ground water assessment
activities. Monitoring wells (MW-1R and MW-2) are 4” recovery wells. Monitoring well MW-3’s well pad
and well casing were previously damaged at grade level and were repaired during the February 2019 site
visit. During repair of the well, the well casing was shortened, and the top-of-casing elevation needs to

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
2
be re-measured. A Site Map showing the locations of the monitoring wells and the structures on-site is
included as Figure 2.

An update to the receptor survey was conducted in January 2013. A total of fourteen water supply wells
were identified within 1,500 feet of the subject site. There are five non-potable water supply wells located
within 1,000 feet of the site. Please note that on July 22, 2021, the property containing WSW-3 was
connected to municipal water; therefore, WSW-3 is no longer potable. Public water is available to the
site and surrounding properties within 1,500 feet of the site. No surface water bodies were identified
within a 500-foot radius of the site and the closest surface water body being an unnamed tributary of Mull
Creek, located approximately 800 feet southeast of the site. Receptor information is included in Table 3.
Adjacent property owner information is included in Table 4. A Site Vicinity Map showing the adjacent
properties and a Zoning Map showing the zoning information are included as Figure 3A and Figure 3B,
respectively.

Two AST incidents (Incident Nos. 91567 and 95863) have been reported on the highway adjacent to the
site. Copies of the NCDEQ Incident Reports are included as Appendix C. A map showing the locations of
additional incidents in the vicinity of the site is shown below:

In accordance with the 2009 CAP and 2016 system redesign, SVE and AS systems were installed at the site
and activated on February 20, 2018. The system installation included the installation and connection of a
total of five AS wells and six SVE wells throughout the contaminant plume. Due to the presence of free
product in OW-2 during previous ground water sampling activities in August 2018, air flow was shut off to
36069
95863
91567
8396
14413 14351

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
3
AS-4. Because free product has not been detected in OW-2 since January 2020, air flow to AS-4 was re-
established on May 19, 2021. The remediation system was shut down and winterized during the January
2022 site visit. To date, six MMPE events have been conducted at the site. A total of approximately
18,052.30 gallons of contaminated ground water and free product have been removed from the site.
Please note that no projected milestones were established in the CAP.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
from previous consultants is included as Appendix D.

On September 20, 2023, ten Type II monitoring wells (MW-1R and MW-2 through MW-10), two
observation wells (OW-1 and OW-2) and three telescoping wells (DW-1 through DW-3) were gauged,
purged and/or sampled in accordance with the NCDEQ guidelines. No free product was observed in any
of the wells. OW-1 appears to have a blockage at approximately 37 feet BGS and was unable to be
sampled. Depths to ground water in the Type II monitoring wells ranged from 32.49 feet to 37.27 feet.
Ground water elevations in the Type II monitoring wells ranged from 61.35 feet to 67.51 feet. Ground
water flow was generally towards the northwest with a horizontal gradient of approximately 0.03 feet per
foot. The vertical gradient between paired wells DW-2 and MW-3 could not be calculated because the
top-of-casing for MW-3 needs to be re-measured. Well construction and gauging information is included
in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A
summary of the current ground water gauging data is shown below:
Well ID
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
MW-1R 30 - 45 45 101.58 35.94 --- 65.64
MW-2 30 - 45 45 NM 34.26 --- NM
MW-3 30 - 45 45 NM 35.29 --- NM
MW-4 30 - 45 45 101.72 35.47 --- 66.25
MW-5 30 - 50 50 100.00 32.49 --- 67.51
MW-6 30 - 50 50 100.96 33.99 --- 66.97
MW-7 30 - 50 50 101.45 34.68 --- 66.77
MW-8 30 - 50 50 101.74 36.65 --- 65.09
MW-9 35 - 50 50 98.62 37.27 --- 61.35
MW-10 35 - 50 50 98.82 34.59 --- 64.23
DW-1 60 - 65 65 NM 37.50 --- NM
DW-2 85 - 90 90 100.06 37.56 --- 62.50
DW-3 115-120 120 NM 40.86 --- NM
OW-1 35 - 50 50 NM 36.45 --- NM
OW-2 35 - 50 50 NM 36.10 --- NM

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. The concentrations of BTEX constituents, MTBE, naphthalene, TAA, TAME, TBA,
isopropylbenzene, IPE, MIBK, n-propylbenzene, styrene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-1R, MW-3, MW-4, DW-2,
DW-3 and OW-2 exceeded the MACs. The concentration of benzene reported in the ground water sample

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
4
collected from DW-2 exceeded the GCL. A summary of the analytical results for ground water samples
collected on September 20, 2023, is included in Table 6. A Ground Water Quality Map based on the
September 2023 data is included in Figure 5. A complete report of laboratory analyses of the ground
water samples collected from the monitoring wells during the September 2023 sampling event is included
as Appendix E. A summary of the current ground water analytical data is shown below:

Contaminant of Concern → Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well ID
Date
Collected
(mm/dd/yy)
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1R 09/20/23 10.2 134 47.8 401 166 96.5
MW-2 09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 2.27
MW-3 09/20/23 <0.180 31.6 89.0 610 5.92 45.8
MW-4 09/20/23 0.212 J <0.220 <0.170 2.06 J 3.18 12.7
MW-5 09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 2.70
MW-6 09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-7 09/20/23 <0.180 <0.220 <0.170 <0.210 0.398 J <0.470
MW-8 09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-9 09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-10 09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
DW-1 09/20/23 <0.180 0.270 J <0.170 <0.210 <0.140 <0.470
DW-2 09/20/23 10,800 25,000 1,860 10,900 19,900 466
DW-3 09/20/23 129 3.12 J <1.70 107 103 14.1
OW-1 09/20/23 NS NS NS NS NS NS
OW-2 09/20/23 1,620 22,700 3,320 22,100 526 1,820

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the May 2017 ground water sampling event as well as the maximum
historical water column height observed in each area. The contaminant plume was divided into four areas
(Areas 1 through 4) based on the benzene concentrations during the May 2017 ground water sampling
event. The contaminant mass has been reduced by 18.4%, 14.7%, 97.2 and 96.1% in Areas 1 through 4,
respectively, when compared to the baseline sampling event. The total contaminant mass for the site has
decreased by 41.1%. Contaminant mass calculations are included as Appendix F. A map of the
contaminant mass areas is included as Figure 6. A chart depicting the overall declining trend in
contaminant mass is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
5

The site is located in the Piedmont Physiographic Province of North Carolina. The soils in the area are the
result of in-place weathering of the underlying bedrock, except along stream valleys where the soils are
comprised of alluvial materials and their weathered products. The water table has a seasonal high depth
to water of approximately 27 to 30 feet BGS.

The remediation system appears to have been effective at reducing ground water contaminant
concentration in the targeted wells; however, the system was not designed to address the deeper
contamination found in telescoping wells DW-2 and DW-3. Based on the contaminant concentrations
present in DW-2, additional remediation will be necessary. Please note that milestones were not
established in the CAP.
3.0 FREE PRODUCT REMOVAL
Free product was historically present in monitoring wells MW-1R, MW-3 and OW-2. To date, six MMPE
events have been conducted at the site. A total of approximately 18,052.30 gallons of contaminated
ground water and free product have been removed from the site. Of the 18,052.30 total gallons removed,
approximately 657.30 gallons of free product were removed. No free product has been identified since
the January 2020 sampling event.
0.00
5.00
10.00
15.00
20.00
25.00
-
10,000
20,000
30,000
40,000
50,000
60,000
70,000
80,000
90,000
Water Column Height (ft.)Total Contaminant Mass (grams)Total Contaminant Mass vs Time
Handy Stop #7
Total Contaminant Mass
(grams)
Average Water Column Height (ft)Linear (Total Contaminant Mass
(grams))

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 6, 2023 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
6
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently
in place at the site.
5.0 CONCLUSIONS
• On September 20, 2023, ten monitoring wells, two observation wells and three telescoping wells
were gauged, purged and/or sampled. No free product was observed in any of the wells. Ground
water flow was generally towards the northwest with a horizontal gradient of approximately 0.03
feet per foot.
• The concentrations of BTEX constituents, MTBE, naphthalene, TAA, TAME, TBA,
isopropylbenzene, IPE, MIBK, n-propylbenzene, styrene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-1R, MW-3, MW-4,
DW-2, DW-3 and OW-2 exceeded the MACs. The concentration of benzene reported in the
ground water sample collected from DW-2 exceeded the GCL.
• Based on this information the risk ranking should remain intermediate risk. GRI recommends
conducting the formerly discussed feasibility study to determine the best remedial strategy for
addressing the contamination remaining in telescoping well DW-2.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Shell Brothers Distributors, Inc. for specific
application to the referenced site in Catawba County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by the NCDEQ and with resources adequate only
for that scope of work. Our findings have been developed in accordance with generally accepted
standards of environmental practices in the State of North Carolina, available information, and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. 11/30/2023 Will this report be submitted
after the established due date?
YES NO

2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO

FIGURES
Copyright (C) 2009 MyTopo, 2006-2018 TomTom
081.2000000° W
081.2000000° W
081.1833333° W
081.1833333° W
081.1666666° W
081.1666666° W35.7535.7535.7333333° N35.7333333° N35.7166666° N35.7166666° N35.7000000° N35.7000000° NSCALE 1:24000
0 1000 2000 3000 4000 5000
FEET
Declination
MN 7.50° W
MN
Figure 1
Site Location Map
Handy Stop #7
1500 Rock Barn Road, Conover, Catawba County, NC
Incident No. 36069
GRI Project No. 3067
Date: 08/15/18
Scale: 1 inch = 2,000 ft.Copyright (C) 2009 MyTopo
Location: 035.7222431° N 081.1843913° W
Site Location
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FIGURE 3A: SITE VICINITY MAPHANDY STOP #71500 ROCK BARN ROADCONOVER, CATAWBA COUNTYNORTH CAROLINAINCIDENT NO. 36069GRI NO. 3067
PREPARED BYGEOLOGICAL RESOURCES, INC.MAY 9, 20181,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
³
0 300150Feet
1 inch = 300 feet
LEGEND
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WSW-11
WSW-10
FIGURE 3B: ZONING MAPHANDY STOP #71500 ROCK BARN ROADCONOVER, CATAWBA COUNTYNORTH CAROLINAINCIDENT NO. 36069GRI NO. 3067
PREPARED BYGEOLOGICAL RESOURCES, INC.DECEMBER 14, 20211,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
³
0 300150Feet
1 inch = 300 feet
LEGEND
"J Water Supply Well
Street Centerlines
Streams
ZONING O-I
ZONING - M-1
ZONING - R-20
ZONING - B-4
ZONING - B-2
Parcels
SSSSSS

TABLES
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner/Operator
1024 Browning Road, Greensboro, NC 27410 336-339-1394
0-031674
Name of Owner or Operator Dates of Ownership / Operation
Shell Brothers, Inc. 02/19/1990 - 10/01/2006
Address Telephone Number
Royal Enterprises Inc. 10/01/2006-Present
Address Telephone Number
322 E. Fisher Street Suite 101, Salisbury, NC 28144-5059 704-633-2434
TABLE 1
UST OWNER/OPERATOR INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
0-031674
Name of Owner or Operator Dates of Ownership / Operation
Page 1 of 1
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 10,000 02/19/90 Steel 8' X 26.6' Fiberglass Current Yes
2 Gasoline Gasoline 10,000 02/19/90 Steel 8' X 26.6' Fiberglass Current Yes
3 Gasoline Gasoline 10,000 02/19/90 Steel 8' X 26.6' Fiberglass Current Yes
4 Diesel Diesel 5,200 02/19/90 Steel 8' X 13.4' Fiberglass Current No
5 Kerosene Kerosene 5,200 02/19/90 Steel 8' X 13.4' Fiberglass Current No
Construction
Details Tank Dimensions
Description
of
Associated
Product Piping
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 01/13/2020 Facility ID # : 0-031674
UST ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Tank Date
Installed
Page 1 of 1
Facility ID # : 0-031674
Well ID.Previous
Well ID.Parcel ID No.Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Municipal
Water
Connected?
Well
Depth
(ft. BGS)
Type of
Well
(Drilled/
Bored)
Well
Casing
Depth
(ft. BGS)
Well
Screen
Interval
(x to y ft.
BGS)
Distance from
source area of
release
(ft.)
Comments
WSW-3 WSW-7 375209251067 Gateway 4 Properties, LLC 785 HIGHWAY 70 SE, SUITE 100
HICKORY, NC 28602-5096
1506 ROCK BARN RD NE
CONOVER, NC 28613 Irrigational Yes Unknown Unknown Unknown Unknown ~520' NE
Interviewed
resident
WSW-4 WSW-8 375209251253 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658-4318
1508 ROCK BARN RD NE
CONOVER, NC 28613
Not In Use/No
pump Yes Unknown Unknown Unknown Unknown ~560' NE
Owner
Confirmed
WSW-5 WSW-9 375209253474 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658-4318
1510 ROCK BARN RD NE
CONOVER, NC 28613
Non-
Potable/garage
use only
Yes Unknown Unknown Unknown Unknown ~735' NE
No water meter
found
WSW-6 WSW-11 375209254897 Edward Elliot 3525 ROCK BARN RD NE
CONOVER, NC 28613
3525 ROCK BARN RD NE
CONOVER, NC 28613 Not in Use Yes Unknown Unknown Unknown Unknown ~1,186' NE
WSW-7 WSW-10 375209253926 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658
3557 ROCK BARN RD NE
CONOVER, NC 28613
Not In Use/No
Pump Yes Unknown Unknown Unknown Unknown ~1,107' NE
WSW-8 WSW-6 375209159389 JERRY WAYNE ISENHOUR 1399 BRANDYWINE
HICKORY, NC 28602-8269
1505 ROCK BARN RD NE
CONOVER, 28613 Irrigational Yes Unknown Unknown Unknown Unknown ~675' NE
Owner
Confirmed
WSW-9 WSW-12 375210364087
3223 JOHN DANIEL DRIVE NE
CONOVER, NC 28613 Yes No Unknown Unknown Unknown Unknown ~1,279' E
WSW-10 WSW-4 375209152625 Potable Unknown Unknown Unknown Unknown Unknown ~1,115' NW
WSW-12 WSW-3 375209152625
Not In Use/No
Power to well Yes Unknown Unknown Unknown Unknown ~581' NW
WSW-15 WSW-15 375213037912 ALTON EUGENE ROBERTS
4211 LANEY ROAD
MAIDEN, NC 28650
1346 ROCK BARN RD NE
CONOVER, 28613 Unknown Unknown Unknown Unknown Unknown Unknown ~1,500' SW
Left a well use
survey at
residence,
survey not
returned.
WSW-16 WSW-17 375213045062 MICHAEL DEAN ROBERTS
1344 ROCK BARN RD NE,
CONOVER, NC 28613-7565
1344 ROCK BARN RD NE,
CONOVER, NC 28613 Unknown Unknown Unknown Unknown Unknown Unknown ~1,234' SW Residence
vacant
WSW-17 WSW-16 375213048172 MARY SHOOK ROBERTS HEIRS
2729 SIDES DR,
CONELLYS SPRINGS NC 28612-7771
1350 ROCK BARN LN,
CONOVER NC 28613 Unknown Unknown Unknown Unknown Unknown Unknown ~1,320' SW
Left a well use
survey at
residence,
survey not
returned.
WSW-18 WSW-13 375213133824 OLD DOMINION FREIGHT LINE, INC 500 OLD DOMINION WAY
THOMASVILLE, NC 27360-8923
102 BANNER ROAD NE
CONOVER, NC 28613
Non-
Potable/Washing
trucks
Yes Unknown Unknown Unknown Unknown ~1,121' SW
WSW-19 WSW-18 375213139813 CHARLES DEAN ROBERTS, LFI
114 BANNER ROAD NE
CONOVER, NC 28613-8116
114 BANNER ROAD NE
CONOVER, NC 28613 Potable No Unknown Unknown Unknown Unknown ~1,253' S Interviewed
resident
Notes:
• Water supply wells are keyed to Figure 3.
• Ft. BGS : Feet below ground surface
• Receptor survey last updated January 2013.
Date: 4/28/2023
TABLE 3
WATER SUPPLY WELL INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
HUNSUCKER FARMS LLC 3223 JOHN DANIEL DRIVE NE
CONOVER, NC 28613 1503 ROCK BARN RD NE
CONOVER, 28613
Page 1 of 1
DATE: 04/27/23 Facility ID #: 0-031674
Parcel ID Address Owner Name Owner Address
375213147933
(site)
1500 Rock Barn Road NE
Conover, NC C.C. Royal Properties, LLC 322 E Fisher Street, Suite 101
Salisbury, NC 28144-5059
375209152625 1503 Rock Barn Road NE
Conover, NC Hunsucker Farms, LLC 3223 John Daniel Drive NE
Conover, NC 28613-8972
375209159389 1505 Rock Barn Road NE
Conover, NC Jerry Wayne Isenhour 1399 Brandywine Hickory
NC 28602-8269
375213240895 1504 Rock Barn Road NE
Conover, NC Estes Express Lines 3901 W Broad St,
Richmond, VA 23230-3962
Note:
• Properties are keyed to Figure 3.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Page 1 of 1
Facility ID # : 0-031674
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
08/23/06 39.85 --- --- 61.73
12/05/07 43.87 43.84 0.03 57.73
10/20/08 43.69 43.66 0.03 57.91
11/24/08 44.15 44.14 0.01 57.44
12/12/08 44.25 --- --- 57.33
08/04/09 40.81 --- --- 60.77
09/06/11 40.89 --- --- 60.69
05/20/13 39.24 --- --- 62.34
02/28/14 36.92 --- --- 62.34
04/08/14 38.13 --- --- 63.45 Pre AS Test
06/16/14 36.71 --- --- 64.87
08/11/14 37.82 37.81 0.01 63.77 Pre-MMPE
08/15/14 42.98 --- --- 58.60 Post-MMPE
09/02/14 38.21 --- --- 63.37
01/19/15 39.21 --- --- 62.37 Pre-MMPE
01/23/15 44.05 --- --- 57.53 Post-MMPE
01/30/15 39.38 --- --- 62.20
04/15/15 39.56 --- --- 62.02
06/15/15 38.96 --- --- 62.62 Pre-MMPE
06/19/15 43.03 --- --- 58.55 Post-MMPE
07/28/15 30.98 --- --- 70.60
04/06/16 36.82 --- --- 64.76
07/11/16 37.41 --- --- 64.17 Pre-MMPE
07/15/16 39.35 --- --- 62.23 Post-MMPE
08/09/16 37.61 --- --- 63.97
05/02/17 40.72 --- --- 60.86
04/19/18 38.38 --- --- 63.20
08/13/18 36.93 --- --- 64.65
10/15/18 36.23 --- --- 65.35
01/22/19 32.60 --- --- 68.98
04/08/19 31.72 --- --- 69.86
07/29/19 31.72 --- --- 69.86
10/08/19 34.25 --- --- 67.33
01/02/20 34.21 --- --- 67.37
10/13/20 29.55 --- --- 72.03
04/08/21 28.78 --- --- 72.80
10/20/21 34.18 --- --- 67.40
04/05/22 36.81 --- 0.00 64.77
04/03/23 33.60 --- 0.00 67.98
09/20/23 35.94 --- --- 65.64
08/23/06 39.56 --- --- NM
12/05/07 DRY DRY DRY NM
10/20/08 DRY DRY DRY NM
11/24/08 DRY DRY DRY NM
12/12/08 38.57 --- --- NM
08/04/09 37.18 --- --- NM
09/06/11 36.75 --- --- NM
05/20/13 36.52 --- --- NM
08/11/14 35.46 --- --- NM Pre-MMPE
08/15/14 35.41 --- --- NM Post-MMPE
09/02/14 35.56 --- --- NM
07/28/15 35.79 --- --- NM
04/06/16 33.99 --- --- NM
05/02/17 36.26 --- --- NM
04/19/18 35.36 --- --- NM
08/13/18 34.20 --- --- NM
10/15/18 NM --- --- NM Blocked By Car
01/22/19 29.42 --- --- NM
04/08/19 29.31 --- --- NM
07/29/19 30.25 --- --- NM
10/08/19 33.84 --- --- NM
01/02/20 31.48 --- --- NM
04/14/20 29.50 --- --- NM
10/13/20 27.00 --- --- NM
04/08/21 27.29 --- --- NM
04/05/22 33.93 --- 0.00 NM
04/03/23 31.73 --- 0.00 NM
09/20/23 34.26 --- --- NM
101.584530-4530408/10/06MW-1R
MW-2 08/10/06 4 30 30-45 45 NM
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 10/02/23
Page 1 of 6
Facility ID # : 0-031674
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 10/02/23
08/23/06 39.49 --- --- 62.51
12/05/07 42.93 --- --- 59.07
10/20/08 43.82 --- --- 58.18
11/24/08 43.99 --- --- 58.01
12/12/08 44.09 --- --- 57.91
08/04/09 41.01 --- --- 60.99
09/06/11 40.45 --- --- 61.55
05/20/13 39.55 --- --- 62.45
06/16/14 36.74 --- --- 65.26
07/28/15 NM NM NM NM
04/06/16 NM NM NM NM
02/28/19 NM NM 0.25 NM
Bailer
Confirmed***03/11/19 33.30 33.27 0.03 NM Pre-MMPE
03/15/19 41.01 --- --- NM Post-MMPE
04/08/19 32.80 NM NM NM F.P. After Bailing
07/29/19 33.37 --- --- NM
09/09/19 33.26 --- --- NM Pre-MMPE
09/13/19 33.43 --- --- NM Post-MMPE
10/08/19 34.08 --- --- NM
01/02/20 34.85 --- --- NM
10/13/20 30.43 --- --- NM
04/08/21 28.94 --- --- NM
10/20/21 37.13 --- --- NM Sheen
04/05/22 36.35 --- 0.00 NM
04/03/23 34.81 --- 0.00 NM
09/20/23 35.29 --- --- NM
08/23/06 38.87 --- --- 62.85
12/05/07 42.18 --- --- 59.54
10/20/08 43.33 --- --- 58.39
11/24/08 43.50 --- --- 58.22
12/12/08 43.66 --- --- 58.06
08/04/09 40.65 --- --- 61.07
09/06/11 39.88 --- --- 61.84
05/20/13 39.19 --- --- 62.53
07/28/15 38.96 --- --- 62.76
04/06/16 37.04 --- --- 64.68
08/09/16 37.32 --- --- 64.40
05/02/17 40.33 --- --- 61.39
04/19/18 38.81 --- --- 62.91
08/13/18 37.36 --- --- 64.36
10/15/18 37.06 --- --- 64.66
01/22/19 35.28 --- --- 66.44
04/08/19 33.43 --- --- 68.29
07/29/19 32.71 --- --- 69.01
10/08/19 34.08 --- --- 67.64
01/02/20 35.07 --- --- 66.65
10/13/20 31.29 --- --- 70.43
04/08/21 29.97 --- --- 71.75
10/20/21 33.90 --- --- 67.82
04/05/22 36.53 --- 0.00 65.19
04/03/23 34.20 --- 0.00 67.52
09/20/23 35.47 --- --- 66.25
12/05/07 37.60 --- --- 62.40
10/20/08 35.35 --- --- 64.65
11/24/08 37.91 --- --- 62.09
12/12/08 37.05 --- --- 62.95
08/04/09 35.45 --- --- 64.55
09/06/11 36.44 --- --- 63.56
05/20/13 33.53 --- --- 66.47
07/28/15 36.19 --- --- 63.81
04/06/16 33.33 --- --- 66.67
05/02/17 35.72 --- --- 64.28
04/19/18 34.31 --- --- 65.69
08/13/18 32.08 --- --- 67.92
10/15/18 31.71 --- --- 68.29
01/22/19 29.56 --- --- 70.44
04/08/19 28.53 --- --- 71.47
07/29/19 28.83 --- --- 71.17
10/08/19 31.82 --- --- 68.18
01/02/20 29.80 --- --- 70.20
10/13/20 26.45 --- --- 73.55
04/08/21 25.67 --- --- 74.33
04/05/22 31.68 --- 0.00 68.32
04/03/23 30.27 --- 0.00 69.73
09/20/23 32.49 --- --- 67.51
NM
4530-4530208/10/06MW-3
MW-4 08/10/06
Well Casing
Blocked
102.00
2 30 30-45 45 101.72
100.005030-5030212/03/07MW-5
Page 2 of 6
Facility ID # : 0-031674
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 10/02/23
12/05/07 43.11 --- --- 57.85
10/20/08 41.06 --- --- 59.90
11/24/08 42.28 --- --- 58.68
12/12/08 42.52 --- --- 58.44
08/04/09 37.72 --- --- 63.24
09/06/11 39.42 --- --- 61.54
05/20/13 34.99 --- --- 65.97
07/28/15 37.89 --- --- 63.07
04/06/16 33.56 --- --- 67.40
05/02/17 37.69 --- --- 63.27
04/19/18 35.38 --- --- 65.58
08/13/18 33.71 --- --- 67.25
10/15/18 NM --- --- NM Blocked by Car
01/22/19 29.01 --- --- 71.95
04/08/19 29.05 --- --- 71.91
07/29/19 30.04 --- --- 70.92
10/08/19 33.77 --- --- 67.19
01/02/20 30.91 --- --- 70.05
10/13/20 28.72 --- --- 72.24
04/08/21 26.93 --- --- 74.03
04/05/22 33.12 --- 0.00 67.84
04/03/23 31.32 --- 0.00 69.64
09/20/23 33.99 --- --- 66.97
12/05/07 41.73 --- --- 59.72
10/20/08 42.83 --- --- 58.62
11/24/08 42.88 --- --- 58.57
12/12/08 43.08 --- --- 58.37
08/04/09 39.86 --- --- 61.59
09/06/11 39.23 --- --- 62.22
05/20/13 38.51 --- --- 62.94
07/28/15 38.17 --- --- 63.28
04/06/16 36.03 --- --- 65.42
05/02/17 49.06 --- --- 52.39
04/19/18 37.89 --- --- 63.56
08/13/18 36.39 --- --- 65.06
10/15/18 49.42 --- --- 52.03
01/22/19 48.99 --- --- 52.46
04/08/19 32.26 --- --- 69.19
07/29/19 31.79 --- --- 69.66
10/08/19 49.53 --- --- 51.92
01/02/20 34.39 --- --- 67.06
10/13/20 30.32 --- --- 71.13
04/08/21 29.05 --- --- 72.40
04/05/22 35.79 --- 0.00 65.66
04/03/23 33.23 --- 0.00 68.22
09/20/23 34.68 --- --- 66.77
12/05/07 44.17 --- --- 57.57
10/20/08 44.51 --- --- 57.23
11/24/08 44.88 --- --- 56.86
12/12/08 45.03 --- --- 56.71
08/04/09 41.35 --- --- 60.39
09/06/11 41.50 --- --- 60.24
05/20/13 39.75 --- --- 61.99
02/28/14 49.65 --- --- 52.09
04/08/14 38.31 --- --- 63.43 Pre AS Test
08/11/14 38.39 --- --- 63.35 Pre-MMPE
08/15/14 38.95 --- --- 62.79 Post-MMPE
09/02/14 38.78 --- --- 62.96
01/19/15 39.88 --- --- 61.86 Pre-MMPE
01/23/15 40.38 --- --- 61.36 Post-MMPE
01/30/15 39.98 --- --- 61.76
04/15/15 39.36 --- --- 62.38
06/15/15 39.49 --- --- 62.25 Pre-MMPE
06/19/15 40.16 --- --- 61.58 Post-MMPE
07/28/15 40.49 --- --- 61.25
04/06/16 37.19 --- --- 64.55
07/11/16 37.98 --- --- 63.76 Pre-MMPE
07/15/16 38.35 --- --- 63.39 Post-MMPE
08/09/16 38.19 --- --- 63.55
05/02/17 41.35 --- --- 60.39
04/19/18 39.49 --- --- 62.25
08/13/18 37.40 --- --- 64.34
10/15/18 36.90 --- --- 64.84
01/22/19 33.63 --- --- 68.11
03/11/19 32.47 --- --- 69.27 Pre-MMPE
03/15/19 32.61 --- --- 69.13 Post-MMPE
04/08/19 32.32 --- --- 69.42
MW-6 12/03/07 2 30 30-50 50 100.96
101.455030-5030212/03/07MW-7
30 30-50 50 101.74MW-8 12/03/07 2
Page 3 of 6
Facility ID # : 0-031674
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 10/02/23
07/29/19 32.68 --- --- 69.06
09/09/19 34.17 --- --- 67.57 Pre-MMPE
09/13/19 34.59 --- --- 67.15 Post-MMPE
10/08/19 49.52 --- --- 52.22
01/02/20 35.40 --- --- 66.34
10/13/20 30.66 --- --- 71.08
04/08/21 29.64 --- --- 72.10
10/20/21 49.70 --- --- 52.04
04/05/22 37.63 --- 0.00 64.11
04/03/23 NM NM NM NM Dry
09/20/23 36.65 --- --- 65.09
01/16/13 42.61 --- --- 56.01
05/20/13 38.64 --- --- 59.98
07/28/15 40.23 --- --- 58.39
04/06/16 36.30 --- --- 62.32
05/02/17 41.02 --- --- 57.60
04/19/18 38.56 --- --- 60.06
08/13/18 37.44 --- --- 61.18
10/15/18 36.84 --- --- 61.78
01/22/19 32.91 --- --- 65.71
04/08/19 31.68 --- --- 66.94
07/29/19 32.81 --- --- 65.81
10/08/19 35.65 --- --- 62.97
01/02/20 35.58 --- --- 63.04
10/13/20 30.76 --- --- 67.86
04/08/21 29.40 --- --- 69.22
10/20/21 36.32 --- --- 62.30
04/05/22 37.49 --- 0.00 61.13
04/03/23 34.08 --- 0.00 64.54
09/20/23 37.27 --- --- 61.35
01/16/13 41.00 --- --- 57.82
05/20/13 38.02 --- --- 60.80
07/28/15 38.90 --- --- 59.92
04/06/16 35.71 --- --- 63.11
05/02/17 39.81 --- --- 59.01
04/19/18 37.68 --- --- 61.14
08/13/18 36.45 --- --- 62.37
10/15/18 36.11 --- --- 62.71
01/22/19 32.94 --- --- 65.88
04/08/19 31.66 --- --- 67.16
07/29/19 32.09 --- --- 66.73
10/08/19 34.44 --- --- 64.38
01/02/20 34.72 --- --- 64.10
10/13/20 30.34 --- --- 68.48
04/08/21 29.20 --- --- 69.62
10/20/21 34.58 --- --- 64.24
04/05/22 36.06 --- 0.00 62.76
04/03/23 33.31 --- 0.00 65.51
09/20/23 34.59 --- --- 64.23
11/24/08 45.16 --- --- NM
12/12/08 46.09 --- --- NM
08/04/09 41.81 --- --- NM
09/06/11 41.95 --- --- NM
05/20/13 40.33 --- --- NM
07/28/15 40.91 --- --- NM
04/06/16 38.09 --- --- NM
08/09/16 38.81 --- --- NM
05/02/17 41.76 --- --- NM
04/19/18 39.88 --- --- NM
08/13/18 38.54 --- --- NM
10/15/18 37.91 --- --- NM
01/22/19 35.08 --- --- NM
04/08/19 33.75 --- --- NM
07/29/19 33.83 --- --- NM
10/08/19 38.18 --- --- NM
01/02/20 36.21 --- --- NM
10/13/20 DRY --- --- NM
04/08/21 30.30 --- --- NM
10/20/21 63.03 --- --- NM Limited Volume
04/05/22 37.97 --- 0.00 NM
04/03/23 33.02 --- 0.00 NM
09/20/23 37.50 --- --- NM
212/03/07MW-8
98.82
11/24/08DW-1
35 35-50 50
98.625035-5035201/02/13MW-9
MW-10 01/02/13 2
101.745030-5030
NM6560-65602
Page 4 of 6
Facility ID # : 0-031674
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 10/02/23
01/16/13 43.28 --- --- 56.78
02/11/13 42.48 --- --- 57.58
05/20/13 40.78 --- --- 59.28
07/28/15 41.66 --- --- 58.40
04/06/16 38.64 --- --- 61.42
08/09/16 39.57 --- --- 60.49
05/02/17 42.31 --- --- 57.75
04/19/18 40.76 --- --- 59.30
08/13/18 39.26 --- --- 60.80
10/15/18 38.55 --- --- 61.51
01/22/19 35.77 --- --- 64.29
03/11/19 34.65 --- --- 65.41 Pre-MMPE
03/15/19 41.03 --- --- 59.03 Post-MMPE
04/08/19 34.47 --- --- 65.59
07/29/19 34.70 --- --- 65.36
09/09/19 36.04 --- --- 64.02 Pre-MMPE
09/13/19 39.01 --- --- 61.05 Post-MMPE
10/08/19 36.20 --- --- 63.86
01/02/20 36.87 --- --- 63.19
10/13/20 34.00 --- --- 66.06
04/08/21 31.75 --- --- 68.31
10/20/21 36.82 --- --- 63.24
04/05/22 38.51 --- 0.00 61.55
04/03/23 35.98 --- 0.00 64.08
09/20/23 37.56 --- --- 62.50
03/26/13 NM NM NM NM
05/20/13 24.31 --- --- NM
07/28/15 43.76 --- --- NM
04/06/16 40.35 --- --- NM
05/02/17 44.73 --- --- NM
04/19/18 41.92 --- --- NM
08/13/18 41.36 --- --- NM
10/15/18 40.43 --- --- NM
01/22/19 37.56 --- --- NM
03/11/19 36.37 --- --- NM Pre-MMPE
03/15/19 36.68 --- --- NM Post-MMPE
04/08/19 36.47 --- --- NM
07/29/19 37.25 --- --- NM
09/09/19 33.73 --- --- NM Pre-MMPE
09/13/19 39.07 --- --- NM Post-MMPE
10/08/19 39.86 --- --- NM
01/02/20 39.18 --- --- NM
10/13/20 35.15 --- --- NM
04/08/21 34.02 --- --- NM
10/20/21 44.35 --- --- NM
04/05/22 40.61 --- 0.00 NM
04/03/23 38.18 --- 0.00 NM
09/20/23 40.86 --- --- NM
02/28/14 37.89 --- --- NM
04/08/14 38.70 --- --- NM
06/16/14 37.38 --- --- NM
08/11/14 38.52 --- --- NM Pre-MMPE
08/15/14 39.60 --- --- NM Post-MMPE
09/02/14 38.91 --- --- NM
01/19/15 39.99 --- --- NM Pre-MMPE
01/23/15 40.91 --- --- NM Post-MMPE
01/30/15 40.13 --- --- NM
04/15/15 39.74 --- --- NM
06/15/15 39.68 --- --- NM Pre-MMPE
06/19/15 40.91 --- --- NM Post-MMPE
07/28/15 40.64 --- --- NM
04/06/16 37.38 --- --- NM
07/11/16 38.17 --- --- NM Pre-MMPE
07/15/16 38.93 --- --- NM Post-MMPE
08/09/16 38.34 --- --- NM
05/02/17 41.46 --- --- NM
04/19/18 39.53 --- --- NM
08/13/18 37.86 --- --- NM
10/15/18 37.26 --- --- NM
01/22/19 34.10 --- --- NM
03/11/19 32.85 --- --- NM Pre-MMPE
03/15/19 33.08 --- --- NM Post-MMPE
04/08/19 34.55 --- --- NM
07/29/19 32.91 --- --- NM
09/09/19 34.46 --- --- NM Pre-MMPE
09/13/19 39.04 --- --- NM Post-MMPE
10/08/19 35.44 --- --- NM
NM5035-5035202/24/14OW-1
DW-3
DW-2 01/03/13 2 85 85-90 90 100.06
NM120115-120115203/26/13
Page 5 of 6
Facility ID # : 0-031674
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 10/02/23
01/02/20 35.53 --- --- NM
10/13/20 35.53 --- --- NM
04/08/21 30.12 --- --- NM
10/20/21 35.61 ------NM Mud
04/05/22 37.16 ---0.00 NM
04/03/23 34.26 ---0.00 NM
09/20/23 36.45 ------NM
02/28/14 38.38 --- --- NM
04/08/14 NM Observed ~3 NM
Equipment
Malfunction, bailer
confirmed
06/16/14 39.30 36.27 3.03 NM
08/11/14 40.27 37.40 2.87 NM Pre-MMPE
08/15/14 43.96 --- --- NM Post-MMPE
09/02/14 39.21 38.16 1.05 NM
01/19/15 40.82 39.01 1.81 NM Pre-MMPE
01/23/15 45.91 --- --- NM Post-MMPE
01/30/15 39.52 --- --- NM
04/15/15 39.14 --- --- NM
06/15/15 39.17 39.11 0.06 NM Pre-MMPE
06/19/15 47.32 --- --- NM Post-MMPE
07/28/15 40.13 --- --- NM
04/06/16 37.84 ₳ ₳ NM Bailer Confirmed
07/11/16 37.28 --- --- NM Pre-MMPE
07/15/16 41.75 --- --- NM Post-MMPE
08/09/16 37.88 37.77 0.11 NM
05/02/17 40.91 --- --- NM
04/19/18 39.04 --- --- NM
08/13/18 38.35 37.19 1.16 NM Bailer Confirmed
10/15/18 37.54 36.72 0.82 NM Bailer Confirmed
01/22/19 33.71 33.41 0.30 NM Bailer Confirmed
03/11/19 32.56 32.53 0.03 NM Pre-MMPE
03/15/19 42.08 --- --- NM Post-MMPE
04/08/19 31.63 31.60 0.03 NM
07/29/19 32.34 32.23 0.11 NM
09/09/19 33.85 33.62 0.23 NM Pre-MMPE
09/13/19 40.03 --- --- NM Post-MMPE
10/08/19 34.81 --- --- NM
01/02/20 34.73 34.72 0.01 NM Bailer Confirmed
04/14/20 31.90 --- --- NM
10/13/20 32.05 --- --- NM
04/08/21 29.02 --- --- NM
10/20/21 34.81 --- --- NM
04/05/22 37.02 --- 0.00 NM
04/03/23 41.79 --- 0.00 NM
09/20/23 36.10 --- --- NM
02/28/14 37.44 --- --- NM
04/08/14 37.06 --- --- NM Pre AS Test
08/11/14 38.25 --- --- NM Pre-MMPE
08/15/14 39.56 --- --- NM Post-MMPE
09/02/14 38.84 --- --- NM
01/19/15 39.62 --- --- NM Pre-MMPE
01/23/15 40.93 --- --- NM Post-MMPE
01/30/15 40.09 --- --- NM
04/15/15 39.52 --- --- NM
06/15/15 39.45 --- --- NM Pre-MMPE
06/19/15 41.45 --- --- NM Post-MMPE
07/28/15 40.46 --- --- NM
04/06/16 37.21 --- --- NM
07/11/16 37.82 --- --- NM Pre-MMPE
07/15/16 39.20 --- --- NM Post-MMPE
08/09/16 38.11 --- --- NM
05/02/17 41.55 --- --- NM
AS-2 03/21/17 05/02/17 2 50 50-55 55 NM 41.63 --- --- NM
AS-3 03/21/17 05/02/17 2 50 50-55 55 NM 40.67 --- --- NM
AS-4 03/21/17 05/02/17 2 50 50-55 55 NM 40.82 --- --- NM
AS-5 03/22/17 05/02/17 2 50 50-55 55 NM 41.19 --- --- NM
Notes:
• * : Reference point for elevation measurements.
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• *** : Well pad was repaired, casing was cut and well was unblocked on February 28, 2019.
• ft BGS : feet below ground surface.
• N/A: Not available.
• NM: Not measured.
• Well construction information (where available) is reproduced from the previous consultants reports and available field notes.
• ₳: No interface probe, bailer checked - 9.73" product w/ scale
NM5035-5035202/24/14OW-2
OW-1 02/24/14 2 35 35-50 50 NM
NM5550-5550202/24/14AS-1
Page 6 of 6
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NE
09/06/11 8,660 36,200 2,790 16,310 905 918 NR NR NR NR NR **801 *171 J **2,290 568 258 <5.0 61,900 31,950 <95 19,160
05/20/13 9,620 38,100 3,590 21,700 889 1,490 NR NR NR NR NR **946 *302 **3,900 932 602 NR 28,400 13,500 <980 16,870
07/29/15 2,880 16,500 2,010 13,600 619 1,420 NR NR NR NR NR **450 *200 **2,530 613 NR NR NR NR NR NR
04/06/16 1,260 10,300 1,360 10,900 335 1,210 NR NR NR NR NR **271 *114 **2,470 759 NR NR NR NR NR NR
08/09/16 2,350 14,100 2,140 16,300 538 1,530 NR NR NR NR NR **350 *208 **3,050 690 NR NR NR NR NR NR
05/03/17 1,380 12,800 1,700 13,200 330 1,060 NR NR NR NR NR **272 *217 **2,820 747 NR NR NR NR NR NR
04/19/18 1,740 14,600 1,360 14,000 255 992 NR NR NR NR NR **256 *119 **2,230 606 NR NR NR NR NR NR
08/13/18 1,420 11,200 1,090 11,500 448 1,150 NR NR NR NR NR **281 *108 J **2,260 646 NR NR NR NR NR NR
10/15/18 1,510 13,000 1,460 12,200 553 1,500 NR NR NR NR NR **249 *162 **2,800 688 NR NR NR NR NR NR
01/22/19 742 11,700 1,440 12,500 748 904 NR NR NR NR NR **196 *128 **2,440 570 NR NR NR NR NR NR
04/08/19 332 10,900 1,660 14,300 259 667 NR NR NR NR NR **52 *122 J **2,410 579 NR NR NR NR NR NR
07/29/19 655 15,600 1,920 13,100 403 720 NR NR NR NR NR **92.7 J *126 J **2,060 534 NR NR NR NR NR NR
10/08/19 1,050 17,600 2,250 13,500 352 1,080 NR NR NR NR NR **97.7 J *163 J **2,450 621 NR NR NR NR NR NR
01/02/20 154 3,740 430 5,990 96.7 381 <200 30.1 J NR * NR * * 17.9 J *33.0 J **1,390 391 NR NR NR NR NR NR
10/13/20 193 2,390 254 5,260 168 469 318 J 29.8 J NR * NR * * 60.3 *34.8 **1,640 346 NR NR NR NR NR NR
04/08/21 58.4 610 55.9 2,390 365 50.7 881 53.8 <2.5 * <2.5 * *97.3 *9.3 J **975 242 NR NR NR NR NR NR
10/20/21 16.1 100 11.7 90.5 286 3.1 J 1,430 35.3 <1.3 <20 <1.3 * * 52.0 *2.1 J **15.4 50.4 NR NR NR NR NR NR
04/05/22 128 1,930 176 2,190 682 107 555 52.3 <6.3 <100 <6.3 * <6.3 153 *9.7 J <6.3 <6.3 390 127 NR NR NR NR NR NR
04/04/23 8.77 140 24.4 507 181 63.4 564 26.7 J <1.60 <16.0 <1.90 17.1 2.42 J 35.2 7.82 J 3.84 J <2.20 <2.20 161 81.1 NR NR NR NR NR NR
09/20/23 10.2 134 47.8 401 166 96.5 203 20.5 J <1.60 78.4 J <1.90 <3.80 3.45 J 17.1 M <0.780 6.00 <2.20 <2.20 198 75.9 NR NR NR NR NR NR
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR **<0.11 *<0.11 **<0.10 <0.10 <0.54 6.8 <35 <130 222 165
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.68 NR <35 <132 <97 <185
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR **<0.16 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.16 J NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 0.17 J 0.96 0.15 J 0.74 J <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 NS NS NS NS NS NS NR NR NR NR NR **NS *NS **NS NS NS NS NS NS NS NS
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * *<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 <0.13 *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 2.27 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NRTetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneMW-1R
MW-2
GCL (mg/l)
Page 1 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
09/06/11 713 3,520 2,200 11,770 19,400 761 NR NR NR NR NR **3,110 *274 **2,530 679 199 <5.0 22,500 25,820 <100 18,610
05/20/13 303 3,670 2,580 14,800 12,100 1,170 NR NR NR NR NR **1,820 *394 **3,360 856 NA NR <35 3,937.5 <980 4,184
07/29/15 NS NS NS NS NS NS NR NR NR NR NR **NS *NS **NS NS NS NS NS NS NS NS
04/06/16 NS NS NS NS NS NS NR NR NR NR NR **NS *NS **NS NS NS NS NS NS NS NS
03/11/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/29/19 697 10,200 1,880 12,500 912 889 NR NR NR NR NR **213 *567 **5,900 1,620 NR NR NR NR NR NR
10/08/19 504 5,950 2,180 13,400 614 804 NR NR NR NR NR **148 *373 **4,080 1,060 NR NR NR NR NR NR
01/02/20 373 7,870 2,460 16,100 629 1,110 511 J 118 J NR *NR **144 *815 **7,060 2,070 NR NR NR NR NR NR
10/13/20 17.0 524 49.3 2,610 326 207 472 48.6 NR * NR * * 66.9 *67.5 **2,400 1,120 NR NR NR NR NR NR
04/08/21 <1.3 1.5 J <1.3 20.3 308 18.1 191 47.2 <1.3 * <1.3 * * 54.9 *3.6 J **209 167 NR NR NR NR NR NR
10/20/21 < 0.63 6.2 2.7 46.1 141 8.8 182 13.1 <0.63 <10 <0.63 * * 27.8 *2.5 **63.0 46.4 NR NR NR NR NR NR
04/05/22 <0.63 23.2 29.7 296 214 30.7 63.5 21.7 <0.63 <10 <0.63 * 5.4 62.4 *4.3 <0.63 <0.63 152 69.9 NR NR NR NR NR NR
04/04/23 <0.180 15.7 35.5 259 8.08 32.2 <1.90 <0.280 <0.160 <0.160 <0.190 <0.380 12.9 2.46 1.03 17.7 <0.220 <0.220 154 65.3 NR NR NR NR NR NR
09/20/23 <0.180 31.6 89.0 610 5.92 45.8 <1.90 <0.280 <0.160 2.84 J <0.190 <0.380 30.8 1.43 <0.078 37.7 <0.220 <0.220 337 118 NR NR NR NR NR NR
09/06/11 12.6 12.8 0.85 13.7 7.8 <0.10 NR NR NR NR NR **1.2 *<0.11 **0.33 J 1.5 <0.56 9.9 861 47.5 J <100 92.2 J
05/20/13 77.9 28.3 4.0 101 4.5 0.56 NR NR NR NR NR **4 *0.20 J **3.8 9.1 <0.66 NR 595 <131 <96 959.6
07/29/15 92.3 5.9 4.7 95.6 5.8 <0.24 NR NR NR NR NR **12 *<0.31 **5.3 13.8 NR NR NR NR NR NR
04/06/16 72.5 1.4 3.1 25.8 5.3 0.30 J NR NR NR NR NR **13.3 *0.14 J **4.9 14.9 NR NR NR NR NR NR
08/09/16 46.2 2.5 2.2 18.8 6.3 0.62 NR NR NR NR NR **15.1 *<0.13 **3 10.2 NR NR NR NR NR NR
05/03/17 30.5 0.55 1.1 7.4 5.6 0.24 J NR NR NR NR NR **12.4 *<0.13 **1.6 6.4 NR NR NR NR NR NR
04/19/18 0.16 J 0.89 <0.13 0.64 J <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 11.8 0.25 J 0.32 J 1.8 5.4 0.15 J NR NR NR NR NR **12.9 *<0.13 **0.24 J 2.9 NR NR NR NR NR NR
10/15/18 13.9 0.29 J 0.30 J 2.5 5.4 0.19 J NR NR NR NR NR **12.3 *<0.13 **0.33 J 1.5 NR NR NR NR NR NR
01/22/19 22.6 0.92 0.38 J 12.3 4.7 0.17 J NR NR NR NR NR **12.6 *<0.22 **1 1.7 NR NR NR NR NR NR
04/08/19 41.2 1.6 0.68 7.1 4.4 <0.13 NR NR NR NR NR **11.4 *<0.13 **0.44 J 1.7 NR NR NR NR NR NR
07/29/19 1.5 0.46 J <0.13 3.9 4.4 0.15 J NR NR NR NR NR **11.1 *<0.13 **0.14 J 0.54 NR NR NR NR NR NR
10/08/19 5.1 0.36 J <0.13 2.5 5.1 0.17 J NR NR NR NR NR **12.7 *<0.13 **<0.13 0.34 J NR NR NR NR NR NR
01/02/20 0.42 J <0.13 <0.13 1.6 4.4 0.19 J 1,530 0.29 J NR * NR * * 8.8 *<0.13 **<0.13 0.37 J NR NR NR NR NR NR
10/13/20 0.75 0.50 <0.13 2.0 3.6 <0.13 985 0.26 J NR * NR * * 9.1 *<0.13 **<0.13 0.35 J NR NR NR NR NR NR
04/08/21 0.23 J 0.17 J <0.13 1.5 3.0 <0.13 702 <0.20 <0.13 * <0.13 * * 7.4 *<0.13 **<0.13 0.44 J NR NR NR NR NR NR
10/20/21 0.84 0.23 J <0.13 2.2 5.7 0.53 2,890 E 0.59 J <0.13 361 <0.13 * * 12.5 *<0.13 **0.40 J 0.97 NR NR NR NR NR NR
04/05/22 0.32 J 0.23 J <0.13 0.44 J 4.9 0.22 J 1,660 0.39 J <0.13 223 <0.13 * <0.13 12.1 *<0.13 <0.13 <0.13 0.21 J 2.3 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 1.29 2.37 <0.470 555 <0.280 <0.160 203 <0.190 <0.380 <0.180 7.31 <0.078 <0.190 <0.220 <0.220 <0.190 0.406 J NR NR NR NR NR NR
09/20/23 0.212 J <0.220 <0.170 2.06 J 3.18 12.7 186 0.348 J <0.160 178 <0.190 <0.380 <0.180 6.98 <0.078 <0.190 <0.220 <0.220 1.19 0.780 NR NR NR NR NR NR
MW-3
MW-4
Page 2 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR **<0.11 *<0.11 **<0.10 <0.10 <0.57 <5.0 <35 <135 <100 <135
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.66 NR <35 102 J <96 1,010
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR **<0.16 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 NR * NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 <0.13 *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 2.70 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 0.237 J <0.180 NR NR NR NR NR NR
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR **<0.11 *<0.11 **<0.10 <0.10 <0.55 7.7 <35 <135 <100 <135
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.66 NR <35 <132 <97 562
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR **<0.16 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 0.34 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 NS NS NS NS NS NS NR NR NR NR NR **NS *NS **NS NS NS NS NS NS NS NS
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 0.30 J <0.13 0.38 J <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 <0.13 *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
MW-5
MW-6
Page 3 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
09/06/11 <0.13 <0.13 <0.15 <0.30 20.7 <0.10 NR NR NR NR NR **76.0 *<0.11 **<0.10 <0.10 <0.54 <5.0 83.0 J <135 <100 <135
05/20/13 <0.10 <0.10 <0.10 <0.22 29.0 <0.15 NR NR NR NR NR **39.3 *<0.10 **<0.10 <0.10 <0.66 NR <35 <131 <96 179 J
07/29/15 <0.17 <0.17 <0.15 <0.43 17.1 <0.12 NR NR NR NR NR **20.3 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 16.1 <0.13 NR NR NR NR NR **10.4 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 11.6 <0.13 NR NR NR NR NR **13.5 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 14.3 <0.13 NR NR NR NR NR **14.7 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 12.3 <0.13 NR NR NR NR NR **2.1 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 11.3 <0.13 NR NR NR NR NR **0.48 J *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 2.5 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 11.6 <0.13 NR NR NR NR NR **1.1 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 10.1 <0.13 NR NR NR NR NR **0.26 J *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 8.7 <0.13 NR NR NR NR NR **0.44 J *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 5.9 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 4.9 <0.13 <2.0 <0.20 NR * NR * * 0.14 J *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 2.9 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 4.2 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 0.63 *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 3.10 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 0.398 J <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/06/11 144 588 184 739 1.6 J 16.0 NR NR NR NR NR **<1.1 *55.0 **243 68.2 16.3 <5.0 4,480 3,978 <95 9,888
05/20/13 156 2,280 759 4,600 <0.10 301 NR NR NR NR NR **0.77 *130 **894 193 48.3 NR 2,490 1,430 <110 5,299
07/29/15 152 662 162 741 <1.6 39.2 NR NR NR NR NR **<1.6 *49.3 **238 52.5 NR NR NR NR NR NR
04/06/16 137 1,180 468 2,750 <1.3 246 NR NR NR NR NR **<1.3 *108 **838 127 NR NR NR NR NR NR
08/09/16 8.1 26.0 7.2 29.9 <0.13 1.6 NR NR NR NR NR **<0.13 *2.5 **9.0 1.5 NR NR NR NR NR NR
05/03/17 182 499 130 477 <1.3 28.4 NR NR NR NR NR **<1.3 *47.3 **139 33.8 NR NR NR NR NR NR
04/19/18 206 531 164 604 <1.3 13.8 NR NR NR NR NR **<1.3 *51.5 **162 42.7 NR NR NR NR NR NR
08/13/18 122 301 98.6 365 <1.3 25.4 NR NR NR NR NR **<1.3 *37.5 **114 33.0 NR NR NR NR NR NR
10/15/18 167 363 92.6 224 <1.3 6.6 NR NR NR NR NR **<1.3 *38.4 **63.1 25.2 NR NR NR NR NR NR
01/22/19 147 522 232 1,120 <0.68 82.5 NR NR NR NR NR **<0.73 *61.7 **349 58.5 NR NR NR NR NR NR
04/08/19 128 416 180 802 <1.3 56.0 NR NR NR NR NR **<1.3 *50.8 **251 39.5 NR NR NR NR NR NR
07/29/19 8.4 11.5 4.7 12.1 <0.13 1.1 NR NR NR NR NR **<0.13 *2.0 **2.6 2.3 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 0.13 J 0.16 J <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 2.1 J <0.20 <0.13 2.1 J <0.13 * * 0.15 J *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 0.34 J <0.13 0.59 J <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 0.26 J *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
MW-7
MW-8
Page 4 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
01/16/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.67 7.6 <35 <131 <96 <131
05/20/13 1.4 0.11 J 0.11 J 1.4 J 0.46 J 0.27 J NR NR NR NR NR **0.38 J *<0.10 **0.17 J <0.10 <0.66 NR <35 <131 <96 228
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR **<0.16 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 0.16 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * *<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 0.31 J <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 <0.13 *<0.13 <0.13 0.84 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 4.51 <0.180 <0.500 <0.078 <0.190 <0.220 0.411 J <0.190 <0.180 NR NR NR NR NR NR
01/16/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.67 <5.0 <35 <133 <98 <133
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.66 NR <35 <131 <96 166 J
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR **<0.16 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 0.25 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 0.18 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 0.35 J <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 * <0.13 <0.13 *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
MW-9
MW-10
Page 5 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
09/06/11 467 4.5 J 43.7 525 708 79.2 NR NR NR NR NR **487 *13.3 **56.5 23.0 15.0 <5.0 2,280 1,614 <110 1,219
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.66 NR <35 <131 <96 156 J
07/29/15 3,220 166 603 3,600 759 460 NR NR NR NR NR **612 *84.3 **707 120 NR NR NR NR NR NR
04/06/16 167 8.8 13.9 79.0 45.9 13.9 NR NR NR NR NR **32.7 *1.5 J **12.6 1.3 J NR NR NR NR NR NR
08/09/16 3,420 37.6 J 533 2,450 826 276 NR NR NR NR NR **641 *48.3 J **418 52.8 NR NR NR NR NR NR
05/03/17 3,370 40.3 J 464 2,460 800 240 NR NR NR NR NR **652 *42.7 J **449 60.8 NR NR NR NR NR NR
04/19/18 0.40 J <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 1,850 8.7 J 193 227 321 57.1 NR NR NR NR NR **240 *17.2 J **78.6 18.3 J NR NR NR NR NR NR
01/22/19 1,320 9.8 J 167 457 402 98.5 NR NR NR NR NR **330 *16.3 **149 11.8 NR NR NR NR NR NR
04/08/19 408 5.2 66.9 195 113 44.5 NR NR NR NR NR **86.3 *8.6 **72.4 6.8 NR NR NR NR NR NR
07/29/19 3,190 51.4 314 1,140 679 111 NR NR NR NR NR **503 *21.9 J **200 21.2 J NR NR NR NR NR NR
10/09/19 4,080 107 611 2,150 789 223 NR NR NR NR NR **632 *36.3 J **361 41.5 J NR NR NR NR NR NR
01/02/20 4,250 122 643 2,820 924 233 5,190 178 NR *NR * *710 *42.3 J **446 42.7 J NR NR NR NR NR NR
04/08/21 7.6 0.49 J 0.72 2.7 220 0.23 J 67.1 31.3 <0.13 * <0.13 * *80.6 *<0.13 **2.4 1.0 NR NR NR NR NR NR
10/20/21 NS NS NS NS NS NS NS NS NS NS NS * * NS * NS * * NS NS NS NS NS NS NS NS
04/05/22 1.3 4.3 0.46 J 2.2 8.6 0.18 J <2.0 0.50 J <0.13 <2.0 <0.13 * <0.13 4.9 *<0.13 <0.13 <0.13 0.19 J <0.13 NR NR NR NR NR NR
04/04/23 0.451 J <0.220 <0.170 <0.210 4.50 <0.470 22.2 0.285 J <0.160 <1.60 <0.190 <0.380 <0.180 1.71 0.618 J <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 0.270 J <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
01/16/13 5,310 14,800 1,350 7,070 2,010 350 NR NR NR NR NR **882 *100 J **777 133 J 52.9 <5.0 43,300 4,110 <96 3,976
02/12/13 5,960 15,700 1,600 8,610 2,230 466 NR NR NR NR NR **921 *136 **1,210 218 NR NR NR NR NR NR
05/20/13 11,000 29,900 2,620 13,500 3,590 556 NR NR NR NR NR **1,820 *219 **1,610 378 130 NR 16,000 J 2,420 <190 433
07/29/15 11,800 28,900 2,520 12,900 7,970 705 NR NR NR NR NR **2,570 *198 J **1,570 343 J NR NR NR NR NR NR
04/06/16 14,300 34,100 3,010 15,700 11,000 816 NR NR NR NR NR **3,380 *241 J **2,020 468 NR NR NR NR NR NR
08/09/16 14,300 33,900 3,060 13,800 13,100 884 NR NR NR NR NR **4,160 *228 **2,130 453 NR NR NR NR NR NR
05/03/17 12,500 31,800 2,390 14,000 10,200 837 NR NR NR NR NR **3,090 *166 J **1,650 384 NR NR NR NR NR NR
04/19/18 13,800 33,600 3,260 17,600 11,700 599 NR NR NR NR NR **3,080 *236 **2,200 535 NR NR NR NR NR NR
08/13/18 16,300 38,400 2,770 15,100 15,800 779 NR NR NR NR NR **4,250 *189 J **1,830 475 J NR NR NR NR NR NR
10/15/18 17,400 44,100 2,970 15,800 15,500 583 NR NR NR NR NR **3,850 *186 J **1,670 412 J NR NR NR NR NR NR
01/22/19 18,500 42,400 3,210 18,600 22,800 801 NR NR NR NR NR **6,480 *212 J **2,220 489 NR NR NR NR NR NR
03/11/19 18,200 41,600 3,060 15,600 19,400 694 NR NR NR NR NR **5,400 *NR **NR NR NR NR NR NR NR NR
04/08/19 14,300 36,600 2,380 11,900 16,600 353 J NR NR NR NR NR **3,930 *132 J **947 277 J NR NR NR NR NR NR
07/29/19 16,900 43,400 2,600 12,500 18,800 325 J NR NR NR NR NR **4,490 *140 J **1,060 318 J NR NR NR NR NR NR
10/09/19 17,300 41,300 2,900 13,700 19,700 568 NR NR NR NR NR **4,900 *155 J **1,300 362 J NR NR NR NR NR NR
01/02/20 17,600 43,500 3,000 15,900 22,700 541 44,500 1,150 NR *NR * *5,390 *163 J **1,320 381 J NR NR NR NR NR NR
10/13/20 18,400 47,300 2,850 16,200 26,000 626 37,100 1,430 NR *NR * *5,940 *193 J **1,660 491 J NR NR NR NR NR NR
04/08/21 12,500 29,200 1,940 10,900 15,600 476 J 29,500 895 J <130 *<130 * *3,950 *<130 **1,260 328 J NR NR NR NR NR NR
10/20/21 14,700 30,900 2,080 11,500 22,500 481 J 53,300 1,250 <130 <2,000 <130 * *5,220 *162 J **1,300 342 J NR NR NR NR NR NR
04/05/22 9,670 19,200 1,750 9,780 13,800 496 15,900 871 <63 <1,000 <63 * 64.4 J 3,680 *287 <63 <63 1,170 1,160 NR NR NR NR NR NR
04/04/23 24.8 30.7 2.67 15.2 32.9 0.872 J 48.5 2.10 J <0.160 <1.60 <0.190 <0.380 <0.180 7.81 0.945 J <0.190 <0.220 <0.220 1.40 0.296 J NR NR NR NR NR NR
09/20/23 10,800 25,000 1,860 10,900 19,900 466 13,000 1,310 <16.0 <160 <19.0 <38.0 40.0 J 3,360 <7.80 120 <22.0 <22.0 1,300 317 NR NR NR NR NR NR
DW-1
DW-2
Page 6 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
03/26/13 0.83 <0.10 <0.10 0.83 J 0.17 J 0.26 J NR NR NR NR NR **<0.10 *<0.10 **0.26 J <0.10 <0.69 NR 265 <134 <99 <185
05/20/13 0.66 <0.10 <0.10 0.49 J 0.13 J 0.16 J NR NR NR NR NR **<0.10 *<0.10 **<0.10 <0.10 <0.66 NR 213 <131 <96 220
07/28/15 4.4 <0.17 0.18 J 4.7 2.1 0.36 J NR NR NR NR NR **1.0 *<0.16 **0.76 <0.14 NR NR NR NR NR NR
04/06/16 10.8 6.2 1.0 18.7 7.7 4.5 NR NR NR NR NR **3.4 *0.25 J **5.2 0.57 NR NR NR NR NR NR
05/03/17 26.3 0.35 J 0.32 J 27.5 17.1 0.91 NR NR NR NR NR **7.5 *0.21 J **3.7 0.22 J NR NR NR NR NR NR
04/19/18 40.7 16.4 2.1 53.1 28.3 1.6 NR NR NR NR NR **14.4 J *0.43 J **8.4 0.69 NR NR NR NR NR NR
08/13/18 42.6 0.67 0.75 45.6 28.7 1.4 NR NR NR NR NR **11.4 *0.46 J **7.8 0.48 J NR NR NR NR NR NR
10/15/18 46.5 0.41 J 0.80 51.3 30.3 1.4 NR NR NR NR NR **12.5 *0.45 J **7.4 0.43 J NR NR NR NR NR NR
01/22/19 50.2 0.37 J 0.51 58.5 29.5 1.2 NR NR NR NR NR **14.7 *0.42 J **9.5 0.41 J NR NR NR NR NR NR
04/08/19 43.7 0.24 J 0.49 J 50.5 24.2 1.0 NR NR NR NR NR **10.9 *0.36 J **6.6 0.33 J NR NR NR NR NR NR
07/29/19 43.5 0.25 J 0.38 J 44.5 19.9 0.92 NR NR NR NR NR **9.9 *0.31 J **5.0 0.20 J NR NR NR NR NR NR
10/09/19 44.5 0.19 J 0.30 J 33.2 16.4 1.1 NR NR NR NR NR **9.4 *0.29 J **4.8 <0.13 NR NR NR NR NR NR
01/02/20 31.7 0.52 0.16 J 25.3 17.0 1.0 113 0.66 J NR * NR * * 8.9 *0.21 J **3.7 0.20 J NR NR NR NR NR NR
10/13/20 43.7 <0.13 0.28 J 17.8 25.3 1.1 146 1.1 NR * NR * * 12.7 *0.28 J **4.2 0.18 J NR NR NR NR NR NR
04/08/21 58.8 3.9 1.5 24.4 26.6 1.5 192 1.1 J <0.25 * <0.25 * * 14.3 *0.62 J **6.3 0.32 J NR NR NR NR NR NR
10/20/21 120 4.2 1.1 J 45.8 50.9 1.6 J 388 2.3 J <0.63 <10 <0.63 * * 27.0 *1.1 J **12.9 1.0 J NR NR NR NR NR NR
04/05/22 212 2.1 J 1.1 J 86.3 90.1 3.4 573 4.3 J <0.63 <10 <0.63 * 5.2 45.6 *1.4 J <0.63 <0.63 31.0 4.0 NR NR NR NR NR NR
04/04/23 241 <2.20 <1.70 95.1 105 6.10 J 546 5.62 J <1.60 <16.0 <1.90 <3.80 6.91 51.8 <0.780 <1.90 <2.20 <2.20 35.70 3.44 J NR NR NR NR NR NR
09/20/23 129 3.12 J <1.70 107 103 14.1 217 5.86 J <1.60 29.6 J <1.90 <3.80 4.55 J 33.2 M <0.780 <1.90 <2.20 <2.20 39.6 4.21 J NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR * * <0.13 *<0.13 * * <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 * * <0.13 <0.13 NR NR NR NR NR NR
04/14/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 * * <0.13 <0.13 NR NR NR NR NR NR
07/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 * * <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR * * <0.13 *<0.13 * * <0.13 <0.13 NR NR NR NR NR NR
01/15/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 * <0.13 * * <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 * * <0.13 *<0.13 * * <0.13 <0.13 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/19 NS NS NS NS NS NS NS NS NR NS NR **NS *NS **NS NS NS NS NS NS NS NS
01/02/20 NS NS NS NS NS NS NS NS NR NS NR **NS *NS **NS NS NS NS NS NS NS NS
01/15/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 4.9 *0.43 J **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/14/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR **<0.11 *<0.11 **<0.10 <0.10 NR NR NR NR NR NR
04/06/16 NS NS NS NS NS NS NS NS NR NS NR **NS *NS **NS NS NS NS NS NS NS NS
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR **<0.11 *<0.11 **<0.10 <0.10 NR NR NR NR NR NR
04/06/16 NS NS NS NS NS NS NS NS NR NS NR **NS *NS **NS NS NS NS NS NS NS NS
WSW-6
WSW-7
WSW-3
WSW-5
WSW-4
DW-3
Page 7 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR **<0.11 *<0.11 **<0.10 <0.10 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
01/02/20 0.14 J <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/28/15 7,090 24,700 2,830 16,200 436 1,390 NR NR NR NR NR **740 *262 **2,700 652 NR NR NR NR NR NR
04/06/16 6,390 24,600 2,710 19,300 256 1,170 NR NR NR NR NR **563 *236 J **3,040 735 NR NR NR NR NR NR
08/09/16 7,740 25,900 3,080 16,000 453 1,220 NR NR NR NR NR **978 *288 **2,760 664 NR NR NR NR NR NR
05/03/17 7,060 21,800 2,610 18,100 486 913 NR NR NR NR NR **973 *232 **2,820 688 NR NR NR NR NR NR
04/19/18 6,400 22,500 2,700 15,100 583 750 NR NR NR NR NR **731 *248 **2,600 659 NR NR NR NR NR NR
08/13/18 5,410 25,600 3,020 19,300 231 J 875 NR NR NR NR NR **510 *284 J **2,930 814 NR NR NR NR NR NR
10/15/18 4,570 24,800 2,710 18,100 184 J 913 NR NR NR NR NR **362 *214 J **2,680 650 NR NR NR NR NR NR
01/22/19 1,970 16,300 2,280 16,900 33.6 J 1,040 NR NR NR NR NR **121 *180 **2,860 685 NR NR NR NR NR NR
04/08/19 1,610 20,400 2,800 20,700 <63 776 NR NR NR NR NR **<63 *205 J **2,890 757 NR NR NR NR NR NR
07/29/19 3,040 24,600 3,220 18,900 110 J 761 NR NR NR NR NR **204 J *238 J **2,720 685 NR NR NR NR NR NR
10/08/19 3,120 22,800 3,240 17,600 227 J 859 NR NR NR NR NR **287 *224 J **2,480 619 NR NR NR NR NR NR
01/02/20 2,340 23,300 3,330 23,400 153 J 862 1,030 J <100 NR * NR * *153 J *266 **3,080 796 NR NR NR NR NR NR
10/13/20 1,130 3,800 315 2,140 306 221 3,860 54.5 J NR * NR * *269 *23.1 J **366 76.7 NR NR NR NR NR NR
04/08/21 416 1,820 203 1,510 124 342 1,090 23.8 J <6.3 * <6.3 * *123 *13.3 J **255 50.0 NR NR NR NR NR NR
10/20/21 NS NS NS NS NS NS NS NS NS NS NS * * NS * NS * * NS NS NS NS NS NS NS NS
04/05/22 NS NS NS NS NS NS NS NS NS NS NS * * NS * NS * * NS NS NS NS NS NS NS NS
04/04/23 28.9 27.0 21.0 796 48.1 59.2 287 6.32 J <1.60 <16.0 <1.90 14.7 2.36 J 26.0 12.5 <1.90 <2.20 <2.20 139 76.6 NR NR NR NR NR NR
09/20/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/28/15 10,800 32,600 2,690 14,100 12,100 682 NR NR NR NR NR **3,360 *266 J **2,180 558 NR NR NR NR NR NR
04/06/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/09/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/03/17 12,100 38,500 3,570 21,200 9,720 1,300 NR NR NR NR NR **3,230 *370 **3,520 845 NR NR NR NR NR NR
04/19/18 12,100 43,400 4,900 28,200 11,800 1,590 NR NR NR NR NR **2,920 *656 **5,490 1,480 NR NR NR NR NR NR
08/13/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/15/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/22/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/11/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/29/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/08/19 7,380 40,000 4,060 21,400 5,110 1,020 NR NR NR NR NR **1,710 *282 J **2,810 731 NR NR NR NR NR NR
01/02/20 FP FP FP FP FP FP FP FP NR FP NR **FP *FP **FP FP FP FP FP FP FP FP
10/13/20 6,520 44,500 4,140 24,700 2,460 1,520 9,780 J 533 J NR *NR * *1,430 *352 J **3,530 883 NR NR NR NR NR NR
04/08/21 4,090 27,200 2,800 21,300 3,610 1,740 8,540 J 519 J <130 *<130 * *1,370 *384 J **4,610 1,200 NR NR NR NR NR NR
10/20/21 722 6,220 1,180 9,310 1,490 1,390 228 J <31 <31 1,250 <31 * *334 *271 * *3410 809 NR NR NR NR NR NR
04/05/22 6,930 30,300 2,490 19,300 1,030 1,860 <2,000 269 J <130 <2,000 <130 * <130 684 *224 J 172 J <130 3,540 961 NR NR NR NR NR NR
04/04/23 2,270 17,300 E 2,670 17,500 1,270 1,470 5,210 260 J <16.0 588 J <19.0 633 82 437 142 217 140 151 3,070 800 NR NR NR NR NR NR
09/20/23 1,620 22,700 3,320 22,100 526 1,820 1080 109 J <16.0 309 J <19.0 <38.0 115 146 <7.80 358 135 <22.0 4,540 1,080 NR NR NR NR NR NR
WSW-8
OW-2
OW-1
Page 8 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
07/28/15 2,640 15,200 1,410 6,830 <82 416 NR NR NR NR NR **<80 *122 J **1,080 299 NR NR NR NR NR NR
04/06/16 3,580 27,500 2,660 14,500 <63 795 NR NR NR NR NR **67.7 J *191 J **1,800 423 NR NR NR NR NR NR
08/09/16 3,510 19,700 2,080 11,000 37.9 J 541 NR NR NR NR NR **94.0 J *192 **1,800 430 NR NR NR NR NR NR
05/03/17 2,870 17,500 1,740 9,170 38.1 J 560 NR NR NR NR NR **104 *186 **1,660 435 NR NR NR NR NR NR
AS-2 05/03/17 7,390 22,100 2,390 14,800 1,560 706 NR NR NR NR NR * *810 *172 **2,020 475 NR NR NR NR NR NR
AS-3 05/03/17 1,930 21,500 3,340 21,000 20,800 1,020 NR NR NR NR NR * *3,230 *322 **3,180 750 NR NR NR NR NR NR
AS-4 05/03/17 2,410 7,980 1,370 6,770 130 266 NR NR NR NR NR **209 *256 **1,770 505 NR NR NR NR NR NR
AS-5 05/03/17 36.7 185 220 2,470 <3.1 334 NR NR NR NR NR **<3.1 *91.5 **1,650 140 NR NR NR NR NR NR
07/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR **<0.16 *<0.16 **<0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/09/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 0.13 J <0.13 0.49 J <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **0.14 J <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR **<0.073 *<0.22 **<0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR **<0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/08/19 NS NS NS NS NS NS NS NS NR NS NR **NS *NS **NS NS NS NS NS NS NS NS
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/14/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
07/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR <0.13 * * <0.13 *<0.13 **<0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR <0.13 * <0.13 <0.13 *<0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/04/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
09/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.380 <0.180 <0.500 <0.078 <0.190 <0.220 <0.220 <0.190 <0.180 NR NR NR NR NR NR
Notes:
• < : Less than the method detection limit specified in the laboratory report.
• MAC: Maximum allowable concentrations, specified in T15A NCAC 2L.0202.
• Results reported in µg/l.
AS-1
• Concentrations in bold exceeded MACs; concentrations in bold and italics exceeded the GCLs.
• GCL: Gross contamination level.
• Other contaminant concentrations that exceeded the MACs are as follows: 05/20/13 - isopropylbenzene, styrene and/or tetrachloroethylene in MW-1R, MW-3, MW-8 and MW-10; 07/29/15 - isopropylbenzene, methylene chloride, styrene and/or tetrachloroethylene in MW-1R, MW-9 and
OW-1; 04/06/16 - isopropylbenzene, styrene, tetrachloroethylene, dibromochloromethane and/or 1,1,2,2-tetrachloroethane in MW-1R, MW-8, MW-9, OW-1, DW-2,WSW-4 and WSW-5; 08/09/16 - isopropylbenzene, methylene chloride and/or styrene in MW-1R, AS-1 and OW-1; 05/03/17 -
PCE, isopropylbenzene, styrene and/or hexachlorobutadiene in MW-1R, AS-3 and/or OW-2; 04/19/18 - PCE, isopropylbenzene, styrene and/or n-butylbenzene in MW-1R and/or OW-2; 08/13/18 - PCE in MW-9; 10/15/18 - methylene chloride and/or PCE in MW-8, MW-9, DW-1, DW-2 and/or
OW-1; 01/22/19 - methylene chloride in MW-1R, DW-1, DW-2 and OW-1, styrene in OW-1; 07/29/19 - o-chlorotoluene, isopropylbenzene and/or methylene chloride in MW-3, DW-1 and/or OW-1; 10/08/19 - isopropylbenzene in (MW-3); bromodichloromethane, dibromochloromethane and
methyl chloride in WSW-3; 01/02/20 - n-buytlbenzene, isopropylbenzene and p-isopropyltoluene in MW-3; tert-butyl alcohol in MW-4; 10/13/20 - methylene chloride and styrene in OW-2.
• FP: Free Product.
• NS: Not Sampled.
• NR: Not Requested.
• *: For laboratory results from prior events, please refer to previous laboratory reports.
TRIP BLANK
Page 9 of 10
Facility ID # : 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 40 70 70 100 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 40,000 30,500 70,000 100000 26,100 70000 700 28,500 24,100 12,000 15,000 NE NE NE NETetrachloroethene(PCE)IsopropylbenzeneMethyl isobutyl ketone (MIBK)Styrene2-Hexanonetert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 2-MethylnaphthaleneDi-isopropyl etherBromodichloromethanetert-Butyl Alcohol(TBA)Analytical Method →
Date: 10/02/23
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneGCL (mg/l)
• For other compounds reported that did not exceed the MACs, refer to the laboratory reports.
Page 10 of 10

APPENDICES

APPENDIX A
State Correspondence

June 6, 2023 Shell Brothers Distributing, Inc.
451 Eugene Street, Apt 2T Greensboro, North Carolina 27401 Attention: Gail Williams
Re: Acknowledgement of Receipt/ Notice of Regulatory Requirements 15A NCAC 2L .0407 Groundwater Monitoring Report Handy Stop #7 1500 Rock Barn Road, Conover Catawba County Incident Number: 36069 Risk Classification: High
Dear Ms. Williams: On May 18, 2023, the Underground Storage Tank Section of the Division of Waste Management, Mooresville Regional Office, received the Groundwater Monitoring Report for the above-referenced site. The reports have been reviewed and will remain in the UST Section’s files. Upon review, the Division has determined that the Corrective Action Feasibility Study, may be delayed until after the next groundwater sampling event. The next groundwater sampling event should be scheduled for October 2023. The Groundwater Monitoring Report must be received by this office no later than November 30, 2023. If you have any questions, please contact me at the address or telephone number listed below. Sincerely,
Brad C. Newton, P.G. Hydrogeologist Mooresville Regional Office
UST Section, Division of Waste Management, NCDENR cc: Joanna Alley – Geological Resources, Inc. (via e-mail) Catawba County Health Department
Site Name City / County /Catawba Incident #36069
Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #63
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:65 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I210A RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO IM AuthProposed
Rate/Price
(Consultant)RO Supv. AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 15 /wells y $110.00 y $1,650.00 $1,650.00 /
4.090 #240 16 /samples y $94.00 y $1,504.00 $1,504.00 /
4.090 #440 3 /samples y $22.00 y $66.00 $66.00 /
4.090 #490 3 /samples y $20.00 y $60.00 $60.00 /
4.090 #510 3 /samples y $15.00 y $45.00 $45.00 /
4.090 #521 3 /samples y $70.00 y $210.00 $210.00 /
4.091 1 /shipment y $60.00 y $60.00 $60.00 /
6.090 1 /report y $1,125.00 y $1,125.00 $1,125.00 /
12.050 1 /trip y $250.00 y $250.00 $250.00 /
12.055 1 /trip y $50.00 y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$5,020.00 $5,020.00 TOTAL:
Total Standard Costs (Not Third Party)$5,020.00 $5,020.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:6/28/23 by:(PM)(Reserved for RO)
RO Review:6/29/23 by:(IM)Joint UST Preapproval Confirmed By:Date1 6/29/2023
RO Supv. Review:6/29/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to workproceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both theUST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
JRA
Proposed
Units / Type
(Consultant)
Brad Newton
YES23-372 October 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
[e-mail]
Shell Brothers Distributors, Inc.Gail Williams
Geological Resources, Inc.
DIRECTED - CAB ONLY
Conover
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010 (Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Handy Stop 7
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
bcn
RHT
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
6/30/23

APPENDIX B
Land Use Information
Date: 12/15/21 Facility ID # : 0-031674
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a O-I Office-Institutional n/a n/a
n/a M-1 General Manufacturing n/a n/a
n/a R-20 Residential Genera n/a n/a
n/a B-4 General Business n/a n/a
n/a B-2 Highway Business n/a n/a
Note:
• Properties are keyed to Figure 3.
APPENDIX B
LAND USE INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Page 1 of 1

APPENDIX C
Incident Reports
NCDEQ Incident Report
RP/Company SHELL BROTHERS DISTRIBUTING
RPAddress 241 1ST AVE DR SE
RPCity TAYLORSVILLE
Contact GAIL SHELL WILLIAMS
RPState NC
TELEPHONE [phone]
IncidentNumber 36069 USTNum MO-7402
IncidentName HANDY STOP NO. 7
FacilID 00-0-0000031674
Address 1500 ROCK BARN ROAD
CityTown CONOVER State NC
ZipCode
DateOccurred 3 /14/2006
DateReported 4 /25/2006
ConfRisk I
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.184286 Latitude 35.722272
County CATAW
SCH 7/21/2006 7/28/2006 10/26/2006
LSA2 11/16/2006 11/29/2006 11/30/2006
CSAM 7/25/2008 8/7/2008 8/7/2008
FPRI 11/19/2008 12/11/2008 12/11/2008
CAP 9/29/2009 10/15/2009 10/15/2009
Monday, October 2, 2023 Page 1 of 5
RMR 11/3/2011 11/22/2011 11/22/2011
FPRS 3/4/2015 4/1/2015 4/1/2015
MRP 8/31/2015 9/29/2015 9/29/2015
MRP 5/27/2016 6/1/2016 6/1/2016
MRP 8/31/2016 9/12/2016 9/12/2016
RMR 7/5/2018 7/19/2018 7/19/2018
INCORRECT. UNABLE TO CORRECT DATABASE.
RMR 8/20/2018 9/5/2018 9/5/2018
RMR 10/26/2018 11/1/2018 11/1/2018
gw monitioring report approved. Capr forwarded to scott ryals.
RMR 12/31/2018 1/17/2019 1/17/2019
CAPR 3/27/2019 4/2/2019 4/2/2019
this report should not be approved per SCR it was not PE stamped. RUST
will not allow deletion of approval date.
Monday, October 2, 2023 Page 2 of 5
RMR 3/27/2019 4/2/2019 4/2/2019
MRP 9/3/2019 9/11/2019 9/11/2019
RMR 12/9/2019 12/17/2019 12/17/2019
MRP 3/2/2020 3/13/2020 3/16/2020
LET 5/5/2020 5/18/2020 5/18/2020
CAPR 5/27/2020 6/1/2020 6/1/2020
approved by scott ryals, stf branch
LET 8/17/2020 8/31/2020 8/31/2020
CAPR 9/11/2020 9/24/2020 9/24/2020
MRP 12/3/2020 12/29/2020 12/29/2020
CAPR 12/3/2020 12/10/2020 12/10/2020
Monday, October 2, 2023 Page 3 of 5
LET 1/27/2021 2/10/2021 2/10/2021
FPRS 2/18/2021 3/3/2021 3/3/2021
CAPR 2/18/2021 3/3/2021 3/3/2021
MRP 5/25/2021 6/7/2021 6/7/2021
CAPR 5/25/2021 6/7/2021 6/7/2021
LET 8/11/2021 8/12/2021 8/12/2021
CAPR 8/27/2021 9/10/2021 9/10/2021
MRP 12/17/2021 1/4/2021 1/4/2021
CAPR 12/17/2021 1/4/2021 1/4/2021
CAPR 2/21/2022 2/28/2022 2/28/2022
Monday, October 2, 2023 Page 4 of 5
RMR 5/12/2022 5/25/2022 5/25/2022
RMR 5/18/2023 6/6/2023 6/6/2023
Monday, October 2, 2023 Page 5 of 5
NCDEQ Incident Information
RP/Company NLS CARRIER CORP Contact
RPAddress 109 WHITE OAK LANE, SUITE 72
RPCity OLD BRIDGE
RPZipCode 08857-
RPState NJ
TELEPHONE [phone]
IncidentNumber 91567
IncidentName NLS CARRIERS DIESEL SPILL
Address I-40 EAST, EXIT 133
CityTown CONOVER State NC
County CATAWZipCode
Lattitude 35.721066 Longitude -81.185174
COMMENT
DateOccurred 1 /27/2020
DateReported 1 /28/2020
CloseOut
FacilID USTNum MO-88772
Mgr BCN
Conf Risk
Site Priority
Tuesday, May 16, 2023 Page 1 of 1
NCDEQ Incident Information
RP/Company STEVENS TRANSPORT Contact
RPAddress 9757 MILITARY PARKWAY
RPCity DALLAS
RPZipCode 75227-
RPState TX
TELEPHONE
IncidentNumber 95863
IncidentName STEVENS TRANSPORT DIESEL SPILL
Address ROCK BARN ROAD & I-40
CityTown CONOVER State
County CATAWZipCode
Lattitude 35.721767 Longitude -81.185766
COMMENT
NFA required at this site, but NFA letter not issued as the RP information was not submitted.
DateOccurred 8 /25/2020
DateReported 9 /25/2020
CloseOut
FacilID USTNum MO-88804
Mgr BCN
Conf Risk
Site Priority
Tuesday, May 16, 2023 Page 1 of 1

APPENDIX D
Historical Soil Quality Information

APPENDIX E
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/3/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-264-0032 Client Project Description: Handy Stop #7
GRI #3067
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/21/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 99
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-264-0032
Page 2 of 99
Report Number:
Sample Summary Table
Client Project Description:
23-264-0032
Handy Stop #7
GRI #3067
Lab No Client Sample ID Matrix Date Collected Date Received
09/20/2023 09:29Aqueous 95901 MW-1R 09/21/2023 13:40
09/20/2023 11:31Aqueous 95902 MW-2 09/21/2023 13:40
09/20/2023 10:33Aqueous 95903 MW-3 09/21/2023 13:40
09/20/2023 10:11Aqueous 95904 MW-4 09/21/2023 13:40
09/20/2023 09:59Aqueous 95905 MW-5 09/21/2023 13:40
09/20/2023 08:58Aqueous 95906 MW-6 09/21/2023 13:40
09/20/2023 10:22Aqueous 95907 MW-7 09/21/2023 13:40
09/20/2023 09:17Aqueous 95908 MW-8 09/21/2023 13:40
09/20/2023 10:47Aqueous 95909 MW-9 09/21/2023 13:40
09/20/2023 10:58Aqueous 95910 MW-10 09/21/2023 13:40
09/20/2023 11:59Aqueous 95911 DW-1 09/21/2023 13:40
09/20/2023 09:45Aqueous 95912 DW-2 09/21/2023 13:40
09/20/2023 12:14Aqueous 95913 DW-3 09/21/2023 13:40
09/20/2023 11:21Aqueous 95914 OW-2 09/21/2023 13:40
09/20/2023 08:15Aqueous 95915 TB 09/21/2023 13:40
Page 3 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-264-0032
Report Limit
Project:Handy Stop #7
V 95901MW-1R
10.2 09/28/2023 18:346200BBenzeneµg/L 1.80
J4.81 09/28/2023 18:346200Bn-Butylbenzene µg/L 1.80
M17.1 09/28/2023 18:346200BDi-Isopropyl Ether (DIPE)µg/L 5.00
47.8 09/28/2023 18:346200BEthylbenzeneµg/L 1.70
J3.45 09/28/2023 18:346200BIsopropylbenzeneµg/L 1.80
166 09/28/2023 18:346200BMethyl tert-butyl ether (MTBE)µg/L 1.40
96.5 09/28/2023 18:346200BNaphthaleneµg/L 4.70
6.00 09/28/2023 18:346200Bn-Propylbenzene µg/L 1.90
J78.4 09/28/2023 18:346200Btert-Butyl Alcohol (TBA)µg/L 16.0
203 09/28/2023 18:346200Btert-Amyl Alcohol (TAA)µg/L 19.0
J20.5 09/28/2023 18:346200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
134 09/28/2023 18:346200BTolueneµg/L 2.20
198 09/28/2023 18:346200B1,2,4-Trimethylbenzene µg/L 1.90
75.9 09/28/2023 18:346200B1,3,5-Trimethylbenzene µg/L 1.80
298 09/28/2023 18:346200Bo-Xylene µg/L 2.10
103 09/28/2023 18:346200Bm,p-Xylene µg/L 4.20
401 09/28/2023 18:346200BXylene (Total)µg/L 2.10
V 95902MW-2
2.27 09/27/2023 15:336200BNaphthaleneµg/L 0.470
V 95903MW-3
5.04 09/27/2023 15:586200Bn-Butylbenzene µg/L 0.180
3.33 09/27/2023 15:586200Bsec-Butyl benzene µg/L 0.200
1.43 09/27/2023 15:586200BDi-Isopropyl Ether (DIPE)µg/L 0.500
89.0 09/27/2023 15:586200BEthylbenzeneµg/L 0.170
30.8 09/27/2023 15:586200BIsopropylbenzeneµg/L 0.180
2.55 09/27/2023 15:586200B4-Isopropyl toluene µg/L 0.089
5.92 09/27/2023 15:586200BMethyl tert-butyl ether (MTBE)µg/L 0.140
45.8 09/27/2023 15:586200BNaphthaleneµg/L 0.470
37.7 09/27/2023 15:586200Bn-Propylbenzene µg/L 0.190
J2.84 09/27/2023 15:586200Btert-Butyl Alcohol (TBA)µg/L 1.60
31.6 09/27/2023 15:586200BTolueneµg/L 0.220
337 09/28/2023 18:586200B1,2,4-Trimethylbenzene µg/L 1.90
118 09/28/2023 18:586200B1,3,5-Trimethylbenzene µg/L 1.80
195 09/28/2023 18:586200Bo-Xylene µg/L 2.10
415 09/28/2023 18:586200Bm,p-Xylene µg/L 4.20
Page 4 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-264-0032
Report Limit
Project:Handy Stop #7
V 95903MW-3
610 09/28/2023 18:586200BXylene (Total)µg/L 2.10
V 95904MW-4
J0.212 09/27/2023 16:226200BBenzeneµg/L 0.180
6.98 09/27/2023 16:226200BDi-Isopropyl Ether (DIPE)µg/L 0.500
3.18 09/27/2023 16:226200BMethyl tert-butyl ether (MTBE)µg/L 0.140
12.7 09/27/2023 16:226200BNaphthaleneµg/L 0.470
178 09/27/2023 16:226200Btert-Butyl Alcohol (TBA)µg/L 1.60
186 09/28/2023 19:236200Btert-Amyl Alcohol (TAA)µg/L 19.0
J0.348 09/27/2023 16:226200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
1.19 09/27/2023 16:226200B1,2,4-Trimethylbenzene µg/L 0.190
0.780 09/27/2023 16:226200B1,3,5-Trimethylbenzene µg/L 0.180
1.39 09/27/2023 16:226200Bo-Xylene µg/L 0.210
J0.668 09/27/2023 16:226200Bm,p-Xylene µg/L 0.420
J2.06 09/27/2023 16:226200BXylene (Total)µg/L 0.210
V 95905MW-5
2.70 09/27/2023 16:476200BNaphthaleneµg/L 0.470
J0.237 09/27/2023 16:476200B1,2,4-Trimethylbenzene µg/L 0.190
V 95906MW-6
0.739 09/27/2023 17:126200BChloroformµg/L 0.220
V 95907MW-7
J5.50 09/27/2023 17:376200BAcetoneµg/L 1.80
J0.398 09/27/2023 17:376200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 95909MW-9
J0.228 09/27/2023 18:276200BChloroformµg/L 0.220
4.51 09/27/2023 18:276200B2-Hexanone µg/L 0.380
J0.411 09/27/2023 18:276200BTetrachloroetheneµg/L 0.220
V 95911DW-1
J0.270 09/27/2023 19:166200BTolueneµg/L 0.220
V 95912DW-2
10800 09/27/2023 21:206200BBenzeneµg/L 180
3360 09/27/2023 20:556200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1860 09/27/2023 20:556200BEthylbenzeneµg/L 17.0
Page 5 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-264-0032
Report Limit
Project:Handy Stop #7
V 95912DW-2
J40.0 09/27/2023 20:556200BIsopropylbenzeneµg/L 18.0
19900 09/27/2023 21:206200BMethyl tert-butyl ether (MTBE)µg/L 140
466 09/27/2023 20:556200BNaphthaleneµg/L 47.0
120 09/27/2023 20:556200Bn-Propylbenzene µg/L 19.0
13000 09/27/2023 21:206200Btert-Amyl Alcohol (TAA)µg/L 1900
1310 09/27/2023 20:556200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
25000 09/27/2023 21:206200BTolueneµg/L 220
1300 09/27/2023 20:556200B1,2,4-Trimethylbenzene µg/L 19.0
317 09/27/2023 20:556200B1,3,5-Trimethylbenzene µg/L 18.0
3360 09/27/2023 20:556200Bo-Xylene µg/L 21.0
7580 09/27/2023 20:556200Bm,p-Xylene µg/L 42.0
10900 09/27/2023 20:556200BXylene (Total)µg/L 21.0
V 95913DW-3
129 09/28/2023 19:486200BBenzeneµg/L 1.80
M33.2 09/28/2023 19:486200BDi-Isopropyl Ether (DIPE)µg/L 5.00
J4.55 09/28/2023 19:486200BIsopropylbenzeneµg/L 1.80
103 09/28/2023 19:486200BMethyl tert-butyl ether (MTBE)µg/L 1.40
14.1 09/28/2023 19:486200BNaphthaleneµg/L 4.70
J29.6 09/28/2023 19:486200Btert-Butyl Alcohol (TBA)µg/L 16.0
217 09/28/2023 19:486200Btert-Amyl Alcohol (TAA)µg/L 19.0
J5.86 09/28/2023 19:486200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
J3.12 09/28/2023 19:486200BTolueneµg/L 2.20
39.6 09/28/2023 19:486200B1,2,4-Trimethylbenzene µg/L 1.90
J4.21 09/28/2023 19:486200B1,3,5-Trimethylbenzene µg/L 1.80
20.9 09/28/2023 19:486200Bo-Xylene µg/L 2.10
85.6 09/28/2023 19:486200Bm,p-Xylene µg/L 4.20
107 09/28/2023 19:486200BXylene (Total)µg/L 2.10
V 95914OW-2
1620 09/27/2023 21:456200BBenzeneµg/L 18.0
51.3 09/27/2023 21:456200Bn-Butylbenzene µg/L 18.0
146 09/27/2023 21:456200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3320 09/27/2023 21:456200BEthylbenzeneµg/L 17.0
115 09/27/2023 21:456200BIsopropylbenzeneµg/L 18.0
526 09/27/2023 21:456200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1820 09/27/2023 21:456200BNaphthaleneµg/L 47.0
358 09/27/2023 21:456200Bn-Propylbenzene µg/L 19.0
Page 6 of 99
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-264-0032
Report Limit
Project:Handy Stop #7
V 95914OW-2
135 09/27/2023 21:456200BStyreneµg/L 22.0
J30909/27/2023 21:456200Btert-Butyl Alcohol (TBA)µg/L 160
1080 09/27/2023 21:456200Btert-Amyl Alcohol (TAA)µg/L 190
J10909/27/2023 21:456200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
22700 09/27/2023 22:106200BTolueneµg/L 220
4540 09/27/2023 21:456200B1,2,4-Trimethylbenzene µg/L 19.0
1080 09/27/2023 21:456200B1,3,5-Trimethylbenzene µg/L 18.0
7220 09/27/2023 21:456200Bo-Xylene µg/L 21.0
14900 09/27/2023 21:456200Bm,p-Xylene µg/L 42.0
22100 09/27/2023 21:456200BXylene (Total)µg/L 21.0
Page 7 of 99

Client: Geological Resources, Inc. CASE NARRATIVE Project: Handy Stop #7
Lab Report Number: 23-264-0032 Date: 10/3/2023
Volatile Organic Compounds - GC/MS Method 6200B Sample 95913 (DW-3)
QC Batch No: V38531/V38530 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Analyte: 1,2,3-Trichlorobenzene
QC Batch No: V38456/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,2,3-Trichlorobenzene
QC Batch No: V38531/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,2,4-Trichlorobenzene
QC Batch No: V38456/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,2,4-Trichlorobenzene
QC Batch No: V38531/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Carbon Tetrachloride QC Batch No: V38456/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Carbon Tetrachloride QC Batch No: V38531/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Chloromethane QC Batch No: V38456/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Page 8 of 99

Analyte: Chloromethane
QC Batch No: V38531/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Di isopropyl ether
QC Batch No: V38531/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Dichlorodifluoromethane
QC Batch No: V38456/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Dichlorodifluoromethane
QC Batch No: V38531/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Ethanol
QC Batch No: V38531/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Hexachlorobutadiene QC Batch No: V38456/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Hexachlorobutadiene QC Batch No: V38531/V38530 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Vinyl chloride QC Batch No: V38531/V38530 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Page 9 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1R
95901 Matrix:
9/20/2023 9:29
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 09/28/23 18:34 6200BMSA
Surrogate: 4-Bromofluorobenzene 89.2 Limits: 70-130%09/28/23 18:3410 MSA V38531
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%09/28/23 18:3410 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/28/23 18:3410 MSA V38531
Surrogate: Toluene-d8 88.8 Limits: 70-130%09/28/23 18:3410 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 10 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1R
95901 Matrix:
9/20/2023 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<18.0 µg/L 18.0 100Acetone 10 09/28/23 18:34 V38531MSA
10.2 µg/L 1.80 5.00Benzene 10 09/28/23 18:34 V38531MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 09/28/23 18:34 V38531MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 09/28/23 18:34 V38531MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 09/28/23 18:34 V38531MSA
<15.0 µg/L 15.0 50.0Bromoform 10 09/28/23 18:34 V38531MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 09/28/23 18:34 V38531MSA
4.81 J µg/L 1.80 5.00n-Butylbenzene 10 09/28/23 18:34 V38531MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 09/28/23 18:34 V38531MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 09/28/23 18:34 V38531MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 09/28/23 18:34 V38531MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 09/28/23 18:34 V38531MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 09/28/23 18:34 V38531MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 09/28/23 18:34 V38531MSA
<2.20 µg/L 2.20 5.00Chloroform 10 09/28/23 18:34 V38531MSA
<2.20 M µg/L 2.20 5.00Chloromethane 10 09/28/23 18:34 V38531MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 09/28/23 18:34 V38531MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 09/28/23 18:34 V38531MSA
17.1 M µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 09/28/23 18:34 V38531MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 09/28/23 18:34 V38531MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 09/28/23 18:34 V38531MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 09/28/23 18:34 V38531MSA
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 09/28/23 18:34 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 11 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1R
95901 Matrix:
9/20/2023 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 09/28/23 18:34 V38531MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 09/28/23 18:34 V38531MSA
<12.0 M µg/L 12.0 50.0Dichlorodifluoromethane 10 09/28/23 18:34 V38531MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 09/28/23 18:34 V38531MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 09/28/23 18:34 V38531MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 09/28/23 18:34 V38531MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 09/28/23 18:34 V38531MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 09/28/23 18:34 V38531MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 09/28/23 18:34 V38531MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 09/28/23 18:34 V38531MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 09/28/23 18:34 V38531MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 09/28/23 18:34 V38531MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 09/28/23 18:34 V38531MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 09/28/23 18:34 V38531MSA
<420 M µg/L 420 2000Ethanol 10 09/28/23 18:34 V38531MSA
47.8 µg/L 1.70 5.00Ethylbenzene 10 09/28/23 18:34 V38531MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 09/28/23 18:34 V38531MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 09/28/23 18:34 V38531MSA
3.45 J µg/L 1.80 5.00Isopropylbenzene 10 09/28/23 18:34 V38531MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 09/28/23 18:34 V38531MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 09/28/23 18:34 V38531MSA
166 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/28/23 18:34 V38531MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 09/28/23 18:34 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 12 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1R
95901 Matrix:
9/20/2023 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<3.30 µg/L 3.30 20.0Methylene Chloride 10 09/28/23 18:34 V38531MSA
96.5 µg/L 4.70 10.0Naphthalene 10 09/28/23 18:34 V38531MSA
6.00 µg/L 1.90 5.00n-Propylbenzene 10 09/28/23 18:34 V38531MSA
<2.20 µg/L 2.20 5.00Styrene 10 09/28/23 18:34 V38531MSA
78.4 J µg/L 16.0 100tert-Butyl Alcohol (TBA)10 09/28/23 18:34 V38531MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 09/28/23 18:34 V38531MSA
203 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 09/28/23 18:34 V38531MSA
20.5 J µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 09/28/23 18:34 V38531MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 09/28/23 18:34 V38531MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 09/28/23 18:34 V38531MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 09/28/23 18:34 V38531MSA
134 µg/L 2.20 5.00Toluene 10 09/28/23 18:34 V38531MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 09/28/23 18:34 V38531MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 09/28/23 18:34 V38531MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 09/28/23 18:34 V38531MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 09/28/23 18:34 V38531MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 09/28/23 18:34 V38531MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 09/28/23 18:34 V38531MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 09/28/23 18:34 V38531MSA
198 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 09/28/23 18:34 V38531MSA
75.9 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 09/28/23 18:34 V38531MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 09/28/23 18:34 V38531MSA
<1.70 M µg/L 1.70 5.00Vinyl Chloride 10 09/28/23 18:34 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 13 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1R
95901 Matrix:
9/20/2023 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
298 µg/L 2.10 5.00o-Xylene 10 09/28/23 18:34 V38531MSA
103 µg/L 4.20 10.0m,p-Xylene 10 09/28/23 18:34 V38531MSA
401 µg/L 2.10 5.00Xylene (Total)10 09/28/23 18:34 V38531
Surrogate: 4-Bromofluorobenzene 89.2 Limits: 70-130%09/28/23 18:3410 MSA V38531
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%09/28/23 18:3410 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/28/23 18:3410 MSA V38531
Surrogate: Toluene-d8 88.8 Limits: 70-130%09/28/23 18:3410 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
95902 Matrix:
9/20/2023 11:31
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 15:33 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%09/27/23 15:331 MSA V38456
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%09/27/23 15:331 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 15:331 MSA V38456
Surrogate: Toluene-d8 98.4 Limits: 70-130%09/27/23 15:331 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
95902 Matrix:
9/20/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 15:33 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 15:33 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 15:33 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 15:33 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 15:33 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 15:33 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 15:33 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 15:33 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 15:33 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 15:33 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 15:33 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 15:33 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 15:33 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 15:33 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 15:33 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 15:33 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 15:33 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 15:33 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 15:33 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 15:33 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
95902 Matrix:
9/20/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 15:33 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 15:33 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 15:33 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 15:33 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 15:33 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 15:33 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 15:33 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 15:33 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 15:33 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 15:33 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 15:33 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 15:33 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 15:33 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 15:33 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 15:33 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 15:33 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 15:33 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 15:33 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 15:33 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 15:33 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 15:33 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 17 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
95902 Matrix:
9/20/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 15:33 V38456MSA
2.27 µg/L 0.470 1.00Naphthalene 1 09/27/23 15:33 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 15:33 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 15:33 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 15:33 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 15:33 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 15:33 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 15:33 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 15:33 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 15:33 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 15:33 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 15:33 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 15:33 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 15:33 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 15:33 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 15:33 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 15:33 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 15:33 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 15:33 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 15:33 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 15:33 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 18 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
95902 Matrix:
9/20/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 15:33 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 15:33 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 15:33 V38456
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%09/27/23 15:331 MSA V38456
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%09/27/23 15:331 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 15:331 MSA V38456
Surrogate: Toluene-d8 98.4 Limits: 70-130%09/27/23 15:331 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 19 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
95903 Matrix:
9/20/2023 10:33
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 15:58 6200BMSA
Surrogate: 4-Bromofluorobenzene 88.6 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: Toluene-d8 95.6 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: 4-Bromofluorobenzene 87.0 Limits: 70-130%09/28/23 18:5810 MSA V38531
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 18:5810 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/28/23 18:5810 MSA V38531
Surrogate: Toluene-d8 93.2 Limits: 70-130%09/28/23 18:5810 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 20 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
95903 Matrix:
9/20/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 15:58 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 15:58 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 15:58 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 15:58 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 15:58 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 15:58 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 15:58 V38456MSA
5.04 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 15:58 V38456MSA
3.33 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 15:58 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 15:58 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 15:58 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 15:58 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 15:58 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 15:58 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 15:58 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 15:58 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 15:58 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 15:58 V38456MSA
1.43 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 15:58 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 15:58 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 15:58 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 15:58 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 15:58 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 21 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
95903 Matrix:
9/20/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 15:58 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 15:58 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 15:58 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 15:58 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 15:58 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 15:58 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 15:58 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 15:58 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 15:58 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 15:58 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 15:58 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 15:58 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 15:58 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 15:58 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 15:58 V38456MSA
89.0 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 15:58 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 15:58 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 15:58 V38456MSA
30.8 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 15:58 V38456MSA
2.55 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 15:58 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 15:58 V38456MSA
5.92 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 15:58 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 15:58 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 22 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
95903 Matrix:
9/20/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 15:58 V38456MSA
45.8 µg/L 0.470 1.00Naphthalene 1 09/27/23 15:58 V38456MSA
37.7 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 15:58 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 15:58 V38456MSA
2.84 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 15:58 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 15:58 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 15:58 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 15:58 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 15:58 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 15:58 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 15:58 V38456MSA
31.6 µg/L 0.220 0.500Toluene 1 09/27/23 15:58 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 15:58 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 15:58 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 15:58 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 15:58 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 15:58 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 15:58 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 15:58 V38456MSA
337 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 09/28/23 18:58 V38531MSA
118 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 09/28/23 18:58 V38531MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 15:58 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 15:58 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 23 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
95903 Matrix:
9/20/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
195 µg/L 2.10 5.00o-Xylene 10 09/28/23 18:58 V38531MSA
415 µg/L 4.20 10.0m,p-Xylene 10 09/28/23 18:58 V38531MSA
610 µg/L 2.10 5.00Xylene (Total)10 09/28/23 18:58 V38531
Surrogate: 4-Bromofluorobenzene 88.6 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: Toluene-d8 95.6 Limits: 70-130%09/27/23 15:581 MSA V38456
Surrogate: 4-Bromofluorobenzene 87.0 Limits: 70-130%09/28/23 18:5810 MSA V38531
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 18:5810 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/28/23 18:5810 MSA V38531
Surrogate: Toluene-d8 93.2 Limits: 70-130%09/28/23 18:5810 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 24 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
95904 Matrix:
9/20/2023 10:11
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 16:22 6200BMSA
Surrogate: 4-Bromofluorobenzene 87.6 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 114 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: Toluene-d8 95.2 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: 4-Bromofluorobenzene 84.4 Limits: 70-130%09/28/23 19:2310 MSA V38531
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/28/23 19:2310 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%09/28/23 19:2310 MSA V38531
Surrogate: Toluene-d8 93.6 Limits: 70-130%09/28/23 19:2310 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 25 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
95904 Matrix:
9/20/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 16:22 V38456MSA
0.212 J µg/L 0.180 0.500Benzene 1 09/27/23 16:22 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 16:22 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 16:22 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 16:22 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 16:22 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 16:22 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 16:22 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 16:22 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 16:22 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 16:22 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 16:22 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 16:22 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 16:22 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 16:22 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 16:22 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 16:22 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 16:22 V38456MSA
6.98 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 16:22 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 16:22 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 16:22 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 16:22 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 16:22 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 26 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
95904 Matrix:
9/20/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 16:22 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 16:22 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 16:22 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 16:22 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 16:22 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 16:22 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 16:22 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 16:22 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 16:22 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 16:22 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 16:22 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 16:22 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 16:22 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 16:22 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 16:22 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 16:22 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 16:22 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 16:22 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 16:22 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 16:22 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 16:22 V38456MSA
3.18 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 16:22 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 16:22 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 27 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
95904 Matrix:
9/20/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 16:22 V38456MSA
12.7 µg/L 0.470 1.00Naphthalene 1 09/27/23 16:22 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 16:22 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 16:22 V38456MSA
178 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 16:22 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 16:22 V38456MSA
186 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 09/28/23 19:23 V38531MSA
0.348 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 16:22 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 16:22 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 16:22 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 16:22 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 16:22 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 16:22 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 16:22 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 16:22 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 16:22 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 16:22 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 16:22 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 16:22 V38456MSA
1.19 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 16:22 V38456MSA
0.780 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 16:22 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 16:22 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 16:22 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 28 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
95904 Matrix:
9/20/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00 V38530 09/28/23 09:00
1.39 µg/L 0.210 0.500o-Xylene 1 09/27/23 16:22 V38456MSA
0.668 J µg/L 0.420 1.00m,p-Xylene 1 09/27/23 16:22 V38456MSA
2.06 J µg/L 0.210 0.500Xylene (Total)1 09/27/23 16:22 V38456
Surrogate: 4-Bromofluorobenzene 87.6 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 114 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: Toluene-d8 95.2 Limits: 70-130%09/27/23 16:221 MSA V38456
Surrogate: 4-Bromofluorobenzene 84.4 Limits: 70-130%09/28/23 19:2310 MSA V38531
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/28/23 19:2310 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%09/28/23 19:2310 MSA V38531
Surrogate: Toluene-d8 93.6 Limits: 70-130%09/28/23 19:2310 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 29 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
95905 Matrix:
9/20/2023 9:59
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 16:47 6200BMSA
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%09/27/23 16:471 MSA V38456
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 16:471 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 16:471 MSA V38456
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/27/23 16:471 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 30 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
95905 Matrix:
9/20/2023 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 16:47 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 16:47 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 16:47 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 16:47 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 16:47 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 16:47 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 16:47 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 16:47 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 16:47 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 16:47 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 16:47 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 16:47 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 16:47 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 16:47 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 16:47 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 16:47 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 16:47 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 16:47 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 16:47 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 16:47 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 31 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
95905 Matrix:
9/20/2023 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 16:47 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 16:47 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 16:47 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 16:47 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 16:47 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 16:47 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 16:47 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 16:47 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 16:47 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 16:47 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 16:47 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 16:47 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 16:47 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 16:47 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 16:47 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 16:47 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 16:47 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 16:47 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 16:47 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 16:47 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 16:47 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 32 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
95905 Matrix:
9/20/2023 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 16:47 V38456MSA
2.70 µg/L 0.470 1.00Naphthalene 1 09/27/23 16:47 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 16:47 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 16:47 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 16:47 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 16:47 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 16:47 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 16:47 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 16:47 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 16:47 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 16:47 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 16:47 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 16:47 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 16:47 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 16:47 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 16:47 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 16:47 V38456MSA
0.237 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 16:47 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 16:47 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 16:47 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 16:47 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 33 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
95905 Matrix:
9/20/2023 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 16:47 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 16:47 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 16:47 V38456
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%09/27/23 16:471 MSA V38456
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 16:471 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 16:471 MSA V38456
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/27/23 16:471 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 34 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
95906 Matrix:
9/20/2023 8:58
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 17:12 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%09/27/23 17:121 MSA V38456
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 17:121 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 17:121 MSA V38456
Surrogate: Toluene-d8 96.4 Limits: 70-130%09/27/23 17:121 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 35 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
95906 Matrix:
9/20/2023 8:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 17:12 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 17:12 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 17:12 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 17:12 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 17:12 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 17:12 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 17:12 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 17:12 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 17:12 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 17:12 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 17:12 V38456MSA
0.739 µg/L 0.220 0.500Chloroform 1 09/27/23 17:12 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 17:12 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 17:12 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 17:12 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 17:12 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 17:12 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 17:12 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 17:12 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 17:12 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 36 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
95906 Matrix:
9/20/2023 8:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 17:12 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 17:12 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 17:12 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 17:12 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 17:12 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 17:12 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 17:12 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 17:12 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 17:12 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 17:12 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 17:12 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 17:12 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 17:12 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 17:12 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 17:12 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 17:12 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 17:12 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 17:12 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 17:12 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 17:12 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 17:12 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 37 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
95906 Matrix:
9/20/2023 8:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 17:12 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 17:12 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 17:12 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 17:12 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 17:12 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 17:12 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 17:12 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 17:12 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 17:12 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 17:12 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 17:12 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 17:12 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 17:12 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 17:12 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 17:12 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 17:12 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 17:12 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 17:12 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 17:12 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 17:12 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 17:12 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 38 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
95906 Matrix:
9/20/2023 8:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 17:12 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 17:12 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 17:12 V38456
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%09/27/23 17:121 MSA V38456
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/27/23 17:121 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 17:121 MSA V38456
Surrogate: Toluene-d8 96.4 Limits: 70-130%09/27/23 17:121 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 39 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
95907 Matrix:
9/20/2023 10:22
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 17:37 6200BMSA
Surrogate: 4-Bromofluorobenzene 89.4 Limits: 70-130%09/27/23 17:371 MSA V38456
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 17:371 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 17:371 MSA V38456
Surrogate: Toluene-d8 95.6 Limits: 70-130%09/27/23 17:371 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 40 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
95907 Matrix:
9/20/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
5.50 J µg/L 1.80 10.0Acetone 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 17:37 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 17:37 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 17:37 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 17:37 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 17:37 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 17:37 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 17:37 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 17:37 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 17:37 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 17:37 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 17:37 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 17:37 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 17:37 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 17:37 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 17:37 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 17:37 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 17:37 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 17:37 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 17:37 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 17:37 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 41 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
95907 Matrix:
9/20/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 17:37 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 17:37 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 17:37 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 17:37 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 17:37 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 17:37 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 17:37 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 17:37 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 17:37 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 17:37 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 17:37 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 17:37 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 17:37 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 17:37 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 17:37 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 17:37 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 17:37 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 17:37 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 17:37 V38456MSA
0.398 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 17:37 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 17:37 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 42 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
95907 Matrix:
9/20/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 17:37 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 17:37 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 17:37 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 17:37 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 17:37 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 17:37 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 17:37 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 17:37 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 17:37 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 17:37 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 17:37 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 17:37 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 17:37 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 17:37 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 17:37 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 17:37 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 17:37 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 17:37 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 17:37 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 17:37 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 17:37 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 43 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
95907 Matrix:
9/20/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 17:37 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 17:37 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 17:37 V38456
Surrogate: 4-Bromofluorobenzene 89.4 Limits: 70-130%09/27/23 17:371 MSA V38456
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 17:371 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 17:371 MSA V38456
Surrogate: Toluene-d8 95.6 Limits: 70-130%09/27/23 17:371 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 44 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
95908 Matrix:
9/20/2023 9:17
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 18:02 6200BMSA
Surrogate: 4-Bromofluorobenzene 89.6 Limits: 70-130%09/27/23 18:021 MSA V38456
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/27/23 18:021 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 111 Limits: 70-130%09/27/23 18:021 MSA V38456
Surrogate: Toluene-d8 94.4 Limits: 70-130%09/27/23 18:021 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 45 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
95908 Matrix:
9/20/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 18:02 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 18:02 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 18:02 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 18:02 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 18:02 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 18:02 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 18:02 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 18:02 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 18:02 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 18:02 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 18:02 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 18:02 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 18:02 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 18:02 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 18:02 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 18:02 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 18:02 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 18:02 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 18:02 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 18:02 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 46 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
95908 Matrix:
9/20/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 18:02 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 18:02 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 18:02 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 18:02 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 18:02 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 18:02 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 18:02 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 18:02 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 18:02 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 18:02 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 18:02 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 18:02 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 18:02 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 18:02 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 18:02 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 18:02 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 18:02 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 18:02 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 18:02 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 18:02 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 18:02 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 47 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
95908 Matrix:
9/20/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 18:02 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 18:02 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 18:02 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 18:02 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 18:02 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 18:02 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 18:02 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 18:02 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 18:02 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 18:02 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 18:02 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 18:02 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 18:02 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 18:02 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 18:02 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 18:02 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 18:02 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 18:02 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 18:02 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 18:02 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 18:02 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 48 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
95908 Matrix:
9/20/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 18:02 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 18:02 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 18:02 V38456
Surrogate: 4-Bromofluorobenzene 89.6 Limits: 70-130%09/27/23 18:021 MSA V38456
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/27/23 18:021 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 111 Limits: 70-130%09/27/23 18:021 MSA V38456
Surrogate: Toluene-d8 94.4 Limits: 70-130%09/27/23 18:021 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 49 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
95909 Matrix:
9/20/2023 10:47
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 18:27 6200BMSA
Surrogate: 4-Bromofluorobenzene 89.2 Limits: 70-130%09/27/23 18:271 MSA V38456
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/27/23 18:271 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/27/23 18:271 MSA V38456
Surrogate: Toluene-d8 97.6 Limits: 70-130%09/27/23 18:271 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 50 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
95909 Matrix:
9/20/2023 10:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 18:27 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 18:27 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 18:27 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 18:27 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 18:27 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 18:27 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 18:27 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 18:27 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 18:27 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 18:27 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 18:27 V38456MSA
0.228 J µg/L 0.220 0.500Chloroform 1 09/27/23 18:27 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 18:27 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 18:27 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 18:27 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 18:27 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 18:27 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 18:27 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 18:27 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 18:27 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 51 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
95909 Matrix:
9/20/2023 10:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 18:27 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 18:27 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 18:27 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 18:27 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 18:27 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 18:27 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 18:27 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 18:27 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 18:27 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 18:27 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 18:27 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 18:27 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 18:27 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 18:27 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 18:27 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 18:27 V38456MSA
4.51 µg/L 0.380 1.002-Hexanone 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 18:27 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 18:27 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 18:27 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 18:27 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 18:27 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 52 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
95909 Matrix:
9/20/2023 10:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 18:27 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 18:27 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 18:27 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 18:27 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 18:27 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 18:27 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 18:27 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 18:27 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 18:27 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 18:27 V38456MSA
0.411 J µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 18:27 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 18:27 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 18:27 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 18:27 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 18:27 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 18:27 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 18:27 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 18:27 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 18:27 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 18:27 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 18:27 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 53 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
95909 Matrix:
9/20/2023 10:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 18:27 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 18:27 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 18:27 V38456
Surrogate: 4-Bromofluorobenzene 89.2 Limits: 70-130%09/27/23 18:271 MSA V38456
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/27/23 18:271 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/27/23 18:271 MSA V38456
Surrogate: Toluene-d8 97.6 Limits: 70-130%09/27/23 18:271 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 54 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-10
95910 Matrix:
9/20/2023 10:58
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 18:51 6200BMSA
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%09/27/23 18:511 MSA V38456
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/27/23 18:511 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 18:511 MSA V38456
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/27/23 18:511 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 55 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-10
95910 Matrix:
9/20/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 18:51 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 18:51 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 18:51 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 18:51 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 18:51 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 18:51 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 18:51 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 18:51 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 18:51 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 18:51 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 18:51 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 18:51 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 18:51 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 18:51 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 18:51 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 18:51 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 18:51 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 18:51 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 18:51 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 18:51 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 56 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-10
95910 Matrix:
9/20/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 18:51 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 18:51 V38456MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 18:51 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 18:51 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 18:51 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 18:51 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 18:51 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 18:51 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 18:51 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 18:51 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 18:51 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 18:51 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 18:51 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 18:51 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 18:51 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 18:51 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 18:51 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 18:51 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 18:51 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 18:51 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 18:51 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 57 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-10
95910 Matrix:
9/20/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 18:51 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 18:51 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 18:51 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 18:51 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 18:51 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 18:51 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 18:51 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 18:51 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 18:51 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 18:51 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 18:51 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 18:51 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 18:51 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 18:51 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 18:51 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 18:51 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 18:51 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 18:51 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 18:51 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 18:51 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 18:51 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 58 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-10
95910 Matrix:
9/20/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 18:51 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 18:51 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 18:51 V38456
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%09/27/23 18:511 MSA V38456
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/27/23 18:511 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/27/23 18:511 MSA V38456
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/27/23 18:511 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 59 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-1
95911 Matrix:
9/20/2023 11:59
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 19:16 6200BMSA
Surrogate: 4-Bromofluorobenzene 90.2 Limits: 70-130%09/27/23 19:161 MSA V38456
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/27/23 19:161 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/27/23 19:161 MSA V38456
Surrogate: Toluene-d8 96.8 Limits: 70-130%09/27/23 19:161 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 60 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-1
95911 Matrix:
9/20/2023 11:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 19:16 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 19:16 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 19:16 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 19:16 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 19:16 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 19:16 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 19:16 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 19:16 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 19:16 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 19:16 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 19:16 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 19:16 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 19:16 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 19:16 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 19:16 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 19:16 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 19:16 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 19:16 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 19:16 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 19:16 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 61 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-1
95911 Matrix:
9/20/2023 11:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 19:16 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 19:16 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 19:16 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 19:16 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 19:16 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 19:16 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 19:16 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 19:16 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 19:16 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 19:16 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 19:16 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 19:16 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 19:16 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 19:16 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 19:16 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 19:16 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 19:16 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 19:16 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 19:16 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 19:16 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 19:16 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 62 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-1
95911 Matrix:
9/20/2023 11:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 19:16 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 19:16 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 19:16 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 19:16 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 19:16 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 19:16 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 19:16 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 19:16 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 19:16 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 19:16 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 19:16 V38456MSA
0.270 J µg/L 0.220 0.500Toluene 1 09/27/23 19:16 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 19:16 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 19:16 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 19:16 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 19:16 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 19:16 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 19:16 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 19:16 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 19:16 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 19:16 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 63 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-1
95911 Matrix:
9/20/2023 11:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 19:16 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 19:16 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 19:16 V38456
Surrogate: 4-Bromofluorobenzene 90.2 Limits: 70-130%09/27/23 19:161 MSA V38456
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/27/23 19:161 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/27/23 19:161 MSA V38456
Surrogate: Toluene-d8 96.8 Limits: 70-130%09/27/23 19:161 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 64 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-2
95912 Matrix:
9/20/2023 9:45
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 09/27/23 20:55 6200BMSA
Surrogate: 4-Bromofluorobenzene 89.4 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: Toluene-d8 95.8 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: 4-Bromofluorobenzene 90.8 Limits: 70-130%09/27/23 21:201000 MSA V38456
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 21:201000 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/27/23 21:201000 MSA V38456
Surrogate: Toluene-d8 94.4 Limits: 70-130%09/27/23 21:201000 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 65 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-2
95912 Matrix:
9/20/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<180 µg/L 180 1000Acetone 100 09/27/23 20:55 V38456MSA
10800 µg/L 180 500Benzene 1000 09/27/23 21:20 V38456MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/27/23 20:55 V38456MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/27/23 20:55 V38456MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/27/23 20:55 V38456MSA
<150 µg/L 150 500Bromoform 100 09/27/23 20:55 V38456MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/27/23 20:55 V38456MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 09/27/23 20:55 V38456MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/27/23 20:55 V38456MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/27/23 20:55 V38456MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/27/23 20:55 V38456MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/27/23 20:55 V38456MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/27/23 20:55 V38456MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/27/23 20:55 V38456MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/27/23 20:55 V38456MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/27/23 20:55 V38456MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/27/23 20:55 V38456MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/27/23 20:55 V38456MSA
3360 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/27/23 20:55 V38456MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/27/23 20:55 V38456MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 09/27/23 20:55 V38456MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/27/23 20:55 V38456MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/27/23 20:55 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 66 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-2
95912 Matrix:
9/20/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/27/23 20:55 V38456MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/27/23 20:55 V38456MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/27/23 20:55 V38456MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/27/23 20:55 V38456MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/27/23 20:55 V38456MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/27/23 20:55 V38456MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/27/23 20:55 V38456MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/27/23 20:55 V38456MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/27/23 20:55 V38456MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/27/23 20:55 V38456MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/27/23 20:55 V38456MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/27/23 20:55 V38456MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/27/23 20:55 V38456MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/27/23 20:55 V38456MSA
<4200 µg/L 4200 20000Ethanol 100 09/27/23 20:55 V38456MSA
1860 µg/L 17.0 50.0Ethylbenzene 100 09/27/23 20:55 V38456MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/27/23 20:55 V38456MSA
<38.0 µg/L 38.0 1002-Hexanone 100 09/27/23 20:55 V38456MSA
40.0 J µg/L 18.0 50.0Isopropylbenzene 100 09/27/23 20:55 V38456MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/27/23 20:55 V38456MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/27/23 20:55 V38456MSA
19900 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 09/27/23 21:20 V38456MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/27/23 20:55 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 67 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-2
95912 Matrix:
9/20/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<33.0 µg/L 33.0 200Methylene Chloride 100 09/27/23 20:55 V38456MSA
466 µg/L 47.0 100Naphthalene 100 09/27/23 20:55 V38456MSA
120 µg/L 19.0 50.0n-Propylbenzene 100 09/27/23 20:55 V38456MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/27/23 20:55 V38456MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 09/27/23 20:55 V38456MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 09/27/23 20:55 V38456MSA
13000 µg/L 1900 10000tert-Amyl Alcohol (TAA)1000 09/27/23 21:20 V38456MSA
1310 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 09/27/23 20:55 V38456MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/27/23 20:55 V38456MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/27/23 20:55 V38456MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/27/23 20:55 V38456MSA
25000 µg/L 220 500Toluene 1000 09/27/23 21:20 V38456MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/27/23 20:55 V38456MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/27/23 20:55 V38456MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/27/23 20:55 V38456MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/27/23 20:55 V38456MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/27/23 20:55 V38456MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/27/23 20:55 V38456MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/27/23 20:55 V38456MSA
1300 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/27/23 20:55 V38456MSA
317 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/27/23 20:55 V38456MSA
<100 µg/L 100 500Vinyl Acetate 100 09/27/23 20:55 V38456MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 09/27/23 20:55 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 68 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-2
95912 Matrix:
9/20/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
3360 µg/L 21.0 50.0o-Xylene 100 09/27/23 20:55 V38456MSA
7580 µg/L 42.0 100m,p-Xylene 100 09/27/23 20:55 V38456MSA
10900 µg/L 21.0 50.0Xylene (Total)100 09/27/23 20:55 V38456
Surrogate: 4-Bromofluorobenzene 89.4 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: Toluene-d8 95.8 Limits: 70-130%09/27/23 20:55100 MSA V38456
Surrogate: 4-Bromofluorobenzene 90.8 Limits: 70-130%09/27/23 21:201000 MSA V38456
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 21:201000 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/27/23 21:201000 MSA V38456
Surrogate: Toluene-d8 94.4 Limits: 70-130%09/27/23 21:201000 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 69 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-3
95913 Matrix:
9/20/2023 12:14
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 09/28/23 19:48 6200BMSA
Surrogate: 4-Bromofluorobenzene 87.8 Limits: 70-130%09/28/23 19:4810 MSA V38531
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%09/28/23 19:4810 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%09/28/23 19:4810 MSA V38531
Surrogate: Toluene-d8 93.6 Limits: 70-130%09/28/23 19:4810 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 70 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-3
95913 Matrix:
9/20/2023 12:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<18.0 µg/L 18.0 100Acetone 10 09/28/23 19:48 V38531MSA
129 µg/L 1.80 5.00Benzene 10 09/28/23 19:48 V38531MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 09/28/23 19:48 V38531MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 09/28/23 19:48 V38531MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 09/28/23 19:48 V38531MSA
<15.0 µg/L 15.0 50.0Bromoform 10 09/28/23 19:48 V38531MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 09/28/23 19:48 V38531MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 09/28/23 19:48 V38531MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 09/28/23 19:48 V38531MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 09/28/23 19:48 V38531MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 09/28/23 19:48 V38531MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 09/28/23 19:48 V38531MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 09/28/23 19:48 V38531MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 09/28/23 19:48 V38531MSA
<2.20 µg/L 2.20 5.00Chloroform 10 09/28/23 19:48 V38531MSA
<2.20 M µg/L 2.20 5.00Chloromethane 10 09/28/23 19:48 V38531MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 09/28/23 19:48 V38531MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 09/28/23 19:48 V38531MSA
33.2 M µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 09/28/23 19:48 V38531MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 09/28/23 19:48 V38531MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 09/28/23 19:48 V38531MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 09/28/23 19:48 V38531MSA
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 09/28/23 19:48 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 71 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-3
95913 Matrix:
9/20/2023 12:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 09/28/23 19:48 V38531MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 09/28/23 19:48 V38531MSA
<12.0 M µg/L 12.0 50.0Dichlorodifluoromethane 10 09/28/23 19:48 V38531MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 09/28/23 19:48 V38531MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 09/28/23 19:48 V38531MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 09/28/23 19:48 V38531MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 09/28/23 19:48 V38531MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 09/28/23 19:48 V38531MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 09/28/23 19:48 V38531MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 09/28/23 19:48 V38531MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 09/28/23 19:48 V38531MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 09/28/23 19:48 V38531MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 09/28/23 19:48 V38531MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 09/28/23 19:48 V38531MSA
<420 M µg/L 420 2000Ethanol 10 09/28/23 19:48 V38531MSA
<1.70 µg/L 1.70 5.00Ethylbenzene 10 09/28/23 19:48 V38531MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 09/28/23 19:48 V38531MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 09/28/23 19:48 V38531MSA
4.55 J µg/L 1.80 5.00Isopropylbenzene 10 09/28/23 19:48 V38531MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 09/28/23 19:48 V38531MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 09/28/23 19:48 V38531MSA
103 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/28/23 19:48 V38531MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 09/28/23 19:48 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 72 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-3
95913 Matrix:
9/20/2023 12:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<3.30 µg/L 3.30 20.0Methylene Chloride 10 09/28/23 19:48 V38531MSA
14.1 µg/L 4.70 10.0Naphthalene 10 09/28/23 19:48 V38531MSA
<1.90 µg/L 1.90 5.00n-Propylbenzene 10 09/28/23 19:48 V38531MSA
<2.20 µg/L 2.20 5.00Styrene 10 09/28/23 19:48 V38531MSA
29.6 J µg/L 16.0 100tert-Butyl Alcohol (TBA)10 09/28/23 19:48 V38531MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 09/28/23 19:48 V38531MSA
217 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 09/28/23 19:48 V38531MSA
5.86 J µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 09/28/23 19:48 V38531MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 09/28/23 19:48 V38531MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 09/28/23 19:48 V38531MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 09/28/23 19:48 V38531MSA
3.12 J µg/L 2.20 5.00Toluene 10 09/28/23 19:48 V38531MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 09/28/23 19:48 V38531MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 09/28/23 19:48 V38531MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 09/28/23 19:48 V38531MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 09/28/23 19:48 V38531MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 09/28/23 19:48 V38531MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 09/28/23 19:48 V38531MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 09/28/23 19:48 V38531MSA
39.6 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 09/28/23 19:48 V38531MSA
4.21 J µg/L 1.80 5.001,3,5-Trimethylbenzene 10 09/28/23 19:48 V38531MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 09/28/23 19:48 V38531MSA
<1.70 M µg/L 1.70 5.00Vinyl Chloride 10 09/28/23 19:48 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 73 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:DW-3
95913 Matrix:
9/20/2023 12:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
20.9 µg/L 2.10 5.00o-Xylene 10 09/28/23 19:48 V38531MSA
85.6 µg/L 4.20 10.0m,p-Xylene 10 09/28/23 19:48 V38531MSA
107 µg/L 2.10 5.00Xylene (Total)10 09/28/23 19:48 V38531
Surrogate: 4-Bromofluorobenzene 87.8 Limits: 70-130%09/28/23 19:4810 MSA V38531
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%09/28/23 19:4810 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%09/28/23 19:4810 MSA V38531
Surrogate: Toluene-d8 93.6 Limits: 70-130%09/28/23 19:4810 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 74 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:OW-2
95914 Matrix:
9/20/2023 11:21
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 09/27/23 21:45 6200BMSA
Surrogate: 4-Bromofluorobenzene 89.8 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: Toluene-d8 96.4 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: 4-Bromofluorobenzene 88.6 Limits: 70-130%09/27/23 22:101000 MSA V38456
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/27/23 22:101000 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 22:101000 MSA V38456
Surrogate: Toluene-d8 94.6 Limits: 70-130%09/27/23 22:101000 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 75 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:OW-2
95914 Matrix:
9/20/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<180 µg/L 180 1000Acetone 100 09/27/23 21:45 V38456MSA
1620 µg/L 18.0 50.0Benzene 100 09/27/23 21:45 V38456MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/27/23 21:45 V38456MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/27/23 21:45 V38456MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/27/23 21:45 V38456MSA
<150 µg/L 150 500Bromoform 100 09/27/23 21:45 V38456MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/27/23 21:45 V38456MSA
51.3 µg/L 18.0 50.0n-Butylbenzene 100 09/27/23 21:45 V38456MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/27/23 21:45 V38456MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/27/23 21:45 V38456MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/27/23 21:45 V38456MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/27/23 21:45 V38456MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/27/23 21:45 V38456MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/27/23 21:45 V38456MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/27/23 21:45 V38456MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/27/23 21:45 V38456MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/27/23 21:45 V38456MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/27/23 21:45 V38456MSA
146 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/27/23 21:45 V38456MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/27/23 21:45 V38456MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 09/27/23 21:45 V38456MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/27/23 21:45 V38456MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/27/23 21:45 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 76 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:OW-2
95914 Matrix:
9/20/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/27/23 21:45 V38456MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/27/23 21:45 V38456MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/27/23 21:45 V38456MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/27/23 21:45 V38456MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/27/23 21:45 V38456MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/27/23 21:45 V38456MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/27/23 21:45 V38456MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/27/23 21:45 V38456MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/27/23 21:45 V38456MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/27/23 21:45 V38456MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/27/23 21:45 V38456MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/27/23 21:45 V38456MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/27/23 21:45 V38456MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/27/23 21:45 V38456MSA
<4200 µg/L 4200 20000Ethanol 100 09/27/23 21:45 V38456MSA
3320 µg/L 17.0 50.0Ethylbenzene 100 09/27/23 21:45 V38456MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/27/23 21:45 V38456MSA
<38.0 µg/L 38.0 1002-Hexanone 100 09/27/23 21:45 V38456MSA
115 µg/L 18.0 50.0Isopropylbenzene 100 09/27/23 21:45 V38456MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/27/23 21:45 V38456MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/27/23 21:45 V38456MSA
526 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/27/23 21:45 V38456MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/27/23 21:45 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 77 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:OW-2
95914 Matrix:
9/20/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<33.0 µg/L 33.0 200Methylene Chloride 100 09/27/23 21:45 V38456MSA
1820 µg/L 47.0 100Naphthalene 100 09/27/23 21:45 V38456MSA
358 µg/L 19.0 50.0n-Propylbenzene 100 09/27/23 21:45 V38456MSA
135 µg/L 22.0 50.0Styrene 100 09/27/23 21:45 V38456MSA
309 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 09/27/23 21:45 V38456MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 09/27/23 21:45 V38456MSA
1080 µg/L 190 1000tert-Amyl Alcohol (TAA)100 09/27/23 21:45 V38456MSA
109 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 09/27/23 21:45 V38456MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/27/23 21:45 V38456MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/27/23 21:45 V38456MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/27/23 21:45 V38456MSA
22700 µg/L 220 500Toluene 1000 09/27/23 22:10 V38456MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/27/23 21:45 V38456MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/27/23 21:45 V38456MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/27/23 21:45 V38456MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/27/23 21:45 V38456MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/27/23 21:45 V38456MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/27/23 21:45 V38456MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/27/23 21:45 V38456MSA
4540 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/27/23 21:45 V38456MSA
1080 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/27/23 21:45 V38456MSA
<100 µg/L 100 500Vinyl Acetate 100 09/27/23 21:45 V38456MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 09/27/23 21:45 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 78 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:OW-2
95914 Matrix:
9/20/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
7220 µg/L 21.0 50.0o-Xylene 100 09/27/23 21:45 V38456MSA
14900 µg/L 42.0 100m,p-Xylene 100 09/27/23 21:45 V38456MSA
22100 µg/L 21.0 50.0Xylene (Total)100 09/27/23 21:45 V38456
Surrogate: 4-Bromofluorobenzene 89.8 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: Toluene-d8 96.4 Limits: 70-130%09/27/23 21:45100 MSA V38456
Surrogate: 4-Bromofluorobenzene 88.6 Limits: 70-130%09/27/23 22:101000 MSA V38456
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%09/27/23 22:101000 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%09/27/23 22:101000 MSA V38456
Surrogate: Toluene-d8 94.6 Limits: 70-130%09/27/23 22:101000 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 79 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
95915 Matrix:
9/20/2023 8:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/27/23 14:19 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%09/27/23 14:191 MSA V38456
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 14:191 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 110 Limits: 70-130%09/27/23 14:191 MSA V38456
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/27/23 14:191 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 80 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
95915 Matrix:
9/20/2023 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/27/23 14:19 V38456MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/27/23 14:19 V38456MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/27/23 14:19 V38456MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/27/23 14:19 V38456MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/27/23 14:19 V38456MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/27/23 14:19 V38456MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/27/23 14:19 V38456MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/27/23 14:19 V38456MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/27/23 14:19 V38456MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/27/23 14:19 V38456MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/27/23 14:19 V38456MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/27/23 14:19 V38456MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/27/23 14:19 V38456MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/27/23 14:19 V38456MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/27/23 14:19 V38456MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/27/23 14:19 V38456MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/27/23 14:19 V38456MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/27/23 14:19 V38456MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/27/23 14:19 V38456MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/27/23 14:19 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 81 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
95915 Matrix:
9/20/2023 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/27/23 14:19 V38456MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/27/23 14:19 V38456MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/27/23 14:19 V38456MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/27/23 14:19 V38456MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/27/23 14:19 V38456MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/27/23 14:19 V38456MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/27/23 14:19 V38456MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/27/23 14:19 V38456MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/27/23 14:19 V38456MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/27/23 14:19 V38456MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/27/23 14:19 V38456MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/27/23 14:19 V38456MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/27/23 14:19 V38456MSA
<42.0 µg/L 42.0 200Ethanol 1 09/27/23 14:19 V38456MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/27/23 14:19 V38456MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/27/23 14:19 V38456MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/27/23 14:19 V38456MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/27/23 14:19 V38456MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/27/23 14:19 V38456MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/27/23 14:19 V38456MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/27/23 14:19 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 82 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
95915 Matrix:
9/20/2023 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/27/23 14:19 V38456MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/27/23 14:19 V38456MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/27/23 14:19 V38456MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/27/23 14:19 V38456MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/27/23 14:19 V38456MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/27/23 14:19 V38456MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/27/23 14:19 V38456MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/27/23 14:19 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/27/23 14:19 V38456MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/27/23 14:19 V38456MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/27/23 14:19 V38456MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/27/23 14:19 V38456MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/27/23 14:19 V38456MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/27/23 14:19 V38456MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/27/23 14:19 V38456MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/27/23 14:19 V38456MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/27/23 14:19 V38456MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/27/23 14:19 V38456MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/27/23 14:19 V38456MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/27/23 14:19 V38456MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/27/23 14:19 V38456MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 83 of 99
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-264-0032
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 09/21/2023
Handy Stop #7
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
95915 Matrix:
9/20/2023 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38455 09/27/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 09/27/23 14:19 V38456MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/27/23 14:19 V38456MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/27/23 14:19 V38456
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%09/27/23 14:191 MSA V38456
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/27/23 14:191 MSA V38456
Surrogate: 1,2-Dichloroethane - d4 110 Limits: 70-130%09/27/23 14:191 MSA V38456
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/27/23 14:191 MSA V38456
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 84 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38456QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38455
Associated Lab Samples: 95902, 95903, 95904, 95905, 95906, 95907, 95908, 95909, 95910, 95911, 95912, 95914, 95915
LRB-V38455 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/27/23 13:3010.01.80<1.80µg/LAcetone
09/27/23 13:300.5000.180<0.180µg/LBenzene
09/27/23 13:300.5000.210<0.210µg/LBromobenzene
09/27/23 13:301.000.420<0.420µg/LBromochloromethane
09/27/23 13:300.5000.160<0.160µg/LBromodichloromethane
09/27/23 13:305.001.50<1.50µg/LBromoform
09/27/23 13:301.000.280<0.280µg/LBromomethane
09/27/23 13:300.5000.180<0.180µg/Ln-Butylbenzene
09/27/23 13:300.5000.200<0.200µg/Lsec-Butyl benzene
09/27/23 13:302.000.920<0.920µg/Ltert-Butyl benzene
09/27/23 13:300.5000.180<0.180µg/LCarbon Tetrachloride
09/27/23 13:300.5000.190<0.190µg/LChlorobenzene
09/27/23 13:300.5000.190<0.190µg/LChlorodibromomethane
09/27/23 13:301.000.430<0.430µg/LChloroethane
09/27/23 13:300.5000.220<0.220µg/LChloroform
09/27/23 13:300.5000.220<0.220µg/LChloromethane
09/27/23 13:300.5000.200<0.200µg/L2-Chlorotoluene
09/27/23 13:300.5000.200<0.200µg/L4-Chlorotoluene
09/27/23 13:300.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/27/23 13:302.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/27/23 13:300.5000.200<0.200µg/L1,2-Dibromoethane
09/27/23 13:300.5000.230<0.230µg/LDibromomethane
09/27/23 13:300.5000.220<0.220µg/L1,2-Dichlorobenzene
09/27/23 13:300.5000.190<0.190µg/L1,3-Dichlorobenzene
09/27/23 13:300.5000.210<0.210µg/L1,4-Dichlorobenzene
09/27/23 13:305.001.20<1.20µg/LDichlorodifluoromethane
09/27/23 13:300.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 12Date:10/03/2023 11:48 AM
Page 85 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38456QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38455
Associated Lab Samples: 95902, 95903, 95904, 95905, 95906, 95907, 95908, 95909, 95910, 95911, 95912, 95914, 95915
LRB-V38455 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/27/23 13:300.5000.150<0.150µg/L1,2-Dichloroethane
09/27/23 13:300.5000.150<0.150µg/L1,1-Dichloroethene
09/27/23 13:300.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/27/23 13:300.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/27/23 13:300.5000.190<0.190µg/L1,2-Dichloropropane
09/27/23 13:300.5000.130<0.130µg/L1,3-Dichloropropane
09/27/23 13:302.000.210<0.210µg/L2,2-Dichloropropane
09/27/23 13:300.5000.200<0.200µg/L1,1-Dichloropropene
09/27/23 13:300.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/27/23 13:300.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/27/23 13:3020042.0<42.0µg/LEthanol
09/27/23 13:300.5000.170<0.170µg/LEthylbenzene
09/27/23 13:303.000.350<0.350µg/LHexachlorobutadiene
09/27/23 13:301.000.380<0.380µg/L2-Hexanone
09/27/23 13:300.5000.180<0.180µg/LIsopropylbenzene
09/27/23 13:300.5000.089<0.089µg/L4-Isopropyl toluene
09/27/23 13:305.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/27/23 13:301.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/27/23 13:301.000.078<0.078µg/L4-Methyl-2-Pentanone
09/27/23 13:302.000.330<0.330µg/LMethylene Chloride
09/27/23 13:301.000.470<0.470µg/LNaphthalene
09/27/23 13:300.5000.190<0.190µg/Ln-Propylbenzene
09/27/23 13:300.5000.220<0.220µg/LStyrene
09/27/23 13:3010.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/27/23 13:3010.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/27/23 13:3010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/27/23 13:3010.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 12Date:10/03/2023 11:48 AM
Page 86 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38456QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38455
Associated Lab Samples: 95902, 95903, 95904, 95905, 95906, 95907, 95908, 95909, 95910, 95911, 95912, 95914, 95915
LRB-V38455 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/27/23 13:300.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/27/23 13:300.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/27/23 13:300.5000.220<0.220µg/LTetrachloroethene
09/27/23 13:300.5000.220<0.220µg/LToluene
09/27/23 13:300.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/27/23 13:300.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/27/23 13:300.5000.160<0.160µg/L1,1,1-Trichloroethane
09/27/23 13:300.5000.096<0.096µg/L1,1,2-Trichloroethane
09/27/23 13:300.5000.180<0.180µg/LTrichloroethene
09/27/23 13:300.5000.180<0.180µg/LTrichlorofluoromethane
09/27/23 13:300.5000.270<0.270µg/L1,2,3-Trichloropropane
09/27/23 13:300.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/27/23 13:300.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/27/23 13:305.001.00<1.00µg/LVinyl Acetate
09/27/23 13:300.5000.170<0.170µg/LVinyl Chloride
09/27/23 13:300.5000.210<0.210µg/Lo-Xylene
09/27/23 13:301.000.420<0.420µg/Lm,p-Xylene
09/27/23 13:3010.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/27/23 13:304-Bromofluorobenzene (S)91.0 70-130
09/27/23 13:30Dibromofluoromethane (S)101 70-130
09/27/23 13:301,2-Dichloroethane - d4 (S)110 70-130
09/27/23 13:30Toluene-d8 (S)96.8 70-130
Page 3 of 12Date:10/03/2023 11:48 AM
Page 87 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38456QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38455
LCS-V38455 LCSD-V38455Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.5 10110642.340.0µg/LAcetone 40-160 4.3 20.0
19.3 96.598.019.620.0µg/LBenzene 70-130 1.5 20.0
20.8 10410420.820.0µg/LBromobenzene 70-130 0.0 20.0
21.7 10910621.220.0µg/LBromochloromethane 70-130 2.3 20.0
21.2 10610821.620.0µg/LBromodichloromethane 70-130 1.8 20.0
22.8 11411823.620.0µg/LBromoform 70-130 3.4 20.0
19.3 96.593.518.720.0µg/LBromomethane 60-140 3.1 20.0
21.9 11011122.120.0µg/Ln-Butylbenzene 70-130 0.9 20.0
21.0 10510921.720.0µg/Lsec-Butyl benzene 70-130 3.2 20.0
21.6 10811022.020.0µg/Ltert-Butyl benzene 70-130 1.8 20.0
26.7 134*132*26.420.0µg/LCarbon Tetrachloride 70-130 1.1 20.0
22.3 11210821.520.0µg/LChlorobenzene 70-130 3.6 20.0
23.5 11812024.020.0µg/LChlorodibromomethane 70-130 2.1 20.0
14.5 72.567.513.520.0µg/LChloroethane 60-140 7.1 20.0
21.0 10510921.720.0µg/LChloroform 70-130 3.2 20.0
11.4 57.0*57.0*11.420.0µg/LChloromethane 60-140 0.0 20.0
19.9 99.510220.420.0µg/L2-Chlorotoluene 70-130 2.4 20.0
20.4 10210521.020.0µg/L4-Chlorotoluene 70-130 2.8 20.0
15.2 76.077.515.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.9 20.0
21.6 10811923.820.0µg/L1,2-Dibromo-3-Chloropropane 70-130 9.6 20.0
18.7 93.597.519.520.0µg/L1,2-Dibromoethane 70-130 4.1 20.0
20.5 10310821.520.0µg/LDibromomethane 70-130 4.7 20.0
22.0 11011222.420.0µg/L1,2-Dichlorobenzene 70-130 1.8 20.0
22.1 11111623.120.0µg/L1,3-Dichlorobenzene 70-130 4.4 20.0
22.0 11011022.020.0µg/L1,4-Dichlorobenzene 70-130 0.0 20.0
10.9 54.5*52.5*10.520.0µg/LDichlorodifluoromethane 60-140 3.7 20.0
Page 4 of 12* QC Fail Date:10/03/2023 11:48 AM
Page 88 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38456QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38455
LCS-V38455 LCSD-V38455Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.4 97.096.519.320.0µg/L1,1-Dichloroethane 70-130 0.5 20.0
21.8 10911021.920.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
20.3 10210520.920.0µg/L1,1-Dichloroethene 70-130 2.9 20.0
18.9 94.598.519.720.0µg/Lcis-1,2-Dichloroethene 70-130 4.1 20.0
19.8 99.010220.320.0µg/Ltrans-1,2-Dichloroethene 70-130 2.4 20.0
15.8 79.084.016.820.0µg/L1,2-Dichloropropane 70-130 6.1 20.0
18.7 93.596.519.320.0µg/L1,3-Dichloropropane 70-130 3.1 20.0
24.7 12412124.220.0µg/L2,2-Dichloropropane 70-130 2.0 20.0
22.2 11111322.520.0µg/L1,1-Dichloropropene 70-130 1.3 20.0
19.8 99.010120.220.0µg/Lcis-1,3-Dichloropropene 70-130 2.0 20.0
21.2 10610721.420.0µg/Ltrans-1,3-Dichloropropene 70-130 0.9 20.0
366 73.283.6418500µg/LEthanol 60-140 13.2 20.0
20.7 10410520.920.0µg/LEthylbenzene 70-130 0.9 20.0
26.7 134*13026.020.0µg/LHexachlorobutadiene 70-130 2.6 20.0
19.2 96.089.517.920.0µg/L2-Hexanone 60-140 7.0 20.0
22.6 11311322.620.0µg/LIsopropylbenzene 70-130 0.0 20.0
23.2 11611723.320.0µg/L4-Isopropyl toluene 70-130 0.4 20.0
16.9 84.590.018.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.3 20.0
19.8 99.010721.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 7.7 20.0
15.9 79.580.516.120.0µg/L4-Methyl-2-Pentanone 60-140 1.2 20.0
15.3 76.583.016.620.0µg/LMethylene Chloride 70-130 8.1 20.0
22.8 11411522.920.0µg/LNaphthalene 70-130 0.4 20.0
20.8 10410420.820.0µg/Ln-Propylbenzene 70-130 0.0 20.0
21.9 11011222.420.0µg/LStyrene 70-130 2.2 20.0
40.3 10199.539.840.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.2 20.0
39.9 99.711144.540.0µg/Ltert-Butyl formate (TBF)40-140 10.9 20.0
Page 5 of 12* QC Fail Date:10/03/2023 11:48 AM
Page 89 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38456QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38455
LCS-V38455 LCSD-V38455Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.2 96.091.518.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 4.8 20.0
38.7 96.710140.340.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 4.0 20.0
23.9 12011322.620.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.5 20.0
17.9 89.592.518.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 3.2 20.0
24.0 12011422.820.0µg/LTetrachloroethene 70-130 5.1 20.0
19.6 98.010220.420.0µg/LToluene 70-130 4.0 20.0
29.8 149*135*27.020.0µg/L1,2,3-Trichlorobenzene 70-130 9.8 20.0
26.7 134*132*26.320.0µg/L1,2,4-Trichlorobenzene 70-130 1.5 20.0
23.2 11612224.320.0µg/L1,1,1-Trichloroethane 70-130 4.6 20.0
19.6 98.098.019.620.0µg/L1,1,2-Trichloroethane 70-130 0.0 20.0
21.5 10810520.920.0µg/LTrichloroethene 70-130 2.8 20.0
23.3 11711823.620.0µg/LTrichlorofluoromethane 60-140 1.2 20.0
20.4 10210621.120.0µg/L1,2,3-Trichloropropane 70-130 3.3 20.0
22.3 11211222.420.0µg/L1,2,4-Trimethylbenzene 70-130 0.4 20.0
22.3 11211523.020.0µg/L1,3,5-Trimethylbenzene 70-130 3.0 20.0
23.9 12014028.020.0µg/LVinyl Acetate 60-140 15.7 20.0
12.5 62.560.512.120.0µg/LVinyl Chloride 60-140 3.2 20.0
21.1 10610521.020.0µg/Lo-Xylene 70-130 0.4 20.0
46.0 11511345.040.0µg/Lm,p-Xylene 70-130 2.1 20.0
19.7 98.510120.220.0µg/L3,3-Dimethyl-1-butanol 70-130 2.5 20.0
92.892.24-Bromofluorobenzene (S)70-130
97.699.2Dibromofluoromethane (S)70-130
1041091,2-Dichloroethane - d4 (S)70-130
98.898.0Toluene-d8 (S)70-130
Page 6 of 12* QC Fail Date:10/03/2023 11:48 AM
Page 90 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
Associated Lab Samples: 95901, 95903, 95904, 95913
LRB-V38530 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 15:1610.01.80<1.80µg/LAcetone
09/28/23 15:160.5000.180<0.180µg/LBenzene
09/28/23 15:160.5000.210<0.210µg/LBromobenzene
09/28/23 15:161.000.420<0.420µg/LBromochloromethane
09/28/23 15:160.5000.160<0.160µg/LBromodichloromethane
09/28/23 15:165.001.50<1.50µg/LBromoform
09/28/23 15:161.000.280<0.280µg/LBromomethane
09/28/23 15:160.5000.180<0.180µg/Ln-Butylbenzene
09/28/23 15:160.5000.200<0.200µg/Lsec-Butyl benzene
09/28/23 15:162.000.920<0.920µg/Ltert-Butyl benzene
09/28/23 15:160.5000.180<0.180µg/LCarbon Tetrachloride
09/28/23 15:160.5000.190<0.190µg/LChlorobenzene
09/28/23 15:160.5000.190<0.190µg/LChlorodibromomethane
09/28/23 15:161.000.430<0.430µg/LChloroethane
09/28/23 15:160.5000.220<0.220µg/LChloroform
09/28/23 15:160.5000.220<0.220µg/LChloromethane
09/28/23 15:160.5000.200<0.200µg/L2-Chlorotoluene
09/28/23 15:160.5000.200<0.200µg/L4-Chlorotoluene
09/28/23 15:160.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/28/23 15:162.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/28/23 15:160.5000.200<0.200µg/L1,2-Dibromoethane
09/28/23 15:160.5000.230<0.230µg/LDibromomethane
09/28/23 15:160.5000.220<0.220µg/L1,2-Dichlorobenzene
09/28/23 15:160.5000.190<0.190µg/L1,3-Dichlorobenzene
09/28/23 15:160.5000.210<0.210µg/L1,4-Dichlorobenzene
09/28/23 15:165.001.20<1.20µg/LDichlorodifluoromethane
09/28/23 15:160.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 12Date:10/03/2023 11:48 AM
Page 91 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
Associated Lab Samples: 95901, 95903, 95904, 95913
LRB-V38530 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 15:160.5000.150<0.150µg/L1,2-Dichloroethane
09/28/23 15:160.5000.150<0.150µg/L1,1-Dichloroethene
09/28/23 15:160.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/28/23 15:160.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/28/23 15:160.5000.190<0.190µg/L1,2-Dichloropropane
09/28/23 15:160.5000.130<0.130µg/L1,3-Dichloropropane
09/28/23 15:162.000.210<0.210µg/L2,2-Dichloropropane
09/28/23 15:160.5000.200<0.200µg/L1,1-Dichloropropene
09/28/23 15:160.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/28/23 15:160.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/28/23 15:1620042.0<42.0µg/LEthanol
09/28/23 15:160.5000.170<0.170µg/LEthylbenzene
09/28/23 15:163.000.350<0.350µg/LHexachlorobutadiene
09/28/23 15:161.000.380<0.380µg/L2-Hexanone
09/28/23 15:160.5000.180<0.180µg/LIsopropylbenzene
09/28/23 15:160.5000.089<0.089µg/L4-Isopropyl toluene
09/28/23 15:165.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/28/23 15:161.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/28/23 15:161.000.078<0.078µg/L4-Methyl-2-Pentanone
09/28/23 15:162.000.330<0.330µg/LMethylene Chloride
09/28/23 15:161.000.470<0.470µg/LNaphthalene
09/28/23 15:160.5000.190<0.190µg/Ln-Propylbenzene
09/28/23 15:160.5000.220<0.220µg/LStyrene
09/28/23 15:1610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/28/23 15:1610.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/28/23 15:1610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/28/23 15:1610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 12Date:10/03/2023 11:48 AM
Page 92 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
Associated Lab Samples: 95901, 95903, 95904, 95913
LRB-V38530 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 15:160.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/28/23 15:160.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/28/23 15:160.5000.220<0.220µg/LTetrachloroethene
09/28/23 15:160.5000.220<0.220µg/LToluene
09/28/23 15:160.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/28/23 15:160.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/28/23 15:160.5000.160<0.160µg/L1,1,1-Trichloroethane
09/28/23 15:160.5000.096<0.096µg/L1,1,2-Trichloroethane
09/28/23 15:160.5000.180<0.180µg/LTrichloroethene
09/28/23 15:160.5000.180<0.180µg/LTrichlorofluoromethane
09/28/23 15:160.5000.270<0.270µg/L1,2,3-Trichloropropane
09/28/23 15:160.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/28/23 15:160.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/28/23 15:165.001.00<1.00µg/LVinyl Acetate
09/28/23 15:160.5000.170<0.170µg/LVinyl Chloride
09/28/23 15:160.5000.210<0.210µg/Lo-Xylene
09/28/23 15:161.000.420<0.420µg/Lm,p-Xylene
09/28/23 15:1610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/28/23 15:164-Bromofluorobenzene (S)90.4 70-130
09/28/23 15:16Dibromofluoromethane (S)100 70-130
09/28/23 15:161,2-Dichloroethane - d4 (S)108 70-130
09/28/23 15:16Toluene-d8 (S)90.2 70-130
Page 9 of 12Date:10/03/2023 11:48 AM
Page 93 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.8 10210843.040.0µg/LAcetone 40-160 5.2 20.0
18.5 92.592.018.420.0µg/LBenzene 70-130 0.5 20.0
20.0 10098.519.720.0µg/LBromobenzene 70-130 1.5 20.0
22.7 11411322.520.0µg/LBromochloromethane 70-130 0.8 20.0
21.5 10810721.420.0µg/LBromodichloromethane 70-130 0.4 20.0
25.4 12712725.420.0µg/LBromoform 70-130 0.0 20.0
18.0 90.090.518.120.0µg/LBromomethane 60-140 0.5 20.0
20.8 10410520.920.0µg/Ln-Butylbenzene 70-130 0.4 20.0
21.1 10610220.420.0µg/Lsec-Butyl benzene 70-130 3.3 20.0
22.4 11210821.620.0µg/Ltert-Butyl benzene 70-130 3.6 20.0
28.2 141*137*27.420.0µg/LCarbon Tetrachloride 70-130 2.8 20.0
21.7 10911122.120.0µg/LChlorobenzene 70-130 1.8 20.0
23.4 11711723.420.0µg/LChlorodibromomethane 70-130 0.0 20.0
12.3 61.564.512.920.0µg/LChloroethane 60-140 4.7 20.0
20.9 10510520.920.0µg/LChloroform 70-130 0.0 20.0
9.44 47.2*44.6*8.9320.0µg/LChloromethane 60-140 5.5 20.0
19.7 98.596.519.320.0µg/L2-Chlorotoluene 70-130 2.0 20.0
20.6 10398.019.620.0µg/L4-Chlorotoluene 70-130 4.9 20.0
13.5 67.5*67.5*13.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.0 20.0
25.9 13012725.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.3 20.0
19.7 98.510220.320.0µg/L1,2-Dibromoethane 70-130 3.0 20.0
21.9 11010120.220.0µg/LDibromomethane 70-130 8.0 20.0
22.9 11511222.420.0µg/L1,2-Dichlorobenzene 70-130 2.2 20.0
23.0 11511522.920.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
22.5 11310821.620.0µg/L1,4-Dichlorobenzene 70-130 4.0 20.0
9.80 49.0*49.6*9.9220.0µg/LDichlorodifluoromethane 60-140 1.2 20.0
Page 10 of 12Date:10/03/2023 11:48 AM
Page 94 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.9 89.588.017.620.0µg/L1,1-Dichloroethane 70-130 1.6 20.0
21.7 10910921.820.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
17.5 87.510120.220.0µg/L1,1-Dichloroethene 70-130 14.3 20.0
17.9 89.591.018.220.0µg/Lcis-1,2-Dichloroethene 70-130 1.6 20.0
19.4 97.092.518.520.0µg/Ltrans-1,2-Dichloroethene 70-130 4.7 20.0
14.8 74.074.514.920.0µg/L1,2-Dichloropropane 70-130 0.6 20.0
18.4 92.093.518.720.0µg/L1,3-Dichloropropane 70-130 1.6 20.0
25.4 12712925.720.0µg/L2,2-Dichloropropane 70-130 1.1 20.0
22.4 11210921.820.0µg/L1,1-Dichloropropene 70-130 2.7 20.0
19.2 96.099.519.920.0µg/Lcis-1,3-Dichloropropene 70-130 3.5 20.0
21.0 10510821.520.0µg/Ltrans-1,3-Dichloropropene 70-130 2.3 20.0
297 59.4*86.8434500µg/LEthanol 60-140 37.4*20.0
20.2 10199.519.920.0µg/LEthylbenzene 70-130 1.4 20.0
27.2 136*131*26.220.0µg/LHexachlorobutadiene 70-130 3.7 20.0
15.4 77.080.516.120.0µg/L2-Hexanone 60-140 4.4 20.0
22.4 11210721.420.0µg/LIsopropylbenzene 70-130 4.5 20.0
23.4 11711422.820.0µg/L4-Isopropyl toluene 70-130 2.5 20.0
15.7 78.581.516.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.7 20.0
20.7 10410521.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0
14.2 71.072.514.520.0µg/L4-Methyl-2-Pentanone 60-140 2.0 20.0
14.6 73.072.014.420.0µg/LMethylene Chloride 70-130 1.3 20.0
25.9 13012224.420.0µg/LNaphthalene 70-130 5.9 20.0
19.9 99.598.519.720.0µg/Ln-Propylbenzene 70-130 1.0 20.0
21.3 10710921.720.0µg/LStyrene 70-130 1.8 20.0
42.1 10510642.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.4 20.0
38.5 96.289.535.840.0µg/Ltert-Butyl formate (TBF)40-140 7.2 20.0
Page 11 of 12* QC Fail Date:10/03/2023 11:48 AM
Page 95 of 99
Quality Control Data
23-264-0032Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
16.2 81.096.519.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 17.4 20.0
38.9 97.298.739.540.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.5 20.0
24.5 12312124.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.6 20.0
17.6 88.083.516.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.2 20.0
24.5 12312124.220.0µg/LTetrachloroethene 70-130 1.2 20.0
19.7 98.596.519.320.0µg/LToluene 70-130 2.0 20.0
32.1 161*157*31.420.0µg/L1,2,3-Trichlorobenzene 70-130 2.2 20.0
29.2 146*144*28.720.0µg/L1,2,4-Trichlorobenzene 70-130 1.7 20.0
24.9 12512124.120.0µg/L1,1,1-Trichloroethane 70-130 3.2 20.0
19.3 96.597.519.520.0µg/L1,1,2-Trichloroethane 70-130 1.0 20.0
22.7 11411322.620.0µg/LTrichloroethene 70-130 0.4 20.0
23.6 11811923.720.0µg/LTrichlorofluoromethane 60-140 0.4 20.0
21.4 10710120.120.0µg/L1,2,3-Trichloropropane 70-130 6.2 20.0
22.4 11211122.120.0µg/L1,2,4-Trimethylbenzene 70-130 1.3 20.0
22.2 11111021.920.0µg/L1,3,5-Trimethylbenzene 70-130 1.3 20.0
25.7 12912725.420.0µg/LVinyl Acetate 60-140 1.1 20.0
10.6 53.0*54.0*10.820.0µg/LVinyl Chloride 60-140 1.8 20.0
21.0 10510320.520.0µg/Lo-Xylene 70-130 2.4 20.0
45.0 11311044.140.0µg/Lm,p-Xylene 70-130 2.0 20.0
18.1 90.596.019.220.0µg/L3,3-Dimethyl-1-butanol 70-130 5.8 20.0
91.090.64-Bromofluorobenzene (S)70-130
98.6102Dibromofluoromethane (S)70-130
1021061,2-Dichloroethane - d4 (S)70-130
96.296.2Toluene-d8 (S)70-130
Page 12 of 12* QC Fail Date:10/03/2023 11:48 AM
Page 96 of 99
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-264-0032
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Caitlyn Cummins Date & Time:09/21/2023 16:59:50
Special precautions or instructions included?
Comments:
Page 97 of 99
Page 98 of 99
Page 99 of 99

APPENDIX F
Contaminant Mass Calculations
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
05/03/17 30.50 0.55 1.10 7.40 5.60 0.24 45.39 40.33 4.67 3.57 ------
04/19/18 0.16 0.89 0.00 0.64 0.00 0.00 1.69 38.81 6.19 0.18 95.1%95.1%
08/13/18 11.80 0.25 0.32 1.80 5.40 0.15 19.72 37.36 7.64 2.54 -1340.2%28.9%
10/15/18 13.90 0.29 0.30 2.50 5.40 0.19 22.58 37.06 7.94 3.02 -19.0%15.4%
01/22/19 22.60 0.92 0.38 12.30 4.70 0.17 41.07 35.28 9.72 6.73 -122.7%-88.3%
04/08/19 41.20 1.60 0.68 7.10 4.40 0.00 54.98 33.43 11.57 10.72 -59.3%-200.1%
07/29/19 1.50 0.46 0.00 3.90 4.40 0.15 10.41 32.71 12.29 2.16 79.9%39.6%
10/08/19 5.10 0.36 0.00 2.50 5.10 0.17 13.23 34.08 10.92 2.43 -12.9%31.8%
01/02/20 0.42 0.00 0.00 1.60 4.40 0.19 6.61 35.07 9.93 1.11 54.6%69.0%
10/13/20 0.75 0.50 0.00 2.00 3.60 0.00 6.85 31.29 13.71 1.58 -43.1%55.7%
04/08/21 0.23 0.17 0.00 1.50 3.00 0.00 4.90 29.97 15.03 1.24 21.6%65.3%
10/20/21 0.84 0.23 0.00 2.20 5.70 0.53 9.50 33.90 11.10 1.78 -43.2%50.3%
04/05/22 0.32 0.23 0.00 0.44 4.9 0.22 6.11 36.53 8.47 0.87 50.9%75.6%
04/04/23 0.00 0.00 0.00 1.29 2.37 0.00 3.66 34.20 10.80 0.67 23.6%81.4%
09/20/23 0.212 0.00 0.00 2.06 3.18 12.7 18.15 35.47 9.53 2.91 -337.6%18.4%
05/03/17 12100.00 38500.00 3570.00 21200.00 9720.00 1300.00 86390.00 40.91 11.59 36954.63 ------
04/19/18 12100.00 43400.00 4900.00 28200.00 11800.00 1590.00 101990.00 39.04 13.46 50666.92 -37.1%-37.1%
08/13/18 FP FP FP FP FP FP FP FP NA FP ------
10/15/18 FP FP FP FP FP FP FP FP NA FP ------
01/22/19 FP FP FP FP FP FP FP FP NA FP ------
04/08/19 FP FP FP FP FP FP FP FP NA FP ------
07/29/19 FP FP FP FP FP FP FP FP NA FP ------
10/08/19 7380.00 40000.00 4060.00 21400.00 5110.00 1020.00 78970.00 34.81 17.69 51559.88 -1.8%-39.5%
01/02/20 FP FP FP FP FP FP FP FP NA FP ------
10/13/20 6520.00 44500.00 4140.00 24700.00 2460.00 1520.00 83840.00 32.05 20.45 63280.00 -22.7%-71.2%
04/08/21 4090.00 27200.00 2800.00 21300.00 3610.00 1740.00 60740.00 29.02 23.48 52637.44 16.8%-42.4%
10/20/21 722.00 6220.00 1180.00 9310.00 1490.00 1390.00 20312.00 34.81 17.69 13261.80 74.8%64.1%
04/05/22 6,930 30,300 2,490 19,300 1,030 1,860 61910.00 37.02 15.48 35371.51 -166.7%4.3%
04/04/23 2,270 17,300 2,670 17,500 1,270 1,470 42480.00 41.79 10.71 16791.75 52.5%54.6%
09/20/23 1,620 22,700 3,320 22,100 526 1,820 52086.00 36.10 16.40 31527.30 -87.8%14.7%
Area 1 MW-4
OW-2Area 2
APPENDIX F
CHANGE IN CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
Page 1 of 4
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
APPENDIX F
CHANGE IN CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
05/03/17 7060.00 21800.00 2610.00 18100.00 486.00 913.00 50969.00 41.46 11.04 13116.70 ------
04/19/18 6400.00 22500.00 2700.00 15100.00 583.00 750.00 48033.00 39.53 12.97 14522.09 -10.7%-10.7%
08/13/18 5410.00 25600.00 3020.00 19300.00 231.00 875.00 54436.00 38.35 14.15 17955.28 -23.6%-36.9%
10/15/18 4570.00 24800.00 2710.00 18100.00 184.00 913.00 51277.00 37.26 15.24 18216.17 -1.5%-38.9%
01/22/19 1970.00 16300.00 2280.00 16900.00 33.60 1040.00 38523.60 34.10 18.40 16523.20 9.3%-26.0%
04/08/19 1610.00 20400.00 2800.00 20700.00 0.00 776.00 46286.00 34.55 17.95 19367.06 -17.2%-47.7%
07/29/19 3040.00 24600.00 3220.00 18900.00 110.00 761.00 50631.00 32.91 19.59 23120.67 -19.4%-76.3%
10/08/19 3120.00 22800.00 3240.00 17600.00 227.00 859.00 47846.00 35.44 17.06 19027.17 17.7%-45.1%
01/02/20 2340.00 23300.00 3330.00 23400.00 153.00 862.00 53385.00 35.53 16.97 21117.89 -11.0%-61.0%
10/13/20 1130.00 3800.00 315.00 2140.00 306.00 221.00 7912.00 35.53 16.97 3129.81 85.2%76.1%
04/08/21 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 30.12 22.38 2303.25 26.4%82.4%
10/20/21 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 35.61 16.89 1738.24 24.5%86.7%
04/05/22 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 37.16 15.34 1578.72 9.2%88.0%
04/04/23 28.9 27.0 21.0 796 48.1 59.2 980.20 34.26 18.24 416.76 73.6%96.8%
09/20/23 NS NS NS NS NS NS 980.20 36.45 16.05 366.72 12.0%97.2%
MW-1R 1380.00 12800.00 1700.00 13200.00 330.00 1060.00 30470.00 40.72
MW-8 182.00 499.00 130.00 477.00 0.00 28.40 1316.40 41.35
Avg.781.00 6649.50 915.00 6838.50 165.00 544.20 15893.20 41.04
MW-1R 1740.00 14600.00 1360.00 14000.00 255.00 992.00 32947.00 38.38
MW-8 206.00 531.00 164.00 604.00 0.00 13.80 1518.80 39.49
Avg.973.00 7565.50 762.00 7302.00 127.50 502.90 17232.90 38.94
MW-1R 1420.00 11200.00 1090.00 11500.00 448.00 1150.00 26808.00 36.93
MW-8 122.00 301.00 98.60 365.00 0.00 25.40 912.00 37.40
Avg.771.00 5750.50 594.30 5932.50 224.00 587.70 13860.00 37.17
MW-1R 1510.00 13000.00 1460.00 12200.00 553.00 1500.00 30223.00 36.23
MW-8 167.00 363.00 92.60 224.00 0.00 6.60 853.20 36.90
Avg.838.50 6681.50 776.30 6212.00 276.50 753.30 15538.10 36.57
MW-1R 742.00 11700.00 1440.00 12500.00 748.00 904.00 28034.00 32.60
MW-8 147.00 522.00 232.00 1120.00 0.00 82.50 2103.50 33.63
Avg.444.50 6111.00 836.00 6810.00 374.00 493.25 15068.75 33.12
MW-1R 332.00 10900.00 1660.00 14300.00 259.00 667.00 28118.00 31.72
MW-8 128.00 416.00 180.00 802.00 0.00 56.00 1582.00 32.32
Avg.230.00 5658.00 920.00 7551.00 129.50 361.50 14850.00 32.02
MW-1R 655.00 15600.00 1920.00 13100.00 403.00 720.00 32398.00 31.72
MW-8 8.40 11.50 4.70 12.10 0.00 1.10 37.80 32.68
Avg.331.70 7805.75 962.35 6556.05 201.50 360.55 16217.90 32.20
OW-1Area 3
07/29/19 7952.68 -8.2% -84.3%
8.7%-18.0%
7047.71 -18.7% -63.3%
5939.61
08/13/18
01/22/19
-4.3%
-16.6%
18.89
7348.1119.98
19.80
5092.1914.84
15.44
-70.3%
--- ---
5575.98 -29.2% -29.2%
10.97
13.0704/19/18
05/03/17 4315.92
Area 4 10/15/18
04/08/19
-37.6%
Page 2 of 4
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
APPENDIX F
CHANGE IN CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
MW-1R 1050.00 17600.00 2250.00 13500.00 352.00 1080.00 35832.00 34.25
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 49.52
Avg.525.00 8800.00 1125.00 6750.00 176.00 540.00 17916.00 41.89
MW-1R 154.00 3740.00 430.00 5990.00 96.70 381.00 10791.70 34.21
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 35.40
Avg.77.00 1870.00 215.00 2995.00 48.35 190.50 5395.85 34.81
MW-1R 38.50 935.00 107.50 1497.50 24.18 95.25 2697.93 29.55
MW-8 57.75 1402.50 161.25 2246.25 36.26 142.88 4046.89 30.66
Avg.48.13 1168.75 134.38 1871.88 30.22 119.06 3372.41 30.11
MW-1R 58.40 610.00 55.90 2390.00 365.00 50.70 3530.00 28.78
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 29.64
Avg.29.20 305.00 27.95 1195.00 182.50 25.35 1765.00 29.21
MW-1R 16.10 100.00 11.70 90.50 286.00 3.10 507.40 34.18
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 49.70
Avg.8.05 50.00 5.85 45.25 143.00 1.55 253.70 41.94
MW-1R 128 1,930 176 2,190 682 107 5213.00 36.81
MW-8 0.00 0.34 0.00 0.59 0.00 0.00 0.93 37.63
Avg.64.00 965.17 88.00 1095.30 341.00 53.50 2606.97 37.22
MW-1R 8.77 140 24.4 507 181 63.4 924.57 33.60
MW-8 NM NM NM NM NM NM NM NM
Avg.8.77 140.00 24.40 507.00 181.00 63.40 924.57 33.60
MW-1R 10.2 134 47.8 401 166 96.5 855.50 35.94
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 36.65
Avg.5.10 67.00 23.90 200.50 83.00 48.25 427.75 36.30
09/20/23
Area 4
(cont.)
421.32 55.8% 90.2%
04/05/22 -1409.7%
10/13/20
01/02/20
21.90 1828.68
04/08/21
98.5%93.7%63.2110.06
48.8% 46.8%2297.82
20.4%
04/04/23 18.40
10/20/21
57.6%
17.20
-4.0%4488.08 43.6%10/08/19 10.12
22.79 996.19 45.5% 76.9%
77.9%14.78 954.25
96.1%60.5%166.3715.71
Page 3 of 4
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
APPENDIX F
CHANGE IN CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
Date Average Water
Column Height (ft)
05/03/17 9.57
04/19/18 11.42
08/13/18 12.21
10/15/18 12.87
01/22/19 15.67
04/08/19 16.50
07/29/19 17.23
10/08/19 13.95
01/02/20 14.70
10/13/20 18.26
04/08/21 20.92
10/20/21 13.94
04/05/22 13.52
04/04/23 14.54
09/20/23 14.42
Note:
• In areas containing free product, the last known contaminant mass without free product is used to calculate the total contaminant mass calculations.
• The air sparging wells have not been included in the total contaminant mass calculations due to the inability to sample the air sparging wells during future ground water sampling events.
• The telescoping wells have not been included in the total contaminant mass calculations due to the inability to calucate a volume.
• The percentage reduction for areas containing free product cannot be caluclated.
67.6%53.5%17,630
-42.3%
74,826
74,245
77,393
-37.6%
-5.6% -50.3%
37,905 -151.6%30.3%
-25.5%9.0%
55,938
41.1%32,063 15.4%
15,065 73.1% 72.3%
Total Contaminant Mass
(grams)Percent Reduction Compared to
Previous Event
Percent Reduction To Date
54,391
70,765
18.0%-2.8%
68,240
74,977
8.2%-38.0%
0.1%
-35.5%
-1.5%
-4.2%
-37.8%
75,078
--- ---
-30.1% -30.1%
81,742
-4.2%
0.8%-36.5%
73,717
Page 4 of 4