8002_Rowan_NeedmoreRoad_CelaneseFibers_Indus_CAER_FID1822747_20231214

A=COM
2023 Corrective Action
Evaluation Report
Needmore Road Landfill
Woodleaf, North Carolina
CNA Holdings LLC.
Project number: 60683034
November 2023
Delivering a better world

Corrective Action Evaluation Report
Project Number: 60683034
Quality information
Prepared by
Jing Zhou, Ph.D., PE
Project Engineer
Distribution List
# Hard Copies PDF Required
Verified by
M. Evelyn Rogers
Program Director
Association / Company Name
Approved by
Mark Hartford, P.G.
Senior Project Manager
0 Electronic file North Carolina Department of Environment Quality, Attn: Jaclynne Drummond
0 Electronic file CNA Holdings LLC, Attn: Michael Simpson
Prepared for:
CNA Holdings LLC
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Prepared by:
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LpENR USE ONLY: ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No ) _ Doc/Event #:
N DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc ).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section. 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
AECOM Technical Services of North Carolina, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jing Zhou Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name. Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006)
Needmore Road Landfill 345 Messick Farm Road, Woodleaf, NC 80-02 .0500 May 16, 2022 and November
28144 1-2, 2022
L I
Environmental Status: (Check all that apply)
Initia!/Background Monitoring ❑ Detection Monitoring Assessment Monitoring ❑X Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells
Leachate monitoring data Surface water monitoring data X
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Intermittent Seep
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
El Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates. sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Hartford, Mark Geologist 864-234-3000
Facility Representative Name (Print) Title (Area Code) Telephone Number
Hartford Mark Digitally signed by Hartford, Mark 12/11/2023 Affix NC Licensed/ Professional Geologist Seal
Date: 2023.12.11 12:14:24-05'00'
Signature Date
10 Patewood Drive, Building 6, Suite 500, Greenville, SC 29615
Facility Representative Address
F-0342
NC PE Firm License Number (if applicable effective May 1, 2009)
Pa%ii ,i mmnno

Corrective Action Evaluation Report
Project Number: 60683034
Table of Contents
1. Introduction................................................................................................................................. 7
1.1 Site Background and History.............................................................................................
7
1.2 Contaminant Distribution...................................................................................................
8
1.3 Site Conceptual Model and Site Risk Assessment............................................................
9
1.3.1 Site Conceptual Model...........................................................................................
9
1.3.2 Risk Assessment....................................................................................................
9
1.4 Regulatory Status............................................................................................................
10
2. Correction Action Summary .....................................................................................................11
2.1 Phytoremediation Activities...............................................................................................11
2.1.1 Initial Tree Planting (2005)....................................................................................11
2.1.2 2007 Tree Replanting............................................................................................11
2.1.3 2012 Tree Replanting...........................................................................................
12
2.1.4 2020 Tree Replanting...........................................................................................
12
2.2 MNAActivities..................................................................................................................12
2.3 Physical and Chemical Changes in Aquifer Conditions and Plume Characteristics.........
12
2.3.1 Ethylene Glycol....................................................................................................
12
2.3.2 1,4-Dioxane..........................................................................................................
13
2.3.3 1,1-Biphenyl and Diphenyl Ether..........................................................................
13
2.3.4 MINA Parameters..................................................................................................
13
2.4 Surface Water and Intermittent Seep...............................................................................
14
2.4.1 Surface Water......................................................................................................
14
2.4.2 Intermittent Seep..................................................................................................
14
3. Conclusion................................................................................................................................
15
4. References................................................................................................................................
16
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Corrective Action Evaluation Report
Project Number: 60683034
Tables
Table 1
May Groundwater and Surface Water Sampling Plan
Table 2
November Groundwater and Surface Water Sampling Plan
Table 3
Groundwater Elevations
Table 4
Groundwater Analytical Summary
Table 5
Surface Water Analytical Summary
Table 6
Intermittent Seep Water Analytical Summary
Table 7
Summary of Detected Constituents in Groundwater
Table 8
Time vs. Concentration Plots — Ethylene Glycol
Table 9
Time vs. Concentration Plots — 1,4-Dioxane
Table 10
Time vs. Concentration Plots — Diphenyl Ether
Figures
Figure 1
Site Location Map
Figure 2
Site Layout Map
Figure 3
Sample Location Map — May 2022
Figure 4
Sample Location Map — November 2022
Figure 5
Groundwater Potentiometric Surface Map — November 2022
Figure 6
1,4-Dioxane Isoconcentration Map — November 2022
Figure 7
1,1-Biphenyl Isoconcentration Map — November 2022
Figure 8
Diphenyl Ether Isoconcentration Map — November 2022
Appendices
Appendix A Sample Field Sampling Forms
Appendix B Sample Chain of Custody Records
Appendix C Well Location Map
Appendix D Field Notes — May 2022 and November 2022
Appendix E Laborotory Reports — May 2022 and November 2022
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Corrective Action Evaluation Report
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Acronyms
bgs
below ground surface
CAER
Corrective Action Evaluation Report
CAP
Corrective Action Plan
COCs
contaminants of concern
DO
dissolved oxygen
ERA
ecological risk assessment
Ft/day
foot per day
Ft/yr
foot per year
HCC
Hoechst Celanese Corporation
HHRA
Human Health Risk Assessment
mg/L
milligrams per liter
MNA
monitored natural attenuation
my
millivolts
NC 2L
North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDEQ
North Carolina Department of Environmental Quality
NPDES
National Polluant Discharge Elimination System
NRLF
Needmore Road Landfill
ORP
oxidation-reduction potential
TEA
terminal electron acceptor
USEPA
United States Environmental Protection Agency
AECOM
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Corrective Action Evaluation Report
Project Number: 60683034
1. Introduction
This Corrective Action Evaluation Report (CAER) provides performance evaluation of the corrective actions
conducted at the Needmore Road Landfill Facility (NRLF) site in Woodleaf, North Carolina. The Corrective Action
Plan (CAP) was submitted in November 2007. This CAER is prepared in accordance with the requirement and
guidance provided by North Carolina Department of Environment Quality (NCDEQ) Division of Waste Management.
1.1 Site Background and History
The NRLF site, located at 345 Messick Farm Road, Woodleaf, Rowan County, North Carolina, was used until 1990 to
dispose of by-products of polyester resin manufacturing from the former Hoechst Celanese plant located on U.S.
Route 70 near Salisbury, North Carolina. These by-products primarily included waste materials containing ethylene
glycol with some other impurities, including 1,4-dioxane, 1,1-biphenyl, and diphenyl ether. There were four main
disposal areas at this site, and they were referred to as Taylor's Pit (0.6 acre), the 14-Acre Site, the 16-Acre Site, and
the Secondary Site (2.6 acres). Taylor's Pit was consolidated into the main part of the landfill prior to final landfill
closure. The site consists of an approximately 243-acre tract of land that is bounded by the South Yadkin River to the
east. The current NCDEQ status of the site is "closed." A site location map is included as Figure 1, and a site layout
map is included as Figure 2.
The landfill lies within the central portion of the Charlotte Metamorphic Belt of the Piedmont Physiographic Province.
Bedrock in this area is composed of a complex series of meta -sedimentary, meta -volcanic, and igneous intrusive rock
types. This geologic matrix has undergone repeated cycles of folding, faulting, metamorphism, and intrusions, which
have resulted in regional northeasterly strike and southeasterly dip directions.
A basic understanding of the geology at the landfill was established during several phases of work, during which
numerous monitoring and extraction wells were installed. Based on an evaluation of the subsurface boring logs, the
site is underlain by diorite, gabbro, and granite bedrock. Some localized gneissic and schistose metamorphism was
noted in several of the borings drilled at the site. These profiles are generally well -weathered and occur in the zone
above the competent rock. From land surface down, the geology of the site is divided into three distinct strata,
including residuum, saprolite, and bedrock. The individual strata vary in thickness and occurrence across the site.
Residuum is encountered from ground surface to approximately 30 feet below ground surface (bgs) and has been
described as a tan to red -brown, micaceous clayey, fine sandy silt. The saprolite at the site can be divided into three
zones saprolite (thickness of 5-35 feet), transition zone (thickness of 15-50 feet), and partially weathered bedrock
(thickness of 40-50 feet).
Groundwater flows predominantly to the northeast towards the South Yadkin River. The estimated hydraulic
conductivities in saprolite/transition zone and bedrock zone are 0.6 — 1.23 feet per day (ft/day). The horizontal
hydraulic gradient in the saprolite unit was estimated at 0.05 feet per foot (ft/ft) and the average hydraulic gradient in
the bedrock was estimated at 0.03 ft/ft. The calculated average groundwater flow velocity is 112 feet per year (ft/yr)
for the shallow groundwater and 134 ft/yr through the deeper groundwater (AECOM, 2007).
Historic remedial activities before the CAP implementation at the landfill include the installation of an impermeable
cover on the landfill, regrading of the surface of the landfill (to improve surface water drainage), and the installation of
groundwater extraction wells. Groundwater was extracted and treated by a UV/peroxide oxidation process and
discharged under a National Pollutant Discharge Elimination System (NPDES) permit. Groundwater extraction was
suspended in June 2002 with NCDEQ approval. In 2004, modifications were made to the drainage system and a
phytoremediation system was initiated to address seepage at the toe of the landfill. The phytoremediation system is
positioned downgradient of the landfill face and upgradient of the intermittent seep location (Figure 2).
Groundwater monitoring data in the reports submitted semiannually from November 2004 through 2007
demonstrated that the groundwater impact had been generally contained and was not expanding. As such, a final
CAP was established in 2007 defining the site remedy as a combination of monitored natural attenuation (MNA) and
phytoremediation. Subsequent monitoring events have reported similarly successful results.
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Corrective Action Evaluation Report
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Groundwater monitoring, surface water monitoring, intermittent seep monitoring, and regular inspections of the
phytoremediation system and landfill cap have been conducted at the site in accordance with the schedule in the
CAP, which was revised in early 2009.
Because concentrations of the primary contaminants of concern (COCs) at the site generally remained stable from
2007 through 2013, indicating that the MNA and phytoremediation systems were effective as designed, AECOM
recommended in the semiannual report submitted to NCDEQ in May 2014 that the monitoring continue to be
conducted semiannually in May and November each year and that the reporting frequency be reduced from
semiannual to annual (AECOM 2014). The NCDEQ approved the reduction of the reporting frequency in a letter
dated September 10, 2014, and an annual site report has been submitted each year since May 2015.
1.2 Contaminant Distribution
The NRLF was used in the past to dispose of plant trash, off -spec fiber, and other wastes and by-products of
polyester resin manufacturing from the Hoechst Celanese Corporation (HCC) plant located near Salisbury, North
Carolina. These by-products primarily included waste materials containing ethylene glycol, 1,4-dioxane, 1,1-biphenyl,
and diphenyl ether. These four constituents are the primary COCs at the site as confirmed by previous investigations
and subsequent periodic groundwater monitoring.
Ethylene glycol was historically detected at concentrations greater than the North Carolina Administrative Code, Title
15A, Subchapter 2L (NC 2L) standard of 14 milligrams per liter (mg/L) in samples collected from six groundwater
monitoring wells: B-01, B-09C, B-10, B-23A, B-23B, and B-32B (AECOM 2007). These wells are located in the main
disposal areas and downgradient of those areas. After June 2004, ethylene glycol was periodically detected at these
six locations, however, its concentrations have been below the analytical reporting limits in all wells sampled since
2019.
The findings over the years confirm the natural attenuation of ethylene glycol. Historical results are interpreted to
indicate that the landfill cap has significantly reduced or eliminated the transport of contaminants from the landfill into
groundwater. Contaminants that had entered the groundwater prior to the installation of the cap are being degraded
or attenuated.
1,4-Dioxane was historically detected in wells near each of the four former disposal sites and the NC 2L standard of
0.003 mg/L was exceeded at all wells in which 1,4-dioxane was detected. The highest 1,4-dioxane concentrations
were detected in samples collected from monitoring well B-01; however, 1,4-dioxane concentrations at this location
have remained generally stable since the treatment system was deactivated in 2002 and remain significantly lower
than the results detected in the mid-1990s. A similar pattern is observed for most other wells with no clear trend
observed in the years since the treatment system was deactivated (AECOM 2007).
Since 2004, 1,1-biphenyl was detected only in samples collected from monitoring well B-10. The 1,1-biphenyl
concentrations detected at B-10 have been below the NC 2L standard (0.4 mg/L) during all the sampling events since
2004, with the exception of the 2008 sample in which the 1,1-biphenyl concentration detected (0.405 mg/L) slightly
exceeded the NC 2L standard.
Diphenyl ether has been historically detected at several wells located near the former disposal sites and at the
downgradient wells. The highest concentrations have been detected in samples collected from monitoring well B-10.
Diphenyl ether concentrations in well B-10 have exceeded the NC 2L standard (0.18 mg/L) in most sampling events
since 2004.
1,1-Biphenyl and diphenyl ether have not been detected in surface water samples. 1,4-Dioxane was detected only
once in surface water samples in 2016 and remains non -detectable since 2016. Ethylene glycol was only detected
once in 2017 and remains non -detectable since 2017.
1,4-Dioxane was detected in intermittent seep samples with concentrations ranging from 0.01 mg/L to 0.67 mg/L.
Other COCs have not been detected in intermittent seep samples.
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Corrective Action Evaluation Report
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1.3 Site Conceptual Model and Site Risk Assessment
A site conceptual model was developed as part of the baseline human health risk assessment (HHRA) and
screening -level ecological risk assessment (ERA) conducted for the site in September 2005 (ARCADIS, 2005). The
summary of findings from the site conceptual model and risk assessments, in addition to the identification of exposure
and sensitive receptor pathways, is presented in the following sections.
1.3.1 Site Conceptual Model
Due to the substantial topographic relief on the site, groundwater in the upland areas is relatively deep and provides
recharge to the lower areas of the site. In the topographically lower areas, groundwater becomes shallower near
Beaverdam Branch and the South Yadkin River, and these areas represent discharge zones for the upland areas,
with groundwater ultimately discharging to the South Yadkin River The historic landfill operation was to place waste
first in the valley that headed up on the site in the 16-Acre Site and in trenches excavated into the native soils in the
other areas. Subsequent precipitation that fell on the open to partially closed landfill areas infiltrated the waste and
leached soluble components from the waste. This process went on at varying degrees of intensity from the time the
wastes were placed in the cells until the waste in the Taylor's Pit Site was consolidated back into the main landfill
area and the geomembrane cap was placed over the 16-Acre and 14-Acre Sites and the Secondary Source in 1996.
After placement of the geomembrane cap, the wastes are interpreted to have continued to drain for some period of
time then the leaching essentially ceased and the waste flux to the groundwater generally stopped.
The waste constituents that leached to the groundwater were distributed through the existing flow field migrating from
where they entered the groundwater system to discharge in the lower areas adjacent to Beaverdam Branch or the
South Yadkin River with the extent of impact being controlled by the quantity of the chemicals in the waste, water
solubility of the chemical, and attenuation potential. The data have shown that in the initial monitoring ethylene glycol
was the primary contaminant along with 1,4-dioxane and the components of DowTherm ATM (1,1-biphenyl and
diphenyl ether). Over the years, the frequency of detection of ethylene glycol decreased as the landfill drained to field
capacity and the ethylene glycol in the groundwater attenuated via biodegradation by the indigenous microorganisms
present and by the mechanical process of advection, dispersion and dilution. This degradation had resulted in the
anaerobic (reducing) groundwater conditions present beneath and downgradient of the landfill. Ethylene glycol has
only been detected sporadically since June 2004 and has not been detected above the NC 2L standard since 2019.
DowTherm ATM is comprised of approximately 26% 1,1-biphenyl and approximately 74% diphenyl ether. 1,1-Biphenyl
and diphenyl ether are aerobically biodegradable with 1,1-biphenyl being more degradable than diphenyl ether. Since
the landfill area is generally anaerobic due to the degradation of the ethylene glycol, these compounds are generally
more persistent that they would be in an aerobic environment, though both have seen significant degradation since
monitoring began. Due to its lower biodegradation potential and greater initial proportion, the diphenyl ether is
generally more widespread than the 1,1-biphenyl with recent detections of 1,1-biphenyl limited to one (1) well (B-10)
and detections of diphenyl ether to four (4) wells (B-10, B-22B, B-23B, and B-24A). 1,1-biphenyl has not been
detected above the 2L since 2008 and diphenyl ether only exceeds the 2L in one (1) well (B-10).
1,4-Dioxane is more recalcitrant and more mobile than 1,1-biphenyl and diphenyl ether and is the most wide -spread
COC on the site. Data gathered from several sites in similar geologic settings have shown that 1,4-dioxane
attenuates at a rate higher than can be attributed simply to the mechanical components of advection, dispersion, and
dilution, and thus is considered slightly biodegradable. Because it is miscible and generally recalcitrant, it provides a
good tracer to document the direction of groundwater flow and the extent of groundwater impact. At this site, 1,4-
dioxane is known to be a by-product of the polymer production and a component of the waste disposed in the landfill.
Thus, as precipitation infiltrated the waste 1,4-dioxane was leached from the waste and migrated laterally and
vertically in the groundwater to document the area of groundwater impact from the landfill operations between the
source and the discharge areas represented by Beaverdam Branch and the South Yadkin River (AECOM 2007).
1.3.2 Risk Assessment
Of the pathways presented in the model, groundwater discharge to surface water is the primary focus. The primary
pathway for COC migration is leaching from the landfill material. This pathway is controlled by the existence and
ongoing maintenance of the landfill cap. During the extreme drought conditions observed in 2002, samples were
collected from the Yadkin River. 1,4-Dioance was not detected (<0.005 mg/L) in weekly samples collected during the
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Corrective Action Evaluation Report
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low flow period. These results indicate that the discharge pathway to the river is not complete to the measured level
(<0.005 mg/L).
Analysis of the groundwater seep samples collected after the deactivation of the extraction system indicated that the
exposure pathway was complete in this area. 1,4-Dioxane was detected in samples collected from this seep at
concentrations ranging from 0.0557 mg/L to 0.893 mg/L. The phytoremediation program was instituted in 2004 to
address this pathway and to date has been effective in reducing 1,4-dioxane concentrations in seep.
Potential exposures to COCs in groundwater, surface water, and sediment at and in the vicinity of the site were
evaluated. The exposure scenarios quantitatively evaluated included potable use of the groundwater and surface
water by hypothetical future residents and commercial workers, incidental exposure to groundwater by hypothetical
future excavation workers, and exposure to sediments by a recreational receptor in the South Yadkin River,
Beaverdam Branch, and the seep. Detected concentrations from data collected prior to 2005 were used to estimate
risks and hazards. The methods used and scenarios evaluated were considered to be representative of worst -case
conditions (ARCADIS, 2005).
The cumulative total site risks and hazards for each human receptor (adult resident, commercial site worker,
excavation worker, and youth wader) were calculated. The results indicated that the excess lifetime cancer risks were
all within the United States Environmental Protection Agency (USEPA) target risk range of 10-4 to 10-6. The non -
cancer hazards were less than the benchmark of 1 for the excavation worker and wading youth. Residential exposure
to groundwater posed a non -cancer hazard exceeding the benchmark of 1 for the potable use exposure pathway, but
not for the inhalation of vapors migrating into a home exposure scenario. Site worker exposure to groundwater when
used as a potable water supply also yielded a non -cancer hazard index slightly greater than the benchmark of 1.
Exposure to groundwater does not occur under current conditions nor is it expected to occur in the future. The landfill
is not in use and no drinking water wells are present on the site. Although a groundwater extraction system remains
at the site, it has not been operated since 2002 and no potable wells are present on the site. As a result, although
these potential hazards based on potable use exist, there is not a current threat to human health (ARCADIS, 2005).
The screening -level ecological risk assessment (ERA) was based on consideration of constituent concentrations in
surface water and sediment compared to surface water and sediment quality thresholds considered protective of
aquatic wildlife. Surface water and sediment sampling locations were selected to identify the maximum potential
concentrations of constituents for use in the risk assessments; thereby, potentially representing the worst -case
scenario.
The screening -level ERA indicated that ecological risk is not a concern for groundwater discharges from the NRLF to
the South Yadkin River or Beaverdam Branch. Therefore, no further actions are warranted on the basis of ecological
risk (ARCADIS, 2005).
1.4 Regulatory Status
The current NCDEQ status of the landfill is "closed." Semiannual monitoring of groundwater and surface water is
conducted at the site.
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Corrective Action Evaluation Report
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2. Correction Action Summary
This section summarizes the corrective actions that have been conducted at the site since 2005, physical
and chemical changes in aquifer and plume, and evaluation of the effectiveness of the corrective actions.
In the 2007 CAP, a combination of MNA and phytoremediation was selected as the site remedy to
address the impact of site COCs on groundwater. MNA and phytoremediation have then been conducted
at the site since 2007, including following activities:
• Continued ongoing maintenance and monthly inspection of the landfill cap;
• Continued ongoing maintenance and inspection of the phytoremediation system;
• Semiannual MNA groundwater sampling and analyses in May and November every year, and
• Semiannual reporting from 2007 to 2014, and annual reporting since 2015.
The May semiannual sampling plan and the November semiannual sampling plan are provided in Table 1
and Table 2, respectively, and the May and November sampling locations are shown on Figure 3 and
Figure 4, respectively. Groundwater elevation data in the most recent reporting year (2022) are
summarized in Table 3, and the groundwater potentiometric surface map for November 2022 is provided
in Figure 5. Analytical results of groundwater samples, surface water samples and intermittent seep
samples collected in 2022 are provided in Table 4, Table 5, and Table 6, respectively. November 2022
isoconcentration maps for 1,4-dioxane, 1,1-biphenyl, and diphenyl ether are shown on Figure 6, Figure
7, and Figure 8, respectively. Ethylene glycol concentrations in 2022 were all below the reporting limits,
therefore, an isoconcentration map for ethylene glycol was not prepared. Historical analytical data for
ethylene glycol, 1,4-dioxane, 1,1-biphenyl, and diphenyl ether from 2004 to 2022 are provided in Table 7.
Sample field sampling form and chain of custody records are provided in Appendix A and Appendix B,
respectively. Well location map is included in Appendix C. Field notes and laboratory reports for the May
2022 and November 2022 sampling events are included in Appendix D and Appendix E, respectively.
2.1 Phytoremediation Activities
Phytoremediation was initiated at the stie in 2005. Subsequent tree replanting activities were conducted
in 2007, 2012 and 2020. Monthly maintenance and inspection of the phytoremediation system has been
conducted since 2007.
2.1.1 Initial Tree Planting (2005)
An area approximately 8,000 square feet in size located at the toe of the landfill was selected for
phytoremediation (Figure 2). With the assistance of Ecolotree°, an EBufferO (engineered forest) was
installed at the site on December 6, 2005. The EBufferO is designed to grow a dense, healthy root zone or
11rhizosphere" that removes water from the existing soils and provides uptake of 1,4-dioxane. This
EBuffer° consisted of 106 13- to 14-foot, rooted DN-34 and DN-21 hybrid poplars. These varieties of
hybrid poplars have proven survival and growth rates when planted in soils containing organic solvents
(AECOM 2007).
2.1.2 2007 Tree Replanting
Following installation, the EBuffer° site continued to stabilize throughout 2006. A strong survival rate was
demonstrated among 65% of the rooted trees planted in December 2005. This was especially evident in
the fertile upland area. The remaining 35% of the area showed lower survival rates. The lack of
establishment was primarily attributed to ponding of surface water, leading to hypoxia of the tree roots. In
April 2007, 46 additional hybrid poplar trees and 52 insurance cuttings were planted at the site. A tree
survival growth audit was performed during this same visit by Ecolotree° personnel with oversight from
Earth Tech. A second tree survival growth audit was performed in August 2007which indicated that 61 % of
the trees showed good growth, 24% showed established or limited growth, and 15 % were dead or dying
(AECOM 2007).
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Corrective Action Evaluation Report
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2.1.3 2012 Tree Replanting
In early May 2011, a storm caused significant damage to approximately twelve trees. A site inspection by
EcolotreeO, Celanese and AECOM was conducted on October 25, 2011. During this site visit it was noted
that some of the remaining trees had been damaged by insects or wildlife.
In March and April 2012, routine maintenance activities of pruning and felling of existing trees and
replanting of new trees occurred to enhance the chance for successful growth. Damaged or unhealthy
trees were removed in March and new trees were planted in April. The maintenance performed to the
phytoremediation system helps to ensure the continued effectiveness of the buffer. As anticipated in the
initial design, a full canopy had been established. Some of the trees which grew more slowly were now
beneath the canopy and were not thriving. This is consistent with the growth plan and did not impact the
system effectiveness.
During the April planting event approximately 30 new trees and 20 whips were added to the existing
healthy trees. The work was inspected by Ecolotree° and a report on this inspection was included in the
November 2011 Semiannual Report (AECOM 2012).
2.1.4 2020 Tree Replanting
The phytoremediation system status was reevaluated in 2019, and another supplemental new tree
planting was conducted at the site in February and March 2020. A total of 12 dead poplar trees were
removed using a mobile crane in February 2020. A total of 100 black willow 4-foot whips were planted in
March 2020. The trees were planted in 6-inch diameter by 12-inch deep holes, and the holes were
backfilled with compost followed by fertilization. Most of the newly planted trees appeared to be in good
health through 2023 (AECOM 2023).
2.2 M NA Activities
MNA activities, including groundwater monitoring, surface water monitoring, and intermittent seep
monitoring, have been conducted semiannually at the site in accordance with the schedule in the CAP,
which was revised in early 2009. The May semiannual monitoring plan and the November semiannual
monitoring plan are provided in Table 1 and Table 2, respectively. The May and November sampling
locations are shown on Figure 3 and Figure 4, respectively.
MNA activities and analytical results were summarized in semiannual reports and submitted to NCDEQ
from 2007 to 2014. Reporting frequency was reduced to annual reporting beginning in 2015. Each annual
report summarizes the results from both the May sampling event and the November sampling event of
that year.
2.3 Physical and Chemical Changes in Aquifer Conditions and Plume
Characteristics
The changes in geochemical conditions and concentrations of COCs over time are critical indicators for performance
evaluation. The following sections summarize the COC concentration changes in groundwater, surface water and
intermittent seep, and the change of geochemical conditions based on evaluation of the MNA parameters. Analytical
results from the most recent reporting year (2022) are used for evaluation of the current site condition, and historical
data from 2004 to 2022 are used for evaluation of condition change.
2.3.1 Ethylene Glycol
Analytical results for ethylene glycol in 2022 are provided in Table 4 and Figure 6. Historic ethylene glycol results
from 2004 to 2022 are presented in Table 7. Trend plots of ethylene glycol concentrations over time in select wells
are presented in Table 8.
Ethylene glycol was historically detected at concentrations greater than the NC 2L standard in samples collected from
wells located in the main disposal areas and downgradient. Ethylene glycol concentrations reduced to below
analytical reporting limits (non -detect) in samples collected beginning in 2007 and remained non -detect until
AECOM
12

Corrective Action Evaluation Report
Project Number: 60683034
November 2012. Fluctuating concentrations of ethylene glycol have been detected at several wells including B-01, B-
09C, B-10, B-23A, and B-236, from May 2013 through November 2018. Some detected ethylene glycol
concentrations May 2013 through November 2018 exceeded the NC 2L standard of 10 mg/L; however, ethylene
glycol concentrations have been below the analytical reporting limits in all wells sampled since 2019.
The low concentrations of ethylene glycol detected and non -detect results in the wells since 2007 support the
ethylene glycol natural attenuation remedy presented in the 2007 CAP. The landfill cap has significantly reduced or
eliminated the transport of ethylene glycol from the landfill into groundwater, and the concentrations of ethylene
glycol, which had entered the groundwater prior to the installation of the cap, decreased or were attenuated. Since
ethylene glycol is fully miscible in water and is mobile, the 2007 CAP anticipated ongoing occasional detections.
Future fluctuations of detections within historical ranges and non -detect results are expected as the remaining
ethylene glycol migrates and rapidly degrades.
2.3.2 1,4-Dioxane
1,4-Dioxane has historically been detected in wells near the four former disposal sites. 1,4-Dioxane results for May
and November 2022 are provided in Table 4 and isoconcentration contours for November 2022 are shown in Figure
5. Historic 1,4-dioxane results from 2004 to 2022 are presented in Table 7. Trend plots of 1,4-dioxane concentrations
over time in select wells are presented in Table 9. The concentration trend plots indicate that 1,4-dioxane
concentrations in most wells are generally either decreasing (B-01, B-10, B-12 [since 2013], B-17C, and B-22B) or
stable (B-09C). Overall, 1,4-dioxane is contained and contaminant mass continues to decrease over time.
2.3.3 1,1-Biphenyl and Diphenyl Ether
Since 2005, the only monitoring well in which 1,1-biphenyl has been consistently detected is monitoring well B-10.
Historic data for 1,1-biphenyl at B-10 have been below the NC 2L with the exception of the 2008 sample in which the
1,1-biphenyl concentration detected (0.405 mg/L) slightly exceeded the NC 2L standard. The historic maximum 1,1-
biphenyl detection was 0.461 mg/L in 1999. 1,1-Biphenyl results from the May and November 2022 monitoring events
are presented in Table 4, and the isoconcentration contour is shown on Figure 8. Historic 1,1-biphenyl results from
2004 to 2022 are presented in Table 7.
Diphenyl ether was historically detected in several wells located near the former disposal sites and at the
downgradient wells. Historically, detected diphenyl ether concentrations ranged from approximately 1.1 to 4.5 mg/L.
The highest diphenyl ether concentrations have consistently been detected in B-10; however, as shown in Table 10,
the diphenyl ether concentrations detected in B-10 demonstrate a decreasing trend since 2009. Diphenyl ether
concentrations detected in other wells are generally below the NC 2L standard of 0.18 mg/L. The May 2022 and
November 2022 diphenyl ether data are presented in Table 4 and historic results from 2004 to 2022 are presented in
Table 7. Trend plots of diphenyl ether concentrations in select wells are shown in Table 10.
The data continue to indicate that migration of 1,1-biphenyl and diphenyl ether is being controlled by the landfill cap
and through natural attenuation mechanisms.
2.3.4 MNA Parameters
The MNA parameters monitored include dissolved oxygen (DO), oxidation-reduction potential (ORP), nitrate as
nitrogen, ferrous iron, sulfate, methane, and alkalinity; the parameter results from the May and November 2022
semiannual events are presented in Table 4.
DO is the most thermodynamically favored electron acceptor used by microorganisms for the biodegradation of
organic chemicals. Typically, microorganisms in the areas containing biodegradable contaminants quickly utilize
oxygen. The consumption of DO due to microbial activity would also result in negative ORP measurements.
Anaerobic microorganisms generally cannot function at DO concentrations greater than 1 mg/L. DO concentrations
less than 1 mg/L were generally detected at the wells currently impacted by the site COCs.
ORP changes in groundwater are usually mediated by biological activity; therefore, ORP can be a valuable
geochemical indicator. ORP measurements less than -50 millivolts (mV) generally are representative of anoxic to
anaerobic conditions and can be found in the areas containing biodegradable contaminants. Evaluating data from
2004 to 2022 revealed that ORP measurements at locations in which ethylene glycol, 1,4-dioxane and diphenyl ether
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13

Corrective Action Evaluation Report
Project Number: 60683034
were detected were generally lower than in surrounding wells. These results are consistent with DO data indicating
the consumption of electron acceptors via biodegradation of site COCs.
Nitrate serves as a terminal electron acceptor (TEA) through the processes of denitrification and nitrate reduction.
The depletion of nitrate is indicative of biological activity. Nitrate was typically not detected in wells containing site
COCs, indicating microorganisms for biodegradation of site COCs in the impacted area have utilized the nitrate.
Ferrous iron, a metabolic product of the biological iron -reducing process, is an indication of reducing conditions and
microbial activity. Elevated ferrous iron concentrations are expected in the areas containing biodegradable organic
chemicals. The data verify the presence of ferrous iron at the areas containing site COCs.
Methane is a final metabolic product. Methane would be produced after all the other electron acceptors are utilized
via the biodegradation process by the microorganisms. The production of methane is direct evidence of biological
activity and the reducing conditions. High methane levels have historically been detected at B-22B, B-23A/B, B-
24A/B, and B-3213, which were also impacted by 1,4-dioxane and diphenyl ether.
Alkalinity is not a TEA, although it can be used as a valuable indicator of microbial activity. Alkalinity reflects the
buffering capacity of groundwater and is most influenced by the carbon dioxide content. Carbon dioxide originates
from the dissolution of carbonates in the aquifer, atmospheric carbon dioxide, and the respiration of microorganisms.
As the sequential electron acceptors (i.e., oxygen, nitrate, ferric iron, and sulfate) are utilized, carbon dioxide is
produced at each metabolic step. Therefore, alkalinity can be expected to increase where biological activity is
occurring. Alkalinity above 500 mg/L has been historically detected in samples collected at the wells close to the
former disposal areas (B-01, B-09C, B-10, B-14, and B-32B) and downgradient wells (B-19B, B-22B and B-23A/B). In
fact, alkalinity levels above 2000 mg/L have historically been measured in B-01, B-09C, B-10, and B-23A/B. Three of
these wells are close to the former disposal areas and contained elevated levels of site COCs. This further supports
the interpretation that degradation of site parameters is occurring.
2.4 Surface Water and Intermittent Seep
2.4.1 Surface Water
Surface water monitoring is conducted at one location (SW-05) during the May monitoring event and at four locations
(SW-03, SW-05, SW-07, and SW-08) during the November event each year. The surface water results are
summarized in Table 5. 1,4-Dioxane, ethylene glycol, diphenyl ether, and 1,1-biphenyl were not detected in samples
from any of the surface water monitoring locations in last five years.
2.4.2 Intermittent Seep
CSW-1 and CSW-2 are monitoring locations associated with the intermittent seep, and both locations have been dry
during numerous monitoring events since the phytoremediation program was initiated. CSW-1 is located at the initial
discharge point of the seep, and CSW-2 is located downstream in the creek bed fed by the seep (Figure 3 and
Figure 4).
Intermittent seep samples collected prior to construction of the phytoremediation system contained 1,4-dioxane at
concentrations at approximately 0.5 mg/L at CSW-1 and lower concentrations at downgradient CSW-2. The 1,4-
dioxane concentrations decreased after the construction of the phytoremediation system and remained below 0.2
mg/L from 2012 through 2019. During the May 2021 and May 2022 monitoring events, the 1,4-dioxane concentration
detected in CSW-1 (0.696 mg/L and 0.667 mg/L, respectively) were higher than in recent sampling events The
elevated 1,4-dioxane concentrations in the intermittent seep may be temporary and monitoring for 1,4-dioxane in the
intermittent seep will continue in future monitoring events to evaluate the concentration trends.
AECOM
14

Corrective Action Evaluation Report
Project Number: 60683034
3. Conclusion
In the 2007 CAP, a combination of MNA and phytoremediation was selected as the site remedy to address the impact
of site COCs in groundwater. MNA and phytoremediation have then been conducted at the site since 2007, including
following activities:
• Continued ongoing maintenance and monthly inspection of the landfill cap;
• Continued ongoing maintenance and inspection of the phytoremediation system;
• Semiannual MNA groundwater sampling and analyses in May and November every year, and
• Semiannual reporting from 2007 to 2014, and annual reporting since 2015.
The primary pathway for COC migration at the site is leaching from the landfill material. This pathway is controlled by
the existence and ongoing maintenance of the landfill cap. Analysis of current and historical results confirm that the
landfill cap has significantly reduced or eliminated the transport of COCs from the landfill into groundwater. COCs that
entered the groundwater prior to the installation of the cap continue to attenuate naturally as confirmed by ongoing
monitoring.
Based on the conceptual site model and long-term monitoring results site contamination is controlled and does not
pose an unacceptable risk to human health or the environment. Based on these monitoring results, MNA with
phytoremediation as described in the CAP continues to be an effective remedy for this site, and there is no need to
implement contingency plan.
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15

Corrective Action Evaluation Report
Project Number: 60683034
4. References
AECOM, 2007. Corrective Action Plan. Needmore Road Landfill Facility, Salisbury, North Carolina. November 2007.
AECOM, 2012. November 2011 Semiannual Report. Needmore Road Landfill Facility, Salisbury, North Carolina. May
2012.
AECOM, 2014. November 2013 Semiannual Report. Needmore Road Landfill Facility, Salisbury, North Carolina. May
2014.
AECOM, 2021. 2020Annual Report. Needmore Road Landfill Facility, Salisbury, North Carolina. May 2021.
AECOM, 2023. 2022Annual Report. Needmore Road Landfill Facility, Salisbury, North Carolina. May 2023.
ARCADIS 2005. Revised Human Health and Ecological Risk Assessment. Needmore Road Landfill Facility,
Salisbury, North Carolina. September 2005.
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16

Corrective Action Evaluation Report
Project Number: 60683034
Tables
AECOM

Table 1
May Groundwater and Surface Water Sampling Plan
CNA Holdings LLC — Needmore Road Landfill
Salisbury, North Carolina
Location
1,4-Dioxane
DowTherm ATM
Ethylene
Glycol
VOCs*
MNA**
B-01
X
X
X
B-09C
X
X
X
B-10
X
X
X
X
B-12
X
X
X
B-17C
X
X
B-22B
X
X
B-23A
X
X
X
B-23B
X
X
X
B-24A
X
X
SW-5
X
X
X
CSW-1
X
CSW-2
X
Notes:
* VOCs to be analyzed annually (November only; revised from CAP schedule of May only)
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
Page 1 of 1

Table 2
November Groundwater and Surface Water Sampling Plan
CNA Holdings LLC — Needmore Road Landfill
Salisbury, North Carolina
Location
1,4-Dioxane
DowTherm
AT
Ethylene
Glycol
VOCs*
MNA**
Expanded
MNA***
B-01
X
X
X
X
X
X
B-09C
X
X
X
X
X
B-10
X
X
X
X
X
X
B-12
X
X
X
B-17B
X
X
X
X
B-17C
X
X
X
X
B-21 B
X
X
B-22A
X
X
X
X
X
B-22 B
X
X
X
X
X
B-23A
X
X
X
X
X
X
B-23B
X
X
X
X
X
X
B-24A
X
X
X
X
B-24 B
X
X
X
X
B-32 B
X
X
X
X
X
CSW-1
X
CSW-2
X
SW-3
X
X
X
SW-5
X
X
X
SW-7
X
X
X
SW-8
I X
I X
I X
Notes:
* VOCs to be analyzed annually (November only; revised from CAP schedule of May only)
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
*** Expanded MNA: TOC, ethane, ethene, methane, carbon dioxide, hydrogen, and volatile fatty acids
Page 1 of 1

Table 3
Groundwater Elevations
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Well ID
Date
Gauged
Top of
Casing TOC
Depth to
Water
Groundwater
Elevation
MSL
Feet below
TOC
MSL
B-01
5/16/2022
756.55
56.06
700.49
11 /2/2022
56.97
699.58
B-09C
5/16/2022
713.44
36.31
677.13
11 /2/2022
39.61
673.83
B-10
5/16/2022
75178
45.38
706.40
11 /2/2022
46.85
704.93
B-12
5/16/2022
677.11
19.23
657.88
11 /1 /2022
21.33
655.78
B-17B
11/1/2022
678.32
18.90
659.42
B-17C
5/16/2022
677.06
16.78
660.28
11 /1 /2022
18.42
658.64
B-21 B
11 /1 /2022
676.73
13.55
663.18
B-22A
11 /2/2022
661.66
4.38
657.28
B-22B
5/16/2022
660.15
1.47
658.68
11 /2/2022
3.15
657.00
B-23A
5/16/2022
665.73
8.13
657.60
11 /1 /2022
8.69
657.04
B-23B
5/16/2022
665.74
7.62
658.12
11 /1 /2022
8.54
657.20
B-24A
5/16/2022
659.10
3.90
655.20
11 /1 /2022
4.20
654.90
B-24B
11/1/2022
659.19
3.28
655.91
B-32B
11/2/2022
744.27
31.83
712.44
Notes:
MSL - mean sea level
NC -not calculated
NM - not measured
TOC - top of casing
Page 1 of 1

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Location
B-01
5/16/2022
B-01-051622
B-01
11/2/2022
B-01-110222
B-09C
5/1612022
B-0SC-051622
B-09C
11/212022
B-09C-110222
B-09C
111212022
B-99C-110222
B-10
5116I2022
B-10-051622
B-10
5,16/2022
B-99-051622
B-10
11/212022
B-10-110222
Collection Date
Sample Name
Chemical Units NC 2L Standard
Organic Compounds
1,1'-Biphenylm
/L
0.4
<0.0500
<0.0435
<0.0435
0.0539
0.0496
0.116
Di hen I ether
m /L
0.18
<0.0500
<0.0435
<0.0435
0.559
0.469
1.19
Ethylene Glycol
m /L
10
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
1,4-Dioxane
Acetone
m /L
m /L
0.003
6
1.58
0.476
0.935
3.47
0.909
3.43
0.164
0.145
0.161
<0.0250
2-Butanone
m /L
4
0.239
0.652
0.644
<0.0050
Chlorobenzene
m /L
0.05
<0.0020
<0.0100
<0.0100
<0.0010
Chloroethane
m /L
3
0.0202
<0.0100
<0.0100
0.0357
1,1-Dichloroethane
m /L
0.006
0.0076
<0.0100
<0.0100
0.0405
1,1-Dichloroethene
m /L
0.35
<0.0020
<0.0100
<0.0100
<0.0010
4-Meth I-2-Pentanone
m /L
0.0237
0.0942
0.09
<0.0050
1,4-Dichlorobenzene
m /L
<0.0020
<0.0100
<0.0100
<0.0010
cis-1,2-Dichloroethene
m /L
<0.0020
0.0108
0.0112
<0.0010
Toluene
m /L
<0.0020
<0.0100
<0.0100
0.0023
Vinyl chloride
m /L
<0.0020
<0.0100
<0.0100
0.002
Trichloroethene
m /L
0.002
<0.0100
<0.0100
<0.0010
X enes, total
m /L
<0.0020
<0.01060
<0.0100
0.0021
MNA Parameters
Alkalinity
m /L
1100
1340
2600
2680
460
430
442
Nitrate -as -nitrogen
m /L
10
<0.040
<0.40
<0.040
<0.40
<0.040
<0.040
<0.40
Nitrite -as -nitrogen
m /L
1
0.046
0.13
<0.040
0.047
<0.040
<0.040
0.059
Orthophosphate as P
m /L
0.64
<0.25
<0.050
<0.12
<0.050 UJ
<0.050
0.052
Sulfate
m /L
250
<1.0
1.9
<1.0
1.4
<1.0
<1.0
<1.0
Total organic carbon 1
m /L
527
19.7
Total organic carbon 2
m /L
--
--
521
--
--
--
--
--
19.6
Total organic carbon 3
m /L
--
--
513
--
--
--
--
--
19.5
Total organic carbon 4
m /L
--
--
503
--
--
--
--
--
19.4
Total organic carbon average
m /L
--
--
516
--
--
--
--
--
19.6
Acetic Acid
m /L
--
--
590
--
--
--
--
--
1.7
Methane
m /L
--
--
17
-
--
--
--
--
16
Ethane
m /L
--
--
<0.0010
--
--
--
--
--
<0.0010
Ethane
m /L
--
--
<0.0010
--
--
--
--
--
<0.0010
Carbon dioxide
m /L
--
--
420
--
--
--
--
--
9.86
Hydrogen
nM
--
--
<1.9
--
--
--
--
--
<1.9
Field Parameters
DissolvedOx en
m /L
0.08
0.26
0.03
0.29
0.45
0.38
Iron, Ferrous
m /L
5.8
4.4
6.0
4.0
2.8
3.4
ORP
mV
-148.4
-118.1
-136.5
-108.0
-85.2
-70.4
pH
SU
6.44
6.68
6.49
6.73
6.34
6.53
Specific Conductance
umhos/cm
2629.0
2713.0
4293.0
5042.0
876.0
882.4
Temperature
degrees C
21.00
18.00
18.20
16.70
19.40
16.30
Turbidity
NTU
19.8
19.9
6.9
6.5
5.5
6.3
Notes:
site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
Bold - Analyte detected by the laboratory
Bold and shaded -Concentration exceeds the NC 2L limit
degrees C - degrees Celsius
mg/L - milligrams per liter
mV - millivolts
NA - Not Analyzed
NC 2L -- North Carolina Administrative Code, Title 15A, Subchapter 2L
NTU - Nephelometric Turbidity Units
SU -standard units
umhos/cm - micromhos per centimeter
UJ: The analyte was analyzed for but was not detected. The reported
quantitation limit is approximated and may be inaccurate or imprecise.
Page 1 of 3

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Location
B-12
5116/2022
B-12-051622
B-12
11/1/2022
B-12-110122
B-17B
11/1/2022
B-17B-110122
B-17C
5/16/2022
B-17C-051622
B-17C
111112022
B-17C-110122
B-21B
111112022
B-21B-110122
B-22A
I1I212022
B-22A-110222
B-22B
5116/2022
B-22B-051622
B-22B
111212022
B-2213-110222
Collection Date
Sample Name
Chemical Units NC 2L Standard
Organic Compounds
1,1'-Biphenyl
m /L
0.4
<0.0100
<0.0083
<0.0091
<0.0083
<0.0100
<0.0100
Diphenyl ether
m /L
0.18
<0.0100
<0.0083
<0.0091
<0.0083
<0.0100
0.029
Ethylene Glycol
m /L
10
--
--
--
--
--
--
--
--
--
1,4-Dioxane
Acetone
m L
m /L
0.003
6
--
off 2.07
--
--
--
--
MID.0432
--
1.07
<0.0250
1.07
--
0.986
<0.0250
2-Butanone
m L
4
--
--
--
--
--
--
<0.0050
--
<0.0050
Chlorobenzene
m L
0.05
--
--
--
--
--
--
<0.0010
--
0.0122
Chloroethane
m /L
3
--
--
--
--
--
--
<0.0010
--
0.0137
1,1-Dichloroethane
m /L
0.006
--
--
--
--
--
--
0.0022
--
<0.0010
1,1-Dichloroethene
m /L
0.35
--
--
--
--
--
--
0.0017
--
<0.0010
4-Meth-2-Pentanone
m /L
--
--
--
--
--
--
--
<0.0050
--
<0.0050
1,4-Dichlorobenzene
m /L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
cis-1,2-Dichloroethene
m L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
Toluene
m /L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
Vinyl chloride
m /L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
Trichloroethene
m /L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
X lenes, total
m L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
MNA Parameters
Alkalinity
m /L
330
357
276
370
412
275
631
830
993
Nitrate -as -nitro en
m /L
10
<0.040
<0.040
<0.40 UJ
<0.040
<0.040
<0.040
<0.40
<0.040
<0.040
Nitrite -as -nitrogen
m /L
1
<0.040
<0.040
<0.040 UJ
<0.040
<0.040
<0.040
0.044
<0.040
<0.040
Orthophosphate as P
m /L
0.068
0.13
0.27
0.12
0.24
0.061
<0.050
<0.050
0.2
Sulfate
m /L
250
1.1
1.4
2.1
<1.0
1.2
14.4
1
<1.0
<1.0
Total organic carbon 1
m /L
3.4
2.8
4.3
7.7
Total organic carbon 2
m /L
3.2
2.8
4.2
5.7
Total organic carbon 3
m /L
3.1
2.8
4.1
5.4
Total organic carbon 4
m /L
3.0
2.8
4.1
5.2
Total organic carbon average
m /L
3.2
2.8
4.2
6.0
Acetic Acid
m /L
0.53
0.63
0.6
0.53
Methane
m /L
0.026
0.024
0.047
0.12
Ethane
m /L
<0.0010
<0.0010
0.0022
0.0029
Ethane
m /L
<0.0010
<0.0010
<0.0010
<0.0010
Carbon dioxide
m /L
154
105
278
346
Hydrogen
nM
<1.9
<1.9
<1.9
<1.9
Field Parameters
DissolvedO en
m /L
1.18
1.85
0.10
1.01
1.68
0.88
0.31
0.04
0.25
Iron, Ferrous
m /L
0.0
0.0
4.0
0.0
0.2
0.3
3.2
3.4
3.8
ORP
mV
93.9
111.8
-32.2
83.3
50.1
30.4
-110.8
-113.8
-100.0
pH
SU
6.42
6.77
6.26
6.60
6.88
6.86
6.78
6.65
6.94
Specific Conductance
umhos/cm
797.0
631.0
435.0
806.0
656.0
534.9
1086.0
1502.0
1694.0
Temperature
degrees C
20.60
18.40
16.60
17.20
16.10
15.90
15.80
16.70
15.90
Turbidity
NTU
1.1
4.9
6.0
1.1
3.6
3.4
8.6
6.1
5.1
Notes:
site -specific target chemical
- no standard specified under 15A NCAC 2L.0202
Bold - Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
degrees C - degrees Celsius
mg/L - milligrams per liter
mV - millivolts
NA - Not Analyzed
INC 2L - North Carolina Administrative Code, Title 15A, Subchapter 2L
NTU - Nephelometric Turbidity Units
SU - standard units
umhos/cm - micromhos per centimeter
UJ: The analyte was analyzed for but was not detected. The reported
quantitation limit is approximated and may be inaccurate or imprecise.
Page 2 of 3

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Location
B-23A
5/16/2022
B-23A-051622
B-23A
11/1/2022
B-23A-110122
B-23B
511//2022
B-2313-051622
B-23B
111112022
B-2313-110122
B-24A
511//2022
B-24A-051622
B-24A
11/1/2022
B-24A-110122
B-24B
1111/2022
B-2413-110122
B-32B
11/2/2022
B3213-110222
Collection Date
Sample Name
Chemical Units INC 2L Standard
Organic Compounds
1,1'-Biphenyl
m /L
0.4
<0.0500
<0.0100
<0.0100
<0.0100
<0.0100
Diphenyl ether
m /L
0.18
<0.0500
0.0612
0.0104
<0.0100
<0.0100
Ethylene Glycol
m /L
10
<5 0
<50.0
<5 0
<50.0
<5.0
1,4-Dioxane
Acetone
m L
m /L
0.003
6
3.15
3.18
5.07
3.01
2.77
0.2
F 0,218
<0.0250
0.118
<0.0250
0.0022
2-Butanone
m L
4
0.857
0.433
<0.0050
<0.0050
Chlorobenzene
m L
0.05
<0.0250
<0.0100
<0.0010
<0.0010
Chloroethane
m /L
3
<0.0250
0.0217
0.0051
0.0054
1,1-Dichloroethane
m /L
0.006
0.0334
<0.0100
0.0049
<0.0010
1,1-Dichloroethene
m /L
0.35
<0.0250
<0.0100
<0.0010
<0.0010
4-Meth-2-Pentanone
m /L
<0.125
<0.0500
<0.0050
<0.0050
1,4-Dichlorobenzene
m /L
<0.0250
<0.0100
<0.0010
<0.0010
cis-1,2-Dichloroethene
m L
<0.0250
<0.0100
<0.0010
<0.0010
Toluene
m /L
<0.0250
<0.0100
<0.0010
<0.0010
Vinyl chloride
m /L
<0.0250
<0.0100
0.0012
<0.0010
Trichloroethene
m L
<0.0250
<0.0100
<0.0010
<0.0010
X lenes, total
m L
<0.0250
<0.0100
<0.0010
<0.0010
MNA Parameters
Alkalinity
m /L
3000
3100
2200
2120
470
474
375
140
Nitrate -as -nitrogen
m L
10
<0.040
<0.40
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
Nitrite -as -nitrogen
m /L
1
<0.040
0.057
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
Orthophosphate as P
m /L
0.79
0.54
0.22
<0.12
<0.050
0.16
<0.050
0.08
Sulfate
m /L
250
7.6
5.4
2.8
2.5
<1.0
<1.0
<1.0
<1.0
Total organic carbon 1
m /L
2560
834
2.3
Total organic carbon 2
m /L
2540
840
1
Total organic carbon 3
m /L
2510
835
<1.0
Total organic carbon 4
m /L
2490
834
<1.0
Total organic carbon average
m /L
2520
836
1.2
Acetic Acid
m /L
2700
1100
<0.50
Methane
m /L
1.7
4.4
2.1
Ethane
m /L
<0.0010
<0.0010
<0.0010
Ethene
m /L
<0.0010
<0.0010
<0.0010
Carbon dioxide
m /L
362
294
67
Hydrogen
nM
<1.9
2.2
<1.9
Field Parameters
DissolvedO en
m /L
0.17
0.82
0.01
0.41
0.42
0.63
0.34
0.60
Iron, Ferrous
m /L
3.0
5.0
3.4
4.2
2.6
3.6
3.6
3.6
ORP
mV
-78.3
-48.9
-130.1
-114.9
-122.2
-115.6
-111.2
-51.3
pH
SU
6.26
6.49
6.47
6.82
6.61
6.87
7.04
6.75
Specific Conductance
umhos/cm
5476.0
5962.0
3984.0
4298.0
750.0
918.0
749.5
274.3
Temperature
degrees C
19.60
17.60
18.10
16.60
18.20
16.10
15.80
16.50
ITurbidity
NTU
4.2
6.2
8.2
6.9
5.7
44.0
5.5
6.9
Notes:
site -specific target chemical
- no standard specified under 15A NCAC 2L.0202
Bold - Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
degrees C - degrees Celsius
mg/L - milligrams per liter
mV - millivolts
NA - Not Analyzed
INC 2L - North Carolina Administrative Code, Title 15A, Subchapter 2L
NTU - Nephelometric Turbidity Units
SU - standard units
umhos/cm - micromhos per centimeter
UJ: The analyte was analyzed for but was not detected. The reported
quantitation limit is approximated and may be inaccurate or imprecise.
Page 3 of 3

Table 5
Surface Water Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Location ID
SW-03
11/1/2022
SW-05
5/16/2022
SW-05
11/1/2022
SW-5-110122
SW-07
11/1/2022
SW-7-110122
SW-08
11/1/2022
SW-8-110122
Collection Date
Sample Name
SW-3-110122
SW-5-051622
Chemical Units NC ISTV
Organic Compounds
Ethylene Glycol
m /L
<5.0
<5.0
<5.0
<5.0
<5.0
1,4-Dioxane
m /L
0.08
<0.0020
<0.0020
<0.0020
<0.0020
<0.0020
1,1'-Biphenyl
m /L
0.86
<0.0087
<0.0100
<0.0087
<0.0087
<0.0087
Di hen I ether
m /L
<0.0087
<0.0100
<0.0087
<0.0087
<0.0087
Field Parameters
DissolvedOx en
m /L
8.33
6.82
8.25
8.29
9.79
ORP
mV
135.2
58.4
173.8
190.6
180.3
H
SU
7.02
7.47
6.96
6.52
6.94
Specific Conductance
umhos/cm
93.4
122.9
93.8
95.3
93.9
Temperature
degrees C
13.80
21.10
13.80
13.80
14.10
ITurbidity
NTU
33.5
6.9
27.0
31.2
93.9
Notes:
degrees C - degrees Celsius
mg/L - milligrams per liter
mV - millivolts
NC ISTV -- North Carolina In -Stream Target Values for Surface Waters
NTU - Nephelometric Turbidity Units
SU - standard units
umhos/cm - micromhos per centimeter
Page 1 of 1

Table 6
Intermittent Seep Water Analytical Summary
CNA Holdings LLC — Needmore Road Landfill
Salisbury, North Carolina
Location ID
CSW-1
5/16/2022
CSW-1-051622
Collection Date
Sample Name
Chemical
Units
Organic Compounds
1,4-Dioxane
mg/L
0.667
Field Parameters
DissolvedOxygen
mg/L
5.38
ORP
my
31.6
pH
SU
6.98
Specific Conductance
umhos/cm
427.2
Temperature
degrees C
16.40
Turbidity
NTU
8.1
Notes:
mg/L — milligrams per liter
my — millivolts
SU — standard units
umhos/cm — micromhos per centimeter
degrees C — degrees Celsius
NTU — Nephelometric Turbidity Units
Page 1 of 1

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-01
Jun-04
<28
4.07
<0.05
0.0723
Nov-04
492
0.202
<0.01
0.0211
May-05
1160
2.93
<2.5
<2.5
Nov-05
<70
3.69
<0.01
0.02
May-06
93.9
2.75
<0.02
0.0419
Nov-06
2000
4.68
<0.01
0.0446
May-07
<140
3.43
<0.01
0.0716
Nov-07
<7
3.01
<0.04
0.0662
May-08
<7
2.15
<0.04
0.0635
Nov-08
<7
3.31
<0.01
0.0565
May-09
<7
2.26
NA
NA
Dec-09
<35
3.54
<0.01
0.0423
May-10
<35
3.56
NA
NA
Nov-10
<35
3.24
<0.01
0.0811
May-11
NA
2.15
NA
NA
Nov-11
<35
3.25
<0.01
0.083
May-12
NA
3.85
NA
NA
Nov-12
<14
3.41
<1
<1
May-13
254
3.07
NA
NA
Nov-13
38.5
2.74
<0.1
<0.1
May-14
796
1.96
NA
NA
Nov-14
648
3.27
<0.01
0.0858
May-15
<5.0
2.89
NA
NA
Nov-15
<50
2.64
<0.01
0.122
May-16
<50
2.37
NA
NA
Nov-16
751
2.18
<0.1
<0.1
May-17
266
0.242
NA
NA
Nov-17
198
1.86
0.0101
0.132
May-18
<10.0
1.93
NA
NA
Nov-18
51.9
2.13
<0.0100
0.0223
May-19
<5.0
1.81
NA
NA
Nov-19
<50.0
1.55
<0.0100
0.0419
May-20
<5.0
1.51
N/A
N/A
Nov-20
<5.0
1.51
<0.0100
0.0300
May-21
<5.0
1.61
N/A
N/A
Nov-21
<5.0
1.65
<0.0091
0.0309
May-22
<5.0
1.53
N/A
N/A
Nov-22
<5.0
1.58
<0.0500
<0.0500
Page 1 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-09C
Jun-04
<70
0.791
<0.5
<0.5
Nov-04
1420
1.04
<0.05
0.0545
May-05
<70
0.776
<0.2
<0.2
Nov-05
363
1.31
<0.01
0.0324
May-06
85.8
0.668
<0.02
0.0492
Nov-06
2020
1.29
<0.01
<0.01
May-07
<140
1.11
<0.01
0.0377
Nov-07
<7
0.995
<0.01
0.0352
May-08
<7
0.486
<0.01
0.0312
Nov-08
<7
1.11
<0.01
0.0438
May-09
<7
0.873
NA
NA
Dec-09
<35
1.15
<0.01
0.0581
May-10
<35
1.03
NA
NA
Nov-10
<35
0.951
<0.01
0.0542
May-11
NA
0.782
NA
NA
Nov-11
<35
1.1
<0.01
0.0451
May-12
NA
1.46
NA
NA
Nov-12
<14
1.15
<0.01
0.0255
May-13
448
0.803
NA
NA
Nov-13
77
0.766
<0.01
0.0272
May-14
288
0.86
NA
NA
Nov-14
406
0.893
<0.01
0.029
May-15
<5.0
0.972
NA
NA
Nov-15
<500
0.909
<0.01
0.0106
May-16
<50
0.954
NA
NA
Nov-16
330
0.796
<0.01
0.0157
May-17
192
0.56
NA
NA
Nov-17
122
0.906
<0.0100
0.0269
Nov-17
NA
0.81
<0.0100
0.026
May-18
<10.0
0.689
NA
NA
Nov-18
197
0.935
<0.0100
<0.0100
Nov-18
NA
0.964
<0.0100
<0.0100
May-19
<5.0
0.85
NA
NA
Nov-19
<50.0
0.886
<0.0100
0.0181
Nov-19
NA
0.848
<0.0100
0.0133
May-20
<5.0
0.756
NA
NA
Nov-20
<5.0
0.743
<0.0100
0.0255
Nov-20
NA
0.686
<0.0100
0.0244
May-21
<5.0
0.852
N/A
N/A
Nov-21
<25.0
0.909
<0.0091
0.0212
May-22
<5.0
0.753
N/A
N/A
Nov-22
<5.0
0.935
<0.0435
<0.0435
Page 2 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-10
Jun-04
<28
0.723
<1
4.63
Nov-04
354
0.592
<0.4
3.33
May-05
647
0.419
0.02
0.193
Nov-05
57.5
0.62
0.31
3.62
May-06
<7
0.328
0.29
3.01
Nov-06
284
0.509
0.28
3.12
May-07
<28
0.564
0.28
3.26
Nov-07
<7
0.413
0.31
3.46
May-08
<7
0.461
0.405
3.22
Nov-08
<7
0.481
0.352
3.12
May-09
<7
0.412
0.319
3.09
Dec-09
<14
0.649
0.391
4.58
May-10
<14
0.417
0.288
2.91
Nov-10
<14
0.39
0.25
2.55
May-11
NA
0.553
0.328
3.34
Nov-11
<14
0.306
0.3
2.53
May-12
NA
0.484
0.157
1.45
Nov-12
<14
0.546
0.165
1.82
May-13
252
0.421
0.106
1.12
Nov-13
<35
0.47
0.157
1.69
May-14
<10
0.599
0.0728
0.73
Nov-14
<10
0.508
0.169
1.84
May-15
<5.0
0.511
0.0828
1.09
Nov-15
<50
0.404
0.192
2.11
May-16
<50
0.42
0.0888
1.16
Nov-16
403
0.33
0.104
1.08
May-17
<5
0.275
0.137 J
1.4 J
May-17
<5
0.257
0.070 J
0.735 J
Nov-17
<5.0
0.327
0.231 J
1.44
May-18
<10.0
0.243
0.146
1.46
May-18
<10.0
0.261
0.178 J
1.57
Nov-18
41.3
0.267
0.0321
0.31
May-19
<5.0
0.328
0.125
1.31
May-19
<5.0
0.312
0.121
1.11
Nov-19
<50.0
0.222
0.085
1.02
May-20
<5.0
0.219
0.0711 J
0.643 J
May-20
<5.0
0.179
0.113 J
1.01 J
Nov-20
<5.0
0.197
0.0694
0.698
May-21
<5.0
0.193
0.127
1.21
Nov-21
<5.0
0.18
0.11
1.14
May-22
<5.0
0.164
0.0539
0.559
Nov-22
<5.0
0.161
0.116
1.19
Page 3 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-12
Feb-04
<7
0.315
<0.01
<0.01
May-04
<7
0.521
<0.01
<0.01
Jun-04
<7
0.775
<0.01
0.0102
Nov-04
<7
0.942
<0.01
0.0115
May-05
<7
0.222
<0.01
0.0108
Nov-05
<7
0.165
<0.01
<0.01
May-06
NA
0.151
<0.01
<0.01
Nov-06
NA
0.216
<0.01
<0.01
May-07
NA
0.118
<0.01
<0.01
Nov-07
NA
0.169
<0.01
<0.01
May-08
<7
0.121
<0.01
<0.01
Nov-08
NA
0.102
<0.01
<0.01
May-09
NA
0.105
<0.01
0.0108
Dec-09
NA
0.128
<0.01
0.0119
May-10
NA
0.11
<0.01
<0.01
Nov-10
NA
0.0946
<0.01
<0.01
May-11
NA
0.11
<0.01
<0.01
Nov-11
NA
0.0761
<0.01
<0.01
May-12
NA
0.13
<0.01
<0.01
May-12
NA
0.132
<0.01
<0.01
Nov-12
NA
3.68
<0.01
<0.01
May-13
NA
3.44
<0.01
<0.01
Nov-13
NA
3.24
<0.01
<0.01
May-14
NA
2.59
<0.01
<0.01
Nov-14
NA
3.27
<0.01
<0.01
May-15
NA
3.09
<0.01
<0.01
Nov-15
NA
2.9
<0.01
<0.01
May-16
NA
2.81
<0.01
<0.01
Nov-16
NA
2.91
<0.01
<0.01
May-17
NA
2.71
<0.01
<0.01
Nov-17
NA
2.76
<0.0100
<0.0100
May-18
NA
2.89
<0.0100 UJ
<0.0100 UJ
Nov-18
NA
3.09
<0.0100
<0.0100
May-19
NA
2.5
<0.0100
<0.0100
Nov-19
NA
2.3
<0.0100
<0.0100
May-20
NA
2.13
<0.0100
<0.0100
Nov-20
NA
2.4
<0.0100
<0.0100
May-21
N/A
1.84
<0.0100
<0.0100
Nov-21
N/A
2.35
<0.0091
<0.0091
May-22
N/A
2.39
<0.0100
<0.0100
Nov-22
N/A
2.07
<0.0083
<0.0083
Page 4 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-17B
Feb-04
<7
2.98
<0.01
<0.01
May-04
<7
2.33
<0.01
0.0125
Jun-04
<7
4.96
<0.01
<0.01
Nov-04
<7
3.11
<0.01
<0.01
May-05
<7
2.83
<0.01
0.0102
Nov-05
<7
1.87
<0.01
0.0107
May-06
NA
2.42
<0.01
<0.01
Nov-06
NA
2.84
<0.01
<0.01
May-07
NA
2.62
<0.01
<0.01
Nov-07
NA
3.33
<0.01
<0.01
May-08
<7
3.52
<0.01
<0.01
Nov-08
NA
2.35
<0.01
<0.01
Dec-09
NA
2.54
<0.01
<0.01
Nov-10
NA
2.75
<0.01
<0.01
Nov-11
NA
2.59
<0.01
<0.01
Nov-12
NA
0.291
<0.01
<0.01
Nov-13
NA
0.113
<0.01
<0.01
Nov-14
NA
0.271
<0.01
<0.01
Nov-15
NA
0.135
<0.01
<0.01
Nov-16
NA
1.93
<0.01
<0.01
Nov-17
NA
0.128
<0.0100
<0.0100
Nov-18
NA
0.0722
<0.0100
<0.0100
Nov-19
NA
0.259
<0.0100
<0.0100
Nov-20 NA
0.0786
<0.0100
<0.0100
Nov-21
N/A
0.138
<0.0100
<0.0100
Nov-22
N/A
0.533
<0.0091
<0.0091
Page 5 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-17C
Feb-04
<7
3.29
<0.01
<0.01
May-04
<7
2.21
<0.01
<0.01
Jun-04
<7
3.01
<0.01
<0.01
Nov-04
<7
3.22
<0.01
0.0117
May-05
<8.5
2.51
<0.01
<0.01
Nov-05
<7
2.44
<0.01
<0.01
May-06
NA
2.68
<0.01
<0.01
Nov-06
NA
2.92
<0.01
<0.01
May-07
NA
2.93
<0.01
<0.01
Nov-07
NA
3.06
<0.01
<0.01
May-08
<7
2.90
<0.01
<0.01
Nov-08
NA
2.10
<0.01
<0.01
Dec-09
NA
2.40
<0.01
<0.01
May-10
NA
1.95
NA
NA
Nov-10
NA
2.39
<0.01
<0.01
May-11
NA
2.02
NA
NA
Nov-11
NA
2.15
<0.01
<0.01
May-12
NA
2.47
NA
NA
Nov-12
NA
3.18
<0.01
<0.01
May-13
NA
3.61
NA
NA
Nov-13
NA
3.1
<0.01
<0.01
May-14
NA
3.71
NA
NA
Nov-14
NA
2.42
<0.01
<0.01
May-15
NA
2.9
NA
NA
Nov-15
NA
1.81
<0.01
<0.01
May-16
NA
0.177
<0.01
<0.01
Nov-16
NA
0.177
<0.01
<0.01
May-17
NA
2.51
NA
NA
Nov-17
NA
1.68
<0.0100
<0.0100
May-18
NA
2.09
NA
NA
Nov-18
NA
1.97
<0.0100
<0.0100
May-19
NA
1.97
NA
NA
Nov-19
NA
1.51
<0.0100
<0.0100
May-20
NA
1.32
NA
NA
Nov-20
NA
1.64
<0.0100
<0.0100
May-21
N/A
1.18
N/A
N/A
Nov-21
N/A
1.37
<0.0100
<0.0100
May-22
N/A
1.66
N/A
N/A
Nov-22
N/A
1.54
<0.0083
<0.0083
Page 6 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-21 B
Jun-04
<7
0.0391
<0.01
<0.01
Nov-04
<7
0.047
<0.01
<0.01
May-05
<7
0.0338
<0.01
<0.01
Nov-05
<7
0.0477
<0.01
<0.01
May-06
NA
0.0348
NA
NA
Nov-06
NA
0.0507
NA
NA
May-07
NA
0.0511
NA
NA
Nov-07
NA
0.0686
NA
NA
May-08
<7
0.0557
NA
NA
Nov-08
NA
0.0598
NA
NA
Dec-09
NA
0.0698
NA
NA
Nov-10
NA
0.0534
NA
NA
Nov-11
NA
0.0573
NA
NA
Nov-12
NA
0.0811
NA
NA
Nov-13
NA
0.0665
NA
NA
Nov-14
NA
0.0832
NA
NA
Nov-15
NA
0.092
NA
NA
Nov-16
NA
0.0685
NA
NA
Nov-17
NA
0.071
NA
NA
Nov-18
NA
0.0703
NA
NA
Nov-19
NA
0.0427
NA
NA
Nov-20
NA
0.0357
NA
NA
Nov-21
N/A
0.0372
N/A
N/A
Nov-22
N/A
0.0432
N/A
N/A
Page 7 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-22A
Feb-04
<7
0.67
<0.01
0.0634
May-04
<7
0.322
<0.01
0.0514
Jun-04
<7
1.06
<0.01
0.0449
Nov-04
<7
0.895
<0.01
0.0427
May-05
<7.9
0.722
<0.01
0.0284
Nov-05
<7
0.572
<0.01
0.0268
May-06
NA
0.949
<0.01
0.025
Nov-06
NA
1.12
<0.01
0.0259
May-07
NA
1.13
<0.01
0.0186
Nov-07
NA
1.3
<0.01
0.0213
May-08
<7
1.18
<0.01
0.0242
Nov-08
NA
1.04
<0.01
0.0214
Dec-09
NA
1.25
<0.01
0.0141
Nov-10
NA
1.74
<0.01
<0.01
Nov-11
NA
1.22
<0.01
<0.01
Nov-12
NA
2.05
<0.01
<0.01
Nov-13
NA
1.71
<0.01
<0.01
Nov-14
NA
1.64
<0.01
<0.01
Nov-15
NA
1.69
<0.01
<0.01
Nov-16
NA
1.48
<0.01
<0.01
Nov-17
NA
1.35
<0.0100
<0.0100
Nov-18
NA
0.767
<0.0100
<0.0100
Nov-19
NA
1.44
<0.0100
<0.0100
Nov-20
NA
1.27
<0.0100
<0.0100
Nov-21
N/A
1.2
<0.0083
<0.0083
Nov-22
N/A
1.07
<0.0100
<0.0100
Page 8 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-22 B
Feb-04
<7
2.64
<0.01
0.0323
May-04
<7
1.9
<0.01
0.0346
Jun-04
<7
2.78
<0.01
0.033
Nov-04
<7
2.72
<0.01
0.0362
May-05
<10.8
2.32
<0.01
0.0351
Nov-05
<7
1.22
<0.01
0.0365
May-06
NA
2.46
<0.01
0.0329
Nov-06
NA
2.33
<0.01
0.028
May-07
NA
2.79
<0.01
0.0284
Nov-07
NA
2.62
<0.01
0.0295
May-08
<7
2.42
<0.01
0.023
Nov-08
NA
1.87
<0.01
0.0236
May-09
NA
2.39
NA
NA
Dec-09
NA
2.14
<0.01
0.0265
May-10
NA
2.01
NA
NA
Nov-10
NA
2.14
<0.01
0.0316
May-11
NA
1.75
NA
NA
Nov-11
NA
1.5
<0.01
0.0251
May-12
NA
1.95
NA
NA
Nov-12
NA
2.08
<0.01
0.0243
Nov-12
NA
2.2
<0.01
0.0227
May-13
NA
1.88
NA
NA
Nov-13
NA
1.69
<0.01
0.0222
May-14
NA
2.05
NA
NA
Nov-14
NA
2.8
<0.01
0.0202
May-15
NA
1.73
NA
NA
Nov-15
NA
1.72
<0.01
0.0117
May-16
NA
1.39
<0.01
0.0119
Nov-16
NA
1.62
NA
NA
May-17
NA
1.87
NA
NA
Nov-17
NA
1.62
<0.0100
0.0367
May-18
NA
1.63
NA
NA
Nov-18
NA
1.51
<0.0100
0.0163
May-19
NA
1.71
NA
NA
Nov-19
NA
1.41
<0.0100
0.0352
Nov-20
NA
1.33
NA
NA
May-20
NA
1.35
<0.0100
0.0312
May-21
N/A
1.33
N/A
N/A
Nov-21
N/A
1.06
<0.0083
0.0484
May-22
N/A
1.07
N/A
N/A
Nov-22
N/A
0.986
<0.0100
0.029
Page 9 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-23A
Feb-04
<7
1.5
<0.01
0.115
May-04
<7
1.21
<0.01
0.0928
Jun-04
<7
2.03
<0.01
0.0911
Nov-04
227
1.45
<0.01
0.0769
May-05
278
1.41
<0.01
0.0108
Nov-05
<70
1.29
<0.01
0.0919
May-06
286
0.711
<0.01
0.0823
Nov-06
255
2.01
<0.01
0.0791
May-07
<70
1.51
<0.01
0.0768
Nov-07
<7
1.45
<0.01
0.112
May-08
NA
1.91
<0.01
0.0936
Nov-08
<7
1.97
<0.01
0.0711
May-09
<7
1.34
NA
NA
Dec-09
<7
1.84
<0.01
0.131
May-10
<7
1.96
NA
NA
Nov-10
<7
1.81
<0.01
0.1
May-11
NA
1.3
NA
NA
Nov-11
<7
2.41
<0.01
0.0884
May-12
NA
2.45
NA
NA
Nov-12
<7
3.35
<0.01
0.0772
May-13
120
2.82
NA
NA
Nov-13
146
2.76
<0.01
0.0755
May-14
<100
3.06
NA
NA
Nov-14
329
3.54
<0.01
0.0708
May-15
<5.0
3.24
NA
NA
Nov-15
<50
3.35
<0.1
<0.1
May-16
<50
3.11
NA
NA
Nov-16
189
2.52
<0.01
0.0349
May-17
393
3.04
NA
NA
Nov-17
244
2.99
<0.0100 UJ
0.0696 J
May-18
<50.0
2.76
NA
NA
Nov-18
192
3.54
<0.0100
0.0257
May-19
<5.0
2.65
NA
NA
Nov-19
<50.0
3.09
<0.0100
0.0589
May-20
<50.0
2.92
NA
NA
Nov-20
<50.0
3.47
<0.0100
0.0431
May-21
<5.0
3.26
N/A
N/A
Nov-21
<25.0
3.42
<0.0091
0.0479
May-22
<5.0
3.15
N/A
N/A
Nov-22
<50.0
3.18
<0.0500
<0.0500
Page 10 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-23B
Feb-04
594
1.67
<0.01
0.124
May-04
<7
1.14
<0.01
0.115
Jun-04
<35
1.76
<0.01
0.101
Nov-04
393
1.82
<0.01
0.0857
May-05
<35
1.29
<0.2
<0.2
Nov-05
<35
1.33
<0.01
0.129
May-06
51.9
0.891
<0.01
0.116
Nov-06
907
1.7
<0.02
0.128
May-07
<70
2.29
<0.02
0.0973
Nov-07
<7
1.94
<0.01
0.128
May-08
<7
2.31
<0.01
0.123
Nov-08
<7
2.54
<0.01
0.112
May-09
<7
1.77
NA
NA
Dec-09
<7
2.46
<0.01
0.183
May-10
<7
2.14
NA
NA
Nov-10
<7
2.02
<0.01
0.0768
May-11
NA
2.15
NA
NA
Nov-11
<7
2.49
<0.01
0.0982
May-12
NA
2.39
NA
NA
Nov-12
<7
3.52
<0.01
0.0811
May-13
120
2.72
NA
NA
Nov-13
82.3
2.88
<0.01
0.0759
May-14
381
3.01
NA
NA
Nov-14
542
3.4
<0.0111
0.103
May-15
<5.0
2.78
NA
NA
Nov-15
<50
3.33
<0.01
<0.01
May-16
<50
2.73
NA
NA
Nov-16
516
2.71
<0.01
0.0275
May-17
512
2.62
NA
NA
Nov-17
<5.0
2.63
<0.0100
0.103
May-18
<50.0
2.53
NA
NA
Nov-18
74
3.04
<0.0100
0.0322
May-19
<5.0
3.4
NA
NA
Nov-19
<50.0
3.08
<0.0100
0.0794
May-20
<50.0
2.63
NA
NA
Nov-20
<50.0
3.15
<0.0100
0.0696
May-21
<5.0
2.69
N/A
N/A
Nov-21
<25.0
3
<0.0091
0.0448
May-22
<5.0
2.93
N/A
N/A
Nov-22
<50.0
3.01
<0.0100
0.0512
Page 11 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-24A
Feb-04
7.8
0.0548
<0.01
<0.01
May-04
<7
0.022
<0.01
<0.01
Jun-04
<7
0.0625
<0.01
<0.01
Nov-04
<7
0.0796
<0.01
<0.01
May-05
<7
0.0885
<0.01
<0.01
Nov-05
<7
0.0726
<0.01
0.0111
May-06
NA
0.105
<0.01
0.0102
Nov-06
NA
0.158
<0.01
0.0126
May-07
NA
0.141
<0.01
<0.01
Nov-07
NA
0.161
<0.01
0.0124
May-08
<7
0.159
<0.01
<0.01
Nov-08
NA
0.125
<0.01
0.0124
May-09
NA
0.113
NA
NA
Dec-09
NA
0.15
<0.01
0.0169
May-10
NA
0.135
NA
NA
Nov-10
NA
0.133
<0.01
0.01
May-11
NA
0.102
NA
NA
Nov-11
NA
0.132
<0.01
0.0118
Nov-12
NA
0.218
<0.01
0.011
May-13
NA
0.126
NA
NA
Nov-13
NA
0.158
<0.01
<0.01
May-14
NA
0.189
NA
NA
Nov-14
NA
0.23
<0.01
0.0124
May-15
NA
0.103
NA
NA
Nov-15
NA
NA
NA
NA
May-16
NA
0.188
<0.01
<0.01
Nov-16
NA
0.155
<0.01
<0.01
May-17
NA
0.0437
NA
NA
Nov-17
NA
0.198
<0.0100
0.013
May-18
NA
0.158
NA
NA
Nov-18
NA
0.0313
<0.0100
<0.0100
May-19
NA
0.231
NA
NA
Nov-19
NA
0.214
<0.0100
<0.0100
May-20
NA
0.162
NA
NA
Nov-20
NA
0.182
<0.0100
<0.0100
May-21
N/A
0.226
N/A
N/A
Nov-21
N/A
0.248
<0.0083
0.0091
May-22
N/A
0.25
N/A
N/A
Nov-22
N/A
0.218
<0.0100
0.0104
Page 12 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-24B
Feb-04
<7
0.0586
<0.01
0.0184
May-04
<7
0.0439
<0.01
0.0178
Jun-04
<7
0.0892
<0.01
0.0146
Nov-04
<7
0.082
<0.01
0.0181
May-05
<7
0.0722
<0.01
0.0194
Nov-05
<7
0.0591
<0.01
0.0165
May-06
NA
0.0746
<0.01
0.0178
Nov-06
NA
0.101
<0.01
0.018
May-07
NA
0.0962
<0.01
0.015
Nov-07
NA
0.102
<0.01
0.0158
May-08
<7
0.113
<0.01
0.0151
Nov-08
NA
0.0877
<0.01
0.0178
Dec-09
NA
0.0931
<0.01
0.0226
Nov-10
NA
0.0896
<0.01
0.0151
Nov-11
NA
0.0874
<0.01
0.0144
May-12
NA
0.103
NA
NA
Nov-12
NA
0.118
<0.01
0.0136
Nov-13
NA
0.0918
<0.01
<0.01
Nov-14
NA
0.103
<0.01
0.0101
Nov-15
NA
NA
NA
NA
May-16
NA
0.0998
<0.01
<0.01
Nov-16
NA
0.122
<0.01
0.0102
Nov-17
NA
0.104
<0.0100
0.0178
Nov-18
NA
0.0485
<0.0100
<0.0100
Nov-19
NA
0.0994
<0.0100
0.0123
Nov-20
NA
0.103
<0.0100
0.0104
Nov-21
N/A
0.12
<0.0083
0.012
Nov-22
N/A
0.118
<0.0100
<0.0100
Page 13 of 14

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Parameter
Ethylene
Glycol
1,4-Dioxane
1,1-Biphenyl
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
10
0.003
0.4
0.18
B-32 B
Jun-04
<28
0.176
<0.01
0.0577
Nov-04
162
0.198
<0.01
0.0575
May-05
<14
0.115
<0.2
<0.2
Nov-05
<14
0.072
<0.01
0.0416
May-06
27.6
0.0818
<0.01
0.0617
Nov-06
344
0.0996
<0.01
0.0558
May-07
<35
0.149
<0.01
0.0414
Nov-07
<7
0.117
<0.01
0.0816
May-08
<7
0.0796
<0.01
0.0329
Nov-08
<7
0.173
<0.01
0.0816
Dec-09
<7
0.104
<0.01
0.0621
Nov-10
<7
0.144
<0.01
0.0566
Nov-11
<7
0.0988
<0.01
0.0399
Nov-12
<7
0.0755
<0.01
<0.01
Nov-13
<7
0.0275
<0.01
0.0106
Nov-14
<10
0.0178
<0.01
<0.01
Nov-15
<50
0.0183
<0.01
<0.01
Nov-16
<5
0.0123
<0.01
<0.01
Nov-17
246
0.0152
<0.0100
<0.0100
Nov-18
<50.0
0.0033
<0.0100
<0.0100
Nov-19
<5.0
0.0041
<0.0100
<0.0100
Nov-20
<5.0
0.0034
<0.0100
<0.0100
Nov-21
<5.0
0.0032
<0.0100
<0.0100
Nov-22
<5.0
0.0022
<0.0100
<0.0100
Notes:
mg/L - milligrams per liter
NA - Not Analyzed
Page 14 of 14

Ethylene Glycol(B-01)
2500
JRp
D
� 2000
c
0 1500
C 1000
v
p 500
U
0
L - - - - - - - - - - - - - - - - -
OC` O5 06 01 00 O°j ^O � ^ry �`h n ^5 ^0 � n0 n yo y^ •y`ti
Date
--s-B-01 tNC 2L Standard
Table 8
Time vs. Concentration Plots - Ethylene Glycol
CNA Holdings LLC - Needmore Road Landfill
Salisbury, North Carolina
Ethylene Glycol (B-09C)
J 2500
O
� 2000
c
0 1500
L
1000
c 500
0
U
0-D
boa hoc hoc hoc hoc boa hoc hoc hoc hoc hoc hoc hoc hoc ��c hoc hoc hoc hoc
Ethylene Glycol(B-23A)
450
J 400
E 350
300
L 250
b 200
C
u 150
cc 100
U 50
0
OQ 05 "I
lac lac lac ��c lac lac lac ��c' ��c lac lac lac ��c �,c ��c lac lac lac ��c
Date
B-23A f NC 2L Standard
Date
B-09C f NC 2L Standard
Ethylene Glycol (B-10)
J 1000
O
E aoo
c
0 6077llr�
0
400
is
u
p 200
U
0
lac lac lac lac lac lac lac lac lac lac lac lac lac lac lac lac lac lac lac
Ethylene Glycol (13-2313)
1000
J
a
£ 800
c
0 000
m
c 400
U
p 200
U
0
O& 6 6 01 0 00 ^O ^h N' ^b ^b Nib^0 N\ ^0 ^O 00 ti^ ryry
Fea F. _AFm,�.oF Fad Fad F Fad, Fea Faa 0, FF0, Fzo "0 0,
a Date
B-23B t NC 2L Standard
Date
tB-10 --M-NC 2L Standard
Page 1 of 1

1,4-Dioxane(B-01)
s
a
3
2
1
0
Date
�B-01 tNC 2L Standard
1,4-Dioxane (B-12)
J 5
E4
3
O
2
c 1Aim
m
a 0
0
O
Date
tB-12 tNC2LStandard
1,4-Dioxane (B-23A)
5
4
3
2
1
0
OA p0 06 6 p0 00 ^O ^^ ^r1, ^0 ^P ^r,D ^0 ^1 ^0 ^O .10 ti^ tiry ' 'J ' J ' J ,Jo -30 30 SOS SOS ,Jcc SO- JO '30 'JO 'JO 'O 30 30 ,Jc'
Date
B-23A f NC 2L Standard
Table 9
Time vs. Concentration Plots — 1,4-Dioxane
CNA Holdings LLC — Needmore Road Landfill
Salisbury, North Carolina
1,4-Dioxane (B-09C)
s
a
3
2
1
0
Date
t B-09C f NC 2L Standard
1,4-Dioxane (B-17C)
J 5
E 4
C 3
O
0 2
C 1
N
O 0
0
ci
Date
�B-17C tNC2LStandard
1,4-Dioxane (B-23B)
5
4
3
2
1
0
pP 00 °0 p' 00 00 ^O ^^ ^ti ^0 ^b ^G� ^0 ^'1 ^0 ^0 .y0 rL^ `j`1'
�° �� SO I°o 3§c' �O ��O SOSO'°N 1pc ��O Sic SO '°N 3po' 30 30 �S
Date
—o—B-23B f NC 2L Standard
4
3
2
1
0
1,4-Dioxane (B-10)
Date
tB-10 tNC2LStandard
1,4-Dioxane (B-22B)
s
a
3
2
-------------------
0
�pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc �pc
Date
tB-22B tNC2LStandard
1,4-Dioxane (B-24A)
0.3
0.25
0.2
0.15
0.1
0.05
0
OA Oh 06 '3A 00 00 "3 '�^ ^.1, ""� ^P ^0 ^6 ^1
SO dot' dot' dot' dot' � � S§c SO SO SO SO
SO
SOc SOc SO
Date
B-24A tNC2LStandard
Page 1 of 1

Diphenyl Ether (B-01)
J 0.5
E 0.4
0.3
0
m 0.2
r 0.1
C 0
01C 01C �JC �JC - fit" 01C �JC �JC 01C 0C �sC
Date
4B-01 tNC2LStandard
0.5
J
0.4
c 0.3
O
0.2
Table 10
Time vs. Concentration Plots — Diphenyl Ether
CNA Holdings LLC — Needmore Road Landfill
Salisbury, North Carolina
Diphenyl Ether (B-12)
J 0.12
0.1
c
0.06
O 0.06
° 0.04
y 0.02
C 0
tiry
HOC sOC ssC �JC �`�(' �JC SO �JO �JC HOC
Diphenyl Ether (B-23A)
Date
tB-12 —0— NC 2L Standard
c 0.1
d
c
c 0
O 5 0 '� 0 0 0 N `I. ^� P h 6 '�
U Off' p p O O O '� '� '�0 '�0 `L0 `L 'L
Date
t B-23A t NC 2L Standard
J 0.5
E 0.4
c 0.3
O
R 0.2
Diphenyl Ether (B-10)
s
J
E n
3
0
2
c 1
U
C
U pa p0 p0 IA p0 p0 IS' IN 0 IO 1P N5 ^O N1 n- NO tip ti� Nry
HOC HOC HOC SJC SJr SO SJC 11OC HOC -OC HOC sJC sJC SOS -OC sJC sJr HOC
Diphenyl Ether (B-23B)
Date
tB-10 tNC2LStandard
c 0.1
d
C1
C 0
1) O ti O P 5 0 A 0 0
It' 06 00 p1 00 O°' ^O '�^ N�. �. '� '� �. �. �.
Date
+B-23B f NC 2L Standard
Page 1 of 1

Corrective Action Evaluation Report
Project Number: 60683034
Figures
AECOM

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User Community
COM 1360 Peachtree NE
� Atlanta, GA 3030309
T: [phone]
FIGURE 1
SITE LOCATION MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
NOVEMBER 2023 60313404
e)ISite Location Map.mxd Splawn, M

C7
B-09C
CONDA B-21
C= SITE
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P REMEDIATI
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L=com
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® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATIONS
INTERMITTENT SEEP SAMPLING LOCATIONS
— — SITE BOUNDARY
sw-a
± 1000 FT DOWN STREAM
OF COOLEEMEE WEIR
N
pr 500' 1,000'
SCALE
FIGURE 2
SITE LAYOUT MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
603
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a
b
B-09C e9
0
1ti B-1
\
LEGEND
®
MONITORING WELL LOCATION
®
SURFACE WATER SAMPLING LOCATIONS
®
INTERMITTENT SEEP SAMPLING LOCATION
— —
SITE BOUNDARY
J---
-
TOPOGRAPHIC CONTOUR
": CSW-2 WAS DRY AND THEREFORE NOT SAMPLED.
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CSW-1
B-22B
B-23B
2 A
m
B-24A
0
B-01®
3-
1° 1
1 6
® 70
� 71
ti I
1� V
1 1,
1 6 0. 400' 800'
7z a
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FIGURE 3
SAMPLE LOCATION MAP
P"=COM MAY 2022
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
60313404
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o B-09C °
1ti
J
SW-3 SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
Q
A
O
V
® J
-1
�-5
22B P
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B-23B
2 A
B-24B
m
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0 MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATIONS
INTERMITTENT SEEP SAMPLING LOCATION
SITE BOUNDARY
TOPOGRAPHIC CONTOUR
SW-8
± 1000 FT DOWN STREAM
OF COOLEEMEE WEIR
I
N
°1
,70
I
ti I
1
0r 400' 800'
SCALE
FIGURE 4
SAMPLE LOCATION MAP
NOVEMBER 2022
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
60313404
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B-09C
1673,831
0t,
(77
rno
0
72o--
705
A\
710 =�
B-32B
[712.44]
rn
can rn 0'
ov o
B-21 B
[663.181
1 B-12 B-17B _ I
fFi-,� 7R1 i
LEGEND
MONITORING WELL LOCATION
GROUNDWATER CONTOUR
(DASHED WHERE INFERRED)
GROUNDWATER FLOW DIRECTION
[657 281 GROUNDWATER ELEVATION (ft msh
B-17C
[658.64]
B-22B
[657.00]
B-22A
[657.28]
- B-23B
[657.20]
-B-23A
[657.04]
B-24B
[655.91] j
�B-24A
[654.90]).
I /
I
0 M 400 m
SCALE DI FEET
FIGURE 5
GROUNDWATER POTENTIOMETRIC SURFACE MAP
NOVEMBER 2022
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
60683034
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/' 1 0
Q �
B-09C
/ 0.935/0.909
70
`N
/ lo�
a
SW-3 <0.0020
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
LEGEND
G MONITORING WELL LOCATION
® SURFACE WATER SAMPLING LOCATION
® INTERMITTENT SEEP SAMPLING LOCATIONS
1.07 1,4-DIOXANE CONCENTRATION (mg/L)
J-0.003— 1,4-DIOXANE ISOCONCENTRATION CONTOUR (mg/L)
(NC 2L STANDARD)
NOTES:
CSW-2 Locations not sampled or analyzed for 1,4-dioxane are not shown.
l'NC2L - North Carolina Administration Code, Title 15A, Subchapter 2L.
� S -5
B-22B < .0020
0.986
B 07
o
B-23B�
3.01
s
.18
B-24B
0.118
6.2 7
� <0. 20
gg o
®1.58
P"=COM
Sal—
SW-8 <0.0020
000 FT DOWN STREAM
,F COOLEEMEE WEIR
,d d I
N
01
,70
I
ti I
01 400' 800'
1
SCALE
FIGURE 6
1,4-DIOXANE ISOCONCENTRATION MAP
NOVEMBER 2022
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
60313404
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0
\S1
I e
i
SW-3 <0.0087
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
LEGEND
® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
<0.0100 1,1-BIPHENYL CONCENTRATION (mg/L)
— 0.1 — 1,1-BIPHENYL ISOCONCENTRATION CONTOUR (mg/L)
(NC 2L STANDARD)
® � NOTES:
Locations not sampled or analyzed for 1,1-biphenyl are not shown.
All concentrations are below the North Carolina Administration Code, Title 15A,
g � Subchapter 2L standard (0.4 mg/L)
S -5
�B-226 " J < \0087
<0.01.0 \
\ 0900\�\ \ <0. SW-7
0
® B0?0500
SW-8 <0.0087
1000 FT DOWN STREAM
DF COOLEEMEE WEIR70
0.1
�4d N
10
1
� .118 1"
1 6
❑ 6A I
� 71
P"=COM
p. 400' 800'
SCALE
FIGURE 7
1,1-BIPHENYL ISOCONCENTRATION MAP
NOVEMBER 2022
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
6031340.
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0
\S1
1 � W
a
b
0
<0. 35/<O. 43 l e9
0
1ti B-12
<0.0 E
II SW-3 <0.0087
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
W-5
0.0087
<0.0087
® BO 0500
0.18
�10
� .19
P"=com
SW-8 <0.0087
1000 FT DOWN STREAM
OF COOLEEMEE WEIR
400' 800'
SCALE
FIGURE 8
DIPHENYL ETHER ISOCONCENTRATION MAP
NOVEMBER 2022
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
6031340
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Corrective Action Evaluation Report
Project Number: 60683034
Appendix A
Sample Field Sampling Forms
AECOM

Well/Piezo ID:
Ground Water Sample Collection Record
Client: CNA HOLDINGS/NRLF Date:
Project No: Time: Start am/pm
Site Location: Woodleaf NC Finish am/pm
Weather Conds: Collector(s) A Hill, J Leaver
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer ❑
a. Total Well Length c. Casing Material _ SS e. Length of Water Column
b. Water Table Depth d. Casing Diameter 2" f. Calculated Well Volume (see back)
WELL PURGING DATA
a. Purge Method Purge Rate ml/min
b. Acceptance Criteria defined (from workplan)
Minimum Required Purge Volume (@ well volumes)
Maximum Allowable Turbidity NTUs
Stabilization of parameters
c. Field Testing Equipment Used: Make Model
Serial Number
d. Acceptance criteria pass/fail
Yes
Has required volume been removed
❑
Has required turbidity been reached
❑
Have parameters stabilized
❑
If no or N/A - Explain below.
SAMPLE COLLECTION:
Method: PUMP TUBING
No N/A
❑ ❑
❑ ❑
❑ ❑
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1,4 DIOXANE/8260
VOA
3
HCL
VOCs/8260
VOA
3
NONE
EG/8015
L a
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
VAR
I VAR
IVAR
I EX MNA
Comments Fe+2 = mg/I START STRIPPING COLLECT H2 SAMPLE
Signature Date
(a-b)

Corrective Action Evaluation Report
Project Number: 60683034
Appendix B
Sample Chain of Custody Form
AECOM

Eurofins Savannah
5102 LaRoche Avenue Chain of Custody Record ,;: eurofins EnvironmentTesting
Savannah, GA 31404
Phone [phone] Phone [phone]
Client Information
Sampler:
Lab PM:
Lanier, Jerry
IJer
Carrier Tracking No(s):
COC No:
Client Contact:
Phone:
E-Mail:
Lanier(a)et.eurofinsus.com
State of Origin:
Page:
Page 1 of 1
Company:
PWSID:
Analysis Requested
Job #:
Address:
Due Date Requested:
o
Z
y
�
m
')
p
°
d
=
2
ii
Z
p
�
}
U,
?
�
E
a
1
1
1
1
1
1
1
1
1
1
1
•�
c
`o
'
z
R
Preservation Codes:
A - HCL M - Hexane
B - NaOH N - None
C - Zn Acetate 0 - AsNa02
D - Nitric Acid P - Na204S
E - NaHSO4 Q - Na2SO3
F - McOH R - Na2S203
G - Amchlor S - H2SO4
H - Ascorbic Acid T - TSP Dodecahydrate
I - Ice U - Acetone
J - DI Water V - MCAA
d K- EDTA W- pH 4-5
C
L - EDA Z -other (specify)
0 Other:
City:
TAT Requested (days):
State, Zip:
Compliance Project: A Yes No
Phone:
PO #:
Purchase Order Required
Email:
WO #:
Project Name:
Project #:
Site:
SSOW#:
Sample Identification
Sample Date
Sample
Time
Sample
p
Type
(C=comp,
G=grab)
matrix
(w=water,
s=sord,
o=w te/oi4
BT=Tissue,
A=Air
N
E
Special Instructions/Note:
Preservation Code:
Possible Hazard Identification
= Non -Hazard = Flammable Skin Irritant Poison B Unknown Radiological
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
= Return To Client 0 Disposal By Lab Archive For Months
Deliverable Requested: I, II, III, IV, Other (specify)
Special Instructions/QC Requirements:
Empty Kit Relinquished by:
Date:
Time:
Method of shipment:
Relinquished by:
Date/Time:
Company
Received by:
Date/Time:
Company
Relinquished by:
Date/Time:
Company
Received by:
Date/Time:
Company
Relinquished by:
Date/Time:
Company
Received by:
Date/Time:
Company
Custody Seals Intact:
A Yes A No
Custody Seal No.:
Cooler Temperature(s) °C and Other Remarks:
Ver: 01/16/2019

Corrective Action Evaluation Report
Project Number: 60683034
Appendix C
Well Location Map
AECOM

0
N
B-29B
37Z28B T—
®B-28A B 2
PT-3
EXT-1 EXT-13
EXT�11
B-16
EXT-101
B-0
A PT-
-27
20A
B-20C
20B /
;e;:
—09
=XT7
—0�
EXT
E T 1
T 5
—1
—19B
1
- 2 A �' EXT-5
B B-21A PT-11
C B-21B 17C EXT E`XT-6 .
B-12� B-22B
XT-4 B-22A
\�17B
T-1 PT 1 EXT-3
XT-19 �2 EXT-7
Qso T— 2 �2 ; s6
23A
X 27
3�T B-40
—2
—2 \��.�`I PT-10)
EXT-23- s� B-24B /
B-24A
B13P —24C :X
B � 24PT)�
B-1 B-25� —
B-0 _ l
B-01 A
B-14 AB-10 B,� 6 /j5 8 � —35
70
EX7-24 B-3
` 32B „ (EXT- 6) ❑
0
B 324 B-30B °
�-37B B-33A ` B®30A
E 25
B 37-33B — — - B15
B-31
• � B-31 B
P"=COM
LEGEND
® MONITOR WELL LOCATION
EXTRACTION WELL LOCATION
PACKER TEST LOCATION
0 200 400 800
SCALE IN FEET
FIGURE 1
WELL LOCATION MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
NOVEMBER 2023
\\na.aecomnet.com\LFS\AMER\Greenville-USGRNI\Legacy\Group\earth\ATLANTA Cadd Files\79747 Salisbury (Needmore)\Monitoring Well Location Map_Nov2023.dwg, 11/13/2023 10:22:12 AM, Adobe PDF

Corrective Action Evaluation Report
Project Number: 60683034
Appendix D
Field Notes — May 2022 and November 2022
AECOM

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Surface Water Collection
Client: CNA HOLDINGS Date: 5/ /22
Time: Start am/pm
Location: Salisbury, NC NRLF Finish am/pm
Weather: Collector(s) RON HIL JEFF LEAVER
r
Field Testing Equipment Used: Make Model Serial Number
YSI PRO + VIA1010ffl
Hach 2100 —493w D 9 t%OG
Point
I
TURBIDITY
0990M
—M
ff ■
3�
Container Type No'. of Containers Preservation Analysis Time
VOA 3 HCL 1,4 DIOXANE
L(a) 2 NONE DOWTHERM A
VOA 3NONE C EG
Signature Date 5/ /22 -

' Well/Piezo l� a�T
i
Ground Water Sample Collection Record
Client: CNA HOLDINGS/NRLF Date: 5/ to /22
Project No: Time: Start � am/pm
Site Location: Woodleaf NC Finish 107 � am/pm
Weather Conds: Collector(s) A Hill J Leaver
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer LJ
a. Total Well Length N/A c. Casing Material _ SS e. Length of Water Column N/A
b. Water Table Depth 330 d. Casing Diameter 2" f. Calculated Well Volume (see back)_ N/A
WELL PURGING DATA
a. Purge Method Low Flow Purge Ratel 190 ml/min
b. Acceptance Criteria defined!,(from workplan)
Minimum Required Purge Volume (@ _NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO + 19E100247
Hach 2100Q 73945
rmmW1
�.11l
Enm
11111111M��M,
I 1I��ACI���MIM
d. Acceptance criteria pass/fait Yes No N/A
Has required volume been removed F2T
0 ❑❑
Has required turbidity been reached
Have parameters stabilized ❑
If no or N/A -Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
,Z
VOA
3
HCL
1,4 DIOXANE/8260
Q
_
-QDwX4effn-A
---
VAR
VAR
VAR
MNA<'
Comments Fe+2 = (a mg/I
Signature Date _ 5/ l /22

Well/Piezo ID: r
Ground Water Sample Collection Record
Client: CNA HOLDINGS/NRLF Date: 5/ 1(6 /22
Project No: Time: Start `D 3 ® am/pm
Site Location: Woodleaf NC Finish i l i "z am/pm
Weather Conds: . SLr"PJt / Collector(s) A Hill J Leaver
—r
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer ❑
a. Total Well Length N/A c. Casing Material _ SS e. Length of Water Column _ N/A
b. Water Table Depth d. Casing Diameter 2" f. Calculated Well Volume (see back) N/A
WELL PURGING DATA
a. Purge Method Low Flow Purge Rateo200ml/min
b. Acceptance Criteria defined .'(from workplan)
- Minimum Required Purge Volume (@ _NA well volumes) NA.
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters I 10%
c. Field Testing. Equipment Used: Make Model Serial Number
YSI PRO+ �19�� Oki toaq
Hach 2101) 2 ;19946 ® � 47-0 C
•11111IM!
IM11111111
N &W- I
rM R
M
M�N=
I
��'®
1111�,14SIM.
_•j1111111
FaM0
&JsNll
Illix"
RIM
R�KMI
-1W.TJ
Win
:.�.��■�
ra
®��
���■
®ate
��
��
�111110.�.
®s►.rr01ff"M
®
d. Acceptance criteria, pass/fail Yes No N/A
Has required volume been removed ❑ ❑
Has required turbidity been reached El 0
Have parameters stabilized ❑ ❑
If no or N/A - Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID Container Type No. of Containers Preservation Analysis Time
VOA-
3
HCL
1;4.DIOXANE/8260
p
VAR
VAR
VAR
MNA
Comments Fe+2 = mg/I
op Ll
Signature Date_ 5/ /22

Well/Piezo ID: �3
Ground Water Sample Collection Record
Client: CNA HOLDINGS/NRLF Date: 5/ p(a /22
Project No: Time: Start ®� am/pm
Site Location: Woodleaf NC Finish �i t t° am/pm
Weather Conds: S Collector(s) ill J Leaver
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer ❑
a. Total Well Length N/A c. Casing Material _ SS e. Length of Water Column _ N/A
b. Water Table Depth D ,[3 d. Casing Diameter 2" f. Calculated Well Volume (see back) _ N/A
WELL PURGING DATA
a. Purge Method Low Flow Purge Rate 1 ® (Al/min
b. Acceptance Criteria defined ,(from workplan)
- Minimum Required Purge Volume (@ _NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters ! 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO + 19E100247
Hach 2100Q 73945
It�Tn'�y�7�l��Ig
NUMM
I. &S
MayrW.up
"411111���ll�����
d. Acceptance criteria pass/fail Yes No N/A
Has required volume been removed ❑ ❑
Has required turbidity been reached ❑
Have parameters stabilized' [ ❑ ❑
If no or N/A - Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1,4 DIOXANE/8260
II&S`
R,
VOA
3
NONE
EG/8015
u
r-•
s"A
-�
.�
VAR
VAR
VAR
MNA
Comments Fe+2 = 3 r0 mg/1
Signature Date 5//22

u
Well/Piezo ID:
Ground Water Sample Collection Record
Client: CNA HOLDINGS/NRLF Date: 5/ 1/:4 /22
Project No: Time: Start tk . am/pm
Site Location: Woodleaf NC Finish J";%0 am/pm
Weather Conds: r - ^'�,, a� i,�9U<i Collector(s) i eaver
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer ❑
a. Total Well Length N/A e. Casing Material _ SS e. Length of Water Column _ N/A
b. Water Table Depth �r�p�'. d. Casing Diameter 2" f. Calculated Well Volume (see back) N/A
WELL PURGING DATA
a. Purge Method Low Flow Purge Rate /40 ml/min
b. Acceptance Criteria defined i(from workplan)
Minimum Required Purge Volume (@ _NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of. parameters! 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO + 19E100247
Hach 2100Q 73945
d. Acceptance criteria pass/fail Yes No N/A'
Has required volume been removed ❑ ❑
Has required turbidity been reached ❑ ❑
Have parameters stabilized ❑ ❑
If no or N/A Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID
Container Type—
i,No. of Containers
Preservation
Analysis
Time
113-2313
VOA
3
HCL
1,4 DIOXANE/8260
<<
VOA
3
NONE
EG/8015
rc'
.yMN
®ewe B
�—"—
`
VAR
VAR
VAR
MNA
tr
Comments Fe+2 = 131 mg YI
Signature Date_ 5/ /22

Well/Piezo ID:
Ground Water Sample Collection Record
Client: CNA HOLDINGS/NRLF Date: 5/l� /22
Project No: Time: Start (la am/pm
Site Location: Woodleaf NC Finish am/pm.
Weather Cords: ,SfiNN'(/ 9t Collector(s) A Hi J Leaver
WATER LEVEL D TA: (measured from Top Well ❑ Piezometer ❑
a. Total Well Length N/A c. Casing Material- _ SS e. Length of Water Column _ N/A
b. Water Table Deoth d. Casing Diameter 2" f. Calculated Well Volume (see back) — N/A
WELL PURGING DATA
a. Purge ethod Low Flow Purge RateO<—y min
b. Accep ance Criteria defined (from workplan)
- Minim m Required Purge Volume (@ _NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO + 410208Q
Hach 21 Ogf -Fe9#5 0 9 d Z0 L
d. Acceptance criteria pass/fail Yes No N/A
Has required volume been removed ❑ ❑
Has required turbidity been reached ❑ ❑
Have barameters stabilized - ❑ ❑
If N/A Explain below.
SAMPLE
Method: PUMP TUBING
No. of Containers Preservation. Analysis Time
Sample ID
;Container Type
VOA
3
HCL
1,4 DIOXANE/82600-09
.-
L a
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
Comments Fe+2
mg/I
Date _51e,C /22

Well/Piezo ICiM
3j 2 2
Ground Water Sample Collection Record
Client:
CNA HOLDINGS/NRLF
Date: 5/ t (P /22
Project No:
Time: Start t"a t
am/pm
Site Location:
Woodleaf NC I
Finish f15 3
am/pm
Weather Conds:
XroRg Collector(s)
A Hill J Leaver
WATER LEVEL D
TA: (measured from Top
Well ®
Piezometer
❑
a. Total Well Lengt
N/A c. Casing Material _
SS
e. Length of Water Column _
N/A
b. Water Table De
th d. Casing Diameter
2"
f. Calculated Well Volume (see
back) _ N/A
WELL PURGING
ATA
Purge Rate��ml/min
a. Purge
Method Low Flow
b. Acceptance
Criteria defined ';(from workplan)
Minim
im Required Purge Volume (@ _NA
well volumes)
NA
- Maxirr
um Allowable Turbidity NA
NTUs
-Stabilization
of parameters 10%
c. Field Testing
Equipment Used: Make
Model
Serial Number
YSI
PRO +
19E100247
Hach
2100Q
73945
Volume
TEMP
pH
Spec. Cond -
TURBIDITY
D.O.
ORP
Time
Remove
ml
C
S'.U.
umhos
NTUs
m /I
MV
Odor
DTW
7,10
INT
a
/V10
1 If S ;cv. %P0, ov I- i ► s�
60 i r1,47
r,
d. Acceptance criteria pass/fail Yes No N/A
Has required volume been removed ❑ ❑
Has required turbidity been reached ❑
Have parameters stabilized' ❑ ❑
If no or N/A - Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING`r ,
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time''`
VOA
3
HCL
1,4 DIOXANE/8260
V9,A
.J96t4-&
m A
VAR
VAR .
VAR
MNA
e'
Comments . Fe+2 = 3 r
Signature

Well/Piezo ID��®��; I
Ground Water Sample Collection Record
Client: C NA HOLDINGS/NRLF Date: 5/ 16 /22
Project No: Time: Start'?RT am/pm
Site Location: Woodleaf NC Finish am/pm
Weather Conds: , '10"S Collector(s) A Hill J Leaver
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer El
r `' a. Total Well Lengt N/A c. Casing Material _ SS e. Length of.Water Column. N/A
b. Water Table Depth d. Casing Diameter 2" f. Calculated Well Volume (see back) _ N/A
WELL PURGING ATA r
a. Purge I vlethod Low Flow Purge Rate !� ml/min
b. Acceptance Criteria defined (from workplan)
Minim im Required Purge Volume (@ _NA_ well volumes) NA
- Maxirr um Allowable Turbidity NA NTUs
- Stabill zation of parameters! 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO + 19EI00247
Hach 21OOQ 73945
go 011WRI,���;r�c��,�r�s�it,�a�:�■r�
�u�`I'1�pe����
fir, j,��-A
■MlL��1I'MMIMMMIX,
fir•
��y�
d. Acceptance
Has required
Has required
criteria pass/fail Yes
volume been removed
turbidity been reached
No
❑
N/A
❑
Have
Darameters stabilized'
❑
❑
If
io or N/A - Explain below.
SAMPLE COLLgCTION: Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
Vf ©rAc,
VOA
3
HCL
1,4 DIOXANE/8260
VOA
3
NONE
EG/8015
t(
V-a
44elm-
_D+awT+emrA
. r..
C,
VAR
VAR
VAR
MNA
f�
Comments Fe+2 =
Signature

Well/Piezo
Ground Water Sample Collection Record
Client: C NA HOLDINGS/NRLF Date: 5/ tG /22
Project No: ITime: Start HZ2 am/pm
Site Location: Woodleaf NC Finish �S2a am/pm
Weather Conds: Collector(s) A Hil J Leaver
WATER LEVEL DATA: (measured from Top Well ❑ Piezometer El
a. Total Well Lengt N/A c. Casing Material _ SS e. Length of Water Column _ N/A
b. Water Table Depth 'Of d. Casing Diameter 2" f. Calculated Well Volume (see back) _ N/A
WELL PURGING DATA
a. Purge Method Low Flow Purge Rate 1(9 ® ml/min
b. Acceptance Criteria defined from workplan)
- Minimum Required Purge Volume (@ _NA well volumes) NA
- Maxi um Allowable Turbidity NA NTUs
- Stabilization of parameters', 10% j
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO + 19E100247
Hach 21000 ` 73945
�� •�
- WAAK
_tNEWNM,
itt�illllr�r�ll�i
t:��l���r'lIC
.�{LpR"��T'���'J
�■_■_•slll�l�ll��l�lelll�
®�a�®
d. Acceptance criteria pass/fail Yes No N/A
Has required volume been removed ❑ ❑
Has required turbidity been: reached ❑ ❑
Have parameters stabilized ❑ ❑
If no or N/A - Explain below.
SAMPLE COLLE CTION: Method: PUMP TUBING
Sam Ie ID
Container Type
No. of Containers
Preservation
Analysis
Time
16-01
VOA
3
HCL
1,4 DIOXANE/82 o0
v
VOA
3
NONE
EG/8015
rr
VAR
VAR
VAR
MNA
e
Comments Fe+2 = An m /I
Signature Date-5/ /22

Well/Piezo
414
Ground Water Sample Collection Record
Client:
GNA HOLDINGS/NRLF
Date: 5/ (� /22
Project No:
Time: Start tG3D am/pm
Site Location:
Woodleaf NC
Finish L am/pm
Weather Conds:
S ollector(s)
A Hill J Leaver
r
WATER LEVEL DATA:
(measured from Top
Well [g Piezometer ❑
a. Total Well Length
N/A c. Casing Material _
SS
e. Length of Water Column _ N/A
�d3g
b. Water Table Depth
th d. Casing Diameter
2"
f. Calculated Well Volume (see back) _ N/A
WELL PURGING CATA
Purge
RateLS®
a.
ethod Low Flow
Purge
ml/min
b. Acceptance
Criteria defined (from workplan)
- Minimum
Required Purge Volume (@ _NA_
well volumes)
NA
-Maximum
Allowable Turbidity NA-
NTUs
- Stabili
ation of parameters 10%
c. Field T
sting Equipment Used: Make
Model
Serial Number
YSI
PRO +
19E100247
Hach
2100Q
73945
LEM=®�
..
�®
• •
®
•..
MIME!
I�II►���!�
r. ..� �IIIIII��u�7[
r61?M111116iv�Mf�
A��
/►ROW
I��i���,pIII�3r�Illllll•
�`� 1 _i]
a
vlSr."..y=-�i1��'���i�`7Q�}�.•tL%-
7Wdii
f��,;A.:�+9�P_7
----®��i®_e•�®
d. Acceptance
criteria pass/fail' Yes
No
N/A
Has required
volume, been removed
El
n
Has required
turbidity; been reached
El
El
Have parameters
stabilized
❑
❑
If no
or N/A - Explain below:
SAMPLE COLLECTION:
Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
-(
VOA
3
HCL
1,4 DIOXANE/826o
d'2
VOA
3
NONE
EG/8015
L a
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
Comments
e+2 = 25 m /l
C4I
3-9q-0Sf 6?rL a7
100 )
Signature
Date _ 5/ /22

..... .....
tyl,% Sje 1&,�r
4.1 L-ot-elion
. WSA
701.
Led QJ
vy)
VV
(y
co latw,
re,45 0�
01, JOA
(ea Cc AfCA-� 5"IlL�
LAVA
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ZZA,

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rw-- =tm3

TAILGATE
SAFETY MEETING
EFM,, Inc. PROJET: C f s,*,b,,, Nc
pRor=c T NO.:
TYPE OF-TWORM
H&S
f ReviSw
1(1nG-- c . U' 3
ATFENDEES
Ramp qwym�
ZA
�. ! t DAI + I L� �L
sptm -21Qr

EQUIPMENT CALIBRATION FORM
Client: Project
'NSTRUMENT: YS L G +
SERIAL NO.:11 �plgw� fO3 fito C-
Calibration
Date
Time
Parameter
Reading
_
Calibration Recorded B J
'
4.00
Lot# 6 C, cl 33 Exp. 3 v
-r
Lot# a( 3 Exp. 7 2:4
7.00
w �` , v
I pH 10.00
r 0- e0
Lot# ') GC, 3 a 1 Exp: 3
S ecific Conductivityjr�
S
LDt# ;.qb t? 0 Exp. Z?
}
ORP
`r.�
i �L1i'L i7Cn L
I
Dissolved Oxygen
ITurbidity
L
Tem erature
E
Ambient Air Pressure
NSTRUMENT:
'ERIAL NO.:
Date
Time
Parameter
Calibration
Reading
Calibration Recorded 13
4.00
7.00
PH 10.00
Lot# Exp:
Lot# Exp:
Lot## Exp:
Specific Conductivity
Lot# Exp-
ORP
Dissolver) Oxygen
Turbidi
V , j
Temperature
Ambient Air Pressure

EQUIPMENT CALIBRATION FORM
Client: € - rf{ Project #.-
4
INSTRUMENT--.j L ?RIO+ 2i60 Q
SERIAL_ NO.. j a /���q-T 1
Calibration
Cate
Time
Parameter
Reading
Calibration Recorded B
4.00
Lot# C, 33 Exp: 3 Z./
7.00
�,
Lot# ' G t..1 ii, 3
10.00
(�. �L,
Lot# cal i Exp: 3 �l
Specific Conductivity
j, V3 U�
Lot# ;�qb i? U Exp- -�
ORP
,
_
Dissolved Oagen
Turbidity
' 0/cam
Temperature
Ambient Air Pressure
NSTRUMENT: (/i G too
`SERIAL NO.; Njg J,�-7 L 3L
Date
Time
Parameter
Calibration
Reading
Calibration Recorded B
r.'�'
4.00
7.00
pN 10.00
L,7 ;,
Lot# Exp--
7 oz,
Lot# Exp:
16-,: i
Lot# Exp.
Specific ConductiviV
Lot# Exp:
ORP�
4 !
Dissolved Oxygen
v
s�v
Turbidity
Temperature
1
Ambient Air Pressure

Surface Water Collection
Client: CNA HOLDINGS
Location; Salisbury, NC NRLF
Weather: fig, (,, 015 Collector(s) A Hill, S Leaver
Date: 111 j 122
Time: Start am/pm
Finish am/pm
0 Field Testing Equipment Used: Make Model Serial Number
YS1 PRO+ 19E100247
Hach 21OOQ 73949
Sample
Point
TEMP
C
I pH
S.U.
Spec- Cond
(umhos}
TURBIDITY
NTUs
D.O.
m 11
ORP
MV
Sample
Time
Notes
CSW-1
bA-'f
CSW-2
U'
L
i
SW-3
l3 7
—7-02-
3 _5
$ _3
SW-5
S''VV-7
�:3•s
C-151
L2S.3
SW-S
[vu ",l
cr{Y
3 :4'
}
.'i`i
ail✓' _
; r� E
Method: GRAB SAMPLE
Container Type
No. of Containers
Preservation
Analysis
Tme
fa)
VOA
3
HCL
1,4 DIOXANE
y,
L(a)
2
NONE
DOWTHERM A
VOA
3NONE
EG
Signature
Date _ 111 1 122

Well/pie z ID:
%-2gA
Ground Water Sample Collection Record
Glient: CNA HOLDINGSINRLF Date: 111 f /22
Project No. Time' Start i3 va. arnlpm
Site Location Woodleaf NC Finish i 3q� amlpm
)heather Conds: -7i7m Collector(s) A Hill„Leaver
v
WATER LEVEL DATA: {measured from Top Well ❑ Piezometer ❑
a. Total Well Length NIA�7 , o. Casing Material —SS e. Length of Water Column NIA
b. Water Table Depth fit: W d. Casing Diameter 2" f. Calculated Well Volume (see back) NIA
WELL PURGING DATA
a Purge Method Low Flow Rum Rate i 00 mllmin
b. Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used' Make Model Serial Number
YSI PRO+ ' { g{ Q ZY7
Hach 2100Q 7 21 5P
OEM
d. Acceptance criteria pass/fail
Yes
No
NIA
Has required volume been removed
®
❑
❑
Has required turbidity been reached
®
❑
❑
Have parameters stabilized
1
❑
❑
If no or NIA - Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID
Container Type
No of Containers
Preservation
Analysis
Time
VOA
3
HCL
1.4 DIOXANE18260
", Ll
ti
VOA
3
HCL
V4Cs18260
a
VOA
3
NONE
EG18015
-,
L(a)
2
NONE
DowTherm A
•�
VAR
VAR
VAR
MNA
—�
VAR
VAR
VAR
EX MNA
,_J
Comments Fe+2 = r m n V. START STRIPPING r COLLECT H2 SAMPLE
Signature Date 111 1 122

WeiUPiezo IQ: 13 — n
Ground Water Sample Collection Record
client: CNA HOLDINGSINRLF Date. 111 122
Droject No: Time: Start j 1 o am/pm
site Location: Woodleaf NC Finish amlpm
Heather Conds: 5itev�V ICollector(s) A HillJ Leaver
WATER LEVEL DATA: (measured from Top
a. Total Well Length NIA c. Casing Material _ SS
b. Water Table Depth 13, 41�- d. Casing Diameter 2"
WELL PURGING DATA
Well ❑ Piezometer ❑
e. Length of Water Column NIA
f. Calculated Well Volume (see back), NIA
a. Purge Method L Flow Purge Rate2M mllmin
b. Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ —NA_ well volumes) NA
- Maximum Allowable Turbidity NA NTLIs
- Stabilization of parameters 10°%
c. Field Testing Equipment Used: Make Model Serial Numbar
.
YSI PRO+
Hach 2100Q —"
d. Acceptance criteria passlfail Yes
No
NIA
Has required volume been removed
❑
❑
Has required turbidity been reached
❑
❑
Have parameters stabilized
❑
M
If no or NIA - Explain below.
SAMPLE COLLECTION:
Method- PUMP TUBING
Sample ID
Container Type
No of Containers
Preservation
Analysis
Time
`
VOA
3
HCL
1.4 DIOXANE182En
hKW
Vow
td E
EG $94
L(a)
2
NONE
DowTherm A
VAR
VAR
VAR
MNq
VAR
VAR
IVAR
EX MNA
Comments Fe-2 = Q., V.rngll _ START STRIPPING ( W 6 COLLECT H2 SAMPLE t �a,TO
Signature '1 T Date III ( 122

WeINPiezo ID•
!`r-
Ground Water Sample Collection Record
Bent: CNA HOLDINGSINRLF Date: 111 F I22
rolectNo: Time: Start t356' amlpm
tie Location: Waodieaf NC Finish31 am/pm
Veather Conds: _ Y . �� Collector(s) A ililf, JfLeaver
WATER LEVEL DATA: (measured from Top Well Q Piezometer ❑
a. Total Well Length NIA c. Casing Material _ SS e. Length of Water Column _ NIA
Sw
6. Water Table Depth 3 Dg d. Casing Diameter 2" f. Calculated Well Volume (see back)
WELL PURGING DATA
a. Purge: Method Low Flow Purge Rate ! 7 (I ml/min
b- Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ ____NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- StabiIization of parameters 10%
c. Field Testing Equipment Used-. Make Model Serial Number
YSI PRO+ j r1;I,,W 7
Hach 210DQ
Time
Volume
Removed [m!
TEMP
C
pH
S.U.(umhos]
Spec. Cond
TURBIDITY
NTUs
D.Q.
m /I
ORP
MV
Odor
DTW
r3SS
INT
/poi
709
7a 0
abf
iiLS
Vi
_X;
r r-�r
• Z
-.fie .7' -
-34
i 1. o-q
2 oac
S T
'i t
r41
2 ca
1 S
��F
74
Alt)
d. Acceptance critena passlfall Yn
N❑o
Nl❑A
Has required volume been removed
Has required turbidity been reached
❑
❑
Have parameters stabilized �9
❑
❑
If no or NIA - Explain below
SAMPLE COLLECTION
Method. PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1.4 DIOXANEI8260
Z7
l�
VOA
3
HCL
VOCsI8260
t
'ODIC'
EG46et9-
L(a)
2
NONE
DowTherm A
{
s
VAR
VAR
VAR
MNA
fl
VAR-
vmt—
­E�
Comments Fe+2 =
Signature
START STRI PPI NG
'--- COLLECT H2 SAMPLE
Date —ill 1 122
NIA

WelliP€ezo ID:
Project No:
Site Location:
Weather Conds:
Ground Water Sample Collection Record
CNA HOLDINGSINRLF
Woodleaf NC
0 "a Collector(s) Hi11,4) Leaver
WATER LEVEL DATA: (measured from Top
a. Total Well Length NIA c. Casing Material _SS
b Water Table Depth 61c1 d. Casing Diameter 2"
Date, 111 ( 122
lima: start 1440 amJpm
Finish amfpm
Well D Piezometer ❑
e. Length of Water Column — NIA
f. Calculated Well Volume (see back) _ NIA
WELL PURGING DATA a. Purge Method Low Flow Purge Ratebo_ mllmin
b- Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ _NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
C. Field Testing Equipment Used: Make Model Serial Number
YSI PRO+ i 0c.,"u7
Hach 21000 41�_
®
11111111MI!
11111
We. 0�lIM111111M
�0B-M=�il�
11111�
`��■I`�■,
d. Acceptance criteria pass/fail Yes
Has required volume been removed RR
Has required turbidity been reached
Have parameters stabilized 9,]
if no or NIA - Explain below. r
SAMPLE COLLECTION:
Method: PUMP TUBING
No NIA
❑ ❑
❑ ❑
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1.4 DIOXANEI8260
S
VOA
3
HCL
VOCsI8260
VOA
3
NONE
EGI8015
L(a)
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
VAR
VAR IVAR
EX MNA
Comments
Fe+2 = �j ;� mgll
%::;Yl START STRIPPING
1
COLLECT lit SAMPLE
Signature
Date
111 1 122

well/Plezo tD 0 ^ 1-79
Ground Water Sample Collection Record
Client- CNA HOLDINGSINRLF Bate: 111 [ 122
Project No, _ Time Start (y Y 6, amlpm
Site Location: Woodleaf NC Finlsh 1 % ! amlpm
Weather Conds'--SL;,4,-jq Collector(s) A Hdf, Leave
WATER LEVEL DATA: [measured from Top Well [g Piezometer ❑
a. Total Well Length NIA C. Casing Material _ SS e. Length of Water Column _ NIA
b. Water Table Depth 7 - ? 0 d. Casing diameter 2" f Calculated Well Volume (see back) _ NIA
WELL PURGING DATA 7
a. Purge Method Low Flow Pu e RatAO0 mllmin
b. Acceptance Criteria defined (from workptan)
- Minimum Required Purge Volume (@ _NA well volumes) NA
Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO+ 7-41 2 ' 7
Hach 21 COO -C IV I! C
®®
�.TURBIDITY■■
■--
RIMr��Mi�ffAlum��■���
�',ir7�rJ=M§ja7A-
�M1
&"]
err
r
■ i��rnammm
M_U
MN�
Em
d. Acceptance criteria passlfail Y
Has required volume been removed
Has required turbidity been reached
Have parameters stabilized
If no or NIA - Explain below.
SAMPLE COLLECTION: Method: PUMP TUBING
No NIA
❑ ❑
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1.4 DJOXANtJ8260
1 c2
VOA
3
HCL
VOCsI8260
VOA
3
NONE
EG18015
L a
2
NONE
DowTherm A
VAR.
VAR
IVAR
I MNA
VAR
I VAR
VAR
I EX MNA
Comments Fe+2 =Yak mgll f-'T tD START STRIPPING � �� COLL-ECT H2 SAMPLE
signature _ r,C _����� Date ____ 111 J 122

WeIVPiezo ID:
Ground Water Sample Collection Record
:Eient: CNA HOLDINGSINRLF Date: I11 1 122
'roject No: Time: Start ibiZz amlpm
cite Location- Woodleaf INC Finish am/pm
Veather Conds. . (. .s Collector(s) HiEI' J Leaver
4
WATER LEVEL DATA: (measured from Top Well M Piezometer ❑
a. Total Well Length NIA �y c. Casing Material _ SS e. Length of Water Column — N/A
b. Water Table Depth �,5 ` d. Casing. Diameter 2" f. Calculated Well Volume (see back)
WELL PURGING DATA ���
a. Purge Method Low flow Pu_r_ge Rate mi/min
b. Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ _NA_ well volumes) NA
- (Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSl PRO+ jg0G0,k
Hach 2100Q
Time
Volume
Removed (ml)
TEMP
C
pH
S.U.
Spec. Cond
(umhos)
TURBIDITY
NTUs
D.0
m fl
ORP
MV
Odor
DTW
INT
is,
-ll
,1
--�.zL(
j
.r
U,
Z-0
it . _
-:0.
[
,
sa,s
— T)
�
14
,�
aq I
4,[G9
r o
0
�f Cr
?
a V
47
j2
I l
jlU
`i�
ray
`fl I
0 Lis
-11U
.�
G7
,t�
h '
v.�r
_ 11
.
d. Acceptance arlteria passlfail Yes
No
NIA
Has required volume been removed
❑
❑
Has required turbidity been reached
❑
❑
Have parameters stabilized
❑
❑
If no or NIA - Explain below.
SAMPLE COLLECTION:
Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1.4 DIOXANE18260
VOA
3
HCL
VOCs18250
VOA
3
NONE
EG18015
L(a)
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
1
VAR
VAR
IVAR
EX MINA
Comments Fe+2 =`1 [, mg11_ _ � START STRIPPING 17 1 COLLECT H2 SAMPLE
Signature���. Date — 111 122
NIA

WeIIIPiezo ID; ig ►7
iJ / cL
Ground Water Sample Collection Record
"lient: CNA HOLDINGSINRLF Date: 111 1 122
Droject No: Time: Start (a . am/pm
Site Location: Woodleaf NC Finish am/pm
Heather Conds: ej21V 4r 7-! Collector(s) A HiICJ Leaver
WATER LEVEL DATA: (measured from Top Well [9 Piezometer ❑
a. Total Well Length NIA c. Casing Material _,SS e. Length of Water Column _ NIA
b. Water Table Depth �' ?� d. Casing Diameter 2" f. Calculated Well Volume (see back)
WELL PURGING DATA j��
a. Purge Method Low Flow Purge Rate _lml/min
b Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ _NA_ well volumes) NA
Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO+ P�Al&" CY
Hach 2100Q ;1 �,_
201-TWOM,
TURBIDITY
NTUs
a ■
U.
C>�tl�yF��J�'Jf�r"�71�.�IIIIIIL�.�r,��.Ey""�ii,►iiE�iii�
111110
+�i��_
—
d. Acceptance criteria pass/fail
Has required volume been removed
Has required turbidity been reached
Have parameters stabilized
If no or NIA - Explain below.
Ye
N!❑A
0
❑
❑
a
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1,4 DIOXANE18260
/ (, "
-
VOA
3
HCL
VOCs18260
VOA
3
NONE
EG18015
�-
L a
2
NONE
DowTherm A
! Y J
VAR
VAR
VAR
MNA
Y
�--
VAR
I VAR
IVAR
EX MNA
Comments Fe+2 = Q: 0 mall Alro f START STRIPPING &II —IL COLLECT H2 SAMPLE
Signaturee.rz. _ _ _ Date _ 111 1 122
d

Well/Piezo Id
44
�l
Ground Water Sample Collection Record
;lient: CNA HOLDINGSINRLF Date: lit l 122
'roject No: Time: Start_ amlpm
ate Location: Woodleaf NC Finish —19amlpm
Weather Conds: �lc�►�►2-,�1G `' ) Collector(s) Hil J Leaver
WATER LEVEL DATA: {measured from Top Well Q Piezometer ❑
a. Total Well Length NIA c. Casing Material _ SS e. Length of Water Column NIA
b_ Water Table Depth t �� d. Casing Diameter 2" f- Calculated Well Volume (see back) _ NIA
WELL PURGING DATA
a, Purge Method Low Flow Purge Rate_ ISO murrain
b. Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ _NA_ well volumes) NA
Maximum Allowable Turbidity NA NTUs
Stabilization of parameters 10%
c. Field Testing Equipment Used. Make Model Serial Number
YSl PRO+ jq 4ck- 47
Hach 21000 'C 1YuRc-
Time
Volume
Removed ml
TEMP
C
pH
S,U.
Spec. Cond
(umhos)
TURBIDITY
NTUs
D.O.
m 11
ORP
MV
Odor
DTW
113
INT
f�7•rF
7.1t
3i3'T
.`�
u
a'
-Aw
a
,
d. Acceptance criteria pass/fail
Yes
No
NIA
Has required volume been removed
171
❑
❑
Has required turbidity been reached
B
❑
❑
Have parameters stabilized
IS
❑
❑
If no or NIA - Explain below -
SAMPLE COLLECTION: Method: PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
Z l3
VDA
3
HCL
1,4 DIOXAHE18260
-
veg
1F
-
veor
E
DowTtieft A
�-
�c
VAR
VAR
VAR
MNA
<<
-V*R
Comments
Fe+2 = 013 mgll START STRIPPING
JVY1
COLLECT H2 SAMPLE
Signature
Date —III
1 122

Well/Piezo ID
'0 ZA
Ground Water Sample Collection Record
;Iient: CNA HOLDINGSINRLF Date. t tl Q 122
'roject No: Time. Start 10d5 amfpm
Re Locatlon• Woodtsaf NC _ Finish 111 W amlpm
Veather Conds: - ?'g Collector(s) (A Hill; J Leaver
WATER LEVEL DATA: (measured from Top
a Total Well Length NIA c. Casing Material _ SS
b. Water Table Depth cJ d. Casing Diameter L
Well Piezorneter ❑
e. Length of Water Column N/A
f. Calculated Well Volume (see back) _ NI6
WELL PURGING DATA
a. Purge Method Low Flow Purse Rate i So mllmin
b. Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO+
Mach 21000 y{
Time
Volume
Removed "mli
TEMP
C
pH
S.U.
Spec. Cored
(umhos)
TURBIDITY
NTUs
D.O.
m li
DRP
MV
Odor
DTW
t7 ZC
INT
i C. 0
. a
1, C
Z
k�Zo
1 71.
G ( 1i
60
- 03 0
1
t'
d Acceptance criteria pass/fail
Yes
Has required volume been removed
Has required turbidity been reached
Have parameters stabilized
If no or NIA - Explain below.
SAMPLE COLLECTION:
Method, PUMP TUBING
No NIA
❑ ❑
❑ ❑
❑ ❑
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
VOA
3
HCL
1,4 DIOXANFJ6260
ICS
VOA
3
HCL
VOCs18260
4
V
L(a)
2
NONE
DowTherm A
It
VAR
VAR
IVAR
MNA
,
C.
VAR
I VAR
IVAR
EX MNA
Comments Fe+2 =
Signature
START STRIPPING
COLLECT H2 SAMPLE
Date 111 -2 122

WeIIIPiezo ID, ^]
1. R
Ground Water Sample Collection Record
;Bent CNA HOLDINGSINRLF Date. 111 I22
Project No: Time: Start !S4 am/pm
iite Location: Woodleaf NC Finish I amlpm
veatherCon ds: -0`s Collector(s) A q!II J Leaver
WATER LEVEL DATA: (measured from Top
a- Total Well Length NIA c. Casing Material SS
b- Water Table Depth d. Casing Diameter 2"
Well Q Piezometer ❑
e- Length of Water Column _ NIA
f. Calculated Well Volume (see back) _ NIA
WELL PURGING DATA
a- Purge Method Low Flow Purge RatePLOL) mllmin
b. Acceptance Criteria defined (from workplan)
- Minimum Required Purge Volume (@ _NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YSI PRO+ 'lot Ptl3zu
Hach2100Q 73 �q<-
�N�"�AF�����
d. Acceptance criteria pass/fail
Yes
No
NIA
Has required volume been removed
®
❑
❑
Has required turbidity been reached
❑
❑
Have parameters stabilized
❑
❑
If no or NIA - Explain below.
SAMPLE COLLECTION:
Method. PUMP TUBING
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
-. f{
VOA
3
HCL
1,4 DIOXANEI8250
119,767
;
VOA
3
HCL
VOCs18250
tir
L(a)
2
NONE
DowTherm A
'•
VAR
VAR
VAR
MNA
'
VAR
VAR
VAR
EX MINA
Comments Fe+2Fe+2 = J2 rn911 i 13 "f _START STRIPPING 17,5V COLLECT H2 SAMPLE
1
Signature Date 111 2 122

Project No:
Site Location:
Weather Conds-
Well/Piezo IDS
�—D
+ L�
Ground Water Sample Collection Record
CNA HOLDINGSINRLF
Woodleaf NC
Collector(s) `�Fiill, Leaver
WATER LEVEL DATA: (measured from Top
a Total Well Length NIA c. Casing Material _ SS
b. Water Table Depth 3q-Q d_ Casing Diameter 2"
Date, 111 l 122
Time. Start 12 H am/pm
Finish amrpm
well ❑ Piezometer ❑
e. Length of Water Column NIA
f. Calculated Well Volume (see back)
WELL PURGING DATA �1
a. Purge Method Low Flow Purge Rate rxC�b mllmin
b. Acceptance Criteria defined {from workplan}
- Minimum Required Purge Volume (g __NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabillzatlon of parameters 10%
c. Field Testing Equipment Used: Make Model Serlal Number
YSi PRO+ 16 e az � -1
Hach 21000 "l?114
Time
Volume
Removed ml
TEMP
C
pH
S.U.
Spec. Cond
umhos
TURBIDITY
NTUs
D.D.
m A
ORP
MV
Odor
DTW
INT
ell
�7
3 %7
� •7
S ii 1
46
d. Acceptance criteria passlfail Yes
Has required volume been removed
Has required turbidity been reached
Have parameters stabllized
if no or NIA - Explaln below.
SAMPLE COLLECTION:
Methods PUMP TUBING
No NIA
Sample, ID
Container Type
No. of Containers
Preservation
Analysis
Time
O
L,
VOA
3
HCL
1,4 DIOXANFJ8260
VOA
3
HCL
VOCs18260
VOA
3
NONE
EG18015
L(a)
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
V
VAR
_
_ & n n
Comments Fe+2 = q'(J mall "J
Signature
WA- COLLECT H2
Date _ 111 122
OC.
NIA

Client:
Project No
Site Location:
':'leather Ccnds:
WeIIlPiezo Ip;
%-3
Ground Water Sample Collection Record.
CNA HOLDINGSINRLF
Woodleaf NC
Colfector(s)
WATER LEVEL DATA: (measured from ToF
a. Total Well Length NIA c- Casing Material ,_ SS
b Water Table Depth - 3 d, Casing Diameter 2"
J Leaver
bate- 111 122
Time. Start amlpm
Finish 11;3 to, am/pm
Well D i Piezometer ❑
e- Length of Water Column_ NIA
f. Calculated Well Volume (see back) _ NIA
WELL PURGING DATA
a- Purge Method Low Flow Purge RataQO ml/min
b, Acceptance Criteria defined (from workpian)
- Minimum Required Purge Volume (@ _NA_ well volumes) NA
Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used. Make Model Serial Number
YSI_ PRO+ R00-Z';I
Hach - — 21000 131-1Lf5'
Time
Volume
I Removed (ml)
TEMP
C
pH
5pen- Cond
(umhos)
TURBIDITY
NTUs
D.O.
m 1l
OR
MV
Odor
DTW
i`'13:7
JINT
(,:
? 5
.3
W`{
5 �Q'
—77. b
U -
a 1.'iL-
iOs—
C&0
f4.q
,G.
77. G
ii-&
'qs--. '
d i 11
In 4
� (I--
3f- u
i` Sp
�� �
R,. 5
4
1�
S
S.
r �
i
d. Acceptance criteria pass/fail
Yes
Has required volume been removed
`;�Q'
Has required turbidity been reached
Ci
Have parameters stabilized
if no or NIA - Explain below -
SAMPLE COLLECTION- Method- PUMP TUBING
No NIA
❑ ❑
❑ ❑
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
B -ri • Z5
VOA
3
HCL
1,4 DIOXANE182B0
1
-V4; PA-
XJO&9h�Lat3'
—
e•
VOA
3
NONE
EG18015
s.
L(a)
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
VAR
I VAR
IVAR.
EX MNA
t
Comments Fe+2 mgll ]�Q_START STRIPPING COLLECT H2 SAMPLE
Signature / `' LJ Date 111 ,,� 122

Well/Piezo ID:
Ground Water Sample Collection Record
:Iient- CNA HOLDINGSINRLF Date: 111 l22
'roject No: Time: Start am/pm
site Location: Woodleaf NC Fi11�nish3 5 - amlpm
Veather Cards: .._.._. Collectors) "A Hlll,� Leaver
WATER LEVEL DATA: (measured from ToF
a. Total Well Length N/A c. Casing Material _ SS
b. Water Table Depth 5�_qj d. Casing Diameter a?"
Well D Piezometer ❑
e. Length of Water Column NIA
f. Calculated Well Volume (see back) _ NIA
WELL PURGING DATA
a. Purge Method Low Flow Purge Rate_ 0-C' mllmm
b. Acceptance Criteria defined (from workplan)
Minimum Required Purge Volume (@ `NA well volumes) NA
- Maximum Allowable Turbidity NA NTUs
- Stabilization of parameters 10%
c. Field Testing Equipment Used- Make Model Serial Number
YSI PRO+ �ClV_wo�g_)
Hach---2100Q --- ;q4c .,
t /
M i�
�I�IIIIII��
d
5.:��
IIIIIN�P�i�i�+l7
m���r�■��
��IIIIIr�E�■
d. Acceptance criteria pass/fail
Yes
Has required volume been removed
E5
Has required turbidity been reached
Have parameters stabilized]
If no or NIA - Explain below -
SAMPLE COLLECTION: Method: PUMP TUBING
No NIA
❑ ❑
❑ ❑
Sample ID
Container Type
No_ of Containers
Preservation
Analysis
Time
D 1
VOA
3
HCL
1.4 DIOXANE18260
'
VOA
3
HCL
VOCs1826D
VOA
3
NONE
EG18015
j
L a
2
NONE
DowTherm A
It
VAR
VAR
VAR
MNA
VAR
VAR
VAR
EX MNA
Comments Fe+2= zy mgll 1 Sb STARTSTRIPPING 1`12Z COLLECT H2SAMPLE
Signature Date —ill a- 122

Client --
Project No:
Site Location:
''leather Conds:
Weil/Piezo ID.
l0
Ground Water Sample Collection Record
CNA HOLDINGSINRLF
NC
Collector(s)
WATER LEVEL DATA: {measured from Top
a_ Total Well Length NIA c. Casing Material _ SS
b Water Table Depth d Casing Diameter 2"
Leaver
Date: I I l22
Time: Start amlpm
Finish i $ amlpm
Well 12 Piezometer ❑
e. Length of Water Column NIA
f. Calculated Well Volume (see back) _ NIA
WELL PURGING DATA
a. Purge Method Low Flow Purge Rate ml/min
b. Acceptance Criteria defined (from workplan)
Minimum Required Purge Volume (@ __NA_ well volumes) NA
Maximum Allowable Turbidity NA NTUs
Stabilization of parameters 10%
c. Field Testing Equipment Used: Make Model Serial Number
YS I PRO+IOcL� 7
Hach 2100Q l y�
rF"10W
•..
�rr�r
>
r�
e�■I�
I■��
d. Acceptance criteria pass/fah Yes
Has required volume been removed
Has required turbidity been reached
Have parameters stabilized
If no or NIA - Explain below.
SAMPLE COLLECTION: Method- PUMP TUBING
Na NIA
❑ ❑
❑ ❑
Sample ID
Container Type
No. of Containers
Preservation
Analysis
Time
"t7 C)
VOA
3
HCL
1,4 DIOXANJ8260
VOA
3
HCL
VOCsl8260
VOA
3
NONE
EG18615
L(a)
2
NONE
DowTherm A
VAR
VAR
VAR
MNA
,
VAR
VAR
IVAR
FCC MNA
Comments Fe+2 =?IV moll # START STRIPPING EIS 4� COLLECT H2 SAMPLE
r
Signature Date^ 111 a 122

Corrective Action Evaluation Report
Project Number: 60683034
Appendix E
Laboratory Reports — May 2022 and November 2022
AECOM

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
June 05, 2022
Jing Zhou
AECOM
1360 Peachtree St.
Suite 500
Atlanta, GA 30309
RE: Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory on May 17, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
" Xr_
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Rob Davis, AECOM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID #: 98019
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

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816 Durst Avenue East
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[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CNA-NRLF-May 2022
92604755
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92604755001
B-01-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755002
B-09C-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755003
B-10-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755004
B-12-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755005
B-17C-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755006
13-2213-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8260D Mod.
CL
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755007
B-23A-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755008
13-2313-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
CNA-NRLF-May 2022
Pace Project No.:
92604755
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755009
B-24A-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
92604755010
SW-5-051622
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92604755011
CSW-1-051622
EPA 8260DMod.
CL
3
PASI-C
92604755012
B-99-051622
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
LRB
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
EPA 9056A
CDC
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-I = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 29

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-01-051622
Lab ID: 92604755001 Collected: 05/16/22
14:59
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L 0.040
1
05/17/22 14:10
Nitrogen, Nitrate
ND mg/L 0.040
1
05/17/22 14:10
14797-55-8
Nitrogen, Nitrite
0.046 mg/L 0.040
1
05/17/22 14:10
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.64 mg/L 0.25
5
05/17/22 15:45
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/23/22 17:45
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1530 ug/L 100
50
05/18/22 22:22
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94 % 70-130
50
05/18/22 22:22
17060-07-0
Toluene-d8 (S)
90 % 70-130
50
05/18/22 22:22
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L 1.0
1
05/27/2212:56
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 29

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-09C-051622
Lab ID: 92604755002 Collected: 05/16/22
14:06
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L 0.040
1
05/17/22 14:11
Nitrogen, Nitrate
ND mg/L 0.040
1
05/17/22 14:11
14797-55-8
Nitrogen, Nitrite
ND mg/L 0.040
1
05/17/22 14:11
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
ND mg/L 0.050
1
05/17/22 15:44
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/23/22 18:03
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
753 ug/L 20.0
10
05/18/22 21:43
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
10
05/18/22 21:43
17060-07-0
Toluene-d8 (S)
85 % 70-130
10
05/18/22 21:43
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L 1.0
1
05/27/2213:41
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-10-051622
Lab ID: 92604755003 Collected:
05/16/22
16:02
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L
0.040
1
05/17/22 14:14
Nitrogen, Nitrate
ND mg/L
0.040
1
05/17/22 14:14
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/17/22 14:14
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
ND mg/L
0.050
1
05/17/22 15:45
M1,R1
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
05/23/22 18:59
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
53.9 ug/L
8.3
1
05/23/22 05:12
05/23/22 19:28
92-52-4
Diphenyl ether (Phenyl ether)
559 ug/L
83.3
10
05/23/22 05:12
05/24/22 11:01
101-84-8
Surrogates
Nitrobenzene-d5 (S)
109 %
10-144
1
05/23/22 05:12
05/23/22 19:28
4165-60-0
2-Fluorobiphenyl (S)
81 %
10-130
1
05/23/22 05:12
05/23/22 19:28
321-60-8
Terphenyl-d14 (S)
112 %
34-163
1
05/23/22 05:12
05/23/22 19:28
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
164 ug/L
5.0
2.5
05/20/22 00:28
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 %
70-130
2.5
05/20/22 00:28
17060-07-0
Toluene-d8 (S)
90 %
70-130
2.5
05/20/22 00:28
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/27/2213:56
14808-79-8
REPORT OF LABORATORY ANALYSIS
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Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 29

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Pace Analytical Services, LLC
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Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-12-051622 Lab ID: 92604755004 Collected: 05/16/22 12:04 Received: 05/17/22 07:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L
0.040
1
05/17/22 14:16
Nitrogen, Nitrate
ND mg/L
0.040
1
05/17/22 14:16
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/17/22 14:16
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.068 mg/L
0.050
1
05/17/22 15:43
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
05/23/22 05:12
05/23/22 19:57
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
10.0
1
05/23/22 05:12
05/23/22 19:57
101-84-8
Surrogates
Nitrobenzene-d5 (S)
93 %
10-144
1
05/23/22 05:12
05/23/22 19:57
4165-60-0
2-Fluorobiphenyl (S)
68 %
10-130
1
05/23/22 05:12
05/23/22 19:57
321-60-8
Terphenyl-d14 (S)
127 %
34-163
1
05/23/22 05:12
05/23/22 19:57
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2390 ug/L
100
50
05/18/22 22:41
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97 %
70-130
50
05/18/22 22:41
17060-07-0
Toluene-d8 (S)
96 %
70-130
50
05/18/22 22:41
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.1 mg/L
1.0
1
05/27/2214:11
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 29

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Pace Analytical Services, LLC
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Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-17C-051622
Lab ID: 92604755005 Collected:
05/16/22
11:07
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L
0.040
1
05/17/22 14:07
Nitrogen, Nitrate
ND mg/L
0.040
1
05/17/22 14:07
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/17/22 14:07
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.12 mg/L
0.050
1
05/17/22 15:24
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1660 ug/L
100
50
05/18/22 23:00
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 %
70-130
50
05/18/22 23:00
17060-07-0
Toluene-d8 (S)
89 %
70-130
50
05/18/22 23:00
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/27/2214:26
14808-79-8
REPORT OF LABORATORY ANALYSIS
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Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 29

leAnalyiical
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: 13-2213-051622
Lab ID: 92604755006 Collected:
05/16/22 12:46
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L
0.040
1
05/17/22 14:17
Nitrogen, Nitrate
ND mg/L
0.040
1
05/17/22 14:17
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/17/22 14:17
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
ND mg/L
0.050
1
05/17/22 15:43
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1070 ug/L
40.0
20
05/20/22 00:47
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99 %
70-130
20
05/20/22 00:47
17060-07-0
Toluene-d8 (S)
92 %
70-130
20
05/20/22 00:47
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/27/2214:41
14808-79-8
Date: 06/05/2022 09:21 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 29

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-23A-051622
Lab ID: 92604755007 Collected: 05/16/22 11:08
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L 0.040
1
05/17/22 14:18
Nitrogen, Nitrate
ND mg/L 0.040
1
05/17/22 14:18
14797-55-8
Nitrogen, Nitrite
ND mg/L 0.040
1
05/17/22 14:18
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.79 mg/L 0.10
2
05/17/22 15:24
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/23/22 19:14
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
3150 ug/L 100
50
05/18/22 23:38
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 % 70-130
50
05/18/22 23:38
17060-07-0
Toluene-d8 (S)
89 % 70-130
50
05/18/22 23:38
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
7.6 mg/L 1.0
1
05/27/2215:26
14808-79-8
Date: 06/05/2022 09:21 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 29

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816 Durst Avenue East
Greenwood, SC 29649
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ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: 13-2313-051622
Lab ID: 92604755008 Collected: 05/16/22 11:56
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L 0.040
1
05/17/22 14:19
Nitrogen, Nitrate
ND mg/L 0.040
1
05/17/22 14:19
14797-55-8
Nitrogen, Nitrite
ND mg/L 0.040
1
05/17/22 14:19
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.22 mg/L 0.050
1
05/17/22 15:41
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/23/22 19:23
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2930 ug/L 100
50
05/18/22 23:58
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 % 70-130
50
05/18/22 23:58
17060-07-0
Toluene-d8 (S)
88 % 70-130
50
05/18/22 23:58
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
2.8 mg/L 1.0
1
05/27/2215:41
14808-79-8
Date: 06/05/2022 09:21 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 29

leAnalyiical
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-24A-051622
Lab ID: 92604755009 Collected:
05/16/22 10:27
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L
0.040
1
05/17/22 14:36
Nitrogen, Nitrate
ND mg/L
0.040
1
05/17/22 14:36
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/17/22 14:36
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
ND mg/L
0.050
1
05/17/22 15:23
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
250 ug/L
10.0
5
05/18/22 21:24
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95 %
70-130
5
05/18/22 21:24
17060-07-0
Toluene-d8 (S)
93 %
70-130
5
05/18/22 21:24
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/27/2215:56
14808-79-8
Date: 06/05/2022 09:21 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: SW-5-051622
Lab ID: 92604755010 Collected: 05/16/22
09:08
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/23/22 17:36
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
05/23/22 05:12
05/23/22 20:27
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
05/23/22 05:12
05/23/22 20:27
101-84-8
Surrogates
Nitrobenzene-d5 (S)
96 % 10-144
1
05/23/22 05:12
05/23/22 20:27
4165-60-0
2-Fluorobiphenyl (S)
66 % 10-130
1
05/23/22 05:12
05/23/22 20:27
321-60-8
Terphenyl-d14 (S)
125 % 34-163
1
05/23/22 05:12
05/23/22 20:27
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
05/18/22 20:46
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99 % 70-130
1
05/18/22 20:46
17060-07-0
Toluene-d8 (S)
92 % 70-130
1
05/18/22 20:46
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 29

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816 Durst Avenue East
Greenwood, SC 29649
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ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: CSW-1-051622
Lab ID: 92604755011 Collected:
05/16/22 10:05
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
667 ug/L
25.0
12.5
05/20/22 00:09
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
102 %
70-130
12.5
05/20/22 00:09
17060-07-0
Toluene-d8 (S)
93 %
70-130
12.5
05/20/22 00:09
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Sample: B-99-051622
Lab ID: 92604755012 Collected:
05/16/22 16:10
Received: 05/17/22 07:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
ND mg/L
0.040
1
05/17/22 14:21
Nitrogen, Nitrate
ND mg/L
0.040
1
05/17/22 14:21
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/17/22 14:21
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
ND mg/L
0.050
1
05/17/22 15:49
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
05/23/22 18:12
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
49.6 ug/L
10.0
1
05/23/22 05:12
05/23/22 20:57
92-52-4
Diphenyl ether (Phenyl ether)
469 ug/L
100
10
05/23/22 05:12
05/24/22 11:30
101-84-8
Surrogates
Nitrobenzene-d5 (S)
69 %
10-144
1
05/23/22 05:12
05/23/22 20:57
4165-60-0
2-Fluorobiphenyl (S)
56 %
10-130
1
05/23/22 05:12
05/23/22 20:57
321-60-8
Terphenyl-d14 (S)
103 %
34-163
1
05/23/22 05:12
05/23/22 20:57
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
145 ug/L
8.0
4
05/20/22 01:07
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 %
70-130
4
05/20/22 01:07
17060-07-0
Toluene-d8 (S)
86 %
70-130
4
05/20/22 01:07
2037-26-5
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/27/2216:11
14808-79-8
Date: 06/05/2022 09:21 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 698674 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755004, 92604755005, 92604755006, 92604755007,
92604755008,92604755009,92604755012
METHOD BLANK: 3647550 Matrix:
Water
Associated Lab Samples:
92604755001, 92604755002, 92604755003, 92604755004, 92604755005,
92604755006, 92604755007,
92604755008,92604755009,92604755012
Blank
Reporting
Parameter
Units Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L ND
0.040
05/17/22 14:01
Nitrogen, Nitrite
mg/L ND
0.040
05/17/22 14:01
Nitrogen, NO2 plus NO3
mg/L ND
0.040
05/17/22 14:01
LABORATORY CONTROL SAMPLE: 3647551
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 100 90-110
Nitrogen, Nitrite mg/L 1 0.99 99 90-110
Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3647552
3647553
MS
MSD
92604635001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/L
6.4
1.5
1.5
7.8
7.8
96
96
90-110
0
Nitrogen, Nitrite
mg/L
ND
1
1
1.0
1.0
99
99
90-110
1
Nitrogen, NO2 plus NO3
mg/L
6.4
2.5
2.5
8.8
8.8
98
98
90-110
0
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3647854
3647855
MS
MSD
92604755005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/L
ND
1.5
1.5
1.5
1.5
99
100
90-110
1
Nitrogen, Nitrite
mg/L
ND
1
1
1.0
1.0
101
101
90-110
0
Nitrogen, NO2 plus NO3
mg/L
ND
2.5
2.5
2.5
2.5
99
100
90-110
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 698744 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755004, 92604755005, 92604755006, 92604755007,
92604755008,92604755009,92604755012
METHOD BLANK: 3647910 Matrix: Water
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755004, 92604755005, 92604755006, 92604755007,
92604755008,92604755009,92604755012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 05/17/22 15:22
LABORATORY CONTROL SAMPLE: 3647911
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Orthophosphate as P mg/L 0.25 0.25 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3648099 3648100
MS MSD
92604755003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L ND 0.25 0.25 0.20 0.23 79 92 90-110 15 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 677840 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755007, 92604755008, 92604755010, 92604755012
METHOD BLANK: 3121020 Matrix: Water
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755007, 92604755008, 92604755010, 92604755012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylene glycol mg/L ND 5.0 05/23/22 15:54
LABORATORY CONTROL SAMPLE: 3121021
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Ethylene glycol mg/L 25 26.0 104 34-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3121022 3121023
MS MSD
5295798001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 17.3 22.4 68 88 39-168 26 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 699072 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92604755001, 92604755002, 92604755004, 92604755005, 92604755007, 92604755008, 92604755009,
92604755010
METHOD BLANK: 3649630
Matrix:
Water
Associated Lab Samples:
92604755001, 92604755002, 92604755004, 92604755005, 92604755007,
92604755008, 92604755009,
92604755010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/18/22 18:12
1,2-Dichloroethane-d4 (S)
%
95
70-130
05/18/22 18:12
Toluene-d8 (S)
%
91
70-130
05/18/22 18:12
LABORATORY CONTROL SAMPLE: 3649631
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.6 93 70-130
1,2-Dichloroethane-d4 (S) % 92 70-130
Toluene-d8 (S) % 89 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3649632
3649633
MS
MSD
92604755010 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 18.3
19.6 92
98
63-136 7
1,2-Dichloroethane-d4 (S)
%
93
101
70-130
Toluene-d8(S)
%
90
93
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 699369 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92604755003, 92604755006, 92604755011, 92604755012
METHOD BLANK: 3651134
Matrix:
Water
Associated Lab Samples:
92604755003, 92604755006, 92604755011, 92604755012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/19/22 17:04
1,2-Dichloroethane-d4 (S)
%
94
70-130
05/19/22 17:04
Toluene-d8 (S)
%
89
70-130
05/19/22 17:04
LABORATORY CONTROL SAMPLE: 3651135
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.7 93 70-130
1,2-Dichloroethane-d4 (S) % 91 70-130
Toluene-d8 (S) % 89 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3651136
3651137
MS
MSD
92604755012 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 145 80
80 228
226 103
101
63-136 1
1,2-Dichloroethane-d4 (S)
%
101
98
70-130
Toluene-d8(S)
%
91
87
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 699794 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92604755003, 92604755004, 92604755010, 92604755012
METHOD BLANK: 3653070
Matrix:
Water
Associated Lab Samples: 92604755003, 92604755004, 92604755010, 92604755012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND
10.0
05/23/22 13:56
Diphenyl ether (Phenyl ether)
ug/L
ND
10.0
05/23/22 13:56
2,4,6-Tribromophenol (S)
%
106
10-144
05/23/22 13:56
2-Fluorobiphenyl (S)
%
99
10-130
05/23/22 13:56
2-Fluorophenol(S)
%
75
10-130
05/23/22 13:56
Nitrobenzene-d5 (S)
%
111
10-144
05/23/22 13:56
Phenol-d6 (S)
%
57
10-130
05/23/22 13:56
Terphenyl-d14 (S)
%
151
34-163
05/23/22 13:56
LABORATORY CONTROL SAMPLE:
Parameter
3653071
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 40.4 81
31-130
Diphenyl ether (Phenyl ether)
ug/L
50 43.5 87
25-130
2,4,6-Tribromophenol (S)
%
136
10-144
2-Fluorobiphenyl (S)
%
98
10-130
2-Fluorophenol(S)
%
72
10-130
Nitrobenzene-d5 (S)
%
104
10-144
Phenol-d6 (S)
%
55
10-130
Terphenyl-d14 (S)
%
147
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 29

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
QC Batch: 700913 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755004, 92604755005, 92604755006, 92604755007,
92604755008,92604755009,92604755012
METHOD BLANK: 3658548 Matrix: Water
Associated Lab Samples: 92604755001, 92604755002, 92604755003, 92604755004, 92604755005, 92604755006, 92604755007,
92604755008,92604755009,92604755012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 1.0 05/27/2212:26
LABORATORY CONTROL SAMPLE: 3658549
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 50 51.6 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3658550 3658551
MS MSD
92604755001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 50 50 51.7 51.9 102 102 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3658552 3658553
MS MSD
92606174006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 14.9 50 50 67.6 66.8 106 104 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALIFIERS
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/05/2022 09:21 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 29

lacmnalyfica('
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CNA-NRLF-May 2022
92604755
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92604755001
B-01-051622
EPA 353.2 Rev 2.0 1993
698674
92604755002
B-09C-051622
EPA 353.2 Rev 2.0 1993
698674
92604755003
B-10-051622
EPA 353.2 Rev 2.0 1993
698674
92604755004
B-12-051622
EPA 353.2 Rev 2.0 1993
698674
92604755005
B-17C-051622
EPA 353.2 Rev 2.0 1993
698674
92604755006
B-22B-051622
EPA 353.2 Rev 2.0 1993
698674
92604755007
B-23A-051622
EPA 353.2 Rev 2.0 1993
698674
92604755008
B-23B-051622
EPA 353.2 Rev 2.0 1993
698674
92604755009
B-24A-051622
EPA 353.2 Rev 2.0 1993
698674
92604755012
B-99-051622
EPA 353.2 Rev 2.0 1993
698674
92604755001
B-01-051622
SM 4500-P E-2011
698744
92604755002
B-09C-051622
SM 4500-P E-2011
698744
92604755003
B-10-051622
SM 4500-P E-2011
698744
92604755004
B-12-051622
SM 4500-P E-2011
698744
92604755005
B-17C-051622
SM 4500-P E-2011
698744
92604755006
B-22B-051622
SM 4500-P E-2011
698744
92604755007
B-23A-051622
SM 4500-P E-2011
698744
92604755008
B-23B-051622
SM 4500-P E-2011
698744
92604755009
B-24A-051622
SM 4500-P E-2011
698744
92604755012
B-99-051622
SM 4500-P E-2011
698744
92604755001
B-01-051622
EPA 8015 Alcohol -Glycol
677840
92604755002
B-09C-051622
EPA 8015 Alcohol -Glycol
677840
92604755003
B-10-051622
EPA 8015 Alcohol -Glycol
677840
92604755007
B-23A-051622
EPA 8015 Alcohol -Glycol
677840
92604755008
B-23B-051622
EPA 8015 Alcohol -Glycol
677840
92604755010
SW-5-051622
EPA 8015 Alcohol -Glycol
677840
92604755012
B-99-051622
EPA 8015 Alcohol -Glycol
677840
92604755003
B-10-051622
EPA 3510C
699794
EPA 8270E 699995
92604755004
B-12-051622
EPA 3510C
699794
EPA 8270E 699995
92604755010
SW-5-051622
EPA 3510C
699794
EPA 8270E 699995
92604755012
B-99-051622
EPA 3510C
699794
EPA 8270E 699995
92604755001
B-01-051622
EPA 8260D Mod.
699072
92604755002
B-09C-051622
EPA 8260D Mod.
699072
92604755003
B-10-051622
EPA 8260D Mod.
699369
92604755004
B-12-051622
EPA 8260D Mod.
699072
92604755005
B-17C-051622
EPA 8260D Mod.
699072
92604755006
B-22B-051622
EPA 8260D Mod.
699369
92604755007
B-23A-051622
EPA 8260D Mod.
699072
92604755008
B-23B-051622
EPA 8260D Mod.
699072
92604755009
B-24A-051622
EPA 8260D Mod.
699072
92604755010
SW-5-051622
EPA 8260D Mod.
699072
92604755011
CSW-1-051622
EPA 8260D Mod.
699369
92604755012
B-99-051622
EPA 8260D Mod.
699369
92604755001
B-01-051622
EPA 9056A
700913
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 06/05/2022 09:21
PM
without the written consent of Pace Analytical Services, LLC.
Page 25 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CNA-NRLF-May 2022
Pace Project No.: 92604755
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92604755002
B-09C-051622
EPA 9056A
700913
92604755003
B-10-051622
EPA 9056A
700913
92604755004
B-12-051622
EPA 9056A
700913
92604755005
B-17C-051622
EPA 9056A
700913
92604755006
B-22B-051622
EPA 9056A
700913
92604755007
B-23A-051622
EPA 9056A
700913
92604755008
B-23B-051622
EPA 9056A
700913
92604755009
B-24A-051622
EPA 9056A
700913
92604755012
B-99-051622
EPA 9056A
700913
Date: 06/05/2022 09:21 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 26 of 29

Awe, CC#_Title: ENV-FRM-HUNI.0083 v01 Sample Condition Upon Receipt
1 euvlSktFrr;E; � — „
Effective Date: 05112/202205/12/2022
Laboratory receiving sa ples:
Asheville ❑ Eden Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
ConditionSample -Client-Name: - - . _ .... . _.-. - - - - �,r Q (� 7
Upon Receipt Project #: WO# : 92�604 1 55
❑ Commercial wave x ❑UPS Other; usps ❑Client �I � Ill.
fill
fill
HEIII�p92604755
Custody Seal Present? ❑Yes Vo Seals Intact? ❑Yes ❑NO
Packing Material: ❑Bubble Wrap []Bubble Bags one ❑ Other
Thermometer:
❑ Ift Gun ID; C"J
Type of Ice: Wet ❑Blue
el Correction Factor:
Cooler Temp; _ Add/Subtract ('C)
Cooler Temp Corrected (- l: 2 3
USDA Regulated $oil ( N/A, water sample)
Did samples arigina In ^a Varantine zone within the United States: CA, NY, or SC
(check maps)? []Yes 11'No
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis 1<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Klatch CDC?
-Includes Date/Time/ID/Analysis Matrix;
Headspace in VOA Vials (55-6mm',
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Yes UNo ❑N/A 1 1
Yes
LJNo
N/A 2.
❑Yes
E2<0
❑N/A 3.
Dyes
o
❑N/A 4,
es
ONO
❑NIA 5.
e
❑No
❑N/A 6,
No
❑N/A
Y
NYes
❑o
❑N/A 1 7,
❑Yes
❑No
N/A a.
❑Yes
❑No
❑N/A 9.
©No /A 1D.
❑No VNIA 1 11.
Date/Initials Person Examining Contents:2243k
Biological Tissue rozen?
[]Yes[]NON/A
❑None
Temp should be above freezing to G°C
[Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source {inter tionally,
Including Hawaii and Puerto Rica)? ❑Yes V No
Comments/Dlscrenancv:
i Field Data Required? ❑Yes
5
Lot ID of split containers:
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
:rrojca-t Manager SRF Review: Date:
Qualfrax ID: 69614 page I of 2 Page 27 of 29

DC# Title: ENV-FRM-HUN1-0083 v01 Sample Condition Upon Receipt
i z�lTf,rurrrr�:
Effective Date: 05112/202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and project # W01t : 92604755
55
within the acceptance range for_ preservation sampies ._ _ PM: BY Due Date: 05/26/22
Exceptions: VOA, CGlifarm, TOC, Oil and Grease, DRO/8i)15 [water) ADC, LLHg CLiEN'r : 97—CNA
"Bottom half of box Is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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pH Adjustment Log for Preserved Samples
Sample ID 'type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Loth
adjusted added 9
i•s�. rrnciicrci Mugu n d U'Ll Im illlcy a11eGSlnU ryUr-En 4arolina compliance sampim, a copyor rm5 iarm wlil be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, Gut of temp, incorrect containers. j
Qualtrax ID:69614
Page 2 of 2 Page 28 of 29
i•s�. rrnciicrci Mugu n d U'Ll Im illlcy a11eGSlnU ryUr-En 4arolina compliance sampim, a copyor rm5 iarm wlil be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, Gut of temp, incorrect containers. j
Qualtrax ID:69614
Page 2 of 2 Page 28 of 29

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_ . Page 29 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
November 23, 2022
Jing Zhou
AECOM
1360 Peachtree St.
Suite 500
Atlanta, GA 30309
RE: Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory on November 02, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Gulf Coast
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
l Xr_
Bonnie Vang for
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Rob Davis. AECOM
?4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 65

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID M 98019
CERTIFICATIONS
Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
North Dakota Certification #: R-195
Arkansas Certification #: 88-0655
Oklahoma Certification #: 2019-101
DoD ELAP Certification #: 6429-01
South Carolina Certification #: 73006001
Florida Certification #: E87854
Texas Certification #: T104704178-19-11
Illinois Certification #: 004585
USDA Soil Permit # P330-19-00209
Kansas Certification #: E-10354
Virginia Certification #: 460215
Louisiana/LELAP Certification M 01955
Washington Certification #: C929
North Carolina Certification #: 618
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 65

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NRLF Celanase November 2022
92634190
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92634190001
SW-7-110122
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
8
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92634190002
SW-5-110122
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92634190003
SW-3-110122
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92634190004
SW-8-110122
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92634190005
B-24A-110122
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92634190006
B-24B-110122
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92634190007
B-12-110122
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92634190008
B-21 B-110122
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92634190009
B-23A-110122
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
LMB
3
GCLA
RSK-175
BDP
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MJP
5
PASI-A
AM23G
SLL2
1
GCLA
92634190010
B-23B-110122
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
LMB
3
GCLA
RSK-175
BDP
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MJP
5
PASI-A
AM23G
SLL2
1
GCLA
92634190011
B-17C-110122
RSK-175
LMB
3
GCLA
RSK-175
BDP
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MJP
5
PASI-A
AM23G
LHM
1
GCLA
92634190012
B-17B-110122
RSK-175
LMB
3
GCLA
RSK-175
BDP
1
GCLA
EPA 8270E
PKS
5
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
SMS
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MJP
5
PASI-A
AM23G
LHM
1
GCLA
92634190013
Trip Blank-01-110122
EPA8260D
SAS
53
PASI-C
92634190014
B-17C-110122 H2
AM20GAX
LMB
1
GCLA
92634190015
B-23A-110122 H2
AM20GAX
LMB
1
GCLA
92634190016
B-17B-110122 H2
AM20GAX
LMB
1
GCLA
92634190017
B-2313-110122 H2
AM20GAX
LMB
1
GCLA
GCLA = Pace Analytical Gulf Coast
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-I = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: SW-7-110122 Lab ID: 92634190001 Collected: 11/01/22 10:57 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol ND mg/L 5.0 1
8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 11/23/2022 05:59 PM
11/08/22 20:01 107-21-1
ND
ug/L
8.7
1
11/04/2215:14
11/05/2212:30
92-52-4
ND
ug/L
8.7
1
11/04/2215:14
11/05/2212:30
101-84-8
79
%
10-144
1
11 /04/22 15:14
11 /05/22 12:30
4165-60-0
66
%
10-130
1
11 /04/22 15:14
11 /05/22 12:30
321-60-8
93
%
34-163
1
11 /04/22 15:14
11 /05/22 12:30
1718-51-0
38
%
10-130
1
11 /04/22 15:14
11 /05/22 12:30
13127-88-3
49
%
10-130
1
11/04/2215:14
11/05/2212:30
367-12-4
89
%
10-144
1
11 /04/22 15:14
11 /05/22 12:30
118-79-6
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L 2.0 1
104 % 70-130 1
103 % 70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11 /02/22 19:08 123-91-1
11 /02/22 19:08 17060-07-0
11 /02/22 19:08 2037-26-5
Page 6 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: SW-5-110122
Lab ID: 92634190002 Collected: 11/01/22
11:23
Received: 11/02/22 07:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/08/22 20:10
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 8.7
1
11/04/22 15:14
11/05/22 12:55
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 8.7
1
11/04/22 15:14
11/05/22 12:55
101-84-8
Surrogates
Nitrobenzene-d5 (S)
69 % 10-144
1
11/04/22 15:14
11/05/22 12:55
4165-60-0
2-Fluorobiphenyl (S)
55 % 10-130
1
11/04/22 15:14
11/05/22 12:55
321-60-8
Terphenyl-d14 (S)
83 % 34-163
1
11/04/22 15:14
11/05/22 12:55
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/02/22 19:27
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
103 % 70-130
1
11/02/22 19:27
17060-07-0
Toluene-d8 (S)
107 % 70-130
1
11/02/22 19:27
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: SW-3-110122
Lab ID: 92634190003 Collected: 11/01/22
11:52
Received: 11/02/22 07:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/08/22 20:20
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 8.7
1
11/04/22 15:14
11/05/22 13:20
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 8.7
1
11/04/22 15:14
11/05/22 13:20
101-84-8
Surrogates
Nitrobenzene-d5 (S)
95 % 10-144
1
11/04/22 15:14
11/05/22 13:20
4165-60-0
2-Fluorobiphenyl (S)
82 % 10-130
1
11/04/22 15:14
11/05/22 13:20
321-60-8
Terphenyl-d14 (S)
107 % 34-163
1
11/04/22 15:14
11/05/22 13:20
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/03/22 14:09
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
109 % 70-130
1
11/03/22 14:09
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
11/03/22 14:09
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: SW-8-110122
Lab ID: 92634190004 Collected: 11/01/22
12:41
Received: 11/02/22 07:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/08/22 20:29
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 8.7
1
11/04/22 15:14
11/05/22 13:45
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 8.7
1
11/04/22 15:14
11/05/22 13:45
101-84-8
Surrogates
Nitrobenzene-d5 (S)
87 % 10-144
1
11/04/22 15:14
11/05/22 13:45
4165-60-0
2-Fluorobiphenyl (S)
72 % 10-130
1
11/04/22 15:14
11/05/22 13:45
321-60-8
Terphenyl-d14 (S)
92 % 34-163
1
11/04/22 15:14
11/05/22 13:45
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/02/22 20:05
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
104 % 70-130
1
11/02/22 20:05
17060-07-0
Toluene-d8(S)
104 % 70-130
1
11/02/22 20:05
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-24A-110122 Lab ID: 92634190005 Collected: 11/01/22 13:34 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
10.0
1
11/04/22 15:14
11/05/22 14:10
92-52-4
Diphenyl ether (Phenyl ether)
10.4
ug/L
10.0
1
11/04/22 15:14
11/05/22 14:10
101-84-8
Surrogates
Nitrobenzene-d5 (S)
72
%
10-144
1
11/04/22 15:14
11/05/22 14:10
4165-60-0
2-Fluorobiphenyl (S)
61
%
10-130
1
11/04/22 15:14
11/05/22 14:10
321-60-8
Terphenyl-d14 (S)
97
%
34-163
1
11/04/22 15:14
11/05/22 14:10
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 02:28
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 02:28
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 02:28
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 02:28
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 02:28
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 02:28
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 02:28
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
11/07/22 02:28
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 02:28
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 02:28
108-90-7
Chloroethane
5.1
ug/L
1.0
1
11/07/22 02:28
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 02:28
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 02:28
74-87-3
Cyclohexane
ND
ug/L
1.0
1
11/07/22 02:28
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 02:28
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 02:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 02:28
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:28
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:28
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:28
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/07/22 02:28
75-71-8
1,1-Dichloroethane
4.9
ug/L
1.0
1
11/07/22 02:28
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/07/22 02:28
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/07/22 02:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/07/22 02:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/07/22 02:28
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/07/22 02:28
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/07/22 02:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/07/22 02:28
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
11/07/22 02:28
100-41-4
2-Hexanone
ND
ug/L
5.0
1
11/07/22 02:28
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
11/07/22 02:28
98-82-8
Methyl acetate
ND
ug/L
10.0
1
11/07/22 02:28
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
11/07/22 02:28
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
11/07/22 02:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/07/22 02:28
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/07/22 02:28
1634-04-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 10 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-24A-110122 Lab ID: 92634190005 Collected: 11/01/22 13:34 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
9056 IC anions 28 Days
Sulfate
Date: 11/23/2022 05:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
1.2 ug/L
1.0
ND ug/L
1.0
99 %
70-130
94 %
70-130
102 %
70-130
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
218 ug/L
8.0
104 %
70-130
105 %
70-130
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
474 mg/L
5.0
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L
0.040
ND mg/L
0.040
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.16 mg/L
0.050
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
ND mg/L
1.0
1 11/07/22 02:28
100-42-5
1 11/07/22 02:28
79-34-5
1 11/07/22 02:28
127-18-4
1 11/07/22 02:28
108-88-3
1 11/07/22 02:28
87-61-6
1 11/07/22 02:28
120-82-1
1 11/07/22 02:28
71-55-6
1 11/07/22 02:28
79-00-5
1 11/07/22 02:28
79-01-6
1 11/07/22 02:28
75-69-4
1 11/07/22 02:28
76-13-1
1 11/07/22 02:28
75-01-4
1 11/07/22 02:28
1330-20-7
1 11/07/22 02:28
460-00-4
1 11/07/22 02:28
17060-07-0
1 11/07/22 02:28
2037-26-5
4 11 /02/22 21:21
123-91-1
4
4
f
I
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11 /02/22 21:21 17060-07-0
11 /02/22 21:21 2037-26-5
11 /03/22 18:14
11 /03/22 01:22 14797-55-8
11 /03/22 01:22 14797-65-0
11 /03/22 03:31
11/03/22 20:51 14808-79-8
Page 11 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-24B-110122 Lab ID: 92634190006 Collected: 11/01/22 14:22 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
10.0
1
11/04/22 15:14
11/05/22 14:36
92-52-4
Diphenyl ether (Phenyl ether)
ND
ug/L
10.0
1
11/04/22 15:14
11/05/22 14:36
101-84-8
Surrogates
Nitrobenzene-d5 (S)
41
%
10-144
1
11/04/22 15:14
11/05/22 14:36
4165-60-0
2-Fluorobiphenyl (S)
30
%
10-130
1
11/04/22 15:14
11/05/22 14:36
321-60-8
Terphenyl-d14 (S)
89
%
34-163
1
11/04/22 15:14
11/05/22 14:36
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/07/22 02:45
67-64-1
Benzene
ND
ug/L
1.0
1
11/07/22 02:45
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
11/07/22 02:45
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/07/22 02:45
75-27-4
Bromoform
ND
ug/L
1.0
1
11/07/22 02:45
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/07/22 02:45
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/07/22 02:45
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
11/07/22 02:45
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
11/07/22 02:45
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/07/22 02:45
108-90-7
Chloroethane
5.4
ug/L
1.0
1
11/07/22 02:45
75-00-3
Chloroform
ND
ug/L
1.0
1
11/07/22 02:45
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/07/22 02:45
74-87-3
Cyclohexane
ND
ug/L
1.0
1
11/07/22 02:45
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/07/22 02:45
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/07/22 02:45
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/07/22 02:45
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:45
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:45
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/07/22 02:45
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/07/22 02:45
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/07/22 02:45
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/07/22 02:45
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/07/22 02:45
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/07/22 02:45
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/07/22 02:45
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/07/22 02:45
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/07/22 02:45
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/07/22 02:45
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
11/07/22 02:45
100-41-4
2-Hexanone
ND
ug/L
5.0
1
11/07/22 02:45
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
11/07/22 02:45
98-82-8
Methyl acetate
ND
ug/L
10.0
1
11/07/22 02:45
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
11/07/22 02:45
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
11/07/22 02:45
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/07/22 02:45
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/07/22 02:45
1634-04-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 12 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-2413-110122 Lab ID: 92634190006 Collected: 11/01/22 14:22 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
9056 IC anions 28 Days
Sulfate
Date: 11/23/2022 05:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
95 %
70-130
90 %
70-130
103 %
70-130
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
118 ug/L
4.0
106 %
70-130
98 %
70-130
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
375 mg/L
5.0
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L
0.040
ND mg/L
0.040
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
ND mg/L
0.050
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
ND mg/L
1.0
1 11/07/22 02:45
100-42-5
1 11/07/22 02:45
79-34-5
1 11/07/22 02:45
127-18-4
1 11/07/22 02:45
108-88-3
1 11/07/22 02:45
87-61-6
1 11/07/22 02:45
120-82-1
1 11/07/22 02:45
71-55-6
1 11/07/22 02:45
79-00-5
1 11/07/22 02:45
79-01-6
1 11/07/22 02:45
75-69-4
1 11/07/22 02:45
76-13-1
1 11/07/22 02:45
75-01-4
1 11/07/22 02:45
1330-20-7
1 11/07/22 02:45
460-00-4
1 11/07/22 02:45
17060-07-0
1 11/07/22 02:45
2037-26-5
2 11 /02/22 21:40
123-91-1
2
2
f
I
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11 /02/22 21:40 17060-07-0
11 /02/22 21:40 2037-26-5
11 /03/22 18:23
11 /03/22 01:26 14797-55-8
11 /03/22 01:26 14797-65-0
11 /03/22 03:32
11 /03/22 21:06 14808-79-8
Page 13 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-12-110122 Lab ID: 92634190007 Collected: 11/01/22 16:47 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
8.3
1
11/04/22 15:14
11/05/22 15:01
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
8.3
1
11/04/22 15:14
11/05/22 15:01
101-84-8
Surrogates
Nitrobenzene-d5 (S)
54 %
10-144
1
11/04/22 15:14
11/05/22 15:01
4165-60-0
2-Fluorobiphenyl (S)
43 %
10-130
1
11/04/22 15:14
11/05/22 15:01
321-60-8
Terphenyl-d14 (S)
88 %
34-163
1
11/04/22 15:14
11/05/22 15:01
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2070 ug/L
80.0
40
11/02/22 21:59
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 %
70-130
40
11/02/22 21:59
17060-07-0
Toluene-d8(S)
101 %
70-130
40
11/02/22 21:59
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
357 mg/L
5.0
1
11/03/22 18:32
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/22 01:38
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/22 01:38
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.13 mg/L
0.050
1
11/03/22 03:35
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.4 mg/L
1.0
1
11/03/22 21:21
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-21B-110122
Lab ID: 92634190008 Collected:
11/01/22 18:04
Received: 11/02/22 07:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
43.2 ug/L
2.0
1
11/02/22 20:24
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
105 %
70-130
1
11/02/22 20:24
17060-07-0
Toluene-d8(S)
107 %
70-130
1
11/02/22 20:24
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
275 mg/L
5.0
1
11/03/22 18:41
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/22 01:39
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/22 01:39
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.061 mg/L
0.050
1
11/03/22 03:35
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
14.4 mg/L
1.0
1
11/03/22 21:36
14808-79-8
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-23A-110122 Lab ID: 92634190009 Collected: 11/01/22 15:12 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Ethylene glycol
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
Date: 11/23/2022 05:59 PM
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L
50.0
10
Analytical Method: RSK-175
Pace Analytical Gulf Coast
1700 ug/L
5.0
1
ND ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
362000 ug/L
45000
50
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
11/08/22 22:00 107-21-1 D3
11 /09/22 08:45 74-82-8
11 /09/22 08:45 74-84-0
11/09/22 08:45 74-85-1
11 /15/22 11:28 124-38-9
ND
ug/L
50.0
5
11/04/2215:14
11/05/2215:26
92-52-4
ND
ug/L
50.0
5
11/04/2215:14
11/05/2215:26
101-84-8
50
%
10-144
5
11/04/2215:14
11/05/2215:26
4165-60-0 D3
29
%
10-130
5
11 /04/22 15:14
11 /05/22 15:26
321-60-8
69
%
34-163
5
11 /04/22 15:14
11 /05/22 15:26
1718-51-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
5070
ug/L
625
25
11/08/22 21:47
67-64-1
ND
ug/L
25.0
25
11/08/22 21:47
71-43-2
ND
ug/L
25.0
25
11/08/22 21:47
74-97-5
ND
ug/L
25.0
25
11/08/22 21:47
75-27-4
ND
ug/L
25.0
25
11/08/22 21:47
75-25-2
ND
ug/L
50.0
25
11/08/22 21:47
74-83-9
857
ug/L
125
25
11/08/22 21:47
78-93-3
ND
ug/L
50.0
25
11/08/22 21:47
75-15-0
ND
ug/L
25.0
25
11/08/22 21:47
56-23-5
ND
ug/L
25.0
25
11/08/22 21:47
108-90-7
ND
ug/L
25.0
25
11/08/22 21:47
75-00-3
ND
ug/L
25.0
25
11/08/22 21:47
67-66-3
ND
ug/L
25.0
25
11/08/22 21:47
74-87-3
ND
ug/L
25.0
25
11/08/22 21:47
110-82-7
ND
ug/L
50.0
25
11/08/22 21:47
96-12-8
ND
ug/L
25.0
25
11/08/22 21:47
124-48-1
ND
ug/L
25.0
25
11/08/22 21:47
106-93-4
ND
ug/L
25.0
25
11/08/22 21:47
95-50-1
ND
ug/L
25.0
25
11/08/22 21:47
541-73-1
ND
ug/L
25.0
25
11/08/22 21:47
106-46-7
ND
ug/L
25.0
25
11/08/22 21:47
75-71-8
33.4
ug/L
25.0
25
11/08/22 21:47
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-23A-110122 Lab ID: 92634190009 Collected: 11/01/22 15:12 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,2-Dichloroethane
ND
ug/L
25.0
25
11/08/22 21:47
107-06-2
1,1-Dichloroethene
ND
ug/L
25.0
25
11/08/22 21:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
25.0
25
11/08/22 21:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
25.0
25
11/08/22 21:47
156-60-5
1,2-Dichloropropene
ND
ug/L
25.0
25
11/08/22 21:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
25.0
25
11/08/22 21:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
25.0
25
11/08/22 21:47
10061-02-6
Ethylbenzene
ND
ug/L
25.0
25
11/08/22 21:47
100-41-4
2-Hexanone
ND
ug/L
125
25
11/08/22 21:47
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
25.0
25
11/08/22 21:47
98-82-8
Methyl acetate
ND
ug/L
250
25
11/08/22 21:47
79-20-9
Methylcyclohexane
ND
ug/L
250
25
11/08/22 21:47
108-87-2
Methylene Chloride
ND
ug/L
125
25
11/08/22 21:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
125
25
11/08/22 21:47
108-10-1
Methyl-tert-butyl ether
ND
ug/L
25.0
25
11/08/22 21:47
1634-04-4
Styrene
ND
ug/L
25.0
25
11/08/22 21:47
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
25.0
25
11/08/22 21:47
79-34-5
Tetrachloroethene
ND
ug/L
25.0
25
11/08/22 21:47
127-18-4
Toluene
ND
ug/L
25.0
25
11/08/22 21:47
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
25.0
25
11/08/22 21:47
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
25.0
25
11/08/22 21:47
120-82-1
1,1,1-Trichloroethane
ND
ug/L
25.0
25
11/08/22 21:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
25.0
25
11/08/22 21:47
79-00-5
Trichloroethene
ND
ug/L
25.0
25
11/08/22 21:47
79-01-6
Trichlorofluoromethane
ND
ug/L
25.0
25
11/08/22 21:47
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
25.0
25
11/08/22 21:47
76-13-1
Vinyl chloride
ND
ug/L
25.0
25
11/08/22 21:47
75-01-4
Xylene (Total)
ND
ug/L
25.0
25
11/08/22 21:47
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
25
11/08/22 21:47
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-130
25
11/08/22 21:47
17060-07-0
Toluene-d8 (S)
100
%
70-130
25
11/08/22 21:47
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
3180
ug/L
100
50
11/03/22 04:54
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
107
%
70-130
50
11/03/22 04:54
17060-07-0
Toluene-d8(S)
99
%
70-130
50
11/03/22 04:54
2037-26-5
2320B Alkalinity
Analytical Method:
SM 2320B-2011
Pace Analytical
Services -Asheville
Alkalinity, Total as CaCO3
3100
mg/L
5.0
1
11/03/22 18:49
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-23A-110122
Lab ID: 92634190009 Collected:
11/01/22 15:12
Received: 11/02/22 07:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.40
10
11/03/22 01:51
14797-55-8
Nitrogen, Nitrite
0.057 mg/L
0.040
1
11/03/22 01:28
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.54 mg/L
0.12
2.5
11/03/22 03:33
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
5.4 mg/L
1.0
1
11/03/22 21:51
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
2560 mg/L
100
100
11/07/22 10:39
7440-44-0
Total Organic Carbon
2540 mg/L
100
100
11/07/22 10:39
7440-44-0
Total Organic Carbon
2510 mg/L
100
100
11/07/22 10:39
7440-44-0
Total Organic Carbon
2490 mg/L
100
100
11/07/22 10:39
7440-44-0
Mean Total Organic Carbon
2520 mg/L
100
100
11/07/22 10:39
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
2700 mg/L
250
500
11/18/2212:05
64-19-7
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-2313-110122 Lab ID: 92634190010 Collected: 11/01/22 16:44 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Ethylene glycol
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
Date: 11/23/2022 05:59 PM
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L
50.0
10
Analytical Method: RSK-175
Pace Analytical Gulf Coast
4400 ug/L
5.0
1
ND ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
294000 ug/L
45000
50
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
11/08/22 22:18 107-21-1 D3
11 /09/22 08:58 74-82-8
11 /09/22 08:58 74-84-0
11/09/22 08:58 74-85-1
11 /15/22 11:35 124-38-9
ND
ug/L
10.0
1
11/04/2215:14
11/05/2215:51
92-52-4
51.2
ug/L
10.0
1
11/04/2215:14
11/05/2215:51
101-84-8
42
%
10-144
1
11 /04/22 15:14
11 /05/22 15:51
4165-60-0
18
%
10-130
1
11 /04/22 15:14
11 /05/22 15:51
321-60-8
81
%
34-163
1
11 /04/22 15:14
11 /05/22 15:51
1718-51-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
2770
ug/L
250
10
11/08/22 20:53
67-64-1
ND
ug/L
10.0
10
11/08/22 20:53
71-43-2
ND
ug/L
10.0
10
11/08/22 20:53
74-97-5
ND
ug/L
10.0
10
11/08/22 20:53
75-27-4
ND
ug/L
10.0
10
11/08/22 20:53
75-25-2
ND
ug/L
20.0
10
11/08/22 20:53
74-83-9
433
ug/L
50.0
10
11/08/22 20:53
78-93-3
ND
ug/L
20.0
10
11/08/22 20:53
75-15-0
ND
ug/L
10.0
10
11/08/22 20:53
56-23-5
ND
ug/L
10.0
10
11/08/22 20:53
108-90-7
21.7
ug/L
10.0
10
11/08/22 20:53
75-00-3
ND
ug/L
10.0
10
11/08/22 20:53
67-66-3
ND
ug/L
10.0
10
11/08/22 20:53
74-87-3
ND
ug/L
10.0
10
11/08/22 20:53
110-82-7
ND
ug/L
20.0
10
11/08/22 20:53
96-12-8
ND
ug/L
10.0
10
11/08/22 20:53
124-48-1
ND
ug/L
10.0
10
11/08/22 20:53
106-93-4
ND
ug/L
10.0
10
11/08/22 20:53
95-50-1
ND
ug/L
10.0
10
11/08/22 20:53
541-73-1
ND
ug/L
10.0
10
11/08/22 20:53
106-46-7
ND
ug/L
10.0
10
11/08/22 20:53
75-71-8
ND
ug/L
10.0
10
11/08/22 20:53
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: 13-2313-110122 Lab ID: 92634190010 Collected: 11/01/22 16:44 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,2-Dichloroethane
ND
ug/L
10.0
10
11/08/22 20:53
107-06-2
1,1-Dichloroethene
ND
ug/L
10.0
10
11/08/22 20:53
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
10.0
10
11/08/22 20:53
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
10.0
10
11/08/22 20:53
156-60-5
1,2-Dichloropropene
ND
ug/L
10.0
10
11/08/22 20:53
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
10.0
10
11/08/22 20:53
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
10.0
10
11/08/22 20:53
10061-02-6
Ethylbenzene
ND
ug/L
10.0
10
11/08/22 20:53
100-41-4
2-Hexanone
ND
ug/L
50.0
10
11/08/22 20:53
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
10.0
10
11/08/22 20:53
98-82-8
Methyl acetate
ND
ug/L
100
10
11/08/22 20:53
79-20-9
Methylcyclohexane
ND
ug/L
100
10
11/08/22 20:53
108-87-2
Methylene Chloride
ND
ug/L
50.0
10
11/08/22 20:53
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
50.0
10
11/08/22 20:53
108-10-1
Methyl-tert-butyl ether
ND
ug/L
10.0
10
11/08/22 20:53
1634-04-4
Styrene
ND
ug/L
10.0
10
11/08/22 20:53
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
10.0
10
11/08/22 20:53
79-34-5
Tetrachloroethene
ND
ug/L
10.0
10
11/08/22 20:53
127-18-4
Toluene
ND
ug/L
10.0
10
11/08/22 20:53
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
10.0
10
11/08/22 20:53
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
10.0
10
11/08/22 20:53
120-82-1
1,1,1-Trichloroethane
ND
ug/L
10.0
10
11/08/22 20:53
71-55-6
1,1,2-Trichloroethane
ND
ug/L
10.0
10
11/08/22 20:53
79-00-5
Trichloroethene
ND
ug/L
10.0
10
11/08/22 20:53
79-01-6
Trichlorofluoromethane
ND
ug/L
10.0
10
11/08/22 20:53
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
10.0
10
11/08/22 20:53
76-13-1
Vinyl chloride
ND
ug/L
10.0
10
11/08/22 20:53
75-01-4
Xylene (Total)
ND
ug/L
10.0
10
11/08/22 20:53
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
10
11/08/22 20:53
460-00-4
1,2-Dichloroethane-d4 (S)
107
%
70-130
10
11/08/22 20:53
17060-07-0
Toluene-d8(S)
100
%
70-130
10
11/08/22 20:53
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
3010
ug/L
100
50
11/03/22 05:14
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
109
%
70-130
50
11/03/22 05:14
17060-07-0
Toluene-d8(S)
100
%
70-130
50
11/03/22 05:14
2037-26-5
2320B Alkalinity
Analytical Method:
SM 2320B-2011
Pace Analytical
Services -Asheville
Alkalinity, Total as CaCO3
2120
mg/L
5.0
1
11/03/22 20:13
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: 13-2313-110122
Lab ID: 92634190010 Collected:
11/01/22 16:44
Received: 11/02/22 07:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/22 01:37
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/22 01:37
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.12
2.5
11/03/22 03:34
D3
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
2.5 mg/L
1.0
1
11/03/22 22:36
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
834 mg/L
25.0
25
11/07/22 09:07
7440-44-0
Total Organic Carbon
840 mg/L
25.0
25
11/07/22 09:07
7440-44-0
Total Organic Carbon
835 mg/L
25.0
25
11/07/22 09:07
7440-44-0
Total Organic Carbon
834 mg/L
25.0
25
11/07/22 09:07
7440-44-0
Mean Total Organic Carbon
836 mg/L
25.0
25
11/07/22 09:07
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
1100 mg/L
100
200
11/17/2213:37
64-19-7
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-17C-110122 Lab ID: 92634190011 Collected: 11/01/22 13:47 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Biodegradation Indicator Gases Analytical Method: RSK-175
Pace Analytical Gulf Coast
Methane
24 ug/L
5.0
1
11/09/22 09:10
74-82-8
Ethane
ND ug/L
1.0
1
11/09/22 09:10
74-84-0
Ethene
ND ug/L
1.0
1
11/09/22 09:10
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
105000 ug/L
45000
50
11/15/22 11:41
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
8.3
1
11/04/22 15:14
11/05/22 16:16
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
8.3
1
11/04/22 15:14
11/05/22 16:16
101-84-8
Surrogates
Nitrobenzene-d5 (S)
32 %
10-144
1
11/04/22 15:14
11/05/22 16:16
4165-60-0
2-Fluorobiphenyl (S)
20 %
10-130
1
11/04/22 15:14
11/05/22 16:16
321-60-8
Terphenyl-d14 (S)
65 %
34-163
1
11/04/22 15:14
11/05/22 16:16
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1540 ug/L
40.0
20
11/03/22 05:33
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
107 %
70-130
20
11/03/22 05:33
17060-07-0
Toluene-d8(S)
99 %
70-130
20
11/03/22 05:33
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
412 mg/L
5.0
1
11/03/22 20:47
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/22 01:24
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/22 01:24
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.24 mg/L
0.050
1
11/03/22 03:31
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.2 mg/L
1.0
1
11/03/22 22:51
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
2.8 mg/L
1.0
1
11/07/22 09:25
7440-44-0
Total Organic Carbon
2.8 mg/L
1.0
1
11/07/22 09:25
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-17C-110122
Parameters
Lab ID: 92634190011 Collected: 11/01/22 13:47
Results Units Report Limit DF
Received: 11/02/22 07:36 Matrix: Water
Prepared Analyzed CAS No. Qual
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
2.8 mg/L
1.0
1
11/07/22 09:25
7440-44-0
Total Organic Carbon
2.8 mg/L
1.0
1
11/07/22 09:25
7440-44-0
Mean Total Organic Carbon
2.8 mg/L
1.0
1
11/07/22 09:25
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
0.53 mg/L
0.50
1
11/08/22 23:25
64-19-7
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-1713-110122 Lab ID: 92634190012 Collected: 11/01/22 15:24 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Biodegradation Indicator Gases Analytical Method: RSK-175
Pace Analytical Gulf Coast
Methane
26 ug/L
5.0
1
11/09/22 09:22
74-82-8
Ethane
ND ug/L
1.0
1
11/09/22 09:22
74-84-0
Ethene
ND ug/L
1.0
1
11/09/22 09:22
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
154000 ug/L
45000
50
11/15/22 11:49
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
9.1
1
11/04/22 15:14
11/05/22 16:42
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
9.1
1
11/04/22 15:14
11/05/22 16:42
101-84-8
Surrogates
Nitrobenzene-d5 (S)
29 %
10-144
1
11/04/22 15:14
11/05/22 16:42
4165-60-0
2-Fluorobiphenyl (S)
15 %
10-130
1
11/04/22 15:14
11/05/22 16:42
321-60-8
Terphenyl-d14 (S)
58 %
34-163
1
11/04/22 15:14
11/05/22 16:42
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
533 ug/L
20.0
10
11/04/22 09:53
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
112 %
70-130
10
11/04/22 09:53
17060-07-0
Toluene-d8(S)
101 %
70-130
10
11/04/22 09:53
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
276 mg/L
5.0
1
11/03/22 20:56
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.40
10
11/03/22 01:52
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/22 01:30
14797-65-0 M1
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.27 mg/L
0.050
1
11/03/22 03:33
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
2.1 mg/L
1.0
1
11/03/22 23:05
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
3.4 mg/L
1.0
1
11/07/22 09:43
7440-44-0
Total Organic Carbon
3.2 mg/L
1.0
1
11/07/22 09:43
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 65

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ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-17B-110122
Parameters
Lab ID: 92634190012 Collected: 11/01/22 15:24
Results Units Report Limit DF
Received: 11/02/22 07:36 Matrix: Water
Prepared Analyzed CAS No. Qual
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
3.1 mg/L
1.0
1
11/07/22 09:43
7440-44-0
Total Organic Carbon
3.0 mg/L
1.0
1
11/07/22 09:43
7440-44-0
Mean Total Organic Carbon
3.2 mg/L
1.0
1
11/07/22 09:43
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
0.53 mg/L
0.50
1
11/08/22 23:47
64-19-7
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 65

leAnalyiical
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ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: Trip Blank-01-110122 Lab ID: 92634190013 Collected: 11/01/22 00:00 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/06/22 22:44
67-64-1
Benzene
ND
ug/L
1.0
1
11/06/22 22:44
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
11/06/22 22:44
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/06/22 22:44
75-27-4
Bromoform
ND
ug/L
1.0
1
11/06/22 22:44
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/06/22 22:44
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
11/06/22 22:44
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
11/06/22 22:44
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
11/06/22 22:44
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/06/22 22:44
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/06/22 22:44
75-00-3
Chloroform
ND
ug/L
1.0
1
11/06/22 22:44
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/06/22 22:44
74-87-3
Cyclohexane
ND
ug/L
1.0
1
11/06/22 22:44
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/06/22 22:44
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/06/22 22:44
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/06/22 22:44
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/06/22 22:44
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/06/22 22:44
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/06/22 22:44
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/06/22 22:44
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/06/22 22:44
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/06/22 22:44
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/06/22 22:44
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/06/22 22:44
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/06/22 22:44
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
11/06/22 22:44
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/06/22 22:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/06/22 22:44
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
11/06/22 22:44
100-41-4
2-Hexanone
ND
ug/L
5.0
1
11/06/22 22:44
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
11/06/22 22:44
98-82-8
Methyl acetate
ND
ug/L
10.0
1
11/06/22 22:44
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
11/06/22 22:44
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
11/06/22 22:44
75-09-2 v2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/06/22 22:44
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/06/22 22:44
1634-04-4
Styrene
ND
ug/L
1.0
1
11/06/22 22:44
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
11/06/22 22:44
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/06/22 22:44
127-18-4
Toluene
ND
ug/L
1.0
1
11/06/22 22:44
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/06/22 22:44
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/06/22 22:44
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
1
11/06/22 22:44
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
11/06/22 22:44
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/06/22 22:44
79-01-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM
without
the written consent of Pace Analytical Services, LLC.
Page 26 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: Trip Blank-01-110122
Parameters
Lab ID: 92634190013 Collected: 11/01/22 00:00
Results Units Report Limit DF
Received: 11/02/22 07:36 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Trichlorofluoromethane
ND ug/L
1.0
1
11/06/22 22:44
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
1.0
1
11/06/22 22:44
76-13-1
Vinyl chloride
ND ug/L
1.0
1
11/06/22 22:44
75-01-4
Xylene (Total)
ND ug/L
1.0
1
11/06/22 22:44
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
11/06/22 22:44
460-00-4
1,2-Dichloroethane-d4 (S)
94 %
70-130
1
11/06/22 22:44
17060-07-0
Toluene-d8(S)
106 %
70-130
1
11/06/22 22:44
2037-26-5
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 65

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-17C-110122 H2 Lab ID: 92634190014 Collected: 11/01/22 14:30 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen ND nM 1.9 1 11/04/22 07:14 1333-74-0
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-23A-110122 H2 Lab ID: 92634190015 Collected: 11/01/22 16:07 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen ND nM 1.9 1 11/04/22 07:26 1333-74-0
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: B-17B-110122 H2 Lab ID: 92634190016 Collected: 11/01/22 16:00 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen ND nM 1.9 1 11/04/22 07:38 1333-74-0
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 65

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Sample: 13-2313-110122 H2 Lab ID: 92634190017 Collected: 11/01/22 17:24 Received: 11/02/22 07:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen 2.2 nM 1.9 1 11/04/22 07:50 1333-74-0
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 65

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Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 704834 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92634190001, 92634190002, 92634190003, 92634190004, 92634190009, 92634190010
METHOD BLANK: 3240206
Matrix:
Water
Associated Lab Samples: 92634190001, 92634190002, 92634190003, 92634190004, 92634190009, 92634190010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethylene glycol
mg/L
ND
5.0
11/07/22 16:39
LABORATORY CONTROL SAMPLE:
3240207
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Ethylene glycol
mg/L
25
28.9
115 34-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3240208 3240209
MS MSD
60414071004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 28.5 31.3 108 120 39-168 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 753313 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Bubble Strip H2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92634190014, 92634190015, 92634190016, 92634190017
METHOD BLANK: 2416757 Matrix: Air
Associated Lab Samples: 92634190014, 92634190015, 92634190016, 92634190017
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hydrogen nM ND 1.9 11/04/22 06:47
LABORATORY CONTROL SAMPLE & LCSD: 2416758 2416759
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Hydrogen nM 12 12 13 106 109 70-130 3 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 65

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 753612 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: Biodegradation Indicator Gases
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92634190009, 92634190010, 92634190011, 92634190012
METHOD BLANK: 2418651
Matrix: Water
Associated Lab Samples:
92634190009, 92634190010, 92634190011, 92634190012
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Methane
ug/L
ND 5.0
11/09/22 07:41
Ethane
ug/L
ND 1.0
11/09/22 07:41
Ethene
ug/L
ND 1.0
11/09/22 07:41 BO
LABORATORY CONTROL SAMPLE & LCSD:
2418652
2418653
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Methane
ug/L
380
350 350
91 90
70-130 1 30
Ethane
ug/L
97
84 84
87 86
70-130 1 30
Ethene
ug/L
120
100 100
83 83
70-130 0 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 65

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 754009 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175 CO2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92634190009, 92634190010, 92634190011, 92634190012
METHOD BLANK: 2420915 Matrix: Water
Associated Lab Samples: 92634190009, 92634190010, 92634190011, 92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Carbon dioxide ug/L ND 900 11/15/22 11:03
LABORATORY CONTROL SAMPLE: 2420916
Parameter
Carbon dioxide
Spike LCS
Units Conc. Result
ug/L 8700 6630
LCS % Rec
% Rec Limits Qualifiers
76 38-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 35 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 735208 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190005, 92634190006, 92634190013
METHOD BLANK: 3826552 Matrix:
Associated Lab Samples: 92634190005, 92634190006, 92634190013
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
11/06/22 21:35
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/06/22 21:35
1,1,2-Trichloroethane
ug/L
ND
1.0
11/06/22 21:35
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
11/06/22 21:35
1,1-Dichloroethane
ug/L
ND
1.0
11/06/22 21:35
1,1-Dichloroethene
ug/L
ND
1.0
11/06/22 21:35
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/06/22 21:35
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/06/22 21:35
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
11/06/22 21:35
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/06/22 21:35
1,2-Dichlorobenzene
ug/L
ND
1.0
11/06/22 21:35
1,2-Dichloroethane
ug/L
ND
1.0
11/06/22 21:35
1,2-Dichloropropane
ug/L
ND
1.0
11/06/22 21:35
1,3-Dichlorobenzene
ug/L
ND
1.0
11/06/22 21:35
1,4-Dichlorobenzene
ug/L
ND
1.0
11/06/22 21:35
2-Butanone (MEK)
ug/L
ND
5.0
11/06/22 21:35
2-Hexanone
ug/L
ND
5.0
11/06/22 21:35
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/06/22 21:35
Acetone
ug/L
ND
25.0
11/06/22 21:35
Benzene
ug/L
ND
1.0
11/06/22 21:35
Bromochloromethane
ug/L
ND
1.0
11/06/22 21:35
Bromodichloromethane
ug/L
ND
1.0
11/06/22 21:35
Bromoform
ug/L
ND
1.0
11/06/22 21:35
Bromomethane
ug/L
ND
2.0
11/06/22 21:35
Carbon disulfide
ug/L
ND
2.0
11/06/22 21:35
Carbon tetrachloride
ug/L
ND
1.0
11/06/22 21:35
Chlorobenzene
ug/L
ND
1.0
11/06/22 21:35
Chloroethane
ug/L
ND
1.0
11/06/22 21:35
Chloroform
ug/L
ND
1.0
11/06/22 21:35
Chloromethane
ug/L
ND
1.0
11/06/22 21:35
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/06/22 21:35
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/06/22 21:35
Cyclohexane
ug/L
ND
1.0
11/06/22 21:35
Dibromochloromethane
ug/L
ND
1.0
11/06/22 21:35
Dichlorodifluoromethane
ug/L
ND
1.0
11/06/22 21:35
Ethylbenzene
ug/L
ND
1.0
11/06/22 21:35
Isopropylbenzene (Cumene)
ug/L
ND
1.0
11/06/22 21:35
Methyl acetate
ug/L
ND
10.0
11/06/22 21:35
Methyl-tert-butyl ether
ug/L
ND
1.0
11/06/22 21:35
Methylcyclohexane
ug/L
ND
10.0
11/06/22 21:35
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
METHOD BLANK: 3826552 Matrix:
Associated Lab Samples: 92634190005, 92634190006, 92634190013
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Methylene Chloride
ug/L
ND
5.0
11/06/22 21:35 v2
Styrene
ug/L
ND
1.0
11/06/22 21:35
Tetrachloroethene
ug/L
ND
1.0
11/06/22 21:35
Toluene
ug/L
ND
1.0
11/06/22 21:35
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/06/22 21:35
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/06/22 21:35
Trichloroethene
ug/L
ND
1.0
11/06/22 21:35
Trichlorofluoromethane
ug/L
ND
1.0
11/06/22 21:35
Vinyl chloride
ug/L
ND
1.0
11/06/22 21:35
Xylene (Total)
ug/L
ND
1.0
11/06/22 21:35
1,2-Dichloroethane-d4 (S)
%
93
70-130
11/06/22 21:35
4-Bromofluorobenzene (S)
%
96
70-130
11/06/22 21:35
Toluene-d8(S)
%
105
70-130
11/06/22 21:35
LABORATORY CONTROL SAMPLE:
Parameter
3826553
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
47.1
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
53.0
106
70-130
1,1,2-Trichloroethane
ug/L
50
52.6
105
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
49.7
99
70-130
1,1-Dichloroethane
ug/L
50
46.5
93
70-130
1,1-Dichloroethene
ug/L
50
49.3
99
70-130
1,2,3-Trichlorobenzene
ug/L
50
56.9
114
70-130
1,2,4-Trichlorobenzene
ug/L
50
55.2
110
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.7
109
70-131
1,2-Dibromoethane (EDB)
ug/L
50
56.9
114
70-130
1,2-Dichlorobenzene
ug/L
50
56.1
112
70-130
1,2-Dichloroethane
ug/L
50
46.3
93
70-130
1,2-Dichloropropane
ug/L
50
51.4
103
70-130
1,3-Dichlorobenzene
ug/L
50
55.0
110
70-130
1,4-Dichlorobenzene
ug/L
50
54.1
108
70-130
2-Butanone (MEK)
ug/L
100
96.9
97
70-134
2-Hexanone
ug/L
100
108
108
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
100
100
70-130
Acetone
ug/L
100
92.1
92
70-133
Benzene
ug/L
50
48.9
98
70-130
Bromochloromethane
ug/L
50
53.0
106
70-130
Bromodichloromethane
ug/L
50
49.8
100
70-130
Bromoform
ug/L
50
55.3
111
70-130
Bromomethane
ug/L
50
37.7
75
45-151 v3
Carbon disulfide
ug/L
50
48.0
96
70-130
Carbon tetrachloride
ug/L
50
48.6
97
70-130
Chlorobenzene
ug/L
50
53.5
107
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
LABORATORY CONTROL SAMPLE:
Parameter
3826553
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloroethane
ug/L
50
49.9
100
39-152
Chloroform
ug/L
50
46.6
93
70-130
Chloromethane
ug/L
50
44.3
89
58-130
cis-1,2-Dichloroethene
ug/L
50
47.1
94
70-130
cis-1,3-Dichloropropene
ug/L
50
52.0
104
70-130
Cyclohexane
ug/L
50
52.4
105
70-130
Dibromochloromethane
ug/L
50
56.3
113
70-130
Dichlorodifluoromethane
ug/L
50
49.0
98
54-133
Ethylbenzene
ug/L
50
52.8
106
70-130
Isopropylbenzene (Cumene)
ug/L
50
53.1
106
70-130
Methyl acetate
ug/L
50
51.2
102
70-130
Methyl-tert-butyl ether
ug/L
50
51.5
103
70-130
Methylcyclohexane
ug/L
50
52.1
104
70-130
Methylene Chloride
ug/L
50
40.3
81
66-130 v3
Styrene
ug/L
50
55.8
112
70-130
Tetrachloroethene
ug/L
50
51.2
102
70-130
Toluene
ug/L
50
48.4
97
70-130
trans-1,2-Dichloroethene
ug/L
50
48.7
97
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.7
105
70-130
Trichloroethene
ug/L
50
51.2
102
70-130
Trichlorofluoromethane
ug/L
50
43.2
86
62-130
Vinyl chloride
ug/L
50
49.0
98
62-130
Xylene (Total)
ug/L
150
161
108
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
Parameter
3826555
Units
92634520002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
ND
20
28.9
145
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
26.5
133
69-142
1,1,2-Trichloroethane
ug/L
ND
20
27.3
137
70-138
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
31.3
157
70-157
1,1-Dichloroethane
ug/L
ND
20
28.1
141
70-150
1,1-Dichloroethene
ug/L
ND
20
31.2
156
70-156
1,2,3-Trichlorobenzene
ug/L
ND
20
26.2
131
70-148
1,2,4-Trichlorobenzene
ug/L
ND
20
25.6
128
70-146
1,2-Dibromo-3-chloropropane
ug/L
ND
20
25.5
127
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
27.0
135
70-138
1,2-Dichlorobenzene
ug/L
ND
20
26.4
132
70-141
1,2-Dichloroethane
ug/L
ND
20
26.7
133
69-143
1,2-Dichloropropane
ug/L
ND
20
28.4
142
68-156
1,3-Dichlorobenzene
ug/L
ND
20
26.5
133
70-143
1,4-Dichlorobenzene
ug/L
ND
20
26.0
130
70-142
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
MATRIX SPIKE SAMPLE:
3826555
92634520002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Butanone (MEK)
ug/L
ND
40
54.0
135
60-157
2-Hexanone
ug/L
ND
40
55.9
140
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
53.5
134
70-141
Acetone
ug/L
ND
40
49.2
123
58-157
Benzene
ug/L
ND
20
26.4
132
70-142
Bromochloromethane
ug/L
ND
20
27.3
137
70-146
Bromodichloromethane
ug/L
ND
20
27.7
139
70-139
Bromoform
ug/L
ND
20
28.2
141
64-140 M1
Bromomethane
ug/L
ND
20
32.0
160
28-192
Carbon disulfide
ug/L
ND
20
27.8
139
70-151
Carbon tetrachloride
ug/L
ND
20
30.8
154
70-148 M1
Chlorobenzene
ug/L
ND
20
26.4
132
70-141
Chloroethane
ug/L
ND
20
35.5
177
58-191
Chloroform
ug/L
ND
20
27.3
137
70-148
Chloromethane
ug/L
ND
20
36.7
183
43-162 M1,v1
cis-1,2-Dichloroethene
ug/L
ND
20
28.1
138
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
27.1
135
70-139
Cyclohexane
ug/L
ND
20
31.7
158
77-149 M1
Dibromochloromethane
ug/L
ND
20
27.4
137
70-144
Dichlorodifluoromethane
ug/L
ND
20
33.8
169
39-171
Ethylbenzene
ug/L
ND
20
26.7
133
70-143
Isopropylbenzene (Cumene)
ug/L
ND
20
27.1
136
70-145
Methyl acetate
ug/L
ND
20
21.4
107
63-146
Methyl-tert-butyl ether
ug/L
ND
20
24.4
122
65-143
Methylcyclohexane
ug/L
ND
20
31.8
159
70-144 M1
Methylene Chloride
ug/L
ND
20
27.4
137
62-149
Styrene
ug/L
ND
20
26.5
133
70-143
Tetrachloroethene
ug/L
ND
20
26.1
130
70-145
Toluene
ug/L
ND
20
26.7
134
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
28.3
142
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
27.7
138
70-139
Trichloroethene
ug/L
ND
20
28.9
141
62-146
Trichlorofluoromethane
ug/L
ND
20
34.9
174
63-153 M1,v1
Vinyl chloride
ug/L
ND
20
37.3
186
61-163 M1,v1
Xylene (Total)
ug/L
ND
60
80.5
134
70-143
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 3826554
92633655008
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
SAMPLE DUPLICATE: 3826554
Parameter
Units
92633655008
Result
Dup
Result
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichlorobenzene
ug/L
ND
1,2,4-Trichlorobenzene
ug/L
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
1,2-Dibromoethane (EDB)
ug/L
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,3-Dichlorobenzene
ug/L
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
10.3J
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Cyclohexane
ug/L
ND
Dibromochloromethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
Ethylbenzene
ug/L
ND
ND
Isopropylbenzene (Cumene)
ug/L
ND
Methyl acetate
ug/L
ND
Methyl-tert-butyl ether
ug/L
ND
Methylcyclohexane
ug/L
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
0.65J
.57J
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
RPD Qualifiers
v1
v1
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
SAMPLE DUPLICATE: 3826554
92633655008 Dup
Parameter Units Result Result RPD Qualifiers
1,2-Dichloroethane-d4 (S) % 93 91
4-Bromofluorobenzene (S) % 94 100
Toluene-d8 (S) % 104 108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 735406 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190009, 92634190010
METHOD BLANK: 3827493
Associated Lab Samples: 92634190009, 92634190010
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
11/08/22 16:39
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/08/22 16:39
1,1,2-Trichloroethane
ug/L
ND
1.0
11/08/22 16:39
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
11/08/22 16:39
1,1-Dichloroethane
ug/L
ND
1.0
11/08/22 16:39
1,1-Dichloroethene
ug/L
ND
1.0
11/08/22 16:39
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/08/22 16:39
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/08/22 16:39
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
11/08/22 16:39
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/08/22 16:39
1,2-Dichlorobenzene
ug/L
ND
1.0
11/08/22 16:39
1,2-Dichloroethane
ug/L
ND
1.0
11/08/22 16:39
1,2-Dichloropropane
ug/L
ND
1.0
11/08/22 16:39
1,3-Dichlorobenzene
ug/L
ND
1.0
11/08/22 16:39
1,4-Dichlorobenzene
ug/L
ND
1.0
11/08/22 16:39
2-Butanone (MEK)
ug/L
ND
5.0
11/08/22 16:39
2-Hexanone
ug/L
ND
5.0
11/08/22 16:39
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/08/22 16:39
Acetone
ug/L
ND
25.0
11/08/22 16:39
Benzene
ug/L
ND
1.0
11/08/22 16:39
Bromochloromethane
ug/L
ND
1.0
11/08/22 16:39
Bromodichloromethane
ug/L
ND
1.0
11/08/22 16:39
Bromoform
ug/L
ND
1.0
11/08/22 16:39
Bromomethane
ug/L
ND
2.0
11/08/22 16:39
Carbon disulfide
ug/L
ND
2.0
11/08/22 16:39
Carbon tetrachloride
ug/L
ND
1.0
11/08/22 16:39
Chlorobenzene
ug/L
ND
1.0
11/08/22 16:39
Chloroethane
ug/L
ND
1.0
11/08/22 16:39
Chloroform
ug/L
ND
1.0
11/08/22 16:39
Chloromethane
ug/L
ND
1.0
11/08/22 16:39
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/08/22 16:39
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/08/22 16:39
Cyclohexane
ug/L
ND
1.0
11/08/22 16:39
Dibromochloromethane
ug/L
ND
1.0
11/08/22 16:39
Dichlorodifluoromethane
ug/L
ND
1.0
11/08/22 16:39
Ethylbenzene
ug/L
ND
1.0
11/08/22 16:39
Isopropylbenzene (Cumene)
ug/L
ND
1.0
11/08/22 16:39
Methyl acetate
ug/L
ND
10.0
11/08/22 16:39
Methyl-tert-butyl ether
ug/L
ND
1.0
11/08/22 16:39
Methylcyclohexane
ug/L
ND
10.0
11/08/22 16:39
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
METHOD BLANK: 3827493
Associated Lab Samples: 92634190009, 92634190010
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Methylene Chloride
ug/L
ND
5.0
11/08/22 16:39
Styrene
ug/L
ND
1.0
11/08/22 16:39
Tetrachloroethene
ug/L
ND
1.0
11/08/22 16:39
Toluene
ug/L
ND
1.0
11/08/22 16:39
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/08/22 16:39
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/08/22 16:39
Trichloroethene
ug/L
ND
1.0
11/08/22 16:39
Trichlorofluoromethane
ug/L
ND
1.0
11/08/22 16:39
Vinyl chloride
ug/L
ND
1.0
11/08/22 16:39
Xylene (Total)
ug/L
ND
1.0
11/08/22 16:39
1,2-Dichloroethane-d4 (S)
%
105
70-130
11/08/22 16:39
4-Bromofluorobenzene (S)
%
96
70-130
11/08/22 16:39
Toluene-d8 (S)
%
100
70-130
11/08/22 16:39
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3827494
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
50
46.7
93
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.3
99
70-130
1,1,2-Trichloroethane
ug/L
50
47.5
95
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethane
ug/L
50
45.3
91
70-130
1,1-Dichloroethene
ug/L
50
48.3
97
70-130
1,2,3-Trichlorobenzene
ug/L
50
49.3
99
70-130
1,2,4-Trichlorobenzene
ug/L
50
48.5
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.5
101
70-131
1,2-Dibromoethane (EDB)
ug/L
50
49.7
99
70-130
1,2-Dichlorobenzene
ug/L
50
48.1
96
70-130
1,2-Dichloroethane
ug/L
50
47.4
95
70-130
1,2-Dichloropropane
ug/L
50
48.6
97
70-130
1,3-Dichlorobenzene
ug/L
50
48.0
96
70-130
1,4-Dichlorobenzene
ug/L
50
47.0
94
70-130
2-Butanone (MEK)
ug/L
100
96.5
96
70-134
2-Hexanone
ug/L
100
105
105
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
96.5
96
70-133
Benzene
ug/L
50
45.1
90
70-130
Bromochloromethane
ug/L
50
47.8
96
70-130
Bromodichloromethane
ug/L
50
48.6
97
70-130
Bromoform
ug/L
50
50.4
101
70-130
Bromomethane
ug/L
50
43.8
88
45-151
Carbon disulfide
ug/L
50
44.4
89
70-130
Carbon tetrachloride
ug/L
50
46.2
92
70-130
Chlorobenzene
ug/L
50
47.3
95
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
LABORATORY CONTROL SAMPLE:
Parameter
3827494
Units
Spike LCS
Conc. Result
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Cyclohexane
ug/L
50
Dibromochloromethane
ug/L
50
Dichlorodifluoromethane
ug/L
50
Ethylbenzene
ug/L
50
Isopropylbenzene (Cumene)
ug/L
50
Methyl acetate
ug/L
50
Methyl-tert-butyl ether
ug/L
50
Methylcyclohexane
ug/L
50
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
47.4
95
39-152
46.1
92
70-130
46.8
94
58-130
46.9
94
70-130
48.8
98
70-130
46.4
93
70-130
48.7
97
70-130
46.9
94
54-133
47.3
95
70-130
47.5
95
70-130
47.8
96
70-130
47.0
94
70-130
46.3
93
70-130
46.5
93
66-130
49.4
99
70-130
44.2
88
70-130
46.2
92
70-130
47.5
95
70-130
50.0
100
70-130
47.7
95
70-130
44.3
89
62-130
50.0
100
62-130
146
97
70-130
97
70-130
103
70-130
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3827495
MS
92634449008 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3827496
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
200
200
160
165
80
83
70-150
3
1,1,2,2-Tetrachloroethane
ug/L
ND
200
200
161
166
80
83
69-142
3
1,1,2-Trichloroethane
ug/L
ND
200
200
162
163
81
81
70-138
0
1,1,2-Trichlorotrifluoroethane
ug/L
ND
200
200
149
164
75
82
70-157
10
1,1-Dichloroethane
ug/L
ND
200
200
155
162
78
81
70-150
4
1,1-Dichloroethene
ug/L
ND
200
200
164
173
82
86
70-156
5
1,2,3-Trichlorobenzene
ug/L
ND
200
200
148
163
74
82
70-148
9
1,2,4-Trichlorobenzene
ug/L
ND
200
200
144
157
72
79
70-146
9
1,2-Dibromo-3-chloropropane
ug/L
ND
200
200
154
157
77
79
68-146
2
1,2-Dibromoethane (EDB)
ug/L
ND
200
200
167
171
84
85
70-138
2
1,2-Dichlorobenzene
ug/L
ND
200
200
157
166
78
83
70-141
6
1,2-Dichloroethane
ug/L
ND
200
200
160
168
80
84
69-143
5
1,2-Dichloropropane
ug/L
ND
200
200
160
170
80
85
68-156
6
1,3-Dichlorobenzene
ug/L
ND
200
200
148
159
74
79
70-143
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 44 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3827495
3827496
MS
MSD
92634449008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
200
200
148
157
74
78
70-142
6
2-Butanone (MEK)
ug/L
644
400
400
925
923
70
70
60-157
0
2-Hexanone
ug/L
ND
400
400
318
325
80
81
68-146
2
4-Methyl-2-pentanone (MIBK)
ug/L
90.0
400
400
420
425
83
84
70-141
1
Acetone
ug/L
3430
400
400
3490
3500
14
17
58-157
0 M1
Benzene
ug/L
ND
200
200
160
166
76
79
70-142
3
Bromochloromethane
ug/L
ND
200
200
160
170
80
85
70-146
6
Bromodichloromethane
ug/L
ND
200
200
157
165
79
82
70-139
5
Bromoform
ug/L
ND
200
200
158
160
79
80
64-140
2
Bromomethane
ug/L
ND
200
200
95.7
123
48
61
28-192
25
Carbon disulfide
ug/L
ND
200
200
137
153
68
77
70-151
12 M1
Carbon tetrachloride
ug/L
ND
200
200
155
165
77
82
70-148
6
Chlorobenzene
ug/L
ND
200
200
157
164
79
82
70-141
4
Chloroethane
ug/L
ND
200
200
173
182
86
91
58-191
5
Chloroform
ug/L
ND
200
200
159
163
80
81
70-148
2
Chloromethane
ug/L
ND
200
200
149
157
75
79
43-162
6
cis-1,2-Dichloroethene
ug/L
11.2
200
200
169
177
79
83
68-151
4
cis-1,3-Dichloropropene
ug/L
ND
200
200
148
155
74
77
70-139
4
Cyclohexane
ug/L
ND
200
200
150
165
75
82
77-149
9 M1
Dibromochloromethane
ug/L
ND
200
200
156
162
78
81
70-144
4
Dichlorodifluoromethane
ug/L
ND
200
200
132
143
66
72
39-171
8
Ethylbenzene
ug/L
ND
200
200
156
163
78
82
70-143
4
Isopropylbenzene (Cumene)
ug/L
ND
200
200
153
164
77
82
70-145
7
Methyl acetate
ug/L
ND
200
200
146
157
73
79
63-146
8
Methyl-tert-butyl ether
ug/L
ND
200
200
162
168
81
84
65-143
4
Methylcyclohexane
ug/L
ND
200
200
148
160
74
80
70-144
8
Methylene Chloride
ug/L
ND
200
200
180
188
72
76
62-149
4
Styrene
ug/L
ND
200
200
157
165
78
83
70-143
5
Tetrachloroethene
ug/L
ND
200
200
139
147
70
74
70-145
5
Toluene
ug/L
ND
200
200
156
168
76
82
70-142
7
trans-1,2-Dichloroethene
ug/L
ND
200
200
152
162
76
81
70-151
6
trans- 1,3-Dichloropropene
ug/L
ND
200
200
149
153
74
76
70-139
3
Trichloroethene
ug/L
ND
200
200
156
169
78
85
62-146
8
Trichlorofluoromethane
ug/L
ND
200
200
149
158
75
79
63-153
6
Vinyl chloride
ug/L
ND
200
200
163
175
82
87
61-163
7
Xylene (Total)
ug/L
ND
600
600
473
500
79
83
70-143
6
1,2-Dichloroethane-d4 (S)
%
104
104
70-130
4-Bromofluorobenzene (S)
%
104
102
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 45 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734464 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190009, 92634190010, 92634190011
METHOD BLANK: 3822645
Matrix:
Water
Associated Lab Samples:
92634190009, 92634190010, 92634190011
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
11/02/22 23:09
1,2-Dichloroethane-d4 (S)
%
106
70-130
11/02/22 23:09
Toluene-d8 (S)
%
99
70-130
11/02/22 23:09
LABORATORY CONTROL SAMPLE: 3822646
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.5 88 70-130
1,2-Dichloroethane-d4 (S) % 105 70-130
Toluene-d8 (S) % 98 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3822647
3822648
MS
MSD
92634230014 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 17.6
18.1 88
91
63-136 3
1,2-Dichloroethane-d4 (S)
%
109
111
70-130
Toluene-d8(S)
%
101
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734466 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190001, 92634190002, 92634190004, 92634190005, 92634190006, 92634190007, 92634190008
METHOD BLANK: 3822656
Matrix:
Water
Associated Lab Samples:
92634190001, 92634190002, 92634190004, 92634190005, 92634190006,
92634190007, 92634190008
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
11/02/22 15:01
1,2-Dichloroethane-d4 (S)
%
94
70-130
11/02/22 15:01
Toluene-d8 (S)
%
103
70-130
11/02/22 15:01
LABORATORY CONTROL SAMPLE: 3822657
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.2 86 70-130
1,2-Dichloroethane-d4 (S) % 106 70-130
Toluene-d8 (S) % 105 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3822658
3822659
MS
MSD
92634190001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 18.4
18.3 92
91
63-136 1
1,2-Dichloroethane-d4 (S)
%
108
98
70-130
Toluene-d8(S)
%
98
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734715 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190003
METHOD BLANK: 3823845
Matrix:
Water
Associated Lab Samples: 92634190003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
11/03/22 13:31
1,2-Dichloroethane-d4 (S)
%
108
70-130
11/03/22 13:31
Toluene-d8 (S)
%
99
70-130
11/03/22 13:31
LABORATORY CONTROL SAMPLE: 3823846
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 18.3 91 70-130
1,2-Dichloroethane-d4 (S) % 107 70-130
Toluene-d8 (S) % 100 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823847
3823848
MS
MSD
92634407001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.7
17.6 99
88
63-136 12
1,2-Dichloroethane-d4 (S)
%
110
113
70-130
Toluene-d8(S)
%
100
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734931 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190012
METHOD BLANK: 3825022
Matrix:
Water
Associated Lab Samples: 92634190012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
11/04/22 07:58
1,2-Dichloroethane-d4 (S)
%
110
70-130
11/04/22 07:58
Toluene-d8(S)
%
101
70-130
11/04/22 07:58
LABORATORY CONTROL SAMPLE: 3825023
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 17.7 88 70-130
1,2-Dichloroethane-d4 (S) % 109 70-130
Toluene-d8 (S) % 100 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3825024
3825025
MS
MSD
92634449002 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 1070 400
400
1410
1490 85
106
63-136 6
1,2-Dichloroethane-d4 (S)
%
114
114
70-130
Toluene-d8(S)
%
103
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734946 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634190001, 92634190002, 92634190003, 92634190004, 92634190005, 92634190006, 92634190007,
92634190009,92634190010,92634190011,92634190012
METHOD BLANK: 3825113 Matrix: Water
Associated Lab Samples: 92634190001, 92634190002, 92634190003, 92634190004, 92634190005, 92634190006, 92634190007,
92634190009,92634190010,92634190011,92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND
10.0
11/04/22 16:19
Diphenyl ether (Phenyl ether)
ug/L
ND
10.0
11/04/22 16:19
2,4,6-Tribromophenol (S)
%
42
10-144
11/04/22 16:19
2-Fluorobiphenyl (S)
%
47
10-130
11/04/22 16:19
2-Fluorophenol(S)
%
22
10-130
11/04/22 16:19
Nitrobenzene-d5 (S)
%
73
10-144
11/04/22 16:19
Phenol-d6 (S)
%
33
10-130
11/04/22 16:19
Terphenyl-d14 (S)
%
118
34-163
11/04/22 16:19
LABORATORY CONTROL SAMPLE:
Parameter
3825114
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 45.9 92
31-130
Diphenyl ether (Phenyl ether)
ug/L
50 45.0 90
25-130
2,4,6-Tribromophenol (S)
%
104
10-144
2-Fluorobiphenyl (S)
%
92
10-130
2-Fluorophenol(S)
%
63
10-130
Nitrobenzene-d5 (S)
%
82
10-144
Phenol-d6 (S)
%
51
10-130
Terphenyl-d14(S)
%
118
34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3825115 3825116
Parameter
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
MS
92634614007
Spike
Units Result
Conc.
ug/L ND
83.3
ug/L ND
83.3
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD
83.3
37.6
38.5
45
46
17-130 2
83.3
38.3
39.6
46
48
16-130 3
38
18
10-144
43
44
10-130
15
8
10-130 SO
50
52
10-144
25
17
10-130
106
92
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 50 of 65

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QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734641 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
METHOD BLANK: 3823420 Matrix: Water
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/03/22 14:42
LABORATORY CONTROL SAMPLE: 3823421
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 50.4 101 80-120
LABORATORY CONTROL SAMPLE: 3823422
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 51.4 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823423 3823424
MS MSD
92634407002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 105 50 50 159 160 108 112 80-120 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823425 3823426
MS MSD
92634422001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 213 50 50 283 274 141 123 80-120 3 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 51 of 65

leAnalyiical
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816 Durst Avenue East
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[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734515 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
METHOD BLANK: 3822975 Matrix: Water
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 11/03/22 01:12
Nitrogen, Nitrite mg/L ND 0.040 11/03/22 01:12
LABORATORY CONTROL SAMPLE: 3822976
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110
Nitrogen, Nitrite mg/L 1 1.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3822977
3822978
MS
MSD
92634154001 Spike
Spike MS
MSD MS
MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec
% Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
19.3 1.5
1.5 20.8
20.8 103
103 90-110 0
Nitrogen, Nitrite
mg/L
0.32 1
1 1.2
1.2 88
87 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3822979
3822980
MS
MSD
92634190012 Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.2
1.1 78 76 90-110 2
Nitrogen, Nitrite
mg/L
ND 1
1 0.89
0.90 86 87 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 52 of 65

leAnalyiical
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816 Durst Avenue East
Greenwood, SC 29649
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QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734527 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
METHOD BLANK: 3823009 Matrix: Water
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 11/03/22 03:30
LABORATORY CONTROL SAMPLE & LCSD: 3823010 3823011
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Orthophosphate as P mg/L 0.25 0.24 0.25 97 100 90-110 3 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 53 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 734611 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
METHOD BLANK: 3823275 Matrix: Water
Associated Lab Samples: 92634190005, 92634190006, 92634190007, 92634190008, 92634190009, 92634190010, 92634190011,
92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 1.0 11/03/2217:51
LABORATORY CONTROL SAMPLE: 3823276
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 50 49.4 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823277 3823278
MS MSD
92634131001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 41.9 50 50 93.1 93.1 102 102 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823279 3823280
MS MSD
92634190009 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 5.4 50 50 55.7 55.5 101 100 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 735190 Analysis Method: EPA 9060A
QC Batch Method: EPA 9060A Analysis Description: 9060 TOC, AVL
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634190009, 92634190010, 92634190011, 92634190012
METHOD BLANK: 3826497
Matrix:
Water
Associated Lab Samples: 92634190009, 92634190010, 92634190011, 92634190012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mean Total Organic Carbon
mg/L
ND
1.0
11/06/22 12:45
Total Organic Carbon
mg/L
ND
1.0
11/06/22 12:45
Total Organic Carbon
mg/L
ND
1.0
11/06/22 12:45
Total Organic Carbon
mg/L
ND
1.0
11/06/22 12:45
Total Organic Carbon
mg/L
ND
1.0
11/06/22 12:45
LABORATORY CONTROL SAMPLE:
3826498
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Mean Total Organic Carbon
mg/L
25
24.2
97
75-125
Total Organic Carbon
mg/L
25
24.7
99
75-125
Total Organic Carbon
mg/L
25
23.6
95
75-125
Total Organic Carbon
mg/L
25
24.1
97
75-125
Total Organic Carbon
mg/L
25
24.4
98
75-125
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3826499
3826500
MS
MSD
92634823004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Mean Total Organic Carbon
mg/L
ND
25
25
25.0
24.6
96
94
75-125
2
Total Organic Carbon
mg/L
1.3
25
25
25.3
24.7
96
94
75-125
2
Total Organic Carbon
mg/L
ND
25
25
25.1
24.2
98
95
75-125
3
Total Organic Carbon
mg/L
1.5
25
25
25.0
24.8
94
93
75-125
1
Total Organic Carbon
mg/L
ND
25
25
24.8
24.5
97
95
75-125
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3826501
3826502
MS
MSD
92634449006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Mean Total Organic Carbon
mg/L
19.6
25
25
46.7
46.8
108
109
75-125
0
Total Organic Carbon
mg/L
19.7
25
25
47.5
48.0
111
113
75-125
1
Total Organic Carbon
mg/L
19.6
25
25
46.6
46.8
108
109
75-125
1
Total Organic Carbon
mg/L
19.4
25
25
45.9
46.0
106
106
75-125
0
Total Organic Carbon
mg/L
19.5
25
25
46.8
46.4
109
107
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 753563 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92634190011, 92634190012
METHOD BLANK: 2418439 Matrix: Water
Associated Lab Samples: 92634190011, 92634190012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Acetic Acid mg/L ND 0.50 11/08/2217:19
LABORATORY CONTROL SAMPLE & LCSD: 2418440 2418441
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 1.9 1.9 94 93 70-130 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 753656 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92634190010
METHOD BLANK: 2418900
Associated Lab Samples: 92634190010
Parameter Units
Acetic Acid mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 11 /17/22 16:51
LABORATORY CONTROL SAMPLE & LCSD: 2418901 2418902
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 1.8 1.9 90 94 70-130 4 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 57 of 65

leAnalyiical
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
QC Batch: 754318 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92634190009
METHOD BLANK: 2422714
Associated Lab Samples: 92634190009
Parameter Units
Acetic Acid mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 11/18/2211:09
LABORATORY CONTROL SAMPLE & LCSD: 2422715 2422716
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 1.9 1.8 95 89 70-130 6 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /23/2022 05:59 PM without the written consent of Pace Analytical Services, LLC.
Page 58 of 65

Pace Analytical Services, LLC
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QUALIFIERS
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
BO Analyte was detected in an associated blank at a concentration greater than the MDL.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
SO Surrogate recovery outside laboratory control limits.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NRLF Celanase November 2022
92634190
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92634190001
SW-7-110122
EPA 8015 Alcohol -Glycol
704834
92634190002
SW-5-110122
EPA 8015 Alcohol -Glycol
704834
92634190003
SW-3-110122
EPA 8015 Alcohol -Glycol
704834
92634190004
SW-8-110122
EPA 8015 Alcohol -Glycol
704834
92634190009
B-23A-110122
EPA 8015 Alcohol -Glycol
704834
92634190010
B-23B-110122
EPA 8015 Alcohol -Glycol
704834
92634190014
B-17C-110122 H2
AM20GAX
753313
92634190015
B-23A-110122 H2
AM20GAX
753313
92634190016
B-17B-110122 H2
AM20GAX
753313
92634190017
B-23B-110122 H2
AM20GAX
753313
92634190009
B-23A-110122
RSK-175
753612
92634190010
B-23B-110122
RSK-175
753612
92634190011
B-17C-110122
RSK-175
753612
92634190012
B-17B-110122
RSK-175
753612
92634190009
B-23A-110122
RSK-175
754009
92634190010
B-23B-110122
RSK-175
754009
92634190011
B-17C-110122
RSK-175
754009
92634190012
B-17B-110122
RSK-175
754009
92634190001
SW-7-110122
EPA 3510C
734946
EPA 8270E
735064
92634190002
SW-5-110122
EPA 3510C
734946
EPA 8270E
735064
92634190003
SW-3-110122
EPA 3510C
734946
EPA 8270E
735064
92634190004
SW-8-110122
EPA 3510C
734946
EPA 8270E
735064
92634190005
B-24A-110122
EPA 3510C
734946
EPA 8270E
735064
92634190006
B-24B-110122
EPA 3510C
734946
EPA 8270E
735064
92634190007
B-12-110122
EPA 3510C
734946
EPA 8270E
735064
92634190009
B-23A-110122
EPA 3510C
734946
EPA 8270E
735064
92634190010
B-23B-110122
EPA 3510C
734946
EPA 8270E
735064
92634190011
B-17C-110122
EPA 3510C
734946
EPA 8270E
735064
92634190012
B-17B-110122
EPA 3510C
734946
EPA 8270E
735064
92634190005
B-24A-110122
EPA 8260D
735208
92634190006
B-24B-110122
EPA 8260D
735208
92634190009
B-23A-110122
EPA 8260D
735406
92634190010
B-23B-110122
EPA 8260D
735406
92634190013
Trip Blank-01-110122
EPA 8260D
735208
92634190001
SW-7-110122
EPA 8260D Mod.
734466
92634190002
SW-5-110122
EPA 8260D Mod.
734466
92634190003
SW-3-110122
EPA 8260D Mod.
734715
92634190004
SW-8-110122
EPA 8260D Mod.
734466
92634190005
B-24A-110122
EPA 8260D Mod.
734466
92634190006
B-24B-110122
EPA 8260D Mod.
734466
92634190007
B-12-110122
EPA 8260D Mod.
734466
92634190008
B-21 B-110122
EPA 8260D Mod.
734466
92634190009
B-23A-110122
EPA 8260D Mod.
734464
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /23/2022 05:59
PM
without the written consent of Pace Analytical Services, LLC.
Page 60 of 65

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Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF Celanase November 2022
Pace Project No.: 92634190
Lab ID Sample ID QC Batch Method QC Batch
92634190010
B-23B-110122
EPA 8260D Mod.
734464
92634190011
B-17C-110122
EPA 8260D Mod.
734464
92634190012
B-17B-110122
EPA 8260D Mod.
734931
92634190005
B-24A-110122
SM 2320B-2011
734641
92634190006
B-24B-110122
SM 2320B-2011
734641
92634190007
B-12-110122
SM 2320B-2011
734641
92634190008
B-21B-110122
SM 2320B-2011
734641
92634190009
B-23A-110122
SM 2320B-2011
734641
92634190010
B-23B-110122
SM 2320B-2011
734641
92634190011
B-17C-110122
SM 2320B-2011
734641
92634190012
B-17B-110122
SM 2320B-2011
734641
92634190005
B-24A-110122
EPA 353.2 Rev 2.0 1993
734515
92634190006
B-24B-110122
EPA 353.2 Rev 2.0 1993
734515
92634190007
B-12-110122
EPA 353.2 Rev 2.0 1993
734515
92634190008
B-21 B-110122
EPA 353.2 Rev 2.0 1993
734515
92634190009
B-23A-110122
EPA 353.2 Rev 2.0 1993
734515
92634190010
B-23B-110122
EPA 353.2 Rev 2.0 1993
734515
92634190011
B-17C-110122
EPA 353.2 Rev 2.0 1993
734515
92634190012
B-17B-110122
EPA 353.2 Rev 2.0 1993
734515
92634190005
B-24A-110122
SM 4500-P E-2011
734527
92634190006
B-24B-110122
SM 4500-P E-2011
734527
92634190007
B-12-110122
SM 4500-P E-2011
734527
92634190008
B-21B-110122
SM 4500-P E-2011
734527
92634190009
B-23A-110122
SM 4500-P E-2011
734527
92634190010
B-23B-110122
SM 4500-P E-2011
734527
92634190011
B-17C-110122
SM 4500-P E-2011
734527
92634190012
B-17B-110122
SM 4500-P E-2011
734527
92634190005
B-24A-110122
EPA 9056A
734611
92634190006
B-24B-110122
EPA 9056A
734611
92634190007
B-12-110122
EPA 9056A
734611
92634190008
B-21B-110122
EPA 9056A
734611
92634190009
B-23A-110122
EPA 9056A
734611
92634190010
B-23B-110122
EPA 9056A
734611
92634190011
B-17C-110122
EPA 9056A
734611
92634190012
B-17B-110122
EPA 9056A
734611
92634190009
B-23A-110122
EPA 9060A
735190
92634190010
B-23B-110122
EPA 9060A
735190
92634190011
B-17C-110122
EPA 9060A
735190
92634190012
B-17B-110122
EPA 9060A
735190
92634190009
B-23A-110122
AM23G
754318
92634190010
B-23B-110122
AM23G
753656
92634190011
B-17C-110122
AM23G
753563
92634190012
B-17B-110122
AM23G
753563
Date: 11/23/2022 05:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 61 of 65

r
rdl,'l� .�arr,titC %junamon upon Receipt
Effective Date. 05/121202205/12/2022
Laboratory receiving samples;
Asheville ❑ Eden❑ Greenwood
❑ Nuniersville V Raleigh[] Me"
SampleClient Name -
Upon Receipt
W041: 926341 9rr,er«,iilp�
Project #:lf ff fj f f
El Commercial ❑FPace ed Ex ❑UPS ❑LISPS Client
❑ ❑Other: 92634;1.80
Custody Seal Present? Dyes
p Seals Intact? �
Dyes �lNo
Packing Material: ❑Bubble Wrap-E[Bubbte Ba s
B ❑None _,ET' Other
Thermometer:
❑ IR Gun ID: a) k-4 r-
�c��v Type
of lee: XJ Net ❑ [clue
Cooler Temp;
Z :� Correction Factor:
Add/Subtract (°C) — (j
Cooler Temp Corrected; Zc Z -3
USDA Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone within the United States; CA, NY, or SC
(check maps)? []yes ❑No
Chain of Custody Present?
Samples Arrived within Hold Time?
Yes
❑No
❑N/a
Short Hold Time Analysis 1,72ltr.]?
es
❑No
❑N/1
Rush Turn Around Time Requested?
es
❑No
❑N/!
❑Yes
ON.
❑N/p
5uffieient Volume?
c,.,f�
Correct Containers Used?
_IYes
�
❑No
❑N/A
-Pace Containers Used?
ores
s
❑No
❑No
❑N/A
❑N/A
Containers Intact?
Dissolved analysis: Samples Fietd Filtered?
❑yes
o
NIA
Sample Labels Match COC?
❑Yes
❑No
/A
Yes
❑No
❑N/A
udes Date/Time/1D/Anatysls Matrix:
/
A-,
ace in VOA Vials j>5-6mm]?
E
Present?❑N/A
s
❑Nonk
Yes
❑No
[IN/A
nk Custody Seals Present?
015CREPANCY
L1a'6s
ONO
❑N/A
7COMM4EN/SAMPLE
�'�
S-/IRS
CLIENT NOTIFICATION/RESOLUTION
{
c
Date/Initials Person Examining Content
sl
Biological Tissue Frozen? r! Z 4 2 Z
Des ❑No,,E_N/A
[]None
Ternpshould be above freezing to 6°C
❑Samples Out of temp criteria. Samples on ice, cooling process
has begun
Did sampfes originate from a foreign source (internationally,
including Hawaii and Puerto Rico)? ❑yes ❑No
Lot ID of split containers:
Field Data Required? ❑Yes ❑No
F_VN—_. _
Person contacted:
Date/Time:
Project Manager SCURF Review:
Date:
-1'F9js ck MattagerSAF Review.
Date: - -
Qualtrax ID: 69614
Page 1 of 2 Page 62 of 65

r uvv
Effective Date: 05/121202205/12/2022
"Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, coliform, TOC, Oil and Grease, wto/8ols (water) oDC, Wig
*"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project wo# + 92'6341'90
PM: NlIG Due Date: 11/11/22
CLIEN'r: 97—CNA
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PH Adjustment Log for Preserved Samples
Sample iD Type of preservative pH upon receipt Date preservation adjusted Time preservation Amount of preservative
adjusted added
NoterWlrerr Wtlr TT4 a discrepancy aT ec Ong vrt Caiolina coniF
Out of hold, incorrect preservative, out of temp, incorrect containers,
a
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Lot N
a copy of this form will be sent to the Nortl+Carolina QENR Ceftificaliun Office ii.e.
2
Qualtrax ID: 69614 Page 2 of 2
Page 63 of 65

Effectivo Date: 05/12/202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and Project #
within the acceptance range for preservation samples.
Exceptlonv VOA, coliform, TOC, Oil and Grease, DR018015 {water} DOC, LLHg
**Bottom half of box is to list number of bottles
***Check ail unpreserved Nitrates for chlorine —
1
2
3
4
5
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11
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PH Adjustment Log for Preserved Sa ples
Sample 1D Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of preservative
adjusted added
tdot2rWtretTtn�th-erLefs a clfscrcpancy aaffectingNorth Cifolina con3f
Out of hold, incorrect preservative, out of temp, incorrect containers.
Lot N
a Copy of this Form will be sent to the North Carolina DENR Certification Office (i.e.
Qualtrax 1D: 69614
Page 2 of 2 Page 64 of 65

N
TEMP in C
Received an Ice
(YIN)
Custody Sealed
Cooler
(YIN)
samples intact
(YIN)
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Z)
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5AMPLE TEMP AT COLLECTION
j
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Page 65 of 65

AECOM AECOM 412.395.8888 tel
Gulf Tower 412.297.5000 fax
707 Grant Street
Fifth Floor
Pittsburgh, PA 15219
Data Assessment Memorandum
To Jing Zhou — AECOM Atlanta Page 1 of 5
CC
Subject Level 2 Data Validation for Needmore Road Landfill
From Gregory A. Malzone — AECOM Pittsburgh
Date August 9, 2022
Limited validation of the analytical data for the water samples was performed on one data package
received from Pace Analytical Services, Inc. in Greenwood, South Carolina. The samples were
collected on May 16, 2022, at the Needmore Road Landfill in North Carolina.
The data were reviewed for conformance to method specifications and the project guidance
document: Supplemental Characterization and Long -Term Monitoring (AECOM, July 2010 Revision
2). Data qualifiers were applied in accordance with the validation criteria set forth in USEPA
Contract Laboratory Program (CLP) National Functional Guidelines for Organic Superfund Methods
Data Review EPA-540-R-20-005, November 2020 and USEPA National Functional Guidelines for
Inorganic Superfund Methods Data Review, EPA-542-R-20-006, November 2020, as they apply to
the analytical methods employed.
Field duplicate relative percent difference (RPD) review and applicable control limits were taken
from the USEPA Region I Laboratory Data Validation Functional Guidelines for Evaluating Organics
Analyses, December 1996 and USEPA Region I Laboratory Data Validation Functional Guidelines
for Evaluating Inorganics Analyses, June 1988.
The following methods were requested on the chain -of -custody (CoC) records:
• Method 8260D — Volatiles by Gas Chromatography/Mass Spectrometry (GC/MS).
• Method 8260D SIM — Volatiles by GUMS in Selected Ion Monitoring (SIM) Mode.
• Method SW 8270E — Semivolatiles (Biphenyl and Diphenyl Ether) by GUMS.
• Method SW 8015M — Ethylene Glycol by GC.
• Method EPA 353.2 Rev 2.0 1993 — Nitrate and Nitrite.
• Method SM 4500-P E-2011- Orthophosphate.
• Method SW 9056A — Sulfate by Ion Chromatography (IC).
• Method SM 2320B E-21-23 — Alkalinity.

AECOM
2
The alkalinity analyses were subcontracted to Con -Test, 39 Spruce Street, East Longmeadow, MA
01028.
Review Elements
Sample data were reviewed for the following quality control (QC) parameters:
• Agreement of analyses conducted with CoC requests.
• Holding times and sample preservation.
• GC/MS hardware tunes, initial and continuing calibrations.
• Method preparation blanks/trip blanks.
• Surrogate recoveries.
• Laboratory control sample (LCS) recoveries.
• Matrix spike/matrix spike duplicate (MS/MSD) recoveries.
• Field duplicate precision results.
Samples
Environmental Field Management (EFM) personnel collected the following water samples from the
Needmore Landfill in North Carolina, as reported under the Pace Analytical Services, Inc. job
number:
92604755
Lab ID
Sample ID
Lab ID
Sample ID
92604755001
B-01-051622
92604755007
B-23A-051622
92604755002
B-09C-051622
92604755008
B-2313-051622
92604755003
B-10-051622
92604755009
B-24A-051622
92604755004
B-12-051622
92604755010
SW-5-051622
92604755005
B-17C-051622
92604755011
CSW-1-051622
92604755006
B-2213-051622
92604755012
B-99-051622
Analytical Results
In general, the data results are valid as reported and may be used for decision making purposes.
Sample data were qualified with "UX (The analyte was analyzed for but was not detected. The
reported quantitation limit is approximated and may be inaccurate or imprecise). See Table 1.
DISCUSSION
Agreement of Analyses Conducted with Chain -of -Custody (COC) Requests
Sample reports were checked to verify agreement with the CoC request. No discrepancies were
noted.
Holding Times and Sample Preservation
All samples were analyzed within the holding times required by the methods.

AECOM
All the coolers were received within the optimal range of 4±2 degrees Celsius (°C).
All the samples were properly preserved as specified by the methods.
GC/MS Tunes, Initial and Continuing Calibrations
GC/MS tuning and calibration summaries were not submitted for validation in this Level II data
package.
Method Preparation Blanks/Trip Blanks
No analytes were detected at concentrations exceeding the reporting limits for the method
preparation blanks. No trip blank was submitted for this round of volatile organic samples.
Surrogate Recoveries
The surrogate recoveries were acceptable for all organic analyses.
Laboratory Control Sample (LCS) Recoveries
LCS recoveries for all the analyses were within the quality control limits.
Matrix Spike/Matrix Spike Duplicate (MS/MSD) Recoveries
MS/MSDs that were performed on non -project samples were not evaluated because matrix
similarity to project samples could not be assumed.
The MS/MSD recoveries on client samples were all within the advisory limits with the following
exception:
Method SM 4500-P E-2011: The B-10-051622 MS orthophosphate recovery was less than the lower
advisory limit, but greater than 30%. The RPD between the B-10-051622 MS and MSD was greater
than the maximum advisory limit. The orthophosphate result for sample B-10-051622 was non -
detect and was qualified "UJ," as possibly biased low and imprecise due to matrix effects.
Field Duplicate Precision Results
A field duplicate was collected on sample B-10-051622. See Table 2 for the calculated relative
percent differences (RPDs) for all compounds for which there were detections. The RPDs between
the original and field duplicate was all within the advisory limits of 0-30%. Field sampling/laboratory
precision and sample homogeneity were acceptable. No data qualifications were required.

AECOM
Table 1
Qualified Analytical Data
Lab
Lab
Validated
Validation
Reason
Sample ID
Method
Analyte
Result
Qual
Result
Qualifier)
Units
Codes2
13-10-051622
SM4500-P-E
Orthophosphate
0.050
U
0.050
UJ
m /L
MS, RPD
': USEPA-defined data validation qualifiers applied in this data evaluation:
UJ: The analyte was analyzed for but was not detected. The reported quantitation limit is approximated and may be inaccurate or
imprecise.
Z: Reason Codes:
MS: The matrix spike recovery was less than the lower advisory limit, but greater than 30%.
RPD: The relative percent difference between the matrix spike and matrix spike duplicate recoveries was greater than the maximum
advisory limit.

AECOM
Table 2
Field Precision
Method
Compound
B-10-051622
B-99-051622
Units
% RPD
2320B
Alkalinity
460
430
m /L
6.7
8270E
Biphenyl
53.9
49.6
/L
8.3
8270E
Di hen I ether
559
469
/L
17
8260D
1,4-Dioxane
164
145
Ng/L
12
Notes:
% RPD: Relative percent difference between the original sample result and the sample duplicate result.

AECOM AECOM 412.395.8888 tel
Gulf Tower 412.297.5000 fax
707 Grant Street
Fifth Floor
Pittsburgh, PA 15219
Data Assessment Memorandum
To Jing Zhou — AECOM Atlanta Page 1 of 5
CC
Subject Level 2 Data Validation for Needmore Road Landfill
From Robert Davis — AECOM
Date April 17, 2023
Limited validation of the analytical data for the water samples was performed on two data packages
received from Pace Analytical Services, Inc. in Greenwood, South Carolina. The samples were
collected on November 1-2, 2022, at the Needmore Road Landfill in North Carolina.
The data were reviewed for conformance to method specifications and the project guidance
document: Supplemental Characterization and Long -Term Monitoring (AECOM, July 2010 Revision
2). Data qualifiers were applied in accordance with the validation criteria set forth in USEPA
Contract Laboratory Program (CLP) National Functional Guidelines for Organic Superfund Methods
Data Review EPA-540-R-20-005, November 2020 and USEPA National Functional Guidelines for
Inorganic Superfund Methods Data Review, EPA-542-R-20-006, November 2020, as they apply to
the analytical methods employed.
Field duplicate relative percent difference (RPD) review and applicable control limits were taken
from the USEPA Region I Laboratory Data Validation Functional Guidelines for Evaluating Organics
Analyses, December 1996 and USEPA Region I Laboratory Data Validation Functional Guidelines
for Evaluating Inorganics Analyses, June 1988.
The following methods were requested on the chain -of -custody (CoC) records:
• Method 8260D — Volatiles by Gas Chromatography/Mass Spectrometry (GC/MS).
• Method 8260D SIM — Volatiles by GUMS in Selected Ion Monitoring (SIM) Mode.
• Method SW 8270E — Semi-volatiles (Biphenyl and Diphenyl Ether) by GUMS.
• Method SW 8015M — Ethylene Glycol by GC.
• Method RSK-175- Dissolved Gases by GUMS.
• Method EPA 353.2 Rev 2.0 1993 — Nitrate and Nitrite.
• Method SM 4500-P E-2011- Orthophosphate.
• Method SW 9056A — Sulfate by Ion Chromatography (IC).
• Method SM 2320B-2011 —Alkalinity.

AECOM
2
• Method 9060A — Total Organic Carbon.
• Method AM23G — Volatile Fatty Acids.
• Method AM20GAX — Hydrogen.
Review Elements
Sample data were reviewed for the following quality control (QC) parameters:
• Agreement of analyses conducted with CoC requests.
• Holding times and sample preservation.
• GC/MS hardware tunes, initial and continuing calibrations.
• Method preparation blanks/trip blanks.
• Surrogate recoveries.
• Laboratory control sample (LCS) recoveries.
• Matrix spike/matrix spike duplicate (MS/MSD) recoveries.
• Field duplicate precision results.
Samples
Environmental Field Management (EFM) personnel collected the following water samples from the
Needmore Landfill in North Carolina, as reported under the Pace Analytical Services, Inc. job
number:
92634190
Lab ID
Sample ID
Lab ID
Sample ID
92634190001
SW-7-110122
92634190010
B-23B-110122
92634190002
SW-5-110122
92634190011
B-17C-110122
92634190003
SW-3-110122
92634190012
B-1713-110122
92634190004
SW-8-110122
92634190013
Trip Blank-01-110122
92634190005
B-24A-110122
92634190014
B-17C-110122 H2
92634190006
B-24B-110122
92634190015
B-23AC-110122 H2
92634190007
B-12-110122
92634190016
B-17B-110122 H2
92634190008
B-21B-110122
92634190017
B-23B-110122 H2
92634190009
B-23A-110122
92634449
Lab ID
Sample ID
Lab ID
Sample ID
92634449001
Trip Blank-02-110122
92634449008
B-99C-110222
92634449002
B-22A-110222
92634449009
B-22A-110222 H2
92634449003
B-22B-110222
92634449010
B-22B-110222 H2
92634449004
B-32B-110222
92634449011
B-32B-110222 H2
92634449005
B-01-110222
92634449012
B-01-110222 H2
92634449006
B-10-110222
92634449013
B-10-110222 H2
92634449007
B-09C-110222

AECOM
Analytical Results
In general, the data results are valid as reported and may be used for decision making purposes.
Sample data were qualified with "UX (The analyte was analyzed for but was not detected. The
reported quantitation limit is approximated and may be inaccurate or imprecise). See Table 1.
DISCUSSION
Agreement of Analyses Conducted with Chain -of -Custody (COC) Requests
Sample reports were checked to verify agreement with the CoC request. No discrepancies were
noted.
Holding Times and Sample Preservation
All samples were analyzed within the holding times required by the methods.
All the coolers were received within the optimal range of 4±2 degrees Celsius (°C).
All the samples were properly preserved as specified by the methods.
GUMS Tunes, Initial and Continuing Calibrations
GC/MS tuning and calibration summaries were not submitted for validation in this Level II data
package.
Method Preparation Blanks/Trip Blanks
No analytes were detected at concentrations exceeding the reporting limits for the method
preparation blanks or trip blanks.
Surrogate Recoveries
The surrogate recoveries were acceptable for all organic analyses.
Laboratory Control Sample (LCS) Recoveries
LCS recoveries for all the analyses were within the quality control limits.
Matrix Spike/Matrix Spike Duplicate (MS/MSD) Recoveries
MS/MSDs that were performed on non -project samples were not evaluated because matrix
similarity to project samples could not be assumed.
The MS/MSD recoveries on client samples were all within the advisory limits with the following
exceptions:
Method EPA 353.2 Rev.02 1993: The B-1713-110122 MS/MSD nitrate and nitrite recoveries were
outside the quality control limits. The nitrate and nitrite results for sample B-1713-110122 and were
qualified. See Table 1.

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Method 8260D: The B-99C-110222 (Duplicate of B-09C-110222) MS carbon disulfide and
cyclohexane recoveries were outside the quality control limits. The carbon disulfide and
cyclohexane results for samples B-09C-110222 and B-99C-110222 were qualified. See Table 1.
Method 8260D: The B-99C-110222 MS/MSD acetone recoveries were outside the quality control
limits. The spike amount was less than 25 % of the sample concentration; therefore, data
qualification was not required.
Field Duplicate Precision Results
A field duplicate was collected on sample B-09C-110222. See Table 2 for the calculated relative
percent differences (RPDs) for all compounds for which there were detections. The RPDs between
the original and field duplicate was all within the advisory limits of 0-30%. Field sampling/laboratory
precision and sample homogeneity were acceptable. No data qualifications were required.
Table 1
Qualified Analytical Data
Sample ID
Method
Analyte
Lab
Result
Lab
Qual
Validated
Result
Validation
Qualifier'
Units
Reason
Codes2
B-1713-110122
353.2
Nitrate
ND
0.40
UJ
mg/L
MS
B-1713-110122
353.2
Nitrite
ND
0.040
UJ
mg/L
MS
B-09C-110222
8260D
Carbon Disulfide
ND
20
UJ
p /L
MS
B-09C-110222
8260D
Cyclohexane
ND
10
UJ
p /L
MS
B-99C-110222
8260D
Carbon Disulfide
ND
20
UJ
p /L
MS
B-99C-110222
8260D
Cyclohexane
ND
10
UJ
p /L
MS
': USEPA-defined data validation qualifiers applied in this data evaluation:
UJ: The analyte was analyzed for but was not detected. The reported quantitation limit is approximated and may be inaccurate or
imprecise.
2: Reason Codes:
MS: The matrix spike recovery was less than the lower advisory limit.

AECOM
Table 2
Field Precision
Method
Compound
B-09C-110222
B-99C-110222
Units
% RPD
8260D
Acetone
3470
3430
N /L
1.2
8260D
2-Butanone
652
644
/L
1.2
8260D
cis- 1,2-Dichloroethene
10.8
11.2
/L
3.6
8260D
MIBK
94.2
90.0
/L
4.6
8260D SIM
1,4-Dioxane
935
909
Ng/L
2.8
Notes:
% RPD: Relative percent difference between the original sample result and the sample duplicate result.

Corrective Action Evaluation Report
Project Number: 60683034
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