NCD980602163_20010608_Warren County PCB Landfill_SERB C_Semiannual Sampling Analysis (TSCA) - 2001-OCR

North Carolina
Department of Environment and Natural Resources
Division of Waste Management
Michael F. Easley, Governor
William G. Ross Jr., Secretary
William L. Meyer, Director
Mr. Craig Brown
Pesticides and Toxic Substances Branch
US Environmental Protection Agency
Atlanta Federal Center
61 Forsyth Street
Atlanta, GA 30303-8960
Dear Mr. Brown:
June 8, 2001
«~~ __ .,;
n n an'-.... ---• MCDEMR
I received a correction to the analytical results of the semiannual monitoring of the Warren County
PCB Landfill. The sample of the influent to the leachate treatment system had been reported as <0.0003
ppm PCBs. The corrected result is 0.0003 ppm PCBs. I have attached an updated table of the sampling
results for your records.
In there are any questions or comments, please call me at [phone] e"-1. 308.
Copy: Mr. Bill Meyer
Mr. Mike Kelly
Mr. Larry Rose
Mr. Harry Zinn
Warren County CAB
Sincerely,
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.eru.state.nc.us
AN EQUAL OPPORTUNITY \ AFFIRMATIVE ACTION EMPLOYER -50% RECYCLED / 10% POST CONSUMER PAPER
--· __ _.. -
Ground Water
1
1A
2
3A
5(deep)
7(shallow)
11
12
Surface Water
RCUS
RCDS
UTUS
UTDS
Sediment
RCUS
RCDS
UTUS
UTDS
Leachate
Influent
Effluent
SEMIANNUAL SAMPLING RESULTS
Warren County, NC PCB Landfill
PCBs
loom)
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.10
<0.10
<0.10
<0.10
0.0003
<0.0001
30-Apr-01
Specific
Conductance
pH (umhos)
6.08 107
6.48 137
6.13 90
6.40 99
6.03 91
5.95 75
5.84 54
5.98 129
7.30 91
7.36 103
7.34 110
7.02 77
6.89 1080
6.76 957
RCUS -Richneck Creek Up Stream
RCDS -Richneck Creek Down Stream
UTUS -Unnamed Tributary Up Stream
UTDS -Unnamed Tributary Down Stream
PMB 06/08/2001
N.C. DEPARTMENT OF HEALTH AND HUMAN SERVICES ST ATE LABO RA TORY OF PUBLIC HEAL TH P.O.BOX 28047, RALEIGH, N.C. 27611 GAS-LIQUID CHROMATOGRAPHY REPORT SHEET ~ JUN 7 "/\,\ I -._,.,"/ PROJECT: Warren Co. PCB Landfill DATE OF ANALYSIS: 05/02-14/01 I SjJ_PERF .. LJND SECTION --PPM mg/L) SAMPLE# Sample Type Aroclor 1260 Aroclor 1016 Other Peaks 012357 (1) <0.0001 <0.0001 012358 (1) <0.0001 <0.0001 012359 (1) <0.0001 <0.0001 012360 (1) <0.0001 <0.0001 012361 j, (1) <0.0001 <0.0001 012362 (1) <0.0001 <0.0001 012363 (1) <0,0001 <0.0001 ll 012364 (I) <0.0001 <0.0001 A" 012365 (2) <0.0001 <0.0001 JJ V 012366 (2) <0.0001 <0.0001 J & p 012367 (2) <0.0001 <0.0001 l ,r" \ 1Y 012368 (1) <0.0001 <0.0001 __ /l&{ ~V', ~,, V 'dl> 012369 Effluent <0.0001 <0.0001 C-p' V 1Plv (Y n 012370 Influent <0.0001 <0~ ------. ~'61 ~ --. -, .... -I •• r • ,_.,. ,. n .... , .... 1. ..... , '"" ...... 1/ • . . . . ,. . ?I • ~ ,n . 0,003 C:\My Documents\Reports\012357.DOC
SAMPLE# 012357 012358 012359 012360 012361 012362 012363 012364 012365 012366 012367 012368 012369 012370 N.C. DEPARTMENT OF HEALTH AND HUMAN SERVICES STATE LABORATORY OF PUBLIC HEALTH P.O.BOX 28047, RALEIGH, N.C. 27611 GAS-LIQUID CHROMATOGRAPHY REPORT SHEET PROJECT: Warren Co. PCB Landfill DATE OF ANALYSIS:_.........,.05 ___ /0 ___ 2 __ -1 __ 4 ___ /0 ___ 1 ______ _ PPM1 mg/L) Sample Type Aroclor 1260 Aroclor 1016 Other Peaks (I) <0.0001 <0.0001 (I) <0.0001 <0.000~ (I) <0.0001 <0.0001 (1) <0.0001 <0.0001 (1) <0.0001 <0.0001 (I) <0.0001 <0.0001 (1) <0.0001 <0.0001 11 (I) <0.0001 <0.0001 (2) <0.0001 <0.0001 (2) <0.0001 <0.0001 (2) <0.0001 <0.0001 (1) <0.0001 <0.0001 Effluent <0.0001 <0.0001 Influent <0.0001 0.0030 '1,_I -Comments: Sample Type: (1) Ground Water (2) Surface Water (3) Soil (4) Sediment JJ Large unidentified peak present. J.t Large Sulfur peak present. Liquid-liquid extraction, analyses by packed and capillary gas-liquid chromatography using electron capture detector. C:\My Documents\Reports\012357.doc
North Carolina
Department of Environment and Natural Resources
Division of Waste Management
Michael F. Easley, Governor
William G. Ross Jr., Secretaay
William L. Meyer, Director
Mr. Craig Brown
Pesticides and Toxic Substances Branch
US Environmental Protection Agency
Atlanta Federal Center
61 Forsyth Street
Atlanta, GA 30303-8960
Dear Mr. Brown:
June 5, 2001
Attached is a table containing the results of the semiannual monitoring of the Warren County PCB
Landfill. The sampling event was conducted on April 30. As in the past no PCBs were found in
groundwater, surface water, leachate effluent or sediment samples collected.
As I indicated in my letter of May 29, initial site preparation for tl1e detoxification and
redevelopment project is starting. Most of the monitoring wells used in our semiannual monitoring events
will be abandoned for the project. That is scheduled for next week. The electrical service to the landfill
will also be upgraded in the near future. Power will not be available to operate the leachate pumping
system for about two months. The system was shut down last week and the water level inside the landfill
was approximately 3-4 feet above the bottom.
Our detoxification contractor, IT Corporation, is preparing and submitting the final designs and
plans for approval. I will be using some of these plans to prepare the request by the state to remediate the
landfill following 40CFR 761.6l(a) as you indicated would be necessary at our meeting in Raleigh in April.
I expect to begin preparing that request shortly.
In there are any questions or comments about the sampling event or any activities associated with
the detoxification efforts and project schedule, please call me at [phone] ext. 308.
Copy: . Bffi Meyer
Mr. Mike Kelly
Mr. Larry Rose
Mr. Harry Zinn
Warren County CAB
Sincerely,
Patricia M. Backus, PE
PCB Landfill Project Manager
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.enr.state.nc.us
AN EQUAL OPPORTUNITY\ AFFIRMATIVE ACTION EMPLOYER-50% RECYCLED/ 10% POST CONSUMER PAPER
Ground Water
1
1A
2
3A
5(deep)
?(shallow)
11
12
Surface Water
RCUS
RCDS
UTUS
UTDS
Sediment
RCUS
RCDS
UTUS
UTDS
Leachate
Influent
Effluent
SEMIANNUAL SAMPLING RESULTS
Warren County, NC PCB Landfill
PCBs
(ppm)
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.0001
<0.10
<0.10
<0.10
<0.10
<0.0003
<0.0001
30-Apr-01
Specific
Conductance
pH (umhos'
6.08 107
6.48 137
6.13 90
6.40 99
6.03 91
5.95 75
5.84 54
5.98 129
7.30 91
7.36 103
7.34 110
7.02 77
6.89 1080
6.76 957
RCUS -Richneck Creek Up Stream
RCDS -Richneck Creek Down Stream
UTUS -Unnamed Tributary Up Stream
UTDS -Unnamed Tributary Down Stream
PMS 06/05/2001
" NC~OL;unmcnl of i.nvironment,
Hco',ILri, & 1-i.wral Re.,;ources
Solid Wutc Muugement Division
SA?v1PLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, Nonh CArolina 27611-3047
Site Number _______________ SamplcID Number/Name ____ •:L_/_3--6~( __________ _
CoilectedBy 4 L, ~~ ID# ---'----'------------------
~J ,._ f...(J. G.11.J G ..111,1iYDate Co llect.ed_i..i....__-~~=-0_· _-_u=·_t _______ Time / '-' ._ r "7
Agency: Hazardous Waste z l) l V ' '., l D\J
Sample Type
E nvironment.al Concentrate
Ground Water (1)
Surface Water (2)
Soil (3)
.,,,-Solid (5)
Liquid (6)
Sludge (7)
_ v Other (4) Other (8)
Solid Waste Superfund
Comments
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
le.c'ld
mercury
selenium
silver
Results (m g/1)
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter ResuH.s(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2 ,4-D
2,4,5-TP(Silvex)
chlordane
hept.acblor
hexachlorobenz.ene -------
hexachlorobutadiene
enJrin
lin&i1e '.~ ,~ -~ ..
mctha.xychl~r
to.xaohene: p c~,R ,1· , .·
-------
FOR LAB USE ONLY
Date Recei~ed .tffi~/-O~ ~f)
. tf)r,e {.A1 g"o .
Date· Firracted ;:;;--,-7-0/1/P
. . -. irPce <-M..~ .
Date Anaj:z
Date Rep. :MAY 2 2 2001
Lab N~~b~r 012J7i
DH·S 3191-(Revised 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalli ir.n
vanadium
zinc
pH
conductivity ______ _
TDS
fl.µh point.--·-~-----
caroon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
I , 4-dichlorobe:uene
1,2-dichloroethane
1,1-dichloroethylene ______ _
2,4-dichloroetbylene ______ _
hept.achlor
hex:acWorobenzene
hex:achlorobutadiene
..,_ hex:achloroethane
methyl ethyl ketone
nitrobenzene
pe:it.achlorophenol
pyridine
tetracWoroethylene
tricbloroethy Jene
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lind.ane
methoxychlor
tox:aphene
2,4-D
2,4,5-TP (Sil vex)
:., ' ...
t
'
" NC .oc•p•nmcnt of Environment,
Hc.iillh, & N•rural Ruourccs
Solid Wutc Marugement Division
SAJ.viPLE Ai~AL YSIS REQlTEST SL.stc ubomory of Public Hc..allh
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North C,rotina 27611-8047
Site Number SampldD NumbedName .:i., I ~ b L -------------___ _,.._ _____ __:_ ___ ~--
Collected By __ H-'---_L-'--',----'-:,_,:::_:vvc..=-______ ID# -------
SiteLoc:i.tion l.JPrAA-CN itll'/ Time IO·. ·z.....o W l'c (.(Ui. N G ,..1 ,viYDate Co !lected_'-/...L·_-___,,b:.....:D:_-......:(:.::.)~-1-::_-::_-::_-::_-::_-::_-::_-::_-::_-::_-::_--=.. ________ ___,
Agency: Hazardous Waste z \J l V 1 ) I o~J
Sample Type
Environment.al
Ground Water (1)
Surface Water (2)
Soil (3)
Concentrate
/ Solid (5)
Liquid (6)
Sludge (7)
~ Ot.he1 (~1 Other (8)
Solid Waste Supe:iu.nd
Comments
VT tJ _'J
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Ac:d: BIN Ext.
Results (mg/I) Parameter ResulLs(mg/l)(mg/kg)
2,4-D
2, 4,5-TP(Silvex)
chlordane
hep t.a-::hlor
hexachlorobenzent -------
bexachloro bu tad i ene -------enurin
li..nGille '• ., .. -,·
·· rnctha.x.ychl~-.
toxaphene" ,. , Pe-£ l,
FOR LAB USE ONLY
Date Received ~'---<-----":..L_---(P .
Date· Ei rracted
===--~'--::--="":T"':=±,,,-......--
' ·-· ' .
Date· .A.n q,]yz.ed ,---"!!'<-_..,.'---,-=_{_.fU:,__ __
Date Rip_urted -.-'-'--------~
Lab Nu~b~r 012372
OHS 3 1 9 [. (R evised 12/93)
an timony
arseruc
barium
beryllium
cadmium
chloride
chromium
cobal t
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallitr.:II
vanadium
zinc
pH
conductivity ______ _
TDS
fl.µh point.·--'-'------
.. ....-, ... .., .. --~. -. -:-:-·: ----. ---' :·
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Organic Compounds
benzene
carbon tetrachlorice
chlordane
chloroben.zene
chloroform
o-creso!
JI-cresol
p-creso!
creso!
1,4-dichlorobe::uene
1,2-dichloroethane
Results(mg/l)
Resul ts (mg/!)
1, 1-dichloroethyl ene ______ _
2, 4-dichloroethy lene
bept.ach..lor
hexachl o ro benzene
hexachlorobutadieoe
... hexachloroethane
methyl ethyl ketone
nitroben.z.eoe
pentacWorophenol
pyridi.r.e
tetrachloroethyleoe
trichloroethyleoe
-------
-------
2, 4,5-trichloropheno l ______ _
2, 4, 6-tricWorophenol
vinyl chloride
endrin
lindane·
methoxycWor
toxaphene
2,4-D
2,4,5-TP (Sil vex)
-------
., NC Defanment of Environment,
Hullh, & N·•wral Resourc es
Solid Wu~ Muugemenl Division
SAMPLE Al~ALYSIS REQUEST St.ate Laboratory of Public He.alth
P.O. Box 28047, 306 N. Wil~ngton St.
Raleigh, Nonh Ciro!im 2761 ]-8047
Site Number _______________ Sample ID Number/Name __ :2. __ ,_·'?>_(._3~-----------
0:illected By 4 L. i ~ 1v ID ti -----'-----'------------------
SiteLocition W1t-ftflCN TT>N LJ ,.)fJUi.i\J G ..l.i,,,iYDat..eCollect.ed_j_,____-_:_...::...1_0_-..c:c0_· I ______ Tirne r1 --~~
Agency : Hazardous W asr.e z l) l I.I ' ') I o\J
Sample Type
Environmental Concentrate
Ground Water (1) _!( Solid (5)
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
~ Other (4) Other (8)
Organic Chemistry
Solid Wa.sr.e Superfund
Comments
Ac. VJ s~J1~-\
Inorganic Chemistry
Parameter
P&T:GC/MS
Ac:d:B/N Ext.
Results (mg/I) Parameter Resul:..S(mg!l)(mg/kg)
2,4-D
2,4,5-TP(Silvex)
chlordane
hept.a~hlor
hexachlorobenzene -------
bexachlorobut.adiene -------
enJrin
lindc.ne '• ,, ,~ .-,
·· rndho.xychl6,r-
toxaphene· 1l'· ,_.. pc...B
FOR LAB USE ONLY
Date Received ~-,-✓-0/-i/P
-. ()Juss (~Yo?f).. -
Date' F i rracted Sc:7-0l1/r'
_.·· .•:~s;£fi(s'O?Q.J-
. Date Anq,]y:z,ed -~ Y.-0/ y'P
Date R6~o.i-ted ----'-'---------
G b Nu~b~r 012373
DH-S 31.91-(Revised 12/93)
anti mony
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalliir.n
vanadium
ZlnC
pH
conductivity ______ _
TDS
fl~h point ------'-'------
.... ··-·· ........... ·-~--. --··•--.-.·
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Organic Compounds
benzene
carbon tetrachlorice
chlordane
chloroben.zene
chJoroform
o-cresol
rr::-cresol
p--cresol
cresol
I, 4-dichlorobem.ene
1,2--dichloroethane
1, 1-dichloroethylene
2, 4-dichloroetby lene
bept.achJor
bexachlorobenzene
bexachlorobutz.diene
..,_ hexachloroethane
methyl ethyl ketone
nitrobenzene
pentachlorophenol
pyridine
tetrachloroethylene
trichloroethy lene
Results(mg/1)
Results(mg/1)
-------
-------
-------
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
---vinyl chloride
endrin.
lindane·
methoxychlor
toxaphene ---· ·
2,4-D
2,4,5-TP. (Sil vex)
\ NC Dqartmcnt of Environment,
Hc:lllh, & N°,wral Rewurccs
• Solid Wutc Muugemem Division
SANIPLE Al'l"ALYSIS REQUEST St.ate Laboratory of Public Hc.ailh
P.O. Bo:x: 28047, 306 N. Wilmington St.
Raleigh, North c~rolina 27611-8047
Site Number SampldD Number/Name P-.. f ~ '-Y -------------------~~----......__ ________ _
CollectedBy 4 L, ~Iv ID# __ ..:._ _ _;_-'-----------------
SiteLoCJ.tion u!1tt1-.1U£N n:>r,J W 11:-(.~ /.i.v.J G ...1 l\li'fDate Co!lected_'j..L..·_:.....-=b'-D_-_(=)_I _______ Time __ J_1-_:_~_o __ _
Agency: Hazardous Waste
/ l) l \/ l ";) I 0\J
Sample Type
Environmental Concentrate
Ground Water (1) ✓ Solid (5)
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
~ Ot.her (4) Other (8)
Organic Chemistry
Solid W ast.e Superfund
Comments ..
R,c..()S S~e J c .:._ ""t
Inorganic Chemistry
TCLP Compounds
Inorganic CompoW1ds
arsemc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter Resul:..S(mg/l)(mg/kg) Organic CompoW1ds Results(mg/1)
2,4-D
2, 4,5-TP(S ilvex)
chlordane
hept.achlor
hexachloroben.zeoe -------
bex.achlorobut.adiene
enJri.n
li.ni:Lme
·· rncthc:.-ychlq.r .
toxaphcne: ' Pc..11 ,1-
-------
FOR LAB USE ONLY
Date Recei~ed · . 5]--J -0/
. (?r~~ (ll( .
Date· Firrad .
.,..-='::-:::;;.--"-~c-r.:5-~<-;,-,,---:
Date Rep_o.rted -~--------
G b N~~b~r 0 12374
DH-S 3191 (Rc,;iscd 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobaJt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
th all i i.r.:n
vanadium
zinc
pH
conductivity ______ _
TDS
fl~h point.·-·--'-'-----'----
carbon tetrachlorice
chlord.ane
chJoroben.zene
chloroform
o-cresol
rr.-cresol
p-cresol
cresol
1,4-dichlorobe:izeoe
1,2-dichloroethane
1,1 -dichJoroethylene ______ _
2, 4-dichloroetbylene
hept.achlor
bexachlorobenzene
bex.achlorobut.adiene
.,_ hex.achl oroethaoe
methyl ethyl ketone
nitrobenzene
pent.achlorophenol
pyridi.ne
tetrachloroethy leoe
tri chJ oroethyleoe
-------
-------
2,4,5-tricWoropheool ______ _
2,4,6-trichlorophenol ______ _
vinyl chl.oride
endrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP. (Sil vex)
\ NC Dcpanmc~( of Environment,
Haith, & Nuual Ruources
Solid Wur..c Marugement Division
SAl\.1PLE ANALYSIS REQUEST St.ate Laboratory of Public Hc.ai(h
P.O. Box :28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
Site Number Sample ID Number/Name )__, \ ~ ',) -----------------------"'--->-<'----------,----
Collected By __ 4...:.....__L__,_,_~c...·c...yv _________ m # ______ _
Si teLoc.1tion uJ P,iJ-/LC N \ON Time / 2 :_ 0 ..:::, w !':(.RG.N G ../,viYDateCollecte.d Lr-7:; [) -o l -~--~--~===============----------~
Agency: Hazardous Waste z C) l V l :, I D\J
Sample Type
Environmenl:11 Concentrate
Ground Water (1) _/'solid (5)
Surface Water (2) Liquid (6)
'-'/ Soil (3) Sludge (7)
_ Other (4) Other (8)
Organic Chemistry
Solid Wa.ste __ Supe:-fund
Comments
~ B '
9l>~> :l ht c~+-t-~,hJ
Inorganic Chemistry
TCLP Compounds
Inorganic CompoW1ds
arsen.ic
barium
cadmium
chromium
lead
mercury
selen.iurn
silver
Results (m g/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter ResulLs(mg/l)(mg/kg) Organic CompoW1ds Result.s(mg/1)
2,4-D
2, 4 ,5-TP(Silvex)
chlordane
bept.acWor
hexachlorobeo..z.ene -------
bexachlorobutadiene
enunn
linda.ne '• ,,•.-,
· methnxychlq.~-.
toxaph0ne ·
J.~' 1 .. Pc.-R
FOR LAB USE ONLY
Date Received . · -5":~ /-Q/ ., .
Date· Firract
•.--,
Date · An<l,lyzed ~-?-<0/
R~port~:By · · ~~--'-------
Date_ R~ioi-ted -· --'-'--------~
La:b Nu~ber 012375
OHS 3 l.91 (Revised 12/.93)
antimony _______ ben.z.ene
arseruc
barium
beryllium
cacim.ium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
s1.1! fa tes
thalli u-;n
vanadium
zinc
pH
conductivity ______ _
TDS
fl~h point_._·_~-----
c:i..rbon tetracblorice
crJord.ane
cWorobeo..z.ene
chloroform
o-cresol
rr:-cesol
p-cresol
cresoi
1, 4-ciichloroben.zene
1,2-dichloroethane
1,1-dichloroethylene ______ _
2,4-dichloroetbylene ______ _
heptachlor
hexachlorobenzene
hexachlorobutz.diene
"' heuchloroethane
methyl ethyl ketone
nitrobe0.2ene
pentachlorophenol
pyridine
tetracWoroethy I ene
trichloroethy lene
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lindane
methoxychl_?r _ f
~x~hene · i
~::~~-TP. (Sil vex) ,.~;, · ~ ,-
'--------':-------.:-~· · ~.~-"1 t~: ----,,ti
-. ~'.-:;:;.;:;•:;~
r
I '
I
I t--
~ NC Elqianment of Environment,
Huith, & N~wral Rewurces
• Solid WutL Man.agement Division
SAlvIPLE Al~AL YSIS REQUEST State ubomory of Public Health
P.O. Box 28047, 306 N. Wilmin~on St.
Raleigh, Nonh Carolina 27611-8047
Site Number Sample ID Number/Name •:Z.., ( 3 .b C... -------------------~~"--------------
Collected By __ 4_-,__L___:.i_:,c....c, J.v ________ rn # _____ _
SiteLoc.1tion L<lP.~/\l Tb r-1 W ;...~fl_6..t<J G ..1,viYDateCollected L(-":;; D -O I -~--~--~===============----------~
Agency: Hazardous W a.s t.e z \J t V , ) I o~J
Sample Type
F'nvironmental Concentrate
Ground Water (1) V Solid (5)
Surface Water (2) Liquid (6)
_ti Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Solid Waste Suoe:-fund --.
Comments
)_
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
se!en.ium
silver
Results(mg/1)
Parameter
P&T:GC!MS
Acid:B/N Ext.
Results (mg/1) Parameter R esuli.s(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2, 4,5-TP(Silvex)
chlordane
hept.a-:::hlor
hexachlorobe:u.ene -------
bexachlorobutadiene -------endrin
li.ndz.rie ',~ ~,
· methe:xychl~~-
toxaphone·
1~-' I •• pc.11
FOR LAB USE ONLY
Dat~ Red:i~ed S-/-6/.
Date· E"irracted -,,,al!E'::---:-:. ......... --:-""'7'C......,.-1-JL,,.,,--
. Date An~ yzed ,-,;~-L..,.-_::_L-...L.L __ _
R~port~;By · · ~~~-'-------
Date Rep_urted ---'-'---------
012376
DH·S 3191 (RcYised 12/93)
·--,. -.·.•
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
f1uoride
iron
lead
manganese _______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalli Lr.II
vanadium
zmc
pH
conductivity _______ _
TDS
fl~h point.·-·--'-'------
c:u-bon tetracWoric!e
chlordane
chlorobenz.ene
chloroform
o-cresol
m-cresol
_, p-cresol
cresol
1,4-dichlorobe::u.ene
1,2-dichloroethane
1,1 -dichloroethylene ______ _
2, 4-dichloroetbylene
beptachlor
hexacbJorobenz.ene
bexachlo robut.adiene
... hexacbJoroethane
methyl ethyl ketone
nitrobe!l2ene
pentacWorophenol
pyridine
tetracb.loroethy Je ne
tri::bJoroethylene
-------
-------
2,4,5-trichlorophenol ______ _
2, 4, 6-trichlorophenol
vinyl cWoride
endrin
lindane·
methoxychlor
toxaphene
2,4-D
2,4,5-TI (Sil vex)
-------
:::,!.:_-. , ;,, ~ ~-------;-------;,---:----...J.......---------------==-===~ J J
----·· '3:l! ~ ... ,,.~:-::~·-~~
' 1·•·1
NC DqiAnment of Environment,
Hd1lh, & N~wral Re.sources
Solid Wu~ Muugemcnt Divi,ion
SAIYIPLE AJ.~ALYSIS REQUEST St..atc Laboratory of Public Health
P.O. Box 18047, 306 N. Wilmington St.
Ralei1:h, North Cuolina 27611-8047
SitcNumber SampldD_Number/Name !l.{ }(1o'] ----------------_______ _,__ __________ _
Colle.ctedBy 4 L, ;__,yV ID# ----'-----'-~----------------
SiteLoC3.tioa ulP.AA€N. rnr1 W /'c"rzR G.N G ..1 ,,,ii'{Date Coll~ted_j-"-·_.:.........:::1_D_--'(=-) _I ______ Time l '2.. : { o
Agency: Hazardous Waste
✓ f) l V , '., I o\J
Sample Type
Fnvironment.al Concentrate
Ground Water (1) ~-Solid (5)
Surface Water (2) Liquid (6)
✓ Soil (3) Sludge (7)
_ Othei" ('11 Other (8)
Organic Chemistry
Solid Waste Superfund
Comments
R F.,
if):.. cs ;-b l't
Inorgartic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium.
lead
mercury
selenium
silver
Results (mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/l) Parameter Result.s(mg/l)(mg/kg) Organic Compounds Results(mg/l)
2,4-D
2,4,5-TP(Silvex)
chlordane
bept.ac:Wor
hexachloroben.zene -------
bexachlorobut.ad iene -------
enJrin
lindz.ne •. ',· -.
·· methc:.xychlq.~-
toxaphene ,. Pc.R 1-
Date Rep_orted -----------
0 12377
OHS JI 9 I (Revised 12/93)
antimony _______ benzene
s.rseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
f1uoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalliir.n
vanadium
ZlJ1C
pH
conductivity ______ _
ms
flq,5h point __ '-'-------
c:irbon tetracblorice
chlordane
chloroben.ze::ie
chloroform
o-cresol
rr:.-cresol
p-cresol
c~esol
I, 4-dichJorobeazene ______ _
1,2-dichJoroethane
1, 1-dichloroethylene ______ _
2, 4-dichloroetbylene
bept.achlor
bexachlorobenzene
bexachlo robut.adiene
..,_ hexachloroethane
methyl ethyl ketone
nilrobenzene
pent.achlorophenol
pyridine
tetrachloroethylene
trichJoroethy lene
-------
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl cW_oride
endrin
lindane ·
melhoxychlor
toxapheoe
2,4-D
2,4,5-TP (Silvex) .-·.:J..:.
NC Dc:-panmem of Environment,
HC::.lth, & N.a.iral Re.sources
Solid Wute Mall.lgemcnt Divi,ion
SAivfPLE Ai~AL YSIS REQUEST State uboratory of Public Health
P.O. Box :23047, 306 N. Wilmington St.
Raleigh, North Carolina 276! 1-8047
Sit.c Number ________________ Sample ID Number/Name ___ :Z.,:.-=_(-'.)-'--1..---=-~----~-------
Site Loc:.ation u.! P:-ft8£ N T:O r-1
Agency: Hazardous W a.ste
✓ C) l lll ') I 0\J
Sample Type
Environmental Concentrate
Ground Water (1) V Solid (5)
Surface Water (2) Liquid (6)
~ Soil (3) Sludge (7)
_ Other (4) Other (8)
Organic Chemistry
Coll~ted By __ 4--'--_l..__,_, .,..,:..::.· .:....:"'-'=--------ID# -------
Solid Waste __ Supe:11.lild
Commenls
R ~
9~ S;, i~~
Inorganic Chemistry
Time / 7..,: IL
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silvei
Results(mg/1)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (m g/!) Parameter Resul:.s(mg/l)(mg/kg) Organic Compounds Resul ts(mg/1)
2,4-D
2, 4 ,5-TP(Si !vex.)
chlordane
bepta::hlor
hexachlorobenz.em: -------
hexachlorobut.adiene -------
enJrio
li.n~1e ,,·:-,·
·· mt:tho.x.ychl~r-.
toxaphene: ,. ✓ ___._P_c..~Ec:____•-~,---,..
FOR LAB USE ONLY
DateRep.uited -:-----'---------
· 012378
DH·S 3 19 J. (Revised l 2/93)
antimony
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalli~
vanadium
ZUlC
pH
conductivity ______ _
TDS
fl~h point _._·--'-'-------
benzene
ca.roan tetracWoric!e
chlordane
chlorobenzene
chloroform
o-cresol
~-cresol
p-cresol
cresol
1,4-dic:1.lorobe:uene
1,2-dichloroethane
-------
1,1-dichloroe:hyleoe ______ _
2, 4-d ichloroetb ylene
beptachlor
hexachlorobeoz.coe
bexachlorobutzdieoe
... hexachloroethane
metbyl ethyl kerone
nitrobeuzene
pentachlorophenol
pyridLne
tetrachloroethyleoe
trichloroethyleoe
-------
-------
2,4,5-trichlorophenol ______ _
2, 4, 6-tricWorophenol
vinyl chloride
endrio.
lind.ane
methoxycWor
toxaphene -· ·
2,4-D
2,4,5-TP (Silvex)
-------
NC 0C1)artment of Environment,
Hullh, & Nao.ial Re,;ources
Solid Wane Man.agement Div ision
SAlvfPLE ANALYSIS REQUEST St.ate Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
R•leii:h, North C>.roli.na 27611-8047
Site Number _______________ SamplcID Number/Name ____ 'll,,~IL...£2>L· _,,t,'-l\-+-----------
Collected By __ 4~L~i..:..~::..cl"-'=--------ID# _____ _
SiteLoc:Hion uJP.-~~ Tb r.f Time f b ~-( b W 11--(.,u.:.w G .,1 JViYDat.e Coll~ted_'-f-'-·-:.....-=-b_D_-....o:l)~· =' ===========---------.:_,
Agency: Hazardous W a.ste
✓ l) l V ' ') i D\J
Sample Type
Solid Waste Supe:-fu.nd
Environment.al Concentrate Comments
Ground Water (1)
Surface Water (2)
~Soil (3)
Liquid (6)
Sl udge (7)
_ Other (4) Utner (8)
Organic Chemistry Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
sele::i.iurn
silver
Results(mg/l)
Parameter
P&T:GC/MS
Acid:B/N Ext.
R esults (mg/I) Parameter Result.s (mg/l)(mg/k.g) Organic Compounds R esults(mg/l)
2,4-D
2, 4 ,5-TP(Silvex)
chlordane
bq it.a:::hlo r
hexachlorobenze:::i e -------
bex.achlorobut.adiene
enu.n.n
li.n&.11e
· metho.xychlq.~-.
toxapheoe· ,'.. , . pc..R ,_
-------
FOR LAB USE ONLY
Date Recei~ed . 5'-J-('J/j//>
. Pc,e-, (,#yo?'"~
Date· F;Hrac:ed /, S.; ~-0 tY,:>
.. -.. f>Cl3 .,.. u.1 r r1 ?i.2r
Date. An .!,lyz.ed ¥ 7-0(--i,P
Report~:By , ~~--------
Pate. Rtp.o.rted -:--------~-
Lab Nu~b~r 012379
DH5 ) 191-(Revised 12/93)
antimony _______ benzene
arseruc
barium
ber;llium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sul fates
th all i Lr.II
vanadium
ZJ.nC
pH
conductivity _______ _
TDS
fl~h point -----'-'------
c:irbon tetracWoride
chlorciane
chJo rooen.zene
chloroform
o-cesol
II!-Ciesol
p~resol
cresoi
1,4-dich.l o robe:uene
1,2-dicWo roethane
1, 1-dichJoroethylene ______ _
2,4-dic hlo roetbyl ene ______ _
bept.achlor
bexacbJ orobenzene
bexac hlorobutadiene
... hexac hloroethane
methy l ethyl ketone
nitroben.zene
pent.achlorophenol
pyridine
tetrachloroeth y I ene
trichJoroethylene
-------
2,4,5-trichJorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin.
linclane ·
methoxychlor __
toxaphenc=
2,4-D
2,4,5-TP (Sil vex)
i;
NC BcpM,mcnt of Environment,
Hl.•llh, &. Na~r•l Re.sources
Solid Wute M1n,gement Division
SA1v1PLE ANALYSIS REQUEST Slate ubomory of Public He.ailh
P.O. Box 28047, 306 N. Wilmington St.
Ralei1;h, North c~rolim 276 I 1-8047
Site Number Sample ID Numbc:-/Name "9,..., { ~ 1 I) ------------------~--------------
Coll wed By 4 ? , .,,., J.v ID# ---'---'--'------------------
W .. R._(Ui';.J G ..111,1iYDat.eCollect.ed_1J....·_:_...::..b_D_-...:;:oc_l ______ Time t 2--: / f
Agency: Hazardous Waste
/ ij l v • ') i o~,j
Sample Type
Environment.ai Conce:itrate
Ground Water (1) ✓ Solid (5)
Surface Water (2) Liquid (6)
V Soil (3) Sludge (7)
-Other ( 4) Other (8)
Organic Chemistry
Solid Waste Supe:iund
Comments
Q~
P .. -z., :-i ¼,
Inorgan.ic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
le.ad
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter ResulLs(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2, 4 ,5-TP(Silvex)
chlordane
bepta(:hlor
hexachlorobeuz.e::ie -------bexachlorobutad iene -------
enJrin
linili.J1e -. ,,·.
· mdha:x.ychlq,r.
toxaphene· 1;' \_" pc.11
FOR LAB USE ONLY
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
si lver
sulfates
thalliu-:rr
vanadium
ZlnC
pH
conductivity ______ _
TDS
fl~h point ___ ·_~-----
carbon tetrachloride
chlordane
chlorobenz.ene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-ciichlorobe:uene
!, 2-dichloroethane -------
I, J-dichloroethylene ______ _
2,4-d ichloroetbylene ______ _
hepc.achlor
hexachl o robenzene
hexachlorobut.adiene -------
-.. hexacbloroethane
--·
methy l ethyl ketone
nitrobeo.zene
pent.achlorophenol
pyridine
tetracbloroethylene
trichloroethylene
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
Lab Nu~b~r 012380
DH·S ;J 19 1-(Revised 12/93)
lindane·
methoxychlor _
toxaphene
2,4-D
2,4,5-TP. (Sil vex)
--.... l··C< ,-.<0;.r.'~·u ~ , -
.• .. '"'
~ .::::·---~~~:x:f·
NC Dqanmem of Environment,
Hulth, & Nuural Re.sources
Solid Wute Management Divi•ion
SA?v!PLE A.J.'\l"AL YSIS REQUEST Slate laboratory of Public Hes.Ith
P.O. Bo:x: 28047, 306 N. Wilmington St.
R•leigh, North Cu-olin• 27611-8047
Site Number _______________ SamplcID Number/Name----=;)__---'. '--1'"""~..,,__'"1_( ___________ _
O:ille.:::ted By __ 4---'--_L_.,_1 .:...::~_c_~..:_ _______ ID# -------
SiteLoc:ition UP.tZ.IUZN. Tt>N W !'-):, .. r2 {i_ l<J G ..,, l'ViYDate Coil~ted_j..l_:......~1:.....:u=---_..:'::::_)_I ______ Time 12.~ Lo
Agency: Hazardous Wa.st.e
~ fy lli, ~ tow1
Sample Type
Environment.al Concentrate
V Solid (5)
Solid Waste Supe:-fund
Comments
R Q-7 Ground Water (1)
Surface Water (2)
✓ Soil (3)
Liquid (6) ~.:..,),~ ~4.,_ --.\; .,-L..._~
Sludge (7)
_ Other (4) Other (8)
Organic Chemistry Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Result.s(mg/1)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter ResuH.s(mg/l)(mg/kg) Organic Compounds Result.s(mg/1)
2,4-D
2,4,5-TP(Silvex)
chlordane
bept.acblor
hexachlorobenz.eoe -------
bexachlorobut.ad iene
7
enJrin
li..n~1e
· rnetheu.ychlq.r .
toxaohene· pC:.11 ,,· •.·.
-------
FOR LAB USE ONLY
. . . .. ·.
Reported;By · · ~........,..,..,......,~---,,----
Date Re~o.rted ----------~
Lab Nu~b~r 012381
DH.S JI 91 (RcVised 12/93)
antimony _______ beuzene
arseruc
barium
beryllium
cadmium
chJoricie
c::i.romiurn
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
th all i Lr.II
vanadium
ZlllC
pH
conductivity ______ _
TDS
fl~h point -----'-'-__ ........;... __
c:irbon tetrachloride
chlordane
chloroben.zene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1, 4-ciichlorobeo..zeoe
1,2-dichloroethane
1,1-dichloroethylene ______ _
2,4-dichloroetbyleoe ______ _
bept.achlor
bexacblorobeo..zene
bexachloro but.adiene
... hexacbloroethane
methyl ethyl ketone
nitrobeuzene
pent.acWoropbenol
pyridine
letracbloroethylene
trichJoroethylene
-------
2,4,5-trichlorophenol ______ _
2, 4, 6-trichlorophenol ______ _
vinyl chloride
endrin.
Iind.ane ·
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Sil vex)
NC Bcpu,mrnt of Environment,
Hc:.illh, & N,rur•l Ruources
Solid Wute M1n.igement Divi•ion
SA.i\1PLE Al~AL YSIS REQUEST SL.ate Lsbomory of Public He.ailh
P.O. Box :28047, 306 N. Wilmington St.
Raleigh, Nonh c~rolina 276! 1-8047
Site N umber _______________ Sample ID. Number/Name ___ . _j___(_3,~_-,_2.. __________ _
Colle::ted By __ H-'--_L_,,_~.c..c-.-J _______ ID# ____ _
Si teLoc.1tion uJ~i¼-:.C rl fD N W., ZrU'i.i'-i G _,, ,viYDat.e Collect.ed_1~---~~-D_-_· (_)_I _______ Time_~l_1._~_2..--"-) __
Agency: Hazardous W a.st.e Solid Waste Supe:iund TCLP Compounds _z ----lj l t, , ') I ovJ
Sample Type Inorganic Compounds Results(mg/l)
Environment.al Concentrate Comments arseruc -barium
R OJ i -
Ground Water (1) ,._.,....,. Solid (5) cadmium --
chromium -
Surfac:: Water (2) Liquid (6) lead ---
-mercury
_::"'Soil (3) Sludge (7) selenium --
silver ----
-;J:..!:;.;;r (4) -Other (8) -
-
-
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/l) Parameter ResuJi.s(mg/1) (mg/kg) Organic Compounds Results(mg/1)
--P&T:GC/MS antimony ben.Zene --
Acid:B/N Ext. arseruc carbon tetrachloride ---2 ,4-D barium chlordane ---
-2, 4,5-TP(Sil vex) beryJl ium -ch.lorobenz.ene -
chlo rdane cadrni urn chlorofo rm ---
-hep:.acWor chloride o-cresol --hexachlorobenzene chromium m-cresol ----
bexachloro but.adiene cobalt p-cresol --
enJrin copper cresol --li.nifu1e .. fluoride 1,4-d icnlorobenzene ---·· merhaxychlq.r .. --
-iron 1,2-<licnloroethane --
toxaobene lead I, 1-dicn.loroethylene
✓ pC:.11 ,, ,_. --•-
-manganese -2, 4-dichloroetby Jene ---mercury -beptachlor
nickel hex.acWoroben.zene ---
nitrate hex.achlorobut.adiene ----;·,.. , selenium ... hexacWoroethane --.. silver methyl ethyl ketone .--FOR LAB USE ONLY sulfates nitroben..z.ene --
Dat~ Received ·. S--:::-/-0/1/P th all i Lr.II pentachlorophenol --vanadium pyridine --. tp~ s-{ /H3'o;J"OJ . ZlJlC tetrachloroethylene -· ·-Date Firracted S-...,.. 7-0/j?r' -pH -tricWoroethylene
· --, · l?GBsI41Y-o~ ·-conductivity -2,4,5-trichlorophenol
Date· r~a)Y,z,ed . S~9-0/~ TDS 2, 4 ,6-trichlorophenol --
. . .. ·. -f1~h point · -vinyl chloride -
Rcported;By endrin ' .•. -----. -, .. ----.. . -. lindane ..
Date. Rep.ai--ted . --. methoxychlor --.. ·-·
Gb N~~b~r 012382 --tox.aphene
--2,4-D • -J ~ .....
-2,4,5-TP (Silvex.) .•-o-~ -----~-t-_ .;E ;:.,.
DH·S 3191 (Revised 12/93) .~._:;>-~i?~i -~---·y ~~-
c .. "·y;:~"e
NC Oqt•rtmcnt of Environment,
Hc:.ldlh, & Na:ural Rewurces
• Solid WuLe Marugemem Divi,ion
SAlvIPLE ANALYSIS REQUEST State Laborawry of Public Hc.a!lh
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Cirolina 27611-8047
Site Number SampleID Number/Name ::L-I 1,.....-i 3 -------------------~~--<---------~--
Collected By 4 L.. ( ~ ;,-J ID t; ---'----'----'-----------------
SiteLoc.1tion ujP;-f2..f2£N. fbN' w ~(.{<.G.l'./ G .,1,vi'{Dat.eCollected_j..1...·_:..-_::)_D_-_:o=-1 ______ Tirne I)_! <-7
Agency: H azru-dous W a.ste
/ l) L v , ';) I o~J
Sample Type
Environment.al Concen trate
Ground Water (1) V solid (5)
Surface Water (2) Liquid (6)
-~Soil (3) Sludge (7)
_ Other (4) Other (8)
Organic Chemistry
Solid Waste Superfund
Co mments
f{. f5
·P_. '> i'hl.,
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/!) Parameter R esuH.s(mg/I)(mg/kg) Organic Compounds Results(mg/l)
2,4-D
2, 4, 5-TP(S ilvex.)
chlo rdane
bept.acblor
hex.achlorobe::izent -------
hex.achlorobu tadiene -------enJrin
li.n&.ne . ,~ ~.
· methe:.xychlq/
toxaohene: pC:.11 1'.' '
FOR LAB USE ONLY
Date Rep_o.rted --~--------
Lab Nu~ber 012383
OHS 3l91-(Revised 12/93)
antimony _______ benzene
arseruc
bari um
beryllium
cadmium
chloride
chrom.iurn
cobalt
copper
fl uoride
1ron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
th all i u-::n
vanadium
Zll1C
pH
conductivity ______ _
TDS
fl.µh poi.nt_·---"----'---
carbon tetracWoric!e
chlordane
chloroben.zene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobe:uene
1,2-:iichl oroethane -------
1, 1-dichloroethylene ______ _
2, 4-dichloroetbylene
hept.achlor
hexacWoroben.zene
hexachlo ro butadiene
"' hexacWoroethane
methyl ethyl ketone
nitrobeuzene
pent.acWorophenol
py ri dine
tetracbloroethylene
tri cbloroethy lene
-------
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lindane ·
methoxychlor .
toxaphen~
2,4-D
2,4,5-TP (Silvex)
NC Department of Environment,
Hallh, & l'l&wral Ruources
Solid Wute Muugemwt Divi•ion
SA1'v1PLE Al'l"ALYSIS REQUEST St.ate Laboratory of Public Hc.ailh
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
Site Number _______________ SamplcID Number/Name _____ :l,,_. _l__:.)_7_i.f,___ ________ _
SiteLoc.1tion fJJ P.AA-CN TT:>N
Agency: Hazardous W a.stc 7 \J l \/ , ') I o~J
Sample Type
Environment.a l
Ground Water (1)
Surface Water (2)
./ Soil (3)
_ Other (4)
Concentrate
v',,., Solid (5)
Liquid (6)
Sludge (7)
Other (8)
Organic Chemistry
Parameter
P&T:GC/MS
Acid: BIN Ext. -
2,4-D -
-2, 4,5-TP(Silvex)
chlordane -
-bept.a~b.lo r
hexachlorobenzeoe --
bexachlorobutadiene -enurin -lindz.ne ... ,· .-,
_ · rne the:.xychlo/
toxaphene·· , .. , . pc £ ,,
... ·_
Results (mg/I)
Reported~By .... -~--------
Date. Re~o.rted ·--'--·,___ ______ ~_
Lab N~~b~r 01.238.1
DfiS 3191 (Revised 12/93)
Coll~ted By __ 4---'---_Z..___,_,_~:._.:N ________ ID# _____ _
Solid Waste __ Superfund
Comments
Ra lC
Inorganic Chemistry
Parameter Resul Ls(mg/1) (mg/kg)
-an timony
arseruc -
barium -
-beryllium
cadmium -chloride -chromium -cobalt -
-copper
fluoride ---iron -
lead -
-manganese
-mercury
nickel -nitrate --selenium -silver .-sulfates -thalli ir.:n: .. -vanadium -
ZillC ---
-pH
·-conductivity ... TDS -
-fl:µh point .. · ..
-. ·'
-
-. -
-
-----
Time f 2,.: >3
TCLP Compounds
Inorganic Compounds
arse::J.Jc
-
barium
cadmium
chromium
lead
mercury
selenium
silver
Organic Compounds
benzene -carbon tetrachloric!e -
chlordane -chloroben.zene -chloroform -
o-cresol -m-cresol -
-p-cresol
cresol -
1,4-dichlorobeo.zeoe -
1,2-<lichJoroethane -
-1, J-dichloroethylene
-2, 4-dichloroetbyleoe
-bept.achlor
bexacWorobe!lZcne -
bexachlorobut.a.d iene -... hexachloroetbane -
-methyl ethyl ketone
nitrobenz.ene -
-pent.acWorophenol
-pyridine
·-tetrachloroethyleoe
-tri::Woroethyleoe
-· 2, 4 ,5-trichlorophenol
-2, 4, 6-trichlorophenol
-vinyl chloride
endrin -lind.ane · -
methoxychl_o r --.
toxaphene ---
2,4-D -
-2 ,4,5-TP (Sil vex)
Results(mg/l)
Results(mg/1)
-
' . -
.. . ... -.,
.. ·,--·~
_.:;_.;_~:;l
..
1:1 .J .i:
··.,-~-c~
i [ l
I r-·
t f
NC 0-::p,nmcnt of Environment,
HC:.lth , & Nrniral Resources
Solid Wute Muugement Division
SA?v.t:PLE A.l'iAL YSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleii;h, Nonh C,rolina 27611-8047
SitcNumber SampldDNumber/Name ;.t_. ( r, I S"° ----------------------~-~----------
!'lame of Site W f'tf?J'..(/\1 Gvf\JTll ~CB Collected By __ 4-'--_L_,,_· ~-1--J----,----ID It _____ _
Agency: Hazardous W a.ste
✓ {j l V l '.) I 0\J
Sample Type
Solid Wa5te __ Superfund TCLP Compounds
Environ.mental Concentrate
Ground Water (1) ✓ Solid (5)
Surface Water (2) Liquid (6)
JL_ Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Comments
\ I
Inorganic Chemistry
Inorganic Com pounds
arsenic
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter R esulLs(mg/I)(mg/kg) Organic Compounds Results (mg/I)
2 ,4-D
2, 4,5-TP(Silvex)
c:-ilordane
hept.ac:hl or
hexachloroben.z.ene -------
hex.achlorobutadiene
enJ.rin
lindz.ne
· rr:etbe:xychlo,r ..
toxaohene· ' 7 PcB ,1·
-------
FOR LAB USE ONLY
. .
Pate Re~orted ---'-"--------~
Gb N~~b~r 012385
OHS J 191-(Revised 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
f1 uoride
iron
lead
mangan~sc ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallii..r.:n
vanadium
Zll1C
pH
conductivity ______ _
TDS
f!:µh point .. · -~~----
c.J.rb on tetracWoric!e
chlorci.ane
chlorobeC2e::ie
chloroform
o-cesol
IJc-cresol
p-cresol
cresol
1,4-ciichloroben.z.ene
1,2-dicn.loroethane
1, 1-dichJoroethylene ______ _
2,4-dichloroetbyiene ______ _
hepc.achlor
hex.acb.lorobenzcne
bexachlo ro but.a.diene
.,_ hex.acb.loroelhane
methyl ethyl ketone
nitrobeuz.ene
pent.achlorophenol
pyridille
tetrachloroethylene
trichJoroethy lene
-------
·2,4,5-trichlorophenol ______ _
2, 4 ,6-trichloropheno! ______ _
vinyl chl.oride
endrin.
linc:Lme
methoxychlor
toxaphene
2,4-D
2,4,5-TP. (Silvex)
: NC [k--t-f«1menc of Environment,
Hulth, & N,wral Re,;ources
Solid Wu<.c Man.igement Division
SAMPLE A.t'l"AL YSIS REQUEST Sc.ate l...abor,tory of Public He.slth
P.O. Box 28047, 306 N. Wilrningion St.
Raleii;h, Nonh c~roli.na 276 l 1-8047
Site Number ________________ SamplcID Number/Name ------=;t_-=---'-(_J_. _t_'-_· _________ _
Collected By __ 4...!..· _L__,_,_~.:....:...N'-----------ID # ______ _
Site Loc.:i. ti on LJ ;:+-tzf<.£ /\/ ro ,✓ W i'-:~~G.1\/ G _,,l\liYD at.e Collect.ed_'1-'----=-~-.)_-_(_)_I ______ Time \2.:. '] F
Agency: H a.z.a.rd o lL5 W a.s te Solid W a.ste __ Supemmd TCLP Compounds -..z --ti l V' ') jC~J
Sample Type Inorganic Compounds Results(mg/1)
Environment.al Concentrate Comments arseruc -barium -RB Ground Water (1) ✓ Solid (5) \L cadmium ---
{1,,,_ +~ ~ ~-<-h J chromium
P~s ."b~ -
Surface Water (2) Liquid (6) lead ----
-mercury
~Soil (3) Sludge (7) sele:i..ium --silver -
-Other (4) -Other (S) -
-
-
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Resul :.S (mg/I) (mg/kg) Organic Compounds Result.s(mg/l)
P&T:GC/MS antimony benzene ----
Acid:B/N Ext. arseruc carbon tetracWoric!e ---2,4-D barium chlordane ---
-2, 4,5-TP(Silvex) beryllium -chlorobenz.e::ie -chlordane cadmium chloroform ---hept.achlor chloricie o-cresol ---
hexachlorobenz.e::ie chror:a.ium IB-c:esol ----bexachloro but.adiene cobalt p-cresol ---
entirin coppe~ cresol ---luidzne ·, ,,·-. fluoride 1, 4-ciichlorooe:uene ---· rnethc:.xychlq,r-. --1, 2-<lichloroethane iron --toxaphene ' --
,_. lead 1, 1-dicWoroethy[ene
✓ pc...£ 1!' --
-manganese -2,4-dichloroetby !enc ---mercury -beptachlor .. nickel hexachloroben.zene ---n.i trate hexachloro but.adiene ----,, selenium ... hexachloroethane --.. silver methyl ethyl ketone .--FOR LAB USE ONLY sulfates nitrobeo.zene --
Date Received . · S:-, /-0 /-VP thalli tr.JI .. pentachloropbenol --vanadium pyridine
. ,p cE'f ( ('(??if#. --
--zinc ·-telrachloroethy Jene
-pH -trichJo roelhylene Date· Firrac~~ S:~'f--0
. --, ~s(/113"'0'~ ·-conductivity -2, 4,5-trichlorophenol
. Date-~ajyzed_ Si-'/'2-t?/ .. TDS 2,4,6-trichlorophenol --
. --·. -f1~h point · -vinyl chloride -
Rcported:By endrin ' -~ --· ---.• .... -, ,l lindane · -. -Date. Re~o.rted -· methoxychlor ---. -. toxaphene --
Lab Nu~b~r 0 12386 --.. 2,4--D ... ----~~ --· 2,4,5-TP (Sil vex) ·.:-··-::1';.."-:,.
DH·S ] 191 (Revised 12/93) ••.:,., .-,.-=·:-~t
i I i
~ ~1-• ~
-·."':.!-'::~-..:__,, -,.,;-
~ NC DC\")•r.ment of Environment,
Hulth, & N•wr•l Re.sources
Solid Wur..c Muugement Divi•ion
SAM:PLE Ai~AL YSIS REQUEST St.ate L,.boraLOry of Public Hc.alth
P.O. Box 28047, 306 N. Wilming-con St.
Raleigh, Nonh C,rolina 27611-8047
Site Number _______________ Samplc:ID NumbedNa.me _____ 'Q...., __ 1-""Jr'--'"1._r ________ _
Collected By __ 4_-,___L__,_,-'~'--'1-v ________ ID R' _____ _
SiteLoc.:i.tion L<lP.t¼<-C.t\/ \ON W ,._.~/l.G'N G ../,vi'fDateColl~ted_j.,_·_-..c..)_D_--'O'--I ______ Time t 2...-:..'-<t_
Agency: Hazardous Waste Solid Waste --Supe:iu.nd TCLP Compounds
..L. --\j t \I , '.) I o.,J
Sample Type Inorganic Compounds Results(mg/1)
Fnvironmental Concentrate Comments arseruc -
barium -
_:::: Solid (5) R. lB /) Ground Water (1) cadmium --
~ "t,-+ ~ ~ -~-;r;_-f-d
chromium
f},,> .. ~L 7'1 -
Surface Water (2) Liquid (6) lead ---
-mercury
~ Soil (3) Sludge (7) selenium --silver -
-Other (4) -Other (8) -
-
-
Organic Chemistry Inorganic Chemistry -
Parameter Resu1 ts (mg/I) Parameter ResuH.s(mg/l)(mg/k.g) Organic Compounds Results(mg/1)
P&T:GC/MS antimony benzene ----
Acid: BIN Exr. arseruc c:irbon tetrachlor-ide ---2,4-D barium chlorclme ---
-2, 4, 5-TP(Sil vex.) beryllium chlorabenzene --chlordane cadmium chloroform ---
hept.ac:Wor chloride o-cresol ---hexachlorobenzene chromium r::c-c~esol ----
bexach.lc ro bu tad i ene cobalt p-cresol ---
-cnJrin copper cresol --
li.nd.z.ne .. ,,.,4, fluoride 1,4-dichlorobenzene ---· methcxychl~r-. --1,2--<lichloroethane iron ---
toxaohene '. lead 1, 1-dichloroethylene 7 pe-11 ,. --1-
-manganese -2, 4-dichloroetbylene ---mercury -hept.achlor
nickel hexachl o robenz.ene ---nitrate hexachlorobutadiene ---. ---selenium ..,_ hexachloroethane --
silver methyl ethyl ketone .----FOR LAB USE ONLY sulfates nitrabenzene --
Date Received S:,-, / -0 t;_fP thallii.r.n pent.achlorophenol --vanadium pyridine --~~ <A'i-roeo 21DC tetrachloroe!hy l ene
Date· EHract~ S--~ -Qjyp --·-
-pH -tri chl oroethylene
... ; f C8s-(¾1lj ·-conductivity -2, 4 ,5-trichlorophenol
Date· An~yzed ::S-/O--.. TDS 2, 4,6-trichloraphenol --.. fl~h·point_ vinyl cW_oride
R~port6d:BY · · ---
endrin. I
--~-.. ·--.. . -. linda.ne .. -Date_ Re~~ed. -·· methoxychlor ---. toxaphene ·-.. 0 1~.!387 --Lab Nu~ber .. 2,4-D --
2,4,5-TP (Sil vex) ;--.:,{~'~ --· ~ .r-'
DHS 31 91 (Revised 12/93) ·:t(_·~~~ ~
"~ ..-.. NCDEtJNR
t>ivision of Waste Management
□ Superfund Section
□ Hazardous Waste Section
□ Solid Waste Section
Organics Lab: ..,,/'
Inorganics Lab: __
CHAIN OF CUSTODY RECORD
.
Project Name: Ut..,,r,:~ &VV\,~ ()c:8. Sampled By: J..1-2..,,,v'<,....-
Site ID # (NCD#) Sampler ID
Location: W C...,y" r '-"'-' -w,""' NC Telephone:(:Lzjj ""t :3, ·2 ")_~Cl
Address: Date Sampled: '-I-) 0 -Q I
Time Sampled:
Sample Types: Soil v Water ✓ Waste Other
Remarks:
Field Sample ;;i_ 11.> ~I 'Ll1 t;..2... ua,&..? 2...., a~ v u ~~r ')_/'/ (.' :z...,3~,
Numbers :I.>( )b I? 2-T 1,I '< ) • ..f 'S 7t> :z..r 1; 1 2t J 7L l..t/]._i 'J. .J...(~i'f
1..,£)'1.> 'J...,·1 )1' 9J.>-"t2 ~
Relinquished By: 7 ~ \-.::::-Date: q /-o, Time: ~ o<> P~
V ' (Siirnature)
Received By: -P~A,a?a~ Date:5-/-~/ Time: ~/0~
(Signature)
Relinquished By: Date: Time:
(Siimature)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
(Si1mature)
Received By: Date: Time:
(Signature)
Result~ Reporte~ I~~ ~ Dah1AY 2 2 200 ffime:
SU ~ature)
LI
(I:\docshare\cocr.fnn)
SAMPLE# 012371 012372 012373 012374 012375 012376 012377 012378 012379 012380 012381 012382 012383 012384 N.C. DEPARTMENT OF HEALTH AND HUMAN SERVICES STATE LABORATORY OF PUBLIC HEALTH P.O.BOX 280~7, RALEIGH, N.C. 27611 GAS-LIQUID CHROMATOGRAPHY REPORT SHEET PROJECT: Warren Co. PCB Landfill DATE OF ANALYSIS: __ 05_/0_2_-l_l_/0_l ______ _ Sample Type Aroclor 1260 Aroclor 1016 Other Peaks Sample# Sample Type Aroclor 1260 Aroclor 1016 (4) <0.10 <0.10 ll 012385 (3) 0.20 <0.10 (4) <0.10 <0.10 ll 012386 (3) 0.13 <0.10 (4) <0.10 <0.10 012387 (3) <0.10 <0.10 (4) <0.10 <0.10 (3) <0.10 <0.10 (3) <0.10 <0.10 (3) <0.10 <0.10 (3) 0.13 <0.10 (3) 0.90 <0.10 (3) 0.36 <0.10 (3) 0.57 <0.10 (3) 0.34 <0.10 (3) l.93 <0.10 (3) 1.34 <0.10 Other Peaks .. Comments: Sample Type: (1) Ground Water (2) Surface Water (3) Soil (4) Sediment 17 Large Sulfur peak present. (Most soils have a small sulfur peak Present) Sonication extraction, anlayses by packed and capillary gas-chromatography using electron capture detector. C:\My Documents\Reports\012371.DOC ~ . ' 4 •
WELL LOG SHEET
Purge/Sample Team: ('l\(?Ju-.v\,-e_ 0r'=(S ov'.'-: Well#: __ ..__ _____ _
' I( ( Comments ( well construction, etc): _4~{,J~G-~\ '-----IJJ--=ce-_l __,l ~= ..... th:..>.-l.S-"-=-l.tt~·>'-------'-.v=€ff--;-~~-.h:,_l<J_....:~:n_.r_l;..j--"3"-',_1_)-__ w_L_-._Z_._f _g
Purge Information
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2. 0 x height of water column (feet)
For bailers; 4 bails = 1 gallon
1 Well Volume (gal): 5 . 3 3 Well Volumes (gal): ____ Purge Equipment: ~-lA-"c,i:Se1 p-~M--f'
Date Purged: ~ /'3Q } D \ -'-t-1 ~~t+-=-__..._-Purge Time Start: Purge Time End: ~l-=G._: _t!t_o ___ _
Did well purge dry? Y ~ Actual purge voiume: f o . C\
Volume5 ,3 Volume ~'.f '-'olume 11'.C, Volume Volume Volume ---
Temp (°C) 2 I . (/1 ·2:1 .s l o1 .9.)
pH Li) z. I. LJ7 . I l (;; d)</;
S. C. i nio . '1 l 0U:> 3 /01, J-
D. 0. N/A N/ A t0l r\
J
Turbidity coo, 3 -Z.1 9 31.o
Sample Information
Sample Date: '--i /3o I o I
l
Sample Time: ihtf D Sample Equipment: hvul!W5 Pu ,y
Water Condition (turbidity, odor, etc.): WeJl pu,ir~eJ ngf.J-@ I/ 3aJJ1 { IC>.q )_,. vCL-v--
cL, · n'ce. ( 6YLC1. @ L{. ) --S' o.-,m,. c(_
£Z· -r ·· WaJ r ) -s,v,,,l'v. ""1 ~ v , c s l vla CA · +o c v <-~-L.-zp ~ l,t,~J Samples Collected (✓): • •,u ~ ' · ,-TJ-.q
VOCs (2 40 ml vials)
_(_ SVOC~(l 2L Amber bottle)
Metals (1 lL HOPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
Temp(°C): [C,.Y pH: t . .J<{ SC(umhos): / <> 7 . ·2... DO(ppm): __ _ Turb(NTUs): J7 -~.
Comments: ----------------------------------
__________________________________ p,cbwells.fun
WELL LOG SHEET
Purge/Sample Team: _ _.L""-'-' _.f4=-s.._:e-~------------Well#: \ A. _ __.__,.,___.___ _____ _
'-{V,b1 ,
Comments (well construction, etc): _T-'---• .\..-'--'-\-½k½"'--=i''-'---''---'ft:j.JI--L--'-. =· ,._____,Q.""oe"IFf-'-t -=-~-i..,'-'----=~~~~-,._l{_/._i.,_f __ lv_c.,_-::_1_._r_b
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Infonnation For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feec)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): ___ 3 Well Volumes (gal): ____ Purge Equipment: _____ _
Date Purged: _L.....,i +/--=-s'-c..~-:;C--'o=· __.__ I l
Purge Time Start: l .. Z.. · .,_ • .--Purge Time End: l 2. : '-t '.::>--~--~--
Did well purge dry? fl> N Actual purge volume: _____ _
Volume Volume Volume Volume Volume Volume ------
Temp (0 C)
pH
S. C.
D. 0 .
Turbidity
Sample Information
Sarnp le Date: __ '1_-~J_O_-_o~(~_ Sample Time: / k. ! < > Sample Equipment: f>,.,_:z I ,L v-
Water Condition (turbidity, odor, etc.): __ 7:_.,,._✓.=b_, '_J ___________________ _
Samples Collected (✓):
1
VOCs (2 40 ml vials)
SVOCs ~l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(°C): __ _ pH: t:. 'f '£ SC(umhos): I a,
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ Turb(NTUs): __ _
_____________________________________ pcbwells.fnn
WELL LOG SHEET Facility: W,-cn:, ~-4 Pee,
Well#: ~ Purge/Sample Team: lar-sc\r'-e_ '-C'~v--l).(-"ct..:_-\-u Q ---------
Comments (well construction, etc): to+..:! X)'t't(i ½ l . ~ 6 P-u,-v<. l. LJ~ ~ Y. I/ ·"
ev I,,,,..,__,."" tL-t,1 Lt\ IL 1 S-~ v :::. )..,), S-) V ::: <t' i·'.>
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information Fo(£),vell: 3 volumes (gallons) = 2.0 x height of water column (feet)
For hailers: 4 bails = 1 gallon
1 Well Volume (gal): ~. ~ 3 Well Volumes (gal): :) S-Purge Equipment: Qglil-JO~S
Date Purged: i\ r?:,c) r -0 \ Purge Time Start: \\ ·_ '}S Purge Time End: ( : GO
Did well purge dry? (i) N A 1 1 ".)~--, ctua purge vo ume: o _./
( t:5 -3) (//R ,V) (9.0 15) (2s-)
Volume L Volume _Q Volume ~rrS Volume 3 Volume Volume --
Temp (°C) dd · Co J j , 0 J.;)._ ~ J [). 8
pH 5,38 lQ . l 1-· [p . d' "J-lo . I -:S
S. C. 9G?.9 q5 . °1 Oj;:). .·7 Cf'O. d)
D.O. --
Turbidity 4,) 4 ['Q, ';)... \ 1 I •7 S-7R
Sample Information
Sample Date: 4 -3,o ~ 0 ( Sample Time: I .' o O Sample Equipment: _______ _
Water Condition (turbidity, odor, etc.): ----------------------
Samples Collected(✓):
VOCs (2 40 ml vials)
/ SVOC~(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
Temp(° C): :}o-8 pH: (e · L3 SC(umhos): '10 · d_. DO(ppm): __ Turb(NTUs): 5 · 7 8 .
_______________________________ _,pcbwells.fnn
WELL LOG SHEET
Purge/Sample Team: Lor':)c~ic~v-/1)t:c),_+o o , Well#: 'h llJ ~3A ·
Comments (well construction, etc): 1o+c0< D< r-+h, (pS:, 5 ~) ~ +o LL) J::i, 0
)
Purge Inf onnation
Conversion Factors: Fo 2" ell: 3 volumes (gallons) = 0,5 x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
1 Well Volume (gal): y . q
Date Purged: iJ -3,()--o I
Did well purge dry? Y ill)
Volume_/
Temp (0 C) /f6 . -~
pH f:.p,Od'
S. C. 10 3. 5--r}1s
D. 0. )/, d--
Turbidity {1)~,y.,~
For bailers: 4 bails = l gallon
3 Well Volumes (gal): J. \ Purge Equipment: C Rv ,..,!>\-:--C:5
{) _/I u,---,, Purge Time Start: -1 , -~---Purge Time End: { 0; '--{ '?>
Actual purge volume: _ _.,d.,.<--L\ __ _
Volume ,J___ Voi-1med · ~ Volume .3 Volume Volume -
i'l . t.c 11, °l I~ 4-
("_p l 3 ( 0 I 3lv {r) 4 -
99 .4-~c1, ·~ CR 4-
£14 , g 49 .g
} ,2-I ,AS o, s -1 .
Sample Infonnation
-
Sample Date: Ll -30--o I Sample Time: IO : w\'5 Sample Equipment: G.gv-,vDC'O>
Water Condition (turbidity, odor, etc.): -----------------------
Samples Collected (✓):
VOCs (2 40 ml vials)
_LsVOCs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
Temp(°C): l'.:b .j pH: (o ,~ SC(umhos): 9 '1 L\ DO(ppm): _· __ Turb(NTUs): 0. 57:
Comments: --------------------------------
_________________________________ pcbwells.frm
. '.
WELL LOG SHEET
Purge/Sample Team: rY\eJe,:.."'-',,e 22r-~";,o·a t:\.c.-·, t V ·, L--t) 0 Pe ,-Well#: '5" ---=------'
Comments (well construction, etc): """'W_'_t..-_U_O._e.-fp_«_..:::.h_,__( ._,)_lf __ _,_D-";~fF-' rfti:......,l~-~'--'0 ..... ~'-'-'--'-'-'----:,_{, =-' Go._o ___ l.J___,c,"'-· _~ _'.Z..!_,f.f_-7--'C/_
Purge Information
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2. 0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): _y_.· __ 3 Well Volumes (gal): ____ Purge Equipment: G,,1.J. .. ~lyp:,, yhtMp
Date Purged: ½ / ?20 / D\ . I
Purge Time Start: I O : c; ~ Purge Time End: I "2. • i L{
Did well purge dry? Y N Actual purge volume: ____ _
Volume S,_ Volume g_ Volume 112_ Volume lL VolumeL2 Volume ---
\L.:.i-~-
Temp (°C) -z.o -z. i °'.?. 1 Cj ,0 -1ct . t iJ..J5 '-10 C>
pH L,2, ()0\ 7) . "'QC"( \JI. Du -lo .OS 12 .',S" 3 3,c,
s. C. iq . '1 YJ'fi . l 9J½.'7) --Gj l . \ l Z.1'5' ·;--... , 5
D.·o. -
N/A N/A N; A-·~1/ ,'l N/11 l -z..l\ 2'5. "2.
Turbidity 52 .L\ Zt..0 . '5 zo,, 2Y .:J Y u. -3
Sample Date: L\ J 3 o / 0 \
Sample Infonnation
Sample Time: \ 2. ' \ '5 Sample Equipment: ¼c(,A,--t..c-l s=o s p, ""'='-p
Water Condition (turbidity, odor, etc.): ,:L 1 'i..-t«., -f'✓.,-6 .'Je ,s 1 -=-yl.e_
Samples Collected (✓):
VOCs (2 40 ml vials)
.j SVOCs@ (l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(0 C): lvt ,7 pH: L. ~ SC(umhos): f '-I
Comments:
Dioxin (1 IL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ Turb(NTUs): zs. 2.
---------------------------------
,.,.. ;..' 1·'" ., .-
WELL LOG SHEET Facility: _______ _ Location: _______ _
'
Purge/Sample Team: Ve G ±o::::i::-~ LcvSC l1 ,f'( cf Q V::: Well#: / ---'--------
I\/-::.. 2.~ 'L
Conversion Factors: Fo " ell: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feec)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): 2 -2-3 Well Volumes (gal): ~ -J Purge Equipment: (~ cl~cVJ
Date Purged: 4-'¼' ~ 0 l Purge Time Start: 3 '. ;,,.. 8 Purge Time End: -------
Did well purge dry? Y (R -Actual purge volume: ~-'8
(7 2--J (ti 4) (5-SJ ( ~-7) (g . 8')
~
Volume j_ Volume 2... Volume2 ~ Volume 3 Volume-± Volume ----
Temp (°C) I <t · l 'M .o 2.0 ~8 :>o· \ d0 -~
pH S--~Gi 6,'-\~ ~-0 I er u s--. t°) ,s-, 45
S. C. 1c, . \ n.s 71 -7) 70 -7 7<:;.o
D. 0.
Turbidity SD 49 .t.l 38-1 J-0-1-{ 5 .,S-
Sample Information
Sample Date: L\ ---?>o .,--0 \ Sample Time: t'.\ ', O ~ Sample Equipment: 41/J ,u....A,-d-,f-½A
Water Condition (turbidity, odor, etc.): 7' <...,LA~""': c1 ~\.-\ , ~ · 'S"' _____ -->....c;.....,_s-----------------
Samples Collected(✓):
V0Cs (2 40 ml vials)
SV0Cs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
Temp(°C): )o -3 pH: 5 .c)c;-SC(umhos): "l'S .o D0(ppm): __ _ Turb(NTUs): \'S 5
Comments:
---------------------~'-------------pcbweUs.frm
WELL LOG SHEET Location: iJ..,,.rr.e-"" .+ .. , ..
Purge/Sample Team: _ ___,,_\.+'-.._--=-----q-----___,-L_,~,v~w~---------Well#: 1 l --__ __;_ ______ _
Comments (well construction, etc): _:).._'_' _v_<.-_l_l __ "T_ .. _~_~ .,_{ --"(()-"-!1'-"-tt,.L..C.· ..___,l-f_2~. ~?-,_2._' -~[)"f'-+-'-t't~-h __ 4J_""1~rv,,,..-~, ~_7_. _1..IJ_" _
I tu i._,, 5'. \ l..
Purge Infonnation
l Well Volume (gal):
Conversion Factors: For 2" well: 3 volumes (g Ions) = 0.5 x height of water column (feet)
For 4" we 11: 3 volumes (gallons) = 2. 0 x height of water column (feet)
For hailers: 4 bails = 1 gallon
----3 Well Volumes (gal): ----Purge Equipment: B ""~ I ~..v"
Date Purged: V-c :;, -~-----Purge Time Start: -~ O ~3 Purge Time End: . -------
Did well purge dry? (f) N Actual purge volume: ------
Volume Volume Volume Vdume Volume Volume ------
Temp (°C) -z_. "2 . 'B
pH ~7 -b4-
S. C. s ·4 .3
D. 0.
Turbidity
Sample Infonnation
Sample Time: ~.t~ 0 f ...... Sample Equipment: ~b~~-~_1 ~-"'----
Water Condition (turbidity, odor, etc.): T -, ~ J ~-~~---------------------
Samples Collected(✓):
__ VOCs (2 40 ml vials)
_£ SVOC~(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(° C): __ _ pH: ----SC(umhos): ---
Comments: 11-... J u\' 12. F.A { l:-_ -/, r J -i_ c. l
Dioxin ( 1 1 L bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ Turb(NTUs): __ _
_/_u-'--1_f _4_{3_.._----'~-e.r_._> -----'("-1>_-"'--'+_.,.'-, .... __..,)a::;..._---'-""i,'il'f-F-fC'><--=->'°"-'-:-'-........,="-'-~....;,_{'1..L---'--'1;;=--•f'-_Wra:::....:~::...J.;__ ___ , -.-=-· --=~c__"-.::...."':;__L_,."-. ___ pcbwells.fim
WELL LOG SHEET
Well#: __ l _2-_____ _
Purge Information
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
,. For bailers: 4 bails = l gallon
l Well Volume (gal): i .'.J 3 Well Volumes (gal): ----Purge Equipment: _____ _
Date Purged: _y>-+-1 3~, --'-fJ/_c...~) ...... l __ · r t Purge Time Start: _-L,i O...c-·_,_Z_cJ~-Purge Time End: __ I _0--'-. =◊--J.L...-_
Did well purge dry? Y N Actual purge volume: '-:\ , J 5
Volume I .1 S-Volumed..i._ Volume '-l .O Volume Volume \.i .1';;,-Volume ----
Temp (°C) 1 ·,. ') t ':3 u. (~ ~ --( C~ .'"'\
pH <...v . C· ,~ "j . "j~ -:;'. (,\ '-" -s-. '1 g
s. C. 1 '-! D. 3 i 3i . l ' s ~ _q 12.'1.'Z. I -
D. 0. " IA N/A t--.\/ A N(A N/:1" I
Turbidity ·:1 ~. Lj JY. ~ \I..Q-1 \ ·2. ·3. I 0 . -;, ::,
Sample Infonn.ation
Sample Date: l1 / 'h o / o I Sample Time: i 0 :.o cl I t --~---
Water Condition (turbidity, odor, etc.): ________________________ _
Samples Collected (✓):
VOCs (2 40 ml vials)
_L_ SVOCs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
Temp(° C): l ~ .q pH: S.9 & SC(umhos): /1J1 .L DO(ppm): __ _ Turb(NTUs): lo,.3
Comments: -----------------------------------
____________________________________ pcbwells.frm
--_____....-. -----~ ----------------~ ---~ -SC a . ,
Peg L-F
f=': e lb /1e_~
Ti Ll'lJ--J;~ r?l-i Te..-i..........,., -wl
/,/ ;l-l5 l o ;'2-e7 )/ J,'1 7,3 '1 1<~
UTDS J();/1 77,/ /, c>:;, /~1.,
I Re o~ 11:()0 l&:t I' 7. 3"' /G,,(p
P.£,1..A~ /2 :oa:, t:/IJ.1 '1, 3D /(j?, 'i
I ~ ~
Ettl~.,~ -3:1~ 1J,.1 ~-7~
I
~ r::,t. # _,_ ~ 4;00 I otD ~-8?
~
!
J11',., -/ A f./ ,' / ,< 131 t:;.4'1 ' . (
.
.
I! k
H ,.,
Ii
-
L
Ii
II
'
Ii
1:
-
r
ll
Monitoring Well Documentation Sheet
Well# I A
Size of Casing 2 ''
Total Well Depth 41, 'LI
(
Depth to Water 43. 3t 1
Water Column Hefght 1./ b'
One Well Casing Volume O. '3 S f I
Three Well Casing Volumes I. I ty l
2" casing gallons per foot= 0.163
4" casing gallons per foot = 0.653
Monitoring Well Documentation Sheet
Well# 1:
Size of Casing 7-11
Total Well Depth 41, S4 '
Depth to Water ~3, '85'
Water Column Height j 3 . 6 9 1
One Well Casing Volume 1, 2..
Three Well Casing Volumes 6. 9-
2" casing gallons per foot= 0.163
4" casing gallons per foot= 0.653
Monitoring Well Documentation Sheet
Well# \L
Size of Casing Z. 11
Total Well Depth 3'?". 4o 1
Depth to Water 7. ~ , 1-::}
Water Column Height '1 , 61 1
One Well Casing Volume I, 5
Three Well Casing Volumes 4.3:
2" casing gallons per foot= 0.163
4" casing gallons per foot = 0.653
WELLS
1 (51. 93)
lA (43 .37)
2 (46.86)
3A (65.58)
5 (61.39)
7 (47.54)
11 ( 42.32)
12 (38.4)
OSW-1
OSW-2
OSW-3
OSW-4
fil:Y
RCUS
RCDS
UTUS
UTDS
( 42) Summerfield
(43) Alson
(54) Davis
(68) O'Neal
Sampling Locations-PCB Landfill
April 2001 Sampling Event
SEDTh'IENTS
RCUS
RCDS
UTUS
UTDS
LEACHATE
INFLUENT
EFFLUENT
POND SOJLS
1 through 10
Monitoring Well Documentation Sheet
Well#L
Size of Casing L
Total Well Depth
Depth to \Vater
Water Column Height
One Well Casing Volume
Three Well Casing Volumes
2" casing gallons per foot = 0.163
4" casing gallons per foot= 0.653
31. l.0 1
5. ]2'
pv.-,-'
P~,·-' 21>
,.._,.. ~ I #,;. ~,~,_.
, ;) ,~it ~ _,,r r...P ;_ <1-I J:;) J
T ~r L'2.. 6 r r-1 i{'", gy
s cQ_ r 11 --:2>
Monitoring Well Documentation Sheet
Well# 5
Size of Casing ~
Total Well Depth &I, '5j'
Depth to Water 36 , bD 1
Water Column Height Z.4, t 1 '
One Well Casing Volume -~~-
Three Well Casing Volumes 11..
2" casing gallons per foot= 0.163
4" casing gallons per foot= 0.653
Monitoring Well Documentation Sheet
Well#~
Size of Casing ~
Total Well Depth b b, 5 ~'
Depth to Water 2~-DD '
Water Column Height 42.. 58 1
One Well Casing Volume b, 9 gq(
Three Well Casing Volumes 7,.,( &,I
2" casing gallons per foot= 0.163
4" casing gallons per foot= 0.653
Monitoring Well Documentation Sheet
Well# L
Ll'' Size of Casing _I__
Total Well Depth 4-b . B" 6 1
Depth to Water 34 , \ I '
Water Column Height I 7-. 1-5'
One Well Casing Volume <?', 3
Three Well Casing Volumes iz_r;'
2" casing gallons per foot= 0.163
4" casing gallons per foot= 0.653
Monitoring Well Documentation Sheet
Well# --
IL 1' Size of Casing __I__
Total Well Depth S"/, j;>'
Depth to Water 4-3 . p '
Water Column Height Ji . l ~ 1
One Well Casing Volume 5 , g, gq{
Three Well Casing Volumes / -& Jql
2" casing gallons per foot= 0.163
4" casing gallons per foot= 0.653
-' NC Department of Environment,
Hullh, & Nawral Ruourccs
Solid Wutc Muugcmcnt Divi,ion
SAMPLE ANALYSIS REQUEST St.ate Laboratory of Public Hcallh
P.O. Box 28047, 306 N. Wilmington St.
Raleii;h, North Carolina 27611-8047
Site Number ______________ SampleID Number/Name _:2_=-___ \_b~'-<~l __________ -c---
Collected By __ 4__,___L_,,_~--'--'-iv _______ ID# _____ _
Time /6 :. '(C Site Location uJPrAA£r,nor.t , \JJ A-(/lfi."'1 l, .1,vJYDateCollected 'j :..-7v D --O 1 ., --'--....::..---'=-r---_-_-_-_-_-_-_-_-_-_-_-_-_-__________ _,
Agency: Hazardous Waste £ t) ti11 '.) 1ovJ
Sample Type
Environmental Concentrate
✓ Ground Water (1) Solid (5)
Surface Water (2) ✓ Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Solid Waste __ Superfund TCLP Compounds
Inorg
Comments
fY\w -I
Inorganic Chemistry
Parameter
P&T:GC/MS
Acid:B/N Ext.
2,4-D
Results (mg/I) Parameter ResuH.s(mg/l)(mg/kg) Organic Compound.s _ Results(mg/1)
2, 4,5-TP(Silvex)
chl ordane
heptachlor
hexachlorobenzene ------hexachlorobutadiene ------
enJrin .·
li.niiane • .. , ,~ ,,..,
_ ·· methaxychlq.r. · ·
toxaphene: ,'. .. -.
✓ PcR ·--
-FOR LAB USE ONLY
Date Received ,S-::-./ -0-/ -vp
Date' Htract~ ~~ ~~OJ--VP
• -, , Pc1i3f(Ms-or..J -·
Date,Amj)yzed s--~-0/1/P
R~por~-d ~
n .. , Rc~Y(';~&m
Lab N~~b~r
-
antimony
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zmc
pH
conductivity
TDS
fl~h point __ -
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichloi-obenzene
1,2-dichloroethane -------
I , 1-dichloroethylene ______ _
2,4-dichloroetbylene
hept.achlor
hexachlorobenzene
hexachlorobutadiene
... hexachloroethane
methyl ethyl ketone
nitrobeo.zene
pent.achlorophenol
pyridine
tetrachloroethylene
trichloroethy Jene
-------
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol
vinyl chloride
endri.n
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Sil vex)
-------
• NC pq,,,rtmcnt of Environment,
l.1.ullh, &· N~rural Re,;ourccs
Solid Wutc Muugcmcnt Division
SM1PLE Al'-iAL YSIS REQUEST Slate uboratory of Public He.ailh
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North c~roli.na 2761 l-8o47
Site Number _______________ SampleID Number/Name __ ·1., __ , _3_,'f_i=--_____ __:__ _____ _
Collected By __ 4_,__L__,_, --=;_,'--'-. ;,-..)..:,__ _______ ID# -------
SiteLoc.:i.tion uJP.~1\/. roll/ , W r-:-~G.i,.J G .1,viYDateColl~ted Lf ;_';; D -O I Time / 6.: ..;,o 7 --'---"----=---------
Agency: Hazardous W a.ste z C) llll '., 10\J
Sample Type
Environmental Concentrate
✓ Ground Water (1) Solid (5)
Surface Water (2) ✓ Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Orgaruc Chemistry
Solid Waste __ Superfund
Comments
Inorganic Chemistry
r-------------------
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2,4,5-TP(Silvex)
chlordane
hept.achlor
hexachlorobenzene -------
hexachlorobut.adiene
enJrin
lindz.ne ',--~,.
·· methcuychlq.~·
-toxaphcne· ' 7 P<=-B ,c·
-------
FOR LAB USE ONLY
Reportd;By •· ---,-,-,---,---'------,----
Date_ R:~p_~~---~--------
Gb N~~b~:-012358
DH·S 3 L9l, (RcVised 12/93)
-
antimony
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese
mercury
nickel
nitrate
selenium
silver
sulfates
thalli tr.n
vanadium
Zll1C
pH
conductivity
TDS
fl~h ·point _. ·
benzene
C:JJDO!l tetrachloride
chlordane
ch1oroben.ze11e
chloroform
o-cresol
m-cresol
p-cresol
cresol
1, 4-dichlorobeme11e -------
1,2-dichloroethane
1, J-dichloroethyle11e ______ _
2,4-d ichloroethylene ______ _
heptachlor
hexachlorobenze11e
bexachlorobut.adie11e
.... hexachJoroethane
methyl ethyl ketone
nitrobenzene
pentachlorophenol
pyridine
tetrachloroethyleoe
trichJ oroeth y le11e
-------
2 ,4,5-trichJorophe11ol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin.
lindane·
methoxychl?r_ .
toxaphene
2,4-D
2,4,5-TP (Sil vex)
'f~<-\:'itf.i".;'._ --:· · :>1·"_<.:.' .. · ··, ,·:' .. ' ..
-~ -.-. ·::::~-s:.::·:::.:~~:-:~--~ rr·:::~:::--::::::· .. -. -;--.-..-:-,:r-,:~:-~.
NC ~q,•ri'mer:it o.f Environment,
Hu.Ith, & N•wr•l Re.sources
Solid w .. r..e Marugcmcnt Division
SA.l'YfPLE Al~AL YSIS REQUEST Su.te laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Cirolina 27611-8047
SitcNumber SampkmNumber/Name 2. ( 3 '{ 9 --------------------~-'------------
Co 11 ec t ed By __ 4-'--_L___,_i :v-'-'--1'--.J _______ m # _____ _
SiteLocation uJP:-~N n:>r,.{ w 14:~G.',<J G .1,viYDateColl~t.ed_Lf.J....'_-..::_~_i)_-_;::o;_· I ______ Time ',~--J<)
Agency: Hazardous Waste 7 lJ t V , ~ I o~J
Sample Type
Environment.al Concentrate
✓ Ground Water (1 )
Surface Water (2)
Soil (3)
Solid (5)
./ Liquid (6)
Sludge (7)
Other ( 4) Other (8)
Solid Waste Supe:-fund
Comments
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Acid : BIN Ext.
Results (mg/I) Parameter Result.s(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2,4,5-TP(Silvex)
chlordane
hept.acblor
hexachl o ro benzene -------
bexachloro but.adiene -------
enJ rin
lind.ane ,, ',· .-,
·· methcxychl(}~-.
toxaphene: · pc£ ,:·
FOR LAB USE ONLY
Date ~eceived · S~/-0/J/P
. _ . f"JCEs{MSoV
Date EHracted 5-.;,..;-orvP
.... -· , . , -(Pi"_A8s
. Date f::n<llyzed _ ~-e_-f-O{Y/'
Report6d!By -· · -.--........---,--'--------
DH-S ~ 191-(Revised 12/93)
antimony ________ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fl uoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalli i.r.:n
vanadium
zmc
pH
conductivity _____ ~_
TDS
fl:µh ·point .-----'-'-----'--
c1rbon tetrachloride
chlordane
chloroben.zene
chloroform
o-cresol
II!-cresol
p-cresol
cresol
1, 4-dichlorobenz.ene
1,2-<lichloroethane
-------
1, J-dichloroethylene ______ _
2, 4-di chloroetbyleoe
hept.achlor
hexacblorobenzene
hexachlorobut.adiene
.... hexacbloroethane
methyl ethyl ketone
nitrobeo.z.ene
pent.achlorophenol
pyridine
tetracbloroethyleoe
trichJoroethy Jene
-------
-------
2,4,5-trichlorophenol ______ _
2, 4, 6-tricWorophenol ______ _
vinyl chloride
endrin
lindane
methoxychlor
toxapheoe ··· · ·
2,4-D
2,4 ,5-TP.. (Sil vex)
. -}~':')?? ~
: ·::•-· •,::_ ~ "-'❖"-::::°" t=-::=:~::~~l ... ~ .. ""';:t
NC C:eii•rt;,e~l o.f Enviroruncnl,
Hullh, & N•OJr&l Re.rnurces
Solid WHte M,rugemenl Division
SA1V1PLE ANALYSIS REQUEST Stste Laboratory of Public Hc.ailh
P.O. Bo:x: 23047, 306 N. Wilmington St.
Raleigh, North C,roli.n& 27611-8047
Site Number _______________ Samplc:ID Number/Name __ 1_1_:"?:....:,)'"--D ______ ....:.._ _____ _
1 I 7 . Collected By __ i--r-'---_i_....:...,_, .:..::"-':...:i'v-=---------ID# -------
Site Location u.J~f'-t Tt>N , W p.)tJUi.v-.J l, ..1/\liYDat.eCollected 'j-'.) D -() I
.? _....J___!:'.~_..::::....;-_ -_ -_ -_ -_ -_ -_ -_ -_ -_ -_-_ -_ -_ ------------
Agency : Hazardous Waste
L, t) l V , ') I o~J
Sample Type
E nvironment.al Concentrate
v Ground Water (1 ) _ Solid (5)
Surface Water (2) ~ Liquid (6)
Soil (3) Sludge (7)
Other ( 4) Other (8)
Organic Chemistry
Solid Waste Super-fund
Comments
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arsemc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter Resul:.S(mg/l)(mg/kg) Organic Compounds Results (mg/I)
2,4-D
2 ,4,5-TP(Silvex)
chlordane
hept.acWor
hexachloroben.zem: -------
bex.achlorobut.adiene -------enJ rin.
li.ndz.ne •, ',· -, .
· metho:x.ychlq.r ..
toxaohene· ' ✓ Pc.B 1l"'
. FOR LAB USE ONLY
Date Received . s ~ i-Oly,P
?>cB!:rrM.soYJ ·
Date' E"irract~ 5-;i_-O/-YP
. · -· , ·pce;-u'1voV
. J?ate ~ajyz.ed_ ,:f~~-CJ/~
R~port~·:By · · ~-..----,--'-------
012360
DH·S) 191-{ReVised 12/93) . ·
antimony ________ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese _______ _
mercury
nickel
nitrate
seleruum
silver
sulfates
thalli tr.II
vanadium
ZlIIC
pH
conduc_tivity ______ _
TDS
fl~h point_ .. _·--'-'------
carbon tetrachloride
chlordane
chloroben.z.ene
chloroform
o-cresol
IJc-cresol
p -cresol
cresol
1,4-dichJoi-obenz.ene
1,2-dichloroethane
1, 1-dichloroethylene
2,4-dichloroetbylene
heptachlor
hexacblorobenune
bexachlorobut.2.diene
... hexacWoroethane
methyl ethyl ketone
nitrobenz.ene
pentacWorophenol
pyridi.ne
tetracWoroeth y l ene
trichJoroethylene
2, 4 ,5-trichJorophenol
-------
-------
-------
-------
-------2,4,6-trichlorophenol ______ _
vinyl cW_oride
endrin
linciane
methoxychlor
toxapheoe
2,4-D
2,4,5-TP.-(Silvex)
'\'•.
' J
NC ~c-pu-i:nci:it of Environment,
Hullh, & N•wral Re,;ourccs
Solid Wut,; Muugement Divi,ion
SAlYIPLE A.J.'l"ALYSIS REQUEST Sc.ate LaboralOry of Public He.silh
P.O. Box 28047, 306 N. Wilmington St.
Ralei~h, Nonh Cuolina 27611-8047
Site Number _______________ SampldD Number/N arne __ -=-cl,=--_l _,-~=---'---( ___________ _
t
Collectw By __ 4--'--_L__,_1 ,,_;-=-· .:....i,...Jc___ ______ ID# -------
SiteLocation uJP.AACN \ON W ":-(/<,fi.~ G .1,,,.;yDateCollected_j...L.·_.:..-...,::b_D_-_,<~)_I ______ Tirne I 2...·. <S ------""-----
Ag ency: Hazardous Waste
✓ \) l l/ i ~ I o..J
Sample Type
Environment.al
~ Ground Water (1)
Surface Water (2)
Soil (3)
Concentrate
_ Solid (5)
✓ Liquid (6)
Sludge (7)
Other ( 4) Other (8)
Solid Waste Supe::fund
Comments
TCLP Compounds
Inorganic CompoW1ds
arseillc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/l)
Organ.ic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter Result.s(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2, 4,5-TP(S ilvex.)
chlordane
hep t.ashJor
hexachlorobenzene -------
bex.achlorobut.adiene -------
enJri.n
lindane ·-,,: :-, .
·· methc:xychlq.r.
toxaphene '
1.l "' ': -Pc£
· .. FOR LAB USE ONLY
Date Receivw ·S"-~ / -0/j/P
PC8.tr111.rov
Date' Firrac:~. _ .,S:...~-0{1/p
' '' . ' ' . ~:1 [/J{Sl7f}
?ate AnaJyzed_ ¥.;i..-otYP
R~port~:BY •· -..-~~-'-------
Date Re~orted --'-'---------
1..a: b N~~~~r 012361
DH-S 31.91 (Revised 12/93)
antimony _______ ben.zcne
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
tron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallitr.n
vanadium
zmc
pH
conductivity ______ _
TDS
fl~h point ·-·---'-'------
c:ubon tetrachloride
chlorrume
c hl o ro ben.z.ene
chloroform
o-cresol
r:c-creso l
p-cresol
cresol
1, 4-dichlorobeuzene
1,2-dichloroethane
1,1-dichloroethylene ______ _
2, 4-dichloroethylene
hept.achlor
hex.achlorobenzene
hex.achlorobutadiene
... hexachloroethane
methyl ethyl ketone
nitrobenzene
pent.achlorophenol
pyridine
tetrachloroethy lene
trichloroethy Jene
-------
-------
2,4,5-trichlorophenol ______ _
2, 4 ,6-trichlorophenol
vinyl chloride
endri.n.
lindane·
methoxychlor
toxaphene
2,4-D
-------
_ 2,4,5-TP. (Silvex.) , -·. ___ _;_=
NC Dq,1r;mc:1t of Environment,
H~lth, & r/&wral Re.sources
Solid WHLC Marugemcnt Divi,ion
SAl\lIPLE A.t'l"AL YSJS REQUEST St.ate Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
SitcNumbc:r Sam.pleID Numbc:r/Namc: :;l.. I ~ S-2-_______________ -----"'-=--'----'---'------------
Collected By __ 4.!..._._L_,_( -=;,_,....:.;,..J...c__ ________ ID# ______ _
Si teLoC3.tion uJP.-AAC/lt T"0/1( iJJ l'r~(Uiv-.J G ..l,viYDat.eCollected '-f -'b D -() I --'---"-----'-;================----------~ Time / i--: 4> ~ --------
Agency : Hazardous Waste Z \J l l/ 1 ~ I o..J
Sample Type
Environment.al Concentrate
✓ Ground Water (1) Solid (5)
Surface Water (2) ./ Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Orgaruc Chemistry
Solid Waste __ Supc::fuod
Comments
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lea.cl
mercury
selenium
silver
Results(mg/l)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter ResulLs(mg/l)(mg/kg) Organic Compounds Results(mg/l)
2,4-D
2, 4 ,5-TP(S ilvex.)
chlordane
hept.a-:hlo r
hexachloro beu.zeoe -------
bex.achlorobu t.adiene
c:nJrin
lindane
·· methcxychl9or .
toxaphene· · 1l ~ ' : · Pc£
-------
FOR LAB USE ONLY
Date Received · S:.-J -(J./ 1,/p
. . <p<:£,S-@f JOV
Date' Hrrac~~ . :£:a.. ~oj1/P
... -.. ~A!!J;y-(,,1,(S~-
·. Date 0,DVY~. ~~.340(1(/'
Report6d:BY :. ~~--------
DH·S 31.91, (Revised 12/.93)
antimony _______ beORoe
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalliu-:n
vanadium
zrnc
pH
conductivity _____ ~_
TDS
fl~h point_. · -~~----
carbon tetrachloride
chlordane
chlorobeu.zene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichJorobeuz.eoe
1,2-dichloroethanc:
1,1-dichloroethylene ______ _
2,4-dichloroethylene ______ _
bc:pt.achlor
hex.achlorobeozeoe
hexachlo robut.adieoe
... hex.achloroethane
methyl ethyl ketone
nitrobeo.z.ene
pentachlorophenol
pyridine
tetrachloroeth y l ene
trichloroethylene
-------
2,4,5-trichJorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lindane·
methoxychlor
toxaphene
2,4-D
__ 2,4,5-TP. (Silvex)
-.,-:,h::-Y(~~i~it·i{,:i0 :;~~~t1t~~;t/1\;:;;;+-;,;; ;~4;~\i--,>:·'.· '/·
·. ·• . . .• :.:•· ·.' ,r ... ,·· ~ •J",_·,. • •• <·:•~ .. -.-;~·-.-::.. -.:·:-~ . . . -.
NC ~c:'partme~l of Environment,
Hu.Ith, & Nawral Re.sources
Solid Wute Muugemcnl Division
SAMPLE A.t'fAL YSIS REQUEST Slate Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North c~rolina 276 I 1-8047
SitcNumbcr SampleIDNumbcr/Name ".l.... I o .S:3 ------------------~~----------------
Site Location l.JP.-~N TT>r-1
Agency: Hazardous Waste
/ \J l V , ') I o\J
Sample Type
Fnvironmental Concentrate
v' Ground Water (1) Solid (5)
Surface Water (2) _x: Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Collected By __ l-t_,___L-'''-:,.,.c....;_IV _______ ID# _____ _
Solid Wa.ste Superfund
Comments
Inorganic Chemistry
Time 1 J;. oo
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/]) Parameter Result.s (mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2 , 4,5-TP(Silvex)
chlordane
hept.acWo r
hexachlorobenzeoe -------
bexachloro butadiene -------enJrin .
li.n&.ne ,, .. ~\ .
·· rnetho.xychl;~·
toxaphene: · 11 ~ I • •• Pc..B
· --FOR LAB USE ONLY
Date Recei~ed S"7 /-CJI-Yf)
-1'£!9 5-CMsl7fJ .
Date· E'{tracted ~ol... -a(f/p -. · · , : . ~Us ( /J,fSZ'J~
Date.An.µy~ ~~a-or-VP
R~port~~By '° -r----s-,.,....,.---::-:::-----
Pate. R"ep_urte:c!. -· ---------~
Lab Nur:r;b~r 012363
DH·S 3l9l-(RcVised l:Z/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thall i tr.:Il
vanadium
ZlilC
pH
conductivity ______ _
TDS
fl~h -point_-----'-'-----'---
c:u-bon tetrachlori~e
chlordane
chJorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dich..loroben.z.ene
1,2-dicn.loroethane
l, 1-dichloroethylene ______ _
2,4-dichloroetbylene ______ _
heptachlor
hexachl o robenzene
hexachlorobut.adiene
.,_ hexacWoroethane
methyl ethyl kecone
nilrobenz.ene
pentachlorophenol
pyridine
tetracWoroeth y I ene
tricbJoroethylene
· 2,4,5-trichJorophenol ______ _
2,4, 6-trichlorophenol
vinyl chloride
endrin.
lindane ·
methoxychlor
toxaphene
2,4-D
2,4,5-TP. (Sil vex)
-------
NC D_c:Ji•nme~: o: Environment,
H"--'llh, & Nawral Ruources
Solid Wutc Marugement Divi,ion
SAM:PLE ANALYSIS REQUEST St.ate uborat0ry of Public Huil.h
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Cuoli.m 2761 l-8047
Site Number _______________ Sample ID Number/Name ___ 1..._'-l -'-?-)_5'";__'{..__ ___ __:_ ______ _
SiteLoc::ition u.JP.-AAE:N roll/
Agency: Haz.ardous Waste
/ lJ t \I , ~ I o~J
Sample Type
Environmental Concentrate
✓ Ground Water (1) Solid (5)
Surface Water (2) ~ Liquid (6)
Soil (3) Sludge (7)
Other ( 4) Other (3)
Organic Chemistry
Collected By __ 4_,__L__,_, _:~c..:,;,-.)...:..,._ _______ m # -------
Solid Waste __ Superfund
Comments
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results (mg/I)
Para.meter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter Resul:..s(mg/l)(mg/kg) Organic Compounds Results(mg/l)
2,4-D
2,4,5-TP(Silvex)
chlordane
hept..a(:hlor
hexachlorobenzene -------hexachlorobut.adiene -------enJrin
lind.ane
· rnethe:xychlq.r .
toxaphene· ,:. ,
7 ~Pc._£=-~•-~~ ---~-
FOR LAB USE ONLY
Date Reci:ived -'-'~--...::...,...-=...-=:...~LJ..--
D ate' Fi rracted -71:::-"'7':::-r---~-"-.C......,--
. ·· .. •· . 01?3' 6 -~ Gb Nu~ber ,_ ._.
DH·S 3 19 I (RcVised 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadrn.i urn
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalli u-;n
vanadium
zinc
pH
conductivity ______ _
TDS
fLµh point ··-·---'-'------
carbon tetracWorice
chlordane
chJorobenz.ene
chloroform
o-cresol
rc-cresol
p-cresol
cresol
1, 4-dichJ oroben..z.ene
1,2-dichloroethane -------
1, 1-dichJoroethylene ______ _
2, 4-dichloroetbylene
beptachlor
bexachlorobenzene
hexachlorobut.adiene
~ hexachloroethane
methyl ethyl ketone
n.itrobenzene
pentachlorophenol
pyridine
tetrachloroethylene
trichloroethylene
-------
-------
· 2, 4,5-trichlorophenol ______ _
2,4,6-tricWorophenol
vinyl chloride
endrin
lind.ane ·
methoxychlor
toxapheoe
2,4-D
_ 2,4,5-TP. (Sil vex)
-------
·---:~,---.. J;!'::·
··-·-•-·.· •. -:-~~:-.....-;::.~~ •iii,
'::,
NC l:?_q,•rtmez:it c.f Environment,
Hulth, & Nacural Re.sources
Solid Wur.e Management Division
SAlVIPLE ANALYSIS REQUEST State Laboratory of Public Hc.aith
P.O. Box :28047, 306 N. Wilmington St.
R•lei1;h, North C,ro!ina 27611-8047
Site Number Samp!cm Number/Name 1.1 -~E; -------------------=--c~~-------------
CDl l ect ed By __ 4---'--_L__,_t _:.~_;_l'V ________ rn # _____ _
W P:-.f:..{Ui.~ G ..,1,.,,,;yDateColl~t.ed L(-'b D -O I -~--..-....._-~;:::===============----------~ Time / .>; 2--D , --------
Agency: Hazardous Waste z {J l V , ~ I o..J
Sample Type
E nvironment.al Concentr.1 te
Ground Water (1) Solid (5)
✓ Surface Water (2) V L iquid (6)
Soil (3) Sludge (7)
Ot.her ( 4) Other (8)
Organic Chemistry
Solid Waste Superfund
Comments
VTu5
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
le.ad
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
R esults (mg/I) Parameter ResuH.s(mg/l)(mg/kg) Organic Compounds Results(mg/l)
2,4-D
2,4,5-TP(Silvex)
chlordane
hept.a-::hlo r
hexachlorobeo.z.ene -------
bexachlorobutadiene -------
enJrin
lind.ane •, ',· .-,
·· methoxychlq.~-
7
toxaphcne· · 1_l ~ l .• . Pc...B
···FOR LABUSE ONLY
Date Re~o.rted -:--------~-
Lab N~~b~r 012365
DH-S 3191, (Revised 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluo ride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
th all i u:n
vanadium
ZU1C
pH
conductivity ______ _
TDS
f1~h point _._·_-'-'------
c1roon tetrachloride
chlordane
chlorobenz.ene
cnloroform
o-cresol
r:c-cresol
p-<:resol
cresol
1,4-ciichlorobe:uene
1,2-dichloroethane
1,1-dichloroethy lene ______ _
2, 4-dichloroetbylene ______ _
bept.achlor
bex.achl o robenz.ene
bexachlo robutz.diene
.,_ hexachloroethane
methyl ethyl ketone
nitrobenzene
pent.achlorophenol
pyridine
tetrachloroethylene
trichloroethylene
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chl_oride
endrin
lindane
methoxychlor
toxaphene ··· · ·
2,4-D
2,4,5-TP (Sil~ex)
k ..
NC !?qartm,;nl :Jf Environment,
Hullh, & N,rur•I Resources
Solid WuLe Muugement Divi,ion
SAM:PLE A.J.'[AL YSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North c ~rolim 27611-8047
Site Number _______________ SampldD Number/Name ___ ..c.;)__....,_(_°)-'.'.)'--b __________ _
SiteLoCJ.tion uJP:--AAe:"i Tt>fl/
Agency: Hazardous Waste
/ C) lll l ~lo~J
Sam ple Type
Fnvironment.a l
_ Ground Water (1)
_:L. Surface Water (2)
Soil (3)
Concentrate
Solid (5)
✓ Liquid (6)
Sludge (7)
Other ( 4) Other (8)
Solid Waste
Collected By __ 4--'--_L__,__, ....:.:_,...:...N ________ ID # _____ _
__ Supe:fund
Comments
Time /2:/,
TCLP Compounds
Inorganic Compounds
arseD.1c
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Acid: BIN Ext.
Results (mg/I) Parameter Results(mg/l)(mg/kg) Or ganic Compounds Results(mg/1)
2,4-D
2,4,5-TP(Silvex)
chlordane
hept.acb.lor
hexachloroben.zene -------bexachloro bu tad i ene -------enJrin
li.nili.ne .. ',~ .~, .
·· rnethe:.xychlq.r.
toxapbene 1; ~: I .· . Pc£
FOR LAB USE ONLY
Date Received . · · c5'; /-(J/1/P
. PG8~(M3t:iir) .
Date· Firracted S--.:1.-(J/1/P
,_ .•:·-,1?C,8~(/1f~
. I)ate' Anqlyzed ~~a----0/ ¥P -. -, --•. . ...
Date R6~orted -· --------~-
Lab Nu~b~r 012366
DH·S 3191 -{Rc:Vised 12/93)
antimony
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese
mercury
nickel
nitrate
selenium
silver
sulfates
thalli ir.:n
vanadium
zinc
pH
conductivity ______ _
TDS
fl~h point ___ ·--"------
: /;J.-f~~J}:.>> .-
-:; ··=-·· ::.,·':':~:-:-.-:_· _. . . . . :_._;-.:
beo.zcoe
carbon tetrachloride
chlordane
chlorobenzeoe
chloroform
o-cresol
rc-cresol
p-cresol
cresol
1, 4-ciichloroben.zene
1,2-dichloroethane -------
1,1-dicWoroethylene ______ _
2,4-dichloroetbylene ______ _
heptachlor
bexachl orobenune
hexachlorobutadieoe
.,_ hexachloroethane
methy l ethyl ketone
nitrobenzene
pentach.lorophenol
pyridine
tetrachloroeth y I ene
trichJoroethy lene
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chl.oride
endrin
lindane·
methoxychlor_ .
toxaphene
2,4 D
2,4,5-TP (Sil vex)
NC Dcj:,.~ment r.f Environment, ., '
H~llh, & NAOJral Re.sources
SA.i\1PLE ANALYSIS REQUEST St.ate Laboratory of Public Hc.aith
P.O. Box 28047, 306 N. Wilmington St.
Solid Wut.e Muugement Division Raleigh, North Cirolina 27611-8047
Site Number SamplcID Number/Name ~I: 5: 7 ------------------~-,..l--~-----------
CollectedBy 4 Li ~IV ID# ---'---'-------------------
SiteL:ic.ation u1A-Nl.€N. TO,-./ W ft':(.~ GI'./ G ..1/\li'fDat.e Coll~t.ed_'j..1...·_:........::b_D_-_o=·-1 ______ Time __ J_?._-._-_.;. __ _
Agency: Hazardous Waste
./, l) l V l '.) I o~J
Sample Type
E nvironment.al Concentrate
Ground Water (1) Solid (5)
v Surface Water (2) ./ Liquid (6)
Soil (3) Sludge (7)
Other ( 4) Other (8)
Orgar:uc Chemistry
Solid Waste Superfund
Comments
Q,c_y 2
Inorganic Chemistry
TCLP Compounds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter ResuHs(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2, 4,5-TP(Silvex)
chlordane
hep t.achlor
hexachlorobenz.ene -------bexachlorobut.adiene
enJri.n .
li.ndz.ne •, '1,' .~,.
· rnethaxychlq,;: . · ·
toxaphe~e: ' ll~' I .·. pc.,B
· .. FOR LAB USE ONLY
Date Received S-:. / -OJ-'1/P
' r'C8S-(A,1~.
Date Firract~ _5-~-0/1/P
. . . . ' .. "f?C.{3s { /f,,f,sq)
Date·~~yzed ~a-01_ 1(L
R~porchi:By · · -.--.---,----------
Pate_ Rep.urte<l __ -_· '----------
0 ub N~~b~r 012367
DH·S 31.91 (Revised 12/93)
antimony _______ beu.z.e ne
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
st.ii fates
thallit.r.II
vanadium
ZlnC
pH
conductivity ______ _
TDS
fl<!.Sh point.·-·-~-----
carbon tetrachloride
chlordane
chl orobenzene
crJoroforrn
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobenz.ene
1,2-dichloroethane -------
1, 1-dichloroethylene ______ _
2,4-dichloroetbylene ______ _
bept.achlor
hexachlorobenz.ene
hexachlorobutadiene
.,_ hexachloroethane
methyl ethyl ketone
nitrobeo.zene
pentachlorophenol
pyridLDe
tetrachloroethy lene
trichJoroethyleoe
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lind.ane
methox.ychl? r _ .
toxaphene
2,4-D
__ 2,4,5-11' (Silvex)
NC I?_c:p•rtmcn( o,f Environment,
Hulth, & N,o.iral Resources
Solid Wur.,e M uugement Division
SAlvIPLE A.t'l"AL YSIS REQUEST St.ote LoboralOry of Public H u lth
P.O. Box 28 047, 306 N. Wilming-con St.
Raleigh, North Cuolim 2761 1-8047
SitcNumber Sampk mNumber/Name Z., ( ,'fS~ ------------------~~~------------
Collected By H Li ;,,, vJ ID If ---'----'------------------
Site Location LlPrM-CN ft>N W 1>:--~_(,G',<J G ..,11ViYDateCollected_'--/...L..·_:.--=:b_D_---'(;;;_.)_I ______ Time / /,,. .-u,,
Agency: Hazardous Waste
✓ 1j t V l ~ I c~J
Sample Type
Environmental Concentrate
v Ground Water (1) _ Soli d (5)
Surface Water (2) V""' Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Solid Waste __ Supe:-fund
Comments
Inorganic Chemistry
TCLP Compou nds
Inorganic Compounds
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter Resuli.s(mg/I)(mg/kg) Organic Compounds Resul ts(mg/1)
2,4-D
2,4,5-TP(Silvex)
chlordane
bept.achlor
hexachlorobenzene -------
hexachlorobut.adiene
enJrio
li..nd.ane
·· methro.ychlq.r
toxaohcne: ' 7 Pc£ ,1·•.
-------
· --FOR LAB USE ONLY
Dace Received :$..-/ -(} /-V /J
.. F'CS~ .
Date' Hrracted s~B-0 I :VP
.. ·' ,·; (J'C,§(/11(~.
. I)ate ~ajyzed . ~a-q/3/P
R~portd!By , -.----.-~-'-------
Date. R~p.ortcd . --'---------~
u b N~~~~r 012368
DH-SJ 1.9 1-(Revised 12/.93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
ni trate
selenium
silver
s~lfates
thalliu:n
vanadium
ZlIIC
pH
conductivity _____ ~_
TDS
fl~h point ----~-----
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
r:c-cresol
p-cresol
cresol
1,4-dichJorobenzene
1,2-dichJoroethane
1,1 -dichJoroethylene ______ _
2,4-dichloroethylene ______ _
heptachlor
hexachlorobenzene
hexachlo robutadiene
... hexachloroethane
methyl ethyl ketone
nitrobeo.zene
pentachlorophenol
pyri dine
tetrachloroethy lene
tri chloroethy lene
-------
2,4,5-trichJorophenol ______ _
2,4,67trichlorophenol ______ _
vinyl chl.oride
endrin.
lindane
methoxychlor
toxaphene ··· ·
2,4-D
2,4,5-TI (Sil vex)
NC D_c:p•rtmc,;it of Environment,
H<.>lth, & N&w ral Resources
Solid Wut.e Muugement Division
SAJ\1PLE ANALYSIS REQUEST St.ate u boratory of Public He.s.ir.h
P.O. Box 28047, 306 N. Wilmington St.
Ra!ei1:h, North c~rolina 27611 -8047
Site Number SampldD Number/Name -rL / ~ .)C\. --------------_____ _;:____:... ___ ...:..._ _____ _
Collected By __ H_!___L~, .,,.;~-.:...:.v-J:__ ______ ID# _____ _
SiteLoc:i.tion ul1t(zfLC./\Ht>r-i , W !':-~(/.~N G ..l,iviYDat.eColl~t.ed 1..r--1 D -o 1 ;, _ _,__,::_ __ .;:::.... r _-_-_-_-_-_-_-_-_-_-_-_-_-_-------------~ Time / ?: /f)
Agency: Ha.z.a.rdous Waste 7 l) l l11) I o~J
Sample Type
Environment.al
Ground Water (1)
Surface Water (2)
Soil (3)
Concentrate
_ Solid (5)
/Liauid (6) -'
Sludge (7)
✓ Other (4) C.Jti:::., (8)
Soiid Waste Superfund
Comments
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC!MS
Acid:B/N Ext.
R esults (mg/l) Parameter ResuH.s(mg/l)(mg/kg)
2,4-D
2, 4,5-TP(Silvex)
chlordane
heptac:hlor
hexachloroben.z.ene -------
bexachlorobutadiene
enJrin
linili..ne ·-',~ .-, .
·· methcuychl~r .
toxaohene·· ✓ pc'..11 iJ''
-------
Date R~p.nrted :-~--------
Gb N~~b~r 01.2369
DH·S 3191-(RcYiscd 12/93)
antimony
arseruc
barium
beryllium
cadmium
chlori de
chromium
cobalt
copper
fluoride
iron
le;:id
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thalli u::u
vanadium
zinc
pH
conductivity ______ _
TDS
fl~h point_._·----'-'-----
TCLP Compounds
Inorganic Com pound.s
arseruc
barium
cadmium
chromium
lead
mercury
selenium
silver
Organic Com pound.s
benzene
carbon tetracWorice
chlordane
chJorobenzene
chloroform
o-cresol
11!-cresol
p-cresol
cresol
I, 4-dichlorobenz.ene
1,2-dichloroethane
I, 1-dichJoroethylene
2, 4-dichloroetbylene
heptachlor
hexachlorobenzene
hexachlorobutadiene ... hexachloroetbane
methyl ethyl ketone
nitrobe02ene
pentachlorophenol
pyridine
tetrachloroethy Jene
trichloroethylene
2, 4,5-trichlorophenol
2,4,6-tricWorophenol
vinyl chloride
endrin.
lindane
methoxycWor ...
toxaphene -
2,4-D
2,4,5-TP (Sil vex)
, r
Results(mg/1)
Results(mg/l)
... ~ _:,,·.;,:·,.•: :',};:"..;,if.#i_•.:~ .
~-
f
.
NC Dc4,'•nmei:,1 pf Environment,
H.,;lth, & N•rural Re.sources
Solid Wut.e Man>gement Division
SAl\iIPLE Al~AL YSIS REQUEST St.ate Laboratory of Public H~lth
P.O. Bo:x: 28047, 306 N. Wilmington St.
Raleigh, North C,rolina 27611-8047
Site Number SamplcID Number/Name 2... f J {, 0 ---------------------------------
Collected By __ 4_,__L____,_,_~:...;v-.,1~-------m # _____ _
SiteLoc.ation U!P.-AA-CN. Tt>N W ":-~{<.fil\J G ./,viYDateCollected 1-r-1:> 0 -() I Time / tt ;,.p;z, ---'----'-----r _-_-_-_-_- _-_-_-_-_-_-_-_-_-_------------
Agency: Hazardous Waste -✓ (:} t II 1 5 I o~J
Sample Type
Environment.al Concentrate
Ground Water (1) _ Solid (5)
Surface Water (2) ✓ Liquid (6)
Soil (3) Sludge (7)
~ Other (4) Other (8)
Organic Chemistry
Solid Waste Superfund
Comments
J~ l'/v.c~-/-
h11 " l<..r< l_j A
1e,,f) I >
Inorga nic Chemistry
TCLP Compounds
Inorganic Compound.s
arsemc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/l)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter ResuH.s(mg/l){mg/kg) Organic Compound.s Resul t.s (mg/I)
2,4-D
2, 4,5-TP(Silvex)
chlordane
bept.achlor
hexachlorobeo..zene -------
bexacWorobutadiene
enJ.rin
linc.ane
· methoxychlq.;: .
toxaphene· '
1l' 1 .' pen
-------
Pate_ Re~orted ·.~--· '--------~-
Lab N~~b~r 012370
DH·S 3l9t.(Rcvised 12/93)
anti mony _______ beUZcne
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
s1.dfates
thallitr.n
vanadium
Z-\llC
pH
conductivity ______ _
TDS
fl.µh point.·-·----'-'------'--
c:irbcn tetrachloride
chlordane
chloroben.zene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobeo..zene
1,2-dichloroethane
1, 1-dichloroethylene ______ _
2,4-dichloroethylene ______ _
beptachlor
bexacWorobenune
bexachlorobutadiene
.,_ hexachloroethane
methyl ethyl ketone
nitrobenz.ene
pentachlorophenol
pyridine
tetracWoroethylene
trichloroethy lene
2, 4 ,5-tricWorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chl.oride
endrin.
lindane
methoxychlor
toxaphene •· · ·
2,4-D
2,4,5-TP (Sil vex)
NCDEHNR
Division of Waste Management
D Superfund Section
D Hazardous Waste Section
D Solid Waste Section
Organics Lab: __
Inorganics Lab: __
CHAIN OF CUSTODY RECORD
Project Name:tJ ,i!..,vr<.,¥'\, l.V'\,~ Pt,,f, Sampled By: [.f L,.._;_,
Site ID # (NCD#) Sampler ID
Location: lh....--r-""""~"" NL Telephone:C:tfl.J '1;3 J •-L -'£D •
Address: Date Sampled: lf-a 0-~ \
Time Sampled:
Sample Types: Soil Water ✓ Waste Other
Remarks:
Field Sample 2-,~ 17 L l ·~f U 3Y,j ~L )ol-' 2..1 a re J....t 3.>L 'Z,.( "->' ~
Numbers Ll 1 ~ '< .. A.1,SS"' .2.,,1 ,1..S-b VJ<lt U J St 7..,/3<37( u a -r..~
Relinquished By: u ~.., .... Date:$"=-/-t:> I Time: 2 !' if t:> I'--,, 67 --<Si1matnre)
_Received By: ,I~ .d. ~~ Date:S -L -()/ Time: ~.-oo/Jo\.
(Signature) l
Relinquished By: Date: Time:
<Si1mature)
_Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
(Si!mature)
_Received By: Date: Time:
(Signature) ___..:::: .
Results Reporte\i : ~---:J ~
/{Sihtature) -'
DaM~ 1 ~ G. 2001Time:
v /
(I: \docshare\cocr .frm)
SAMPLE# 012357 012358 012359 012360 012361 012362 012363 012364 012365 012366 012367 012368 012369 012370 N.C. DEPARTMENT OF HEALTH AND HUMAN SERVICES STATE LABORATORY OF PUBLIC HEALTH P.O.BOX 28047, RALEIGH, N.C. 27611 GAS-LIQUID CHROMATOGRAPHY REPORT SHEET PROJECT: Warren Co. PCB Landfill DATE OF ANALYSIS: _____ 05 __ /0._2_-1_4 ___ /0 ____ 1 ______ _ PPM1 mg/L) Sample Type Aroclor 1260 Aroclor l O 16 Other Peaks (1) <0.0001 <0.0001 (1) <0.0001 <0.0001 (1) <0.0001 <0.0001 (I) <0.0001 <0.0001 (1) <0.0001 <0.0001 (I) <0.0001 <0.0001 (1) <0.0001 <0.0001 ll (1) <0.0001 <0.0001 (2) <0.0001 <0.0001 (2) <0.0001 <0.0001 (2) <0.0001 <0.0001 (I) <0.0001 <0.0001 Effluent <0.0001 <0.0001 Influent <0.0001 <0.0003 y -Comments: Sample Type: (1) Ground Water (2) Surface Water (3) Soil (4) Sediment 1' Large unidentified peak present. ~ Large Sulfur peak present. Liquid-liquid extraction, analyses by packed and capillary gas-liquid chromatography using electron capture detector. C:\My Documents\Reports\012357.DOC