NCD980602163_19991203_Warren County PCB Landfill_SERB C_Semiannual Sampling Analyses (TSCA) - 1999-OCR

..._
-GOVERNOR --~i0:1
-1
BILL HOLMAN
SECRETARY
. .. . ~
'
WILLIAM L ; MEYER ,·f
DIRECTOR _ . .,.. ·, ;;,_ .,::, , :-.,~\{)f t~:~r~ · ·. t :e~}t:f.~.iI rr;
.... -. ; . :J:N:~1
f;'t':f/~
.,
.~ .. ;,.,C"'~ :•-: ·~ .. ~: ~, j ... -1~· ,;. ... ~ ' i
. _.,.?,.., _·tAU' = ... ~·i:: ~i.}.J
~ '/,L<._.;}.✓JUIU ,__..__f!_.,
1/;7~_L>u..,_.~ ~• NORTH CAROLINA DEPARTMENT OF
~hENVIRONMENT AND NATURAL RESOURCES
~,,. ... .:We~
~j\j' DIVISION OF WASTE MANAGEMENT
Mr. Craig Brown
Pesticides and Toxic Substances Branch
US Environmental Protection Agency
Atlanta Federal Center
61 Forsyth Street
Atlanta, GA 30303-8960
Dear Mr. Brown:
December 3, 1999
Attached is a table containing the results of the semiannual monitoring of the Warren
County PCB Landfill. The sampling event was conducted on October 25 and 26 . As mentioned
in a previous letter, I did ensure that the pH and specific conductance were measured for both
groundwater and surface water samples with the exception ofwell lA Well IA is essentially dry
and it is difficult to obtain enough material for all tests.
In there are any questions or comments, please call me at [phone] ext 308.
Copy: Mr. Bill Meyer
Mr. Mike Kelly
Sincerely,
Patricia M. Backus, PE
PCB Landfill Project Manager
liiltA ·-·••·• 1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699·1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE 919·733-4996 FAX 919•71 5·3605
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER • 50% RECYCLED/I 0% POST·CONSUMER PAPER
. " •
Ground Water
1
1A
2
3
5(deep)
?(shallow)
11
12
Surface Water
RCUS
RCDS
UTUS
UTDS
Sediment
RCUS
RCDS
UTUS
UTDS
Leachate
Influent
Effluent
Semiannual Sampling Results
Warren County, NC PCB Landfill
October 25-26, 1999
Specific
PCBs Conductance
(ppm) pH (umhos)
<0 0001 4.86 112
<0.0001 ** **
<0 0001 6.10 129
<0.0001 6.60 136
<0 0001 5.52 92
<0.0001 6.40 99
<0.0001 5.04 238
<0.0001 5.68 94
<0.0001 6.97 110
<0 0001 6.92 109
<0.0001 7.01 109
<0.0001 7.12 114
<0.10
<0.10
<0.10
<0.10
<0.0001 6.94 1006
<0 0001 7.14 1007
RCUS -Richneck Creek Up Stream
RCDS -Richneck Creek Down Stream
UTUS -Unnamed Tributary Up Stream
UTDS -Unnamed Tributary Down Stream
** -Not enough sample to_ test
PMB 12/03/1999
' ', 1 1 l ~); ~l Jc/, nrncr.t o( E:-1viron.mcnl,
' 'Hu.i'Vl, & N,rnra.l Rc..s.ou rcci
Solid WuLc M1r.i~cmcn1 Divi,ion
~:.i..::: :....i::~::?:..:=-:-· :.:· :.:~..:~:.:: ::=-i..:.::: ?.~,:~:.:~~: ~:~,~~;;::;:;-
Sit..cNumbcr Sam?icill ~~u:::::c:!~~=-01.0 I b I ------------------=--:--.:.......c... __________ _
tz ":JDC of Sit.e LlJ ~R,61\1 if/Wjl( , Pee L.4t.J lJFtU-Coll~:~ :Sy _+/-f_,__.Z,,-'-1...) c..,,.,V..a~'--------ill~ -------
SiteLocation LJ ~6! £>,J:[otJ , 1'k
..)
Dat.eCclk.::~ /a~ 1-5"~ 'f'q ----------='---;------~----_-_-_-_-_-_-_-_-~---------===-
Agency: Hazardous W astc . / Solid Wastz
Sample Type
Environment.al Concentrate
Ground Water (1) -~]id (5)
Surface Water (2)
,/ Soil (3)
_ Other (4)
Liquid (6)
Sl udge (7)
_ Other (8)
Comme...'1ts
I Organic Chemistry Inorganic Chemis..r:,·
~----------+------
TCLP Comp~unds
l::or-;::.::ic Cor.:1;-ouncs
z-:::.::.::
-----~----
:S:: .... :..::.::.:=.
' Parameter Re:sults (mg/I) Parameter Rcul:..S(r.!g.':)(~g:~:-1':~.,.=.-C:r.-·:-c--•::.•,-,.-',
:O&T:GC/MS
Acid:B/J~ E.:..t.
2,4-D
·2,4 ,5-TP(Sii J:_:;;_)
-::h lorda.oe
bept.zcbJcr
hexa cnlorcb~::::.zens
hexachloreib l!l.2.d it.ne.
cndrin
1 i.nd.2..ne
mcthoxych.ior
toxaoh e.ne
-------
_,/ f,cB ,s e~o-1.lO_~~ .~
I
& li2ue._ Lt.WJ .f"t-i s;oe: c f .fd !
f , ___ I
---IIEATTACHED SHEET(!) !
FOR LAB USE ONLY
Dal:: R cpor1cd -----------
U.tJ Number
2..DtiII:CiiY
E..rse:rt1c
b.riurr:.
b:::·yl!iu:::
cacirr~ur::
c:iror::Liu;:::
cooall
coppe~
fl uoride
iron
IT12.I1£2-""'!e5: ______ _
nickel
ui trar::
silvc:
sulfa.,::s
v a...-riaCl L!C
TDS
fi~h poi:i: _______ _
----· --------
. -' .. . _,.__ -.:,,--. ~----""
--.:---=-:.-:..: .----;"',---~., .. -------~ ------
-

·
-·--4.--.. ~ .... ,_~----·
--. -·-.:· ·:__-c·· :··::::.::
--..::__-=-:-~:,...-~c-~: .. · ~-.a. ----
. . . .-_...::.. __ ,... .. ~-:....--=----
. . . --:.. . __ . __ ._. ___ . ~.__:: __ :
. . . -.-... -:----:::,--,·-::--
---=-· -~•-;--.,-.-=------
. . . -. ----::=-=--... -~~
.. ----__ .._ ___ __
' t.1 1 ~ '. ~ :~,q~r.rr.cnl of Enviroruncnl, SAAIPLE .-\.:~Al YSIS REQl t-5~ ~:.i.:~ ;.__i::.:::-:.:..:::-· :::· :.=--..:::::: :-:~:::
l • · · Hu Ith, &. N1rur1I Ruourcc,
Sol,d Wut.o M1n.agcmcn1 Divi,ion
? -,::._ ~ :!2-:::;' :: =~ ~,. ·,;,r:.:_-.:.::_;-..::c. .S:...
?...t~=:;::. ~::=-~ W.;-:.:.:.::.J. :::.:-52:-!i:..:.-;
ti 2.fDC of Si~ l.JJ ~R, b rJ ~clWTl( , Pc.8 LM fJAll-Coll ~:e.d By --/rl-.,__..2.,,-......,, ,v'--"-·=w ______ ill~ -------
Si tcLocati on u A-'i<,iQ fi}J :I?,rJ ' Ne., Date Cc II ~~ __ /c_o_-_1.___,:_-s-_~_· -~-'q'---____ T :.=c t 3 . 0 ~ . J
Agency: Hazardous W a.ste . / Solid Waste
Sample Type
Environment.al
Ground Water (1)
Surface Water (2)
_ Soil (3)
Concentr:a te
Solid (5)
t/ Liquid (6)
Sludge (7)
~Other (4) Othr.r (8)
Comme.'lts
Orgaruc Chemistry Inorganic Chemis-L...:.--::•·
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/J) Pararneter Rcu.l~(r::.g:l}{r:::g:"'.~:·
2 ,4-D
·2, 4 ,5 -TP(Silvex)
chlordane
hq,LacWor
hexachloro ben.z.ene
bcxachlorobu Ladiene -------cndri.L
1 i.ucizne
mcthoxychlor
tO~i.iphr:n~: F)ua i_s
SiEATTAC!,!EO SHf.FT(SJ
L._ _____ --·-·· . ------------
FOR LAB USE Ot\fL Y
D2t~ Reoor1ed -----------
T 0 b Number 993637
:,.ntirr:cny
s.rseruc
c2.crr.:.1uG::1
., , .. Cfl.....ionce
c:iro,-,-,iu.:::
cobalt
coppe~
fiuorid~
iron
i:.:;d
,-.jcxc.!
r~t .at!'.
S' 1 l t-::. ~i:: ._, • ....,L ........
TDS
TCLP Com~'.)unds
l::o~s:.ic Cor:J.~-0u.nc.s
----·-----
___ .. _. ____ ..
--·----=---:.-.:> ---------
. --. . -
.. ,.:_--:.:..:,,--.-,;,,---~2.-----~---------. -----....._.:: .. __ ,..._.-:;
----~c.::.... ------·--· ... ..:... -.. . -. ·-:... ·-· _..__ .. : ~ ,,..
:-c::· ---.. --==~..:~=---
·--.:--. .._ ___ __
l • • ' \ -. , ·1-. 1-lll ~:-_,;-~ r~tri·.cni 1Jf !:.~":\'1:-..::.:rl.mq1-{,
i 'H -cJ.llh, &: N,run.l RC-1oi..:r::cs:
So!ic W,nc M,rugcmcnl Divi,ion
Sit.cNumbcr ----------------SampicID :'lu:::::.-c:-.•;-;~::
, ...... 2-..i.:...--.·--.· ::· ?·..::::.:= ::~:::
?.S·_ ~_;: :2!~-;. :;:c :-~-·;.r:·-..:..--:;-_:::_ S:...
?J.:::::::;::. ~~,::-0:: ~=--=-..=.::.1 ::5; 2-_!,:.:::;
rar:ccofSit.c Li) fM.l';.G°t\i Gs11VW , Pel?> LA-rJOFtll-Coilc::~By __j._,_f__,_Z,,...Ll.\.LcY-"--"-'w'---_______ 8= --------
Sitd...0c:=.tion L) "''«N &N:ll,,(\)
Ha:z.ardOlL<; w E.Stc "/ Solid W1:.ste TCLP Com~'.:lunds
Sample Type T -a~::..=ic C o□;-0u.nC..S
Environment.a l Comme..rir,
/ GP:nmd Waler (1)
Surface Water (2)
_ Soiid (5)
7-Liquid (6)
M u.J-\ RE·CERl-_-c'"_fO_.::...
Soil (3) Sludge (7)
Other (L) Other (8)
0:-g:::ru c Chemistr;
, .. : ..
D2t:: Rcpor1~-' _/ / C2{3-_? f
993613 I
----------------
---------·----·-----------
------------
,,.J,' ,·--''' .---. . -· '. ···--
,,...,,.:.., •. 11
~J '-L, .::.. ' ._
Iil!oric::
,,:-•-,t·:-~~-'~
---------
------
11=9 tf 3d r3-_ 9 c,3-c;--37----------
_._..:.:,.:.. : ...... -:..,:,, -·-•;.-....
---.. -. ---. ______ --·----·. -., ..... ···-----------·
-.. -·--~ . -·. ----~----·-----------·----~-
--··-·--.. -~
_.=------------------
. . . -______ ...__. ---..:· __ ., _:::_::
·-, f--ic;. D"--J•~mcr:t of E~vircnr:ic:1l1 r ,
' 'Hullh, & N,rur.l R,..,ourcc1
Solie Wut.c M1n.agemcn1 Divi,ion
~:.i...:.: ~=~=-"!.:.::-.-_ _. =---~-.. ::.......:._
? . ~,:~:.:~~: i~~~-::~:~~~~;:_
Site Number Sam?lclD ~l!r::°::c.'~'=-=:. 0 J..O l Y S----------------------"-L......::. __________ _
~ a_.mc of Site Lu /h~J{ b l\l GefWT'( ' Pee, LA-tJ DP/ll-Coll~::.:i By -+1+..L... ____JZ,,....,_\...t:="----------ID= --------
SitcLoc.ation L) P<'{U?, &rJY?:irJ , Ne.. J
Haz2rdous W a.ste / Solid W:o.stc
Sample Type
Environment.al
~ Ground Water (1 )
Surface Water (2)
Soil (3)
_ Other (4)
Concentrc te
Solid (5)
;;!!:Liquid (6)
Sludge (7)
_ Other (8)
Comme-'lts
--------------------------------
Organic Chemistry
Para..rn et er
:2 ,4-D ----------·-1· .
• .. ,, ...... ,.1 •. ,-·.;-. ... ;, ~~J l ~,-~
/ .. J......•'· ·'·.· -
6::i~cl,_:c•c•:rntacren~------------~-"· ----------·--::n~i::;i.n
~ i.IJ ::·,~ l ~
'-,, --...... -;, ;, • ,-,, ~-, . I j \ • • - )
_;L_ p_is_l_~----·---~-C.•POOlff°\-i
---·--------·-·-··-------------
SEE ATT.ACHEQ_Sl:IJ!JJ_S}__ ______ ~
FOR LAB USE ONLY
-···········.
.. ......: ::-1,J ----·--···----
TDS
Date Rwortc.d -------------
993G14
TOY Com~~unds
----·-----
------------
-------------
--··· -·--. ·... . ---. -. -.,.,
----· -----_-_-__ .. --··
----~---· ------....::--~-
. . -~·---=---·-..._ .. --:.-......:. ··---
_::.. ... ·---_:-----
--. _______ .. -.----
. . -. ---·---~-__ ... _.....__
_.:..._ :-:.:-:.::.=.... -----.,..~ ..... -------
--~::------
·,
) '' : Nff S,1r-:.:.:J.\1mc.rt of 'E.:ivircruncnl, ,.
' l-l c..,,IL'i,
0
& N,rual Ruourccs
Sol:u Wu~ M,n..a~cmcnl Divi,ion
SitcLoc.ation LJ P<'B,..IQ GrJ"'@rJ , 'j\/e,
7
Agency: Hazardous V,' ast.c. . / Solid W!'..St.c.
' '
Sample Type
Environment.al
..£ Ground Water (l)
Surface V,later (2)
Soil (3)
_ Other (4)
Concentrate
_ Solid (5)
~iquid (6)
Sludge (7)
Other (8)
Organic Chemistr;
Par:.!..'Tieter
P&T:GC/J;;S
J. ,t,-D
~·1:; ,5-TF(Si! ve>-:·i
:nlordan::
::1~p1.zcbJc,r
hra.xa:[J,J:-c bu l.?.ci i r:::e
enciri.n
·1wd.21 e ·
mcthoxyc!--Jor
Result<: (':!g/l)
L ... ·--···•-·---
Date Reported -------
Gb Num':xr 993615
Comrne...'l~
VY\ U) 2.
Pc..r3..'11ete,·
\ .... ""•--·• ;:, ... _ .._J•, •• } :. , ..... ....:...
' . ..L.·.: ___ --
fl uorici:..
,._ .... ,,...,,,,,-. .. •, .. -
------· ----
TDS
--------------
~:..t..:= ~=~=-!.:..::-.· :::-:.:•..:::..::: :-:-:..i..:::: ?.~::~:.:~~: i~~::~~;~~:r-
TCLP Comf:~unds
----·-----
-... -.. --____ ,.
_________ ,. ___ ------------
-----------·-----. -------·----
------------------------
---,.--I_·····:·-'.·.-.·, I _-,-~_.--·-.-; .. ••-,-~-
. . -. . -. _,._ __ --~ ·--. ·---··--_.._··
----·--. ·-'-... ': __ -
-.r -------.. --, -----~--.... ..,·_. ---
-------.,.--x -.. ---___ , ___ _
-..--•-:----,-.-----~--. --
-. -.
... --------.... ------~-__ ..:._ --: __ -__ --_____ -'.: ___ .
-------
--. --.-. ---.
' . i
' 'H.u.!lh, '&. ~,run.I Ruourccs
Solie! WuLc. isi ,rugcmcnt Division
Sit.c Number ______________ Sam:::i:::ID :--/ l!cc=-':--; ~:: __ O_l,~O_l...:__j_.·_I.,__ ________ _
S i t C Lo C3. [ j OD LJ l'<'f<,~ &}J "y'o (\.) 1 J
/,gcncy: H 2.Z.2.rdous W .aB Le
,,, ✓ Solid Was~
Sa.r::nple Type
Environment.21
_£ Ground Water (1)
Surface Water (2)
Soil (3)
_______ Olbcr (4)
Concentrate
Solid (S)
~ Liquid (6)
Sludge (7)
_ Other (8)
O-:-;:::.:ruc Chemistry
Commt:-'1ts
In or g a ru c Ch ~L.:.-::•
-------------'------------------------
Resul t.s (mg/!) Parameter
. . . ---. . /-. :;a: 1-·. :!,· r....;=.:. s...rse.ruc
b..ri,rrr:
\ ·: :: :-;,: iiJ"~:is:::.nz.::;nr, . --: .. : ·..: .:......:..... -:_._:. ,1 • L• ... ;; .: ,_ .. h.:[~;i r~.;_;1J ~=L~ ie:r:~
J·.• -----;-,J,G:~~k fi uoriC!!
'.:lctno}\·:_--. ~ or
}?..C.8 ls ____ ~()-~ t;J_(!_qj_f>~i
!
--------! !
-----------
------------
,,..'""!'10~',.. •.. _.,r• ---------ms
Dat:: Reportd
!J93616 ---------------
--------·-·
TOY Comp'.:lunds
l::o:-;::..cic Coo;::-ouncis
----··-------
-------------
-----------
----------------------
. . . -. .,,._ ____ ;,,. ___ . --.. ·. _ ... ·
-----· . _____ ---. -___ .,_, .. _,._,_._ -_-
. , ··--. -. -----------·--·---.· -•.... -.. --------·-····· ·----· ·-· -
·· .... -,·---------••·· ... -----------------·
' -.. , -. . ,. ___ ·. _____ . -----
-:.-: : =-=--..: =-=~. ---:
-•--~ :_~.:: ::.::::.-~ ~-.::::::-::c~
---··---.r.··-= --··----··-----
-. . ·_. __ .___. ___ .... ___ ,_~•.
. -... ___ :::_=
------•---
'I 'NC "' ' ( --1 L;,?;.n:-7~cn. o !:.~v1rorJ11cnl1
' 'Hu.Ith, 6.: N,u.:rr.l Ruourccs
Solie Wuu. Muuccmcnl Divi,ion
Sft...:\·IPLE A . .:'\.li YSI.5 REQl t:-5-:::-':.t.:= ....-1::::::: .. · __ --------....&....-?.~::~:.:~2:-: ~~~-~;;;~~~;~
Sit.cNumbcr SampicID :\'t.::::.:::c!:-;=:: 0 ).__C) I l.f ~ --------------------:-----"--~------------
!'Ja,mcofSit.e Lu ~R,bi\l ~dWT'I' Pc~ LA-tJDFIU--Ccllc::~By_-+/,-~(J-_Z,,~,~l'Y~~~------!I:l= __ _ ---
Si le Location LJ f"R_~ &N "J"l:,N , f;/<..,
J
Agency: Hazardous W asr.c -/ Solid Waste
Sample Type
Environment.al
~ Ground Water (1)
Surface Water (2)
Soij (3)
Ot.bcr (4)
r-----------
Concentrate
_ Soiid (5)
~Liquid (6)
Sludge (7)
Other (8)
! Or;;:: ... .>-. ·:--::s.('r;;i..st r; l ,---··---------
_ :. , 5-TP(S: !-,·•~;:)
er. '.1 ·rdiln--:
br:. pL?.cb.:c,r
Results (mg/1)
--··-·------
----------
hr:-~:-,._-r_~'.~:ro bu 1_::-i ~ ~[I~----
,:ndr,.n
j:_,,:2.ne,'
I I.
.v. 'J>CB !Y _______ <.o, ooo~!
I
---------
FO:i<: LAB USE ONLY
D2t:: Reportd ---------
I i
Comme..'lts
Inorganic Che.mis-L..:.-:•
Parameter
HISe.r.uc
Cari um
C2.GIT.!.H..! C.'l
coc=-.lt
c~pp:::-
fiuorid~
iron
i ::.'.:C.
ITl211 £2..."'!eS~
C..: trat'2
' . se.:::.~L!W
siivc.:-
TDS
fl.:..sh 'OC~t
---------
----------·
------
------------
TOY Comp'.:lunds
=-.!.:::.::::
----·----------.-•·-------
---------.:
----------. --· ·----------
-. -·-·-'--··-_-· -. _____ ..._ _____ ._
--• --•-r • .a. ______ .,. ____ _
. ----. -. ,.:___·-·-.... ---_.-·•-::_-t""' ___ .. ;.._~--
---------------
------·. --,------~---•-:.
-..---"'."---, .. --·-··-·-.--. __ ....,_ ______ --~ ---. -·
-_ ... .,. ------..... ·-----·----------
r:::· -~:::-::===-=-----
-__ -_ · _____ . _-___ _
::-
'' .. I I t • I I -. NC: D9•~rr.cr-.~ o( !:.:1v1rcrunc.nl,
' 'Hu.llh, & N,rur,1 Rc.<Ourccs
Solid Wane Mrn.1~cmcnl Divi,ion
Site Number Sam?iclD ~l!:=:'c:c.'~c..:=:. -------------------
SiteLoc.ation LJ Pr'{?,,r?, fil.JYbN ,
J
Agrncy: Ha:z.ardous Waste / Solid Waste
Sample Type
Environment.al Concentrate Comme..'ltS
V . Ground Water (1) _ Solid (5) JI}') w (
Surface Water (2) :i:;Liquid (6)
Soil (3) Sludge (7)
Olber (4) Other (8)
k .;. ,,~. rg::w..i c_ Ct2:r.~..'..::.·y ______ i __ Inorganic CherrJs:r:,
1 ~ ---~·---------n r:.:.• ~J t:; (rng/J) P arar.1eter F .. e5ult.s(2g:.-l)(:::-:~:·~=~~•
! Ft -·.'T: GC/Jv·.f 3 ____ ---·•··· ___ ··-----·.I;~-=~; ... ~·
-------•----
, ' . ~ ::e)'.~CJU:)r;:; "J~:r J:..::..:.Je
}.1.r:.\J,:·.}J~~·;ut)~~L:;("f~.'J~-------
~_:.:-~c :~ r: .
. ::_i ;~ ~ :·. ',• .. . ·---··-.... ___ i J?~~~ .. --_____ <::"~ ~ 0 O(! 'fpn.!
i -. l
I
:r·oR LAB USE ONLY
:-?_,.._,... .... :,_,_
D 2te Repor1c.d ------------
993618
CO'.)~:~.~ . , ,
fluorice
niC:-.:;:;!
n.:trat'e
sii ve:
TDS
----------
----·----------
·-----·------
?.S. ~_.:: :!2---!--::, :;:,::;; ~;_ ·w~..:.::;--=::. .5::..
?J..::=:;::. ~=~~ ~.1.~:.:=..i :.:-5:}-!(:..:."7
TCLP Comp'.:lunds
----·-------
-... ---------·
-------------·-----
-------·------------
---= __ -.:: -~---: "".::::::: ·------·----
•·· . -· • ---. ---1. -'. ·--·--·-·-.... _.__ -------• ..
,==..· -=.::.:,...=--===-:::.=:. --
-. . . --·-:------· _-_--·-
. . . --------_..__ __ -_.__'
.:._ -=: ___ -_--____ -=-----------
..: --:::=-=-------~-.---------·--:--. .__ ___ _
'I < 1.._r -, I I --' · · :,C Dc:.p.l.:-1IT':.cn: of .t:..:1','\:--:)r..mcnt,
'Hu.Ith, & N.o.ir•I Ruourcc,
So!;d WHtc. M1r..1i;cmenl Divi,ion
SAAIPLE .-\..:'\.li y5-r, REQl T-5-:-~:.i..:= ~:::-'!:..::-.· ---':'-.... ·:_ :..:-J....:._ ?.~::~:.:~~: ~~~-:~:;~~~r
0 '01 5-0 SiLcNumkr Sar:::?i:::lD :'iu::::'::-c.:!:;~:: .1-... -----------------------------------
SitcLoc.ition L) Pry(,~ £,JycrJ ,
J
Agency: Hazardous W a.ste / Solid Waste
Sample Type
Environrnent21
~Ground Water (1)
Surface Water (2)
Soil (3)
_ Other (4)
-:;: __ :-; , S-'I}'(Si Ive~~)
-::id C rOi ~~,:
' . ' ~ : : t. ;;_2 C' :'.J :: .. ;--:-_; "JCL..:.:...1...1 C:.
Concentrate
_ Solid (5)
~Liquid (6)
Sludge (7)
Olbcr (8)
.. ,_ .. -------
------·----·----•--· t-,:. :-·.a.c if.: ... 1 ::_; ~)U ~:::di~--1~ --------·--·--·
........ ~ -. ... . ' __,,. __ ; j i
<0,000~
!
----! ---
--·-·--·-. ------I
FOR LAH L;.31:'. Oi'~LY I
Date R t::-;c : ,·~d · Q CT 2 7 1999 fY
?CS~h!JUV ;_::: ~:: =::,: I c.:Ol c:.d _LO-:_,;?._ 8'-99-V1 KAt
;z=t!B5--(Afso1!)
Date An aiy:ul /O-;;J!f_~9Yp
Date Rcoortc.d ------------
!J93G19
TlL'OOCC
TDS
TCLP Comp'.:lunds
--------·-·
Comme..rits
If ----··------
------------
------__;:_:_
--···-···-..:--->-----·------
-----------
-. . .
'---···. --~~· .-·-.... .,
-. -......... _ .... n---.... :-'_,._ ....... .
-· ... -----. ---. ·-·-·· . ___ .... __ . ___ ..
. . . . ---· ., --·-,_, __ . ------
--. ··--. ----
--.----..;.
I ,1,. 1NQ-·u~:p.1.1nrr.cr; of E:ivironmcnt,
· 'Hu.llh, '& N,o.,al Ruourcc,
Soli'd WuL<. M ,rugcmcnt Divi,ion
SA.MJJLE .-1..:'\.li YSE REQlTS'T
Site N umber ______________ Sarn?i::!D ?\L!:::;.:--:::.'":\'~:: __ 0---'--l_-'-:-()_l...c.....:1J--:c___i{---'-----------
~2:illcof Site L1J ft~J{bN 0:;<f'WW , Po~ Lr+1Jl)P/ll-C.')]]c:::~By_-4/,.c..,4:__..L'""--'-'' t'Y=·,N.,___ _______ ID= --------
Sit c Lo c.a ti on u ~~ fi}.J:[l:,N '
J
Agency: H:u.ardous Waste -/ Solid Wast=
Sample Type
Environment.al Concentrate
✓
--
Ground Water (1) _ Solid (5)
Surface Water (2) ~ L iquid (6)
Soil (3) Sludge (7)
Other (4) _ Other (8)
Orga nic Chemist:r;' I I ____ I ___ ••
)In 0
Parameter_
T'&T:C:'~/J,l;S
Rf.:'.:uEs ::, ,g li; 1 T\,:::rrieter
J. -: ...:: -:-, , ... ; ~ • ,-·.;,...;u. ;:.u· 1 '< .r:~; l .
-~~--~ ,.';-TP(Sil·.,;~~~~
,:!1!orri~.a:e
--------~--,------
r!e-.~--:::;cH'~~ :·~ bu t..dc'. I : •. -:c ----···-----· -··-
lC~r...
·pc,13(.5
·--.... ·--·---····
.. SEE AJTACHED SHEET{!)
FOR LAB USE ONLY
Rc'.Jortcd By
--•. ••·;•'-',. V
Cz.ri :..::::
f1uorid~
=..!...!:':'.
TDS
Comme..'lts
,1-.
----------
----------·-----
---------
·-----------
--------------Dai:: 'Fi_c.ponc.d ------------
99Jfi20
TCLP Ccmp'.:lunds
1-,:i_:-;cic Coc;-0unds
----·-------.----~-,-------
---. --_: __ ,.-._,_,_ .... ~ --.. _· ...
. . . . ----~---. . ~_...;:,.--""\ ____ ' --:._-::
-. . -..
_-:._ •-a --.. -·-~-... :.".
. . . .. -c __ .. : :::._.~ ~:: .... =~
---~
-r:::r-:-~~,..... __ :_ __ -.
. -
---. -_ . ____ ...... -:---
... __ . ____ ::_::
.::::.::..:..::~
-·. ___ .. ----
:_ .._,;:._ ----
~ _., ' NC; r.);:?Anrr.cr.; of E:ivircn..'T,r.nl,
· ·Hu.Ith,·& N,wnl Ru ourcc,
Solid Wu~ Min.1~emcn1 Divi,ion
~:.J...:=: 2-..i::::-:.~:--· ::-?·.;::.::: :-:~:::
?.S . ~;;: :~2-:-::-. ;:c ~;. ·,;r:.:_--_:=:;--=::. s.:_
:J.::=:;::. ~::-..:: c~:-:.=-i ::-5~:-!c.:..--;
Sit!:.N umbcr Sam?iclD ~uc:.-=.,~c..=::: 01,C) I ~)..__ --------------------'--------------
fl 2:llJC: or si le Lu MR 6 l\f e,efwTV , Pw LA-rJ DAU-0:>11 ~:e.:i :s y _-4-J:...L.4:_2""-,,, , ...... cY..,:..·=w _______ m ~ -------
SiteLoc.ation LJ P<.i,,'((, fiJJ:l?-N , 1',k, Da~Ccll~~ __ /;.....:oc....-_1...~5_-~___:'f_q.___ ____ T:.=c ·1 u -, .r
J
Ag ency: Haz.ardous Waste . / Solid WP..S~
Sample Type
Environment.al
_ Ground Water (i)
✓ Surface Water (2)
Soil (3)
_ Other (4)
Concentrate
_ Solid (5)
~ Liquid (6)
Sludge (7)
Other (8)
Organic Chemistry
P:u-2.n1eter,
P&T:GCl!',iS
2,4-D
Resuit.s (rng/l)
::\ 4 , 5-TP(Si 1 ve:::)
bexac h)·o:cbuL?.d l ~D~
i V'..'.
tnd n;-:~
iiD~n~;
n2ethoxych..i or
tox 2.!)bt·nc
Rc,JOrte.d By
D2.t ::: Rcoort:::.d
------·-·--~ --
Q_, CJ'?_Off P-"'-
-----------
993621
Comme..'lt<;
u,u 5 -5 <.)
l.u c, ;· g ;._ n.i c Ch e.::n.i.s LT:·
f1niTn i-'. er
-· -----------
lfO!l
1 :
... -----•.. ----
-----------
ITJS
-------------
-------------
TCLP ComI,:~unds
l::. G :-; ==-.::..: C ( 0 D ;:-0 UD. CS
----·-----------~··------
------·-----
. . . --·-_. -----.. --.;
-----· ... -.· ..
----··•--;::,,.-·•::,..-•_, ---------·--·--~
-.... --,,. ... , ___ ·-------· -·-.. _, ..
--.. . --. · ..... ~ -· . -•--·---· -. -·-·· ·-···--
-_,.---•· --... --__ . -------..... -.. -----
---------------~ ·------·---
--,.--•-_--.,....--------.
__ ,.,,._ -----------·. ----
----------
··--·-·-------
·.•. ,.,.c-;?..,1 \ ---r.., 1 !...M,1a 1trr:cnt of .:::.:1v1rc:n..'11cnt1
· Huith, l: N,wal Ruourcc,
Solia W1<1.e M11ugcmcnl Divi,ion
SAl\-IPLE A.:'\.li YSIS R.EQl t.-57 <·,·-;_..t----,.•--: :::· ?-.:::~: :-:.-=..t.:.:::
?.S·. =-::.;:: :!~"7. :::,:;. ~;_ ·,;r:.:_-..:..::;-..=c. ~:...
:-1.::::::;:: . .\::-..: ~=-=-::=..1 :.:5::-!i:..:.-;
SitcNumbcr Sar:i.piclD:--:t.:::::-=:~c.:=:: OJ....01 S 3 -----------------~--~----------
SitcLoc.ation LJ P<f?,;R fi'rJ:[l;,rJ ,
J
i,gcricy: Hazardous W ast.e / Solid WE.Ste
Sample Type
Environment.al
_ Ground Water (1)
~ Surfa::e Water (2)
Soil (3)
__ Other (4)
Concentrate
~ 1-iquid (6)
Sludge (7)
_ Other (8)
Organic Cl1emistry
1-:J.r;:,..:neler
P&T:GC/MS
Re:sul ts (mg/l)
FOR LAB U.3£ ONLY
Date R:-__-:t :vcd · OCT 2 14 1889 fj)
--pc.e~Mso~
0a::: L,ra:tcci J.0--<8"-1'?Jt8KM
~$' r .M:s-o-o ..
Dale AnaJyzul lo -r?..,9.~97-vp
D2t~ Rcpo:-tcd ------------
99:3622
Comme.!1ts
UTDS-
Inc :-gan.i c Cb e.mi._::--;-.i--:-,
._,_ .. -. ·-::
------------
-----··----
C.":J !"lci:..!::: ·:'. ~: ---------TDS
-----· ---·------
TCLP Comp~unds
=-=-:::..:.:::
----·-------
-,,,,..---· ----.. ~
.... ,-·-,.· ·--.. -........ ---'
. . . --·---· ----._,~'--
. -,_·,:_. ____ ,...·_~_-__ -::_:-,
-~ ..
.• ::..........:. __ ;_ •'--••W~ ••~_-:_•
-. ----~ ·--: ··.-·---.-.·-~---►-...
. . ------.... ..,.. ---·• -==--~
.:.::..:-...:::::...::..:::
-_,-r-~....-·----_ _.._ ___ -. ----
..: -..
'~'C..Jr I l r -. 1 1 .. J·tp.i.nrr.c.ni o ~;:v1rcmncnt,
· · H ullh, & N,w ril F:.u ourcct
Solid Wut.c Muugcmc:,t Divi,ion
Si tc Nurnbc~ --------------SampicID ~L!::::::c:~:.=:: __ o_..,_1._6_l_S---,tf __________ _
~ il!Dc or Si 1.e lJJ M.R r t\l Gvwrv , Pc8 LA-t.J LJPtu....c.o11 c:::eo By _.,.../..f_,__,2 __ .,'-"-, '"""c:Y ...... ~~------ID~ --------
SiteLoc.ation LJ 1"..gr?, @J]"l:;N , 1'.k.,
..)
Agency: H a:z.a.rd ous W a.5 te . / Solid Ws..st.c
Sample Type
Environment.al
_ Ground Water (1)
1 Surface Water (2)
Soil (3)
Concentrate
Solid (5)
· ~Liquid (6)
Sludge (7)
Other (8)
TCIY Comp~unds
T-c.:-;::.cic CoD~-0unc.s
Comme..'lts
----·-----
--·-·• ----------------------------------' O r g::r::.ic Ch~mistry Inorganic Ch e.m_is--c..:.-:•·
.Results (mg/I) Parameter-
_1/
·'.!;4,~-T})(Si~
'-'f'1lo:-Ca11r:
--.. -------
-------------6e:r.rJc:!'.!...lt1~·0L•,\J!2.d: ":!;~
rnunn ' I ·-·· --·--------·--I
---------------I
1 -P~,B J_,5__ ___ --~O,OOIJ/l'l'n--l --
1
F0i7, L;..1 USE ONLY
I
I I 7
R.c,:,or:eci By
993623
2ob2..l t
CS:?f:~:
fi uoric::
iron
;:;r;
2.:):1G t1:.:: ·::;-: --------TDS
-------------
-------------
. ---·----------
-....
~--'----· -~-----·---··•::·
---··-•--.... ·------·
--... . . -. _____ .:.-.::::..::~c:::--=r:-:~-:-.. :-.::.::. ----
-. '"---· --__ ... ._ ~---·
-~-.------·-·----·---···--·-·-. -
-·· -Y.: __ . __
__ ..:._ -:: __ -..... --__ ......... -~=-·
-------
--~--.-.· ___ _
·-:-::-----.,..
I '.•. ,l I ,J,, 1 I NC C-.. :-:p, nmcni of E:,viron.rn cnl,
· HulL~, J.:. N1rur1l Ruourcc,
Solid WuLc M 111-1gement Divi,ion
~:.t.:= ;_J.:~:-!.:..:~: :.:· :~..:::.::. :-:~:::
?.S . ~ 2~2-:"7, :;:,::. ~;_ \:,r~...:.::~..:::.:. ~:..
:-t.i::::;:: . .:\~:-~ W.:-=.:.:=..1 ::5:. :-!C.:."7
Sit.c.N umbcr Sar:::i?iclD Nu::::cc:!~c..:=:. ----------------------:---------------
~ ?:ID C of Sile Lu ~Rb IV ~efW TV , Pc6 LA-rJ iJFtU-Collc:::ed B:-· _ ..... /,-J-~_2,,~,~rY~·vV~------ID~ -------
SitcLoe2.tion LJ A:'{{,f;! &N:Js,rJ , f_:/c, DaL'.:Cclk.:::~ __ /c_o_~_1.~5"_-_· _'f'.~q~ ____ Y.-:: t 1, Lo
J
Agency: Ha.zzrdous W astc · / .'.:;olid Waste
Sample Type
:Envi ronrn ent.a I
_ Ground Water (1)
~Surface Water (2)
Soil (3)
__ Otber ( ,;)
Concentrate
_ Solid (5)
-a.Liquid (6)
Sludge (7)
Olhcr (8)
1 Org:n:!..ic Che:::,i._str/
Comme.'lts
Reos -5,._J
Inorganic Chc:n.i~-~-:--
~---·--------------------~-----------------
P 2.r21r. eter
~ ,4-D
~
1
: 4 1 5-11..,~.:> j vc:.~)
:.: ;,1 'J rd.it;-, e.
-·-------
~c. xac}W01·i,) ~-~j l..Gd ienc
;~;~:\, ~: -I'.:L_h~:c} .. .c,CJ.
to::•.~-\~\~;.-...
FOR LAB USE Oi\fL Y
Rc:JO rl t.d By
[)at:: ReportW -----------
?.ar2.!n P:ter Reul~ (r:!g/I}(r:""!g .. ·;:-;~•
:?.I1t1::cc:::1y
lfl..ln
nicie!
n.:trar-::
s::::.:iiL!rr:
sii-...'e.:
S! .. dfatcs
pri
ms
---·------·-·
-------·-----
--·-----
----------------
TCLP Comp~unds
T-cr;2cic Cor:1;:-0unC..S
----·-----
--. __ ._ __ -=-_ . ______ ..•.. ·'"
---------
____ .... ,,..,;;:-----· ----
----·---·--~---.... ~-~-.
--.--··-.:_:._,,:,_=:...._::•'•~·:-
..:..: __ -__ -· ____ . ___ ·
-------
---
"'-l r1· '··' ' f -. : L:. !..-:~":--.rr.cnt o .t.nv1ronmcnl,
Hu ltl:, ·& N,wr&l Ru ourccs
Solid Wu~ Min.a~cmcnt Divi,ion
SAAIPLE _-\.:\Al YSIS R.:E:Qt'T-5 -:::-
Si!.c.Numbcr SampiclD?\u::::::.-c !:S::::=~ QJ__()f S-b --------------------:----~-----------
Si tc Location lJ Pr'{l~ filJ :[brJ
Agency: Hazardous W to.Ste / Solid Waste
Sample Type
Environmen Lal
Ground Water (1)
Surfasc Water (2)
_ Soil (3)
_.L Other (4)
Concentrate
~olid (5)
Liquid (6)
Sludge (7)
_ Other (8)
Orgacic Chemistry
Pararneler-
?,'-~T:GC/M S
·~2;:: ,S -'1:P(Si] ,,c,~)
cf":1ord;oc.
h ~x1chJornben.zt.Je.
Results (mg/:)
------t-,;xa,• hloro t· u ~:l iene
{ ;: .1 r.1: ·~
i i..l.~ c.~; J:)
fTH t~nt,,,,-..J--. j!"':-.--•'--· ...... Ii . .':·-J.. • ...,..
~( ...... :_ :--.r-1:-.:1 ~
------
-------------------
FOR LAB uSE ONLY
L:6 Numb:, 99JG25
Comme..'1ts ·
Inorganic Cbcrrli:-:-c..:.-:,·
------·---------
---------------
co c?J t
fi uorici:-:
1ro:1
m2..11 g::.:-~s~ ______ _
su 1fE..Lt:.S:
TDS
ib . .s:-i pc0: _______ _
---··-----------
----------·-·-------
-------·-------
TCLP Comp~unds
==:!.:..::.::
----·-----
____ .. _.
--: ~:.::..:==
. -. . . ~=-== _=.:_-=-=-=._:...:-::::
--·---------
-~ .. --r-i.-.--,,:,,---;;.-,;a,...
--... : ... :-. ··--:-,-·•· .. _.: ........
----
-.. ---·---·,--------'-'----·= ........ ·-'--=-· _,:: _ __:: __ ---.. -::. . --._ -.. ·-·--.. • .. --
. . -...... -:.----:::,-:--·--:-~ -
. ---. _ _: ___ ~ -_:__. -_..._ ___ -
-, __ ----------
. . . . . -------......... _ .... · _..____
·-.. ~-__ ..._ ___ _
.:. --..
, 1 •'-1r·1•·,1 1 r -· 1 • 1• 1~'-;..;fp•1'"'..rncn1 01 !:.;1v1rnn.mcnt,
·Hult.~,"& Nawal Ru ourcc1
Solid W u1.c Muugcmcnl Divi,ion
Si~Numbcr S=picID ?\L!:::::-=-'~:;.::::: 0 2,() I ,)7 -----------------______ :., __ ,___ __________ _
fi 2!Dc of Site /JJ ftvtR,61\1 ~v•diV , Pc.8 LA-r.J DFtll-Collc:::~ By _-4,:./-l--:..L..-JZ,,'-Ll... =tY=·VV"'-------ID t -------
SiteLocation L.J l'<'-R,~ fi>J']cN , ~le,
J
Ag ency: H az.ard o us Was t.e . / Solid Waste
Sample Type
Environmenf2l Concentrate
Ground Water (1) ~Soiid (5)
Surface Water (:2) Liquid (6)
_ Soil (3) Sludge (7 )
_!!' Other (4) -Other (8)
Organic Ch emistry
Pa.r2 .. rn eter
f&T:GC/\1S
·2, 4, .:.-'fP(SiJ vc.~)
-:nh,ci r:i:ic
Lt pl.acbJcr
Results (mg/])
hr.xa chk~oDt:!12.:'.m.
tn::achlt.>robut.aciene ------end ri.o
1in~16':
rnethor\,crtior -·---·-·-----
FOR L.o..B USE Ol\rr.., Y
· Da i,· ~~:-t;\'~ OCT 2 7 1999 eQ c?-'r ---8f ?'fs>oyg·· ·--
0 ,.:c Ext::c.::.,c.c: 11.-/-?'?VP rPC!3cr-(Atro?iiT __ _
Date AnaJyz.uJ_//_-.:i.,.-.. 9~---
Rc?ortc.d By
Dat~ Reported -----------
99:1626
Comme.r1ts
UT f) ) . srm
Inorgank CL.c:.r1l..is".:.r~,-
c2crr.:2:..::::
co:;:::=: . , .
fkorici::
nicxc!
r.:tra •-::
TDS
...,_ , .
112..Sh pcL1: _______ _
--------------
TCLP Com~'.)unds
• -,:::-;:::..ci c Coo ;:-0 u.nc.s
----·-----
--------.-
·-· --=··. -------
----· ,..~ ... ~-----·-•..• 1,.. __ ..._, ___ =._:.,
---·---· ,--__ ,._...:.-,_\..,:_
-----~ ... ·-'-•-----·· .. --~
-. . . ---------·-· ·:.. •· . - -.. . ::: ___ .. =-: -~~---·-:...
-. -. :-1=::.· -::.::.:.=:-:::_:.:.:::=:.
-. . -·----~--;:----~-=
-·~. -:: __ -__ -------. ___ -______ _
----.,,·--~-----
-_,_··--=---
S:i .. AIPLE . .\.:"'\.li YSI.5 REQlTST
Hu.lt.h, & N,wr•I Ruourca
Solid WuLc Muugcmcnl Divi,ion
?.C:·. ~ 2~2---;:=, ~=c ~;. ·,;,r:.=.:=:;-..::c. .s:...
:J.~t:;::. ~:::-~ U:-:...:=J. 2:-5 ;:-!c.:.-:;
Site Number Sarn:)id.D ;'\uc:::c.'~=:: 0 )__() / r-g -------------__ ____;_-:--...:___::.._ _________ _
!'1 <lfTic a r si 1.e Lu MR. 6 N 0> vw rv , Pc8 LA-rJ DFtu.-0i11 ~:~ B:---J..l~...L-2,.,'-"'--'-, =c".Y=:V-"--------m = -------
SitcLocation U f":'&r?. fi}Jyt,i\/ , :;,
Agency: Hazardous W a.st.e / Solid Was:~
Sample Type
Environment.al Concentrate
Grounc.l Water (1) ~Solid (5)
Surface Water (2) Liquid (6)
Soil (3) Sl udge (7)
L Other (4) _ Other (8)
Organic Chemistry
?2.r2-meler
P&T:GC/MS
2,4-D
?, 4 ,5-TP(S:lve:-:)
chlcrch:w
bcpt.zdJor
R esul ls (mg/I)
bcxachlo: obut.3dicuc -------cndri_;:,
lincL.i1 ....
. ·\' •' .. mclhoxychJor
i :.uxaohe.ne ----·----I
.:P. C.:B.~~------~·Q-' l'2.pp~
FOR LAB U3E ONl, Y
Date Reported
993627
Comme.-'1ts
rQcu1:> -5~0
Par2-rneter
-----------
tluor:i:i::
: "r --i I 1;,, ·-·
TDS
----------
---------·--·---------
----------·------
TOY Comp~unds
l::.o:-;~c Co□p-0unc.s
----·-----
------------------
-----.:·-. ------
": _:_-==~:..: ,.....:__ :""".,;.--... --. ------------·
. . :·---":· --. ,.,. --.~•-··-.---
~---c:: , -==-:: =-= ·--~ -. . .
-. -. --·-:----.-.--~---•->
.. __ .......... ::_-,,.._ ... ·::=_:;
SA.AIPLE . .\.:"\".li YSE REQl tS"T ~:.i..:!: 2...J.:::::?:.:~-· ==· ?·..::::..::. ::.~:::.
i
i
I
Hu.Ith; & N,wr.l Ruourcc,
Sol"id Wut.c Mrn..1~cmcnt Divi,ion
SitcLoc.ation LJ ,,..,~~ firJYbN , ~le, :,
Agency: Hazardous W a.ste . / Solid Waste
Sample Type
Environment.al Concentrate
Ground Water (1)
Surface Water (2)
Soil (3)
t/ Olber (4)
~olid (5)
Liquid (6)
Sludge (7)
_ Other (8)
Organic Chemistry
Comme..'lts
Inorganic Chem.is:c,·
'-·····-----------------'-----------------
Y2.,·2.rneter
?&T:GC/MS
·:· ,i ,5 -T?(Si1vex)
:;-:I ordace
nc:ot2.cb.lor
li ~ xa,:JJoro ~.:cn.zene
Results (mg/I)
-------
• 1-::,.achlorc-Lu tad iene
rndri..u ·
.. ~--::ncia!,i;; >fl .. ~n::lhnxychlor
:,~x::::n:=·.rie
-------
JL .P. c.__,.· \1-/~S: __ ~e_. /1)-/'-P--M-
-·------·-·---------
Dat:: Reportd -----------
993G28
Parameter
2.r1tiwc.:.iy
s.rseruc
'carium
b::·yl!iu:::
c2drr:.iu::
C:::U-0'3ciC
cobalt
copp~;
f1 uoricie
non
IT!e~~l.!rV
cG trare
siiver
TDS
------------
---·------·-
-------------
?.~,:~:.:~2;.: ~~~-:~;;;~~~;~
TCI.P Com~~unds ·
I.::.ar-;::.::ic Cor::1pour:r,
-..... ------:
---------_,. __ ., --------------
____ ,.,.,..---------
-. -~ -.:.:.:.._ ---··-. -.... • -..
_, _,_ --=----\... -
. --..-..";'-::,......-,...,,~---·--··-
. -.. -:... ·-.__...,_ .... ~_-. ___ .:
--·· . __ ._...._ .. _..__-· -
-. . .. .. . _ .. __ ......... __ ; -'---•'-_.__
-·--=---
... -.. --..::-:.:.::.
---------------· ...
---·-···---
' J ~~Q !~_7 .-.11r..c.n: oi E.:ivironmcnl,
· Hu.Ith,'& NlO.i al Ruour:c,
Soliu Wute Muugcmcnl Divi,ion
~:..i.::: ::....i:::::-:!.:..::-:-· =:· ?·...:::.:= :":u_::: ?.~,:~:.2
~~: i~~-;~;;~~:r·
Site Number Sar:::i.Dicill ~t.:::::::c: . .-~~:: 0 l,C) l & i) -----------------'-~--'--'-""--"=-----------
~2:IDCOf Site Lu ~R.,N it1ww , Pc~ LA1JOFtU-eo11c:::~B:--_-'-'/-l--_,___,L""""-'-,=rY=:V"--------ID= -------
Si tcLoc.ati on LJ t".'&ri! fir{:Tl)rJ .J 1'k Date Cc ll~~ __ /c_c)_· _-_1.$_~,..,_--;---~-=.q-:'.=.-=.-=.-=.-=.-=.-=.-=.-=.-=.-=._.1 ·_-_:: __ JI_, _u_c_~-===--
Agency: Hazardous W a.ste . / Solid Ws.ste
Sample Type
Environment.al Concentrate Comme.'lts
Ground Water (1) Solid (5) L~.,_,_.~ •~ k I N r ~v ~ (
Surface Water (2) / Liquid (6) _;Lc..._o.c....v-l=---le--=<~..c.l.-"--~L~1-'-'k'~Cc....· Uf--1----
_ Soil (3)
::;; Olbcr (4)
Org:rn..ic Chemistry
Sludge (7)
Other (8)
In or g a n.i c Ch e.m.is-L..:.-:, ·
----· --------------'-----------------
:?arame!er
P&T:GC/MS
Results (mg/I) Pararn ete.r Reul~ (cg.'i; (r:: f ~:;:,
:'., 4 ,5 -TP(Silve::)
li::oL?.cbfo r
---------b:-:.i:.?.C ;i1 <.)fO ~ u 12.ci i CDC
cndr.n
li.ndane
mctnoxyr.hJor
---
<O. Of1~.l.ff"'I
SU:ATTACHED SHEET(!) -1
tox~rihcn!:.
. \L .I~_c:r,-''is..s=-----
I ···• -· ·-· ·----------· --i
---·--~-----------
F01~ LAB USE ONLY 1
· Date Res:c:-:c~ . OCT 2 7 1999 {2,
. (J> C85 (/11:S-0 !)
:)at: htra-::,tcci_lf) --Z.9-9".?V.P '
. ?='C..B~{MS"OV
Date AnaJy~ //-/-:-99Vf'
D,.,: Reported -----------
G b Number 993G29
2.nt irr:~nv
s..rse::-.:JC
l::2...ri ur:-.
b::--,·l!;u:::::
c:.:.:o;:l~.r.::.
cobalt
C??P=:'"
fi uor:ici:
iron
nici:!
r:::tra:,·
5 ... , .. r-,,,,~
siiv c;
,r.,i;;, ........
ms
---·---
~ ' .
jl2..5:,_. PC!...:1: ---'-------
TCLP Comp~unds
I.:: or; ::..::i c Co r-;-0 un C.S
----··---------~-,------
-... -... -· ----·
--------·-·-•··-----
---------
. --.
. -'-----_:::_ -. ----
-------__ . __ ·-·--·
--,--;..=-· -····---
·-.. . -. .:....---,,..-, .-..--r--;;:.-:-',.
. -·--:---·-··· ... ------------------
-------· .--------._1--.
. ---... ___ --------·------
-----
-------·--·--· ---------------------
'NL Ct:;, ... ;mcnt of E:iviroruncnl,
' i-lul~~.·&: N•wr.l Ruourccs
Sol'i'd Wu~ M1ru~cmcnl Divi,ion
SAi\IPLE .-\.. "\ . .\l YSI.5 RE:Ql TS-:-~:..i.:= ~::::::.:..::-:.· =:-?-..::::.:: ::~::: ?.~,:~:.:~:: ~~~-:~;;~~:t·
~ 2:ffiC of Si~ w ~R. 61\1 ~dWi'( , Pee LA-rJ /JFtll-Coll c.::~ By --1+_,_-'L""""-'-1 =rY=:V.__ ______ ID= -------
SitcLocation LJ f\',&~ G>J:IArJ , 1'k
J
Agency: Hazardous WaB~ . / Solid W!:..S~
Sample Type
Environment.al Concentrate
Ground Waler (i)
Surface W2tcr (2)
_ Soil (3)
~Ct.her (4)
7
Sludge (7)
_ Other (8)
Chemistry
' . . . ri:::,x~chlorobeL..7:..ue
ii.Dill!.!,~
rn:thc". :,<c ~J 0 T
R2Sul ts (mg/I)
::·,:.··::,:,~-J~· -------
..L. _f_s;_8~§!.____ _ _ _ "< 0 d)O/ll,-.~
SEE ATTACHE _ .. _ ----· ---------·· _____ P.5Hm:1-t-.(S-1--
993630
Comme..'lts
Inorganic Ch cmis-L!.-:•
Parameter
2.ntin:cnv
ars~r1.1c
tariurr-.
be:-yl!ie::::
c::.cic-Ju::::
co c?..l t
C~?P~;-
fluorid::--
1ron
i:.::c
nickc!
r...itrat-e
siivc~
ms
TCLP Comr;'.Junds
----·-----
-»-.. -· --:
. ---. . ---. ,• . .,,_~_,. '-.,·--------·------
. -. --... ,.,,.=~-, .. ,, -~------.-
___ ,,,_ .. _. -----.~ .... ~.,,__., -·-____ ... -·---. __ ._ ____ _
• -·-----•--__ r ..___. -
-·----------.. -·--------
=---:-:.=:..::....::
-. -~ -__ . _____ ._-... _____ _
·-:----------
=-._:. ____ _ ----------
'. t 1!~c' ~·.1C?!r.rr.cnt oi E:ivircnr11cnl1
' Ht.J.llh .' & N,rual Ru ourccs
So:id Ww.c Muur cmcnt Divi,ion
~:..!..:.= ~==~=-:::.::-:-· ==-?-·..:~:..:: =-:-=-i_::: ?.~,:~:.=~~: ~~::~~~~~:~S:_
Ol..01 £2-
~ ~c of Si~ U/ ~R r; N. Gc.1wrv , Pc6 LA-tJ OFtll-Collc:::~ By _-4,:./_,_f_JL--'-1..) =rY=·111,i.__ ______ m = -------
SitcLocation W Ajl!Q QJ:[orJ 1 1-,:/c., . J
Agency: Hazardous W a.s t.e . / Solid W a,tc
Sa mple Type
Envir onment.a l Concentrate
Ground Water (1 )
Surface Water (2)
_ Soii (3)
~Olh::r (4)
V Solid (5)
Sludge (7)
_ Other (8)
Or;aruc Ct.ernistry
Pa.r2.1:1 eter Results (mg/I)
bept.achJor
h:.: X?chJ-:,robe~r.e -------b:::.x ach.iorc") buL-=>~d i t.ne
::1 ;_ f1ll
; ill Q2...: l ,.,
s clhr::·, :rucr
-~-_P~8.!~------~;10~~~ ,-, i
I --·-------I
SffATTACHro SHEET($) I
j
i ·--·-----~, ;
FOR LAB USE 0 1\~ Y
D2t~ Reported -----------
993631
Comme.'ltS
lnc,rgarJ c Ch :::.rn.i.5-:..:.--:,
c2.cr:n11.2=::
c:hJoild~
circ, ;.:-.:.i u. =
co'oalt
CO?~!:~
fiu oric~
!fOD
.,.,...,_,,..,,...,1.-,.· ..... -. ---· .
t'.,. • .-r. 1 l l -r, •'' ·--'--· .:... ..
TDS
---·------
·--------
fl:1.5h pct.:;~ _______ _
·---------
TCLP Comp~unds
l::or;:2..cic Co□;:::-ounc.s
----·---------~-,------___ .. _.
--:
: . ..:.,_..:.:r-:...;,....._:...,,.--_,-,;,,,,.. ---
_;_ ..... ~c-
----~::::..;.~:-:::--·~---:---·
--. -.. . ::.._ ._,.__._ __ .. --· __ .::
. -. -. ·----~ ---: _ ..... ----~--
-y-;-::----r-:::=· ===. --
-. ..:... -: __ -.... --_____ . ~---______ _
-__ .... --·---=-:--::=· ~ ........ · ------
... -.. · --. .._ ___ __
--r .----•----. --.· , ___ _
---·------
~-'C' ~Jc?•:"i.rr:cnt of E~viron.rncnt,
· · Hu llh,'& N,nial Ru ourcc,
Soli~ Wu~ M1n.1 gcmcn1 Divi,ion
~:.i.:= 2-i:::'!.:..:~.-:.:-?-..:~~= :-:~:::. ?.~,:~:.:~~: ~~~-:~;;~~:;~
Site Number Sam?icID Nur:::::c::~c.:=c O l_() / iJ -------------------:--~-----------
~ a.me of Si tc Lu IM.R. 61\1 ivwN , PG1!3 LA-rJ l)ftll-0:)llc:::~ By -..... /d-:..,__,Z,,......._, -'-"',.,=~<--------ill~ -------
Si tcLoc.ation LJ Pr{?.,'R f0,.1'9],N , ,,.:k.,
J
DatcCclk.:::~ /o~ 2-S-~ 'fq T:.:=c /<f.• Lf c ----~-,-_-_-_~_-_-_:.-_-_-_-_-_-_-_-_-____ -_____ _.:,:=-
Agency: Hazardous W a.stc . / Solid Waste
Sample Type
E nv ironment.a l Concentrate Comme..'lts
Ground Water (i) ✓ Solid (5)
Surface Water (:2)
_ Soij (3)
Liquid (6) _Lo-=-· ---'1,v __ l-.,, __ t-~l~_L_;-~L,_-----<j!-f1---
Sludge (7 )
~Other (4) Other (8)
Organic Ch2mistry Inorgani c Che.m.is-c...:.-::.-
Paramet.er
P&T:GC!MS
Resulb (mg/I} Parameter Res u..l1.::;r:!g':)(::'!f-~:;
If ...,___
7., 4 ,5-TP(Si] Ve)'.)
ch!orriace
bcr,t.acWor
h:·.;;ad·Jorobcn.z.~nt:
bo:achJorobut.adien~-
cndrin
li.ndzn e
mcthoxychl or
-------
---·---·---I
_'i~s-~e-~:_· --5 g.Jeff?"'-+·-
-------------··---···--I ~~ Cr~_ce,_ If '!.._e_(_s _S....Jilf-ec.'~, i
-SEEAl1ACHEO SH£ET(!) ·---I
I
FOR LAB USE ONLY . -----·7
OCT 2 7 1999 f,
7~c:.e;-/,A1YC:' .rg
:)~~: L,ra:ted _·,pbJ~(:,io~
Date Analyze.cl. / /-,;i__-9 9V/J
-r
L.:ib Numb(:, 993G32
2.n ti.IIC!l)-'
arser-.:.1c
cariu~
cacirrjur.2
ciT0:-,lu=.
cocalt
CO_?F-~
fl uorid:!
!f0!1
mc:-::u:-:,·
nici<c!
ni trace
siiver
TDS
----------
TCLP Comp~unds
1-cs:'.2..cic Co□;-0unc.s
----·----------·~·------
-----------·
s: .. :.::..:.:::=
-••• -----..::--_,__ :> ---------------
----=--, ------
-------•--~.::.=r-~ ! ,-,--'"-,----=--,------------. . -
.. --··· l,,. .. __ .__,_ .. • --_-
--------· -·----_ ·--.. -.,.---------
. . ---~---~--------
--... -=----------::)-~' -·····-····----. ---. . ____ .. -----· -, ____ ' -
-_ ·-------.------------
--~. ---------_ -------------
.. -.,---'-------
---~------
I I I
I !
: \~(!' dq:,.nmcnt of E:1viroruncr-.t,
· HuiLh,' & N,rurol Ruourcc•
Solid Wu~ Muu~cmcm Divi,ion
?.S .. ~ :~2-:--;, ~:c ~;_ ·'d~~;--=c. .S:...
:J.!e:;:::. ;\~:-~ W:=.:..:=...i :::-5: :-!~..:.;
SitcNumbcr Sampi::ID~uc::.-c.'~=:: 02.01 /.lf -----------------:--...:.......:..--'------------
~ ~c of Site Lu MJl..b N i .. 1'(1/T'( , Pc.¥3 LA-tJ DFtU-Colkc:~ By _-+/,J-:...t.._Z,'-'--'-' ,L.>(Y<..L.v\l"----------ID= -------
SitcLoc.ation LJ,,,f{J?,filJ"7oN , ~le, DateCcllcc·~,.; /u-1..J~ 'fq 'i'-c (-lf·, lfb . ---7 ---=--=--:::...:::t..--~-~-~----_-_-_-_-_-_-_-_-_-___ -___ -__ ___::=-
Agency: Hazardous Waste . / Solid Wi:..ste
Sample Type
Environment.al
Ground Water (1)
Surface Water (2)
Soil (3)
Concentratf'._
Liquid (6)
Sludge (7)
$-Other (4) Other (8)
Comme.'lts
Organic Chemistry Inorganic Chcrr1.i~-..:.-:,-
Parameter
P&T:GC/MS
Ac:d:B/N Ext.
2,4-D
·2, 4,5-TP(Silve:c:)
chlordane
hepl.2.cb.lor
hexachlorobcl.lZene
bexachlorobu!::diene
cndrin
li.rJSmATTACHEDSHEE-~n-=S'l __
mcthoxychJor
-toxaon~ne . --·-____ I --
~ Pcs 1~:J.lll!)__a, /9__~r~
I
¥ii !lcb/2i.~J--I~-~-n_d cle~ r~11iJ, ";;:_ . . .I f':_c, llilil.::!_f'r~Lf ~ ~ Si n-7 ~ I '?Y.' _
+o Ax:.tt.C/r, v: Id/~,. --·--·-
FOR LAB USE ONLY
Reported By
D2t~ Rcportd ----------
L.:::b Number 993633
2.ntin:cnv
e.rse::-JC
carius
b~:-vil;u;:::
cacrr~u:::.
c:i:o,--.,iil=:
co:::al i
co;:,pe.~
fi uoride.
1ron
n.ir.x:::1
va.'12.Ci:.i~
---------
---___ ., ______ _
-------
,..,"n(i:1r-•••;•r:_· ______ _
TDS
-·----------
TCLP Comp'.:lunds
T -Qr-; ::..=...i C C (j □ ;:-0 llil c.s
~:..::::
-----···------___ .. _.
--:
-. ---..... --:·--_-.--~-··•-:::.-•;.---,-.
--. ___ .._ ---··. _.---·--··
T ::::.' -=-::..:.::-::==-===· ---·.----~ --·---
·-· ·-------.-·--
__ .:._ ---· .... · ·---~. ----______ _
.. ---. ----------
l ·. 1
' .. ~'..-~c_"':.~c_:J~nrncnt of E:1vircruncnt,
'
Hu.lLh: & N,rual Ruourccs
Solid Wane Maru~cmcnl Divi,ion
Site Number SampidD ?'-iu:::::-c.'~== 0 J._Q I /;) ------------------------'--'"---"'------------
~ <l!De or Si tc L1J MR i; 1\1 ~<l'v,nv , PU:3 LA-tJ OFtll-Coll c.::c6 By --+-/-1-_,___.Z,_,__,__, L..>Crv=·wc...._ _____ ill i ------.:......
SiteLoc.ation L.J ~-&6! G',J:[l:,rJ , Ne
J
Date Cclb:· _,.; __ /c_a_-_.::t.....,:'j'c....-----'-~--'-q ____ T :.=c l'f; '-( f '
Agency: Hazardous W a.stc . / Solid Waste TCLP Comp~unds -·
Sample Type
Environment.al Concentrate
Ground Water (1) ~Solid (5)
Surface Water (2) Liquid (6)
x Soil (3) Sludge (7)
_ Ot.ber (4) _ Other (8)
Organic Chemistry
Comme.."lts
'? P,V ()
Inorganic Chcmi.s--c.-:•
----·-----____ ,, .. __ -----___ .. _ ..
--:
,---· ! ?2..:2.rn eler
P&T:GC/MS
ft.c;d:B/N Ext.
2,4-D
?., 4 , 5-TP(Silvex)
-::n l..-,rd212c
r.r.;'.,.; ::hJorobem.ene
Resul t.s (mg/1)
-------br:xachloro bu t.ad i enc
tndrin
EDGEJ7C
rnctnoxycl--j or
to ~~(.;.'.1hene
-------
.L pc~:s I sef?-6 ~ti, / ~ f-1-~. · ~
I
~,€ Tn:~r.e /-e;;e I s:usf"' (_ fe.d,J
----I
-------
FOR LAB USE ONLY
D2t:: Rcpor1Cll -----------
0 9~£>'34 L6 Numocr aJ .... \.
2.nti:o:c:w
arsc;--...1,..:
emu:::;
b~:-y 11 i u r:.
cacirrj-..:~
c:irociu::.
cooaJl
coppe~
fluoride
iron
IJ'i2J1g2...""!eS~ _____ _
ri--, 11;, •-:
TDS
Jl:;.S:1 poi_,: _______ _
, -. __ ,.__ __ ,:,,,_ -_. -·--~
-----~-----~ ----------
----. .
. ·-_.....,___.:,·--.._?". . -"'--·----------___ -:::..:. . --··-: : ... ·-_.--... -..,,.
---=-~::::=:c::-~::_._. ~=~ -·-·-··---··· . -----
-. . -,..:._~-~r-c: ___ .,.. _::
. -. -.. . -_-::__ ... _._ __ ·.__._ --· ·:....:.....:.~==::.
------------.... ----·--
. ----.. ____ .._r;:. __ :-~~
. . -.
--------~~-----
-_;._ ·---------.__'.'.: ____ _ -------
__ ,. ________ --
------·----
t '•,1 1 ·'.~c·~~;~r.mcnt oi E:ivironmcnt,
Hull!l: & N1D.Jr•I Ruourcu
Solid Wu~ Muugcmrnl Divi,ion
~:.J..:=: :...i::::-~:..::-:-· =:-?--..:~::= ::~::: ?.~,:~~.:~~: i~~-~;;;~~:;~
Si1.eNumbcr SampicID :'\u::::::-=:°;\~:: 0 l,('.) l 6~ ---------------------------------
ti~ e of Site Lu ~R.bl\l ~(/'rt/TV, PclB Lr+rJOP/ll-Coll~:edBy_...1,:./,./--:..;__JL'-'..l-l=rY~~w,,__· ------ID= -------
SiteLocation UP<:R,~QJ'71,/\) , t-,;/c, DateCclb::~ /0~1-s< 'fq Y,-c /'(~ 't'J
. ---J -----='-;~~~~~~~~~~~~~-----------==~
Agency: Hazardous W B..'lte . / Solid Waste
Sample Type
Environmental
Ground Water (i)
Surface Water (2)
✓ Soil (3)
__ Otber (4)
Concentr:ate
~olid (5)
Liquid (6)
Sludge (7)
_ Other (8)
Orgaruc Chemistry
Comme..'ltS
Inorganic Chem.is-c..:.-:•
P:1rameter Results (mg/1) Parameter Rcu..l:.S(r::g.·I'!(r:?g ·~s:•
P&T:GC/MS
AciJ:B/1~ ExL.
2,4-D
2,4 ,5 -TP(Silvc:)
chlord~e
ht:..,t.zcbJor
he:xichloroben.z.ene -------bi:::-.achlorobu t..ad iene
.::n dri.o
lindane
m~thoxych.i or
~Gx .:un~0~
-------
:_£_ J_i__~-~W-o) 1i:JJ-p.pi:A-
~-~1\1=r~~~£~ S!is;i·+-"rS,_,_} __
L_ __
FOR LAB USE ONLY
Rc?O rtc.d By
D2tc Reported -----------
G b Nu mber 993G3S
~,tir::ccnv
carium
be:y·11iu~
c2.cirrj u::=
c::iro!:2.iu=.
cooalt
fluoride
non
i:::.:d
nickel
n.itra~
silver
sulfat::s
t!;..:..lE~=
:::.o!1ci~::::-.·:~.--______ _
TDS
TCLP Comp'.:lunds
!.::.ar;::.=:ic Cor.:1p-0unc.s
--·---;,,.--a-.=-_______ . __
~ _..:..--=:f'"~: ___ :_.-:----~::-
--. -· __ · : ___ r-.. _;:'.: __ -
-.!...-"_::_:... :r.·-:-.-,..-:-.:_.·. _ _,,
. -~~--. ~r::--·------
-. .. ·=-~---· ...., __ ;.___::, __ ,_:
. . _::..· ----.... --~=
·----~ -----· -• .......... '••
. . . . . ________ ..,,...,. -·~-=
--:--~_.::.._. ___ ---:..~--r--.
.;. -_ .. --. ------
---··-----
-------
-----
-------
• ' ' ' • f,. 1'.t'CDEtti~R
Division ~f Waste Management
□ Superfund Section
□ Hazardous Waste Section
□ Solid Waste Section
Organics Lab: V
Inorganics Lab: __
CHAIN OF CUSTODY RECORD
Project Name: WAt{p_;:AJ GvN;y __ I-Avoc:;-,1-L Sampled By: µ-z_,:.,.,..,
Site ID # (NCD#) Sampler ID
Location: l..Je.A""n~lv·~ Ait:G Telephone:~
Address: Date Sampled: I o --1.f /4 , ·-C.f4
Time Sampled:
Sample Types: Soil Water Waste Other
;,
Remarks:
Field Sample 0 -LD,'--{j 01..-<.> . 'l '-l ~ 6LD 7'1..cP Q'L.o1 'it 01.....Dttfb 62..D l'::i ct. d2»7 S"l:)
Numbers C, ·1..-0 J.. r:1 0 ·1..-01,1"L bJ..-D:1 L2 1">"1.-07 '2__1:f._ ,~"l...-c:Js-:5"' 6 ·z...,;,7 s-' C>l.,07,'!{_,
01..-.:.'?y~ 6. 1.-C>t ~Cj QU)i t,<> b'"LC ,t:.1 D "'L D "1 <... -,____ C l.,v '1 (., 3 D 2-o "7 G.'J...
~1-o r& s-e:, ").,,Q 7 u:. D,-0 7.lc C;,1.,<Y1 {.,g
Relinquished By: -~=7 ~ Date: lo -2f]~ecc; Time: )/·~s-
(Si1mature)
Received By: /1~; -t. LfJ--vYJL<--i.,er-Date:/ cJ -J,-7-7'? Time://-' 'I)-
I
(Signature)
Relinquished By: Date: Time:
(Sienature)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
(Si1mature)
Received By: Date: Time:
9 ·:=n"\e)
Results Reported: __i~✓d Yl.P~£ Date~'=?-~/ Time:
(1i'g!)d'ture) . ,
(I :\docshare\cocr. frm)
N.C. DEPARTMENT OF HEAL TH AND HUMAN SERVICES STATE LABORATORY OF PUBLIC HEALTH P.O.BOX 28047, RALEIGH, N.C. 27611 GAS-LIQUID CHROMATOGRAPHY REPORT SHEET PROJECT: Warren CounlJI Landfill DATE OF ANALYSIS: 10/28/99-11/10/99 (PPM) SAMPLE# PCB Hydrocarbons Sulfur Aroclor(l 260) 993628 <0.10 NA NA 993629 <0.0001 PRESENT ND 993630 <0.0001 ND ND 993631 <0.10 ND ND 993632 <0.10** ND ND 993633 0.14*** PRESENT ND 993634 <0.10** ND ND 993635 0.13 ND ND 993636 <0.10** ND ND 993637 <0.0001 ND ND GCREP.DOC 1/99 REV ND=NONE DETECTED, NA=NOT ANALYZED *=Tentatively identified as n-butyl benzenesulfonamide **=Trace levels suspected ***=Artifacts and degradation products present, similar to Aroclor1016. Phthalate(s) Unidentified Peak(s) NA NA PRESENT * ND ND ND * ND ND PRESENT ND ND ND ND ND ND ND ND ND PAGE2OF 2 , ,
N.C. DEPARTMENT OF HEALTH AND HUMAN SERVICES STATE LABORATORY OF PUBLIC HEALTH P.O.BOX 28047, RALEIGH, N.C. 27611 GAS-LIQUID CHROMATOGRAPHY REPORT SHEET PROJECT: Warren County Landfill DATE OF ANALYSIS: 10/28/99-11/10/99 ----(PPM) SAMPLE# PCB Hydrocarbons Sulfur Phthalate(s) Unidentified Peak(s) Aroclor(1260) 993613 <0.0001 NA NA NA NA 993614 <0.0001 PRESENT ND ND ND 993615 <0.0001 NA NA NA NA 993616 <0.0001 NA NA NA NA 993617 <0.0001 NA NA NA NA 993618 <0.0001 NA NA NA NA 993619 <0.0001 NA NA NA NA 993620 <0.0001 ND ND ND ND 993621 <0.0001 NA NA NA NA 993622 <0.0001 NA NA NA NA 993623 <0.0001 NA NA NA NA 993624 <0.0001 NA NA NA NA 993625 <0.10 NA NA NA NA 993626 <0.10 ND PRESENT ND ND 993627 <0.10 NA NA NA NA GCREP.DOC 1/99 REV ND=NONE DETECTED, NA=NOT ANALYZED PAGE 1 OF 2
-·-
.. ---------___ D--t-
2 n '. r ~ , e>-).,~ ------·-----------
_________ 3A ___ _
_____ S"c._ ______ n_.: c"1__ts>-1.5,J_ ____ ~_._Y_2..._ 11.. '1
C. .'( '11. L --
---___ J! __ _ __ /k)__.:::> __ lo_-'2.._, ____ s_-"°_'I_ J,J_i~ __ l.:,_-,~/ ____ l_2._r_2 ____ _
--------------n ..
--------· -----------·---------------------
------------~~~l --_ l'f: ~ ____ l_p__:_2--_>_ __ -----7 . .,,_, -----Io~ . .tf _____ --____ --------------_ -----
.F:-~ Q_5 _ _ _ _1/!_ ~ _ -~v_.::._L'i __ _
_ }N ______ I /o.,..:,.
g PF ,s, .x:-7 . I'{ -_(_o _ Y-7
--------------------···------..
. ___ fl~ 0--_ I_ ---5-_[ft~~---ID -l-'--1 \ -
_ --------M.Jt:.~ _ l __ ~i~~_(b_-).,c.8~
___________ ---~~-~~:3 ';1 _l'i~~o-_ _J_o_:~c.-'\.~ ______ _
(«-' ~_s-__ S-:L __ \
---- -l l/« ½. S-5"_ ~ ( -2---
jlt:l-t1' >-: l )
_______ Lo-1....~ ________________ _
-------------------
-------------------
-----------------------·· ----------
NCD r:HNR
Divisio;1 of Waste Management
□ Super:i.md Section
□ Hazardous Waste Section ,· □ Solid W aste Section
Organics Lab: V
Inorganics Lab: __
CHAIN OF CUSTODY RECORD
Project Name: lJJAR.~AJ ~vrv,':f.. l.Avoi:;, L..<..... Sampled By: I-+ 2-.~-
Site ID# (NCD#) Sampler ID
Location: [_J.....,..,--G!:l,~>\.... AIL Telephone:~
Address: Date Sampled: I 0-2.s ,/2., -cf'1
Time Sampled:
Sample Types: Soil Water Waste Other
,
Remarks:
-
Field Sample 0 '-1,.D t '-{ '.::( C> 1....0 ' '-l ->r 61....0 7'1Je. Cl. 1..0 7. r£ / 01...0"1'-I:[ bl..01~C/ "lJ,)7 S1.:J
1 Numbers C "1,,.0 '7 1 I l>'-0 '1 t:"2.... bU>:J. r:J ~i..-07'5'1 akc:i ~-:s' 6 -z_.::>7 <' Dl.£J7,0
e, 1.. ~ '7 s-~ i) 'l-C>t f''1 Q'l..,07 ~,.) b~tbl c, 'LC7 <:. "l....... C1..,o1(.:.3 C, 2-.c ·7 <.'f_
() 1-<;, ,6 s-C:,"'l..-0 7 (:.(.. D""LO 7,/., C:>"'L-07tZ
Relinquished B y : Date: -Time:
..
(Si2nature)
Received By: Date: Time:
(S ignature) ..
I
Relinquished By: Date: -· Time: II
(Si gnature l
..
I Received By: Date: Time: --·-·-
(Signature)
f\.elinquished By: Date: Time:
(Si2nature)
Received By: Date: Time:
(Signature)
Results Rep01ied: Date: Time:
(Si gnature)
(I :\docshare\cocr .frrn)
WbLL LOG SHEET Facility: Warren Cou'ntv PCB Landfill Location: Warrenton
I .
Well#: __ ___._ _____ _
--.--·
'· Comments (weli c~nstruction, etc): _________________________ _
Conversion Factors: For 2" well: 3 vol = 0.5 x height of water column (feet)
Pur~e Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
--. _-·: .;.~=-:; .. --:;,,_:_. -·.
1 Well--~V~iJ~~(~al):
For bailers: 4 bails == l gallon ·
S-~c.. I. 3 Well Volumes (gal): ____ Purge Equipment: ?,...._\....C~ Q.,~
• .•• 'I"
Date Purged:·:-Jo h.t., h'I
Did well p1,1rge dry? (!) N
Purge Time Start: I O : '-(. c
Actual purge volume: t/f al
Purge Time End: l O If o -------
Volume 0 v$fmi~ VolumeW" VolumeY,-Volume Volume ---
Temp (0 C) . 17. st /7,'/ cc
pH ~ ,/y L/.8'6
s. c: , ~ J. v~r 111-1,{,(r
D. 0.
Turbidity 12 , q ,1/Tl.f I,_ .c/ Niti i I
Sample Information
Sample Date: (',;,/2,..,/j5.
Water Conditio~odor, etc. ):_/_J._.q_N_nt ____________________ _
Samples Collecttd (✓):
emp(°C):
VOCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bottle)
_Metals (1 IL HDPE bottle)
---pH: ----SC(umhos): ---
Dioxm (1 lL L•ct!le)
Pest./Herb. (1 21.. amber bottle)
DO(ppm): __ _ Turb(NTUs): __ _
omments: kJdf-~J p,d·j,.,J ~ ±-o vofv..,. > u... [ o-2S Aq !,,_,-/ e.v~~ ,.,,..f J; ;lrq_,
-t-I
t"-''-"'--"-=-=:,-..,:~--;-c.__.....__..-""'-!<C>'----....:.~.:..::__-..!/...!::()-:......-....:::.)......:.t>=-_. ---------..-----~c---1--~---pcbwdls.frm
'P'"'"1' '-I 5«..I b~.-. ~tt r..,,, -1-l,..).,. -~ 1/z_
C. t,~ ... -f .s '-, le "f~"' l"'-4'! c..lv.1 ~ .
Facility: Warren Couhty PCB Landfill Location: Warrenton
'.Purge/Sam?le Team: tJ l.€.M--: L-. ~ . ~~~_:IL q Well#: ---------
;----?.~··.
,Comments (well construction, etc): ________ --_· _______________ _ -"'( oe,_ --,L~, --4,u4 ;-7. ~OJ I x:-~ -::; -:_:./ -5
Conversion Factors: For 2" well: 3 volumes (gallons) = .5 x height of water col (feet)
Purg:e Information For 4" well: . 3 volun{~-~'(g~lons). = 2.0 x height of water column (fe~t)
1 Well Volume (g~l): ~
Date Purged: · / D/::;s"( '11
J I :
Did well purge dry? Y N
VoluI?e _fl
Temp ("C) ,.,. tl,2°LJ
pH 5, {i
S. C: /0 8. q
D. 0.
Turbidity
0ample Date: / Q /J \ /55 ___,,..........,_, ~,-1--L-.L---
For bailers: 4 bails := 1 gallon -· -·
3 Well Volu~e_s (gal): ·/(j,S8~Purge Equipment: _____ _
') 3c Purge Time Start: ex...; fY'\_
. , Purge Time End: ______ _
Actual purge volume: _____ _
Volume _J_ VolumeQ_ Volumec:2J;i_ Volume.3_ Volume
{~ I ( d(....
L,,~7 ;,}')/
/oi . o Io g. I
I '10 -Iv
Sample Information
Sample Time: -----
-=--'-
Sampie Equ ipmern:: -------
\Vater Condi tion (turbidity, odor , etc.): ---------------------
Samples Coll ected (✓):
✓
emp(°C):
VOCs (2 40 rrJ vials)
SVOCs/PCBs (1 2L Amber bottle)
Metals (1 IL HDPE bottle)
---pH: __ _ SC(umhos): ---
Dioxin (l 1L bottle)
Pest./Herb. (1 2L amber bottle)
.,1
DO(ppm): ___ Turb(NTUs): __ _
omments :--!F-\N--"'--'lli-><..>..+-f-'-"'O c\~111..1.L.l,n;t'-'-"-J )..___,~"'---'--"1~( n_o--'-'yu-'-=-o't(,--=-----.:i;~~~o,,!::>-+c-FfJ~-__..[__.iNrl~),_____,~~:~"'""-,u_to_-__.(t(".L->---=-=-0...Ch-~
j'-----LL--'---'-'-':..u.A..--\,l,,ll.l....l,"'--1..:=--lf~~4--'r-'(j)"'-=--~"'-'--"-""-"--"~:..o....:...,~-"'--~~e::u__-,l,<!~--¥~,..1LU<>..1..J4fl..-~~~~;L--pcbwclls.fnn
'WELL LOG SHEET · Facility: Warren County PCB Landfill Location: Warrenton
.· Purg:;Sampie Team: --:re' 'mittfN,0;, /& ,/J, f,,, dcztfz Well #: __ {) __ /_.· ___ _ . . 0 7
c4T,eilf h (weil construction, etc) L/11 w-d} Lj &, 1;1., ' ~ wdi,,, 3 If, ,/ .!,t L
3 fo , / ; -/ (J "1 ~ 1
X 2 == ;?.I £:........,,,::,~a.,_,_1i.;;.._o '7'-".S'-----=----------------
Conversion Factors: For 2" well: volumes (gallons) == 0.5 x height of water column _(feet)
Purge Information
1 Well Volume (gal): -~---
Date Purged: · !Dps;l9f
Did well purge dry? Y (~)
VoluI?e fJ_
Temp (0 C)
pH
S. C. I q . q
D. 0 .
Turbidity
Sample Date: ~j.) 17 7
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For hailers: 4 bails = 1 gallon
3 Well Volumes (gal): :) /,.S-2-Purge Equipmentj>:imlhy~·
Purge Time Start: // ,' L../ 0 Purge Time End: /3 L5
Actual purge volume: :J (jc)/Jn/}_5.
Volume / Volume2ll-Volume3 Volume
"'l_/,5 w.s-
,·. 2 I C,to
13 ,Jj
I J :i_g '-
{),OD
Sample Information
Sample Time: . / 3 / ~
~ ..... Sample Equipment: _______ _
Water Condition (turbidity, odor, etc.): ______________________ _
Samples Collected (✓):
Temp(°C):
Comments:
· V OCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bot.t!e)
Metals (1 lL HDPE bottle)
---. pH: ---SC(umhos): ---
Dioxin (1 lL bottle)
~est./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): __ _
--------------------------------
_________________________________ pcbwells.frm
, WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: ~nd/, SJ<Ab/t';(J&tlh lulktr·wen #: _3""-'ff-+------
1
. UI
Comments (well construction, etc): ------------------------5?; · I -/1,Y 2 j7J q cl 3' '-/7 / :::. ~/J X ., ~ == d {)
1 Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
1 Well Volume (gal): --;f
Date Purged:. /o lzsh t
For hailers: 4 bails = 1 gallon
3 Well Volumes (gal): d. Q .... Purge Equipment: Grwdb IJ,w ~
-.) f I
J J Purge Time Start: 0 9 L/S-: Purge Time End: /D ,35,._ __
Did well purge dry? Y N Actual purge volume: ;;/ faa//4., j
Volu1:1e J2 Volume_L__ Volumec2_ Velum;;;>~ Volume 3 · Volume --
Temp (0 C) ,,, J ), (f /1,?.... /7, )-/1. I 17 I;}._,
pH t .29 C.,y' u-~1 fl,j--c.f c;, -~O
S. C. //0.-1 //1, :l ;o:;-. 7 I /3~-, 3' /J)il
~
Turbidity I I i ~-11 S-,0 ,z. l.JS-J,g7
Sample Information
Sample Date: i u /;z.s}q ~ Sample Time: lo 3~ Sample Equipment: -------77
Water Condition (turbidity, odor, etc.) : ___ ~l/~~~u~~.----C-/4~t'.-CVJ.,._,__ _____________ _
Samples Collected (✓):
Temp(°C):
VOCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
---pH: __ _ SC(umhos): ---
Comments : ) I {)J p f v1 rh I J1h. '-f"'.c J/JJ G f h ~
1
__ Dioxin (1 lL bottle)
~st./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): __ _
-----1.--'Ce:n,, ..... · '-IQ...l.:..1'\--._,fr.,,__~G-'-"lv, ...... l..__.l<'-'--n~1ti ....... tc __ q'---'-0---,,°""-'-l-f'-+/ ...... !f.....,~,,...,lf-'>-k-=-(h,-../,'-=-/--'-'IN:.....:.......l-{.:;._r ________ PCbwells.(rrn
'I .L LUG-~.H ... Kl:i~T Facility: Warren Cou·ntv PCB Landfill Location: Warrenton
'Purge/Sc.'.Ilp!e Team: 'ir ll-i. L' ~ <;;::t:<~ ,,i G .
' . ' /Ov . _ Comme~s (·}/ell construction, etc):
;J,_-;r,,<.cr'~ dY,?>:>1 ~·0.Gs-~
Conversion Factors: For 2" well: 3 volumes (gallo 0 .5 x height of water column (feetf • ·
Purge Information . '4-_ ;~~ :~i~;~'.: ! ~~~~m~s 1(~~:l~r;:) = 2.0 x height of water colu~;~f~~t{_;;~ ::·~;:
I Well Volume (gal):~. 3 Well Volumes (gal): l-.l, I Purge Equipment: --P4-_ ..... 1....,_· Y.12-"'-_____ +-<--·._
I ,3A..l..oA Purge Time Start: rrrv----'---............ ~-Date Purged: · IO f b-15°1 ----'-+/ ~d..f---Purge Time End: -------
@,· \,~ (Jv, Q. . ..
Did well purge dry? y Actual purge volume:
() :''
..
V0Iu1:1e J2 Volume_/ Volume .1:_ Volume l:J.z, Volume.3_ Volume -
Temp (0 C) •·'/7, 1#~ '90,/0c. Jq, s-~~ ,~. 3 ·\~ (t.'10~
pH ), 37 5. '-f&; 5.&~ S.v1 5. S:2
S. c: oor, .1'. q-5, :L;,0 q3, '.i,lS 1 l '{f,$ q 2. ~)J~
D. 0 . ----· -· -I
l1 Tu,bidity ~ i1fv~ 4 n-ru~ 3nhi<,. J;11M ::Jt1fu')
Sample Information
S · L rio? ample Turn;:---~~---Sample Equipment: --------
Warer Condition (turbidity, odor, etc.): --------------------------
Samples C ol lected(✓):
f omments:
VOCs (2 40 ml vi2.ls)
SVOCs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber botrle)
SC(umhos)·:CJ1.j__ DO(ppm): __ Turb(NTUs): tLnfJS:
----------------------------------
, . -WELL LOG •SHEET Facility: Warren Cou·nty PCB Landfill Location: Warrenton
-. ·-
.. Purge/Sample Team: ::»::a ti ,d/-,t. Sk.n ftk),,/tt,;fb /JLAe,/c4fwell#: _1----'--d--'--f __ _ al
Comments (wel1 construction, etc): ------------------------
ft;' -3S, /
onversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of wa
Purge Information
1 Well Volume (gal): :J.,
Date Purged:. 1vH11
Did well purge dry? Y . N
Volume _{2
Temp (°C) ,.,.
pH
S. C.
D. 0 .
Turbidity
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For hailers: 4 bails = 1 gallon
3 Well Volumes (gal): ,5112:: Purge Equipment: tjn,,m/k ~~ u 1 1·
· Purge Time Start: /Ljz;u Purge Time End: l~-0
Actual purge volume: _£}5~ ·
Iv '\_, \
Volume Volume~ Volume3-Volume
l CC. 0 J<j 1
';J.-b &J. J
/ 1.J. 6 i7-;J
Sample Information
Sample Date: / D Jz<j1 J Sample Time: ___ _ Sample Equipment: _______ _
Water Condition (turbidity, odor, etc.): / S-/ v? 2 // o o ,:J n f"'; I'£!½ 77 Oj ls-UJJ 0 4 ;;)..________
IQS7(aGj LDD r 55? 3 /23S Lj<3Dj /:i='fD; 'f'l:z) 1r'fs:; L/13
Samples Collected (✓):
. Temp(°C):
VOCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
---pH: __ _ SC(umhos): __ _
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)_
DO(ppm): __ _ Turb(NTUs): ---
_________________________________ pcbwclls.frm
-w ~LL LUG SHEET Facility: Warren Cou·ntv PCB Landfill Location: Warrenton
ConversioifFactors: -For 2". well:" 3 volu.riie((g~loris) ~ 05 x height of water ·coluinri (feetf:::r :~~L _ . ---1-~~-.=-:-:····--.;;._ .•. ·._:.-·;·· -·-.. ,--:~;'·--=--=---~-.. .. . . -~--. _ ... ----~:··.·-:c..:..=.~---::;.;.,,;;!--;~~-;.----.:·. Purge Information --. _ . . .. __ · : ··, For 4 \ well: .3 vohimef (gallons) = 2.0 x:height of water column~(feet)'f!':~•u;:;~~• :-_;· ·
. l Well VoluineJgal): . . ' .. 'E,'.J'¥cl1rv~1~~!~i~~r[:Ii~~';:;,¼~eiquip~llt4iti~~;,,: ~ . <
Date Purged;·. , . ~rg~ Time s~L-i:~._/i: _ Purge Time End:.: -~]~I:'Tfff~~t~·::_ -------
Did well purge dry?. Y N ,· _;\c~_al P1:!Fg~ volume: __ · _____ _
. Volume
Temp (0 C) . · •1 t· I t:
pH j . C ,f
s.c:
D . 0 .
Turbidity
Sample Date: -------
Voiume ··.: , Volume .· -~-: ~:., .Volume Volume -··•.-:.· -T"
Sample Information
Sample Time: ------Sample Equipment:
Water Condition (turbidity , odor, etc.): __________________________ _
Samples Collected (✓):
emp(°C):
omments:
VOCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bottle)
Metals (1 1L HDPE bottle)
---pH: SC(urnhos): · -------
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber botrle)
DO(ppm): __ _ Turb(NTUs): ----
r,-__ 5_ .... __,_Le.;_1 _ _..=:~ +_;___/_/_: :.,_)o __ 6 ....>:.'l._..:....l.=..D_-_2.._~_-_~_r _ __:_A,J;:..::..,:____.:..J....:....:__'/_, "1t_1-~...!, ... _-_(---6~~~--'pcbwells.frm
WELL LOG SHEET Facility: Warren Cou·nty PCB Landfill Location: Warrenton
Well#: J;L ----~------
'comments (well construction, etc): LI_.. ---------------
!() : 5.i2' ~.OS'; I'-'
Purge Information
1 Well Volume (gal): I ff-A' .
Date Purged: · / () /.:;f J5c,
I l
Did well purge dry? Y (~)-
Volume 0 -
Temp (0 C) '1 ~ 1 l( CG
pH 5 '6 i
S. c: I ~10. I IA~
!I " -··
. or 2 well: 3 volumes (gallons) = 0.5 x height of watt
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailer~: 4 bails = I gallon
3 Well Volumes (gal): fb JfJ'"y Purge Equipment: !h!;ktf
Purge Time Start: / D ':..;-/f11A Purge Time End: ID~
eJ u,11, Actual purge volume : --A~,-----'--'-'"""''--
Volume _L Volume 2. -Volume 2'/3
17. ( c<: n. '3Cc.., I~, l"c
r·-1 _), -~ s: ~3 5 , 7~
C)S",3 µ~ q4. ~ µ) 9L{.4-')
-· --·
c.'t. .. l'J
Volume..a_ Volume ±.1/2.
l~oL 1'{5\_
'J.12m 5<e~
9~.1 LI) qy,4 ,µ\
,.... -~· -.
Turbidity ,~e t1 tu'> IL{~ ~M ~ (Ith, 1li11h••, ~':>n~ Wntv')
'
Sample Date : (D/i~Lss --+, "'---,,--..,__-
Sample Information
Sample Time: /O~u Sample Equipment: --------
Water Condition (turbidity, odor, etc.): ______________________ _
Samples Collected (✓):
VOCs (2 40 ml vials)
_L SVOCs/PCBs (1 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
,,.1
emp(°C): /~.3°c pH: 5, (p~ SC(umhos): C/9. cf DO(ppm): _-_· _ Turb(NTUs):
f omments: Jvrfmi, ~ .5 hJ,,, t ·f.i y,( /e,)t Mt d.nff'"y
-t:----------------------------------pcbwclls.frm
JAMES B. HUNT JR.
GoVERNOR
WAYNE MCDEVlff
SECRETARY
WILLIAM L. MEYER
DIRECTOR
Mr. Q-aig Brown
Pesticides and Toxic Substances Branch
US Environmental Protection Agency
Atlanta Federal Center
6 I Forsyth Street
Atlanta, GA 30303-8960
Dear Mr. Brown:
m NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
November 1, 1999
DIVISION OF WASTE MANAGEMENT
NOV 1999
'r . ,,.. '"'~'ti
" 'vlilertt · · ·,on
This letter is to document our recent telephone conversation concerning the semiannual
monitoring at the Warren County PCB Landfill.
I reviewed the Notice of Non-Compliance from 1997 and the referenced Letter of
Approval dated December 14, 1981. Neither required that the results of the semiannual
monitoring events be reported to EPA However, this can be done in the future and I will place a
copy of this letter in our files for future reference.
Our records confirmed, as you had indicated, that that state did send you the results from
the monitoring event conducted in November of 1997. Since then four other monitoring events
have been conducted with the most recent occurring October 25 and 26 of last week. The results
of the first three events are shown in the attached table. In reviewing the data, I noticed that the
pH and specific conductance had not been recorded for every groundwater and surface water
sample. I provided the samplers with a copy of the Notice of Non-Compliance that reiterates this
requirement to ensure that all these measurements were taken during last week's event and that
they will be taken in the future. I will send you a copy of the results of the last monitoring event
when the PCB analyses are completed.
In there are any questions or comments, please call me at [phone] ext. 308.
Copy: Mr. Bill Meyer
Mr. Mike Kelly
Sincerely,
Patricia M. Backus, PE
PCB Landfill Project Manager
401 OBERLIN ROAD, SUITE 1 SO, RALEIGH, NC 27605
PHONE 919•733-4996 FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER• SO% RECYCLED/I 0% POST-CONSUMER PAPER
i'
Semiannual Sampling Results
, Warren County, NC PCB Landfill
Mav 18-19, 1998 October 26-27, 1998
Specific
PCBs Conductance
(ppm' pH
Ground Water
1 <0.0001 5.71
1A <0.0001
2 <0.0001 5.84
3 <0.0001 5.21
5(deep) <0.0001 5.71
7(shallow) <0.0001 5.44
. 11 <0.0001
12 <0.0001 5.40
Surface Water
RCUS <0.0001
RCDS <0.0001
UTUS <0 0001
UTDS <0 0001
Sediment
RCUS <0.10
RCDS <0.10
UTUS <0.10
UTDS <0.10
Leachate
Influent 0.0002 6.59
Effluent <0.0001 7.10
RCUS -Richneck Creek Up Stream
RCDS -Richneck Creek Down Stream
UTUS -Unnamed Tributary Up Stream
UTDS -Unnamed Tributary Down Stream
(umhos)
100
100
54
88
72
159
1201
589
Specific
PCBs Conductance
(ppm) pH (umhos)
<0.0001 5.95 1289
<0.0001
<0.0001 5.96 1125
<0.0001 6.36 1217
<0.0001 6.00 1076
<0.0001 5.67 88
<0.0001
<0.0001 5.47 1152
<0.0001
<0.0001
<0.0001
<0.0001
<0.10
<0.10
<0.10
<0.10
0.0004 6.70 1536
<0.0001 6.33 840
April 19-20, 1999
Specific
PCBs Conductance
(ppm] pH (umhos)
<0.0001 6.08 104
<0.0001
<0.0001 5.84 97
<0.0001 6.09 111
<0.0001 6.20 90
<0.0001 5.98 76
<0.0001
<0.0001 6.17 111
<0.0001
<0.0001
<0.0001
<0.0001
<0.10
<0.10
<0.10
<0.10
0.0006 6.82 989
<0.0001 6.68 829
PMS 11/01/1999
.., t
...
MEMO
DATE: March 8, 1999
TO:
FROM:
William Meyer -Director, Division of Waste Management
Harry Zinn -Superfund Section ~J
RE: Warren County PCB Landfill Sampling Plan
On October 25,26, and 27 we plan to perform the semi-annual sampling at the Warren
County PCB Landfill, in accordance with the permit issued by the US EPA. The samples we have
typically collected consist of the following:
1. One deep and one shallow monitoring well located in each of the four sides of the
landfill (eight total).
2. A surface water and a sediment sample from upstream and downstream of the
possible point of entry of site runoff into an unnamed tributary (four total).
3. A surface water and a sediment sample from upstream and downstream of the
confluence of the unnamed tributary and Richneck Creek (four total).
4. A grab sample of the sand filter media and the carbon filter media (two total).
5. A rinsate blank from the field deconning of the pumps ( one sample).
In addition to these samples we will be collecting three discrete surface soil samples from the area
between the inlet pipe and the outfall pipe in the leachate retaining pond on the north side of the
landfill.
NCDEHNR
Division of Waste Management
Organics Lab: /
Inorganics Lab: __
□ Superfund Section
□ Hazardous Waste Section
□ Sol id Waste Section
CHAIN OF CUSTODY RECORD
Project Name: WMul~N Cvl\J 'f1f E._l(Q LIi',; IJ Ftl.i-Sampled By: l:1:--z..,.~""
Site ID # (NCD#) Sampler ID
Location: l)pc(lf/.,2u TblJI_ Telephone:~ z;, "> 2,,<'i o l -v+ 3>i3
Address: Date Sampled: -L,1.,, ('f/;z,:, -q,r
Time Sampled:
Sample Types: Soil ✓ Water ✓ Waste Other ✓ r: 7-k,. /?t~t,~
;,
Remarks: 6 l..o "-1> ~ l> ~ S" ...,"'J n,(1"-e.r m..,J.,:-..,
6.t..'2{:,}~ r1 +-~ c.... ,.,(, ... "\. '4-~-rn~, ~
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Field Sample 6 2-0 c.. 'l--1 6.l..-0£."LL.. C,'l.,.::,·.f>"l.. "":) () 4, 0£, "l.,L( C>l-0(..'l...-) 6'l.-o~-z...-~ 6LDip_?-.7 I
Numbers 6Lt> 6:z..~ 6=t-O&l..4 b 1.-o'-"3v O"L.o'=, ") j o-i.,,.o b 3"2... 6\....~<o.]"3> O'l.,._oG.~
C.L.-Ob"3', c.'l..<> b) l.. c,"l,,o '->] O"'l...-<=>G.)6 01..-06~1 O~<=>b4~
Relinquished By: ·"k✓-. (__,__:;_ Date: t:f--21-11 Time: /1:/S-, ~ -
fSionature) ?-'
Received By: --y'k,_/Z-:, ,.J" if~ Date: IJ-»--IJ!I Time: ////S ---
(Signature)
Relinquished By: Date: Time:
rs i s:>nature)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
fSi onature)
Received By: Date: Time:
(Signature)
--------Results Reported / IL/?~~ -Date: .y / 7 --? 9 Time:
c~#ii-e'(I
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(I :\docshare\cocr.frm)
!''..C,-i)cpartmcnt of Environment,
I li :•}i11, & Natural Resources
So!i.\ W,1stc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field Sample Number; :: ·• O.L.O .6 ".2._ .I -------------------------------
Name of Site UJAf<.R.f.N Guf\JN Peg LA,MDP 11st'c Location_W~-~-'--'--'-(t~··t!:~W_· ...... Jb_,J_. ________ _
Collected By J.J.. 2, ,,.y,J ID# ___ Date Collected · 4-1,,D '-f\')·· ·
Agency: Hazardous Waste · Solid Waste _____::::::_ Superfund
Sample Type
Environmental Concentrate Comments
✓Ground water (1) Solid (5) mw I
__ Surface water (2) ~Liquid (6) ___________ _
Soil (3) _ Sludge (7) -------------
Other (4) _ Other (8) __________ _
Organic Chemistry Inorganic Chemistry
·I. Para1:1eter ResuJte(mg/1) I -P&T:GC/MS
Parameter Results(mg/l)(mg/kg)
! Acid:B/N E;:!.
MTBE
. ✓ 'p.c,f'~--< o. o '"' I
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
F1uoride
!ron
uad
I __ hianga~cse
__ Mercury
I: ·-______ ______ Nitrate
Sdcnium t-·· , I Siiver l Radiochemistry = Sulfates
Ii•····-.. •··--• ----------, Z;nc
, Pi!rume,:, Results (PCl/1) i --pH
':rc:-:s . .c..iph~ ! --Co:1ci:1ctivity ·--,---------j ___ TDS
•. TOC ,-------, ___ _ Microbiology
;-···•·····•---,--·-·----·-•··----·--·-----7
i i-'aranidcr Ri:sails (Co!,iJOOml) i --. ' •-------! ---________ i
I ,-1 -----------------. i I
-------
----·---
----··-·--
· .. :-;~: ~:.::,TCLP Compounds
Inorganic Compour:ds
Arser,ir
B~ium
Results(mg/1)
-~~ E i \J,...,' E_.,....8-,------
Lead = Mer(MY 1 9 1_.9-..99.,__ __ _
Selenium = ~FtRFUND SE .... :C:;...;..T.;....10_\\' __ _
Organic Compounds
benzene
carbon tetrachlorici::
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichiorobenze'le
1,2-dichloroethane.
R1:mlts(mg/l)
----
------
1, 1-dichloroethykr. ~
--2,4-dinitrotoluenc ------
__ heptachlor
hexachlorobenzer.e
hexachlarcb~tadien~
hexachlo:roethanc
methyl ethyl ketc:',e
nitrobe!lzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethyl,.ne
__ trichloroethylene
________ ,,
------
2,4,5-trichlorophenol
--2,4,6-trichlorophenol ---~~~~----_-_-_-_-
~--vinyl chloride
endrin
lindane
Dat c Received '-/-;). J-q 9 17 d ~~21...:~~~-::::--:.. --~....-~"-'-methoxychlor
PCB {/1,f~ _ -_ tGxaphc~e
DJlc Extractc.:<l Lf _:.2:?-Yf'J(t.JJ/ Date 5'-/7 -t:j' q--u-2,4-D
f'C8 r.A1JV7. !)91238 _ 2,4,5-TP (Silvex)
Daic Analyzed ~-A6-9 Yi Lab Number
i)I IS 3191 (Revised 2/91) ~eq S-1 /.ffiBfJ. -#--+-->1~1--1-~-3...,,_-f,..----71r-=71 ' ~S:-----7-6--_ -_-_--:_-_----~---------'
N.C Department of E11vironment,
l lcoll'h, & Natural Resources
Solid ·waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number :.: Field Sample Number . . 61..-o ,.'2....1---------'--------------------------
Name of Site UJ A (lR.f:_N GvNN . p CB LA--tJDP 1'sft'e Locati~n_·~W_M-'---'-R.~t!:~W~Tb_Al ________ _
Collected By lJ-2, ,,.y·,J ID# ___ Date Collected · 4-J.a ·-'t 5
Agency: Hazardous Waste . , · Solid Waste ----=::::_ Superfund TCLP Compounds ----..
s~mple Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
V Ground water (1) yn l,.) iA --Solid (5) Cadmium ---
~Liquid (6)
Chromium --__ Surface water (2) Lead --Mercury
Soil (3) _ Sludge (7) --Selenium .;
--Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parameter Re:;ults(mgfl:· Parameter Results(mg/l)(mg/kg) Organic Compounds Resul~(mg/1)
_P&T:GC/MS Arsenic bt:nzene ----Acid:B/N Ext. Barium .::.:.rbon tetrachloride ------MTBE Cadmium chlordane
✓ PC£ ----<o. ooo/ .nn..l Chloride chlorobenzene -----,, Chromium chloroform ------__ Copper c,-cresol ----F1uoride rn-cresol --------__ ___. Iron __ p-cresol --Lead cresol ------j-v --__ Manganese 1,4-dichlorobenzene ---,.• .. · __ Mercury 1,2-dichloroethane --,, . --... -Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ------······-··---· Zinc heJG:chlorobutadiene ----Parnmeter Resclts (PCi/1) _pH hexachloroeth2ne --__ Gross Alpha --Conductivity --methyl ethyl kerone
Gross Beta TDS nitrnbenzene --------------·--· TOC __ pcl1tachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
•--__ trichloroethylene
Para,neter Results (Col/!OOml) I __ 2,4,5-trichlorophenol
----2;4,6-trichlorophenol
--vinyl chloride ------endrin --lindane
4-J.J-qq nd --Date Received Reported by methoxychlor --,Pee ('A:SV~ --t~x~phene
Date Extracted L/-,2.3-'7fT6$ Date Reported --2,4-D
/'C,8(M~ 991239 _ 2,4,5-TP (Silvex)
Date Analyzed 'f-~-9?'Y/' Lab Number --Dl lS 3J<Jl (Revised 2/91)
N.C Department of E;;vironment,
I Jcal:h, & Natural Resources
Solict'Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number ---------------Field Sample Number.·. . 0 ,-i_D, b ")._. "3.
UJ r p -p1U-· · · ·
Name of Sile A (?.R.f_N \...()UflJ]Y · CB LA-tJD Site Location_. -=-LJ----"-M_.__-'-'lt=e:=-'-W'---'--]b-'--IJ _________ _
Collected By lJ-2, ,,y,J ID# ___ Date Collected ·, 4-1 -'l '-.fV\: Time I 'I,' 2<{
Hazardous Waste
..
Solid Waste · V Superfund ·,: ···.-: :. ·, .. TCLP Compounds Agency: -- ----,.
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium
✓Ciround water (1) Solid (5) /Y) lJ 1.:. Cadmium·· --
~quid (6)
Chromium --__ Surface water (2) Lead --__ Mercury
Soil (3) _ Sludge (7) Selenium ., --Silver --_ Other_(4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parameter Resolts(mc/1) Para~;eter Results (mg/I)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ----· --Acid:B/N Ext. Baritim carbon tetrachloride -------' ···---MTBE Cad:nium chlordane
-✓ -··· --. Pc..B <t:J,000/~&t Chloride chlorobenzene ---.. Chromium chloroform ------__ Copper o-cresol ----r1uoride m-cresol ·---· -------Iron __ p-cresol ---;'":! Lead cresol --·-... +. ----.;:" __ Manganese 1,4-dichlorobenzeut.: ------:-,-.,-----•."H __ Mercury 1,2-dichloroethane: --'.,\. ~itrate = 1,1-dichloroethylene ... ,: . ----Selenium 2,4-dinitrotoluene --·-Silver __ heptac!ilor -----Rt.diochemistry Sulfates hexachlorobenzen~ ----••••••-•••---•-••---•a--Zinc hexachlo:-obutadien:: ----l'aramder !~esu!t.5 (PCi/1) _pH hexachloroethane ---__ Gross > ipha _ --methyl ethyl ketor:c ! . 1--Conductivity
Gross B:ta TDS nitrobe:13e:1e -------·-1 I TOC __ pentachk,rophenol --
--__ pyridine
Mkrobiology --_·_ tetrachloroethylene
--· __ trichloroethylene I --I Parl:lmeter Results (Col/"JOOml) __ 2,4,5-trichloropheno1 I --__ 2,4,6-tri::!:-Joropheno! I ----I
__ vinyl chlcride I ----endrin --lindane
Date Received 4-cJ.) 4 q Od Reported by --
--methoxychlor
rPC8 ('Afsot} __ tc~aphene
Dale Exlrac!c.:<l L/ ;2.J--9'f'YP_fl'( Dale Reporled --2,4-D
r'MtAI~ 391240 --2,4,5-TP (Silvex)
Dale.: AnalyLc.:d l./-~ 6-91/r' Lab Number --I I)! IS 3 191 (Revised 2/91)
N.C. Department of Environment,
I ka)th, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number ---------------Field Sample Number · , 01-o , ~ l., t./.
___ ,e._ __ =-=.=---------
Name of Sile (J} AB-~N GurvN p CB LA-,JOf 11str'e Location_W-"'--'-MJ-.,___,_R.=e:=W.;...-L.Tb.;;...IJ ________ _
Collected By ----------ID# ___ Date Collected __ . 4_._--'-19....._·~_'t_j__,__· .. __ ., ._,._. ·_· Time_~f _l:-L~O~--
Agency: Hazardous Waste Solid Waste · vSuperfund
--.·I·-
Sample Type
Environmental Concentrate Comments
✓Ground water (1) Solid (5) rnw ~,.,
__ Surface water (2) ~Liquid (6) 7 _Soil (3) _ Sludge (7)
_ Other.(4) _ Other (8)
Organic Chemistry
. Parameter Results (mg/I)
I P&T:GC/MS
: _ Acid:B/N Ext.
' MTBE
-✓ PC-8
I ------------·--!
! '--------
!
' . ~.;b ! _____ ,_, ___ --------
t ~~~-! -_;··
I t-------------·-
! Radiochemistry
i ~ ·····-· ----·------·----j
; Parnmeter Resul~ (~· 2!/1)
, __ GroE.s Alpha -------' Gross Beta
'
! l i Microbiofogy
Inorganic Chemistry
Par::meter Results(mg/l)(mg/.kg)
Arsenic
Eari~-n
Cadmium --Chloride·
Chromium --__ Copper
Fluoride ·.
Iron --Lead ----------__ Manganese
Mercury
--Nitrate
--Selenium
Silver --
Sulfates
Zinc --_pH
__ Conductivity _______ _
TDS --TOC
· '. ·. ::: TCLP Compounds
Inorganic Compounds
Arsenic --Barium --Cadmium -
Chromium --Lead
Mercury
--Selenium
Silver
Organk Compounds
benze:-:.~
carbon te~rachl0ride
Results(mg/n
.·,
Results (mg/!)
---------chlordwr.-
i
--chlorobenzene -· I
o-cresol 1
chl0rvform
m-crcsor · I =-~-_ p-creso! -------_-
1
l
cresol ----1,4-dichluroben2.ene
__ 1,2-dic:-iloroethane ------_-_ j
__ 1,1-dichlorocthylene , j
__ 2,4-dinitrotoluene t
__ heptachlor
hexach!orobenz.ene -------hexachlorobut:::.diene ---------hexachloroethanc ----------' methyl erhyl ketone i
--n:trober.::'.:.ene --===--~=----------! = pentachlorophciiol j
_ pyridine I.I
__ tetrachloroethylene 1
f i Parameter
!
Re~ults (Col/100ml)
I __ trichioroethyiene I -------1 2,4,5-trichlorophenol I
--2,4,6-t:-ichlorophe~o! ------! I I I
------
Date Received '-/-J.. J -q q :17dReported by ________ _
f-'_eB(Af~
Date Extractr.:.J/./-~3:-ffVp..,J,/ Date Reported PCLJ ~ " ---,,,,,-S9....,...,1--=2=--=4,--1-
Dalc Analyzr.:.d ~--'.~-9'fYI' Lab Number ----------1)1 IS 3191 (Revised 2/91)
--vinyl chloride ·· ! ------1 endrin ,
=== lindane ------1
__ methoxychlor ------1
~o;;:aphc:1e
2,4-D = 2,4,5-TP (Silvex)
' i
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N.C. Department of Environment,
I iclllih, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
. i' '"1
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number ---------------Field Sample Number<: , · · .<:''it--o (, ;LS"°
Name of Site (J} Af?~N Gu(\.{11( p CB LA-,JDP 11st"'e Locati~~--w.:::..·· _· ·.:_~_,_' _,_tt=e::=w'-'-' ..... Tu~"'---------
Collected By JJ-2, ,,.y,J ID# ___ Date Collected .. ,·l.j-l,'1 '~fl-j -Time /S:'(S
Agency: Hazardous Waste Solid Waste ~ Su~erfund ·;J ,_· ...... TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
✓Groundwater (1)
Barium
() LJ S"·. --Solid (5) Cadmium ---
-tqllld(6)
Chromium --__ Surface water (2) Lead --Mercury
_Soil (3) Sludge (7) --Selenium \ --Silver --_ Other.(4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter , Results(mg/1) Parameter Results 1;".1g/l) ( mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ------_ Acid:B/N E;...:. Bari~m carbon tetrachloride ----MTEE Cadmium chlorciane
-✓ PCB ----------<O, "OO/,a,-,AC Chloride chlorobenzene -----,, Cbrcmiilnl chloroform ------Copper o-cresol ----F1uoric;.:: --m-cresol -------
~ Iron __ p-cresol ----->'f Lead cresol ------
--:.,:,~ ~ . -----__ Manganese 1,4-dichlorobenzene --
--~ __ Mercur; 1,2-dichloroethane
Nitrat~ = 1,1-dichloroethylene ----Selenium · 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry· Sulfates hexachlorobenzene ----··•···-··---Zinc hexachlorobutadiene ----P,mtmeter Results (PCi/1) _pH hexachloroethane -----__ G!·oss Alph.:: __ Conductivity --methyl eihyl ketone
Gross Beta TDS nitrcber..zene ··• ~-------·---------··-TOC __ pentachlorophenol --
--__ pyridbe
Microbiology --__ tetrachloroethylene
----trichloroethylene
?aramder Results (Col/iOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----_· _ vinyl chloride
endrin --lindane
D<ite Received 4-;l_/-q9 7kJ Reported by --
--methoxychlor
PCB(if1$oi!:} ...... V'\.,...1-.o.,.P __ 1.VAup••'-"'''"-"
Dale Extracted ,¥-_zj'-~JNDatc Reported --2,4-D
/JCB(/11.SO? . 991242 --2,4,5-TP (Silvex)
Date Analyzed (f-~7-1/trVP Lab Number --DI IS 3191 (Revised 2/91)
r l I '
I
N.C. Department of Erivironment,
I lc:ilih, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
i' · ..
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field Sample Number · D 1.J,.o. (,, .Z.,,b -------------------------------
Name of Site 'JJ AflR£N
Collected By IJ-211,YtJ
Curvw p cg LA-,JDf 1~e Location_W~· _frp,----'---'-'ft'---'e::~J,,J~Jb~· _,J ________ _
ID# ___ Date Collected_,_4......_-_;I=--".,_· '_-_ft_-j-'-'• _ _. _ _.·_. __ Time_--"-/_,_;--'-/=) __
Agency: Hazardous Waste · Solid Waste ~Superfund '' : , TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/ Ground water (1)
Barium /VI (.J l --Solid (5) Cadmium---
~iquid(6)
Chromium --__ Surface water (2) Lead --__ Mercury
_Soil (3) _ Sludge (7) Selenium ·l --Silver --Other (4) --,.,. _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parameter Results (mg/I) . Parameter-Results(ng/1) (mg/;,g) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----__ Ac:d:B/N Ext Barium carbon tetrachloride · -------------MT3E Cadmium chlordane
✓_p~ <:o. ooo{~ = Chloride ·---chlorobenzene --· Chromium chloroform --[= Copper --
-· o-cresol ----Fluoride m-crcsol --
-----:r. i · Iron __ p-crcsol
•,:· 1-Lead cresoi --1----,; I __ Manganese 1,4-dichlorobenzene --~: -----., , Mercury 1,2-dichloroethane --~ -.. j = Nitrate = 1,1-dichloroethylene --1--Selenium · 2,4-dinitrotoluene --Silver __ heptachlor l ·-Radiochemistry ' Sulfates hexachlorobenzene !----·········-------·· ~ Zir.c hexachlorobutadiene --Par.tme!er Result£ (PCi/1) . pH hexachloroethane ! --Conductivity --G:-css Al,!ha methyl ethyl ketone ---1 ----
' I
I . ;
i TDS -------i--L.; :-oss Ber::. mtrober.~ne _______ !
1----------------(1--TOC
Microbiology 1=----------------
Paramtkr Results (Col/ltlOml)
Date Received 4-J /-C/,q 17,1 Reported by ________ _
ft'-8 ( ,tf"S"OiO
Dale Extractcc.14(-..z.?-9o/V§L--;v'Datc Reported~~------
/JC-8~~~~ 991243
Dal e AnalyLcd ¥-.ol?:1"11/P Lab Number ________ _
DI IS 3191 (Revised 2/91)
pentachlorophenol = pyridine
__ tetrachloroethyle1'e-
--trichloroethylene
------
__ 2,4,5-trichlorophenol _____ _
2,4,6-tricl-Joropheno! = vinyl chloride
endrin
lindane
methoxychlor
__ toxaphene
2,4-D
_ 2,4,5-TP (Silvex)
i
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I f I i I ! i i
N.C. Department or Environment,
I Jc;i.lih, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number · ---------------Field s~~mple Number.,.. .c:; 1-0 ( ~ 1 -------..c:.---=--..:..-------
Name of Site UJAB.Rf.N Gutv]y PCB LA-tJDf1'st'e Location_····=W~~_,_·· _,_f{-"-·=e::.:.:..f.l_.Tb...::..;.;:N ________ _
Collected By lJ-2, ,,.y,J ID#_· ___ Date Collected .· 4-1:.0 '-ft-5, , · Time q: 'fS
Ageng~ Hazardous Waste Solid Waste ~ Su~erfund '.: ;. ., , .... · .. · TCLP Compounds ----·-
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
_!{'Ground water (1) I t --Solid (5) (nW Cadmium -
--Chromium --__ Surfac~. water (2) 1iquid (6) Lead --Mercury
_Soil (3) _ Sludge (7) --Selenium .,
--Silver --_ Other_(4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parameter · Results (mg/I) Parameter Results(mg/1} (mg/kg) . Organic Compounds Results(mg/1)
__ P&T:GC/MS Arsenic . benzene j ·---I --_ Acid:B/N Ext. Bariure carbon tetrachloride ----· MTBE Cadmium chlordane -✓ PGB <0.()011/,-. -----·--· ¥ Chloride chlorobenzene ----,, Chrominn chloroform ------__ Copper o-cresol ~~ :---Fluoride. f-m-cresol --Iron __ p-cresol ----Lead crcsol ------_-__ -t,-__ Mangau::.se 1,4-dichlorobenzene --·----
----Mercury --1,2-dichloroethane
--Nitrate I __ 1,1-dichloroethylene --Selenium I 2,4-dinitrotoluene I --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----...... ~.----· Zinc h::xachlorobutadiene ----P2.rarnelt!r R.esu!t~ (PC!jl) _pH hexachloroeth2ne --__ Gross Alpha ! __ Conduc~;•:ily --methyl ethyl ketone
Gross Betz. . TDS nitrober.zen~ --------TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
·-__ trichloroethylene --P~rameter Results (ColilOOm!) --__ 2,4,5-trichlorophenol
2,4,6-trich!oropheno! ------vinyl chloride ------endrin --
Date Received J../-;;J./-99 fl's.1
lindanc --Reported by --methoxychlor
A±s~ __ !cxapher:e
Date E>lrnctcd E-V~ Dale Reported --2,4-D
991244 _ 2,4,5-TP (Silvex)
Da tt: Analyf:.ct(!,. ~7-99Jl'P Lab Number --DI IS ]191 (Revised 2/91)
I
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N.C. Department of Environment,
I lcalil-1, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number · Field Sample Number'::· OJ...,o ;' "L-'& ·, ---------------------------------
Name of Site llJ A(?~N
Collected By IJ-2, ,.y',J
Gul\,{Ty -PCB LPc-MDf11st'e Locati~n_·_W;:;;..._;MJ-c......:..._..:....;/{,=·e:="'--'JbL.....;;......;,J_· __ -'_· ' ____ _
ID#_· ___ Date Collected ·" Y-1 "I '-.'l J .•,.
Agency: Hazardous Waste
Sample Type
Environmental Concentrate
_ Solid (5)
/J(_yiquid (6)
Solid Waste · · VSuperfund --.,.
Comments
J Ground wal'!r (1)
__ Surface water (2)
Soil (3) ; ~ludge (7) __________ _
Other (4) ---Other (8) __________ _
Organic Chemistry Inorganic Chemistry
I
_ Parameter Resclts(mg/1)
_P&T:GC/MS
Parameter
Arsenic:
Results(mg/l)(mg/kg) I
1
__ Acid:B/N Ext.
' MTBE
✓ PC-8 <~. tlOO/.n~ ,,
-------------
Radiochemistry
--····-··--------------t I P..:r-umeter Results (PCi/1)
· Gross Aipha
It. --G --------ro~.s tleta ·---------------
Microbiology
,--------------
Parameter Results (Col/100ml)
-----,-
Uariui;r; --Cadmium --------··-·--Chlc:£de
Chromium ----Copp~r
Fiuoride
!ran·· --Lead
____ Mangc1nesc
__ .·Mercury
Nitrate
Selenium
Silver --Sulfa~~s
Zinc --_pH
--------
------·-
-------
__ Conc.iu;:-tivity ______ _
TDS --TOC
Date Received 4-;J. /-C/Cf 1/;J Reported by
/Ji~'A1soi:> ------
Date Exlraclc<l ~~Jlv"Dale Reported _______ _
Dale Anal~ -, ~p Lab Number 99l245
DI IS 3191 (Revised 2/91)
:;i: : ..... :·TCLP Compounds
Inorganic Compounds
Arsenic
Barium --Cadniium -
Chromium --Lead
Mercury
--Selenium
Silver
Results(mg/1)
I•, •. · •' ·)
Results(mg/1) Organic Compounds
benzene
--carbon tetrachloride i ---------chlordane •
--chlorobenzene
chloroform
o-cresol
m-cresol
--p-cresol
--cresol ----1,4-dichlorobenzene _____ _
1,2-dichloroethane
--1,1-dichloroethylene i
_ 2,4-dinitrotoluene ------i
__ heptachlor •
hexachlorobenzene I
--I hexachlorob::tadienc 1 === hexachloroethane _______ ,
__ methyl ethyl ketone ______ 1
nitrobenz.~ne i
--pentachlorophenol ------i = pyridine I
__ tetrachloroethylene
trichloroethylene j
--2,4,5-trichlorophenol i
--2,4,6-trichlorophenol ------I = vinyl chloride · i
endrin
iindane ----methoxychlor
__ !c~aphene
2,4-D = 2,4,5-TP (Silvex)
------1
I
N.C. Department of Euvironment,
I lco,Hb, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number· · Field Sample Number :Q 1....0 l "--9 -------------------=------------•• ! 'r ..
Name of Site (J) A R.RE-N GuftJN p CB L,\1..IDf 11st'e Location_W-'--· _MJ-""---'-R.-"-'e:~t.J-'----'-Tb_N ________ _
Collected By JJ.-2, ,.,,i,J ID# ___ Date Collected · 4-1 q ·-fl.J .
Agency: Hazardous Waste Solid Waste ~ Superfund ~ TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
tl,~ ~ ~-k..· Barium
__ Groundwater (1) --Solid (5) Cadmium---
-~quid(6)
Chromium
__ Surface water (2) --Lead --Mercury
_ Soil (3) _ Sludge (7) --Selenium --
✓Other (4)
Silver
_ Other (8) --
--
--
--Organic Chemistry Inorganic Chemistry ---
. Parameter Results(mg/1) Parameter Resc!ts (mg/l)(mg/kg) OrgBnlc Com!•ounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----_ Acid:BjN Ext. Bariuc r.arb,)n tetrachloride ----· --MTBE Cadmium chlordane
✓ Pc.,B ----chlorobe;zene -< 0 • 0001.f!f'AI Chloride --· --Chromium chloroform ------
--_·_Copper o-cresol --Fluoride· m-i::resoi ------· -Iron __ p-~resol --~~~;-· --Lead crcsol ----i ---.;:· __ Manganese 1,4-dichlorobenzene .: . --,•• I --··-·.:-• __ Mercury 1,2-dichloroethane --';·: ..
Nitrate = 1,1-dichloroethylene ----. Selenium 2,4-dinitrotoluene --= heptachlor . Silver ---· Radiochemistry Sulfates hei::achlorobenzene
l ...... _ .. _ --I ---Zinc hexachlorobutadi:::ne I Parameter --Results (PCi/1) _pH I i __ Gross Alpl12 I = ~~;ductivity I
I Grass Bern.
I
-· -TOC --
--Microbiology --I
Parameter Results (Colj lOOml) I === ___ _
Date Received J../ -;J)-qq "(/2j Reported by f'CBt/t-1.wv -------
Date Extracted 4' _.:..23-'fJ1/6u#Date Reported _______ _
f'C/3 {MsOV. 0 91,:,,,.. 6
Dal t.: Analyzed Jf-.::Z7-9/.f Vr' Lab Number ~ -~..._
D I IS 3!91 (Revised 2/91) ---------
! ! . . ;
--hex.ach!oroethane --
--methyl ethyl k~tone
r.i~:-cber..zene. --__ pentachioropl.enol
__ pyridine
__ tetrachloroethylene
_ tnchloroethylene _ I
_2,4,5-trichlorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindane
methoxychlor
tc~aphene
2,4-D
_ 2,4,5-TP (Silvex)
'-----------------~
I
N.C: Dcpartm~nt of E~vironment,
I lc:,llh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number · Field Sample Number · ·. @:WO b ,> :?, ---------------__ __,,.::......:;.......=.....=----------
Name of Sile UJ ARRE.N GvNN p CB LA-?JDf 11st°e Location_W=--"-Mi..,_· _,_ft-=e::=W'-'--LJb-"---'-,J ________ _
Collected By I.J-2, ,,1,J ID# ___ Date Collected · 4-1 ·1 ·-~ ~ ,Time ------
Agency: Hazardous Waste Solid Waste ~Superfund .. .... ·:..:. TCLP, Compounds ----
Sample Type foorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
_hGround water (1)
. Barium
Q, C-U 5 ---Solid (5) Cadmium --
_{surface water (2) ,,'.~ttu;d (6)
Chromium --Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium \ --Silver --_ Other (4) _ Other (8) --
----Organic Chemistry Inorganic Chemistry --
. Parameter Results(mg/1) Parameter-Results(mg/l)(mg/kg) : Organk Compounds Results(mg/1)
I _P&T:GC/MS Arsenic --__ Acid:B/N fa.t Barium . --MTBE --Cadmium
✓ PC-8 <o.ooolq,'!l----Chloride --,-Chromium ----
--__ Copper
Fluoride -----Iron ---------Lead ----
--__ Manganese .. __ Mercury ,. --Nitrate ----Selenium --Silve: --Radio.chemistry --Sulfates
······-·· Zinc --Parameter Results (PCi/1) _pH
__ Gross Alpha __ Conduclivity
Gross Bet:i. TDS ----TOC --
--Microbiology --
--Parameter Result~ {Col/100ml) --
----
----
Date Received 4-.J _q91/.::f Reported by
PJ.8(~
O;itc Extracted lf:-2'-f'lYtJ7/oatc Reported _______ _
Dale Analyt:~;r~ Lab Number 9 91247
DI IS 3191 (Revised 2/91)
benzer.:; --t. carbcn tet:·ach;oride , . --. chlo:-dane --;
!----chlorobenzene
chloroform
i ,.
I i I
I !
I
I
i I
I I ' !
i
--o-cresol ---m:.crescl
n-cresol --· cresc,l --· 1,4-dichlorobenzene --1,2-dichloroethane --1, 1-dichioroethylen:;
2,4-dinitrotoluene = heptachlor
hexachlorobenzene --h~xachlorobutadiene --hexachloroethane --
--methyl ethy! ketone
nitrcbenzen~ --·-__ pentachlorc,phenol
__ pyridine
tetrachloroethvlene --., __ trichloroethyiene
__ 2,4,5-trichlorophenoi
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin --lindane --
--methoxychlor
__ tc;:aphene
2,4-D
__ 2,4,5-TP (Silvex)
--
-···.
--
--
~~-'
--
---
-
N.C: D_cpartmcnt of En.vironment,
1 lcattlr, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field Sample Number ·.: 62..o b~ I _____ .;;:;....;; _________ _ ---------------
Name of Site (JJ A R~N G UA,(fy p CB LA-,,.u)f. 1'tte Location_w=-·· ---'-~-'-'-R.-=.;e:=-J,J'-'--'-7b~,J ________ _
Collected By lJ-2, ,,,i,J ID# ___ ·-·_-Date Collected · Y-14 '-~-~-Time ------
' TCLP Compounds Agency: Hazardous Waste Solid Waste -~Superfund :.-. ' --
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium R.,cns ---Ground water (1) _ Solid (5) Cadmium ... --
/ Surface water (2) ~Liquid (6)
Chromium --Lead --Mercury
Soil (3) _ Sludge (7) --Selenium ·,
--Silver --_ Othe~_(4) Other (8) ------Organic Chemistry Inorganic Chemistry --
_ Parameter Results(mg/1) Parameter Results(mg/i) (mg/kg) · Organic Compornds Rest•lts(mg/1)
_P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Ba:-ium carbon tetr,·:cLlorici:: ----MTBE Cadmium· chlordane
~ PcB <O• ooo/ .f?f.A ----Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol -·-----
--Iron __ p-cresol --I-...:. Lead cresol --------"(:_' __ Manganese 1,4-dichiorober:zcn..: ----t· __ Mercury 1,2-dichloroe~•,ane --= l,l-dichloroethyle:1-; --Nitrate --Selenium · 2,4-dinitrotolue.ne. --= h:.-:ptachlor Silver --Radiochemistry Sulfates hexachlorobenzene --······-··
I L
I ,--Zinc h,:.xachlorob~tadic::~ -I --P,:!r,im,.ter Results (PCi/1) -pH I hexacL'.0roethane
Gross Alµha -------Gross Bet:i.
Microbiology
Conductivity
TDS
TOC
I -------. ----·--·--!
--
--methyl ethyl keton~ --n:trober..zen~ = pentachlorophcno:
__ pyridine
--tetrach!oroethylene
trichloroeth iene -y
Parameter Results (Col/lOOml) _______ ' __ 2,4,5-trichiorophenol _____ _
__ 2,4,6-trichlorc:phenol _____ _
vinyl chloride
endrin
iindane
Date Received L/-J /-9q 77d Reported by ________ _ methoxychlor
(JJ ~ { M soy-_)
Dale Extracted q-.:z.,-if"l]t.:e'Datc Reported~9...,_ '9~1 ... -4=-r,~~~-aJ..--
(FC,8{M~ ~ ....
Dalc AnalyLed l/-~Y-9'91'P Lab Number ----------
2,4-D
_ 2,4,5-TP (Silvex)
1)1 IS 3191 (Revised 2/91)
I
I
i
N.C. Department of Environment,
I lca!1h,, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS. REQUEST State Laboratory of Public Heallh
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number · Field Sample Number · 0 L 8' ;3 2--.. ---------------___ ..;._ ____ :---------
Name of Site (.)) A (?Rf.N GvNN p CB LfttJDf 1'stte Location_;::_w---'-~-'---'-R.,=e:=>J'-'----'-Tb..;:;..·...;;.·~-" ·_··_· .. _. _ .. :._· · ____ _
Collected By JJ-2, r,,Y-,J ID# ____ Date Collected 'Y-1·1 ·-ft.4,. : ' j , '•n,:Ti-me _____ _
Agency: Hazardous Waste ----Solid Waste ~ Superfund ' , :_,. 1. i c : TCLP· Compounds
Sample Type Inorganic Compoun~ Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium --__ Groundwater (1) Solid (5) UTU.5 Cadmium ---Chromium
VSurface water (2) ,quid(6)
--Lead --Mercury
Soil (3) _ Sludge (7) --Selenium ',
--Silver --_ Othet(4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parn"1eter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Rest•Jts(mg/1)
_ :t·&T:GC/MS Arsenic benzene ----__ Acid:B /N Ext. Barium carbon te~rachloride --------··-·----MTBE Cadmium chlordane
~-✓-PC-8 --------------::-o. Ot:>Olh>AA Chloride chlorobenzene ----II Chromium chloroform ------
·-__ Copper o-crcsol --Fluoride -m-cresol --------
--Iron __ p-cresol --.' Lead cresol --------
--.:,: __ Manganese 1,4-dichiorobcnzene --:.· __ Mercury 1,2-dichloroethane --.. ., Nitrate = 1,1-dichloroethylene ----... Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene -----------r .. ~::;ameter Zinc hexachlorob,, tadiene
P.esults (PCi/1) ----_pH he~chloroetham.; I Gro:;s A!pha __ Conductivity = methyl ethyi keton'! I ---Grc:::s Beta TDS nitrnber.zene . ··-----·-..---TOC __ pcntachioropheno: --
--__ pyridine
Microbiology --__ tetracr.loroethylene
--__ trichioroethyicne
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenoi
I 2,4,6-t:-ichlorophencl ------vinyi chloride ---
------endrin --lindane
Date Received if-;;J. I-99 1ld --Reported by methoxychlor --/J<!.i~ (/11~ tf"'\V">...,&.,~.,..a, --1-v,..upa.•w•rw
Date Extracted Lf-~~-f1'Jl'/'vA("Datc Reported --2,4-D
,'~j-f.,#1.~;;, 991249 _ 2,4,5-TP (Silvex)
DJlc Analyzed 'l-,,,?.'g-'19l(p Lab Number I DI IS 31')1 (Revised 2/91) --
I
! I i
I I
N.C. Dcpartm~nt or E~vironment,
I Ic;;i°th, & Natural Resources
Solid Waste Management Division
Site Number
SAMPLE ANALYSIS REQUEST State uboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Field Sample Number · .0)._o,(:, "J ~ -------=----------.. / p LL-.
Name of Site UJ Af?Rf-N ~UrvN CB LA?JOf 1 Site Location_l,J=--· _.;_M..:........:...ft=e::=W-'--'-Tl?~IJ ________ _
Collected By IJ-2, ,,y',J ID# Date Collected 4-1 q -'t j Time ------~-----'--'----..______ -------
Agency: Hazardous Waste --Solid Waste ~ Superfund ... TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium v-, 05 ---__ Groundwater (1) _ Solid (5) Cadmium --Chromium ✓ Surface water (2) --
t4uid (6) Lead --Mercury
_ Soil (3) _ ludge (7) --Selenium .·,
--Silver --_ Other(4) _ Other (8) --
----Qrganic Chemistry Inorganic Chemistry --
. Param~~er Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_ P . .:::T:GC/M;:; Ars~nic benzene ----__ Acici:3/H :Cx::. Barium carbon tetrachloride i --·-MTBE Cadmium chlordane
✓ PC\3 --------
< "· 000/ £JO;t{ Chloride chlorobenzene ----I, Chromium chloroform ------
--__ Copper o-cresol . ·---Fluoride m-cresol --.... ----· --
--Irc:i __ p-cresol -·· --,, Lead cresol ... ---· ----•'<' • __ Manganese 1,4-dichlorobenzeoe --... --;>,: __ Mercury 1,2-dichloroethane --
--Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluenc ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobe!"'zene; -------······-·--·-Zi.ic hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane r ----__ Gross Alph2 __ Conductivity i methyl ethyl ketone i --I G,oss 3::ta TDS nitroben:xne --·· ·-·.·---------· -·-TOC __ pentachlorophcnol --
--__ pyridine
Microbiology --__ tetrnchloroethylene
__ trichioroethyiene --P,H"amettr Results (Cul/lOOn1l) __ 2,4,5-trichlorophenoi ! --_ _I -----2,4,6-trichloropheno! ·
--vinyl chloride · I ------I endrin --lindane I
Date R eceived 4-JI-q 17.:J Reported by --I methoxychlor --✓ tn -,,,...hPnP tP $5-[/1-1:s::T~
Dale Exlraclc.:<l lf-~-f-?~ Ji¥" Dale Reported _______ _
Oak AnalyLc.:ffff!-~;;/2e Lab Number , 991250
--,v X:.....,y••-••..,
2,4-D
_ 2,4,5-TP (Silvex)
DI IS 3191 (Revised 2i91)
!
!
N.C Department of Environment,
I lea.Ii~, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number _______________ Field Sample Number . : 6 "1...--o 6 1> <../ ..
Name of Sile (JJ A f?.,R.f.N Gurvw p CB LA-1-ADP 11stre Location_· ~Lv_Mi-'---'-IJ....--"-'e::-"-f,J~Jl;,-,J ________ _
Collected By JJ-2, ,.y',J ID# ___ Date Collected 4-Ii ·-fl-j ·.,-Ti.me ------
Agency: Hazardous Waste Solid Waste ~ Superfund ·:··. ,._ TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate .. Comments Arsenic --
~ Solid (5)
.... Barium
-Q..c...us S°'< J I,..._~~> ---Ground water (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury
_ Soil (3) _ Sludge (7) --Selenium ·\ --
/ Other_(4)
Silver --_ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parameter Resuh"(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
__ P&T:GC/MS Arsenic benzene --------__ Acid:B/N i:xr. I Barium . carbon tetrachlo:-ide --· --MTBE Cadmium chlordane
✓ Pc-B -----·--· --
< "' /() f1f>m, Chloride chlorobenzene ·----.. Chromium chloroform ----·· ----___ Copper o-cresol --
--1
__ Fluoride m-cresol -----Tron __ p-cresol ---I Lead cresol --·•/ Manganese 1,4-dichlorobenzeoe ------I Mmury 1,2-dichloroethane
--· __ Nitrate --1,1-dichloroethvlene --. · 2,4-dinitrotoluene
I---
I __ Selenium
, __ Silver = heptachlor I -Radiochemistry 1--Sulfates hexachlorobenzene ------·····-. Zinc hexachlorobut:::diene
Results (PCi/1) j = pH --Paramt~.:r hexachlorocthane --__ Gross AJp!1a l __ Conductivity --methyl ethyl kete:ne
Gro£s Bet:! ! TDS nitrobenzene -.. --i--TOC -----. __ penlachlorophenol i i --
I --__ pyridine
Microbiology __ tetrachloroethyJene I --I __ trichJoroethylene f ----------! ! Parameter Res11lls (Col/iOOml) __ 2,4,5-irichlorophenoi i 1-2,4,6-trich.!orophe::wl I I I --I= • I l = vinyl chloride I ·-endrin --
4-;;i I -q 9 M lindane
Date Received --Reported by methoxychlor --
Dale Exlraclc<l fCB :4:-J6.c,qA Dale Reported
__ tcx:iphene
--2,4-D
tf.'~~(7'81)_ \ 991251 _ 2,4,5-TP (Silvex)
DJ[(: Anlllyzcoo-<lfu Lab Number --DI IS 3191 (Revised 2/91)
N.C. Department of Erivironment,
I lea.Ith, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number _______________ Field Sample Number ' . 6 '.Lo, ")S-:
Name of Site UJAR~N Gvl\,{tl( Pc& LA-tJDP 1'st-e Location_.;::..l,J_ . .:._Ml..,____,_R....;:ce::=..:..:....w ...... Tb...:c___;;,J ________ _
Collected By lJ-2, ,,y,J ID# ___ Date Collected .· 4-1&[ ·~~-5. .Time ------
Agency: Hazardous Waste Solid Waste ~ Superfund
Sample Type
Environmental Concentrate Comments
__ Groundwater (1)
__ Surface water (2)
_Soil (3)
~lid(5)
. _ Liquid (6) __________ _
_ Sludge (7) __________ _
V Other (4) --'
_ Other (8) __________ _
Organic Chemistry Inorganic Chemistry
. Parameter
_P&T:GC/MS
_ Acid:B/N Ext.
MTBE
i ✓ Pc..8 ~
Resu!t::.(mg/1)
---------
q,/Oppt>t
,;ammeter
Arsenic
Barium --Cadmium -· Chloride
Chromium ------. ______ __ Copper
I. 1~~---/.-~-~~--~~:ride
Results(mg/1) (mg/kg)
-----··--! ~ , ______ __ Lead
I --__ ..,..'.,.... ___ _______ __ Manganese __ Mercury
I __ ______ _______ __ Nitrate
Selenium
'-----···-----------Silver
---TCLP Compounds
Inorganic Compounds
Arsenic
Barium --Cadmium-
Chromium --Lead
Mercury
--Selenium
Silver
Organic Compounds
benzene --carbon tetrachloride
Results(mg/1)
Results(mg/1)
---------chlordane
chlorobenzene --ch loroform
o-cresol --m-crcsol = p-cresol
cre:;ol ----1,4-dichlorobenzene _____ _
1,2-di chloroethane
--1,1-dichloroethylene
_· 2,4-dinitrotoluene ===========--.---
I . . Radiochemistry === Sulfates
---------hcptachlor ------·
l., ____________ -----------t
i Parameter !
Zinc --Results (PCi/!) _ pH I __ Gross Alpha i __ G~oss Beta
I TOC
__ Conductivity -------TDS . ________ , ··--------
I Microbiology I = _-_-_-_-_-_-_-
It--P-a-ra-n--,-et_e_r _____ R_e_s_u-It_s _(_C_o_i/_l_[,0-m--1) .... , = --------
hexachlorobenzene I I --------hcx~:::hlorobutadiene ---------he:v.2chloroethane ----methyl ethyl ketone _____ _
nitro!Jenzene ------' pe .. tachlorophc,101 = pyridine
__ tetrachloroethylene
--trichloroethylene
__ 2, 4, 5 -tr i ch Io ro p hen o I
__ 2, 4, 6-tr i c hl o ro p hen o I
vi n y I chloride
--endrin
lindane
---------------------------------
Date Received J...i-;:L /-C/ 9 7Jd Reported by methoxychlor --------------------tax ::i p hen e
Dale Extracted ~{S 1--L0-lfl ltm Date Reported 2,4-D ~
.PC!.Bs(t,A,'a"Om ~9-9-1-2~5~2--__ 2,4,5-TP (Silvex)
Date Analyzed' i/-3/J-91YP Lab Number
Dl!S 3191 (Revised 2/91) ----------.__ _____________ _
N.C: Department of E~vironment,
I Jc;:lih, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
. r
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
she Number · · Field Sample Number '::.· C>~ 61> f, ---------------------~~--------
Name of Site UJ Af<.Rf..N Gurvw p CB LA-).,U)P1'st-e Location_W"--MJ-_,__.a...fl=-E:=-W_7b..__N_· __ ~_------
Collected By IJ-2,,,.,·,J ID# ____ . Date Collected ·· 4-1· . ·-.'l4,·-· _; · Time
Agency: Hazardous Waste
Sample Type
Environmental Concentrate Comments
__ Groundwater (1)
__ Surface water (2)
_Soil (3)
~ Solid (5)
~_tz/, Liquid (6) __________ _
_ Sludge (7) __________ _
✓ Other (4) _ Other (8) __________ _
Organic Chemistry Inorganic Chemistry
Results (mg/I) Farameter
Arseliic --
Results (mg/I) (mg/kg)
Inorganic Compo!.Inds
Arsenic --Barium --Cadinium·-
Chromium --Lead . · ' ..
Mercury
· .-.. -. -Selenium ----Silver
Organic Compounds
benzene --
------
Results(mg/1)
·\
Results (mg/I) . Parameter ·
_P&T:GC/MS
_ Acid:B/N Ext.
MTBE
✓Pen
--.oarium· -·
Cadmium
-------.1 ·-C,-.rbon tetrachloride------
chlordane
--------· -------
--Chl0ffde
Chromium ----Copper
Fluoricie
Iron --Lead
__ Manganese
__ Mercury
Nitrate
--chloroberii.ene --chloroform
o-cresol --x.-cresoL --p-cresol
· -cresol ----1,4-dichlorobenzene _____ _
_______ ' __ 1,:2-dichloroethane
__ 1,1-dichloroethylene _____ _
__ Selenium __ '1,4-dinitrotoluene
__ Silver __ heptachlor
Radiochemistry Sulfates j hcxachlorobenzene
······-··----------·--------===Zinc -------, --== hexachlorobut~diene _____ _
Parameter Result.: (PCi/1) __ pH __ hexach!oroethane -
__ Gro~s Alpha _______ __ Conductivity -------1 __ methyi ethyl ketone _____ _
Gross Beta __ TDS i ni~robe!lzene
T0C --pentachlorophenol 11 ---= pyridine
.
1-P-ar_a_m_e_t_eMr_i_cr_o_b_i_o_I_o_gy _____ =--==------I === ~;it;:~;::;~;~ne --------I
1 Results (Col/lOOml) __ _______ __2,4,5-trichlorophenol !
j __ __ _ ________ 1 _ 2,4,6-trichlorophenol i
1-----~~& !
i __ endrin -1.
lindane
Date Received 4-;).J-qq M Reported by ______ _
Dal e Extracl c<l Pc12+✓10..-b\'l ~
fJCB~~
Da1 c Analyze d 'l-.9o-99VP
D I IS 3191 (Revised 2/91)
Date Reported
Lab Number
-9----9--,,-12_5__,.3--
----------
=== methoxychlor __ !
__ tcx3p!-:ene
_2,4-D
_ 2,4,5-TP (Silvcx)
I ------, ------i
I ---i
i
N.C I?cpartmcnt of E~vironment,
I lc::-lth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number _______________ · Field Sample Number_·: _ ___.:D=-.:-:i...=--=o::........:.(;.i..J.,;,......1~--------
Name of Site UJ Af<.Rf-N
Collected By IJ-2, ,.,i,J
.. . . . LL-.
GvNN PuB UttJOP I Site Location~uJ::...:......:fr--lP,~/t=e:=W......1Tu--=-::Al ________ _
ID# · . ;, • Date Collected · Y-1 . ·-~ j ·. Time ------
Agency: Hazardous Waste .: '·Solid Waste _.::::::_Superfund -----
Sample Type
Environmental Concentrate Comments
S<J,~!"'-+.) ~Solid (5) L/T Os·. Ground water (1)
__ Surface water (2) _Liquid (6)
_Soil(3) _ Sludge (7)
_L_ Other ( 4) _ Other (8)
Organic Chemistry Inorganic Chemistry
_ Parameter Results (mg/I) Parameter Result..,(mg/1) (mg/kg)
_ P&T:GC/MS Arsenk --_ Acid:B/N Ext. · Barium --MTBE Cadmium
✓ ~CB --<O•/OR'>fl Chloride --Chromium -----
--Copper
--Fluoride -------Iron -----Lead ----•,~\ __ Manganese --
-1·.' __ Mercury --
Nitrate ----' Selenium . --·-Silver --Radiochemistry Sulfates --·····-·· --Zinc
Pan:!7eter Results (PCi/1) ~_pH
__ Gross Alpha · __ Conductivity
·::iross Beta TDS ----TOC --
--Mkrobiology --
--Parameter Results (Col/JOOml) --
---··----
----
Date Received J..J--;l}-9C/ '17d Reported by ---------
Dal c Extracted~ .tf--2.0_.C)q ll-n1Date Reported --------
Dol t.: Analyzed~~ Lab Number __ 9_S_1_2_5_4 __
I) I IS 3 I 'JI ( Revised 2/91)
I I
I
·. TCLP Compounds
Inorganic Compounds
Arsenic --_ Barium ---Cadmium --Chromium --Lead --Mercury
--Selenium --Silver --
--
--
--
--
Organic Compounds ·
benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-cresol --__ p-cresol
cresol --1,4-dichlorobenzene --1,2-dichloroethane = 1,1-dichloroethylene
· 2,4-dinitrotoluene --__ heptachlor
hex:achlorobenzene --hex:achlorobutadier.e --hex:achloroethane --
--methyi ethyl ketone
nitrobenzene = pentachlorophe:101
__ pyridine
__ tetrac:hloroethylene
__ trichioroethyiene
__ 2,4,5-trichlorophenol
2,4,6-trichlorcphenol = vinyl chloride
--endrin
hndanc
methoxychlor
__ tcxaphene
2,4-D
_ 2,4,5-TP (Silvex)
Results(mg/1)
... .\ .. •
;.•
Results(mg/1)
--
I ;
N.G. Department of E~vironment,
I k:ith, & Natural Resources
Sulid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number _______________ Field Sample Number · C) ",l_~ C ~ _g . ·
Name of Sile UJ AflRf.N GvNN p CB ~DP1'sfte Location_. =-LJ--'-/lrfl..,__,_f{=:e:;=~c.:......L.Tl?~N ________ _
Collected By IJ-2, ,,y,.J Date Collected .. ~" Y-19, ·-~ 4,. 1 • , .. ,Time ------
Agency: Hazardous Waste Solid Waste ·. ·. v Superfund
:
Sample Type
Environmental Concentrate Comments
_Groundwater (1) ~ Solid (5) ~ A110' M /~. )11:eJ-1"--
-Surface water (2) / Liquid (6) ~> ,1/L 1-/21' ~ le.vc (y
Soil (3) _ Sludge (7) __________ -_
~ Other (4) _ Other (8) __________ _
Organic Chemistry Inorganic Chemistry
.. Parameter Results(mg/1) Parameter R~sults(mg/;)(mg/kg)
_ P&T:GC/MS ______ __ Arsenic
__ Acid:B/N Ext. ______ Barium
I MTBE .---=------C&dmiul'l1 ✓ PC-8 e.-.,'!) t>1•'IJl,P/'m., ~ Chlori~e I __ ______ ______ Chromium .
1 __ -..-----..,,. -,-,,..----__ Copper
I J!_ ~-L-n-:...__ , Fluoride
.A / .--Cut • -• Iron • ---~-=--""'~ ~ I -----c----I _ Lead I __ ·· · ______ __ Manganese
__ . ______ __ Mercu:rj'
Nitrate
Selenium --Silver --Radiochemistry Sulfates
f ··· .. ·-··-------------t -_-_-_Zinc
I Parameter Results (PCi/1) __ ;;H I ___ Gross Alpha __ Conductivity ______ _
, Gro~s Beta TDS i --------------TOC
Microbiology
------Parameter Results (ColiHJ0ml)
1-
Date Received 4-:J.J-C/9 7Jd Reported by _______ _
Dale Extraclc<l f Cf>4,16 ✓9C114'n Date Reported --------
Dal c AnalyL.cd~~ Lab Number 991255
D I IS 3191 (Revised 2/91 )
: .;•, •. •:c TCLP-Compounds
Inorganic Compounds
Arsenic --Barium --Cadmium -
Chromium --Lead .::
Mercury
--. Sele~um
Silver --
Organic Compounds
benzene --carbon tetrachloride
Results(mg/1)
Results(mg/1)
---------chlordane;-----chlorobenzene
--
chloroform
o-cresol
m-cresol
--p-cresol
cresol
-----·---
--------
--------
----1,4'-dichlorobenzene ______ 1
1,2-dichloroethane
--1,1-dichloroethylene
--. 2,4-dinitrotoluene --------= heptachlor
bexachlorobenzene ----------hexachlorobutadiene ---------hexachloroethane I = methyl ethyl ketone ------1
__ niirob~!lzene ; ------, per.tachlorcphenol = pyridine --------
__ tetrachloroethylene
trichloroethylene ________ _
_ 2,4,5-trichlorophenol ______ I
2,4,6-tri(:hlorophenol
--vinyl chloride
endrin --lindane ----methoxychlor
tov"AnhP"P
--I:" _2,4-D
_ 2,4,5-TP (Silvex)
------
N.C: I:?epartmcnt of Environment,
I lc;;ith, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
. :" .'. •·,
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolfn~· 27611
Site Number ' · · Field Sample Number.'.: 0 'l...o f..3 9 ---------------
I • ·:,,,·.; ,-•:? ~;~:.i ~•~;·J_
' .
Name of Site UJ Af?._Rf-N Guf\.JN . p CB LA--,JDf 1'sft'e ~cat~on_w~· _M_,_· _,_R.-'-i!:-'->J_· ~Th_._-,.J __ ._·: :_· _.,:~_-.·. _____ _
Collected By IJ-2, ,,itJ .,.,·:•-: · '· · · · ID#_-__ ·_ .. Date Collected . · Y-1 :f ·~ 'V\-.• i , •. 1. · .. Tµne _____ _
Agency: · . vSriperfund
--:-!•
Hazardous Waste -· Solid Waste
.-.:.,.
Sample Type Inorganic Compounds
Arsenic
Results(nig/1) -2: ·
Environmental Concentrate Comments · ·
_Groundwater (1) ~ Solid (5) CA-g.f1>c,,j · h~:ti&;: Y'1~J ~
_ Surface water (2) · _· · Liquid (6) P'"'~<;. ~lo/«-1-/27'4 Llv~ & ·
. , ...
--Barium
.. --·Cadiiiiwn•-· · -.,:._:,, •' · ,.: ·
Chromium --Lead ·:
Soil (3)
_L Other ( 4)
Mercury
__ Sludge (7) ____________ .. -.. ===Selenium ---'·, -:.>·, • ~;,,,.· :'
_ Other (8) __________ _
Organic Chemistry Inorganic Chemistry
. Parameter
_F&T:GC/MS
_ Acid:B /N Ext.
?-ATF~
Results(mg/1) Parameter Results(mg/1) (ll1g/kg)
✓~--
-----·---------
Radiochemistry
······-··-------------~
Panm~ter Results (PCi/!)
__ Cros~ A.lpha ______ _
G,oss 3era
--
--
--
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
--
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium --Silver --Sulfates
Zinc --_pH
__ Conductivity
TDS _._.,_,_______ --
TOC
Microbiology ,--------------· -------
Parameter Results (Col/lOOml)
-·----------
Date Received 4-,;J J-q q 17;} Reported by
--------
-------
----------
Dalt: Extraclt:<l fCf:>4--2,0,qq \l:h'.J Date Reported
fe£5-cM~ -99-1--2--=-ss~-
Datt: Analyzt:d q-.,:f0-99YP Lab Number _________ _
DI IS 31 91 (Revised 2/91 )
Silver
. ~ .. , ... . : ..
Organic Compounds Results(mg/1)
benzene .··. ··· --carbon tetrachloride ---------
--
--
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
--p-cresol
cresol ----1,4'-dichlorobeiv.ene · _-·_· · ____ _
1,2-dichloroethane = 1,1-dichloroethyl~ne _____ _
__ · 2,4'-dinitrotoluene·
__ heptachlor
hexachlorobenzene
hexachlorobutadiene ---------hexachloroethane
__ methyl ethyl ketone _____ _
nitrobenzene --pentachlorophennl = pyridine
__ tetrachloroethyh.!ne
__ trichioroethylene
__ 2,4,5-trichlorophenol ______ !
2,4,6-trichlorophenol I = vinyl chloride · _____ _
endrin --lindane
__ methoxychlor
__ tcxaphe~e
_2,4-D
_ 2,4,5-TP (Silvex)
i
N.C.·Dcpartmcnt or Environment,
I lc.i'th, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sitc·Number ·' -·-, '·> ·.•; ·: ::_,,,'·Field Sample Number,fr ,_, .;, ... ,D'l..-D bl.-(<-=-
Name of Site UJ AflRf;.N GurvN 'P·cg '.\~~0P.1~e ~~at~:~-,' w~ ft,;;~ JbN .; ,'
Collected By IJ-2,,,y,J Time -------...
Agency: Hazardous Waste .:· •a ~\·•:solid Waste'' ;:_:,\tvsuperfund S1,;_;~,(~,-:,-;;;;:;;~; TCLP Compounds ---~-· .. : . :-:. a._;.t .... J~ \;_&1 .. -· ; ~~--...:.. --il~q
Sample Type ., .. ·, " ;·:.· .i" .• _.-_,; . -~--~),....:_: ._, :ir--·.:_ Inorganic Compounds Results(mg/1)
Environment.al Concentrate '· ,· Arsenic Comments ·.,·;,·' · ----
5eJ '' ... ·+ ·--.. , . r:, k Barium ¥ -__ Ground v-ater (1) Solid (5) ·,,.:.,¢.,,: -.. t\.. • { ' :,:• .... -.... ; Cadmium --
Pc,? ~ fbl "-H1~ Chromium
__ Surface water (2) _ Liquid (6) Llz-ve.Is · Lead --Mercury
Soil (3) _ Sludge (7) .... _.:. ., -~ '~ Selenium ' --Silver --__yOther (4) .. _ Other (8) ·-.. ., --
--'· --Organic Chemistry Inorganic Chemistry_ --. ' '.
. Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organ!,· Compounds Results(mg/1)
_P&T:GC/MS Arsenic · -. benzene -
----__ Acid:B/N Ext. , __ Barit!m carbon tetrachloride ---
MTBE . f: Cadmium chlordane
✓ ~C.,B (/~O) ~ ~ Chloride . -,-. chlorobenzene --chloroform Chromium --------· • ,_Copper o-creso! --~dnv , Fllloride m-cresol
4k-~;)~Iron ----
-· __ p-cresol
_ . t I-Lea~ _ cresol ---
--., I __ Ma?~a~ese --1,4-dichlorobenzene
__ Mercury· -1,2-dichloroethane --•r•· --Nitrate 1,1-dichloroethylene ----Selenium .. 2,4-dinitrotoluene ----Silver __ heptachlor
Radiochemistry j = S~lfate!> hexachlorobenzene ----······-··· 1 __ Zmc hexach!or0~,utadiene. --Parnmeter Results (!>Ci/I) ! pH hexachloroethane I = Conductivity
--__ Gross Alpha --methyl ethyl ketone
Gress Bera _________ 1 __ TDS nitrobe~zene ----·-= pentachloropher,ol TOC --
--__ pyridine
Microbiology --__ tetrachloroethylene
trichloroethylene --P,1rameter Results (Coljl 00ml) _2,4,5-trichlorophenol --
----------__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane '--t-.2) _qq-n:J --Date Received Reported by methoxychlor --
pc b 4--10J.f0U11 Date Reported
__ toxaphene
Dale Extracte<l 2,4-D --t1'~f{A1 S'CJ?() _) 991257 _ 2,4,5-TP (Silvex)
Dale Analyzed 'f-.30-991/P Lab Number --DI IS 31 'JI ( Revised 2/91 )
I
I I
C-DEHNR
ivision of Solid Waste Manai;ement
J Superfund Section
J H~ous Wusk Section
a"solid Wuste Section
Organics Lab: -:----Inorganics Lab: --
CHAIN OF CUSTODY RECORD
Project Name: pc,13 /,~ Sampled by: L► /2.-,.c_.
Site ID # (NCD#) Sampler 1D l m --
Location: t-1~ "{!;, Telephone:_(_) :;2 31,...~ tq 2. v 2-~7
Address: Date Sampled: ~ /7-2-~ .-
Time Sampled: -, 7
Sample Types: Soil Water Waste Other ~
Remarks: Le&~~
Field Sample (j!-11 L<i'l>?-v
Numbers
r\
Relinquished by: ;faAJJv. 't(o~ Date: /..//41-/"? Time: I?/ 5:1
t3'ignature) \ '( I , I
--------~ J--;p~--~------------------Date:________ '91 ---------------------------
Received by: Time: /::Z..:5'7
(Signature) ¥~-
Relinquished by: Date: Time:
(Signature)
-----------------------------------------------------------------------------------------------------------------Received by: Date: Time:
(Signature) -
Relinquished by: Date: Time:
(Signature) ------------------------------------------------------------------------------------Received by: Date: Time:
(Si.mature)
----
Results Reporte~~ / ~-~-~-ytl_r.1 0 Date: 'i;-2.tJ-9 9Time:
( ~J_gfi'}[Ure)
-
\:\COCR.f-RM)
I
>/
NC·Depanmcnt of Environment,
Hc.alth, &. Natural Ruourcc,
Solid Wut.e Mana&cmcnt Divi,ion
SAMPLE ANALYSIS REQUEST St&tc Laboratory of Public Hc.alth
P.O. Box :!8047, 306 N. Wilmington St.
Ralcii;h, Nonh Carolina 27611-8047
SiteNumber SamplelDNumber/Name /'{ Z 'i I -------------------------------
Name of Site __ (1_G'.'.--'-8----=-c_F-_______ Collected By __ L_. _,z.. __ yC.... _______ ID #_/_IIV ___ _
Sitel.ocation---1t..-i,_b-') .... a--'-r .... r:_~---'---t_o_· _____ DateCollected __ 7J..,_,.../_2._2.~/r'-'-q_,__ _____ Time_"""'q'-""-:_7'"'"-'-c, __ _
Agency: Hazardous Waste ~ Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments arsenic -
k£.?t:/,e1/4 ,. k{lueJ barium ·--Ground Water (1) Solid (5) cadmium ---chromium -Surface Water (2) Liquid (6) lead ---
-mercury
Soil (3) Sludge (7) selenium ---silver -
-Other (4) -Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS antimony benzene ---Acid:B/N Ext-arseruc carbon tetrachloride ---. 2,4-D barium chlordane ---2, 4,5-TP(Sil vex) beryllium -chlorobenzene --chlordane cadmium chloroform ---hept.achlor chloride o-cresol ---hexachlorobenzene chromium m-cresol ---bexachlorobut.adiene cobalt p-cresol ---endrin copper cresol ---lindane fluoride -1,4-dichlorobenzene --
methoxychlor iron -1,2-dichloroethane --toxaphene lead 1, 1-dichloroethylene 2 f?or(jotfy ~--t:J,()0O6~ manganese 2,4-dichloroethylene -
~hufs p,.eye-..,;;r-th
-mercury -heptachlor
nickel bexachlorobenzene --. ~~l'JAA,l-]q ,ra_,;-r,. , nitrate bexachlorobutadiene v --selenium ... hexachloroethane --silver -methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobenzene --
Li--».-99'i(p thallium pentachlorophenol --Date Received vanadium pyridine
PC/3;. ( ,,11ioi> --zinc tetrachloroethylene
Date Extracted '/-,;i. 6-tfYf' -pH -trichloroethylene
tf)c.s~ fl',{J'O?' &cq fr,_ conductivity -2,4,5-trichlorophenol
Date Anfil~-99~ "-TDS 2, 4, 6-trichlorophenol -flash point -vinyl chloride
-endrin -Reported ~
--lindane
Date Report S--~ O-'1 f.... --methoxychlor
9912?9 --toxaphene
Lab Number 2,4-D --
--2,4,5-TP (Silvex)
DHS 3 I 91 (Revised I :!/93)
NC Depart:'nent of Environment,
Heallh, & Natural Rcwurce,
Solid Wast& Manai:ement Divi,ion
SAMPLE ANALYSIS REQUEST St.ate Laborat.ory of Public Heallh
P.O. Box 28047, 306 N. Wilmington St.
Raleii;h, North Carolina 27611-8047
Site Number Sample ID Number/Name / </ 2 f Z-_______________ -------------------
Name of Site __ l/4_t=_t_3_L_C _______ CollectedBy __ L_._!ln--________ ID# I tf2)
SiteLoc.1tion ~ {;.o DateCollected lr,/2.z.../ 'ff Time 9~ oS--
-----------'--------..t....., I -------------------
Agency: Haz.ardous Waste \/'solid Waste __ Superfund TCLP Compounds
Sample Type
Environmental Concentrate
Ground Water (1) Solid (5)
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Comments
~-Ef& l
Inorganic Chemistry
Inorganic Compounds
arsenic
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
2,4-D
2,4,5-TP(Silvex)
chlordane
heptachlor
hexachlorobenzene ------
hexachlorobutadiene
endrin
lindane
methoxychlor
lo]tphene
✓ ll:dt
------
FOR LAB USE ONLY
Date Received I/-~ -<t'1Yf'
(Pcg§-(Hs-vt)
Date Extrac -=-=-:::r-:-::-:::=-':=.....-'-_;_.._,_ __
Date Analy ~
Reported By
Date Reported _________ _
Lab Number 991280
OHS 3191 (Revised 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zinc
pH
conductivity -------TDS
flash point -------
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobenzene _____ _
1,2-dichloroethane
1, 1-dichloroethylene _____ _
2,4-dichloroethylene
heptachlor
hexachlorobenzene
hexachlorobutadiene
... hexachloroethane
methyl ethyl ketone
nitrobenzene
pentachlorophenol
pyridine
tetrachloroethylene
trichloroethylene
------
------
2,4,5-trichlorophenol _____ _
2,4,6-trichlorophenol _____ _
vinyl chloride
endrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
C-DEHNR
ivision of Solid Wask Manal:!ement
J Supi:rfund Si:ction
J !ju:umlous Wusk Si:ctloa
3"solid Wuste Si:ction . . _ .
Organics Lab: :----Inorganics Lab: ✓
. ..
•""• -• .. ••,r,, J.
CHAIN OF CUSTODY RECORD ..
Project Name: Pc 6 L f .
Site ID# (NCD#) ________ _
Location: W~ Co
Address: --------------
Sample Types: Soil ------
Field Sample ;ll>tf. ~
Numbers
Water
. -. '
Sampled by: C .. ~
Sampler 1D I tFl> -------------Te 1 e phone:_ L) 2.p:-t)' q1.,
Date Sampled: y/i i-Jqt;
Time Sampled: -T
)c. '2-57
Waste Other ✓ -----
Relinquished by:_~.../....!,,::.~-L.::::::::~~-U.--____:=----Date· tJime · / {)} t..fX?
Received by:'----.,_.-,.-2...~~!::::=!:~~""--~~.z.~ ::::::::::~~::...L.:L--_--_--_--_---_----DateGj-39 Li-ime:__._f o_~-~----
Relinquished by: _______________ _ Date: __ _ Time: -----
r
I (Signature) :
--------------------------------------------------------------------------------------------------------·-----------i
Date:___ Time:_____ l
(Signature) I ============================================;(
Relinquished by:________________ Date:___ Time:_____ I/
(Signature) !!
Received by:
-----------------------------------------------------------------------------------------------------------------------
Received by: Date: ---Time: ____ _
(Signature)
Results Reported:
N_C Dcpat1ment of Environment,
Hulth, &. Nawral Ruourcc,
Solid Waste Manai:cmcnl Divi,ion
SAlvfi>LE ANALYSIS REQUEST S1&1e Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Ralcii:h, North Carolina 27611-8047
Sit.e Number------'----------,---SamplelD Number/Name ___ :J-_o_,_~_'2--__________ _
Name of Sit.e _f◄_c_·l3 ___ L_F_-______ Co_llected By __ l_-_~ _________ ID# / , ..
Site Location w~ C,_' O Dat.eCollected y I 7... ,_ / '9 f Time ------------------'-,1----+,-.. -:..-=..-:..-_-:..-:_-_-:..-:..-:..-:..-:..-_-:..-:. __ -:...-:..-:.-:.-:..-:..-:..::.::.::.====--.
Agency: Haz.ardous Wast.e ..,...........Solid Wast.e __ Superfund
Sample Type
Environmental Concentrate Comments
Ground Water (1) Solid (5) /.._Lt:.d~ -
Surface Water (2) Liquid (6) Xr,{(y~
Soil (3) I Sludge (7)
~ther (4) Other (8)
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Results (mg/I) Parame~er Re:sult@(mg/kg)
antimony
Acid: BIN Ext.
2,4-D
2,4,5-TP(Silvex)
chlordane
heptachlor
hexachlorobell.2.ene _____ _
hexachiorobutadiene ______ _
endrin
lindane
methoxychlor
toxaphene
FOR LAB USE ONLY
Date Received ----------
Date Extracted _________ _
Date Analyzed ___ ~------
R~rted ~ ~=~-~~----
Date Reported 7/u!~ 9
OOS08'.b MAY 4 9 Lab Number . ----------
DHS 3191 (Revised 12/93)
arsenic
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zinc
pH
conductivity ______ _
TDS
fizsfi . -
L ~.LC-le...+-,,-,.,,......., _ __,---1--+t-...-...
TCLP Compounds
Inorganic Compounds
_ arseruc
barium ,
cadmium
chromium
lead
mercury
selenium
silver
Organic Compounds .
benzene
Results(mg/1)
Results(mg/1)
carbon tetrachloride ______ _
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobenzene ______ _
1,2-<lichloroethane
1, 1-dichloroethylene ______ _
2,4-dichloroetbylene ______ _
heptachlor
hexachlorobenzene
hexachlorobutadiene ______ _
... hexachloroethane
methyl ethyl ketone
nitrobenzene
pentachlorophenol
pyridine
tetrachloroetby Jene
trichloroethylene
2, 4,5-trichlor::iphenol _____ _
2,4,6-trichlorophenoJ ______ _
rinyf chloric!e
endrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
NC Department of E,nvironmcnt,
Health, &. Nawral Ruources
Solid Wu~ Manaicment Divi,ion
SAMPLE ANALYSIS REQUEST State Labor.tory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Ralcii:h, North Carolina 27611-8047
Site Number _______________ SamplelD Number/Name -~r?:~O----=b--'=-3=------------
Name of Site fc IJ L ?" Collected By __ l,;_._~ ___ ._· ___ --'-__ · ID# --/ re
SiteLocation lv~ 4 · DateCollected 'I /42,,, /# ,_ Tim~_-·_-____ _ ---,"-""-~1.,,..'":.. .... _ ..... _-_-:_-_-_-_-_-_-_-_-_-_-:_ _________ -,
Agency: Hazardous Waste c.,./'Solid Waste __ Super-fund
Sample Type
Environmental Concentrate Comments
-Ground Water (1) -Solid (5)
-Surface Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
~ Other (4) -Other (8)
Organic Chemistry Inorgaruc Chemistry
Parameter
P&T:GC/MS
Results (mg/I) Parame~er Resul~(mg/kg)
_ antimony
-
-
-
-
-
-
-
-
Acid:B/N Ext.
2,4-D
2,4,5-TP(Silvex)
chlordane
heptachlor
hexachlorobenzene
hexachlorobutadiene
endrin
lindane
methoxychlor
toxaphene ·
\
'
FOR LAB USE ONLY
arseruc -barium -
-beryllium
cadmium -chloride -chromium -cobalt -
-copper
fluoride -iron -lead -
-manganese
-mercury
nickel -nitrate -selenium -silver -suifates -thallium -Date Received vanadium -----------
ZlllC -Date Extracted -----------pH
_ conductivity ______ _
Date Analyzed TDS ----,---------
Reported By _,__ffi---t-JJ\-+,~--V ivoint1 5Jt,,71q .
199
¾®Cie-z.--0-. .......-1 -
Date Reporte4--.nr,..,0 ,... M~" ____ . __
Uvc~JGJ 11H T ;';) _______ /( vs~rt,J<d
DHS 3191 (Revised 12/93)
Lab Number
~tP~~-
TCLP Compounds
Inorganic Compounds
arseruc --barium , -cadmium -chromium -lead -
-mercury
selenium -silver -
Organic Compounds
-
-
-
-·
-
-
--
-
-
-
-·
-
-
-
-
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-<iichlorobenzene
1,2-<lichloroethane
1, 1-dichloroethylene
2,4-dichloroethylene
heptachlor
hexachlorobenz.ene
hexachlorobutadiene
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
,,S-AA'Y)
Results(mg/1)
Resul l5 (mg/I)
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: l+11Rft-,V Li,..,,·vv Well#: _Yn_w_'----1 ----
Comments (well construction, etc): __ l -_+_,-=-t---=-O-=l!.-..._e_+--=('--5_--'--/ ._'i '>-=------'O;:_--e~e t_4-'----'-~--LJ-'-Pr'-'-~~-9..,:__'i_. ,_'i ___ _
Conversion Factors: For 2" well: 3 volumes (gallons) = 0 .5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): 5.), 3 Well Volumes (gal): 1s-.r:;fJ Purge Equipment: &1'_,~J-4'.:,, ~J .-FL..'-'
,·
Date Purged: -'1-~ -'l ~ Purge Time Start: / u: V> Purge-Time End_: -------
Did well purge dry? Y
' 7A.. <--,__
N , Actual purge volume : 1125 ( < rl' ----
Volume V Volume Volume S,·•.J Volume Volume Volume -----
Temp (0 C) 11-'3 I f. q Ir. C
pH {, -I fo. I t-c> r
S. c: '{J -c) / o).__t) I "1, 2-
D. 0 .
Turbidity J,, [) () r-' 7 /., . '-/. 'i cf
Sample Date: ~ l!r 14
Sample Information
Sample Time:-~/_/._.-_Z--_D __ Sample Equipment: t~v ..),-(; /}__,--:f'
Water Condition (turbidity, odor, etc.):_C_le_-4,_,...__;_>-_7--+--...,ce~-----------------
Samples Collected(✓):
__ · VOCs (2 40 ml vials)
✓s~(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(°C): )Lt. pH: {o 'l SC(umhos): __ _
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): 1/. i'Y
, :omments: L.Jt,({ flvj.._JJ Ov-r "----l /0-'l{S,, '-/.U-7.e__/ ......... > ev=rj
___ .;c_f,._=r----,1....:..:le'---l,.......:.t. )'---e,,li......;(;__~_J __ /i,1,/;_,,_0._1_!_!....;.~-==.C---"----{ ._..,..~r-cl_____;,.~'--"=--,r ___;½.=---...;4_✓_-_______ pcbwclls.frm
WELL LOG SHEET Facility: Warren Cou·nty PCB Landfill Location: Warrenton
Purge/Sample Team: --+-/-ht'----'----U.g_=(W __ Z----'-'--1/Vt_~ ________ _ Well#: /YJ vi I A -------=~----
Comments ( well construction, etc): ...;....:2..,-=-'-' -=W:c...t.,:c..J<ut'-'---_1:'..._ .. '--\-_ .. _l -=o-=i~pp....:~--=---='..L..:3:....:.. ~-1----=0...::.e:p-fLthi...:..:--..:....:~:___u_~~=------L(1...-=-----· 'i __ _
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): /1./ 4 3 Well Volumes (gal): µ,t)--Purge Equipment: Z ,,-;;_
r
Date Purged: · t-f-1 q__ 'i'i Purge Time Start: A/ ,4 ----'----Purge Time End: -------
Did well purge dry? Y
Volume Volume Volume Volume Volume Volume ------,
Temp (0 C) ,.,.
pH
S. c:
D . 0.
Turbidity
Sample Date: l( ~ J...~ -14
Sample Information
Sample Time: _l_c_~_J~-'----Sample Equipment: \1 -rl < v---------
Water Condition (turbidity, odor, etc.):T..,,.J.,;j 5 .. q~ -C..IL~c-t-e-J ~"f,...,'>' I (,"tu-.J-:i ... $
I <-Pt 4:h ll ~ c-l ... '1 c:.-+-;tr ~c.tf ""-r ""'-~ ~.., ..,,,.~J c-tl~J ,1;,vo/.1,..,.,.,. /,4
~-ll..~C,O
Samples Collected (✓):
VOCs (2 40 ml vials)
_I_ SVOCstfPC&)l 2L Amber bottle)
Metals (1 IL HDPE bottle)
Temp(°C): ---pH: ----SC(umhos): ---
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): ---Turb(NTUs): ---
Comments: __ N_;c.,----'fJ,._ ..... _r-"-"..., ___ L_-1-__ ) _.,_,,., __ 7:...::..v...;./_t..:.._,...::..:J_rL-_6, ___ c,,,_~_c,_~.....;;...=;.J __________ _
___________________________________ pcbwells.frm
Facility: Warren County PCB Landfill Location: Warrenton
. ':::· .
. Plltge/Sample Team: R. Rober-ls /c. 0 Id,,-
/
\Vell #: MW-2
r,lf' i-~.S6"
Comments (well construction, etc): _4-'--'
1
_._P_._l/...;..C. __ ___,10J_A_;_P_;_R_ld\_(;\_o,-'--s-w_L_·_3_...:;_b_:_. :.....,1 3"'-"b=-""=f--· ____ _
/ l'> , -, 3 k,q_ ~.,. c.,/ u Y'f'./".J
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
Purge Information .
1 Well Volume (gal): 3 Well Volumes (gal): '2. 1 • 4-(;" Purge Equipment: ~ r ""' J Ce.: p ...,,.,...,,,
I I
Date Purged:· 11?\ A()g.og Purge Time Start: --+!_7.-,_·. -~ _5 __ Purge Time End: _ _..'2~; =2e-..-4...--__
Did well purge dry? Y ~. Actual purge volume: 1-\ , S"-'
,.1.S / '{. <
'v,·+· I Volume '4 Volume .J_ Volume C Volume~ Volume Volume ., ' ----
Temp (0 C) ,., lei "C ')..0,/ A..O ,5" ,Zo,q
pH s-_q<(.. 5-,q O s-. ~g 5'", ~ 1-
S. c: / !{_f. 7 Io 7.f. fi.i.f OJC. 7
B . e.
Turbidity (.JS q, 1.1, J_. /7 1 3.S-
Sample Date: A A fe ~
Sample Information
Sample Time: ,Z. •, 1-4 Sample Equipment: 5.--v~d <:s f V)"f, p
Water Condition (turbidity, odor, etc.):_.!:,--=C.,,,=-~v-___________________ _
Samples Collected(✓):··
VOCs (2 40 ml vials)
/ SVOCs/~l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(°C): Z.O,P) pH: s.i4 SC(umhos):
Comments: IA' IL ::i w,A~r d--rA
°''· 7
o.s·A,)',.__J
Dioxin (1 IL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): fV/4 Turb(NTUs): 4. $ S'
rM, b 6,-1{ ... /1'\ "{-1-J( (I . l,, LJ.t. s-,, 2
t
.L'...!..::::...i---------------------------------pcbwells.frm
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
. Purge/Sample Team: R. fo1~r±..r / C, O!cl.r
I
\"Vell #: rnw-3A
mf' C'S. S-8 '
,..., ti . Comments (well construction, etc): .t-S.$ __ -,-----'--Pi~A_,_P__..fl."----P,_o,-'--q-'-_s_[..J_L __ '2_~_._Cf_2._1_b_M_p ____ _
I I
Purge Information
4-1.&C, Wll.-t/l,i-ulvll"n
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
For 4" well: 3 vole;nes (gallons) = 2.0 x height of water column (feet)
1 Well Volume (gal):
For bailers: 4 bails = 1 gallon
3 Well Volumes (gal): 1.o,4,3 Purge Equipment: /jrvNd fl'>s p vm. p
I l
Date Purged: · t°l APt. l"l'?G) Purge Time Start: /0~ oC? a,,.. Purge Time End : __._\-'--l _1
, 1_3 ___ _
Did well purge dry? Y Actual purge volume: '1-3 °'Al ----v--
Volume i.i;.l;"-1 Volume I Volume.1:_ Volume 3 Volume Volume
Temp (0 C)
pH
S. C.
:i;i. e.
Turbidity
Sample Date:
,., 15. " /~.4 t£?,s
G.o7 Coo 6 , 10
10tvl (rJS,? /o'3. 9
--'1,0~ (,0,,0 2. (6
Sample Information
t°l APR 10,0,q Sample Time: ~/,_1/_:/u_-r ...... __
---
l°t.5
Qi .o~
llt.3
/ ,c, ~
Sample Equipment: :Jv-vt-1df.s
Water Condition (turbidity, odor, etc.): __ __,,_,...>=......__ __________________ _
Samples Collected(✓): ·
V OCs (2 40 ml vials)
v SV0Cs@(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 IL bottle)
Pest/Herb . (1 2L amber bottle)
·Temp(°C): /°} .5 pH: 6',oq SC(umhos): --11..L . .2 DO(ppm): L Turb(NTUs): /. G3
Comments: ------------·----------------------
____________________________________ pcbwells.frm
WELL LOG SHEET Facility: Warren Cou·nty PCB Landfill Location: Warrenton
Purge/Sample Team: E /KIC__ l(J-(_£ / 13 6 7J ,;1[3 0/?
. l Well#: /hW -5
Comments (well construction, etc): J..1
' LJ~\\ T,,.\-..l Oerrl.. ,t::>'I OGfdL -hr t.J~ ?,7_'9c)
Conversion Factors: For 2" well : 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information
1 Well Volume (gal): 3. 5
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = I gallon
3 Well Volumes (gal): / /. S" Purge Equipment: &r.., .... J..J:.s-Qv ...... ~
Date Purged:· 4 /t°I /99,'
Did well purge dry? Y N
Volu1:1e _j_
Temp (°C) :i. ,. +
pH lo.:27 ·
S. c: 18.5
D. 0.
Turbidity .99
Sample Date: 4 /1q /9q
1 I
Purge Time Start: L: ":) 0 pro Purge Time En~i: J : '( -S-p..,._
Actual purge volume: /~ °""""J_
p"
Volume± Volume_Q
0-Hef .so""1''e
Vo!fii!Jle,J-Volume Volume o/o ,'1l --
J__O. CJ -:1_ 0 • 6
b, 2 ~.2
97.6 90~2
/,/3 , q7 -~6
Sample Information
Sample Time: JL/ S--Sample Equipment: --------
Water Condition (turbidity, odor, etc.): _______________________ _
Samples Collected(✓):
V OCs (2 40 ml vials)
V SVOCs~ 1 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
Temp(°C): 2-f>J-pH: t. 2-SC(umhos): ~o;L DO(ppm): ---Turb(NTUs): 0,q 7
1 Comments: ---------------------------------
__________________________________ pcbwclls.frm
·• -L -~· ·,;._, :;· .. ·_:. -~ .
. -WELLLOGSHEET ', Facility: Warren County PCB Landfill Location: Warrenton •. -. . ,', ~ ._... . -..... .
.. Plirie/Sample Team: R. Ko bq.-+J / c. old ~
I
\\'ell#: ffiW, 7
f'V\ f' 4"1., 5,t
CoII1.II1ents (well construction, etc): --==Z=-'' ........... s s~ ___ 10J____;,A_f''-'-"R__,__1 4--'---'oi'-9..._s_w_·_L_":J-=---+_,_,'="''X?"'--' b_wt-=+f _____ _
, 1..' '4 ~ ... 4fl. .-
Purge Information .
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5. x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): -2...\\ 3 Well Volumes (gal): C. q2. Purge Equipment: Jr u,x/.f;,,r Fw"f
Date Purged: · I °' AV' R CJ 0, Purge Time Start: 3 : I S-Purge Time End: _4.._:_2_5-' ___ _
Did well purge dry? Y @, Actual purge volume: _ _._I 0'-'----,4a._,_A_\.._, _
0
.:J.n '.,:/.,·.._./
Volume Z.. Volume 3 Volume'?J_<-£ Volume 1-.Q.}A Volume Volume _j_ ., -
Temp (°C) '-'" iCfr '8 ;q_!) ~c>,3 2.c>, 6 '2 t . 6 2~3
pH . 5.66 ~( 72-:j,6 ( S.BS J; f§Cf S ,9~
S. c: ?75._? 80,7 &,.o 9S:'f 250~5 76~0
D. 0 .
Turbidity . Z.3.S-31-, "3 4~/) 4-o .6 4-o,4 -1-f, 1-
Sample Date: rq Af f<of')
Sample Information
Sample Time: -4-+-'-: _IS-__ Sample Equipment: 5rur1ck::.r b u .,,.,,_D
I
Water Condition (turbidity, odor, etc.):_~~~--------------------
' Samples Collected (✓): •.
VOCs (2 40 ml vials)
X SVOCs@(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle) ·
\
17 l'J pH·. ·5.0.0o Temp(°C): 1,,L-, 7 _ -1 _ SC(umhos): ~ DO(ppm): l'r/fr Turb(NTUs): 4-l . t
Commen~: ________________________________ _
__________________________________ pcbwells.frm
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: _[J-"---c2.,__--'--J-+-t _S-'-"( oiJ....,"'~c ........ c/ __ 1t-'--~---'--L{+---L--'--, --'-IV-'--~--Well#:
Comments (well construction, etc): 2 ''Wt...11 fcA.,( O"-pt\. <{l..31.. ·0':'(l±{_ +. w~ 3,g,,,\-I.JC.. '-I,"
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For hailers: 4 bails = 1 gallon
1 Well Volume (gal):___ 3 Well Volumes (gal): ____ Purge Equipment: b"" ;-tt r-
Date Purged: · L/-( 'l -1 'i.
Did well purge dry? Y
Purge Time Start: r~: oo ------Purge Time End: l ': '-I 0 -------
N Actual purge volume: /CJ J,;;/e,,,-) f...,"T~J -ti-ff ,,,.,_['1 ½_J,..._-;-/e...,-
t3 eAt ~
Volume Volume Volume Volume Volume Volume ------,
Temp (°C) ,.,.
pH
s. c:
D. 0.
Turbidity
Sample Information
Sample Date: Sample Equipment: ~b_<-_.-/_c _,,,-____ _
Water Condition (turbidity, odor, etc.): ~,..._,..-7"u,,.£L'j --"-"--~--------------------
Samples Collected(✓):
Temp(°C):
VOCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bottle)
Metals (1 IL HDPE bottle)
---pH: ----SC(umhos): ---
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): ---
WELL LOG SHEET Facility: Warren Cou·nty PCB Landfill Location: Warrenton
Purge/Sample Team: E «IG fQ. Te,E /f3vB 7,/f 6 0 ~
7
Well#: / J_ -~-------
Comments (well construction, etc): '< we-it c:::,,..-=-=--'-----------------------
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): /, 5 3 Well Volumes (gal): "4 Purge Equipment: _____ _
Date Purged: · 4 /19 /,°i, , I Purge Time Start: I O : 3 0 Purge Time End: --+-,/~)_/_5 __
Did well purge dry? Y @,
. '3 -~c,1/. .
Volume _! ,
Temp (°C) f7.S
pH ~ro. 51
S. C. I oi .S
D. 0 . ./-8-o/o
Actual purge volume:
2 '!IQ(.
Volume 2 Volume --
2[_3 \. I _/
~ -~/
(,_I h -\. ,/ r
D· VV
102 .<g ~,_,\"'
, \../ .,£....._ V -
Turbidity 57,, I 7b-R ~
Volume 3 Volume_£ Volume --
2 ('.)_) 2?.7
C:,_22 6 ,.;7
1 oo.'.) //I. D
~ q3 14~ qr_ re
Sample Information
Sample Date: _4_,__/_f-'-9.___ Sample Time: . / )J ,S-Sample Equipment: Cr.,, -.P~ ~'"' ~
Water Condition ~, odor, etc.) :--=9'-J __ ---=C,:>«...:..>'"'-'--'+_.:..v...c__j_~p-=-v-'-r"{~''Vt.,q.._....:...,,.....:.""..:...c.h_· J _ _;-tt.c.:..:..:....re..,.<-=--_..,....,J<--"-< ..... r:-« ....... s~..L-'1'--'-.r:e, ___ _
-h... I b:-) 'hr ~ .... """1' Le.> --e .,-e...
Samples Collected(✓):
VOCs (2 40 ml vials)
V SVOCsl@l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(°C): ---pH: ---SC(umhos):
1 Comments:
---
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): ---
---------------------------------
________ .,--_________________________ pcbwclls.frm
f: ~ ~ ~r ~-~ 0 ~ // .
"NC Department of Environment,
Hcallh, &. Na111ral Reaourc:es
Solid WaSIC Mana&ement Division •
SAMPLE ANALYSIS REQUEST State Laboratory of Public: Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
SitcNumbcr _____________ SamplclDNumbcr/Namc __ /_i_2---'-i'--'.J __________ _
NamcofSitc fc,,{3 L.F CollectedBy __ L_, _/<._o_~ _______ ID# I" 0
SiteLocation (AJ,Y-011, Cc, · DateCol!ected __ ~_/ __ ,;J_</_~/_"i_f ___ Time / (2 1 a o
Agency: Hazardous W astc V Solid Waste __ Superfund
Sample Type
Environmental Concentrate Comments
Solid (5) Ground Water (1)
Surface Water (2)
✓ Soil (3)
_ Other (4)
Liquid (6) Scef, 'Y,Lv>/: #-
Sludge (7)
I
Other (8)
Organic Chemistry
Parameter
P&T,:GC/MS
Acid:B/N Ext.
2,4-D
_ 2,4,5-TP(Silvex)
chlordane
_ heptachlor
bexachloroben.zene
Results (mg/I)
------hcxachlorobutadiene ------cndrin -lindane
_ methoxychlor
_ t~phene
lL. ~f3s
FOR LAB USE ONLY
Date Received /;, -,:Z//-99 VP
l'C-8.i(MY~.J
Date Extracted 6 -~Y-991/P
DateAn~~~4~
R,pon ~ ~~
Date Re ed;:; ;+--"_-f'--,f--....--
1.ab Number
CHS 3191 (Revised 12/93)
Inorganic Chemistry
Parameter Results(mg/l)(mg/kg)
_ antimony
-
arsenic
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zinc
pH
conductivity ______ _
TDS
flash point ______ _
TCLP Compounds
Inorganic Compounds
arsenic -barium -cadmium -chromium -lead -
-mercury
selenium -silver --
-
-
Organic Compounds
benzene -carbon tetrachloride -chlordane -chlorobenzene -chloroform -o-cresol -m-cresol --p-cresol
cresol -
-1,4-dichloroben.iene
-1,2-dichloroethane
-1, 1-dichloroethylene
-2,4-dichloroethylene
-heptachlor
bexachlorobenzene -hexachlorobutadiene -... hexachloroethane -
_ ~.·ti cthyl ketone
• §}_fro ne
~n , ?•phenol
-~yridil)ef
_ tetrachloroethylene
_ trichloroethylcne
Results (mg/I)
Results (mg/I)
_ 2,4,5-trichlorophenol _____ _
_ 2,4,6-trichlorophenol _____ _
_ vinyl chloride
endrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
" ...
NC Department of Environment,
Health, & Narural Re&0urces
Solid Wutc Manajement Divi,ion
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
Site Number ______________ Sample ID Number/Name __ /;__i_2._8_~'-f.__ __________ _
Name of Site _.,_@_~_,!3,oe.__LF;;;..;... ________ CollectedBy_---=L=-'--aaip~~'-=--------ID #_--'-/_t,_o __
Site Location (.,UH" r: C.IA C.:1 Date Collected ,J ~ l{ /-r9 Time I ?>' /,)0
I
Agency: Hazardous Waste ~ Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments arsenic -
~c D~
barium -Ground Water (1) Solid (5) cadmium ---chromium -Surface Water (2) Liquid (6) '5cJ,w,..,<.J JJ 2. lead ----mercury v Soil (3) Sludge (7) selenium --silver -_ Other (4) -Other (8) ---Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS antimony benzene ---Acid:B/N Ext. arseruc carbon tetrachloride ---2,4-D barium chlordane ---2,4,5-TP(Silvex) beryllium chlorobenzene ---chlordane cadmium chloroform ---heptachlor chloride o-cresol ---hexachlorobenzene chromium m-cresol ---hexachlorobutadiene cobalt p-cresol ---endrin copper cresol ---lindane fluoride 1,4-dichlorobenzene ---methoxychlor iron 1,2-dichloroethane ---
t~aP.hene lead I , 1-dichloroethylene ---~ ~i3 s <O,/0-/?,Rnt -manganese -2,4-dichloroethylene
--mercury -heptachlor
nickel hexachlorobenzene ---nitrate hexachlorobutadiene ---selenium ... hexach!oroethane --silver -methyl ethyl ketone -FOR LAB USE ONLY sulfates ni tro benzene --
6~LJ-99VP -thallium pentachlorophenol -Date Received -vanadium pyridine -d'UJ.f (.Af~ -zinc tetrachloroeth y I enc
Date Extract~-~-99Vp -
-pH -trichloroethylene
j-v1(3'p,OJ -conductivity -2,4,5-trichlorophenol
Date Analyzed 6-~9-991/P TDS 2,4,6-trichlorophenol --
-flash point -vinyl chloride
Reported By -endrin -lindane --Date Reported --methoxychlor
.i ~ 2Ul~4 --toxaphene
Lab Number 2,4-D --
--2,4,5-TP (Silvex)
DHS 3 I 91 (Revised I 2/93)
NC Department of Environment,
Health, & Nawral RCJ1ources
Solid Wute Manaiement Divi&ion
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
Site Number ______________ Sample ID Number/Name __ /Y_2_~_:S-___________ _
Name of Site ........ f1.-'C:::=B'--__ <.._F= _______ Collected By ___ '-_• _/_~_e,_c;_<-______ ID # __ 1_0 _0 __ _
Site Location We:,. ~t: i: ~ (!'Q Date Collected ,; ;'J'f /4'i Time LIJ1 100 .
Agency: Hazardous Waste ✓ Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments arseruc -
AC DS:
barium -Ground Water (1) Solid (5) cadmium ---
Sedi~J.:11--chromium
Surface Water (2) Liquid (6) 3 lead ---
-mercury
..,,,,, Soil (3) Sludge (7) selenium --silver -_ Other (4) -Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS antimony benzene ---Acid:B/N Ext. arsenic carbon tetrachloride ---2,4-D barium chlordane ---2,4,5-TP(Silvex) beryllium chlorobenzene ---chlordane cadmium chloroform ---heptachlor -chloride o-cresol --bexachlorobenzene chromium m-cresol ---bexachlorobutadiene cobalt p-cresol ---endrin copper cresol ---
-lindane -fluoride 1,4-dichlorobenzene -methoxychlor iron 1,2-dichloroethane ---
~aphene lead 1, 1-dichloroethylene --v7 c:::.l?>, <O,ltJ,#nt -manganese -2,4-dichloroethylene
--mercury -heptachlor
nickel hexachlorobenzene ---nitrate hexachlorobutadiene ---selenium ... bexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene ---thallium pentachlorophenol
Date Received 6 -o'<~ -99 VP --vanadium pyridine -I) e..<3j--.J't:'foJ zinc ' tetrachloroethylene
Date Extracted i -~1'-9'7-V/J --
-pH -trichloroethylene
P<!-8,.s( A1317?0 J -conductivity -2,4,5-trichlorophenol
Date Analyzed ~ -.:::l..'9-99VP TDS 2, 4, 6-trichlorophenol --
-flash point -vinyl chloride
Reported By --endrin
lindane --Date Reported --methoxychlor
'J~::}2 0 1" 5 --toxaphene
Lab Number 2,4-D --
--2,4,5-TP (Silvex)
DHS 3191 (Revised 12/93)
I
l
NC Department of Environment,
Health, & Nawral Ruourccs
Solid Wutc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, North Carolina 27611-8047
Site Number ______________ Sample ID Number/Name __ /_¥_2._~__.f, __________ _
Name of Site Pc .B <-.F Collected By __ L_. _./?_o~s_c ________ ID# / o 0
Site Location We ,,.}""C."' C" I Date Collected t: I 2.'f /9"1 Time ID ·e o
I r-
Agency: Hazardous Waste '-Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments arseruc -
Ac vc:; -barium
Ground Water (1) Solid (5) cadmium ---
iccl1 "Y,,J-tJ:.. i -chromium
Surface Water (2) Liquid (6) -lead --
-mercury
..,.........-Soil (3) Sludge (7) selenium --silver -_ Other (4) -Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS antimony benzene ---Acid:B/N Ext. arsenic carbon tetrachloride ---
2,4-D barium chlordane ---2,4,5-TP(Silvex) beryllium chlorobenzene ---chlordane cadmium chloroform ---beptachlor -chloride o-cresol --hexachlorobenzene chromium m-cresol ---hexachlorobutadiene cobalt p-cresol ---
endrin copper cresol ---lindane -fluoride 1,4-dichlorobenzene --methoxychlor iron 1,2-dichloroethane ---
_ ~a~ne lead 1, 1-dichloroethylene --v' ~ 1. <0,/0~ -manganese -2, 4-dichloroethylene
--mercury -heptachlor
nickel bexachlorobenzene ---nitrate hexachlorobutadiene ---selenium ... hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene --thallium pentachlorophenol
Date Received 6 -Pl'I -99Vf' --vanadium pyridine --PCB'J-(MTDn>J zinc tetrachloroethy Jene
Date Extracted 0 -,;;2. "8" -99-V,P --
-pH -trichloroethylene
(/l~J~J -conductivity -2,4,5-trichlorophenol
Date Analyzed '2 -;..:?9 -99VP TDS 2, 4, 6-trichlorophenol --
-flash point -vinyl chloride
Reported By -endrin -lindane --Date Reported --methoxychlor
::1!12 0,7;6 --toxaphene
Lab Number 2,4-D --
--2,4,5-TP (Silvex)
DHS 31 91 (Revised 12/93)
..
I
NC Depanment of Environment,
Health, & Narural Re.aource,
Solid Wutc Management Division
SAMPLE ANALYSIS REQUEST S1&1e Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleigh, Nonh Carolina 27611-8047
SiteNumbcr Sa.mplelDNumber/Name / <j 2 i'1 ---------------------~-----------
NameofSite ,0~.,6 LF Co II ec t ed By L . Rt> E---
Site Location Wc1Y-rc...-.. Co .· Date Collected 6, IL '-f /e,9 Time J [) .' l) 0
' I ,
Agency: Hazardous Waste L Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments arsenic -
l?cP~ barium -Ground Water (1) Solid (5) cadmium ---s:~ efl wt• d J. -chromium
Surface Water (2) Liquid (6) £ -lead --
✓ Soil (3) -mercury
Sludge (7) selenium --silver -_ Other (4) -Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS antimony benzene ---Acid:B/N Ext. arseruc carbon tetrachloride ---2,4-D barium chlordane ----2,4,~-TP(Silvex) -beryllium chlorobenzene -chlordane cadmium chloroform ---beptachlor chloride o-cresol ---hexachlorobenzene chromium m-cresol ---hexachlorobutadiene cobalt p-cresol ---endrin copper cresol ---lindane fluoride 1,4-dichlorobenzene ---methoxychlor iron 1,2-<lichloroethane ---
~hene lead 1, 1-dichloroethylene ---<O./IJff&.. manganese 2,4-dichloroetbylene ~ Bs --
--mercury -heptachlor
nickel bexachlorobenzene ---nitrate hexachlorobutadiene ---selenium ... hexachloroethane ---silver -methyl ethyl ketone
FOR LAB USE ONLY sulfates nitrobenzene --thallium pentachlorophenol
Date Received 6~4-9WP --
-vanadium pyridine -{PC,8:S yi:>70) zinc tetrachloroethylene
Date Extracted ~ ~-~~ ---pH -trichloroethylene PC8 {/tfTt770 -conductivity -2,4,5-trichlorophenol
Date Analyzed t,-"'-9-99VP -TDS 2, 4, 6-trichlorophenol --flash point -vinyl chloride
Reported By -endrin -lindane --Date Reported --methoxychlor
9!J 2 0,1? --toxaphene
Lab Number 2,4-D --
--2,4,5-TP (Sil vex)
DHS 3191 (Revised 12/93)
NCDEHNR
Division of Waste Management
D Superfund Section
Organics Lab: /
Inorganics Lab: __
D Hazardous Waste Section
D Solid Waste Section
CHAIN OF CUSTODY RECORD
Project Name: w P<~R ~/\J l,.,,,v'r1f pe r:;_ L11-µ /J FtLJ.. Sampled By: 1:1:, ~.~A/
Site ID # (NCD#) Sampler ID
Location: tJ P< flu 1..1 Tb 'JI_ Telephone:~ z:, J, 2---X o l -::.::+3>13
Address: Date Sampled: G/ ✓ <f/;i.,a .... '14'
Time Sampled:
Sample Types: Soil ✓ Water ✓ Waste Other ✓
• ;::: 7-6:..-m~/":..,
;,'
Remarks: 6 '.Lo"-1:, '& . ,.-tu_ $' ---"-J n,/~.,. m~J,,~ ,:,
D ,L,Q ~ '_Ii "i r1 -\--kc__ c,.,,_ .,....(,\7 "'\.. i; H-t--rYl~J , -"'-
'
rS.) .. t...~t:> u -hL 5.~J ,...:., o,,-f <---/i~ b..,,, IJ ,/e. C>•, ·-fi,., J .. --v) -Fi ifr,,_
Field Sample 62.,,~ G..';L..l 6 .l,i.:> (. ·1.. L lY'.l ... .;, ·t, "l... ".) D"\..O~'1...~ o ·J...O~ "2..-S-6)....o b ·z....G. 6-:;....or,:;1._ 7
Numbers 62..o 62...~ 6~0(';.2.A l> ).....() '""3 <'.) 0'1..o(;,.) j t> "2,o b 3 "2... 6)..0G,.} 3 _cn_or:,~
C>-"l...-o b '.> ', c,1.-<'.)~)(.. o-i-o '->'1 ()J .... <>'-"> g 01....06)'t 02...o(:;,_<-/.~
Relinquished By: -~ :(~ Date: ?f--2-(~ 11 Time:_l/:~_ ---4
(Siirnature),,,...,.
Received By: --Yk~ ,d, (?a1~k1_...., Date: !I::_;? t--lj__t/ Time: //.'JS ··-
(Signature)
Relinquished By: Date: Time: --
(Sil'nature)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
(Siirnature)
Received By: Date: Time:
(Signature)
~
Results Reported{_ J L ~~a,,,C__ Date: S:-/7-?1 Time:
(~~e)rr
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~:.c i)cpartmcnt of En.vironmcnt,
li.·:,,i,,, & Natu ra l Resources
So!i .'s W:,stc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sit(: Number Field Sample Number ·. Q)....,.O .{:, -:t... I ----------------. .
Name of Site VJ AflRf.N GuNN PCB LA-MOP 1'st'c Location_W~· ---'-f(f),-'---'-{{,...C..e::C...C.w-'-·-LTu_N_· _______ _
Collected By IJ-2, l'y,J ID# ___ Date Collected · \,!-1,D '-fl-j ·
Agency: Hazardous Waste · Solid Waste --=::::::_ Superfund
Sample Type
Environmental Concentrate Comments
_~Ground water (1) Solid (5) rnw I
__ Surface water (2) ~Liquid (6) ____________ _
_ Soil (3) Sludge (7) __________ _
_ Other (4) Other (8) __________ _
Organic Chemistry Inorganic Chemistry
Para1:1eter
P&-i':GC/MS
Acid :B/N E;:t.
l\1TBE
Resul•-:(mg/1) Parameter Results (mg/I) (mg/kg)
/'pc.,_B __
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
1
1
--·-· --------· Jron IJ.:ad
1
1
_______ ------__ Mangar.cse
__ Mercury
I
-= Nitrate ---Sdcnium
.. Radiochemistry I= ~'.:;r::e,
1 · ~>~~~·;:::~;~:-····---R-cs--u-lt_s_(_P_C_!,-11-) j ---!:c
! --Co:1ciuclivity
·-·--I ---' TDS ---1-----
1 TOC
Microbiology
-------
.----... -.... --
-------
--------
··· -~·TCLP Compounds
Inorganic Compounds
Arser,;(
B::i.:ium
Results (mg/I)
-~~Fl\, .... ;E--0----
Lead = Merf~iY 1 9 1 ..... 9 ....... 9~--------
Selenium = ~\Sf:RFUND SE.....,:C'--'-T_IO_f1
__ _
Organic Compounds
benzene
R~rnlts(mg/1)
carbon tetrachlor~ii:: ,
chlordane
chlorobenzene
chloroform
O•cresol
m-cresoI
__ p-cresol
cresol
------·--;
I f
! -------"~ 1,4-dichiorobenze•1e ______ j
1,2-dichloroethanc. l
__ 1,1-dichlorot:.thykn~ ·--~ !
2,4-dinitrotoluenc l
__ heptachlor ___ · i
hexachlorobenzece -----------
hexachlorcbtadien~ l ------, hexachlorneth:1.nc !
i methyl ethyl ketc•,;,;> _____ 1
nitrobenzene • ---... -~·--· .. ·-· ~--~-
--pentachloropheno[ ;
pyridine ________
1
!
__ tetrachloroethylrne ______ 1
__ trichloroethylene ----------·-,
2,4,5-trichlorophenol
--2,4,6-trichlorophenoi ------j
~-vinyl chloride ---------l
endrin ______ I
lindane ------1'
methoxychlor ______ I
tcxaphc~e
-j/ 2,4-D
2,4,5-TP (Silvex)
.S:7
N.C. Department of E1lvironment,
I lca!t'r:, & Natural Resources
Solid Was1c Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Strcel
Raleigh, North Carolina 27611
Site Number .: · Field Sample Number . . 01.-o C.:.L "2-
Name of Site UJAR.R£N GvNN -P.CB ~DP11st'e Locati~n_W;:;..· --'-NJ-..,__,_P-.=e:=~..:...-LJb.c:....N....:..--·---------
Collected By IJ-2, .,JttJ ID# ___ Date Collected __ l-_.._j--'-1'""=--·· _. ·_-_'t_J..__ ___ .Time /->·.IS"'
Agency: Hazardous Waste ·Solid Waste _.:::::::_Superfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) _ Solid (5) rnw iA Cadmium --
;,;tc91quid (6)
Chromium --__ Surface water (2) Lead --__ Mercury
Soil (3) Sludge (7) Selenium \
--Silver --_ Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Rr:,ults(mgfi:' Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I)
_P&T:GC/MS Arsenic benzene ·-----Acid:B/N EY.1:. Barium .::r..rbon tetrachloride --------MTBE Cadmium chlordane
✓ PCB ----·-· --··-~-_ <e_.ooo~ Chloride chlorobenzene ----Chromium chloroform --------__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-cresol ----------Lead i::resol ------.,. __ Manganese 1, ~-dichlorobenzene -------
--__ Mercury l ,'Z-dichloroethane ---Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene -------······-··--·-·--Zinc hexachlorobutadiene ----Parameter Resclts (PCi/1) _pH hexachloroeth2.ne --__ Gross Alpha __ Conductivity methyl ethyl kewne --Gross Bet3. TDS nitrobenzene --·-----------·-·-·· -· ---TOC _· _ pcntachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene -~--trichloroethylene ----Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --__ 2;4,6-trichlorophenol ----------vinyl chloride
endrin --lindane
Date Received 4-J.J-qq77d --Reported by methoxychlor --tfJcS('/11-SV~ --tcx~phene
Date Extracle<l t./-;23-"/rtf:$ Date Reported --2,4-D
f' C-6 (MS??Y_) 991239 --2,4,5-TP (Si lvex)
Date Analyzed L/--~-9'J'yp Lab Number
Ill IS 31 111 (Revised 2/91) --
N.C Ocpartm~nt of E:;vironment,
I lc~l,h, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number Field Sample Number ·. 0 :-J: • .JJi •b ')_ "3. ---------------
Collected By IJ-2, t>,Y-,J ID# ___ Date Collected ' 4-1,q '-ft-'\ • . -Time / 'f-, 2 '{
Agency: Hazardous Waste Solid Waste __.:::::_Superfund .. . -~ 1 •• TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
~Ground water (1) /Y) lJ ~ --_ Solid (5) Cadmium --
~iquid (6)
Chromium --__ Surface water (2) Lead --__ Mercury
__ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
.. Parameter Results(m~/1) Para"ieter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC_/MS Arsenic benzene ------Acid:B/N Ext. Barivm carbon tctrachlorid~ ------··-·-MTBE Cad:nium chlordane --~ Pc..\j ~O, OO(J/~4;. "--Chloride
-----· --chlorobenzene --.. Chromium chloroform ------
-----__ Copper o-cresol --Fluoride m-cresol ·--------
--Iron __ p-cresol ---Lead cresol ------
-----,.-----__ Manganese --1,4-dichiorobenzeu(;
--__ Mercury ----1,2-dichloroethane
--!'7itrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --·--Silver __ heptachlor -----Radiochemistry Sulfates hexachlorobenzene ----······-····-·-•·--•·~·-···--·-· .. ·-Zinc hexachlorobutadien~ --Parameter !~esults (PCi/1) _pH hexachloroethane ---
·--Gross /'. :pha --Conductivity __ methyl ethyl ketor:::
Gross Beta TDS nitrobe:13ene ~-.. -.. --. ----------·-TOC __ pentachk,rophenol --
--__ pyridine
Mkrobiology --_-_ tetrachloroethylene
---__ trichloroethylene --Parameter Resuits (Col/J 00ml) __ 2,4,5-trichloropheno1 --
----__ 2,4,6-tric!-Jorophencl
----__ vinyl chloride
endrin --lindane
Date Received 4-cJ )-19 1Jd Reported by --
--methoxychlor
tf'CB (AfSOt} __ tcxaphene
Dale Extraclc.:<l Lf ;23-yYV~ Dal_e Reported --2,4-D
/JMrAI~ $91240 _ 2,4,5-TP (Silvex)
Dale Analyt.c.:d l/-~ 6-91/f' Lab Number --1)1 IS 319 1 (Revised 2/91)
.
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i ' j
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;
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' .
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l\'.C.· Department of Environment,
I ka)th·, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field Sam pie Number. . · : 0 :t-o , (, l.:, '-1 , ------~-------------------------
Name of Site (J} ARR£N GvNN P cg L,ttt.JDP 11sft'e ,Locati~n_. ~w_·_~--'---'--tl....C...e:....C...J,J_· ~Jb_lJ_· ________ _
Collected By IJ-2, y,j,J ID# ___ Date Collected · \.,l-15 ·-~-'\· .r. · .Time J/; /0
Agency: Hazardous Waste Solid Waste ~Superfund .. TCLP-Compounds •' ----
Sample Type Inorganic Compounds Results(mg/n
Environmental Concentrate Comments Arsenic --
~Ground water (1)
Barium rnw 7:;f; --_ Solid (5) Cadmium --
~LiqWd (6)
Chromium --__ Surface water (2) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium .,
--Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. Parameter Results(mg/1) Par-meter Results (mg/I) (mg/kg) Organic Compounds Results (mg/!)
_P&T:GC/MS Arsenic benze=--i~ ·-------Acid:B/N Ext. Eari;;:n carbon te~rach l0ridc ----·---MTBE Cadmium chlofdiwe
--✓ PC.\3 ~.ooo~~ ---Chloride. ------. chlorobcnzene --Chromium chl0rc,form ------__ Copper o-cresol ----Fluoride m-cre;so! ------
-:I --Iron __ p-creso! ----Lead cresol -------· --.... :-__ Manganese 1,4-dichlurobenzene ---~----__ Mercury 1,2-dic:-iloroethane >
-------. ----I C Nitrate 1, l-dichl0rocthylene ------,.
Selenium 2,4-dinitrotoluene -----·-Silver __ heptachlor -----Radiochemistry Sulfates hexachlorobenzene -----·····-·----Zinc hexachlorobutudiene ----Parnmeter R It'-r·•"i/1) _pH hexachlorocthane esu ._. ,-,____ --·------. __ Gross Alpha _________ __ Conductivity __ methyl ethyl ketone I -I Gross Beta TDS nitrober.~ne -. --= pentachlorophcnol -------------· -TOC --
--__ pyridine
Microbiofogy --__ · tetrachloroethylene ,·--------I trichloroethyiene I ----! Parameter Re:-nlts (Col/100ml) __ 2,4,5-trichlorophenol
I --I i -----__ 2,4,6-trichlorophe:iol ! I vinyl chloride I ------endrin --
Date Received '-}-;}... J -q q 17dReported by
lindane
--methoxychlor
{J_eB(A1~ --toxaphc;1e
0;.itc Extractc<l°(/-;?3~-p.JA! Date Reported --2,4-D
PeB0tvZ1~" 991241 _ 2,4,5-TP (Silvex)
Dale Analyzed "/--<~-YP Lab Number --1)1 IS 3191 (Revised 2/91)
i
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l
N.C. Department of Environment,
I lc~ltli, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field Sample Number-, , · 0,?-,o {. LS° ---------------
Collected By lJ-2, ,,.y',J -ID# ___ Date Collected __ l-..... i-__,_l·__..1_'-_fl_j....._ ___ Time / S: l(--5
Agency: Hazardous Waste Solid Waste ~Superfund ··}; TCLP Compounds -- --
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --
_('-Groundwater (1)
Barium
/I) l,J ~---_ Solid (5) Cadmium --
~iqllid (6)
' Chromium --Surface water (2) Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium ' --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results ~~1g/l) (mg/kg) Organic Compounds Results (mg/I)
_P&T:GC/MS Arsenic benzene ------_ Acid:B/N E::-.1:. Barii.;m carbon tetrachloride ----------MTBE Cadmium chlordane
·--✓ PCB ----------·----<o, ~oo/,ao.nf. Chloride chlorobenzene -----,, Chromium chloroform --------__ Copper o-cresol -----Flucric:-: m-cresol ·--·-----Jron __ p-cresol -----·-Lead cresol --------·-----__ ,;,....;_ ___ . -__ Manganese --1,4-dichlorobenzene
-__ Mercury 1,2-dichloroethane ----1,1-dichloroethylene -----~-----Nitrati: --·------2,4-dinitrotoluene ' Selenium ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-····-·-·--· Zinc hexachlorobutadiene ----Purameter Results (PCi/1) _pH hexachloroethane ----------__ Grnss Alph<---Conductivity --methyl ethyl ketone I Gross Beta TDS nitrcbenzene .. ··------. ~···--· ------!
TOC __ pentachlorophenol I --
----pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene I i>aramder Results (Col/iOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol --
----__ vinyl chloride
endrin --lindane 4-:1/-qq M --Date Received Reported by methoxychlor --·~ .... l,.o ... ,., f)CB(il't~~
Dale Extracte~~ ~~'3'7ve\.71/Datc Reported __
9
_
9
_
1
_
2
_
4
_
2
__
Dale Analyzed L/-~7-1/9-VP Lab N'i.1mbcr ---------
__ \.vXupuva1v
2,4-D
_ 2,4,5-TP (Silvex)
1) l IS 31')1 (Revised 2/91)
N.C. Department of Environment,
I k;ilth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field Sample Number ·. D ~ -' Z,,t> ______ __;;_..;c.. _______ _ ---------------
Collected By IJ-2,rJl-,J ID# ___ Date Collected · 4-1 '1· ·-~-:'\ ' , ·
Agency: Hazardous Waste ·Solid Waste ~Superfund ----
Sample Type
Environmental Concentrate Comments
/ lY'l lJ J L Ground water (1) Solid (5)
~iquid (6) Surface water (2)
Soil (3) _ Sludge (7)
_ Other (4) Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Results (mg/I) Parameter Results (ng/1) (mgf"g)
_P&T:GC/MS Arsenic ----Ac:d:B/N Ext. Barium -------·----·--MTJE Cadmium
✓ _?CB <o. ooos~ = Chloride
·-•·-
· Chromium --
--__ Copper
Fluoride ----
-------, _Iron
Lead --I = Manganese ----:-· ------
-----,. 1 __ Mercury
Nitrate ----Selenium --Silver ·-Radiochemistry I Sulfates I , __
........ , -----·----·• ---J Zir:c
Parameter Results (PCi/1) , pH ! --Conductivity __ G:·oss Al[)ha
,--:!" r t~ 1-~-OS., Be.u , TDS
------
1
, _To_c_-__
Microbiology
Parameter Results (Coi/lOOml)
Date Received i.f-;J.. J-9q 77'j Reported by _______ _
~(pt~·-orr)
Date Extracte<l ij-:..Z.;?--97i'~Date Reported~~------
,PCB~~~oV 991243
Dal e Analyzed 4/-o?_ 7--r7yp Lab Number
DIIS 3191 (Revised 2/91) ---------
i
TCLP Compounds
Inorganic Compounds Results (mg/I)
Arsenic --Barium --Cadmium --Chromium --Lead --__ Mercury
Selenium .·,
--Silver --
--
--
--
--
Organic Compounds Results (mg/I)
benzene --carbon tetrachloride ---chlordane --chlorobenzene --chloroform --o-cresol --m-crcsol --__ p-crcsol
cresoi --1,4-dichlorobenzene --
--1,2-dichloroethanc I 1,1-dichloroethylene
2,4-dinitrotoluene --__ heptachlor ,,
hexachlorobenzene --hexachlorobutadiene --hexachloroethane --
--methyl ethyl ketone ' .., i mtrober.zene ··-· 1
__ pentachlorophenol I
__ pyridine 1·.
__ tetrachloroethylene.
trichloroethylene I
2,4,5-trichlorophenol _____ _
2,4,6-tricrJorophenol I
--vinyl chloride ---
endrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
------
.__ _______________ __,
NC "Department of Environment,
Hc.allh, & Narural Ruources
Solid Wutc Man.agcment Division
SA1\1PLE ANALYSIS REQUEST St.ate Laboratory of Public Hc.allh
P.O. Box 28047, 306 N. Wilmington St.
Raleii:h, North Carolina 27611-8047
Site Number Sample ID Number/Name /'{ 2. 'i 1 -----------------"'-----------------
Name of Site &s Cr Collected By l. ,z.. >-<-ID# I QV ---------"'-------------------------------
SiteLocation----,1,""',b-.) .... a"'-'--r ..... r:_.,,....,__,;_ ..... t"--"-o_· _____ Date Collected __ 7J~/_2._2-....,jr,_ ,_ ..... _-iq:::==========--T-im_e _____ ~C/.::-_-'-_:::.,,,,_'?_ ....:;;.-0=====~
Agency: Hazardous Waste _iL' Solid Waste __ Superfund TCLP Compounds
Sample Type
Environment.al Concentrate
Ground Water (1) Solid (5)
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Organic Chemistry
Comments
Inorganic Chemistry
Inorganic Compounds
arsernc
barium
cadmium
chromium
lead
mercury
selenium
silver
Results(mg/1)
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results (mg/I)
2,4-D
2,4,5-TP(Silvex)
chlordane
heptachlor
hexachlorobenzene ------hexachlorobutad:ene ------endrin
lindane
methoxychlor
toxaphene 2 fc.-o-r(jo11kj t:J, ()0O6(f?Ol:
&,-nG.cls jJ,.eJ~ th c:f, ~o~flq ra--. , V ------
Reported
Lab Number 991279
DHS 3191 (Revised 12/93)
antimony _______ benzene
arseruc
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zinc
pH
conductivity -------TDS
fl~hpoint ----'------
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobenzene ______ _
1,2-dichloroethane
1, 1-dichloroethylene ______ _
2,4-dichloroethylene
heptachlor
hexachlorobenzene
hexachlorobutadiene
... hexachloroethane
methyl ethyl ketone
nitrobenzene
pentachlorophenol
pyridine
tetrachloroethylene
trichloroethylene
-------
-------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lind.ane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
NC Dcpart:nent of Environment,
Health, & Narural Resources
Solid Wu~ Management Division
SAMPLE ANALYSIS REQUEST State Labontory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Raleii,:h, North Carolina 27611-8047
Site Number ______________ Sample!D Number/Name -~L~i'--2--'fL.-2-___________ _
Name of Site __ A_t:_· (3 __ L_r _______ CollectedBy __ L_-_lln-________ ID# __ J_ro_· __ _
Site Location ~ Co Date Collected t.J-/z. 2,. / d'if ------"--"--"'---'------.L.., I -t-r Time_..._9_}_0_· -S: __
Agency: Hazardous Waste \/"solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic CompoWlds Results(mg/1)
Environmental Concentrate Comments arseruc -
u,~-Eff4~ barium -Ground Water (1) Solid (5) cadmium ---1 chromium -Surface Water (2) Liquid (6) lead ---
-mercury
Soil (3) Sludge (7) selenium ---silver -
-Other (4) -Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic CompoW1ds Results(mg/1)
P&T:GC/MS antimony benzene ---Acid:B/N Ext. arsenic carbon tetrachloride ---2,4-D barium chlordane ---2,4,5-TP(Silvex) beryllium chlorobenzene ---chlordane cadmium chloroform ---heptachlor chloride o-cresol ---
hexachlorobenzene chromium m-cresol ---
hexachlorobutadiene cobalt p-cresol ---
endrin copper cresol ---lindane fluoride 1,4-dichlorobenzene ---
methoxychlor iron 1,2-dichloroethane ---
t/tphene lead 1, 1-dichloroethylene
c/ d, .!" b.t)(Jl'Jl'/VIAI --
-manganese 2,4-dichloroethylene -,, mercury heptachlor ---nickel hexachlorobenzene ---nitrate hexachlorobutadiene ---selenium ... hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nit ro benzene --
Date Received '-/-,,;i._,;l.. -<t''f-Vf' thallium pentachlorophenol --vanadium pyridine
(Pcg§-e,sP'i:J --
ZillC tetrachloroethylene
Date Extracted l/ -,Z 6 -Yo/ J/f' --
-pH -trichloroethylene
~MJ~ -conductivity -2,4,5-trichlorophenol
Date Analyzed S:-//-97/P -TDS 2, 4,6-trichlorophenol -
-flash point -vinyl chloride
Reported By -endrin -lindane --
Date Reported --methoxychlor
991280 --toxaphene
Lab Number 2,4-D --
--2,4,5-TP (Silvex)
DHS 3191 (Revised 12/93)
N.C Department of Environment,
I lc.!.lth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number Field S;:,mple Number.: · & 1.......() ( 1......l ----------"--'-----------------------
Name of Site fJJARR-f-N . CvNN PCB LMJOf 11sfte Location_\w=-·· -·-'--~-'--'-K-"''l!:=-·;_,;_w_._Tb...;,..._;_N ________ _
Collected By IJ.. 2, f>1,,J ID# ___ Date Collected · Y-'1.D '-!t '\ Time _ _,q_:_'1-'----"'~--
Agency: Hazardous Waste · Solid Waste ~ Superfund
Sample Type
Environmental Concentrate Comments
_ Solid (5) _!{"G round water (1)
__ Surface water (2)
Soil (3)
~Liquid (6) ________ _
Ts_ Sludge (7) _________ _
_ Other (4) Other (8) -------------
Organic Chemistry Inorganic Chemistry
. Parameter Results (mg/I) Results (mg/I) (mg/kg) . Parameter
Arsenic
Bariull!
Cadmium
Chloride
Chromil'ln
__ P&T:GC/MS
_ Acid:B/N Ext.
MTBE
-✓ Pc.,2 ¥"
Radiochemisti♦y
__ Copper
Fluoride
Iron
Lead
__ Mangau;;se
Mercurv
--,I Nitrate
Selenium
Silver
Sulfates
.......... -···-·-·---------·-~ Zinc
P2rameter
__ Gross Alpha
Gross Bet,:
Result!, (PC!/1) __ pH
______ i __ Conduc~;vity
Microbiology
Para III eter . Results (Col/100ml)
b ate Received l./-;J. J-C/9. 17d
Aili~
Date fat'"clc<l ~1/e,:,,,/
DJIL: A naly~(!,.~9Jl'P
1)1 IS J l'J I (llcviscd 2/91 )
TDS
TOC
Reported by ----------
Dale Reported --------
Lab Number 991244 ----------
' j
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cres61
__ p-cresol
crcsol
1,4-dichlorobenzene
1,2-dichloroethane
Results (mg/I)
Results (mg/I)
---·----
-----
1, 1-dichloroethylene
--2,4-dinitrotoluene ------
--heptachlor
hexachlorobenzene
h::xachlorobutadiene I ------hexachloroeth2.ne
methyl ethyi ketone ------=== I
nitrober.zen~
__ pentachlorophenol -----!
__ pyridine I
__ tetrachloroethylene
__ trichloroethylene ,• ·
__ 2,4,5-trichlorophenol ______ ;
2,4,6-trichlorophenol I = vinyl chloride
endrin
lindanc
methoxychlor
__ toxaphene
2,4-D
__ 2,4,5-TP (Silvex)
'
I
I
I
I
N.C. Department of Environment,
l lcalih, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
0 . ..., ,-v Site Number · Field Sample Number : · · ).....p ; -.i:---o: ·-,. ----------------.,
Name of Site llJ ARR.fN G VNN . p CB LMJDP1~e Locati~~--_w:;_·· -'Ml'-. '-----'--'ft=· e:~W'--Tu~rJ.;_. _. __ -_-'.!_.) _· -----
Collected By !J-2, rJ!,;J ID# Date Collected .• • Y-1 q '-"l '1, ----
Agency: Hazardous Waste Solid Waste _.:::::_Superfund -._. · TCLP Compounds --· --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/ Ground wal~r (1) l )..___; --_ Solid (5) /Y1 tu Cadmium !1 ,: --Chromium --Surface water (2) iquid (6) Lead ..
--__ Mercury
Soil (3) udge (T) Selenium " ·l --Silver ---. _ Ot:ier ( 4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --I
---j
. Parameter Resclts(mg/1) Parameter Results (mg/I) (mg/kg) ! Organic Compounds Results(mgil)
_P&T:GC/MS Arsenir. I benzene ----__ Acid:B/N Ext. T> • carbon tetrachloride _..,anurr. ---·---MTBE Cadmium chlordane
✓ -'--------··-·-----Pc:;J3 <-o.~oo~ Chloride chlorobenzene ~ --Chromium chloroform ----__ Copp'.!r o-cresol ------Fluoride m-cresol ------· --Iron __ p-cresol ----------. -Lead cresol ----------·
--_____ Manganese 1,4-dichlorobenzene --
--__ Mercury ·---1,2-dichloroethane -
--Nitrate 1, 1-dichloroethylene --Selenium 2,4-dinitrotoluene ~-----Silver __ heptachlor -
Radiochemistry. --
Sulfat".'.s hexachlorobenzene --· ----·---······-··--· Zinc hexachlorob:.:tadienc ----Purumeter Results (PCi/1) pH hexachloroethane -----·
--Gross Alpha __ Condu-::tivity --methyl ethyl ketone
Gro:,s Beta TDS nitrobenz~ne ·------·----· -----------TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--_._ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --2, 4,6-trichlorophenol ----= vinyl chloride
-~
----endrin --lindane
Date Received 4-~;2 /-C/ 1' 1bJ Reported by --
--methoxychlor
__ toxaphene
'
I
' I
I
~g 2,4-D ~ Dale Extraclc<l ~~tv7/Datc Reported
S91Z45 --~ . __ 2,4,5-TP (Si lvex)
Dale AnalyLc <l -~ · ~ Lab Number
I)I IS 31'J I (ltcvi~cd 2/91) --
N.C. Depurtm.:nt of Euvironment,
J lc;ilth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
. ,.; ...
Sile Number Field Sampie Number QL-<:) l l..-Cf ---~---------------------------
Name of Site ,JjARRf-N Guf\J]Y p CB UnJOf 11st'e Location_W~· _MJ,~A..-'-e:-'-~~Tl?_N ________ _
Collected By IJ-. 2, .,.y',J ID# ___ Date Collected __ \,~l_--_l _q_· __ ft_-~J ____ Time I L l ">o
Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -----
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium -Q ·-. k --Ground water (1) _ Solid (5) ( V\, ~ c.._ Cadmium --
l/&fl:iquid (6)
Chromium --Surface water (2) Lead --__ Mercury
Soil (3) Sludge (7) Selenium ' --
/other (4)
Silver --Other (8) --
--
--Organic Chemistry Inorganic Chemistry ---
_ Parameter Results (mg/I) Parameter Resc!ts (mg/I) (mg/kg} OrgRnic Com!,ounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Bariu~ c;irb,)n tetrachloride ----·--· --·-MTBE Cadmium chlordane
✓ pc.,3 --------·· --chlorobe
0
nzene ---· < O. 000/f?flM. Chloride ----·-Chromium chloroform ------_-_Copper o-cresol ------fluoride m-r.:reso[ ------Iron __ p<:rcsol --------Lead crcsol -----------__ Manganese --1,4-dichlorobenzene --
--__ Mercury --1,2-dichloroethane
Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor ---·· Radiochemistry Sulfates hexachlorobenzene --------······-··--·----Zinc hexachlorobutadi:ne ----Parameter Results (PCi/1) _pH hexach!oroethane ------__ Gross Alpha __ Conductivity i --methyl ethyl ke.tone
Gross Beta TDS . r.bober.zene -· .. ---~-= --TOC __ penlachiorophenol ---
--__ pyridine
Microbiology --__ tetrachloroethylene
-I __ trichloroethylene -----Parameter Results (Col/lOOml) ! __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ----
------vinyl chloride
endrin --lindane
Date Received /..}-;l)-qq r7d Reported by --
--methoxychlor
/JC8~V __ toxap hene
Dale Exlraclc<l /,t--9l~Dale Reported --2,4-D
I' CB (MsOV. 991246 _ 2,4,5-TP (Si lvex)
Dalt: Analyzed ¥-~7-99J//' Lab Number --DI IS :li'Ji (llcviscd 2/91)
N.C. Department of Environment,
I lc~lth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number ---------------Field Sample Number . · . @)"';O 6 ,1, ~-
Collected By IJ-2, iv1',J ID# ____ Date Collected_~\,l~-~1_1~'---~-':\~----· Time _____ _
Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds ----
Sample Type foorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --
_£Ground water (1)
Barium e., c,,u s --_ Solid (5) Cadmium --
_/surface water (2) ~quid(6)
Chromium --Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium ' --Silver --_ Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg)··: Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic I bcnzer.: ------Acid:B/N fa.t Barium . carbcn tet :·aci,'.oride ; --.--. --MTBE Cadmium ' chlo~dane
✓ PCB ---. ----<o,ooo~.M.-Chloride ' chlorobenzene --I -··-Chromium chloroform -------__ Copper ·1 o-cresol ----Fluoride . m-cresG1 --------Iron • __ p-cresol --_.., __ --i Lead I crcsc,l ------· --· L
------__ Manganese l --1,4-dichlorobenzene --
--__ Mercury ! --1,2-dichloroethane --Nitrate __ 1,1-dichioroethylen~ __ ----Selenium · 2,4-dinitrotoluene. -------· Silve: heptachlor ----Radiochemistry Sulfates hexachlorobenzene --.. i ---· ······-··--·----· Zinc I h~xachlorobutadiene
Results (PCi/1) ----Parameter _pH hexachloroethanc
i --~--·-__ Gross Alpha __ Conductivity I --methyl ethyl ketone ~-·· . Gross Bet3 TDS I nitrcbenzene -------··-! ----TOC __ pentachlornphenol --
----pyridine
Microbiology --__ tetrachloroethylene
,-__ trichloroethyiene l --i Parameter Result~ {Col/lOOml) --
·----
----
4-.d--191!.::! Dale Received Reported by
D,lc E,lrncl:'.:Li~~alc Repmted _______ _
Dal<.: Ancdyz~~W4vp Lab Number 991247'
DI IS 319 1 (llcviscd 2/91)
I __ 2,4,5-trichlorophenoi
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin --lindane --
--methoxychlor
__ toxaphene
2,4-D
2,4,5-TP (Silvex)
--
---
--
N.C. Department of Environment,
I k afth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Sile Number · Field Sample Number ---------------------------------
Nam e of Site UJARRf-N GuNN P U-CB L,4-~.H)f.} Site Location_. ~l,J_MJ,~· ~P-..--'--'-t::_>J~Tu_N ___ ·_·---_____ _
Collected By lJ.. 2, t»Y-,J ID# ___ ,,Date Collected · 4~14 '-.'l'\ ' .Time ------
Agency: Hazardous Waste . Solid Waste ' ~ Superfund ' TCLP . Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium R,,cos --Ground water (1) _ Solid (5) Cadniium --
~ Liquid (6)
Chromium
/ Surface water (2) --Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium .\ --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry ---
. Parnmeter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compm:nds Resvlts(mg/1)
__ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Ba;ium carbon tetr,;cUorici,: ------MTBE Cadmium. chlordane
~ Pen <:O, oool.f!iA ----Chloride chlorobenzene ----Chromium chloroform -·· ----__ Copper o-cresol ----Fluoride m-cresol ----------•· Iron __ p-cresol ---· --Lead cresol ---------....... __ Manganese 1,4-:-dichiorober:zen-: ----: __ Mercury 1,2-dichloroet;,ane ----·--Nitrate __ l,l-dichloroethyle11'~ ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor . --Radiochemistry Sulfates hexachlorobenzene ----······-··---Zinc hexachlorobutadicr:e ----P<1 rameter Results (PCi/1) _pH hexacb 0rocthane -------·---
--Gross Al µha --Conductivity --methyl ethyl ketone. --Gross Beta TDS nitrober..zen~ --------·--------= pentachlorophcnoi TOC --
--__ pyridine
Microbiology --__ tetrachloroethylene
----· trichloroethylene
Parameter Results (Cpl/lOOml) --__ 2,4,5-trichiorophenol __ , --__ 2, 4,6-trichlorcphenol
----__ vinyl chloride
endrin --lindane
4-J. J-99 77d --Date Received Reported by methoxychlor --
j)~ (AifS-~ --tox3phene
___ U Date Ex tracted '-1-,,;i,,-3)t.-,/Dale Reported 991248 --2,4-D
~C,(JCM~ _ 2,4,5-TP (S ilvex)
Dat t.: AnalyLed ~,l..1-9'91'P Lab Number --Ill IS 3!'Jl (ltcviscd 2/91) ---
I
i
N.C. Department of Environment,
I lca!ttc, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number _______________ Field Sample Number O jL.O b ,3<L , ....
Name of Site (J) ARR£N GvNN . PCB LA-Mt>P1's1te Locati~n w frP, ~e:w Jb1
~;.· ".'<'.> .;~·'-:
Collected By IJ-2, ,.Jl,,J ID# ____ Date Collected \j-lj '-Kj , , .. , "":·J'.ime _____ _
Agency: Hazardous Waste Solid Waste ~Superfund ,;,• ,. ,c. TCLP,,Compounds ----
Sample Type Inorganic Compound.! Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium --U 'TU .5 __ Groundwater (1) _ Solid (5) --Cadniium
Chromium
~Surface water (2) --
'Liquid (6) Lead --Mercury
Soil (3) Sludge (7) --Selenium ·,
--Silver --Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
_ Pnroneter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Rest'l~(mg/1)
:t·&T:GC/MS Arsenic benzene ------___ Acid:B/N Ext. Barium carbon te~rachloride --------••-,.·-----MTBE Cadmium chlordane
~✓--PC-2 ---------------<O, l:>OO/ Ll':>At Chloride chlorobenzene ----,, Chromium chlorofcrm --------__ Copper o-crcsol ·---Fluoride m-cresol ---------
---· Iron __ p-cresol ----Lead cresol ------------
--.. __ Manganese --1,4-dichiorobcnzene
---__ Mercury 1,2-dichloroethane -.. Nitrate = 1,1-dichloroethylene -----
< Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene --------------·····--~···----Zinc hexachlorob:r tadiene ----~·"rnmt!ler Results (PCl/1) _pH hexachloroethanc ·-__ Gross Alpha __ Conductivity --methyl ethyi ketone
Gross Ber:i TDS nitrober.zene . ""-------------TOC __ pentachloropheno! --
--__ pyridine
Microbiology ----tetrachloroethylene
--__ trichioroethyiene --Parameter Results (Col/100ml) --__ 2,4,5-trichlorophenoi
------~4,6-trichlorophenc! ----
------vinyl chloride
endrin --lindane Lf-;1J-C/911d --Date Received Reported by methoxychlor --f'(!JJ~{llf~ toxaphe~e
Dale Extraclc.:<l Lf -~~~-79J/l;'J✓-oatc Reported --
--2,4-D
~~ j-(/11_J77!J'7
991249 _ 2,4,5-TP (Silvex)
Dale.: AnalyLc.:<l 'l-~"K-991/P Lab Number --
1)1 IS 3 1')1 (H.cviscd 2/91)
l
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I
N.C. Department of Environment,
I k:;lth, & Natu ra l Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laborato ry of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Si te Number _______________ · Field Sample Number . ,0 .)_oJ:, J 3
Name of Site fJJ Af<.~N GvNN . p CB LA-, •. H>f.1'sfte ~cation_W~· --'-f('P,~P-.,=e:;=/v-'---'--Jb-'--N ________ _
Collected By }J.. 2, ,.y',J ID# . Date Collected Y-1.q'-.'t j Time ------~-'----'---'-----..______ -------
Agency: Hazardous Waste Solid Waste __i::::::_ Su per fund TCLP Compounds ----
Sample Type Inorganic Compounds Resul!s (mg/I)
Environmental Concentrate Comments Arsenic --Barium
VT05 --__ Groundwater (1) _ Solid (5) Cadmium --
~quid (6)
Chromium ✓ Surface water (2) --Lead --Mercury
_Soil (3) _1Sludge (7) --Selenium .·,
--Silver --Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
. ParamP.~er Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
__ P .:.:T:GC/M;:; Ars:!nic benzene --Acid:3/i".; 1:.:..:. Barium carbon tetrachloride ----i -·---·-MTBE Cadmium chlordane ✓' _p.i&___ ~;,. 000/a;ftA.. ----Chloride chlorobenzene -------,, Chrnmium chloroform ------__ Copper o-cresol --·---Fluoride m-cresol --·-·-·• ----------Irc:i __ p-cresol ---.. --Lead cresol --------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ---------· ----Selenium 2,4-dinitrotoluenc ----Silver heptachlor ----Radiochemistry Sulfates hexachloroberzene ---------······-··-·-·------Zi.1c hexachlorobutadiene --Parameter ?.esults (PCi/1) _pH hexachloroethane ---
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ---·· ._,__;-4 _____ ---·-TOC __ pentachlorophcnol --
--__ pyridine
Microbiology ----tetrnchloroethylene
__ trichloroethyiene --Paramettr Results (Col/lOOml) __ 2,4,5-trichlorophenoi . I --
-----__ 2,4,6-trichlorophenol .
----__ vinyl chloride
endrin --lindane I
Date Received 4-J. J -i}q 1kf Reported by --I --methoxychlor t/J Cf/!. (Ms-err, __ toxaph ene
Date Extract ed ~-ff~Ji¥Date Reported --2,4-D
A(~..., 991250 _ 2,4,5-TP (S ilvex)
Dale A nalyLed '(jfl_;:t.,1-99t/? Lab Number ., --I) I IS 31 'Ji ( llcviscd 2/91)
N.C. Department of Environment,
I lc;,li\ & Natu ra l Resources
Solid Waste Management Divisio n
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number ---------------Fieid Sample Number_. ___ . :_O_~,_-i...._. _o__,b""--'1,==--'.j.L...-_____ _
Name of Site (J} A (.lRf_N GUNN PCB L~DP 11sfte Location_--=-LJ----=--MJ---'---'-fl=t::=J.Jc.:........L.Tu..::::....:...:N_· · ________ _
Coll ected By IJ-2, t'f,;.} ID# ___ Date Collected Y-1 ".\ ·-fl -".\ · .-Time
!
Agency: Hazardous Waste Solid Waste ~Superfund
Sample 'Iype
Environmental Concentrate Comments
~ Solid (5) Q._c..u s __ Ground water (1)
__ Surface water (2)
__ Soil (3)
__ Liquid (6) ____________ _
_ Sludge (7) __________ _
./ Other (4) Other (8)
Organic Chemistry Inorganic Chemistry
.. Parameter Result" (mg/I) Para met,::, Results (mg/I) (mg/kg)
-· P&T:GC/MS
_ Acid:B/N cxc.
MTBE
✓ PcQ
-------
--------
--------------
-----·---------
Arsenic
Barium
Cadmium ·--Chloride
. Chromium ----Copper
Fluoride
Tron --. Lead -----------___________ . __ Manganese
-
I
-_
1
. __ Mercury
· Nitrate ------• __ Selenium 1----------------~-Silver
······-. ······-~a~_io_c_h_e_m_is_t_ry ____ , = ~~~ftes
-
Results (PCi/1) j = pH
__ Gross Ai pha _______ 1 Conductivity _______ _
G:-o~s Beta ! --TDS -----~~---1--
~
-------11 =TOC
Microbiology _
,---------------l
---------
I I Parameter
I ·----
Results (Col/lOOml) --1 -------
--------
Date Received 4-;).. J -q 9 7)..:/ Reported by ---------
D ;.i l c Extr;.iclc<l fc.B 1-)6..qq~ Date Report ed ________ _
DJt c AnolyLcff/!aet.Tive Lab Numbc r ___ 9_9_i_Z_S_1 __
D I IS ]l 'JI (!Zr.vised 7./91)
TCLP Compounds
Inorganic Compounds
Arsenic
Barium --Cadmium
Chromium --Lead
Mercury
--Selenium --Silver
Organic Compounds
benzene --carbon tetrachio:-ide
Results (mg/I)
Results (mg/I)
---------chlordane
chlorobenzene --chloroform
o-cresol
m-cresol --__ p-cresol
cresol --1,4~dichlorobenzetie --1,2-dichloroethan:e
--1,1-dichloroethvlene --. ,
2,4-dinitrotoluene --
--heptachlor
hexachlorobenzene --. ----
hexachlorobutadiene --hexachloroethane --__ methyl ethyl ket011e _____ _
nitrobenzene --------·---pentachlorophenol
· __ pyridine -------
__ tetrachloroethylene
trichloroethylene
--2,4,5-irichlorophenol --------
--2,4,6-trichlorophenol = vinyl chloride --------
endrin --lindane ----methoxychlor
__ tcxaphene
_ 2,4-D ~ _ 2,4,5-TP (Silvex)
---
,-Jra4-~~?-MS
-..,,;,..., d' c / a ~ .,___ ~
~~~·~
fvJ..,) /) (!_ft;
N.C. Department of Erivironmcnt,
I IcaJ1h., & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Caroli~• 27611
Sile Number _______________ Field Sample Number.:: . ().;:Lo , ")_r .
. Name of Site UJ AR~N" Gul\{tY . Peg LA-MDf 1~e Location . LJ.~ ~tif.J TblJ . -~ -.
Collected By lJ-2, ,./,.J ID# ___ . Date Collected . Y-141 •~.'t·J
Agency: Hazardous Waste . ·Solid Waste ----' ~Superfund · ... TCLP Compounds
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --
~J,~~+~ Barium
__ Ground water (1) R.c.0'>'' --
~lid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --__ Mer~ury
_Soil (3) _ Sludge (7) Selenium :' --Silver
V Other (4) _ Other (8) ----
--
--Organic Chemistry Inorganic Chemistry --
1
., Parameter Resul t'.'J (mg/I), :!arameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I)
_P&T:GC/MS Arsenic benzene -·---, _·Acid:B/N Ext. Barium carbon tetrachloride -------MTBE Cadmium · chlordane
, ✓ Pen ~ . <o,/Of'/UM ~---chlorobenzene Chloride ----Chromium chloroform. -------
~a~ Copper o-cresol
i, __ Fluoride --
I
m-cresol --Iron __ p-cresol ··--Lead crcsol
I ----' __ Manganese 1,4-dichlorobenzene ----
--__ Mercury 1,2-dichloroethane --
--Nitrate __ 1,1-dichloroethylene --
' Selenium · 2,4-dinitrotoluene ,. -----Silver __ hcptachlor , .. ---
.. Radiochemistry Sulfates hexachlorobenzene -------······-··--···--· Zinc hex:::~hlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --_ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene --·-----~----
I TOC __ pentachlorophenol ----__ pyridine --Microbiology --__ tetrachloroethylene
__ trichloroethylene --Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane
Date Received t-/-;;_/-9 9 M --Reported by __ methoxychlor
Dale Exlraclc<l m~ 1'·L0-G"lllm Dale Reported
_._ tox:1phene
--2,4-0 mw:,To1iJJ 991252 _ 2,4,5-TP (Silvex)
Dal c Analyze -~Yf' Lab Number --DI IS 1191 (Revised 2/91)
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N.C:' Department of E~vironment,
I lc~lth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number · · Field Sample Number ' · Q>l.,:c., fi i> f,--·-,., --------------------'---~...._._ _______ _
Collected By IJ-2, ,.Jl-,,J ID# ___ . Date Collected Y-1 · . •-ft'\ Time ------
Agency: Hazardous Waste -solid waste __::::::_ Superfund
Sample Type
Environmental Concentrate Comments
__ Groundwater (1)
__ Surface water (2)
Soil (3)
~ Solid (5) _U_,_T_i..f_s_· __ 5-_' _J_~-~~(. ".\~~-:)_
~Liquid (6) ________ _
Sludge (7) _________ _
✓ Other (4) Other (8) -------------
Organic Chemistry
. Parameter
_P&T:GC/MS
_· Acid:B/N Ext.
MTBE
✓ Pc.,B
Results (mg/I)
---------------
-------··· ------
Radiochemistry
······-··------·---------
Parameter Result: (PCi/1)
__ Gro~s Alpha ______ _
Gross Beta
Microbiology
Inorganic Chemistry
Parameter
Arsecic
Results(mg/1) (mg/kg)
.uarium --Cadmium --Chloride --Chromium --__ Copper
Fluoricie --Iron --Lead --__ Manganese
__ Mercury
Nitrate --Selenium --Silver --
Sulfates --Zinc --_pH
__ Conductivity
TDS --TOC
'
·-: ::u TCLP Compounds
Inorganic Compo~nds
Arsenic --Barium --Cadmium
Chromium --Lead . --' .
Mercury
--Selenium --•
Silver
Organic Compounds
be::1zene --
·• .,
c,.rbon tetrachloride
Results (mg/I)
\.
Results(mg/1)
·-------chlordane -··------chlorobenzene --chloroform
o-cresol --iL.-cresol --. _ p-cresol
crcsol ----1,4-dichlorobenzene _____ _
__ 1,:2-dichloroethane
1,1-dichloroethylene
_ 1,4-dinitrotoluene ------
--heptachlor
h1=xachlorobenzene
hexachlorobutadiene ---------hexachloroethane
__ methyi ethyl ketone
ni~robenzene
·-pentachlorophenol = pyridine
. __ tetrachloroethylene
-------
---------
j Parameter Results (Col/lOOml)
trichloroethyicne _________ .:__ !
_ 2,4,5-trichlorophenol i
I
Date Received
Dale ExtractcJ PCf>+ .... 10~ti_ ~
PCB~fM'O'f9
Dale Analyzed '1-.30--99VP
Ill IS 1191 (ll.cviscd 2/91)
2,4,6-trichlorophenol I = vinyl chloride '
endrin --lindane --Reported by -----------methoxychlor
__ toxaphene !
Date Reported __ 2,4-D ----=-----------·-i 991253 _ 2,4,5-TP (Silvex) I
Lab Number _________ ~-----------~~-=-----]
N.C. Dcpartm~nt of E~vironment,
I lc~·lth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Dox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
• "• I
Site Number _______________ Field Sample Number_.·. __ O=-;"l.... __ o~f....,J.,,_"1 ________ _
Name of Site UJ ARR£N
Collected By IJ-2, i-Jl-,J
~ -'i'; :. ". • Ll-.. Gurvw ; P,GB LA->JOP I Site Location_W~.f((J.,_· "--'-(Z,-=--'-t:;'~/v~Jl?~N ________ _
ID#_· ___ Date Collected · \1-1 . ·-~ J Time ------
Agency: Hazardous Waste ·• '·Solid Waste _.:::::.Superfund TCLP Compounds ----
Sample 'l)'pe Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
5-<.J,~~ ..... +.) Barium
~S.olid (5) U,os · --__ Groundwater (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury
Soil (3) _ Sludge (7) --Selenium :·.-,.· .,
--Silver --_L Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --,.
_ Parameter Results (mg/I) Parameter Result-. (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride -------MTBE Cadmium chlordane
✓ Pc,8 ----<O *//)H'M Chloride chlorobenzene ----Chromium chloroform -------__ Copper o-cresol .----Fluoride m-cresol ---------Iron __ p-cresol -----Lead cresol -------
--__ Manganese --1,4-dichlorobenzene -
--__ Mercury 1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----l Selenium 2,4-dinitrotoluene ----·-Silver __ heptachlor .. --Radiochemistry Sulfates hexachlorobenzene ----······-··--·-Zinc hexachlorobutadiene ----Results (PCi/1) Pan:!7eter .. _PH hexachloroethane ---__ · Gross Alpha __ Conductivity I --methyl ethyl ketone
Gross Beta TDS l nitrobenzene ------TOC . I __ pentachlorophenol --I --I __ pyridine
Mkrobiology ----tetrachloroethylene
--__ trichloroethyiene --Parameter Results (Col/lOOml) __ 2,4,5~trichlorophenol --
---------__ 2,4,6-trichlorophenol .. vinyl chloride ------.. endrin --lindane
;_;-;;n-99 "11d --Date Received Reported by methoxychlor --
Dale Extraclc<l ft-B ~-2.0--9q \l-n1Date Reported
__ toxaphene
2,4-0 --
Dalc Analyzed~~~ 99125'4 _ 2,4,5-TP (Silvex)
Lab Number --1)1 IS 3l'JI (llcviscd 2/91)
I I
I
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N.C'. Department of Environment,
l lc'.t lh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site. Number · Field Sample Number ·. .c)L~. C :>;•g-·· -------------------'---'=-------'=----------
Name of Site. fJJ A f?.,R£N GUNN ;p CB LA1,H>f 1'sfte Location_· _LJ"'-· ---'-MJ,.,___,_ft:,=' e::=>J-'--'-Tb.;;;...N-'---__ . -_, ~--_· ____ _
Collected By IJ. 2, ,.y',J ID#_.·. ___ ·, Date Collected . :i:.vj-19, :-<=t J .' ·
Agency: Hazardous Waste ·. ·Solid Waste ~Superfund
Sample Type
Environmental Concentrate
.. .. Comments ·
__ Ground water (1)
__ Surface water (2)
_ Soil (3)
~So.lid. (5) s; fl(',/. 0: Fil~v--. m~it:__
·/_L1qwd(6) b,,1/L-fh1~4 Leve/;
Sludge (7) -------------
x_ Other (4) 0th er (8)
Organic Chemistry Inorganic Chemistry
· ... ,TCLP-Compounds
Inorganic Compounds
Arsenic --Barium --Cadmium
Chromium --Lead ·;,
__ Mer~ury
Selenium --Silver
Results (mg/I)
,------------------------------
.. Parameter Results (mg/I). Parameter R~sults (mg/;) (mg/kg)
·--P&T:GC/MS ______ __ Arsenic
__ Acid:B/N Ext. ______ Barium
I MTBE . --Cidmium
✓ pc.,3 (LA€€) ()1 .,'U,P,,Om. ~ Chlori~e I __ ______ _______ Chromium
! __ -..-----,--.....-,.------__ Copper
I J!_~Lh:,-' _ Fluoride
/7 /~----,n,,,, • -~ Iron ' ........ ~~---><a;~ ~ I ____ I _ Lead
I __ · ______ __ Manganese
__ ______ _______ __ Mercury
Nitrate
Selenium --Silver --Radiochemistry Sulfates
!······-··-···---------------.1 -_-_-Zinc
I Parameter Results (PCi/1) __ ?H ! _____ Gross Alpha·_______ __ Conductivity ______ _
------·-
· Gross Beta TDS
l --··-----------
1 TOC
Microbiology
------Parameter Results (Col/liiOml)
-----
Date Received 4-;)_ J-99 7Jd Reported by ---------
Organic Compounds
benzene --
--
--
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
--p-cresol
cresol --
Results (mg/I)
-------
---------
--------
---------1,4.:-dichlorobenzene ______ _
__ 1,2-dichloroethane
1,1-dichloroethylene
--_. 2,4-dinitrotoluene ---------
= heptachlor
hexachlorobenzene ----------hexachlorobutadiene ---------hexachloroethane
__ methyl ethyl ketone _____ _
nitrobenzc;ne --per.tachlarophenol
=pyridine -------~----
__ tetrachloroethylene
__ trichloroethylene __________ _
__ 2,4,5-trichlorophenol I
__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
. endrin --lindane ----methoxychlor
D a I. c Extraclt<l f (()4✓M3_...Cfq~ Dale Reported_______ =· = ~~t6he~e ~
f=:eE (A-f.fo?o_l 991255 _ 2,4,5-TP (Silvex)
D:.i lc Analyzed 4-30---99}'/' Lab Number
DI IS ]!'JI (llcviscd 2/91) -----------
L..------------------
N.C. ~cpartmcnt of Environment,
I k ~Hh; & Natural Resources
S,Jlid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Dox 28047, 306 N. Wilmington Street
Raleigh, North Caroli~~-276,11
Site Number ··' _. " Field Sample Number.';, .0 :Lo~,?>-~
Name of Site()JA(?-R.fN Gu NW -P.GB LA-MDf 11st'e ~cat~~n ·. LJ~ ~~Al ,Tb1J · ,.,:,!_~-,(i;.~:
Collected By lJ-2, ,,y',.J
·A• $,J<-, •'·' •',
Hazardous Waste ~ Superfund
. . . ·,_. . . '/~·\~~~~~~ :-:~~~ '.
Agency: ·Solid Waste -_t..J' ,·0,1?.t.,,TCLP,.Compounds · ·.,.!,J.'\l'::t . ----.l . . •..•• ,., .-i·:i'
. -; j)}·':::?~·:~.:~?t ~
Sample Type .. \.
Inorganic Compounds ResultS(mg/1)' .
Environmental Concentrate Comments · · : Arsenic . .. _!-~.:'-. ~"':. ,• '•
~. ·---Barium :•·
~Solid (5) CAg.j)J.:.~' ncri,~;. ·r,~J ~ --·cadmium __ Ground water (1) :,'.--.-:i i-;!.· :·-:.. --
P,;,~~~~l,t__ Gi-ve-0 Chromium ' .. 1-1-,.,'4 --__ Surface water (2) Liquid (6) Lead··: ; ; _._._ t .. !.:.-~:,: -~. ·J --Mer_cury
_ Soil (3) _ Sludge (7) .-. -Sele~iuni ··-'·, ,._, _:~·-, <-' ·\
--Silver --_JC_ Other (4) Other (8) ,_. -f.' .. ' ·-----
--
--Organic Chemistry Inorganic Chemistry --
. Parameter Results(mg/D Parameter Results(mg/1) (D,~kg) Organic Compounds Results (mg/I)
_F&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride -----?-.-iTE:2 Cadmium chlordane
✓ ~ ---·---chlorobenzene <: (b_lfl lf'O< Chloride -----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ----··----Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4'-dichlorobenzene ·
--__ Mercury --1,2-dichloroethane
Nitrate __ 1,1-dichloroethyl~ne ----Selenium 2,4-dinitrotoluene· · ' . . . ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----...... ______ Zinc hexachlorobutadiene ----Results (PCi/l) Parameter _pH hexachloroethane --__ Gross A.lpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------..... .-r-.... ----· --TOC __ pentachlorophenol --
--__ pyridine
Microbiology __ tetrachloroethy!cne .--__ trichloroethylene -----·· Parameter Results (Col/100ml) __ 2,4,5-trichlorophenol i --
--· --· __ 2, 4,6-trichlorophenol ..
----__ vinyl chloride
endrin --lindane
Date Received 4-,;;_ I -q q 7/c:J --Reported by methoxychlor --
Dale Extracle<l '\)Cf:>4-2,0,qq \0:Y) Date Reported
__ tcxaphene
--2,4-D
~~5-_jM?~ 991256 2,4,5 -TP (Silvex)
Dale AnalyLed -'0-99'Vp Lab Number --
I)\ IS 31'JI (!Zcviscd 2/91)
N.C. Department of Environment,
1 k~'lh, & Natural Resources
S<Jlid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Caroli~a 27611
Sili:: Number ,.:,, Field SampleNumber,i\,,.~ .:,.,.iD)-D b'-1. u
Name of Site UJ AR-REN GvNN ~P-di~or.·,~~;~~at~~:,:·~t)1:~·~~~ Tb~ ' .,._.
Collected By lJ-2, ,,y;J
Agency: Hazardous Waste
Sample Type
Environment.al Concentrate
Ti.me
· Inorganic Compounds
Arsenic
Barium
------
Results(mg/1)
__ Ground -.water (1)
__ Surface water (2)
_Soil (3)
~Other (4)
¥S~lid (5)
_ Liquid (6)
· · ;. ~; Cadmium
_ Sludge (7) __________ · ·_·· __ · '·
Other (8) __________ _
Organic Chemistry Inorganic Chemistry
. Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg)
P&T:GC/MS ______ Arsenic = Acid:B/N Ext. _______ , = Baril!m
MTBE f Cadmium ✓ PG2 (/~oJ ~ = Chloride ______ _
. Chromium ----· ----------· • __ Copper
1._,~fr ,1?1../ ! Fiuoride
J;vv~ ,i/4.o-~~.E"_. Iron
L__ r I-Lead
___ _ __ __ __ __ __ __ __ __ __ ·. I __ Ma?~a~ese ------------=J--~;;~~?---= Selenium
Silver
-------
-·-----
-------
······-····--~-adiochemistry ____ I = ~~~f:te!>
Parameter Results (PCi/1) 1 pH
__ Gross Alpha _______ '1· = Conductivity =---------
Gress Beta · TDS --· ----·--·-···-·---l --
--------
----------TOC
Microbiology
P.-1rameter Results (Col/lOOml)
Date Received 1-f-;;J._) _qq-n.J Reported by ______ _
Dale Extraclcd ___Kb 4-;10J:f9~ Date Reported --,-----~--tf) c.t;J 5-{ A1 ~tJ'j'C> .J 9 ·91257
Dale Analyzed 'f-30-991/P Lab Number ________ _
DI IS Jl'JI (llcvi,cd 2/91)
Chromium --' Lead
Mercury
· .-., -, Selenium --Silver
--'
Organk Compounds
benzene --carbon tetrachloride
Results (mg/I)
---------
--
--
chlordane
chlorobenzene
chloroform
o-creso!
m-cresol
--p-cresol
cresol ----1,4-dichlorobenzene ______ _
1,2-dichloroethane
--1,1-dichloroethylene
· · 2,d-dinitrotoluene ------
--heptachlor
hexachlorobenzene --hexach!or:Jbutadiene ---------hexachloroethane
__ methyl ethyl ketone _____ _
nitrobenzene --pentachlorophe!lol = pyridine
__ tetrachloroethylene
trichloroethylene
--2,4,5-trichlorophenol
--2,4,6-trichlorophenol ------= vinyl chloride
endrin --lindane ----methoxychlor
__ toxaphene
_2,4-D
_ 2,4,5-TP (Silvex)
I
I
f:-DEHNR
ivision of Solid Waste Mana~ement
;J Supufund Section
J H~ous Wusk Section
2"solid Waste Section
Organics Lab: -:----Inorganics Lab: --
11
CHAIN OF C:USTODY RECORD
Project Name: pc,,.13 l--~ Sampled by: L~ (2.,.,__
Site ID# (NCO#) Sampler 1D l m .
Location: vf~ G-P Telephone:_(_) ) '.3 3 ,....tJ (tf z. V 2-~ 7
Address: Date Sampled: ~ L.,_ 2-~ •
j Time Sampled: -, 7
Sample Types: Soil Water \Vaste Other ~
Remarks: Le~~~
I
Field Sample (.j_ZU I <i'-Slz.,,
Numbers
,-. -
Relinquished by: ;i:aAJJv. tie~ Date:1-//41.../t,? Time: /Z./5:1
~ignature) \ '( I I
Received by:------· J6.,,c/4~-J -tJ?~ ·----------------Date:~/9f--Time:-J:2../5'? _______
(Signature) 7
I Relinquished by: Date: Time:
(Signature)
. ---------------------------------------------------------------------------------------------------------------------------
Received by: Date: Time:
(Signature) -
Relinquished by: Date: Time:
(Signature)
--------------------------------------------------------------------------------------------------------------------------
Received by: Date: Time:
( SiJ!nature)
-----
Results Reporte~ 1~-~~ j/1._,lr.1. 0 Date: '02-tJ-9 7Time: -
( ;)Jzn¥□re)
-
\:\COCR.Fru-.f)
I
~-DEHNR
vision of Solid Waste Management
1 Su pt:rfun<l Scclion
J ~-~:z.urd~-~,s_.,,Wu:;tt: Scctl~a
l°Solid Wuste Settion .· •.·
Organics Lab: ---Inorganics Lab: V
CHAIN OF CQSTODY·RECQRD
Project Name: fc, 6 Lf ·
Site ID # (NCD#) __ -=--------
1..Dcation: W~ Co
Address: --------------
Sample Types: Soil _____ _ Water
Sampled by: l .. ~
Sampi'er ID / trt> -------------Telephone:_(_) *I)(. qz
Date Sampled: yji zj;Jq<;
Time Sampled: -I · ·
}c. 2,..57
\Vaste Other J
Remarks: __ L...:..t_J._~_.:;_;_~...;.<t....:.:i:e......_ _______________________ _
Field Sample ;Lot(. :i..
Numbers
2t>(,6 7
Relinquished by: _______________ _
(Signature)
Received by:
(Signature)
Relinquished by:
(Signature)
Date: ---Time: -----
Date: Time:
Date: Time:
. ----------------------------------------------------------------------------------------------------------------------
, Received by: Date: ---Time: -----(Signature)
Results Reported:
I , l r,.,-. ,...,._ .-,o, I \
(
I
I
NC Department of En_vironment,
Hc.allh , &. Natural Ruourcc,
Solid Wu~ Manai:cment Div i,ion
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hc.allh
P.O. Box 28047, 306 N. Wilmington St. .
Ralcii:h, North Carolina 27611-&04(_.'-:·
-:.··:::..,•'~-. -/·~-.
Site Number------'-----------SamplelD Number/Name ___ :J..._o_,_<._7--___________ :_:,,:_l ~-·.-•.. ~--~:,,_;:. ·
NameofSite fct3 LF. CoHectedBy l-[2_q,_,-ID# I,.,. -----------------------------
Site Location w~ LO DateCollected y/2-.--/q f Time ------------------'-,1----+, -.-----~----=----_-_-_-_-_-_-_-_-___ -_-_-_-_-:..-:..-:..-:..-:.-:.-:.::.::.=-,
Agency: Hazardous Waste .,......,...Solid Waste __ Superfund
Sample Type
Environment.al Concentrate Comments
Ground Water (1) Solid (5) I...L(J.d~ -
Surface Water (2) Liquid (6) 7Ylf(u~
Soil (3) I Sludge (7)
/o'ther (4) Other (8)
Organic Chemistry Inorganic Chemistry
Parameter
P&T:GC/MS
Results (mg/I) Parame~er RC5ul~(mg/kg)
Acid:B/N Ext.
2,4-D
2,4,5-TP(Silvex)
chlordane
hept.acblor
hexach.l orobenzene ------hexachlorobut.adiene
endrin
lindane
methoxychlor
toxaphene
------
FOR LAB USE ONLY
Date Received ----------
Date Extracted ----------
Date Analyzed ___ . ______ _
Reported By 'Ztii7\
Date Reported ~--{"--!.(f__,_f_? __
00508'.o MAY 4 9 Lab Number. . ----------
DHS 3191 (Revised 12/93)
antimony
arsenic
barium
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
mnnganese ______ _
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zinc
pH
conductivity ______ _
TDS
-fusb point ___ __;:~--
L ~~--------.,__1-""H'~
TCLP Compounds
Inorganic Compowids
arseruc
barium ,
cadmium
chromium
lead
mercury
selenium
silver
Organic Compounds
benzene
carbon tetrachloride
chlord.an~
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
l, 1-dichloroethylene
2, 4-dichloroetbylene
heptachlor
hexachlorobenzene
hexachlorobutadiene
.... hexachloroetbane
methyl ethyl ketone
nitrobenzene
pentachlorophenol
pyridine
tetrachloroethylene
trichloroethylene
Results(mg/1)
Results(mg/1)
-------
-------
-------
-------
2,4,5-trichlorophenol _____ _
2,4,6-trichloropbenol ______ _
vinyf cbloride
endrin
lind.ane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Sil vex)
I
I
I
NC Department of E,nvironment,
Health, &. N,wr,1 Ruourcc,
Solid W"~ Mana~cmcm Divi,ion
SAMPLE ANALYSIS REQUEST St.ate uboratory of Public Health
P.O. Box 28047, 306 N. Wilmington St.
Ralei~h. North Carolina 27611-8047
Site Number _______________ Sample ID Number/Name -~rt:~0'--"{.~'"---'3=--· _________ ·,_· __ _
Name of Site fe, IJ Lt::' Collected By __ {.;.._._llin,,.__· __ -_·----'----·ID II · · I ,-,,
SiteLocation lv~ 4 · DateCollected '-I /1.-~ /qt; .· Ti~d,.. ---'-,,~--+1.,;:-~~..::..::..::..::..::..::..::..::_-..::..::..:: __ .::.::.::.::.::.::.::.::.::.::.::.::.:::.::.::--.
Agency: Hazardous Waste (../'Solid Waste __ Superfund
Sample Type
Environmental Concentrate Comments
--Ground Water (1) -Solid (5)
-Surface Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
~ Oilier (4) -Other (8)
niJ 1000 ...JL
Organic Chemistry Inorganic Chemistry
Parameter Results (mg/I) Parameter Resul~(mg/kg)
P&T:GC/MS antimony --
Acid:B/N Ext. arseruc --2,4-D barium --
-2,4,5-TP(Silvex) -beryllium
chlordane cadmium --
heptacWor chloride --hexachloro b~n.z.ene ch.romium --
h:xachlorobutadiene cobalt --e.idrin copper --lindane fluoride --methoxychlor iron --toxaphene · lead --
--manganese
--mercury
nickel --nitrate --
selen.iurn -silver -FOR LAB USE ONLY sulfates -thallium -Date Received vanadium -
ZlIIC -Date Extracted pH -_ conductivity _____ ~_
Lab Number
Date Analyzed ___ --,--_____ _ TDS
Reported By ~
5
-/' r)Q V ~t,oint1
~1 1 •
199
~~-;._e--2..-0~._ i--
Date Reportednnr-ryp.,-t1>l'' -~--__ _ Uvc.~0.c,J H1 ~ ----~*· v~":rf,j <J
DHS 3191 (Revised 12/93)
*f~~-
TCLP Compounds
Inorganic Compounds
arseruc -barium • -cadmium -chromium -lead -
-mercury
selenium -silver -
-
-
-
Organic Compounds
-
-
-
-
-
-
-
-
-
-
-
-·
-
-
-
-
beuzene
carbon tetrachloride
chlordane
c:hloroben.zene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobeuzene
1,2-dichloroethane
1, 1-dichloroethylene
2,4-dichloroetbylene
beptachlor
hexach!orobenzene
bexachlorobutadiene
methoxychlor
toxapbene
2,4-D
2,4,5-TP (Silvex)
Results(mg/1)
Result.s(mg/1)
I
WELL LOG SHEET Facility : Warren Countv PCB Landfill Location: Warrenton
Purge/Sample Team: ----'--/+,--'---A----'f{C....:rt+--V-2_v_""_·Vv __________ _ Well#: Yhw /
Comments (well construction, etc): _l_._+_,---'-l _0_e.._.._e_+~~-5_/ ._1 ::, ___ O_-e __ p._t_~o.__te_LJ_~-'---'---9_Y_._r_~----
Conversion Factors: For 2 " well : 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information
1 Well Volume (gal): _5_,~2, __
.·
Date Purged: · i /'U -'l J
For 4 " well: 3 volumes (gallons) = 2 .0 x height of water column (feet)
For bailers: 4 bails = I gallon
3 Well Volumes (gal): ; )-. 5 iJ Purge Equipment: G u~J..C~ ~J : FL..<---
Purge Time Start: !u : 2.-t> Purge Time End: -------
Did well purge dry? Y N , Actual purge volume: !../ls ( < f,_J ----
Volume c) -,
Temp (°C) ftg .'j
pH G -I
S. C. '[J _o
D. 0.
Turbidity / .. [.) ()
/;D: w
Sample Date: _....L..1j_-l_!J_,,_14-'----
< . 'j "--<-,.._(
Volume Volume 35-,_/ Volume -
/ i, q / f. (,
l -I !,.of<
/ ol,< .) I<) '1, 2--
s-,7b . 11. t../ cf
Sample Information
Sample Time: -~/_/ _ _. _2....-0 __
Volume Volume ---
Water Condition (turbidity, odor, etc.): C. le,._,--------'---+-"~-----------------
j Samples Collected (✓):
I
__ · VOCs (2 40 ml vials)
✓S'~l0~(1 2L Amber bottle)
Metals (1 IL HDPE bottle)
Temp(°C): )ft,(,, pH: lo 'l' SC(umhos):
!Comments: LJ<--(( I Pv vr& Ov:~ ,c_--l / 0~ I.{S,, '-f .2S1~ /
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): Turb(NTUs): 1/. o/'/
"-'"--> ()<.,.._,(.'J
f,. le l,..t-) {,,1l1rr1 ,4,1-/i,,. 0( ti 17.:,C, 1.~,.,. -cl ;:_, '/2_ t, /. pcbwells.frm
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: --+fhrg--'-'----'~ll+rf-_Z-----=-..:..,rli_~ _________ _ Well#:
Comments (well construction, etc): _2.,~'-' ~W~-(._.,~U'--'-i --~~..,_\--_ .. _t ~o---1 .. p,._·~--L{~3_:_~ 1 __ 0---1~1'-'t:b_to~_LJ._~~-'-{L'-----_·~---
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): /I.I 4 3 Well Volumes (gal): ,.{//.J-Purge Equipment: Z ,,--!;,,,..
,·
Date Purged: -vf-1 q__ '[q Purge Time Start: kA ------Purge Time End: -------
Did well purge dry? Y N,
Volume Volume Volume Volume Volume Volume ------,
.Temp (0 C) 1/
pH
S. c:
D. 0.
Turbidity
Sample Date: I.(~ J-u -'l4
Sample Information
Sample Time: _l_o_~ ·_1~---Sample Equipment: () ~ rl < v---------
Water Condition (turbidity, odor, etc.) :_T.=-\J '--',.l,'-'--';j_S"_ .. ___,~--~---C,_l=(e_~~~-.J-~,c,.,...,f'f,-,..,,~>-~t~I ,_~ __ J,_,_:5"_ ... _~--+-=
l <..r+ w .. ( l -r--e. ~ ... ~ e.. +-;ff
~-ll..~00
Samples Collected (✓):
VOCs (2 40 ml vials)
_}_ SVOCs@s)l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Temp(°C): ---pH: ___ _ SC(umhos): ---
4;~~ J,,4
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): ---
Comments: __ M_· ..:;;...,:,_P,._,.,_,,.--=...,'-,,...-~ ~ __ J _ . .,.._v--__ Tt......;v;_;/'----'---6,_;;;:J__.__Zfi,,--__ c,,,_~_-_e:-~----'-=-J ___________ _
________ --,--__________________________ ,pcbwells.frm
WELL LOG SHEET ·•.· . Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: R. Rab,,..,A..r /c. o id., .. I ·well#: M 1..J-2.
Y)\p 4-G.~f;
Comments (well construction, etc): _4_'_' ..... P~Vc ___ ,....,.OJ_A_P_R_I ~_O\_o,~.s_w_L_· _3_6_, '~3~,._b~!'\-4-f-·------
/ ll, ! 3 klo.+ev-c:.c,iur,,N
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information . For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For baiters: 4 bails = 1 gallon
1 Well Volume (gal): 1 . /5"° 3 Well Volumes (gal): '2.1.4-b Purge Equipment: :Jr,,,-,J 4 .s F"""';
Date Purged:· 1v'\ APJ2..0?) Purge Time Start: _ _,.1_2--_·._~_,5 __ Purge Time End: _ _.:Z~; -=2=-1+---
Did well purge dry? Y ~. Actual purge volume: 'L \ , S-
tioJ ,·+ · I Voume '4 -
Temp (0 C) , ... 11 "c
pH .s-_.q-{
S. c: /14. 7
-B. e.
Turbidity (,j:S-
Sample Date: A A fl? o/3
/, 1-S / 11, <
Volumej_ Volume 2: Volume-3._ Volume Volume ---
').._ D . I ).__o ,S' ,Zo,O)
:;;-, q 0 s-.~g $", ~ 1-
lo 7J, fl.!-/ 06'. 7
q,,1,~ 2-17 4 3.S-
Sample Information
Sample Time: '1_ •, 1:4-Sample Equipment: Srv"'d C:,,5 r"l"'\10 I
, Water Condition (turbidity, odor, etc.):~...=::L!:-i---___________________ _
Samples Collected(✓):
VOCs (2 40 ml vials)
/ SVOCsl@l 2L Amber bottle)
__ Metals (1 lL HDPE bottle)
11 Temp(°C): Z.0,0\ · pH: 5, tg4 . SC(umhos): °Ii;. 7
I
I I Comments: ;.,t, [L . ()
Dioxin (1 IL bottle)
Pest./Herb. (1 2L amber bottle) ·
DO(ppm): ;v/4 Turb(NTUs): 1-, S S"
~"'-+--------,----_ __:___ _____________________ pcbwclls.frm
• ;,.; ~·.' ;.,1.. •
-WELLLOG•SHEET Facility: Warren County PCB Landfill Location: Warrenton
. . . .
. Pur'g~;~~mple Team: R, Kaberf .£ / C, OIJ-r
' , . I \Vcll #: rnW-3A
Mf C'5>. ~g I
Comments (well construction, etc): )_" S:.$' Pl Apg ,c,,~q s/,!JL '2.?,,'f2. I btv1p ---,---~~~-~------, --,+-----
4-1. &'1 !04.{,i.y, u lv111n
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 voh!:nes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): \Q ,G\4 3 Well Volumes (gal): '2.o,4,3 Purge Equipment: 0rvNd ft>s pump
I I
Date Purged: · · l°l Ape '"'">'? Purge Time Start: /0; o'? a,,.. Purge Time End : ___._\-'--l _', 1_3 ___ _
Did well purge dry? Y @, Actual purge volume: 1-3 'jA l
Volume ii-1-ti,d Volume I Volume 1.. Volume 3 Volume Volume ---/
Temp (0 C) ,.r /5, ~ /~.4 (£;>,;-\°l.5
pH G.o7 C o o 6 , Io Q,.o°)
S. c: tOt q (rJS,? /o3. '1 1 l L 3
El . e.
Turbidity ...,., j O (, I I q, 0 2. rs I c:, ~
Sample Information
Sample Date: i°I APR 1 °1">".2 Sample Time: / / ~/u 1'~ Sample Equipment: Jv-,.1r,JJ:s Pvmf .
I
Water Condition (turbidity, odor, etc.): __ -+>C---"\a._=.......,/,\~r ___________________ _
Samples Collected(✓):·.
VOCs (2 40 ml vials)
✓ SVOCs@(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
1 ·2·T~mp(~C): /°} .5' · pH: · 6'. oq SC(umhos): -1.LL.2 DO(ppm): L Turb(NTUs): J. G 3 I .... ,, ·.
I c;mnients:
____________________________________ ,p,;bwells.frm
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: E /ATC '-KJ[_E_/1J 6TJ 'f'/1'801?
l
Well#: [hW -5
Lv ::
Conversion Factors: For 2" well: Jvolumes (gallons)= 0.5 x height of water column (feet)
Purge Information
1 Well Volume (gal): 3. 5
Date Purged: · 4; / {°{ /9.o/
Did well purge dry? Y N
Volu1;1e _j_
Temp (0 C) ':l I, t-
pH b. J7 ·
S. c: 18.5
D. 0.
Turbidity .99
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
3 Well Vc-lumes (gal): //, S' Purge Equipment: &-r..,,,JJ:.~ Q..,,_f
Purge Time Start: '],::) 0 prn Purge Time End : J : 't ~ p·~
Actual purge volume: /-:L, ,,,,,.,_)_
;:?
Volume± Volume _Q_ G-H~f .5o""\,ft'
Y0°¥t~r,J...-Volume Volume --
J..0,,7 -:1.0 .6
b, 2 ~. 2_
97.6 90~2
/,/3 • q7 -~6
Sample Information
Sample Time:. JL/ s--Sample Equipment: --------
Water Condition (turbidity, odor, etc.): _______________________ _
Samples Collected (✓):
VOCs (2 40 ml vials)
·v SVOCs~l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
I Temp(°C): pH: DO(ppm): ---Turb(NTUs): C>,'t 7
I
I CoI11IIlents: I ----------------------------------
________ ..,....-_________________________ pcbwells.frm
•, · ...
. -i~~ ·~ .;.:~·k -· · · · ·
··.WELLLOGSHEET ·-Facility: Warren County PCB Landfill Location: Warrenton
I
. ··::, __ \_·.·. ·· · . ·. ---, i I /-, ,
Purge/Sample Team: R. & bertJ / L'.. Olds
~ . ~. . J \\' e 11 # : O'\ W ~ :J
f'V\ 1P 4-1 .. s t
Comments (well construction, etc): ~2.._"_s-s~------,-r'-'J_·_A_,_R~~I 'l~°'~•_o,~s_w_· _L_~,......+~,,-,.c:X>~'-lo_M~, +-e _____ _
, 1..' '4 ....., "'4~ i,--
Purge Information .
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5. x height of water column (feet)
For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = 1 gallon
1 Well Volume (gal): '2-. \ \ 3 Well Volumes (gal): C. q2. Purge Equipment: 3r uNJ..r;,-r F ""f
Date Purged: · i °' l\t'R ~ 0, Purge Time Start: 3 : I S-Purge Time End: _4_,_:_2_5" ___ _
Did well purge dry? Y @, Actual purge volume: -~\ o.........,...~~f-._\~, _
~ ::i. (\_ '.,-+, ·.,__ r
Volume _J_ Volume -2... Volume 3 Volume !..J_.R. Volume~A Volume , . --
I Temp (0 C) v/Cf,«g ;q_s-~o.3 2c>, t '2 -C.,6 2~3
pH . £,6G ),7 2 :j,6 ( S . B_t; j; /§Cf S ,9~
S. c: ?6,J 80 ,7 §a.o 9f-i 810 ,5 76~0
D. 0.
Turbidity Z.3.5:' 31--.~ 4~/) 4-o .6 1-o. 4 1-f, 1--
Sample Date: _r1 ....... A~f.._,(<,_..__o>"}..J-+ __
Sample Information
Sample Time: _4 __ : _IS-__ Sample Equipment: _jcc....-.-_u-'-r1_d_~_.r--;r:,='-''-'-I'---'-,~ 1-"-r::>_
I
Water Condition (turbidity, odor, etc.):_~~=--------------------
Samples Collected (✓): ·.
VOCs (2 40 ml vials)
:>< SVOCs~(l 2L Amber bottle)
Metals (1 lL HDPE bottle)
Dioxin (1 lL bottle)
, Pest./Herb. (1 2L amber bottle)
\ .. \
" 11 pH·. . 5. °'~ Temp(°C): 1,-t..,,-:;; _ ~, \d SC(umhos): ~ DO(ppm): ~ Turb(NTUs): 4=\. 1:--
I Comments: ________________________________ _
__________________________________ pcbwells.frm
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: _(J-"---c2_ ,,__-'--J -+-t _5 ....>...:,( eff-. ,;:'1...-'C,,.'-U, [ __ tti----'---~----'--L{+--L_;_, _;;_N _;_~--Well#:
Conversion Factors: For 2" well : 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For bailers: 4 bails = l gallon
1 Well Volume (gal):___ 3 Well Volumes (gal): ____ Purge Equipment: 6 ..... ;-h_,
Date Purged: · '-i ~ r "( -'1 "-
Did well purge dry? Y
Purge Time Start: r~: oc:., ------Purge Time End: l c.: '-I ~ -------
N -Actual purge volume : /a h,,__--;/e..,,-) f~'7~J---h-lf b"-{'1 1/LJ,..._-:-(,_,_
t3 ~I ~
Volume Volume Volume I Volume Volume Volume ------,
Temp (0 C) 1/
pH
S. c:
D. 0 .
Turbidity
Sample Information
Sample Date: V/-Lo -'t "\ Sample Time: 1 ~ er_ -S-Sample Equipment: b,._,---; c ,,..-
Water Condition (turbidity, odor, etc.) :_=~"-'-,-.,,-'--L-__,_Tc_u_,,_c_j _,'J _________________ _
Samples Collected (✓):
Temp(°C):
VOCs (2 40 ml vials)
SVOCs/PCBs (1 2L Amber bottle)
.Metals (1 lL HDPE bottle)
---pH: __ _ SC(urnhos): ---
Dioxin (1 lL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): ---
----~-r:vzl-'--_~_,(~{...,.. -~~-~r:J~-'=rt~+~· ·~e-~_~"t~'-+1~1~--f ________________ pcbwells.frm
WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton
Purge/Sample Team: E «IC-~Ice /13vB 7,/f o{) ~
7
Well#: / J_ ~--------
Comments (well construction, etc): 'c lJe..t'l cx...---=c.=..:..~---------------------
Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet)
Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet)
For hailers: 4 bails = I gallon
1 Well Volume (gal): J, 5 3 Well Volumes (gai): 4 Purge Equipment: _____ _
Date Purged:· -1-/19 /!°i, • I
Did well purge dry? Y . @,
. . "3 .'f'I.
Volume J_ ,
Temp (0 C) /~J.S
pH ~~.51
S. C. (01>.S
D . 0. ~
Purge Time Start: I O ; 3 0 Purge Time End: --+--,/~)_/_.) __
Actual purge volume:
.2 0aL
Volume 2 Volume --
2[_3 \.. I _/
~-. -:)/
?; _ I b -\. :/ I
O· VV
I 02 -~q __J,____ r) \ "'
T V ,,L._ ~
Volume 3 Volume_f_ Volume --
2 (9_) 2?.7
G-22 6 ~/7
I oo ,:) //I, D
I . Turbidity S7. I 7b-8 ~ ~ 93 143 qr. B I
Sample Date: 4 /fq
Sample Information
Sample Time: /)JS--Sample Equipment: Cr-., -.Pf::s Pv --=i>
Water Condition ~, odor, etc.): ___:9.:_J __ ---=C,""""'-'r\,'--'+_, ::......,-'--~---i::f-=v...:..."-=+'t-=-' ~-'4--'.,.,-'""..:...h_' _J _-t:....;c~c.:...,-, ..... E=<-___.SL>,c..1"""' .... c .... « ....... s .... s ,..,1 .re'-""'---
-tv r b,"i 't~ 5.,.,~ ~ > ,_ "'.,-e..-
) Samples Collected (✓):
I VOCs (2 40 ml vials)
·✓ SVOCs/@1 2L Amber bottle)
Metals (1 lL HDPE bottle)
I Temp(°C): ---pH: ---SC(umhos): __ _
Dioxin (1 IL bottle)
Pest./Herb. (1 2L amber bottle)
DO(ppm): __ _ Turb(NTUs): ---
I Comments: _________________________________ _
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