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Home My WebLink AboutNCD980602163_19970619_Warren County PCB Landfill_SERB C_EPA Report on Split Samples-OCR( 4APT-TS MEMORANDUM :JUN 1 g igg7 SUBJECT: EPA Report on Split Samples from the Warren County PCB Landfill Investigation FROM: Craig Brown EPA, Region 4 TO : / Mike Kelly Patrick Barnes Joel Hirschhorn Enclosed, please find a copy of the subject report prepared by Jonathan Vail of the Science and Ecosystems Support Division of EPA Region 4. I have not had a chance to compare EPA' s data to the State's data on the corresponding splits. If you have any questions on the report, you can contact me at (404) 562-8990, Beverly Hudson at (404) 562-8816, or Jon Vail at (706) 355-8611 . • ,_,\,;Wasir ·· , JUN 23 1997 I ' f ... ,, .. ·: '".:--,:-,'0"':·. 4SES-EI U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, SCIENCE and .ECOSYSTEMS SUPPOR'l' DIVISION ATHENS, GEORGIA 30605-2720 MAY 2 7 1997 MEMQRANDUM SUBJECT: FROM: THRU: TO: Transmittal: Report On Spl1t Samples Collected At The Warren County Landfill Site, Warren County, North Carolina. SESD Project N~: 97 171 (RAS) & 97-0157 (Dioxin). Jonathan Vail /.,,£ Hazardous Was Sec~-. Archie Lee, Chief ---/ L Hazardous Waste Secti~~~ Beverly Hudson, RPM N9rth Site Management Branch Waste Management Division During the week of March 10, 1997, split samples were collected when I conducted the Technical Systems Audit at the Warren County PCB Landfill Site. The following report of findings summarizes the results. A total of 8 samples were split: 1 leachate, 3 ground water, 1 surface water, 1 sediment and 2 soil samples. All of the above environmental media samples were collected, preserved, handled, and documented according to the requirements and procedures found in the USEPA, Region 4, Environmental Investigations Standard Operating Procedures and Quality Assurance Manual, (EISOPQAM), May, 1996. The results indicate that low concentrations of PCBs and Dioxins were detected only in the landfill leachate, soil and sediment samples. However, no PCBs or Dioxins were found in the grouno. water or surface water samples. Table 1 lists the analytical data, summary for the leachate, ground water and surface water and Table 2 lists the analytical data summary for the soil and sediment sample results. The laboratory data sheets are included as Appendix A. Also attached are copies of the site map and the Receipt For Samples _which lists the samples that were split. On the far right side of the form are the working group's sample identification information. Please call me at (706) 355-8611. if you have any questions or comments on this investigation. Attachments cc: Craig Brown, NSMB Thoman, EIB TABLE 1. ANALYTICAL DATA SUMMARY FOR LEACHATE, GROUND WATER AND SURFACE WATER SPLIT SAMPLES. WARREN COUNTY PCB LANDFILL SITE, WARREN COUNTY, NORTH CAROLINA. EWN MI.J3A MI.J3 BI.J3 SI.J2 LEACHATE GROUNDI.JA GROUNDWA GROUNDI.JA SURFACEI.JA 03/13/97 03/12/97 03/12/97 03/11-/97 03/12/97 1510 1515 1810 1343 1315 METALS SCAN Units Amount Nte Amount Nte Amount Nte Amount Nte Amount Nte Analyte -_,_ --.... . . - ARSENIC UG/L 9 J BARIUM UG/L 270 96 46 290 37 CADMIUM UG/L 2 J COBALT UG/L 20 J 4 J 4 J CHROMIUM UG/L 6 J 69 J 31 J COPPER UG/L '6 J 17 J 20 J NICKEL UG/L 12 J 55 37 J LEAD UG/L 61 VANADIUM UG/L 14 J 13 J 4 J ZINC UG/L 35 44 76 2 J ALUMINUM UG/L 2800 J 3300 J 2400 J 94 J MANGANESE UG/L 1700 600 2 J 250 140 CALCIUM UG/L 87000 23000 2100 21000 6000 MAGNESIUM UG/L 48000 5600 1100 13000 2800 IRON UG/L 81000 J 6000 J 2600 J 570 J SODIUM UG/L . 58000 15000 3900 19000 4700 POTASSIUM UG/L 35000 8400 2600 6900 1400 EXTRACT ABLES SCAN Units Amount Nte Amount Nte Amount Nte Amount Nte Amount Nte Analyte 1,4JDICHLOROBENZENE UG/L 2 J DI·N·OCTYLPHTHALATE UG/L 24 J (3-AND/OR 4-)METHYLPHENOL UG/L 15 PHENOL UG/L 5 J EXTRACTABLES·Miscellaneous Compounds Units Amount Nte Amount Nte Amount Nte Amount Nte Amount Nte Compound 15 UNIDENTIFIED COMPOUNDS UG/L 400 J 2 UN !DENT IF I ED COMPOUNDS UG/L 50 J 6 UNIDENTIFIED COMPOUNDS UG/L 90 J BENZENEACETIC ACID UG/L 300 JN BENZEMEPROPANOIC ACID UG/L 4 JN CAPROLACTAM UG/L 2000 JN 200 JN CARBOXYLIC ACIDS UG/L 9 JN DIHYDROINDAZOLONE UG/L 8 JN DIMETHYLPHENOL(NOT 2;4) UG/L 20 JN OLEYL .ALCOHOL UG/L 3 JN PESTICIDES/PCB SCAN Units Amount Nte Amount Nte Amount Nte Amount Nte Amount Nte Analyte PCB-1248 (AROCLO~ 1248) UG/L 4.8 N PCB-1260 (AROCLOR 1260) UG/L . 16 DIOXINS SCAN Units Amount Nte Amount Nte Amount Nte Amount Nte Amount Nte Analyte OCTACHLOROOIBENZOOIOXIN '.' p I NG/L 0.69 PENTACHLOROOIBENZOFURAN (TOTAL) NG/L 0.014 J HEXACHLOROOIBENZOFURAN (TOTAL) NG/L 0,016 J 1,2,3,4,7,8,9-HEPTACHLOROOIBENZOFURAN NG/L 0.013 J OCTACHLOROO!BENZOFURAN NG/L 0. 12 TEQ (TOXIC. EQUIV. VALUE, FROM l·TEF/89 NG/L 0.0009 J 0 0 0 0 ***FOOTNOTES********************************************************************-********************~* ·· ·material was analyzed for· but not detected. J ·estimated value. N ·preslll1>tive evidence of presence of material. TABLE 2. ANALYTICAL DATA SUMMARY FOR SOIL AND SEDIMENT SPLIT SAMPLES. YARREN CCXJNTY PCB LANDFILL SITE, YARREN COUNTY, NORTH CAROLINA. LCP1 LCP3 sos SOIL SOIL SEDIMENT 03/13/97 03/13/97 03/12/97 1140 1215 1230 METALS SCAN Units Amount Nte Amount Nte Amount Nte Analyte ARSENIC MG/KG 3.1 4.4 BARIUM MG/KG 40 so 130 CADMIUM MG/KG 1.4 JN 1.9 JN 0.81 J COBALT MG/KG 3 •. 1 J 3.6 J 12 J CHROMIUM MG/KG 18 J 32 J 14 J COPPER MG/KG 13 21 . 18 NICKEL MG/KG 4.9 4.4 J 6.2 J LEAD-MG/KG 8.6 14 J 8.4 SELENIUM MG/KG 0.94 J VANADIUM MG/KG. 80 130 53 ZINC MG/KG 120 78 34 TOTAL MERCURY MG/KG 0.29 ALUMINUM MG/KG 12000 J 23000 J 10000 J MANGANESE MG/KG 200 120 380 CALCI.UM MG/KG· 2300 J 530 J 1300 J MAGNESIUM MG/KG 500 700 1900 IRON MG/KG 30000 48000 21000 SODIUM MG/KG 190 POTASSIUM MG/KG 560 950 1300 % MOISTURE % 29 32 62 EXTRACTABLES·Miscellaneous Compounds Units Amount Nte Amount Nte Amount Nte Compound 1 UNIDENTIFIED COMPOUND UG/KG 800 J 4 UNIDENTIFIED COMPOUNDS UG/KG 4000 J 8 UNIDENTIFIED COMPOUNDS UG/KG 10000 J CARBOXYLIC ACIDS UG/KG 300 JN 300 JN 4000 J TETRAHYDRONAPHTHALENE UG/KG 800 JN PEST! C IDES/PCB SCAN Units Amount Nte Amount Nte Amount Nte Analyte PCB-1260 (AROCLOR 1260) UG/KG 100 VOLATILES SCAN Units Amount Nte Amount Nte Amount Nte Analyte ACETONE UG/KG 84 33 N DIOXINS SCAN Units Amount Nte Amount Nte Amount Nte Analyte OCTACHLOROOIBENZODIOXIN NG/KG 76 200 150 TETRACHLOROOIBENZOFURAN (TOTAL) NG/KG 1.2 J PENTACHLOROOIBENZOFURAN (TOTAL) NG/KG 2.1 J TEQ (TOXIC . EOUIV. VALUE, FROM I-TEF/89 NG/KG 0.076 0.2 0.15 ***FOOTNOTES******************************************************************** ---material was analyzed for but not detected. J -estimated value. N -pres~tive evidence of presence of material. ~ N I w♦• I $ LCP1 MW3A 00 MW3 SDS./\ SW2 ( _\ o-·-0 EWN Sand Filter Carbon Filter Leachate Collection Pond (Dry) Warren County PCB Landfill NOTE: Sketch or site features and spllt sample lacatlo~s are approximate an~ not to scale. ~ ~ IE: pr\ A·\ Figure 1. Split Sample Loc_atio_ns, .. 0 BW3 Approx Im ately 2 miles east. ~ L ... s! / \ ::~~=~ ~:~~:~.PN~~t~~nadr:111i:~te, APPENDIX A LABORATORY DATA SHEETS WARREN COUNTY PCB LANDFILL SITE WARREN COUNTY, NORTH CAROLINA ........, METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/01/97 15:36 . Sample 3676 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC . Program: NSF Case Number: 25349 Id/Station: BW3 MD Number: ME66. Media: GROUNDWA RESULTS UNITS 2400J UG/L 6U UG/L 5U UG/L 290 UG/L 2U UG/L 1U UG/L 21000 UG/L 31J UG/L 4J UG/L 20J UG/L 2600J UG/L 3U UG/L 13000 UG/L 250 UG/L 0.10U UG/L 37J UG/L 6900 · UG/L 3U UG/L 1U. UG/L 19000 UG/L 4U UG/L 4J UG/L 76 UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON D Number: ME66 LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. ·N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: . Beginning: 03/11/97 13:43 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. Li-material was analyzed for but not detected. the number Is the minimum quanlitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. . · C-confirmed by gems: 1.when no value is reported, see chlordane.constituents 2.constituenls or metabolites of technical ·chlordane ----METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTEO'0S/01/97 15:36 . Sample 3677 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349. Id/Station: SD5 MD Number: ME67 Media: SOIL RESULTS 10000J 1.8UJ 1.9U 130 2U 0.81J 1300J 14J 1.2J 18 21000 8.4 1900 380 0.29 6.2J 1300 1.4U 0.79U 190 2.2U 53 34 62 UNITS MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG % ANALYTE ALUMINUM· ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON D Number: ME67 LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC % MOISTURE lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/12/97 12:30 Ending: K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling-and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value Is reported, see chlordane c~nstituents 2.constituents or metabolites of technical chlordane ...,,. .. 'METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/01/9715:36 ' Sample 3678 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF . Case Number: 25349 Id/Station: SW2 MD Number: ME68 Media: SURFACEWA D Number: ME68 RESULTS .UNITS ANALYTE 94J UG/L ALUMINUM 6U UG/L ANTIMONY 5U UG/L ARSENIC 37 UG/L BARIUM 1U UG/L BERYLLIUM 1U UG/L CADMIUM 6000 UG/L CALCIUM 1UJ UG/L CHROMIUM 2U UG/L COBALT 1U UG/L COPPER 570J UG/L IRON 3U UG/L LEAD 2800 UG/L MAGNESIUM 140 UG/L MANGANESE o.fou UG/L TOTAL MERCURY 3U UG/L NICKEL 1400 UG/L POTASSIUM 3U UG/L SELENIUM 1U UG/L SILVER 4700 UG/L SODIUM 4U UG/L THALLIUM 2U UG/L VANADIUM 2J UG/L ZINC lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NA I-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/12/97 13: 15 Ending: K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. 'resampling and reanalysis is necessary for verification. · C-conflrmed by gems: 1.when no value is reported, see chlordane constituents 2·.constituents or metabolites of technical chlordane 4iElALS SAMPLE ANALYSIS EPA -REGION IV SESD, A.THENS, GA PRINTED 05/01/97 15:36 Sample 3679 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: MW3A MD Number: ME69 Media: GROUNDWA RESULTS UNITS 3300J UG/L 6U UG/L 5U UG/L 96 UG/L 1U UG/L 1U UG/L 23000 UG/L 69J UG/L 4J UG/L 17J UG/L 6000J UG/L 3U UG/L 5600 UG/L 600 UG/L 0.10U UG/L 55 UG/L 8400 UG/L 3U UG/L 1U UG/L 15000 UG/L 4U UG/L 13J UG/L 44 UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON D Number: ME69 LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC lnorg Contractor: INCHVT Org Contractor: IEA Printed by: John Mcconney Collected By: Beginning: 03/12/97 15: 15 Ending: A-average value. NA-rrot analyzed. NAl-lnterferences. J-estlmated value .. N-presumptive evidence of presence of material. K-actual vaiue Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane ca -~ 'ETALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 05/01/97 15:36 Sample 3680 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC . Program: NSF Case Number: 25349 Id/Station: MW3 MD Number: ME70 Media: GROUNDWA D Number: ME70 . RESULTS 9UJ 6U 5U 46 1U 1U 2100 2UJ 1U 1U 20UJ 3U 1100 2J 0.10U 3U 2600 3U 1U 3900 4U 2U 2U UNITS UG/L· UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L· UG/L UG/L UG/L UG/L UG/L 'UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOT AL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence or material. Printed by: John Mcconney Collected By: Beginning: 03/12/97 18:10 Ending: K-actual value Is known to be less than value given. L-actual value is known to be gre~ter than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmect by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites or technical chlordane ~ METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 05/01/97 15:36 Sample 3681 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC . Program: NSF Case Number: 25349 Id/Station: LCP1 MD Number: ME71 Media: SOIL RESULTS 12000J 0.91UJ 3.1 40 1U 1.4JN 2300J 18J 3.1J 13 30000 8.6 500 200 0.1U 4.9 560 · 0.94J 0.39U 60U 1.1U 80 120 29 UNITS MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG % ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON D Number: ME71 LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC % MOISTURE lnorg Contractor: INCHVT Org Contractor: IEA A-average value: NA-not analyzed. NA I-interferences. J-estimated value .. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/13/97 11 :40 Ending: K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-conflrmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical ·chlordane· Sample 3682 FY 1997 Project: 97-0171 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 ld/Station:LCP3 MD Number: ME72 Media: SOIL RESULTS 23000J 0.99UJ 4.4 50 1U 1.9JN 530J 32J 3.6J 21 48000 14J 700 120 0.1U 4.4J 950 2U 0.42U 70U 1.2U 130 78 32 UNITS MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG MG/KG % ANALYTE ALUMINUM. ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM. CALCIUM CHROMIUM COBALT COPPER IRON D Number: ME72 LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC % MOISTURE EPA -REGION IV SESD, ATHENS, GA lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/13/97 12: 15 Ending: PRINTED-05/01/97 15:36 K-actual value is known·to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-conflrmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane , METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 05/01/9715:36 Sample 3683 FY 1997 Project: 97-0111 METALS SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: EWN MD Number: ME73 Media: LEACHATE RESULTS .UNITS 2800J UG/L 6U UG/L 9J UG/L 270 UG/L 1U UG/L 2J UG/L 87000 UG/L 6J UG/L 20J UG/L 6J UG/L 81000J UG/L 61 UG/L 48000 UG/L 1700 UG/L o.1bu UG/L 12J UG/L 35000 UG/L SU UG/L 1U UG/L 58000 UG/L 4U UG/L 14J UG/L 35 UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM . CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON D Number: ME73 LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value·. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/13/97 15: 1 O Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-conflrmed by gems: 1.when no value is reported, see chlordane constituents 2:constituents or metabolites of technical chlordane EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, A-THENS, GA PRINTED 05/07/97 15:52 Sample 3676 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: BW3 MD Number: ME66 Media: GROUNDWA RESULTS 10UR 10UJ 10UR 10UJ 10UJ 10UJ 10UR 10UJ 10UR 10UJ 10UJ 10UJ 10UJ 10UR 10UR 10UR 10UR 10UJ 10UJ 10UJ 10UJ 10UR 10UJ 10UJ 10UR 25UR 10UJ 25UJ 10UJ 10UJ 10UJ 25UJ 10UJ 25UR 25UR 10UJ 10UJ 10UJ UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L D Number: ME66 ANALYTE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE . ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4, 5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE HOLDING TIMES EXCEEDED( 40 CFR 136, OCTOBER 26, 1984) Printed by: Yolanda Brown Collected By: Beginning: 03/11 /97 13:43 Ending: lnorg Contractor: INCHVT Org Contractor: IEA RESULTS· UNITS 10UJ UG/L 10UJ UG/L 25UJ UG/L 25UR UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 25UR UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L ANALYTE 4~HLOROPHENYLPHENYLETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE OI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE -BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE D1-N-OCTYLPHTHALA TE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE _ DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE A-average value. NA-not analyzed. NAl-interferences. J-estimated value. · N-presumptive evidence of presence of material. K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and r'eanafysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constitlients or metabolites of technical chlordane ~-EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3676 FY 1997 Project: 97-0171 MISCELLANEOUS COMPOUNDS Facility: WAR~EN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: BW3 MD Number: ME66 Media: GROUNDWA RESULTS UNITS 200JN 9JN 90J D Number: ME66 ANALYTE CAPROLACTAM CARBOXYLIC ACIDS 6 UNIDENTIFIED COMPOUNDS lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda 'Brown Collected By: Beginning: 03/11 /97 1343 Ending: K-actual value is known to be less than value given. L-actual value is known to be grec!ter than value given. LI-material was analyzed for but not detected. th.e number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmea by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Q.4 :-.. . -----~XTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3677 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC · Program: NSF Case Number: 25349 ld/Station:SD5 MD Number: ME67. Media: SOIL RESULTS 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UR 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 2200UJ 890UJ_ 2200UJ 890UJ 890UJ . 890UJ 2200UJ 890UJ 2200UJ 2200UJ 890UJ 890UJ 890UJ UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG D Number: ME67 ANALYTE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL . 1, 3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-0,CHLOROPHENOL . 1,2,4-TRICHLOROB.ENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE . . HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE EXCESSIVE HOLDING TIME lnorg Contractor: INCHVT Org Contractor: IEA RESULTS 890UJ 890UJ 2200UJ 2200UJ 890UJ 890UJ 890UJ 2200UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ 890UJ. 890UJ 890UJ 890UJ 890UJ 63 A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 12:30 Ending: UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG. UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % ANALYTE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE. FLUORANTHENE PYRENE BENZYL BUTYL PHTHALA TE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALATE . BENZO(B.AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE % MOISTURE K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. . C-confirmecl by gems: 1.when no value is reported, see chlordane _constituents 2.constituents or metabolites of technical chlordane """ EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTE0 05/07/97 15:52 Sample 3677 FY 1997 Project: 97-0171 MISCELLANEOUS COMPOUNDS Facility: WARREN COUNTY PCB LANDFILL , NC. Program: NSF Case Number: 45349 Id/Station: SD5 MD Number: ME.67 Media: SOIL D Number: ME67 RESULTS UNITS 800JN 4000J 10000J ANALYTE TETRAHYDRONAPHTHALENE CARBOXYLIC ACIDS . 8 UNIDENTIFIED COMPOUNDS lriorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 12:30 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane , EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3678 FY 1997 Project: 97-0171 EXTRACT ABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: SW2 MD Number: ME68 Media: SURFACEWA RESULTS .UNITS 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10UR UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 25U UG/L 10U UG/L. 25U UG/L 10U UG/L 10U UG/L 10U UG/L 25U UG/L 10U UG/L 25U UG/L 25U UG/L 10U UG/L 10U UG/L 10U UG/L D Number: ME68 ANALYTE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE. lnorg Contractor: INCHVT Org Contractor: IEA . RESULTS 10U 10U 25U 25U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U A-average value. NA-not analyzed. NAl-interferences. J-eslimated value·. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 13:15 Ending: UNITS UG/L UG/L UG/L UG/L. UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 0I-NsBUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE 0I-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZP-A-PYRENE INDENO (1,2,3-CO) PYRENE DIBENZO(A, H)ANTHRACENE BENZO(GHl)PERYLENE K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2:constituents or metabolites of technical chlordane ~ ·'exTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, A:THENS, GA PRINTED 05/07/97 15:52 Sample 3679 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: MW3A MO Number: ME69 Media: GROUNDWA RESULTS 5J 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 25U 10U 25U 10U 10U 10U 25U 10U 25U 25U 10U 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L _ UG/L -UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L D Number: ME69 ANALYTE PHENOL BIS(2~CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSOOI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-0ICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTAOIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TR ICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-0INITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITf;<OPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 15: 15 Ending: lnorg Contractor: INCHVT Org Contractor: IEA RES UL TS-UNITS 10U UG/L 10U UG/L 25U UG/L 25U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L . 10U UG/L 10U UG/L 10U UG/L 10U UG/L 24J UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L 10UJ UG/L ANALYTE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE ~BROMOPHENYLPHENYLETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 01-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALA TE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE 01-N-OCTYLPHTHALA TE BENZO(B A~D/OR K)FLUORANTHENE BENZO-A-PYRENE INOENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE A-average value. NA-not analyzed. NAl-interferences. J-estimated value. · N-presumptive evidence of presence of material. K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanafysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane W# _, ' EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3679 FY 1997 Project: 97-0171 MISCELLANEOUS COMPOUNDS Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: ·25349 Id/Station: MW3A MD Number: ME69 Media: GROUNDWA RESULTS UNITS 2000JN 3JN 400J D Number: ME69 ANALYTE CAPROLACT AM OLEYL ALCOHOL 15 UNIDENTIFIED COMPOUNDS lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yoland~ Brown Collected By: Beginning: 03/12/97 15: 15 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane XTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3680 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC . Program: NSF Case Number: 25349 Id/Station: MW3 MO Number: ME70 Media: GROUNDWA D Number: ME70 RESULTS 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 25U 10U 25U 10U 10U 10U 25U 10U 25U 25U 10U 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE PHENOL' BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-D1CHLOROPHENOL . 1,2,4-TRICHLOROBENZENE NAPHTHALENE . 4-CHLOROANIL,INE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE · , HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TR ICHLOROPHENOL 2,4,5-TRICHLOROPHENOL . 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE lnorg Contractor: INCHVT Org Contractor: IEA RESULTS 10U 10U 25U 25U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U A-average value. NA-not analyzed. NAl-interferences. J-estimated value. ·N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: , Beginning: 03/12/97 18:10 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/1,. ANALYTE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB). PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 0I-N-BUTYLPHTHALA TE· FLUORANTHENE PYRENE BENZYL BUTYL PHTHALA TE 3,3'-DICHLOROBENZIQINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE D I-N-OCTYLPHTHALA TE BENZO(B.AND/OR K)FLUORANTHENE BENZO~A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. . · C-confirmed by gems: 1.when no value is reported, see chlordane.constituents 2.constituents or metabolites of technical ·chlordane ~ EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTE0-05/07/97 15:52 Sample 3681 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: LCP1 MO Number: ME71 Media: SOIL RESULTS UNITS 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UR 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 1200UJ 460UJ 1200UJ 460UJ 460UJ 460UJ 1200UJ 460UJ 1200UJ 1200UJ 460UJ 460UJ 460UJ UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG . UG/KG UG/KG UGti<.G UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG D Number: ME71 ANALYTE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-0ICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENO~ N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4, 6-TRICHLOROPHENOL 2,4, 5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-0INITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL OIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE EXCESSIVE HOLDING TIME lnorg Contractor: INCHVT Org Contractor: IEA RESULTS 460UJ 460UJ 1200UJ ·1200UJ 460UJ 460UJ 460UJ 1200UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 460UJ 29 A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 11: 40 Ending: UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % ANALYTE 4-CHLOROPHENYL PHENYL ETHER FLUORENE . 4-NITROANILINE 2-METHYL-4,6-0INITROPHENOL NsNITROSOOIPHENYLAMINE/DIPHENYLAMINE ~BROMOPHENYLPHENYLETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE D1-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE D I-N-OCTYLPHTHALA TE BENZO(B ANO/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A, H)ANTHRACENE BENZO(GHl)PERYLENE % MOISTURE K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling.and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane .. EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3681 FY 1997 Project: 97-0171 MISCELLANEOUS COMPO_UNDS Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: LCP1 MD Number: ME71 Media: SOIL D Number: ME71 RESULTS .UNITS ANAL YTE 300JN CARBOXYLIC ACIDS 800J 1 UNIDENTIFIED COMPOUND lnorg Contractor: INCHVT Org Contractor: IEA _ A-average value. NA-not analyzed. NAl-interferences. J-estimated value·. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 11:40 Ending' K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected .. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2:constituents or metabolites of technical chlordane ~ EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, A.THENS, GA PRINTED 05/07/97 15:52 Sample 3682 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: LCP3 MD Number: ME72 Media: SOIL D Number: ME72 lnorg Contractor: INCHVT Org Contractor: IEA Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 12:15 Ending: RESULTS 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UR 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG ANALYTE RESULTS· UNITS ANALYTE 1200UJ 480UJ 1200UJ 480UJ 480UJ 480UJ 1200UJ 480UJ 1200UJ 1200UJ 480UJ 480UJ 480UJ . UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG PHENOL BIS(2~CHLOROETHYL) ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2, 4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TR ICHLOROPHENOL 2,4,5-TR ICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALA TE EXCESSIVE HOLDING TIME · 480UJ 480UJ 1200UJ 1200UJ 480UJ 480UJ 480UJ 1200UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 480UJ 31 A-average value. NA-riot analyzed. NAl-interferences. J-estimated value.· N-presumptive evidence of presence of material. UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG. UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % 4-CHLOROPHENYLPHENYLETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 01-N-BUTYLPHTHALA TE .FLUORANTHENE PYRENE . BENZYL BUTYL PHTHALA TE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE l31S(2-ETHYLHEXYL) PHTHALA TE 01-N-OCTYLPHTHALA TE BENZO(B A~D/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE. BENZO(GHl)PERYLENE % MOISTURE K-actual va_lue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane -XTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3682 FY 1997 Project: 97-0171 MISCELLANEOUS COMPOUNDS Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 ld/Station:LCP3 MD Number: ME72 Media: SOIL RESULTS UNITS 300JN 4000J D Number: ME72 ANALYTE CARBOXYLIC ACIDS 4 UNIDENTIFIED COMPOUNDS lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda1Brown Collected By: Beginning: 03/13/97 12: 15 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmea by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESO, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3683 FY 1997 Project: 97-0171 EXTRACTABLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: EWN MD Number: ME73. Media: LEACHATE D Number: ME73 RESULTS 10U 10U 10U 10U 2J 10U 10U 10U 15 10U 10U 10U 10U 10U 10U 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 25U 10U 25U 10U 10U 10U 25U 10U 25U 25U 10U 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L --UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL . BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL N-N ITROSODI-N-PROPYLAM I NE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-N ITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DlCHLOROPHENOL . 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADI ENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE . HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4, 5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE lnorg Contractor: INCHVT Org Contractor: IEA RESULTS 10U 10U 25U 15U 10U 10U 10U 25U 10U . 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 15: 10 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L l,JG/L UG/L UG/L UG/L ANALYTE ~CHLOROPHENYLPHENYLETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4~ROMOPHENYLPHENYLETHER HEXACHLOROBENZENE(HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE. FLUORANTHENE PYRENE BENZYL BUTYL PHTHALA TE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE D1-N-OCTYLPHTHALATE . BENZO(B.AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound m~y or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane .constituents 2.constituents or metabolites of technical chlordane ., -. ' EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SES0, ATHENS, GA PRINTEO' 05/07/97 15:52 Sample 3683 FY 1997 Project: 97-0171 MISCELLANEOUS COMPOUNDS Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: EWN MD Number: ME73 Media: LEACHATE RESULTS UNITS 20JN 300JN BJN 50J 4JN D Number: ME73 ANALYTE DIMETHYLPHENOL(NOT 2,4) BENZENEACETIC ACID DIHYDROINDAZOLONE 2 UNIDENTIFIED COMPOUNDS BENZENEPROPANOIC ACID lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 15: 10 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane c9nstituents 2.constituents or metabolites of technical chlordane PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3676 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: BW3 . MD Number: ME66 Media: GROUNDWA RESULTS .UNITS 0.050UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 0.10UJ UG/L 0.10UJ UG/L 0.10UJ UG/L 0.10UJ UG/L 0.10UJ UG/L 0.10UJ UG/L 0.1°0UJ UG/L 0.50UJ UG/L 0.10UJ UG/L 0.10UJ UG/L 0.050UJ UG/L 0.050UJ UG/L 5.0UJ UG/L 1.0UR UG/L 2.0UJ UG/L 1.0UJ UG/L 1.0UJ UG/L 1.0UJ UG/L 1.0UJ UG/L 1.0UJ UG/L D Number: ME66 ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'~DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-000 (P,P'-000) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENORIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) . PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984) lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/11/97 1343 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. ·resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3677 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 ld/Station:SD5 MD Number: ME67 Media: SOIL RESULTS 4.6U 4.6U 4.6U 4.6U 4.6U 4.6U 4.6U 4.6U 8.9U 8.9U 8.9U 8.9U 8.9U 8.9U 8.9U 46U 8.9U 8.9U 4.6U 4.6U 460U 89UR 180U 89U 89U 89U 89U 89U 63 UNITS UG/KG UG/KG UG/KG UG/KG UG/KG · UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % D Number: ME67 ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 {AROCLOR 1248) PCB-1254 (AROCLOR 1254) -PCB-1260 (AROCLOR 1260) % MOISTURE lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. ·N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 12: 30 Ending: K-actual value is known to be less than value given. L-actuai value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane ~ PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 1~:52 Sample 3678 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: SW2 MD Number: ME68 Media: SURFACEWA D Number: ME68 RESULTS 0.050U 0.050U. 0.050U 0.050U 0.050U . 0.050U 0.050U 0.050U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.50U 0.10U 0.10U 0.050U 0.050U 5.0U 1.0UR 2.0U 1.0U 1.0U 1.0U 1.0U 1.0U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L . UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE'.) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN · ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda' Brown Collected By: Beginning: 03/12/97 13:15 Ending K-actual value Is known to be less than value given. L-actual value is known to be gre11ter than value given. U-material was analyzed for but not detected. tt:ie number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane .. ,. __ -PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3679 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: MW3A MD Number: ME69. Media: GROUNDWA D Number: ME69 RESULTS 0.0S0U 0.0S0U 0.0S0U 0.0S0U 0.0S0U 0.0S0U 0.0S0U 0.0S0U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.S0U 0.10LJ 0.10U 0.0S0U 0.0S0U 5.0U 1.0UR 2.0U 1.0U 1.0U 1.0U 1.0U 1.0U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR · ALDRIN HEPT ACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR END~IN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248)· PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NA I-interferences. J-estimated value. · N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 15:15 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound m~y or may not be present. resampling and reanalysis is necessary for veriJication. . C-confirmed by gems: 1.when no value is reported, see chlordane.constituents 2.constituents or metabolites of technical chlordane 1llll'F"" PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3680 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility:· WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: MW3 MD Number: ME?0 Media: GROUNDWA D Number: ME70 RESULTS 0.050U 0.050U 0.050U 0.050U 0.050U 0.050U 0.050U 0.050U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.50U 0.10U 0.10U 0.050U 0.050U 5.0U 1.0UR 2.0U 1.0U 1.0U 1.0U 1.0U 1.0U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) OIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-000 (P,P'-O00) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN.ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) . PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lriorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presuniptive evidence of presence of material . Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 18:10 Ending: K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane . ~ PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3681 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: LCP1 MD Number: ME71 Media: SOIL RESULTS .UNITS 2.4U 2.4U 2.4U 2.4U 2.4U 2.4U 2.4U 2.4U 4.6U 4.6U 4.6U 4.6U 4.6U 4.6U 4.6U 24U 4.6U 4.6U 2.4U 2.4U 240U 46UR 94U 46U 46U 46U 46U 100 29 UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % D Number: ME71 ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE {P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) % MOISTURE lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning 03/13/97 11 :40 Ending K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for blit not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. 'resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2-.constituents or metabolites of technical chlordane ... PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3682 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: LCP3 MD Number: ME72 Media: SOIL RESULTS UNITS 2.5U UG/KG 2.5U UG/KG 2.5U UG/KG . 2.5U UG/KG 2.5U UG/KG 2.5U . UG/KG 2.5U UG/KG 2.5U UG/KG 4.8U UG/KG 4.8U UG/KG 4.8U UG/KG 4.8U UG/KG 4.8U UG/KG 4.8U UG/KG 4.8U UG/KG 25U UG/KG 4.8U UG/KG 4.8U UG/KG 2.5U UG/KG 2.5U UG/KG 250U UG/KG 48UR UG/KG 97U UG/KG 48U UG/KG 48U UG/KG 48U UG/KG 48U UG/KG 48U UG/KG 31 % D Number: ME72 ANALYTE ALPHA-BHC BETA~BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) % MOISTURE lnorg Contractor: INCHVT Org Contractor: IEA A-average v.alue. NA-not analyzed. NAl-interferences. J-estimated value. ·N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 12: 15 Ending: K-actual val.ue Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane PESTICIDES/PCB SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3683 FY 1997 Project: 97-0171 PESTICIDES SCAN Facility: WARR.EN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: EWN MD Number: ME73 Media: LEACHATE RESULTS 0.050U 0.050U. 0.050U 0.050U 0.050U 0.050U 0.050U 0.050U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.10U 0.50U 0.10U 0.10U 0.050U 0.050U 5.0U 1.0UR 2.0U 1.0U 1.0U 4.8N 1.0U 16 UNITS UGtl· UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ·uG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L D Number: ME73 . ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENOOSULFAN II (BETA) 4,4'-000 (P,P'-OOO) ENOOSULFAN SULFATE· 4,4'-ODT (P,P'-ODT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE . PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: INCHVT Org Contractor: IEA A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. . Printed by: Yolanda Brown Collected By: Beginning: 03/13/97 15: 10 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3676 FY 1997 Project: 97-0171 VOLATILES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: BW3 MD Number: ME66. lnorg Contractor: INCHVT Org Contractor: IEA Media: GROUNDWA RESULTS 10U 10U 10U 10U 10U 10U 10U 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10l:/ 10U 10U. 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L D Number: ME66 ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1,2-DICHLOROPROPANE . CIS-1, 3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE. BROMOFORM METHYL ISOBUTYL KETONE METHYLBUTYLKETONE · TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES A-average value. NA-not analyzed. NAl-interferences. J-estimated value. · N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/11 /97 13: 43 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the mi_nimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. . C-confirmed by gems: 1.when no value is reported, see chlordane. constituents 2.constituents or metabolites of technical ·chlordane ~ VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3677 FY 1997 Project: 97-0171 VOLATILES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: SD5 MD Number: ME67 lnorg Contractor: INCHVT Org Contractor: IEA Media: SOIL RESULTS 27U 27U 27U 27U 27U 33N 27U 27UR 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 63 UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG %. D Number: ME67 ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE. CARBON DISULFIDE · 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE . 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOT AL XYLENES % MOISTURE A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 12:30 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3678 FY 1997 Project: 97-0171 VOLATILES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: SW2 MD Number: ME68 lnorg Contractor: INCHVT Org Contractor: IEA Media: SURFACEWA RESULTS UNITS 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10UR UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L 10U UG/L. 10U UG/L 10U UGIL 10U UG/L 10U UG/l 10U UG/l 10U UG/l D Number: ME68 ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE .CHLORIDE ACETONE CARBON DISULFIDE 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1,2-DICHLOROPROPANE . CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE TRANS-1, 3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOT AL XYLENES A-average value. NA-not analyzed. NA I-interferences. J-estimated value·. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning 03/12/97 13: 15 Ending: K-actual value is known to be less thar-1 value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2:constituents or metabolites of technical chlordane ~!':" VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, AJHENS, GA PRINTED 05/07/97 15:52 Sample 3679 FY 1997 Project:· 97-0171 VOLATILES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: MW3A MD Number: ME69 lnorg Contractor: INCHVT Org Contractor: IEA Media: GROUNDWA RESULTS 10U 10U 10U 10U 10lJ 10U 10U 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L .UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L D Number: ME69 ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1, 1-DICHLOROETHENE ( 1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE . 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-0I CHLOROETHANE METHYL ETHYL KETONE' 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1,2-0ICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE TRANS-1, 3-0I CHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOT AL XYLENES A-average yalue. NA-not analyzed. NAl-interferences. J-estimated value .. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: Beginning: 03/12/97 15: 15 Ending; K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3680 FY 1997 Project: 97-0171 VOLATILES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 Id/Station: MW3 MO Number: ME70 lnorg Contractor: INCHVT Org Contractor: IEA Media: GROUNDWA D Number: ME70 · RESULTS 10U 10U 10U 10U 10U. 10U 10U 10UR 10U 10U 10U 10U 10U 10U 1ou· 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L U.G/L UG/L UG/L UG/L . UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM · 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE: BROMODICHLOROMETHANE 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE . TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYLISOBUTYLKETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda' Brown Collected By: Beginning: 03/12/97 18: 10 Ending: K-actual value is known to be less than value given. L-actual value is known to be gre;iter than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirm~ by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 05/07/97 15:52 Sample 3681 FY 1997 Project: 97-0171 VOLATILES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC . Program: NSF Case Number: 25349 ld/Station:LCP1 MD Number: ME71 lnorg Contractor: INCHVT Org Contractor: IEA Media: SOIL RESULTS 14U 14U 14U 14U 14U 14U 14U 14UR 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 29 UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % D Number: ME71 ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1,2-DICHLOROPROPANE ·. CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLQROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE. BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOT AL XYLENES % MOISTURE. A-average value. NA-not analyzed. NAl-interferences. J-estimated value. ·N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By: . Beginning: 03/13/97 11: 40 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. . · C-confirmed by gems: 1.when no value is reported, see chlordane _constituents 2.conslituents or metabolites of technical chlordane .,.. VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED-05/07/97 15:52 Sample 3682 FY 1997 Project: 97-0171 VOLATiLES SCAN Facility: WARREN COUNTY PCB LANDFILL , NC Program: NSF Case Number: 25349 · Id/Station: LCP3 MD Number: ME72 lnorg Contractor: INCHVT Org Contractor: IEA Media: SOIL D Number: ME72 RESULTS 14U 14U 14U 14U 14U 84 14U 14UR 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 14U 31 UNITS UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG % ANALYTE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE. CARBON DISULFIDE 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE (TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1, 1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE. METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1, 1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOT AL XYLENES % MOISTURE A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: Yolanda Brown Collected By Beginning: 03/13/97 12:15 Ending: K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling.and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane , XINS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3666 FY 1997 Project: 97--0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF ROANOKE RAPIDS, NC Id/Station: BW3 Media: WATER RESULTS 0.02U 0.02UJ 0.05U 0.05UJ 0.05U 0.05U 0.05U 0.05UJ 0.05U 0.05UJ 0.11U 0.02U 0.02UJ 0.05U 0.05U 0.05UJ 0.05U 0.05U 0.05U 0.05U 0.05UJ 0.05U 0.05U 0.05UJ 0.1U 0 UNITS NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L D Number: BW3 ANALYTE 2,3,7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3, 7,8,9-HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLORODIBENZODIOXIN 2, 3, 7 ,8-TETRACHLORODIBENZOFU RAN TETRACHLORODIBENZOFURAN (TOT AL) 1,2,3, 7,8-PENTACHLORODIBENZOFURAN 2, 3,4, 7,8-PENTACHLORODI BENZOFWRAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,7,8,9-HEXACHLORODIBENZOFURAN 2, 3, 4,6, 7, 8-HEXACHLOROD I BENZOFURAN HEXACHLORODI BENZOFURAN (TOT AL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89) SAS Number:DIOX Org Contractor: SWOK Printed by: John Mcconney Collected By: Beginning: 03/11/97 13:43 Ending: A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value .. N-presumptlve evidence of presence of material. . PRINTED 05/09/97 15:13 K-actual value is known to be less than _value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be ,present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane OXINS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3667 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF. · ROANOKE RAPIDS, NC Id/Station: S05 Media: SOIL RESULTS 4.8U 4.8UJ 12U 12UJ 12U 12U 12U 12UJ 12U 12UJ 150 4.8U 4.8UJ 12U 12U 12UJ 12U 12U 12U 12U 12UJ 12U 12U 12UJ 24U 0.15 58 UNITS NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG . NG/KG NG/KG NG/KG NG/KG NG/KG "NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG % D Number: SD5 ANALYTE 2,3, 7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZOOIOXIN (TOTAL) 1,2,3·, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZOOIOXIN (TOT AL) 1,2, 3, 4, 7, 8-HEXACHLOROD I BENZODIOXI N 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN . 1,2,3, 7,8,9~HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN (TOTAL) . 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOOIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZOFURAN 2,3,4, 7,8-PENTACHLOROOIBENZOFURAN PENTACHLORODIBENZOFURAN (TOT AL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6, 7,8-HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE SAS Number:DIOX Org Contractor: SWOK A-average value. NA-nol analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/12/97 12:30 Ending: PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constiluents or metabolites of technical chlordane INS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3668 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF ROANOKE RAPIDS, NC Id/Station: SW2 Media: WATER RESULTS 0.02U 0.02UJ 0.05U 0.05UJ 0.05U 0.05U 0.05U 0.05UJ 0.05U 0.05UJ 0.1U 0.02U 0.02UJ 0.05U 0.05U 0.05UJ 0.05U 0.05U 0.05U 0.05U 0.05UJ 0.05U 0.05U 0.05UJ 0.1U 0 UNITS NG/L NG/L NG/L NG/L NG/L · NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L . NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L D Number: SW2 ANALYTE 2,3, 7,8-TETRACHLORODI BENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3, 7,8,9-HEXACHLORODIBENZOD(OXIN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOT AL) OCTACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZOFURAN. 2,3,4, 7,8-PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN (TOT AL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6, 7,8-HEXACHLORODI BENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN · HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89) SAS Number:DIOX Org Contractor: SWOK Printed by: John McOonney Collected By: Beginning: 03/12/97 13: 15 Ending: A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptlve evidence of presence of material. . PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number Is the minimum quantilalion limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed l>Y gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane OXINS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3669 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF ROANOKE RAPIDS, NC Id/Station: MW3A Media: WATER RES UL TS UNITS 0.02U NG/L 0.02UJ NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05UJ NG/L 0.1U NG/L 0.02U NG/L 0.02UJ NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.05U. NG/L 0.05U NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.1U NG/L 0 NG/L D Number: MW3A ANALYTE 2,3, 7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLOROOIBENZODIOXIN (TOT~L) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3, 7,8,9-HEXACHLORODIBENZODIOXI N HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL) 1, 2, 3, 7, 8-PENT ACHLOROD I BENZOFURAN 2, 3,4, 7,8-PENT ACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6,7,8-HEXACHLOROOIBENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN (tOTAL) OCTACHLORODIBENZOFURAN TEQ (TOXIC. EQUIV. VALUE,. FROM I-TEF/89) SAS Number:DIOX Org Contractor: SWOK A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney· Collected By: Beginning: 03/11./97 15: 15 Ending: PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-materlal was analyzed for but not detected. the number Is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. C-confirmed by gems: 1.when no value is reportetl, see chlordane constituents 2.constituents or metabolites of technical chlordane •hfox1NS -SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3670 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL ROANOKE RAPIDS, NC Program: SSF SAS Number:DIOX . Id/Station: MW3 Media: WATER D Number: MW3. Org Contractor: SWOK RESULTS UNITS 0.02U NG/L 0.02UJ NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05UJ NG/L 0.1U NG/L 0.02U NG/L 0.02UJ NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05U NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05U NG/L 0.05UJ NG/L 0.1U NG/L 0 NG/L ANALYTE 2,3, 7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2, 3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6,7,S~HEXACHLORODIBENZODIOXIN. 1,2,3, 7,8,9-HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL}· OCTACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZOFURAN 2, 3,4, 7,8-PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6, 7,8-HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6, 7,8-HEPT ACHLORODIBENZOFURAN 1,2, 3,4, 7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN. (TOTAL) OCTACHLORODIBENZOFURAN TEQ (TOXIC. EQUIV. VALUE, FROM I-TEF/89) A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/12/97 18:10 Ending: PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number Is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling.and reanalysis Is necessary for verification. C-:eonfirmed by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or meta.bolltes of technical chlordane XINS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3671 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF ROANOKE RAPIDS, NC Id/Station: LCP1 Media: SOIL RESULTS 2.8U 2.8UJ 7.0U 7.0UJ 7.0U 7.0U 7.0U 7.0UJ 7.0U 7.0UJ 76 2.8U 1.2J 7.0U 7.0U 2.1J 7.0U 7.0U 7.0U 7.0U 7.0UJ 7.0U 7.0U 7.0UJ 14U 0.076 29 UNITS NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG % D Number: LCP1 ANALYTE 2, 3, 7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3, 7,8,9-HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL) OCT ACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOT AL) 1,2,3, 7,8-PENTACHLORODIBENZOFURAN 2, 3, 4, 7 ,8-PENT ACHLORODI BENZ OF URAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6, 7,8-HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEQ (TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE SAS Number:DIOX Org Contractor: SWOK A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value .. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/13/97 11 :40 Ending: PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. · C-confirmed by gems: 1.when no value Is reported, see chlordane constituents 2.c,:onstituents or metabolites of technical chlordane XINS SAMPLE ANALYSIS EPA -REGION IV SESD, A,:HENS, GA Sample 3672 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF . ·ROANOKE RAPIDS, NC Id/Station: LCP3 Media: SOIL RESULTS 2.9U 2.9UJ 7.4U 7.4UJ 7.4U. 7.4U 7.4U 7.4UJ 7.4U 7.4UJ 200 2.9U 2.9UJ 7.4U 7.4U 7.4UJ 7.4U 7.4U 7.4U 7.4U 7.4UJ 7.4U 7.4U 7.4UJ 12U 0.2 32 UNITS NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG NG/KG % D Number: LCP3 ANALYTE 2,3, 7,8-TETRACHLORODI BENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3,7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9~HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN. HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZOFURAN 2;3,4, 7,8-PENT ACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6, 7,8-HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6, 7, 8-HEPT ACHLORODIBENZOFURAN 1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEQ (TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE SAS Number:DIOX Org Contractor: SWOK A-average value. NA-not analyzed. NA I-Interferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/13/97 12: 15 . Ending:. PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number-is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-confirmed by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane 'INS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Sample 3673 FY 1997 Project: 97-0157 DIOXIN SCAN Facility: WARREN CO PCB LANDFILL Program: SSF ROANOKE RAPIDS, NC Id/Station: EWN Media: WATER RESULTS UNITS 0.02U NG/L 0.02UJ NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.05U · NG/L 0.05U NG/L 0.05UJ NG/L 0.05U NG/L 0.09UJ NG/L 0.69 NG/L 0.02U NG/L 0.02UJ NG/L 0.05U NG/L 0.05U NG/L 0.014J NG/L 0.05U NG/L 0.05U NG/L 0.05U . NG/L 0.05U NG/L 0.016J NG/L 0.05U NG/L 0.013J NG/L 0.05UJ NG/L 0.12 NG/L 0. 0009J NG/L D Number: EWN ANALYTE 2,3, 7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7,8-PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXI N 1,2,3,6, 7,8-HEXACHLORODIBENZODIOXI N 1,2,3, 7,8,9-HEXACHLORODIBENZODLOXIN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLORODIBENZODIOXIN 2,3, 7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL). 1,2,3, 7,8-PENTACHLORODIBENZOFURAN 2,3,4, 7,8-PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,7,8,9-HEXACHLORODIBENZOFURAN 2, 3, 4, 6, 7, 8-HEXACHLORODI BENZOFURAN HEXACHLORODIBENZOFURAN (TOT AL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN . HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89) SAS Number:DIOX Org Contractor: SWOK A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Printed by: John Mcconney Collected By: Beginning: 03/13/97 15: 10 Ending: PRINTED 05/09/97 15:13 K-actual value Is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. · C-conflnned by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane )DJ~/,,\ . ~~Environmental Consultants /iil.,rn110, f'11rl.,nd a,nd t!loeocl1Jt0>0, Inc. ; 'i~~:/ ~@ ' . ., ~ ~D ,,~" «~H. a i, _./ ~ > \I . 2) \ '@' = \\ ::-= -.... EGEND SURFACE WATTR SAMPLE (SW) SEDIMENT SAMPLE (SS) EXISTING SURFACE WATER STATIONS ~ EXISTING WELL (MW) A HYDRO PUNCH SAMPLES @ NEW WELL CLUSTER (MW) ® 0 NEW WELL, POSSIBLE CLUSTER NEW DEEP WELL (MW) 01-21-1997 0':"44 AH. WARREN COUNTY PCB LANDFILL EXISTING & PROPOSED MONITORING SITES FIGURE 3-1 I 1 · t"' .. I.,, ,ii ~EPA REGION 4 RECEIPT FOR SAMPLES ENVIRONMENTAL SERVICES DIVISION COLLEGE STATION ROAD U.S. ENVIRONMENTAL PROTECTION AGENCY ATHENS, GEORGIA 30613-7799 PROJECT NO. PROJECT NAME . NAME & LOCATION OF FACILTY/SITE h "f<. : 91-ot'll Lv:.i.vH;..__ [c,, l".._tf(,'/( ~-;1-( W,lv-r--t~ Cv. Le-\.,.__J{,1/ S'if~ w_---~:::\ 1 ",:,., p · , SAMPLEiµ~GNtY;:;JJ .:tt S O"-{o c:,..,._ W"-v-I'<"' Co· N C (04'1-Ji.....: 01" . ) . \ ' .(, t Id copy(w~ ➔id) ' 19<:l...7 a. al SPLIT . l1Jc,1-£-i•~1 :J < 0 a: STATION LOCATION/DESCRIPTION NO, OF EPA SAMPLES EPA SAMPLE TAG NO.'S/REMARKS /&t-ov.~½:t-STATION NO. 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