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Home My WebLink AboutNCD980602163_19970508_Warren County PCB Landfill_SERB C_Monitoring Wells - PCB Sampling Results, April 1997-OCRN.C. Department of Environment, I lcallh, & Nalur~! Re:;:oY,~ccs Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ ----'0)."'-"""'0---'2~J__._-i-f--------- Name of Site W ft RR tDJ C,V/1/T'( ¼o ELL£-Site Location __ { .... ,y"-'-ft-'-'8 ...... &""'t!:'--'-AJ~_G_v_ll/_rf~------- Collected By ----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ___:::::_ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ~ Ground water (1) t<.TB '!> --_ Solid (5) Cadmium --Chromium ---? J;t 'e-16) __ Surface water (2) Lead --=---qm --__ Mercury __ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry --... Parameter · . ( Results(mg/1) ~arameter Results(mg/1) (mg/kg) Organic Compound!'! Results(mg/1) _ P&T:GC/MS ./ Arsenic benzene --✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- 1-. Hexb. Chloride chlorobenzene -----~'-1-JJ <t>,oo I Chromium chloroform ----_ ~':/4s-r.P <·0.001 __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dini trotol uene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----·······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- Date Rccc;,cd cf~ /J-C/71U}a-~'j,_~ ,/J~ lindane --__ methoxychlor &iii ms:, ----__ toxaphene Dale Exlraclc<l UtfJ q "}.,,/ f 7,/3;{) Dal eporle~ -5-: q ~ -9 7 --2,4-D r11f!S", 1 6)J"4 ~· lli.lbJ _ 2,4,5-TP (Silvex) Dale Analyzed J/·.J..l/,'17 t/,)../-1 7/Y) Lab Number --DI IS 3191 (ltcviscd 2/91)/31J ''·'--· ucpartmcnt of Environment, I lcalth, & Natural Resources Solid Waste Managem~nt Division . . ~AMPL~ ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O"a.~0'"'7'2... ------"--"'=-=-"-.......... -=-L-------- Name of Site Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds --- --- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) ,-g 1. --_ Solid (5) Cadmium --Chromium --,?2 < Litft!kt (6) __ Surface water (2) Lead --__ Mercury . Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) i)'arameter . Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) P&T:GC/MS Arseruc benzene ------✓ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- _.\L_ L-1:e-rb . Chloride chlorobenzene -----i:1-J) <o.oo / Chromium chloroform ----<o.oo l __ Copp~r o-cresol =s--TP --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene ----Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----···•··-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --tetrachloroethylene -- ----trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ---vinyl chloride --endrin -- L/----!I-C/1 ~ lindane --Date Received Reported by methoxychlor 8IJ/l --"151-<,t __ toxaphene D:it e ExlractcJ 'l-l?-'i7 i/-,),j-fJf.3{) Dale Reported 2,4-D . -.. -.. --li,J>, '}-711 f:.t~97 ~7138 ' __ 2,4,5-TP (Silvex) f'15j 5',4 Date Analyzcdq-,N-17 Lab Number --DI IS 319 1 (Revised 2/91)~ ~- 1,.1...... ucpanmcn1 or .tnvironmcnt, I lcalth, & Natural Resources Solid Waste Managcm~nt Division ' ' ;:::iANl.t'L~ ANALYM~ IU:(JU.EST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number 02..0091"3 ___ _..;; __ ---'---"'-------------------------- Name of Site WARR, e, IJ f'ovl\f T'<'. ½o FJU-.. Site Location __ -"'-W=-'-1+.:...J.8:..i.&,._,~="";:;:__-G_v-',v'-ty'-'--------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) A:W·:l · --_ Solid (5) Cadmium --Chromium < 1si;m(6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter ~sults(mg/1) DParameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS ~ Arsenic benzene --✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- ~ L-1:e:rb . Chloride chlorobenzene -----cJ//-J> <o,oo( Chromium chloroform -----~Yt r_-]E_ <o,oo I __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene ----Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene . ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- L/-/1--11 J1/&---lindane --Date Received Reported by methoxychlor 6~4 --/fl.::rlS:I __ toxaphene Dale Exl raclcJ '/-~-97 t/:J.1-9 713.iJ Dale Rep.orted --2,4-D $~9-JYI e,Jlt 9'?1 j 8 b; __ 2,4,5-TP (Silvex) . J>is, r . 1 Date AnalyLcd v-)i/~97 tt~Zf P&_ Lab Number --DI IS 31')1 (ltcviscd 2/91).6() N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste 1':!an;gemcnt _Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O . Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ ~-'-~_,;:...._;6;:..._~.._-_y-L-------- Name of Site WARR, f!:.;J lovtVTI( ½o p/U..... Site Location __ =W"'--'-Pr'-'-R=&o..:::€=A.t"--_G_v_"'~!:t...__ ______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) J 0:3· --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ~ '" Lead 4( 12 ttqoid (6) --__ Mercury _ Soil (3) Sludge (1) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- . ,.,, Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS ~ Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------- _L L+~c.b. . Chloride chlorobenzene -----,efj 'i -1) <o.oo/ Chromium chloroform ---- -d.} ~ S-T.£. <0,00/ Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC -__ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- i.f-//-97 Ub lindane Date Received -- Reported by methoxychlor --&Jlt /Yl.5i_>,/ __ toxaphene D;itc ExtractccJ 3/;/J-97 { .. 2l-'l 7~lJ Date Reported --2,4-D /:)~9--7YI (?;.0.4 971.36L 2,4,5-TP (Silvex) Date Analyzed ~:j§·-~7 ':/_~l)-91 Lab Number DI IS 3191 (Revised 2/91)/!JJ{) w -- ,,.L. ucpartmcnt of Environment, I lcalth, & Natural Resources Solid Waste Managem,ent Division ' ' ~AM.l:'L~ ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ --=e>_·-=--2..=o=---=-e,_·-z ........... S:._ ______ _ Name of Site WARR, e,;J lov1t1T'( 0wo p/U..... Site Location __ -"'Wc,,c_:,A-..:..,Rl!,J&t>.,;€::::cA,/~_C:,_.,;_/1/=-ty'--'-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste _:::::_ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ✓Groundwater (1) SB Barium , --_ Solid (5) Cadmium --Chromium _ Surface water (2)= 'Q2 Uqtrtli"C6) --Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ...... Parameter Re-;ults(mg/1) )Parameter Results (mg/I) (mg/kg) Organic Compound11 Results(mg/1) _P&T:GC/MS __,., Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- _\L.. L-1-~c.b.. Chloride chlorobenzene -----rij</-1> <o,oo t Chromium chloroform ----_ ~1½'£-EP <0,001 Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin --lindane Date Received j/..-//--?7 ~ Reported by -- --methoxychlor t l>\67S:! __ toxaphene D:.i le Exlraclcc.J -17 1/-;J.J-'tJ/!JI,{) Dale Reported --2,4-D ~<Jm1 ~ ::?J71~b'i 2,4,5-TP (Silvex) m:,-,s. t 1/,Z-f-97 Lab Number Dale AnalyLcd y-j,J./-97 l)J IS 31')1 (Revised 2/91 )~ (b/) -- N.C. Department of Environment, I lcallh, & Natural Resources Solid Waste Management Division ' . ' SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number 6'a.o () '"7 '-' --------~-------- Name of Site LJ ARR, ~Al CovtVT'( ¼o EfU..... Site Location __ _..W-"---'-fr_./<.=&-'-'~'-'--A.l~_G_v_/1/_ty~-------- Collected By -----------ID# Date Collected Ti.me ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ✓Groundwater (1) Barium PS ~ --_ Solid (5) . Cadmium --Chromium --__ Surface water (2) ,:::? t:fitiier-(6) Lead --__ Mercury _ Soil (3) Sludge (1) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- _lL._ L-1:e:rb. Chloride chlorobenzene ---- --:21l/-,l) <o, oo J Chromium chloroform ---- --d 1 'l-t s=-rP <o, 00 1 __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichl orobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroe thane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- 4-1/-?___J U/&--Reported by lindane Date Received --__ methoxychlor &vYt /J.t JI J,/ __ toxaphene Date Extractcc..l J./-/t,-97 t./-J/-1/76'J Date Reported 2,4-D · 8/J/JIYI -- fr) s-, r: / /!,IJlt ~;-/1.Jbu __ 2,4,5-TP (Sil vex) Da te Analyzed '-/-Lf-"17 <.f~l/-97 Lab Number DI IS Jl'Jl (l~cviscd 2/91),Bdi J!fD -- 1'-.L. Uepa rtment of Environment, I lcalth, & Natural Resources Solid Waste Management Division ' . ' ~AMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Rllleigh, North Carolina 27611 Site Number Field Sample Number l>~oo-r.., -------~------------------------- Name of Site LJ A-RR, e:_ ;J Cov/1/T'( Gwo F[U.... Site Location __ ..,_W"'-'-f+'-'8..:..1.&....:~c.c...AJ.-"---_G_v_ll/~!:f___._ ______ _ Collected By -----------ID# D ate Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) --_ Solid (5) J b 1-\ ~ Cadmium --Chromium ::.!: 6:-t . . l:(o) --__ Surface water (2) Lead --4 --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter (y.esults(mg/y} Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- 1-Lie:rb . Chloride chlorobenzene -----.:?1 <L -.J) <o,Oof Chromium chloroform -~¼S-TP ----<o,oo / Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol --vinyl chloride ------endrin --lindane '-J;il-11 J{k) --Date Received R eported by methoxychlor --8!,J /JI S1 s-. I __ toxa ph ene D:.ilc Exlraclc.:J 3/-/v,-97 1/ -)...</-17 gi) Dale Reported --2,4-D 81fJ1 ;:T/J1 f;,i.)7}-9tt138~ __ 2,4,5-TP (Silvex) /11s~/ y-LJ -97 Lab Number Dale AnalyLcd '/:-·-°t] -- l)J IS 3191 (ltcviscd 2/91)/5Jl. 80 N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste l\1an~gement pivision SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ O_'t._t>_p""-'-,._.a..__ ______ _ Name of Site W ft RR, ~Al Cov/1/T/( Lt.to E[U.... Site Location ___ /,J~1+.....,R'-'-'&~~~A-/~_C:,_e,1_,v_ry~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ✓Groundwater (1) Barium R 1t trt --3 --Solid (5) Cadmium --Chromium --__ Surface water (2) r".qz" Ilq-iiii (6) Lead --__ Mercury _ Soil (3) _ Sludge (1) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter ~sults(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- __L L-1:e:rb . Chloride chlorobenzene -----,;'?, <./ -J) <o,oo/ Chromium chloroform -~~S-if ----<o .oo 1 __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----·······-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ · 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vin yl chloride ------endrin -- !J-1I-97 Ulv lindane --Date Received Reported by __ methoxychlor SVIJ hJS7)-. / __ toxaphene Dale Exlractc.:t.i '-/-//r-97 >/-). 'f-771:J,() Dale Reported 2;4-D .... " --134.:nn 13µ 4-~"'7l.3~u __ 2,4,5-TP (S ilvex) Da le AnalyLcd ';-!J,f:-47 (f--z..,z-517 Lab Number DI IS 3191 (Revised 2/91)/?,il) tW -- I· ,,.L. u cpartmcnt ol tnV1ronment, I lcalth, & Natural Resources Solid Waste Managcl)1cnt Division ~AMl'L~ ANALYSIS .KEQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ___ O'--'-'\~o'---"t,'--~1-0\__._ _______ _ Name of Site WARR e,IJ loV/1/T'( ½D EJU...... Site Location __ ""LJ=.;.:_1+.:...1.8='--'-'~=IJ.=-_C,_..,1_,v'-ry'-'-------- Collected By -----------ID# Dale Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) ALB --_ Solid (5) • ) Cadmium --Chromium ...z_iTZJT I €ts) --__ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- -· ....., Parameter Results(mg0,, Parameter Results (mg/I) (mg/kg) Organic Compound!i Results(mg/1) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- ~ Lie-rb . Chloride chlorobenzene ----i -J) <o,oo / Chromium chloroform ----= -~i s--r/J <CJ,OO I Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- --2,4,6-trichlorophenol -- ----~ vinyl chloride endrin -- Date Received ef-//-</7 U/~eported by lindane -- --methoxychlor /3M 111 s-, S: I __ toxaphene D:ilc Exlractcr.J i/--1t -9 7 '-/-). '/-97;1JDalc Reported _-_-2,4-D ., --~ $ "1 ;::Tfr) !:JJ* ~:t,1.3~~ __ 2,4 ,5-TP (Silvex) Dale Analyzed tJ_Qf.J1 --z.2,-!fj Lab Number --l)J IS 31')1 (ltcviscd 2/91 )0<l) /3 i-.L. Uepartmcnt of Environment, l lcalth, & Natural Resources Solid Waste Managem~nt Division ' . . .SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ __:::t>~l..~o~o~g'""'c)'---------- Name of Site WARR, tDJ ~V/1/T'(' 4wo p/U..... Site Location __ ..J.<W=-..e.l'r.:..,8~&--'-'~=A.J..=;___G_v_,v"-ry:.......L.. ______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: · Hazardous Waste Solid Waste __.:::::__ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) --Solid (5) DR )l 1 Cadmium --Chromium :~?±hmii~ --__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/!D Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----_L Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·-----~ Lif!:.t::.b.. Chloride chlorobenzene -:{t-:JJ <0,001 ----Chromium chloroform ----_ ~<./.s--rP <o,ool Copper o-cresol --l --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --_. _ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----·······-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ---- ----= vinyl chloride endrin -- L/----fl-Y7 Jlt-Reported by lindane Date Received --methoxychlor --.MIJ /1JSir, I f __ toxaph ene D:.itc Extractcc.l ~?i,4 7 '-/-,LV-9JloDatc Reported --2,4-D 40-m gJ,A 2,4,5-TP (Silvex) D l 111SiS: f ate Ana yLcd '-/-Z~17 4 ~vZ-~ab Number ~713~2 --DI IS 3191 (Revised 2/91)/3<{) 15~ ,,.L. Ucpartmcnt of Environment, I lcalth, & Natural Resources Solid Waste Managcmi:nt Division . . . ~AMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Site Number ----------------Field Sample Number ____ O-'')...=-=•~<>~l~I ________ _ Name of Site LJ ARR, ~Al Covil/Tl( ½o EfU..... Site Location __ .... W=--:..1t.:...18.;:.,.&.,..,~~A..1-"--_C:,_t,1_111'-ry'-'-______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) R~AP., 3 --Solid (5) . Cadmium --C Chromium ~~ --__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- -...... Parameter Results (mg/11 ~Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- __lL._ L-1:.~t::.b. Chloride chlorobenzene -------3t y-:JJ <o,oo/ Chromium chloroform -----~4~r--T/J <0,001 __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury . 1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ------Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ---- ••••u-•• Zinc hexachlorobutadiene ' ----Parametu Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene -· __ trichloroethylene --Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --2,4,6-trichlorophenol ------vinyl chloride ------endrin -- lf-//-f7 VVReported by lindane --Date Received methoxychlor --f3N/l /1/n )-. / vP __ toxaphene Date Extractc.:c.J '-/-1/r97 '-/-~ Y~9J&9 Dale Reported --2,4-D ,Bi)/ :57Y\ ~,0/r :}""/1393 __ 2,4,5-TP (Silvex) Dale Analyzed {')!]f)n '-f-l..,'Z-'flab Number --DI IS 3191 (llcviscd 2/91)/3£) pJJL r,.L.:. Ucpartmcnt of Environment, I lcalth, & Natural Resources Solid Waste Managem,ent Division ' . ' :SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number __ __:O_~.::.._o-=.t,...,..:,:&::......::2--;__,--------- Name of Site WARR, e-. N t°ovtVT/( Lrno p[U-Site Location __ """W=-..:..f'r.:....,R.:.,./(.>....:~=JJ=---G_J_,v=-ry'-'-------- Collected By ID# Date Collected Time --------------------------------- Agency: Hazardous Waste Solid Waste ~Superfund Sample Type Environmental Concentrate Comments ✓Groundwater (1) __ Solid (5) A:s H '3 __ Surface water (2) \-< Lrquid (6r ____________ _ Soil (3) _ Other (4) _ Sludge (7) __________ _ _ Other (8) __________ _ Organic Chemistry Parameter _P&T:GC/MS ✓ Acid:B/N Ext. MTBE -·- __IL_ _1-l-e:rb . -i];<f -JJ -r2t ½f -TI? Results(mg/1) <o,oo J < D -Doi Radiochemistry ······-···--------------1 Parametu Results (PCi/1) __ Gross Alpha -------Gross Beta Microbiology Parameter Results (Col/lOOml) Inorganic Chemistry Parameter Arsenic Barium --Cadmium --Chloride Chromium --Copper --Fluoride Iron --Lead Results (mg/I) (mg/kg) __ Manganese __ Mercury Nitrate Selenium --Silver -- Sulfates Zinc --_pH __ Conductivity ______ _ TDS --TOC Date Received JJ-//-17 ,t/'{,..--Reported by ________ _ bN/1 h!S)S"./ /J D:.ile ExlractccJ '-/-/1j7 '-/,,2'/-9J..iJ/J Dale Reported BS..,-JYVI bJJlf -~-7-1_3_9_4_' - Dale AnalyLcd';i:1l,{h lf,·t!J-.l.!7/JIJJLab Number ________ _ DI IS 3191 (llcviscd 2/91 '/3'5:J TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead __ Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride Results (mg/I) Results (mg/I) ------,-----chlordane chlorobenzene --chloroform o-cresol --m-cresol __ p-cresol cresol __ 1,4-dichlorobenzene ______ _ __ 1,2-dichloroethane __ 1,1-dichloroethylene ______ _ __ 2,4-dinitrotoluene __ heptachlor -- hexachlorobenzene hexachlorobutadiene , hexachloroethane --methyl ethyl ketone ______ _ nitrobenzene ----pentachlorophenol __ pyridine __ tetrachloroethylene trichloroethylene _ 2,4,5-trichlorophenol ______ _ 2,4,6-triehlorophenol = vinyl chloride ------- endrin --lindane ----methoxychlor __ toxaphene _2,4-D 2,4,5-TP (Silvex) f\.L . Ucpartmcnt of Environment, I lea Ith, & Natural Resources Solid Waste Management Division . ' ' SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ 0__,2.~o-C).._..gL,3.,,._ _______ _ Name of Site WARR, ~Al lov!VT'{ 1=M,o p[U.... Site Location __ ..... W=...,1+...:...fl=f(,~e::=A./=-_G_v_/1/~rf...__ ______ _ Collected By ID# Date Collected Time --------------------------------- Agency: Hazardous Waste Solid Waste ~Superfund Sample Type Environmental Concentrate Comments ✓Groundwater (1) __ Solid (5) __ Surface water (2) _2-J i~ ___________ _ _ Soil (3) _ Other (4) Sludge (7) __________ _ _ Other (8) __________ _ Organic Chemistry Inorganic Chemistry Parameter _P&T:GC/MS Results(mg/1) ...... 1 Parameter Results (mg/I) (mg/kg) ____ __.,..-Arsenic ✓ Acid:B /N Ext. MTBE -·- _IL_ lkrb. --z~-]) _ S -Tf' <.0,00/ <O, DO / Radiochemistry Barium --Cadmium --Chloride Chromium --Copper --Fluoride Iron --Lead __ Manganese __ Mercury Nitrate Selenium --Silver -- Sulfates ······-··---------------1 Zinc --Parameter Results (PCi/1) _pH __ G ross Alpha -------__ Conductivity ______ _ Gross Beta TDS --TOC Microbiology Parameter Results (Col/lOOml) Date Received t/-f/-Cf 7 lvt-- 8IJ/t rJt SI s. 1 0;.itc Extract eu '/--/71 1 </-.l-J/-97 i'P l3W,.::r1"" J?,JJ/f Dale A nalyzed ~~f~ V-Vl-'fl- DI IS 3191 (Revised 2/91)8& ~ Reported by --------- Date Reported _______ _ Lab Number --------- TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead --__ Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-cresol -- --p-cresol cresol --1,4-dichlorobenzene --1,2-dichloroethane -- --1,1-dichloroethylene 2,4-dinitrotoluene -- --heptachlor hexachlorobenzene --hexachlorobutadiene --hexachloroethane -- Results (mg/I) Results (mg/1) --methyl ethyl ketone _____ _ nitrobenzene -- --pentachlorophenol __ pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------= vinyl chloride endrin --lindane -- --methoxychlor __ toxaphene __ 2,4-D , ·-· 2,4,5-TP (S ilvex) 1,.<... u cpanmcnt ot environment, I lea Ith, & Na tural Resources Solid Waste Managemi:nt Division ' ' ' ~AMYL.I:!.: ANALYSIS KE(..!UEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ___ t>:......=1-::0~<>~B~l-f...._· · _______ _ Name of Site WA-RR, t::. Al lov111rv Lrno F[U.... Site Location. __ ..J.<W=-..!.fr..:.J/<.~&:ic~:::::.:Al..:::......._G_c,1_11/.:......:_ty.,__ ______ _ Collected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds ------ Sample 1)'pe Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) A J '3· --Solid (5) Cadmium --Chromium --£Pi 3q1iliP(b) __ Surface water (2) Lead -- --Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter U esults(mg/lL Parameter Results (mg/I) (mg/kg) Organic Compoundi. Results (mg/I) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- _\L_ 1./:erb . Chloride chlorobenzene ---- --;;J,' '-./ -J) <-o, oo l Chromium chloroform :1/'4 ,-r/J ---- --<0,001 __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexach lorobenzene ----····~·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene trichloroethylene --Parameter Results (Col/lOOml) --_ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vin yl chloride endrin -- Date Received fl.-/{ -97 U/&- lindane -- Report ed by --methoxychlor IJM4 /11 S't 'l-, I __ toxaphene DJle Exlraclc<l 1//7-97 t/--Zf-97~ Dale Reported .. 2,4-D 64..'ffil f;).)/t-9~,1a9u --_ 2,4,5-TP (Silvex) ~¾' 4-l,,'Z,,,qb Lab Number Dale AnalyLcd ~-97 --DI IS 3191 (ltcviscd 2/91)/31) fj i'-.L. Ucpartmcnt of Environment, I lcalth, & Natural Resources Solid Waste iY/an~gement pivision SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ ()_i.~o_d_C~~~-------- Name of Site WARR, ~Al t"ov/1/T/( L+-,,n pfU..... Site Location __ ...,.W=--..:.Pr-'-'f.=f,.J.-'t!::=AA~_G_v_,v'-ty-'---'-_______ _ Collected By -----------ID# Date CoUected Time ---------------------- Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) Rf>r: --_ Solid (5) -~ Cadmium --Chromium ~( 6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter ~esults(mg/i Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- 1--1-&-rb . Chloride chlorobenzene ---- --i ~-1) <0,00 ( Chromium chloroform ---- --1(s-r/J <o,oo / Copper o-cresol --Fluoride --m-cresol ' ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene ----Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····••--·• Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2;4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- t/--1/-</7 Jl/<e-Reported by lindane --Date Received __ methoxychlor !3/Jft />JS-1S: I __ toxaphene D:.ilc Ex lraclcJ j;J,1 JJ1 c/-zf,,Jz8iJ Date Reported 2,4-D -. --. µ-1>1 /3.JJ/t-__ 2,4,5-TP (Silvex) tn :51S: I 97139,.£ Dale Analyzed 'l-3og/ lf,b?j/J Lab Number --DI IS 3191 (Rcviscd2/91) i) i'-.L. Ucpartmcnt of Environment, I kalth, & Natural Resources Solid Waste Man?gement ,Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ ~_'2._~_0_~S~'-~-------- Name of Site WARR, ~Al loV/1/T'{ ~Q E[U.... Site Location __ ..,,.L,J=--=-f'r.:...t.8-=-i.&.,_,t!:c.;..A-'=--_G_v_/1/'-ty'---'-______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~ Superfu.nd TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) --_._ Solid (5) -RA:.>R l Cadmium -- ~ Chromium --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (T) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter ~suits~ Parameter Results (mg/I) (mg/kg) Organic Compoundi. Results(mg/1) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- ~ lie:rb. Chloride chlorobenzene -----;),/-/-]) <o,oo I Chromium chloroform _ dJ':f;S--T/J ----<o,ool __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ' ----Parametu Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol 2,4,6-trichlorophenol ------vinyl chloride ------endrin -- Date Received ~ //-97 -U/4---Reported by lindane -- --methoxychlor 13t1 IJis,s. 1 __ toxaphene D:.i le Extracted iJ. 717 t/~.2-J1~9J.8L) Dale Reported --2,4-D C-1'/V\ t9;Jft 9"71, ,-· __ 2,4,5-TP (Silvex) Date Analyzed ~!J{47 tf-2-,3-5/J Lab Number J!:;tj --DI IS 3191 (Revised 2/91)'8(9 /!3)] r,.L. ucpartmcnt of Environment, 1 lcallh, & Natural Resources Solid Waste Management Division . . . :,AMP L~ ANALYSIS REQUEST Slate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ __,0::_~.,;_•___,0::_.,;_i_,;___ ______ _ Name of Site WARR t:::,;J t°ovtVTI.( ½o p[U..... Site Location __ _...W~Pr..:...B~&l}..;~~A-'=-_G_v_/1/=-rf'----'-------- Collected By -----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) JOW --_ Solid (5) ) Cadmium --Chromium ~(o} --__ Surface water (2) Lead --__ Mercury _-Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter [R;sults(mg/~ Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_L Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------- _L_ L-1.~c_b. . Chloride chlorobenzene -,;J,,<j_-j) <o,oo I ----Chromium chloroform -~~~<::-r/J ---- <f) I [K) I Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- If-if.-97 /.{/(r lindane Date Received --Reported by methoxychlor --/3/JA ..,.5',S. I __ toxaphene Date Exlractc.:J t/-17.fi7 t/-.Zf-JJ.i4)Datc Reported --2;4-D 81°'™ fJJ.Jlt ~71.J~!-, 2,4,5-TP (Silvex) Dale A nalyzc.:d f115.!5r;_~7 '1_ /2,3.-97 Lab Number I) I IS J l ')J ( l~cviscd ~/91) .,_g,!) /23i9 -- 1,.L. u epartment or Environment, I lcalth, & Natural Resources Solid Waste Managem,ent Division :SAMl'L~ ANALYSIS REQUEST State Laborotory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number _____ ()=:--::2..=-.0==-=0"--""S:....13..__ _____ _ Name of Site LJ ARR, ~Al t"ov/1/T'(' 4-,,0 p[Lt-Site Location __ -"'-W=-.:...A-:..,.R:.i;/?.L..::~=AJ"---_G_e,1----'-11/--'-!:f....,__ ______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste _.::::::_superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --. Barium ✓ Ground water (1) ADJ . ~ " -- Solid (5) Cadmium --Chromium --__ Surface water (2) ~tritl (6) Lead -- --Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ~ Parameter Results(mg/11, )Parameter Results (mg/I) (mg/kg) Organic Compound!i Results(mg/1) --P&T:GC/MS Arsenic benzene ----✓ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- 1-Lkrb. Chloride chlorobenzene ---- --~~-:D <0,00/ Chromium chloroform ----<o,oo I __ Copp~r o-cresol --•. v-TP --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····~·-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ---- ----= vinyl chloride endrin -- 4--i{-{f7llJJ:> lindane Date Received --Reported by methoxychl or --/3}.Jlf 1>7SiS./ __ toxaph ene D:ile Exlraclc<l t./ ✓17 ,Cj7 t/2!-f 7/i4)Dat_e Reported --2,4-D {3}03"M ~'}4-2,4,5-TP (Silvex) Date Analyzed ~~• 1 ':f:t,,3-fJ Lab Number 9"7140u DILS 3191 (Revised 2/91r"JJ 131.9 -- i'-.L. Department of Environment, I lcallh, & Natural Resources Solid Waste l\fan~gement ,Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh·, North Carolina 27611 Site Number ----------------Field Sample Number ____ ~--•--=O;........:f"'---',L..-------- Name of Site WARR,~ Al t"ovl\f T'{ ½o F[U...... Site Location __ .1£W=-.!..1t:..LB:.i:&'--"e=:::.:.:Ai:,____C:,_v--=-ll/....:...!:f....,__ ______ _ Collected By -----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- - - Sample Type , Inorganic Compounds Results (mg/I) Environ mental Concentrate Comments Arsenic --Barium ✓ Ground water (1) 93 --_ Solid (5) C...fft Cadmium --Chromium ~ l::lquid ( 6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Q_esults(mg/li 1 Parameter Results (mg/I) (mg/kg) Organic Compound!i Results (mg/I) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachJ oride ----MTBE Cadmium chlordane -·-----~ L-1:.~~b . Chloride chlorobenzene -;;J,//-Y <o.oo / ----Chromium chloroform -e3;' <:4 ,-TP ----< 0,00 / Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichJorophenol ----= vinyl chloride endrin -- L(.--((-{7 /;(/<:...--Reported by lindane Date Received --methoxychlor 8).}lt l>i,n~ I --__ toxaphene Dale Exlraclc.:u 1r/7-91 '/-Zf-97&,P Dale Reported 2,4-D &)0JM -- !!fa* !j•71.40J.. __ 2,4,5-TP (S ilvex) ~),/ y-U;); Lab Number Dale Ana lyLcd --?0 -1] -- DI IS 3191 (llcviscd /91) ~ZS! 1,.\....... ucpunmcnl Ol .tnvuonment, 1 lcallh, & Natural Resources Solid Waste Management Division ' . ' .::,ANlt'L~ A.NALY~l~ KE(JUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number l>:LoO,() ----------------______ _.....=----------- Name of Site WARR, t::.iJ t"ov/1/TI( Lw,0 p/U.... Site Location __ ""'W~Pr.:...r.8.:..i.f..,__,t!:=~=--G_v_111'-ry'--'--------- Collected By ----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) o DA '3 --_ Solid (5) Cadmium --Chromium ~I. ·et (6) --__ Surface water (2) Lead ---sq □ --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Vesults(mg/li Parameter Results (mg/I) (mg/kg) Organic Compound!! Results(mg/1) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- 1-... .l-1:ecrb. Chloride chlorobenzene ---- --~t~f-TP <O,oo l Chromium chloroform ---- --<O,QO / Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichl orobenzene -- ----Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- 4--ll--C/7 v~ Reported by li ndane --Date Received methoxychlor --l!>/Jft f>t S7 J, / __ toxaphene o~tc Extractc.:u '-h J-3/J tf--L,f ✓'IJIJrf} Dale Reported 2,4-D .. , lHJ1.:TM --8).)/r ~t71.40~ __ 2,4,5-TP (Silvex) Dute AnulyLcd'y-:71~'.....9 7 l.f"l,,~ Lab Number --DI IS 3191 (Revised 2/91)~ I , .... 1...,. ut.:pilnmcnl O[ r..nvtronment, 1 lcallh, & Natural Resources Sulid Waste Managemi:nt Division ' ' ' .::,AN1J:'L~ ANALl:'.~l~ lU:(JUE.ST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ ---=O=---=~=-::o:......=o_,.....__._I _______ _ Name of Site WARR, e_ Al t"ov/1/ T'{ ½o pf Lt-. Site Location __ .J.<W=-..:.1t.:..i.P.=&-'-'t!::=AA~_G_v_/l/"--ty'-L... ______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) ps G: --Solid (5) i Cadmium --Chromium --...-6 f i qw1i ~) -__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter C Results(mg/1~ Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- _L_ L-1:e:rb . Chloride chl orobenzene ---- --;)_I <j_ -. 7) <_(} I 0() ( Chromium chloroform r;;;J:'j_,~Lf!. ---- ---c:o,oo f Copper o-cresol I -J --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ---- ······-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride ----endrin -- L/--( (~7 u/Cr lindane Date Received --R eported by methoxychlor 8;.Jlf /hr;~ I --__ toxaphene Dale Exlraclc.:<l t/1Jf7 i/:-30 -11 fl)Dalc Report ed 2,4-0 84J#J -- ms,S: I t3J.JA-(' 971.,lO" · 2,4,5 -TP (Silvex) Dale Analyzed y-'f ,?1 '1_-)-3-1] Lab Number DIIS 3l'JJ (Revised 2/91)_t3& /311) J -- i\.C. lJepartment of Environment, I Icallh, & Natural Resources Solid Waste fyfan~gement ,Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ O_'t...:::. -=-"-O=-'\-=-="L-=-------- Name of Site WARR, tDJ Cov/1/T'{ Lwo Flu..._ Site Location __ ..i.::W~1t:..L8~&1..!:t:::.:.:AJ"--_G_e,1---=-"'-=-rf....,__ ______ _ Collected By -----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste __:::::_ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) c_c. 3. --_ Solid (5) Cadmium --Chromium ~rl(6f: --__ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter lfusttlts(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------- _L L-1:ecrb . Chloride chlorobenzene ---- ;J_ ~-1) <!_.(),DO I Chromium chloroform ----= ~ 1£-T/J <o, 00 1 Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ---- ••••H-•• Zinc hexachl orobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ---- ----= vinyl chloride endrin -- lf--//-C/7 Jl,.t,-Reported by lindane Date Received --methoxychlor 13//A--~Jl'f", I --__ toxaphene Da le Exlraclcu ~iJ,tf7 '-1~30 -'1 7 f>IJ Dale Reported 2,4-D 8£J~l>1 --004 971il04 2,4,5-TP (S ilvex) r.,, =s-tS-. I Da le Analyzed .,:-,,017 ~,za-11 Lab Num ber DI IS Jl'Jl (Revised 2/91)/3& &Q -- I I 1,.L. ucpartmcnt ot tnvtronmcnt, I lcalth, & Natural Resources Solid Waste Management Division .:,AMYL~ ANALY.Sl.S KE(JU.EST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ _.__. _0_2._c)_·6_~~------- Name of Site WA: RR, ~Al t'ovt11 Tl{ Lr,.,0 EJLL-Site Location __ _J.<W~l+..:.,8~&ll.ct?:e:::.:AA~---=C:,--'--v-"':....:.....!'Y.,__ ______ _ Collected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ✓Groundwater (1) J Barium oK '.3 --_ Solid (5) Cadmium -- ~ ~ Chromium --__ Surface water (2) -:::: Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter 0 / ~ Results (mg/12.-Parameter Results(mg/1) (mg/kg) Organic Compoundi. Results (mg/I) _P&T:GC/MS Arsenic benzene ----___L" Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·-----_iL Lkrb. Chloride-chlorobenzene ---- --2-J tJ -J) <o,oo / Chromium chloroform ---- --~j~ r..:r-P <o,CO I __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dicliloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----·······-··-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ . Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- f_f-If -~7 file;? lindane Date Received --Reported by __ methoxychlor -6iJlf MSTS, I __ toxaphene Date Extracted ~-g,;--1 7 tf ,30-<j 7f} Date Reported --2,4-D $ '.i-' I t<-\6i t3.;JA ::t714Ul __ 2,4,5-TP (Silvex) 1'1 S-I >• I Dale Anal yLed £-S-,'i7 lj-.23;1JLab Number .:> --DI IS Jl'Jl (lleviscd 2/91)&0 "·'---· ucpunmcm 01 1:.nvironmenl, l lcalth, & Natural Resources Solid Waste Management Division . ' ' ~ANlt'L~ ANALl'.~l~ .K.1!:(JUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ 0~2.._.0_G_ct_C,+--·-·· ______ _ Name of Site WARR, t::.Al t"ov/1/T/( ½o FJU-. Site Location __ =W=-'-A-..... B~f.'""'t!:-'-A,(~_G_v_lt/_rf~------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) mm m-.. } --_ Solid (5) Cadmium --Chromium ~qzld~) --__ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Results (mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- _\L 1-1:e:rb. Chloride chlorobenzene <o,oo I ---- ~~-_l) Chromium chloroform ----=:, .s-rP <:o,oo I __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene ----Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexach lorobenzene ----···••·-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol 2,4,6-trichlorophenol ----= vinyl chloride ----endrin -- i-f,-(f-7"rttM lindane --Date Received Reported by methoxychlor oµA---r,,s,r., __ toxaphene D:.ile Exlraclc<l</-/ 7-9 7 t/--Jo-97 ff} Dale Reported 2,4-D -.. --/JiqJITI, ,o 6, _ 2,4,5-TP (Silvex) n,Si S I /31-)4 Dale AnalyLcd 5:-f-cn y-z--1-?J Lab Number ;:17 :.i,,Ob --DI IS 319 1 (Revised 2/91)/!J,5) l,3if) i,.c. Department of Environment, l lcallh, & Natural Resources Sulid Waste ~an~gemcnt .pivision SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ O_~_c>_D_-t____;:S"''--------- Name of Site W It RR, e-,;J lov111rl( ½o F[U...... Site Location __ ..w:W:s<-!.1+.:...J&c::.i/1..,_,~:::.:"-'=--C:,_e,1_,v:::.._ry'--'-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ✓ Ground water (1) B1-. Barium "3 . --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ~(6) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter 6esults(mgLi >Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----✓ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- ~ 1./:e:rb . Chloride chlorobenzene ----~' 'l.-.1) <::.o ,oo I Chromium chloroform = ~:~£-TP ----<..O , 00 / Copper o-cresol --Fluoride --m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexach lorobenzene ----········-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------T0C __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- L/-ff-{/7 tvt--lindane Date Received --Reported by methoxychlor B,vA--- /115/5../ __ toxaphene D:.ile Extraclcu t/-17--97 '/--.:ft:)-9 z~ate Reported --2,4-D i3i),-;:rM1Ul(n n-_ VJ !l11tl0p-t' 2,4,5-TP (Silvex) f'tlS-tS-, I ~ Da le Analyzed s-r:...q7 y-b)iJl Lab Number --DI IS 3191 (lteviscd 2/91).dQ i'\.L. Ucpartment of Environment, I lcalth, & Natural Resources Solid Waste Man~gem.ent pivision :SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O~~o ,, -------------------------------- Name of Site WARR, ~ ;J t"ov/1/T'( ½o FILL--. Site Location __ ..._W-"-'-f'r'--'-f<=&"-'t!::;.;c...AJ-"--_G_v_fl/'-ry_._ ______ _ Collected By -----------ID# Date Collected Time ----------------------.. Agency: Hazardous Waste Solid Waste _:::::_ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ✓Groundwater (1) 8DRJ ~ --Solid (5) Cadmium --Chromium ~(6) -- __ Surface water (2) Lead --__ Mercury _·_Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry ----Parameter Results (mg/!).., )Parameter Results (mg/I) (mg/kg) Organic Compound~ Results (mg/I) _ P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane -·----- ~ L±e:rb. Chloride chlorobenzene <.0 1-00 I ---- --2, tj__-::P Chromium chloroform ~; ':4 'S.-rf. ---- ---<.0,00 1 __ Copp~r o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- i.-f-/(-</7 ft,h lindane --Date Received Reported by methoxychlor EV,4 --/11.i'IS. / __ toxaphene D:.ile Extraclc<l 1/-/7 -9 7 Y..3o --9~ Date Reported --2,4-D 8 Jl?:7111, liJGi &o,7 _ 2,4,5-TP (Silvex) ,.,,---, t3ff:J-97 Lab Number ~7140t1 Da te A nal yzcd ,s:?P-M --1)1 IS 3191 (Revised 2/91) ~ N.C. Department of Environment, I lcalth, & Natural, Resournes Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ ....;.O_~~0-=--=0::...'l~l _______ _ Name of Site lJ A fl,R, ff: N C, vY\.q-y ~O f/Luite Location __ ...::lJ'----'/+',....:....:..:R..:....,tt'-"t;.'.~A/..:,___~=v.:...;N::.....:....t'f..__ _______ _ Collected By ID# Date Collected Time -------------------------------- Agency: Hazardous Waste Solid Waste __L_Superfund Sample Type Environmental Concentrate Comments __ Ground water (1)_:::@C Ssl1d (5) Tr'\ ss __ Surface water (2) __ Liquid (6) ___________ _ ✓Soil (3) _ Other (4) _ Sludge (7) __________ _ _ Other (8) __________ _ Organic Chemistry Inorganic Chemistry Parameter _P&T:GC/MS v Acid:B/N Ext. MTBE -- Results (mg/I) Parameter Arsenic Barium --Cadmium --Chloride ✓ De-13 <Q.IJ'()pm. ✓ Z ,'t-n ,<o,)d),/41 = Chromium -L 2.1 'ft 5'-TP '( o , JDfl-'11 _ Copper _ EHthzitl <"•L'f'f /t'\. _ Fluoride Results (mg/I) (mg/kg) _ L1NdANE <o-~~ _ Iron --2!JE--t4oxvc/t4R</. 0~& Lead Jii WH~NE <,;J.~ ff!_~ __ Manganese _(i4.~ <o.~A'\ _Mercury --2/J ~ <o# IP1J!fb1 Nitrate Jl~)Df ~~, ,~-. };;bf>,.-. Selenium r·· -,..,, ·=,-,,. : .. 1 -c,,... ~,,,a;..~..__ . Silver --Radiochemistry Sulfates ······-----------------1 Zinc --Parameter ,Results (PCi/1) __ pH __ Gross Alpha -------__ Conductivity ______ _ Gross Beta TDS --TOC Microbiology Parameter Results (Col/lO0ml) Date Received 4 ~ / {--4 7 ukReported by ________ _ /JPM -IY-9 7 "2h:t: Date E~f!tf5:J§i";f~4,l8r.f Date Reported _______ _ ~"'1-F+=s, 4-,<3-?7VP 1 Dat e AnalyzcdM:Q S:::l 5--fe·-9z/J£)_ Lab Number ':J7 40 :, DI IS 3191 (Revised 2/91) /3<J'!'f-l 1/-'f7.6~ TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium Chromium --Lead __ Mercury Selenium Silver · Organic Compounds benzene --carbon tetrachloride Results (mg/I) Results (mg/I) --------- -- -- chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol cresol __ 1,4-dichlorobenzene _____ _ __ 1,2-dichloroethane __ 1,1-dichloroethylene _____ _____ __ 2,4-dinitrotoluene __ heptachlor -- hexaehlorobenzene hexachlorobutadiene hexachloroethane --methyl ethyl ketone _____ _ · nitrobenzene ----pentachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol _____ _ __ vinyl chloride endrin --lindane ----methoxychlor __ toxaphene _ 2,4-D _ 2,4,5-TP (Silvex) \ . I N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ ___,O=::......;~.;:__o_o::........:'ie...:l..=------- Name of Site lJ A R.R. i?; N C, v '/\.(r)' Ul-No f/u-5ite Location ___ w---"A',_.;...:.R.Yt:.....:.;;;.(!:_tc/.,___~ac..v'....;N~!Y_._ _______ _ Collected By ID# Date Collected Time -------------------------------- Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments __ Groundwater (1) ~6Mif{j' L.e~s __ Surface water (2) _ Liquid (6) ~Soil (3) _ Sludge (7) _ Other (4) _ Other (8) Organic Chemistry Parameter _ P&T:GC/MS v Acid:B/N Ext. MTBE -- Results (mg/I) ; i ,~B-J) ~~',ffiffl -L 2-,~s--rP <o, JD P/JM -EAiek,u <o./o~--L.,uoius: < o,,,:,tJ'AA,.,, 1!LE¢4oxveA/4,,e_ < /,, o iPpm 3f!l'1fr,we ~'.f$ if ;;fjt&a,_:<::,/f g::{' ~/~,i.Tui:T;AJ -~,,..., ~,,. _...,.- I/ Radiochemistry ······--------------___j Parameter ,Results (PCi/1) __ Gross Alpha -------Gross Beta Microbiology Parameter Results (Col/lO0ml) Inorganic Chemistry Parameter Results (mg/I) (mg/kg) Arsenic Barium --Cadmium --Chloride Chromium ----Copper -- Fluoride Iron Lead __ Manganese __ Mercury Nitrate Selenium --Silver --Sulfates Zinc --_pH __ Conductivity ______ _ TDS --TOC Date Received 1./-//-C/7 /lh Reported by t!,µ"'lrt./-t 7 -7hBJJ. ---------- f'c 8-t PEST~ -.a.2,.-,7.YI' D:.ile Exlraclt:UfeSJ.> -:S:-t:'i?d Dale Reported _______ _ pc8Y'PEST ~-..23:::Y-T'(P Dat e Analyzed ~A-1 {2'f;-:.f{~ Lab Numbcr __ ~_,_;_1_4_1_· _l, __ _ DIIS 3191 (Revised 2/91) TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead -- --Mercury Selenium --Silver -- -- -- -- -- · Organic Compounds benzene --carbon tetrachloride Results(mg/1) Results(mg/1) --------- -- -- chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol cresol ----114-dichlorobcnzene --1,2-dichloroethane ------ __ 1,1-dichloroethylene _____ ____ __ 2,4-dinitrotoluene __ heptachlor hexachlorobenzene hexachlorobutadiene ' ---------hexachloroethane ----methyl ethyl ketone _____ _ · nitrobenzene ----pentachlorophenol __ pyridine __ tetracWoroethylene __ trichloroethylene __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol _____ _ __ vinyl chloride endrin --lindane ----methoxychlor __ toxaphene _ 2,4-D __ 2,4,5-TP (Silvex) N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Managem~nt Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ ....;.~_"-'_·_t>_. O___,'f..._l,_· _______ _ Name of site lJ A R.R.'~ N [p v Y\.ny ~ o f /LLlite Location __ ..;;_w____;_/+'._;R..;.:i't~~--''1/'--_c--=-.;...,..;;_N..::....,._'fV.....___ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium 3 6 S6iid (SJ f-lE.~J -- __ Ground water (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --__ Mercury ~Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) · Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------v Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Pc.B ✓ .::: o. Io /Jf'flt. Chloride chlorobenzene ------✓ 2,'1-.D <O,LOIJIJM Chromium chloroform ----v ~:its-rP <o,,o~p~ __ Copper o-cresol --_ E/\ldeitl <o,/Oj>pat Fluoride m-cresol ----L /;,1.clA#E= ~o.~d~ ·iron __ p-cresol --Lead cresol '1li.r:t/toxyc4fo,e :< J. ~ ----_:JJ:l)(A.ollEde <,a. ff?""-__ Manganese __ 114-dichlorobcnzene ~ ~o.lfi<'opf)I"'\ __ Mercury --1,2-dichloroethane -J:'~t!,M,,tg <D, le71finL Nitrate __ 1,1-dichloroethylene -,,0/e,,,e.fe'></t/e<r."!_~ .. __ Selenium 2,4-dinitrotoluene -::DJ'&/'T>/:!_i .I ""'<:I,,~---, , Silver __ heptachlor Radiochemistry Sulfates hexachlorobenzene ----······--Zinc hexachlorobutadiene ' ----Parameter ,Results (PCi/1) ._pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --_. _ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Received lf ,.-/ (-rz ~ Reported by lindane --__ methoxychlor /JCB. /31..JAj.;.t 7 ¾ .{) __ toxaphene ¥ /JE-~ -'-31/P 2,4-D · Dale Exlraclcu P1SJS-rS--f7 Dale Reported --~fA~Ep ~714 1 J.. __ 2,4,5-TP (Silvex) Dale AnalyLcd ~·:,, ,~;!J ,r,, Lab Number --DI I.S 3191 (llcviscd 2/91) ' ·- N.C. Department of Environment, I lea Ith, & Natural R~sourccs Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number _____ . _0_~-=--0'---=l,)'-•"f ........ '-/.__ ____ _ Name of Site lJ A B-.R '?; N C, v Y\.( tY ~O fJt,.LBite Location ___ lJ_tt-,_R--'-'tl'-'-"-~-N~-~"-v--'n.J--"--'-'fY........_ _______ _ Collected By ID# Date Collected Time --------------------------------- Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments __ Ground water (1) :2!'.C Suiid (5) __ Surface water (2) Liquid (6) ___________ _ ~Soil (3) _ Sludge (7) __________ _ _ Other (4) Other (8) Organic Chemistry Parameter P&T:GC/MS v Acid:B/N Ext. MTBE ✓ Pc.B ..L _?-,'i-;b -L~I./.S-TP __ ENd/4.,u Results(mg/1) Radiochemistry Inorganic Chemistry Parameter -- Arsenic Barium Cadmium Chloride Chromium --Copper Fluoride Iron Lead Results (mg/I) (mg/kg) __ Manganese __ Mercury Nitrate Selenium Silver Sulfates Zinc Parameter ,Results (PCi/1) . _ pH __ Gross Alpha -------Gross Beta Microbiology Parameter Results (Col/lO0ml) Conductivity TDS TOC Date Received L-/= /I-97 ~ Reported by t:J)JJ?fl{ -, 7 -t; 7 8 ---------~ fCAY'PUf" 9-..U• 7JIP D:.ile Exlraclt:<l /'157f S -S'--.f2tB;,J2, Dale Reported _______ _ -Pe.t:31-~ q-..:e-5'7VP '::1?11::11 ~~. D:.ite A nalyzt:d57.l, I 5'-~-'17.i.i> Lab Number ~ - TCLP Compounds Inorganic Compounds Arsenic Barium Cadmium Chromium Lead __ Mercury Selenium Silver · Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol Results (mg/I) Results (mg/I) ------ __ 114-dichlorobcnzene _____ _ 1,2-dichloroethane __ 1,1-dichloroethylene ------2,4-dinitrotoluene __ heptachlor hexach lorobenzene hexachlorobutadiene ' hexachloroethane methyl ethyl ketone nitrobenzene __ pentachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene ------ ------ __ 2,4,5-trichlorophenol _____ _ __ 2,4,6-trichlorophenol _____ _ __ vinyl chloride endrin lindane __ methoxychlor __ toxaphene 2,4-D __ 2,4,5-TP (S ilvex) DI IS 3191 (Revised 2/~'f--.J.'t ?~e:Q_ ----------.__ _______________ --A STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C . 27611 ORGANIC CHEMICAi ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD # COMPOUND TYPE UNITS N-nitrosodimethvlamine }f'J/~3D bis(2-chloroethyl)ether 2-chloroohenol ohenol 1 3-dichlorobenzene 1 4-dichlorobenzene 1,2-dichlorobenzene bis(2-chloroisooroovl)ether hexachloroethane N-nitroso-di-n-oroovlamine nitrobenzene isoohorone 2-nitroohenol 2,4-dimethvlohenol bis(2-chloroethoxy)methane 2 4-dichloroohenol 1 2 4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro~resol hexachlorocvclooentadiene 2 4 6-trichloraphenol 2-chloronaohthalene acenaohthvlene dimethyl ohthalate 2 6-dinitrotoluene acenaohthene 2 4-dinitroohenol 2 4-dinitrotoluene 4-n itroohenol fluorene 4-chloroohenvlohenvlether diethvl ohthalate 4 6-dinitro-o-cresol diohenvlamine azobenzene 4-bramohenvlohenvlether hexachlorobenzene oentachloroohenol ohenanthrene anthracene dibutvl ohthalate fl uoranthene J -Estimated value. ,r S0/11:,So /0/330 'So/11,,,_,;o /0/~30 l J, Sol ~l,,50 /tJ/'330 I ~I SOIIIDSO /t)/.~.':/0 \j,. m"bL llz.O/SOIL. '//~?R:I q•Ji.-:U./l./- dOZ)1/ ~Oc> 7,.,1 ( J ) l{ua/ J.}nm,r.1 ,...ua/1 ~ 1 IA-I.A.- -/ ,, ,, K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. t:/7/-?/1S- ,iil._OZJ7~ c / > ..._ua/1 }~ I.A / \. C/71.~R~ ~07<.f ( I > ,...ua/1)~ 1.A- / ' , 97[?¥7 ;;l®7S ( I > .....-UQ/ 1.,.. L "·-' \A / ,, u· -Material was analyzed for but not detected. The nurber NA -Not analyzed. is the Hinirrun Detection Limit. mTJL ----1/ -Tentative identification. ~I -On NROC List of Priority Pollutants. CJ) C/"7/.~x'x' .;{cf?)7~ ua/1 J.-..n - I.A- ,. ', , STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C . 27611 ORGANIC OlEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO l/7/3fl_ ~ l/7/.~f'C/ CJ7I·«:S C-/ 7 J:?%1~ EXTRACT ABLES FIELD# d(fllt I dtJlJ?,)._ ?J7J7q ;;:2.d?> 7 c/ (X)MPOONO TYPE c / l c I l c / ) c / ) UNITS ...-uo/1 ~1 .,..u<J/1 ~ .,..uq/1 ~ ua/1 ~ ovrene J0/.33/J I A..__ v{ _ vl.-1/l - benzidine so/1160 butyl benzvl ohthalate 10/.:1~0 benz(a)anthracene chrvsene J, 3 3--dichlorobenzidine SOI ~1:,5() / bis(2~thvlhexvl)ohthalate /()/.330 ,, di-n-octvl phthalate IO/.J3o /OK.. benzo(b)fluoranthene so/11,no IA- benzo(k)fluoranthene benzo(a)pvrene i ndeno ( l , 2, 3--cd) pyrene dibenzo(a.h)anthracene / I / f benzo(q,h, i)oervlene \I' "l/ \/ ,, ,, aniline i..!"O/J"·"ll lA-LA -IA -u_ benzoic acid benzvl a lcoho 1 4--ch loroani 1 i ne ~ 1/. dibenzofuran '" l.330 2--methylnaphthalene 2--methvlohenol ~ 4--methy 1 pheno 1 ..,, 2-nitroani 1 ine S-o/J~~o 3-ni troani 1 ine 4-ni troani 1 i ne / I ) , 2 4 5-trichlorophenol ~" \V \I '\ I ,!/ n7-Hl=R Cl)fr1 PfJUA.J1}5 --,............. ~ CNllOLN!:l Tlf Tl +/-r-J r -J (-) (-J r7E"JIT1f'nr'E l'DENTI FNl/tnoJJ ----- mn1- J -Estimated value . H"O/ SfJlt- K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. .cr7/~2'7 ~t:07-r c /) ~an' .. J/1. ,. \., /OK.: (,A_ J " I tA.,_ I \V .,-.. 1'+1 '---"' U -Material was analyzed for but not detected. The nc..rrt>er NA -Not analyzed . is the HinilTUTl Detection Limit. f>")l)L.. -1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants . 97/~~ ~tf?r7h c / l ..... IJQ/1 ~ IA \. / I DK IOI/ 1./4_ / ~/ LA- I ,1 ,-.,,. l +,J - STATE LABORATORY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C . 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD # COl1POUND TYPE UNITS N nitrosodimethvlamine /fl/ 2':fl"t bis(2-chloroethvl)ether 2-chloronhenol ohenol 1 3-di chlorobenzene l 4-dichlorobenzene 1.2-dichlorobenzene bis(2-chloroisooroovl)ether hexachloroethane N-nitroso-di-n-oronvlamine nitrobenzene isoohorone 2-nitrnnhenol 2.4-dimethvlohenol bis(2-chloroethoxv)methane 2.4-dichloroohenol 1.2.4-trichlorobenzene naohthalene hexachlorobutadiene 4--chloro-m-cresol hexachlorocvclooentadiene 2.4.6-trichloroohenol 2-chloronaohthalene acenaohthvlene dimethvl ohthalate 2.6-dinitrotoluene acenaohthene 'I/ 2.4-dinitroohenol SO/JtoSo 2.4-dinitrotoluene iol~~o 4-nitroohenol so/21.,;o fluorene /0/~30 4-chlornnhenvlohenvlether I diethvl ohthalate J, 4 6-dinitro----0--cresol SOI ~(,,50 diohenvlamine /()/330 azobenzene I 4-branoohenvlohenvlether l hexachlorobenzene '4/ oentachloroohenol .SOIIIASO ohenanthrene /IJ/~~/) anthracene dibutvl ohthalate fl uoranthene ', I,' J -Estimated value. m"bL Hz.0/SO/l- C/7/.~,Y'-I '-17/-MO ~t:m77 J.JZ>7V c I l . c I l - /ua/f ' " lJQ/1 ~ IA--VL- I I 'I ,, K -Actual value is known to be less than value given . L -Actual value is known to be greater than value given . ~7/~/ lf7 / ~'f,,.,J. "2rJZJ l '-1 ~(JZ)"x0 , c I > ( J ) r ua/1 ~ .. lJQ/1 )-"- lA-\A.- I I \, I 'I '1 7/~'f':7., ~v-, ( J ) lJQ/ 1 " LA-- r '\, U -Material was analyzed for but not detected. The nurber NA -Not analyzed. is the Hininun Detection Limit. m])L ----1/ -Tentative identification. ~I -On NRDC List of Priority Pollutants. lf7/ :.{Gf <J, ·7&;~.2. < I l ua/1 ~ \.A-- / \V STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST ., RALEIGH, N.C. 27611 ORGANIC D-lEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO '171-3YCf q7J890 C/7/...:f'i I q7J :..&;).. EXTRACT ABLES FIELD # ,?-olr77 ,.., --.9 ,r-yL)/ ,., -q L:?7.10 I ~Rt) 00f1POONO TYPE ( J_ ) ( J > c / > UNITS r uo/1 ~i uo/1 ~ uq/1 ~ µq/1 ~1 ovrene J0/33tl I A-lA ~ t-A--LA- benzidine .'\/J/J/60 butyl benzvl ohthalate /0/JJ~O benz(a)anthracene l chrvsene J, / / 3 3-dichlorobenzidine SO) 'th.'i'O \ "I bis(2~thvlhexvl)ohthalate /()/ i.30 /0/C. I '],::_ di-n-octyl phthalate /()/.J3o LA---IA- benzo(b)fluoranthene SO/Jln'O benzo(k)fluoranthene benzo(a)pyrene i ndeno ( 1 2 3-cd) pyrene dibenzo(a h)anthracene J I I I benzo(q h i)oervlene \., ' I ,, \I ',, aniline sa/J1,_,rc; IA --Lt<--(A_ CA- benzoic acid benzvl alcohol 4-chloroaniline "" ,I' dibenzofuran /() l.330 2--methvlnaohthalene 2-methvlphenol j 4-methylphenol ,J, 2-ni troani 1i ne s-o/Jt.'i'"o 3-nitroani 1 ine 4-nitroani line I I I I 2.4 5-trichlorophenol \JI \' \. ,, '\ t'JT/1.Ft'_ {10 /hl'tJU A}.])$ : ---..,.....,,. ~ 11A P" ,v Ae / Jrth ·-f' I -[-} (-} r+1 f -J-) (7EJJT'1Tl f £ 11)e).m FJ!AflfllJ ---- - m1H- J -Estimated value. H"O/ Sr;/1- K -Actual value is known to be less than value given. C/7./_ -(<[~ ~!?/ ( I ) ,.. uq/1 ' l/\-- I \ IA.- J \ I -r-1 ...._.,,.. L -Actual value is known to be greater than value given. U -Katerial was analyzed for but not detected. The nurber is the Minirn.m Detection Limit . NA -Not analyzed. l/ -Tentative identification. ~I -On NROC List of Priority Pollutants. '77/~qy, ~-'Z7X"~ , uo/~ LA-- r \I /OK v\,_ r I ... V { I \/ -----( -' ~ BASE/NEUTRAL AND ACID EXTRACT ABLES COl1POUND N nitrosodimethvlamine bi s(2-ch loroethvl )ether 2-chloroohenol ohenol l 3-dichlorobenzene l 4-dichlorobenzene 1 2-dichlorobenzene bis(2-chloroir-----·. ])ether hexachloroethane N-nitroso-di-n-oronvlamine nitrobenzene isnnhorone 2-nitrnnhenol 2 4-dimethvlohenol bis(2-chloroethoxv)methane 2 4-dichloroohenol l 2 4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro-m--cresol hexachlorocvcl=ntadiene 2 4 6-trichloroohenol 2-chloronaphthalene acenaohthvlene dimethvl ohthalate 2 6-dinitrotoluene acen;mhthene 2 4-dinitrnnhenol 2 4-dinitrotoluene 4-nitrnnhenol fluorene 4-chloroohenvlohenvlether diethvl ohthalate 4.6-dinitro-o-cresol diohenvlamine azobenzene 4-brmnnhenvlohenvlether hexachlorobenzene r>Pntachlornnhenol ohenanthrene anthracene dibutvl ohthalate fl uoranthene J -Estimated value. STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC Q-IE11ICAL ANALYSIS LAB NO C,7/~C/~ C/7 1--:q//J C/7 I --f <f' 7 c.r7J-i'/Y FIELD # ~9..-'5 ·z..:rn ~(f )A'/?.J .¥') bdlJY/A TYPE ( 1 ) ( /-) - UNITS I uQ/1 " ,..uQ/]~ r l,IQ/]~I llQ/l ~ /f'J/~31:J -,,( -1/l ----i-A-IA ,, so.1/r,,so I0/330 so/J,,..,;o /0/~30 I ,J, 5o/Jlb,o /()/330 I j 'V so/11oso J/J/~.':JO I I / / ~i,, ,v \I \ { \:/ K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. 7":J/1~'7 -uRJY7 c / l r µg/l ~ l.A - r \/ U -Material was analyzed for but not detected. The nurber NA -Not analyzed. is the 11inirrun Detection Limit. m])L ----l/ -Tentative identification. -~/ -On NRDC List of Priority Pollutants. 'f7/0/)/} '7A'J7J )f >? OONO pyrene benzidine butyl benzvl phthalate benz(a}anthracene chrvsene 3.3--<lichlorobenzidine bis(2-ethvlhexvl)phthalate di-n~tyl phthalate benzo(b)fluoranthene benzo(k)fluoranthene benzo(a)ovrene i ndeno ( I • 2. 3-cd) pyrene dibenzo(a.h)anthracene benzo(Q. h. i )oervlene aniline benzoic acid benzvl alcohol 4--ch l oroan i l i ne dibenzofuran 2--01ethvlnaohthalene 2--fflethylphenol 4--methvlohenol 2-ni troani line 3-nitroaniline 4-ni troani line 2,4,5-trichlorophenol OTltEI!-c?om ftJl/A,WS. ; Cllff.DLAe'TlffVI (JEPTlmVI! INVi7Flfll-1il\JJ J STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST ., RALEIGH, N.C. 27611 ORGANIC _OiEMICAL ANALYSIS LAB NO G/"7/39i '17J3q/L1 97/~C/7 q7J3l/P FIELD# ~.9~ ;um~~ 2,,t}?;,P~ ~J?h TYPE ( /) UNITS (uo/1 ~ .uQ/l 1--... r u<1/ l ~~ i,iq/l~ I0/.13ll .LIL-IA -lA-1/L. so/JhSO /0/J!JJO J, SOI ih.'i'() lie/ 3.30 /O/.J3o so/11:no I / / / \" \ 'I \' '\ I '.s-0/11,~_,rn LA-LA-\A -lA- ~ I/ /0 /3:JIJ ~ \V Soflt."'"o / / I / ~/ ..._ I \ \. I 'I ....-::,... .....-.=... ---'-I-/ -) (-J (+J ( -J ~ ----- mn1- J -Estimated value. H'"O/ $()/l- K -Actual value is known to be less than value gi ven. '?71-NC/ ~J.>7 er is the Minirrun Detection Limit . NA -Not analyzed. 1/ -Tentative identification. ~/ -On NROC Li st of Prior ity Pollutants. 19'7/</tR; "7t:7ZJ.P2 ( 1 ) "uo/l'~ LA / ,, lA_ / '\ I ~ I -) '---"' STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD # COMPOUND TYPE UNITS N nitrosodimethvlamine /Q/~3D bis(2-chloroethvl)ether 2-chloroohenol ohenol l 3-dichlorobenzene l 4-dichlorobenzene l 2-dichlorobenzene bis(2-chloroi=roovl)ether hexachloroethane N-nitroso-di-n--oroovlamine nitrobenzene i <;00horone 2-nitroohenol 2.4-dimethvlohenol bis(2-chloroethoxvlmethane 2.4-dichloroohenol 1.2.4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro-m-cresol hexachlorocvclooentadiene 2. 4.6-trich lornnheno l 2-chloronaohthalene acenaohthvlene dimethvl ohthalate 2.6-dinitrotoluene acenaohthene 'V 2.4-dinitrnnhenol S0/JhS0 2.4-dinitrotoluene /()/330 4-nitrnnhenol .SO/tlil.,;O fluorene 10/~30 4-chloroohenvlohenvlether I diethvl ohthalate J, 4.6-dinitro--0-eresol So/JIL,.'iO diohenvlamine /()/330 azobenzene I 4--brmnnhenvlohenvlether hexachlorobenzene 'V nPntachlornnhenol so/105"0 ohenanthrene JtJ/~.":/0 anthracene dibutvl ohthalate fl uoranthene "" J -Estimated value. m1)L /-12..0/SOIJ_. C/7/<f.n/ Q71</Od- 7,,dl)f/Lj "U}?)llO ( J ) c I > "ua/ l 1 •• ua/l tmtlm. -II\__ -,.A_ / / -../ \V K -Actual value is known to be less than value given . L -Actual value is known to be greater than value given. C/711../0 ~ '17/YOY- ?A!Jc)q I LLIZM~ ( J ) ( J ) v uall' .. ,.,.uq/1 ~ -,.A l/L.. / .,. \V '/. ll/lYb.\ .:/4:::l?)Cj ~ 1 J ) r ua/1 -~ ii\._ / \ I u· -Material was analyzed for but not detected. The nurber NA -Not analyzed. is the Mininun Detection Limit. mIJL .... -- l/ -Tentative identification. - ~I -On NROC List of Priority Pollutants . Q7/Y/Jffi "/-t:0W r I l . UQ/]~ IA - / ' V STATE LABORATOOY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C . 27611 ORGANIC D-lEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO C/71¥01 1/7/Vo;z '-1'71</o -Z, C/~</o</ f/'7/</o'5 EXTRACT ABLES FIELD# ;q;o,V'1' ~9 0 ~,7-// -z-.t'JtJ9 .,}-·~~ TYPE r I l _[ I l r I > r / > ( /) COMPOOND UNITS r uqil ~ """ua/1 ~ r uq/1 ~( "uq/1 ~< ....-110/ 1 -;., ovrene /()/33/J IA_ t.A. IA IA - benzidine _'\11/1/tJSO butyl benzvl ohthalate JOl.330 benz(a)anthracene chrvsene "' 3 3-dichlorobenzidine S()///J() bis(2-ethvlhexvl)ohthalate lo/.330 di-n-octyl phthalate IO/.J3o benzo(b)fluoranthene so/11-no benzo(k)fluoranthene benzo(a)pyrene i ndeno ( 1 2 3-cd) pyrene dibenzo(a h)anthracene f I / / benzo(q h i)pervlene \ .I ,, \ I ~ I \ I aniline s-a/Jh_'io LA--\A-IA-IA- benzoic acid benzvl alcohol 4-chloroani line "-, dibenzofuran /() /33() 2--01ethvlnaohthalene I 2--01ethylpheool j 4-fflethvloheool 'ii-' 2-nitroani 1 ine S-o/;~~o 3-nitroani 1 ine 4-ni troani line I I I I 2 4 5-trichloroohenol ,JI' \ I \ I ,, '\. I u ,riCT\ (lntnltJIIIAJJJ<; ,: ~ /'?-.. ~ ~ fl Af' /!.tJLI+{!, I MT ~r I +-!-{-) l -J :-m,/V'F {+ J {-) (~n llc 1./)l!M"J FJt!/tntL' -.....__. ,. mnL- J -Estimated value. HzO/ S0/1.- K -Actual value is known to be less than value given. L -Actual value is known to be ·greater than value given. U -Po\aterial was analyzed for but not detected. The nurber is the Minirru-n Detection Limit . NA -Not analyzed. 1/ -Tentative identification. ~I -On NRDC List of Priority Pollutants . V\ / \' LA- I ,, ~ { -) - lq7/Yl?h ~v 1 I l ...-i,iq/l ~a LA.__ / \' ~ I '\ I -., ' (-J - STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO EXTRACT ABLES FIELD# COl1POUNO TYPE UNITS N nitrosodimethvlamine JrJ/ ./3n bis(2-chloroethvl)ether 2-chloroohenol phenol l 3-dichlorobenzene 1.4-dichlorobenzene l. 2-di ch l orobenzene bis (2-ch loroi sooroovl )ether hexachloroethane N-nitroso-di-n-ornnvlamine nitrobenzene isoohorone 2-nitrnnhenol 2.4-dimethvlohenol bis(2-chloroethoxv)methane 2 4-dichloroohenol 1 2 4-trichlorobenzene n,mhtha 1 ene hexachlorobutadiene 4-chloro-m-cresol hexachlorocvclnnPntadiene 2 4 6-trichloroohenol 2-chloronaohthalene acenaohthvlene dimethvl ohthalate 2 6-dinitrotoluene acenaohthene 'V 2 4-dinitrnnhenol SO/JtoSO 2 4-dinitrotoluene ioI~~o 4-nitrnnhenol 'SO/Jt.,'iO fluorene 10/~30 4-chloroohenvlohenvlether I diethyl ohthalate J, 4.6-dinitro-o-cresol 501 ~/,,"0 diDhenvlamine /0/330 azobenzene I 4-braroohenvlohenvlether hexachlorobenzene ~,, oentachloroohenol solltnS"O ohenanthrene Jl'J/.~':fo anthracene dibutvl ohthalate fl uoranthene 'I" J -Estimated value. m1)L H-z..0/SO/I- l-17/ 'IV-I q7/YOY ~.,,_;:;< -ZOZ)q&; ( ) < I ) v uq/1 ~ _,u0/l ~ -I.IL-·1A~ I I '\. I \ K -Actual value is known to be less than value given . L -Actual value is known to be greater than value given. C/7/'-/0q '-f7i¥I/J ;kf"ZJ(J./ ;?~'1'~1.. ( ~) (-1} ,m:z;(' ua/k a ~wkq., l/C-V\.....- I I \ I 'I/ C/7/<-// I ~</,~ ( =3 ) ~ua/ka, lA - i / ,1 U -Haterial was analyzed for but not detected. The nuroer NA -Not analyzed . is the Hinirrun Detection Limit. rnTJL -----l/ -Tentative identification. ~I -On NRDC List of Priority Pollutants. Cf7/<.//,;J... ~<µ./ (~ ~uQ/kal v ..._ - ·- I \. I STATE LABORATORY OF PUBLlC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST ., RALEIGH , N.C. 27611 ORGANIC D-lEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO '17/C/'01 <./ //1/0'>( f/71</D<-t C-/7/Y/O 1V7 /'fl I EXTRACT ABLES FIELD# U'7)(l \ ~C/IA ~t.J,/ ~'•/.:?_ COf1POONO TYPE ( I ) < I ) ( ::; ) (=?) UNITS Cua/i. 1 \Jq/1 ltm:tm_ -~C a/ka ,~a/kQ' ovrene Jo/~3o I.IL-LA---A-~ benzidine _'\/1 /11!60 butyl benzvl ohthalate /0/.330 benz(a)anthracene l chrysene J, I 3 3-dichlorobenzidine '/~'{() SOI \' bis(2~thvlhexvl)ohthalate /()/.330 J Ole._ di-n-octyl phthalate /0/.J~o 1.A- benzo(b)fluoranthene so/11:no benzo(k)fluoranthene benzo(a)pyrene i ndeno ( l 2 3-cd) ovrene dibenzo(a h)anthracene I I I I benzo(q h i)pervlene \ .I \ \ \I ,I ,·,. aniline S'CJ/Jt,,1,0 V--t ,,.__ lA---lA..- benzoic acid benzvl alcohol 4-ch 1 oroan i 1 i ne "" ,I' di benzofuran ttJ l.330 2-methylnaphthalene 2-methvlohenol 4---0-ethvlohenol ,J, 2-nitroaniline S'o/Jt.~o 3-nitroaniline I 4-nitroani 1 ine I I I I 2 4 5-trichlorophenol ',j I' \. I \ I \I \I , (JTJIE1!.. (! (!)/YJ tht I iJ..j) __'.) :· /?,. ~ ~ ~ (1/~ [JebLA/177'TrV] , +I-TRA(!_fl +-) {-J (-) r-J fn::NTA-7711£ tlJ0JJJP1(1AlJo/J --.._,___ ..... _ - fYl1)L J -Estimated value. HzO/ $()/£- K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given . U -Material was analyzed for but not detected. The nurber is the Mini11U11 Detection Limit . NA -Not analyzed. l/ -Tentative identi fication. ~/ -On NROC Li st of Priority Pollutants. "2,,tJO½~ ( ~) ~ q I k q ~ ~ / \I L,.... _ I I \I ~ { -J - "7/~ ~ ·-"7...,m."11 w -v.....- ( -c,) ,-rrrd, a/kq} l/4..= r \ I l ,.._ ~ I I '\ I ......=---..... i( -) -- •, .. .. '., ~·I, •• ~• , I ,r 'I .: ... ' i' ·.~ ,I l• .. ,, ' . .. ' . ·~ J.J 1.. -· .-i •. • ~ •• ,. '1.·:11 • ./j ·~, ":, (,;. '. ~. ': , I l,;ii, • t_• ~ .. . , .. ,..1 ' . • 1. 1!!' .. ., . > . '. , . . ' I ... . ~. <..._ '1, I .,.-.1.~t. •·, .l~ ~, .. N.C. Department of Environment, I lea Ith, ~ Natural, Resources Solid Waste Management Divisipn SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ---------------Field Sample Number ___ --=0:.-..;1..;:;...0.;;;;._;:0'-'i ........ S:'--------- Name of Site WA RR.EN 0, vfll Tl{ LA:No E tl-L Site Location __ ..:;.W~A--'-'({._..R.=i!:=AJ,..___~..;...;__u..;_:AJ,_N:........i.... ______ _ Collected By ID# Date Collected Time -------------------------------- Agency: Hazardous Waste Solid Waste ✓superfund Sample Type Environmental Concentrate Comments ✓ Ground water (1) __ Solid (5) \ _ Surface water (2) /Liquid (6) ___________ _ _ Soil (3) ) _ Sludge (7) __________ _ _ Other (4) _ Other (8) Organic Chemistry Inorganic Chemistry Parameter Results (mg/I) (mg/kg) Zinc Parameter Results (PCi/1) _ pH __ Gross Alpha -------Conductivity -------Gross Beta TDS TOC Microbiology Parameter Results (Col/lOOml) TCLP Compounds Inorganic Compounds Arsenic Barium Cadmium Chromium Lead __ Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride Results(mg/1) Results (mg/I) chlordane ------ chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1, 4-dichlorobenzene 1,2-dichloroethane ------ __ 1,1-dichloroethylene _____ _ 2, 4-dinitrotol uene __ heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane ------ __ methyl ethyl ketone _____ _ nitrobenzene pentachlorophenol = pyridine __ tetrachloroethylene __ trichloroethylene 2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ --vinyl chloride endrin Date Received J./-//-q7 VP . /J lindane ~ · ,t1...l r--~ethoxychlor --~ ......... ---------toxaphene 6".--0 7 -9 7 2,4-D _ 2,4,5-TP (Silvex) D:itc Extractc<l 'f-/'l-97Jlta!G Date R Dale Analyzed __!i:i7--g77/p Lab Number ___ ~...,· .._.7._· .... l "-'1/4:.._.1 1,_·-..,,,u"---_ DI IS 3191 (Revised 2/91) # '/711/13-q 7 I V3~ ... ~• --y~• ••"""'"• Vl L.,IIV11Ul11l1Cnl1 l lcallh, & Natural Resources Solid Waste Management Division ' State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ -....:O~~~-.....:l>c....-:¥c....=,;__ ______ _ Name of Site LJA RR Ef\J Lb cJrJ Tl{ Lw op LI-L Site Location __ ...::LJ~A....:...i..:({""'R.._.t:5=AJ""---__ L<9_v--',v-=--=--'N__.__ ______ _ Collected By ----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) ,B l --_ Solid (5) Cadmium --Chromium --__ Surface water (2) /Liquid (6) Lead --__ Mercury __ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results ( mg/I) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc..B <o. O()Olfl.-1'1\. Chloride chlorobenzene --✓ P1;;n t Chromium chloroform = Stf',e.,i/ <o.oouk(;~ ----__ Copper o-cresol --Fluoride m-cresol _ 4¥ck,Ne-~o. 0 44. "' ----~ <; o~ ot? I bo..m. Iron p-cresol ----~~£ "<' 0 . t)/1 J !,,,, ..... Lead cresol --__ eA: 31e <:O .ooo.Y,,..,,.~ __ Manganese 1,4-dichlorobenzene ---~,,..,d/4..e "<"O ,OOP/.:.,~ __ Mercury 1,2-dichloroethane -- _ i~L.JJP/N-< t7. 4 0~~ Nitrate __ 1,1-dichloroethylene rl¥f;,1d~lt/E <::o.ooo~ Selenium 2,4-dinitrotoluene --Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol -------__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- L/-Jl-171/P lindane Date Received --Reported by __ methoxychlor __ toxaphene D:.i le Extraclc<l ~-/1/-9 7-,ifWG Date Reported ----2,4-D Dal e Analyzed ~-/'7-?'TYP ~7141 ~ 2,4,5-TP (Silvex) Lab Number --DI IS 3191 (Revised 2/91) l lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sam pie Number ___ ---..::t,::.._)..::....::...6-=="-"-=--..,..:__------- Name of Site We RR E/IJ 0:, Ufl) TY Lwo E (.U-Site Location __ ..::W=...:A~Rc<..,R.._,,e;:::e;AJ:>,L_ _ _::;L<9..::.......u...:.A.f.::e....!...'?Y..:L.-______ _ Collected By ----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) Solid (5) AW I Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc.g <e,. 0001/f'M Chloride chlorobenzene ----✓ Pe:n. Chromium chloroform ----_ ENt/Aw <o.ooo/ naJl'I.. __ Copper o-cresol -- --L-,NdAlle. <o.tJoo!::. LJ/JM. Fluoride m-cresol ----_7>1e-t/J,2xyc/i!,,,~< o. oo I f0M Iron __ p-cresol --_ JO X4f_t/Otl€ < 0, 0 0 ::i flfnt Lead cresol ----_ C/2laMA#E<.O ,oco~111 __ Manganese --1,4-dichlorobenzene _ 111(t1eA~A.. --co.ooo;;,; __ Mercury --1,2-dichloroethane -.~ELiW.1N <o.ooo~ Nitrate 1, l-dichloroethylene ----JkpfA7,/,,e !foJKf/c-<0.oco ffM. Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····•---·• Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane ---·-· __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenoi -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ------vinyl chloride --endrin --lindane Date Received ~1_1-qz--,;p --Reported by __ methoxychlor D:itc Extracted £/-/4'-97"1//JlvG Dale Reported --toxaphene --2,4-D ~ _ 2,4,5-TP (Silvex) D:i lc AnalyLcd L/-f2-(} z00 Lab Number ~-21.~i.~ DI IS 3191 (Revised 2/91) -- I"·'--· .1.,..1\ .. pUJ llllCfll Ul cnvtronment, I lea Ith, & Natural Resources Solid Waste Management Division . . State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number _____ o ....... _~_o_e>_'(....:....,ole..,._------- N am e of Site LJA RR E;r,J ~ t.JrJ TV Lw op c,l-L Site Location __ ....:.LJ:..;:_;A~~""R,,>..;i!:=AJ..___~:....::....-c./..:..:A.f=-.:...N.i_ ______ _ Collected By ----------ID# ____ Date Collected __________ Ti.me _____ _ Agency: Hazardous Waste Solid Waste ✓ S u per fund TCLP Compounds ---- Sample Type Inorganic Compounds Result.s (mg/I) Environmental Concentrate Comments Arsenic --Barium J D --✓ Ground water (1) _ Solid (5) I Cadmium --Chromium -- /Liquid (6) __ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------<o.aotJ/ £M>m. ✓ peg Chloride chlorobenzene n ----✓ Pen. Chromium chloroform ---- --ENtl/!.i;./ <O I t:U)O I __ Copper o-cresol --_ kLH dM/e <o ,ooo.:i.... .Fluoride m-cresol ---- ~L!,<:O ,OQ/ Iron __ p-cresol -- £ <o. 00..2.. Lead cresol ----~-<: O. CJO <P~ __ Manganese --1,4-dichlorobenzene -Ued..t1c.A/tJ1<... <::. o . o o o I __ Mercury 1,2-dichloroethane ---, , -~fu ,.--~OXJQ€ <O • C,eJ~/ Nitrate 1,1-dichloroethylene ----I 7>;ka--'<iN <o. ooo/ Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hex.achlorobenzene ----····••--·• Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hex.achloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --.. __ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Dale Received 'f://---9 2 YP --Reported by methoxychlor --__ toxap hene D:ite Exlraclc<l ~/J/-97Vt'liJGDale Reported 2,4-D . .. . .. -- L/-17-771/P ~71.~'.lt.t _ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --l)IIS 3191 (Revised 2/91) I lca lth, & Natural Resources Solid Waste Management Division U.n..J.>J.J. JLJJ.:., ./'U'lft.L.1.:)1.:) ~\l_U£..:).l State Laboratory of Public Health P.O. Bo x 28047, 306 N. Wilmington Street Raleigh, North Caroline 27611 Site Number ----------------Field Sample Number ____ _..;:_0_2....:c-o---=b_t{....,__,,__ _____ _ Name of Site WA RR e;,v Lb cJf\J Tl/ LA:N op Ll-L Site Location __ ...::W=-=A_,_,_,T<..""'8,...,f!::.N:..>,<__...:c~...:c-u-.:A..f-"-..!..N..::L-______ _ Coll ected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) BB --_ Solid (5) \ Cadmium --Chromium -- __ Surface water (2) /Liquid (6) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) --P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc...B < 0 . C)()O / ./f!.nl Chloride chlorobenzene ------✓ Pe;n , Chromium chloroform ----_ &N@i,/ <O,cJOO /~ __ Copper o-cresol --_ J.,',/dAN~ -<o.ooc~ Fluoride m-cresol -- ~,e < ,o. 0 0 , ~ Iron __ p-cresol _7ox1-f21-1G#e <.t:J.00 ,;~ ... -Lead cresol --(fj./" {j/fj/../E "'". o oo'd /'h;ti __ Manganese 1,4-dichlorobenzene --= "H~;;t;~A:--<o .0001 ¼n1 __ Mercury 1,2-dichloroethane ~c4/d/fl_E,d;JpX1;/e<1J, ~ 00, ~n\ --Nitrate 1, 1-dichloroethylene --II _ I>irf!!l;liv <o ,o o o~ .,, Selenium 2,4-dinitrotoluene Ju ,,/,,,, . ·e ./IOA I?< rt v, ---- Radioc{emistry I' • Silver heptachlor ---- Sulfates hexachlorobenzene ----····•-----·• Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivi ty --methyl ethyl ketone G ross Beta TDS nitrobenzene ------TOC __ pentachiorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received "l-/1 -97·-Vp --Reported by __ methoxychlor __ toxaphene Dale Exlraclc<l '1-/S--97Vl}WG Dale Reported 2,4.,D . -- Dale A nalyzed L/-/7-~ Lab Number ~~j_i.'tfi __ 2,4;5-TP (S ilvex) --DI IS 3191 (llcviscd 2/91) •.. ....,. --y~a .,.,._..,~ V l L...JIVl!Ulllllt:ll l1 I Icalth, & Natu ral Resources Solid Waste Management Division State uboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ ~/)'-"'2,....,0"'--=t>--==.r.=---'I> ______ _ Name of Site WA: RR E)J Lb Utv T<{ LA:N op c.l.-L Site Location __ ....:W=-A'-'-'-B-:....8.-"'e;.=1v..___~.:....::....-v....:.cA..f,,_,_'N.:x._ ______ _ Collected By ----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓superfund Sample Type Environmental Concentrate Comments / Ground water (1) _ Solid (5) \ __ Surface water (2) /Liquid (6) ___________ _ Soil (3) _ Sludge (7) __________ _ _ Other (4) _ Other (8) ___________ _ Organic Chemistry Parameter Results(mg/1) P&T:GC/MS Acid:B/N Ext. MTBE ~ pc..B <o.o oo'ffet\ __i_ Pen. Mft,,<dwe < 0 .000,;z.,pm. t .Nd~';/ < 0 ; ODO~ -L/m. "<::O,poe,,:2 a10{ ,r ~~~~~ < '2• a t21f112n1 -"'-9e::.LL~c=--$ 0 . '"' """' Inorganic Chemistry Parameter Arsenic Barium Cadmium Chloride Chromium __ Copper Fluoride Iron Lead Results (mg/I) (mg/kg) __ Manganese __ Mercury ....... -==.:..=:,:::...::..,~'"'""--Nitrate Selenium Silver Sulfates Zinc Parameter Results (PCi/1) _ pH __ Gross Alpha G ross Beta ------- __ Conductivity ______ _ TDS TOC Microbiology Parameter Results (Col/l00ml) Date Received L/-//-97,te Report ed by _______ _ D:ile Exlraclc<l L/-IS-9zVe wa Dale Reported _______ _ Dal e Analyzed t/-/7-9?'1/,,0 Lab Number ___ -;J-=--' _·t_i_,_~_J.._O_·_ DI IS 3191 (Revised 2/91) TCLP Compounds Inorganic Com pounds Arsenic Barium Cadmium Chromium Lead __ Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane __ 1,1-dichloroethylene 2,4-dinitrotoluene heptachlor hexachlorobenzene hexachlorobutadiene hexachloroelhane Results (mg/I) Results(mg/1) ------ ------ ------ ------ methyl ethyl ketone nitrobenzene ------ pentachlorophenol pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophenol _____ _ 2,4,6-trichlorophenol --vinyl chloride ------ endrin lindane melhoxychlo r __ toxa phene 2,4°D 2,4,5-TP (Silvex) 1 lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number _____ o_,_;;;___cC>____;O_.$"-'--'I'-------- Name of Site WA RR EN 0:, vrv TV Lwo E u .. .L Site Location ___ LJ_A~'f?..~/?.~t!:~AJ--~--c/-A.I~?"/~------- Collected By ----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium JDH --✓ Ground water (1) _ Solid (5) 1 Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc.B < o.ooo/Pj,?m Chloride chlorobenzene ---- _i__ P~n . r Chromium chloroform _ E.lld~,tl ---- <0.000~ __ Copper o-cresol -L 11i.lc/AN€ --<o. ooo -naN. Fluoride m-cresol ----__211cfAoxvr.A/,-u-, -<.O . 00 J .dl:nt Iron __ p-cresol __Jl;y ,4/J)/@,/'5 -< C'. t,'7.;z:flP.nL Lead cresol --_{M/pAdAIVE <o-ooo.:Zn'>'1! __ Manganese --1,4-dichlorobenzene ____Jj_f{!t;AeAh& <:o, ooo/!:li,Af --Mercury --1,2-dichloroethane ~t::1 • oo.u I~ Nitrate __ 1,1-dichloroethylene --1) p.dOdf~ Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----·····--·-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichJoroethylene Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane 4 -1I-q7J/I) --Date Received Reported by methoxychlor -- t/-lS-f/7Vf!P.JG Date Reported __ toxaphene Dat e Extractc<l 2,4-0 _ ..... .. . ... , .... ._, .. ':.J . -- :.171.1-,ti.~ __ 2,4,5-TP (Silvex) Dale A nalyzed 'f-/3-97-VP Lab Number --DI IS 3191 (Revised 2/91) ---~r ---···-·•• ~•--•••11.v11•••---••~, I lcallh, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street RBleigh, North Carolina 27611 Site Number ----------------Field Sample Number _____ C'.>_)._o____;;_o...::S'::......o,l,. ______ _ Name of Site WAR.REN 0>UrJT</ LA:NOfl.1.-L Site Location __ ..=LJ...::.....:.A...!-!..::"f{.uB....,,t!:=1,1..,,.___....:.~..::...._c..1...:Al.,,_,_'ry.::,._ ______ _ Collected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- Rem Barium --✓ Ground water (1) _ Solid (5) ' Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------< l).Ol)IJ Lf!!.r>t ✓ pc..B Chloride chlorobenzene ----✓ Pen. Chromium chloroform ---- --e.rtdJ? . ./t-1 <o. ooo I {f'/11 __ Copper o-cresol L./;l@tle -- --<::o , oooLM-. Fluoride m-cresol ----711etk,xyeAht1< ,, Iron __ p-cresol <o,, "t7 &-92m. . --_p .>Ulf»'EHE. Lead cresol -<.,t;,,'70. /!ftrl\, ----~/MNc < 0 • CJtJ0:1..~ __ Manganese --1,4-dichlorobenzene _:Ji~olA(?#~ <P . o~tf I P'JN __ Mercury --1,2-dichloroethane ~kAZ f::ox,i/e<o . Ot'O/~ Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene J) I aJJR.J I/ < 0 , fl) ()0 / ---·-Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----···••-•--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --.. __ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- Date Received l./--/f-9?VP lindane --Reported by --methoxychlor Dale Extrac lc<l L/-/s-97-v'P.WBDalc Reported __ toxaphene 2,4-0 .... --. --.--.. ----J _ 2,4,5-TP (Silvex) Date AnalyLcd '-/-/S-97 1/P Lab Number tr7/4l t~~·z u DI IS 3191 (ll evised 2/91) -- .. -· --y-• ••••'-"' V l L.,J1YlJ.Utllllc;llL1 I lea Ith, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 2&047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Site Number ----------------Field Sample Number ____ -=Oc....'--=--•-t>_S"_,I~------- Name of Site WARR~/\J LbvfllTI./ LA:rJopc,U-Site Location __ --=LJ:...=:.....:A....:...i..:1{""'8,._,,€.=AJJL-_..c..~~u....:.A..1.:::.....:...'N..::L-______ _ Collected By -----------ID# ____ Date Collected __________ Time ______ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ALB --✓ Ground water (1) _ Solid (5) I Cadmium --Chromium --/Liquid (6) __ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (1) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc..B <q;, tJ oo L.fl!1tl Chloride chlorobenzene ----✓ Pen. Chromium chloroform ----£/'-.1d1t.1N -< ~, (JO;, I li)!2d1. __ Copper o-cresol = LhldANt: ---<o . t1 oo.:i M1>1 Fluoride m-cresol --~ <0,0~1i;: Iron p-cresol --Lead cresol ~ <o ,oo ~ --<o.t>oo;;i_,-.n,w __ Manganese --1,4-dichlorobenzene ~ <::: o. o oolt,~,, •. __ Mercury --1,2-dichloroethane ~Ae/2b.e Ei2f-p,,,4,:< O . 00 o"I :n,,,,., Nitrate 1, 1-dichloroethylene .... Selenium --'J)/£L:J>R;W <:t,. OOo/pph\. 2,4-dinitrotoluene --Silver heptachlor ----Radiochemistry Sulfates hexach lorobenzene ----····--·· Zinc hexachlorobutadiene , ----Parameter Results (PCi/1) --pH hexachloroelhane --__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- 'f-ll-?7JIP lindane --Date Received R eported by methoxychlor -- f:IS-97"/lf,:WGDale Reported __ toxaphene Dale Extracl c<l 2,4-D . ··-. ------J _ 2,4,5-TP (S ilvex) Dale A nalyzed lf-/;?-Jt/7 7/ P Lab Number ~7:i,.JZJ.. --DI IS 3191 (IZcvised 2/91) I , ......... L-1'-jJUJ \IIIClll UL cnYironment, l lcallh, & Natural Resources Solid Waste Management Division . . State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Field Sample Number _____ O_~_O_O_S-=:---.'-f+--------Site Number ----------------., Name of Site lJA RR erv ~ Ur,J Tl/ LA:rJ Q EL 1-L Site Location __ ...,;;W..;:.....;A--'-'-'B,"--'R.'--"t!:=-AJ..,,.._ __ ~_e,1-',t,/-=--=-fy ...... · _· ------- Collected By ----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) _ Solid (5) Of!,K, ' Cadmium --Chromium --__ Surface water (2) /Liquid (6) Lead --__ Mercury Soil (3) Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) --P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc..B <:o.ooo~ Chloride chlorobenzene ----_L Pf;H, Chromium chloroform _ ENd1vil <a. oooJq""' ----__ Copper o-cresol --_ /..11w:/AA1E. <:o. ooo-3/)e'/)\ Fluoride m-cresol --- ?ifEt/2ox,J11A/pi5!.. <o. o a ~m. Iron p-cresol ---------7J,XAt> JJENIE <o. o o A Lead cresol _J!,J/,..!.d,IJ. .'E!' ~c, .oa-.... -------__ Manganese 1,4-dichlorobenzene --_1/e m'Ae.A4 n c::: t:,. o d" I f:v..-' __ Mercury 1,2-dichloroethane "J/.1j,,=:"-L{;,,RE;:,ox✓~<O , OOo~ --Nitrate __ 1,1-dichloroethylene :P!€t-PP.,;~ < o . ooot;fo/11.. Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received '-1--LL-q_ 71/P Reported by --__ methoxychlor ',f./,S-97J/tulbDate Reported __ toxaphene Date Extraclc<l 2,4-D --- I-IT-97-YP ~7i.~2 A: _ 2,4,5-TP (Silvex) Dal e Analyzed Lab Number --DI IS 3191 (Revised 2/91 ) I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ t:>_L_~_o"'"'S';;..._r _______ _ Name of Site WARR.EN LbU/1/T'{ LwofLU-Site Location __ -=W-=-'A-'-'-'B,""'R.'--"e;=N"""---...;_L8-'--c.1-'A..1.:....:...'N..:L-______ _ Collected By ID# Date Collected Time --------------------------------- Agency: Hazardous Waste Solid Waste ✓superfund Sample Type Environmental Concentrate Comments / Ground water (1) __ Solid (5) BPAB I _ Surface water (2) /Liquid (6) ___________ _ Soil (3) _ Other (4) Sludge (7) __________ _ _ Other (8) ___________ _ Organic Chemistry Inorganic Chemistry Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) _ P&T:GC/MS ______ __ Arsenic __ Acid:B/N Ext. ______ __ Barium __ MTBE ______ __ Cadmium ✓ pc..g <o.ooolffh\ _ Chloride ✓ Pen , ______ __ Chromium __ L/JV t/,4t(t; -<:: o . 0 002.J Fluoride -G.!d,1?/N <o.apo/e __ Copper ~t/20.xvcAh,-?_ < o . oo/J'(?'.l = Iron 7ox,Z,Hd6 <:::.t:J. 00#14 , Lead _&4/(d4#€ -<::"O ,Ouo.? ,.,.,.,.. Manganese _ tl_e. o6u:A/4& < o . oo o I;,;,,. i.:_,_ Mercury Jk/f.t'ld6,;z_!j:!'?20✓./~o . Ot,o~f;,i--~ Nitra~e J)1EI.JJ/Z11v1 -<.o, ooo!f?p,i,<, __ Selenmm Silver --Radiochemistry Sulfates Zinc --Parameter Results (PCi/1) _pH __ Gross Alpha -------__ Conductivity ______ _ Gross Beta TDS --TOC Microbiology Parameter Results (Col/l00ml) Date Received 'f--/ /-171/.P Reported by ______ _ D:.itc Exlraclcu L/-/5-"?'7-V/J Dale Reported ______ _ Dale Analyzed Lf--/3'-971/t!_ Lab Number ___ ~_,._/_J._~_z_.' u_·· _ DI IS 3191 (Revised 2/91) TCLP Compounds Inorganic Com pounds Arsenic --Barium --Cadmium --Chromium --Lead __ Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride Results (mg/I) Results(mg/1) --------- -- -- chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol cresol ----1,4-dichlorobenzene ______ _ __ 1,2-dichloroethane __ 1,1-dichloroethylene --2,4-dinitrotoluene __ heptachlor hexachlorobenzene -- ------- hexachlorobutadiene , ---------hex a ch lo roe thane ----methyl ethyl ketone nitrobenzene ---------__ pentachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophenol ______ _ 2,4,6-trichlorophenol = vinyl chloride ------- endrin --lindane ----methoxychlor __ toxaphene _ 2,4-D _ 2,4,5-TP (Silvex) • .. ..,_ . ._.. '-y ... • ••"'-"' Vl L,IIV11Ullll1CflL1 l lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Rale_igh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ ___::_O_:t._c>_o-..::~_,'-=------- Name of Site WA RR E:!\A 0> cJ"' Tl{ Lw o E u..L Site Location. __ ..::LJ~A....!..L0{{"-'8,...,,l:5::::.;AJc,,,__-=.~-=--u--'A.f.:::.....:...N..:i.._ ______ _ Collected By ----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Com pounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --/ Ground water (1) A:tSH _ Solid (5) ' Cadmium --Chromium --/Liquid (6) __ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ---- ✓ pc..B <o,ooo/~ Chloride chlorobenzene ------✓ Pe;;n ! Chromium chloroform -~~IN ----<t:J ,t:Joo/ ~ __ Copper o-cresol --J./llt.r,1/✓€ <:o. ooo3~ Fluoride m-cresol -------1J1 rl-/2 o )(.y{',f /v,g_ ~ 0. 00 J' l,~"' Iron __ p-cresol ...EX~€ -<:::' o, oo.d ~.,.,,.. --Lead cresol ----___{Jef /,udftle -<: 0, ooo~ __ Manganese --1,4-dichlorobenzene ~ <::0.000 1,,,.. __ Mercury --1,2-dichloroethane 'ltcdA~ r, ,de< o ,goo I Nitrate 1, 1-dichloroethylene ----7) /€L.Z} /< 1)/ <:: 0 ;<:JOOl/f'h, Selenium 2,4-dinitrotoluene ,_ __ --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --.. --pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin --lindane 'f-//-977/P --Date Received Reported by __ methoxychlor . L/-/s-9Z!IP __ toxaphene D:ile Exlraclc.:<l Dale Reported 2,4-D . . -~ -, ', . -- Dale Analyzc.:d L/-/'5?'-97 :::00Lab Number ~7 . ,-:1 2 ~ _ 2,4,5-TP (Silvex) --DI IS 3191 (Revised 2/91) -· --r ---•••-••• ---~ &.Jll•I.LV 11111'-lll1 l lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 2S047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ___ ~C>..::~.......,o"'--·-=•::.........$'~7L-______ _ Name of Site WA RR ~N Lb u"' ry LA:No p tl.-L Site Location __ -=W~A....:....i...:{{.u/?.=6:=¼.,,.__..;_~-'-v-=-A.f=-=--'ry-'L-______ _ Collected By ----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ~BAB -I --✓ Ground water (1) _ Solid (5) Cadmium --Chromium -- /Liquid (6) __ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ PLB <o .t1o o'ffn Chloride chlorobenzene ----✓ Pe,~, Chromium chloroform ---- --t=t-JR/tl -<:~. t:JtPO/, ~ __ Copper o-cresol --L-JNc/ANc <:O,LJ ~c'-1 .n~ ... Fluoride m-cresol ---- _p/~o~e/J/p£ <CJ.t:;10/) ~ Iron p-cresol ----_""T"~~;;;E ~o.oO?nn'""\ Lead cresol ----_(!/[/~tit= < o .co~~~ ( __ Manganese --1,4-dichlorobenzene ~ <<l-Ot:>D/.~ __ Mercury --1,2-dichloroethane '€ <.0 ,'100/ !fut Nitrate 1, 1-dichloroethylene -----o; E..t...VP-1>/ <(),tJOtl1pprr1 Selenium 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ---- •• .. •d-•-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone G ross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --.. __ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichl orophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Receive d L/-/1-9711? --Reported by rn ethoxychlor -- l./-/5-?7J/P __ toxa phene D:.ile Exlrac lc<l Dale Reported 2,4-D -- L/-/'?-'97 -VP Lab Number :::t"li . .J2~ _ 2,4,5-TP (Silvex) Dale A nalyLcd --DI 1.S 3191 (llcvised 2/91) ---r --·•••-••• ..,. -•••t.LVUlll'--11\.I I lea Ith, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number -Ol.• O S8 -----~-~~------------------------ Name of Site LJARRE;N 0>vt1JTV LA-NOfLl.-L Site Location __ _cW_A'-'-'-/<.=R.~e;~N~_C,, __ v""'"A.J"-'-N....__ ______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) AJ ·· ' --Solid (5) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- --· --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/I)(mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pcB <O. 0-Q /--ff'#' Chloride chiorobenzene ----~ Pe;n, Chromium chloroform _E/ld1<1N ----~o,ooo/i,am Copper o-cresol ----_L//1/i'!fAVE <;0,(}00~ !.--Fluoride m-cresol ___'?//ef-A,x .. ~-JJ __ <tJ, tJO / ~.., ----Iron __ p-cresol --____:;p x~hJ.10!€ ~0.00:5~u7M Lead cresol l'/iZ.o ,l,d,,., N"c= <: o .ooo..1.lJnt:kf... ----__ Manganese --1,4-dichlorobenzene ~ <:o .,,,,,,; 7'12' __ Mercury --1,2-dichloroethane JJE<o.ooo-:;,. ~ Nitrate __ 1,1-dichloroethylene 1,--7,) Ro/ < O, ot:70 fl,DA\ . Selenium 2,4-dinitrotoluene --Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ---- ••••M-•• Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene. Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received '-f -//-'J ?V/> --Reported by __ methoxychlor L/-/S-971/f' __ toxaphene D:.ile Exlraclctl Dale Reported 2,4-D -- ~7'.1•1~~ 2,4,5-TP (Silvex) Dale Analyzed ~Q-971/P Lab Number --DI IS 3191 (Revised 2/91) , .. __.. --y,.. ... ., ..... , V l '-JIV11UllUlCllt1 l lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Field Sample Number ____ __;C>__:::'2'-o-'-. ...;:oa.......,::$'_\.....i... _____ _ Site Number ---------------- Name of Site lJA RR EIIJ C, vr.1 Tl( LA:No p c,l-L Site Location __ ....:::LJ..::.....;.A--'--'-""f?......,R.'""6:=N..,,.__-=-~-"--u-'-AJ:::.....:....'?Y.i.._ ______ _ Collected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ----- Sample Type Inorganic Com pounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) Solid (5) R <pp --) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) --P&T:GC/MS Arsenic benzene ----_ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc..g < p , P(l_Q.¥/2-t:!:f Chloride chlorobenzene ----_.!L P~,I , Chromium chloroform ----~,_, __ -; <:~_,O t:')tJ/ --y .,.r.lC.11'11 __ Copper o-cresol b!I dAAI e --<:tJ,~dO~ Fluoride m-cresol --2!f_.ef/,p XVl'hft7~ -<: 0 , o o I ----Iron p-cresol ----~_Af'P'_../_ <::o,oc,.;l. Lead cresol ?J.J>-l-/ ~ /Ye ----<::o, ootJ.2, __ Manganese 1,4-dichlorobenzene -- ~""°o .ooo / __ Mercury --1,2-dichloroethane '€<.o ,ooo/ Nitrate 1,1-dichloroethylene -----N -C:::.O,dt?t7/ Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····•---·• Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --,. __ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane l/-//-97 -ye_ Reported by Date R eceived --__ methoxychlo r 'I-/.S--9 7Vf' --toxaphene Dale Exlraclc.:<l Dale Reported 2,4-D ---·-· -- ~ /3'-97-VP ::1~;?·i i~' 2,4,5-TP (Silvex) D;i lc A nalyLc.:d Lab Number --DI IS 3191 (llevised 2/91) I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sam pie Number ___ __;;;_C>--='"-o-----=o~ft:,._;;.0-'-.. ______ _ Name of Site WARRE)J Lbt.Jr.1P{ Lwoptl-L Site Location ___ W_A~({~R,~e:~.v ___ ~_c..1_,v~!'Y~------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste ----Solid Waste ✓superfund TCLP Compounds Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) Solid (5) RAJ fl ' Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc..g < 0,. 0001.fp'n Chloride chlorobenzene --✓ Pe:n . Chromium chloroform -----~d~iN <O. ooa!:f,~ __ Copper o-cresol ---a,iJ/4"1 -<,:,.0002. Fluoride m-cresol --2.!fi ~ ti: . <::o. ow111 ----Iron __ p-cresol --_:/p.. ENE <"Q,0 ~ Lead cresol ().,. 1~·,,, -'A #c <o. oo;f4~ ----__ Manganese 1,4-dichlorobenzene --_J/aofA('_A/p,R < 0 , Ot:1~ __ Mercury 1,2-dichloroethane -- ~/d,<1 ljox,'dE< ", oo ~ Nitrate __ 1,1-dichloroethylene ---·7>,ELJ;,,e.,//.J <:o, 000/rff'r,1. Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----·····--·· Zinc hexachlorobutadiene , ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trithlorophenol ------vinyl chloride --endrin --lindane Date R eceived I./--Ll-97VP --Reported by __ methoxychlor 'f-l~-97-vP __ toxaphene DJlc ExtraclcJ Date Report_ed 2,4-0 -· -- DJ[c Analyzed (/ /8'-97-VP Lab Number ~ .. ,:t.~ZLJ _ 2,4,5-TP (Silvex) --DI IS 3191 (Revised 2/91) I lea Ith, & Natural Resources Solid Waste Management Division ,.__,,,.....,.,_, .... ._ A..J.&:.J ~,rs..,&_j..1.....,.1.t,J 1.~v_u.1..:.tu..1.. ::.tatc uiooratory ot l'ubhc Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number _____ O___:_:~;::__o_0::....__:::1.=--JL._ _____ _ Name of Site WA: RR EN 0> vrJ Tl.{ LA:N o E <,l--L Sile Location ___ ....::W:=..:A...!...e:1?..~R...,,t:.:""AJ'-"'-_..:::~..:::.....:<,/--=AJ~N..:i.._ ______ _ Collected By ----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium J· t) tJ - ' --/ Ground water (1) _ Solid (5) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results ( mg/I) Parameter Results ( mg/I) (mg/kg) Organic Compounds Results(mg/1) _-_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ PCB <: P . ooo I Pf!-!!J. Chloride chlorobenzene ----_i_ Pen. Chromium chloroform ----_ E lld-"!./>I <O,~~ __ Copper o-cresol _L /~d&/E --Fluoride m-cresol <0 ,(!00 '111 ----.1/l_c-fAoxlirJ/aA <:o ~oo~ Iron p-cresol ----_1o~lJ 0./ €. Lead cresol <O , 00. ----~he24A'c: ~o. OCJ0-3/fhf __ Manganese --1,4-dichlorobenzene _Ji~ <::O, O"Oll:PA'I __ Mercury --1,2-dichloroethane Nitrate 1, 1-dichloroethylene l-b/t!!JL£ <o,ooo~-----'JJ, 'e: L.PR/t./ -< o -""" fll'm Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----·······-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --.. --pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- 4-!l-97VP lindane Date Received --Reported by methoxychlor --__ toxaphene Dale Exlractc;J ~-/6--97VP Dale Reported 2,4-0 -- Dale Analyze d L/--/3-97-VP 91:i:-iZ~ _ 2,4,5-TP (Silvex) Lab Number --DI IS 3191 (Revised 2/91) , .. .,_, • ......,,,_y u • .i11-..11L Vl .C.IIVIIlJnffiCn(, 1 lea Ith, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ __:O:c....z,l,---="'-"t>e;_C,=-=>..,.=-·-------- Name of Site Wei RR E)J Cc, Ur.} ri.1 Lw op L l-L Site Location __ ....;:LJ:..:::.....:A~{{:.i.,;R.,,_,6=.:,,,v'-----'-L6>...::...,_v.....:A.f.=.....:..'N..::,__ ______ _ Collected By ----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium .A DJ-, --/ Ground water (1) _ Solid (5) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc.B -<.o, ot:1&1lj?,enf.. Chloride chlorobenzene ----✓ Pe;sr • Chromium chloroform = ENdA,il ----<d . 000/#"' __ Copper o-cresol --_.?/i/o'ANE "<t7. LJt:/0.? -~·· Fluoride m-cresol ----~,, Iron __ p-cresol ~o.t:104,,,, -- ~"""''"'"'"-Lead cresol ~M <o ,oo t:1'.:1~ ----__ Manganese --1,4-dichlorobenzene -21~/fJt:A/4 tf< < /J • 0 '7t:I /.o~ __ Mercury --1,2-dichloroethane -, '-~ L./ -&'~ox/ 't:-<:.t:7 ,dqf(f Nitrate __ 1,1-dichloroethylene I~• '•;,1 ,r v--. 1£L:1>~1 <O, t){JQ/fPnt Selemum 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- 4 -1I-97-,/p lindane Da te R eceived --Reported by __ methoxychlor D:.ilc Extraclc<l ?-/0 -971/P Dale Reported __ toxa phene --2,4-0 Da le AnalyLcd //-/F-9'ZV,O Lab Number 9 7 l.,-l3v _ 2,4,5-TP (S ilvex) --DI IS 3191 (llevised 2/91) ,,.\..... . .ucjJc.JnJncnr or tnvtronmcnt, I Icalth, & Natural Resources Solid W~sle Ma~agement Division .:,ANll'LE ANALY.Sl.S ~(JU~.ST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ O_~_o_c::>_;'---~L......------- Name of Site LJARRef\A ~1.hv;l( LA-NofLU-Site Location. __ -=LJ:..::-:.A...:...,.::f..uR.,_,,,e:.::,_:A,1.,.,__..::.G<S>..::._v....:.AJ,:_:__N.;x__ ______ _ Collected By -----------ID# ____ Date Collected __________ Time ______ _ Agency: Hazardous Waste Solid Waste ✓ S u per fund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium C·E·H --✓Groundwater (1) _ Solid (5) .. , Cadmium --Chromium --__ Surface water (2) /Liquid (6) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _·_ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ PCB <:,tJ , o o o !j;l!.m Chloride chlorobenzene ----✓ Pen. Chromium chloroform ----_E.lld~✓-11 -<:'o ,ooPl/'f!m __ Copper o-cresol -- -~ H t.7A/il € <:o, ""°.:Z,o/?m Fluoride m-cresol ----___g~Jp;e ~O.oo~ Iron __ p-cresol --Lead cresol _1P= ;;.,.,-€ <C1,t0o"-?~ -•d --~ .1? n'.,,J N' ~ -<:: c;;,. "o.rf .,;, ,..~ Manganese 1,4-dichlorobenzene "°1-Jl!:. ~.L, ~ A ,l /_.A -C:::-o, (2 (7 0 /~ ~---- --Mercury --1,2-dichloroethane r., u ~ //_,., .tiJO)(J4€-<c;l', OC'd~ Nitrate __ 1,1-dichloroethylene --/ ':,z}/cLPR~:.V <o.oc,o~P" Selenium 2, 4-d in it rot o I u en e ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----·····~·-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --.. --pyridine Microbiology --__ tetrachloroethylene --__ tricWoroethylene Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date R eceived lf-LL-'17Vf!. --Reported by __ methoxychl or ~l6-97YP __ toxaphene Da le Exlraclc<l Dale Reported 2,4-D ' .. --- Dale Analyzed L/-Lg-'771/'p · ~tJL ,'13 ·· _ 2,4,5-TP (Silvex) Lab Number !j ,.s_ ---DI IS JJ'J J (IZeviscd 2/91) I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number ____ O_)..;_e_O_-_'-_'fL--------- Name of Site WA RR Ef\J Cc:, UflJ rt{ LA:N op 1, l.-L Site Location __ ....;:;LJ~A....:....L.:({....,R.=6=1u..,,.__...;_~-'-v....:.A.1.:......:...?Y_.__ ______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium J D··A·. I. --✓ Ground water (1) _ Solid (5) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ PCB <tJ, t'OO /-lf2!!1 Chloride chlorobenzene ----✓ Pen. Chromium chloroform ----_ Gld.RJil < d 1 (20d/_fp-,A Copper o-cresol ~iilt/At./e. --- <0,000-¥P" Fluoride m-cresol --~ <o.ocl -"-"-Iron __ p-cresol --<.:,, ~.o! ~'--Lead cresol ----~/. ~dAH'£ ~o. opd,.J ~-__ Manganese 1,4-dichlorobenzene .2fe,:>~!U!A/ote <O, Ot:J09!;: --__ Mercury --1,2-dichloroethane ~ <o,ooP LILJ-. Nitrate __ 1,1-dichloroethylene ---::l) < O. t:)CJO lj:fom._ Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----·····--·· Zinc hexachlorobutadiene , ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --.. __ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-triehlorophenol --vinyl chloride ------endrin --lindane Date R eceived !J._ -/ f -C/71/P --Reported by __ methoxychlor 'f--/6-97J/P Date Reported __ toxaphene Dale Exlraclc<l 2,4-0 ~ -- 'f-l r-97Yf' ,....,,-. 3 ·· _ 2,4,5-TP (Silvex) Dale A nalyzed Lab Number ':Ja1.. ~,. ,;,,.; --D II S 3191 (Re vised 2/91) I lea Ith, & Natural Resources Solid Waste Management Division U.nLI.TAA JLJ.1-;J .n.J. 'IH...1.J.J. .::).l.::) 1'.L\.l_ U.C,.::) .l :O.tate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number ___ --=tl''--'--J..--"-t>_O_'-.... $'"---------- Name of Site LJei RR E:A~ C, cJr.1 TY LA:N op tl-L Site Location __ ....:;.W~A~f{...,R,-=e;=N.,,._ __ L<S>_u....;_AJ:::.....:....'?Y.....__ ___ _..;. __ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- p .s ·c;. Barium ✓ Ground water (1) ' --Solid (5) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------. ✓ pc..B < o, ll(')ot .H..t>\. Chloride chlorobenzene ----✓ Pen, Chromium chloroform ----END/ti t/ <o,ooo/ P{1hl.. __ Copper o-cresol --_L✓-//dAlle <"e,,~t:1.P~"t\_ Fluoride m-cresol ----m~:z~& <o. d()/~uvn Iron __ p-cresol --Lead cresol :£1!.X, ~M -c::::o • .,.,, r-'.J ~ ----11:~ue -<o,,..,--,'~ __ Manganese 1,4-dichlorobenzene --·~ ~0,0011:l;~ __ Mercury --1,2-dichloroethane .,,. 1,1JE.<O, IA--1,,1 Nitrate --1, 1-dichloroethylene /, . i//E"•r.-t:V~ ;j_O. OOo/,on'n Selenium 2,4-dinitrotoluene MA . •-~ )l • ~,/).A_ f ,",), ~ ~J -- f a· :t · II . / Silver __ heptachlor ~a 10c em1stry Sulfates hexachlorobenzene ----····-~--· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin --lindane 'f -J/=f71/£!.__ Reported by --Date Received __ methoxychlor 9 -/6 -971(P __ toxaphene D:ile Extraclc<l Date Reported 2,4-0 -- ::i?l.--,J 3~ 2,4,5-TP (Silvex) Dale AnalyLcd 9-/8-9711/) Lab Number --DI IS 3191 (Revised 2/91 ) · -. -• --r .... • .,.,._.,., V l &..,IIVllUIIIJlClll, 1 lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number ____ 6___;;U> __ ~_,_·_C_·. _______ _ Name of Site Wei RR EAA ~ u"' Tt( Lfbvo f t,1.-L Site Location ___ LJ_A~{{~R.~t!:~AJ ___ ~_v_A.f~'?Y~------- Collected By ----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium cc. I --✓ Ground water (1) _ Solid (5) Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------_ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ pc..g < 0. ~00 l.Jf!."'-Chloride chlorobenzene ----✓ i!/J~:o Chromium chloroform <O,oot:J/..t:20.w ----__ Copper o-cresol --L./Ald'AAI= ~o . 0002".-... Fluoride m-cresol Zl1£t/47xyeidtll"l..-< o. ot?/ .. ~ ----Iron p-cresol ----~X .t1.n~IE#G ~4.00.: --Lead cresol __f!h 11-"-11H£ <o. O Ot:7.. .:-.,, ~ Manganese --1,4-dichlorobenzene -1:/~-f:,4-L.I.,-"<:P, 000 J '/Jnn ,.. --__ Mercury 1,2-dichloroethane ~ I/ -./ ¼ , J:",,, ,nf ~ ~ -- 1 ,~ .,;e,. faJ'! "vi <P. l?d j' 4'lA' L-Nitrate __ 1,1-dichloroethylene lf'J)/ eL-.I)J;ziiv -<0,00011,1'1 Selenium 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobu tadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --.. --pyridine Microbiology --__ tetrachlornethylene --__ trichloroethylene Par ameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- 4-LL-171/e Reported by lindane Date R eceived --__ methoxychlor i/-l'1-97-VP __ toxaphene Date Ext racted Dale Reported 2,4-D .. -- Lf-L~271'P B?:i.~ ~ _ 2,4,5-TP (Silvex) Dale A nalyzed Lab Number --DI IS 3191 (llevised 2/91) · · -· --r~• ........... '·" '-'UVILV UlllC.II L, I lea Ith, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O . Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ o_'\._fP_b_'-_'"1 ________ _ Name of Site LJA RR E)J ~ cJflJ Tl( Lw op u . .L Site Location __ ...:LJ=-..;A~P..:.,_R.,._,e:=1,1,.___~:....;;:___c/-'-'A.J=-::.-Ni_ ______ _ Collected By ID# Date Collected Time -------------------------------- Agency: Hazardous Waste Solid Waste ✓superfund Sample Type Environmental Concentrate Comments ✓ Ground water (1) __ Solid (5) Jot<,' __ Surface water (2) /Liquid (6) ___________ _ _ Soil (3) _ Sludge (T) __________ _ _ Other (4) _ Other (8) ___________ _ Organic Chemistry Parameter Results(mg/1) _P&T:GC/MS _ Acid:B/N Ext. MTBE ~ pc...B -<'O . 000(#41 __.!t._ Pen. =£k;fjj£ :; . ~ ...:m . . _<.:=.,......::...::c~.a..:.. ..... Inorganic Chemistry Parameter Arsenic Barium Cadmium Chloride Chromium __ Copper Fluoride Iron Lead Results (mg/I) (mg/kg) -=:~!'.:!:~~~!"I __ Manganese Radiochemistry Parameter Results (PCi/1) __ Gross Alpha -------Gross Beta Microbiology Parameter Results (Col/lO0ml) __ Mercury Nitrate Selenium Silver Sulfates Zinc pH Conductivity TDS TOC ------- Date Received l/-//-9'7VP Reported by ________ _ Da te Extractct.! L/ -/fa -97 --VP Date Reported _______ _ Dale A nalyLcd 9'-/l'-971/P Lab Number ___ "J_7_._'.l._··_i J_·r _~_. · __ DI IS 3191 (Revised 2/91) TCLP Compounds Inorganic Com pounds Arsenic Barium Cadmium Chromium Lead __ Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results (mg/I) Results(mg/1) ------ ------= 1,1-dichloroethylene _____ _ 2,4-dinitrotoluene heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane methyl ethyl ketone nitrobenzene pentachlorophenol pyridine __ tetrachloroethylene ------ ------ trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ --vin yl chloride endrin lindane methoxychlor toxaphene 2,4-D _ 2,4,5-TP (Silvex) · ·· -• --r-• ••••-••• ,._,~ .L.,JJVJJ.Vlllll~lll1 I kalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ o~ __ l.-_,._o__;,::c.......,811:._ _______ _ Name of Site lJARR,,EI\J 0>UrvT<I Lwope,1...L Site Location __ _:W::..=:....A:...,..r..f{,.,_R,.,,_e;=AJ,L__~=..;::.._u...:.;Af"-!...Ni.._ ______ _ Collected By -----------ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ✓ S u per fund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) _ Solid (5) N>b\ Jr, r Cadmium --Chromium --__ Surface water (2) /Liquid (6) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) --P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ PCB ~o.noa/.--Chloride chlorobenzene ,, I ----✓ P1;;n • Chromium chloroform = 5.ldtou ---- -=:' 0 1 O oo I nn1111 __ Copper o-cresol --_4tvd4tle <"o,a,,,....✓-.'--Fluoride m-cresol ----~E't-A.,xy cA/11/~, ~tJ I J',/;-Iron p-cresol ----~ <(},tJt)).>n.t,~ Lead cresol ---<.c?, 0..,..,, ,f ___ __ Manganese 1,4-dichlorobenzene --1i~~ < O , e,o~,r;,,.,,, Mercury --1,2-dichloroethane ' A :t~t:.-!'O.Oi"V-'I'-~, ... --Nitrate 1, 1-dichloroethylene --':J)/eCJ)R1tl <o . o'1P/pp,1 Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----..... ~--·• Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity melhyl ethyl ketone --Grnss Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ------vinyl chloride --endrin --lindane Date R eceived 'I-II -971/P --Reported by methoxychlor -- 'I-It, -'1'7 1/P __ toxaphene D:.itc Exlraclct.l Dale Reported 2,4-D -- Dale Analyzed !'--/%-971/.I? ~7l.~3L 2,4,5-TP (Silvex) Lab Number --DI IS 3191 (Revised 2/91 ) · -. -• --r-• ••••-••• v• J.Jll'IJ.lUIIIIICIIL, I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ O--'l.._o---=O'-'C. __ ,...L... ______ _ Name of Site WA RR Ef\J ~ <hJ Ttl LAN o E Ll-L Site Location. __ ..:::W~A...!...l..::({i:.R...,,€.:::N""'--..::c~-=--c./....:lfJ!:...!..N.::i...._ ______ _ Collected By ID# Date Collected ___________ Time --------------------- Agency: Hazardous Waste Solid Waste ✓superfund Sample Type Environmental Concentrate Comments ✓ Ground water (1) Solid (5) RT _ Surface water (2) /Liquid (6) ___________ _ _ Soil (3) _ Other (4) _ Sludge (7) __________ _ Other (8) Organic Chemistry Inorganic Chemistry Parameter Results(mg/1) _P&T:GC/MS _ Acid:B/N Ext. MTBE ~ pcB <o,~0<,W,,,, _L_ p ~ . Parameter Arsenic Barium Cadmium Chloride Chromium __ Copper Fluoride Iron Lead Results (mg/I) (mg/kg) -"<-L""""""-"'-''-=-..::::!~~~~~,u __ Manganese ,..........~~~~ --=-...:....::~:..=..'1',#:#.=Y __ Mercury Nitrate Selenium ,_-.,rn__ Silver Sulfates Zinc Parameter Results (PCi/1) pH __ Gross Alpha -------__ Conductivity ______ _ Gross Beta TDS TOC Microbiology Parameter Results (Col/l00ml) Date Received L/--/I-C/71//J Reported by ________ _ D:.ilc Extraclcc.l 'f-/C, -9 7 J/P Date Reported _______ _ Dale AnalyLcd 'f-/ (J-'17Vp Lab Number ___ ':J_·'_?_l.._._'-.1_i,3_''u' __ DI IS 3191 (Revised 2/91) TCLP Compounds Inorganic Com pounds Arsenic Barium Cadmium Chromium Lead Mercury Selenium Silver · Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1,4--dichlorobenzene 1,2-dichloroethane 1, 1-dichloroethylene 2,4-dinitrotoluene heptachlor hexachlorobenzene hexachlorobutadiene hexachloroelhane melhyl elhyl ketone nitrobenzene __ . pentachlorophenol __ pyridine __ tetrachloroethylene trichloroethylene Results (mg/I) Results(mg/1) ------ ------ ------ ------ ------ _ 2,4,5-trichlorophenol _____ _ 2,4,6-trichlorophenol --vinyl chloride ------ endrin lindane __ methoxychlor __ toxaphene 2,4-D _ 2,4,5-TP (Silvex) l lcalth, & Natural Resources Solid Waste Management Division ._,,.,._._,.._.._ ..._,~ n.!"lfl.1..,.1..:J.l.:J n.L\l_U£,0.I. State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number O l 0011) --~~~-~~------------------------- Name of Site LJARRE;l\,I Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓Su per fund TCLP Compounds --- --- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --/ Ground water (1) _ Solid (5) 8Dll~ -' Cadmium --Chromium /Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ ✓ peg <o, O PP/ .n-Chloride chlorobenzene ,, ----✓ Pf;H , Chromium chloroform = Ei)/t/rllil <o,ooq~ --__ Copper o-cresol --Fluoride m-cresol --~ <o,p<1,;. 1 '-------2JJ. "<" o ~ o-o I 11/?At Iron __ p-cresol ~ <:o, o a "f. --Lead cresol --_(½¼,~/{£ ~o.oo~J:,I __ -__ Manganese 1,4-dichlorobenzene -- ~<:0,400''-__ Mercury --1,2-dichloroethane -~1tlc<"u. o~~b/.a w-Nitrate __ 1,1-dichloroethylene -;JJ /A/<: o, 0001;;,~ Selenium 2,4-dinitrotoluene i.,.-----,, Silver heptachlor --Radiochemistry Sulfates hexachlorobenzene ----···----. Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --.. --pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride ------endrin -- 'f-J /-'17-,/p lindane Date Received --Report ed by __ methoxychlor L/-/t,-971,/p __ toxaphene Da te Extracted Date Reported 2,4-D -- ~7'll. ~ 3 b _ 2,4,5-TP (Silvex) Da le A nalyLcd li_-/Y-971/P Lab Number --DI IS 3191 (llcvised 2/91) ~if'J~ ( (~ I Jo~~ I fclj \j )f, ~ 0C ~ ~ ~ / ~ \.,__}ul\ s.+ l ~ I 1(),-.l Ac~ ....-:-: ---- II : IF.,,: ! ·1 r .. •. 1 ' • I l ., ,. I ; ~ l ... -~: r "I \.. -\. ·-<-~ •I .,'. . . ~; :. ~~ ii·" 1. I . I. ~~ . .. . ~;~ . ·1 .-..;, --~ ~ ,· '\' ,.)...••'' ., },' ... ,..._./' ) :., . ' ..... ;- ' . l ·' ., N.C. Department of Environment, lkallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laborato.ry of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number ____ D_<..~O_O_'t_1 _______ _ Name of ~te 6J It R.R.f:-N C:::vN Y'{ l..,wlJ ft U--Site Location __ W_A-~B.~t<~e~A/~_C_v_111_ty~------- Collected By -----------ID# Date Collected Time ---------------------- I Agency: Hazardous W a'.ste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) KTB -':I --_ Solid (5) Cadmium --Chromium ✓Liquid (6) --__ Surface water (2) Lead --__ Mercury _Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) ✓r&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----.... ____ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta . TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --- ~port0 )i 1.:-R./U v•J~ 0 lindane L/-J/-971/;0 --Date Received __ methoxychlor Date~orted t//3o/f7 __ toxaphene Dale Extraclc<l 2,4-D --, _ 2,4,5-TP (Silvex) Dale AnalyLcd 4-1~41 tv, Lab Number -:l7 :.l~ ~ --D I IS J l'J I (Revised 2/91) I lcallh, & Natural Resources Solid Waste Management Division ................. , ... A A-J&:,J r>...l.,.t'"1...LJ.A.ti.JAL' .l.~'l_U.I..JU..I. .:,cace uooratoxy or t'uo11c Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number O~f> o-t g -----=--~~~'--------------------------- Name of Site uJ fr {s((f:-N i: ul\l 1'<1 Gwo Ff LL Site Location __ W_.:....;A~B-:..,..t{~e,"'-A/~_C,_c/_i'll--'-'--iy..__ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds --- --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ' g Barium / Ground water (1) "i --_ Solid (5) Cadmium --Chromium ✓Liquid (6) --__ Surface water (2) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----···~---·• Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received tf-/J-q,71/f> --Reported by methoxychlor --__ toxaphene Date Exlractcc..1 Dale Reported 2 4-D --·' . '-I~ I (.p -q 7 1JJ ~7ll.~4u 2,4,5-TP (Silvex) Dat e AnalyLcd Lab Number --DI IS 3191 (Revised 2/91) .I , .. ._ • .....,._.}--'u' ~1111,..Jll Ul C..fiVlIUnmCn(, I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Pu blic Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North urolina 27611 Site Number ----------------Field Sample Number ____ 0_.2.._<>--=0'---1....._,..L..... ______ _ Name of Site uJ ft PJ{{:.,N i: ul\l t'f l...,w/J F / c.J._. Site Location _ __;W:__A-'--!.C8-'-'-'{{,._,_e,"'-A/=---_____;:C,=-c/..:...:clll'--'fy'-'------- Collected By -----------ID# ____ Date Collected ___________ Time _____ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ✓' Ground water (1) A-w '-f --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead --. __ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----··•-~---• Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received L,t-/ /-q ?VP --Reported by methoxychlor -- --toxaphene D:ilc Extraclc<l Date Reported 2,4-D -- '-/-J{_q .,,q7 Nt 7 '4 ' __ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number ':J '..l~ .. --DI IS 3191 (Revised 2/91) I ~---U\..}JUJ llliClll Ul cnV1ronmcnt, I Icalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number· _ __:!r§~·~-,~•litfel!l!:el__~0~4,~()~l~6~(}~-- Name of Site 0J fr f<R.f:.-N C:::: Ui\,(('{ L,wl) ff U--Site Location_---'W__,A-~f?,._,_t,_,_,e;c....;:A/'----_C,.;;:....::_c,1.....;..M;.:_iy.:.....1-_____ _ Collected By -----------ID# Dale Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) J t) '( -- _ Solid (5) Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) /P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride -·---MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ---- ··••►•-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received L/-//-q71/ /2 Reported by --methoxychlor --__ toxaphene DJle Exlraclc<l Date Reported 2 4-D ~-~---< ~----' . 'f-;J;J-17 NT ~?l.1"14~ . 2,4,5-TP (Silvex) Dale Analyzed Lab Number --DI IS 3191 (Revised 2/91) . ·•~· --y ............ ,~ VI. L,IIVlJ.VlllnCnl, I lea Ith, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ___ <::l-'--2....=.....c.t>---al._O"--'-I _______ _ Name of Site 0J fr f<R,{;.,N i:; ul\l Y'( L__,wl) Ft U-. Site Location __ LJ_~A~B-~t<~e~A/~_C,_c/_1t1_iy~------ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type f · . Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium Si --J Ground water (1) _ Solid (5) Lf Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene -------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --. Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····~·-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- 1./-/ J~ C/7 -VP lindane --Date Received Reported by __ methoxychlor --toxaphene D:i le Extraclc<l Dale_ Reported 2 4-D .. ----·--·-' ---. '-l·cU-°11 NT ~'?l.~14~ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --I) I IS J I 'Jl ( Revised 2/91) .,.\...,. u 1.:punmcnt Ot tnvuonmcnt, 1 lea Ith, & Natural Resources Sulid Waste: Managc:mc:nt Division State: Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North uirolina 27611 Sile Number ----------------Field Sample Number __ _:e>'---a...,:=c..::o'---Lf-=O:.....t...=--------- Name of Site 6J ft &R{:.,N i: Ut\l JY Gwl) FI U-Site Location __ ---=w=--=--~A-~B-:.Lls>..!.e.!.:.A/~--=C,=-=-c/..:..::fll:.....:iy~ _____ _ Collected By -----------ID# Dale Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- Ps Barium / Ground water (1) y --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) /P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO-Oml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received 1/-//-L'f 7 1/P --Reported by __ methoxychlor __ toxaphene Dale Extraclc<l Dale Reporled 2,4-D --~• ,,... -- 1~-C/7 N1 ..:J7 l.~41-u 2,4,5-TP (Silvex) Dale Analyzed Lab Number --1)1 IS 3191 (Revised 2/91) '1 , ... .._. u '--pc.11 u11c nl uc cnvtronmcnt, llcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh , North Carolina 27611 Sile Number ----------------Field Sample Number ___ 0_2._t>_f_o __ ~~--------- Name of Site 0) ft B,R-CN C: Ul\l \Y Gwl) EI lJ._. Site Location __ W'--A-~B-:.Lt.,,._,_e,"--A/"--__,;;:C,...,;;__c,1-'--'n.1'-''fy_.__ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) En vironmental Concentrate Comments Arsenic --Barium JD H --✓ Ground water (1) _ Solid (5) 3 Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead -- --Mercury _ Soil (3) Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichl orobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····-·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received Lf-Jl,-qn'P --R eported by methoxychlor -- --toxaphene 0;,i le Exlraclc<l Date R~ported 2,4-D --... -- Date Ana lyLcd_!i_-J 3 -Vur ~7 l.-J4~ __ 2,4,5-TP (Silvex) Lab Number DI IS 3191 (Revised 2/91) -- ~· I Icalth, & Natural Resources Solid Waste Management Division t.....1r>...L•.&.& .&....1.&..:.1 .r1..1.,.l"1..LI.I..J.I.U .nJ.J\.,,l.U.C,U.l. ~late Laboratory of Public Health P.O. Box 2&047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ ___:0::....~=--:0=:;_:;l--=e>::..........i'{.___· . ._• ______ _ Name of Site 0) fr B,R,f:._r..J i: UI\J T'i 4trJlJ FI LL Site Location. _ ___;w::.,_::_.!,...A-!.L:R.:.L{{~e-1:Al~___;C,:::.:::....:v....:.ll,(;,.__:_iy..1,__ _____ _ Collected By -----------ID# Date Collected Time --------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) RA-,n ~ --_ Solid (5) Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead --__ Mercury _· Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····-·-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyrid ine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- Lf-J J-111/P lindane Date' Received --Reported by methoxychlor --__ toxaphene Date Extractc<l Date Reported 2,4-D ....... -. , ..... -- '-/-J.3-CJ? NT ~:r11. -~ ~c. __ 2,4,5-TP (Si lvex) Dale AnalyLc.:d Lab Number --DI IS 3191 (Revised 2/91) , ......... ..., ... t'"'' ~•11\,,IIL UL L:,UVIIUnmcnc, I lcalth, & Natural Resources Solid Waste Management Division Site Number uftl.Y.lrLic, 1\..l"IALl.:)1.:) Kr..\,JUt.:)1 Field Sample Number ---------------- State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 ----------------- Name of Site U) fr B,ftf:._N i: Ut\1 Y'( ~l) EI U-Site Location _ ___;W'---..:A--I..c.B-1.C>.{{.,,,.e:.:...:,A/c___C,::::..-=--c/....:..lt/;;:._ty.:.....,__ _____ _ Collected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium J Ground water (1) _ Solid (5) A!.B --"'i --Cadmium Chromium --✓Liquid (6) __ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachl orobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received 'I-I /-971/P --Reported by __ methoxychl or --toxaph ene Da le Exlraclc<l Date Reported 2,4,~D ._ ----- 't--;;:341 tJ-r ~:f,l.1141 '/ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --I)! IS 3191 (Revised 2/91) '·--· ...., .... }-''-'' LIIICIIL Ul cnVlronment, I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ 0_.2._t:>___.:./_O_b=---------- Name of Site 0J fr RR:CN i: ul\J Y'( W l) F / U-Site Location. _ ___:W:....:....;A-~8-~ts..,_6.c..;Al::__~C,:..::....:....v.:..::l'll_:cfy_.L_ _____ _ Collected By -----------ID# ____ Date Collected __________ Time ______ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --; Barium / Ground water (1) DRtl --_ Solid (5) y Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----__ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Received LJ-/ /-f 7-g/f) lindane --Reported by --methoxychlor __ toxaphene Dale Extraclcu D_atc Reported 2,4-D .. -., -- '-(J,3 ✓q1 NT ';J',1-~~u 2,4,5-TP (Silvex) Dale Analyzed Lab Number --DI IS 3191 (Revised 2/91) I lcallh, & Natural Resources Solid Waste Management Division un..J.TJ.J. .1...,~ tt.J.'CJ-\.LJ..::>.l.::> ~\!_UC.:> .l State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number O 4 ()IO.., ------~~~------------------------ Name of Site 0) ft B,R,f:._r-.J c::: Ut\.(('{ MNIJ FI LL Site Localion __ w_.:...A-'"'"f?.,..../s,,_,e"'-A/-'--_C_v_l'L/""'--'-ty..__ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) RPA& --_ Solid (5) "' Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) ✓P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ · 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received l.f-//-c[7 1/f> --Reported by __ methoxychl or __ toxaphene D;,ilc Extraclc<l D ale Reporled 2,4-D .. ... . ... -- 'f-J.3_ ;<:l_1Ail 'r ' • 2,4,5-TP (S il vex) Dal e AnalyLcd Lab Number ';J~,l.. .:. ½,....) --DI IS 3191 (Revised 2/91) I lcallh, & Natural Resources Solid Waste Management Division Un>J.TAA .J...~ n.J_ 'lft.LJJ. .:JJ..:J =\l_U.C..u .l State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ___ ...;;;_6_2.__.:.,o_t _6____,.,8;......_ ______ _ Name of Site Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) _ Solid (5) A-s ti l/ -- --Cadmium Chromium ✓Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --ConductiviLy __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane lf -,; 1--1'1 rt' --Date Received Reported by methoxychlor --__ toxaphene Dale Exlraclc.:<l Date Reported 2,4-D _ .. , .. -· -- 'J'7l.., 15 v __ 2,4,5-TP (Silvex) Dale AnalyLc.:d i.f ~J3_-C/1 rfC Lab Number DI IS 3191 (llevised 2/91) ' -- I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ C>_~_O__:.I_O_C,.....__ _______ _ Name of Site uJ f'r B,R,-f;_N i: uA11'{ ~IJ f I LL Site Location _ ____:W=--=--~A-!.1.:f?.:.1.t{~e~Al..::...._____:C,=-cv....:.n.t~iyJ........_ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Res.ults (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) R!>A8 '-/ --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) --Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutad iene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received Lf-11 -7 71/P --Reported by methoxychlor --__ toxaphene D;ile Extraclc<l Date Reported 2,4-D -- '--J-J.3 81 NJ '[J·;::,._ ' 4"' 2,4,5-TP (S ilvex) Dal e AnalyLcd Lab Number ~.,:)J:,,, --DI IS 3191 (lteviscd 2/91) . ··-· ....., ... P""'~•11 1.-1H uL 1.:.,nvironmcnt, I lea Ith , & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ 0-=--:2..=-->__,l___:_( -="-------- Name of Site lJ ft fsR,~N C:::: u/l/ 1'( k+,..cl) Ff LL Site Location __ l,J_-'-A-'-'-R.::..Lt{.,_,6..._A/-"--_C,~v--'n1-'--'-iy..,__ _____ _ Collected By -----------ID# Date Collected Time --------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium A-J --J Ground water (1) _ Solid (5) ':i Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ✓r &T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----.... _. ___ Zinc hexachl orobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Da te R eceived t/--/1-92-,/P --Reported by --methoxychlor __ toxaph ene Da le Exlraclc<l D ale Repo rted 2,4-D -- Date Analyzed 'f-~ 8-9'1 ~ ~7l.:.~5A., __ 2,4,5-TP (S ilvex) Lab Number --DI IS Jl'Jl (Revised 2/91) , ... ..__. u 1.;p...i1 l111cnl uc cnvuonmcnt, I lea Ith, & Natural Resources Solid Waste Management Division ~AJ.Ylt'L~ ANALl'.~l~ 1<£,l.JU~~T State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ 0_2._o~f...,l........,I'---------- Name of Site 6.J fr B,Rf:..N i: u,,,(TY kw I) EI U-Site Location __ w;:__.!....A-C-'-'f?e..<.({....,,e;""-A/..::,_____;C,=-=--c/.....:..n.J;;.:__:_iyL_ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) R.PF-'-f --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates he:xachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received Lf-//-9 77/,P --Reported by --methoxychlor __ toxaphene Date Extraclr.:<l Dale Reported 2,4-D -- J7J..,:l53 __ 2,4,5-TP (Silvex) Dale Analyzr.:d J./-J,.3-9_'7 /\IT Lab Number --DI IS 3191 (Revised 2/91) · -· --r-• .,,.,....,. VL &..JUVl.lVllll1Clll1 I lcalth, & Natural Resources Solid Waste: Managc:mc:nt Division State: Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ 0_2_t>_l_l2,~~------- Name of Sile uJ fr Rft~N i:u/\J ,y 4tNDF[ c.J.._ Site Location __ w_'--'A-'-'8-C.,./s~e~A/~_C,_c/_fll_iy~------ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium RAJR --'i --/ Ground water (1) _ Solid (5) Cadmium --Chromium ✓Liquid (6) --__ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----.,.. _____ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity __ methyl ethyl k~tone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received Lf-//--9711/J Reported by --__ methoxychlor __ toxaphene D;ite Extractc<l Date Reported 2,4-0 . . .. -- ~--;1,.t 5'-'.t 2,4,5-TP (Silvex) Dale Analyzed l/,;).3-CJ_1rvr Lab Number --DI IS 319 1 (Revised 2/91) I lcallh, & Natural Resources Solid Waste Management Division uNo..1•.1.1 .1..,c, ft.l'l~J. .:,1..:, 1'..C\l_UC.:, .I. State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ t>~~-=-I>_/_/....,,~::.._ ______ _ Name of Site uJ f'r g&,-e.,Ni C:: ul\l Y'{ l__,wlJ ft U-Site Location __ --=W=--=-~A-J.::.R.:.i..:tl..J.e~Al::...._--=C,=..:....c/..:..::n.tc...:iy...1-_____ _ Collected By -----------ID# Date Collected Time --------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) Jl)f,J , "' --_ Solid (5) Cadmium --Chromium --__ Surface water (2) ~Liquid (6) Lead -- --Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- --- --- Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Micro bi o Io gy --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received L/-llf'z--VP --Reported by methoxychlor --__ toxaphene Dale Exlraclc<l Dale Reported 2,4-D -- 1 -;J.'-{-97 NT -:J'";:n.--;s~ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --l)J IS J l'Jl (lleviscd 2/91) , .. .....,. . ._,,._yu, \111"--IIL Vl 1..:.0VllU0ffiCfl{1 I lcalth, & Natural Resources Solid Waste Management Division S1a1e Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street RBlcigh, North Carolina 27611 Sile Number ----------------Field Sam pie Number ___ --=C>c.........:~:.....•;__:.f.3../_'f.,.__ _______ _ Name of Site 0J fr R,&,e:.-N i.:uN JY l.,w1J FI LL Site Location_--'W'--!..-'A-CL:R.:.L.f_,._,,e;"""A/-"---=C,=-=--v..:..;;n.1:....:iy_,__ _____ _ Collected By -----------ID# ____ Dale Collected ___________ Time _____ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) -- _ Solid (5) M>J ~ Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead -- --Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ · Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexach lorobenzene ----····~·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received L/-// ..t'.17-VP --Reported by methoxychlor -- --toxaphene Dale Exlraclcu Dale Reported 2,4-D -- .:Jr,?'J..· t 5 ,. _· _ 2,4,5-TP (Silvex) Dale AnalyLcd__!j-J,'f-qt NT Lab Number '-<,_ \..1,1 --DI IS 3191 (ltevised 2/91) , •. ..__ . .....,.._y,•u lllll..lH Ul C..l1VlfU0ffiCn(1 I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number ~2.o fir --------=-------------------------- Name of Site uJ fr BR.~N i: U/\.11:Y Lwl) EI U-Site Location __ w:__.:.....A-:.J.CR.::.L{{.,._,(:,""'A/--=---C,;;:;..;;_c/_;.n,/.;.:__:_ty_,__ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium J Ground water (1) --_ Solid (5) C ~M-'-f Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----···--·-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received L/-11-977#' --Reported by __ methoxychlor --toxaphene D:.ile Exlraclc<l Date Reported 2 4-D --, .. 'f,J.J:{91 A1T ~?l.· ,(:::, ·.,-, 2,4,5-TP (Si lvex) Dale Analyzed Lab Number --DI IS 3191 (Revised 2/91) -~r -•····-••• ...,.. -•••I.LVll llll..lit1 I lcallh, & Natural Resources Solid Waste Management Division u.nu.•.1..1. .a..,.c, ~'l~.1.J.lJ ~'-l._U.L:,J.I. :::>talc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ___ ""'t:>~1..~d~f~t ~'---------- Name of Site lo ft 8,Rf:-N c:::: Ul\l T'f kwl) FI U--Site Localion __ w_-'-'A-'-'-'R.'-'-1<-"-"e;"'--A/-'---_c_c/_tl/~TY....._ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) -- Solid (5) J t>A 'i Cadmium --Chromium --✓Liquid (6) __ Surface water (2) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) ✓P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·-Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ G ross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received 1/-11-9' 7 -1/ ,0 --Reported by __ methoxychlor --toxaphene D;ite Ex tractc<l Date Reported 2,4-D -- '-/-~J.f-9 7 Nr "J"ll. '" lJ _ 2,4,5-TP (Silvex) Dale A na lyLcd Lab Number ·,,t J --D I IS 3191 (llevised 2/91) , ·•-• ._..-..t'Ullllll,.,IH Ul L,UVlIUfimC:0[1 I lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O . Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number t> 2.. 6 I I, ------~~------------------------- Name of Site Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) ps 6-'-f --_ Solid (5) Cadmium --Chromium ✓Liquid (6) --__ Surface water (2) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----__ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----... 4--•· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nilrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Dat e Received i/-/ /-C/7 1/P --Reported by __ methoxychlor --toxaphene D:i le Extraclc<l D ale Reported 2,4-D -- 4-cJ-4-47 N-J Lab Number ';j',' l,, i; ~ ~ __ 2,4,5-TP (Silvex) Dale AnalyLcd JJ .. ,; --DI IS 3191 (Revised 2/91) I lea Ith, & Natural Resources Solid Waste Management Division Un..J.TAA J..;C, Hu."ltt.L.1.0J.a ~v..uc.0.1. State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number -----------------O~o .// f ---------------- Name of Site u) ft 8,R.{:..N i: U,\I T'i L,r.tl) Et LL Site Location __ w_-'-A--'-'8-"-'/s...,_,.,e_A/~_C_v_/'l,/_iy~------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) --_ Solid (5) c.c 'f Cadmium --Chromium --~Liquid (6) __ Surface water (2) Lead -- --Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------__ , Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene ----Mercury 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----••-.---· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane 'f-/1 -qJJlf' --Date Received Reported by methoxychlor --__ toxaphene Date ExtractcJ Dale Reporled 2,4-D -- 4-;J.'-f-97 NJ Lab Number ::f7 JL · t b '-..· 2,4,5-TP (Silvex) Dale AnalyLcd --DI IS 3191 (Revised 2/91) ------~····· ... ··~, I lea Ith, & Natural Resources Solid Waste: Managc:mc:nt Division .._,,.1..-...,.-..-. .LJ&..:.J r»,..J. .. ~..a. v.a.u .1.'-..LJ'l. LJ.LjU ..1. :>tatc: uooratory ot t'ubhc Hc:alth P.O. Box 28047, 306 N. Wilmingtol) Street Ralc:igh, North Carolina 27611 Sile Number Field Sample Number ____ (>_\.._t>--'-f """"(_'I...___ _____ _ Name of Site 0J ft R,R.f:-N i: ul\l Y'( ~IJ FI u.... Site Location __ L,J_'-'ACL:R.'-'-({,._,,e;'""A/~_C,c:....;_v--'-n.1~iy...__ _____ _ Collected By -----------ID# Dale Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- Jofl Barium / Ground water (1) y --_ Solid (5) Cadmium --Chromium ~Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓r&T:GC/MS Arsenic benzene ----_ Acid:B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----.... ____ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane 4-JJ-f71IP --Date Received Reported by __ methoxychlor --toxaphene D~le ExtraclcJ Dale Reported 2,4-D __ -- J'/'.L1°J6 ....... _ 2,4,5-TP (Silvex) Date AnalyLcd '-1-J. J./--97 )JT Lab Number --1)1 IS 3191 (Revised 2/91) ''·'--· ucpanmcnt ot environment, I lcalth, & Natural Resources Solid Waste Management Division .:::,AM.t'L.t: ANALYSIS KE(JU.t;ST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street RBleigh, North Carolina 27611 Sile Number Field Sample Number 01...• t 2..c) _______ ......,,"'-='------------------------- Name of Site 0) fr R.R,-e:..Ni ~ ul\l ,y ~I) F / L.L Site Location __ W___,A-c...:..L.::8-.L..l~..,_6<C...;A/=------"'C,-"--v""'"'it/--'-iy.....__ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) --_ Solid (5) ,NIP\ NI "f Cadmium --Chromium ~Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor · --Radiochemistry Sulfates hexachlorobenzene ----.... _____ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachlorocthane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane L/-Jl-?7 1(P --Date Received Reported by methoxychlor --__ toxaphene D:ilc Exlraclc<l Dale Reported 2,4-D -- 4~~'-I-C/1!JII. ~'11..-t b~:v 2,4,5-TP (Silvex) Dale Analyzed Lab Number --DI IS 3191 (Revised 2/91) I lcallh, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number 02.• \ '2-l -----~----------- Name of Site 6J fr B.R-CN i: Ut\l T'f'. Lwo FI LJ._. Site Location __ w_'-'A'-'-'&'--'-/s,.,,e"'-A/-'--_C_v_n.1-'--iy..___ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) 8-T '-( --_ Solid (5) Cadmium --.. Chromium ✓Liquid (6) --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) /P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----' Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane ¥-11-✓qz -yp --Date Received Reported by methoxychlor --__ toxaphene Dale Exlractc<l Dale Reported 2,4-0 -- '-/--;).tf--C/1 AIL J 'l l, .:ibd __ 2,4,5-TP (S ilvex) Dale Analyzed Lab Number --DI IS 3 191 (Revised 2/91) l lcalth, & Natural Resources Solid Waste Management Division uno...i.• ,.,. .uc, n.i. -.ftLJ. .:,1.u .l'-.C,\.l_ uc,u J. ::itate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Strt:et Raleigh, North Carolina 27611 Sile Number Field Sample Number ____ lJ_~_•__,jc...::t=l..-'--------- Name of Site Collected By -----------ID# Dale Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) En vi ronmen ta! Concentrate Comments Arsenic --Barium --/ Ground water (1) _ Solid (5) ~i> RJ 'i Cadmium --Chromium ✓Liquid ( 6) --__ Surface water (2) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --·Lead cresol ------ ----Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received 1/-[/-?'71/.,0 --Reported by __ methoxychlor __ toxaphene Dale ExlraclcJ Date Reported 2,4-0 -- 4 -J.6-17 lv'T J'l'i• }'0'7~ __ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --DI IS 3191 (Revised 2/91) I lcalth, & Natural Resources Solid Waste Management Division u~T,1.,1. LI~ tt..J. '1./1,.L.J. .:,J..:, ~v.. UC.u .I. ~tate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sam pie Number __ ___;IJ:;__::;'2.:.....t>__.(_,.lCIIE..J3.., ________ _ Name of Site 6J fr B,R,{:.,N i:ut\l Tit 4tr:tlJ Ft LL Site Location _ __;.W~A-~R....,.({.,..e;c....::A/'---_C,.:::..::;._v_:.tt1.:e.....:_fy.___ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) C ·AN --_ Solid (5) . '1 Cadmium --Chromium --__ Surface water (2) ✓Liquid (6) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver -- _ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ---- Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----... ·--·· Zinc hexachlorobutadiene ' ----Parametu Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received I'/-~//-17# -- Reported by methoxychlor -- --toxaphene D;.ile Exlraclc<l Dale Reported 2,4-D -- t./-J!5-q1 NT ;;j; ' 'l 2,4,5-TP (Silvex) Date Analyzed Lab Number , Jl., ,dJ '-' --DI IS 3191 (Revised 2/91) , ........ ..., -t' .... ~"''"·"~ v1. LUV11Vl11fiCn(1 l lcalth, & Natural Resources Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Rakigh, North Carolina 27611 Sile Number ----------------Field Sample Number __ ---=0-~c...=....co'--t-'-~-~ ..... ·~-------- Name of Site uJ ft R.R:CN i: u/\l Y'{ 0wo f / U-Site Location __ W_A-::.....:...<..:R.:.Ll<.,_,,B"""A/~_C,;c..;;_v.....;.ll/.;.:.....;.....iy..__ _____ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium / Ground water (1) _ Solid (5) C~H-T -- "" --Cadmium Chromium -- __ Surface water (2) ✓Liquid (6) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ , Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganes~ 1,4-dichlorobenzene -- ----Mercury 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin lindane Date Received 1./-/1 -9'71/P -- Reported by --methoxychlor __ toxaphene Dale Exlraclcc.J Date Reported 2,4-D -- 1-:26 -97J'/T ·iJ• ,'J.. ~su 2,4,5-TP (Silvex) Dale Analyzed Lab Number --DI IS 3191 (ltevised 2/91) NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: ,.,,/ (i, Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: l:.J~:-.r u,..._ Lc,n \~-y Sampled By: __ ~_-+_· ,_ . .f-_t'_J ____ _ Site ID# (NCD#) ______ _ Sampler ID _________ _ Location: -------------Telephone:(__) _______ _ Address: Date Sampled: y-, 'i -'i y.'( Time Sampled: _________ _ Sample Types: Soil Water ~ Waste Other Remarks: Tl'Y\55 Lsss "T At.J JD 8 M 1 IU r; . d<.A,H .. , Jl)IJJ A-DJ 1 c. E f-1 J .J DA -::1~PJ~G-<--JJ~c~c.~JI-''=\ o~~..:.iJ-r'ri~f>'l~f'17;1~~~~--------- c... A-N -'-1 C..Ef-f f-'-1 Field Sample Numbers Relinquished B (Signature) Time: Date: #J? Time: __ _ Date: 1/-<'l-<9? Time: ___ _ Date: lf.-l!-77 Time: /1: uS Date: Time: ---STATE IABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS * ~ PURGEA.BLE COMPOUNDS LAB NO q1143q q '114-'-I-D FIELD NO ;;ooq? ;2DOCJ6 COMPOUND TYPE ( , ) LI ) ~fW ,fr,~ ppm ~b ppm_i CHLOROMETHANE JO II I A VINYL CHLORIDE 10 BROMOMETHANE ~o Clll.ORO!:THANE 10 TRICHLOROFWOROM!:l'IIANE ,o ' V ACETONE ;1.0 ;;l. 3 1.1-DICHLOROETHEN!: 5 /J IODOIBTHAln'! .... 1 METUTLZN!: CHLORIDE I :sl c.... CARBON DISULFIDE /I TRAl'l'S-1,2-DICHLOROETHEN!: ,/ ACRn.ON?TRILE ~ l, l·DICHLOROETHANE 5 2-BUT ANON!: :io CIS-1,2-DICHLOROETHENE 5 "I ' I/ CHLOROFORM +rnre~ l.ln 1.1.l·TRICHLOROETHANE IL 11 CARBON TETRACHLORIDE BEl'IZEl'fl: 1,2-DICHLOROETHAN'E TRICHLOROETHJi;lfE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE ,v ,v '\ I c -POS!tr~~ LA r-; c-ol'!,A~tN F\Tic ~ o" B,:io:.6-P-c--,...__i c. J -Estimated value X -Actual value i■ known to be le■■ than value given. L -Actual value i ■ known to be greater than value given. ":5 q,J'-/-4-I oiooqq ( I ) / ppb ppm I 1 -V 19 f 1 t t ::r, c...., I ' " I rr-s I ...t lj 11 - ...., l Q?/ Lf4.:l.. 97/Lf'l-3 ;20100 cJ.O 10 I L / ) ( I ) 'ppb}pm lppb}ppm_ , ,f I l - , \I l j,c... I 1 ,/ -h""fl ('(~ - i l _/ "I ,v 0 -Material wa■ analyzed for but not detected. The uumber i■ the Minimum Detection Limit. RA -Not analyzed. 1/ -Tentative identification. ~I -CCMPo\lf!lD RW P!6L'f OE.Tl:Cr-R6U:. OHU( IN I-Hett CCNc.£NTR!ITTc:N$, ✓ -S~PLa t-t1'4tL'f PILIA.T~o. ~DL.t~ 00 1"k'T"' AfPLf. ([J q7 I lfLfLf ;20 /Del ( , ) (PpO}ffJtT? 11 -• ,v PURGCOM.ORG DEHNR 3065-0 (10/93) -11-·,soprcp<-tl aicohol +en+Cl-"t/vely iden+i'+ied STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WlllONGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q,,43Cf C,'7 I Lf-4() q7 14-4-1 q114-4-J. q?/l-/'f3 FIELD NO :2()()9? ;woqe c:2ooqq c:20100 ;2010/ COMPOUND TYPE ,,.-:b,._ ( ) ( ( ) ( , ) ( I ) L / ) i,sg~.!> tppb)ppm (ppllj f' pn, (pp~ pp,ti {pp~ f Prn l(n;ti)ppm DIBROMOMETHANE 5 Lf fl_ I J I ' 0....- 4-METHTL-2-Pl!:NTANONE JO CIS-1,3-DICHLOROPROPl!:NE J:. ,/ '-' TOLUENE +-rnrl" TRANS-l,3-DICHLOROPROPl!:?a IL- 1,1,2,2-TETRACRLOROETBAl'fE l, 1,:2-TRICRLOROETHANE ,I ,/ 2• HEXAl'l'O?a JO +r-ar~i/ TETRACHLOROETHl:NE .5 U- DIBROMOCHLOROMETHANE ETHYLENE DIBROMIDE CHLOROBENZENE 1,1,1,2-TETRACHLOROETHANE ZTHYL BENZENE XTU:NES STTlUNE ,/ BROMOFORM 10 TRANS-1,4-DICHLOR0-:2-BUTENE go 1,2,3-TRICHLOROPROPANE -5 \/ 1,4-DICRLOROBENZENE +rnrio ~ 1,2-DICHLOROBENZENE ~v u_ l,2-DIBROM0-3-CHLOROPROPANI!: ~() VINTI, ACETATE ;J.00 \I \I \I/ ,; \V c -fOS"!Met.E &rAa ~11-,lf\1'\0tJ oR J -Estimated value 0 X -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The number is the Minimum. Detection Limit. NA -Not analyzed. 1/ -Tentative identification. i, -coMPou.r-i o R~l-1,:1e1..y D61EcTf\8LE CIJt.Y ,~ H•G-H co~c£/'ll~,~s. ✓.,. ~MPLE 1-f \fiij l'( 01 l.~T€D, MW-s Do ~ (WPL'f. DEHNR 3068-0 (10/93) q7 llf'fi./- ;;a J O ;;J_ ( ) ) (ppb}ppm /A_ \ I PURGCOM.ORG ---STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047-306 N. WILMINGTON ST •• RALEIGH. NC 27611 ORGANIC C.HEMlCAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q?/4'-1-5 91 J4Lf& FIELD NO c:20103 .1010 lf COMPOUND TYPE ( ' l C I l M~r;'f C;>l'b ~pb)ppm 1-i,b ppm_ CHLOROMETHANE JO I.(_ 11 VINYL CHLORIDE 10 BROMOIIETHANE ;tO CHLOROETHANE 10 TRICHLOROFLUOROM!;'I'H.A.NE ,o ' I ,v ACl!:TOlm ;J.O Hos 7 "°;lJ ('.., 1.1-DICHLOROETBENE 5 I 1 -/ .,A._ IODOKETHAll'I: IBTHTIZNE CHLORIDE CARBON DISULFIDE TRANS-1,2-DICHLOROETHENE ·V ACRTLONITRll.Z I -~ l .l·DICHLOROETHANE I 5 2-BUTANONE I ;io Cts-1.2-DICHLOROETHENE 5 CHLOROFORM 1.1.l·TRICHLOROETHANE CARBON TZTRACHLORIDE BEl'IZZNE 1.2-DICHLOROl!:THA?fE TRICHLOROl!:TH.cl'(E 1.2-DICHLOROPROPANE BROMODICHLOROMETHANE ,'J '\ ' V - . C -P~l i'?4! L.,·, B C'C)N':-'f,i',\/f-0'-TiC ~ OK B,K ~c,-P-c--1'.i c . J -B■timated value X -Actual value is known to be le■■ than value given. L -Actual value is known to be greater than value given. I I 91 I 't'f7 ;)_{) 105 ( I l /ppb ppm 1.A- \/ 91/'-1-'f§ 97/J.f'-19 ;2.0 /0 {.p ~OJD7 (_ I l ( I l !(;Jpb)pprn l(ipb)pprn_ I 1 -fl 'v' +racP c , t ~ ,I \ I/ U -Material was analyzed tor but not detected. The number ia the Minimum Detection Limit. 111A -Not analyzed. 1/ -Tentative identification. "%_1 -ca~PO\oU~D Rai l"e1..·1 OeTECrf\61..f. ONU( IN fH6-i-l Cctl/c.£NTRIIT7cNS, ✓ -SMPL6. HI '1-½L'f DILkTI:.O, ,..01..'~ Oo ~ f+f f>Lf. DEHNR 3065-0 (10/93) 971450 ~108 c I l /ppb )ff)n-1 u - I I \v PURGCOM.ORG ; STATE IABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO 9714'-/-5 9 7/t/4~ 9 '7/'-/'f7 q'1J 4Ll-8 971 4--¥/ FIELD NO ;}.0/03 ;lOIOLf-~OIDS ;20/0~ c:20107 COMPOUND TYPE ( ' ) J_ , ) ( I ) (j ) ( / ) n~~:s /ppb ppm /pp~ ppttl p;;ri)p~ fpb)pp,n F1Ji7ppm DIBROMOMETHANI!: 5 LI--{.1 -,, u -u..- 4-METHTL-2-PENTANONE JO CXS-1,3-DICHLOROPROPENE ~ -.., TOLUJ!:NE TRANS-l,3-DICHLOROPROPENE l, l,2,2-TETRACHLOROETBAm; l, 1,2-TRICHLOROETHMJ.: '\v 2-JmXAl'fONE JO n:TRACHLOROETHJtNE -5 DlBROMOCHLOROK!:TRANE ETHTUNE DIBROMID!; CHLOROBl:NZEJ'f!: l, l, l ,2-n:TRACHLOROl:THANJ!: ZTHYL 3?::'!Zl!:NE nu;~ STTREN!: ' V BROMOP'ORM 10 TRAlffl-1,4-DlCHLOR0-2-BUTI!:NE <to 1,2,3-TRICHLOROPROPANE 5 1, 4-DICHLOROBl:NZ!!NE I 1,2-DICHLOROBl:~ ~ 1,2-DIBROM0-3-CHLC>ROPROPANE: d.0 I VINYL AC!:TATI'; a.oo 'V ,/ \,/ '\. I ,; . C-f~~i~ LAS ~lt,l(-\1'\0._i oR BA«GKo~l). J -Estimated value ~ -Actual value is known to be leas than value given. L -Actual value ia known to be greater than value given_ cr -Material was analy-,:ed for but not detected-The number ia the Nini.mum Detection Lilllit. ID. -Not analy-,:ed. 1/ -Tentative identification. i, -ccMP01.i.r-iv Rft.1~e1..y De•ECf~SLE C#Jt.Y '" HU7H cot,tef1'TAAT',a~s. ✓ -SAMPLE H\GWty 0l'-4Tt0, /-14>U~ Do >Jot Rf'PL'f. DEHNR 3068-0 (10/93) 911'-f50 ;;w JO'is ( f ) (fpt ppm U- ,/ PURGCOM.ORG ----STATE IABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q7145 f 91145:1._ FIELD NO ;J.0/0q J.0/10 COMPOUND TYPE ( J ) ( I ) MD~ (ppb lppb ppm ~b ppm CHLOROM!:THANJ!: JO LI ~ I I VINTI. CHLORIDE 10 BROMOIIETHAlfE ;io CHLOR0.1!:THANE 10 TRICBLOROFLUOROMl!:THANE ,o ... I/ ACl!:TOlff: ;J.O 3 J",C- l.l•DICBLOROl!:THl!:N'l!: 5 IL- IODOJa:THA1fE KETHTU:NI: CHLORIDE CARBOI' DISUl.FIDE TRA!'IS-l,2•DICBLOR0.1!:THEN.I!: ,/ ACRYLONlTRllZ I ~ l, l •DICBLOR0.1!:THANE 5 2-BUT.Al(ONE I :i.o CIS-1,2-DICHLOROl!:THENE 5 CHLOROFORM l. l.l• TRICBLORO!:THANE CARBO!{ Tl!:TRACBLORIDE 81!:ll'Z!:NE 1.2-DICBLOROl!:THAl'IE TRICBLOROl!:"I'RBfE 1.2-DICHLOROPROP.Al(E BROMODICHLOROMl!:THANE ,/ \ I ,I -C -P05!>{;,~ L.;; i? C"ON -:-f,i"l /f'IF'tiCll,I; O~ 0 1-KK.CrKC-l'\.i D. J -E■tilu.ted value X -Actual value is known to be le■■ than value given. L -Actual value is known to be greater than value given. q7Jl-f53 c).OJ/1 ( r i 15P6)ppm I 1 I "'I 97l'f6J./-911465 c).. 0 /),;)_ ;2D JI 3 ( ) ) ( , ) ('ppb]ppm ·ppb)pprn, 11 i L \/ ../-r-11,~ I A~ \ ·, I U -Material was analyzed for but not detected. The number i■ th• Minimum Detection Limit. IIDI. • Hot analyzed. 1/ -Tentative identification. 11 -COfo\f'o'-l'51D RUA P.E;L"f 0E.TEC"l'\6L£ oH!.¥ ,N fHcH CcflJc.£1'irRflT1cNS. ✓ -S~PL&i H1'1-¼L'f OILkTE.O, ~OL!~ Do ~ f+ff'L(, 97I45/p ;;uJ I I 'f ( I ) ~pl:: R='rr? i I _/ '\/ --1-r-nrP c... • 1 - '11 I :r,c.. I ~ I I I ' ( PURGCOM.ORG DEHNR 3065-0 (10/93) ...JL.,.. \ + + _J , \'"I ; de v1f,'·',,'°'~. ~· l5opro~ \ a l coho en w-, Vl Y , , i-, \,o . ------~ ' I STATE IABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILJIINGTON ST .• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABIZ COMPOUNDS LAB NO C/?l'-1-5 I 971'/-SJ._ C/71'+53 9,1454 q7J'f55 FIELD NO .;Jo ID9 ,;20/10 ;lo I I I ;}__QI I c:;;2 .201 )'3 COMPOUND TYPE ( \ ) ( , ) ( I ) ( I ) ( I ) r;,o~~ pt:b lppb)ppm /ppb ppn1 fpB)pptti fr~pp,n ~ppm DIBROMOMETHANE 5 LA--U-u.-LA--LA- 4-MJ!:THTL.2-Pl!:l'ITANOl'rE JO CIS-1,3-DICHLOROPROP!!:l'rE J: ---., TOLUJ!:!'1: TRANS-1,3-DICHLOROPROP!!:NE l, l,2,2 -'n:J'RACHLOROETHA!O!: l , 1,2-TlUCHLOROE"I'HM!: ... v 2-HEXA!{ONE JO T!:TRACHLOROETB!:!'1: ,5 DraROMOCHLOROIU:THANE ETHYU::-r!: DIBROMIDE I CHLOROBENZEN!: l, l, l ,2•T!:TRACHLOROETHANE ZTHYL 3!::l'Zl!:NE ::rTUN!:S ~ ' I BROMOFOIUI JO TRAlfS-1,4-DICHLOR0-2-BUTENE io 1,2,3-TlUCHLOROPROPAN!: 5 1,4-DICHLOROBENn:NE I 1,2-DICHLOROBENZ!:NE ~ 1,2-DIBROM0-3-CHLOROPROPAN!: d-0 VINYL ACl!:TAT!: a.oo \ I \V '\ / ' '/ ... V . C -i5'o5Si~ LAS ~~U-l ;'f\O~ oR J -Estimated value ~ -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. ~ -Material was analyzed for but not detected. The number is the Minimum Detection Liait. lllA -Not analyzed. 1/ -Tentative identification. i, -ccMPou.,~ <> Rf L.1~0LV oeTEc.T~eLE OIJLY ,., H~H col'lC£1' ~,a~s ✓ -~MPLe HI GW LY 01· LkTEo , ftil>U~ Do ~ "fWPL'f . • DEHNR 3068-0 (10/93) q 71'-/-S&, ;J 01/ L/- ( I ) Vp pt) ppm Lt \/ PURGCOM.ORG --srATE LABORATORY OF PUBLIC HEALTH PO BOX 28047-306 N. WILMINGTON ST .• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS 1'-- PURGEABLE COMPOUNDS LAB NO q 71 4-57 q,11'-158 q 11 45Cf q'7 I 'f ~l ~Cf? llf-CD I FIELD NO ;;l0/15 ;2.0 II (p ;)..O/l 1 ;2.0 ll<t' ;:20 /19 COMPOUND TYPE ( I ) ( I ) ( I ) ( 1 ) ( I ) M~6f ~ppm( ,,---,,,- ~b ppm (pp b)ppm /pp b)ppm_ (;>l'b f¥1b ppm 1 CHLOROME'l'HAN!: JO iA LA--L,L.. u__ ( J VINYL CHLORIDE ,o BROIIOIIB'I'BANE .;io CHLOROETHAl'flt ID TRICHLOROP'LUOROia:TH.Al'fl!: ID '\ I/ '\ I ACl!:TOlfJ: ;J..O +-1 c.. l"nf'P +r"ac.e, l. l·DICHLORO!:THENE 5 IODOIIETHA!fE IIETHT1.El'fE CHLORIDE CARB01" DISULl"IDI!: TRAN'S-1.2•DICHLOROl!:THENE ,V ACXTI.ONI'I'RIU: ~ l . l-DICHLOROl!:TH.ANE !5 2-BOTANONE ~o CIS-l.2-DICHLOROl!:THENE s CBLOROJl'ORII l. l.l· TRICHLOROETHAN!: CARB01" TETRACHLORIDE B!:1"ZENJ: l.2•DICHLOROl!:THA1"E TRICBLOROETHea; l .2-DICBLOROPROPANE BROIIODICHLOROMl!:THANE ,[/ \ ,V c -r~,~~ L.., r-; c-oNT;;;,,qr-,iP.,;c~ OK B,.:io:.l'Kc -"'-i c. J -B■tuiated value X -Actual value i■ known to be le■a than value given. L -Actual value i■ known to b• greater than value given. I l I I I ,1 '\ / U -Material was &n&lyzed tor but not detected. The number ia th• Minimum Detection Limit. ID. -Hot analyzed. 1/ -Tentative identification. "%./ -COMPOl.l~O Ra-4 f'eL'f OE.TECll'\6U:. ON~ '"' fHcH CCNc.E:NTT<IITTcNS, ✓ -SAAPLa Hl'1-tl..'f OILLlTE.D, ~01.,l~ Do N0r f+f f'Lf. . LL- .., V '- (j) q 714/.Q;;. ;}..0/U) ( I ) (ppt:) ff)rr/ I l _ ,I +r-r1r,-. C. u__ I ,f DEHNR 3065-0 (10/93) '-¥--156f)rap'1 I CUccih O ( +e n+ct+i VE' 'Y ·,ckrrhi,e~GCOM.ORG ! ' STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILJIINGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO 97/'-I 5 7 q,/'f58 FIELD NO ;20/15 ;;lO I I lo COMPOUND TYPE c I ) ( I ) /?,~~~ (ppb)ppm , ~pl, ppn1 -DIBROMOMETHANE b fl__, f.A. - 4-METHTL-2-P!:NTANONE JO CIS-1,3-DICHLOROPROPJ!:NE ;:: '-./ TOLU!:lf!: TRANS-1,3-DICHLOROPROPJ!:NE l. l ,2,2-T!:TRACHLOROETBA!f!: l. l.2-TRICHLOROETHA:a: -.1/ 2-HEXAll'ONE JO T!:TRACHLOROI!:THJ!:lf!: -5 DIBROMOCHLOROIU:I'HANE l!:THYl.E:'f!: DIBROMIDE CHLOROBENZEl'JE l. l ,l ,2-T!:TRACHLOROETHANE ZTHY1. 3~22:'fE J::YU!f!:S STTRE1'f!: ,/ BROMOFORJil 10 TRAlffl-l,4-DICHLOR0-2-B'O'TENJI: io l.2.3-TRlCHLOROPROPAN1: 5 l , 4-DICHLOROBENZ!:NI!: I 1,2-DICHLOROBENZENE ·~ l,2-DIBROM0-3-CHLOROPROPAJa d.0 VINYL AC!:T ATE dt(.)0 \ \( c -f'~<!>i~ LAa ~,t-1r-rnotJ oR 0 J -Estimated value ~ -Act ual value is known to be le•• than value given. L -Actual value is known to be greater than value given. U -Material was analY%•d for but not detected. The number is ID. -Not analy:ed. 1/ -Tentative identification. 1, -ccMPou.r-iv Rf LIP.BL'I DcTi:cr~e,L.£ CfJt.Y ,~ HU7H ✓-SPIMPLE HIG~ty 01·~~0, Ml>t.>s Do ~ Prf'PL'f . DEHNR 3068-0 (10/93) 1'7 J'f-59 q,1 %1J C/71'-flol ~D/17 ;lO//B :20//Cf ( ' ) L.J ) l I ) 1/ppb pprr, 'ppb' pprn ~o)ppm u._ fl_ __, ~I/ 3:J LA- \ V +rn r" I A - ,V ,V the Minim.um Detection Lilait. q714w._ ;201 ;w ( I ) (ppt)ppm I I I PURGCO.M.ORG ---STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 • 306 l'f. WILMil'fGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PVRGEABU: COMPOUNDS LAB NO q7 l'--/-t.P3 97/L/-f.p'f q11Jfti;5 q 714t.of.p FIELD NO ~JJ.I :J..01~ ;}_o J;B d-01 J.tf COMPOUND TYPE ( / ) ( , ) ( I ) ( ' ) ( ) M~~ (Pl'b <PP~ ppm ~Jy ppm lppb ppm ~ppm ppb ppm_ CHLOROMETHANJ! JO Lt~ I 1 /1 ~ v.- VINYL CHLORIDE ,o BROIIOIIO:THANE ~o CHLOROETHANE 10 TRICHLOROFLUOROK!:THAJ'(!; ,o ,I ,/ ACETOR ;2.0 +,a,-e.. c.. +-. C, f{'}t"e, l, l •DICHLOROETH!:NE 5 '"'"~ i .1._ IODOKETHA!R: i :aa:nrnzNE CHLORIDE ~ :S1C... CARBON DISULFIDE , J TRANS-1.2-DICHLOROETH!:Nl!: ,✓ ACRn.ONITRIU: .;20 l , l·DICHLOROETBANE I s l-BUTANONE :i.o CIS-1,2-DICHLOROETHENE 5 '\ CHLOROFORM /,Ci:, s l, l,l•TRICHLOROETHAN'E ; J CARBO!I TETRACHLORIDE BE!IZ!:NE 1,2-DICHLOROETHANE TRICHLOROETHefE 1,2-DICHLOROPROPANE BROIIODICHLOROMETHAN'E ,/ ' I \ I ,v "'v -c-POS!>r "ya L-,B c-o"'-:-,:-,,,,q l'-IRTic~ o" o ,;ic,::.'-"~c--1\.i C . J -Kati.mated value X -Actual value is known to be le■■ than value given. L -Actual value is known to be greater than value gi-ren. U -Material was analyzed for but not detected. The number i• th• Kini.mum Detection Limit. 111A -Not analyzed. 1/ -Tentative identification. I,1 -CCl'-\P0'-1.~D Rw P-eL'( 0E.TEC~6L£ OHC( IN fHc-H CcNc.£N~cNS. ✓ -Si¥1PLa t-11'1-tl.'f 01L1A.TE.o, ~OL.'~ Oo ,-k,T"" APPL'(. DEHNR 3065-0 (10/93) ( ) ppb fPfY1 I PURGCOM.ORG ---STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q114(.p!) q114-w '-I q 7 f Lfu,5 q ?J%(p FIELD NO ;20 J;lJ .:2.()/.;2,;1. ;}_()J;).3 ;J.O I :2 J./- COMPOUND TYPE ,1.__ l ) ( J ) ( I ) ( I ) ( ) M~S)-, ('ppb lpp ~pptn ~Jvppm Vppb',)pm /ji@Jppm ppb ppm, CHLOROIIETHANE JO Lt~ ll VINYL CHLORIDE 10 BROIIOIIETHANE d.0 CHLOROETHANE iO TRICHLOROFWOROIIETHAl'fE ·o I , ACETONE ,;io l,l-DICHLOROETHENE ;::: ..... 1 IODOIBTHA!fE 11!:TBYLENE CHLORIDE CARBON DISULFIDE TRANS-1,2-DICHLOROETHl!:NE ~ ►7 ACR!LONITRIU: :;IC) 1, l•DICHLOROETHANE ,::::- .J 2-BUTANONE ;LO Cis-1,2-DICHLOROETHl!:NE 5 CHLOROFORM l,l,l·TRICHLOROETHANE CARBON TETRACHLORIDE BENZENE l,2-DICHLOROETHAl'll!: TRICHLORO~ l,2-DICHLOROPROPANE BROIIODICHLOROIIETHANE ,/ ,, "I C -pc,::,..,,"...;;,: .... B <'...:..N TAi''H N ATiO ~ ,::" B,:ic.K.6-KC ... "-.l D. J -Kati.mated value X -Actual value i■ known to be le■■ than value given. L -Actual value i■ known to be greater than value given. I l. -LA.- ,1/ "I / U -Material wa■ analyzed for but not detected. The number i■ th• Ninillll.Dll Detection Lim.it. RA -Not analyzed. 1/ -Tentative identification. 11 -coMPo\ol.r!D Rw l"\i}L"f OE.Te:::rABl£ oHCf 1N EHeH CCNC£NTRIIT1cNS. ✓ -SAAPL~ H1'4½L'1 01LL1.T1:.o • .MDL!~ Do r,k,'r"" APPLY. DEHNR 3065-0 (10/93) ( ) ppb ,::prr, PURGCOM.ORG • 1I • I ... . ,.I • ' . I, / .. , '1 , ,i 1+i t ·1 I . ' 1, j, ' . . ~ .. ,, . . . .,. _,· . j' ., . I i ~ , • I •. ,! ·-' f 1' # . I r I ., 11 . ' .. i ,. . j ,I 'I .... ' < j • ,. t ·1, ·1 l-lt f. 4 . , . .. , ~-.: • r ~-\ I ,. --. • . . , I ,r .. , ' . '" . ' I < ~ ..... ~.,◄• ~ ·.,. ,, - I, t j. ~ t r, • .. . . ... ~ , : ., \ . -. . ... ' t; I ·. ., i f•.:. . .. •• .. ., J.:a ·;· .. .i1 ! , " ~ ~ .. _j '. ,, . It• ,, 1 ~~ .. I• '., t .. • '>! ' ~ , Ff"·: . _, ,· ! {_ ., -◄ a. .. "1', i,.. t' ,· t:.,.. . "-J1 ~ ..... i. -I .• ' . ' t .: • r.. "" . . ~ ·, ~-I . / \, ;. . . . :'t•jl :~ . (~ I' 11 ..... • I •I . 11j:"j .. .,. -,.·~. ~ .l ' ' . , ~N.C. Def-'3rtment of Environplent, I lcaith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratoiy of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ____ ___, __________ Field Sample Number ___ C}_(--'Cj'_'l_2..__,_/ _______ _ \ Site Location Name of Site_-=W'-=-AA"-"--'R_€AJ_· ---'--; .c=0Jc.=.:cJ::.L;t/~71/....._ __ ------------------- Collected By ----------ID# ___ Date Collected 3 •-' / 1-q I Time _____ _ Agency: Hazardous Waste Solid Waste /superfund TCLP Compounds Sample Type Environmental Concentrate Comments __ Ground water {1) -v/Sotitt(S) P)S 1 _ Surface water (2) _ Liquid (6) ___________ _ ~ Soil (3) Sludge (7) _________ _ _ Other (4) _ Other (8) __________ _ Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE 5 r~d? _J£ RE-< 1 1112 lz': ]l@S::~ Results(mg/1) Radiochemistry Inorganic Chemistry Parameter Results(mg/1) (mg/kg) Arsenic Barium Cadmium Chloride Chromium __ Copper Fluoride Iron Lead __ Manganese Mercury --Nitrate Selenium Silver Sulfates Parameter Zinc Results (PCi/1) _ pH __ Gross Alpha Gross Beta ------- Microbiology Parameter Results (Col/lOOml) Date Received 3 -I J..-CJ 7 13£2 Pei$5- D.ile Extracted 3-dZ0-9'7:J/P l'CBs- __ Conductivity ______ _ TDS TOC R Inorganic Compounds Arsenic Barium Cadmium Chromium Lead Mercury --Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol --cresol 1,4-dichlorobenzene 1,2-dichloroethane --1,1-dichloroethylene 2,4-dinitrotoluene __ heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane Results (mg/I) Results(mg/1) ------ ------ ------ ------ methyl ethyl ketone --nitrobenzene ------ --pentachlorophenol = pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ --vinyl chloride --endrin lindane methoxychlor __ toxaphene 2,4-D _ 2,4,5-TP (Silvex) D.itc AnalyLcd3 -~zyp DI IS 3191 (Revised 2/91) ti-<f70'i67-c; 7ozrf~-------- • N.C. Department of Environment, I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number eJ l q q 1-L ----~-------------------------- Name of Site l.»trR/{e-tl/ Cu-it1 rt Site Location ------------------- Collected By ----------ID# Date Collected .3 -l (--=t, Time --------~~-~--------- Agency: Hazardous Waste Solid Waste /superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- .B R ( Barium --=.2<.5olid (5) --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- ✓ Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results ( mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane x ·.#NA-o/12 ----Chloride chlorobenzene ----✓ it~ <".Io s:vJAf. Chromium chloroform ~ , , ----__ Copper o-cresol --Fluoride m-cresol ----Iron __ p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----····••·-••--· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- 3 ,,.,J--97.i£J lindane Date Received Reported by = methoxychlor Date Extractc~"t.0 -977/,P __ toxaphene Date Reported --2,4-D d)Ces r,-1 n~Sl _ 2,4,5-TP (Silvex) Dale AnalyLed .3-~-97-VP Lab Number .._. ,-~-W -..JU --DI IS 3191 (Revised 2/91) • N.C. Department of Environment, I lcalth, & Natural Resources So!id Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ---------------Field Sample Number CJ I C\ '1 ·L~ ---------------- Name of Site __ l)~A: ...... A_..._.R, .... '1;3'-'-W...___t:.---'-u_l'li_· __ r ___ v __ Site Location ------------------- Collected By ----------ID# Date Collected 3-1 f -4 I ----Time ------ Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ·--"' 0 <solid ( 5) B tt B-l Barium --__ Groundwater (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- JL Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --PcB ----_j£_ < O , I Q-fl!L!t Chloride chlorobenzene ----Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol --------__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2, 4-dinitrotol uene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··---Zinc hexachlorobutadiene ----Results (PCi/1) Par-ct meter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -I J.--9 7 18/.1) Reported by = methoxychlor tPeB.s __ toxaphene Date Extracted ,3-.-'<0-97i/f' Date Reported 2,4-D tf'f!8s 0704-:-.,(;9 = 2,4,5-TP (Silvex) Dale AnalyLed 3 -~27Vf' Lab Number ....,. u .,, --DI IS 3191 (Revised 2/91) , N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----.-----------Field Sample Number ___ 0_1_9_Cf-·~z__L/ ______ _ Name of Site uJ IJ1UJJZil ~!LIT:/ Site Location ------------------- Collected By ----------ID# Date Collected y / (-17 Time ---------~--'-~----------- Agency: Hazardous Waste Solid Waste ✓ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ' CE ) --__ Ground water (1) .,-. v Solid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- ../ Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------..L e~ < (). IO {12./r\... Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium __ 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·•-·-•-Zinc hexachlorobutadiene ----Pardmeter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- Date Received .3-lol -1 7 /J £, lindane --Reported by __ methoxychlor /'al!"'-__ toxaphene Date Extracted 3-.:?O -?7Vp Date Reported 2,4-D PCB~ n-00 · = 2,4,5-TP (Silvex) .... ;' 0 70 Dat e AnalyLed 3-::2S'-97VP Lab Number --DI IS 3191 (Revised 2/91) .N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ 0~-_.I ..... Cf .......... c:r_L=-Y'-_____ _ Site Location Name of Site &J frtB, ~ ll/ lavvvry Collected By ------------------- ----------ID# Date Collected J ~ ( /-Cf., Time ----------==-'-'---"----------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- 13 J -I Barium ' --__ Groundwater (1) .-=-v Solii:f.( 5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- /soil (3) Mercury Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results ( mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane 2 pc..e, < 0 ,, / I) DDnt ----Chloride chlorobenzene ----, , Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----·······-··---Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride -endrin -- Date Received 3 -J,).. -9 7 B £J lindane --Reported by __ methoxychlor tflaB"f __ toxaphene Date Extracted 3-~d-f'7f P Date Reported 2,4-D Pe.i" ~70t.~71 = 2,4,5-TP (Silvex) Dale Analyzed 3-~9 71,/P Lab Number --DIIS 3191 (Revised 2/91) . N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O) t:t1 Lb ------'"-'--'-~--'-'""------------------------- Name of Site W frf,.P.,,t::'W ~ rt,( r( Site Location ------------------- Collected By ----------ID# Date Collected -:1, -/ /-? 7 Time -----------''--'--'-........... ----------- Agency: Hazardous Waste Solid Waste _JL.._Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- I f<p -Barium ) --__ Groundwater (1) ·--V Sofic.=(5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- ✓ Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results ( mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --()L/:, ----.JL_ <o, l•ffJ111. Chloride chlorobenzene ----Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··--· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -1.;.-q 7 sJJ Reported by = methoxychlor (Pl!L1~ __ toxaphene Dale Extracted 3--2. d -"97Yp Date Reported 2,4-D ~~ ~70872 = 2,4,5-TP (Silvex) Dale Analyzed~,R!;f-92:VP Lab Number --DIIS 3191 (Revised 2/91) .N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O I '1 '1 1. < ---=--'----------------------------- Name of Site l,; trf.. A.,elV ~I,./ IV rt Site Location ------------------- Collected By ----------ID# Date Collected 3..,, //-17 Time -------'"-"---------------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ( fYlBB-\ Barium --__ Ground water (1) "-=v Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- _!soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane _L P?f) <P•/Of12m,, ----Chloride chlorobenzene -----,-Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··--·-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -1,).-C) 7 /]A) --Reported by __ methoxychlor ~~ __ toxaphene Date Extracted -.:i.t:J-9711,/ P Dale Reported 2,4-D Peas-:)70373 = 2,4,5-TP (Silvex) Dat e AnalyLed 3-.;J..S-97'VP Lab Number --DI IS 3191 (Revised 2/91) ·N.C. Department of Environment, I lcalth, & Natural Resources Solfd Waste :-tanagement Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ O~l _q__.1_"l-____ '2:" __________ _ Name of Site tJ 4'-V'~ ~•'V rt Site Location ------------------- Collected By ----------ID# Date Collected i -C,/ -~I Time -------------------- Hazardous Waste Solid Waste ~ TCLP Compounds Agency: ----__ Superfund Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium sB-1 --_ Ground water (1) ,_::..... v ' Solid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- ✓soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --Pc.B <o-7~,zi ------1L.. Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Results (PCi/1) Par.,meter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received 3 -;J C/ 7 AdJ Reported by = methoxychlor (l,)l!.8~ __ toxaphene Dale Extraclcd 3-~-'/71/,P Date Reported 2,4-0 Dale Ana(!lf~-:J...S-9?VP Lab Number !;70874 = 2,4,5-TP (Silvex) --DIIS 3191 (Revised 2/91) . N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ C,_)_'1_j ____ ~_q,__ _____ _ Name of Site /4) <& r-1<-Y\. C....,../\-fy Site Location ------------------- Collected By ----------ID# Date Collected "") -ti -Cl 7 ----Time Agency: Hazardous Waste --Solid Waste --✓superfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- R, s·t I Barium ✓ Ground water (1) --_ Solid (5) Cadmium -- ;;-VL Uqllid (6) Chromium --__ Surface water (2) Lead --Mercury Soil (3) Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane z Pc£> <0,(1QO~ ----Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ----= p-cresol Iron ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2, 4-dinitrotol uene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-·-·-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology __ tetrachloroethylene ' ----__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -1~-q 7 6 £J --Reported by __ methoxychlor <Pee s-__ toxaphene Dale Extracted 3 • /? -9 7 J/5'JM Date Reported --2,4-D 1-'f!S s-n.7007r:-_ 2,4,5-TP (Silvex) Dal e AnalyLcd 3-/9-971/P Lab Number ..... u J --DIIS 3191 (Revised 2/91) -N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ______________ Field Sample Number __ CJ_j'"""~-q-~.a......-0'---______ _ Site Location Name of Site uJ fr/Jf{t;:;ltj 4 ,.nv ft( Collected By ------------------- ID# Date Collected '3 -t/-97 Time -------------------- Agency: Hazardous Waste Solid Waste r Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- V Ground water {1) ~ rt B-1 Barium --Solid (5) Cadmium -- -~< 6) Chromium --__ Surface water (2) Lead --Mercury _Soil {3) _ Sludge (7) --Selenium --Silver --_ Other (4) Other (8) -- ----Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --P<A ----...\L <D, cltJO/ ppm Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··--· Zinc hexachlorobutadiene ----Results (PCi/1) Pardmeter _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -/ ,)--<; 7 Jdil" --Reported by __ methoxychlor Dale Exlraclc~-~~-97-VP __ toxaphene Dale Reported --2,4-D Pees-0 -0,--,..-.,6 _ 2,4,5-TP (Silvex) Date AnalyLcd 3-/9-?71/P Lab Number v If' 01 --DI IS 3191 (Revised 2/91) -N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ _,_l _q_.__4,_· ..... 7>_J ______ _ Name of Site /4J A-'AA-C:ltl Cv{oJ:[1/ Site Location ·------------------- Collected By ----------ID# Date Collected ) ..,,l I-91 Time ---------'-'---'---'----------- Agency: Hazardous Waste Solid Waste /superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- /Ground water (1) KB -/ Barium --_ Solid (5) Cadmium -- ..;;=. v /Liqoiti (6) Chromium --__ Surface water (2) Lead --Mercury _Soil (3) Sludge (7) --Selenium --Silver --_ Other (4) Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results ( mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ..JL PLB ----<tJ •IJPPlffM Chloride chlorobenzene ----y-Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol --------__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··--· Zinc hexachlorobutadiene ----Parameter Results (PCl/1) _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -I). 4 7 /9tQ --Reported by __ methoxychlor Date Exlrac~Cj!/ ?-'l._7i/P __ toxaphene Date Reported 2,4-D Pee} 0""'1(]rt7 f-1 = 2,4,5-TP (Silvex) Dale Analyzed 3-/9._-2_7-VP Lab Number .... " u ' --DI IS 3191 (Revised 2/91) ·N.C. Department of Environment, l lcalth, & Natural Resources Sul_id Waste ;>1anagement Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number ____ O=-_l :f_.__9.__3_2 ______ _ Site Location Name of Site lJf1;Pj?,(£1L/ c;v/Jl['f ------------------- Collected By ID# Date Collected ") -f ( -q ·7 Time ------------------------------ Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments i/ Ground water (1) Solid (5) __ Surface water (2) _Soil (3) _ Other (4) Organic Chemistry Parameter P&T:GC/MS L Acid:B/N Ext. MTBE E ~ A Results(mg/1) Radiochemistry Parameter __ Gross Alpha ____ .__ __ Gross Beta Microbiology Parameter Results (Col/lOOml) Date Received .3 -/ .t-c; 7 I:]£ Date Extracte<l.&1fA .3-1,l.-"i' 7 Bil Chromi Coppe --Fluo ·ae Selenium Silver Sulfates Zinc _pH __ Conductivity ______ _ TDS TOC Reported by ________ _ Date Reported _______ _ Date Analyzed Lab Number -----------------DI IS 3191 (Revised 2/91) TCLP Compounds Inorganic Compounds Arsenic Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol --cresol 1,4-dichlorobenzene 1,2-dichloroethane 1,1-dichloroethylene 2,4-dinitrotoluene __ eptachlor h chlorobenzene hex Results(mg/1) Results ( mg/1) ------ ------ ------ hexacti roethane methyl e I ketone --nitrobenze ------ --pentachloro enol __ pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ --vinyl chloride --endrin lindane --methoxychlor = toxaphene 2,4-D _ 2,4,5-TP (Silvex) N.C. Department of Environment, I lcalth, & Natural Resources Soli_d Waste ~anagement Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ o_;_q~9~3_3 ________ _ Site Location Name of Site V AR Rlf)J' Cut,...rry Collected By -------------------- ID# Date Collected Time --------------------------------- Agency: Hazardous Waste Sample Type Environmental Concentrate _L Ground water (1) __ Surface water (2) _Soil (3) _ Other (4) Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE Results(mg/1) Solid Waste __ Superfund Chromi Coppe --Fluorl le Comments i~;;.:~ese elenium t-----------------t Iver Radiochemistry Parameter __ Gross Alpha Gross Beta Results (PCiJ Microbiology / Date Received .3 --j.,l-9 7 ~~ Sulfates Zinc pH = Conductivity ______ _ TDS ,--TOC Reported by ---------- Date Extracted Date Reported ------------------~70879 Dale Analyzed Lab Number -------------------DIIS 3191 (Revised 2/91) TCLP Compounds Inorganic Compounds Arsenic Barium Cadmium Chromium Lead Mercury --Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol = p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane 1,1-dichloroethylene 2,4-dinitrotoluene __ eptachlor h chlorobenzene hexach roethane --methyl et . I ketone --nitrobenzen --pentachloropli ol = pyridine __ tetrachloroethylen Results(mg/1) Results(mg/1) ------- ------- ------- trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------- --vinyl chloride --endrin lindane = methoxychlor __ toxaphene --2,4-0 _ 2,4,5-TP (Silvex) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ 0_/_'1____!,.,C/~3;...'j..,__ ______ _ Name of Site bJ lh'Z-!ltSIIJ ~JtV?:Y Site Location -------------------- Collected By _________ _ ID# Date Collected ) -I/ 4 f Time ---------'---'---------- Agency: Hazardous Waste Solid Waste ~ Superfund Sample Type Environmental Concentrate Comments VGround water (1) _ Solid (5) PS-I _ Surface water (2) ~a(6) __________ _ _Soil (3) _ Other (4) Organic Chemistry Parameter P&T:GC/MS 7 " Acid:B/N Ext. MTBE ~ #38 Results(mg/1) Inorganic Chemistry // Results(mg/1) (111g/kg) Chromium __ Copper Fluoride / Iron / _ __,, ____ _ Lead . Manganc~e __ Mercu~ Nitratf -Sel~ium t--------------t = syver Radiochemistry ,Sulfates ...... _ .. _____________ __,, --/Zinc Parc1meter Results (PCl/1) __ Gross Alpha ______ _ Gross Beta Microbiology Parameter Date Received 3 -1,). -7 7 u.ef) Dale Exlractcd&v'.43-M-97.//£1.. -✓--pH "C Conductivity ______ _ TDS TOC Reported by ________ _ Date Reported _______ _ :J70[18 0 Dale Analyzed Lab Number --c------------------1)1 IS 3191 (Revised 2/91) TCLP Compounds Inorganic Compounds __ Arsenic / Barium --Cadmiµtn -~rhium j{~rcury --. ' Selenium ~ Silver .,- Organic Compounds benzene carbon tetrachloride Results(mg/1) Results (mg/I) chlordane ------ chlorobenzene chloroform o--cresol m-cresol --p-cresol --cresol 1,4-dichlorobenzene ------1,2-dichloroethane --1,1-dichloroethylene --2,4-dinitrotoluene ------= heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane methyl ethyl ketone nitrobenzene pentachlorophenol __ pyridine __ trachloroethylene ------ ------ tr hloroethylene --2,4, trichlorophenol --2,4,6-·chlorophenol ------ --vinyl c oride --endrin lindane methoxychlor = toxaphene __ 2,4-D _ 2,4,5-TP (Silvex) N.C. Department of Environment, l lcalth, & Natural Resources Soljd Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratoiy of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number C) / q q ) S---------------------- Site Location Name of Site tJ trfl: 8 ££ ft,/ ------------------- Collected By ID# Date Collected -:S, ...,,. , 7 -q 7 Time --------------------------------- Agency: Hazardous Waste Solid Waste / Superfund Sample Type Environmental Concentrate Comments /Ground water {1) Solid (5) TCLP Compounds Inorganic Compounds __ Arsen~ B •efm --~mium / Chromium /Lead /-- Results(mg/1) __ Surface water (2) _Soil (3) . Mercury ,,/' --Selenium ------------,' Silver _ Other (4) Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE ~P-e rl= ~ ,'Peit Results(mg/1) Radiochemistry Parameter Result'· (PCi/1) __ Gross Alpha Gross Beta ---}-,----/ I Parameter Date Received _3 _ p -9 7 ~£; / Inorganic Chemistry ResuJts(mg/1) (mg/kg) Chromium Copper --Fluoride Iron Lead Manganese Mercury Nitrate Selenium Silver Sulfates Zinc \ \ \ \ \ pH = Conductivity ______ _ TDS TOC Reported by --------- Dale Extracted Date Reported ---------------- Dale Analyzed Lab Number -----------------1) I IS 3191 (Revised 2/91) Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol = p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) ------ ------= 1,1-dichloroethylene _____ _ 2,4-dinitrotoluene = heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane methyl ethyl ketone nitrobenzene pentachlorophenol __ yridine __ t rachloroethylene ------ ------ tri loroethylene --2,4,5-ichlorophenol --2,4,6-t hlorophenol ------ --vinyl ch ride --endrin lindane --methoxychlor = toxaphene 2,4-D = 2,4,5-TP (Silvex) N.C. Department of Environment, I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ ...:C)=---(_q..__q ___ , ___ ?, ___ G. ______ _ Site Location Name of Site __ U) __ ,.__,_r_~ ___ C-=_...1.....;""-....;.....;:±v..------------------------- Collected By -----------ID# ___ Date Collected __ ~J_ ...... ___,(;{_:4'_,_, ___ Ti.me _____ _ Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments /Groundwater (1) Solid (5) Surface water "2_~iqaltl (6) ___________ _ Soil (3) _ Other (4) Organic Chemistry / Inorganic Chemistry TCLf Compounds _,. ,~ I anic <;-0mpounds Results(mg/1) Arse'nic ~ ar i um 'Cadmium _._ , Chromium ·· Lead Mercury --Selenium Silver -------- Par~eter ___LL_P&T:GC/MS _ Acid:B/N Ext. Results(mg/1) Res-.lts(mg/l)(mg/kg) Organic Compounds benzene Results(mg/1) MTBE Radiochemistry ... ·' l , , Parc1meter Results (PCl/1) __ Gross Alpha __ --,,.../_,, __ _ Gross Beta / Parameter Date Received 3 -/J 1 7 /!},(_() Chromium Copper --Fluoride Iron -,, Lead _!_ Manganese , Mercury --Nitrate Selenium Silver Sulfates Zinc _pH __ Conductivity TDS TOC Reported by ________ _ Dale Extracted Date Reported ------------------/(')""'10 P 8? ...,.. " u~. "'-Dal e An alyLcd Lab Number --,------------------1)1 IS 3191 (Revised 2/91) carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol --cresol 1,4-dichlorobenzene 1,2-dichloroethane ------- ------- --1,1-dichloroethylene --2,4-dinitrotoluene ------- heptachlor hexachlorobenzene nitro nzene pentac rophenol = pyridine tetrachloroet Jene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------- --vinyl chloride --endrin lindane melhoxychlor = toxaphene 2,4-D = 2,4,5-TP (Silvex) -N.C. Department of Environment, 1 lcalth, & Natural Resources Soli_d Waste ~anagement Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O I ~r q ·3> I ------~-------------------------- Site Location Name of Site W q..,.,~ G J ~ /4, -------------------- Collected By ID# Date Collected Time --------------------------------- Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments /Ground water (1) Solid (5) ps-\,t _ Surface water (2) ..S /tlqu1d (6) ___________ _ _ Soil (3) _ Other (4) Pa'"""eter _L P&T:GC/MS _ Acid:B/N Ext. MTBE Sludge (7) ------------- -Other (8) Inorganic Chemistry Results(mg/l);(mg/kg) ,. lUDl Copper --Fluoride =Iron / Lead , --I __ Man~nese _Me~pury TCLP Compounds Inorganic Compounds Arsenic Bar· m Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) Results(mg/1) ------- ------- --1,1-dichloroethylene --2,4-dinitrotoluene ------- Nit'tate ~:elenium Silver Radiochemistry 7 Sulfates ------~~ __ heptachlor ······-··--·--------------t / Zinc Parameter Results (PCi/1) __ Gross Alpha Gross Beta ------- Microbiology / Parameter Results <7'~/lOOml) Date Received 3 -/..). _c/ 7 /] £) , pH = Conductivity TDS TOC Reported by ---------- Dale Exlradcd Date Reported ------------------ Date AnalyLcd Lab Number ~70883 -------------------DI IS 3191 (Revised 2/91) hexachlorobenzene chloroethane met ethyl ketone nitrobe ne pentachlor = pyridine __ tetrachloroethylene ------- trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------- --vinyl chloride --endrin lindane = methoxychlor __ toxaphene 2,4-D _ 2,4,5-TP (Silvex) -N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O I q ct ·3 "E" __ .,.=._....a...._;._.;._..;;:'------------------------- S it e Location ------------------- Collected By _________ _ ID# Date Collected Time -------------------- Agency: Hazardous Waste Solid Waste ✓superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- \.J G /ti-i Barium ~Ground water {1) --_•_ Solid ( 5) Cadmium --✓ Chromium _ Surface water (2) _;~ liquid (6) --Lead --Mercury _Soil (3) _ Sludge (7) --Selenium --Silver --_ Other (4) Other (8) ---- --Organic Chemistry Inorganic Chemistry -- P/peter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··--Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3'-/.,}.-77 15;.,{; Reported by --__ methoxychlor __ toxaphene Date Extracted Date Reported 2,4-D Dale Analyzed 3-18-97 Ni l:"'l>--•or.)s • = 2,4,5-TP {Silvex) Lab Number ._, t" ~>' ~~ --DI IS 3191 (Revised 2/91) NCDEHNR Division of Waste Management if Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: V Inorganics Lab: __ . CHAIN OF CUSTODY RECORD Project Name: f'c5 (_ r-Sampled By: s +-2. +c: Site ID # (NCD#) Sampler ID Location: c0 at-1-e l'\ Telephone:6}j_) 73 ~ ,.... o , j 2- Address: Date Sampled: .3-/_f-'J-+ Time Sampled: Sample Types: Soil V Water ✓ Waste Other Remarks: ?Jv--&:, VI ( /' ,e --..) Field Sample ,5l-15 -i tJBJ -t t1 5-( K.8-l T'!i!2_-L R5B-L tt 6R-I Numbers R.8 ·-l ER..-I /3.:J -( 56-l u ' Relinquished By:__t;'_,, .I /4;;~ Date: 1-LI::. q1-Time: 11/.' o:> (Siimaturn1 Received By: -~;23_::- (Signature) Date:.7--//-y::z Time: / yo s- Relinquished By: .~ ~___::._ Date: -::>-11...!}_~ Time: 7;?' >- (Si 2:nature) Received By: ~-~ ~ Date: 3-1)--z 7 Time: q:o,s- (Signature) Relinquished By: Date: Time: (Si2:nature) Received By: Date: Time: (Signature) -I . Results Rep(rted: -~ ,Lf:A_ e /u?~ DateV/Jo/17 Time: (Sjgnah1re) r r ' '---)/ -·-·-~--- NCDEHNR C Drvls10n of Waste Managemen __, D Superfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab:~.'><~- Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: LJ -"\V--r<. N c_,._,;J -tt Sampled By: s+-A-k Site ID# (NCD#) Sampler ID Location: Telephone:~ ·7 ·3'3 ·· 2 1·, b Address: u(l.✓("e ':,J<'cl NC Date Sampled: L \. WAR 10)0) 1 I Time Sampled: Sample Types: Soil Water X: Waste Other Remarks: Los I :14•31-1-l Field Sample Numbers -· Relinquished By:~~~ C -----z> ~ -/._ . \ {~1 ,..~ .J Date: i 1 1ViAv:.q7 Time: C-. 'f:.8 pr..r1 (Siimature) Received By: ~~-;J--::. Date J .. //.c;c Time: t,,:l(2 (S ignature) Relinquished By: "/~ ~:___..__ Date: .:J · /2>17 Time: ';,'· u > (Si2:na~ _....... Received By: 7$J_,( ~lA--04 Date: ?-/~ -9 7 Time: f :o ) (Signature) Relinquished By: Date: Time: (Siimature) Received By: Date: Time: ~gnature) Results Repdrted: ~ R 11 w-/L!!..;,"'_l/ Datc1'/:?o/f 7 Time: ' (~ --.... , v.: ...... ,nature) . I/ . NCDEHNR Organics Lab: Y::. Division of Waste Management Inorganics Lab: __ □ Superfund Section □-Hazardous Waste Section □ Solid Waste Section CHAIN OF CUSTODY RECORD Project Name: PC... B c~i c1 Sampled By: Czhf.-r: I Site ID # (NCD#) Sampler ID Location: wa v ,,--~ Lo Telephone:e_q£{) 7 ':J ~--;)-<?so} Address: Date Sampled: ~!u zq-:; Time Sampled: Sample Types: Soil Water ·~ Waste Other Remarks: {). ~ ~ -t C $ Field Sample Q~S-l QCT-3 De=r-1 J ~;\{--4; Numbers Relinquished By: , ~8 ~'-I~ Date: ,It// tl Time: &i} ./V I ti . , (Signature) Received By: ~~ Date: >-(.1-9 1 Time: §_00 . _,..., (Signature) Relinquished By: .~ ;J-~ Date: '>-·1 L-o/·? Time: 9'~ (., s- (SiEmature) Received By: ~ ~~ Date: ,3-r -2. -'l 7 Time: 9 .' 0.) (Signature) Relinquished By: Date: Time: (SiPnature) Received By: Date: Time: (Signature) -,, . Results Repotd: l ~ c{.(, file&(_ Date:1/L1¥?7 Time: (S/gi~Mu{e) v ~.C. Dep:irtment of Environment, • l lcal.,I;, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number _ __;:O~/_q_q_~_;;_q _______ _ Site Location Name of Site W rt1l/{6fl/ CV(l,l "[t ------------------- Collected By _________ _ ID# ___ Date Collected 3~ ( 2.,,-q, Time ------ Agency: Hazardous Waste Solid Waste _L Superfund Sample Type Environmental Concentrate Comments ✓ Ground water {1 Solid (5) 4ri tr r ...a__~ Soil (3) _ Other (4) Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE __L Pc.-R L ~EST Results(mg/1) I Results(mg/lJ(mg/kg) I __ Chromium /____a1.-,... ____ _ Copper /1 _ __._ ____ _ Fluoride --I _Iron / Lead' t.:riganese __ ercury itrate ~ S~lenium t-----------------4 / Silver Radiochemistry Parctmeter __ Gross Alpha -----,,r:..-- Gross Beta Microbiology Parameter Results (Col/lOOml) Date Received .3 -J 3 -'j' 7 d JS) Date Extracted -------- Sulfates Zinc _pH __ Conductivity ______ _ TDS TOC Date Analyzed Lab Number ----------------- TCLP Compounds Inorganic Com,P6;nds __ Arseni~,/ Barium --Cadfuium =~omium -fM:r:ury L Selenium / Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) Results(mg/1) ------ ------ --1,1-dichloroethylene --2,4-dinitrotoluene ------ = heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane ------ __ ethyl ethyl ketone _____ _ m obenzene --pen chlorophenol = pyrid1 e __ tetrach roethylene trichloro ylene --2,4,5-trichlo phenol --2,4,6-trichloro enol ------ = vinyl chloride endrin lindane = methoxychlor __ toxaphene 2,4-D _ 2,4,5-TP (Silvex) DIIS 3191 (Revised 2/91) -#{?) O ?9S-_ q 7 0 '?L.,,l......,_ ___________ ----,1 Purpose: Preparation: Enforcement and compliance with the N.C. Solid and Hazardous Waste Management Rules. A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (1) container (i.e., ground or surface water) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplicate container. Do not submit an analysis request form without any parameters indicated. Equivalent measurements: ppm = µg/ml = mg/I = µg/g = mg/kg ppb = µg/1 = µg/lOOOg = µg/kg DEFINITIONS/INSTRUCTIONS Site Number -A unique twelve-digit site/location identifier (i.e., the EPA identification number). Field Sample Number -A unique six-digit sample identifier which is pre-printed on the sample label. Name of Site -Name of facility, landfill, etc. Site Location -City and county. Collected By -Name and staff identification number of collector. Date and Time Collected -Self-explanatory. Environmental -A sample of a naturally occurring substance such as ground water, surface water, or soils which may be contaminated. Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents, or drummed wastes. Comments -Lists details regarding sample or sample point (e.g., sample location, well number, phase separation, and/or odors. Inorganic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. Organic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP Compounds -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP can only be performed on solid or semi- solid samples. For totals of the inorganic parameters, check ( ✓ ) the corresponding parameter under Inorganic Chemistry. Microbiology and Radiochemistry -Contact the Raleigh office prior to sampling either of these. Distribution: Disposition: 1. Send or deliver the original to the State Laboratory of Public Health. 2. The Lab then sends a copy (with results) to the Solid Waste Management Division. 3. The Solid Waste Management Division sends a copy to the field person or collector. This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schedule as published by the North Carolina Division of Archives and History Additional forms may be ordered from: Solid Waste Management Division Hazardous Waste Section P.O. Box 27687 Raleigh, NC 27611 N .C. Department of Environment, · I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ____ C>::;___I q...;._q---''{_o ______ _ Site Location Name of Site l.J fc(l,R (i,Af Cv,vtt ------------------- Collected By _________ _ ID# ____ Date Collected __________ Time _____ _ Agency: Hazardous Waste Solid Waste ./ Superfund Sample Type Environmental Concentrate Comments J);M 3 Y:t> A,J R~ 3 1 TCLC, Compounds / Inorganic C9J;ounds Arseµ,ic ---''/ Bartum --/I Cadmium ~hromium -f-~ad , Mercury 1-1 -Selenium Results(mg/1) V Ground water {1) __ Surface water (2) _Soil (3) / Silver _ Other (4) Organic Chemistry Parameter P&T:GC/MS ✓ Acid:B/N Ext. MTBE ~ fl.e,..j_, Results(mg/1) /" organic Chemis~ / / Results(mi/1) (mg/kg) I Barium / ..,__...._ ____ _ Cadmium )------- --Chloride ;,'; __ \....,_ ____ _ _ Chromiuny,' __ \~-.----- -Copper;/ __ \.....,,._ __ _ __ Fluoriq¢' ,, Iron / --I _Le~d __ ¥anganese _;/'fercury / Nitrate T Selenium --------------,~ Silver Radiochemistry Sulfates ······-··----------------t Zinc _pH __ Conductivity ______ _ /. Results (Plli/1) Parameter __ Gross Alpha ____ .,...... __ Gross Beta TDS TOC Parameter Results (Col/lOOml) Date Received .3 ---/ J --77 8 ~ Reported by --------- Dale Extracted 6Pll3-l '/-'17.i~Jl'M Date Reported _______ _ Date Analyted Lab Number --,-----------------1)1 IS 3191 (Revised 2/91) Organic Compounds benzene carbon tetrachloride Results(mg/1) chlordane ------ chlorobenzene chloroform o-cresol m-cresol p-cresol --cresol 1,4-dichlorobenzene 1,2-dichloroethane ------ ' --1,1-dichloroethylene ...--2,4-dinitrotoluene ------= heptachlor --~xachlorobenzene __ he~chlorobutadiene _____ _ hexa~loroethane methy ethyl ketone --nitroben ne ------ --pentachlo phenol = pyridine tetrachloroetli lene trichloroethyle~ 2,4,5-trichlorophe I _____ _ 2,4,6-trichloropheno --vinyl chloride ------ --.--endrin lindane methoxychlor = toxaphene 2,4-D = 2,4,5-TP (Silvex) N.C. Department of Environment, · l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number __ 0~/----'-9_c;_;_'-f-'--#-/ _____ _ Site Location Name of Site &J frRR. <£.,f\l C,Jfll ry ------------------- Collected By ID# Date Collected 3-l )_-en Tim'e -------------'-------, ---------------- Agency: Hazardous Waste Sample Type Environmental Concentrate ~ Ground water (1) __ Surface water (2) _Soil (3) Solid Waste ~ Superfund Comments ~:t ~> _ Other (4) __ Other (8) _______________ / Organic Chemistry Inor~nic Chemistry' I Par,meter Results(mg/1) Parameter \ / ~lts(m~)(mg/kg) _/_ P&T:GC/MS _ Acid:B/N Ext. MTBE Arsenic Barium Cadmium Chloride I / Chromium \ Copper ,' \ Fluoride / -------- Iron Lead / =May ianese Mercury --Nitrate __J'Selenium t-----------------t _l_ Silver / Sulfates ;--------------Zinc Radiochemistry Parameter Results (PCi/Jj _pH __ Conductivity ______ _ TDS __ Gross Alpha / Gross Beta -----7--- TOC Microbiology Parameter Results (Col/lOOml) Date Received 3 -/ -3 7 7 ~tJ} Reported by --------- Date Extracted Date Reported ----------------("V"':' (\ ~ q....., Date AnalyLed Lab Number •-· r,h ... .1&.• t --,--------DI IS 3191 (Revised 2/91) TCLf Compounds I Results(mg/1) Inorganic;o. '.pounds Arsen· --I --------Bari in --C;uhnium -------- --Chromium -,L-,,Lead , Mercury -1 -Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol ... -.-cresol .:;-1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) ------ ------ = ,l -dichloroethylene _____ _ __ 2,~ initrotoluene __ hepta lor hexachl obenzene hexachloroe ane methyl ethyl --nitrobenzene pentachloropheno --pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ = vinyl chloride endrin lindane = methoxychlor __ toxaphene __ 2,4-D _ 2,4,5-TP (Silvex) N.C. Department of Environment, • 1 lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ---------------Field Sample Number __ -=0_'_)_'1~tt~L/-L---________ _ Site Location Name of Site uJ fr/tRC:li /4..,11\,( 1 Y ------------------- Collected By ID# Date Collected 3 ~{ L--Cf t Time ----------------------'------------- Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments V Ground water {1} __ Surface water (2) Soil (3) Siu e (7) __________ _ _ Other (4) Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE _L PcA ..L ~S'T" Results(mg/1) Radiochemistry Pardmeter Results (PCi/1) __ Gross Alpha ______ _ Gross Beta Microbiology Parameter I r sults (Col/lOOml) Date Received 3 -;3 L) J t3& ~rganic Chemistry Parameter '~sults(mg/1) (mg/kg) Arsenic · -------Barium Cadmium Chloride Chromium __ Copper Fluoride Iron Lead __ Manganese Mercury --Nitrate Selenium Silver Sulfates Zinc _pH __ Conductivity ______ _ TDS TOC Reported by --------- Dale Extracted ________ Date Reported _______ _ Dale AnalyLed Lab Number -----------------1)) IS 3191 (Revised 2/91) TCftP. Compounds / Inorganic Cotnpounds Arsenic =B~i:'um 9 Admium 7 thromium _, Lead J__ Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol --cresol 1,4-dichlorobenzene Results(mg/1) Results(mg/1) ------ " 1,2-dichloroethane ------ ~ 1,1-dichloroethylene ---•\i,4-dinitrotoluene ------ --he tachlor he hlorobenzene hexac orobutadiene --hexachlo11~ethane ------ methyl eth~ ketone --nitrobenzene ------ --pentachlorophe ol = pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------= vinyl chloride endrin lindane = methoxychlor __ toxaphene 2,4-D = 2,4,5-TP (Silvex) N .C. Department of Environment, · I Icalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number __ -=6:c......:.l:1....._1 ... ·_':f.._· .... 3._ ______ _ Name of Site /J(±({/U£1{ Site Location -------------------- Collected By ---------- Agency: Hazardous Waste Sample Type Environme I Concentrate /4round water __ Surface water (2) _Soil (3) _ Other (4) Organic Chemistry Results(mg/1) Parameter P&T:GC/MS ✓ Acid:B/N Ext. MTBE ...L Jt--,.. h Radiochemistry Pa rd meter __ Gross Alpha -----,----Gross Beta Parameter Solid Waste __ Superfund Bari Cad Qhlo Chr C Selenium Silver Sulfates Zinc _pH Comments __ Conductivity ______ _ TDS TOC Date R eceived 3 -/ 3 -77 t3& Reported by --------- Dale Extracled./JPA...7-l'f-f7.,/ll}'-,M Date Reported _______ _ Dale Analyzed Lab Number --,----------------1)1 IS 3191 (Revised 2/91) Compounds IUm admium Chromium Lead Mercury --Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol --cresol 1,4-dichlorobenzene 1,2-dichloroethane 1,1-dichloroethylene 2,4-dinitrotoluene heptachlor exachlorobenzene h chlorobutadiene hexa loroethane Results(mg/1) Results(mg/1) ------ ------ ------ ------ --methy thyl ketone --nitroben ne ------ --pentachlor henol = pyridine tetrachloroeth ne trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ --vinyl chloride --endrin lindane = methoxychlor __ toxaphene 2,4-D _ 2,4,5-TP (Silvex) N.C. Department of Environment, · I lcalth, &. Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ CJ_/ q ____ c._1 </ ............ Cf'-. ______ _ Name of Site l/!f1tuu ~1,J7Y Site Location ------------------- Collected By ----------ID# Date Collected ) ~ / L-9 --, Time ----__ _._..________ ------- Agency: Hazardous Waste Solid Waste t/'Superfund TCLP Compounds -- -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ' _.tL' Ground water {1} -~d(5) /?lrl(J-L-/ --Cadmium --Chro_mium --Lead __ Surface water (2) ~ --__ Mercury _Soil (3) _Sludge ( Selenium ', ' ---; Silver _ Other (4) _ Other (8) " •, --' , ----Organic Chemistry Inorganic Chemistry , -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results ( mg/I) V P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride ',. chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Mangan~$C 1,4-dichlorobenzene --__ Mercury = 1,2-dichloroethane ----Nitrate __ 1,1-dichloroethylene --Sel,e'nium 2,4-dinitrotoluene Silver = heptachlor --Radiochemistry Sulfates hexachlorobenzene ----hexachlorob .µtadiene ······-··-Zinc Results (PCi/1) --= hexachloroeth,ne Parameter ,_, _pH __ Gross Alpha __ Conductivity __ methyl ethyl ket~ne Gross Beta TDS nitrobenzene \ \ ----= pentachlorophenol TOC --__ pyridine "· --Microbiology --__ tetrachloroethylene __ trichloroethylene I --Parameter Result t (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane , Date Received 3 · I J -7 7 /lJ ~ Reported by = methoxychlor __ toxaphene Dale Extracted Date Reported 2,4-D '°""" :)OO = 2,4,5-TP (Silvex) Dale AnalyLed Lab Number ....., . --DI IS 3191 (Revised 2/91) N.C. Department of Environment, · 11ca1th, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ---------------- Name of Site W ~N Site Location ------------------- Collected By ----------ID# Date Collected ';;>---tl--Cf I Time -------'------'----------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds -- -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- CB I -I Barium _·•_Groundwater (1) --Solid (5) Cadmium -- _}{ Surface water (2) ~uid(6) Chromium --Lead --Mercury _Soil (3) _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results ( mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane JL PcB ----<O. IJIJtJ/f?l!K Chloride chlorobenzene --Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Results (PCl/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------2,4,6-trichlorophenol ----= vinyl chloride endrin -- Date Received ,J -L] ·-7 2 r-1& lindane Reported by = methoxychlor p .; __ toxaphene Dale Extract~.3-/ ~-C/ 7-VP Date Reported --2,4-D p ~---2"'='0301 _ 2,4,5-TP {Silvex) Dal e AnalyLc ~-L9-9 7YP Lab Number --DIIS 3191 (Revised 2/91) ·N.C. Department of Environment, · I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number D I "ff:(i.f £,, -----~~~-------- Name of Site l,J tcati£tv C..V,fl,( 11/ Site Location ------------------- Collected By ----------ID# Date Collected ·1 -n .. -97 Time -------'--'--'--.....;....___ ------ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- DA, I Barium --_·_Ground water (1) Solid (5) Cadmium -- ✓ Surface water (2) ~quid(6) Chromium --Lead --Mercury Soil (3) Sludge (7) --Selenium --Silver --_ Other (4) Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --PCB ----_:L_ <~. IJtJIJ/ f/rfl Chloride chlorobenzene ----r Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----..... ·-·•-·-• Zinc hexachlorobutadiene ----Par.1meter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- 3·-L J-9J /)£} lindane Date Received Reported by = methoxychlor ~~~ __ toxaphene Date Extracted -/i-CJ?"VP Dale Reported 2,4-D Pe.B-5-~""""n~a~ = 2,4,5-TP (Silvex) Date AnalyLed 3-19 .L/7 VP Lab Number "J . Ja.1 I.{.. --DI IS 3191 (Revised 2/91) N.C. Department of Environment, · I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ____ O.:;;..._,__/ _'f.,_____.C,_'f...._"'1 _____ _ Name of Site __ W __ "°_A_ll_it:,_"-1 __ 0_·_v_<N_:7Y ___ _ Site Location ------------------- ID# Date Collected .3-( 2---<f, Time --------------------Collected By ---------- Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- CA-I Barium --__ Groundwater (1) Solid (5) Cadmium -- V surface water (2) ~uid (6) Chromium --Lead --Mercury _Soil (3) Sludge (7) --Selenium --Silver --Other (4) _ Other (8) -- ----Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --Pc13 ----~ < tJ. tJ oo I ./f!!lJ Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Results (PCl/1) Paramekr _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --2,4,6-trichlorophenol ----= vinyl chloride ----endrin --lindane Date Received 3-1 :J ·-9 ZtfJ iJJ Reported by = methoxychlor ~~~ __ toxaphene Dale Extracted -/"!-97-VP Date Reported 2,4-D Pcss o~n"1,O<7 = 2,4,5-TP (Silvex) Dale Analyled 3 -/9-971/P Lab Number ~..,_ t~' .... _.., .•• .,) '-., --DI IS 3191 (Revised 2/91) N.C. Department of Environment, · I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number __ O_l_~_-_'1_L--f_~ _______ _ Site Location ------------------- Collected By ----------1 D # ___ Date Collected ___ ~_-_l_~_-_q~7'---_ Time _____ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- DJ -l Barium --__ Ground water (1) Solid (5) Cadmium -- ~face water (2) Chromium --_ Liquid (6) Lead --Mercury _Soil (3) _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --ecB <tJ,IJtU,lnn... ----v Chloride chlorobenzene --I I Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium __ 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Results (PCl/1) Pardmeter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Received 3 -13-97 IBJ.0 lindane --Reported by __ methoxychlor /JeB " __ toxaphene Date ExtractcdJ-/f-971/,0 Date Reported 2,4-D ~~ ~70304 = 2,4,5-TP (Silvex) Date AnalyLcd_-/2_-971/P Lab Number --DI IS 3191 (Revised 2/91) N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ____ o_l_'1_Cf_Y_J.,__ ____ _ Name of Site lJ-/t-(}./.-8/,./ Site Location ------------------- Collected By ----------1 D # ___ Date Collected __ _:3;:__-....:./_& __ q_7.:__ __ Time _____ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ~d(5) ~-Q-l Barium --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- ~Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ✓ pc£> < o,10 Pf'l"t ----Chloride chlorobenzene ------r Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene ----__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----·······-•·--· Zinc hexachlorobutadiene ----Results (PCl/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ~ 2,4,6-trichlorophenol ----= vinyl chloride ----endrin -- 3 -!J -<f 7 19.J) Reported by lindane Date Received = methoxychlor /JetJ} __ toxaphene Date Extracted .$-.;?.cJ-97VP Date Reported 2,4-D PC!Br ~70~0S = 2,4,5-TP (Silvex) Dale Analyzed 3-::lS'-97-VP Lab Number --DI IS 3191 (Revised 2/91) N.C. Department of Environment, · I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ---------------Field Sample Number _____ O __ l _q------'q'-· S-_o _____ _ Name of Site /4)"' r r ~i'\. 6v4 ·rt Site Location ------------------- Collected By ----------ID# ___ Date Collected ___ :>~-...,. ..... /-=1--~~-9........;_7 __ Time _____ _ Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- _ Ground water (1) ~lid (5) Barium /V CB -I --Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- _L Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) -- ----Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results ( mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ..L fcp <IJ, IO#m._ ----Chloride chlorobenzene ----Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··--· Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/100ml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Received 3 / 3 -z J;G;../) Reported by lindane = methoxychlor /JC$~ __ toxaphene Date Extracted 3-~0-CJ7V,P Dale Reported --2,4-D Pt!B.s ''~o~o _ 2,4,5-TP (Silvex) Dale Analyzed 3-;l5-9'TYf' Lab Number ._:, ~ G --DIIS 3191 (Revised 2/91) N.C. Department of Environment, · I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number __ ~Q_/~'t_c_L_' S-__ J ______ _ Name of Site __ LJ ____ kfv __ R...-__ <:C-_-_t,../ __ ,_..;_tV-'-cf ___ _ Site Location ------------------- Collected By ----------ID# Date Collected '3,. ~ ( ~ -Q.. 7 Time ---------=:;..._.,__ __ _.___ ------ Agency: Hazardous Waste Solid Waste /superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ~lid(5) $J)-I Barium --Ground water (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- / Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane v e~ <(),/0 ,,,.,,, --Chloride --chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ----= p-cresol Iron ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-·•-·-•-Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --2,4,6-trichlorophenol ----= vinyl chloride ----endrin --lindane Date Received 3 -/3 -7 7c3f) Reported by --__ methoxychlor Pee~ __ toxaphene Date Extracted 3'-;2.IJ-t:/7-Yf' Date Reported 2,4-D p~ !J?0:-J07 = 2,4,5-TP (Silvex) Date AnalyLed -~S-9:z:yp Lab Number --DI IS 3191 (Revised 2/91) N.C. Department of Environment, · I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ---------------Field Sample Number ___ """tJ'--'-l q_7_~-"'--2-__ · ____ _ Name of Site Site Location ------------------- Collected By ----------ID# Date Collected Time -------------------- · 1t '-". Agency: I Hazardous Waste Solid Waste __ Superfund TCLP Compounds Sample Type Environmental Concentrate / Ground water (1) __ Surface water (2) _Soil (3) _ Other (4) Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE V PCB ✓ Pe 21 Results(mg/1) Comments PA-B-J I / I I Parameter Arsenic Barium Cadmium Chloride Results(mg/1) (aig/kg) Chromium Copper --Fluoride \ / \/ I I I I Iron / ______ _ Lead / / \ '\ =Manga~~e __ Merc~ry Results (mg/I) Inorganic C7'ounds --f:t'um -------- --Gliromium ~Lead , Mercury -_-/ -Selenium 1= Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) ------ ------ _Nit~e __ SeJenium --1,1-dichloroethylene -------• --2,4-dinitrotoluene ------t-------------~ __ ~ilver Radiochemistry -/Sulfates ······-··----------------1 1 Zinc Parameter Results (PCl/1) / pH __ Gross Alpha -------✓• __ Conductivity ______ _ Gross Beta TDS TOC Microbiology Parameter Results (Col/lOOml) Date Received 3 ~iJ-97 t3A) Reported by _______ _ Date Extracted Date Reported ---------------- Dale Analyzed Lab Number --,----------------1) I IS 3191 (Revised 2/91) ~ heptachlor · hexachlorobenzene exachlorobutadiene ------exachloroethane __ m thyl ethyl ketone _____ _ nitr benzene penta hlorophenol = pyridin tetrachlo thylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol ------ --vinyl chloride --endrin lindane __ methoxychlor __ toxaphene 2,4-D _ 2,4,5-TP (Silvex) ·N.C. Department of Environment, · l lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratoiy of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ---------------Field Sample Number ____ 6___,_/_;q_Cf_,_•_S"""_,3 _____ _ Site Location ------------------- Collected By ----------ID# Date Collected 3-1 'L-'}7 Time --------=--...;,_, _ __,_ _ _,____ ------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Envir2anmental Concentrate Comments Arsenic 7 --Barium PA-8 -J --__ Ground water (1) Solid (5) Cadmium --Chromium --__ Surface water (2) quid (6) Lead ----Mercury _Soil (3) Siu (7) ---Selenium ----Silver --_ Other (4) Other (SJ --'\. -- t ~ganic Chemistry --Organic Chemistry -- Parameter Results (mg/I) Parameter i;fsults(mg/l)(mg/kg) Organic Compounds Results ( mg/I) P&T:GC/MS Arsenic benzene / Acid:B/N Ext. ----Barium ' carbon tetrachloride ----MTBE Cadmium I chlordane ------t¥tw Chloride ' chlorobenzene -.c... ----Chromium chloroform ------__ Copper o-cresol ----Fluoride I m-cresol ------Iron __ p-cresol ----Lead cresol ------__ Manganese ' 1,4-dichlorobenzene ------__ Mercury 1,2-dichloroethane --Nitrate ~ 1,1-dichloroethylene -- --Selefnium _ 2,4-dinitrotoluene Silver heptachlor ----he~chlorobenzene Radiochemistry _,1Sulfates --······-·•--·-Zinc hexachlorobutadiene Parameter Results (PCi/1) L-pH --hexach oroethane __ Gross Alpha 1 __ Conductivity = methyl etpyl ketone Gross Beta ' TDS __ nitrobenzel\e ----I TOC __ pentachloroj,henol -- / --__ pyridine Microbiology I __ tetrachloroethylene / --__ trichloroethylene Results (~lOOml) --Parameter __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ---- ----__ vinyl chloride endrin -- 3-1:'3--9 z~;J lindane Date Received Reported by = methoxychlor __ toxaphene Dale Extradc<l8,()dJ'-/t -9~.J1WI Date Reported 2,4-D > = 2,4,5-TP (Silvex) Ory ~09 Dale AnalyLcd Lab Number .,..,, f l.1 6 ~,i · --DI IS 3191 (Revised 2/91) N.C. Department of Environment, · l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number --------------- Name of Site W 1¥/Yl.);[, f\J ~ ✓ Nt'f Field Sample Number __ d_/_q __ q_s-~y~-------- Site Location ------------------- Collected By _________ _ ID# Date Collected ·;:,...-1 L,-qr Time -------~------------ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- /Ground water (1) 18 ~B -L/ Barium --s 'd (5) Cadmium ----Chromium ~aid --Lead 1 __ Surface water (2) --__ Mercury Soil (3) _ Sludge (7) Selenium \ -- "'---,"-Silver --Other (4) _ Other (8) --'"-, -- Inorgani~Cl)emistry --Organic Chemistry -- Pa✓feter Results(mg/1) Parameter Results(mg/Q (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --_Copper o-cresol --Fluoride m-cresol ----= p-cresol Iron ----Lead cresol --------__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene , ----······-·•-·-• Zinc hexachlorobutadiene ----Parameter Results (PCl/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone \ Gross Beta TDS nitrobenzene '~ ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results ((jcSI/lOOml) __ 2,4,5-trichlorophenol I ------__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Received 3 -J 3--CJ 7 &£J lindane Reported by = methoxychlor __ toxaphene Date Extracted Date Reported 2,4-D ~ DlO = 2,4,5-TP (Silvex) Date An alyzed Lab Number .._,.• ,' --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number cJ I q '1 S-S:-------------------------------- Name of Site l.tJ ('r(Q_fu=-A.J GuN r:y Site Location ------------------- Collected By ----------ID# Date Collected 3 _ / ~-"r ·-rr Time --------'-"------~--------- Agency: Hazardous Waste Solid Waste /superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arse~ic ~lid(5) -- p1t-B-ti --Barjum v Ground water (1) , dmium --Chromium --~~d(6) __ Surface water (2) Lead ....._ / __ Mercury _Soil (3) Sludge (7) Selenium ; I --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- P✓meter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene ----__ Mercury __ 1,2-dichloroethane Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··---Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene -, __ trichloroethylene ' --I Parameter Rt lts (Col/lOOml) __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ---- ----__ vinyl chloride endrin -- Date Received 3-12-9213£) lindane --Reported by __ methoxychlor __ toxaphene Date Extracted Date Reported 2,4-D 0.?(}""\11 = 2,4,5-TP (Silvex) Dale Analyzed Lab Number "'~'-~ltJ.,.., --DI IS 3191 (Revised 2/91) .J N.C. Department of Environment, -I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratoiy of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number () ( Cf ~-)-6 -------------------------rr, l I - ; ' Name of Site __ uJ_frrl,,-----',U'--· _r...;..t __ Cc._v_w_fy_._ __ _ Site Location i ------------------- Collected By ID# Date Collected > -/~ ~9 ' Time ------------------------------ Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments /Ground water (1) Solid (5) _ Surface water (2) ~d (6) ___________ _ _Soil (3) _ Other (4) _ ludge (7) __________ _ _ Othe (8) __________ _ Organic Chemistry Parameter P&T:GC/MS = Acid:B/N Ext. MTBE v ~C;B V P~.>T Results(mg/1) Radiochemistry .... ,, ________________ __, Parameter Results (PCi/1) __ Gross Alpha Gross Beta ------- Microbiology Parameter Results (Col/lOOml) f I Inorganic Chemistry . Parameter Results(mg/1) (mg/kg) __ Arsenic. Barium --Cadmium --Chloride Chromium --__ Copper -- Fluoride Iron Lead __ Manganese Mercury --Nitrate Selenium --Silver --Sulfates Zinc --_pH •. __ Conductivity ______ _ TDS --TOC Date Received 3 -i} -9 7 iJ l) Reported by --------- Dale Extracted ________ Date Reported _______ _ Date Analyzed Lab Number DI IS 3191 (Rcvise_d...,...2/-:-9--,1)______ --------- TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium Chromium --Lead Mercury --Selenium Silver Organic Compounds benzene --carbon tetrachloride Results (mg/I) Results(mg/1) --------- -- -- chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol cresol ----1,4-dichlorobenzene _____ _ 1,2-dichloroethane --1,1-dichloroethylene --2,4-dinitrotoluene ------= heptachlor hexachlorobenzene hexachlorobutadiene ---------hexachloroethane --methyl ethyl ketone --nitrobenzene ------ --pentachlorophenol = pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophcnol 2,4,6-trichlorophen~l ------ vinyl chloride --endrin --lindane --methoxychlor = toxaphene __ 2,4-D _ 2,4,5-TP (Silvex) .__ _______________ _. N.C. Department of Environment, · I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ ()_! _,C(.__q_S-_1 ______ _ Name of Site /,J/}~.1~ tl Ccv/L{_ yy Site Location ·------------------- Collected By ----------ID# Date Collected b'-"-0,,, -q·7 Time ----______ ....J_..___,____ ------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- /Groundwater (1) [>A:{3:>-~ Barium --Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury _Soil (3) ludge (7) --Selenium ----Silver --_ Other (4) Otli (8) ------ ''\'\ --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene / Acid:B/N Ext. ----Barium carbon tetrachloride ----MTBE Cadmium chlordane --!f<:r6 ---- .....iL... Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··--·-Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethyle\ __ trichloroethylene --Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol --I __ vinyl chloride --j endrin --lindane 3 -13 -97 /};JJ Date Received --Reported by __ methoxychlor __ toxaphene Date Extractc<l,&JA:3-/V-9~J/M Date Reported 2,4-D :}70313 = 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --DI IS 3191 (Revised 2/91) Purpose: Preparation: Enforcement and compliance with the N.C. Solid and Hazardous Waste Management Rules. A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (1) container (i.e., ground or surface water) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplicate container. Do not submit an analysis request form without any parameters indicated. Equivalent measurements: ppm = µg/ml = mg/I = µg/g = mg/kg ppb = µg/1 = µg/lOOOg = µg/kg DEFINITIONS/INSTRUCTIONS Site Number -A unique twelve-digit site/location identifier (i.e., the EPA identification number). Field Sample Number -A unique six-digit sample identifier which is pre-printed on the sample label. Name of Site -Name of facility, landfill, etc. Site Location -City and county. Collected By -Name and staff identification number of collector. Date and Time Collected -Self-explanatory. Environmental - A sample of a naturally occurring substance such as ground water, surface water, or soils which may be contaminated. Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents, or drummed wastes. Comments -Lists details regarding sample or sample point (e.g., sample location, well number, phase separation, and/or odors. Inorganic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. Organic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP Compounds -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP can only be performed on solid or semi- solid samples. For totals of the inorganic parameters, check ( ✓ ) the corresponding parameter under Inorganic Chemistry. Microbiology and Radiochemistry -Contact the Raleigh office prior to sampling either of these. Distribution: Disposition: 1. Send or deliver the original to the State Laboratory of Public Health. 2. The Lab then sends a copy (with results) to the Solid Waste Management Division. 3. The Solid Waste Management Division sends a copy to the field person or collector. This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schedule as published by the North Carolina Division of Archives and History Additional forms may be ordered from: Solid Waste Management Division Hazardous Waste Section P.O. Box 27687 Raleigh, NC 27611 · .ision of Waste Management □ Superfund ec 10n □ Hazardous Waste Section □ Solid Waste Section Organics Lab: i-/ Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: wc..rr-e-.,,.. eov .... +y pco l .___J F.'II Sampled By: 2). kv~rJ .,. )u4n So., . Site ID # (NCD#) Sampler ID Location: Telephone:~ 733 -~80 1 Address: Date Sampled: 3/n-L12 Time Sampled: ~ Sample Types: Soil Water / Waste Other Remarks: A~cf:: ~? 2~ ~ , • ,MR-\ AJ'R J L\.~R. '-1 Field Sample Numbers ------ Relinquished By: D~ Quµ Date: 1L,2 117 Time: /2. ··: o c) \ (Si1mature) Received By: ~~---2----Date: .3 -,L-'i 7 Time: /2: <JC) --(Signature) Relinquished By: -?~ _J.__:__ Date: 3,-J3 -'17 Time: 9 _.2--e;, (Sirmature) = Received By: ~-/._Q,. J1LR~ Date: 3 -11-~1'7 Time: 9.' 2-o (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time: (Signature) ~ Results Reported: ~J./4, ~~A.Pc~ Date: t//Yl/17 Time: (Sig'nefref ,. , \./ / NCDEHNR . Division of Waste Management Organics Lab: ·✓· Inorganics Lab : __ □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section CHAIN OF CUSTODY RECORD I Project Name: yl/3 Lttnd{z'Jl Site ID# (NCD#) --------- Location: WCtVf(A1 U). Address: Sample Types: Soil ---Water ✓ Remarks: Field Sample Sampled By:~~-~------ Sampler ID _________ _ Telephone: C1!1)~73~~~' 2_8~()~J ___ _ Date Sampled: ________ _ Time Sampled: _________ _ Waste Other ------ !Numbers Date: 3/r~/11 Time: 12:1"° r I Received By: ~~~--L --(-S-ig-nn-tu-re~).e..----==c........,~----- Date: "3-tz._.--~-, Time: /2,·£.r" Date:"J--1J ~q7 Time: 9 >ZP Received By: ~l 2.Jk ~ Date: 3-13-97 Time: 9 .' ~ (Signature) Relinquished By: ____________ _ Date: ----Time: ---- Si nature Received By: ---------------Date: Time: (Signature) Date: Time: ---- NCDEJ-INR _ Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: __ Jnorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: fe,r3 LF-Sampled By: S ra ./-e_ Site ID # (NCD#) Sampler ID Location: W ?-:t: r-e 16 c ? Telephone:(__) 7;3 -ob9z Address: Date Sampled: d-/Z -1 7 Time Sampled: Sample Types: Soil ✓ Water ✓ Waste Other Remarks: H.0R SJ)-) Nc8-l A-tZ-1 0.)-l CA-/ DA-I C &T~ I ~~ Field Sample Numbers Relinquished By: _.r:_, ,. ,. ,. ~ ~ Date:3 -/2-?7 Time: 5/5°'0 V { (Sifmature) Received By: ~,,J-~ Date: ".> -rz-1, Time: r:ro (Signature) Relinquished By: -7 / J__:_ Date: )·-13 -9 7 Time: '?.· ~ -/ . 77 ~ (Sie:nature) Received By: AlL ,(_, ~ ) J L L 1,L.-'7"" Date: 3 -13-$' 7 Time: 9 .' 20 (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time: ~nature) -. Results Rep~d: Ji-. I!/-;,; .f!.~ Date:l//~/~7 Time: / , wini mrer····--- V ~~:;;~~~:~ D Superfund Section Organics Lab:_/_ Inorganics Lab: __ -2:< □ Hazardous Waste Section □ Solid Waste Section CHAIN OF CUSTODY RECORD Project Name: w~ [.,v.,.,J y 1":>C ;3 t,_.___,,J F,. I I Sampled By: D. Q 1.1..,.,fvr-J I -J .,l,.,..50,.. Site ID # (NCD#) Sampler ID Location: Telephone:~ 733 -290/ Address: Date Sampled: 3[1-i.,/97 Time Sampled: Sample Types: Soil Water ~ Waste Other Remarks: Field Sample ? AiJ--I ~1r9,..,, OA:8-3 ~frB-3 PA-13-tf Bl'r e ._; 'I Numbers -------------- I Relinquished By: o~D-/fo"A Date: 3/11,/77 Time: ?-{) :<!JO V ~ ' (Sie:nature) Recei·led By: ·---? / -->--:__ -Date: J.-rL-"'t, Time: 2..), cro ✓/ (Signature) / Relinquished By: ~ ?~ Date: ~-L~-17 Time: q _: '-" (SiP-nature) ,,,~ Received By: ~ ,1J2v~ Date: 3--132-J Time: 9,' Zo (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time: ~ ignature2 - Results Re~ed/4 U·--t!111\. ~/l~~~ Date: Y/.?o/ '1 Time: 'v'signature) , , -- N.C. Department of Environment, I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number _ _:0=---f_J'1!,_'j..L.3.-..8 _______ _ Name of Site N ,tJ-1i1<,-iftJ C v MTY ---"--'--"-.a..;...:.=----------Site Location -------------------- Collected By ----------ID# Date Collected b -/? __ q, 7 ----Time Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ~olid (5) /J?/e ·-1 Barium --__ Groundwater (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- V soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) -- ----Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --P43 ----L <Q,/'2pf>t", Chloride chlorobenzene ----r Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --· Radiochemistry Sulfates hexachlorobenzene ----······-·· ... --Zinc hexachlorobutadiene ----Results (PCl/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity methyl ethyl ketone Gross Beta TDS --nitrobenzene ----= pentachlorophenol TOC -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Rep~ ~/1/'!:L lindane Date Received 3 -/</, 9Z ALJ --__ methoxychlor d)CB.:S-__ toxaphene Dale Extracted 3 -_;;._()-97yp Date eported ~/f'7 2,4-D p~--J = 2,4,5-TP (Silvex) ,...,,....,~"'"'Irr Date Analyzed ;-?,6 -9?1/P Lab Number • s t ~ \.. --DI IS 3191 (Revised 2/91) j:/:-C/) u 9? tf -C/ v'lli Purpose: Preparation: Enforcement and compliance with the N.C. Solid and Hazardous Waste Management Rules. A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (1) container (i.e., ground or surface water) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplicate container. Do not submit an analysis request form without any parameters indicated. Equivalent measurements: ppm = µg/ml = mg/1 = µg/g = mg/kg ppb = µg/1 = µg/lOOOg = µg/kg DEFINITIONS/INSTRUCTIONS Site Number -A unique twelve-digit site/location identifier (i.e., the EPA identification number). Field Sample Number -A unique six-digit sample identifier which is pre-printed on the sample label. Name of Site -Name of facility, landfill, etc. Site Location -City and county. Collected By -Name and staff identification number of collector. ,, .... ;,-. Date and T{me Collected -Self-explanatory. Environmental -A sample of a naturally occurring substance such as ground water, surface water, or soils which may be contaminated. Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents, or drummed wastes. Comments -Lists details regarding sample or sample point (e.g., sample location, well number, phase separation, and/or odors. Inorganic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. Organic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP Compounds -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP can only be performed on solid or semi- solid samples. For totals of the inorganic parameters, check ( ✓ ) the corresponding parameter under Inorganic Chemistry. Microbiology and Radiochemistry -Contact the Raleigh office prior to sampling either of these. Distribution: Disposition: 1. Send or deliver the original to the State Laboratory of Public Health. 2. The Lab then sends a copy (with results) to the Solid Waste Management Division. 3. The Solid Waste Management Division sends a copy to the field person or collector. This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schedule as published by the North Carolina Division of Archives and History Additional forms may be ordered from: Solid Waste Management Division Hazardous Waste Section P.O. Box 27687 Raleigh, NC 27611 N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number _____ (~_'.)....;_l _q_· Ci....:.I_J.;:.._--'?=------- Name of Site lJ trR-R/2...N lo ,.,,. "1 ·ry Site Location ------------------- Collected By ----------ID# Date Collected 1 -/1 ·-q 7 Time ----__ --:::;_ .......... .__-'----------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- -~Solid (5) PJ D -· I Barium s --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- ✓ Soil (3) __ Mercury _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene 7 Acid:B/N Ext. ----Barium carbon tetrachloride ----MTBE Cadmium chlordane 7 Pl/l --------· ----< o , Io .pp.,iL Chloride chlorobcnzent ------✓ /+t-.--..h Chromium chloroform ----1'.le .,+:: ~ __ Copper o-cresol --_ &1d~1'N <O./j"fnt Fluoride m-cresol L,N~ ----<t:J .~ ~"" Iron __ p-cresol ---ftf€tl111x~ /1111< --< I. t:) ,J,,,,m,,. Lead cresol =-roef':t/; ----~""~ __ Manganese --1,4-dichlorobenzene ,:;/ -<IJ• i fl'M __ Mercury 1,2-dichloroethane =~¼S"---·-<o•/fJl'M Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-·-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ! --__ pyridine Microbiology --__ tetrachloroethylene - --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --,,, 3 I_f te Received 3 -f</, 'l Z t.fJJ.P '-?ls-176~ ~.:S'?/ tf'Cl'Js .;,-~CJ-?7V~ D:ile Exlractc:<l ,Bu,9 3-ll -97 g[J Reported by --methoxychlor --toxaphene Dale Reported --2,4-D ,.Ocs r/N ~-~6_9 ?--V p 9":"" ""'f"tA---2,4,5-TP (Silvex) Dale AnalyLc:d &J,1_,i?f:.•'i.' 11)5:_;f' Lab Number ~--', I! DIIS 3191 (Revised 2/91) /J'5) '-/·I 7 -- N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ ---'C,"----'I_Cf.._•q--"--'S--'---c-'-\ ______ _ Name of Site _ ___._i.,_J_,Af.....___~=·,...,--=--C.,_., -"J'---'-'-,'l.l-''N----'-----Site Location ------------------- Collected By _________ _ ID# ___ Date Collected ___ 3:;__-__,/'--J,_-_c,....:..-_7 ___ Time _____ _ Agency: Hazardous Waste Solid Waste ✓ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- A is-i Barium _Lsolid (5) --__ Groundwater (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- £ Soil (3) __ Mercury _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmit•m chlordane 7 pep , __ --<(),/()~ Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ -·-Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ---- ···••-•-··-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity methyl ethyl ketone Gross Beta TDS --nitrobenzene ------TOC __ pentachlorophenol -- '-------__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3r / Y-97 f3£} --Reported by --methoxychlor PUJ} toxaphene Dale Extractc<l 3 .. ~ / -9 71/p --Date Reported --2,4-D ~r41 :)~1(l""'F:.8 _ 2,4,5-TP (Silvex) ' '1-...J:1'-, )1 Dale AnalyLcd -~~-97-yp Lab Number --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ .;;;;;.6 --'1'-'t.:.... _q--=-'...;:o'---------- Name of Site _ __.i...,A,L..l .:.....M=BL......C...~-"'1_· _~_;....;;'Jv\/c..:....L..,_~4-----Site Location ------------------- Collected By ----------ID# Date Collected ~ ~ /3 -f 7 Time ----____ .,_,_ ___ --'---------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium __ Groundwater (1) t/ Solid (5) l-[3 -I --Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- / Soil (3) Mercury _ Sludge (7) --Selenium --Silver --Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) __ P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --P48 ---·---_.IL <O,l0.f!/2.M Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene ----__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroet.hane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- 1 --/<l 91 JBJJJ lindane Date R eceived --Reported by __ methoxychlor ~,J --toxaphene Da te Extracted -~/-971/p Date Reported --2,4-D /?ee,5-O";'!"O".f;Q _ 2,4,5-TP (Silvex) Dale Analyzed 3--<~-97-YP Lab Number ._, J ... ,. ----DI IS 3191 (Revised 2/91) N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number 6/ q '-f "6 / ----~--~----------------------- Name of Site lJ.~1{[;£. Iv ~vJ.Vl·-r,t Site Location ------------------- Collected By _________ _ ID# ____ Date Collected __ '?,...;:_;._ __ /LJJ~--'J._-J-'-----Time _____ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- AD,D Barium lL._ Solid (5) i .) --__ Ground water (1) Cadmium ---Chromium --__ Surface water (2) Liquid (6) Lead -- ~Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) __ P&T:GC/MS Arsenic benzene ----_1L. Acid:B/N Ext. Barium carbon tetrachlcride ----MTBE Cadmium chlordane --()CJ:> ---- ..\cl__ < tJ. I tJ #-""-Chloride chlorobenzene G:>1 ----../ Chromium chloroform ------v ~rb __ Copper o-creso! ----E,t1o'J1?.1'tl <"0, /" 17/nt Fluoride m-cresol ------_ L,AtdA#E <Q~.:J..ilq2a Iron __ p-cresol --~ i Lead cresol <t-0-:pe,..,._ ----_-ZO~E <;l,IJ 1P!'-__ Manganese --1,4-dichiorobenzen~ -;//-/:-2> <l!J . / f/?M __ Mercury --1,2-dichloroethane _ ~ ½S-Tf> < o~ i ~/YI Nitrate __ 1,1-dichloroethylene --, Selenium 2,4-dinitrotoluenc ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----········-·· Zinc hexachlorobutadiene Parameter Results (PCi/1) __ Gross Alpha Gross Beta -- Microbiology Parameter Results (Col/lOOml) -- -- rn 3 Date Received 3 ~;1-97 8~ -If-f'111/J. ~ /,ea 3-~l-971/P Dale Exlrac:;~,q3-1 f ·fJ~J() PeS½ d-,l,6-971//' Dale AnalyLcd /)PA 3 ,.J.r/:/i7 ?/-::{ii DI IS 31'Jl (Revised 2/91)//1!)~/ 7 ----_pH hexachloroethane -- --Conductivity __ methyl ethyl ketone: TDS nitrobenzene ----T0C __ pentachlorophenol -- --__ pyridine --__ tetrachloroethylene --__ trichloroethylene --__ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol --__ vinyl chloride endrin --lindane --Reported by --methoxychlor __ toxaphene Dale Reported --2,4-D Lab Number_97OJ 70 2,4,5-TP (Silvex) -- N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ____ O_· _1 _C(_Ci_t ....:<.::.::..2-.--='--------- Name of Site lJbRRw CovNry Site Location ------------------- Collected By ----------ID# ____ Date Collected __ 3..:;._.-.....L...:p;....-_'1-'---'7 ____ Time _____ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ~lid (5) Barium ~L B -I --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- c/soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----__ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --B;S <. O,. IO .f!l!.1YL -------_:L Chloride chlorobcnzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----·······-·· Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Reccived ___ 3, / 'f, 97 A& --Reported by --methoxychlor . /Pf!B~ __ toxaphene Date Extracted 3-~l-97-VP Date Reported 2,4-D f-'ees = 2,4,5-TP (Silvex) Date AnalyLcd 3 -;{G-97--VP Lab Number 01-«"l'n.')~1 t • ....; { • ..J, .. ....,.. ~ --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ O_i_q_· q..!-C~=:3;...._ _______ _ Name of Site WMR AV G v,v N Site Location -------------------- Collected By -----------ID# Date Collected ·:3 '"' 13-e.(7 ----Time Agency: --Hazardous Waste Solid Waste ___ Superfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --.$olid (5) Barium P0 D -Y --__ Groundwater (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- J" Soil (3) --Mercury Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- P✓meter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ---- --Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --· __ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --. __ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received J-1i/-l}-7 g61) --Reported by --methoxychlor __ toxaphene Dale ExlraclcC.: .. Date Reported 2,4-0 --- 0 ...., 0,,...,-✓ z _ 2,4,5-TP (Silvex) Date Analyzed 3 -d.0--97 NT Lab Number -..JI ( --...'' --DI IS 3191 (Revised 2/91) N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number ----------------Field Sample Number ____ (!)_l _Cf_'i_' _t;;_' Y.__ ______ _ Name of Site LJM R0J Site Location -------------------- Collected By -----------ID# Date Collected OJ -13 -17 Time ----__ _;_;...._;...._ .... ___ _._____ ------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- / Solid (5) Barium A-p·D·-'--f --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- ~Soil (3) Mercury _ Sludge (7) --Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) ~P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ -·-__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- 1--__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received J-1</-<J 1 ~tl) --Reported by --methoxychlor --toxaphene Dale Exlraclc<l Dale Reported 2,4-D -- ~70~73 _ 2,4,5-TP (Silvex) Dale Analyzed ~3-d0-27 1vr Lab Number --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ -..:·6'--'-J ..... 9_q......._.&c....:S"'==--------- Site Location ------------------- Collected By ----------ID# ____ Date Collected __ ....._3,_-_./'-'3"'--·-~._-, ____ Time _____ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- i solid (5) Barium CD -) --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- J Soil (3) __ Mercury _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) ---- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene ------_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --Pc,iJ ---- _.\L_ < o-/O ff,.,._ Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene --= heptachlor · Silver --Radiochemistry Sulfates hexachlorobenzene ----·••-·•---·• Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Received 3 -I y -9J /1£.> lindane --Reported by --methoxychlor Dale Extra~~/-97VP --toxaphene Date Reported --2,4-D -p~; (")t'~o~~ 2,4,5-TP (Silvex) .~,· ,~•l'':il -- Date AnalyLcd -~6-97-,/,P Lab Number --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ___ o;;;;...·_1 ""'"'t_j ._• ~'_.'-' ..... ~ _______ _ Site Location ------------------- Collected By ----------ID# ___ Date Collected __ _,,,3_,_..,_,_{ '}=-----____._7_1=------Time _____ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ~ Solid (5) Barium pj R-\ --__ Ground water (1) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- / Soil (3) __ Mercury _ Sludge (7) Selenium --Silver --Other (4) _ Other (8) ---- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I) --P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --PcB ----./ <tJ./IJ-fr>M Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----···••·•·-·· Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin -- Date Received 3-/ 1/--? 1 /3'° lindane --Reported by --methoxychlor p~✓ __ toxaphene D:.ile Exlractc<l :.,,;;z._/-971/P Dale Reported --2,4-D Pea~ ').~n,,...~~ _ 2,4,5-TP (Silvex) Dale Analyzed 3-~ -97,YP Lab Number ._;; , ....,., __ •• .t. 1 --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number ------------------------------- Name of Site /)t8ff.16>N <cv,ipty Site Location ------------------- . Collected By ----------ID# Date Collected .'.3-( > -'1"1 Time ---------------------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- NtJ V -I Barium --__ Groundwater (1) _ Solid (5) Cadmium --Chromium ~ Liquid (6) --__ Surface water (2) Lead --__ Mercury Soil (3) Sludge (7) Selenium -- $~~# Silver --_ Other.(8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane 7 9 l--f) (i;i."!) th OOt?~rp-4 ----Chloride chlorobenzene v ee-.\, ----7-Chromium chloroform ------£Aid .If'._/,/ <tJ . c,oo//f!#... __ Copper o-cresol ----L ,/l/cl4A/c <:o. o,::,o~ Fluoride m-cresol ----'711ezAc;xl/t:?A,6 -c <a,oo / Iron __ p-cresol --_//fYA£Jl/€#e <0.00..;2_ Lead cresol ---- --~/,}_.ttdA/.~ <.<'. t:?a ~.;;i.._ __ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane Nitrate __ 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ---- ••O-OM-00 Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ G ross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane 3-11-9713£) --Date Received Reported by methoxychlor --Pee¥;~ --toxaphene Da le Exlradc<l ' -Lf -97-VP Date Reported --2,4-D pefJ_;/~e:sT o"'-'0~?€ _ 2,4,5-TP (Silvex) Dale AnalyLcd 3 -/f-'97)1'P Lab Number ..., If ~, --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ ._6~1,-...::9:J...g_,_=~.....::~=--------- Name of Site_-----=cW----'-frl-'--'--Q..U-_· ___:;~-....;..~-'-=-'H--'---Site Location ------------------- Collected By ----------ID# Date Collected "3 ..-,(::,-ti.,, Time ---------"---'--"'-"'-----=------------ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- J/ot/-~ Barium --__ Groundwater (1) Solid (5) Cadmium -- Zuquid (6) Chromium --__ Surface water (2) Lead --Mercury Soil (3) Sludge (7) --Selenium ---#~ Silver --Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ✓ Acid:B/N Ext. ----Barium carbon tetrachloride ----MTBE Cadmium chlordane _lL_ Fkd> ----Chloride chlorobenzene ------2i(':l.-.1J <o,oo l#m Chromium chloroform _ ,;;; '45" -rP ----<o. tl.O.lA-il.M __ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----···--·--·· Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Date Received 3.. -L '/...-9z IE~ --Reported by --methoxychlor t?J.5'15 3-ltJ-1176fl __ toxaphene Dale Exlraclc<l.t3&t!J-17 ·9z.&1) Dale Reported --2,4-D ~J.)ff /kSi f ::J7U:}77 _ 2,4,5-TP (Silvex) Dale Analyzcd3-).l/-<j7 '-1 -/-97 Lab Number DI IS 3191 (Revised 2/91)'pf.) 8& -- N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O . Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number _ ___;:6~t ...... Cf__.<f_,G"'-' _9,....._ _______ _ Name of Site_--1L.....,.Ji:>C..L..,4E....._...ri,,....,e::;::;_...;;w_____.C,__,,,.....;;;..U..:..:N._tr~---Site Location ------------------- Collected By ----------ID# ___ Date Collected 1, v {3 -q 1 Time Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- QAS -3 Barium --__ Ground water (1) Solid (5) Cadmium --Chromium t/ Liquid (6) --__ Surface water (2) Lead --Mercury _Soil (3) _ Sludge (7) --Selenium --Silver --~~~ _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ✓ Lt'z,r h ----Chloride chlorobenzene ---- ,~-J) <.o, OOJlf}M Chromium chloroform ----<o, oo /Pfhl __ Copper o-cresol =d s-fP --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene ----trichloroethylene Parameter Results (CoJ/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -J'I-97 BJD --Reported by methoxychlor --/JJ~) 3-1'14 717,/J __ toxaphene Dale Extracted 8~d 3 -L 7 ·· £7.P,J{) Date Reported --2,4-D ~~ hlSiS" ~"":,{1~t-f8 2,4,5-TP (Silvex) Date AnalyLcd 3 -.l'/-97 "''BY ...., u. ,( --Lab Number DIIS 3191 (Revised 2/91 )13io -- N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number _ ___,6-=c..il.__'.1_.__'.'(r'"1--=....;:;0:;;__ _______ _ Name of Site _ ___.:;~__,_fl&<~c...:.."E-=-N..i-__..G"""'-v_l'...,\1-'r .......... e __ _ Site Location ------------------- Collected By ----------ID# Date Collected 3 ~ /3 -C( '7 Time ----------"''--'-=---->------------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- Qfr&-1 Barium --__ Ground water (1) _ Solid (5) Cadmium -- V Liquid (6) Chromium --__ Surface water (2) Lead --Mercury _ Soil (3) _ Sludge (7) --Selenium -- $a~ Silver --_ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --e c.B {p.i,tJ) ---- ...JL 0 , () 0 ~ flll-"" Chloride chlorobenzene ----v l,?t~.,-7 Chromium chloroform --C°Nc:l~,'iJ ---- ---c'(J ,t:)t:JO / __ Copper o-cresol --L-./1-./ cf A 1✓~ < d . t,t:JtJ,;2_ Fluoride m-cresol = 71,fa~(JxycA/4/!.. < cJ. oo 1 ----Iron __ p-cresol --_,--.,, <tJ, 0 0 ,.;;J__ Lead cresol --L.0£.A £1&.61/€ C/2 /4---u/4/V'c ----<LJ • ~Ot!J;;L__ __ Manganese 1,4-dichlorobenzene ---- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----···•····-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -~ i/!Jf-1)_ --Reported by --methoxychlor (}JCS~~ __ toxaphene Dale Exlraclc<l 3-19--9-Z-V~ Date Reported --2,4-D f'~(-J6t· ~70:r)'°/9 _ 2,4,5-TP (Silvex) Dale AnalyLcd · './ -??VP Lab Number --DI IS 3 I 91 (Revised 2/91) N.C. Department of Environment, I Icalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number ------------------------------- Name of Site lu@Alf.\V G I.INT't Site Location ------------------- Collected By ID# Date Collected 3 -/3 -4 'l Time ------------------------------ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- ·::,[solid (5) :Cs-B-l Barium --__ Ground water (1) Cadmium -- ~urface water (2) ~ Chromium --. 1qwd (6) Lead --Mercury _Soil (3) _ Sludge (7) --Selenium 1 --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --Pl ,8 ----..JL. <O,OPOIIJl?m Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol --------Iron __ p-cresol --Lead cresol --------__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --2,4,6-trichlorophenol ----= vinyl chloride -----endrin ~-,v-91 &J Re~ed bJ )_ ~ ~ ~/t&:Jll ? lindane Date Received __ methoxychlor Dale Extractc'3~~-97J/J' __ toxaphene Dale Re/!)1fud .W:!",/ fl 2,4-D P<j~ _ 2,4,5-TP (Silvex) Lab Number <1 •-1 "') Q 0 Date AnalyLcd ~/9-977/P -....,-,., ....;, ~,l l J --DI IS 3191 (Revised 2/91) ---9 t') t>; N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number __ ~Q~\q~q~_7,_7_• _______ _ Name of Site f;Jtte-R e:N G-,.J N r"1( Site Location ------------------- Collected By ----------ID# Date Collected 3v f'3 -ct, Time -------------------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- E... z_ fV1 -:;, Barium --__ Groundwater (1) _, Solid (5) Cadmium -- / Liquid (6) Chromium --__ Surface water (2) Lead --Mercury _Soil (3) _ Sludge (7) --Selenium \ --Silver -- -~Other~ Other (8) --L.,.e ..... ~ -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene ----✓ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --l±'~b ----v Chloride chlorobenzene --------,J,lj-JJ <.0,00/pPYn Chromium chloroform .2.: 'i,. r.-TP ---- --<Q, fl.fl./~ __ Copper o-cresol ---y-1 ;-Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene ----Pardmeter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -;y ~97 L'd& --Reported by __ methoxychlor t>JS'/ S-3 -1 9 -97 t¾J_ __ toxaphene Dale Exlraclc<l&/,1 .3-L z-27 fl{) Date Reported 2,4-D MA-/Jt S1 ~-...,.n-s1 = 2,4,5-TP (Silvex) Dale AnalyLcd3~J.~ '{-1:J, Lab Number ,.,J r 'l,..r..,.; < . , --I)( IS 3191 (Revised 2f}lj) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number --------------- Name of Site _ _.{"-d--'--'Afl"-'-'-&.._~....:.tV.,,___G_·_<./_I\J"-7:t.:...J... __ _ Field Sample Number __ ___..;:;;.0_1 _'i_1-'-7'-·=2>'--------- Site Location ·------------------- Collected By ----------ID# Date Collected :::Z,-/ 3 -'f 7 Time -------="--''--""'---'-"---------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium E.?.-th -~I --Cadmium __ Ground water (1) Solid (5) -- V Liquid (6) Chromium __ Surface water (2) --Lead --Mercury _ Soil (3) Sludge (7) --Selenium ' --~~ Silver _ Other (8) -- -~ ------Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg). Organic Compounds Results (mg/I) _P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------VcB ✓ < (), ()fJOJ.nu,, Chloride chlorobenzene -:7 ----t>:< rt Chromium chloroform ------ --f;ddg,f./ <o. 0001 __ Copper o-cresol -- --t./NdANE <O,(Jel".2, Fluoride m-cresol --= p-cresol _7'>fedmrytAIM <.Cl, OtJ/ Iron ---/0){.;Jf!I.I.. ~ c < t!J• '106--Lead cresol , ---- --__ Manganese --1,4-dichlorobenzene --__ Mercury __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····••--·•--· Zinc hexachlorobutadiene ----Results (PCi/1) Parctmeter _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol ----= vinyl chloride endrin --lindane Date Received 3 -I c/ -9 7 SIJJ --Reported by __ methoxychlor ~~/)'.u=c __ toxaphene Dale Exlraclcd_-19-9 7 Dale Reported 2,4-D p(!.8;/..oesr 1-"f --~ .... , = 2,4,5-TP (Silvex) Date AnalyLcd 3-19-971/P Lab Number --· # J ,.;. l JA,, --DIIS 3191 (Revised 2/91) NC Dcpanmcnt of Environment, Hullh, & Nawal Rc,ourcei Solid Wa•L<; ~laru1,cmcn1 Divi•ion SAMPLE ANALYSIS REQUEST Sl.4tc uboratory of Publi, Hc.,.lth P.O. Box 28047, 306 N. Wilmini;ton St. R•lcii;h, North Carolin• 270 I l-~047 Sile Number ______________ Sumplc!D Number/Nu.me __ C>_--'j.__'?_'1_<_'-f ..... · __________ _ Name of Sit.c __ W---=flr;~,L_A.,_~__,_-~--~...i...i...Cf-1---Collated By ___________ ID# ____ _ SiteLoeation DatcCo!kctcd ~ --{ )-Cf f Time ---------------------"--'---L---=---------------- Agency: Hazardous Wast.e Solid Wastc -/ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Result.s(mg/1) EnvironmenL'1I Concentrate Comments arscruc - ~L-,/1\-vl barium - Ground Water (1) Solid (5) cadmium ---chromium - Surface Water (2) X Liquid (6) lead -- -mercury Soil (J) Sludge (7) selenium ---~ilver -·I Or.'ncr (4) Other (8) -~~ - - -Organic Chemistry Inorganic Chemistry - Parameter Raults (mg/I) Para.meter Re:Sults(mg/l)(mg/kg) Organic Compounds ,Rcsult..s(mg/1) / P&T:GC/MS antimony bcnz.enc --- Acid:B/N Ext. 11r5C!UC carbon tetrachloride --- 2,4-D barium chlordane ---2,4,5-TP(Silvcx) beryllium chJorobcnune ---chlord!l!lc cud mi um chloroform --- -hept.achJor chloride o-crcsol --hexachJoroben.z.ene chromium m-cresol --- -hcxachJorobuw.c.licnc cobalt p-crcsol -- c:ndrin copper crcsol ---lindane fluoride 1,4-dichlorobenz.ene ----methoxychlor -iron I ,2-dichJoroethanc --toxaphenc: lead I, 1-dichJorocthylc:ne -- --nunganesc: -2, 4-d ichloroct!Jy lcnc --mercury -hcpt.ach.lor nickel hcxach.lorobenunc ---nitrate: hcxachlorobuta<liene ---selenium hcxachlorocthane -- -silver methyl ethyl kc:tone -FOR LAB USE ONLY sulfates nitrobe112enc: -- 3 -/'l-97/)i) thallium pcnlJ.ichlorophcnol --Date Received vanadium pyridine -- -zinc 1c:trachJorocthy lc:ne -Date Extracted pH trichJoroc:thy Jene ---conductivity -2 ,4 ,5-trich.lorophenol Date Analyz.cd 3-l<if -91 Nr -TDS 2 ,4,6-trichlorophenol - -fla.:;h point -vinyl chloride Reported By -c:nc.Jrin -]inc.lane --Date Reported --mcthoxychlor 'i..,..n,,....fg ,,. --toxaphcne Lab Number ' -"• /I .... 2,4-D -- --2,4,5-TP (Silvcx) OHS 3191 (RcviscJ 12/9]) NC Department of Environment, Hc.allh, & N1t:ur.l Rc,ourcci. Soli~ W1•1.<: t.t.n.ai;cmcru Divi•ion SAMPLE ANALYSIS REQUEST State Laboratory of Public Hc.illh P.O. Box 28047, 306 N. Wilmin;;ton St. R•lcii;h, North Carolina 2701 l-li047 Sit.cNumbcr ______________ Sample ID Numbcr/Nume ____ ___:C>:...." ....,_l_,4'-C(t->--....:~5,c..._ _______ _ Name of Site -~LJ~Pr:Jf-.&=€..=-i..lY~· ____::G,::......,-'I.A:;...ir\J..>(......lr,'-'-+---Colkcted By ____________ ID# _____ _ SiteLocation _______________ Date Collected __ ).z, _-_l...:>:.........-_q...;_-_7 _____ Time ______ _ - Agency: Haurdous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Resulb(mg/1) EnvironmenL'll Concentrate Comments arscnic -barium NaV-<-t - Ground Water (I) Solid (5) cadmium ---chromium -✓ Surface Water (2) Liquid (6) lead --- -mc:rcury Soil (3) Sludge (7) selenium --- ~Oilier (4) , ~ilvcr -Other (8) --L-st:_"-dv.-k - -Organic Chemistry Inorganic Chemistry - Parameter Re:;ults (mg/I) Parameter Re:;ults(mg/l)(mg/kg) Organic Compounds _Rc::;ulb(mg/1) ✓ P&T:GC/MS antimony ben.z.cne --- Acid:B/N Ext. lif5CnJC carbon tetrachloride ---2,4-D barium chlordane --- 2,4,5-TP(Silvex) beryllium chJorobenzcne ---chlordane cudm.iurn chloroform --- -bepLachJor chloride o-cresol --hexachlorobenzene chromium m-cre:;ol --- -hexachlorobuLac..liene cobalt p-cresol --endrin copper cresol ---!inc.Jane fluoride 1,4-dichlorobenzene ----methoxychlor -iron 1,2-dichJoroethane - -toxaphene lead I, 1-dichJoroethylene -- --manganese -2,4-d ichloroetllylenc --mercury -hepwch..lor nickel hexachJoroben.z.ene ---nitrate bexachlorobut.ac..liene ---selenium hexachloroethane -- -silver methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobc112enc ---thallium penLachloropbenol . 3-J i-9 Zll/.0 -Dare Received vanadium pyridine -- -zinc tetrnchJoroethylene -Date Extracted pH trichJoroethylene -- 3 -l{!v q7 NL -conductivity -2,4,5-trichJorophenol Date Analyzed -TDS 2,4,6-trichlorophenol - -fla~h point -vinyl chloride Reported By --endrin lindane --Date Reported --methoxychlor ( ,....f(),,....,r, ~ toxaphene ~ • J,J!l,.. ("'1i;. --Lab Number 2,4-D ----2,4,5-TP (Silvex) DHS 319 I (RcviscJ I 2/93) NC Department of Environment, Hull.!!, & Narur•I Rc,ourcc, Solid Wa•L<: t.larui;cmcni Divi•ion SA."J\,fPLE ANALYSIS REQUEST Stiitc uboratory of Public Hc.:alth P.O. Box 28047, 306 N. Wilmini;ton St. R•kii;h, North Carolina 27011-80'17 Site Number--------------Sample ID Number/Na.me ____ D::::::..-4l_:t~9.,__'_r_,__G _______ _ Name of Site Gu ltlt ±1 Collcctctl By ____________ ID# _____ _ SiteLocation ______________ DatGCollcctctl ___ 3_-..e.(_.s_-_q_1 ______ Time ______ _ - Agency: Hazardous Wast.c Solid WastG __ Superfu.nd TCLP Compounds ---- Sample Type Inorganic Compow1ru Result.s(mg/1) EnvironmenL'll Concentrate Comments arseruc - &tt-R~i barium - Ground Water (1) Solid (5) cadmium --✓Liquid (6) chromium - Surface Water (2) !Cl.Id -- -mercury Soil (3) Sludge (7) selenium --- ~ Other (4) . fc ~ilver - -Other (8) -l,..~ - -Organic Chemistry Inorganic Chemistry - Parameter Raults (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounru ,Rcsult.s(mg/1) V P&T :GC!MS antimony bc:Jl.Une --- Acid:13/N Ext. arscruc carbon tetrachloride ---2,4-D barium chlordane --- -2,4,5-TP(Silvcx) -beryllium chlorobc:II.Z.(!nc -chlordane cadmium chloroform --- -heptachlor -chloride o-cresol -hcxachloroben.zene chromium rn-cresol --- -hcxachlorobutadiene cobalt p-crcsol --endrin copper cresol ---lindane fluoride 1,4-dichloroben.zene ----methoxychlor -iron 1,2-dicWoroethane - -toxaphene -lead I, 1-dicWoroethylene - --manganese -2, 4-dichloroelby !enc --mercury -hc:pwchlor nickel hcxachlorobenune ---nitrate hexacWorobut.adiene ---selenium hexachloroc:tha.ne -- -silver lllCLhyl ethyl ketone -FOR LAB USE ONLY sulfates ni1roben2ene -- 3 -1'1--97 l!Jl) -thallium pcnlllchlorophenol -Date Recci vcd vanadium pyridine -- -z.mc tetracWoroethylene -Date Extracted pH tricWoroethylcne -- J .,/fi-9? N1 -conductivity -2,4,5-trichlorophenol Date Analyzed TDS 2,4,6-trichlorophenol -- -flash point -vinyl chloride Reportctl By -endrin -lindane --Date Reported --mc:thoxychlor ,,.,,,.....O"~r --toxaphene Lab Number -...J' ff , ... ·--( J..,. 2,4-D -- --2,4,5-TP (Silvc:x) DHS 3191 (RcviscJ 12/93) NC Department of Environment, Hc...11.h, & Narur.l Rc.-ourcc, Solid w •• t.: t.lan.ai:cmcm Divi.ion SM1PLE ANALYSIS REQUEST S!Alc Laboratory of P\Jblic Hc.:dlh P.O. Box 28047, 306 N. Wilmini;ton St. Ralci.;h, North Carolina 27011-8047 Sile Number _______________ Sample ID Number/N=e ------"O-L..f -1V'-· _Cf,___7,__r __________ _ Name of Site -~L ... 1.1'--'kfx,,'-'--'"-'-W""'-"--...... 4/ __ ~_--~H.._ __ Colkctc!<l By ___________ ID It ____ _ 3 13 '.f::J.. .2-~] Time ____ _ Site Location Dat.cColkctw ---------------- Agency: Haz.ardous Wa.st.e Solid WastG __ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s RbulLS(mg/1) Environmental Concentrate Comments arsen.ic -barium ~olid (5) H f11 I -Ground Water (1) cadmium --chromium f::t°' 3 - Surface Water (2) Liquid (6) lead --- -mercury _JLSoil (J) Sludge (7) sel enium --silver - -Other ( 4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds ,Rc:;ulLS(mg/1) P&T:GC/MS antimony ben.unc: ---:;:r, Acid:13/N Ext. --11r~cruc carbon tetrachloride ---2,4-D <O•I PPM barium chlordane ---2,4,5-TP(Silvcx) <n . I PP,n beryllium chJorobcnzcne ---chlordane <tJ,~ Pf'tH rndmium chloroform --- -beptachJor <D,/ 1¥111 chloride o-cresol --hc:xac hJorobenzene <d,/ PfU" chromium m-cresol ---hexachJorobutadiene ,-cobalt p-cn:sol ---endrin <O,ltpm copper cn:sol ---lindane <IJ,:J._f',PM fluoride 1,4-dichlorobenzene --- -methoxychlor <J.Oppnt iron 1,2-dichJoroethane -- -toxaphenc: <.:2.,() #"" lead l, 1-dichJoroethylene pee --v' < t:J :10/!l'P' manganese 2,4-dichloroctl..Jy !enc -&:~f -- _:L -mercury -hcpt.ach.lor ✓ f+<rh nickel bcxachJorobenzcne ----nitrate bexachlorobutadiene --selenium hexacWoroctbane --silver methyl ethyl ketone --FOR LAil USE ONLY sulfates nilroberucne -- Date Received 3-Jy -97 IJJ) thallium penlllchlorophenol --vanadium pyridine }f '-i JiO Pf..iJ/fhr3-~l -'/7,Y P --21nc tetrachlorocthylene --Date Extracted l]II_B._ 'l..-L(:!i.Zld.£l -pH -trichJoroethy lcne Jby,'br 3 -~7tf-YP -conductivity -2, 4 ,5-trich.lorophenol TDS 2,4,6-trichlorophenol Date Analyzed &uA~:lA7~ --ifS'IS--1-97 fl,L!ih point vinyl chloride --Reported By endrin --lindane --Date Reported --methoxychlor ,-,. lJ0-1 "'qf --toxapheoe Lab Number ~._./ I ., " ( , 2,4-D -- --2,4,5-TP (Silvcx) Dl!S 3191 (R,viscJ 12/9]) NC Department of Environment, Hc.allJl, & Narur•I Rc,ourcc, Solid Wa,i..: ~larui:cmcnl Divi,ion SANQ>LE ANALYSIS REQUEST SLl&tc uboratory of P\iblic Hc..lth P.O. Box 28047, 306 N. Wilmini;ton S1. Ralcii;h, North Carolina 27ol l-W•l7 Siu: Number ______________ Sample ID Number/Name ____ 0~[_1~'t~i _¥ ________ _ Name of Sit.e _ __.cLJ __ ~---'--->--4.J.-r--=-"--''-+-"-t----Collect~ By _____________ ID# _____ _ SiteLocation DateCollectro J --l( -47 Time --------------------~----------------- Agency: Hazardous WasLC Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1ds Rbult..s(mg/1) EnvironmenL'il Concentrate Comments arsenic -barium ~olid (5) /L (h ( - Ground Water (1) cadmium -• -chromium J<m 3 -Surface Water (2) Liquid (6) !cud --- -mercury ~Soil (3) Sludge (7) selenium --~ilvcr - -Other (4) -Other (8) - - - Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Para.meter Result5(mg/l)(mg/kg) Organic Compounds _Rc:;ults(mg/1) P&T:GC/MS antimony bcnz.enc: ---L Acid:B/N Ext. 11rscruc carbon tc:lrachloride ~=f~ -- 2,4-D barium chlordane ---2,4,5-TP(Silvcx) beryllium cruoroben.zcnc: ---chlordane: <t>,:J..Pfm cu<lrruum chloroform --- -bc:ptncruor <P,./ ppat chloride o-cresol -- -hc:xachlorobenz.ene <O,/ P,P/11 chromium m-cresol -- -hc:xachlorobuta<lic:ne ' cobalt p-crc:sol --endrin <(),/ ffhl coppa cresol --- -lindane <O,:Ll'f'd' fluoride: 1,4-dichlorobenz.enc: ---methoxychlor < I, 0 'f'f?nl iron 1,2-dichloroethane ---toxaphene <:;J..,t>~M lead I, 1-dichloroethykne pe& <o,7~,qnt --./ ma.nganese 2, 4-dichloroctl.Jy !enc --- ✓ f e-~-t mercury hept.ach.lor --✓ 1:±-o/'~ nickel hcxachlorobenune ----nitrate hc:xachlorobuta<lienc: --selenium hexach.loroetbane --silver methyl ethyl ketone --FOR LAil USE ONLY :.ulfutc:s rutroberucne -- D,,.1te Receiv~ 3-I 'f-9 7 /3~ thallium pc:ntachlorophenol --vanadium pyridmc ~fr,iJo P Ct3.f//l:sr3 -::a-97-yp -- -ZIOC tc:trachloroethylene -Date Extracted/J.f:!./J.3.,l f -~J&i) -pH -trichlorocthylcne />Ca/PttSr 3-:Z.7 -97VP -conductivity -2,4,5-trichlorophenol Date Ana.lyz.ed~ ... H'-97~ TDS 2,4,6-trichlorophenol --h/$1 -1 -97 fl,L!>h point vmyl chloride --Report~ By endrm --lindanc: --Date Report~ --methoxychlor '"_,.....,.n~R"'"." --toxaphene Lab Number ..,JI ' ., .. .1 ( " 2,4-D -- --2,4,5-TP (Silvex) OHS 3191 (Rcvi,cJ 12/93) ~ NC Dcpartmcnl of Environmcnl, Hc: . .idLh, & Nacur•I Rc,ourcc, Solid Wa,Lc ~farui;emcnl Divi.ion SAMPLE ANALYSIS REQUEST Sl4lc Laboral.Ory of Pl,blic He.11th P.O. Box 28047, 306 N. Wilmini;lon SL Rolcii;h, North Carolin• 2701 l-~0•17 Si1.e Number ______________ Sample ID Number/Numc: ___ __.fJo<.-+/-'l+-'1-1--t~Cf ________ _ Name of Site _ __./.,__/2!_,_~---'--~~w_' __ C,v. __ .~.a..:Pz~-Colk.ctc<l By ____________ ID# _____ _ SiteL:ication _______________ DatcColle.:tc<l ___ 1_--_>_-_-_Cf_' _' _____ Time ______ _ Agency: Hazardous Wast.e Sample Type Environmental Ground Water (1) Surface Water (2) ✓ Soil (3) Concentrate :1/fioHd (5) Liquid (6) Sludge (7) _ Other (4) Other (8) Solid Waste / Superfund Comments TCLP Compounds Inorganic Compow1d.s arsc:ruc burium cadmium chromium lcac.l mercury selenium silver Result.s(mg/1) Organic Chemistry Inorganic Chemistry Parameter P&T:GC/MS Results (mg/I) Parameter Re:sults(mg/l)(mg/kg) Organic Compounds .Rc.sult.s(mg/1) ~ Acid:B/N Ext. 2,4-D <O. I f/Jflt 2, 4 ,5-TP(Silvc:x) <i-=-0'--'-, ... J .... ~ .... ~ .... _Y'1..,_....._ chlordane: < 01:l /?J'A1 hepl.!lch!or <(), / {!2~ hexachloroben.z.ene -<~P~,-,'--il~rF-J'JI\...~~ hc:xachlorobuUtc.lic:ne 1 c:ndrin lindane methoxychlor toxaphenc: fG8 1-k-,,:b FOR LAB USE ONLY D;i.te Received . 3-I Y -9 ] /liS) rn_f l,{~9,,h tPIJ81 -.2.1-9 71//' Date ~ractc<l """•-,.i'7 '/J /J(!,S's;~ 3-.2..7-971/P Date AnaJyzed~V/t:3-.z..f' 47idJ SiS't/-1-t'/1 J.I) Reporte.:l By Date Reported ---------- Lab Number DHS 31 91 (Rcvi5cJ 12/93) antimony _______ bc:n..z.cnc: 11r~CllJC barium beryllium cuc.lmium chloride chromium cobalt copper fluoride iron lead nunganesc: ______ _ mercury nickd nitrate selenium silver sulfutes thallium vunadium 21nc pH conductivity ______ _ TDS fl.L'>h point ------- cu.rbon tetrachloride chlordane: chlorobc:n.unc: chl oroform o-crcsol m-cresol p-crc:sol crc:sol I ,4-dichloroben.z.ene ______ _ 1,2-dichloroethane 1,1-dichlorocthy!ene ______ _ 2,4-dichloroctbylenc ______ _ hc:pt.ich.Jor hc:xachloroben:z.cnc bexachlorobuwc.liene hexachloroctbune methyl ethyl ketone nitrobenune pc:nLuchlorophenol pyridine tetrachlorocthylene trich!orocthylene ------- 2,4,5-trichlorophenol ______ _ 2,4,6-trich!orophenol ______ _ vinyl chloride: cnc.lrin lindane mc:thoxychlor toxaphene 2,4-D 2,4,5-TP (Silvc:x) NC Dcpartmcnl of Environment, Hc.ali.h, & Narur•I Rc•ourcc, Solid Wa,L<: J,,fan.ai;cmcm Divi,ion SAMPLE ANALYSIS REQUEST St4tc l.AboraLOry of Pliblic H,s:dlh P.O. Box 28047, 306 N. Wilmini;ton St. R.!cii;h, North Carolina 27011-80•;7 Sile Number ______________ Sample ID Number/Name ____ 6__,_I 'l_q __ ~_O ________ _ Name of Sir.e _ ___:::l,;_~L..hf::--'--'--f).4V __ '---_G_v_~-=--t1__,_ __ Collected By ____________ ID# _____ _ SiteLoe2.tion DatcColkcted )-3 -1. 7 Time ------------------'-"-------"----'--------------- Agency: Hazardous Wast.e Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Resu.JLS(mg/1) EnvirorunenL'll Concentrate Comments arsc:ruc - ~lid (5) barium l,J tvi-I - Ground Water(!) cadmium --chromium w n1--3 -Surface Water (2) Liquid (6) lead --- -mercury _...---s'oil (3) Sludge (7) selenium --~ilvc:r -_ Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter Resu.lts(mg/l)(mg/kg) Organic Compounds ,RcsulLS(mg/1) P&T:GC/MS antimony bc:nunc: --_L Ac id:13/N Ext. l!fSeruc cu.rbon tetrachloride --1,4-D ~~,J~$1 -barium chlordane ---1,4,5-TP(Silvc:x) beryllium chJorobc:nzc:ne -·--chlordane: <Q• 2.-ppm cadmium chloroform --- -hepLachJor <O , I f'f'rtl chloride: o-crc:sol -- -hc:xachloroberu.ene <o, I .ffd' chromium m-cresol -- -hexachlorobutadic:ne ' cobalt p-crc:sol --endrin <o./ Pfitn copper crc:sol ----lindane <0, :i...pµ fluoride 1,4-dichlorobc:nzene --mc:thoxychlor <Io'-iron 1,2-dichJoroc:thanc: -<d,"1},';,, -- -tox?hc:nc: lc:ad 1, 1-dichJoroc:thylene -- ./ c.l3 < D, ID#u. manganese: 2, 4-dichloroc:tby lc:nc: --/ Pt:?;$T mercury hcpwchJor -v"' --l±ea:b nickel hc:xachJorobenzcue --- -nitrate bc:xachlorobutadienc: --selenium hc:xachloroc:tbanc: --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitroberu.cnc: -- D)l-le Received . 3 -/'t_-</1 ifiS} thallium pcnlllchloropbenol --vanadium pyridine: --zrnc (n J ~}-'>J~ 1-'etJ~3 -~1-'n71p · Dare xtracted BM'J3 -t f--')J/jf) --tc:trachJoroc:thylc:ne pH trichJoroc:thy !enc --PC.9/Pssr 3 -.27-'??VP -conductivity -2,4 ,5-trichJorophenol Date Analyzed &Jtr~LS--1.i ]j;f TDS 2,4,6-trichlorophenol --/>IS7 :r -1 -97 · flash point vinyl chloride --Reported By endrin --lindane --Date Reported --mc:thoxychlor 0..,.~ ,,...,ClO toxaphene .__,, /, ,J • ("'i ... , --Lab Number 2,4-D -- --2,4,5-TP (Silvcx) Dl!S 3191 (Rcvi5cJ 12193) NC Dcpanmcnl of Environment, Hc..all./l, & Narur•I Re•ourco1 Soli.J Wa,I.<: ~l1rui;cmen1 Divi,ion SMfPLE ANALYSIS REQUEST Sl.4te Laborauiry of Public Hc.tlth P.O. Box 28047, 306 N. Wilmini;ton St. R•kii;h, North Carolina 2701 l-H0~7 Site Number _______________ SamplclD Numbcr/Nlllllc ____ C>_' _l_q_C(.1....--_8"_( ________ _ Name of Site _ _;::UJ:::;;.;:;._._~~--=N'-"--_~_;, ---'--"-M-+----Collected By ____________ ID# _____ _ SiteLocation _______________ Dat.cCollected __ ._2-_-_1 _<zs_-_Cf.:...1._· ______ Time _______ _ Agency: Haz.ardous Wll.Ste Solid Waste ✓Supcrfund TCLP Compounds ---- Sample Type Inorganic Compow1ds RbullS(mg/1) EnvironmenL'll Concentrate Comments arsenic - -~ Solid (5) barium 1? M B-1 - Ground Water (1) cadmium --chromium - Surface Water (2) Liquid (6) lead --- _/soil (3) -mercury Sludge (7) selenium --:;ilvcr - -Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter ResullS(mg/l)(mg/kg) Organic Compounds .R~ull'i(mg/1) P&T:GC/MS antimony bcnune --- Acid:B/N Ext. !irSCfUC cllfbon tetrachloride ---2,4-D barium chl ordane --- -2,4,5-TP(Silvcx) -beryllium chlorobcnz.cne -chlordane cadmium chloroform --- -bepwchlor -chloride o-crcsol -hexachlorobenzene chromium m-cresol --- -hcxachlorobuLadicne cobalt p-creso! --endrin coppa crcsol ----lindane fluoride 1,4-dichlorobenzene -- -melhoxychlor -iron 1,2-dicWoroethanc -_ tox,henc lead 1, 1-dicWoroethylene --L C..8 < O, LO f¥.i1. -nunganese -2, 4-dichlorocllly !enc ;-mercury hcpwchJor ---nickel hcxachloroben:Lcne ---nitrate bc:xachlorobuta<liene ---selenium hexachlorocthane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nilroberuenc -- 3 -1'1--97Sd> thallium pc:n Luchlorophenol --Date Received vanadium pyridine ~ee ---21nc tclracWoroethylc:ne 3-~I-C/7-VP -Date Extracted pH tricWorocthylcne --Pt$ -conductivity -2,4,5-lricWorophenol Date Analyzed .3-:Z7-9 7-y'P -TDS 2,4,6-lrichlorophc:nol - -fla~h point -vinyl chJori<lc Reported By endri.n --lindnnc: --Dale Reponed -melhoxychlor -0..-~o,....9r --loxapheoe Lab Number 4J' f t_ j "' ' 2,4-D -- --2 ,4,5-TP (Silvcx) DIIS 3 I 91 (Rcvi~eJ 12/93) NC Dq,artment of Environment, H1;,11lLh, & Natur•I Rc,ourcc, Solid Wa,Lc t>lanai;cmcm Divi,ion SAMPLE ANALYSIS REQUEST Staltc Laboratory of Public Hc:.illh P.O. Box 28047, 306 N. Wilmini;lon Sl. R•lcii;h, Norlh Carolina 2701 l-H047 Sile Number---------------Sa.mplc!D Numbcr/Nlllllc ___ o_·_,_l'!_._j..._-....;;8"c...·_"t-_________ _ Name of Site __ LJ:..-_~:;....:....-'----..,,, __ U> __ i.1_vv+-r _____ Collcctc.l By _____________ ID It _____ _ SiteLocation Dat.cCollccted 2 ...., I~ -q 7 Time --------------------------'------------- Agency: Haurdous Waste --Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compow1d.s ResuJt.s(mg/1) EnvironmenL'll Concentrate Comments arsenic - ~VE-1 barium - Ground Water (1) Solid (5) cadmium --- ✓ Liquid (6) chromium - Surface Water (2) le.ad -- -mercury Soil (3) Sludge (7) selenium ---:silver ~ Other (4) - -Other (8) - - - Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter ResuJts(mg/l)(mg/kg) Organic Compounds .Rcsult.s(mg/1) P&T:GC/MS antimony bcnz.enc ---Acid :B/N Ext. lirSC!lJC carbon tttrachloride ---::!,4-D barium chlordane --- -::!,4,5-TP(Silvex) -beryllium ch.lorobcnzcne -chlordane cadmium chloroform --- -bepLach.lor -chloride o-crcsol - hexachloroben.z.ene chromium m-crcsol --- -hexachlorobu Lad icne cobalt p-crcsol --cndri.n copper cn:sol ----lindane fluoride 1,4-dichloroben.z.ene -- -mcthoxychlor -iron 1,2-dich.loroethanc --toxaphenc -lead l, 1-dichJoroethylcne -PcB <(), (JIJIJ?~At. -✓ -manganese -2,4-dichloroctbylcne --mercury -hcptachlor nickel hcxach.lorobenune -----nitrate bexach.lorobuta<liene -selenium hexachlorocthane -- -silver methyl ethyl ketone -FOR LAB USE ONLY sulfates nitroberucne ---thallium penwchlorophenol Date Receivc.l 3 -IY.-f2 .SJ[) - -vanadium pyridine · PeBt - -zinc tetrach.loroethylene Date Extracted 3-/ 9 -971//J - -pH trich.loroethy lene Date Ana.ly~~-/9-97]/f' - -conductivity -2, 4 ,5-trich.lorophenol -TDS 2,4,6-trichlorophenol - -fl,(!;h point -vinyl chloride Reportc.l By endrin --lindane --Date Reported --methoxych.lor ,. .... 10"'9,.,,. toxaphene "~J ,. ; ,_ ~-J. --Lab Number 2,4-D -- --2,4,5-TP (Silvex) Dl!S 3191 (RcviseJ 12/93) NC Dcpar1ment of Environment, Hullh, & Natur•I Rc,oun:c, Solid Wa.L<: Marui;c:mcnl Divi.ion SAl'v!PLE ANALYSIS REQUEST SLl&tc uboratory of Public H...,.Jlh P.O. Box 28047, 306 N. Wilmini;ton St. R•kii;h, North Carolina 27011-80'17 Site Number ______________ Sa.mplc ID Numbcr/N!Ullc ___ D_l_~_.__'1.__f_· --="::>:::--_______ _ Name of Sit.e _ __,l,..->"--..... er~R.u..U..:..=.-'--w __ lp_;_,-U'--M-'-'--!Y_.__ Collected By ____________ ID# _____ _ SiteLocation _______________ DateCollcctcd __ ___;:"3;_-_~_-_--_9_7 _____ Time ______ _ Agency: Hazardous Wast.e Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Results(mg/1) EnvironmenL'il Concentrate Comments arsenic - ~Solid (5) 111 -( bo.rium IV! - Ground Water (1) cadmium -- ft1M-3 chromium -Surface Water (2) Liquid (6) le.id --- -mercury L Soil (3) Sludge (7) selen.iurn --:;ilvcr -_ Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Re::sults (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds ,Rcsults(mg/1) P&T:GC/MS antimony benune ✓ Acid:B/N Ext. --?-11rscruc carbon tttrachloride --fg:'{$% -2,4-D -barium chlordane - -2,4,5-TP(Silvcx) -beryllium chJorobcnz.cne --chlordane < 0. :i.. Pf?A1 cadmium chloroform -- -bepwchlor <,J, I ~M -chloride o-cresol - -hcxach.lorobenzene < lh I R)?-11 -chromium m-cresol - -hcxach.lorobutadicne ' cobalt p-crcsol -- endrin <(), 'eprr. copper crcsol ---li.ndane <o,f fluoride 1,4-dichlorobenzene -<l,IJZ: ---methoxychlor iron 1,2-dichloroethane --toxaphenc <:I.,()·,:-lead l, 1-dichJoroethylene / pc.a -- 7 <D,/ not -manganese -2, 4-d ichloroctby lcnc P,e,,,-t mercury heptachlor 7 l,b, rb --nickel hex.achloroben.zcne ---nitrate bexachlorobuU!diene ---selenium hex.achloroethane -- -silver methyl ethyl ketone -FOR LAil USE ONLY sulfates nit roberuene -- -thallium penwchlorophcnol -vanadium (1/1 3 D~ Received 3 -/ '/ -97 /3.i) ;£r ,,.q £f;;_/Peor3~--?7-Y/-' Date xtracted_b_3-t_K.-'i.zS[) - - -pyridine zrnc tetrachJorocthylcne -pH trichJorocthy lcne -PC.i/flssr 3 -.2.7-97-Y/J - -conductivity -2,4,5-trichlorophenol Date Analyzed ~µA 3 -2f"-97Jj -TDS 2,4,6-trichlorophenol -hJS-, :S-'/--I -9 ] -lh.:;h point vinyl chloride -Reported By · endrin --lindane --Date Reported --methoxychlor 01'"1{)'"'10,-., .._,rt .. ;,...t.it-\i. --tox.aphene Lab Number 2,4-D -- --2,4,5-TP (Silvex.) DHS 3191 (Rcvisc,d 12/93) NC Dcpanmcnt of Environment, Hullll, &. Narur.1 Rc,ourcc, Solid Wa•L<: t.laiui;cmcnt Divi•ion SANIPLE ANALYSIS REQUEST St.Ille: l..AbouLOry of P\ibli.: Hc.illh P.O. Box 28047, 306 N. Wilmini;ton St. Rolcii;h, North Carolina 2701 l-~047 Sit.c Number ______________ SamplclD Number/Name: ----=6'--'-I....Jj.._j'...J,......:g=::....L'/ _________ _ Name of Sit.c _-4(,c.Li:.......:...fr&Mw...::.=~:.iN-+-__,b~· ...::u_•fl/_._11-f_.____ Collected By ____________ ID# _____ _ SiteLocation _______________ Dat.cCollect.c<l ____ 3-__ ,_--_9'-'--_· ______ Time _______ _ . Agency: Hazardous WasLe Solid Wasu: __ Supc:rfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Result.s(mg/1) EnvironmenL'll Concentrate Comments arsenic - g ; J barium (Yl - Ground Water (1) Solid (5) cadmium ---chromium ./ -Surface: Water (2) Liquid (6) lead --- -mercury Soil (3) Sludge (7) selenium ---~ilvc:r - -=,other (4) -Other (8) -:,, - -Organic Chemistry Inorganic Chemistry - Parameter Resul15 (mg/I) Parameter Result.s(mg/l)(mg/kg) Organic Compounds ,Rcsult.s(mg/1) P&T:GC/MS antimony bc:nz..ene --- Acid:13/N Ext. 11rseruc carbon tttrachloride ---2,4-D barium chlordane: --- -2,4,5-TP(Silvc:x) -bc:ryllium chJorobc:nzcne - -chlordane: < a. "t?tb~ cudmium chloroform -- -beplllchlor < (7, "o,:,/ Pf'd' -chloride= o-crc=sol - -hc:xachlorobenz..ene < d. t1t117 ~ -chromium m-cresol - -hc:xachlorobutadic:ne I cobalt p-creso! -- endrin < "· ooo/AR,n copper crcsol ---lindane <',::J,t:JIJP,;1...,t,µ fluoride 1,4-dichJorobenz..ene ----methoxychJor <O, 00/ #hf -iron 1,2-dichloroethanc: - -toxaphc:nc: <0,110~.n, lead I , 1-dichloroethylene p~ --✓ <O•t?PO~ manganese 2,4-dichloroc=tl.Jylcnc: :e-.!~-F --~ -mc:rcury -hc:ptach.lor nickel hc:xachloroberu.cne ---nitrate bexachlorobutadiene ---selenium hcxachloroethane -- -silvc=r lllethyl ethyl kc:tone -FOR LAil USE ONLY sulfutc=s ni1roberucne -- 3 -1'1-97 .it) -thallium pc:n1.achlorophenol -Date: Received vanadium pyridine . ~(!&J_j-f/r -- -z.inc tc:trachlorocthylene Date Extracted "E-?-97Yf' - -pH -trichlorodhy kne ;P~'J-1965, -conductivity -2, 4,5-trichlorophen_ol Date Analyzed -'9-97-y'p -TDS 2,4,6-trichlorophc:nol - -fl ,i.:;h point -vinyl chloride= Reported By -endrin - lind.ane --Date Reported --mc:thoxychlor cr)~ff)""'I~,,_ toxaphene ...J .__,,. .. • ._ --Lab Number 2,4-D -- --2,4,5-TP (Silvc=x) DHS 3191 (RcviscJ 12/93) NC Dc-putrncnl of Environment, Hullh, & Natllr•l Rc,ourcc, Solid Wa•l<a t,farui,:cmcnl Divi ,ion SAMPLE ANALYSIS REQUEST Sllalc Laboratory of Publi, Hulth P.O. Box 28047, 306 N. Wil mini;1on S1. R•lcii;h, North Carolina 2701 l-M0'17 Sit.cNumbcr ______________ Samplc!D Number/Nllillc ____ (J_J_C,....__.1~~~5:.__ ______ _ Name of Site UJ vNfy Colb.:t~ By ____________ ID# _____ _ SiteLocation _______________ DateCollectdl __ _;)::;__--_I._-_Cf_, ______ Time ______ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1ds Result.s(mg/1) EnvironmenL'l l Concentrate Comments arsenic - 3 barium Y½ B - Ground Water (1) Solid (5) cadmium ---;z ~ -chromium Surface Water (2) / Liquid (6) lead -- ~e/4.d+--mercury Soil (3) Sludge (7) selenium ---. . ~ilver ~ilier (4) ~ - -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter Re:sul L5 (mg/1) (mg/kg) Organic Compounds ,Rbult..s(mg/1) ~)&T:GC/MS antimony benune --Acid:B/N Ext. llf!:>CfUC carbon tetrachloride -- -2,4-D <o. o o 1 l'/JtVl barium chlordane -- -2,4,5-TP(Silvex) <o ,oo,f,,Ml -beryllium chlorobenz.cne -chlordane cudm.ium chloroform --- -beptachlor -chloride o-cresol -hexachlorobenzene chromium m-cresol --- -hexachJorobuLac..!iene cobalt p-creso! --endnn copper creso! --- -linc..!ane fluoride 1,4-dichlorobenzene -- -methoxychlor -iron 1,2-dichlorocthane - _ to;tene -lead 1, 1-dichloroethykne -.,,-v-b -manganese -2,4-dichloroetbylcne --mercury -heptach.lor nickel hexachloroberucne ---ni Irate hexachlorobuuidiene ---selenium hexachloroethane -- -silver methyl ethyl keione -FOR LAB USE ONLY sulfates nitroberuenc -- 3 -p/-9 7&0 -thallium pent.achlorophenol -Date Receiv~ vanadium pyridine --/JJSi'i .3-J<i -9719& -zinc tetrachloroethylene Date Extractw.8.lltl .3-12 -~-:z ,B& --pH -trichJoroethy lene Date Analyze<l/JJ.,/1-3-..i-</~9 2 IJJ_tfJ -conductivity -2,4,5-trichlorophenol -TDS 2,4,6-trichlorophenol -/)/-rJ)-'f-J --17 ~ -fl a~h point vinyl chloride -Reportw By endri.n --lindane --Date Reportw -methoxychlor - ""', ""1 .f'•. ""Y} f . --tox aphene Lab Number ~ , .. , ,. ...,. 2,4-D -- --2,4,5-TP (S ilvex) Dl!S 3191 (R cviscJ 12/93) NC Dcpartmcnl of Environment, Hc...lL.h, & Narural Rc•ourccs Solid Wa•Lc l',fan..;:cmcn1 Divi,ion SAMPLE ANALYSIS REQUEST S!Atc Laboratory of P\Jblic Hulth P.O. Box 280-17, 306 N. Wilmini;1on S1. Ralcii;h, North Carolina 2701 l-~047 Sile Number ______________ Sample ID Number/Na.me ___ O_(_'{_CJ.;...(_~___;;b'-. ________ _ Name of Site __ G.)_--'.~--'-_.;...;._.----=N."--_(3_u_N_ty;....!_. __ Col!cett!<l By ____________ ID# _____ _ SiteLocation _______________ DatcColkcted ___ "'b_-_C_-_'f'--7....,__ _____ Time ______ _ - Agency: Hazardous Waste Solid Wast.c __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1ds Resu.H.s(mg/1) EnvironmenL'll Concentrate Comments arsenic - <-1 barium fJ1 g - Ground Water (1) • Solid (5) cadmium --- / Liquid (6) chromium - Surface Water (2) lead -- -mercury Soil (3) Sludge (7) selenium --- ~Other (4) :,ii ver - -Other (8) - - -Organic Chemistry Inorganic Chemistry - beter Rc;ults (mg/I) Parameter Resu.1 ts (mg/l)(mg/kg) Organic Compounds .Re:sult.s(mg/1) &T:GC/MS antimony bcnunc --Acid:ll/N Ext. arscruc carbon tttrachloride ---2,4-D barium chlordane --- -2,4,5-TP(Silvex) -beryllium chJorobcnzene -chlordane cadmium chloroform --- -hepwchlor -chloride o-crcsol -haachlorobenzene chromium m-cresol --- -hcxachlorobutadicne cobalt p-crcsol --cndrin copper crcsol ---lindane fluoride 1,4-dichlorobenzene --- -methoxychlor iron 1,2-dichloroethane ---toxaphene -lead 1, 1-dichloroethylene ---manganese -2, 4-d ichloroetl.Jy lcne --mcrcury -hepwchJor nickel hcxachJoroberu.cne ---nitratc bexachlorobut.adiene ---selenium hexacWoroetha.ne -- -silver 111cthyl ethyl ketone -FOR LAB USE ONLY sulfates ni1roberuenc -- 3 -/ 'I -9 7 && -thallium pcntachloropbcnol -Date Recei vt!<l vanadium pyridine -- -21nc tetrachloroethylene -Date Extracted pH trichJoroethykne -- 3-/8--c;-; /\IT -conductivity -2,4,5-trichJorophenol Date Analyzed TDS 2,4,6-trichlorophenol -- -Jhsh point -vinyl chloride Reported By endrin --lindane --Date Reported --methoxychlor "' t""1 n """ :1 r:-toxaphene ,...,l' i....i • '" ..... --Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3191 (Rcvi~eJ 12/93) NC Dcpanmcnt of Environment, Hullll, & Nawr,I Rc,our,c, Solid w •• ~ hl•n.ai:cmcnl Divi,ion SAMPLE ANALYSIS REQUEST S!Jatc Laborai.ory of Publi, H""llh P.O. Box 28047, 306 N. Wilmini;ton St. Ralcii,;h, North Carolina 27011 -8047 Site Number ______________ Sample ID Numbc::r/Name ----'0_" ..... {_:(~9~8>"_7~-------- Name of Site __ L,,;..._.;...AA_;._..~-~-&_1 _· c.,1----'--;..,_·w ___ Collected By ____________ ID It _____ _ Sitel.Dcation _______________ DatcCollecttil ___ ' .... )~--S-_-_'<_1 _____ Time _______ _ - Agency: Hazardous Wast.e Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1ds Re:;uJLS(mg/1) Environment.'ll Concentrate Comments arsc::ruc - ·j Solid (5) J PrB -<A barium - Ground Water (1) cadmium --chromium -Surface Water (2) Liquid (6) lc::ad --- -mercury ~Soil (3) Sludge (7) selenium --~ilvcr - -0thc::r (4) -Other (8) - - - Organic Chemistry Inorganic Chemistry - Parameter Re:Sults (mg/I) Parameter Re:.uJ ts (rng/l)(mg/kg) Organic Compounds .Rbull.:i(mg/1) P&T:GC/MS antimony bcn.z.enc:. --_/ Acid:13/N Ext. arscruc carbon tetrachloride --2,4-D barium chlordane ---2,4 ,5-TP(Silvc::x) beryllium chlorobcn.z.c::nc:. ---chlordn.nc:: cadmium chloroform --- -bepLachJor chloride:: o-crc::sol --hc::xachloroben.z.ene chromium m-crc::sol --- -hc::xachloro bu tad icnc:. cobalt p-crc::sol --endrin copper crcsol --- -lindane f1uoride 1,4-dichloroben.z.ene -- -methoxychlor iron 1,2-dichlorodhanc -- toxf'ihc::nc:: lc::ad 1, 1-dichJoroc:.thylene v eJi//:i 6oJ 't'I. I P/'tt1 -- -m.:u1ganesc:: -2, 4-d ichloroctby lc::nc l-A '.:., ~~ .. -.,,~~ ;J'l!L." , ... -macury -hcpt.J.ch.lor nickc:.l bcxachlorobenzcne -~_d_d,,,d1,n> t: a ir e rs--- -nitrate bexachJorobuCJldiene --selenium hexacbloroetbane --silvc::r methyl c::thyl kclone --FOR LAil USE ONLY sulfates n.i1robenunc -- 3-1'1-978[;; -thallium pcnuichloropbc::nol -Date Received vanadium pyridine --fCIJ ,i-.:l4-97;f P 21nc 1etrach1oroethylene --Date Extracted BJJd ~~L 'fl4 '1A -pH -trichloroethy Jene PCB ~-S-97 7/P -conductivity -2,4,5-trichJorophenol Date AnalyzedBµA 3-2,.'[-,97 Bf) TDS 2,4,6-trichlorophc::nol -- -fl,L!>h. point -vi.nyl chloride:: Reported By endrin --lind.ane --Date Reported --methoxychlor ,....,, .... 10,,-,.,or toxaphene -t . ., ... 1 --Lab Number 2,4-D -- --2,4 ,5-TP (Silvc::x) Dl!S 3 l 91 (R,viscJ 12/93) NC Dcpartmcnl of Environment, Huh.h, & Narual Re•ourccs Solid WdL<: Man.a,:emcru Divi,ion SAl'vfPLE ANALYSIS REQUEST SIJlle Laboratory of Public Hc..:.Jth P.O. Box 28047, 306 N. Wilmini;ton St. R•leii;h, North C.rolina 2701 l-li047 Site Number ______________ SlllllplcID Numbcr/Nu.mc ___ O=--_,_\<(+-'Cj..._f_~---------- NameofSit.e ---"lw<.,,-v;:...·..LMA,.-'-..L.:!....!C..::~-N~_Co_...::v_V\J-=-N __ Collected By ____________ ID# _____ _ SiteLoc.itioo _______________ DateCollected ____ :).__-_L,_~--'-7 _____ Time ______ _ Agency: Hazardous Waste Solid Waste ._./Superfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Result.s(mg/1) EnvironmenL'll Concentrate Comments arscruc - j A-B-Bf} burium ~olid (5) -Ground Water (1) cadmium --chromium -Surface Water (2) Liquid (6) !cud --- -mercury _--soil (3) Sludge (7) selenium --:.ilvcr -Other (4) Other (8) --- - -Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Orgaruc Compounds ,Rc;:;ult.s(mg/1) P&T:GC/MS antimony bcn.unc ✓ Acid:13/N Ext. --arscruc ca.rboo tetrachloride ---2,4-D barium chlordane ----2,4,5-TP(Silvc:x) -beryllium chlorobcn.zcnc: -chlordane: cadmium chloroform --- -hepLachJor -chloride o-crcsol -hcxachlorobenz.ene chromium m-cresol --- -hc:xachlorobutadicne cobalt p-crc:sol --endrin copper cresol ---lindane fluoride 1,4-dichlorobenz.ene ----methoxychlor -iron 1,2-dichloroethanc -1oxaphc:nc -lead 1, 1-dichlorocthylcne ~ ,ee,~o) 90,rtf1!111 - -ma.nganese -2, 4-d ichlorocl!Jy !enc .~_s /;"'-~r pJ~<t, I-a /Jfo -mercury -hepwch.lor _d;i./tlL ,,,.,,, r tr vhfiu H) -nickel hexachloroben.zcne / -nitrate hc:xachlorobutadiene ---selc:nium hc:xachlorocthane ---silvc:r ruc:thyl ethyl ketone -FOR LAil USE ONLY sulfates nilroberucnc -- Date Received . 3 -/Y -97 fj,Q -thallium penlllchlorophcnol - -vanadium pyridine -. ~ 3-.1~-97V,:, -zinc telrachloroethylc:ne -Date Ex I rac tedl:!,µ A3--J 'i -4'7 M -pH -trichloroethy Jene Pc:.B 'I-S-97Vp -conductivity -2,4,5-trich.lorophenol Date Analyzed &llf 3 -2.~17 /JJ_ TDS 2,4,6-trichlorophenol -- -lhsh point -vinyl chloride Reported By -c:ndrin - lindane --Date Reported --methoxychlor ~ .... 40 '"':q ---toxaphene Lab Number ....... , ,; -...;'.,. 2,4-D -- --2,4,5-TP (Silvcx) DHS 31 91 (Rcvi~etl 12/93) NC Dcpanmcnt of Environment, Hullll, & Nao.ir•I Rc.ourcc, Solid Wa•l.c Marui:cmcni Divi•ion SM1PLE ANALYSIS REQUEST SiJatc Laboratory of Publi.: Hc.ilth P.O. Box 28047, 306 N. Wilmini;ton St. R•lcii;h, North Carolina 27ol l-W·l7 Sit.c Number ______________ Su.mp le ID Number/Nu.me ___ O__,_\ _'t,,_j_._-'~'--'1.,__ _______ _ Name of Site __ LJ____,~--'-....:...A_V_¾j_.___G> __ uM~YY~-Collected By ____________ ID# _____ _ SiteLocation _______________ Dat.cCo!lected __ ___,;>~--'5:;_ ... _-_':z"'---'1-· ______ Time _______ _ Agency: Haz.Mdous Waste Solid Wast.: __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Results(mg/1) EnvironmenL'll Concentrate Comments arseruc - ::;;;solid (5) p~ barium ..1A0-- Ground Water (1) cadmium --chromium -Surface Water (2) Liquid (6) lead --- ~Soil (3) -mercury Sludge (7) selenium --~ilver - -Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter R~ults (mg/I) Parameter R~ul ts (mg/I) (mg/kg) Organic Compounds .Rcsults(mg/1) P&T:GC/MS antimony bcnunc ✓Acid :B/N Ext. --arseruc carbon tetrachloride --2,4-D barium chlordane --- -2,4,5-TP(Silvex) -beryllium chJoroben.:z.cne -chlordane cadmium chloroform --- -bepi.achJor -chloride o-cresol -hexachJorobenz..ene chromium m-cre.sol --- -hexachJorobut.adiene cob.Jt p-cresol --endrin copper crcsol --- -lindane fluoride 1,4-dichlorobenzene -- -methoxychJor -iron 1,2-dicWoroethane -toxaphene/J, _ lcac.J 1, 1-dich.Joroethylene ,7 p"t:..P, 1/:1./oO. ~ -- f:J?Jd s ov<-rW d',1u c.1 • -nunganese -2,4-c.lichloroctliylene -mercury -heptachJor J]/4M, f, f/lV:J -r 4. V" /-/ e,. /-5 nickd hc:xach.loroberuene --nitrate bexachlorobutadiene ---selenium hexachloroethane -- -silver methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobc:112.Cnc -- 3 -J'/,?7B~ thallium pc:nwch.lorophenol --Dace Received vanadium pyridine --~ .;J-~~-97J/P -z.inc 1etracWoroethylene -Dace Extracted ~'A!?-a:._-7.'"]r:l,() -pH -trich.Jorocthy lcne ftB i/-S-9-:nlP -conductivity -2,4,5-tricWorophenol Date Analyzed ~A:3-,15:-27B..Q -TDS 2,4,6-trichlorophenol - -fl,1,.';h point -vinyl chloride Reported fly -c:ndrin -lindane --Date Reported -melhoxychlor - :--.~ "10"' --toxaphene Lab Number ~-·f ,,. •✓ .. ,.,~ ... 1t 2,4-D -- --2,4,5-TP (Silvex) OHS 3 I 91 (Rcvi,cd 12/93) NC Dcpartmcnl of Environment, HulU'l, & Narur•I Rc:•ourccs Solid W1•1<: l'>l1rui;cmcru Divi•ion SA.~LE ANALYSIS REQUEST S1Ja1c: Laboratory of Public Hc.ilth P.O. Box 28047, 306 N. Wilmington St. R1ki.i;h, North Carolin, 27ol l-~047 Sit.c Number _______________ Sample ID Number/Name ____ 0_/ _.1_1...:.......,<f.__0 _________ _ NameofSite vJ ~ ~aW 0~"(l{ Collected By ID# ____ _,_....:.,___;__.a,_ ____ _,;___ --------------------- Sitel.Dcatioo DateCollect«I ·; :§~q 7 Time ----------------------""--'---------------- - Agency: Hazardous Waste Solid Waste __ Supi:::rfund TCLP Compounds ---- Sample Type Inorganic Compow1ds Results(mg/1) EnvironmenL'll Concentrate Comments arsen.ic - ~Solid (5) NIA -Tit barium - Ground Water (1) cadmium --chromium - Surface Water (2) Liquid (6) lead --- -mercury .../ Soil (J) Sludge (7) selenium --~ii ver - -Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Rc;ults (mg/I) Parameter Re:;ults(mg/l)(mg/kg) Organic Compounds .Rcsults{mg/1) P&T:GC/MS antimony bc:nunc ✓ Acid:B/N Ext. -- !if!>C!UC carbon tetrachloride ---:2,4-D barium chlordane --- -:2,4 ,5-TP(Silvcx) -beryllium chJo robc:n.zcne -chlordane cadmium chloroform --- -bcpt.achJor chloride o-c reso1 --hcxachlorobenzene chromium m-crcsol --- -hcxachlorobutac.Jiene cobalt p-creso! --cndrin copper crc:sol ---line.Jane fluoride I ,4-dichlorobenzeoe ----mcthoxychlor iron 1,2-dichloroethane -- tox2hene ~ lead 1, 1-dichloroethykne --.,,,-t,S :t~o) ~ 7, '.tf20' -manganese -2, 4-dichloroetliy lcne rF-iA s ~~<4 ~ h kf -mercury -hc:pwch.lor ·::.a) lvt f I t::. 4A/h' ht c fr nickel hc:xachloroben.zcne / ---nitrate bcxachlorobutac.Jiene --selenium hexachloroctbane --silver llletbyl ethyl ketone --FOR LAB USE ONLY sulfates n.itroberu.cne -- . 3 -I </--97 t9 ;.0 thallium penuichlorophenol --Date Received vanadium pyridine --. ~ $-;J.l/-97YP 21nc let rachloroeth y Jene Date Extracted 'IJ!ilf 3 -LJ..-<j__z&() ---pH -rrichloroethy lcne 00 l/-s-=-?7J/I-' -conductivity -2,4,5-trich.lorophenol Date Analyzed MA 3 -..lr-91&9. TDS :2, 4 ,6-trichlorophenol -- -fl ash point -vinyl chloride Reported By emlrin -- lindane --Date Reported --mc:thoxychlor ...-1c,,.,.or---toxapheoe Lab Number • .,J ( \.-·, .. 1....., 2,4-D -- --2,4,5-TP (Silvex) DHS 3 !9! (Rcvi1cJ 12/93) NC Dcputmenl of Environment, Hc.ah.h, & Nall.Ira) Rc,ourcc, Soli.J w .. 1.: hlarui;c:mc:m Divi,ion SAMPLE ANALYSIS REQUEST S1.1&tc: Laboratory of Publi~ Hc:.1llh P.O. Box 28047, 306 N. Wilmini;ton St. Ralc:ii,:h, North Carolina 27011-~047 Site Number _____________ Sll!Ilplc!D Number/Nllille ____ O___:.\_~_q._q-'-'-f ________ _ Name of Site lJ fr(lA,,..& W Gviv"M Collcct~ By ___________ ID//' ____ _ Site Location ______________ Date Collcctcd ____ >_-_0_-!{____.__f ____ Time ______ _ Agency: Haurdous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type lno~anic Compow1ds Re:;ult.s(mg/1) EnvironmenL'1I Concentrate Comments arseruc - ~olid (5) -'NI A--GA barium -Ground Water (1) cadmium --chromium - Surface Water (2) _ Liquid (6) le.id -- _0oi1 (3) -mercury Sludge (7) selenium --:;ilver - -Other ( 4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter Re:;ul ts(mg/l){mg/kg) Organic Compounds ,Rbult..s(mg/1) P&T:GC/MS antimony benzene -v"Acid:B/N Ext. --arscruc carbon tetrachloride --- :2,4-D barium chlordane ---:2,4,5-TP(Silvex) beryllium ch.lorobcnzcne ---chlordane cadmium ch.loroform --- hepwch.lor chloride o-cresol ---hexachlorobeo..z.ene chromium rn-cresol --- -hcxachlorobutadiene cob.ill p-cn~sol --endrin copper crcso] ---lindane fluoride 1,4-dichlorobeo..z.ene --- -methoxychlor -iron 1,2-dich.loroethane -_ tox.ph,n,031 . lead l, 1-dich.loroethylene -- -manganese 2, 4-d ichloroctliy lcne V f'Cfz 1/~ 0}~ -. ' . ,t(' -1,1.(,. • heptach.lor {~4L~;M r €!;_; 'cf s -mercury -nickel hc:x.ach.lorobenz.ene --ni tralc hexachlorobutadiene --seh:nium hexachlorocthane --silver methyl ethyl ketone --FOR LAil USE ONLY sulfates nitrobe.rucnc: -- 3 ~1/-97/U) thallium penuichlorophenol --Date Recei v~ vanadium pyridine --~~ .3-..i~-97-vP 21nc tetrach.loroethylcne Date Extracted /31.)/J-3t.f..-42AD -- -pH -trich.loroethy Jene pa,e 'f-S-97-V,.O -conductivity -2,4 ,5-trichlorophenol Date Analyzed BAJ/t 3 -2 f -77 /4 Q -TDS 2,4,6-trichlorophenol - -fl,j_!;h point -vinyl chloride: Reported By --endrin lindane --Date Reported --methoxychlor r-~~1 Ao toxaphene _.,.· • · t: __ •rl --Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3 I 91 (Revised 12/93) NC Dcpartmcnl of Environment, Hc.alLh, & Nalllr1I Rc,'°urcc, Soli~ Wa,t.: Marui,:cmcnl Divi,ion SAMPLE ANALYSIS REQUEST S!Jttc: Laboratory of Public He.tlth P.O. Box 28047, 306 N. Wilmini;1on St. R•lcii,:h, North Carolina 2701 l-H047 Siu:Numbcr _____________ Sa.mplcIDNumbcr/Na.me CJ j9' q C, 2- Name of Sit.e -----=U) __ M_. ---"-'&_._c_M __ &c....1 _l.AN __ rv~-Collated By ____________ ID# _____ _ SiteLDc.ation _______________ Dat.cCollectcd __ -'3=::--....::L:..___-_q_, _____ Time ______ _ Agency: Hazardous Wasc.c Solid Wasu: __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s Rbu.llS(mg/1) EnvironmenL'll Concentrate Comments arsenic - ~olid (S) PA barium N '/\ --Ground Water (1) cadmium --chromium -Surface Water (2) Liquid (6) le.id --- -mercury _.!L Soil (J) Sludge (7) selenium --~ilver - -Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Rc;ults (mg/I) Parameter Re:;uJts(rng/l)(mg/kg) Organic Compounds ,Re:sul lS(mg/1) P&T:GC/MS antimony ben.z.ene --/ Acid:B/N Ext. 11r!.CillC carbon tttrachloride --2,4-D barium chlordane ----2,4,5-TP(Silvc::x) -beryllium chJoroben.z.cne -chlordane cadmium chJorofonn --- -beptuchlor -chloride o-cresol -hcxachloroben.z.ene chromium m-crcsol --- -hexachlorobut.adiene cobalt p-cresol --cndrin copper cresol ---li.ndane fluoride 1,4-dichlorobcnzene ----mcthoxychlor -iron 1,2-dichlorocthane -loxAhene lead 1, 1-dichloroelhy Jene ~ ~l?,(f:i6~) /S0,51F1 -- -manganese: -2, 4-dichloroel11ylene mercury heptach.lor _£t .. ~ 5!"' a&~,r --nickel hexachloroben.zene --nitrate bexachlorobutadiene ---selenium hexachloroetha.ne ---silver methyl ethyl kelOne -FOR LAil USE ONLY :.ulfutes ni1robcn2enc -- Dale Received J-/Y,-97 ,8~ -thallium penlllchlorophenol - -vanadium pyridine -. ~.,-3 -...1-Y-97111 -zinc telrachloroethylene Dale Exlracted &JA-3i f -z_ 2£1~ - -pH -trichloroc::thy Jene PcB "I-S!-97YJ -conductivity -2,4,5-trichlorophenol Date Analyzed f>,.JP,,3~2,(p -£ 78 -TDS 2,4,6-1richlorophcnol --11.t.!ih point -vinyl chloride Reporlcd By endrin -- lindane --D ate Reported -methoxychlor -! t4"-1l ~r11 .,,, -toxaphene ....,,_,: ~ ... -Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3191 (Rcvi~eJ 12/93) NC Department of Environment, Hullh, & Natural Rc.wurcc, Solid Wu1c Ma11Ai;cmclll Divi,ion SAMPLE ANALYSIS REQUEST S1a11c: uboratory of Public Hulth P.O. Box 28047, 306 N. Wilmini;ton St. Ralcii;h, North CarolillA 27611-8047 Site Number _______________ Samplc:ID Number/Name: _________________ _ Na.meofSite WAf!_l<-E,J e.ou NT y Collectc:dBy _____________ lD# _____ _ Sitel.ocation ______________ DateCollected __ 2_-_2_a_-_9__.,7 ______ Time ______ _ Agency: Haz.a.rdous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compowid.s Result.s(mg/1) Environment.'ll Concentrate Comments arseruc - /5LA-tJ Jc:. 5/tlJJ> barium -Ground Water (l) Solid (5) cadmium ---chromium -Surface Water (2) Liquid (6) -lead ---mercury Soil (3) Sludge (7) selenium --- ✓Other (4) silver --Other (8) ---Organic Chemistry Inorganic Chemistry - Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compowids Rcsulls(mg/1) -P&T:GC/MS antimony bc:nz.enc: --Acid:B/N Ext. lirSC:IUC carbon tetrachloride ----2,4-D -barium chlordane --2,4,5-TP(Silvex) -beryllium -chlorobc:nzc:ne chlordane cadmium chloroform --- -heptachlor -chloride: o-crc:sol -hexachlorobenz.ene chromium m-cresol --- -hexachlorobut.adic:ne cobalt p-cresol --endrin copper crc:sol ----lindane fluoride 1,4-dichlorobenz.ene -- -methoxychlor -iron 1,2-dichloroethane -toxa~e -lead l, I -dichloroc:thylc:ne -ve_ <O, JO '¥1-tJJ -manganese -2,4-dichloroc:thylc:nc: r mercury heptachlor ---nickel hc:xachlorobenzene ---nitralc: bexachlorobutadiene ---selenium hexachloroc:lhane ---silvc:r methyl ethyl ketone -FOR LAB USE ONLY :.ulfates nitrobenzc:nc: -- 3-1'1-9713& -thallium pc:n!Jtchlorophenol -Date Received vanadium pyridine:: --. ,pee~ -z.inc tetrachloroethylene Date Extracted 3 -;1.t/-CJ7VP --pH -trichloroc:thylc:nc: Date AnaJyJ~f S-</7VP -conductivity -2, 4 ,5-trichlorophenol -TDS 2,4,6-lrichlorophenol --flu.sh point -vinyl chloride:: Reported By --endrin lindane --Date Reponed --methoxychlor r'"!,•-11 0-()r.., --toxaphenc: Lab Number . 'C qA. 2,4-D ----2,4,5-TP (Silvex) OHS 3 I 91 (Revised 12/93) Na6EHNR Division of Waste Management D Superfund Section D Hazardous Waste Section □ Solid Waste Section Organics Lab: __ Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: (c u u Sampled By: "5,..2 fc Site ID # (NCD#) Sampler ID Location: l,v.a v-~.,.. Co. Telephone:L_J 733-061-i..... Address: Date Sampled: 3-/2.-Cf? Time Sampled: Sample Types: Soil Water ✓ Waste Other Remarks: ~ /f),Q-\ ~ Field Sample Numbers ----· --·--·-----. Relinquished By: ~,4 • A 62 ✓-~ Date: :J -·12 _q7 Time: ll :50 (S il'nature) I Received By: ~~;;--=-Date: 3 -o<,--CfJ Time: / -:' 50 (Signature) Relinquished By: ~~']-::-Date: )-'lf-4 --r Time: /~-· &'-i ~ (Si!rnature) Received By:__:-;&..t/ ~ lk..e,.,,;;Z Date: 3-;'-/-97 Time:/ C.: DO (Signature) Relinquished By: Date: Time: (Siimature) Received By: Date: Time: (Signature) Results Rep~?i~~---£~#__/ Date: 1/Y .3"l7/f 7 Time: / , - NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: X Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: w I\"'"'€ .J C.IAH-rt Sampled By: SiAic Site ID # (NCD#) Sampler ID Location: Telephone:(lf/4') "1.3? zfD/ Address: Date Sampled: -:J 7 I J /'f"') Time Sampled: Sample Types: Soil Water 'I. Waste Other /LG I ~f J fl I ./ ... SLB-1 , ---/ Remarks: CD-I PJ D-l /> a A/(.-I QRR..-3 ,.AOP Y "BJ D y .., Ai)~ i ,) ,,_.. ~ ,~ R i-j ,,, 6 ZM I E z.. ;i., '3 -. c.-v>7 t./ J ,../V DI/ I ~ov ~"\ .,,.1v o ✓ '-/ .,'4£.-1 /:t SR-l Field Sample Numbers Relinquished By: .s-t ... •rl Fcrp../" Date: ~/11/1117 Time: /,:,, (Signature) ~ vy Received By: % Date: J -0-11 Time: 17 1 v'D ?-]__:__ (Signature) ~ Relinquished By: 7./-7 ,,3~ (Sii:mature) Date: 3-N~97 Time: ("~-..>=- Received By: 7&:u~/1<.tJ Date:3 -J</-97 Time: /t, ! ~ (Signature) Relinquished By: Date: Time: (Sii:mature) Received By: Date: Time: ~ure) Results Repoe ed: J-4.,, ;f~---Date:W5//l 7 Time: :gti/t ,, ,, /" / (Si ture) ., V NC-DEHNR Division of Solid Waste Management D Superfund Section ,El. Hazardous Waste Section D Solid Waste Section Organics Lab:~ Inorganics Lab: ... K..._- {<~..._\,\-~ .¢,."w,v.,\~ \.,e \fV\e-..'\-c:~ -\-o r~·<-~ ~. 0etr V\f ':> 7 Toe\ r{: rsc\.-\ Y\o{A s;, ,· e"'-t c. 1'idv,SOv5 f C 6 4"'<' {:; I J CHAIN OF CUSTODY RECORD Project Name: f> (._ ~ \... e,..,._~ Q,~ Sampled by: <;_A ~~ te. ~ (>{e. Site ID# (NCO#) Sampler ID Location: w A.::ilt::2 io:1 (o"'-...... ~::) Telephone: M ) !]~3 -J \') g j ~3) Address: ' Date Sampled: !2 }'Z i }~:I Time Sampled: ''l ·. '2,£) t:J'I'-",. Sample Types: Soil i Water Waste Other Remarks: \-\Y\\ l Lee e, Ll. (_ I ( ,·c.e ) a_j --I • I ··~ . Urn?l I A{\)/ Ill: Field Sample I Numbers Relinquished by: sa..,.....~)/_cf ~,rove q ate: ::J jzi },1 Time: 3·,4o~t'""\ (Signatu~e) ! Received by: ••··••• ~~n~l;:e) .. :..._ .. ' .. ,-·--·······-·············Date:~ "GJT<r? ·Time:· 3 . '.:I a· /'i,,_._ •··• Relinquished by:M.A M "'~ J A Date:~/ J /c,7 Time: { ( £g Ar-v--:- (Signature) Q . Received by: -?~ 2-~ Date:J -~) -". 7 Time: I/-':;_..., ✓• (Signature) Relinquished by: -JL ~-Date:>-tV-9, Time: 1,. <.!JC. ,, ,7' ~ (Signature) ~ -----------------.----i.fl.t ----------------------------------------------------------------------------------------------------Received by: ~,,(, ~ Date:3 ·-Jf-97 Time: /6: cR> ,, t<:~ature) Results Repo~~ }f /UA/L-Date: ~cA Time: 'g,{a£ure) / ~ (A:\COCRFRM) .. Page_of_ SOLID WASTE MANAGEMENT DIVISION Receipt for Samples Name of Firm Firm Address Firm Owner, Operator, or Agent Title SAMPLE ~QLLECTED SAMPLE TYPE NUMBER DATE!TIME WATER:sorL:oTHER - Receipt for the sample(s) descnbed · above is hereby acknowledged: Signature of Inspector Title l2YPLICATE SAMPLE §aHPLE LOCATION OFRD 1ACPT!RJCTD ONSITE!OFFSITE Rece1pt/reJect1on of duplicate or split samples is hereby acknowledged: Signature of Firm Owner, Operator, or Agent Title Comments: _________________________________ _ (A:\COCR.FRM) NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: / Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: fee, 4,.,_J+i I ( Sampled By: S~t-e.. Site ID # (NCD#) Sampler ID Location: <.,.J' o-.,rQ,, Co..,,...+-'t Telephone: (j_fl_) 73 3 -~17 ~ Address: Date Sampled: 3/'-l/'17 Time Sampled: t_o 30 Sample Types: Soil ~-Water Waste Other Remarks: All f" i e Id sa. ""'~ le f\\/W\.J,.q,') Cd{fec.J~c:O f' ('G"YY\ Sa.O'Y'e vJQ. { ( / "c « I-, cm Field Sample ~A.A -I \~ Numbers w~-10. KM -3 Relinquished By: · z~ {)&~ Date: 3/1.r/q7 Time:"JJ)..3D (Siimature) Received By: -2~;3~ (Signature) Date: ;>-"l -1 1 Time: 2-42 t :J o Relinquished By: #----=--r= ;!i---::-. Date: ;:,-f<I-?, Time: /~.Oc> (Si1mature) Received By: '7(!uLf,<tk~-r Date: 3-1 'I~ 97 Time: /t:,:cf?:) - (Signature) Relinquished By: Date: Time: (Si !'nature) Received By: Date: Time: ~ignature) . Results Rep~ / ~~-Date:l/'/.J>Vl.7 Time: natur~ / / ' - NCDEHNR Division of Waste Management D Superfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab: ✓ Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: Pc e, Le\nJ.h I( Sampled By: cs~f-e Site ID # (NCD#) Sampler ID Location: W-o..rret"'\ (d, /v r._ Telephone:~ 733 -?-.n8 Address: Date Sampled: 3[5/Cf, Time Sampled: i L.('-(0 Sample Types: Soil y Water Waste Other Remarks: A ti -f:1' t' ( J ~a ~le t'\ v W'\ lofrs ~/cen. -.f ,(l'w\ San"~ v--' ~ { ( Id c c-_f ,u"' .. Field Sample OM-r 0-, 4 ~ Numbers 9, ., :c:: 01"\-:, Relinquished By: T~9tvJ,i.v, Date: 3/5 /c;7 Time: aoos (Si1mature) T Received By: ~>--~ Date: ';>-S--4r"1. Time:"1-o c>: .. '> /' (Signature) Relinquished By: 7/4 r 7 ~ __,_ Date: 3i--ry-t? 1 Time: / (,; .0 cJ (Si1mature) Received By: ~&~ Date: 3 -/ 'I:-~7 Time: /(:,: ~ (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time: (Signature) Results Reported: (\ / /!./le~ Date :l//471/ t?/ Time: ' (~ ,, , ,. , ,/' I' ~natll_r.~- II NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: __ Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: Pcf3 lG\.~~~ 11 Sampled By: S~t-~ Site ID # (NCD#) Sampler ID Location: lv'o...rr-eV\. C.o V 1'\ -1-'f Telephone:CTd) 733 -~178 ; 3/3 /?7 Address: Date Sampled: Time Sampled: / (; 3 0 Sample Types: Soil 'i Water Waste Other Remarks: All fie / J Sa.-~ ( ~ nvrnlo ers. fo.J:.er-. --f,o/Y\ SQ..""'-(( V,./ '?_ I/ { cl C<A..i-i O Y\ c Field Sample w fl\ -, ~ 5" Numbers ~'0,R W,A -3 Relinquished By: ;,!,-r ~ 0 /2 ~ ffe,.,,t Date: 3/ 3 /'f7 Time: ~0/0 (Si1mature) 1 Received By: ~ rJ .. Date: J/3/f7 Time: ;;10: 1 J -~,- (Signature) Relinquished By: 7 ~ T-'--Date: 3-$-q,,7 Time:/4:-: 0 ° (Siimature) 7 Received By: ~&<_~ Date: 3-J</-9 7 Time:/~: CJ'V (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time: _(filgnature) ~ Results Rep(rted: ) "~~, f. /!L&'-l.A' Date:1/Pd/_9 Time: cs£9"tture) ) ,, ~-------- NCDEHNR Division of Waste Management D Superfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab: -- Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project N ame:_~p _c_-----=-[2 _____ _ Sampled By:_5,c_·_,_t:,..,_k-'-------- Site ID # (NCD#) ---------Sampler ID _________ _ Location: Wt,,,c.,,.e,"" Co....,,,..h Address: ------------ Telephone:('1<~) 7 ·~ 3 ·-L-1 7 8 Date Sampled: 2.. /;z ( '( 7 Time Sampled: / f : o o ,1 ~ Water X Waste Other Sample Types: Soil~ --------- Remarks: ------------------------------- Field Sample S"o; ( Numbers Relinquished By: (Signature) Relinquished By: ~ ] ~ Si nature ,. Received By: ~ ~ ~ Results Rep Date: "5>/¥11 1 Time: /3 : ... c.:- Date: 3 7'-~, Time: 7~.: O'-CJ Date: 3 -/'/-jJ Time:/(:, . .' de) Date: NCDEHNR Division of Waste Management D Superfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab: Y Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: Pc 0 L,ll'-j ('; { I Sampled By: s tu..+ e Site ID # (NCD#) Sampler ID Location: Wo.. r-.-e"" (Glv/'\➔'_f.. Telephone:~ 733 -;) .. ..i)'i Address: Date Sampled: 3/6/97 Time Sampled: 0 Cf '-t5 Sample Types: Soil X Water Waste Other Remarks: r:::;eid Sc{ ,.,..fJ I~ s. ~ I( S0...h-f2-( eJ -(, <TrA. Sb. t'Y' e (..,Je / I I oc,, . .:/;'q'y\ i Field Sample MM -/ Numbers _MM -3 Relinquished By: T~~~ Date: 3/6/ct? Time: 2030 (Siimature) Received By: A? 2:r~ ::, Date: '"J~--i-, Time : -i-o~ ;, ..., (Signature) Relinquished By: ?/4_.-:, J..--::-, (Siimature) 1 Date: 1 ..... f'f-47 Cr'" Time: /C" ~ Received By: -t&u ilt.., n~d4 -1-Date: 3 ~ I</· 97 Time:/?;~ (Signature) Relinquished By: Date: Time: (Siimature) Received By: Date: Time: ~ture) Results Repoit~d: ~ ~/Un./ Date: ~.5ij fl:J Time: . c-s/mlature) / / ~ ........ (I :\docshare\cocr. frm) NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: X Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: 'Pc 6 Lu..f'J{,· I ( Sampled By: S 1-c,.. ~ e Site ID # (NCD#) Sampler ID Location: Uvo.. ( ,r --e" (ovn"ty Telephone:(9 19 ) 7 3 3 · ;J..17 8 Address: Date Sampled: 3/6 /c;-7 Time Sampled: r 7 15 Sample Types: Soil Water ·x Waste Other Remarks: 1-; e ( J sa. W'-/J It> r-rivmb er S "--I ( S"-'~f I~ d .f'r ,.l"Y" S C<.i'l"P ( 4 cuf,~ -- Field Sample )/413 --I ------· ---------------- Numbers /I\B-3 ---·--------- ,NI (3 -'-/ -·--------------·----·----------·- Relinquished By: ~a~ Date:_ 3/C/cr--, Time:d__Q_3_o __ (Signature) ---- Received By: ~ ~ ' Date: 3--zl.--? 7 Time: -z.,-,~0 <.. (Signature) Relinquished By: ~J~ Date: 3.-/f{._-'f7 Time: / (\ ~ (Siimature) Received By: ~Lk-~ Date:3-/f-97 Time:/~: ~ (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time : (Signature) --- Results Repo~~1;;;.'.!~";f~1-... R ,A~~.F Date:C/..?~? 7 Time: , / ,.,.. (l:\docshare\cocr.frm) NCDEHNR Division of Waste Management Organics Lab: / Inorganics Lab: __ □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section CHAIN OF CUSTODY RECORD Project Name: frudw~ f'1r1 .... J Pc5 La.,,~..(;1 I Sampled By: VJ,~ 2!~, Site ID # (NCD#) I Sampler ID Location: i).Jcr)·•t,t,t-(,,.,,, ) N c.., Telephone:(~1-,) B7z -zc,,,1oo Address: S£ ltoo4-Date Sampled: '3 ''5"-<;)"'7 Time Sampled: I 5·, ?o ..\-It, ~tS" Sample Types: Soil x Water Waste ',< Other (emarks f'w, T,i.~~• -PA-~~ {.;", "Pelo I P.:>N A -"-,;c,..;;. kttl:J. ~ 15 f!/5~ ~(> 1 St • .!s-- I I I It I i I i Field Sample JAB-,A lJJA-'TA j.N;13~ I -I JA~-~A NIA-BA ,'ttd!:> eB 1 Numbers I JAB PA kl1A ::PA ----------- i. Relinquished By: wa-bcl/ ;~: _,/. Date: 5/tQ(f>1 Time: 9 iZf ! (Signature) / Received By:~~ ~ Date: a 4, /q7 Time: 11 2 ... :1..--- I I I I I (Signature ' 1, I Relinquished By: e ~ I! f) .J,;,o Date :~~4-J Time: lj__/S-1 rMimature) / I I Received By: ~~~~ Date: J -~_.c;7 Time:_.u.>~7 (Signature) Relinquished By: 2~ 3,_:_ Date: 'z--rY-"?7 Time: /G°J.~ --(Signat~_.....,...- Received By: ~Lk~ Date:3-/¢-J 7 Time: /C: ~ re,· ~.,"ture) / ,-~------.._ Results Repo~: ,JL_ .L,/[~~ Date:~h~A7 Time: ,,,, (S~f -~-1.----I' r ,, (I :\docshare\cocr. frm) BASE/NEUTRAL ANO ACID EXTRACT ABLES CONPOUNO N-nitrosodimethvlamine bis (2-chloroethvl )ether 2-ch 1 orooheno 1 phenol 1 3-dichlorobenzene 1.4-dichlorobenzene 1.2-dichlorobenzene bis(2-chloroisooroovl)ether hexachloroethane N-nitroso-di-n-oroovlamine nitrobenzene isoohorone 2-nitrooheno 1 2,4-dimethylphenol bis(2-chloroethoxv)methane 2.4-dichloroohenol 1,2.4-trichlorobenzene nanhthalene hexachlorobutadiene 4-chloro--m-cresol hexachlorocyclooentadiene 2.4.6-trichloroohenol 2-chloronaohthalene acenaohthvlene dimethyl phthalate 2.6-dinitrotoluene acenaohthene 2,4-dinitroohenol 2.4-dinitrotoluene 4-nitroohenol fluorene 4-chloroohenvlohenvlether diethvl ohthalate 4,6-dinitro-o-cresol diohenvlamine azobenzene 4-braroohenvlohenvlether hexachlorobenzene oentachloroohenol ohenanthrene anthracene dibutyl phthalate fl uoranthene J -Estimated value . STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC ~EHICAL ANALYSIS LAB NO :q7oq~7 C/70'17O (170977 q7oq7Ji1 FIELD# /C/CJ.5 °)( /o/C/l, I /<-j'-//,, f) J qt:;/; q TYPE (3 ) (~) ( &,) ( IA ) UNITS ~luo/kq ~I\Jq/kq ~q/l~a rua/1 ~ Jr,/ :il'iifA I..<.~ lA.. ~ IA-I.A.- _, / ·v ..J...IA l/4-- W' SO/lloSO I0/330 S"O/Jt,,_,;o /0/~30 I J, 5011"150 /tJ/330 I 'V .SOIIIAS"O /tJ/~.10 / / / / " ,. \,/ \I \I .... , K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. l/7otrf?J Jqq7,1.. (///) r uo/1 ~ -fi-- / \ / u· -Material was analyzed for but not detected. The nurber NA -Not analyzed. is the Hininun Detection Limit. mIJL ----l/ -Tentative identification. fl -On NROC List of Priority Pollutants. Cl) C/ 7 t} 9' ff,o l'-J''-/7 7 ( ~) ~o/ka) f A. - / \ I BASE/NEUTRAL ANO ACID EXTRACT ABLES STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST ., RALEIGH, N.C. 27611 ORGANIC Q-IENICAL ANALYSIS LAB NO q7oq/17 C/7/)C/170 Q7o 977 q7oc1 1,J' FIELD# !9'i Cx' JtJCj{,/ I 1/9/./.R '/9'91,9 TYPE ( ~) ( \) ( /,,,,) ( IA ) l/JC)C/.PI I '19 7,,.1... ( ~) (X)f'1f>OOND UNITS ·rmdua/kq ~~uq/kq ! ua/1 }IDAT! ~q/l J,,._JJ...a.. ,ruq/1 ~ pyrene Jo/.~3a IA, I ,< lA -I /4- benzidine ,S'tJ/JhSO butyl benzyl phthalate /0/.3EO benz(a)anthracene l chrvsene J, 3,3--dichlorobenzidine S()) '/1:,S() bis(2~thvlhexyl)phthalate !/()/.3.30 di-n-octvl ohthalate IO/.J3o benzo(b)fluoranthene S0/1"5"0 benzo(k)fluoranthene benzo(a)ovrene i ndeno ( 1 2 3-<:d) ovrene dibenzo(a h)anthracene / / / / benzo(a h i)oerylene \ / 'I ,, \I \' ani 1 ine s-a II" liO IA-(..,<_ vL-I.A ~ benzoic acid benzyl alcohol 4-<:h l oroan i l i ne ~ ,I' dibenzofuran ltJ /.:Bo 2~thylMPhthalene I 2~thvlohenol j 4-fflethylphenol ~, 2-ni troani 1 i ne S'o/Jt..cro 3-nitroani line 4-nitroani line I / / I 2.4 5-trichlorophenol ~I \i I \I \I \I/ ----tc' 14 ~ f'oAJ F1 ~ .IY'\ e'.l:> +I -(-) {-) {-) ( -,) A Y 6,C.//h <; -- . mnt- J -Estimated value. H.l.0/ Sc/1- K -Actual value is known to be less than value given . L -Actual value is known to be greater than value given . U -Material was analyzed for but not detected. The nuroer is the Nininun Detection Limit. NA -Not analyzed . l/ -Tentative identification. ~/ -On NROC List of Priority Pollutants . lA-- / \I LA ~ / \/ _,....--...,. (-/ 7/0'-/,.P/,,,, /Y97 7 ( ~) ..I.IBi::Y'"uq/kq J i .A / ,, u / \. -{-) - STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC ~EHICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD# COHPOUND TYPE UNITS N-nitrosodimethvlamine Jr,/ :?31} bis(2-chloroethyl)ether 2-chloroohenol phenol 1,3-dichlorobenzene 1,4-dichlorobenzene 1.2-dichlorobenzene bis(2-chloroisooroovl)ether hexachloroethane N-nitroso-di -n-proovlamine nitrobenzene isoohorone 2-nitroohenol 2,4-dimethylphenol bis(2-chloroethoxv)methane 2.4-dichloroohenol 1,2,4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro--m-cresol hexachlorocyclcpentadiene 2.4.6-trichloroohenol 2-chloronaphthalene acenaohthylene dimethvl ohthalate 2.6-dinitrotoluene acenaohthene 2.4-dinitroohenol 2.4-dinitrotoluene 4-nitroohenol fluorene 4-chloroohenvlphenvlether diethyl phthalate 4 6-dinitro-o-cresol diphenvlamine azobenzene 4-braooohenvlohenvlether hexachlorobenzene ~ntachloroohenol phenanthrene anthracene dibutvl ohthalate fl uoranthene J -Estimated value. ,., S0/li,SO /()/3~0 S0/lw50 /0/~30 I ,J, SOI ~,;,so /IJ/330 I l 'V S"O//~SO Jt'J/~30 "j~ m1)L Hz..0/SO/J._ C/"'71)( 1'Y7 9709YV ., J f/ i'1'17c.t /7 (. :: -) (--~) 1i?(ua/kq' ':2rL 1 {i;q/k<lJ IA-u-- I I ' I ' I K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. 'f7t)f/jlq /'l'IYO (_ ::n ~\Ja/ka'"' I .,c ~ I '\ I q7CJ99.J... J</ct y _3 ( _~) ~ua/kai ~ I \' "170 YC/9- l GflJfr5' ct,,) ..,...ua/l~a ~ I "1./ u· -Material was analyzed for but not detected. The nurber NA -Not analyzed . is the Hininun Detection Limit. m])L ----1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. -~7/_J '/'fA /Y~1K7 k~l - u<i/ l ua/ka ) v(._...: I ,, °?3ok vL LA- /. Olo"7 I STATE LABORATORY OF PUBLIC HEALTH P.O . BOX 28047 -306 N. WILMINGTON , ST., RALEIGH, N.C. 27611 ORGANIC OlEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO C-/'7OC/½ CJ 7 OC/.f? JI 1c.171'_)1/AX/ q709'/,,,2 EXTRACT ABLES FIELD# /~tj7? J997CJ I 99,P() JC/t/£~ C0'1POOND TYPE ( q } (3 }. ( ~) (, ~) UNITS Y&J,,¥'uo/kQ ~~Q/kq ~uQ/kQ tIJltt'.'."" u Q / k ci) pyrene /0/.~~tl u...::: LA-IA-A benzidine so/1hSo butyl benzvl phthalate /0/.3.30 benz(a)anthracene chrvsene J, 3.3-<lichlorobenzidine Sf)) 'lh.'i'IJ bis(2~thvlhexvl)phthalate Jo/.3.3o di-n-octyl phthalate IO/.J3o benzo(b)fluoranthene .so/1"1S'o benzo(k)fluoranthene benzo(a)pvrene indeno(l,2.3--cd)pyrene dibenzo(a.h)anthracene I / / / benzo(Q. h. i )oervlene \~ 'I \ I ,I "\. I aniline l<allhs-r-lA-1/1 -u.. -IA- benzoic acid benzvl a lcoho 1 4--ch loroani 1 i ne "'-1/. dibenzofuran ltJ l.330 2-methvlnaohthalene 2-methvlphenol ~ 4-methylphenol "' 2-ni troani line s-o/J~~o 3-nitroaniline 4-nitroaniline I I / I 2.4.5-trichloroohenol ~I \ \ll \ I \' -~ ----,,. f'(!b~ C!.olv ;:=, ~,n e:n ·-1-/ -(-} ( -J {-) r -J BY t"-,.,tF.l/'11 S --, m1H .. J -Estimated value . H"O/ ,5(')/1- K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given . (1) r ~ _,,-;...,...._ ·/ 7 JL/717 '?7~99lfl /9t:J?...'\ /C/{jfr>7 ( /,:,) ( ~} 'tJq/l~ ~u Q / k Q J I.A.-f'()n LA- I / \' ' I LA-'IA- / / \ I \ V .,,,,,---....._ ~ ( -,) { + J -- U -Material was analyzed for but not detected. The nurber NA -Not analyzed . is the Mininun Detection Limit. ()')J)t.., -l/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. STATE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO '-1 70W7 C/ 7 /)C.ff.f Y CJ-, ., ., Ir✓ I -1 "f '-17/{)£)0 Q7/0/'J J EXTRACT ABLES FIELD # r-JqS! V I 9'1'?-T /'990,ri Jt;t}9/ , ) qqq, ,,,J.- COMPOUND TYPE (..3) ( ~) ( ~) ( ~) (~ UNITS ,i:m!:l( uQ/kQ ., ~(uQ/kQ, -~Yua/k<l' .-£n/kQ -~ u a/k a. N-nitrosodimethvlamine /()/ ;/~ IL-. I A. -I A I.A.. --I-' -. bis(2-chloroethyl)ether 2-chloroohenol phenol I 1 3-dichlorobenzene '\, 1 4-dichlorobenzene J (. 1/07 1.2-dichlorobenzene _, IA-- bis(2-chloroisooroovl)ether hexachloroethane N-nitroso-di-n-oroovlamine nitrobenzene isoohorone 2-nitroohenol 2.4-dimethvlohenol bis(2-chloroethoxv)methane 2,4-dichloroohenol 1.2.4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro-m--cresol hexachlorocvclooentadiene 2.4.6-trichloroohenol I 2-chloronaphthalene \ acenaohthvlene ~~nt" dimethvl phthalate vL 2,6-dinitrotoluene acenaohthene ,,, 2.4-dinitroohenol S0/JhSO 2,4-dinitrotoluene I0/330 4-nitroohenol 'SO/!w.~O fluorene /0/~30 4-chloroohenylphenylether ' diethvl ohthalate "' 4.6-dinitro--0-cresol so/Jl'Atro diphenvlamine /()/330 azobenzene I 4-brcmophenvlphenvlether hexachlorobenzene '11 I I I oentachloroohenol SO//~SO \I \ , \ phenanthrene JtJ/330 33oK l.ooo ,,, anthracene 33ok:.. 'l./-/n7 I.A- dibutvl ohthalate t.,L u-I I LA- fl uoranthene \I q/J()Q ~-J~~ '\ '-, I '700 , , , J -Estimated value. K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. u· -Material was analyzed for but not detected. The nurber NA -Not analyzed. is the Mininun Detection Limit . m'J)L ... ---1/ -Tentative identification. ~/ -On NRDC List of Priority Pollutants . ( ) lJQ/1 ua/kq BASE/NEUTRAL ANO ACID EXTRACT ABLES COMPOONO ovrene benzidine butyl benzvl ohthalate benz(a)anthracene chrvsene 3,3--dichlorobenzidine bis(2--ethylhexyl)phthalate di -n--0etvl ohthalate benzo(b)fluoranthene benzo(k)fluoranthene benzo(a)ovrene i ndeno ( l 2 3-cd) ovrene dibenzo(a h)anthracene benzo(a h i )oerylene aniline benzoic acid benzvl alcohol 4-ch 1 oroan i 1 i ne dibenzofuran 2-n'ethvlna.ohthalene 2-methyl pheno 1 4-n'ethvlohenol 2-ni troani 1 ine 3-nitroani 1 ine 4-nitroani 1 ine 2,4.5-trichloroohenol F--rA.s fi__CJ/JFJ/Une1) .R V tn~/1115" STATE LABORATORY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC D-!Et1ICAL ANALYSIS LAB HO C/7/JW7 q 76</Cfx' qJV-/7~/ C/7/0tJO FIELD# !9'C/ K¥ J'-f'-1,Yf /'t'9'C//) IC/C/t'l I TYPE ( ~) ( ~) ( -=s ) ( ~) UNITS ~,a/lea --~,.!Q/lca ') ..-.ld£uq/lca ~..: q I le a-:> J0/.3~" ll},t/,:i.""? ~.<./i,,, I A -LA- 50/1hSO . LL-'LA- J0l.330 LA-v<- l /,:J.,3)3 /4 JD/ J, 1,; (f){)0 2/ f?OO SO) lhStJ I L t --., l..t - 10/3.30 F I - /O/.J~o \I \v so/11£0 ?~ -3 -'>, I J. r?oo , A. , I A.~ , I I' / ,,, " '\ I '\. I \' S'O/JhS'O I~ IA -Lil-IA.- "' ,, '" 1.=r-:111 ' ~" s-o/Jt.~o I J I I -..J:t \ I \ ' \I _.,,._ _.......,,_ ,,-;.-..... ~ +J.-r+J (+} I +-J ( + J , ----'----""' - m])t... J -Estimated value. H2..0/ St:JIL- K -Actual value is known to be less than value given. c.t'7/00/ IY'C/tJ-2... ( ~-) ~uq/lca lR3~ , IA / \ LA .. ~ / \ ~ f+) '--./ - L -Actual value is known to be greater than value given . U -Material was analyzed for but not detected. The nurber NA -Not analyzed . is the t1i ninun Detection Limit . (}'JJ)t.. -l/ -Tentative identification. ~I -On NROC List of Priority Pollutants . ( ) uq/1 ua/kq ---STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMJNGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q70 66 +-9709 @3 q7C9 gif cn oC/6 5 910995 FIELD NO 1993B I qq7 4 ,qq75 IC/97&, /998 4, COMPOUND TYPE ( I > ( '1 ) ( t ) (4 ) ( 1-) M06';t (Pp~ ppm v~qi ppm. ~e,Jppm l6 p9.lppm / ,, (ppb ppb ppm, CHLOROMETHANE JO i A I 1 1 /J I 1 VINYL Clll.ORIDE 10 BROMOMETHANE '10 CHLOROETHANE JO TRICHLOROFLUORO~ ·o ) ., ,/ ,1 \ ' ACETONE ,;}_Q 3 .r,c.,. g -S;C. 4<.o q 7 1.1-DICHLOROETHENE ;:.: ,J i1 .A -I A. L(_ IODOMETHAl'n: +raceJL t METHYLENE CHLORIDE \ I;._., ~J CARBON DISULFIDE +r-rir,o -1--., (') (' -p J -n-{)C.l" - TRANS-1,2-DIClll.OROETHENE ~ :; ; 1 / J J ACRTLONITRILE ~ l,l•DICHLOROETHANE 5 ,1 ,v ,v :l-BOTAN'ONE .... ,o ~ Jt 5 -sc. Lf.3 CIS-l,2•DICHLOROETHENE 5 L,L, u__ I 1 CHLOROFORM l, l.l•TRICHLOROETHANE CARBON TETRACHLORIDE \I ,J BENZ!:NE 1 °3 I :r l,2•DICHLOROETHANJ: l,A......-, I J. _ TRICHLOROETH.SoNE l.2•D1Clll.OROPROPANE BROMODICHLOROMETHANE ,1 '\ I/ \j \I/ ..._, \ J c-f"c,',•,. r,....,;_ .. ,.;-;; <.:..:...-.1 ,Ai''H NF'T,CN ,.:K B,-to::.c,-P-c ~N o . . J -Estimated value K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The number is the Minimum Detection Limit. 111'.A -Not analyzed. 1/ -Tentative identification. "i.1 -ccMfo"'-P'o Ra.1 l"\6L'f OE-TE:CTA6U:.. oNt¥ 1N fticH Ct!N!£N~t:N".i. ✓-SAAPL&i Hltiltl.'f OILl.lTE.O, ~0~~ Do r,k,'r f+ff>Lf. DEHNR 3065-0 (10/93) co ( ) ppc {Prr'J PURGCOM.ORG STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047-306 N. WILMINGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q1ore4 cr709g3 FIELD NO l '19 3 'ef' /'1q7q COMPOUND TYPE L I l ( t/J tii~~"j V'ppb" ppm (ppb f prr, DIBROMOMETHANE 5 j ,l_ LL- 4-METHTL-2-PENTANONE ,o CIS-1,3-DICHLOROPROPENE ,:: -..., TOLUENE TRANS-1,3-DICHLOROPROPENE l, 1,2,2-T!:TRACHLOROETBAl'fE l, 1,2-TRICHLOROETHAlfl: ,V 2-HEXMONE iC TETRACHLOROETHER t:; -. ...; DmROMOCHLOROMETHANE I ETHYLENE DmROMIDE CHLOROBENZER 1, l, 1,2-T!:TRACHLOROETHANE ETHYL BENZENE XTLENES STYRENE " / BROKOP'ORM ,c TRANS-1,4-DICHLOR0-2-BUTENE re 1,2,3-TRICHLOROPROPANE 5 1,4-DICHLOROBENZENE I 1,2-DICHLOROBENZENE ~ l,2-DIBROM0-3-CHLOROPROPANE ---; ,., :.;7'-\-' VINYL ACrrATE XC 'I \/ . C. .. i',·-•,~»ij'-<:. l-RP, -.c N-;-;:\hi.1~,~n{,.~ o R t::1Ro;.c.-i<t"w,~i) . J -Estimated value X -Actual value is known to be leas than value given. L -Actual value is known to be greater than value given. q10994 ;9 9·7 5 <4 ) ppl/ p P'f1 J1 ,1/ +rnc P IL \I :3o u....... +r-nrl°, +vrirt:J~ IL " (~\ :2_:5 1'.A ~ \ q7098S q7oq95 /9 9 7Co J998(o ( ii_ ) ( 4 ) (15pb)pp,n tfpo ppm ' ' ,(_ \ ,I ;). "3" q1 11 I l \ I + ror e_.l.J , , - ,1/ +rnce.. /1 -,y +-r()r P +rctrP +r-1'1 r -P ) :l ·..1 { .A - \I \ ;], 3 -1---rnr P +rt:tr e I A LL--I ~ w' . O -Material was analyzed for but not detected. The number is the Minimum Detection Limit. ID. -Not analyzed. 1/ -Tentative identification. 1t -COMPoU1..iv R.t LIA6L'( PciECTf\'6l£ (;N i .. '{ /t-,j Hl<r-H CCI !C(NTJ<A T j , .. n l~i" ✓" :';i;:.iNPL f-H l~·H L'f u/t .. LlT(D . H i",'L;"; :)e; )v.::-t l'-'('}',_•/. DEHNR 3068-0 (10/93) ( ) ppb ppm PURGCOM.ORG ---STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047-306 N. WILMINGTON ST .• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABI.E COMPOUNDS LAB NO q7oq7;;_ 970Cl73 FIELD NO I 9ctCQ3 19q &'f COMPOUND TYPE ( 3 ) (3 ) ( ) ( ) ( ) rj,~~~ /pp tV ppm (ffb)ppm ppb ppm pp b ppm pp b ppm_ CHLOROMETHANE J O I 1 I 1 VINYL CHLORIDE 10 BROIIOMETHANE ;zD CHLOROE'I'HANE 10 TRICHLOROFLUOROMETHANE ,o \. I ACETONE ;;io ;;_ J,l. l, 1-DICHLOROETBl!:NE 5 { I IODOla:THAl'fl!: Kl!:TBYLENE CHLORIDE CARBO!'( DISULFIDE TRAl'fS-1,2-DICHLOROETHENE ,/ ACRYLONTI'RILE ~ 1,1-DICHLOROETHANE .::-J 2-BUTANONE :LO Cis-1,2-DICHLOROETHENE s CHLOROFORM 1,1,1-TRICHLOROETHANE ' CARBOl'l TETRACHLORIDE BENZENE ' 1,2-DICHLOROETHAl'IE ' TRICHLOROl!:TIU<l'll!: 1,2-DICHLOROPROPANE BROIIODICHLOROIIETHANE " ✓ \ V ' I/ C-Po~•,."~ i,..,1f1 <.:.:..1'-1 ,fli'l\!N P T iCN c':K BtKK.6-P-c--1\.iD. J -Estimated value ~ -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. 0 -Material was analyzed for but not detected. The number is the Ninimum Detection Limit. RA -Not analyzed. 1/ -Tentative identification. "%,_I -Clllli\f'O\ol~D Rw l'\eL"f OE.TEC'i"A6Lc. ON~ IN fHcH CCN!£Nm,iric:NS, ✓ -SAAPLa HI 'ltL.'f OILIA.TE.o. ~OL!1' 0c 1'ktr" f+ff>Lf. DEHNR 3065-0 (10/93) - ( ) ppb A'ri'1 PURGCOM.ORG , STATE IABORATORY OF POBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO q7oqn q7o q73 FIELD NO 1qq(p.'3 I qg 6, 'f COMPOUND TYPE ( 3 ) ( 3 ) ( ) ( ) ( ) M o~-s {11pb /p pb ppm (pP 'o) f pn, ppb PfJ"f1 pp b pprn ff'O ppm DIBROMOMETHANE 5 /1 l.1 4-METHTL-2-PENTANONE ,o CIS-1,3-DICHLOROPROPENE ,:.: ,/ ..__, TOLUENE +f'ace._ TRANS-1,3-DICHLOROPROPENE Ii l, l ,2,2-TETRACHLOROETBA!fE l , l ,~TRlCHLOROETHME ' >I ~HEL\!fONE JO TETRACHLOROETHE!fE t:; _, DIBROIIOCHLOROMETHANE ETHYLENE DIBROMIDI': CHLOROBENZEl'f1t l, l, 1,2-TETRACHLOROETHAl'fE ETHYL BENZENE XTLENES STTREl'fE ,I/ BROMOP'ORII ,c TRAlfS-1,4-DICHLORO-~BUTENE gr, L · 1,2,3-TRlCHLOROPROPANE 5 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE -../ 1,2-DIBROM0-3-CHLOROPROPANE do VINYL ACETATE ;)..(':(_' \ t-, -~ I '\. I C. -i'c.~~-c,, •~i..i'.:: ._ (-\ P., Cc :--i-:-;:\i,,U :-..lil TK, I\, () R. i3?.ct:.c--i<c lj ~ l)' J -Estimated value ~ -Actual value is known to be le■■ than value given. L -Actual value is known to be greater than value given. O -Material wa■ analyzed for but not detected. The number i■ the Minimum Detection Limit. ID. -Not analyzed. 1/ -Tentative identification. JI -COMPoU.J..i i) R~I-IP.8LY DcTECTf\E,U!. CN,_'{ iN HICr H ccr !CCNTRAT iC~l.'.'ic ✓ ·· :S,'1 ,-..,PL.r:: Hl(,·i1 L';" Di 1_,,;f "f:D . f,lDL•1 ~D I\,~ i'.J,f'fL'/. DEHNR 3068-0 (10/93) ( ) ppb ppm PURGCOM.ORG ., ' • -'\I ,......t· • ', .-· .~. ~ .;~f· ·~· , ... ,_. .-(. ... ''. -,,. { ' ;r ~ ' ... < ..!--. .;- ~ .. ___ : ~·· . ' '' '.· . . . ... J I,. NCDEHNR Division of Waste Management D Superfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab:_·~- Inorganics Lab:~ CHAIN OF CUSTODY RECORD Project Name: r,J'J-~ CcNrJir Sampled By: ..f147F Site ID # (NCD#) Sampler ID Location: Telephone:(CJ14') i.U 7..tfl/ Address: Date Sampled: 3/ 11/-,? Time Sampled: Sample Types: Soil Water ~ Waste Other Remarks: Field Sample / p J _D .,,s-A-DO) ) -0 ,Art-~ E--Zi11 -5' /1.f t:,(/--~ Numbers Relinquished By: S..f••..-t p.~1-v-Date: Z/,Jft? Time: l '): II> (Signature) ~p-~ Received By: -<'}_,L _ 4~ Date: J. -/.1 -q 'J Time: /7,c.rcr , , --(Signature) Relinquished By: ~ ~~7-'-Date: J-/'1-'i 7 Time: 1'$""_:Y-0 Received By: (Signa%~ ----~14/~~ Date: C:..( Time:_{.J;J J (Signature) Relinquished By: Date: Time: (Signature) Received By: Date: Time: (Signature) -/ -- Results Reported: /h/ .0 / ,6/4,~~-~ Date: 2,,&~99--Time: (Signatuf{) --V (/ V N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O I 7 0~·2_ --~----------------------------- Name of Site __ /.,,J----'' cf._-.......... A=e;..w=-._.-_G __ '-'_· ;-,.{__.__._N_.___ ___ _ Site Location ------------------- Collected By ----------ID# Date Collected :::1 -/ 3 -':} f Time ----___ ..,;.i__,_~~~----------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments ✓ emc .I )/oi1 , 5 / Bariu / Ground water (1) Solid (5) ~Cadmium / ✓ Chromium / __ Surface water (2) ✓Liquid (6) _L_Lead A. vMe1/, Soil (3) _ Sludge (7) ~ Selenium "-.. ✓ Silver "-v Other (4) _ Other (8) -\ -~Jv-.:k ,/ -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) r1ur 'htW Organic Compounds Results(mg/1) P&T:GC/MS / Arsenic L.CJ -<Jd.. benzene ---- --Acid:B/N Ext. ,./ Barium O ~di8 --carbon tetrachloride MTBE _1L_ Cadmium <.Q, CJ 5 chlordane -----Chloride chlorobenzene ------ --..L Chromium L..O_o :5 chloroform --__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-cresol ----__L_Lead 0,..6-5 cresol ---- --__ Manganese --1,4-dichlorobenzene --/Mercury L...~-G D,~...5 --1,2-dichloroethane Nitrate __ 1,1-dichloroethylene --,./ Selenium <o✓ tJQS-2,4-dinitrotoluene --_,,/,L_ Silver L.Q .. c.2~ __ heptachlor Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichl~roethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by ~ -~ --methoxychlor __ toxaphene D:i te Extracted Date Reported 2,4-D oo:i649 M~R 1797 --_ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number --I) I IS J l 'JI ( llcviscd 2/91) N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ O=...,lc....J.L-..;;a:;__;;;.~--3L,_ ______ _ Name of Site __ l,_J_AA_. _~_-_,tV_c_-_· .... _·\-\/,~-r_t.__ __ _ Site Location --------------------- Collected By -----------ID# ___ Date Collected_--=3:...--1~3_-_•7,_7~---Time _____ _ Agency: Hazardous Waste Solid Waste ~ Superfund Sample Type Environmental Concentrate Comments _ Ground water (1) __ Solid (5) ~? {V}-5 _ Surface water (2) . i/ Liquid (6) ___________ _ Soil (3) Sludge (7) __________ _ / Other (4) ~ _ Other (8) _________ _ L,.z.-..,,J~ Organic Chemistry Parameter P&T:GC/MS Acid:B /N Ext. MTBE Results(mg/1) Inorganic Chemistry Parameter ~ Arsenic / Barium _L_ Cadmium Chloride Results(mg/1) _ I) .,,:.. CJ. v .;J, ./ Chromium L.. o ~ c .5 __ Copper Fluoride Iron ...tL Lead .:::....c _c::,,5 __ Manganese .L._ Mercury .t.... o _ oac,,S Nitrate _L_ Selenium <:::_ () •. 00 _s- i-----------------4 / Silver L..~-Q--d Radiochemistry Sulfates Zinc Parameter Results (PCi/1) pH __ Gross Alpha -------__ Conductivity ______ _ Gross Beta TDS TOC Microbiology Parameter Results (Col/lOOml) Date Received Reported by --------------------'--- Date Extracted Date Rep~rted ----u03,___,65_0_M---AR-.--1-7<J_7_ Date AnalyLcd Lab Number ----------1) I IS 3191 (Revised 2/91) TCLP Compounds Inorg ic Compounds . Ars ·c /Barium _L,Cadmium _.,,,-Chromium _LLead _L Mercury / Seleni -:7si r Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane __ 1,1-dichloroethylene 2,4-dinitrotoluene __ heptachlor hexachlorobenzene hexachlorobutadiene hexachloroethane methyl ethyl ketone nitrobenzene __ pentachlorophenol __ pyridine tetrachloroethylene trichloroethylene Results(mg/1) ------- ------- ------- ------- ------- __ 2,4,5-trichlorophenol ______ _ 2,4,6-trichlorophenol --vinyl chloride ------- endrin lindane methoxychlor __ toxaphene 2,4-D 2,4,5-TP (Silvex) N.C. Department of Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ---------------Field Sample Number ____ 6_1 _,_o_,,G.,_~_4-t...i.·_-______ _ Site Location ------------------- Collected By _________ _ ID# Date Collected 3 ~ I~ -11 Time --------"''-------"'-----'------------ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Ino ' ic Compounds Resu~g/1) Environmental Concentrate Comments / Ars IC ult~-) /Barium / --__ Groundwater (1) _ Solid (5) / Cadmium / c:/Liquid (6) _L Chromium / __ Surface water (2) L~v -,L.... Mercury ""-. Soil (3) _ Sludge (7) / Seleniu '\. /~) _L_ Silver \ _ Other (8) \ -i t<---7 \ "'--- \ Organic Chemistry Inorganic Chemistry \ -- Parameter Results (mg/I) Parameter Results(mg/'}" g;Og Organic Compounds Results (mg/I) _ P&T:GC/MS V Arsenic <0 _c::..,;:;..,_ benzene --/Barium _ Acid:B/N Ext. a_;J,tj carbon tetrachloride --MTBE /Cadmium L....G .-e>.!:; chlordane ----Chloride chlorobenzene ------✓ Chromium -'...... D-05 chloroform ---- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol -- --i../ Lead 0-0~ cresol -- --__ Manganese 1,4-dichlorobenzene -- --/Mercury L.... Q ~ CQ c,S 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene --( c2, oo.c --/ Selenium 2,4-dinitrotoluene 7 Silver -- .L.._ D -c,:;;i __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····-·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene · ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane --Date Received Reported by --methoxychlor __ toxaphene Date Extractc.:<l Date Reported 2,4-D --00:\651 M~R l. 7Cf7 _ 2,4,5-TP (Silvex) Dale Analyzed Lab Number --DI IS 31')1 (Revised 2/91) 'NGDEHNR Division of Solid Waste Management D Superfund Section )Q. Hazardous Waste Section D Solid Waste Section Organics Lab:_ Inorganics Lab:-' {{e-:,. ....... \-\-~ s""-cv...\6 'v:>e. \f\,\IM'\-c:J --\-o P~·c~ (\. 0a.. \l\e ~ 7 ~oe \ \-l : rsc\--\ hJ:>{-f\ ~~,·e"'-t e:. ,qdu,·<x,v-5 ,f c 6 "\-o.. ~ r:.· I J CHAIN OF CUSTODY RECORD Project Name: f C.S'? \-~.--.t-Q\\ Site ID# (NCD#) ________ _ Location: W MY:e w Co"'-"'-"-=> ( Address: Sample Types: Soil __ ___._.x,.___ Field Sample Numbers Water Sampled by: Sa.,,..~rn-~~,e. Sampler ID ____________ _ Telephone: M) '] '?:>'S _;) I '1 g :x 'ls\ Date Sampled: _ ___,....__........._...__ ______ _ Time Sampled: Waste Other ---------- Relinquished by: S a-byo ~01>ye Date: :J Ju )51 Time: 3 ·.L(o ft"'\ (Signatu~e) Received by: -----~ -~ -~. ),. -----' --, ----------------------------------Date :,;J;)_§}t 7 -Time: -3 --'/ a -(o.-__. ----Signature) ., Date:~ J c,7 Time: I / £0 &-v---- ----------------------------- Received by: --:7~"',,2~ Date:J·<~ -'\7 Time: //.->'-' (Signature) · Relinquished by: ~ ~-__:;:-. Date: .J-)YJr7 Time:l :}°:· ;O Received by: ------~~~--·-------Date: ____ "' -----------Time: --/J: I O _________ _ (Signat1,1 ) Results Reported: Date: ·U>y? o/)fime: ___ _ (A:\COCRFRM) NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab:_~ Inorganics Lab:-6_ CHAIN OF CUSTODY RECORD Project Name: Pc6 Lc\r-.J f; I I Sampled By: ~+"'t-e Site ID # (NCD#) Sampler ID Location: Wq r f ~ '" C<Jvf\i-:t. Telephone:~ 733 -;;z.r7~ Address: Date Sampled: 3/t(c,7 Time Sampled: I 715 Sample Types: Soil Water 'X Waste Other Remarks: Field Sample Mv3 -5 ---- Numbers ---· Relinquished By: 'T~tv~ Date: 3/t ('f, Time: d-~~o (Sie:nature) Received By: 7../4 -~~ j:> Date: 3-t-?7 Time: '2..,i;> •~ (Signature) Relinquished By: "9t<.. -;;p .;J_~ Date: 3-/1/~ 7 Time: IS.JS'? (~~ Received By: Date: <-t. Time :_LIL£) -~ (Signature) Relinquished By: Date: Time: (Sie:nature) Received By: Date: Time: (SignatureL A' ~--....--.~ Results Reported: ##/~/ Lr/4~ ~ Date:~me: (Signature) -(./ V - (I :\docshare\cocr. frm) NCDEHNR Division of Waste Management D Superfund Section D Hazardous Waste Section D Solid Waste Section Project Name: fee, Site ID# (NCD#) CHAIN OF CUSTODY RECORD w..~+i I I Sampled By: S~-l-e_ Sampler ID Organics Lab: ____ Inorganics Lab:.L Location: w"--rr4,, Co v ,-.. +-'t Telephone:(EU 7 3 3 --A./7 ~ Address: Date Sampled: 3/Lf/'17 Time Sampled: (_o 30 Sample Types: Soil ~-Water Waste Other > Remarks: A I I f" i e rJ sa. ""'~Ir n.vW\.b.Qr':> CcJ {( ec-l~cP f'r~ Sa t'Y'C """ Q I ( I i,c .,, I-, ...,.._ Field Sample f!4 -;A. KM-S Numbers w~-10 ----- ~ ~ 3 Relinquished By: 7~ {)&dfav, Date: 3/1-1/<,17 Time: "J_+)3D (Sienature) Received By: -?.~~3~ Date: 2-'.z'.-7_7 Time: 2-u2. t3 0 7 (Signature) Relinquished By: ~-_)_::__ Date:";)--IY-77 Time: /.0.50 (Si~ ~ C.-( Time: (J,,,.: J<} Received By: :~~=-Date: (Signature) Relinquished By: Date: Time: (Siimature) Received By: Date: Time: (Signature]./ ,, ,A ,I Results Reported: /1/(1// p ~/// ~.,,__ Date: :2,,it~9;2I-ime: (Signature) ~ C/ V p NCDEHNR Division of Waste Management Organics Lab: -~ Inorganics Lab: y □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section CHAIN OF CUSTODY RECORD . Project Name: Pc6 Le1nd..hll Sampled By: -s+c,_f--e Site ID # (NCD#) Sampler ID Location: Wo.. r,. ~" ((J, N c_ Telephone:~ 733 -?--r,g Address: Date Sampled: 3 [5 /1.7 Time Sampled: i L.f lf 0 Sample Types: Soil y Water Waste Other Remarks: Al I -(1' () { J ~a. rr-(-!_ ( E' t'\V'n"\ bt>rs +c...k: e"' --fr OW\ Sa vr--(> (.l,J ~ ( ( { <JC c, ftO'Y) .. Field Sample t;)--tt"--1 0,,vt-s- Numbers "' " :c:: =P,iil I i!, Relinquished By: ·y~9tv-~ Date: 3/5 /cf7 Time: aoos . I (Swnature) Received By: -:2,£..~ ~~ Date: 3--s;-~,;7 Time: ZooJ (Signature) Relinquished By: '?~ ~~ Date: >-1'~-<.7 Time: /5! §7.J (Si~ 7 ~ Date: '(:.. Time: LJ:__rd_ Received By: . 7t?~ ~ (Signature) Relinquished By: Date: Time: (Signature) Received By: Date: Time: (Signature)/ ,,. .,_ I Results Reported: //{;/K/ I /4/u,,&:_ ---Date:~ime: (Signature) -..... V NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: __ Inorganics Lab: __ CHAIN OF CUSTODY RECORD Project Name: Pc~ lo..1-\.d f:?~ 11 Sampled By: S1°'-t-~ Site ID# (NCD#) Sampler ID Location: l.Ll0-.rre"'-Co v 1'\ --1-'l Telephone:CT.d) 733-~178 J 3/3/?7 Address: Date Sampled: Time Sampled: / & 3 O Sample Types: Soil i Water Waste Other Remarks: At! f1'e./J sa_-~(-P f\vm.bQrs. k I, e r---f r olY\ SQ""'-(: LV ~-If ( cJ C°'--i-i a I'\ c Field Sample ~-aa,,, ,....,., \,v' ;V\ -S" Numbers ~f)~ ~~,Q ---~ Relinquished By: 1~-0/~ Date: '3/_ 3 /'f7 Time: d-0 / 0 (Siimature) 1 Received By: -~;3,~ Date: 3/-::>lf? Time: :;i_e>: 1 J (Signature) Relinquished By: J/~;J~ Date: 3--L'.0-17 Time: I ,Js S-u (Sig™ . ~ Date: Time: / .. /:: Fd Received By: ==--~ ~ c-r (Signature) Relinquished By: Date: Time: (Siimature) Received By: Date: Time: (Signatur;,) / ./ -•. Results Reported: //li/ ~ /4/4 ~A Date: 2/A'.'3/9;)'.Time: (Signature) V v-- NCDEHNR Division of Waste Management D Superfund Section Organics Lab: __ Inorganics Lab: v D Hazardous Waste Section D Solid Waste Section CHAIN OF CUSTODY RECORD Project Name: VvdrYCn C&Mk Pcl3 Lci,,A.(;1 I Sampled By: VJ,~t. 2!_1-/4-'' Site ID # (NCD#) I Sampler ID Location: i;Jc;c_,-,t,i,r(c.-, , N c.., Telephone:(<;1<;>) B1Z-·Z<o'°D Address: se. lho4-Date Sampled: '3 'S"'-97 Time Sampled: 15'1 ?0 { (b:lt;' Sample Types: Soil x Water Waste \( Other Remarks: Ktv, =fjt,&Al ~ ~~,t~ ~ =Pc;~ Lfl.:JNA -~ !.:,~re~~~- f2lv'I 1313 1 Pb ~L~ -for.> J-.fd~f. -z¥~ Field Sample j~e, =FA-*'~ 'f!!A JAE2-BB 1 Numbers .:fA:e, SA ~r, BA ~A~ Pt> j:tJe ~;.,-~IA~A I Relinquished By: waffi I/ lfeddo. Date: 5frp/<)7 Time: 9iZZ (Signature) / Received By: li--:::r fl, 5<--Date: a4, ;9 7 Time: 1 ' 2-'1--- (Sign~ 7 T Relinquished By: -fJ _,.__, kn6o Date :~,/4 ,4)1 Time: tt_,'S-1 (§{enature) / r Received By: I Date: J-r:;.-47 Time:~. ;)~7 ✓-?.~~ (Signature) Relinquished By: ~ ---;:;r: ;)~ Date:3-1~-47 Ti1ne: { ,T!j6 (Sign~~ ~ ~ ~ Time: 1.rn Received By: = /-. ~. ~ Date: (Signature) ~ .,-,. A Results Reported: JI// /<.4' L/4~ Date: 2.tL~ 7 fa1ne: (Si.ghature f -.._., V - (I:\docshare\cocr. frm) I I ! NCDEHNR Division of Waste Management □ Superfund Section □ Hazardous Waste Section □ Solid Waste Section Organics Lab: __ lnorganics Lab:_x__ CHAIN OF CUSTODY RECORD Project Name: pc B L:.t"'-J f'i I t Sampled By: s fu. +--e Site ID # (NCD#) Sampler ID Location: U-/Qr r ~ ,.._ Cc,c.ud't-Telephone:~ -, 3 3 -~, 7 8 Address: Date Sampled: 3 It /t; 7 Time Sampled: OC/45 Sample Types: Soil 1 Water Waste Other Remarks: Field Sample ;vt,M____:__§_ Numbers - Relinquished By: T~IV~ Date:3/6" /q7 Time: ;;i.__63a (Signature) - Received By: ~~ s~ Date: 3-6-1 1 Time: ~ ";::,.:, (Signature) _,,,,,- Relinquished By: ~ 1 -:}---=::-Date: :;3>-13/..c:;7 Time: /fl _ro (S~~~ Received By: Date: ,:, Time: /J,:-_rc:> (S ignature) Relinquished By: Date: Time: (Siirnatu re) Received By: Date: Time: ---- (Signatur ) / ; -A Results Reported: ff .17//:Y' p /4 ~ Date: :n//£'r 1')[ime: ~gn.ahlre) --v-I/ V . (l:\docshare\cocr.frm) NC Department of Environment, H"ILh, & Narual Rc1ourcc, Solid Wa•l.c l>l•ru~cmcni Divi•ion SA.WLE ANALYSIS REQUEST Sw.te Laboratory of Public Hc.ilth P.O. Box 28047, 306 N. Wilminbton St. R•lcii;h, North Carolina 27ol l-W47 Site Number _______________ Su..rnple ID Number/Na.me __ ...:.0_1_7-=0_· _E-J_, '1_,_ __________ _ Name of Sit.c _ _..:._u_..:;:~~A.::..:~:_-... :_N_;_. _Co_::;__J.c...:i,J_;_1Y'----'-----Collected By ____________ ID//' _____ _ SiteLoCJ.tioo _______________ Dat.cCo!lected ____ 3_-__::~:...-_q...;__;-; _____ Time ______ _ - Agency: Hazardous Waste Solid Wa.stc / Supcrfund TCLP Compounds ---- Sample Type lnorganic Compow1ds Roult.s(mg/1) EnvironmenL"d Concentrate Comments arseruc -barium lM &-5 -Ground Water (1) Solid (5) cadmium --- _/ Liquid (6) chromium -Surface Water ('.2) lead -- -mercury Soil (J) Sludge (7) selenium ---~il ver _L Other (4) -Other (8) -- - -Org:rnic Chemistry Inorganic Chemistry - Para.meter Raults (mg/I) Parameter Re:;ult.s(mg/1)'6 !!111!!' Orgaruc Compounds _Rc:;ult.s(mg/l) P&T:GC/MS antimony beuune ---Acid:TI/N Ext. ✓ lir5CCUC L. C-o;;J.... carbon tetrachloride --- -'.2,4-D __L barium Cl -c.::$ chlordane - -'.2, 4 ,5-TP(Silvex) -be ryll ium chJorobcn.zcnc: -chlordane: ..,/ cud mi um L._ D -c.5 chloroform --- -bc:pLnchlor -chloride o-crcsol - -hc:xachlorobenzene ✓ chromium <. D -D.!5 m-c rc:sol -- -hcx.achlorobu uu.licnc cobwt p-crcsol --cndrin copper crcsol ---I i.ndane fluoride 1,4-dichlorobenzenc ----mcthoxychlor -iron l ,'.2-dichJorocthane -toxaphc:nc: ..,/ lead <o-o.5 1, 1-dichloroethykne -----manganese -2, 4-d ichloroelliy !enc -/ mercury· L..u , 000 -S -hepwch.lor nickel hexachlorobcn.zcnc -----nitrate hc:x.achlorobutadiene (o .. oos--/ selenium hex.ach.loroethanc /silver - L._ C>-D'5. -l.llclhyl c:1hyl kelone FOR LAil USE ONLY sulfates ni I robcnune --thallium pcnwchlorophcnol --Date Received vanadium pyridine -- -z.inc tctrachJo~octhylcnc -Date Extracted pH trichJorocthylene -- -conductivity -2 ,4 ,5-trichJorophenol Date Analyzed -TDS 2,4,6-trichJorophc:nol - -fl.~h point -vi.nyl chloride Reported By cndri.n --lindane --Date Reported -mc:thox.ychlor - Lab Numb903652 MAR 1797 -toxapheoe - --2,4-D --2,4,5-TP (S ilvcx.) Df!S 3191 (R cvi,cJ 12/?J) N.C. Department of Environment, l lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ___ ----"CJ"--'-) -'7'--'-1.._l 72....__· _______ _ Name of Site W A R,R.E, "" Cov rHY l@o h (J._ Site Location __ ~w~,..~il~t.~s:--=M~~0-<-V~-N~JY~--------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste _L_ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments ✓ Arsenic ..C:.g.w.::1, --✓ Barium a -<..<.z3 __ Groundwater (1) ~ Solid (5) Tr\ 55 ✓ Cadmium <..... L),.,_ 'C~~ .JL::._ Chromium L....c_ c-5 __ Surface water (2) Liquid (6) ✓ Lead <-0-0 5 --_L Mercury L.'.. 0 -i ..::L.__ Soil (3) _ Sludge (7) _x_ Selenium < Q.. a a 4-Silver .::.. c, _ :::,.$ _ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ' ! Parameter Results(mg/1) Parameter V Arsenic Results ( QJ"" (mg/kg) Organic Compounds Results(mg/1) : _ P&T:GC/MS <#'t,0 benzene I --:7· Barium ---_ Acid:B/N Ext. carbon tetrachloride ----MTBE ✓Cadmium < q , B chlordane ------Chloride chlorobenzene ------ --✓ Chromium -a~ chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol -- --v Lead ~a cresoi -- --__ -Manganese --1,4-dichlorooenzene --✓ Mercury C. 0.( --1,2-dichloroethane --Nitrate __ 1,1 -dichloroethylene --~~~ ,/Selenium 2,4-dinitrotoluene --✓ Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol --__ vinyl chloride --endrin --lindane --Date Received Reported by --methoxychlor toxaphene --Dale ExtractcJ Dale Reported 2,4-D ~0/~ff7 t~PR 1197 = 2,4,5-TP (Silvex) Dale AnalyLcd Lab Num er • --• ·· 1 --DI IS 3191 (Revised 2/91) N.C. Department of Environment, I lcallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O 1 '7 0{,, O ---=-----'-------------------------- Site Location Name of Site (,,_/ MB,b 11/ ~ll'J'T!'. ------------------- Collected By ID# Date Collected ·:=1i ~ /3 -'c 7 Time -------------- Agency: Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments _ Ground water (1) / Solid (5) __ Surface water (2) Liquid (6) ___________ _ I Soil (3) Sludge (7) __________ _ / Other (4) f lf'e( _ Other (8) __________ _ Organic Chemistry Inorganic Chemistry Parameter _ P&T:GC/MS _ Acid:B/N Ext. Results (mg/I) Parameter ✓ Arsenic / Barium / Cadmium Results~ (mg/kg) <' l(. Q MTBE Chloride / Chromium __ Copper Fluoride Iron / Lead __ Manganese L Mercury Nitrate ""T Selenium t---------------~ / Silver Radiochemistry ..... ,_, _____________ -f Parameter Results (PCi/1) __ Gross Alpha -------Gross Beta Microbiology Parameter Results (Col/lO0ml) -- Sulfates Zinc _pH __ Conductivity TDS --TOC <lo (to Date R eceived Reported by ----------------- Dale Ex lr ac lc<l Dale Reported ----0036=--S ...... 3""'D'"MA..,...,R ...... 17._,,~r"T-7- Dat c AnalyLcd Lab Number DI IS 3191 (Revised 2/91) --------- TCLP Compounds Inorganic Compounds Results(mg/1) LArsenic L.. o _ <::).d--, / Barium o -..:3/i· _L Cadmium < c -a 5 /Chromium ~ o _ a .5 / Lead L'....o ~ c;;; / Mercury L.....c-~ D ) / Selenium ..( a __ c ili / Silver L'.. <J _ q.5 Organic Compounds benzene --carbon tetrachloride Results(mg/1) --------- -- -- chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol cresol ----1,4-dichlorobenzene --1,2-dichloroethane ------ __ 1,1-dichloroethylene _____ _ __ 2,4-dinitrotoluene __ heptachlor hexaehlorobenzene --hexachlorobutadiene ---------hexachloroethane ----methyl ethyl ketone nitrobenzene --__ · pentachlorophenol __ pyridine __ tetrachloroethylene trichloroethylene = 2,4,5-trichlorophenol _____ _ __ 2,4,6-trichlorophenol _____ _ __ vinyl chloride endrin --lindane ----rnethoxychlor __ toxaphene _ 2,4-D _ 2,4,5-TP (Silvex) .___ _______________ __, - N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number 6-, ·7 () 6 I ---~~~------------------------- Name of Site LJ A:::R-:&1:Clv Site Location ------------------- Collected By _________ _ ID# Date Collected J -/J~/7 Time -----------'-'--'----------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Typ~ Inorganic Compounds Results(mg/1} Environmental Concentrate Comments / Arsenic L<)_c,:;:J... PJD-5 ...,,LBarium C) ~5 <'c __ Groundwater (1) _ Solid (5) -,L.. Cadmium L. a_ o.5 _LChromium ~ ~-o .!5 __ Surface water (2) Liquid (6) /Lead -<( e:::.-0~ /Mercury ZD_r.l _ Soil (3) _ Sludge (T) ~elenium .c__ -a .. c ,;). /Silver C:.. Q-G~ / Other ( 4) R-/tN --_ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I} Parameter Results .... (mg/kg} Organic Compounds Results(mg/1} P&T:GC/MS -../ Arsenic <v .. o benzene ------_ Acid:B /N Ext. ✓ Barium 3S-carbon tetrachloride --MTBE ...i.::::::_ Cadmium </O chlordane ----Chloride chlorobenzene ------✓ Chromium <co chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------✓ Lead CID cresol ------ --__ -Manganese 1,4-dichlorobenzene -- --L Mercury L. o -o:J 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene ----~ t/,!. 0 v Selenium --2,4-dinitrotoluene __iL_ Silver <t..o. __ heptachlor Radiochemistry Sulfates hexachlorobenzene ----·······-•· Zinc hexachlorobutadiene ----Parameter Results (PCi/1} --pH --hexachloroethane __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane --Date Received Reported by --methoxychlor __ toxaphene DJle Exlraclc<l Date Reported 2,4-D {?93654 f1AR 17'7 --_ 2,4,5-TP (Silvex) Dale Analyzed Lab Num --DI IS 3J'JJ (Revised 2/91) NC Dcputmcnt of Environment, HccalL!l, &. Narual Re,ourcc1 SoliJ Wa•L<: hlanai;emcni D,vi,ion SAMPLE ANALYSIS REQUEST Si.late Laboratory of Pliblic Hc,dth P.O. Box 28047, 306 N. Wilmini;lOn St. Ralcii;h, North Carolin• 270 I l-W47 01701'' Site Number ________________ Su.mp le ID Number/Name _______ :::=..~c,'-'.Jae....... _________ _ Name of Site---={µ;__..:..., M__,_"-...:...fl_~_J_\\i_· _·Le-=-1~J_1vt;-'·-'~-<---Collcctc..:l By ____________ ID# _____ _ SiteLoe.1tioo ______________ Dau::Collcctc..:l __ ___:')__-_L_1:"..:...·_-_cr.:...· .1...7 _____ Time ______ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compow1ds RouJL:i(mg/1) EnvironmenL'1I Concentrate Comments V arseruc L..c .. c.·-:J.-. - H-v111 -5 ✓ barium "-<a..3 - Ground Water (1) _:--'Solid (5) V cadmium <.. c,. -~ --..JL. chromium L.._ D -c,.!5 Surface Water (1) Liquid (6) ✓ !Cl.Id L... = -c,..'.'.5 --/ mercury z.. 0-C, 1· ~Soil (3) Sludge (7) ---;:;;" selenium <.,o .a?,. -✓ ~il ver L'.., c.. -6 !;j - -Ot.hc:r ( 4) -Other (8) - - - Org:rnic Chemistry Inorganic Chent.stry - Parameter Raults (mg/I) Parameter Re::;uJ•• g,tr)(mg/kg) Organic Compounds .Rbulb(mg/1) P&T:GC/MS ~antimony bc:lll.cnc -- Acid:13/N Ext. ._..LL: lif5CfUC < t./. () cu.rbon tc:trachlondc --:2,4-D -1{ barium ?,l(<> chlordane -- -:2, 4 ,5-TP(Sil vc:x) beryllium chJoroben.z.cne 7 -chlorda.nc: cadmium <10 chJoroform --- -hcpLUchJor -chloride o-crcsol -hexachlo ro ben.z.ene / chromium 2-c m-cre~ol -- hc:xachlo ro bu Lad i enc cobalt p-cresol ---c:ndri.n copper crc:sol ---lindane f1uoride 1,4-dichloroben.zene --- -methoxychlor -iron 1,2-dichloroethanc -<lo -toxaphcne ~ lead 1, 1-dichJoroethy lcne - --rrunganese -2, 4-d ichloroctby lc:nc -~ mercury L.-o~I hcptach.lor -nickel hc:xachJorobcnzcnc -----nitrate bexachlorobuta<liene ~to 0 -~ selcni um hexachlorocthane -Vsi!vcr methyl ethyl ketone -FOR LAil USE ONLY sulfates rulroberuc:nc --thallium pent.uchlorophcnol --Date Recc:ivc..:l vanadium pyridine -- -zinc tetrachlorocthylene -Date Extracted pH trichlorocthylenc: -- -conductivity -2,4,5-lrichlorophenol Date Analyzed -TDS 1,4 ,6-trichlorophenol - -Jhsh point -vinyl chloride Reported Ily end ri.n -- lindane --Dace Rcponc..:l OO:Jt;55 MAR 17'11 --methoxychlor -toxaphene -Lab Number --2,4-D --2,4,5-TP (Silvcx) OHS JI 91 (Rcvi,cJ 12193) NC Department of Environment, Hc.alU'l, & NaOH•I Rc•our~ci Solid Wa•t.c hlan.ai;cmcm Divi•ion SAMPLE ANALYSIS REQUEST St.le LaboraLOry of Publi~ He->lth P.O. Box 28047, 306 N. Wilmini;ton St. R,lci~h. North Carolin• 27ol t-ij0,-!7 Site Number ______________ Sample ID Number/Name ____ O=-\.,_1_;_.:O::...-=0;;....'-..c........ ________ _ Name of Sit.c ___ LJ_:::_r...:..M..:...:._v...:...M_· _i:;1.1_....::G=-1.1---=]l.{.,__r(.__,__ Collected By _____________ ID# _____ _ SiteLocation _______________ Dat.cCollectdl __ ,_·_3_ . .,_t-f_✓_1_1_;__ _____ Time ______ _ . Agency: Hazardous Wa.st.c Solid Waste L/' Supcrfu.nd TCLP Compounds ---- Sample Type Inorganic Compow1ds Re:;uJLS(mg/1) Environment.al Concentrate Comments / arsenic <. C -e>:J-.. 7 barium ,_ 39 I-< /J,,7-5' - Ground Water (1) ,._/ Solid (5) / cadmium L., D-c.5 -- -+ chromium ~o-05 Surface Waler ('.2) Liquid (6) -,L lead ✓---D -Q.5 --_L mercury L_D~O) _:-"'soil (3) Sludge (7) / ~elen.ium < a~a 2, --/ ~ilvcr -<... 0 -~ - -Other ( 4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Raults (mg/I) Parameter RbuJl5--)(mg/kg) Organic Compounds .RDulLS(mg/1) P&T:GC!MS antimony bcn.une --✓ lif5CruC <:'.'. ¼ 0 -Acid:13/N Ext. carbon tetrachloride -7 -'.2,4-D bi.lfium :a,c:o chlordane --- -'.2,4 ,5-TP(Silvex) -beryllium chJorobcnz.c:ne -chlordo.nc ✓ cud mi um <to chJoro form --- -bepIBchlor -chloride o-cresol -hcxachJ o ro beru.ene ✓ chromium 18 cn-crcsol --- -hexachJorobutaJienc cobalt p-cresol --endrin copper crcsol ---lllldane 0uoridc 1,4-dichJorobenzene --- -methoxychJor -iron 1,2-dichloroethane - -loxaphcne V lead ~co 1, 1-dichloroethy!ene ---nu.nganese -2,4-dichloroctlly lene -L macury L...-c,_) -hcpwclllor --nickel bexachl oro befll.Cne --nitrate bcxachlorobutaJiene -<<t .. o -v selenium hcxachloroctbane -- -t,L silver <" t'() methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobenunc -- -thallium penl.J.lchlorophenol -Date Received vanadium pyridine -- -zinc tctrachloi-octhykne -Date Extracted pH trichlorocthy lcne -- -conductivity -2,4 ,5-trichlorophenol Date AnaJyzcd -TDS '.2, 4 ,6-trichlorophenol - -fl,~h point -vinyl chloride Reported l3y cndrin -- lind.J.ne -Date Reported - --mcthoxychlor Lab Numb!)O:lf;56 M~R 17CJ7 -toxapheoe - --'.2,4-D --'.2,4,5-TP (Silvcx) D11S ]191 (Rcvi,cJ 1:2/9]) NC Dcputmcnt of E:1vironmcnt, Ho..lUJ, & Nan.iril Rc . .ourccs Solid Wa,1.c l',lan.ai;cmcni Divi,ion SAMPLE ANALYSIS REQUEST S1.11c LaboraLOry of Public Hc..,.llh P.O. Box 28047, 306 N. Wilmini;ton SL R•lci,:h, North Carolina 27C>l 1-li0-17 Site Number ______________ Su.mp le ID Number/Numc __ O_t_7 __ 6_b_l~---------- Name of Sit.c __ LJ_· .!....P'"P-tt~c:• -=£c..;...W_--=C.,=7 --'v-,\,l~'-'"C-f'-. _,____ Collected By _____________ ID# _____ _ SiteLllCJ.tion _______________ DatcCollecrd ___ >-__ t"----q'-:7_,_ ______ Time _______ _ - Agency: H .az.a.rd o us Was t.e Solid Wa.st.c / Superfund TCLP Compounds ---- Sample Type lnorga.ruc Compow1ds RtsulLS(mg/1) En vi ronmenL'l I Concentrate Comments / arsenic ~C-.:::C.d-, --;?"" b . 1_j4:. D~-5' anum ✓Solid (5) - Ground Water (1) ..,,/ cadmium -i_ o_e-..15 -7' chromium -<:..o _ o .:5 Surface Water (2) Liquid (6) --::;;,--· lcud L.. a _05 ---;T mercury -4'..c~l v Soil (J) Sludge (7) / selc:n.ium L.. D-0¢ ----,/ ~ilvcr L.c..-c,.S - -Oilier (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Raults (mg/I) Parameter Re:;uJts~(mg/kg) Organic Compounds Rt::iulLS(mg/1) P&T:GC/MS antimony bc:uune --Acid:B/N Ext. / 11rscn.ic (l.(;D carbon tetrachloride ----:;::;,-barium - -2,4-D /7:o chlordane - -2,4 ,5-TP(Silvcx) beryllium chJorobc:n.zcne --chlordane / cadmium <to chloroform --- -bcpuichJor ch.Jo ride o-cresol -- -hcxachloro benzene __L chromium ('lD m-cresol -hcxachloro bu 1.ac..l i enc co bu.1 t p-cresol ---endrin --copper -cresol lindane fluoride I ,4-dichlorobenzene --- -mcthoxychlor iron 1,2-dichJoroethanc --lOXaphcne / lead <·la I, 1-dichJorocthykne --- --rrunganese -2, 4-d ichloroctl.Jy !enc -/ mercury ..L.. c:,_ \ heptach..lor --nickel hexachlorobcn.zcne ---nitrate bcxachlorobutnc..liene --< lf.. D ~ selenium hexachloroetbane -./ silver <lo methyl ethyl ketone -FOR LAil USE ONLY :;ulfutes nitrobefl.2.c:nc --thallium pcnt.uchlorophenol --Date Received vanadium pyridine --2.JnC tctrachJorocthylcne Date Extracted -- -pH -trichJorocthylc:ne -conductivity -2, 4 ,5-trichJorophenol Date Analyzed -TDS 2,4,6-trichlorophenol - -jfa.,h point -vinyl chloride Reported By endrin -- lindane --Date Reponed -mcthoxychlor Lab Numbe?OJ657 MAR 1797 - --toxaphene :Z,4-D -- -OHS 3191 (Rcvi,cJ 12/9)) -2,4,5-TP (Silvex) NC DqJ&nmcnl of Environment, H"lt.h, & NanH1I Rc.ourcci Solid Wa,Lc ~lana0cmcnt Divi•ion SAMJ>LE ANALYSIS REQUEST St.otc uboratory of Publi.; H""'llh P.O. Box 2~0-17, 306 N. Wilmin,;ton St. R•lcii,:h, North Carolina 2701 !-ij047 Sit.cNumbcr ______________ S!UilplclD Numbcr/N!Uilc ___ 8_1 1_~_6~Z: __________ _ Name of Sit.e ---'-l.J---"A-R.,_,, .;..;:;,.:C/4.=· .,_1-'-Y'---~C:z,-' ~VM-'--~TV___._ __ Collected By ____________ ID h' _____ _ SiteLoCJ.tion Dat.cCollect.cd ·'3,-3 -11 1 Time ---------------------'=---""-'---'--------------- . ✓Superfund Agency: Hazardous Waste Solid Wast.c TCLP Compounds ---- Sample Type Inorganic Compounds Roulb(mg/1) EnvironmenL1l Concentrate Comments ...L arseUJC L.e:._a:J.., / barium l -?s.f\ _::Solid (5) l.JM5 - Ground Water (1) / cadmium L-.o_e,5 --/ chromium <D -0 5 - Surface Water ('.?.) Liquid (6) _L_ !cud -<. C ) -C,-5 --/ mercury L... CJ_ C l -/ Soil (J) Sludge (7) ,/ selenium <._ 0 -D 2, --- / ~ilver .L....o_c-,s - -Oilier ( 4) -Other (8) - --Organic Chemistry Inorganic Chemistry - Parameter Raults (mg/I) Parameter Re:;ults~(mg/kg) Organic Compounds Rbulb(mg/1) P&T:GC/MS antimony oellZcne --- Acid:13/N Ext. / uscnic <'/.0 carbon ttlrachloride - / barium -'.?.,4 -D l1r''1 chlordane --• - -'.?.,4 ,5-TP(Silvc::x) beryllium chJorobe11.2ene -- chlordane ./ cadmium <10 chloroform --- -hepIBchlor chloride o-cresol -- -hexachl o ro ben.z.ene _k"chromium ~-')__ m-cresol - -hc::xachlorobu t.aJiene cobalt p-cresol -- c:ndrin copper cresol ---li.nJane fluoride 1,4-dichJoroben.zenc: ----methoxychlor -iron 1,2-dicWoroethane - -toxaphcnc: /lead <le> J, 1-dicWorocthylcne ----nunganese -2, 4-d ichloroct!Jy lcnc -_L_ mercury L... 0-GC/ -hc:µtach.lor -nickel hexachJorobenzc:nc -- -nitrate bcxachJorobutaJic:ne -<i;l ,) -/ selenium hexachloroetbane 7 silver - -<to -methyl ethyl ketone FOR LAB USE ONLY :rnlfutc:s nil ro bt:ll2Cnc --thallium penlllchlorophc:nol --Date Recei val vanadium pyridine --z.inc 1ctrach1oroethylc:ne --Date Extractw pH trichloroethylcnc: -- -conductivity -2,4,5-trichlorophenol Date Ana.lyz.cd TDS :?., 4 ,6-trichl orophc:nol -- -Jl;~h point -vinyl chloride Reportw Ily c:nJ rin --lindane -- Date RepolJo3658 MAR 11,1 -methoxychlor - Lsb Number --toxaphene -:?.,4-D - -OHS JI 9 I (Rcvi ,cJ 12/93) -2,4,5-TP (Silvcx) NC D9llnmcnt of Enviroruncnt, H""'llh, &. NatlH•I Rc.ourcc1 Soli.J Wa,L<: l>larui;cmcnt Divi,ion SAMPLE ANALYSIS REQUEST Slate Laborat.ory of Publi,: Hc.,lth P.O. Box 28047, 306 N. Wilmini;ton St. R•lci1,;h, Non.h Caroli n• 27ol l•W'17 Site Number _______________ SumplcID Numbcr/Nume ___ ....:6:........:.1_1_6_· _J,..l'-...:::0=----------- Name of Sit.c _ _.\=,,u,_·._c::-'-~-'Rv-=-=e_v\t~_Co-_'_vi.,1_.,_r-f-"--__ Collected By ____________ ID# _____ _ Site Location Date Colkct.cd "2:,-5 _ q 1 Time ----------------___ __;:__....::.;. __ ..:.______ -------- Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type lno~anic Compow1d.s Re:sult.s(mg/1) EnvironmenL'll Concentrate Comments ___L arsenic ..C..c:>-o :J.... / barium o_tao Ground Water (1) _:: Solid (5) JPr~ -BB / cadmium Z 0-C>;J --/ chromium -< ~-C:.~ Surface Water (2) Liquid (6) ~ l=d a_;~) --7 mercury Lo_c.,j ~Soil (J) Sludge (7) / selenium ..::....o_c:,:J., --;r-~ilver ~ C>-0§ - -Other (4) -Other (8) - - -Organic Chemistry Inorganic Chemistry - Parameter Rault.s (mg/!) Parameter Resu.lt.s.-)(mg/kg) Organic Compounds Rbull:i(mg/1) P&T:GC/MS antimony bcn.une --- Aci d:13/N Ext. ✓ 11r5CfUC < '-1, ('\ cubon ttlrachloride -7 -2,4-D ba.rium ·:;)..6 chlordane --- -2,4 ,5-TP(Silvex) -beryllium chlorobcflZCne -chlordane :./ cud mi um ~to chloroform --- -heplllchlor -ch.lo ride o-c resol - -hexachlorobenz.ene ✓ chromium ·::10 m-cresol -- -hexach.lorobuUJ.dicne coba.lt p-cresol --endrin copper crcsol ----lmdane fluoride 1,4-dichlorobenz.ene ---mcthoxych.lor iron 1,2-dichloroethanc --:7" lead 9 B. - -toxaphenc --1, 1-dichloroethylene --rn:uiganese -2, 4-d ichloroctlly lcnc -;/ mercury -'.o_.:-.39 hcpwch.lor -- --nickel hexach.lorobenzcne --nitrate bcxachlorobutadiene --::;--, selenium 2?;.g -hexachloroclhane -::;,,' silver - --methyl ethyl ketone FOR LAil USE ONLY .sulfates nitroben:z.cne -- -thallium penlllchloropbcnol -Date Received vanadium pyridine --z.rnc 1e1rachlorocthylcne --D ate Extracted -pH -trich.lorocthylcne -conductivity -2,4,5-trichlorophenol Date Ana.ly:w:I -TDS 2, 4 ,6-trichlorophc:nol - -11.t.sh point -vinyl chloride Reported Ily cndrin -- lincLine --Date Reponed -methoxychlor La -00,3659 MAR 1797 - -toxaphene -b Number 2,4-D -- -DHS] 191 (Rcvi,cJ 12/9)) -2,4,5-TP (Silvcx) NC Dcputment of Environment, HC-llll.tl, &. N•OJral Rc,ourccs Solid WoL.: l>l•tu~cmcnl Divi,ion SA.MPLE ANALYSIS REQUEST StJitc Laboratory of Publi.: Hc..1llh P.O. Box 2~047, 306 N. Wilminbton S1. R•lcii,:h, North Carolina 270! l-~0-17 Si1.e Number _______________ Sll!Ilplc ID Numbcr/N=e ___ C> __ (_7_0_L_1 _________ _ Name of Site ___ LJ___,~'-'--..;.__J.---'·:;_-t\,_,._J __ G_·, _v_'>v(_.__Tt.f~-CDllc:ctcd By ____________ ID# _____ _ SiteLocation Date Collected 3 -5 -er, Time ---------------------=-"----------------- Agency: Hazardous Was1..e Solid Wasu:: __ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compow1d.s ResuJts(mg/1) EnvironmenL1l Concentrate Comments / arsen..ic < C. -u .J,. 7 barium I.,. c::,O ~olid (5) .JA-B-PB - Ground Water (1) / cadmium ~0-DO -- ...L chromium <... D -0!:l Surface Water (2) Liquid (6) / !cud ~ -59 --~ mercury ""-D-b' ~Soil (J) - Sludge (7) / selenium < O -o:), -- ~ ~ilver <D-C~ Other (4) Other (8) --- - -Organic Chemistry Inorganic Chemistry - Parameter Raults (mg/I) Parameter Re:;uJts~(mg/kg) Organic Compounds ,Rc:;ult.s(mg/1) P&T:GC/MS antimony lienunc ---Acid:!3/N Ext. ✓ l!f~cnic <½n ca.rbon tttrachloride -- -2,4-D / bil.fium ;i_ 0 chlordane - -2, 4 ,5-TP(Silvc:x) beryllium chJoroben.z.cne --chlord!lilc: ✓ cadmium (to chloroform --- -hepwchJor chloride o-cresol / chromium - -hc:xachlorobenzene /.{., rn-cresol -- -hexachlorobutadic:ne cobalt p-crcsol --cndrin copper crcsol ---lindane f1uoride 1,4-dichlorobenzene --- -mc:thoxychlor iron 1,2-dichJorocthane -l&o - -IOxaphcne ✓ lead l, 1-dichJorocthylcne ---manganese -2, 4-dichlorocll.Jy !enc -✓ mc:rcury .t....a .. c,3 -heptachlor -nickel hcxachloroben.zcne ---nitrate bcxachlorobutnc.lienc -:::-,, selenium <<..r,,o -hexacWoroetbane -:;;,-silver (lo - --methyl tthyl ketone FOR LAB USE ONLY :.ulfutes nitroberucnc ---thallium penlllchlorophenol -Date Received vanadium pyridine --zinc tetrachlorocthylcne --Date Extracted pH trichJoroethylene -- -conductiviry -2,4,5-trichlorophenol Date Analyzed TDS 2,4 ,6-trichlorophenol -- -lla.:;h point -vinyl chloride Reported By cnt!rin -- lindane --Date Reported -methoxychlor 003660 MAR 1797 - --toxaphene Lab Number 1,4-D ----2,4,5-TP (Silvcx) OHS J 191 (Rcvi,cJ 12/9)) NC Department of Environment, HulLh, & Narur•I Rc1ourcc1 SoliJ w •• i.: ~l,n.ai;cmcni Divi,ion SA.~LE ANALYSIS REQUEST St.Ille l...abonwry of P\Jbli,; Hc.-illh P.O. Box 28047, 306 N. Wilmin.;ton St. R,lcii;h, North Carolina 270! 1-W•i? Site Number ______________ Sample ID Number/Name ___ 6_J_l_O~_-Z;;...._""L _________ _ Name of Site __ .;_L/~tt..-1..~!___p._tJ:._N...:.-_~_, .-:....::_,N__,__ Collc:cted By ____________ ID# _____ _ SiteLoc.ition Dat.cCollcct.cd 6-& .,,, 9 7 Time -------------------------------------- - Agency: Haz.ardous Waste Solid Waste __ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compow1ds Re:;uJLS(mg /1) EnvironmenL1l Concentrate Comments / arseruc ~ = -= ::;i..__ 7 barium '~-3Q Ground Water (1) Solid (5) /l/1 /✓1 ~ / cadmium <:. o _c.;,5 --7 chromium L-..Q 0,.~ Surface Water (1) Liquid (6) -r lcac.l .L...._~c,5 ---r- --,,L mercury L...D ~ r..2 j Soil (J) Sludge (7) / selenium L_ 0-~d---. --- / ~ilvcr ..::!._ = -,::::,...S -Other (4) -Other (8) - - - Organic Chemistry Inorganic Chemistry - Parameter Rault.s (mg/I) Para.meter ResuJts~(mg/kg) Organic Compounds ,Rt::iulb(mg/1) P&T:GC/MS antimony bcn.unc: --- Acid:B/N Ext. J uscruc < l/, 0 ca.rbon tetrachloride --- 1,4-D ,./ barium /:Ju chlordane --- -1,4 ,5-TP(Silvex) -beryllium chJorobc:n..z.cnc -chlordane ✓ cuc.lm.ium < /<) chloroform --- -bepLachJor chJoric.le o-cresol --hexachJoroben.zene ✓. chromium <to m-cresol --- -hexachJo ro bu t.aJ icnc cobalt p-cresol --endrin copper cresol ---lindane flu oride 1,4-dichJorobcn.zene . --- -mcthoxychJor iron 1,1-dich..lorocthanc / lcac.1 <10 - -toxaphenc: --1, 1-dichJorocthylene -manganese: -2, 4-d ichlorocl!Jy lcnc -✓ mercury ,c;,o_c_-::,9 -hcpt.ach.lor nickel bcxach..lorobcnzcnc: ---nitrate bcxachJorobutnJiene --:;;, selcni um <t;.f -hexachloroclhanc / -silver lllt:tbyl clhyl kclone --FOR LAB USE ONLY :.ulfutcs n.i t ro berucn c: -- -thallium pcnwchlorophenol -Dare Received vanadium pyridine --2.inc tctrach..lo.rocthylcne --Dare Extracted -pH -trichJorocthy !enc -conductivity -2,4,5-trich..lorophenol Date Analy:w:1 -TDS 1,4,6-trichlorophcnol - -fl,i.:;h poinr -vinyl chJoric.lc Reported I3y enc.lri.n -- lindanc --Date Reported methoxychlor -- Lab Nu mbe903661 MAR 17CJ7 --tox aphene 2,4-D -- --2,4,5-TP (Silvcx) Dl!S 3191 (Rcvi,cJ 12/9]) NCDEHNR Division of Waste Management D Superfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab: --c--- Inorganics Lab: v--" ( CHAIN OF CUSTODY RECORD Project Name: l.J,,,_ rN.-.. C.,..,.,,_.fy Site ID # (NCD#) --------- Sampled By: _ __,,.9_· · . .__#.,,-=------- Sampler ID _________ _ Location: ------------Telephone:(__) _______ _ Address: Date Sampled: 1/-, 7 L/-f -if-'7 Time Sampled: ________ _ Sample Types: Soil Water ~ Waste Other Remarks: Trrus 1 LE:S5 1 H-Ef\ DVV!l\ k T B T CA-Al A-0 Field Sample Numbers Received By:2;;1/;~ (Signature) C E' I-+ J 0A P ..S G-Cc Date: YphJ Time: __ _ Date:y:-1:,-<P 7 Time: ___ _ Date: V-11'~7 Time: //4' 2.. c Date: « Time:g : ';)__/ 1 11.:J1u11 o.:. 1"lalura1 Kcsourccs Solid Waste Management Division _P.O. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Sile Number ----------------Field Sample Number ___ O~~"-'~/_,'f ________ _ Na me of Site L,.J A R,R.e, J\.l C ov cl t:::t' Lmq ~1 LL Site Location __ --=W.;c._:A_,_,«,..,.,t...,._1c,._'.,,M~....,,(,_,· c""',u"--'-'-1\J"-"IY'-'----------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste ✓ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments ✓ Arsenic <. 0-C,d., --✓ Barium C:J _ 'l 5 __ Groundwater (1) __;[_ Solid (5) LES 5 v Cadmium -<-0-C.·5 _.k'.:'.:_ Chromium L~ C: ~ C:.5 __ Surface water (2) Liquid (6) ✓ Lead --<c.c,-5' --.!::C_Mercury L... ,:-~ -I .::,[_ Soil (3) Sludge (7) _L Selenium <:.(JQ ·'J.._ --d-Silver <.. C: -.::::-5 _ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results~ (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS V Arsenic (({., c benzene ---:7 Bari um ---_ Acid:B/N Ext. ·J] carbon tetrachloride ----MTBE ✓Cadmium <cr,.v chlordane ------Chloride chl orobenzene ------✓ Chromium ?--0 chloroform ------ --Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ---- --v Lead <q,.r: cresoi -- ----Manganese 1,4-dichlorooenzene -- --✓ Mercury < O,j 1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----<'. Cf~ Q --/ Selenium --2,4-dinitrotoluene ✓ Silver <q.,j/ __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene , ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------.. TOC pentachlorophenol ---- --__ pyridine Microbiology --tetrachloroethylene --trichloroethylene --Parameter Results (Col /lO0ml) --2,4,5-tr.ichlorophenol ---- --2,4,6-trichlorophenol ---- ------vinyl chloride endrin --lindane --Date Received Reported by --methoxychlor --toxap hene D:it e ExtractcJ Dale Reported 2,4-D 004988 APf\ 1197 --_ 2,4,5 -TP (Si lvex) Date AnalyLcd Lab Number --DI IS 3191 (IZcviscd 2/91) I tcalth, &. Natural Resources Solid Waste Management Division _P.O. Box 23047, 306 N. Wilming1on Street Raleigh , North Carolina 27611 Site Number ----------------Field Sample Number ____ 0_[7_...._l_,._1_5.,___ ______ _ Name of Site W AUE,~ CovcffY LttMo hl.L Site Location __ --'W--'A~R~t.~~=M~~G~-,-M~N~IY~--------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste _L_Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments ✓ Arsenic --L!._ a_ Od,. ✓ Barium C~IJ.- __ Groundwater (1) ~ Solid (5) H-ES5 ✓ Cadmium Z O-o5 .JL:::_ Chromium L__OvC5 __ Surface water (2) _ Liquid (6) ✓ Lead < D -e:5 --__L Mercury <-0.\ v Soil (3) Sludge (7) _!L_ Selenium { Q.Q ·l _,d_Silver ~-C ,_c.':)._5 _ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results~ (mg/kg) Organic Compounds Results (mg/I) _ P&T:GC/MS V Arsenic ~1:c benzene ----::::7 Barium ---_ Acid:B/N Ext. carbon tetrachloride ----MTBE ✓Cadmium <ct,! chlordane ------Chloride chlorobenzene ------✓ Chromium ·::;2.0 chloroform ------Copper o-cresol ------Fluoride m-cresol ------ --Iron __ p-cresol --1,f --v Lead cresoi -- ----Manganese --1,4-dichloruoenzene --✓ Mercury < o. l --1,2-dichloroethane Nitrate 1, 1-dichloroethylene ------/Selenium {. <£ C} --2,4-dinitrotoluene ✓ Silver <q,k" heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --tetrachloroethylene -- --trichloroethylene Parameter Results (Col/lOOml) --2,4,5-trichlorophenol ---- --2,4,6-trichlorophenol ----vinyl chloride ------endrin --lindane --Date Received Reported by methoxychlor -- --toxaphene Date Extractc.:t.l Date Reported 2,4-D 004989 APR 1197 --__ 2,4,5-TP (Silvex) Dale.: Analyzed Lab Number --DI IS 3191 (llcviscd 2/91) ' 11cil1ln, OL J'latural Kcsourccs Solid Waste Management Division _?.O. Box 2E047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ ---'0~ ..... 1-,_,___._I L,_/ .... ~.__ _____ _ Name of Site L,J A(tR.E, "-". Cov,-ff':{ l@o hl...L Site Location __ _.c,W__,A~R.~t.~s:~-=M~~G~·.c_-'Af~:r",(~IY~--------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste __L_ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments / Arsenic <:c-c:;), --✓ Barium 0~ 8G: __ Ground water (1) ___::!_ Solid (5) 0 T>l A ✓ Cadmium ...::__ Q_,::-,5' _L Chromium -C:..0-0 5 __ Surface water (2) _ Liquid (6) ✓ Lead ---< -~ L -c-..:5 _L Mercury <.. c:, -'i _y__ Soil (3) _ Sludge (7) _K_ Selenium <0, Q 'd.. _d,_Silver L_,, L~-C .!5 _ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results ~(mg/kg) Organic Compounds Results (mg/I) _ P&T:GC/MS V Arsenic < l/.-C) benzene ----;::::7 Barium ---_ Acid:B/N Ext. hlf carbon tetrachloride ----MTBE ✓Cadmium <'?,f: chlordane ------Chloride chlorobenzene ----1?! --✓ Chromium chloroform ---- --__ Copper o-cresol -- Fluoride m-cresol ------ --Iron p-cresol ---- --v Lead < q,g, cresoi -- ----Manganese --1,4-dichlorooenzene --✓ Mercury <( O,l --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----(...<£_I. Q /Selenium --2,4-dinitrotoluene ✓ Silver ( 9, J::::: heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene , ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha Conductivity methyl ethyl ketone ----Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --tetrachloroethylene --trichloroethylene --Parameter Results (Col/lOOml) --2,4,5-trichlorophenol ----2,4,6-trichlorophenol ------ ------vinyl chloride endrin --lindane --Date Received Reported by methoxychl or -- --toxaphene Date Extracted Dale Reported 2,4-D 004990 APR 119 7 -- --2,4,5-TP (Silvex) Date Analy1cd Lab Number --I)I IS 3191 (llcviscd 2/91 ) N.C. Department of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number ____ O_J_,---"(....;;.(_i _______ _ Name of Site L1Aftg€N C,,JAJ.'f'l( lA-"lOFlLL-Site Location_--=Wc.;....i.A...:...rt=t\..,.e::.:..N"----=C:,;.._c;_v-"""..c:.....1.\':::Y_._ _______ _ Collected By __________ _ ID# Date Collected Ti.me ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium KTB --✓ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1)w,g:'f If) Organic Compounds Results(mg/l) _P&T:GC/MS ✓-Arsenic <IJ,, 0( benzene --✓ Barium _ Acid:B/N Ext. /),. (J ·i carbon tetrachloride --MTBE v Cadmium < {2_.,_Q OJ--chlordane -------Chloride chlorobenzene ------ --✓Chromium <o, Di chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ---- --✓Lead (O., oo ,-cresal ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury 4 0 ' CCJ05 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium <a.oo~-2,4-dinitrotoluene ----✓ Silver <:o, ◊.J-heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachloi-ophenol -- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) __ 2,4,5-trithlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ melhoxychlor __ toxaphene D:.ite Extraclc<l Dale Re0rted 2,4-D 04991 ~PR 11 97 --_ 2,4,5-TP (Silvex) Dale An.:Jlyzcd Lab Number --DI IS 3191 (Revised 2/91) I lc~lth, & Natural Resources Solid Waste Management D ivision UC'>J.TAA .&....1.1..:J i"1J. ,r>...J.....J.L U.I.U .l'-..,L..,'...,[_ '-'~~ .&. -,,a,r: LiiUUf<Hury 0 1 ruo11c Health P.O. Box 28047, 306 N. Wilmingion Street Raleigh, Nonh Carolina 27611 Site Number Field Sample Number O ,-, l f S -------~~------------------------ Na me of Site LlAfl.;i{£N ~Vt-1.'f\( LA-~OF\U.... Site Location_--=W----'-A-'-'ltL.:>..L>t(,..,.e:'-'-N_.__----'~~u"""'N~l'::Y___,_ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Age ncy: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) TB --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver ---_ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (•a,0 w) Organic Compounds Results ( mg/l) _ P&T:GC/MS ✓ Arsenic <o. Cl I benzene ----Acid:B/N Ext. ✓ Barium <o. OJ carbon tetrachloride ------MTBE v Cadmium <o.oo.r chlo:dane ------Chloride t:hlorobenzene ----<o.ol --✓Chromium chloroform ------Copper o-cresol ------Fluoride m-cresol ------Iron p-t:resol ------ --vLead < o. oo~ cresol ---- --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury .:(o _.::,..:::.a..5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium C 0 -l!OJ 2,4-dinitrotoluene ----..,,--Silver <o.os= heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexa chlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --tetrachloroethylene -- --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by --methoxychl or __ toxaphene D:.it e Exlr aclc.:c.l Dale Re()orled 2,4-0 . 04992 APR 11 97 --__ 2,4,5-TP (Silvex) Dol e AnolyLc.:d Lab Number --DI I~ Jl'JI (Revised 2/91) I lc:ilth, & Na tural Resources Solid Waste Management Division ._.,~,..a.A A.JA..J r>...&..,ri...L..1.&.U.A.U .&~""'l_ ..__,.&.J..._, .&. , .. H O.L'. .. L,O,VVIO.\U l J Ul r uo11c t1ca1tn P.-0. Box 2S047, 306 N. Wi lmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number _____ O_l_i_,__1._l......_C}+-------- Name of Site lJA{t«f'N Cou,-.J.T"-{ LA-~OFtU.. Site Location_~LJ__._A~&'-"'-"~~e;~N~_~_u_"'-'~l':::Y~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: --Hazardous Waste · Solid Waste / Superfund TCLP Compounds Sample Type Inorganic Compounds Results (mg/I) En vironmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) AW --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Oth er (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/!) Parameter Results (mg/1) Iii ~,O ~ Organic Compounds Results (mg/l) _ P&T :GC/MS ✓ Arsenic <o, o I benze ne ----_ Acid:B/N Ext. v Barium J,. Ol( carbon tetrachloride --MTBE v Cadmium <o .. oos chl o,dane -------Chloride chl orobenzene ----<o,ot --✓Chromium chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------Iron <a&OO,~-__ p-cresol ----✓Lead cresol ------ --__ · Manganese 1,4-dichl orobenzene -- --✓Mercury <O-D00.5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium ( /), OQ.J 2,4-dinitrotoluene ----(().,l),J ✓ Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----··••--·· Zinc hexachl orobut adiene ----Parameter Results (PCi/1) pH · hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyr idine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-tri'chlorophenol ----__ 2,4 ,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by --meth oxychlor __ toxaphene D~lc Extractcc.1 D ale Reported -2,4-D 004993 APR 1197 --__ 2,4,5-TP (S ilvcx) Dale AnalyLcd Lab Number --DI IS 3191 (IZcviscd 2/91) , -. .._,, LJ .._.}-'._.,.,,..._.,, V l L.,IIVl.1.V IIJll\,,l ll, l lcallh, & Natural Resources Solid Waste Management Division Ur1....LT.A.I. J..JA:.J r1...1..,~.1...,JJ.U J.'-...L.,,"'-<_VAJU.&. ..:><dtc Ll!uuracory or t'uOt,c Health ?·.o. Box 2&)47, 306 N. Wilmington Street Raleigh , North Carolina 27611 Site Number Field Sample Number ____ O _ _,_f_,,__,_1....:::,1,..aoe....::;.t; ______ _ Name of Site GJ A'({,-p£N G, u ,J.11-( LA-A.{ p Flu..... Site Location_~LJ~A~fl.~i1~e;~N~-~-u~f\./~l':::Y~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- • Barium ✓ Ground water (1) -~ T) --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(rng/1) '"-@,'le Organic Compound:j Results (mg/l) _ P&T:GC/MS ✓ Arsenic <o,o 1 benzene --✓ Barium _ Acid:B/N Ext. <01:0l carbon tetrachloride --MTBE v Cadmium <o.oor_ chl o,dane ------Chloride l'.hlorobenzene ------ --✓Chromium <o ... o t chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol -- --✓Lead <0,.00:.C cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury -4..(J _ DDD :5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium (o. 60d--2,4-dinitrotoluene ----.,,.-Silver <_o, tl£ heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) __ 2,4,5-tiichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vin yl chloride endrin --lindane --Date Received Report ed by __ methoxychlor __ toxaphene D:ite Exl raclc<l D ale Reported 2,4-D --004994 APR 11 97 __ 2,4,5-TP (Silvex) Dale Analyzed Lab Num ber --DI IS 3191 (ll cviscd 2/91) , ~ ....... 1.....n .. puJ l111cJu U l c11vuun1ncnc, l lcalth, & Natural Resources Solid Waste Management Division uH..J.T.lJ: LC. ftl iH...L.1. .:,1.:, ~"-VC.u .l .:,tate uoo ratory of Public Health P.O. Box 2.8047, 306 N. Wilmington Street R..aiei~, North Carolina 27611 Site Number Field Sample Number O (, ll.1 -----=---'--'----'--=--~----------------------- Collected By -----------ID# Date Collected Ti.me ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium B 8 --✓ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/1) 'Jis/lRR) Organic Compounds Results (mg/I) _ P&T:GC/MS ✓ Arsenic <·o, o r benzene --✓ Barium Acid:B/N Ext. C>~O C. carbon tetrachloride ----MTBE v Cadmium < D.-O◊J-chlo:-dane -------Chloride L'.hlorobenzene ------ --✓Chromium <o~ D l chloroform -- --Copper o-cresol ---- Fluoride m-cresol ------ --Iron p-cresol --(o,o a.r -- --vLead cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury L_ C -w O C-..::, 5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium ~ o, oo.r 2,4-dinitrotoluene ----...,,-Silver <:o, 6-.r-heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····-·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --tetrachloroethylene -- ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene D:.ite Exlraclc.:J Dale Rep(Y(f~995 ~PR 1197 2,4-D ---__ 2,4,5-TP (Silvex) Dale A nal yzed Lab Number --DIIS 3191 (llcviscd 2/91) I ICJlth, & Natural Resources Solid Waste Management Division ._., ............... ~.a....1 ~,~..a..u.a.u .,...._.,_,"'-._a-J.._.. ... ,.J\o.u .. L-Ovu1a~u1y Ul ruo11c Health P:O. Box 28047, 306 N. Wilmingion Street Raleigh, No rth Carolina 27611 Si le Number ----------------Field ·sample Number _____ C>~l;.._'7-'---'t'-='1.=-l...-=------- Name of Site lJ 1, f-.tl,£N G, u ~ff'-< LA-"' o Flu... Site Location _ __;;LJ_.A-'-'--"8,...,tt,...,.i;:'--N._,___C::,_u~"'-'~l':::Y__._ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ?S --✓ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (T) Selenium --Silve r --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I}~ g;ittl) Organic Compounds Results (mg/l) P&T:GC/MS ✓ Arsenic <a~ol benzene ------Acid:B/N Ext. v Barium C2e ,;;) g carbon tetrachloride --MTBE v Cadmium <0.00-.1 -chlo:-dane -------Chloride chlorobenzene ----< 6,D { --✓Chromium chloroform ------Copper o-cresol ------Fluoride m-cresol ------ --Iron p-cresol ---- --✓Lead <o.60J-cresol ---- --__ -Manganese 1,4-di chlorobenzene -- --✓Mercury ..C:::::.o _c,oo5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene --<"o.[) o ,r --✓Selenium 2,4-dinitrotoluene ----✓ Silver < o. o .. C heptachlor ----Radiochemistry Sulfates hexachl orobenzene ----····-·-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroe thane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------ TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- lindane --Date Received Reported by __ methoxychlor __ toxaphene D:.ite Exl ractc<l Date Reported 2,4-D --00i;99C APR 11 97 __ 2,4,5-TP (Silvex) D:.i te Analyzed Lab Numl::ier --DI IS Jl'J I (IZcviscd 2/91) ''·'--· , ... n .... p u11111cnl u1 cnvuunmcnr, I lcalth, & Natural Resources Solid Waste Management Division ..:Jf-1..J.Y.lC-LC, l-li~tt..L.lulu nL\l_V.C...:J.l :,tate uooratory ot Public Health P.O. Box 28047, 306 N. Wilmingion Street Raleigh, North Carolina 27611 Site Number Field Sample Number O t-i t~~ ------'-"--'....,_.___ _______ _ Na me of Site G.J A ftfl,£N G, 1..1 r,J. T'-{ LA-~ o Fl LL-Site Location _ __cW__._er-'-"'it'-=-"t\--><e:'--N.~_C,_o_V~/\.l~Y::Y~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) J DH -- _ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) '4£ g/kf) Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <01:DI benzene ----_ Acid:B/N Ext. ✓ Barium t2 rD ?:: carbon tetrachloride --MTBE v Cadmium <o,oor_ chlordane ------Chloride chlorobenzene ------✓Chromium Or() I chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ----✓Lead <o~oa.c cresol ------ --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury ~Cl-ooo.5 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----✓Selenium < 0, 06-.!--2,4-dinitrotoluene ----......-Silver <o.of heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene Dale Exlraclcu Dale Reported 2,4-D ··· · ... --004997 APR 1197 --2,4,5-TP (Silvex) Dale Analy1cd Lab Number --DI IS 3191 (!Zcviscd 2/91) 1 ... ,._, l.."--}J<.l'l111cnl u1 cnvuunmcnr, I lcJllh, & Natural Resources Solid Waste Management Division ::,tatc Laboratory of Public Health P~O. Box 2&)47, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Site Number ----------------Field Sample Number ___ --=C>'--'-1_-Y-'--.,_I "l..~'1------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Envir.onmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) 8 Am --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/1)..wo:'l llt Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <o ~o t benzene ----_ Acid:B/N Ext. ✓ Barium /'J. D. ""± carbon tetrachloride --MTBE V Cadmium <o .. oos::: chlo:dane -------Chloride chlorobenzene ----(o,.o -- --✓Chromium ; chloroform ---- --Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol --<o .oor --✓Lead cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury .C... a_ uo_O 5 --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----✓Selenium <o, o~--1-2,4-dinitrotoluene ----.,,--Silver <o,, o ..r heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-tr1chlorophenol ----__ 2,4,6-trichJorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene D:.ile Extraclc<l Date R eported 2,4-D --004998 APR 1197 2,4,5-TP (Silvex) Dale Analyzed Lab Number --DI IS 319 1 (l~cviscd 2/91) 1 lcalth, & Na1ur.:1l Resources Solid Waste Management Division P:0. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O I c 1'.l,. S------~-~--------------------------- Site Loca tion_---=-LJ___._A.,__.tl=l\~["-N._,__--"C::._v""""""'--'-'-l':::1/___._ _______ _ Collected By -----------ID# Date Collected Ti.me ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) _ Solid (5) AL-B Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I; fMJ,O~ Organic Compounds Results (mg/I) _ P&T:GC/MS ✓ Arsenic <·o" o I benzene ----_ Acid:B/N Ext. ✓ Barium I). 0 6 carbon tetrachloride --MTBE v Cadmium ( o .. 00.J chlordane -------Chloride chlorobenzene ------ --✓Chromium <·o-0 I chloroform ---- --Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol --<o 1O0J----✓Lead cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury < 0-6 005;;;; 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene --<IJ,.O(JS---✓Selenium 2,4-dinitrotoluene ----✓ Silver {/J, 0:-!-__ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- lindane --Date Received Reported by __ methoxychlor __ toxaphene D;,it e Extractc.:J Date Reported 2,4-D -- 004999 APR 11 97 __ 2,4,5-TP (Silvex) Dal e Anc1l yzc.:d Lab Number · --DI IS 3191 (H.cviscd 2/91) 1 ... -....... ucJ.JUi l111cnl u1 cnvuonmcnr, l lcallh, & Natural Resources Solid Waste Management Division :>late Laboratory of Public Health P.-o . Box 2&047, 306 N. Wil mington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O If ["l. b -------~"--"'------------------------- Name of Site LJ A flf{£N Co u r.J.T"'-( LA-"{ p Fl LI--Site Location_~W___._A~tl~rt~t?;~N.~_C:_o_v~f\.l~Y::::Y~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) DR ~ --_ Solid (5) Cadmium --Chromium --__ Surfa ce water (2) / Liquid (6) Lead -- --Mercury Soil (3 ) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/1) ( a,ftaw) Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <:o.o I benzene --v Barium _ Acid:B/N Ext. f)., 07= carbon tetrachloride --MTBE v Cadmium < o. oo .C _ chlo:-dane ------Chloride chlorobenzenc ------✓Chromium < o. 0 ( chloroform ---- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----✓Lead <o,aor cresol ------ --__ -Manganese --1,4-dichlorobenzene --✓Mercury <o_ac-~os --1,2-dichloroethane --Nitrate 1,1-dichloroethylene --<o,oa...e --✓Selenium 2,4-dinitrotoluene ----.,,.--Silver <o,. or heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroe thane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Re ported by __ methoxychlor __ toxaphene D~le Exlraclcc.l D ate Reported 2,4-0 .. --{ir"l cnn,., APR 1197 2,4,5-TP (Silvex) ~\.J. __ ~·0 .' --DJ!e Analyzed Lab Number ---1)1 IS 31')1 (H.cviscd 2/91) ,,.\.... uepar1mcn1 or t:.nvuonment, l lcalth, & Natu ral Resources Solid Waste Management Division .:,AfYH'L.t ANALr.:,1~ Kt\,lU.t.:,1 State Laboratory of Public Health P.-0. Box 28047, 306 N. Wilming1 on Street Raleigh, North Carolina 27611 Site Number Field Sample Number O t-, l'l..., ----~~-~------------------------- Name of Site lJ Arzf<£N C.u "'-'0< LA-"' o FtU-Site Location_---=LJ--'-A-'-IZ..,,_._,&..,.e;::.:..N..,______;:C::,~u_,"'-'-"-'--'1':::Y_,_ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) RPAB --_ Solid (5) Cadmium --Chromium --__ Surfa ce water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/1)-6 m't'I) Organic Compounds Results (mg/l) _P&T:GC/MS ✓ Arsenic (o, or benzene ----_ Acid:B/N Ext. ✓ Barium 0 ✓119 carbon tetrachloride --MTBE v Cadmium (o.oos: chlo:dane -------Chloride t.:hlorobenzene ------ --✓Chromium <o,6( ch loroform -- --Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ----✓Lead C . -cresol ----Ot:t2d,I -- --__ -Manganese --1,4-dichlorobenzene --✓Mercury .C::..~-CK:>c:,5 --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----✓Selenium <o .. {)Q.C 2,4-dinitrotoluene ----✓ Silver (o.os-__ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alph a --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Paramet er Results (Col/lO0ml) --__ 2,4,5-tri'chlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lind ane --Date Received R eported by __ methoxychlor __ toxaphene D;ile Exlraclc:t.l Dale Reported 2,4-D -- L b N bOO .SOO1 APR 1197 __ 2,4,5-TP (S ilvex) Dale Analy,:cd a um er --DI IS JJ'JI (ll.evised 2/91) l'·"--· u~pu11111cnl 01 c nv1ronmenr, I lea Ith, & Natural Resources Sulid Waste Management Division ::,late Labo ratory of Public Heal th P.-0. Box 2S047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number O ,..,. f")_ 'g _____ .;.._; __ -=------------------------- Name of Site LJ A l\«£N C, u "'-T1-< LA-~ p F\ LI-. Site Location_~LJ:.=....L.A.!Jlll::::.~u...i.c[c:..:N.:,__..::::C:,.:::..:..u.:..::l'-l:,__l':Y.,__,__ _______ _ Collected By -----------ID# Date Collected Ti.me ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) /;las,'I«) Organic Compounds Results(mg/J) P&T:GC/MS ✓ Arsenic (o,D { benzene ----✓ Barium _ Acid :B/N Ext. (). O 8 carbon tetrachloride --MTBE v Cadmium ((),oo,.C_ chlo:-dane ------Chloride chlorobenzene ------ --✓Chromium .( IJd2 t chloroform --__ Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol --<o, 00£ -- --✓Lead cresol ---- --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury L..L_--:::,_ L°O>C>t:::, ~ --1,2-dichloroethane --Nitrate 1,1-dichloroethylene . ----✓Selenium <a.oo::-C 2,4-dinitrotoluene ----✓ Silver <o,D C heptachlor ----Radiochemistry Sulfates hexach lorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha __ Co nductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Param eter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vin yl chloride endrin --lindane --Date Received R eported by __ methoxychlor __ toxaphene 0Jle Extracted Dale Reported 2,4 -D --oo .~on2 APR 1197 __ 2,4,5-TP (Silvex) 0Jte AnalyLcd La bNumb er · '"· -· --DIIS 3191 (l~cviscd 2/91) I lcallh, & Natural Resources Solid Waste Management Division --------·-·--------""'-----~--~-.__...,...., .... ~ ..... ~.r '-'l 'U Utll.. ,,cdll{l P:O. Box 28047, 306 N. Wilmington Stn:et Raleigh, North urolina 27611 Sile Number ----------------Field Sample Number ____ O_f_i_l_2..--"-1j,__ ______ _ Name of Site lJ Aft1?£N C.v ,J,T'( LA-~ p F\LL-Site Location_---=W_.,A-'--&L"-Uo&...,.e'.:..:...N_,__-----"Co---'--v-"~-'· ..... t::Y_· .___· _______ _ Collected By -----------ID# Dale Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium RBAB --✓ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (rng/1)" AsO\t) Organic Comp_ounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <o,o I benzene ----_ Acid:B/N Ext. ✓ Barium t2, o l carbon tetrachloride --MTBE v Cadmium <o.oa,C . chlo:-dane ------Chloride chlorobenzene ------,/'Chromium <Od) ( chloroform ----Copper o-cresol ------Fluoride m-cresol ------Iron p-cresol ------✓Lead ~ o, oo,C cresol ------ --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury L_C)_;:,,_,c,..$ 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----,/'Selenium <0-00,\..--2,4-dinitrotoluene ----.,..-Silver ( De D,.C heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alp ha __ Conductivity --meth yl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pen tachlorophenol ---- --__ pyridine Microbiology --tetrachloroethylene -- ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trlchlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene D:.ite Extraclc.:<l Dale Reported 2,4-D 00500~1 APR ll 91 --__ 2,4,5-TP (S ilvex) Date Analyzc.:d Lab Number --DI IS 3191 (Revised 2/91) I lcalt h, & Natural Resources Solid Waste Management Division .. Ho.~1.... L,dUUtalury u1 r uo 11c Health P.O. Box 28047, 306 N. Wilming10n Street Raleigh, North Carolina 27611 Site Number . .J Field Sample Number C> ,, I ~ ~ ----~--~~------------------------ Name of Site lJ AJ{.&£N G.u ,J,T'-{ LA-~ o Ft LL-Site Locatiori_--=W___._A...,__._,,1t ...... t<,...,.t;''-'-N-"-------"C,---'o_u"""',...;--'---'-l'::Y__._ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ G round water (1) _ Solid (5) A:·J Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I)~ g;'lptJ Organic Compounds Results (mg/l) _ P&T :GC/MS ✓ Arsenic <o,o I benzene --v Barium _ Acid:B/N Ext. a, o' ca rbon tetrachloride --MTBE v Cadmium ( o ' bQ ~-chlo,dane -------Chloride ch lorobenzenc ------ --✓Chromium <o. t) I chlo roform -- --Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ---- --✓Lead (o. oo c:: cresol ---- --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury L_o _ c,oQ..S 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium <o.oo.S-2,4-dinitrotoluene ----..,.-Silver <:o, o ..c heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ G ross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pen tachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trii.:hlorophenol ----__ 2,4,6 -trichlorophenol ----__ vinyl chloride endrin --lindane --Date R eceived R eported by __ methoxychlor __ toxa phene D:.ilc Extraclc<l D ate Reported 2,4 -D --oo\soo4 APR 1197 --2,4,5-TP (S ilvex) Dale A nalyLc d Lab Number --DI IS 31')1 (ll.cviscd 2/91) I lcalth, & Natural Resources Solid Waste Management Division ~"......._ • ..._ ... ..&.J.L.J ~,C>,.,.A...J.&.U.&.U "''---"-"''-l.~-....J~.&. J lau.: LAuu Ja~u1y or r uo11c Hcaltl"'l r.Q. Box 2&)47, 306 N. Wilmingion Street Raleigh, North Carolina 27611 Si te Number ----------------Field Sample Number ___ _,6e:::....L..l1_.__._l_.:!>,L\_.__ ______ _ Name of Site LJ A ft"P£N C, u f.J. '0( LA-A.Io Flu... Site Location _ _;:W~er-"--rzL.:>.LI,rt ..... e:::..:..N..i._____.:~;;_;;;_U_;f\.l~l'::Y_,_ _______ _ Collected By -----------ID# ____ Date Collected ___________ Time ______ _ Agency: --Hazardous Waste Solid Waste / Superfund TCLP Compounds Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments . Arsenic --Barium ✓ Ground water (1) Rt> F --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury Soil (3) _ Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results(mg/1)'8im'I~ Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic < 0., Ol benzene --_ Acid:B/N Ext. v Barium t2, 01,· carbon tetrachloride --MTBE v Cadmium < o, ooJ-chlo:-dane -------Chloride i.:hlorobenzene ------ --✓Chromium <o , or chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol -- --✓Lead <o, oi,,,C cresol ---- --__ -Manganese 1,4--dichlorobenzene -- --✓Mercury 4. e:, -~D-5 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----✓Selenium <o~o oC 2,4-dinitrotoluene ----✓ Silver <o. o..C heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·-Zinc hexachlorobutadiene . ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----_ .. _ vinyl chloride endrin --lindane --Date Received Reported by methoxychlor --__ toxaphene D:il e Extractc<l Date Reported 2,4-D --e,,9'"00C ~PR, 1 97 2,4,5-TP (Silvex) Dale Analyzed Lab Num\/e .J '-,J L.i. --DI IS 319 1 (l{cviscd 2/91) I lc:ilth, & Natural Resources Solid Waste Management Division ........ .-....,_ ........ ,11,..J ,1...-.....,4A...A-J ............... .-.--x----P.D. Box 2S047, 306 N. Wilmington Street R.alcig.h, Nonh Carolina 27611 Site Number Field Sample Number 611 I~ l.. -------...c....a<....:;;;;=------------------------ Name of Site G.J A f-,)Z£N G, u ,.,rr-< LA-A:' p Fl LL-Site Location_---"W------'-A-'-'R'-"-'-",1""'e:'--N-'--_C:,_u~"-'~T'::Y~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) BAJ ft --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (1) Selenium --Silver --_ Other (4) --Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) '6,s,011) Organic Compounds Results (mg/I) _ P&T:GC/MS ✓ Arsenic < o ,o I benzene ----_ Acid:B/N Ext. v Barium I), 0 "J carbon tetrachloride --MTBE v Cadmium <t?,6oC chlordane ------Chloride chlorobenzene ------✓Chromium < o. O f chloroform ------ --Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol --✓Lead <orb()£ cresol ------ --__ · Manganese 1,4-dichlorobenzene -- --✓Mercury .c'....o .. --,oc,5 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene ----✓Selenium ('·o ~ooS: 2,4-dinitrotoluene ----..,,--Silver <o, o..C heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ' -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by --methoxychlor __ toxaphene D:ile Exlractc.:<l Date Reported 2,4-D -- Lab NumbQPSQQt APR 11 97 __ 2,4,5-TP (Silvex) Dale AnalyL<.:d --I)/ IS 3191 (ltcviscd 2/91) .. ..._.. . ._. -r~• .,.,..,_,., Vl .a....,IIYI.I.VIIIU\.,llll I lc:ilth, & Natural Resources Sulid Waste Management Division UC:L.L.Y.&.A. ~.a.:., ~-,r1...L.J..l.U.A.U .&'-..L-,1'..,[_ '--,1&...JLJ .A. vlol~ LAvu1d1u1)' u l ruo11c Health P.D . Box 28047, 306 N. Wilmington Street R.lieigh, North Carolina 27611 Site Number Field Sample Number () I~ t~ ~ -------~~------------------------ Name of Site lJ Af-,'R£N ~u,J,T1-( LA-'-'PFlU.... Site Location_--=-LJ__,__A.:..,.8,=l\~~N'-'--_Co~_u'-'-N'-'tl~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments . Arsenic --Barium ✓ Ground water (1) J -DW --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (rng/l)~s,-e Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <a,o t benzene ----_ Acid:B/N Ext. ✓ Barium c), 0 l( carbon tetrachloride --MTBE v Cadmium <c>,ooc _ chlo.:-dane ------Chloride chlorobenzenc ------ --✓Chromium (:v.eit chloroform --__ Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ---- --✓Lead <o.DoS-cresol ---- --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury L'... ,-..,_c,!'.:.2c:,S 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene --<o, ooS:: --✓Selenium 2,4-dinitrotoluene ----✓ Silver <o. or: __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----.... ____ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride 'endrin --lindane --Date Received R eported by __ methoxychlor __ toxaphene D:.ile Exlraclc<l Dale Reported 2,4-D -- Lab NumJ1P50Q7 APR 1197 __ 2,4,5-TP (Silvex) Dal e AnalyLcd --DI IS 3191 (lleviscd 2/91) .. ._., .__,..,_yu,\111'-IH U L J.....UVU Vl1111CIJL1 l lcalth, & Natural Resources Solid W aste Management Division .:,cate uooratory ot t'ubl1c Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number _____ O_l_'(_-'-1 'l=-'1-+------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) At)J -- Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _. Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) •g;'lt,' Organic Compounds Results(mg/l) P&T:GC/MS ✓ Arsenic < o,o t benzene ✓ Barium --_ Acid:B/N Ext. O,r) 6 carbon tetrachloride --MTBE v Cadmium <o.oo, ch lo:dane ------ Chloride chlorobenzene ----< 0, Cl { --✓Chromium chloroform ----Copper o-cresol ------Fluoride m-cresol ------ --Iron p-cresol ----✓Lead < l?,, 00 .r;:: cresol ------ --__ -Manganese --1,4-dichlorobenzene --✓Mercury <o_c:c:>=5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium <o,oo.S-2,4-dinitrotoluene ----✓ Silver <01:0~ heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone G ross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ rnethoxychlor __ toxaphene D:it e ExtractcJ Date Reported 2,4-D --005008 ~PR 1197 __ 2,4,5-TP (Silvex) D;.itc Analyzed Lab Number --1)1 IS 3191 (llcviscd 2/91) I lc:ilth, & Natural Resources Solid Waste Management Division Ur>..J.T.1..1. .LI.&..:.-1'"1.l .,~..1. U.lU .l'-...L,,'-l... ...__,.,.,_U .A. J <a,c: urnorarnry or t'uo11c Health P:O. Box 28047, 306 N. Wilmingrnn Street Raleigh, North Carolina 27611 Site Number Field Sample Number 01.., •~~ ___ ___;:::;__--'----'"----='----------- Na me of Site lJ A ftfl,E;N 0:, u ,J.T'-( LA-~ o F\ u... Site Location_--"LJ___,_A--'--'-"ll.....,1\...,.€"-N._,___~_v~N~l'::Y~-------- Collected By -----------ID# Date Collected Ti.me ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- ; Barium ✓ Ground water (1) C.. ~ M --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (T) Selenium --Silver ---_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) wa,'lst, Organic Compounds Results (mg/I) _ P&T:GC/MS ✓ Arsenic <:: o.o ( benzene --✓ Barium Acid:B/N Ext. Q, /() carbon tetrachloride --MTBE v Cadmium <o.-Qo --4---chlo:-dane -------Chloride chlorobenzene ----(o,o I -- --✓Chromium chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ---- --vLead <o.-oc£ cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury ~ L)> -c.OD.5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium $<2 · oo_F 2,4-dinitrotoluene ----..,.,-Silver heptachlor --O,Q,..S --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ penlachlorophenol -- --__ pyridine Microbiology ----tefrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-tdchlorophenol ----__ 2,4,6-trichlorophenol ----__ vin yl chloride · endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene DJlc Exlraclc<l Dale Reported 2,4-D -- 005009 hPR 11 97 __ 2,4,5-TP (Silvex) Dale Analyzed Lab Number · --1)1 IS 3191 (Revised 2/91) ----,--····-··---_ ....................... , I lcalth, & Natural Resources Solid Waste Management Division ....,.,a...,i.,..,.., A.J~ ~,~ ... u.a.u •'--"-'"'-..._,,...._....,..._ .. .na.L'-LAuuJ.alury ul ruo11c He:an n P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number Dr, l;i Ga --------~~----------------------- _ Name of Site lJ Afl1?£N C, v ,J,'0( LA-"' O Ft u... Site Location LJ A&& ~N C:.v"-' t::Y -----='---'-'-'-" .......... =--'--"--"---'--'-'-....__. ________ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium --✓ Ground water (1) Solid (5) JDA Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (T) Selenium --Silver ~ --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) "tiiu:'"' Organic Compounds Results (mg/I) _ P&T:GC/MS ✓ Arsenic ~QlO l benzene ----_ Acid:B/N Ext. ✓ Barium O,o ~ carbon tetrachloride --MTBE v Cadmium <o< 60 ,_ chl ordane ------Chloride chlorobenzene ----I -- --✓Chromium Z6, C chloroform ---- --Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol -- --✓Lead <o.oo-.!-cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury ..C::..c::,_c:,~6-5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene --(6~00£ --✓Selenium 2,4-dinitrotoluene ----..,...-Silver <o-oc heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hex.achloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) __ 2,4,5-trithlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene D:.ite Extraclc:<l Dale Reported 2,4-D 005010 APR 11 97 --__ 2,4,5-TP (Silvex) Dale AnalyLc:d Lab Number --DI IS 3191 (ltcviscd 2/91 ) I lcallh, & Natural Resources Solid Waste Management Division ~~,.-..a. .A..JLJ r:1,.,1.-,~.1. u.1.u .L'-...&...J'-,[_ .....,.&..Jt.J .a. '-Jld.lc Lavurdiury or ruo11c Health P.O. Box 28047, 306 N. Wilmington Street R.alcig.h, North Carolina 27611 Site Number Field Sample Number o,-i. ,~.., -------~------------------------- Name of Site lJ A ~g£N 0, <hi. "f"I.( LA-"' o Flu,._ Site Location_---=LJ--1.A..:..fti..::,..u.t<...,.e::.:..N~---"G;...;0;_1.1-'"'.=...1.l'::Y__..__ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic -- PS Barium ✓ Ground water (1) c,... --_ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (1) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) IJ&mf~ Organic Compounds Results ( mg/l) _ P&T:GC/MS ✓ Arsenic <o,o 1 benzene --✓ Barium _ Acid:B/N Ext. ()' II carbon tetrachloride --MTBE v Cadmium <Co C QC, ) chlo:-dane -------Chloride chlorobenzene ------ --✓Chromium Co. o l chloroform -- --Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol --{CJ,60-.J -- --✓Lead creso l ---- --__ · Manganese --1,4-dichlorobenzene --✓Mercury L_ o_'----:,o o..5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----✓Selenium ~~, IJO'-C 2,4-dinitrotoluene ----.,.....-Silver o,o r heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene D~te Exlraclc<l Dale Reported 2,4-D --005011 APR 11 97 __ 2,4,5-TP (Silvex) Date Analyzed Lab Number --1)1 IS 31'!1 (Revised 2/91) I lcalth, & Natural Resources Solid Waste Management Division P.O. Box 2&047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Sile Number Field Sample Number ____ O-"'----'\'--,--'--l'--'~ ........ &'.__ _____ _ Site Location LJ /!&I\ ~N C:.v"·-'l'':Y ----'---'--'--'-' ........ "---'----~~~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium cc. --✓ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead --__ Mercury Soil (3) Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) •m'I~ Organic Compounds Results(mg/l) _ P&T:GC/MS ✓ Arsenic <o, DI benzene ----_ Acid:B/N Ext. v Barium I), 0 6 carbon tetrachloride --MTBE v Cadmium <o .ooJ-_ chlordane ------Chloride chlorobenzene ------ --✓Chromium 12. o I chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ---- --✓Lead (t;, OoS-cresol ---- --__ -Manganese --1,4-dichlorobenzene --✓Mercury ~:.. Z")_,.::,r,1.r~5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----< a_,. O()j ✓Selenium 2,4-dinitrotoluene ----.,,..-Silver <o~or heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------ TOC __ pentachlorophenol -- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxaphene D:.ile Exlraclt:<l Dale Reported 2,4-D --005012 APR 11 97 2,4,5-TP (Silvex) Date AnalyLt:d Lab Number --DI IS 3191 (ltcviscd 2/91) , -. ....,. ,._,.._y .. •••11.._.u• Vl J...-IIYI.L V 11111l..llL1 I lcal lh, & Natural Resources Solid Waste Management Division ur1..1..,A.&. .LJ£..:..I r1.J.-,/"1..J....,..L.U.I.U J.~'-l_ .._,,A...J.._, .&. ..,, .. ,c L-dUUrdtury or ruo11c Health P."O. Box 23047, 306 N. Wilmingion Street Raleigh, North Carolina 27611 Site Number Field Sample Number b ·I-,· t ') C\ ----------------------------------- Name of Site GJ A ftf?,£.A/ C, v Nol'( LA-AJ p F\ u.... Site Location_---"LJ'---'A..:....,.:,~,._,l\...,.e;:..:..N..,__----.::~~u~"''-'-'-'l'::Y_.._ _______ _ Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) _ Solid (5) J 0 t( --Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (cg;11~ Organic Compounds Results ( mg/I) _ P&T:GC/MS ✓ Arsenic Co. o I benzene ----Acid:B/N Ext. ✓ Barium Q,.66 carbon tetrachloride --MTBE v Cadmium <. O,DO~C chlordane -------Chloride chlorobenzene ------ --✓Chromium <o. o I chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol -- --✓Lead <or c20 t: cresol ----1,4-dichlorobenzene --__ -Manganese -- --✓Mercury <.a. c,c.,C>-5 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene --{o. oo..C --✓Selenium 2,4-dinitrotoluene ----✓ Silver (o,or heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexa chloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane --Date Received Reported by __ methoxychlor __ toxap hene 0;.itc Exlractcc.l Dale RepQQd 2,4-D Sot~J APR1197 --__ 2,4,5-TP (Si lve.x) Date Analyzed Lab Number --DI 1:i 3191 (Revised 2/91 ) I lcallh, & Natural Resources Solid Waste Management Division ---·------··-------X. ---- P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number Field Sample Number C> (f I 'f<3 -----'------''-------------------------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results (mg/I) En vi ronmen ta! Concentrate Comments Arsenic --Barium --✓ Ground water (1) Solid (5) A1 "' Pt Cadmium --Clrromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) (iiil!,1 11~ Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <a.ol benzene --_ Acid:B/N Ext. ✓ Barium D < 0 9 carbon tetrachloride --MTBE v Cadmium <o.-oos chlo:-dane ------Chloride chlorobenzene ----( o,. o I -- --vChromium chloroform ----Copper o-cresol ------Fluoride m-cresol ------ --Iron __ p-cresol -- --✓Lead <o .. oor cresol ---- --__ -Manganese 1,4-dichlorobenzene -- --✓Mercury < 0 ,. ,-,c;,b -~ 1,2-dichloroethane -- --Nitrate 1, 1-dichloroethylene --( 6, QOJ~ --vSelenium 2,4-dinitrotoluene ----.,,.-Silver < o~t>£ heptachlor ---- Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------ TOC pentachlorophenol ---- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trithlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- lindane --Date Received Reported by __ methoxychlor __ toxaphene D:1lc Exlraclc<l. Date Reported 2,4-D 005014 APR 1197 --2,4,5-TP (Silvex) Dc.11c Anc.1lyzcd Lab Number --DI IS 3191 (llcviscd 2/91) I I lcalth, & Natural Resources Solid Waste Management Division P.Q. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Site Number ----------------Field Sam pie Number ___ __,C,ac--'-\--'1,___l.,_'1-"'-IL--_____ _ Name of Site uJ Mt1{£N C, u "'-T1-f LA-~ o Fl LI-. Site Location_--"W---'-tr-'-lt...,._,,l\..,.e:'-N...,___~_u~N~l':::Y~-------- Collected By -----------ID# Date Collected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium ✓ Ground water (1) BT --Solid (5) Cadmium --Chromium --__ Surface water (2) / Liquid (6) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter Results (mg/I) "-_Bag5'ht) Organic Compounds Results (mg/I) _ P&T:GC/MS ✓ Arsenic <o, o I benzene --✓ Barium Acid:B/N Ext. {), () 6 carbon tetrachloride ----MTBE v Cadmium <o.OQC_ chlo:dane ------Chloride chlorobenzene ----(o.o t --✓Chromium chloroform ------Copper o-cresol ------ Fluoride m-cresol ------Iron p-cresol ----<o .. ooj---✓Lead cresol ------ ----_Manganese --1,4-dichlorobenzene --✓Mercury L.... 0 -0r-1c~"z 1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----( o, oor: --✓Selenium 2,4-dinitrotoluene ----.,....-Silver < D, O.C: heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ' ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --tetrachloroethylene -- ----trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol __ vinyl chloride ---- endrin --lindane --Date Received Reported by --methoxychlor __ toxaphene DJtc Extractc<l Date Reported 2,4-D --~nc::0-..1 t: APR 1197 2,4,5-TP (Silvex) \.lV.\ ~ t .,.'t_ :.....:.l Date Ana lyLcd Lab Number --I)I IS 3191 (llcviscd 2/91) l lcallh, & Na tura l Resources Solid Waste Management Division -------a-•a-------X. ---- P:O. Box 28047, 306 N. Wilming1on Street Raleigh, North Carolina 27611 Site Number Field Sample Number e. ,·._, r 1.f'i,... -----~--~~----------------------- Name of Site GJ A'(l:(l,£N G, v N.TY LA-~ o Flu.... Site Location _ __;::LJ~A..:..Jt1,,_,,_l\u...,,:["-N.,_____;;~c...;;._1.1_,f\-l..c.:....i.t:Y_,_ _______ _ Collected By -----------ID# Date CoUected Time ---------------------- Agency: Hazardous Waste Solid Waste / Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium RORJ --✓ Ground water (1) Solid (5) Cadmium . --Chromium --__ Surface water (2) / Liquid (6) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Pam meter Results (mg/I) Parameter Results (mg/I~ r.;i.:'lll'" Organic Compounds Results (mg/l) _ P&T:GC/MS ✓ Arsenic <o~ 01 benzene ----_ Acid:B/N Ext. ✓ Barium D,QJ carbon tetrachloride --MTBE v Cadmium <o~oor chlo:dane -------Chloride chlorobenzene ----( o, o I --✓ Chromium chloroform ------ --Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol --<0.00-£: -- --✓Lead cresol ---- --__ -Manganese --1,4-dichlorobenzene ✓Mercury c:::· 1,2-dichloroethane --< (_c, -~ c-:-. .r>---' -- --Nitrate 1,1-dichloroethylene ----✓Selenium t Q •. Od~ 2,4-dinitrotoluene ----..,.,.-Silver heptachlor --t>, D l --Radiochemistry Sulfates hexachlorobenzene ----····--·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nilrobenzene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroethylene ----trichloroethylene Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol --__ vinyl chloride --endrin --lindane --Date Received Reported by --met hoxychlor --toxaphene D:.ilc Extract cJ Dale Reported 2,4-0 005016 APR 119 7 --__ 2,4 ,5-TP (Silvex) Dale Ana lyzed Lab Number --DI IS 3191 (llcviscd 2/91)