NCD980602163_19961023_Warren County PCB Landfill_SERB C_Field Sampling Plan-OCR

MEMORANDUM
TO: PCB Landfill Working Group
FROM: Patrick Barnes, P. G., Science Advisor
DATE: October 23, 1996
SUBJECT: Amendments to the Draft Sampling Plan Dated, October 2, 1996
It is my opinion that the referenced plan should be amended by the following list of items:
1. Include a table of contents identifying all components of the plan including
figures, tables, and appendices.
2. Include the jointly agreed to supplemental sampling and testing plan
developed by BF A as an appendix. This is needed to provide critical
support to the proposed new testing locations.
3. SECTION ENTITLED "FIELD SAMPLING OVERVIEW"
a. Include a description of the project background, as previously agreed to so that
the Plan will function as stand alone document.
b. Identify who will be the site manager, safety officer, and the
individual disciplinary task leaders.
c. Last sentence of the oversight paragraph, change "a site safety
briefing" to a daily site safety briefing.
d. Amend safety plan to include safety issues associated with drilling
activities.
e. Change "History of the Site" section of the safety plan to reflect
recent analytical data.
f. Add definition as to what constitutes being "involved" as described in
the final sentence of the first page.
g. Include a site plan showing the conceptual layout of exclusion zones
and safe zones.
h. Define "crucial elements" as mentioned in the third paragraph of the
second page.
4. SECTION ENTITLED "ANALYTICAL REQUIREMENTS AND QUALITY
ASSURANCE"
a. Clarify apparent contradiction in paragraph entitled "Blank Samples." Paragraph
states that equipment rinseate blanks will be prepared to check decontamination
procedures then two sentences later the text states that equipment rinseate
blanks will not be needed.
b. Under Chain of Custody subsection, item number one, change shipment to
delivery.
c. Include a copy of the sample analysis request and receipt of samples form
indicated under item number two and three.
d. Critical portions of each of the standards referenced should be included as an
appendix to this plan.
e. At the end of this section add the following :
Reporting Procedure-Every laboratory asked in this effort will be instructed not
to provide any data, preliminary or final, verbally or in writing t the State unless
the same information is provided simultaneously to both Science Advisors.
5. SECTION ENTITLED "LANDFILL CONTENT SAMPLES"
a. Immediately after "Purpose" include a reference to the location of the samples.
b. Change the phrase "a soil sample needs to be taken" to "will be taken."
c. Under "Field Sampling Method" include an appendix reference to all necessary
equipment and procedures.
d. Under "Sampling Personnel Requirements" describe the proposed "air sampling."
e. Under "Field Equipment Required' include a table listing all necessary equipment.
f. Under "Quality Assurance" add a general description of the anticipated
laboratory QNQC. For examole what quantity of matrix spikes and matrix spike
duplicates are anticipated.
6. SECTION ENTITLED "LANDFILL LEACHATE SAMPLES"
a. Include field sampling location immediately after "Purpose."
b. Third sentence under "Field Sampling Method." What is considered a sufficient
sample?
c. Under "Field Equipment Required," we may want to consider dedicated
samples-.;:;,,
7. SECTION ENTITLED "GROUNDWATER SAMPLING PLAN"
A Include "Field sampling locations" immediately after "Purpose."
b. Add the word representative before samples in the first sentence of the
"Purpose" subsection.
c. Under second sentence of "Field Sampling Method," after "Purge the Well" add
"field test for equilibration using pH temperature and specific conductance.
Add more specific reference to EPA SOPs, i.e., what page number, what paragraph.
Also tie to an appendix of this document. The second to last paragraph of "Field
Sampling Methods" needs to include a decontamination procedure for submersible
pump.
Under "Field Equipment Required" State proposed procedure to ensure integrity of
samples.
8. SURFACE WATER AND SEDIMENT SAMPLES
a. Move subsection on field sampling location to just below "Purpose."
b. Under "Field Sampling Location" add the following :
the exact location of stream and sediment samples will be determined in
the field by the Science Advisors.
Add one additional sediment sample location to be collected at the confluence of
Richneck Creek and the Unnamed Tributary.
9. SECTION ENTITLED "SEDIMENTATION BASIN SUBSTRATE
SAMPLES"
a. Move "Field Sampling Locations" to directly after "Purpose."
10. SECTION ENTITLED "CARBON FILTRATION BED SAMPLES"
a. Move "Field Sampling Locations" to directly after "Purpose."
I •. •' ..
11. ADD SECTION ENTITLED "TEST BORING SOIL SAMPLES" and
appropriate sampling and testing procedures .
. FIGURES
a. Add a site location map.
b. Add a smaller scale approximately l" = 50' site map.
TABLES 1 and 2
a. Add test boring analysis for two horizons at each new location adjacent to
the landfill i.e., MWlA, MW5, and MW7 and each of the background
wells.
b. Add sediment sample at the confluence ofRichneck and The
Unnamed Tributary.
FIELD SAMPLING PLAN
FOR WARREN COUNTY PCB LANDFILL
DRAFT DRAFT DRAFT
October 2, 1996
Prepared for
Joint Warren County and State PCB Working Group
by
North Carolina Department of Environment,
Health, and Natural Resources
Division of Waste Management
FIELD SAMPLING OVERVIEW
FIELD SAMPLING OVERVIEW
TEAM ORGANIZATION
All field efforts by staff of the Division of Waste Management or its contractors will be lead by the
Division Site Manager of the field effort. A Site Safety Officer will be appointed by the Director
of the Division and will be independent of the direction of the site manager.
The field team, reporting to the site manager, will consist of adequate numbers of staff to safely
complete all required field sampling, labeling, and reporting tasks in an efficient manner.
Individual members of the field team will coordinate with the disciplinary task leader developing
the methodologies and protocols for the field sampling and analysis effort. These disciplines may
include the following:
Environmental chemistry
Environmental engineering
Hydrogeology
Environmental toxicology
Environmental statistics
Analytical chemistry
In addition, two (2) representatives of Triangle Labs will be present for all sampling events. Tbis
is necessary to comply with independent chain of custody and sample labelling requirements.
OVERSIGHT
The Science Advisor(s) to the Joint Warren County and State PCB Landfill Working Group will
directly oversee all field activities of the Division of Waste Management and contractors at the
field sampling effort. All oversight individuals must be currently trained by 40-hour OSHA
hazardous waste worker standards and must attend a site safety briefing held by the Site Safety
Officer prior to field activities.
SITE SAFETY
A site safety plan has been prepared for this sampling and analysis event. All individuals present
during this effort as team members, oversight personnel, or observers will be required to adhere to
the requirements of this plan. The Site Safety Officer will be the authority for the site safety plan's
implementation. Tbis authority is separate from the authority of the site manager, who has the
overall field sampling plan responsibility.
All State and outside contractor personnel involved in sampling activities must be 40 hour OSHA
trained.
PUBLIC AND MEDIA OBSERVATION
Members of the Working Group, the public, and media representatives are invited to observe the
field sampling activities provided they observe established safety requirements. All observers to
the site with the exception of the Science advisor or other properly trained staff must be
accompanied at all times while on the property.
The Site Safety Officer will establish a zone for each sampling activity where only properly
trained professionals will be allowed to enter. However, these areas are expected to be small and
will be temporary during actual preparation and sampling efforts. Safe zones will be established
where interested members of the Working Group or other citizens or their representatives will be
allowed to observe the field work.
Crucial elements of the sampling event will be video taped. This tape will be made available upon
request.
All observers present during the sampling program within the landfill area (beyond the locked
cross wire on the access road to the landfill) will be required to attend a site safety briefing, sign a
statement that they have received this instruction, and must obey the directions of the site safety
officer and their escort. Observers present during the sampling are required to be properly attired,
including long-sleeved shirts, long pants, and sturdy shoes (e.g. work boots, hiking boots, or
athletic shoes). Chemical protective overboots will be provided upon request. Any deviation from
required attire will be allowed solely at the discretion of the site safety officer.
ANALYTICAL REQUIREMENTS & QUALITY ASSURANCE
CHEMICAL TEST METHODS
The required analytical methods for the various samples are as shown in Tables 1 and 2. Triangle
Labs will perform the analyses for dioxin and furan samples. All other analyses will be performed
by the State Laboratory (Environmental Science Lab). The analytical methods to be used and their
corresponding MDLs are as follows.
CONSTITUENT
PCB
Volatile Organics
Semivolatile Organics
Pesticides and Herbicides
Dioxin'Furans
Metals
SW-846 METHOD
8081/8080
8240
8270
8081-8141
8290-1311
(Various)
MDL
Soil = 0.1 ppm/water = 0.1 ppb
see Table 3
see Table 3
see Table 3
S.0ppq
SAMPLE CONTAINERS
The required sample containers are as listed in Table 1. Triangle Labs personnel will provide all
containers for the Dioxin and Furan samples. The State Field Personnel will provide sample
containers for all remaining analyses.
BLANK SAMPLES
It is expected that this sampling campaign will cover two days. As a result, a "set" of "trip blank"
samples containing organic-free water will be prepared to accompany the sample containers for
each day of sampling. Triangle Labs will be given the "dioxin/furan" blanks and the State will
take the remainder for each day of sampling. Equipment rinseate blanks will be prepared as a
means to verify that proper decontamination procedures were followed. There should be one
rinseate blank per sampling media per day generated. Field decontamination between sampling is
not expected to be performed therefore equipment rinseate blanks should not be needed. These
blanks are as follows and are listed in Table 2.
NUMBER DESCRIPTION
34 TRIP 1 -Trip Blank for Day 1
35 TRIP 2 -Trip Blank for Day 2
36 SOIL 1 -Soil equipment rinseate sample Day 1 or 2
3 7 WATER 1 -Groundwater equipment rinseate sample Day 1
38 WATER 2 -Groundwater equipment rinseate sample Day 2
39 WATER 3 -Surface water equipment rinseate sample Day 1 or 2
PHYSICAL CUSTODY OF SAMPLES
Chain-of-custody shall be maintained for all samples taken from sample collection, transport and
analysis by all parties involved. Sample handling will be conducted as follows.
1 -All sample containers will be filled by DWM Field Staff.
2 -All filled sample containers for Dioxin/Furan analysis will be given to Triangle Lab personnel.
3 -Mr. Patrick Barnes of BF A, Inc. will receive the filled sample containers from Triangle Labs
and provide all sample labelling and/or coding.
4 -Triangle Lab personnel will take the Dioxin/Furan samples to their laboratory for analysis.
S -All other samples will be taken by the DWM Field Staff to the Environmental Science Lab
(State Lab) for analysis.
CHAIN OF CUSTODY DOCUMENTATION
The Division of Waste Management uses standard forms to document sample chain of custody.
Samples of these forms and are included at the end of this sampling plan.
Chain of custody record -this form accompanies all samples from the time they are
placed in the container and labeled through shipment to the laboratory and finally
accompany the data from the laboratory back to the requesting authority. This
"chain-of custody" record, where each subsequent handler of the sample or data
acknowledges custody and responsibility for the sample is a high-order quality
control procedure.
2. Sample analysis regyest -this form accompanies samples from the field to the
laboratory. It identifies individual samples uniquely by listing the unique sample
identification number from the sample label and directs the analytical laboratory to
perf onn the appropriate analysis on each sample. This function will be performed
by Mr. Patrick Barnes ofBFA, Inc. This form will be filled out in advance of the
sampling event and provided to Mr. Barnes.
3. Receipt of samples fonn -this form is used when the original sampling team
releases split, duplicate, or original samples to another person or group.
4. Filed sample labe11in~ as noted earlier will be conducted by Mr. Patrick Barnes of
BF A, Inc. After the samples have been labelled, this infonnation will be included
on the Sai:nple Analysis Request Form in# 2 above .
All methods and protocols used during the Warren County PCB Landfill environmental
characteriz.ation will be published protocols or standards, or modifications of such necessary for
the specific conditions of this effort and approved by the Science Advisors. All planned field
sampling activities and subsequent chemical analyses follow or are derived from:
U.S. Environmental Protection Agency, May 1996, Environmental Investigations Standard
Operating Procedures and Quality Assurance Manual (EISOPQAM).
N.C. Department of Environment, Health, and Natural Resources, Division of Waste Management,
1993, Sample Collection Guidance Document.
Occupational Safety and Health Administration Directorate of Technical Support. 1990.
Instruction CPL 2-2.20B CH-1, Chapter 1 Personal Sampling for Air Contaminants.
U.S . Environmental Protection Agency Office of Solid Waste. 1994. SW-846. Test Methods for
Evaluating Solid Waste Physical Chemical Methods.
Sampling and analysis methods not modelled after the above published methods are considered
survey or research methods and will be used in addition to, not in replacement of, published
methods, where applicable and approved by the science advisors.
All sampling and analysis of samples will be conducted under standard chain-of-custody methods
of the Division of Waste Management, which comply with all federal environmental regulatory
requirements.
LANDFILL CONTENT SAMPLES
PURPOSE;
To collect two sets of soil samples (wet and dry) within the landfill to determine chemical and
physical content and to provide data to support the detoxification activities of the landfill. Also, a
soil sample needs to be taken at a seep located outside the landfill fence on the west side.
FIELD SAMPLING METHOD
Both the landfill content (soil) samples and the seep sample will be acquired by hand auger or
other suitable manual methods. Three or more continuous soil column samples will be acquired.
These samples will be sleeved in PET plastic tubes. Soil samples from the seep area will use
Teflon liners. Sub-samples from these columns will be directed for chemical analysis. Additional
bulk landfill content samples will be acquired for bulk physical analyses.
FIELD SAMPLING LOCATION
All landfill content samples will be taken at or within the central air vent for the landfill and is
shown in Figure 1 as a triangle within the fenced area of the landfill. Table 2 identifies these
samples as Number 41 and 42, "LANDFILL SOILS".
The seep sample location is indicated in Figure 1 as the darkened triangle labelled as the
hydropunch sample. Table 2 identifies this sample as Number 40 "HYDRO PA".
SAMPLING PERSONNEL REQUIREMENTS
Air sampling and site preparation will occur one day before the major field sampling exercise. On
the main sampling day, two trained field staff will be required for sample preparation, record
keeping, and general field support activities.
FIELD EQUIPMENT REQUIRED
Field equipment will include an array of chemically-clean sample containers and sample collection
and preparation devices for handling soil samples. Sample containers, labels, and sample
preservation and storage(transhipment) containers will also be required. Sample container
requirements are as shown in Table 1. Equipment to decontaminate sampling devices and sample
containers will be required to prevent cross contamination of samples.
PERSONAL PROTECTIVE EQUIPMENT
Level D protective equipment for sampling personnel will be required. This includes long-sleeved
shirts, long-legged pants, safety shoes, impact protective eye ware, and disposable surgical gloves.
ANALITICAL METHODS
Both the landfill content samples and the seep samples are to be analyzed for the following
constituents as shown in Tables I and 2:
Landfill Contents
PCBs
Dioxin/Furan
SVOC (BN/AE)
voe
Metals
Other
particle size distribution
engineering classification
liquid limit
plasticity index
moisture content
organic matter
nutrients
QUALITY ASSURANCE
Seep sample
PCB
Dioxin/Furan
All Quality Assurance requirements for this phase of the sampling are as noted in the OVERVIEW
section.
LANDFILL LEACHATE SAMPLES
PURPOSE
To collect water samples at the leachate inlet and outlet at Warren County PCB Landfill to
determine chemical content.
FIELD SAMPLING METHOD
The method used in collecting samples of leachate from the landfill will follow those used in
previous leachate sampling efforts. Use of the sample sampling method will allow comparison of
previously acquired data to the new infonnation. Sufficient sample will be withdrawn from the
leachate collection system sampling port and from the inlet on the filter system to conduct the
required chemical analyses. In addition, a sample will be drawn from the outlet from the filter
system. A variety of sample sizes and containers is required. Samples for organic chemical
analysis may be filtered, and ,hQili the liquid fraction and the filter media will be submitted for
analysis. This would be necessary with samples with high particulate content to detennine the
actual location of any complex organic molecules, i.e., are they in the water itself or in the solids
suspended in the water.
FIELD SAMPLING LOCATION
The leachate collection system engineered into the design of the landfill includes an access or
sampling port located near the pump house on the north end of the fenced area. A diagram of the
sampling port is enclosed. One sample is to be taken from both the Leachate Inlet and Leachate
Outlet. The locations for these samples are shown in Figure 1 as squares on the north end of the
landfill. One sample location is inside the fenced in area, the other is outside the fenced in area.
These samples are numbered as 19 and 20 in Tables 1 and 2.
SAMPLING PERSONNEL REQUIREMENTS
Two teams of two hydrogeological sampling personnel will complete this task along with the
sampling of the monitoring wells during the main sampling day's efforts. Two representatives
from Triangle Labs will be present for the sampling as noted in the OVERVIEW section.
FIELD EQUIPMENT REQUIRED
Standard, portable field sampling equipment will be required. A variety of sample bottles (listed
in Table 1) will be available to be properly labeled for the required organic and inorganic analyses.
Portable decontamination equipment will also be employed to prevent any cross-contact with the
chemistry from one sample to another.
PERSONAL PROTECTIVE EQUIPMENT
Level D protective equipment for sampling personnel will be required. This includes long-sleeved
shirts, long-legged pants, safety shoes, impact protective eye ware, and disposable surgical gloves.
ANALYTICAL METHODS
The Landfill Leachate Samples are to be analyzed for the following constituents as shown in
Tables 1 and 2:
PCBs
Dioxin!Furan
SVOC (BN/AE)
voe
Metals
Other (Secondary drinking water parameters, i.e. BOD, COD, turbidity, pH, etc.)
QUALITY ASSURANCE
All Quality Assurance requirements for th.is phase of the sampling are as noted in the OVERVIEW
section.
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GROUNDWATER SAMPLING PLAN
PURPOSE
To collect and analyze samples from the groundwater monitoring wells and to determine the depth
(elevation) of groundwater in each well at the time of sampling.
FIELD SAMPLING METHODS
Standard field methods will be used to sample the groundwater monitoring wells. The basic
process is to measure the water level; purge the well; and obtain the sample.
All water levels and well depths are to be measured to the nearest 0.01 ft below the surveyed
measuring point (i.e. the top of the well casing). Prior to measuring the water levels, non-vented
or scalable well caps should be removed to allow the water level to equilibrate. The measuring
device will be decontaminated between each well per standard EPA protocol.
After measuring the wells, the wells are purged to remove stagnant water. Purging equipment
must not compromise sample integrity. When purging is completed to protocol specifications, the
samples should be taken within a 24 hour time span.
The samples taken from the wells should have a turbidity of 10 NTU or below. This can be
accomplished with a low-flow sampling techniques (i.e. a low flow peristaltic pump). Appendix E
of the "Environmental Investigations Standard Operating Procedures and Quality Assurance
Manual", (EISOPQAM) published by the U.S. EPA (May 1996) provides procedures on the use of
peristaltic pumps for groundwater sampling.
If the peristaltic pump cannot be used (i.e. due to depth to groundwater), a low flow sampling
system called a GRUMDFUS is acceptable. Conversations with EPA Region IV indicate that this
sampling system is acceptable provided that proper decontamination procedures are followed.
Since these decontamination protocols are not covered by the EISOPQAM, these will need to be
specifically developed for this sampling activity.
All samples to be analyzed for organic chemicals will be maintained at a temperature below 4
degrees C to maintain any organic chemicals in the sample. All groundwater sampling preserving
protocols will be per the standard EPA protocols outlined in the USEP A EISOPQAM (May 1996).
FIELD SAMPLING LOCATIONS
The monitoring wells to be sampled are located as shown in Figure 1 and are listed in Tables 1 and
2. The sample numbers indicated in Tables 1 and 2 are 1 to 18. Figure 1 shows the original
monitoring wells are designated as small circJes with a dot and the newer wells are designated as
hexagons.
Note that the background wells are not explicitly shown on Figure 1. These will be located 1-2
miles off site in the NW, SW, and SE quadrants.
SAMPLING PERSONNEL REQUIREMENTS
A minimum two person field team from DWM will take all samples from the monitoring wells.
Containers provided by Triangle Labs for the dioxin and furan samples will be filled by DWM
staff. Triangle Labs will provide a two person team for the sampling event.
FIELD EQUIPMENT REQUIRED
Groundwater sampling equipment must be constructed of materials and properly prepared so as to
not compromise the physical integrity of the sample. The use of low flow pumps for taking
samples must include provisions for thorough decontamination and/or replacement of necessary
pump internals to assure no cross contamination occurs between the wells.
PERSONAL PROTECTIVE EQUIPMENT
Level D protective equipment for sampling personnel will be required. This includes long-sleeved
shirts, long-legged pants, safety shoes, impact protective eye ware, and disposable surgical gloves.
ANALYTICAL METHODS
The Groundwater Samples are to be analyzed for the following constituents as shown in Tables 1
and 2:
PCBs
Dioxin!Furan
SVOC (BN/AE)
voe
Metals
Other (Secondary drinking water parameters, i.e. BOD, COD, turbidity, pH, etc.)
QUALITY ASSURANCE
All Quality Assurance requirements for this phase of the sampling are as noted in the OVERVIEW
section.
SURFACE WATER AND SEDIMENT SAMPLES
PURPOSE
To collect and analyze water and stream sediment samples to determine the presence of PCBs or
dioxins and furans.
FIELD SAMPLING METHOD
Standard field methods for collecting samples of flowing water and stream bottom sediments will
be used. Care must be taken to minimize disturbance of the stream, e.g., downstream samples
taken before upstream, water samples taken before stream bottom sediment samples, and all
sample collection equipment and containers carefully decontaminated by organic-free methods
before and after use. Subject to the amount of flow present in the stream at the time of sampling,
surface water samples are obtained by standing downstream of the water to be sampled, turning
the container sideways, partially submerging the container allowing water to fill the container with
minimal agitation. Floating debris must be prevented from entering the sampling container.
Stream substrate samples are collected by forcing a hollow tube into the sediment to a depth of up
to 8", followed by capping the tube before removing it from the sediment, then transferring this
collected material to the sample container that will be sent to the laboratory. This step is repeated
until adequate quantity of sample is acquired. In the event of a rocky or impenetrable substrate, a
glass sample container is used in place of the sample tube. In this case, substrate is collected by
secondary container and transferred.
FIELD SAMPLING LOCATIONS
The surface water and sediment sampling locations are located either along Richneck Creek, the
unnamed tributary, or in the draws that lead to the streams as shown on Figure 1. Tables 1 and 2
list 6 surface water samples and are numbered 21 through 26. The locations for the 6 surface
water samples are as shown on Figure I. The original surface water sampling locations are shown
on Figure I as circles with crosses and the additional surface water sampling locations are simply
shown as circles.
There are 4 sediment samples required and these are shown in Figure 1 as triangles near the
surface water sampling locations. These are numbered in Tables 1 and 2 as 27 through 30.
SAMPLING PERSONNEL REQUIREMENTS
Two individuals will be required to perform this sampling event. The two hydrogeological
sampling personnel will conduct this effort. Two representatives of Triangle Labs will be present
for this phase of the sampling as noted in the OVERVIEW section.
FIELD EQUIPMENT REQUIRED
Sample collection equipment, and portable decontamination equipment will be required. Sample
container requirements are noted in Table 1 ." ·
PERSONAL PROTECTIVE EQUIPMENT
Level D protective equipment for sampling personnel will be required. This includes long-sleeved
shirts, long-legged pants, safety shoes, impact protective eye ware, and disposable surgical gloves.
ANALYTICAL METHODS
The Surface Water and Sediment Samples are to be analyzed for the following constituents as
shown in Tables 1 and 2:
PCBs
Dioxins/Furan
QUALITY ASSURANCE
All Quality Assurance requirements for this phase of the sampling are as noted m·the OVERVIEW
section.
SEDIMENTATION BASIN SUBSTRATE SAMPLES
PURPOSE
To sample and analyze soils from the sedimentation basin.
FIELD SAMPLING METHOD
Standard soil field sampling method will be employed. Three soils samples will be taken by
appropriate field collection devices, then transferred to a properly prepared and labeled container
for laboratory analysis for PCBs, dioxins and furans. The soil samples need only be taken at a
depth of 3 to 5" due to the nature of PCBs in binding to the surface substrate. Low levels of PCBs
(near the detection limit) were found in these substrate materials in earlier sampling activities in
this same basin.
FIELD SAMPLING LOCATIONS
The sedimentation basin is located outside the main landfill fence to the
north of the landfill. It can be identified as a depression in the ground, that is completely
vegetated by grass and some taller weeds. The sedimentation basin has never routinely held any
liquid and was used only briefly during the first year following closure of the landfill. The
sampling locations are numbered 31 through 33 in Tables 1 and 2 and are located as follows:
Overflow Pipe Base
Center of Pond
Discharge Pipe Outlet
SAMPLING PERSONNEL REQUIREMENTS
Two sampling personnel will be required to perform this activity. However, the time required
should be one to two hours, thus, these individuals may be detailed from other activities. In
addition, two representatives of Triangle Labs will be present for this phase of the sampling as
noted in the OVERVIEW section.
FIELD EQUIPMENT REQUIRED
Routine organic chemical sampling equipment will be used in acquiring these samples. Sample
container requirements are as noted in Table 1.
PERSONAL PROTECTIVE EQUIPMENT
Level D protective equipment for sampling personnel will be required. lltls includes long-sleeved
shirts, long-legged pants, safety shoes, impact protective eye ware, and disposable surgical gloves.
ANALYTICAL METHODS
The Sedimentation Basin Substrate Samples are to be analyzed for the following constituents as
shown in Tables I and 2:
PCB
Dioxin/Furan
QUALITY ASSURANCE
All Quality Assurance requirements for this phase of the sampling are as noted in the OVERVIEW
section.
SAND AND CARBON FILTRATION BED SAMPLES
PURPOSE
To sample and analyze sand, carbon and sediment from the filtration portions of the on site
treatment facilities.
FIELD SAMPLING METHOD
Standard soil field sampling method will be employed. Two samples will be taken by appropriate
field collection devices, then transferred to a properly prepared and labeled container for
laboratory analysis for PCBs, dioxins and furans, and other constituents as noted in Tables 2 and 3.
The samples will be taken under the filtration fabric to a depth of 3-5 " due to the nature of PCBs
in binding to the surface substrate. Low levels of PCBs have been detected in the leachate water
pumped from the landfill during a couple of sampling events over the years since the landfill was
constructed.
FIELD SAMPLING LOCATIONS
The filtration beds are located at the northern end of the landfill near the leachate collection pipes.
The filtration beds are part of the leachate water treatment system and are contained in two
concrete "septic tanks". The first bed is of sand and the second is a carbon filtration bed. This
system has been used to filter water pumped out of the leachate collection system on a monthly
basis. One sample will be taken under the protective fabric cloth in each of the two beds.
SAMPLING PERSONNEL REQUIREMENTS
Two sampling personnel will be required to perform this activity. However, the time required
should be one to two hours, thus, these individuals may be detailed from other activities. In
addition, two representatives of Triangle Labs will be present for this phase of the sampling as
noted in the OVERVIEW section.
FIELD EQUIPMENT REQUIRED
Routine organic chemical sampling equipment will be used in acquiring these samples. Sample
container requirements are as noted in Table 1.
PERSONAL PROTECTIVE EQUIPMENT
Level d protective equipment for sampling personnel will be required. This includes long-sleeved
shirts, long-legged pants, safety shoes, impact protective eye ware, and disposable surgical gloves.
ANALYTICAL METHODS
The sand and carbon filtration samples, identified as samples #43 and #44 in Tables 2 & 3, are to
be analyud for the following constituents as ·shown in those tables:
PCB
Diox.in/furan
SVOC (BN/AE)
voe
Metals
QUALITY ASSURANCE
All Quality Assurance requirements for this phase of the sampling are as noted in the OVERVIEW
section.
5A
..
·LANDFILL SAMPLE MAP
FIGURE 1
I
I
I -
I
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,
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~ Cl) u ' u _.g .s ;; ~ ~ .;; -8 ·15 .>! ,,
tll " CJ
SAMPLING AND ANALYSIS PLAN
TABLE 1
I .
I
· I
I
SAMPLE LOCATION I MW-ta-NEW EAST 2 MW-I b-NEW EAST 3 MW 2-EXISTING NW PCB LANDFILL SAMPLING AND ANALYSIS PLAN SAMPLE NUMBER SAMPLE TYPE ANALYSES GROUNDWATER PCB DIOXIN BN/AE voe METALS O11--IER GROUNDWATER PCB DIOXIN BN/AE voe METALS O11--IER GROUNDWATER PCB DIOXIN BN/AE voe METALS O11-IER CONTAINERS & NUMBER 2 liter amber I Triangle Labs I 2-liter amber I 40-ml septum cap 2 I liter plastic I 2 liter amber I Triangle Labs I 2-liter amber I 40-ml septum cap 2 t liter plastic t 2 liter amber l Triangle Labs l 2-liter amber t 40-ml septum cap 2 t liter plastic t
·, Page 2, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 4 MW 3-EXISTING GROUNDWATER PCB 2 liter amber 1 WEST DIOXIN Triangle Labs 1 BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS I liter plastic I OTHER 5 MW-3a NEW WEST GROUNDWATER PCB 2 liter amber 1 DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic 1 OTHER 6 MW-4 EXISTING GROUNDWATER PCB 2 liter amber 1 SW DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic 1 OTHER 7 MW-4a NEW SW GROUNDWATER PCB 2 liter amber I DIOXIN Triangle Labs 1 BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic I OTHER
~ Page 3, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 8MW-SNEWN GROUNDWATER PCB 2 liter amber t DIOXIN Triangle Labs t BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTHER 9MW-SaNEWN GROUNDWATER PCB 2. liter amber t DIOXIN Triangle Labs t BN/AE 2-liter amber 1 voe 40-ml septum cap . 2 METALS 1 liter plastic l OTHER 10 MW-6 NEW SE GROUNDWATER PCB 2 liter amber 1 DRAW DIOXIN Triangle Labs 1 BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTHER 11 MW-7NEW GROUNDWATER PCB 2 liter amber 1 SOUTII DIOXIN Triangle Labs 1 BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTHER
'1'!' Page 4, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 12MW-7aNEW GROUNDWATER PCB 2 liter amber I sourn DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic I OTIJER 13 MW-8NEWNE GROUNDWATER PCB 2 liter amber I DRAW DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTIJER 14 MW-9NEWN. GROUNDWATER PCB 2 liter amber 1 DRAW DIOXIN Triangle Labs I BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS 1 liter plastic I OTIJER 15 MW-t0NEWN GROUNDWATER PCB 2 liter amber I DRAW DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septmn cap 2 METALS 1 liter plastic 1 OTIJER
Page S, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 16 BACKGROUND GROUNDWATER, PCB 2 liter amber I WELL I BACKGROUND DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic I O11-IER l7BACKGROUND GROUNDWATER, PCB 2 liter amber I WELL2 BACKGROUND DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic I O11-IER 18 BACKGROUND GROUNDWATER, PCB 2 liter amber I WELL3 BACKGROUND DIOXIN Triangle Labs I BN/AE 2-liter amber I voe 40-ml septum cap 2 METALS I liter plastic 1 O11-IER 19LEACHATE LANDFILL LEA CHA TE PCB 2 liter amber 1 INLET DIOXIN Triangle Labs 1 BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS t liter plastic I O11-IER
Page 6, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 20LEACHATE LANDFILL LEACHATE PCB 2 liter amber 1 OUTI..ET DIOXIN Triangle Labs 1 BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS 1 liter plastic 1 O11-IER 21 SW-I SOUTI-1 UT SURF ACE WATER PCB 2 titer amber 1 NEW UNAMED TRIBUTARY DIOXIN Triangle Labs 1 O11-IER 22 SW-2 SOUTI-1 SURF ACE WATER PCB 2 titer amber 1 WESTUTNEW UNAMED TRIBUTARY DIOXIN Triangle Labs I O11-IER 23 urns EXISTING SURF ACE WATER PCB 2 liter amber 1 UNAMEDTRIBUTARY DIOXIN Triangle Labs 1 O11-IER
'·' Page 7, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 24 RCUS EXISTING SURF ACE WATER PCB 2 liter amber I (BELOW BRIDGE) RJCHNECK CREEK DIOXIN Triangle Labs I OTIIER 25 RCDS EXISTING SURF ACE WATER PCB 2 liter amber I RJCHNECK CREEK DIOXIN Triangle Labs I OTIIER 26RCUSNEW SURF ACE WATER PCB 2 liter amber 1 (ABOVE BRIDGE) RICHNECK CREEK DIOXIN Triangle Labs I OTIIER 27 USSS-ABOVE SEDIMENT PCB 12S ml solid cap 1 BRIDGE ON ROAD DIOXIN Triangle Labs OTIIER
'•,, Page 8, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 28BBBELOW SEDIMENT PCB 125 ml solid cap 1 BRIDGE ON RC DIOXIN Triangle Labs 1 O11-tER 29 SS-1 SE ORA W SEDIMENT PCB 125 ml solid cap 1 ONUT DIOXIN Triangle Labs 1 O11-tER 30 SSND NORA W SEDIMENT PCB 125 ml solid cap 1 ONRC DIOXIN Triangle Labs 1 OTI-IER 31 PS-I OVERFLOW POND SOIL PCB 125 ml solid cap l PIPE BASE DIOXIN Triangle Labs l • OTI-IER
Page 9, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 32 PS-2 CENTER OF POND SOIL PCB 2 liter amber l POND DIOXIN Triangle Labs 1 OTHER 33 PS-3 DISCHARGE POND SOIL PCB 2 liter amber 1 PIPE OUTLET DIOXIN Triangle Labs 1 OTHER 34 TRIP I BLANK PCB 2 liter amber l BLANK DIOXIN Triangle Labs 1 BN/AE 2-liter amber t voe 40-ml septum cap 2 METALS t liter plastic l OTHER 35TRIP2 BLANK PCB 2 liter amber t BLANK DIOXIN Triangle Labs I BN/AE 2-titer amber t voe 40-ml septum cap 2 METALS I liter plastic t OTHER
Page 10, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 36 SOIL l SOIL BLANK PCB 125 ml solid cap l DIOXIN Triangle Labs l OTIIER 37WATER l WATER BLANK PCB 2 liter amber l DIOXIN Triangle Labs l OTIIER 38WATER2 WATER BLANK PCB 2 liter amber l DIOXIN Triangle Labs l OTIIER 39WATER3 WATER BLANK PCB 2 liter amber l DIOXIN Triangle Labs l OTIIER
Page 11, PCB LANDFILL SAMPLING & ANALYSIS PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 40HYDROPA SOIL FROM SEEPING PCB 2 liter amber I AREA ON OUTSIDE OF DIOXIN Triangle Labs 1 LANDFILL OTHER 41 LANDFILL SOILS SOIL AND SEDIMENT PCB 125 ml solid cap 1 SAMPLES FROM VENT DIOXIN Triangle Labs 1 PIPE IN LANDFILL: BN/AE 2-liter amber 1 DRY SAMPLE voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTHER 42 LANDFILL SOILS SOIL AND SEDIMENT PCB 125 ml solid cap 1 SAMPLES FROM VENT DIOXIN Triangle Labs 1 PIPE IN LANDFILL: BN/AE 2-liter amber 1 WET SAMPLE voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTHER 43 SANDFIL TER SOIUSAND/SEDIMENT DIOXIN 12S ml solid cap 1 FROM THE SAND BN/AE Triangle Labs 1 FILTER BED voe 2-liter amber 1 METALS 40-ml septum cap 2 OTHER 1 liter plastic 1
Page 12, PCB LANDFILL SAMPLING & PLAN SAMPLE SAMPLE NUMBER SAMPLE TYPE ANALYSES CONTAINER& LOCATION NUMBER 44 CARBON FILTER CARBON/SEDIMENT PCB 125 ml solid cap 1 FROM CARBON FILTER DIOXIN Triangle Labs 1 BED BN/AE 2-liter amber 1 voe 40-ml septum cap 2 METALS 1 liter plastic 1 OTHER
SAMPLING LOCATION AND ANALYSIS PLAN
TABLE2
DRAFT SAMPLING LOCATION/ANALYSIS PCB LANDFILL
ANALYSIS
SAMPLE ID
LOCATION
GROUNDWATER
I MW-la-NEW EAST
2 MW-lb-NEW EAST
3 MW 2-EXISTING NW
4 MW 3-EXISTING WEST
5 MW-3a NEW WEST
6 MW-4 EXISTING SW
7 MW-4a NEW SW
8MW-5NEWN
9MW-5aNEWN
10MW-6NEW S.EDRAW
11 MW-7 NEW SOUTH
12 MW-7a NEW SOUTH
13 MW-8 NEW N. E. DRAW
14 MW-9NEWN. DRAW
15 MW-l0NEWW. DRAW
16 BACKGROUND WELL J
17 BACKGROUND WELL 2
18 BACKGROUND WELL 3
PCB
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
DIOXIN/ BN/AE voe METALS
FURAN
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
✓ ✓ ✓ ✓
Background wells located 1-2 miles off-site in NW, SW and SE quadrants. Attached is list of constituents and
detection leve]sfor each analytical test. Wells m2-6,8,9 and 10 may require a nest ifhydrogeological
conditioning warrants.
Total Samples/ Analysis
40 total; PCB 40; Dioxin/Furans 40; BN/AE 23; VOC 23; METALS 23 x7= 161 (As, Ba, Cd, Cr, Pb, Hg, Se)
DRAFT SAMPLING AND ANALYSIS PCB LANDFILL
SAMPLE IP
LOCATION
LEACHEATE
PCB
19 LEACHEA TE INLET
20 LEACHEA TE OUTLET
SAMPLE IP
LOCATION
SURFACE WATER
21 SW-1 SOUTH UT NEW
22 SW-2 SOUTH WEST UT NEW
23 UTUS EXISTING
2-4 RCUS EXISTING (Below Bridge)
25 RCDS EXISTING
26 RCUS NEW (Above Bridge)
SAMPLE IP
LOCATION
SEDIMENT
27 USSS-ABOVE BRIDGE ON RD
28 BB BELOW BRIDGE ON RC
29 SS-1 SE DRAW ON UT
30 SSND N DRAW ON RC
SAMPLE IP
LOCATION
POND SOIL
31 PS-1 OVERFLOW PIPE BASE
32 PS-2 CENTER OF POND
✓
✓
33 PS-3 DISCHARGE PIPE OUTLET
DIOXIN/ BN/AE
FURAN
✓
✓
PCB
✓
✓
✓
✓
✓
✓
PCB
✓
✓
✓
✓
PCB
✓
✓
✓
✓
✓
DIOXIN/
FURAN
✓
✓
✓
✓
✓
✓
DIOXIN/
FURAN
✓
✓
✓
✓
DIOXIN/
FURAN
✓
✓
✓
.
voe METALS
✓ ✓
✓ ✓
SAMPLE IP
LOCATION
BLANKS
34 TRIP 1
35TRIP2
36 SOIL 1
37WATER 1
38WATER-2
39WATER-3
40 HYDRO PA
41 LANDFILL SOILS
SAMPLE IP
LOCATION
SOIL SAMPLE
40HYOROPA
41 LANDFILL SOILS (WET)
42 LANDFILL SOILS (ORY)
SAMPLE IP
LOCATION
FILTER BEDS
43 SANO FILTER
44 CARBON FILTER
DRAFT SAMPLING AND ANALYSIS PCB LANDFILL
PCB
✓
✓
✓
✓
✓
✓
✓
✓
PCB
✓
✓
✓
✓
✓
DIOXIN/
FURAN
✓
✓
✓
✓
✓
✓
✓
✓
DIOXIN/
FURAN
✓
✓
✓
✓
✓
BN/AE voe
✓ ✓
✓ ✓
✓ ✓
BN/AE voe
✓ ✓
✓ ✓
✓ ✓
✓ ✓
METALS OTHER
✓
✓
✓ ✓
METALS OTHER
✓ ✓
✓ ✓
✓ ✓
✓ ✓
Other for landfill soils include particle size distribution engineering classification, liquid limit, plasticity Index, moisture
content, organic matter, nutrients
STATE LABORATORY CHEMICAL ANALYSIS SHEETS
TABLE3
I . ---· .
I
II
, BASE/NEUTRAL AND ACID
EXTRACT ABLES
CD1POOND
;
-nitrosodimethvlamine
. is (2~h loroethvllether
.. ..rh 1 orl'll')heno 1
henol
3-dichlorobenzene
,.4-dichlorobenzene
2-dichlorobenzene
is(2~hloroisooroovllether
. exachloroethane
lf~itroso-di-n-rl"ll'lvlamine
trobenzene
ttt>horone
'.r-fl it ropheno 1
.~4-dimethvlohenol
1s(2~hloroethoxvlmethane
, 4-d i ch 1 orooheno 1
2 4-trichlorobenzene
, aohtha 1 ene
r. ~xachlorobutadiene
i -ch 1 oro -ffl~reso 1
1 ~xachlorocvcl~ntadiene
4 6-trichloroohenol
~hloronaohthalene
, "'enanhthvlene
1• 5methvl 0htha late
,~6-dinitrotoluene
cenaohthene
~4-dinitroohenol
4-dinitrotoluene
.. nitroohenol
r uorene
ikhloroohenvl0henylether
,riethvl Dhthalate
J1.6-dinit~resol
iohenvlanh~
~obenzene
henvl0henvlether
~xachlorobenzene
entachloroohenol
,t,enanthrene
l!'lthracene
(ibutvl Dhthalate
r1uoranthene
-Estimated value.
STATE LABORATORY OF MLJC HEAL TH
P.O. BOX 28047 -306 N. WIIJUNGTOH, ST., RALEIGH, N.C. 27611
LAB NO
FIELD #
TYPE
UNITS
'~ /. :r.:, J"j
I
i~/J/ .... t,
✓O/~~eJ
,r,,/, f/A-:J',
/()/.., ~::u,
"' "5"""0) lu<fj
1/t"J/~~
.
l"il,1 1/,,...l:;n
110/~~D
. ' ,
mJ>L-
H:a.O/.SOIL
MGAN!C OfE1'1ICAL ANALYSIS
( ) ( ) ( ) ( )
:
-Actual value is known to be less than value given.
( )
-Actual value Is lcnown to be greater than value given.
~
-flaterial .-as analyzed for but not detected. The nUli>er is the "ininun Detection Limit. (7r71>L..)
-Not analyzed. . -----Tentative identification.
-On NROC List of Priority Pollutants.
( )
I ...
.
STATE LABORATORY OF PUBLIC HEAL TH
I P.O. BOX 28047 -306 N. WlL"lNCTON. ST •• RALEIGH, N.C. 27611
ORCNIIC OENICAL ANALYSIS
rE/NEUTRAL AHO ACID LAB NO
EXTRACTABLES FIELD I
~o TYPE ( ) ( ) ( ) ( ) ( ) ( )
UNITS
,•rrene Ir./:/?/">
~~hzidine 5{j//LC/'I
,~'tvl benzvl 0hthalate /t:J/':t~
J~z(alanthracene
:hrvsene ~ I
1 .~-dichlorobenzidine .~) ,,,.~
, S(2-ethvlhexyll0hthalate JrJ)':f:IJ)
I -n-«tvl ohthalate JO/?~/">
~ nzo(b)fluoranthene rn /J, <'l"I
• nzo(klfluoranthene
• inZo(a)oYl"ene
(jeno (1 2 3-cdlovrene
I ~nzo(a.h)anthracene I
-enzo(a h i )~rvlene ' I
I iJine i::r/v .e::n
, nzoic acid
,enzvl alcohol
1 chloroaniline ' I
I t>enzofuran lril?=?ll
· IN"thvlnanhthalene
' ITl'!thyli:,henol
ITl'!thvl0henol
,iitroaniline 'v"1 '/J ~-
nitroani line
. i,,; troani line I
~ 5-tridlloroohenol ' I
I
'l'n~'-
-Estimated value. t-\-:L-0/.SOU •
. -Actual value is known to be less than value given.
l-Actu.al value is known to be greater than value given.
-Material was analyzed for but not detect~. The nLll't>er
-Not analyzed.
, -Tent.ative identification.
is the !,ininun ~tection .!:_imit. (MllL-)
( -On NROC List of Priority Pollutants.
,..
STATE LABORATOR!' OF POBLlC BEALTB
PO BO% 28047 • 306 K. WILIIINGTON ST., JlAIZIGB. lfC 27611
ORGANIC CHEHTCAL ANALYSIS
.
JIVHGEABlZ COJIPOVM>S I.All NO
I FIELD NO
) I COJIPOtllVD TYPE ( ) ( ) ( ) ( ) ( ( ) I ~~~ ffJb ppm ppb ppm. I C b PPb ppm ppb ppm ppb pprn tJpb ,:P"1
I c:m.oaoMZTIWB :J.O
I
f/) ~c:m.oamz
I ac)IIOllftBAJIZ ~{.)
I cm.oaoZ'nlAlft JO
TaJCID.OaGn.l:IOllOIIETBAn JO Ii
I, ACZTOIIZ .;io
1.1-1>1cm.oaorrain 5 I IODOIIIIZ'TIIAlff I
I I I
IIETJff1Zn CIU.OIUDZ
CAJIBO" l)JSl1LnI>Z I
fltAlfa. l.2·1>1CB1.0JtOETBZ:orll: J,
ACxn.DlffT1Ul.ll: ~
I 1.l•l>ICBLOROZTILVIZ 5
S-St7f AIIOIIZ :l.D
Cla-l.2•l>ICHLOllOrn!IZ.'fZ 5
Clll.OltOl'OIUI I I i I l.1. l•TaJCBLOltOETHA."111:
I I c:Aa90K Trr'aACBLOJm>Z
UIIZZIIZ I
I l,2•1>1CBLOJt0ffBA!n I
TaJCZ.OROrnlll'Z I
1,2·1>1CBLOltOPJtOPA!n I
II llllOlllODICBl.Oao~ Ji ..
I
I
I
C• pc,:,o,.,r,~ ..AA c.:.~,,.,~1f'IF\r,cN CR 8Ac~!r£c .. rJC. ;, -l■tiaate4 -.&111• .
~ -Actual -.&111• i■ bow= to II• 1••• than -1,ae ViYeD. L • Actual Yalu• i ■ JtnowD to II• vraat■r tbai:i Tal,ae giT■D.
V • Mat■rial •a• &D&lyse4 for 11\lt Dot 4atecte4, ft• Dl&llber i• tb• Mizi.iaua DetectioD Lia.it. I JD.• •ot &D&lysed. I 1/ • TeDtatiYe ideDtification.
I 1 -c:t1,-\fo\ilJSP Rw ~eL)' OETfC"iR6&.f. D'4!.¥ '"' 1ue~ cnlc.£N~cNS.
I V -SAMPL.£ HI '1-IL)' DILLlTE.0, ~DL.•~ 00 ~ Ptft>1.y.
DEBNR S065-0 (10/Sl3) PtJRGCOK.O RG
l
I.
I I
.PVR~ BIi: Q:>JDIODM)S
CO.IIPOOND
STATE LABORATORY OF POBLIC BEALTB
PO BO% 28047. 8061'. WIUIINGTON ST .. RAIEIGB. !fC 27611
ORGANIC cm:mcu. ANALYSlS
LAB NO
FIELI>l'lO
TTP£ ( ) ( ) ( ) ( ) ( )
n,~~~ ppb ppm ppb ppm ,,pb pp,ti ppt FPtn ~t, (Jf>rn.
DIDOMmmTIIAR 5
.aanrn.-S-nJrTAl'OR ,o
c:za.1.Ntcm.oa0PIIOPPS .5
TOUJUE
TL\Jfl-l>DJCSL0aon.0PZIIZ
1.1.2.2•T'ZTUCIILOllOfflWfE
1.1,,-n1aa.oaorT11An ' V
s-~on JO
ftTltACm.OltOE'T'Dln 5
lltBltOMOCB1.01tOKrt11A!n
rnrn.zn DIJlltOam>E
aa.o1tOUNnn
1,1.l.2•'TZT1UCll1.0ltO1r:T11AlfE
ffBTl.all:ftZZ!n
XT1Z2'D I
8TT1IUE J;
aaoworoltM ;o
~ 1.4-DICm.c>ltO-,-atrnn 'lo
1,2,,-fflc:m.oaoPaOPAXE ..5
1,4-DICB1.01tOHN%El'fZ I
1.2-111c:m.oao•~ ~I
1.2•DIJllt0MO-S-CJa.OltOPROP.UZ ,;,. t)
Ymn.ACZTAff ;J.CJO
-C -i'r:--~"'>,r,'-C £-AS Cc.~M1>.l,~T\C.N eiP.. f.l?i(.s;.C.-t<(UNJ), J • Satiaated Talue
~ • Actual Tal\le i• bown to b• 1••• than -la• •:l•ec.
L -Actual •alue i• bown to be greater than -lue •:l-n.
V • •aterial wa• analyzed for but Dot detected. 'l"h• D'lmber i• tll• M!Dimm DetectioD Liait. n • Jlot analyzed.
1/ • Tentati•e identification. It -COMPoi.i.tJr, R.EL1~s1..y pt;Tfc.T~6LE. O,H.V iN ,..,,-,; '" ICCN7J;:AT la>J:~. ✓ .. :s;-ir-1Pi-f ril'.,·HLY l>iLL;1£0. ~i)c.~ i>c ~-, P.f'i'L}o/.
!>EHNJl 3068-0 (10/93)
.
( )
ppb ppm
PURGCOH.ORG
I -
N. ··c. DEPARTMENT 0F ENVIRONMENT, t£AL TH, & NATI.W.L RESMCES
DIVISIOH 0F LABORATORY SERVICES, ENVIRONMENTM. SCIENCES SECTIOH P.O. BOX 28047 -306 N. WILMINGTOH ST, RALEIGH, N.C. 27611
uboratory No. ______ _ MGEABLE CXIMPCl.WDS Date of Analysis ____ _
CDIPQJIO 119/l a>MPOONO
Dichlorodifluoranethane v'Ch 1 oroben zene
Chloranethane v'Ethvlbenzene
.'Vinvl Chloride 1.1.1.2-Tetraehloroethane
8rcm:methane v'o-Xvlene
Chloroethane v'm-Xvlene
Trichlorofluoranethane v'o-Xvlene
v'l.1-0ichloroethvlene v'Stvrene
Methyl~ Chloride Brcm>fonn
tert-8utvl Nethvl Ether 1-----lbenzene
v'trans-1 2-0ichloroethvlene 1 1 2.2-Tetrachloroethane
I 1 tther 8rambenzene
1.1-0ichloroethane n-Proovlbenzene
2.2-0ichlo ·ne 1.2 3-Trichlo ne
v'cis-1 2-0ichloroethvlene 2-Ch 1 oroto 1 uene
Chlorofonn 1.3 S-Trinethvlbenzene
(BOO 8""1)Ch loranethane 4-Chlorotoluene
v'l. 1 1-Trichloroethane tert-8utv1 Benzene
1 1-0ichlo ne Pentachloroethane
-1Carbon Tetrachloride 1.2.4-Trinethvlbenzene
~nzene sec:-8utvl Benzene
-11.2-0ichloroethane o-I ltoluene
n rich 1 oroet hv 1 ene 1.3-0ichlol"Obenzene
-11.2-0ichlo -·ne v'l.4-0iehlol"Obenzene
Bromodichloranethane n-8utv1benzene
DibrO'IOll!thane v'l.2-0ichlorobenzene
v'Toluene Bis (2-Chloroisool"ODvll Ether
1. 1.2-Trichloroethane 1 2-0 i braoo-3-Ch 1 o----· ne
v'Tetrachloroethvlene 1 2 4-Triehlol"Obenzene
1.3-0ichlo ·ne Hexachlorobutadiene
Dibr'O!Dchloranethane Nanhthalene
1.2-Dibrcm,ethane CEDBl 1.2.3-Trichlol"Obenzene
1-Ch lorohexane
CDl£NTS:
flDL -flinl11111 Detection Limit for water (EPA Method 502.2), Is 1.0 119/l.
J -Estimated value.
IC -Actu.1 value is known to be less than value 9ivtn. l -Actual value Is known to be grNter than value 9iven. U -Material was analyzed for but not detKted.
NA -Not analyzed. 1/ -Ttntative identification.
-1 -Regulated voe T -Tr1halaiethane
N.C. Dept. of Enviromient, Health, & Natural Rtsources DEHNR 3068~ (Rev. 10/92 Laboratory Services)
11S32E 0-18
119/1
SITE HEALTH AND SAFETY PLAN
SITE HEALTH AND SAFETY PLAN
A. General Information
-Site Name Warren County PCB Landfill o & M
location lust off SR l 6Q4 Warren County NC
Proposed Date of Investigation
Date of Briefing
Date of Debriefing
Health Department Official Contacted
Date of Contact
ID t NCD 980 6P2 ]63
Site Investigation Team: All site personnel have read the Site Health and Safety Plan
and are familiar with its provisions.
Personnel Responsibilities 5i1nature
Plin Preparation:
Prepared By: ____________ _
Reviewed By: --------------
8. SITE /WASTE CHARACTERISTICS
Waste Type(s) __Lliquid __LSolid _Sludge _Gas
Characteristics _Corrosive _Ignitable _Radioactive
Volatile X Toxic Reactive Other -- --
List Known or Suspected Hulrds (physical, chemical biological or radioactive)
on Site and their toxicological effects. Also, if known, list chemical amounts
HAZARD WARNING PROPERTIES TLV
Odpr Threshold con -DA data
(mild hydrocarbon odor>
0 5mg/m1
Facility Description: Size: Total -J 42 aqes
Landfill • 2.54 acres
Buildings : mme
Unusual Features on Site (dike integrity, power lines, terrain, etc.):
History of the Site:
none known
Between June, 1978 and August, 1978, over 30,000 gallons of industrial liquid waste material identified as
PCBs (Arochlor 1260 and Arochlor 1262) were discharged deliberately along the shoulders of approzximatley
150 miles of NC highways. In June, 1979, EPA approved a tract of land (previously used for agriculture) in
Warren County as the disposal site for the PCB<ontaminated roadside soil. The landfill (constructed in 1983-
1984 and permined under the Toxic Substances Control Act -TSCA) contains about 40,000 cubic yards of soil
contaminated with PCBs. The concentration of PCBs in the landfill ranges from 46 to 200 ppm, averaging
about 135 ppm.
C. HAZARD EVALUATION
Ibe site can be toured io level P protection,
Steekoed safety shoes and chemical protection overboots shall be worn by all staff involved in sampling
activities. lnvididuals touring or observing the site shall wear substantial laceup shoes with chemical protective
overboots. Long sleeve pants and shirts are required.
D. WORK PLAN INSTRUCTION
Map or Sketch Attachedl W
Perimeter ldentif tedl W
Command Post Identified? ng
Zones of Contamination ldentifiedl w
Personal Protettive Equipment/Level of Protection: ___ c x_o .
Modifations: lbe site an be toured and sampled in level P protection Steel-toed work boots wm be wpm
while sampJina PE or PVC slaves wm be wom while colleaina water or soil samples Jhe HNU ac OVA wm
be used to monitor breathina zone a;r while soil au1erin1 and samplins of sails Ivvek suits wm be wpm wbile
1u1erin1 tt is recommended that no obsecveD be allowed within 10 meters of the samplin1 sites Level P
P«:rsonnel protective equjpment iocludio1 chemical protective boots wifl be required of all obsecveD
Observers are 10 be ibCornpaoied at all times by a person properly trained by 29 CFR l 9]0 l 20 to ◄Cthr
Jtandards
Surveillance Equipment:
____ HNU
____ OVA
____ Combustable Gas Meter
Decontamination Procedures
----Detector Tubes and Pumps
02 Meter ----
Radiation Monitor ----
___ level C Respirator wash, respirator removal, suit wash (if needed),
suit removal, boot wash, boot removal and glove removal.
_X_level D Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modi fiat ions ---------------------------
EMERGENCY PRECAUTIONS
Route o{ £xPA$vce fiat Aid
f= . . . . . . . . . . . . . . . . . . . . . . irri1ate immedi;neh,
Skin • • • • • • • • • • • • • • • • • • • • • • 19ap and water wash
Inhalation • • • • . • • • • • • • • • • • • • fresh air and artificial mairation
ln1e:sti0O • • • . . . . . . . . . . . . . . . 1et rnecfical 1nenti0n immediately
Location of Nearest Phone: vokoowo
Nurest Hospital (Address and Phone Number)
Marja Parham Hospital Ruic Creek Road at 1:85 Heodersoo NC 2ZS36
c;;ao handle cbemically contaminated patients
Emergency Transportation Systems (Phone Numbers)
Fire ID
EMS ID
Rescue Squad ID
Emergency Route to Hospital Travel west 00 SR 1604 tbeo tum left onto SR 112 5 lust past Coke5bury
tum cieht 0010 SR 1510 then left onto SR 1001 Stay on SR 1001 votil just outside of Heodersao theo turn
cieht onto SR l 508 which will lead you to l:BS, Take l:BS South to the Ruic Creek Road exit the hospital is
weli marked
I EQUIPMENT CHECKLIST
_ Air purifying respirator
,_Cartridges for respirator
l_OustMask •.
X OJ lndiator 1:x Eye Wash Unit
_X_HNU
X First Aid Kit =X_3 gal. Distilled H20
Rainsuit -X Cloves {PE/PVC/nitrite/cloth)
J_Boo~oot Covers
X OVA ,--' X Combustable Gas Meter
,--Radiation Monitor 1-1_Detector Tubes and Pump
J_ Coveralls (tyvek/saranex)
_X_ Eye Protection
_X_Hard Hat
X Decontamination
--Materials.
•.
Chemical Emergency Information Centers
I ASHEVILLE
I 704-25S,+190
I
'CHARLOTTE
704-379-5827
jOURHAM
, 1-800-672-1697
I GREENSBORO I , 919-37~105
Poj5on Control Ct:oiec • State Cogrdjnator
Duke University Medical Center
Telephone: [phone]
P.O. Box 3024
Durham, NC 27710
Weste!" NC Poison
Control Center
Memorial Mission Hosp.
509 Biltmore Ave. 28801
Mercy Hospital
2001 Vail Ave, 28207
Duke Univ. Med. Center
Box 3007, 27710
Moses Cone Hospital
1200 N. Elm St. 27420
HENDERSONVILLE
704-693-6522
Ext. 555,556
HICKORY
704-322~&49
JACKSONVILLE
919-577-2555
WILMINGTON
919-343-7046
Margaret R. Pardee
Memorial Hospital
Fleming SL, 28739
Catawba Mem. Hosp.
Fairgrove Chur. Rd 28601
Onslow Mem. Hospital
Western Blvd. 28540
New Hanover Mem. Hospital
2131 S. 17th St. 28401
•
PROJECT MANAGERS PROJECT ACTIVITY REPORT
PROJECT MANAGER: _____ _ PROJECT: __________ _
INVESTIGATION DATE: ____ _
Materials Used (Pieue insert• number in the blank)
Air Purifying respirator cartridges
-Detector tubes
-Eye Wash Units
-First Aid Kit
-Cloves (polyethylene) I= ClovesCPVO
I Respirator Worn By
_ Cloves (nitrite)
_ Cloves (cloth)
Boot covers :::=: Coveralls (tyvek)
_ Coveralls (saranex)
_ Auger Brushes
Approximate Time in Respirator
Air Monitoring Data (Include Calibration Reading)
1
HNU: ________________________ _
10VA: -------------------------
Combustable Gas Meter:
I -------------------
Radiation Meter: I -------------------
! tf the maximum peoonal protective equipment as outlined in the Hazard
Evaluation Section was not used, please justify:
1---------------------------
Visitors Present Organization Represented
DLJSR/Revised 10/J / '1 <&