26076_1601 South Boulevard Brownsfield Assessment Final Report 20230911

BROWNFIELDS ASSESSMENT REPORT & RECEPTOR SURVEY
1601 SOUTH BOULEVARD SITE
1601 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT ID. 26076-22-060
ECS PROJECT NO. 49:15946-E
PREPARED FOR
SOUTH END 1, LLC
September 11, 2023
1

September 11, 2023

Ms. Bill Schmithorst
NCDEQ, DWM, NC Brownfields Program
217 West Jones Street
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Reference: Brownfields Assessment Report & Receptor Survey
1601 South Boulevard Site (Formerly McCorkles Cleaners Site)
1601 South Boulevard
Charlotte, Mecklenburg County, North Carolina
Brownfields Project ID: 26076-22-060
ECS Project No. 49:15946-D
Dear Mr. Schmithorst:
ECS Southeast, LLP (ECS) has prepared this Brownfields Assessment Report & Receptor Survey detailing
the activities and results of the soil and sub-slab soil gas sampling that was conducted at the subject
site and to identify potential receptors in the site area. These activities were conducted, and this report
was prepared in general accordance with the approved Brownfields Assessment Work Plan (ECS Project
No. 49:15946-D) dated June 23, 2023, and approved by the Brownfields Redevelopment Section on June
28, 2023. This report was developed at the request of the North Carolina Department of Environmental
Quality (NCDEQ) – Brownfields Redevelopment Section.

ECS appreciates the opportunity to provide our environmental consulting services to you on this project.
If you have any questions concerning this report or this project, please contact us.

Sincerely,

ECS SOUTHEAST, LLP

Scott Young, P.G. Roger A. Smith, P.G.
Senior Environmental Project Manager Senior Principal Geologist
704-525-5152 704-525-5152
[e-mail] [e-mail]

NC Corporate Geology License #C-553
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

TABLE OF CONTENTS

1.0 PROJECT INFORMATION ................................................................................................................... 2
2.0 PREVIOUS INVESTIGATIONS .............................................................................................................. 4
3.0 OBJECTIVE OF THE ASSESSMENT ...................................................................................................... 4
4.0 FIELD ACTIVITIES ............................................................................................................................... 5
4.1 Utility Locate ..................................................................................................................................... 5
4.2 Sub-Slab Soil Gas Sample .................................................................................................................. 5
4.3 Soil Samples ....................................................................................................................................... 6
5.0 RESULTS............................................................................................................................................. 7
5.1 Sub-Slab Soil Gas Soil Analysis ........................................................................................................... 7
5.2 Soil Sample Analysis .......................................................................................................................... 8
5.3 NCDEQ Risk Calculator Results .......................................................................................................... 8
5.4 Brownfields Receptor Survey ............................................................................................................ 8
5.5 Investigative Derived Waste ............................................................................................................. 9
6.0 CONCLUSIONS AND DISCUSSION ...................................................................................................... 9

FIGURES
Figure 1 USGS Topographic Map Figure 2 Previous Sample Location Map Figure 3 Current Sample Location Map Figure 4 Soil Samples Exceedances Map Figure 5 Groundwater/Soil Gas Exceedances Map

TABLES
Table 1 Summary of Sub-Slab Soil Gas Samples Analytical Results Table 2 Summary of Soil Samples Analytical Results

APPENDICIES
Appendix A Field Sampling Notes Appendix B Laboratory Analytical Reports and Chains-of-Custody Forms Appendix C Boring Logs Appendix D NCDEQ Risk Calculator Output Appendix E Brownfields Receptor Survey Form and Figures
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

1.0 PROJECT INFORMATION

The subject property (Figure 1) is identified by Mecklenburg County GIS as Parcel Identification Numbers
(PINs) 12307312 (1601 South Boulevard), 12307313 (1605 South Boulevard), 12307314 (1609 South
Boulevard), and 12307308 (1612 Cleveland Avenue), and are owned by South End I, LLC, and PIN
12307315 (1617 South Boulevard) owned by Maria P. Kyritsis and Joana P. Pandrinopoulos. The combined
area of the five site parcels totals 0.846 acres. Currently, the site is planned for redevelopment as office,
above-ground parking, commercial/retail and multi-family residential (tower) with associated
recreational and amenity areas, including green space/dog park and EV charging stations.

The approximate 0.611-acre portion of the subject property located at 1601 to 1609 South Boulevard and
1612 Cleveland Avenue consists of one building and paved parking areas. The approximate 3,726-square
foot single-story building was constructed in 1940, is located at 1601 South Boulevard, and previously
consisted of two restaurants, Sandwich Max and Beijing Chinese. This portion of the assessment site
received eligibility from the Brownfields Redevelopment Section (BRS) on December 16, 2022, and was
initially assigned the name McCorkles Cleaners and Brownfields Project No. 26076-22-060, now known as
the 1601 South Boulevard Brownfields Site.

ECS previously conducted a Phase I Environmental Site Assessment (Phase I ESA) for this portion of the
subject site (ECS Project No. 49:15946 dated January 14, 2022). During this Phase I ESA, the following
recognized environmental conditions (RECs) were identified:

• ECS considered the potential for the former onsite drycleaners (in approximately 1944) to impact
the subject property to be a REC for the subject property.
• Based on the distance from the subject property and documented groundwater contamination,
ECS considered the potential for the offsite CC Dickson facility to impact the subject property to
be a REC.
• Based on the documented groundwater contamination above the North Carolina Department of
Environmental Quality (NCDEQ) Standards and distance from the subject property, ECS
considered the facility at 1620 South Boulevard to be a REC for the subject property.
• Based on the groundwater and soil gas detections above the applicable levels and distance to the
subject property, ECS considered the potential for the Dilworth Auto Service facility to impact the
subject property to be a REC.
• ECS considered the potential for the former adjacent gas stations and auto repair facility to the
north, northwest, and west to impact the subject property to be a REC.
• ECS considered the potential for the former adjoining/adjacent drycleaners to the northeast and
northwest to impact the subject property to be a REC.
• Based on proximity, length of operation, and potential for an undocumented release to migrate
and impact the subject property, ECS considered the Brakes 4 Less auto repair facility to represent
a REC for the subject property.

The approximate 0.235-acre subject property located at 1617 South Boulevard is developed with a 405-
square foot vacant office building that was reportedly originally constructed in 1939. A metal awning is
attached to the rear of the building. The southeastern half of the subject property is currently leased to
Graystar for parking and a construction trailer. On March 8, 2023, South End I, LLC submitted an amended
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

Brownfields Application to add this parcel to the initial McCorkles Cleaners Brownfields Project. ECS
previously conducted a Phase I ESA for this portion of the subject site (ECS Project No. 49:18794-A dated
February 3, 2023) also. During this Phase I ESA, the following RECs were identified:

• ECS considered the potential for a former adjacent drycleaner approximately 50 feet northeast
(in approximately 1944) to impact the subject property to be a REC for the subject property.
• ECS considered the potential for former adjacent gas stations and an auto repair facility to the
north, northwest, and west to impact the subject property to be a REC.
• ECS considered the potential for the former adjoining/adjacent drycleaners to the northeast and
northwest to impact the subject property to be a REC.

In an effort to determine if the subject property has been adversely affected by the identified RECs, ECS
was requested to conduct an Environmental Assessment at the site. The results of these assessment
activities were summarized in ECS’s Environmental Assessment Services Report, dated April 18, 2023 (ECS
Project Nos.: 49:15946-B and 49:15946-C).

As part of the assessment activities, ECS collected two exterior soil gas samples, nine soil samples, and
four groundwater samples. The previous sample locations are shown on Figure 2. Review of the
laboratory analytical results for the exterior soil gas samples indicated 1,3-butadiene in the SG-1 and SG-
2 samples and tetrachloroethene (also known as perchloroethene or PCE) and trichloroethene (TCE) in
the SG-2 sample at concentrations greater than their respective NCDEQ Residential Vapor Intrusion
Screening Levels (VISLs).

Methylene chloride in each of the soil samples collected; PCE in soil samples SB-7, SB-8, and SB-9; and
benzo(a)pyrene in soil samples SB-1 and SB-8 were detected at concentrations greater than their
respective Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs). The concentrations of
benzo(a)pyrene detected in soil samples SB-1 and SB-8 were also greater than its Residential PSRG.
Arsenic in soil samples SB-1 and SB-4, lead in soil sample SB-1, and mercury in soil sample SB-5 were
detected at concentrations greater than their respective Protection of Groundwater PSRGs. In addition,
arsenic in each of the soil samples collected; hexavalent chromium in soil samples SB-1, SB-2, SB-8, and
SB-9; lead in soil samples SB-1 and SB-4; and mercury in soil sample SB-5 were detected at concentrations
greater than their respective Residential PSRGs.

PCE in the TW-1, TW-3, and TW-4 groundwater samples; TCE in the TW-1 groundwater sample; and total
and dissolved total chromium in the TW-2 groundwater sample were detected at concentrations greater
than their respective North Carolina 2L Groundwater Quality Standards (NC2LGWQS). The concentrations
of PCE and TCE detected in the TW-1 groundwater sample were greater than their respective Residential
Groundwater VISL.

Based upon the results of the SG-1 and SG-2 exterior soil gas samples and the TW-1 groundwater sample,
ECS input the detected concentrations for each sample into the NCDEQ Risk Calculator to evaluate the
risk of volatile organic compounds (VOCs) in vapor migrating into indoor air through vapor intrusion. The
results of the NCDEQ Risk Calculator indicated the concentrations detected in the SG-1 exterior soil gas
sample did not exceed the Hazard Index for the Residential risk classification; however, the concentrations
detected in the SG-2 exterior soil gas sample did exceed the Hazard Index for the Residential Risk
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

Classification. The results of the NCDEQ Risk Calculator indicated the concentrations detected in the TW-
1 groundwater sample did exceed the Hazard Index for the Residential risk classification.

Based upon the results of a Kick-Off Meeting on May 24, 2023, with South End 1, LLC, their environmental
attorney, ECS and the NCDEQ Brownfields Project Manager, ECS prepared a Brownfields Assessment Work
Plan (Work Plan) to address the data gaps identified by the North Carolina Brownfield Redevelopment
Section (BRS). ECS submitted the Work Plan (ECS Project No. 49:15946-D) on June 27, 2023, which was
subsequently approved by the BRS on June 28, 2023.

2.0 PREVIOUS INVESTIGATIONS

As discussed above, ECS has previously conducted multiple environmental assessments at the site.
Previous assessment activities conducted on the various parcels include the following:

• Phase I ESA dated January 14, 2022 (ECS Project No. 49:15946). The assessment activities are
described above in Section 1.0.
• Phase I ESA dated February 13, 2023 (ECS Project No. 49:18794-A). The assessment activities are
described above in Section 1.0.
• Environmental Assessment Services Report dated April 18, 2023 (ECS Project Nos. 49:15946-B &
49:15946-C). The assessment activities are described above in Section 1.0.

3.0 OBJECTIVE OF THE ASSESSMENT

The objective of this Brownfields assessment was to conduct the following sampling activities:

• The advancement of seven soil borings to varying depths and collection of up to 17 soil samples,
plus one duplicate, for laboratory analysis.
• The collection of three sub-slab soil gas samples, plus one duplicate, for laboratory analysis.
• Completion of a Brownfields Receptor Survey.

The soil samples collected were submitted for various laboratory analysis depending on the area in which
they were collected including VOCs by EPA Method 8260, Semi-Volatile Organic Compounds (SVOCs) by
EPA Method 8270, RCRA Metals by EPA Method 6020/7471, and hexavalent chromium by EPA Method
7199.

The sub-slab soil gas samples collected were submitted for laboratory analysis of VOCs by EPA Method
TO-15.

The sampling activities were conducted in general accordance with the Work Plan prepared by ECS dated
June 27, 2023, and approved by the BRS on June 28, 2023. This assessment was also conducted in general
accordance with the NCDEQ Division of Waste Management’s (NCDWM) Inactive Hazardous Site
Program’s Guidelines for Assessment and Cleanup (Revised September 2022), and Science and Ecosystem
Support Division (SESD) guidelines.

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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

4.0 FIELD ACTIVITIES

4.1 Utility Locate

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities. In addition, ECS contracted with KCI
Associates of NC to further evaluate the boring areas of private utilities.

4.2 Sub-Slab Soil Gas Sample

Number and Sample Location

In accordance with the approved Work Plan, ECS collected three sub-slab soil gas sample (SS-1, SS-2, and
SS-3) at the approximate locations shown on Figure 3.

Sample Collection

On August 1, 2023, ECS installed a VaporPin® using a hammer drill to penetrate through the concrete slab
at each sample location. Once the concrete slab was penetrated, a new VaporPin® with a new silicon
sleeve was inserted in the concrete slab in general conformance with manufacturer’s recommendations
(Vapor Pin Enterprises, Inc.). The VaporPin® setup was allowed to equilibrate for at least 20 minutes prior
to leak testing. The vapor point was connected to a batch certified 1-liter Summa canister, which was
used to collect the sample. The Summa canister was fitted with a five-minute flow regulator.

Prior to collecting the sub-slab soil gas sample, helium gas was used as a quality assurance/quality control
(QA/QC) measure to confirm the integrity of the probe seal at the sample location. A shroud that enclosed
the fittings, sample train, and Summa canister was placed over the newly installed vapor point and filled
with helium. The sample tubing and tracer gas tubing was placed through the shroud wall via rubber
grommets. During the purging stage, the cylinder was flooded with helium via the hose placed through
the shroud wall. A Model MGD-2002 Multi-Gas Leak detector was connected to the probe tube and the
air stream being purged was measured for helium. A helium concentration of less than ten percent helium
detected within the shroud was considered acceptable. During leak check activities, helium
concentrations remained above 10 percent in air by volume in the shroud and below 10 percent of the
concentration of helium inside of the shroud in the sample train. In addition to the leak check, a shut-in
test was conducted to assess for leaks in the fittings and regulator. Copies of the field sampling notes are
included in Appendix A.

Following purging, ECS checked and noted the vacuum on the Summa Canister before initiating the
sampling procedure. The sampling procedure was terminated when the vacuum reading was
approximately five inches of mercury.

Sample Analysis

Following sample collection, the Summa canisters were repackaged and delivered to Pace Analytical
Services, LLC. Chain-of-custody (COC) protocol was utilized throughout the collection and transport of the
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

samples. The sub-slab soil gas samples collected were submitted for laboratory analysis of VOCs by EPA
Method TO-15. A copy of the COC is included in Appendix B.

For QA/QC purposes, one duplicate sub-slab soil gas sample (SS-DUP) was collected from the same
location as SS-1 and analyzed for the same compounds as the record sample.

4.3 Soil Samples

Number and Sample Location

In general accordance with the Work Plan, on August 4, 2023, ECS requested the certified driller advance
soil borings via direct push technology (DPT) drill rig at seven locations as discussed below:

• Soil borings E-1 and E-2 were advanced in the area of the proposed deeper elevator shafts to
approximate depths of 15 feet below ground surface (ft bgs).
• Soil borings P-1 and P-2 were advanced in the areas of the proposed building footprint where
deeper foundations are expected that will require excavation of the soils to approximate depths
of 15 ft bgs.
• Soil boring P-3 was advanced in an area that previously was not sampled to an approximate depth
of 15 ft bgs.
• Soil borings DP-1 and DP-2 were advanced in the area planned to be developed as a dog park to
approximate depths of five ft bgs.

The soil boring locations are shown on Figure 3. Boring logs for each soil boring are included in Appendix
C.

Sample Collection

ECS provided a project professional to collect soils continuously from the ground surface to the
termination depth of the soil borings. The soils were collected over the length of the boring in
approximately 5-foot intervals and screened in the field by placing a portion of the soil into a resealable
plastic bag and measuring for volatile organic vapors using a photoionization detector (PID) after allowing
to set for approximately 15 minutes. As described in the approved Work Plan, the remaining soils from
each interval were placed into a separate resealable container and set aside in a cooler with ice for
potential sampling purposes. The soil samples to be submitted to the laboratory for analysis were
collected from the separate soils that were stored on ice rather than those which were allowed to
volatilize for the collection of the PID readings.

Soil samples were collected from the zero to five ft bgs interval in soil borings DP-1 and DP-2, and from
the five to 10 ft bgs and 10 to 15 ft bgs intervals in soil borings E-1, E-2, P-1, P-2, and P-3. Copies of the
field sampling notes are included in Appendix A.

Sample Analysis

Following sample collection from the resealable containers into laboratory-supplied sample containers,
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

the sample containers were placed on ice in a cooler, maintained under COC protocol and delivered to
Pace. For samples that were not delivered to Pace at the end of the sample day, the ice within the sample
cooler was checked at a minimum of once daily and replaced, if necessary, until the samples were
delivered to Pace. Additionally, according to the COC and sample receiving form attached to the
laboratory report from Pace, the sample coolers arrived at the lab with ice intact and the measured
temperatures of all coolers arrived below 6° C, which is within the EPA sample temperature range (i.e.,
between 0° C to 6° C). The soil samples collected were submitted for laboratory analysis of VOCs by EPA
Method 8260, SVOCs by EPA Method 8270, RCRA Metals by EPA Methods 6020 and 7471, and hexavalent
chromium by EPA Method 7199.

Additionally, concentrations detected greater than the laboratory method detection limit but less than
the laboratory reporting limit were reported by the laboratory and flagged with a J-flag qualifier, indicating
the reported concentrations were estimated. It is ECS’ opinion that based on the constituents and
concentrations that were detected, the lack of these constituent concentrations reported to their
respective Standards is not anticipated to substantially change the risk considering the land use
restrictions and vapor mitigation that are planned for the site redevelopment. Additionally, most of the
site will be covered by buildings or paved surfaces, and final grade soil sampling will be conducted to
confirm any exposed, surficial soils meet residential PSRGs. A copy of the COC is included in Appendix B.

For QA/QC purposes, duplicate soil sample SB-DUP was collected as a duplicate of the record soil sample
P-2 from the 10 to 15 ft bgs interval. The duplicate soil sample was analyzed for the same compounds as
the record sample.

5.0 RESULTS

5.1 Sub-Slab Soil Gas Soil Analysis

Review of the laboratory analytical results for the sub-slab soil gas sample indicated chloroform in sub-
slab soil gas sample SS-2; PCE in sub-slab soil gas samples SS-1, SS-DUP, SS-2; and TCE in sub-slab soil gas
sample SS-2 at concentrations greater than their respective Residential VISLs.

Additional compounds were detected in the SS-1, SS-DUP, SS-2, and SS-3 sub-slab soil gas samples
collected at concentrations greater than the laboratory method reporting limits, but less than their
respective Residential VISLs.

A summary of the sub-slab soil gas sample analytical results is included as Table 1 and the laboratory report
is included as Appendix B.

Quality Control

A duplicate sub-slab soil gas sample SS-DUP was collected as a duplicate of sub-slab soil gas sample SS-1
and analyzed for VOCs using EPA Method TO-15. The results of the duplicate sample were similar to those
detected in SS-1. A Level II QA/QC package was performed by the laboratory.

The results are summarized in Table 1 and the laboratory report is included as Appendix B.

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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

5.2 Soil Sample Analysis

Review of the laboratory analytical results indicated the following compounds were detected at
concentrations greater than their respective Residential PSRGs:

• Benzo(a)anthracene – in soil sample P-3 (5-10 ft bgs)
• Benzo(a)pyrene – in soil samples E-1 (5-10 ft bgs, E-2 (5-10 ft bgs), and P-3 (5-10 ft bgs)
• Benzo(b)fluoranthene – in soil samples E-1 (5-10 ft bgs) and P-3 (5-10 ft bgs)
• Dibenz(a,h)anthracene – in soil samples E-1 (5-10 ft bgs) and P-3 (5-10 ft bgs)
• Indeno(1,2,3-cd)pyrene – in soil sample P-3 (5-10 ft bgs)
• Naphthalene – in soil sample P-3 (5-10 ft bgs)
• Arsenic – in soil samples E-1 (5-10 ft bgs), E-2 (5-10 and 10-15 ft bgs), P-1 (5-10 ft bgs), P-2 (5-10
and 10-15 ft bgs), SB-DUP (5-10 ft bgs), P-3 (5-10 and 10-15 ft bgs), DP-1 (0-5 ft bgs), and DP-2 (0-
5 ft bgs)
• Hexavalent Chromium – in soil samples E-2 (10-15 ft bgs), P-1 (5-10 ft bgs), P-2 (5-10 and 10-15 ft
bgs), SB-DUP (5-10 ft bgs), P-3 (5-10 and 10-15 ft bgs), and DP-2 (0-5 ft bgs)

A total of 12 constituents of concern were detected at concentrations greater than their respective
Protection of Groundwater PSRGs in the various soil samples collected. Additional constituents of concern
were detected in each of the soil samples collected at concentrations greater than the laboratory method
detection limits, but less than their respective PSRGs.

A summary of the soil sample analytical results is included as Table 2 and the laboratory reports are
included as Appendix B.

Quality Control

Laboratory results of duplicate soil sample SB-DUP, that was collected as a duplicate of soil sample P-2 (10-
15 ft bgs), were similar to those detected in the record sample. A Level II QA/QC package was performed
by the laboratory.

The results are summarized in Table 2 and the laboratory report are included as Appendix B.

5.3 NCDEQ Risk Calculator Results

In light of the sub-slab soil gas sample results, ECS input the highest concentration of each compound
detected in each of the sub-slab soil gas samples in to the NCDEQ Risk Calculator. Based on the results of
the NCDEQ Risk Calculator, the concentrations detected in the sub-slab soil gas samples exceeded the
Hazard Index for the Resident Risk Classification. Output from the results of the NCDEQ Risk Calculator is
presented in Appendix D.

5.4 Brownfields Receptor Survey

ECS performed a Brownfields Receptor Survey. The results of the Brownfields Receptor Survey did not
identify any water supply wells within approximately 1,000 feet of the subject site and the site is provided
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Brownfields Assessment Report & Receptor Survey 1601 South Boulevard Site
Brownfields Project Number 26076-22-060
ECS Project No. 49:15946-E
September 11, 2023

water and sewer from a municipal (Charlotte Water) source. The nearest surface water body to the
subject site is an unnamed tributary to Irwin Creek located approximately 1,600 feet to the northwest of
the subject site. Underground utilities were noted in the vicinity of the site at the locations identified on
the figure included in Appendix E. Also, the Brownfields Receptor Survey form is included in Appendix E.
5.5 Investigative Derived Waste

In accordance with the approved Work Plan, Investigative Derived Waste (IDW) generated from the soil
borings (i.e., soil cuttings) were thinly spread onsite in the vicinity of the boring location.

6.0 CONCLUSIONS AND DISCUSSION

Based on the results of the sampling presented above, as well as the receptor survey conducted for the
site, ECS has the following overall conclusions:

• Chloroform in sub-slab soil gas sample SS-2; PCE in sub-slab soil gas samples SS-1, SS-DUP, SS-2;
and TCE in sub-slab soil gas sample SS-2 were detected at concentrations greater than their
respective Residential VISLs. Additional compounds were detected in each of the sub-slab soil gas
samples collected at concentrations greater than the laboratory method detection limits, but less
than their respective Residential VISLs.
• Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, dibenz(a,h,)anthracene,
indeno(1,2,3-cd)pyrene, naphthalene, arsenic, and hexavalent chromium were detected in
various soil samples collected at concentrations greater than their respective Residential PSRGs.
Based on the concentrations detected, it is possible that the arsenic and hexavalent chromium
concentrations identified may be naturally occurring concentrations in site soils and not an
indication of a release or impacts. Additional constituents of concern were detected in several
soil samples collected at concentrations greater than their respective Protection of Groundwater
PSRGs.
• The results of the NCDEQ Risk Calculator for the sub-slab soil gas samples indicated the
concentrations detected exceeded the Hazard Index risk threshold for Residential usage.
• Based on the results of the Brownfields Receptor Survey, no water supply wells are located within
1,000 feet of the subject site and the site is provided water and sewer from Charlotte Water. An
unnamed tributary to Irwin Creek is located approximately 1,600 feet northwest of the subject
site.

Based upon the results from this Brownfields Assessment Report and the prior assessment activities
conducted at the property, potential vapor intrusion concerns can be managed with appropriate vapor
mitigation. Additionally, management of impacted soils and groundwater (as well as vapors and other
potential unknowns) that may be encountered during construction activities will be addressed in a
Brownfields approved Environmental Management Plan (EMP). Figure 4 depicts the compound
concentrations detected greater than their respective Residential PSRGs in the soil samples collected
during various site assessments conducted by ECS. Figure 5 depicts the compound concentrations
detected greater than their respective NC2LGWQS in the groundwater samples collected, as well as
exterior soil gas and sub-slab soil gas sample concentrations that were greater than their respective
Residential VISLs during the various site assessments conducted by ECS.
FIGURES
FIGURE 1USGS TOPOGRAPHIC MAP
1601 SOUTH BOUELVARD PROPERTY1601 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:15946-E
SOURCE:
USGS 7.5’ TOPOGRAPHIC MAP
CHARLOTTE EAST, NC 2022
SCALE:
AS SHOWN
SITE
FIGURE 2PREVIOUS SAMPLE LOCATIONS MAP
1601 SOUTH BOUELVARD PROPERTY1601 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:15946-E
SOURCE:
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED JUNE 20, 2023
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE PREVIOUS SOIL SAMPLE LOCATION
APPROXIMATE PREVIOUS GROUNDWATER SAMPLE LOCATION
SB-6/SG-2
SB-3/SG-1
TW-4
TW-3
TW-1
TW-2
SB-7
SB-4
SB-8
SB-2
SB-1
SB-5
SB-9
APPROXIMATE PREVIOUS EXTERIOR SOIL GAS SAMPLE LOCATION
FIGURE 3CURRENT SAMPLE LOCATIONS MAP
1601 SOUTH BOUELVARD PROPERTY1601 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:15946-E
SOURCE:
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED JUNE 20, 2023
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE SOIL SAMPLE LOCATION
APPROXIMATE SUB-SLAB SOIL GAS SAMPLE LOCATION
APPROXIMATE PROPOSED
BUILDING FOOTPRINT
SS-1/SS-DUP
SS-2
SS-3
P-1
P-2/SB-DUP
E-1
E-2
P-3
DP-1
DP-2
FIGURE 4
SOIL SAMPLES EXCEEDANCES MAP
1601 SOUTH BOUELVARD PROPERTY
1601 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:15946-D
SOURCE:
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED JUNE 20, 2023
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE PROPOSED SOIL SAMPLE LOCATION
APPROXIMATE PROPOSED
BUILDING FOOTPRINT
P-1
P-2/SB-DUP
E-1
E-2P-3
DP-1
DP-2
SB-6
SB-3
SB-7
SB-4
SB-8
SB-2
SB-1
SB-5
SB-9
FORMER DRYCLEANERS
(134 East Park Ave., 212
East Park Ave., 1527
South Blvd.
Sample Depth 2 – 5 ft bgsBenzo(a)pyrene – 0.16 mg/kg
Arsenic – 9.63 mg/kgHexavalent Chromium – 0.60 J mg/kgLead – 412 mg/kg
Sample Depth 1.5 – 5 ft bgsArsenic – 8.60 mg/kg
Sample Depth 1 – 5 ft bgsArsenic – 2.65 mg/kgMercury – 5.64 mg/kg
Sample Depth 1.5 – 5 ft bgs
Benzo(a)pyrene – 0.27 mg/kgArsenic 1.10 J mg/kgHexavalent Chromium – 0.764 J mg/kg
Sample Depth 5 – 10 ft bgs
Benzo(a)pyrene – 1.7 mg/kgBenzo(b)fluoranthene – 2.4 mg/kgDibenz(a,h)anthracene – 0.31 J mg/kg
Arsenic – 3.87 mg/kg
Sample Depth 5 – 10 ft bgsBenzo(a)pyrene – 0.17 J mg/kgArsenic – 2.22 mg/kg
Sample Depth 10 – 15 ft bgsArsenic – 2.05 mg/kg
Hexavalent Chromium – 2.09 mg/kg
Sample Depth 1.5 – 5 ft bgsArsenic – 4.32 mg/kg
Sample Depth 1.5 – 5 ft bgs
Arsenic – 4.73 mg/kg
Sample Depth 1 -5 ft bgsArsenic – 2.51 mg/kg
Sample Depth 4 – 6 ft bgsArsenic – 1.64 mg/kg
Sample Depth 1.5 – 5 ft bgs
Arsenic – 0.816 J mg/kgHexavalent Chromium – 1.95 mg/kg
Sample Depth 5 – 10 ft bgsArsenic – 0.905 J mg/kg
Hexavalent Chromium – 0.587 J mg/kg
Sample Depth 5 – 10 ft bgs (SB-DUP)Arsenic – 3.96 mg/kgHexavalent Chromium – 2.21 mg/kg
Sample Depth 10 – 15 ft bgsArsenic – 3.23 mg/kgHexavalent Chromium – 1.90 mg/kg
Sample Depth 5 – 10 ft bgsBenzo(a)anthracene – 5.5 mg/kg
Benzo(a)pyrene – 5.7 mg/kgBenzo(b)fluoranthene – 6.9 mg/kgDibenz(a,h)anthracene – 0.97 mg/kgIndeno(1,2,3-cd)pyrene – 3.3 mg/kgNapthalene – 2.2 mg/kg
Arsenic – 2.48 mg/kgHexavalent Chromium – 1.09 J mg/kgSample Depth 10 – 15 ft bgsArsenic – 0.747 J mg/kgHexavalent Chromium – 0.418 J
Sample Depth 0 – 5 ft bgsArsenic – 9.07 mg/kg
Sample Depth 0 – 5 ft bgsArsenic – 3.20 mg/kg
Hexavalent Chromium – 2.66 mg/kg
NOTE: ONLY COMPOUNDS DETECTED GREATER THAN RESIDENTIAL PSRGS ARE SHOWN.
FIGURE 5
GROUNDWATER/SOIL GAS SAMPLES
EXCEEDANCES MAP
1601 SOUTH BOUELVARD PROPERTY
1601 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:15946-D
SOURCE:
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED JUNE 20, 2023
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE GROUNDWATER SAMPLE LOCATION
APPROXIMATE SUB-SLAB SOIL GAS SAMPLE LOCATION
APPROXIMATE PROPOSED
BUILDING FOOTPRINT
SS-3
SG-2
SG-1
TW-4
TW-3
TW-1
TW-2
APPROXIMATE EXTERIOR SOIL GAS SAMPLE LOCATION
FORMER DRYCLEANERS
(134 East Park Ave., 212
East Park Ave., 1527
South Blvd.
Tetrachloroethene – 34.6 µg/LTrichloroethene – 14.5 µg/L
Total Chromium – 17.6 µg/L
Tetrachloroethene – 1.3 µg/L
Tetrachloroethene – 1.2 µg/L
1,3-Butadiene – 34.3 µg/m3
1,3-Butadiene – 7.4 µg/m3
Tetrachloroethene – 60,800 µg/m3
Trichloroethene – 734 µg/m3
Tetrachloroethene – 740 µg/m3
Chloroform – 8.47 µg/m3
Tetrachloroethene – 64,100 µg/m3
Trichloroethene – 235 µg/m3
None above Residential VISL
NOTE: ONLY COMPOUNDS DETECTED GREATER THAN NC2LGQS OR RESIDENTIAL VISLS ARE SHOWN.
SS-2
SS-1/SS-DUP
TABLES
Table 1
Summary of Sub-Slab Soil Gas Samples Analytical Results
1601 South Boulevard Site
1601-1617 South Boulevard & 1612 Cleveland Avenue
Charlotte, Mecklenburg County, North Carolina
ECS Project Nos.: 49:15946-E
Sample ID SS-1 SS-DUP*SS-2 SS-3
Initial Laboratory Vacuum Reading (in Hg)-30 -30 -30 -30
Initial Sample Vacuum Reading (in Hg)-29 -26 -30 -28
Final Sample Vacuum Reading (in Hg)-5 -5 -5 -5
Sample Date 08/01/23 08/01/23 08/01/23 08/01/23
Acetone 51.3 40.4 36.6 2,470 NE
Benzene 0.738 0.648 4.44 5.81 12
2-Butanone (MEK)7.22 5.54 7.34 175 35,000
Carbon Disulfide 3.67 3.42 1.23 1.20 4,900
Chloroform 1.92 <0.349 8.47 <0.349 4.1
Chloromethane 1.11 1.23 0.925 0.636 630
Cyclohexane 5.75 1.36 <0.259 3.40 42,000
Dichlorodifluoromethane (Freon 12)5.64 <0.678 3.96 1.72 700
Ethanol 26.0 26.8 27.5 402 NE
Ethylbenzene 0.767 J 0.715 J 1.67 30.1 37
4-Ethyltoluene <0.384 0.488 J 0.425 J 2.13 NE
Heptane 0.622 J <0.425 2.28 2.87 2,800
Hexane 1.08 J <0.726 3.60 3.18 4,900
2-Hexanone (MBK)2.35 J <0.544 <0.544 38.5 210
Methylene Chloride 1.29 <0.340 <0.340 <0.340 3,400
4-Methyl-2-pentanone (MIBK)1.41 J <0.313 0.807 J 29.4 21,000
Methyl tert butyl ether <0.233 <0.233 <0.233 3.05 360
2-Propanol (Isopropanol)6.93 7.13 4.84 204 1,400
Propylene <0.160 <0.160 <0.160 10.8 21,000
Styrene 1.13 0.476 J 2.04 26.2 700
Tetrachloroethene 740 616 64,100 141 280
Toluene 3.19 <0.328 5.05 38.8 35,000
1,1,1-Trichloroethane <0.400 <0.400 1.16 <0.400 35,000
Trichloroethene 1.37 0.873 J 235 2.03 14
Trichlorofluoromethane (Freon 11)1.49 1.33 1.99 1.85 NE
1,1,2-Trichlorotrifluoroethane 0.730 J <0.608 1.43 J <0.608 35,000
1,2,4-Trimethylbenzene 1.14 <0.375 2.29 8.39 420
1,3,5-Trimethylbenzene <0.382 <0.382 0.746 J 4.54 420
2,2,4-Trimethylpentane <0.621 <0.621 0.710 J 24.2 NE
Total Xylenes 3.41 1.86 J 5.25 38.6 700
Notes:
Results presented in micrograms per cubic meter (µg/m3)
in Hg = inches of mercury
Residential VISL = NCDEQ-DWM Residential Exterior Vapor Intrusion Screening Level (July 2023)
* = SS-DUP sample is a duplicate sample of the SS-1 record sample.
NE = No Standard Established
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Residential VISL
Residential
VISL Volatile Organic Compounds by EPA TO-15
Table 2
Summary of Soil Samples Analytical Results
South Boulevard Properties
1601-1617 South Boulevard & 1612 Cleveland Avenue
Charlotte, Mecklenburg County, North Carolina
ECS Project Nos.: 49:15946-E
SB-DUP*DP-1 DP-2
08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23 08/04/23
5 - 10 10 - 15 5 - 10 10 - 15 5 - 10 10 - 15 5 - 10 10 - 15 5 - 10 5 - 10 10 - 15 0 - 5 0 - 5
Acetone 0.093 J <0.051 <0.049 <0.067 <0.056 <0.048 <0.062 <0.070 <0.072 <0.039 <0.045 <0.047 <0.056 25 14,000
Benzene 0.0079 <0.0032 <0.0030 <0.0042 <0.0035 <0.0030 <0.0038 <0.0043 <0.0045 <0.0024 <0.0028 <0.0029 <0.0035 0.01 1.2
2-Butanone (MEK)0.046 J <0.038 <0.036 <0.050 <0.042 <0.036 <0.046 <0.052 <0.054 <0.029 <0.034 <0.035 <0.042 17 5,500
Chloromethane <0.0066 <0.0067 <0.0064 <0.0088 <0.0074 <0.0063 <0.0081 <0.0092 0.032 <0.0051 <0.0059 <0.0062 <0.0073 0.015 23
Methylene Chloride <0.022 0.024 J <0.021 <0.029 <0.024 <0.021 <0.026 <0.030 <0.031 <0.017 <0.019 <0.020 <0.024 0.025 58
Naphthalene 0.26 0.0070 J <0.0040 <0.0055 <0.0046 <0.0040 <0.0051 <0.0057 <0.0059 0.0066 <0.0037 <0.0039 <0.0046 0.39 2.1
Tetrachloroethene 0.12 <0.0025 0.043 0.021 <0.0028 <0.0024 <0.0031 <0.0034 <0.0036 0.042 <0.0022 <0.0023 0.0064 J 0.0063 17
Toluene 0.0074 J <0.0055 <0.0052 <0.0072 <0.0061 <0.0052 <0.0067 <0.0075 <0.0078 <0.0042 <0.0049 <0.0051 <0.0060 8.3 990
1,2,4-Trimethylbenzene 0.037 <0.0047 <0.0045 <0.0062 <0.0052 <0.0045 <0.0057 <0.0065 <0.0067 <0.0036 <0.0042 <0.0044 <0.0052 12 63
Total Xylenes <0.0045 <0.0046 <0.0043 <0.0060 <0.0050 <0.0043 <0.0055 0.023 <0.0064 <0.0034 <0.0040 <0.0042 <0.0050 9.9 120
Acenaphthene 0.64 <0.15 <0.16 <0.17 <0.14 <0.16 <0.17 <0.18 <0.19 2.3 <0.15 <0.15 <0.16 16 720
Anthracene 0.81 <0.14 <0.15 <0.16 <0.13 <0.15 <0.16 <0.21 <0.17 3.5 <0.14 <0.14 <0.15 1,300 3,600
Benzo(a)anthracene 1.6 <0.15 0.15 J <0.16 <0.14 <0.15 <0.16 <0.18 <0.18 5.5 <0.14 <0.14 <0.15 0.35 1.1
Benzo(a)pyrene 1.7 <0.15 0.17 J <0.17 <0.14 <0.15 <0.17 <0.18 <0.18 5.7 <0.15 <0.15 <0.16 0.12 0.11
Benzo(b)fluoranthene 2.4 <0.15 0.26 J <0.16 <0.14 <0.15 0.25 J <0.18 <0.18 6.9 <0.14 <0.14 <0.15 1.2 1.1
Benzo(g,h,i)perylene 1.1 <0.17 <0.17 <0.19 <0.16 <0.17 <0.19 <0.20 <0.21 3.8 <0.17 <0.16 <0.17 NE NE
Benzo(k)fluoranthene 0.88 <0.15 <0.16 <0.17 <0.14 <0.16 <0.17 <0.18 <0.19 2.7 <0.15 <0.15 <0.16 12 11
Butylbenzylphthalate 47 <0.18 <0.19 <0.21 <0.17 <0.19 <0.21 <0.22 <0.22 <0.17 <0.18 <0.18 <0.19 290 290
Chrysene 1.7 <0.16 0.22 J <0.18 <0.15 <0.16 0.20 J <0.19 <0.19 5.5 <0.16 <0.15 <0.16 36 110
Dibenz(a,h)anthracene 0.31 J <0.17 <0.17 <0.19 <0.16 <0.17 <0.19 <0.20 <0.20 0.97 <0.17 <0.16 <0.17 0.38 0.11
Dibenzofuran 0.24 J <0.16 <0.16 <0.18 <0.15 <0.16 <0.18 <0.19 <0.19 0.90 <0.16 <0.15 <0.16 10 16
bis(2-Ethylhexyl)phthalate 0.22 J <0.17 <0.17 <0.19 <0.16 <0.17 <01.9 <0.20 <0.21 <0.15 <0.17 <0.16 <0.17 14 39
Fluoranthene 3.9 <0.15 0.53 <0.17 <0.14 <0.15 0.39 J <0.18 <0.18 11.2 <0.15 <0.15 <0.15 670 480
Fluorene 0.56 <0.15 <0.16 <0.17 <0.14 <0.16 <0.17 <0.18 <0.19 1.7 <0.15 <0.15 <0.16 110 480
Indeno(1,2,3-cd)pyrene 0.91 <0.17 <0.17 <0.19 <0.16 <0.18 <0.19 <0.21 <0.21 3.3 <0.17 <0.17 <0.18 3.9 1.1
1-Methylnaphthalene <0.15 <0.17 <0.16 <0.17 <0.14 <0.16 <0.17 <0.18 <0.19 2.2 <0.15 <0.15 <0.16 0.11 18
2-Methylnaphthalene 0.17 J <0.17 <0.18 <0.19 <0.16 <0.18 <0.20 <0.21 <0.21 2.4 <0.17 <0.17 <0.18 3.1 48
Naphthalene 0.38 J <0.15 <0.15 <0.17 <0.14 <0.15 <0.17 <0.18 <0.18 2.2 <0.15 <0.14 <0.15 0.39 2.1
Pentachlorophenol <0.41 <0.43 <0.43 <0.48 <0.40 <0.44 0.63 J <0.51 <0.52 <0.39 <0.42 <0.41 <0.44 0.0083 1.0
Phenanthrene 3.3 <0.14 0.39 J <0.16 <0.13 <0.15 0.20 J <0.17 <0.17 15.6 <0.14 <0.14 <0.15 NE NE
Pyrene 2.7 <0.18 0.40 J <0.20 <0.17 <0.18 0.32 J <0.21 <0.21 12.9 <0.18 <0.17 <0.18 440 360
Arsenic 3.87 0.656 J 2.22 2.05 0.905 J 0.493 J 1.27 J 3.23 3.96 2.48 0.747 J 9.07 3.20 5.8 0.68
Barium 62.8 20.6 30.0 161 21.7 10.9 94.2 179 282 104 31.4 194 25.3 580 3,100
Cadmium 0.543 J <0.119 <0.115 0.260 J <0.122 <0.114 <0.144 <0.145 0.144 J <0.102 <0.118 0.423 J <0.124 3.0 1.4
Total Chromium 39.0 9.80 32.0 46.9 12.3 5.61 J 172 53 46.7 44.4 5.7 46.8 632 ------
Trivalent Chromium 39.0 9.80 32.0 44.8 11.7 5.6 171 51 44.5 43.3 5.2 46.8 629 360,000 23,000
Hexavalent Chromium <0.316 <0.356 <0.344 2.09 0.587 J <0.339 0.690 J 1.90 2.21 1.09 J 0.418 J <0.333 2.66 3.8 0.31
Lead 67.6 1.60 J 9.73 37.3 7.14 1.30 J 49.0 6.60 15.8 21.2 7.33 268 15.3 250 400
Mercury 0.0971 <0.0251 0.0259 J <0.0282 0.0528 J <0.0239 <0.303 <0.304 <0.0295 0.0398 J <0.0248 0.205 0.0313 J 1.0 4.7
Selenium 0.582 J 0.296 J 0.708 J 1.45 J <0.257 <0.239 0.841 J 3.31 J 3.96 J 0.873 J <0.248 1.30 J 0.837 J 2.1 78
Silver <0.107 <0.121 <0.117 <0.135 <0.124 <0.115 <0.146 <0.146 <0.142 <0.104 <0.119 0.245 J <0.125 3.4 78
Notes:
All results presented in milligrams per kilogram (mg/kg)Value to right of “<” symbol are laboratory method detection limits. Laboratory method reporting limits may be found in the laboratory report.
Compounds not shown were not detected J = Estimated concentration detected between laboratory method reporting limit and detection limit
VOCs = Volatile Organic Compounds Trivalent Chromium Concentration = Total Chromium Concentration - Hexavalent Chromium Concentration
SVOCs = Semi-volatile Organic Compounds VALUE = concentration greater than the laboratory method detection limit
PSRG = NCDEQ Preliminary Soil Remediation Goals (July 2023)VALUE = concentration greater than the Protection of Groundwater PSRG
* = SB-DUP is a duplicate sample of the P-2 (10 - 15) record sample VALUE = concentration greater than the Residential PSRG
Residential
PSRG
Protection of
Groundwater
PSRG
P-3
Sample Date
Sample Depth (x to y ft bgs)
E-2 P-1 P-2
Total Metals By EPA Methods 6010/7471/7199SVOCs by EPA Method 8270VOCs by EPA Method 8260Sample ID E-1
APPENDIX A
Field Sampling Notes
APPENDIX B
Laboratory Analytical Reports
Chains-of-Custody Forms
#=CL#
August 16, 2023
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92681077
92681077
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
SOUTH BOULEVARD
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on August 07, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 136
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
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EPA# TN00003
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Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
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Kentucky UST Certification #: 16
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Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
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Kentucky UST Certification #: 84
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Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 136
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID Matrix Date Collected Date Received
92681077001 P2-5 Solid 08/04/23 09:10 08/07/23 09:15
92681077002 P2-10 Solid 08/04/23 09:12 08/07/23 09:15
92681077003 E2-5 Solid 08/04/23 09:28 08/07/23 09:15
92681077004 E2-10 Solid 08/04/23 09:30 08/07/23 09:15
92681077005 E1-5 Solid 08/04/23 09:41 08/07/23 09:15
92681077006 E1-10 Solid 08/04/23 09:45 08/07/23 09:15
92681077007 P3-5 Solid 08/04/23 09:54 08/07/23 09:15
92681077008 P3-10 Solid 08/04/23 09:58 08/07/23 09:15
92681077009 P1-5 Solid 08/04/23 10:38 08/07/23 09:15
92681077010 P1-10 Solid 08/04/23 10:40 08/07/23 09:15
92681077011 DP-1 Solid 08/04/23 10:59 08/07/23 09:15
92681077012 DP-2 Solid 08/04/23 11:05 08/07/23 09:15
92681077013 DUP-1 Solid 08/04/23 00:00 08/07/23 09:15
92681077014 TB Water 08/04/23 00:00 08/07/23 09:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 136
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92681077001 P2-5 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077002 P2-10 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077003 E2-5 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077004 E2-10 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077005 E1-5 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077006 E1-10 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 136
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077007 P3-5 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077008 P3-10 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077009 P1-5 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077010 P1-10 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077011 DP-1 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 136
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SW-846 1 PASI-CKDF
SM 2540G 1 PANMT
EPA 7199 1 PANVSS
92681077012 DP-2 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANJAV
EPA 7199 1 PANVSS
92681077013 DUP-1 EPA 6020B 7 PANLD
EPA 7471B 1 PANAKB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANJAV
EPA 7199 1 PANVSS
92681077014 TB EPA 8260D 63 PASI-CJJK
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 136
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92681077001 P2-5
Arsenic 1.27J mg/kg 08/13/23 15:10 J1.68EPA 6020B
Barium 94.2 mg/kg 08/13/23 15:104.21EPA 6020B
Chromium 172 mg/kg 08/13/23 17:0816.8EPA 6020B
Lead 49.0 mg/kg 08/13/23 15:103.37EPA 6020B
Selenium 0.841J mg/kg 08/13/23 15:10 J4.21EPA 6020B
Benzo(b)fluoranthene 0.25J mg/kg 08/13/23 17:140.49EPA 8270E
Chrysene 0.20J mg/kg 08/13/23 17:140.49EPA 8270E
Fluoranthene 0.39J mg/kg 08/13/23 17:140.49EPA 8270E
Pentachlorophenol 0.63J mg/kg 08/13/23 17:14 C80.98EPA 8270E
Phenanthrene 0.20J mg/kg 08/13/23 17:140.49EPA 8270E
Pyrene 0.32J mg/kg 08/13/23 17:140.49EPA 8270E
Percent Moisture 32.9 %08/08/23 13:36 N20.10SW-846
Total Solids 59.4 %08/10/23 06:57SM 2540G
Chromium, Hexavalent 0.690J mg/kg 08/14/23 18:21 J,MH1.68EPA 7199
92681077002 P2-10
Arsenic 3.23 mg/kg 08/13/23 15:131.69EPA 6020B
Barium 179 mg/kg 08/13/23 17:118.45EPA 6020B
Chromium 53.0 mg/kg 08/13/23 15:138.45EPA 6020B
Lead 6.60 mg/kg 08/13/23 15:133.38EPA 6020B
Selenium 3.31J mg/kg 08/13/23 15:13 J4.23EPA 6020B
Xylene (Total)0.023 mg/kg 08/09/23 05:130.022EPA 8260D
m&p-Xylene 0.012J mg/kg 08/09/23 05:130.022EPA 8260D
o-Xylene 0.011J mg/kg 08/09/23 05:130.011EPA 8260D
Percent Moisture 37.2 %08/08/23 13:36 N20.10SW-846
Total Solids 59.1 %08/10/23 07:07SM 2540G
Chromium, Hexavalent 1.90 mg/kg 08/14/23 18:471.69EPA 7199
92681077003 E2-5
Arsenic 2.22 mg/kg 08/13/23 16:241.35EPA 6020B
Barium 30.0 mg/kg 08/13/23 16:243.37EPA 6020B
Chromium 32.0 mg/kg 08/13/23 16:246.74EPA 6020B
Lead 9.73 mg/kg 08/13/23 16:242.70EPA 6020B
Selenium 0.708J mg/kg 08/13/23 16:24 J3.37EPA 6020B
Mercury 0.0259J mg/kg 08/15/23 13:57 J0.0539EPA 7471B
Benzo(a)anthracene 0.15J mg/kg 08/13/23 18:090.44EPA 8270E
Benzo(a)pyrene 0.17J mg/kg 08/13/23 18:090.44EPA 8270E
Benzo(b)fluoranthene 0.26J mg/kg 08/13/23 18:090.44EPA 8270E
Chrysene 0.22J mg/kg 08/13/23 18:090.44EPA 8270E
Fluoranthene 0.53 mg/kg 08/13/23 18:090.44EPA 8270E
Phenanthrene 0.39J mg/kg 08/13/23 18:090.44EPA 8270E
Pyrene 0.40J mg/kg 08/13/23 18:090.44EPA 8270E
Tetrachloroethene 0.043 mg/kg 08/09/23 05:480.0076EPA 8260D
Percent Moisture 24.9 %08/08/23 13:36 N20.10SW-846
Total Solids 74.2 %08/10/23 07:07SM 2540G
92681077004 E2-10
Arsenic 2.05 mg/kg 08/13/23 14:36 ML,PH1.56EPA 6020B
Barium 161 mg/kg 08/13/23 14:36 ML3.91EPA 6020B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 136
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92681077004 E2-10
Cadmium 0.260J mg/kg 08/13/23 14:36 J1.56EPA 6020B
Chromium 46.9 mg/kg 08/13/23 14:36 MH7.82EPA 6020B
Lead 37.3 mg/kg 08/13/23 14:36 ML3.13EPA 6020B
Selenium 1.45J mg/kg 08/13/23 14:36 J,PH3.91EPA 6020B
Tetrachloroethene 0.021 mg/kg 08/09/23 23:280.010EPA 8260D
Percent Moisture 33.2 %08/08/23 13:36 N20.10SW-846
Total Solids 63.9 %08/10/23 07:07SM 2540G
Chromium, Hexavalent 2.09 mg/kg 08/14/23 19:131.56EPA 7199
92681077005 E1-5
Arsenic 3.87 mg/kg 08/13/23 16:271.24EPA 6020B
Barium 62.8 mg/kg 08/13/23 16:273.09EPA 6020B
Cadmium 0.543J mg/kg 08/13/23 16:27 J1.24EPA 6020B
Chromium 39.0 mg/kg 08/13/23 16:276.19EPA 6020B
Lead 67.6 mg/kg 08/13/23 16:272.48EPA 6020B
Selenium 0.582J mg/kg 08/13/23 16:27 J3.09EPA 6020B
Mercury 0.0971 mg/kg 08/15/23 14:020.0495EPA 7471B
Acenaphthene 0.64 mg/kg 08/13/23 19:050.42EPA 8270E
Anthracene 0.81 mg/kg 08/13/23 19:050.42EPA 8270E
Benzo(a)anthracene 1.6 mg/kg 08/13/23 19:050.42EPA 8270E
Benzo(a)pyrene 1.7 mg/kg 08/13/23 19:050.42EPA 8270E
Benzo(b)fluoranthene 2.4 mg/kg 08/13/23 19:050.42EPA 8270E
Benzo(g,h,i)perylene 1.1 mg/kg 08/13/23 19:050.42EPA 8270E
Benzo(k)fluoranthene 0.88 mg/kg 08/13/23 19:050.42EPA 8270E
Butylbenzylphthalate 47.0 mg/kg 08/14/23 16:148.5EPA 8270E
Chrysene 1.7 mg/kg 08/13/23 19:050.42EPA 8270E
Dibenz(a,h)anthracene 0.31J mg/kg 08/13/23 19:050.42EPA 8270E
Dibenzofuran 0.24J mg/kg 08/13/23 19:050.42EPA 8270E
bis(2-Ethylhexyl)phthalate 0.22J mg/kg 08/13/23 19:050.42EPA 8270E
Fluoranthene 3.9 mg/kg 08/13/23 19:050.42EPA 8270E
Fluorene 0.56 mg/kg 08/13/23 19:050.42EPA 8270E
Indeno(1,2,3-cd)pyrene 0.91 mg/kg 08/13/23 19:050.42EPA 8270E
2-Methylnaphthalene 0.17J mg/kg 08/13/23 19:050.42EPA 8270E
Naphthalene 0.38J mg/kg 08/13/23 19:050.42EPA 8270E
Phenanthrene 3.3 mg/kg 08/13/23 19:050.42EPA 8270E
Pyrene 2.7 mg/kg 08/13/23 19:050.42EPA 8270E
Acetone 0.093J mg/kg 08/09/23 06:220.16EPA 8260D
Benzene 0.0079 mg/kg 08/09/23 06:220.0079EPA 8260D
2-Butanone (MEK)0.046J mg/kg 08/09/23 06:220.16EPA 8260D
Naphthalene 0.26 mg/kg 08/09/23 06:220.0079EPA 8260D
Tetrachloroethene 0.12 mg/kg 08/09/23 06:220.0079EPA 8260D
Toluene 0.0074J mg/kg 08/09/23 06:220.0079EPA 8260D
Trichloroethene 0.037 mg/kg 08/09/23 06:220.0079EPA 8260D
Percent Moisture 21.3 %08/08/23 13:37 N20.10SW-846
Total Solids 80.8 %08/10/23 07:07SM 2540G
92681077006 E1-10
Arsenic 0.656J mg/kg 08/13/23 16:31 J1.40EPA 6020B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 136
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92681077006 E1-10
Barium 20.6 mg/kg 08/13/23 16:313.49EPA 6020B
Chromium 9.80 mg/kg 08/13/23 16:316.98EPA 6020B
Lead 1.60J mg/kg 08/13/23 16:31 J2.79EPA 6020B
Selenium 0.296J mg/kg 08/13/23 16:31 J3.49EPA 6020B
Methylene Chloride 0.024J mg/kg 08/09/23 06:40 C90.032EPA 8260D
Naphthalene 0.0070J mg/kg 08/09/23 06:400.0080EPA 8260D
Percent Moisture 24.6 %08/08/23 13:37 N20.10SW-846
Total Solids 71.6 %08/10/23 07:07SM 2540G
92681077007 P3-5
Arsenic 2.48 mg/kg 08/13/23 16:341.20EPA 6020B
Barium 104 mg/kg 08/13/23 16:343.00EPA 6020B
Chromium 44.4 mg/kg 08/13/23 16:345.99EPA 6020B
Lead 21.2 mg/kg 08/13/23 16:342.40EPA 6020B
Selenium 0.873J mg/kg 08/13/23 16:34 J3.00EPA 6020B
Mercury 0.0398J mg/kg 08/15/23 14:07 J0.0479EPA 7471B
Acenaphthene 2.3 mg/kg 08/13/23 20:000.39EPA 8270E
Anthracene 3.5 mg/kg 08/13/23 20:000.39EPA 8270E
Benzo(a)anthracene 5.5 mg/kg 08/14/23 14:212.0EPA 8270E
Benzo(a)pyrene 5.7 mg/kg 08/14/23 14:212.0EPA 8270E
Benzo(b)fluoranthene 6.9 mg/kg 08/14/23 14:212.0EPA 8270E
Benzo(g,h,i)perylene 3.8 mg/kg 08/13/23 20:000.39EPA 8270E
Benzo(k)fluoranthene 2.7 mg/kg 08/13/23 20:000.39EPA 8270E
Chrysene 5.5 mg/kg 08/14/23 14:212.0EPA 8270E
Dibenz(a,h)anthracene 0.97 mg/kg 08/13/23 20:000.39EPA 8270E
Dibenzofuran 0.90 mg/kg 08/13/23 20:000.39EPA 8270E
Fluoranthene 11.2 mg/kg 08/14/23 14:212.0EPA 8270E
Fluorene 1.7 mg/kg 08/13/23 20:000.39EPA 8270E
Indeno(1,2,3-cd)pyrene 3.3 mg/kg 08/13/23 20:000.39EPA 8270E
1-Methylnaphthalene 2.2 mg/kg 08/13/23 20:000.39EPA 8270E
2-Methylnaphthalene 2.4 mg/kg 08/13/23 20:000.39EPA 8270E
Naphthalene 2.2 mg/kg 08/13/23 20:000.39EPA 8270E
Phenanthrene 15.6 mg/kg 08/14/23 14:212.0EPA 8270E
Pyrene 12.9 mg/kg 08/14/23 14:212.0EPA 8270E
Naphthalene 0.0066 mg/kg 08/09/23 06:570.0060EPA 8260D
Tetrachloroethene 0.042 mg/kg 08/09/23 06:570.0060EPA 8260D
Percent Moisture 15.4 %08/08/23 13:37 N20.10SW-846
Total Solids 83.4 %08/10/23 07:07SM 2540G
Chromium, Hexavalent 1.09J mg/kg 08/14/23 19:29 J1.20EPA 7199
92681077008 P3-10
Arsenic 0.747J mg/kg 08/13/23 16:37 J1.38EPA 6020B
Barium 31.4 mg/kg 08/13/23 16:373.45EPA 6020B
Chromium 8.65 mg/kg 08/13/23 16:376.89EPA 6020B
Lead 7.33 mg/kg 08/13/23 16:372.76EPA 6020B
Percent Moisture 23.6 %08/08/23 13:37 N20.10SW-846
Total Solids 72.5 %08/10/23 07:07SM 2540G
Chromium, Hexavalent 0.418J mg/kg 08/14/23 19:34 J1.38EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 136
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92681077009 P1-5
Arsenic 0.905J mg/kg 08/13/23 16:41 J1.43EPA 6020B
Barium 21.7 mg/kg 08/13/23 16:413.57EPA 6020B
Chromium 12.3 mg/kg 08/13/23 16:417.14EPA 6020B
Lead 7.14 mg/kg 08/13/23 16:412.86EPA 6020B
Mercury 0.0528J mg/kg 08/15/23 14:17 J0.0571EPA 7471B
Percent Moisture 19.9 %08/08/23 13:37 N20.10SW-846
Total Solids 70.0 %08/10/23 07:07SM 2540G
Chromium, Hexavalent 0.587J mg/kg 08/14/23 19:39 J1.43EPA 7199
92681077010 P1-10
Arsenic 0.493J mg/kg 08/13/23 16:44 J1.33EPA 6020B
Barium 10.9 mg/kg 08/13/23 16:443.32EPA 6020B
Chromium 5.61J mg/kg 08/13/23 16:44 J6.65EPA 6020B
Lead 1.30J mg/kg 08/13/23 16:44 J2.66EPA 6020B
Percent Moisture 25.6 %08/08/23 13:37 N20.10SW-846
Total Solids 75.2 %08/10/23 07:07SM 2540G
92681077011 DP-1
Arsenic 9.07 mg/kg 08/13/23 16:481.30EPA 6020B
Barium 194 mg/kg 08/13/23 17:1413.0EPA 6020B
Cadmium 0.423J mg/kg 08/13/23 16:48 J1.30EPA 6020B
Chromium 46.8 mg/kg 08/13/23 16:486.52EPA 6020B
Lead 268 mg/kg 08/13/23 17:1410.4EPA 6020B
Selenium 1.30J mg/kg 08/13/23 16:48 J3.26EPA 6020B
Silver 0.245J mg/kg 08/13/23 16:48 J0.652EPA 6020B
Mercury 0.205 mg/kg 08/15/23 14:220.0522EPA 7471B
Percent Moisture 23.4 %08/08/23 13:37 N20.10SW-846
Total Solids 76.7 %08/10/23 07:07SM 2540G
92681077012 DP-2
Arsenic 3.20 mg/kg 08/13/23 16:511.44EPA 6020B
Barium 25.3 mg/kg 08/13/23 16:513.61EPA 6020B
Chromium 632 mg/kg 08/13/23 17:1872.2EPA 6020B
Lead 15.3 mg/kg 08/13/23 16:512.89EPA 6020B
Selenium 0.837J mg/kg 08/13/23 16:51 J3.61EPA 6020B
Mercury 0.0313J mg/kg 08/15/23 14:25 J0.0578EPA 7471B
Tetrachloroethene 0.0064J mg/kg 08/10/23 02:370.0087EPA 8260D
Percent Moisture 27.6 %08/08/23 13:37 N20.10SW-846
Total Solids 69.2 %08/10/23 12:48SM 2540G
Chromium, Hexavalent 2.66 mg/kg 08/14/23 20:101.44EPA 7199
92681077013 DUP-1
Arsenic 3.96 mg/kg 08/13/23 16:551.64EPA 6020B
Barium 282 mg/kg 08/13/23 17:218.19EPA 6020B
Cadmium 0.144J mg/kg 08/13/23 16:55 J1.64EPA 6020B
Chromium 46.7 mg/kg 08/13/23 16:558.19EPA 6020B
Lead 15.8 mg/kg 08/13/23 16:553.28EPA 6020B
Selenium 3.96J mg/kg 08/13/23 16:55 J4.10EPA 6020B
Chloromethane 0.032 mg/kg 08/10/23 02:540.023EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 136
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92681077013 DUP-1
Percent Moisture 38.4 %08/08/23 13:37 N20.10SW-846
Total Solids 61.0 %08/10/23 12:48SM 2540G
Chromium, Hexavalent 2.21 mg/kg 08/14/23 20:161.64EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-5 Lab ID:92681077001 Collected:08/04/23 09:10 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.27J mg/kg 08/13/23 15:10 7440-38-2 J08/10/23 09:481.68 0.168 5
Barium 94.2 mg/kg 08/13/23 15:10 7440-39-308/10/23 09:484.21 0.256 5
Cadmium ND mg/kg 08/13/23 15:10 7440-43-908/10/23 09:481.68 0.144 5
Chromium 172 mg/kg 08/13/23 17:08 7440-47-308/10/23 09:4816.8 0.998 10
Lead 49.0 mg/kg 08/13/23 15:10 7439-92-108/10/23 09:483.37 0.167 5
Selenium 0.841J mg/kg 08/13/23 15:10 7782-49-2 J08/10/23 09:484.21 0.303 5
Silver ND mg/kg 08/13/23 15:10 7440-22-408/10/23 09:480.841 0.146 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 13:52 7439-97-608/14/23 20:110.0673 0.0303 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 17:14 83-32-908/11/23 15:350.49 0.17 1
Acenaphthylene ND mg/kg 08/13/23 17:14 208-96-808/11/23 15:350.49 0.17 1
Aniline ND mg/kg 08/13/23 17:14 62-53-308/11/23 15:350.49 0.19 1
Anthracene ND mg/kg 08/13/23 17:14 120-12-708/11/23 15:350.49 0.16 1
Benzo(a)anthracene ND mg/kg 08/13/23 17:14 56-55-308/11/23 15:350.49 0.16 1
Benzo(a)pyrene ND mg/kg 08/13/23 17:14 50-32-808/11/23 15:350.49 0.17 1
Benzo(b)fluoranthene 0.25J mg/kg 08/13/23 17:14 205-99-208/11/23 15:350.49 0.16 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 17:14 191-24-208/11/23 15:350.49 0.19 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 17:14 207-08-908/11/23 15:350.49 0.17 1
Benzoic Acid ND mg/kg 08/13/23 17:14 65-85-008/11/23 15:352.4 1.0 1
Benzyl alcohol ND mg/kg 08/13/23 17:14 100-51-608/11/23 15:350.98 0.37 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 17:14 101-55-308/11/23 15:350.49 0.19 1
Butylbenzylphthalate ND mg/kg 08/13/23 17:14 85-68-708/11/23 15:350.49 0.21 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 17:14 59-50-708/11/23 15:350.98 0.34 1
4-Chloroaniline ND mg/kg 08/13/23 17:14 106-47-808/11/23 15:350.98 0.38 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 17:14 111-91-108/11/23 15:350.49 0.20 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 17:14 111-44-408/11/23 15:350.49 0.18 1
2-Chloronaphthalene ND mg/kg 08/13/23 17:14 91-58-708/11/23 15:350.49 0.19 1
2-Chlorophenol ND mg/kg 08/13/23 17:14 95-57-808/11/23 15:350.49 0.18 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 17:14 7005-72-308/11/23 15:350.49 0.18 1
Chrysene 0.20J mg/kg 08/13/23 17:14 218-01-908/11/23 15:350.49 0.18 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 17:14 53-70-308/11/23 15:350.49 0.19 1
Dibenzofuran ND mg/kg 08/13/23 17:14 132-64-908/11/23 15:350.49 0.18 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 17:14 95-50-108/11/23 15:350.49 0.18 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 17:14 541-73-108/11/23 15:350.49 0.17 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 17:14 106-46-708/11/23 15:350.49 0.19 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 17:14 91-94-108/11/23 15:350.98 0.33 1
2,4-Dichlorophenol ND mg/kg 08/13/23 17:14 120-83-208/11/23 15:350.49 0.19 1
Diethylphthalate ND mg/kg 08/13/23 17:14 84-66-208/11/23 15:350.49 0.18 1
2,4-Dimethylphenol ND mg/kg 08/13/23 17:14 105-67-908/11/23 15:350.49 0.20 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-5 Lab ID:92681077001 Collected:08/04/23 09:10 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 17:14 131-11-308/11/23 15:350.49 0.18 1
Di-n-butylphthalate ND mg/kg 08/13/23 17:14 84-74-208/11/23 15:350.49 0.16 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 17:14 534-52-108/11/23 15:350.98 0.46 1
2,4-Dinitrophenol ND mg/kg 08/13/23 17:14 51-28-508/11/23 15:352.4 1.5 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 17:14 121-14-208/11/23 15:350.49 0.19 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 17:14 606-20-208/11/23 15:350.49 0.18 1
Di-n-octylphthalate ND mg/kg 08/13/23 17:14 117-84-008/11/23 15:350.49 0.19 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 17:14 117-81-708/11/23 15:350.49 0.19 1
Fluoranthene 0.39J mg/kg 08/13/23 17:14 206-44-008/11/23 15:350.49 0.17 1
Fluorene ND mg/kg 08/13/23 17:14 86-73-708/11/23 15:350.49 0.17 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 17:14 87-68-308/11/23 15:350.49 0.21 1
Hexachlorobenzene ND mg/kg 08/13/23 17:14 118-74-108/11/23 15:350.49 0.19 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 17:14 77-47-4 v208/11/23 15:350.49 0.28 1
Hexachloroethane ND mg/kg 08/13/23 17:14 67-72-108/11/23 15:350.49 0.19 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 17:14 193-39-508/11/23 15:350.49 0.19 1
Isophorone ND mg/kg 08/13/23 17:14 78-59-108/11/23 15:350.49 0.22 1
1-Methylnaphthalene ND mg/kg 08/13/23 17:14 90-12-008/11/23 15:350.49 0.17 1
2-Methylnaphthalene ND mg/kg 08/13/23 17:14 91-57-608/11/23 15:350.49 0.20 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 17:14 95-48-708/11/23 15:350.49 0.20 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 17:14 15831-10-408/11/23 15:350.49 0.20 1
Naphthalene ND mg/kg 08/13/23 17:14 91-20-308/11/23 15:350.49 0.17 1
2-Nitroaniline ND mg/kg 08/13/23 17:14 88-74-408/11/23 15:352.4 0.40 1
3-Nitroaniline ND mg/kg 08/13/23 17:14 99-09-208/11/23 15:352.4 0.38 1
4-Nitroaniline ND mg/kg 08/13/23 17:14 100-01-608/11/23 15:350.98 0.37 1
Nitrobenzene ND mg/kg 08/13/23 17:14 98-95-308/11/23 15:350.49 0.23 1
2-Nitrophenol ND mg/kg 08/13/23 17:14 88-75-508/11/23 15:350.49 0.21 1
4-Nitrophenol ND mg/kg 08/13/23 17:14 100-02-708/11/23 15:352.4 0.94 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 17:14 62-75-908/11/23 15:350.49 0.16 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 17:14 621-64-708/11/23 15:350.49 0.18 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 17:14 86-30-608/11/23 15:350.49 0.17 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 17:14 108-60-108/11/23 15:350.49 0.23 1
Pentachlorophenol 0.63J mg/kg 08/13/23 17:14 87-86-5 C808/11/23 15:350.98 0.48 1
Phenanthrene 0.20J mg/kg 08/13/23 17:14 85-01-808/11/23 15:350.49 0.16 1
Phenol ND mg/kg 08/13/23 17:14 108-95-208/11/23 15:350.49 0.22 1
Pyrene 0.32J mg/kg 08/13/23 17:14 129-00-008/11/23 15:350.49 0.20 1
Pyridine ND mg/kg 08/13/23 17:14 110-86-108/11/23 15:350.49 0.15 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 17:14 120-82-108/11/23 15:350.49 0.19 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 17:14 95-95-408/11/23 15:350.49 0.22 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 17:14 88-06-208/11/23 15:350.49 0.20 1
Surrogates
Nitrobenzene-d5 (S)69 %08/13/23 17:14 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)64 %08/13/23 17:14 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)56 %08/13/23 17:14 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)58 %08/13/23 17:14 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-5 Lab ID:92681077001 Collected:08/04/23 09:10 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)60 %08/13/23 17:14 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)98 %08/13/23 17:14 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 04:56 67-64-108/08/23 21:440.19 0.062 1
Benzene ND mg/kg 08/09/23 04:56 71-43-208/08/23 21:440.0097 0.0038 1
Bromobenzene ND mg/kg 08/09/23 04:56 108-86-108/08/23 21:440.0097 0.0032 1
Bromochloromethane ND mg/kg 08/09/23 04:56 74-97-508/08/23 21:440.0097 0.0029 1
Bromodichloromethane ND mg/kg 08/09/23 04:56 75-27-408/08/23 21:440.0097 0.0037 1
Bromoform ND mg/kg 08/09/23 04:56 75-25-208/08/23 21:440.0097 0.0034 1
Bromomethane ND mg/kg 08/09/23 04:56 74-83-9 v2,v308/08/23 21:440.039 0.030 1
2-Butanone (MEK)ND mg/kg 08/09/23 04:56 78-93-308/08/23 21:440.19 0.046 1
n-Butylbenzene ND mg/kg 08/09/23 04:56 104-51-808/08/23 21:440.0097 0.0061 1
sec-Butylbenzene ND mg/kg 08/09/23 04:56 135-98-808/08/23 21:440.0097 0.0043 1
tert-Butylbenzene ND mg/kg 08/09/23 04:56 98-06-608/08/23 21:440.0097 0.0034 1
Carbon tetrachloride ND mg/kg 08/09/23 04:56 56-23-508/08/23 21:440.0097 0.0036 1
Chlorobenzene ND mg/kg 08/09/23 04:56 108-90-708/08/23 21:440.0097 0.0055 1
Chloroethane ND mg/kg 08/09/23 04:56 75-00-3 M108/08/23 21:440.019 0.0075 1
Chloroform ND mg/kg 08/09/23 04:56 67-66-308/08/23 21:440.0097 0.0081 1
Chloromethane ND mg/kg 08/09/23 04:56 74-87-308/08/23 21:440.019 0.0081 1
2-Chlorotoluene ND mg/kg 08/09/23 04:56 95-49-808/08/23 21:440.0097 0.0034 1
4-Chlorotoluene ND mg/kg 08/09/23 04:56 106-43-408/08/23 21:440.0097 0.0054 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 04:56 96-12-808/08/23 21:440.0097 0.0037 1
Dibromochloromethane ND mg/kg 08/09/23 04:56 124-48-108/08/23 21:440.0097 0.0054 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 04:56 106-93-408/08/23 21:440.0097 0.0043 1
Dibromomethane ND mg/kg 08/09/23 04:56 74-95-308/08/23 21:440.0097 0.0021 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 04:56 95-50-108/08/23 21:440.0097 0.0035 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 04:56 541-73-108/08/23 21:440.0097 0.0030 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 04:56 106-46-708/08/23 21:440.0097 0.0025 1
Dichlorodifluoromethane ND mg/kg 08/09/23 04:56 75-71-8 M108/08/23 21:440.019 0.0098 1
1,1-Dichloroethane ND mg/kg 08/09/23 04:56 75-34-308/08/23 21:440.0097 0.0040 1
1,2-Dichloroethane ND mg/kg 08/09/23 04:56 107-06-208/08/23 21:440.0097 0.0064 1
1,1-Dichloroethene ND mg/kg 08/09/23 04:56 75-35-408/08/23 21:440.0097 0.0040 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 04:56 156-59-208/08/23 21:440.0097 0.0033 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 04:56 156-60-508/08/23 21:440.0097 0.0082 1
1,2-Dichloropropane ND mg/kg 08/09/23 04:56 78-87-508/08/23 21:440.0097 0.0029 1
1,3-Dichloropropane ND mg/kg 08/09/23 04:56 142-28-908/08/23 21:440.0097 0.0030 1
2,2-Dichloropropane ND mg/kg 08/09/23 04:56 594-20-708/08/23 21:440.0097 0.0073 1
1,1-Dichloropropene ND mg/kg 08/09/23 04:56 563-58-608/08/23 21:440.0097 0.0046 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 04:56 10061-01-508/08/23 21:440.0097 0.0026 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 04:56 10061-02-608/08/23 21:440.0097 0.0033 1
Diisopropyl ether ND mg/kg 08/09/23 04:56 108-20-308/08/23 21:440.0097 0.0026 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-5 Lab ID:92681077001 Collected:08/04/23 09:10 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 04:56 100-41-408/08/23 21:440.0097 0.0045 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 04:56 87-68-308/08/23 21:440.019 0.016 1
2-Hexanone ND mg/kg 08/09/23 04:56 591-78-608/08/23 21:440.097 0.0093 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 04:56 98-82-808/08/23 21:440.0097 0.0033 1
p-Isopropyltoluene ND mg/kg 08/09/23 04:56 99-87-608/08/23 21:440.0097 0.0048 1
Methylene Chloride ND mg/kg 08/09/23 04:56 75-09-208/08/23 21:440.039 0.026 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 04:56 108-10-108/08/23 21:440.097 0.0093 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 04:56 1634-04-408/08/23 21:440.0097 0.0036 1
Naphthalene ND mg/kg 08/09/23 04:56 91-20-308/08/23 21:440.0097 0.0051 1
n-Propylbenzene ND mg/kg 08/09/23 04:56 103-65-108/08/23 21:440.0097 0.0034 1
Styrene ND mg/kg 08/09/23 04:56 100-42-508/08/23 21:440.0097 0.0026 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 04:56 630-20-608/08/23 21:440.0097 0.0037 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 04:56 79-34-508/08/23 21:440.0097 0.0026 1
Tetrachloroethene ND mg/kg 08/09/23 04:56 127-18-408/08/23 21:440.0097 0.0031 1
Toluene ND mg/kg 08/09/23 04:56 108-88-308/08/23 21:440.0097 0.0067 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 04:56 87-61-608/08/23 21:440.0097 0.0078 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 04:56 120-82-1 IK08/08/23 21:440.0097 0.0081 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 04:56 71-55-608/08/23 21:440.0097 0.0050 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 04:56 79-00-508/08/23 21:440.0097 0.0032 1
Trichloroethene ND mg/kg 08/09/23 04:56 79-01-608/08/23 21:440.0097 0.0078 1
Trichlorofluoromethane ND mg/kg 08/09/23 04:56 75-69-408/08/23 21:440.0097 0.0053 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 04:56 96-18-408/08/23 21:440.0097 0.0049 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 04:56 95-63-608/08/23 21:440.0097 0.0057 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 04:56 108-67-808/08/23 21:440.0097 0.0032 1
Vinyl acetate ND mg/kg 08/09/23 04:56 108-05-408/08/23 21:440.097 0.020 1
Vinyl chloride ND mg/kg 08/09/23 04:56 75-01-408/08/23 21:440.019 0.0049 1
Xylene (Total)ND mg/kg 08/09/23 04:56 1330-20-708/08/23 21:440.019 0.0055 1
m&p-Xylene ND mg/kg 08/09/23 04:56 179601-23-108/08/23 21:440.019 0.0066 1
o-Xylene ND mg/kg 08/09/23 04:56 95-47-608/08/23 21:440.0097 0.0043 1
Surrogates
Toluene-d8 (S)101 %08/09/23 04:56 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)103 %08/09/23 04:56 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)107 %08/09/23 04:56 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 32.9 %08/08/23 13:36 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 59.4 %08/10/23 06:5708/10/23 06:431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-5 Lab ID:92681077001 Collected:08/04/23 09:10 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.690J mg/kg 08/14/23 18:21 18540-29-9 J,MH08/13/23 18:151.68 0.429 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-10 Lab ID:92681077002 Collected:08/04/23 09:12 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.23 mg/kg 08/13/23 15:13 7440-38-208/10/23 09:481.69 0.169 5
Barium 179 mg/kg 08/13/23 17:11 7440-39-308/10/23 09:488.45 0.514 10
Cadmium ND mg/kg 08/13/23 15:13 7440-43-908/10/23 09:481.69 0.145 5
Chromium 53.0 mg/kg 08/13/23 15:13 7440-47-308/10/23 09:488.45 0.500 5
Lead 6.60 mg/kg 08/13/23 15:13 7439-92-108/10/23 09:483.38 0.167 5
Selenium 3.31J mg/kg 08/13/23 15:13 7782-49-2 J08/10/23 09:484.23 0.304 5
Silver ND mg/kg 08/13/23 15:13 7440-22-408/10/23 09:480.845 0.146 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 13:54 7439-97-608/14/23 20:110.0676 0.0304 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 17:42 83-32-908/11/23 15:350.53 0.18 1
Acenaphthylene ND mg/kg 08/13/23 17:42 208-96-808/11/23 15:350.53 0.18 1
Aniline ND mg/kg 08/13/23 17:42 62-53-308/11/23 15:350.53 0.21 1
Anthracene ND mg/kg 08/13/23 17:42 120-12-708/11/23 15:350.53 0.17 1
Benzo(a)anthracene ND mg/kg 08/13/23 17:42 56-55-308/11/23 15:350.53 0.18 1
Benzo(a)pyrene ND mg/kg 08/13/23 17:42 50-32-808/11/23 15:350.53 0.18 1
Benzo(b)fluoranthene ND mg/kg 08/13/23 17:42 205-99-208/11/23 15:350.53 0.18 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 17:42 191-24-208/11/23 15:350.53 0.20 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 17:42 207-08-908/11/23 15:350.53 0.18 1
Benzoic Acid ND mg/kg 08/13/23 17:42 65-85-008/11/23 15:352.6 1.1 1
Benzyl alcohol ND mg/kg 08/13/23 17:42 100-51-608/11/23 15:351.1 0.40 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 17:42 101-55-308/11/23 15:350.53 0.20 1
Butylbenzylphthalate ND mg/kg 08/13/23 17:42 85-68-708/11/23 15:350.53 0.22 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 17:42 59-50-708/11/23 15:351.1 0.37 1
4-Chloroaniline ND mg/kg 08/13/23 17:42 106-47-808/11/23 15:351.1 0.41 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 17:42 111-91-108/11/23 15:350.53 0.22 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 17:42 111-44-408/11/23 15:350.53 0.20 1
2-Chloronaphthalene ND mg/kg 08/13/23 17:42 91-58-708/11/23 15:350.53 0.21 1
2-Chlorophenol ND mg/kg 08/13/23 17:42 95-57-808/11/23 15:350.53 0.20 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 17:42 7005-72-308/11/23 15:350.53 0.20 1
Chrysene ND mg/kg 08/13/23 17:42 218-01-908/11/23 15:350.53 0.19 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 17:42 53-70-308/11/23 15:350.53 0.20 1
Dibenzofuran ND mg/kg 08/13/23 17:42 132-64-908/11/23 15:350.53 0.19 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 17:42 95-50-108/11/23 15:350.53 0.19 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 17:42 541-73-108/11/23 15:350.53 0.19 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 17:42 106-46-708/11/23 15:350.53 0.20 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 17:42 91-94-108/11/23 15:351.1 0.36 1
2,4-Dichlorophenol ND mg/kg 08/13/23 17:42 120-83-208/11/23 15:350.53 0.21 1
Diethylphthalate ND mg/kg 08/13/23 17:42 84-66-208/11/23 15:350.53 0.19 1
2,4-Dimethylphenol ND mg/kg 08/13/23 17:42 105-67-908/11/23 15:350.53 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-10 Lab ID:92681077002 Collected:08/04/23 09:12 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 17:42 131-11-308/11/23 15:350.53 0.19 1
Di-n-butylphthalate ND mg/kg 08/13/23 17:42 84-74-208/11/23 15:350.53 0.18 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 17:42 534-52-108/11/23 15:351.1 0.49 1
2,4-Dinitrophenol ND mg/kg 08/13/23 17:42 51-28-508/11/23 15:352.6 1.6 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 17:42 121-14-208/11/23 15:350.53 0.20 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 17:42 606-20-208/11/23 15:350.53 0.19 1
Di-n-octylphthalate ND mg/kg 08/13/23 17:42 117-84-008/11/23 15:350.53 0.21 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 17:42 117-81-708/11/23 15:350.53 0.20 1
Fluoranthene ND mg/kg 08/13/23 17:42 206-44-008/11/23 15:350.53 0.18 1
Fluorene ND mg/kg 08/13/23 17:42 86-73-708/11/23 15:350.53 0.18 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 17:42 87-68-308/11/23 15:350.53 0.23 1
Hexachlorobenzene ND mg/kg 08/13/23 17:42 118-74-108/11/23 15:350.53 0.21 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 17:42 77-47-4 v208/11/23 15:350.53 0.30 1
Hexachloroethane ND mg/kg 08/13/23 17:42 67-72-108/11/23 15:350.53 0.20 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 17:42 193-39-508/11/23 15:350.53 0.21 1
Isophorone ND mg/kg 08/13/23 17:42 78-59-108/11/23 15:350.53 0.23 1
1-Methylnaphthalene ND mg/kg 08/13/23 17:42 90-12-008/11/23 15:350.53 0.18 1
2-Methylnaphthalene ND mg/kg 08/13/23 17:42 91-57-608/11/23 15:350.53 0.21 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 17:42 95-48-708/11/23 15:350.53 0.22 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 17:42 15831-10-408/11/23 15:350.53 0.21 1
Naphthalene ND mg/kg 08/13/23 17:42 91-20-308/11/23 15:350.53 0.18 1
2-Nitroaniline ND mg/kg 08/13/23 17:42 88-74-408/11/23 15:352.6 0.43 1
3-Nitroaniline ND mg/kg 08/13/23 17:42 99-09-208/11/23 15:352.6 0.41 1
4-Nitroaniline ND mg/kg 08/13/23 17:42 100-01-608/11/23 15:351.1 0.40 1
Nitrobenzene ND mg/kg 08/13/23 17:42 98-95-308/11/23 15:350.53 0.24 1
2-Nitrophenol ND mg/kg 08/13/23 17:42 88-75-508/11/23 15:350.53 0.23 1
4-Nitrophenol ND mg/kg 08/13/23 17:42 100-02-708/11/23 15:352.6 1.0 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 17:42 62-75-908/11/23 15:350.53 0.18 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 17:42 621-64-708/11/23 15:350.53 0.20 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 17:42 86-30-608/11/23 15:350.53 0.19 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 17:42 108-60-108/11/23 15:350.53 0.25 1
Pentachlorophenol ND mg/kg 08/13/23 17:42 87-86-508/11/23 15:351.1 0.51 1
Phenanthrene ND mg/kg 08/13/23 17:42 85-01-808/11/23 15:350.53 0.17 1
Phenol ND mg/kg 08/13/23 17:42 108-95-208/11/23 15:350.53 0.23 1
Pyrene ND mg/kg 08/13/23 17:42 129-00-008/11/23 15:350.53 0.21 1
Pyridine ND mg/kg 08/13/23 17:42 110-86-108/11/23 15:350.53 0.17 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 17:42 120-82-108/11/23 15:350.53 0.21 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 17:42 95-95-408/11/23 15:350.53 0.24 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 17:42 88-06-208/11/23 15:350.53 0.22 1
Surrogates
Nitrobenzene-d5 (S)66 %08/13/23 17:42 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)52 %08/13/23 17:42 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)38 %08/13/23 17:42 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)49 %08/13/23 17:42 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-10 Lab ID:92681077002 Collected:08/04/23 09:12 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)49 %08/13/23 17:42 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)66 %08/13/23 17:42 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 05:13 67-64-108/08/23 21:440.22 0.070 1
Benzene ND mg/kg 08/09/23 05:13 71-43-208/08/23 21:440.011 0.0043 1
Bromobenzene ND mg/kg 08/09/23 05:13 108-86-108/08/23 21:440.011 0.0036 1
Bromochloromethane ND mg/kg 08/09/23 05:13 74-97-508/08/23 21:440.011 0.0032 1
Bromodichloromethane ND mg/kg 08/09/23 05:13 75-27-408/08/23 21:440.011 0.0042 1
Bromoform ND mg/kg 08/09/23 05:13 75-25-208/08/23 21:440.011 0.0038 1
Bromomethane ND mg/kg 08/09/23 05:13 74-83-9 v208/08/23 21:440.044 0.034 1
2-Butanone (MEK)ND mg/kg 08/09/23 05:13 78-93-308/08/23 21:440.22 0.052 1
n-Butylbenzene ND mg/kg 08/09/23 05:13 104-51-808/08/23 21:440.011 0.0069 1
sec-Butylbenzene ND mg/kg 08/09/23 05:13 135-98-808/08/23 21:440.011 0.0048 1
tert-Butylbenzene ND mg/kg 08/09/23 05:13 98-06-608/08/23 21:440.011 0.0039 1
Carbon tetrachloride ND mg/kg 08/09/23 05:13 56-23-508/08/23 21:440.011 0.0041 1
Chlorobenzene ND mg/kg 08/09/23 05:13 108-90-708/08/23 21:440.011 0.0063 1
Chloroethane ND mg/kg 08/09/23 05:13 75-00-308/08/23 21:440.022 0.0084 1
Chloroform ND mg/kg 08/09/23 05:13 67-66-308/08/23 21:440.011 0.0091 1
Chloromethane ND mg/kg 08/09/23 05:13 74-87-308/08/23 21:440.022 0.0092 1
2-Chlorotoluene ND mg/kg 08/09/23 05:13 95-49-808/08/23 21:440.011 0.0039 1
4-Chlorotoluene ND mg/kg 08/09/23 05:13 106-43-408/08/23 21:440.011 0.0061 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 05:13 96-12-808/08/23 21:440.011 0.0042 1
Dibromochloromethane ND mg/kg 08/09/23 05:13 124-48-108/08/23 21:440.011 0.0061 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 05:13 106-93-408/08/23 21:440.011 0.0048 1
Dibromomethane ND mg/kg 08/09/23 05:13 74-95-308/08/23 21:440.011 0.0023 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 05:13 95-50-108/08/23 21:440.011 0.0039 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 05:13 541-73-108/08/23 21:440.011 0.0034 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 05:13 106-46-708/08/23 21:440.011 0.0028 1
Dichlorodifluoromethane ND mg/kg 08/09/23 05:13 75-71-808/08/23 21:440.022 0.011 1
1,1-Dichloroethane ND mg/kg 08/09/23 05:13 75-34-308/08/23 21:440.011 0.0045 1
1,2-Dichloroethane ND mg/kg 08/09/23 05:13 107-06-208/08/23 21:440.011 0.0072 1
1,1-Dichloroethene ND mg/kg 08/09/23 05:13 75-35-408/08/23 21:440.011 0.0045 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 05:13 156-59-208/08/23 21:440.011 0.0037 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 05:13 156-60-508/08/23 21:440.011 0.0093 1
1,2-Dichloropropane ND mg/kg 08/09/23 05:13 78-87-508/08/23 21:440.011 0.0033 1
1,3-Dichloropropane ND mg/kg 08/09/23 05:13 142-28-908/08/23 21:440.011 0.0034 1
2,2-Dichloropropane ND mg/kg 08/09/23 05:13 594-20-708/08/23 21:440.011 0.0083 1
1,1-Dichloropropene ND mg/kg 08/09/23 05:13 563-58-608/08/23 21:440.011 0.0052 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 05:13 10061-01-508/08/23 21:440.011 0.0030 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 05:13 10061-02-608/08/23 21:440.011 0.0038 1
Diisopropyl ether ND mg/kg 08/09/23 05:13 108-20-308/08/23 21:440.011 0.0029 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-10 Lab ID:92681077002 Collected:08/04/23 09:12 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 05:13 100-41-408/08/23 21:440.011 0.0051 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 05:13 87-68-308/08/23 21:440.022 0.018 1
2-Hexanone ND mg/kg 08/09/23 05:13 591-78-608/08/23 21:440.11 0.011 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 05:13 98-82-808/08/23 21:440.011 0.0037 1
p-Isopropyltoluene ND mg/kg 08/09/23 05:13 99-87-608/08/23 21:440.011 0.0054 1
Methylene Chloride ND mg/kg 08/09/23 05:13 75-09-208/08/23 21:440.044 0.030 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 05:13 108-10-108/08/23 21:440.11 0.011 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 05:13 1634-04-408/08/23 21:440.011 0.0041 1
Naphthalene ND mg/kg 08/09/23 05:13 91-20-308/08/23 21:440.011 0.0057 1
n-Propylbenzene ND mg/kg 08/09/23 05:13 103-65-108/08/23 21:440.011 0.0039 1
Styrene ND mg/kg 08/09/23 05:13 100-42-508/08/23 21:440.011 0.0029 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 05:13 630-20-608/08/23 21:440.011 0.0042 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 05:13 79-34-508/08/23 21:440.011 0.0029 1
Tetrachloroethene ND mg/kg 08/09/23 05:13 127-18-408/08/23 21:440.011 0.0034 1
Toluene ND mg/kg 08/09/23 05:13 108-88-308/08/23 21:440.011 0.0075 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 05:13 87-61-608/08/23 21:440.011 0.0088 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 05:13 120-82-1 IK08/08/23 21:440.011 0.0092 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 05:13 71-55-608/08/23 21:440.011 0.0057 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 05:13 79-00-508/08/23 21:440.011 0.0036 1
Trichloroethene ND mg/kg 08/09/23 05:13 79-01-608/08/23 21:440.011 0.0088 1
Trichlorofluoromethane ND mg/kg 08/09/23 05:13 75-69-408/08/23 21:440.011 0.0060 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 05:13 96-18-408/08/23 21:440.011 0.0055 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 05:13 95-63-608/08/23 21:440.011 0.0065 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 05:13 108-67-808/08/23 21:440.011 0.0037 1
Vinyl acetate ND mg/kg 08/09/23 05:13 108-05-408/08/23 21:440.11 0.022 1
Vinyl chloride ND mg/kg 08/09/23 05:13 75-01-408/08/23 21:440.022 0.0055 1
Xylene (Total)0.023 mg/kg 08/09/23 05:13 1330-20-708/08/23 21:440.022 0.0062 1
m&p-Xylene 0.012J mg/kg 08/09/23 05:13 179601-23-108/08/23 21:440.022 0.0075 1
o-Xylene 0.011J mg/kg 08/09/23 05:13 95-47-608/08/23 21:440.011 0.0048 1
Surrogates
Toluene-d8 (S)100 %08/09/23 05:13 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)105 %08/09/23 05:13 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)108 %08/09/23 05:13 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 37.2 %08/08/23 13:36 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 59.1 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P2-10 Lab ID:92681077002 Collected:08/04/23 09:12 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.90 mg/kg 08/14/23 18:47 18540-29-908/13/23 18:151.69 0.431 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-5 Lab ID:92681077003 Collected:08/04/23 09:28 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.22 mg/kg 08/13/23 16:24 7440-38-208/10/23 09:481.35 0.135 5
Barium 30.0 mg/kg 08/13/23 16:24 7440-39-308/10/23 09:483.37 0.205 5
Cadmium ND mg/kg 08/13/23 16:24 7440-43-908/10/23 09:481.35 0.115 5
Chromium 32.0 mg/kg 08/13/23 16:24 7440-47-308/10/23 09:486.74 0.399 5
Lead 9.73 mg/kg 08/13/23 16:24 7439-92-108/10/23 09:482.70 0.134 5
Selenium 0.708J mg/kg 08/13/23 16:24 7782-49-2 J08/10/23 09:483.37 0.243 5
Silver ND mg/kg 08/13/23 16:24 7440-22-408/10/23 09:480.674 0.117 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0259J mg/kg 08/15/23 13:57 7439-97-6 J08/14/23 20:110.0539 0.0243 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 18:09 83-32-908/11/23 15:350.44 0.16 1
Acenaphthylene ND mg/kg 08/13/23 18:09 208-96-808/11/23 15:350.44 0.16 1
Aniline ND mg/kg 08/13/23 18:09 62-53-308/11/23 15:350.44 0.17 1
Anthracene ND mg/kg 08/13/23 18:09 120-12-708/11/23 15:350.44 0.15 1
Benzo(a)anthracene 0.15J mg/kg 08/13/23 18:09 56-55-308/11/23 15:350.44 0.15 1
Benzo(a)pyrene 0.17J mg/kg 08/13/23 18:09 50-32-808/11/23 15:350.44 0.15 1
Benzo(b)fluoranthene 0.26J mg/kg 08/13/23 18:09 205-99-208/11/23 15:350.44 0.15 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 18:09 191-24-208/11/23 15:350.44 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 18:09 207-08-908/11/23 15:350.44 0.16 1
Benzoic Acid ND mg/kg 08/13/23 18:09 65-85-008/11/23 15:352.2 0.95 1
Benzyl alcohol ND mg/kg 08/13/23 18:09 100-51-608/11/23 15:350.89 0.34 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 18:09 101-55-308/11/23 15:350.44 0.17 1
Butylbenzylphthalate ND mg/kg 08/13/23 18:09 85-68-708/11/23 15:350.44 0.19 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 18:09 59-50-708/11/23 15:350.89 0.31 1
4-Chloroaniline ND mg/kg 08/13/23 18:09 106-47-808/11/23 15:350.89 0.35 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 18:09 111-91-108/11/23 15:350.44 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 18:09 111-44-408/11/23 15:350.44 0.17 1
2-Chloronaphthalene ND mg/kg 08/13/23 18:09 91-58-708/11/23 15:350.44 0.18 1
2-Chlorophenol ND mg/kg 08/13/23 18:09 95-57-808/11/23 15:350.44 0.17 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 18:09 7005-72-308/11/23 15:350.44 0.17 1
Chrysene 0.22J mg/kg 08/13/23 18:09 218-01-908/11/23 15:350.44 0.16 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 18:09 53-70-308/11/23 15:350.44 0.17 1
Dibenzofuran ND mg/kg 08/13/23 18:09 132-64-908/11/23 15:350.44 0.16 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 18:09 95-50-108/11/23 15:350.44 0.16 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 18:09 541-73-108/11/23 15:350.44 0.16 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 18:09 106-46-708/11/23 15:350.44 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 18:09 91-94-108/11/23 15:350.89 0.30 1
2,4-Dichlorophenol ND mg/kg 08/13/23 18:09 120-83-208/11/23 15:350.44 0.17 1
Diethylphthalate ND mg/kg 08/13/23 18:09 84-66-208/11/23 15:350.44 0.16 1
2,4-Dimethylphenol ND mg/kg 08/13/23 18:09 105-67-908/11/23 15:350.44 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-5 Lab ID:92681077003 Collected:08/04/23 09:28 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 18:09 131-11-308/11/23 15:350.44 0.16 1
Di-n-butylphthalate ND mg/kg 08/13/23 18:09 84-74-208/11/23 15:350.44 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 18:09 534-52-108/11/23 15:350.89 0.41 1
2,4-Dinitrophenol ND mg/kg 08/13/23 18:09 51-28-508/11/23 15:352.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 18:09 121-14-208/11/23 15:350.44 0.17 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 18:09 606-20-208/11/23 15:350.44 0.16 1
Di-n-octylphthalate ND mg/kg 08/13/23 18:09 117-84-008/11/23 15:350.44 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 18:09 117-81-708/11/23 15:350.44 0.17 1
Fluoranthene 0.53 mg/kg 08/13/23 18:09 206-44-008/11/23 15:350.44 0.15 1
Fluorene ND mg/kg 08/13/23 18:09 86-73-708/11/23 15:350.44 0.16 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 18:09 87-68-308/11/23 15:350.44 0.19 1
Hexachlorobenzene ND mg/kg 08/13/23 18:09 118-74-108/11/23 15:350.44 0.17 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 18:09 77-47-4 v208/11/23 15:350.44 0.25 1
Hexachloroethane ND mg/kg 08/13/23 18:09 67-72-108/11/23 15:350.44 0.17 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 18:09 193-39-508/11/23 15:350.44 0.17 1
Isophorone ND mg/kg 08/13/23 18:09 78-59-108/11/23 15:350.44 0.20 1
1-Methylnaphthalene ND mg/kg 08/13/23 18:09 90-12-008/11/23 15:350.44 0.16 1
2-Methylnaphthalene ND mg/kg 08/13/23 18:09 91-57-608/11/23 15:350.44 0.18 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 18:09 95-48-708/11/23 15:350.44 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 18:09 15831-10-408/11/23 15:350.44 0.18 1
Naphthalene ND mg/kg 08/13/23 18:09 91-20-308/11/23 15:350.44 0.15 1
2-Nitroaniline ND mg/kg 08/13/23 18:09 88-74-408/11/23 15:352.2 0.36 1
3-Nitroaniline ND mg/kg 08/13/23 18:09 99-09-208/11/23 15:352.2 0.35 1
4-Nitroaniline ND mg/kg 08/13/23 18:09 100-01-608/11/23 15:350.89 0.34 1
Nitrobenzene ND mg/kg 08/13/23 18:09 98-95-308/11/23 15:350.44 0.21 1
2-Nitrophenol ND mg/kg 08/13/23 18:09 88-75-508/11/23 15:350.44 0.19 1
4-Nitrophenol ND mg/kg 08/13/23 18:09 100-02-708/11/23 15:352.2 0.86 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 18:09 62-75-908/11/23 15:350.44 0.15 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 18:09 621-64-708/11/23 15:350.44 0.17 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 18:09 86-30-608/11/23 15:350.44 0.16 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 18:09 108-60-108/11/23 15:350.44 0.21 1
Pentachlorophenol ND mg/kg 08/13/23 18:09 87-86-508/11/23 15:350.89 0.43 1
Phenanthrene 0.39J mg/kg 08/13/23 18:09 85-01-808/11/23 15:350.44 0.15 1
Phenol ND mg/kg 08/13/23 18:09 108-95-208/11/23 15:350.44 0.20 1
Pyrene 0.40J mg/kg 08/13/23 18:09 129-00-008/11/23 15:350.44 0.18 1
Pyridine ND mg/kg 08/13/23 18:09 110-86-108/11/23 15:350.44 0.14 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 18:09 120-82-108/11/23 15:350.44 0.17 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 18:09 95-95-408/11/23 15:350.44 0.20 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 18:09 88-06-208/11/23 15:350.44 0.18 1
Surrogates
Nitrobenzene-d5 (S)71 %08/13/23 18:09 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)73 %08/13/23 18:09 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)73 %08/13/23 18:09 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)65 %08/13/23 18:09 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-5 Lab ID:92681077003 Collected:08/04/23 09:28 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)67 %08/13/23 18:09 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)93 %08/13/23 18:09 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 05:48 67-64-108/08/23 21:440.15 0.049 1
Benzene ND mg/kg 08/09/23 05:48 71-43-208/08/23 21:440.0076 0.0030 1
Bromobenzene ND mg/kg 08/09/23 05:48 108-86-108/08/23 21:440.0076 0.0025 1
Bromochloromethane ND mg/kg 08/09/23 05:48 74-97-508/08/23 21:440.0076 0.0022 1
Bromodichloromethane ND mg/kg 08/09/23 05:48 75-27-408/08/23 21:440.0076 0.0029 1
Bromoform ND mg/kg 08/09/23 05:48 75-25-208/08/23 21:440.0076 0.0027 1
Bromomethane ND mg/kg 08/09/23 05:48 74-83-9 v208/08/23 21:440.030 0.023 1
2-Butanone (MEK)ND mg/kg 08/09/23 05:48 78-93-308/08/23 21:440.15 0.036 1
n-Butylbenzene ND mg/kg 08/09/23 05:48 104-51-808/08/23 21:440.0076 0.0048 1
sec-Butylbenzene ND mg/kg 08/09/23 05:48 135-98-808/08/23 21:440.0076 0.0033 1
tert-Butylbenzene ND mg/kg 08/09/23 05:48 98-06-608/08/23 21:440.0076 0.0027 1
Carbon tetrachloride ND mg/kg 08/09/23 05:48 56-23-508/08/23 21:440.0076 0.0028 1
Chlorobenzene ND mg/kg 08/09/23 05:48 108-90-708/08/23 21:440.0076 0.0044 1
Chloroethane ND mg/kg 08/09/23 05:48 75-00-308/08/23 21:440.015 0.0059 1
Chloroform ND mg/kg 08/09/23 05:48 67-66-308/08/23 21:440.0076 0.0063 1
Chloromethane ND mg/kg 08/09/23 05:48 74-87-308/08/23 21:440.015 0.0064 1
2-Chlorotoluene ND mg/kg 08/09/23 05:48 95-49-808/08/23 21:440.0076 0.0027 1
4-Chlorotoluene ND mg/kg 08/09/23 05:48 106-43-408/08/23 21:440.0076 0.0042 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 05:48 96-12-808/08/23 21:440.0076 0.0029 1
Dibromochloromethane ND mg/kg 08/09/23 05:48 124-48-108/08/23 21:440.0076 0.0043 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 05:48 106-93-408/08/23 21:440.0076 0.0033 1
Dibromomethane ND mg/kg 08/09/23 05:48 74-95-308/08/23 21:440.0076 0.0016 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 05:48 95-50-108/08/23 21:440.0076 0.0027 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 05:48 541-73-108/08/23 21:440.0076 0.0023 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 05:48 106-46-708/08/23 21:440.0076 0.0020 1
Dichlorodifluoromethane ND mg/kg 08/09/23 05:48 75-71-808/08/23 21:440.015 0.0077 1
1,1-Dichloroethane ND mg/kg 08/09/23 05:48 75-34-308/08/23 21:440.0076 0.0031 1
1,2-Dichloroethane ND mg/kg 08/09/23 05:48 107-06-208/08/23 21:440.0076 0.0050 1
1,1-Dichloroethene ND mg/kg 08/09/23 05:48 75-35-408/08/23 21:440.0076 0.0031 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 05:48 156-59-208/08/23 21:440.0076 0.0026 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 05:48 156-60-508/08/23 21:440.0076 0.0064 1
1,2-Dichloropropane ND mg/kg 08/09/23 05:48 78-87-508/08/23 21:440.0076 0.0023 1
1,3-Dichloropropane ND mg/kg 08/09/23 05:48 142-28-908/08/23 21:440.0076 0.0024 1
2,2-Dichloropropane ND mg/kg 08/09/23 05:48 594-20-708/08/23 21:440.0076 0.0057 1
1,1-Dichloropropene ND mg/kg 08/09/23 05:48 563-58-608/08/23 21:440.0076 0.0036 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 05:48 10061-01-508/08/23 21:440.0076 0.0021 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 05:48 10061-02-608/08/23 21:440.0076 0.0026 1
Diisopropyl ether ND mg/kg 08/09/23 05:48 108-20-308/08/23 21:440.0076 0.0020 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-5 Lab ID:92681077003 Collected:08/04/23 09:28 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 05:48 100-41-408/08/23 21:440.0076 0.0035 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 05:48 87-68-308/08/23 21:440.015 0.012 1
2-Hexanone ND mg/kg 08/09/23 05:48 591-78-608/08/23 21:440.076 0.0073 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 05:48 98-82-808/08/23 21:440.0076 0.0026 1
p-Isopropyltoluene ND mg/kg 08/09/23 05:48 99-87-608/08/23 21:440.0076 0.0037 1
Methylene Chloride ND mg/kg 08/09/23 05:48 75-09-208/08/23 21:440.030 0.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 05:48 108-10-108/08/23 21:440.076 0.0073 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 05:48 1634-04-408/08/23 21:440.0076 0.0028 1
Naphthalene ND mg/kg 08/09/23 05:48 91-20-308/08/23 21:440.0076 0.0040 1
n-Propylbenzene ND mg/kg 08/09/23 05:48 103-65-108/08/23 21:440.0076 0.0027 1
Styrene ND mg/kg 08/09/23 05:48 100-42-508/08/23 21:440.0076 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 05:48 630-20-608/08/23 21:440.0076 0.0029 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 05:48 79-34-508/08/23 21:440.0076 0.0020 1
Tetrachloroethene 0.043 mg/kg 08/09/23 05:48 127-18-408/08/23 21:440.0076 0.0024 1
Toluene ND mg/kg 08/09/23 05:48 108-88-308/08/23 21:440.0076 0.0052 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 05:48 87-61-608/08/23 21:440.0076 0.0061 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 05:48 120-82-1 IK08/08/23 21:440.0076 0.0064 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 05:48 71-55-608/08/23 21:440.0076 0.0039 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 05:48 79-00-508/08/23 21:440.0076 0.0025 1
Trichloroethene ND mg/kg 08/09/23 05:48 79-01-608/08/23 21:440.0076 0.0061 1
Trichlorofluoromethane ND mg/kg 08/09/23 05:48 75-69-408/08/23 21:440.0076 0.0042 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 05:48 96-18-408/08/23 21:440.0076 0.0038 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 05:48 95-63-608/08/23 21:440.0076 0.0045 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 05:48 108-67-808/08/23 21:440.0076 0.0025 1
Vinyl acetate ND mg/kg 08/09/23 05:48 108-05-408/08/23 21:440.076 0.016 1
Vinyl chloride ND mg/kg 08/09/23 05:48 75-01-408/08/23 21:440.015 0.0039 1
Xylene (Total)ND mg/kg 08/09/23 05:48 1330-20-708/08/23 21:440.015 0.0043 1
m&p-Xylene ND mg/kg 08/09/23 05:48 179601-23-108/08/23 21:440.015 0.0052 1
o-Xylene ND mg/kg 08/09/23 05:48 95-47-608/08/23 21:440.0076 0.0034 1
Surrogates
Toluene-d8 (S)101 %08/09/23 05:48 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)102 %08/09/23 05:48 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)106 %08/09/23 05:48 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.9 %08/08/23 13:36 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 74.2 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-5 Lab ID:92681077003 Collected:08/04/23 09:28 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/14/23 18:52 18540-29-908/13/23 18:151.35 0.344 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-10 Lab ID:92681077004 Collected:08/04/23 09:30 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.05 mg/kg 08/13/23 14:36 7440-38-2 ML,PH08/10/23 09:481.56 0.156 5
Barium 161 mg/kg 08/13/23 14:36 7440-39-3 ML08/10/23 09:483.91 0.238 5
Cadmium 0.260J mg/kg 08/13/23 14:36 7440-43-9 J08/10/23 09:481.56 0.134 5
Chromium 46.9 mg/kg 08/13/23 14:36 7440-47-3 MH08/10/23 09:487.82 0.463 5
Lead 37.3 mg/kg 08/13/23 14:36 7439-92-1 ML08/10/23 09:483.13 0.155 5
Selenium 1.45J mg/kg 08/13/23 14:36 7782-49-2 J,PH08/10/23 09:483.91 0.282 5
Silver ND mg/kg 08/13/23 14:36 7440-22-408/10/23 09:480.782 0.135 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 13:59 7439-97-608/14/23 20:110.0626 0.0282 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 18:37 83-32-908/11/23 15:350.49 0.17 1
Acenaphthylene ND mg/kg 08/13/23 18:37 208-96-808/11/23 15:350.49 0.17 1
Aniline ND mg/kg 08/13/23 18:37 62-53-308/11/23 15:350.49 0.19 1
Anthracene ND mg/kg 08/13/23 18:37 120-12-708/11/23 15:350.49 0.16 1
Benzo(a)anthracene ND mg/kg 08/13/23 18:37 56-55-308/11/23 15:350.49 0.16 1
Benzo(a)pyrene ND mg/kg 08/13/23 18:37 50-32-808/11/23 15:350.49 0.17 1
Benzo(b)fluoranthene ND mg/kg 08/13/23 18:37 205-99-208/11/23 15:350.49 0.16 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 18:37 191-24-208/11/23 15:350.49 0.19 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 18:37 207-08-908/11/23 15:350.49 0.17 1
Benzoic Acid ND mg/kg 08/13/23 18:37 65-85-008/11/23 15:352.4 1.0 1
Benzyl alcohol ND mg/kg 08/13/23 18:37 100-51-608/11/23 15:350.97 0.37 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 18:37 101-55-308/11/23 15:350.49 0.19 1
Butylbenzylphthalate ND mg/kg 08/13/23 18:37 85-68-708/11/23 15:350.49 0.21 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 18:37 59-50-708/11/23 15:350.97 0.34 1
4-Chloroaniline ND mg/kg 08/13/23 18:37 106-47-808/11/23 15:350.97 0.38 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 18:37 111-91-108/11/23 15:350.49 0.20 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 18:37 111-44-408/11/23 15:350.49 0.18 1
2-Chloronaphthalene ND mg/kg 08/13/23 18:37 91-58-708/11/23 15:350.49 0.19 1
2-Chlorophenol ND mg/kg 08/13/23 18:37 95-57-808/11/23 15:350.49 0.18 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 18:37 7005-72-308/11/23 15:350.49 0.18 1
Chrysene ND mg/kg 08/13/23 18:37 218-01-908/11/23 15:350.49 0.18 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 18:37 53-70-308/11/23 15:350.49 0.19 1
Dibenzofuran ND mg/kg 08/13/23 18:37 132-64-908/11/23 15:350.49 0.18 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 18:37 95-50-108/11/23 15:350.49 0.18 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 18:37 541-73-108/11/23 15:350.49 0.17 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 18:37 106-46-708/11/23 15:350.49 0.19 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 18:37 91-94-108/11/23 15:350.97 0.33 1
2,4-Dichlorophenol ND mg/kg 08/13/23 18:37 120-83-208/11/23 15:350.49 0.19 1
Diethylphthalate ND mg/kg 08/13/23 18:37 84-66-208/11/23 15:350.49 0.18 1
2,4-Dimethylphenol ND mg/kg 08/13/23 18:37 105-67-908/11/23 15:350.49 0.20 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-10 Lab ID:92681077004 Collected:08/04/23 09:30 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 18:37 131-11-308/11/23 15:350.49 0.18 1
Di-n-butylphthalate ND mg/kg 08/13/23 18:37 84-74-208/11/23 15:350.49 0.16 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 18:37 534-52-108/11/23 15:350.97 0.45 1
2,4-Dinitrophenol ND mg/kg 08/13/23 18:37 51-28-508/11/23 15:352.4 1.5 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 18:37 121-14-208/11/23 15:350.49 0.19 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 18:37 606-20-208/11/23 15:350.49 0.18 1
Di-n-octylphthalate ND mg/kg 08/13/23 18:37 117-84-008/11/23 15:350.49 0.19 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 18:37 117-81-708/11/23 15:350.49 0.19 1
Fluoranthene ND mg/kg 08/13/23 18:37 206-44-008/11/23 15:350.49 0.17 1
Fluorene ND mg/kg 08/13/23 18:37 86-73-708/11/23 15:350.49 0.17 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 18:37 87-68-308/11/23 15:350.49 0.21 1
Hexachlorobenzene ND mg/kg 08/13/23 18:37 118-74-108/11/23 15:350.49 0.19 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 18:37 77-47-4 v208/11/23 15:350.49 0.28 1
Hexachloroethane ND mg/kg 08/13/23 18:37 67-72-108/11/23 15:350.49 0.19 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 18:37 193-39-508/11/23 15:350.49 0.19 1
Isophorone ND mg/kg 08/13/23 18:37 78-59-108/11/23 15:350.49 0.22 1
1-Methylnaphthalene ND mg/kg 08/13/23 18:37 90-12-008/11/23 15:350.49 0.17 1
2-Methylnaphthalene ND mg/kg 08/13/23 18:37 91-57-608/11/23 15:350.49 0.19 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 18:37 95-48-708/11/23 15:350.49 0.20 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 18:37 15831-10-408/11/23 15:350.49 0.20 1
Naphthalene ND mg/kg 08/13/23 18:37 91-20-308/11/23 15:350.49 0.17 1
2-Nitroaniline ND mg/kg 08/13/23 18:37 88-74-408/11/23 15:352.4 0.40 1
3-Nitroaniline ND mg/kg 08/13/23 18:37 99-09-208/11/23 15:352.4 0.38 1
4-Nitroaniline ND mg/kg 08/13/23 18:37 100-01-608/11/23 15:350.97 0.37 1
Nitrobenzene ND mg/kg 08/13/23 18:37 98-95-308/11/23 15:350.49 0.23 1
2-Nitrophenol ND mg/kg 08/13/23 18:37 88-75-508/11/23 15:350.49 0.21 1
4-Nitrophenol ND mg/kg 08/13/23 18:37 100-02-708/11/23 15:352.4 0.94 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 18:37 62-75-908/11/23 15:350.49 0.16 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 18:37 621-64-708/11/23 15:350.49 0.18 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 18:37 86-30-608/11/23 15:350.49 0.17 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 18:37 108-60-108/11/23 15:350.49 0.23 1
Pentachlorophenol ND mg/kg 08/13/23 18:37 87-86-508/11/23 15:350.97 0.48 1
Phenanthrene ND mg/kg 08/13/23 18:37 85-01-808/11/23 15:350.49 0.16 1
Phenol ND mg/kg 08/13/23 18:37 108-95-208/11/23 15:350.49 0.22 1
Pyrene ND mg/kg 08/13/23 18:37 129-00-008/11/23 15:350.49 0.20 1
Pyridine ND mg/kg 08/13/23 18:37 110-86-108/11/23 15:350.49 0.15 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 18:37 120-82-108/11/23 15:350.49 0.19 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 18:37 95-95-408/11/23 15:350.49 0.22 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 18:37 88-06-208/11/23 15:350.49 0.20 1
Surrogates
Nitrobenzene-d5 (S)76 %08/13/23 18:37 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)54 %08/13/23 18:37 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)37 %08/13/23 18:37 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)65 %08/13/23 18:37 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-10 Lab ID:92681077004 Collected:08/04/23 09:30 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)66 %08/13/23 18:37 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)76 %08/13/23 18:37 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 23:28 67-64-108/09/23 15:460.21 0.067 1
Benzene ND mg/kg 08/09/23 23:28 71-43-208/09/23 15:460.010 0.0042 1
Bromobenzene ND mg/kg 08/09/23 23:28 108-86-108/09/23 15:460.010 0.0034 1
Bromochloromethane ND mg/kg 08/09/23 23:28 74-97-508/09/23 15:460.010 0.0031 1
Bromodichloromethane ND mg/kg 08/09/23 23:28 75-27-408/09/23 15:460.010 0.0041 1
Bromoform ND mg/kg 08/09/23 23:28 75-25-208/09/23 15:460.010 0.0037 1
Bromomethane ND mg/kg 08/09/23 23:28 74-83-908/09/23 15:460.042 0.033 1
2-Butanone (MEK)ND mg/kg 08/09/23 23:28 78-93-308/09/23 15:460.21 0.050 1
n-Butylbenzene ND mg/kg 08/09/23 23:28 104-51-808/09/23 15:460.010 0.0066 1
sec-Butylbenzene ND mg/kg 08/09/23 23:28 135-98-808/09/23 15:460.010 0.0046 1
tert-Butylbenzene ND mg/kg 08/09/23 23:28 98-06-608/09/23 15:460.010 0.0037 1
Carbon tetrachloride ND mg/kg 08/09/23 23:28 56-23-508/09/23 15:460.010 0.0039 1
Chlorobenzene ND mg/kg 08/09/23 23:28 108-90-708/09/23 15:460.010 0.0060 1
Chloroethane ND mg/kg 08/09/23 23:28 75-00-308/09/23 15:460.021 0.0081 1
Chloroform ND mg/kg 08/09/23 23:28 67-66-308/09/23 15:460.010 0.0088 1
Chloromethane ND mg/kg 08/09/23 23:28 74-87-308/09/23 15:460.021 0.0088 1
2-Chlorotoluene ND mg/kg 08/09/23 23:28 95-49-808/09/23 15:460.010 0.0037 1
4-Chlorotoluene ND mg/kg 08/09/23 23:28 106-43-408/09/23 15:460.010 0.0058 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 23:28 96-12-808/09/23 15:460.010 0.0041 1
Dibromochloromethane ND mg/kg 08/09/23 23:28 124-48-108/09/23 15:460.010 0.0059 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 23:28 106-93-408/09/23 15:460.010 0.0046 1
Dibromomethane ND mg/kg 08/09/23 23:28 74-95-308/09/23 15:460.010 0.0022 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 23:28 95-50-108/09/23 15:460.010 0.0038 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 23:28 541-73-108/09/23 15:460.010 0.0033 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 23:28 106-46-708/09/23 15:460.010 0.0027 1
Dichlorodifluoromethane ND mg/kg 08/09/23 23:28 75-71-8 L1,v108/09/23 15:460.021 0.011 1
1,1-Dichloroethane ND mg/kg 08/09/23 23:28 75-34-308/09/23 15:460.010 0.0043 1
1,2-Dichloroethane ND mg/kg 08/09/23 23:28 107-06-208/09/23 15:460.010 0.0069 1
1,1-Dichloroethene ND mg/kg 08/09/23 23:28 75-35-408/09/23 15:460.010 0.0043 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 23:28 156-59-208/09/23 15:460.010 0.0036 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 23:28 156-60-508/09/23 15:460.010 0.0089 1
1,2-Dichloropropane ND mg/kg 08/09/23 23:28 78-87-508/09/23 15:460.010 0.0031 1
1,3-Dichloropropane ND mg/kg 08/09/23 23:28 142-28-908/09/23 15:460.010 0.0033 1
2,2-Dichloropropane ND mg/kg 08/09/23 23:28 594-20-708/09/23 15:460.010 0.0080 1
1,1-Dichloropropene ND mg/kg 08/09/23 23:28 563-58-608/09/23 15:460.010 0.0050 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 23:28 10061-01-508/09/23 15:460.010 0.0029 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 23:28 10061-02-608/09/23 15:460.010 0.0036 1
Diisopropyl ether ND mg/kg 08/09/23 23:28 108-20-308/09/23 15:460.010 0.0028 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-10 Lab ID:92681077004 Collected:08/04/23 09:30 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 23:28 100-41-408/09/23 15:460.010 0.0049 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 23:28 87-68-308/09/23 15:460.021 0.017 1
2-Hexanone ND mg/kg 08/09/23 23:28 591-78-608/09/23 15:460.10 0.010 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 23:28 98-82-808/09/23 15:460.010 0.0036 1
p-Isopropyltoluene ND mg/kg 08/09/23 23:28 99-87-608/09/23 15:460.010 0.0052 1
Methylene Chloride ND mg/kg 08/09/23 23:28 75-09-208/09/23 15:460.042 0.029 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 23:28 108-10-108/09/23 15:460.10 0.010 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 23:28 1634-04-408/09/23 15:460.010 0.0039 1
Naphthalene ND mg/kg 08/09/23 23:28 91-20-308/09/23 15:460.010 0.0055 1
n-Propylbenzene ND mg/kg 08/09/23 23:28 103-65-108/09/23 15:460.010 0.0037 1
Styrene ND mg/kg 08/09/23 23:28 100-42-508/09/23 15:460.010 0.0028 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 23:28 630-20-608/09/23 15:460.010 0.0040 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 23:28 79-34-508/09/23 15:460.010 0.0028 1
Tetrachloroethene 0.021 mg/kg 08/09/23 23:28 127-18-408/09/23 15:460.010 0.0033 1
Toluene ND mg/kg 08/09/23 23:28 108-88-308/09/23 15:460.010 0.0072 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 23:28 87-61-608/09/23 15:460.010 0.0085 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 23:28 120-82-108/09/23 15:460.010 0.0088 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 23:28 71-55-608/09/23 15:460.010 0.0055 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 23:28 79-00-508/09/23 15:460.010 0.0035 1
Trichloroethene ND mg/kg 08/09/23 23:28 79-01-608/09/23 15:460.010 0.0085 1
Trichlorofluoromethane ND mg/kg 08/09/23 23:28 75-69-408/09/23 15:460.010 0.0058 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 23:28 96-18-408/09/23 15:460.010 0.0053 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 23:28 95-63-608/09/23 15:460.010 0.0062 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 23:28 108-67-808/09/23 15:460.010 0.0035 1
Vinyl acetate ND mg/kg 08/09/23 23:28 108-05-408/09/23 15:460.10 0.022 1
Vinyl chloride ND mg/kg 08/09/23 23:28 75-01-408/09/23 15:460.021 0.0053 1
Xylene (Total)ND mg/kg 08/09/23 23:28 1330-20-708/09/23 15:460.021 0.0060 1
m&p-Xylene ND mg/kg 08/09/23 23:28 179601-23-108/09/23 15:460.021 0.0072 1
o-Xylene ND mg/kg 08/09/23 23:28 95-47-608/09/23 15:460.010 0.0046 1
Surrogates
Toluene-d8 (S)101 %08/09/23 23:28 2037-26-508/09/23 15:4670-130 1
4-Bromofluorobenzene (S)99 %08/09/23 23:28 460-00-408/09/23 15:4670-130 1
1,2-Dichloroethane-d4 (S)109 %08/09/23 23:28 17060-07-008/09/23 15:4670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 33.2 %08/08/23 13:36 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 63.9 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E2-10 Lab ID:92681077004 Collected:08/04/23 09:30 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.09 mg/kg 08/14/23 19:13 18540-29-908/13/23 18:151.56 0.399 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-5 Lab ID:92681077005 Collected:08/04/23 09:41 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.87 mg/kg 08/13/23 16:27 7440-38-208/10/23 09:481.24 0.124 5
Barium 62.8 mg/kg 08/13/23 16:27 7440-39-308/10/23 09:483.09 0.188 5
Cadmium 0.543J mg/kg 08/13/23 16:27 7440-43-9 J08/10/23 09:481.24 0.106 5
Chromium 39.0 mg/kg 08/13/23 16:27 7440-47-308/10/23 09:486.19 0.366 5
Lead 67.6 mg/kg 08/13/23 16:27 7439-92-108/10/23 09:482.48 0.123 5
Selenium 0.582J mg/kg 08/13/23 16:27 7782-49-2 J08/10/23 09:483.09 0.223 5
Silver ND mg/kg 08/13/23 16:27 7440-22-408/10/23 09:480.619 0.107 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0971 mg/kg 08/15/23 14:02 7439-97-608/14/23 20:110.0495 0.0223 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene 0.64 mg/kg 08/13/23 19:05 83-32-908/11/23 15:350.42 0.15 1
Acenaphthylene ND mg/kg 08/13/23 19:05 208-96-808/11/23 15:350.42 0.15 1
Aniline ND mg/kg 08/13/23 19:05 62-53-308/11/23 15:350.42 0.17 1
Anthracene 0.81 mg/kg 08/13/23 19:05 120-12-708/11/23 15:350.42 0.14 1
Benzo(a)anthracene 1.6 mg/kg 08/13/23 19:05 56-55-308/11/23 15:350.42 0.14 1
Benzo(a)pyrene 1.7 mg/kg 08/13/23 19:05 50-32-808/11/23 15:350.42 0.15 1
Benzo(b)fluoranthene 2.4 mg/kg 08/13/23 19:05 205-99-208/11/23 15:350.42 0.14 1
Benzo(g,h,i)perylene 1.1 mg/kg 08/13/23 19:05 191-24-208/11/23 15:350.42 0.16 1
Benzo(k)fluoranthene 0.88 mg/kg 08/13/23 19:05 207-08-908/11/23 15:350.42 0.15 1
Benzoic Acid ND mg/kg 08/13/23 19:05 65-85-008/11/23 15:352.1 0.91 1
Benzyl alcohol ND mg/kg 08/13/23 19:05 100-51-608/11/23 15:350.85 0.32 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 19:05 101-55-308/11/23 15:350.42 0.16 1
Butylbenzylphthalate 47.0 mg/kg 08/14/23 16:14 85-68-708/11/23 15:358.5 3.6 20
4-Chloro-3-methylphenol ND mg/kg 08/13/23 19:05 59-50-708/11/23 15:350.85 0.30 1
4-Chloroaniline ND mg/kg 08/13/23 19:05 106-47-808/11/23 15:350.85 0.33 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 19:05 111-91-108/11/23 15:350.42 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 19:05 111-44-408/11/23 15:350.42 0.16 1
2-Chloronaphthalene ND mg/kg 08/13/23 19:05 91-58-708/11/23 15:350.42 0.17 1
2-Chlorophenol ND mg/kg 08/13/23 19:05 95-57-808/11/23 15:350.42 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 19:05 7005-72-308/11/23 15:350.42 0.16 1
Chrysene 1.7 mg/kg 08/13/23 19:05 218-01-908/11/23 15:350.42 0.15 1
Dibenz(a,h)anthracene 0.31J mg/kg 08/13/23 19:05 53-70-308/11/23 15:350.42 0.16 1
Dibenzofuran 0.24J mg/kg 08/13/23 19:05 132-64-908/11/23 15:350.42 0.15 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 19:05 95-50-108/11/23 15:350.42 0.15 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 19:05 541-73-108/11/23 15:350.42 0.15 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 19:05 106-46-708/11/23 15:350.42 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 19:05 91-94-108/11/23 15:350.85 0.29 1
2,4-Dichlorophenol ND mg/kg 08/13/23 19:05 120-83-208/11/23 15:350.42 0.17 1
Diethylphthalate ND mg/kg 08/13/23 19:05 84-66-208/11/23 15:350.42 0.16 1
2,4-Dimethylphenol ND mg/kg 08/13/23 19:05 105-67-908/11/23 15:350.42 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-5 Lab ID:92681077005 Collected:08/04/23 09:41 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 19:05 131-11-308/11/23 15:350.42 0.15 1
Di-n-butylphthalate ND mg/kg 08/13/23 19:05 84-74-208/11/23 15:350.42 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 19:05 534-52-108/11/23 15:350.85 0.40 1
2,4-Dinitrophenol ND mg/kg 08/13/23 19:05 51-28-508/11/23 15:352.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 19:05 121-14-208/11/23 15:350.42 0.16 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 19:05 606-20-208/11/23 15:350.42 0.16 1
Di-n-octylphthalate ND mg/kg 08/13/23 19:05 117-84-008/11/23 15:350.42 0.17 1
bis(2-Ethylhexyl)phthalate 0.22J mg/kg 08/13/23 19:05 117-81-708/11/23 15:350.42 0.16 1
Fluoranthene 3.9 mg/kg 08/13/23 19:05 206-44-008/11/23 15:350.42 0.15 1
Fluorene 0.56 mg/kg 08/13/23 19:05 86-73-708/11/23 15:350.42 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 19:05 87-68-308/11/23 15:350.42 0.18 1
Hexachlorobenzene ND mg/kg 08/13/23 19:05 118-74-108/11/23 15:350.42 0.17 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 19:05 77-47-4 v208/11/23 15:350.42 0.24 1
Hexachloroethane ND mg/kg 08/13/23 19:05 67-72-108/11/23 15:350.42 0.16 1
Indeno(1,2,3-cd)pyrene 0.91 mg/kg 08/13/23 19:05 193-39-508/11/23 15:350.42 0.17 1
Isophorone ND mg/kg 08/13/23 19:05 78-59-108/11/23 15:350.42 0.19 1
1-Methylnaphthalene ND mg/kg 08/13/23 19:05 90-12-008/11/23 15:350.42 0.15 1
2-Methylnaphthalene 0.17J mg/kg 08/13/23 19:05 91-57-608/11/23 15:350.42 0.17 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 19:05 95-48-708/11/23 15:350.42 0.17 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 19:05 15831-10-408/11/23 15:350.42 0.17 1
Naphthalene 0.38J mg/kg 08/13/23 19:05 91-20-308/11/23 15:350.42 0.14 1
2-Nitroaniline ND mg/kg 08/13/23 19:05 88-74-408/11/23 15:352.1 0.35 1
3-Nitroaniline ND mg/kg 08/13/23 19:05 99-09-208/11/23 15:352.1 0.33 1
4-Nitroaniline ND mg/kg 08/13/23 19:05 100-01-608/11/23 15:350.85 0.32 1
Nitrobenzene ND mg/kg 08/13/23 19:05 98-95-308/11/23 15:350.42 0.20 1
2-Nitrophenol ND mg/kg 08/13/23 19:05 88-75-508/11/23 15:350.42 0.18 1
4-Nitrophenol ND mg/kg 08/13/23 19:05 100-02-708/11/23 15:352.1 0.82 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 19:05 62-75-908/11/23 15:350.42 0.14 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 19:05 621-64-708/11/23 15:350.42 0.16 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 19:05 86-30-608/11/23 15:350.42 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 19:05 108-60-108/11/23 15:350.42 0.20 1
Pentachlorophenol ND mg/kg 08/13/23 19:05 87-86-508/11/23 15:350.85 0.41 1
Phenanthrene 3.3 mg/kg 08/13/23 19:05 85-01-808/11/23 15:350.42 0.14 1
Phenol ND mg/kg 08/13/23 19:05 108-95-208/11/23 15:350.42 0.19 1
Pyrene 2.7 mg/kg 08/13/23 19:05 129-00-008/11/23 15:350.42 0.17 1
Pyridine ND mg/kg 08/13/23 19:05 110-86-108/11/23 15:350.42 0.13 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 19:05 120-82-108/11/23 15:350.42 0.17 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 19:05 95-95-408/11/23 15:350.42 0.19 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 19:05 88-06-208/11/23 15:350.42 0.17 1
Surrogates
Nitrobenzene-d5 (S)71 %08/13/23 19:05 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)67 %08/13/23 19:05 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)73 %08/13/23 19:05 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)67 %08/13/23 19:05 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-5 Lab ID:92681077005 Collected:08/04/23 09:41 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)67 %08/13/23 19:05 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)95 %08/13/23 19:05 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 0.093J mg/kg 08/09/23 06:22 67-64-108/08/23 21:440.16 0.051 1
Benzene 0.0079 mg/kg 08/09/23 06:22 71-43-208/08/23 21:440.0079 0.0031 1
Bromobenzene ND mg/kg 08/09/23 06:22 108-86-108/08/23 21:440.0079 0.0026 1
Bromochloromethane ND mg/kg 08/09/23 06:22 74-97-508/08/23 21:440.0079 0.0023 1
Bromodichloromethane ND mg/kg 08/09/23 06:22 75-27-408/08/23 21:440.0079 0.0030 1
Bromoform ND mg/kg 08/09/23 06:22 75-25-208/08/23 21:440.0079 0.0028 1
Bromomethane ND mg/kg 08/09/23 06:22 74-83-9 v208/08/23 21:440.031 0.024 1
2-Butanone (MEK)0.046J mg/kg 08/09/23 06:22 78-93-308/08/23 21:440.16 0.038 1
n-Butylbenzene ND mg/kg 08/09/23 06:22 104-51-808/08/23 21:440.0079 0.0050 1
sec-Butylbenzene ND mg/kg 08/09/23 06:22 135-98-808/08/23 21:440.0079 0.0035 1
tert-Butylbenzene ND mg/kg 08/09/23 06:22 98-06-608/08/23 21:440.0079 0.0028 1
Carbon tetrachloride ND mg/kg 08/09/23 06:22 56-23-508/08/23 21:440.0079 0.0029 1
Chlorobenzene ND mg/kg 08/09/23 06:22 108-90-708/08/23 21:440.0079 0.0045 1
Chloroethane ND mg/kg 08/09/23 06:22 75-00-308/08/23 21:440.016 0.0061 1
Chloroform ND mg/kg 08/09/23 06:22 67-66-308/08/23 21:440.0079 0.0066 1
Chloromethane ND mg/kg 08/09/23 06:22 74-87-308/08/23 21:440.016 0.0066 1
2-Chlorotoluene ND mg/kg 08/09/23 06:22 95-49-808/08/23 21:440.0079 0.0028 1
4-Chlorotoluene ND mg/kg 08/09/23 06:22 106-43-408/08/23 21:440.0079 0.0044 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 06:22 96-12-808/08/23 21:440.0079 0.0031 1
Dibromochloromethane ND mg/kg 08/09/23 06:22 124-48-108/08/23 21:440.0079 0.0044 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 06:22 106-93-408/08/23 21:440.0079 0.0035 1
Dibromomethane ND mg/kg 08/09/23 06:22 74-95-308/08/23 21:440.0079 0.0017 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 06:22 95-50-108/08/23 21:440.0079 0.0028 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 06:22 541-73-108/08/23 21:440.0079 0.0024 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 06:22 106-46-708/08/23 21:440.0079 0.0020 1
Dichlorodifluoromethane ND mg/kg 08/09/23 06:22 75-71-808/08/23 21:440.016 0.0080 1
1,1-Dichloroethane ND mg/kg 08/09/23 06:22 75-34-308/08/23 21:440.0079 0.0032 1
1,2-Dichloroethane ND mg/kg 08/09/23 06:22 107-06-208/08/23 21:440.0079 0.0052 1
1,1-Dichloroethene ND mg/kg 08/09/23 06:22 75-35-408/08/23 21:440.0079 0.0032 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 06:22 156-59-208/08/23 21:440.0079 0.0027 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 06:22 156-60-508/08/23 21:440.0079 0.0067 1
1,2-Dichloropropane ND mg/kg 08/09/23 06:22 78-87-508/08/23 21:440.0079 0.0024 1
1,3-Dichloropropane ND mg/kg 08/09/23 06:22 142-28-908/08/23 21:440.0079 0.0025 1
2,2-Dichloropropane ND mg/kg 08/09/23 06:22 594-20-708/08/23 21:440.0079 0.0060 1
1,1-Dichloropropene ND mg/kg 08/09/23 06:22 563-58-608/08/23 21:440.0079 0.0038 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 06:22 10061-01-508/08/23 21:440.0079 0.0021 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 06:22 10061-02-608/08/23 21:440.0079 0.0027 1
Diisopropyl ether ND mg/kg 08/09/23 06:22 108-20-308/08/23 21:440.0079 0.0021 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-5 Lab ID:92681077005 Collected:08/04/23 09:41 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 06:22 100-41-408/08/23 21:440.0079 0.0037 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 06:22 87-68-308/08/23 21:440.016 0.013 1
2-Hexanone ND mg/kg 08/09/23 06:22 591-78-608/08/23 21:440.079 0.0076 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 06:22 98-82-808/08/23 21:440.0079 0.0027 1
p-Isopropyltoluene ND mg/kg 08/09/23 06:22 99-87-608/08/23 21:440.0079 0.0039 1
Methylene Chloride ND mg/kg 08/09/23 06:22 75-09-208/08/23 21:440.031 0.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 06:22 108-10-108/08/23 21:440.079 0.0076 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 06:22 1634-04-408/08/23 21:440.0079 0.0029 1
Naphthalene 0.26 mg/kg 08/09/23 06:22 91-20-308/08/23 21:440.0079 0.0041 1
n-Propylbenzene ND mg/kg 08/09/23 06:22 103-65-108/08/23 21:440.0079 0.0028 1
Styrene ND mg/kg 08/09/23 06:22 100-42-508/08/23 21:440.0079 0.0021 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 06:22 630-20-608/08/23 21:440.0079 0.0030 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 06:22 79-34-508/08/23 21:440.0079 0.0021 1
Tetrachloroethene 0.12 mg/kg 08/09/23 06:22 127-18-408/08/23 21:440.0079 0.0025 1
Toluene 0.0074J mg/kg 08/09/23 06:22 108-88-308/08/23 21:440.0079 0.0054 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 06:22 87-61-608/08/23 21:440.0079 0.0064 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 06:22 120-82-1 IK08/08/23 21:440.0079 0.0066 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 06:22 71-55-608/08/23 21:440.0079 0.0041 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 06:22 79-00-508/08/23 21:440.0079 0.0026 1
Trichloroethene 0.037 mg/kg 08/09/23 06:22 79-01-608/08/23 21:440.0079 0.0063 1
Trichlorofluoromethane ND mg/kg 08/09/23 06:22 75-69-408/08/23 21:440.0079 0.0043 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 06:22 96-18-408/08/23 21:440.0079 0.0040 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 06:22 95-63-608/08/23 21:440.0079 0.0047 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 06:22 108-67-808/08/23 21:440.0079 0.0026 1
Vinyl acetate ND mg/kg 08/09/23 06:22 108-05-408/08/23 21:440.079 0.016 1
Vinyl chloride ND mg/kg 08/09/23 06:22 75-01-408/08/23 21:440.016 0.0040 1
Xylene (Total)ND mg/kg 08/09/23 06:22 1330-20-708/08/23 21:440.016 0.0045 1
m&p-Xylene ND mg/kg 08/09/23 06:22 179601-23-108/08/23 21:440.016 0.0054 1
o-Xylene ND mg/kg 08/09/23 06:22 95-47-608/08/23 21:440.0079 0.0035 1
Surrogates
Toluene-d8 (S)99 %08/09/23 06:22 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)105 %08/09/23 06:22 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)107 %08/09/23 06:22 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.3 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.8 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-5 Lab ID:92681077005 Collected:08/04/23 09:41 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/14/23 19:18 18540-29-908/13/23 18:151.24 0.316 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-10 Lab ID:92681077006 Collected:08/04/23 09:45 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.656J mg/kg 08/13/23 16:31 7440-38-2 J08/10/23 09:481.40 0.140 5
Barium 20.6 mg/kg 08/13/23 16:31 7440-39-308/10/23 09:483.49 0.212 5
Cadmium ND mg/kg 08/13/23 16:31 7440-43-908/10/23 09:481.40 0.119 5
Chromium 9.80 mg/kg 08/13/23 16:31 7440-47-308/10/23 09:486.98 0.413 5
Lead 1.60J mg/kg 08/13/23 16:31 7439-92-1 J08/10/23 09:482.79 0.138 5
Selenium 0.296J mg/kg 08/13/23 16:31 7782-49-2 J08/10/23 09:483.49 0.251 5
Silver ND mg/kg 08/13/23 16:31 7440-22-408/10/23 09:480.698 0.121 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 14:04 7439-97-608/14/23 20:110.0559 0.0251 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 19:33 83-32-908/11/23 15:350.44 0.15 1
Acenaphthylene ND mg/kg 08/13/23 19:33 208-96-808/11/23 15:350.44 0.15 1
Aniline ND mg/kg 08/13/23 19:33 62-53-308/11/23 15:350.44 0.17 1
Anthracene ND mg/kg 08/13/23 19:33 120-12-708/11/23 15:350.44 0.14 1
Benzo(a)anthracene ND mg/kg 08/13/23 19:33 56-55-308/11/23 15:350.44 0.15 1
Benzo(a)pyrene ND mg/kg 08/13/23 19:33 50-32-808/11/23 15:350.44 0.15 1
Benzo(b)fluoranthene ND mg/kg 08/13/23 19:33 205-99-208/11/23 15:350.44 0.15 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 19:33 191-24-208/11/23 15:350.44 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 19:33 207-08-908/11/23 15:350.44 0.15 1
Benzoic Acid ND mg/kg 08/13/23 19:33 65-85-008/11/23 15:352.2 0.94 1
Benzyl alcohol ND mg/kg 08/13/23 19:33 100-51-608/11/23 15:350.87 0.33 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 19:33 101-55-308/11/23 15:350.44 0.17 1
Butylbenzylphthalate ND mg/kg 08/13/23 19:33 85-68-708/11/23 15:350.44 0.18 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 19:33 59-50-708/11/23 15:350.87 0.31 1
4-Chloroaniline ND mg/kg 08/13/23 19:33 106-47-808/11/23 15:350.87 0.34 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 19:33 111-91-108/11/23 15:350.44 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 19:33 111-44-408/11/23 15:350.44 0.16 1
2-Chloronaphthalene ND mg/kg 08/13/23 19:33 91-58-708/11/23 15:350.44 0.17 1
2-Chlorophenol ND mg/kg 08/13/23 19:33 95-57-808/11/23 15:350.44 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 19:33 7005-72-308/11/23 15:350.44 0.16 1
Chrysene ND mg/kg 08/13/23 19:33 218-01-908/11/23 15:350.44 0.16 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 19:33 53-70-308/11/23 15:350.44 0.17 1
Dibenzofuran ND mg/kg 08/13/23 19:33 132-64-908/11/23 15:350.44 0.16 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 19:33 95-50-108/11/23 15:350.44 0.16 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 19:33 541-73-108/11/23 15:350.44 0.15 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 19:33 106-46-708/11/23 15:350.44 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 19:33 91-94-108/11/23 15:350.87 0.29 1
2,4-Dichlorophenol ND mg/kg 08/13/23 19:33 120-83-208/11/23 15:350.44 0.17 1
Diethylphthalate ND mg/kg 08/13/23 19:33 84-66-208/11/23 15:350.44 0.16 1
2,4-Dimethylphenol ND mg/kg 08/13/23 19:33 105-67-908/11/23 15:350.44 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-10 Lab ID:92681077006 Collected:08/04/23 09:45 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 19:33 131-11-308/11/23 15:350.44 0.16 1
Di-n-butylphthalate ND mg/kg 08/13/23 19:33 84-74-208/11/23 15:350.44 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 19:33 534-52-108/11/23 15:350.87 0.41 1
2,4-Dinitrophenol ND mg/kg 08/13/23 19:33 51-28-508/11/23 15:352.2 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 19:33 121-14-208/11/23 15:350.44 0.17 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 19:33 606-20-208/11/23 15:350.44 0.16 1
Di-n-octylphthalate ND mg/kg 08/13/23 19:33 117-84-008/11/23 15:350.44 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 19:33 117-81-708/11/23 15:350.44 0.17 1
Fluoranthene ND mg/kg 08/13/23 19:33 206-44-008/11/23 15:350.44 0.15 1
Fluorene ND mg/kg 08/13/23 19:33 86-73-708/11/23 15:350.44 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 19:33 87-68-308/11/23 15:350.44 0.19 1
Hexachlorobenzene ND mg/kg 08/13/23 19:33 118-74-108/11/23 15:350.44 0.17 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 19:33 77-47-4 v208/11/23 15:350.44 0.25 1
Hexachloroethane ND mg/kg 08/13/23 19:33 67-72-108/11/23 15:350.44 0.17 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 19:33 193-39-508/11/23 15:350.44 0.17 1
Isophorone ND mg/kg 08/13/23 19:33 78-59-108/11/23 15:350.44 0.19 1
1-Methylnaphthalene ND mg/kg 08/13/23 19:33 90-12-008/11/23 15:350.44 0.15 1
2-Methylnaphthalene ND mg/kg 08/13/23 19:33 91-57-608/11/23 15:350.44 0.17 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 19:33 95-48-708/11/23 15:350.44 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 19:33 15831-10-408/11/23 15:350.44 0.18 1
Naphthalene ND mg/kg 08/13/23 19:33 91-20-308/11/23 15:350.44 0.15 1
2-Nitroaniline ND mg/kg 08/13/23 19:33 88-74-408/11/23 15:352.2 0.36 1
3-Nitroaniline ND mg/kg 08/13/23 19:33 99-09-208/11/23 15:352.2 0.34 1
4-Nitroaniline ND mg/kg 08/13/23 19:33 100-01-608/11/23 15:350.87 0.33 1
Nitrobenzene ND mg/kg 08/13/23 19:33 98-95-308/11/23 15:350.44 0.20 1
2-Nitrophenol ND mg/kg 08/13/23 19:33 88-75-508/11/23 15:350.44 0.19 1
4-Nitrophenol ND mg/kg 08/13/23 19:33 100-02-708/11/23 15:352.2 0.84 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 19:33 62-75-908/11/23 15:350.44 0.15 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 19:33 621-64-708/11/23 15:350.44 0.16 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 19:33 86-30-608/11/23 15:350.44 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 19:33 108-60-108/11/23 15:350.44 0.21 1
Pentachlorophenol ND mg/kg 08/13/23 19:33 87-86-508/11/23 15:350.87 0.43 1
Phenanthrene ND mg/kg 08/13/23 19:33 85-01-808/11/23 15:350.44 0.14 1
Phenol ND mg/kg 08/13/23 19:33 108-95-208/11/23 15:350.44 0.19 1
Pyrene ND mg/kg 08/13/23 19:33 129-00-008/11/23 15:350.44 0.18 1
Pyridine ND mg/kg 08/13/23 19:33 110-86-108/11/23 15:350.44 0.14 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 19:33 120-82-108/11/23 15:350.44 0.17 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 19:33 95-95-408/11/23 15:350.44 0.20 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 19:33 88-06-208/11/23 15:350.44 0.18 1
Surrogates
Nitrobenzene-d5 (S)73 %08/13/23 19:33 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)66 %08/13/23 19:33 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)54 %08/13/23 19:33 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)69 %08/13/23 19:33 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-10 Lab ID:92681077006 Collected:08/04/23 09:45 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)70 %08/13/23 19:33 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)105 %08/13/23 19:33 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 06:40 67-64-108/08/23 21:440.16 0.051 1
Benzene ND mg/kg 08/09/23 06:40 71-43-208/08/23 21:440.0080 0.0032 1
Bromobenzene ND mg/kg 08/09/23 06:40 108-86-108/08/23 21:440.0080 0.0026 1
Bromochloromethane ND mg/kg 08/09/23 06:40 74-97-508/08/23 21:440.0080 0.0024 1
Bromodichloromethane ND mg/kg 08/09/23 06:40 75-27-408/08/23 21:440.0080 0.0031 1
Bromoform ND mg/kg 08/09/23 06:40 75-25-208/08/23 21:440.0080 0.0028 1
Bromomethane ND mg/kg 08/09/23 06:40 74-83-9 v208/08/23 21:440.032 0.025 1
2-Butanone (MEK)ND mg/kg 08/09/23 06:40 78-93-308/08/23 21:440.16 0.038 1
n-Butylbenzene ND mg/kg 08/09/23 06:40 104-51-808/08/23 21:440.0080 0.0050 1
sec-Butylbenzene ND mg/kg 08/09/23 06:40 135-98-808/08/23 21:440.0080 0.0035 1
tert-Butylbenzene ND mg/kg 08/09/23 06:40 98-06-608/08/23 21:440.0080 0.0028 1
Carbon tetrachloride ND mg/kg 08/09/23 06:40 56-23-508/08/23 21:440.0080 0.0030 1
Chlorobenzene ND mg/kg 08/09/23 06:40 108-90-708/08/23 21:440.0080 0.0046 1
Chloroethane ND mg/kg 08/09/23 06:40 75-00-308/08/23 21:440.016 0.0062 1
Chloroform ND mg/kg 08/09/23 06:40 67-66-308/08/23 21:440.0080 0.0067 1
Chloromethane ND mg/kg 08/09/23 06:40 74-87-308/08/23 21:440.016 0.0067 1
2-Chlorotoluene ND mg/kg 08/09/23 06:40 95-49-808/08/23 21:440.0080 0.0028 1
4-Chlorotoluene ND mg/kg 08/09/23 06:40 106-43-408/08/23 21:440.0080 0.0044 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 06:40 96-12-808/08/23 21:440.0080 0.0031 1
Dibromochloromethane ND mg/kg 08/09/23 06:40 124-48-108/08/23 21:440.0080 0.0045 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 06:40 106-93-408/08/23 21:440.0080 0.0035 1
Dibromomethane ND mg/kg 08/09/23 06:40 74-95-308/08/23 21:440.0080 0.0017 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 06:40 95-50-108/08/23 21:440.0080 0.0029 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 06:40 541-73-108/08/23 21:440.0080 0.0025 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 06:40 106-46-708/08/23 21:440.0080 0.0021 1
Dichlorodifluoromethane ND mg/kg 08/09/23 06:40 75-71-808/08/23 21:440.016 0.0081 1
1,1-Dichloroethane ND mg/kg 08/09/23 06:40 75-34-308/08/23 21:440.0080 0.0033 1
1,2-Dichloroethane ND mg/kg 08/09/23 06:40 107-06-208/08/23 21:440.0080 0.0053 1
1,1-Dichloroethene ND mg/kg 08/09/23 06:40 75-35-408/08/23 21:440.0080 0.0033 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 06:40 156-59-208/08/23 21:440.0080 0.0027 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 06:40 156-60-508/08/23 21:440.0080 0.0068 1
1,2-Dichloropropane ND mg/kg 08/09/23 06:40 78-87-508/08/23 21:440.0080 0.0024 1
1,3-Dichloropropane ND mg/kg 08/09/23 06:40 142-28-908/08/23 21:440.0080 0.0025 1
2,2-Dichloropropane ND mg/kg 08/09/23 06:40 594-20-708/08/23 21:440.0080 0.0061 1
1,1-Dichloropropene ND mg/kg 08/09/23 06:40 563-58-608/08/23 21:440.0080 0.0038 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 06:40 10061-01-508/08/23 21:440.0080 0.0022 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 06:40 10061-02-608/08/23 21:440.0080 0.0027 1
Diisopropyl ether ND mg/kg 08/09/23 06:40 108-20-308/08/23 21:440.0080 0.0022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-10 Lab ID:92681077006 Collected:08/04/23 09:45 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 06:40 100-41-408/08/23 21:440.0080 0.0037 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 06:40 87-68-308/08/23 21:440.016 0.013 1
2-Hexanone ND mg/kg 08/09/23 06:40 591-78-608/08/23 21:440.080 0.0077 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 06:40 98-82-808/08/23 21:440.0080 0.0027 1
p-Isopropyltoluene ND mg/kg 08/09/23 06:40 99-87-608/08/23 21:440.0080 0.0039 1
Methylene Chloride 0.024J mg/kg 08/09/23 06:40 75-09-2 C908/08/23 21:440.032 0.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 06:40 108-10-108/08/23 21:440.080 0.0077 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 06:40 1634-04-408/08/23 21:440.0080 0.0030 1
Naphthalene 0.0070J mg/kg 08/09/23 06:40 91-20-308/08/23 21:440.0080 0.0042 1
n-Propylbenzene ND mg/kg 08/09/23 06:40 103-65-108/08/23 21:440.0080 0.0028 1
Styrene ND mg/kg 08/09/23 06:40 100-42-508/08/23 21:440.0080 0.0021 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 06:40 630-20-608/08/23 21:440.0080 0.0031 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 06:40 79-34-508/08/23 21:440.0080 0.0021 1
Tetrachloroethene ND mg/kg 08/09/23 06:40 127-18-408/08/23 21:440.0080 0.0025 1
Toluene ND mg/kg 08/09/23 06:40 108-88-308/08/23 21:440.0080 0.0055 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 06:40 87-61-608/08/23 21:440.0080 0.0065 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 06:40 120-82-1 IK08/08/23 21:440.0080 0.0067 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 06:40 71-55-608/08/23 21:440.0080 0.0042 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 06:40 79-00-508/08/23 21:440.0080 0.0027 1
Trichloroethene ND mg/kg 08/09/23 06:40 79-01-608/08/23 21:440.0080 0.0064 1
Trichlorofluoromethane ND mg/kg 08/09/23 06:40 75-69-408/08/23 21:440.0080 0.0044 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 06:40 96-18-408/08/23 21:440.0080 0.0040 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 06:40 95-63-608/08/23 21:440.0080 0.0047 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 06:40 108-67-808/08/23 21:440.0080 0.0027 1
Vinyl acetate ND mg/kg 08/09/23 06:40 108-05-408/08/23 21:440.080 0.016 1
Vinyl chloride ND mg/kg 08/09/23 06:40 75-01-408/08/23 21:440.016 0.0041 1
Xylene (Total)ND mg/kg 08/09/23 06:40 1330-20-708/08/23 21:440.016 0.0046 1
m&p-Xylene ND mg/kg 08/09/23 06:40 179601-23-108/08/23 21:440.016 0.0055 1
o-Xylene ND mg/kg 08/09/23 06:40 95-47-608/08/23 21:440.0080 0.0035 1
Surrogates
Toluene-d8 (S)102 %08/09/23 06:40 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)104 %08/09/23 06:40 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)106 %08/09/23 06:40 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.6 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.6 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:E1-10 Lab ID:92681077006 Collected:08/04/23 09:45 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/14/23 19:24 18540-29-908/13/23 18:151.40 0.356 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-5 Lab ID:92681077007 Collected:08/04/23 09:54 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.48 mg/kg 08/13/23 16:34 7440-38-208/10/23 09:481.20 0.120 5
Barium 104 mg/kg 08/13/23 16:34 7440-39-308/10/23 09:483.00 0.182 5
Cadmium ND mg/kg 08/13/23 16:34 7440-43-908/10/23 09:481.20 0.102 5
Chromium 44.4 mg/kg 08/13/23 16:34 7440-47-308/10/23 09:485.99 0.355 5
Lead 21.2 mg/kg 08/13/23 16:34 7439-92-108/10/23 09:482.40 0.119 5
Selenium 0.873J mg/kg 08/13/23 16:34 7782-49-2 J08/10/23 09:483.00 0.216 5
Silver ND mg/kg 08/13/23 16:34 7440-22-408/10/23 09:480.599 0.104 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0398J mg/kg 08/15/23 14:07 7439-97-6 J08/14/23 20:110.0479 0.0216 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene 2.3 mg/kg 08/13/23 20:00 83-32-908/11/23 15:350.39 0.14 1
Acenaphthylene ND mg/kg 08/13/23 20:00 208-96-808/11/23 15:350.39 0.14 1
Aniline ND mg/kg 08/13/23 20:00 62-53-308/11/23 15:350.39 0.15 1
Anthracene 3.5 mg/kg 08/13/23 20:00 120-12-708/11/23 15:350.39 0.13 1
Benzo(a)anthracene 5.5 mg/kg 08/14/23 14:21 56-55-308/11/23 15:352.0 0.66 5
Benzo(a)pyrene 5.7 mg/kg 08/14/23 14:21 50-32-808/11/23 15:352.0 0.68 5
Benzo(b)fluoranthene 6.9 mg/kg 08/14/23 14:21 205-99-208/11/23 15:352.0 0.66 5
Benzo(g,h,i)perylene 3.8 mg/kg 08/13/23 20:00 191-24-208/11/23 15:350.39 0.15 1
Benzo(k)fluoranthene 2.7 mg/kg 08/13/23 20:00 207-08-908/11/23 15:350.39 0.14 1
Benzoic Acid ND mg/kg 08/13/23 20:00 65-85-008/11/23 15:352.0 0.85 1
Benzyl alcohol ND mg/kg 08/13/23 20:00 100-51-608/11/23 15:350.79 0.30 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 20:00 101-55-308/11/23 15:350.39 0.15 1
Butylbenzylphthalate ND mg/kg 08/13/23 20:00 85-68-708/11/23 15:350.39 0.17 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 20:00 59-50-708/11/23 15:350.79 0.28 1
4-Chloroaniline ND mg/kg 08/13/23 20:00 106-47-808/11/23 15:350.79 0.31 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 20:00 111-91-108/11/23 15:350.39 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 20:00 111-44-408/11/23 15:350.39 0.15 1
2-Chloronaphthalene ND mg/kg 08/13/23 20:00 91-58-708/11/23 15:350.39 0.16 1
2-Chlorophenol ND mg/kg 08/13/23 20:00 95-57-808/11/23 15:350.39 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 20:00 7005-72-308/11/23 15:350.39 0.15 1
Chrysene 5.5 mg/kg 08/14/23 14:21 218-01-908/11/23 15:352.0 0.72 5
Dibenz(a,h)anthracene 0.97 mg/kg 08/13/23 20:00 53-70-308/11/23 15:350.39 0.15 1
Dibenzofuran 0.90 mg/kg 08/13/23 20:00 132-64-908/11/23 15:350.39 0.14 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 20:00 95-50-108/11/23 15:350.39 0.14 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 20:00 541-73-108/11/23 15:350.39 0.14 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 20:00 106-46-708/11/23 15:350.39 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 20:00 91-94-108/11/23 15:350.79 0.27 1
2,4-Dichlorophenol ND mg/kg 08/13/23 20:00 120-83-208/11/23 15:350.39 0.15 1
Diethylphthalate ND mg/kg 08/13/23 20:00 84-66-208/11/23 15:350.39 0.14 1
2,4-Dimethylphenol ND mg/kg 08/13/23 20:00 105-67-908/11/23 15:350.39 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-5 Lab ID:92681077007 Collected:08/04/23 09:54 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 20:00 131-11-308/11/23 15:350.39 0.14 1
Di-n-butylphthalate ND mg/kg 08/13/23 20:00 84-74-208/11/23 15:350.39 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 20:00 534-52-108/11/23 15:350.79 0.37 1
2,4-Dinitrophenol ND mg/kg 08/13/23 20:00 51-28-508/11/23 15:352.0 1.2 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 20:00 121-14-208/11/23 15:350.39 0.15 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 20:00 606-20-208/11/23 15:350.39 0.14 1
Di-n-octylphthalate ND mg/kg 08/13/23 20:00 117-84-008/11/23 15:350.39 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 20:00 117-81-708/11/23 15:350.39 0.15 1
Fluoranthene 11.2 mg/kg 08/14/23 14:21 206-44-008/11/23 15:352.0 0.67 5
Fluorene 1.7 mg/kg 08/13/23 20:00 86-73-708/11/23 15:350.39 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 20:00 87-68-308/11/23 15:350.39 0.17 1
Hexachlorobenzene ND mg/kg 08/13/23 20:00 118-74-108/11/23 15:350.39 0.15 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 20:00 77-47-4 v208/11/23 15:350.39 0.23 1
Hexachloroethane ND mg/kg 08/13/23 20:00 67-72-108/11/23 15:350.39 0.15 1
Indeno(1,2,3-cd)pyrene 3.3 mg/kg 08/13/23 20:00 193-39-508/11/23 15:350.39 0.16 1
Isophorone ND mg/kg 08/13/23 20:00 78-59-108/11/23 15:350.39 0.18 1
1-Methylnaphthalene 2.2 mg/kg 08/13/23 20:00 90-12-008/11/23 15:350.39 0.14 1
2-Methylnaphthalene 2.4 mg/kg 08/13/23 20:00 91-57-608/11/23 15:350.39 0.16 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 20:00 95-48-708/11/23 15:350.39 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 20:00 15831-10-408/11/23 15:350.39 0.16 1
Naphthalene 2.2 mg/kg 08/13/23 20:00 91-20-308/11/23 15:350.39 0.13 1
2-Nitroaniline ND mg/kg 08/13/23 20:00 88-74-408/11/23 15:352.0 0.32 1
3-Nitroaniline ND mg/kg 08/13/23 20:00 99-09-208/11/23 15:352.0 0.31 1
4-Nitroaniline ND mg/kg 08/13/23 20:00 100-01-608/11/23 15:350.79 0.30 1
Nitrobenzene ND mg/kg 08/13/23 20:00 98-95-308/11/23 15:350.39 0.18 1
2-Nitrophenol ND mg/kg 08/13/23 20:00 88-75-508/11/23 15:350.39 0.17 1
4-Nitrophenol ND mg/kg 08/13/23 20:00 100-02-708/11/23 15:352.0 0.76 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 20:00 62-75-908/11/23 15:350.39 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 20:00 621-64-708/11/23 15:350.39 0.15 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 20:00 86-30-608/11/23 15:350.39 0.14 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 20:00 108-60-108/11/23 15:350.39 0.19 1
Pentachlorophenol ND mg/kg 08/13/23 20:00 87-86-508/11/23 15:350.79 0.39 1
Phenanthrene 15.6 mg/kg 08/14/23 14:21 85-01-808/11/23 15:352.0 0.65 5
Phenol ND mg/kg 08/13/23 20:00 108-95-208/11/23 15:350.39 0.18 1
Pyrene 12.9 mg/kg 08/14/23 14:21 129-00-008/11/23 15:352.0 0.80 5
Pyridine ND mg/kg 08/13/23 20:00 110-86-108/11/23 15:350.39 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 20:00 120-82-108/11/23 15:350.39 0.16 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 20:00 95-95-408/11/23 15:350.39 0.18 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 20:00 88-06-208/11/23 15:350.39 0.16 1
Surrogates
Nitrobenzene-d5 (S)69 %08/13/23 20:00 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)68 %08/13/23 20:00 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)72 %08/13/23 20:00 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)50 %08/13/23 20:00 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-5 Lab ID:92681077007 Collected:08/04/23 09:54 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)41 %08/13/23 20:00 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)78 %08/13/23 20:00 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 06:57 67-64-108/08/23 21:440.12 0.039 1
Benzene ND mg/kg 08/09/23 06:57 71-43-208/08/23 21:440.0060 0.0024 1
Bromobenzene ND mg/kg 08/09/23 06:57 108-86-108/08/23 21:440.0060 0.0020 1
Bromochloromethane ND mg/kg 08/09/23 06:57 74-97-508/08/23 21:440.0060 0.0018 1
Bromodichloromethane ND mg/kg 08/09/23 06:57 75-27-408/08/23 21:440.0060 0.0023 1
Bromoform ND mg/kg 08/09/23 06:57 75-25-208/08/23 21:440.0060 0.0021 1
Bromomethane ND mg/kg 08/09/23 06:57 74-83-9 v208/08/23 21:440.024 0.019 1
2-Butanone (MEK)ND mg/kg 08/09/23 06:57 78-93-308/08/23 21:440.12 0.029 1
n-Butylbenzene ND mg/kg 08/09/23 06:57 104-51-808/08/23 21:440.0060 0.0038 1
sec-Butylbenzene ND mg/kg 08/09/23 06:57 135-98-808/08/23 21:440.0060 0.0027 1
tert-Butylbenzene ND mg/kg 08/09/23 06:57 98-06-608/08/23 21:440.0060 0.0021 1
Carbon tetrachloride ND mg/kg 08/09/23 06:57 56-23-508/08/23 21:440.0060 0.0023 1
Chlorobenzene ND mg/kg 08/09/23 06:57 108-90-708/08/23 21:440.0060 0.0035 1
Chloroethane ND mg/kg 08/09/23 06:57 75-00-308/08/23 21:440.012 0.0047 1
Chloroform ND mg/kg 08/09/23 06:57 67-66-308/08/23 21:440.0060 0.0050 1
Chloromethane ND mg/kg 08/09/23 06:57 74-87-308/08/23 21:440.012 0.0051 1
2-Chlorotoluene ND mg/kg 08/09/23 06:57 95-49-808/08/23 21:440.0060 0.0021 1
4-Chlorotoluene ND mg/kg 08/09/23 06:57 106-43-408/08/23 21:440.0060 0.0034 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 06:57 96-12-808/08/23 21:440.0060 0.0023 1
Dibromochloromethane ND mg/kg 08/09/23 06:57 124-48-108/08/23 21:440.0060 0.0034 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 06:57 106-93-408/08/23 21:440.0060 0.0027 1
Dibromomethane ND mg/kg 08/09/23 06:57 74-95-308/08/23 21:440.0060 0.0013 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 06:57 95-50-108/08/23 21:440.0060 0.0022 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 06:57 541-73-108/08/23 21:440.0060 0.0019 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 06:57 106-46-708/08/23 21:440.0060 0.0016 1
Dichlorodifluoromethane ND mg/kg 08/09/23 06:57 75-71-808/08/23 21:440.012 0.0061 1
1,1-Dichloroethane ND mg/kg 08/09/23 06:57 75-34-308/08/23 21:440.0060 0.0025 1
1,2-Dichloroethane ND mg/kg 08/09/23 06:57 107-06-208/08/23 21:440.0060 0.0040 1
1,1-Dichloroethene ND mg/kg 08/09/23 06:57 75-35-408/08/23 21:440.0060 0.0025 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 06:57 156-59-208/08/23 21:440.0060 0.0021 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 06:57 156-60-508/08/23 21:440.0060 0.0051 1
1,2-Dichloropropane ND mg/kg 08/09/23 06:57 78-87-508/08/23 21:440.0060 0.0018 1
1,3-Dichloropropane ND mg/kg 08/09/23 06:57 142-28-908/08/23 21:440.0060 0.0019 1
2,2-Dichloropropane ND mg/kg 08/09/23 06:57 594-20-708/08/23 21:440.0060 0.0046 1
1,1-Dichloropropene ND mg/kg 08/09/23 06:57 563-58-608/08/23 21:440.0060 0.0029 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 06:57 10061-01-508/08/23 21:440.0060 0.0016 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 06:57 10061-02-608/08/23 21:440.0060 0.0021 1
Diisopropyl ether ND mg/kg 08/09/23 06:57 108-20-308/08/23 21:440.0060 0.0016 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-5 Lab ID:92681077007 Collected:08/04/23 09:54 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 06:57 100-41-408/08/23 21:440.0060 0.0028 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 06:57 87-68-308/08/23 21:440.012 0.0099 1
2-Hexanone ND mg/kg 08/09/23 06:57 591-78-608/08/23 21:440.060 0.0058 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 06:57 98-82-808/08/23 21:440.0060 0.0020 1
p-Isopropyltoluene ND mg/kg 08/09/23 06:57 99-87-608/08/23 21:440.0060 0.0030 1
Methylene Chloride ND mg/kg 08/09/23 06:57 75-09-208/08/23 21:440.024 0.017 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 06:57 108-10-108/08/23 21:440.060 0.0058 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 06:57 1634-04-408/08/23 21:440.0060 0.0023 1
Naphthalene 0.0066 mg/kg 08/09/23 06:57 91-20-308/08/23 21:440.0060 0.0032 1
n-Propylbenzene ND mg/kg 08/09/23 06:57 103-65-108/08/23 21:440.0060 0.0021 1
Styrene ND mg/kg 08/09/23 06:57 100-42-508/08/23 21:440.0060 0.0016 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 06:57 630-20-608/08/23 21:440.0060 0.0023 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 06:57 79-34-508/08/23 21:440.0060 0.0016 1
Tetrachloroethene 0.042 mg/kg 08/09/23 06:57 127-18-408/08/23 21:440.0060 0.0019 1
Toluene ND mg/kg 08/09/23 06:57 108-88-308/08/23 21:440.0060 0.0042 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 06:57 87-61-608/08/23 21:440.0060 0.0049 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 06:57 120-82-1 IK08/08/23 21:440.0060 0.0051 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 06:57 71-55-608/08/23 21:440.0060 0.0031 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 06:57 79-00-508/08/23 21:440.0060 0.0020 1
Trichloroethene ND mg/kg 08/09/23 06:57 79-01-608/08/23 21:440.0060 0.0049 1
Trichlorofluoromethane ND mg/kg 08/09/23 06:57 75-69-408/08/23 21:440.0060 0.0033 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 06:57 96-18-408/08/23 21:440.0060 0.0031 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 06:57 95-63-608/08/23 21:440.0060 0.0036 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 06:57 108-67-808/08/23 21:440.0060 0.0020 1
Vinyl acetate ND mg/kg 08/09/23 06:57 108-05-408/08/23 21:440.060 0.012 1
Vinyl chloride ND mg/kg 08/09/23 06:57 75-01-408/08/23 21:440.012 0.0031 1
Xylene (Total)ND mg/kg 08/09/23 06:57 1330-20-708/08/23 21:440.012 0.0034 1
m&p-Xylene ND mg/kg 08/09/23 06:57 179601-23-108/08/23 21:440.012 0.0041 1
o-Xylene ND mg/kg 08/09/23 06:57 95-47-608/08/23 21:440.0060 0.0027 1
Surrogates
Toluene-d8 (S)100 %08/09/23 06:57 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)104 %08/09/23 06:57 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)111 %08/09/23 06:57 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.4 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.4 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-5 Lab ID:92681077007 Collected:08/04/23 09:54 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.09J mg/kg 08/14/23 19:29 18540-29-9 J08/13/23 18:151.20 0.306 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-10 Lab ID:92681077008 Collected:08/04/23 09:58 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.747J mg/kg 08/13/23 16:37 7440-38-2 J08/10/23 09:481.38 0.138 5
Barium 31.4 mg/kg 08/13/23 16:37 7440-39-308/10/23 09:483.45 0.210 5
Cadmium ND mg/kg 08/13/23 16:37 7440-43-908/10/23 09:481.38 0.118 5
Chromium 8.65 mg/kg 08/13/23 16:37 7440-47-308/10/23 09:486.89 0.408 5
Lead 7.33 mg/kg 08/13/23 16:37 7439-92-108/10/23 09:482.76 0.136 5
Selenium ND mg/kg 08/13/23 16:37 7782-49-208/10/23 09:483.45 0.248 5
Silver ND mg/kg 08/13/23 16:37 7440-22-408/10/23 09:480.689 0.119 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 14:15 7439-97-608/14/23 20:110.0551 0.0248 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 20:28 83-32-908/11/23 15:350.43 0.15 1
Acenaphthylene ND mg/kg 08/13/23 20:28 208-96-808/11/23 15:350.43 0.15 1
Aniline ND mg/kg 08/13/23 20:28 62-53-308/11/23 15:350.43 0.17 1
Anthracene ND mg/kg 08/13/23 20:28 120-12-708/11/23 15:350.43 0.14 1
Benzo(a)anthracene ND mg/kg 08/13/23 20:28 56-55-308/11/23 15:350.43 0.14 1
Benzo(a)pyrene ND mg/kg 08/13/23 20:28 50-32-808/11/23 15:350.43 0.15 1
Benzo(b)fluoranthene ND mg/kg 08/13/23 20:28 205-99-208/11/23 15:350.43 0.14 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 20:28 191-24-208/11/23 15:350.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 20:28 207-08-908/11/23 15:350.43 0.15 1
Benzoic Acid ND mg/kg 08/13/23 20:28 65-85-008/11/23 15:352.2 0.93 1
Benzyl alcohol ND mg/kg 08/13/23 20:28 100-51-608/11/23 15:350.86 0.33 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 20:28 101-55-308/11/23 15:350.43 0.17 1
Butylbenzylphthalate ND mg/kg 08/13/23 20:28 85-68-708/11/23 15:350.43 0.18 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 20:28 59-50-708/11/23 15:350.86 0.30 1
4-Chloroaniline ND mg/kg 08/13/23 20:28 106-47-808/11/23 15:350.86 0.34 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 20:28 111-91-108/11/23 15:350.43 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 20:28 111-44-408/11/23 15:350.43 0.16 1
2-Chloronaphthalene ND mg/kg 08/13/23 20:28 91-58-708/11/23 15:350.43 0.17 1
2-Chlorophenol ND mg/kg 08/13/23 20:28 95-57-808/11/23 15:350.43 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 20:28 7005-72-308/11/23 15:350.43 0.16 1
Chrysene ND mg/kg 08/13/23 20:28 218-01-908/11/23 15:350.43 0.16 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 20:28 53-70-308/11/23 15:350.43 0.17 1
Dibenzofuran ND mg/kg 08/13/23 20:28 132-64-908/11/23 15:350.43 0.16 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 20:28 95-50-108/11/23 15:350.43 0.16 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 20:28 541-73-108/11/23 15:350.43 0.15 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 20:28 106-46-708/11/23 15:350.43 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 20:28 91-94-108/11/23 15:350.86 0.29 1
2,4-Dichlorophenol ND mg/kg 08/13/23 20:28 120-83-208/11/23 15:350.43 0.17 1
Diethylphthalate ND mg/kg 08/13/23 20:28 84-66-208/11/23 15:350.43 0.16 1
2,4-Dimethylphenol ND mg/kg 08/13/23 20:28 105-67-908/11/23 15:350.43 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-10 Lab ID:92681077008 Collected:08/04/23 09:58 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 20:28 131-11-308/11/23 15:350.43 0.16 1
Di-n-butylphthalate ND mg/kg 08/13/23 20:28 84-74-208/11/23 15:350.43 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 20:28 534-52-108/11/23 15:350.86 0.40 1
2,4-Dinitrophenol ND mg/kg 08/13/23 20:28 51-28-508/11/23 15:352.2 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 20:28 121-14-208/11/23 15:350.43 0.17 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 20:28 606-20-208/11/23 15:350.43 0.16 1
Di-n-octylphthalate ND mg/kg 08/13/23 20:28 117-84-008/11/23 15:350.43 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 20:28 117-81-708/11/23 15:350.43 0.17 1
Fluoranthene ND mg/kg 08/13/23 20:28 206-44-008/11/23 15:350.43 0.15 1
Fluorene ND mg/kg 08/13/23 20:28 86-73-708/11/23 15:350.43 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 20:28 87-68-308/11/23 15:350.43 0.19 1
Hexachlorobenzene ND mg/kg 08/13/23 20:28 118-74-108/11/23 15:350.43 0.17 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 20:28 77-47-4 v208/11/23 15:350.43 0.25 1
Hexachloroethane ND mg/kg 08/13/23 20:28 67-72-108/11/23 15:350.43 0.16 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 20:28 193-39-508/11/23 15:350.43 0.17 1
Isophorone ND mg/kg 08/13/23 20:28 78-59-108/11/23 15:350.43 0.19 1
1-Methylnaphthalene ND mg/kg 08/13/23 20:28 90-12-008/11/23 15:350.43 0.15 1
2-Methylnaphthalene ND mg/kg 08/13/23 20:28 91-57-608/11/23 15:350.43 0.17 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 20:28 95-48-708/11/23 15:350.43 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 20:28 15831-10-408/11/23 15:350.43 0.17 1
Naphthalene ND mg/kg 08/13/23 20:28 91-20-308/11/23 15:350.43 0.15 1
2-Nitroaniline ND mg/kg 08/13/23 20:28 88-74-408/11/23 15:352.2 0.35 1
3-Nitroaniline ND mg/kg 08/13/23 20:28 99-09-208/11/23 15:352.2 0.34 1
4-Nitroaniline ND mg/kg 08/13/23 20:28 100-01-608/11/23 15:350.86 0.33 1
Nitrobenzene ND mg/kg 08/13/23 20:28 98-95-308/11/23 15:350.43 0.20 1
2-Nitrophenol ND mg/kg 08/13/23 20:28 88-75-508/11/23 15:350.43 0.19 1
4-Nitrophenol ND mg/kg 08/13/23 20:28 100-02-708/11/23 15:352.2 0.83 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 20:28 62-75-908/11/23 15:350.43 0.15 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 20:28 621-64-708/11/23 15:350.43 0.16 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 20:28 86-30-608/11/23 15:350.43 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 20:28 108-60-108/11/23 15:350.43 0.21 1
Pentachlorophenol ND mg/kg 08/13/23 20:28 87-86-508/11/23 15:350.86 0.42 1
Phenanthrene ND mg/kg 08/13/23 20:28 85-01-808/11/23 15:350.43 0.14 1
Phenol ND mg/kg 08/13/23 20:28 108-95-208/11/23 15:350.43 0.19 1
Pyrene ND mg/kg 08/13/23 20:28 129-00-008/11/23 15:350.43 0.18 1
Pyridine ND mg/kg 08/13/23 20:28 110-86-108/11/23 15:350.43 0.14 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 20:28 120-82-108/11/23 15:350.43 0.17 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 20:28 95-95-408/11/23 15:350.43 0.20 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 20:28 88-06-208/11/23 15:350.43 0.18 1
Surrogates
Nitrobenzene-d5 (S)73 %08/13/23 20:28 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)65 %08/13/23 20:28 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)73 %08/13/23 20:28 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)68 %08/13/23 20:28 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-10 Lab ID:92681077008 Collected:08/04/23 09:58 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)71 %08/13/23 20:28 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)98 %08/13/23 20:28 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 07:14 67-64-108/08/23 21:440.14 0.045 1
Benzene ND mg/kg 08/09/23 07:14 71-43-208/08/23 21:440.0071 0.0028 1
Bromobenzene ND mg/kg 08/09/23 07:14 108-86-108/08/23 21:440.0071 0.0023 1
Bromochloromethane ND mg/kg 08/09/23 07:14 74-97-508/08/23 21:440.0071 0.0021 1
Bromodichloromethane ND mg/kg 08/09/23 07:14 75-27-408/08/23 21:440.0071 0.0027 1
Bromoform ND mg/kg 08/09/23 07:14 75-25-208/08/23 21:440.0071 0.0025 1
Bromomethane ND mg/kg 08/09/23 07:14 74-83-9 v208/08/23 21:440.028 0.022 1
2-Butanone (MEK)ND mg/kg 08/09/23 07:14 78-93-308/08/23 21:440.14 0.034 1
n-Butylbenzene ND mg/kg 08/09/23 07:14 104-51-808/08/23 21:440.0071 0.0045 1
sec-Butylbenzene ND mg/kg 08/09/23 07:14 135-98-808/08/23 21:440.0071 0.0031 1
tert-Butylbenzene ND mg/kg 08/09/23 07:14 98-06-608/08/23 21:440.0071 0.0025 1
Carbon tetrachloride ND mg/kg 08/09/23 07:14 56-23-508/08/23 21:440.0071 0.0026 1
Chlorobenzene ND mg/kg 08/09/23 07:14 108-90-708/08/23 21:440.0071 0.0041 1
Chloroethane ND mg/kg 08/09/23 07:14 75-00-308/08/23 21:440.014 0.0055 1
Chloroform ND mg/kg 08/09/23 07:14 67-66-308/08/23 21:440.0071 0.0059 1
Chloromethane ND mg/kg 08/09/23 07:14 74-87-308/08/23 21:440.014 0.0059 1
2-Chlorotoluene ND mg/kg 08/09/23 07:14 95-49-808/08/23 21:440.0071 0.0025 1
4-Chlorotoluene ND mg/kg 08/09/23 07:14 106-43-408/08/23 21:440.0071 0.0039 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 07:14 96-12-808/08/23 21:440.0071 0.0027 1
Dibromochloromethane ND mg/kg 08/09/23 07:14 124-48-108/08/23 21:440.0071 0.0040 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 07:14 106-93-408/08/23 21:440.0071 0.0031 1
Dibromomethane ND mg/kg 08/09/23 07:14 74-95-308/08/23 21:440.0071 0.0015 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 07:14 95-50-108/08/23 21:440.0071 0.0025 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 07:14 541-73-108/08/23 21:440.0071 0.0022 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 07:14 106-46-708/08/23 21:440.0071 0.0018 1
Dichlorodifluoromethane ND mg/kg 08/09/23 07:14 75-71-808/08/23 21:440.014 0.0072 1
1,1-Dichloroethane ND mg/kg 08/09/23 07:14 75-34-308/08/23 21:440.0071 0.0029 1
1,2-Dichloroethane ND mg/kg 08/09/23 07:14 107-06-208/08/23 21:440.0071 0.0047 1
1,1-Dichloroethene ND mg/kg 08/09/23 07:14 75-35-408/08/23 21:440.0071 0.0029 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 07:14 156-59-208/08/23 21:440.0071 0.0024 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 07:14 156-60-508/08/23 21:440.0071 0.0060 1
1,2-Dichloropropane ND mg/kg 08/09/23 07:14 78-87-508/08/23 21:440.0071 0.0021 1
1,3-Dichloropropane ND mg/kg 08/09/23 07:14 142-28-908/08/23 21:440.0071 0.0022 1
2,2-Dichloropropane ND mg/kg 08/09/23 07:14 594-20-708/08/23 21:440.0071 0.0054 1
1,1-Dichloropropene ND mg/kg 08/09/23 07:14 563-58-608/08/23 21:440.0071 0.0034 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 07:14 10061-01-508/08/23 21:440.0071 0.0019 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 07:14 10061-02-608/08/23 21:440.0071 0.0024 1
Diisopropyl ether ND mg/kg 08/09/23 07:14 108-20-308/08/23 21:440.0071 0.0019 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-10 Lab ID:92681077008 Collected:08/04/23 09:58 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 07:14 100-41-408/08/23 21:440.0071 0.0033 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 07:14 87-68-308/08/23 21:440.014 0.012 1
2-Hexanone ND mg/kg 08/09/23 07:14 591-78-608/08/23 21:440.071 0.0068 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 07:14 98-82-808/08/23 21:440.0071 0.0024 1
p-Isopropyltoluene ND mg/kg 08/09/23 07:14 99-87-608/08/23 21:440.0071 0.0035 1
Methylene Chloride ND mg/kg 08/09/23 07:14 75-09-208/08/23 21:440.028 0.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 07:14 108-10-108/08/23 21:440.071 0.0068 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 07:14 1634-04-408/08/23 21:440.0071 0.0026 1
Naphthalene ND mg/kg 08/09/23 07:14 91-20-308/08/23 21:440.0071 0.0037 1
n-Propylbenzene ND mg/kg 08/09/23 07:14 103-65-108/08/23 21:440.0071 0.0025 1
Styrene ND mg/kg 08/09/23 07:14 100-42-508/08/23 21:440.0071 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 07:14 630-20-608/08/23 21:440.0071 0.0027 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 07:14 79-34-508/08/23 21:440.0071 0.0019 1
Tetrachloroethene ND mg/kg 08/09/23 07:14 127-18-408/08/23 21:440.0071 0.0022 1
Toluene ND mg/kg 08/09/23 07:14 108-88-308/08/23 21:440.0071 0.0049 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 07:14 87-61-608/08/23 21:440.0071 0.0057 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 07:14 120-82-1 IK08/08/23 21:440.0071 0.0059 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 07:14 71-55-608/08/23 21:440.0071 0.0037 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 07:14 79-00-508/08/23 21:440.0071 0.0023 1
Trichloroethene ND mg/kg 08/09/23 07:14 79-01-608/08/23 21:440.0071 0.0057 1
Trichlorofluoromethane ND mg/kg 08/09/23 07:14 75-69-408/08/23 21:440.0071 0.0039 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 07:14 96-18-408/08/23 21:440.0071 0.0036 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 07:14 95-63-608/08/23 21:440.0071 0.0042 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 07:14 108-67-808/08/23 21:440.0071 0.0024 1
Vinyl acetate ND mg/kg 08/09/23 07:14 108-05-408/08/23 21:440.071 0.015 1
Vinyl chloride ND mg/kg 08/09/23 07:14 75-01-408/08/23 21:440.014 0.0036 1
Xylene (Total)ND mg/kg 08/09/23 07:14 1330-20-708/08/23 21:440.014 0.0040 1
m&p-Xylene ND mg/kg 08/09/23 07:14 179601-23-108/08/23 21:440.014 0.0048 1
o-Xylene ND mg/kg 08/09/23 07:14 95-47-608/08/23 21:440.0071 0.0031 1
Surrogates
Toluene-d8 (S)102 %08/09/23 07:14 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)104 %08/09/23 07:14 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)106 %08/09/23 07:14 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.6 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.5 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P3-10 Lab ID:92681077008 Collected:08/04/23 09:58 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.418J mg/kg 08/14/23 19:34 18540-29-9 J08/13/23 18:151.38 0.352 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-5 Lab ID:92681077009 Collected:08/04/23 10:38 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.905J mg/kg 08/13/23 16:41 7440-38-2 J08/10/23 09:481.43 0.143 5
Barium 21.7 mg/kg 08/13/23 16:41 7440-39-308/10/23 09:483.57 0.217 5
Cadmium ND mg/kg 08/13/23 16:41 7440-43-908/10/23 09:481.43 0.122 5
Chromium 12.3 mg/kg 08/13/23 16:41 7440-47-308/10/23 09:487.14 0.423 5
Lead 7.14 mg/kg 08/13/23 16:41 7439-92-108/10/23 09:482.86 0.141 5
Selenium ND mg/kg 08/13/23 16:41 7782-49-208/10/23 09:483.57 0.257 5
Silver ND mg/kg 08/13/23 16:41 7440-22-408/10/23 09:480.714 0.124 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0528J mg/kg 08/15/23 14:17 7439-97-6 J08/14/23 20:110.0571 0.0257 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/13/23 20:56 83-32-908/11/23 15:350.41 0.14 1
Acenaphthylene ND mg/kg 08/13/23 20:56 208-96-808/11/23 15:350.41 0.14 1
Aniline ND mg/kg 08/13/23 20:56 62-53-308/11/23 15:350.41 0.16 1
Anthracene ND mg/kg 08/13/23 20:56 120-12-708/11/23 15:350.41 0.13 1
Benzo(a)anthracene ND mg/kg 08/13/23 20:56 56-55-308/11/23 15:350.41 0.14 1
Benzo(a)pyrene ND mg/kg 08/13/23 20:56 50-32-808/11/23 15:350.41 0.14 1
Benzo(b)fluoranthene ND mg/kg 08/13/23 20:56 205-99-208/11/23 15:350.41 0.14 1
Benzo(g,h,i)perylene ND mg/kg 08/13/23 20:56 191-24-208/11/23 15:350.41 0.16 1
Benzo(k)fluoranthene ND mg/kg 08/13/23 20:56 207-08-908/11/23 15:350.41 0.14 1
Benzoic Acid ND mg/kg 08/13/23 20:56 65-85-008/11/23 15:352.1 0.89 1
Benzyl alcohol ND mg/kg 08/13/23 20:56 100-51-608/11/23 15:350.82 0.31 1
4-Bromophenylphenyl ether ND mg/kg 08/13/23 20:56 101-55-308/11/23 15:350.41 0.16 1
Butylbenzylphthalate ND mg/kg 08/13/23 20:56 85-68-708/11/23 15:350.41 0.17 1
4-Chloro-3-methylphenol ND mg/kg 08/13/23 20:56 59-50-708/11/23 15:350.82 0.29 1
4-Chloroaniline ND mg/kg 08/13/23 20:56 106-47-808/11/23 15:350.82 0.32 1
bis(2-Chloroethoxy)methane ND mg/kg 08/13/23 20:56 111-91-108/11/23 15:350.41 0.17 1
bis(2-Chloroethyl) ether ND mg/kg 08/13/23 20:56 111-44-408/11/23 15:350.41 0.15 1
2-Chloronaphthalene ND mg/kg 08/13/23 20:56 91-58-708/11/23 15:350.41 0.16 1
2-Chlorophenol ND mg/kg 08/13/23 20:56 95-57-808/11/23 15:350.41 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 08/13/23 20:56 7005-72-308/11/23 15:350.41 0.15 1
Chrysene ND mg/kg 08/13/23 20:56 218-01-908/11/23 15:350.41 0.15 1
Dibenz(a,h)anthracene ND mg/kg 08/13/23 20:56 53-70-308/11/23 15:350.41 0.16 1
Dibenzofuran ND mg/kg 08/13/23 20:56 132-64-908/11/23 15:350.41 0.15 1
1,2-Dichlorobenzene ND mg/kg 08/13/23 20:56 95-50-108/11/23 15:350.41 0.15 1
1,3-Dichlorobenzene ND mg/kg 08/13/23 20:56 541-73-108/11/23 15:350.41 0.15 1
1,4-Dichlorobenzene ND mg/kg 08/13/23 20:56 106-46-708/11/23 15:350.41 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 08/13/23 20:56 91-94-108/11/23 15:350.82 0.28 1
2,4-Dichlorophenol ND mg/kg 08/13/23 20:56 120-83-208/11/23 15:350.41 0.16 1
Diethylphthalate ND mg/kg 08/13/23 20:56 84-66-208/11/23 15:350.41 0.15 1
2,4-Dimethylphenol ND mg/kg 08/13/23 20:56 105-67-908/11/23 15:350.41 0.17 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-5 Lab ID:92681077009 Collected:08/04/23 10:38 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/13/23 20:56 131-11-308/11/23 15:350.41 0.15 1
Di-n-butylphthalate ND mg/kg 08/13/23 20:56 84-74-208/11/23 15:350.41 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/13/23 20:56 534-52-108/11/23 15:350.82 0.38 1
2,4-Dinitrophenol ND mg/kg 08/13/23 20:56 51-28-508/11/23 15:352.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/13/23 20:56 121-14-208/11/23 15:350.41 0.16 1
2,6-Dinitrotoluene ND mg/kg 08/13/23 20:56 606-20-208/11/23 15:350.41 0.15 1
Di-n-octylphthalate ND mg/kg 08/13/23 20:56 117-84-008/11/23 15:350.41 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/13/23 20:56 117-81-708/11/23 15:350.41 0.16 1
Fluoranthene ND mg/kg 08/13/23 20:56 206-44-008/11/23 15:350.41 0.14 1
Fluorene ND mg/kg 08/13/23 20:56 86-73-708/11/23 15:350.41 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 08/13/23 20:56 87-68-308/11/23 15:350.41 0.18 1
Hexachlorobenzene ND mg/kg 08/13/23 20:56 118-74-108/11/23 15:350.41 0.16 1
Hexachlorocyclopentadiene ND mg/kg 08/13/23 20:56 77-47-4 v208/11/23 15:350.41 0.24 1
Hexachloroethane ND mg/kg 08/13/23 20:56 67-72-108/11/23 15:350.41 0.16 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/13/23 20:56 193-39-508/11/23 15:350.41 0.16 1
Isophorone ND mg/kg 08/13/23 20:56 78-59-108/11/23 15:350.41 0.18 1
1-Methylnaphthalene ND mg/kg 08/13/23 20:56 90-12-008/11/23 15:350.41 0.14 1
2-Methylnaphthalene ND mg/kg 08/13/23 20:56 91-57-608/11/23 15:350.41 0.16 1
2-Methylphenol(o-Cresol)ND mg/kg 08/13/23 20:56 95-48-708/11/23 15:350.41 0.17 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/13/23 20:56 15831-10-408/11/23 15:350.41 0.17 1
Naphthalene ND mg/kg 08/13/23 20:56 91-20-308/11/23 15:350.41 0.14 1
2-Nitroaniline ND mg/kg 08/13/23 20:56 88-74-408/11/23 15:352.1 0.34 1
3-Nitroaniline ND mg/kg 08/13/23 20:56 99-09-208/11/23 15:352.1 0.32 1
4-Nitroaniline ND mg/kg 08/13/23 20:56 100-01-608/11/23 15:350.82 0.31 1
Nitrobenzene ND mg/kg 08/13/23 20:56 98-95-308/11/23 15:350.41 0.19 1
2-Nitrophenol ND mg/kg 08/13/23 20:56 88-75-508/11/23 15:350.41 0.18 1
4-Nitrophenol ND mg/kg 08/13/23 20:56 100-02-708/11/23 15:352.1 0.80 1
N-Nitrosodimethylamine ND mg/kg 08/13/23 20:56 62-75-908/11/23 15:350.41 0.14 1
N-Nitroso-di-n-propylamine ND mg/kg 08/13/23 20:56 621-64-708/11/23 15:350.41 0.15 1
N-Nitrosodiphenylamine ND mg/kg 08/13/23 20:56 86-30-608/11/23 15:350.41 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/13/23 20:56 108-60-108/11/23 15:350.41 0.20 1
Pentachlorophenol ND mg/kg 08/13/23 20:56 87-86-508/11/23 15:350.82 0.40 1
Phenanthrene ND mg/kg 08/13/23 20:56 85-01-808/11/23 15:350.41 0.13 1
Phenol ND mg/kg 08/13/23 20:56 108-95-208/11/23 15:350.41 0.18 1
Pyrene ND mg/kg 08/13/23 20:56 129-00-008/11/23 15:350.41 0.17 1
Pyridine ND mg/kg 08/13/23 20:56 110-86-108/11/23 15:350.41 0.13 1
1,2,4-Trichlorobenzene ND mg/kg 08/13/23 20:56 120-82-108/11/23 15:350.41 0.16 1
2,4,5-Trichlorophenol ND mg/kg 08/13/23 20:56 95-95-408/11/23 15:350.41 0.19 1
2,4,6-Trichlorophenol ND mg/kg 08/13/23 20:56 88-06-208/11/23 15:350.41 0.17 1
Surrogates
Nitrobenzene-d5 (S)71 %08/13/23 20:56 4165-60-008/11/23 15:3510-130 1
2-Fluorobiphenyl (S)73 %08/13/23 20:56 321-60-808/11/23 15:3510-130 1
Terphenyl-d14 (S)93 %08/13/23 20:56 1718-51-008/11/23 15:3510-130 1
Phenol-d6 (S)47 %08/13/23 20:56 13127-88-308/11/23 15:3510-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-5 Lab ID:92681077009 Collected:08/04/23 10:38 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)38 %08/13/23 20:56 367-12-408/11/23 15:3510-130 1
2,4,6-Tribromophenol (S)53 %08/13/23 20:56 118-79-608/11/23 15:3510-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 07:32 67-64-108/08/23 21:440.18 0.056 1
Benzene ND mg/kg 08/09/23 07:32 71-43-208/08/23 21:440.0088 0.0035 1
Bromobenzene ND mg/kg 08/09/23 07:32 108-86-108/08/23 21:440.0088 0.0029 1
Bromochloromethane ND mg/kg 08/09/23 07:32 74-97-508/08/23 21:440.0088 0.0026 1
Bromodichloromethane ND mg/kg 08/09/23 07:32 75-27-408/08/23 21:440.0088 0.0034 1
Bromoform ND mg/kg 08/09/23 07:32 75-25-208/08/23 21:440.0088 0.0031 1
Bromomethane ND mg/kg 08/09/23 07:32 74-83-9 v208/08/23 21:440.035 0.027 1
2-Butanone (MEK)ND mg/kg 08/09/23 07:32 78-93-308/08/23 21:440.18 0.042 1
n-Butylbenzene ND mg/kg 08/09/23 07:32 104-51-808/08/23 21:440.0088 0.0055 1
sec-Butylbenzene ND mg/kg 08/09/23 07:32 135-98-808/08/23 21:440.0088 0.0039 1
tert-Butylbenzene ND mg/kg 08/09/23 07:32 98-06-608/08/23 21:440.0088 0.0031 1
Carbon tetrachloride ND mg/kg 08/09/23 07:32 56-23-508/08/23 21:440.0088 0.0033 1
Chlorobenzene ND mg/kg 08/09/23 07:32 108-90-708/08/23 21:440.0088 0.0050 1
Chloroethane ND mg/kg 08/09/23 07:32 75-00-308/08/23 21:440.018 0.0068 1
Chloroform ND mg/kg 08/09/23 07:32 67-66-308/08/23 21:440.0088 0.0073 1
Chloromethane ND mg/kg 08/09/23 07:32 74-87-308/08/23 21:440.018 0.0074 1
2-Chlorotoluene ND mg/kg 08/09/23 07:32 95-49-808/08/23 21:440.0088 0.0031 1
4-Chlorotoluene ND mg/kg 08/09/23 07:32 106-43-408/08/23 21:440.0088 0.0049 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 07:32 96-12-808/08/23 21:440.0088 0.0034 1
Dibromochloromethane ND mg/kg 08/09/23 07:32 124-48-108/08/23 21:440.0088 0.0049 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 07:32 106-93-408/08/23 21:440.0088 0.0039 1
Dibromomethane ND mg/kg 08/09/23 07:32 74-95-308/08/23 21:440.0088 0.0019 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 07:32 95-50-108/08/23 21:440.0088 0.0032 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 07:32 541-73-108/08/23 21:440.0088 0.0027 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 07:32 106-46-708/08/23 21:440.0088 0.0023 1
Dichlorodifluoromethane ND mg/kg 08/09/23 07:32 75-71-808/08/23 21:440.018 0.0089 1
1,1-Dichloroethane ND mg/kg 08/09/23 07:32 75-34-308/08/23 21:440.0088 0.0036 1
1,2-Dichloroethane ND mg/kg 08/09/23 07:32 107-06-208/08/23 21:440.0088 0.0058 1
1,1-Dichloroethene ND mg/kg 08/09/23 07:32 75-35-408/08/23 21:440.0088 0.0036 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 07:32 156-59-208/08/23 21:440.0088 0.0030 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 07:32 156-60-508/08/23 21:440.0088 0.0075 1
1,2-Dichloropropane ND mg/kg 08/09/23 07:32 78-87-508/08/23 21:440.0088 0.0026 1
1,3-Dichloropropane ND mg/kg 08/09/23 07:32 142-28-908/08/23 21:440.0088 0.0027 1
2,2-Dichloropropane ND mg/kg 08/09/23 07:32 594-20-708/08/23 21:440.0088 0.0066 1
1,1-Dichloropropene ND mg/kg 08/09/23 07:32 563-58-608/08/23 21:440.0088 0.0042 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 07:32 10061-01-508/08/23 21:440.0088 0.0024 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 07:32 10061-02-608/08/23 21:440.0088 0.0030 1
Diisopropyl ether ND mg/kg 08/09/23 07:32 108-20-308/08/23 21:440.0088 0.0024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-5 Lab ID:92681077009 Collected:08/04/23 10:38 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 07:32 100-41-408/08/23 21:440.0088 0.0041 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 07:32 87-68-308/08/23 21:440.018 0.014 1
2-Hexanone ND mg/kg 08/09/23 07:32 591-78-608/08/23 21:440.088 0.0085 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 07:32 98-82-808/08/23 21:440.0088 0.0030 1
p-Isopropyltoluene ND mg/kg 08/09/23 07:32 99-87-608/08/23 21:440.0088 0.0043 1
Methylene Chloride ND mg/kg 08/09/23 07:32 75-09-208/08/23 21:440.035 0.024 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 07:32 108-10-108/08/23 21:440.088 0.0085 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 07:32 1634-04-408/08/23 21:440.0088 0.0033 1
Naphthalene ND mg/kg 08/09/23 07:32 91-20-308/08/23 21:440.0088 0.0046 1
n-Propylbenzene ND mg/kg 08/09/23 07:32 103-65-108/08/23 21:440.0088 0.0031 1
Styrene ND mg/kg 08/09/23 07:32 100-42-508/08/23 21:440.0088 0.0023 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 07:32 630-20-608/08/23 21:440.0088 0.0034 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 07:32 79-34-508/08/23 21:440.0088 0.0023 1
Tetrachloroethene ND mg/kg 08/09/23 07:32 127-18-408/08/23 21:440.0088 0.0028 1
Toluene ND mg/kg 08/09/23 07:32 108-88-308/08/23 21:440.0088 0.0061 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 07:32 87-61-608/08/23 21:440.0088 0.0071 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 07:32 120-82-1 IK08/08/23 21:440.0088 0.0074 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 07:32 71-55-608/08/23 21:440.0088 0.0046 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 07:32 79-00-508/08/23 21:440.0088 0.0029 1
Trichloroethene ND mg/kg 08/09/23 07:32 79-01-608/08/23 21:440.0088 0.0071 1
Trichlorofluoromethane ND mg/kg 08/09/23 07:32 75-69-408/08/23 21:440.0088 0.0048 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 07:32 96-18-408/08/23 21:440.0088 0.0044 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 07:32 95-63-608/08/23 21:440.0088 0.0052 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 07:32 108-67-808/08/23 21:440.0088 0.0029 1
Vinyl acetate ND mg/kg 08/09/23 07:32 108-05-408/08/23 21:440.088 0.018 1
Vinyl chloride ND mg/kg 08/09/23 07:32 75-01-408/08/23 21:440.018 0.0045 1
Xylene (Total)ND mg/kg 08/09/23 07:32 1330-20-708/08/23 21:440.018 0.0050 1
m&p-Xylene ND mg/kg 08/09/23 07:32 179601-23-108/08/23 21:440.018 0.0060 1
o-Xylene ND mg/kg 08/09/23 07:32 95-47-608/08/23 21:440.0088 0.0039 1
Surrogates
Toluene-d8 (S)99 %08/09/23 07:32 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)102 %08/09/23 07:32 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)109 %08/09/23 07:32 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.9 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.0 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-5 Lab ID:92681077009 Collected:08/04/23 10:38 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.587J mg/kg 08/14/23 19:39 18540-29-9 J08/13/23 18:151.43 0.364 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-10 Lab ID:92681077010 Collected:08/04/23 10:40 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.493J mg/kg 08/13/23 16:44 7440-38-2 J08/10/23 09:481.33 0.133 5
Barium 10.9 mg/kg 08/13/23 16:44 7440-39-308/10/23 09:483.32 0.202 5
Cadmium ND mg/kg 08/13/23 16:44 7440-43-908/10/23 09:481.33 0.114 5
Chromium 5.61J mg/kg 08/13/23 16:44 7440-47-3 J08/10/23 09:486.65 0.393 5
Lead 1.30J mg/kg 08/13/23 16:44 7439-92-1 J08/10/23 09:482.66 0.132 5
Selenium ND mg/kg 08/13/23 16:44 7782-49-208/10/23 09:483.32 0.239 5
Silver ND mg/kg 08/13/23 16:44 7440-22-408/10/23 09:480.665 0.115 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 14:20 7439-97-608/14/23 20:110.0532 0.0239 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/15/23 13:43 83-32-908/14/23 17:160.45 0.16 1
Acenaphthylene ND mg/kg 08/15/23 13:43 208-96-808/14/23 17:160.45 0.16 1
Aniline ND mg/kg 08/15/23 13:43 62-53-308/14/23 17:160.45 0.17 1
Anthracene ND mg/kg 08/15/23 13:43 120-12-708/14/23 17:160.45 0.15 1
Benzo(a)anthracene ND mg/kg 08/15/23 13:43 56-55-308/14/23 17:160.45 0.15 1
Benzo(a)pyrene ND mg/kg 08/15/23 13:43 50-32-808/14/23 17:160.45 0.15 1
Benzo(b)fluoranthene ND mg/kg 08/15/23 13:43 205-99-208/14/23 17:160.45 0.15 1
Benzo(g,h,i)perylene ND mg/kg 08/15/23 13:43 191-24-208/14/23 17:160.45 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/15/23 13:43 207-08-908/14/23 17:160.45 0.16 1
Benzoic Acid ND mg/kg 08/15/23 13:43 65-85-008/14/23 17:162.2 0.96 1
Benzyl alcohol ND mg/kg 08/15/23 13:43 100-51-608/14/23 17:160.89 0.34 1
4-Bromophenylphenyl ether ND mg/kg 08/15/23 13:43 101-55-308/14/23 17:160.45 0.17 1
Butylbenzylphthalate ND mg/kg 08/15/23 13:43 85-68-708/14/23 17:160.45 0.19 1
4-Chloro-3-methylphenol ND mg/kg 08/15/23 13:43 59-50-708/14/23 17:160.89 0.31 1
4-Chloroaniline ND mg/kg 08/15/23 13:43 106-47-808/14/23 17:160.89 0.35 1
bis(2-Chloroethoxy)methane ND mg/kg 08/15/23 13:43 111-91-108/14/23 17:160.45 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 08/15/23 13:43 111-44-408/14/23 17:160.45 0.17 1
2-Chloronaphthalene ND mg/kg 08/15/23 13:43 91-58-708/14/23 17:160.45 0.18 1
2-Chlorophenol ND mg/kg 08/15/23 13:43 95-57-808/14/23 17:160.45 0.17 1
4-Chlorophenylphenyl ether ND mg/kg 08/15/23 13:43 7005-72-308/14/23 17:160.45 0.17 1
Chrysene ND mg/kg 08/15/23 13:43 218-01-908/14/23 17:160.45 0.16 1
Dibenz(a,h)anthracene ND mg/kg 08/15/23 13:43 53-70-308/14/23 17:160.45 0.17 1
Dibenzofuran ND mg/kg 08/15/23 13:43 132-64-908/14/23 17:160.45 0.16 1
1,2-Dichlorobenzene ND mg/kg 08/15/23 13:43 95-50-108/14/23 17:160.45 0.16 1
1,3-Dichlorobenzene ND mg/kg 08/15/23 13:43 541-73-108/14/23 17:160.45 0.16 1
1,4-Dichlorobenzene ND mg/kg 08/15/23 13:43 106-46-708/14/23 17:160.45 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 08/15/23 13:43 91-94-108/14/23 17:160.89 0.30 1
2,4-Dichlorophenol ND mg/kg 08/15/23 13:43 120-83-208/14/23 17:160.45 0.17 1
Diethylphthalate ND mg/kg 08/15/23 13:43 84-66-208/14/23 17:160.45 0.16 1
2,4-Dimethylphenol ND mg/kg 08/15/23 13:43 105-67-908/14/23 17:160.45 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-10 Lab ID:92681077010 Collected:08/04/23 10:40 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/15/23 13:43 131-11-308/14/23 17:160.45 0.16 1
Di-n-butylphthalate ND mg/kg 08/15/23 13:43 84-74-208/14/23 17:160.45 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/15/23 13:43 534-52-108/14/23 17:160.89 0.42 1
2,4-Dinitrophenol ND mg/kg 08/15/23 13:43 51-28-508/14/23 17:162.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 08/15/23 13:43 121-14-208/14/23 17:160.45 0.17 1
2,6-Dinitrotoluene ND mg/kg 08/15/23 13:43 606-20-208/14/23 17:160.45 0.16 1
Di-n-octylphthalate ND mg/kg 08/15/23 13:43 117-84-008/14/23 17:160.45 0.18 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/15/23 13:43 117-81-708/14/23 17:160.45 0.17 1
Fluoranthene ND mg/kg 08/15/23 13:43 206-44-008/14/23 17:160.45 0.15 1
Fluorene ND mg/kg 08/15/23 13:43 86-73-708/14/23 17:160.45 0.16 1
Hexachloro-1,3-butadiene ND mg/kg 08/15/23 13:43 87-68-308/14/23 17:160.45 0.19 1
Hexachlorobenzene ND mg/kg 08/15/23 13:43 118-74-108/14/23 17:160.45 0.17 1
Hexachlorocyclopentadiene ND mg/kg 08/15/23 13:43 77-47-408/14/23 17:160.45 0.25 1
Hexachloroethane ND mg/kg 08/15/23 13:43 67-72-108/14/23 17:160.45 0.17 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/15/23 13:43 193-39-508/14/23 17:160.45 0.18 1
Isophorone ND mg/kg 08/15/23 13:43 78-59-108/14/23 17:160.45 0.20 1
1-Methylnaphthalene ND mg/kg 08/15/23 13:43 90-12-008/14/23 17:160.45 0.16 1
2-Methylnaphthalene ND mg/kg 08/15/23 13:43 91-57-608/14/23 17:160.45 0.18 1
2-Methylphenol(o-Cresol)ND mg/kg 08/15/23 13:43 95-48-708/14/23 17:160.45 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/15/23 13:43 15831-10-408/14/23 17:160.45 0.18 1
Naphthalene ND mg/kg 08/15/23 13:43 91-20-308/14/23 17:160.45 0.15 1
2-Nitroaniline ND mg/kg 08/15/23 13:43 88-74-408/14/23 17:162.2 0.36 1
3-Nitroaniline ND mg/kg 08/15/23 13:43 99-09-208/14/23 17:162.2 0.35 1
4-Nitroaniline ND mg/kg 08/15/23 13:43 100-01-608/14/23 17:160.89 0.34 1
Nitrobenzene ND mg/kg 08/15/23 13:43 98-95-308/14/23 17:160.45 0.21 1
2-Nitrophenol ND mg/kg 08/15/23 13:43 88-75-508/14/23 17:160.45 0.19 1
4-Nitrophenol ND mg/kg 08/15/23 13:43 100-02-708/14/23 17:162.2 0.86 1
N-Nitrosodimethylamine ND mg/kg 08/15/23 13:43 62-75-908/14/23 17:160.45 0.15 1
N-Nitroso-di-n-propylamine ND mg/kg 08/15/23 13:43 621-64-708/14/23 17:160.45 0.17 1
N-Nitrosodiphenylamine ND mg/kg 08/15/23 13:43 86-30-608/14/23 17:160.45 0.16 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/15/23 13:43 108-60-108/14/23 17:160.45 0.21 1
Pentachlorophenol ND mg/kg 08/15/23 13:43 87-86-508/14/23 17:160.89 0.44 1
Phenanthrene ND mg/kg 08/15/23 13:43 85-01-808/14/23 17:160.45 0.15 1
Phenol ND mg/kg 08/15/23 13:43 108-95-208/14/23 17:160.45 0.20 1
Pyrene ND mg/kg 08/15/23 13:43 129-00-008/14/23 17:160.45 0.18 1
Pyridine ND mg/kg 08/15/23 13:43 110-86-108/14/23 17:160.45 0.14 1
1,2,4-Trichlorobenzene ND mg/kg 08/15/23 13:43 120-82-108/14/23 17:160.45 0.18 1
2,4,5-Trichlorophenol ND mg/kg 08/15/23 13:43 95-95-408/14/23 17:160.45 0.20 1
2,4,6-Trichlorophenol ND mg/kg 08/15/23 13:43 88-06-208/14/23 17:160.45 0.18 1
Surrogates
Nitrobenzene-d5 (S)41 %08/15/23 13:43 4165-60-008/14/23 17:1610-130 1
2-Fluorobiphenyl (S)32 %08/15/23 13:43 321-60-808/14/23 17:1610-130 1
Terphenyl-d14 (S)42 %08/15/23 13:43 1718-51-008/14/23 17:1610-130 1
Phenol-d6 (S)38 %08/15/23 13:43 13127-88-308/14/23 17:1610-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-10 Lab ID:92681077010 Collected:08/04/23 10:40 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)37 %08/15/23 13:43 367-12-408/14/23 17:1610-130 1
2,4,6-Tribromophenol (S)60 %08/15/23 13:43 118-79-608/14/23 17:1610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/09/23 07:49 67-64-108/08/23 21:440.15 0.048 1
Benzene ND mg/kg 08/09/23 07:49 71-43-208/08/23 21:440.0075 0.0030 1
Bromobenzene ND mg/kg 08/09/23 07:49 108-86-108/08/23 21:440.0075 0.0025 1
Bromochloromethane ND mg/kg 08/09/23 07:49 74-97-508/08/23 21:440.0075 0.0022 1
Bromodichloromethane ND mg/kg 08/09/23 07:49 75-27-408/08/23 21:440.0075 0.0029 1
Bromoform ND mg/kg 08/09/23 07:49 75-25-208/08/23 21:440.0075 0.0026 1
Bromomethane ND mg/kg 08/09/23 07:49 74-83-9 v208/08/23 21:440.030 0.023 1
2-Butanone (MEK)ND mg/kg 08/09/23 07:49 78-93-308/08/23 21:440.15 0.036 1
n-Butylbenzene ND mg/kg 08/09/23 07:49 104-51-808/08/23 21:440.0075 0.0047 1
sec-Butylbenzene ND mg/kg 08/09/23 07:49 135-98-808/08/23 21:440.0075 0.0033 1
tert-Butylbenzene ND mg/kg 08/09/23 07:49 98-06-608/08/23 21:440.0075 0.0027 1
Carbon tetrachloride ND mg/kg 08/09/23 07:49 56-23-508/08/23 21:440.0075 0.0028 1
Chlorobenzene ND mg/kg 08/09/23 07:49 108-90-708/08/23 21:440.0075 0.0043 1
Chloroethane ND mg/kg 08/09/23 07:49 75-00-308/08/23 21:440.015 0.0058 1
Chloroform ND mg/kg 08/09/23 07:49 67-66-308/08/23 21:440.0075 0.0063 1
Chloromethane ND mg/kg 08/09/23 07:49 74-87-308/08/23 21:440.015 0.0063 1
2-Chlorotoluene ND mg/kg 08/09/23 07:49 95-49-808/08/23 21:440.0075 0.0027 1
4-Chlorotoluene ND mg/kg 08/09/23 07:49 106-43-408/08/23 21:440.0075 0.0042 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/09/23 07:49 96-12-808/08/23 21:440.0075 0.0029 1
Dibromochloromethane ND mg/kg 08/09/23 07:49 124-48-108/08/23 21:440.0075 0.0042 1
1,2-Dibromoethane (EDB)ND mg/kg 08/09/23 07:49 106-93-408/08/23 21:440.0075 0.0033 1
Dibromomethane ND mg/kg 08/09/23 07:49 74-95-308/08/23 21:440.0075 0.0016 1
1,2-Dichlorobenzene ND mg/kg 08/09/23 07:49 95-50-108/08/23 21:440.0075 0.0027 1
1,3-Dichlorobenzene ND mg/kg 08/09/23 07:49 541-73-108/08/23 21:440.0075 0.0023 1
1,4-Dichlorobenzene ND mg/kg 08/09/23 07:49 106-46-708/08/23 21:440.0075 0.0020 1
Dichlorodifluoromethane ND mg/kg 08/09/23 07:49 75-71-808/08/23 21:440.015 0.0077 1
1,1-Dichloroethane ND mg/kg 08/09/23 07:49 75-34-308/08/23 21:440.0075 0.0031 1
1,2-Dichloroethane ND mg/kg 08/09/23 07:49 107-06-208/08/23 21:440.0075 0.0050 1
1,1-Dichloroethene ND mg/kg 08/09/23 07:49 75-35-408/08/23 21:440.0075 0.0031 1
cis-1,2-Dichloroethene ND mg/kg 08/09/23 07:49 156-59-208/08/23 21:440.0075 0.0026 1
trans-1,2-Dichloroethene ND mg/kg 08/09/23 07:49 156-60-508/08/23 21:440.0075 0.0064 1
1,2-Dichloropropane ND mg/kg 08/09/23 07:49 78-87-508/08/23 21:440.0075 0.0023 1
1,3-Dichloropropane ND mg/kg 08/09/23 07:49 142-28-908/08/23 21:440.0075 0.0023 1
2,2-Dichloropropane ND mg/kg 08/09/23 07:49 594-20-708/08/23 21:440.0075 0.0057 1
1,1-Dichloropropene ND mg/kg 08/09/23 07:49 563-58-608/08/23 21:440.0075 0.0036 1
cis-1,3-Dichloropropene ND mg/kg 08/09/23 07:49 10061-01-508/08/23 21:440.0075 0.0020 1
trans-1,3-Dichloropropene ND mg/kg 08/09/23 07:49 10061-02-608/08/23 21:440.0075 0.0026 1
Diisopropyl ether ND mg/kg 08/09/23 07:49 108-20-308/08/23 21:440.0075 0.0020 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-10 Lab ID:92681077010 Collected:08/04/23 10:40 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/09/23 07:49 100-41-408/08/23 21:440.0075 0.0035 1
Hexachloro-1,3-butadiene ND mg/kg 08/09/23 07:49 87-68-308/08/23 21:440.015 0.012 1
2-Hexanone ND mg/kg 08/09/23 07:49 591-78-608/08/23 21:440.075 0.0072 1
Isopropylbenzene (Cumene)ND mg/kg 08/09/23 07:49 98-82-808/08/23 21:440.0075 0.0026 1
p-Isopropyltoluene ND mg/kg 08/09/23 07:49 99-87-608/08/23 21:440.0075 0.0037 1
Methylene Chloride ND mg/kg 08/09/23 07:49 75-09-208/08/23 21:440.030 0.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/09/23 07:49 108-10-108/08/23 21:440.075 0.0072 1
Methyl-tert-butyl ether ND mg/kg 08/09/23 07:49 1634-04-408/08/23 21:440.0075 0.0028 1
Naphthalene ND mg/kg 08/09/23 07:49 91-20-308/08/23 21:440.0075 0.0040 1
n-Propylbenzene ND mg/kg 08/09/23 07:49 103-65-108/08/23 21:440.0075 0.0027 1
Styrene ND mg/kg 08/09/23 07:49 100-42-508/08/23 21:440.0075 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/09/23 07:49 630-20-608/08/23 21:440.0075 0.0029 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/09/23 07:49 79-34-508/08/23 21:440.0075 0.0020 1
Tetrachloroethene ND mg/kg 08/09/23 07:49 127-18-408/08/23 21:440.0075 0.0024 1
Toluene ND mg/kg 08/09/23 07:49 108-88-308/08/23 21:440.0075 0.0052 1
1,2,3-Trichlorobenzene ND mg/kg 08/09/23 07:49 87-61-608/08/23 21:440.0075 0.0061 1
1,2,4-Trichlorobenzene ND mg/kg 08/09/23 07:49 120-82-1 IK08/08/23 21:440.0075 0.0063 1
1,1,1-Trichloroethane ND mg/kg 08/09/23 07:49 71-55-608/08/23 21:440.0075 0.0039 1
1,1,2-Trichloroethane ND mg/kg 08/09/23 07:49 79-00-508/08/23 21:440.0075 0.0025 1
Trichloroethene ND mg/kg 08/09/23 07:49 79-01-608/08/23 21:440.0075 0.0061 1
Trichlorofluoromethane ND mg/kg 08/09/23 07:49 75-69-408/08/23 21:440.0075 0.0041 1
1,2,3-Trichloropropane ND mg/kg 08/09/23 07:49 96-18-408/08/23 21:440.0075 0.0038 1
1,2,4-Trimethylbenzene ND mg/kg 08/09/23 07:49 95-63-608/08/23 21:440.0075 0.0045 1
1,3,5-Trimethylbenzene ND mg/kg 08/09/23 07:49 108-67-808/08/23 21:440.0075 0.0025 1
Vinyl acetate ND mg/kg 08/09/23 07:49 108-05-408/08/23 21:440.075 0.015 1
Vinyl chloride ND mg/kg 08/09/23 07:49 75-01-408/08/23 21:440.015 0.0038 1
Xylene (Total)ND mg/kg 08/09/23 07:49 1330-20-708/08/23 21:440.015 0.0043 1
m&p-Xylene ND mg/kg 08/09/23 07:49 179601-23-108/08/23 21:440.015 0.0051 1
o-Xylene ND mg/kg 08/09/23 07:49 95-47-608/08/23 21:440.0075 0.0033 1
Surrogates
Toluene-d8 (S)103 %08/09/23 07:49 2037-26-508/08/23 21:4470-130 1
4-Bromofluorobenzene (S)104 %08/09/23 07:49 460-00-408/08/23 21:4470-130 1
1,2-Dichloroethane-d4 (S)111 %08/09/23 07:49 17060-07-008/08/23 21:4470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.6 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 75.2 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:P1-10 Lab ID:92681077010 Collected:08/04/23 10:40 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/14/23 19:44 18540-29-908/13/23 18:151.33 0.339 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-1 Lab ID:92681077011 Collected:08/04/23 10:59 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 9.07 mg/kg 08/13/23 16:48 7440-38-208/10/23 09:481.30 0.130 5
Barium 194 mg/kg 08/13/23 17:14 7440-39-308/10/23 09:4813.0 0.793 20
Cadmium 0.423J mg/kg 08/13/23 16:48 7440-43-9 J08/10/23 09:481.30 0.111 5
Chromium 46.8 mg/kg 08/13/23 16:48 7440-47-308/10/23 09:486.52 0.386 5
Lead 268 mg/kg 08/13/23 17:14 7439-92-108/10/23 09:4810.4 0.516 20
Selenium 1.30J mg/kg 08/13/23 16:48 7782-49-2 J08/10/23 09:483.26 0.235 5
Silver 0.245J mg/kg 08/13/23 16:48 7440-22-4 J08/10/23 09:480.652 0.113 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.205 mg/kg 08/15/23 14:22 7439-97-608/14/23 20:110.0522 0.0235 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/15/23 14:11 83-32-908/14/23 17:160.42 0.15 1
Acenaphthylene ND mg/kg 08/15/23 14:11 208-96-808/14/23 17:160.42 0.15 1
Aniline ND mg/kg 08/15/23 14:11 62-53-308/14/23 17:160.42 0.17 1
Anthracene ND mg/kg 08/15/23 14:11 120-12-708/14/23 17:160.42 0.14 1
Benzo(a)anthracene ND mg/kg 08/15/23 14:11 56-55-308/14/23 17:160.42 0.14 1
Benzo(a)pyrene ND mg/kg 08/15/23 14:11 50-32-808/14/23 17:160.42 0.15 1
Benzo(b)fluoranthene ND mg/kg 08/15/23 14:11 205-99-208/14/23 17:160.42 0.14 1
Benzo(g,h,i)perylene ND mg/kg 08/15/23 14:11 191-24-208/14/23 17:160.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 08/15/23 14:11 207-08-908/14/23 17:160.42 0.15 1
Benzoic Acid ND mg/kg 08/15/23 14:11 65-85-008/14/23 17:162.1 0.91 1
Benzyl alcohol ND mg/kg 08/15/23 14:11 100-51-608/14/23 17:160.85 0.32 1
4-Bromophenylphenyl ether ND mg/kg 08/15/23 14:11 101-55-308/14/23 17:160.42 0.16 1
Butylbenzylphthalate ND mg/kg 08/15/23 14:11 85-68-708/14/23 17:160.42 0.18 1
4-Chloro-3-methylphenol ND mg/kg 08/15/23 14:11 59-50-708/14/23 17:160.85 0.30 1
4-Chloroaniline ND mg/kg 08/15/23 14:11 106-47-808/14/23 17:160.85 0.33 1
bis(2-Chloroethoxy)methane ND mg/kg 08/15/23 14:11 111-91-108/14/23 17:160.42 0.18 1
bis(2-Chloroethyl) ether ND mg/kg 08/15/23 14:11 111-44-408/14/23 17:160.42 0.16 1
2-Chloronaphthalene ND mg/kg 08/15/23 14:11 91-58-708/14/23 17:160.42 0.17 1
2-Chlorophenol ND mg/kg 08/15/23 14:11 95-57-808/14/23 17:160.42 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 08/15/23 14:11 7005-72-308/14/23 17:160.42 0.16 1
Chrysene ND mg/kg 08/15/23 14:11 218-01-908/14/23 17:160.42 0.15 1
Dibenz(a,h)anthracene ND mg/kg 08/15/23 14:11 53-70-308/14/23 17:160.42 0.16 1
Dibenzofuran ND mg/kg 08/15/23 14:11 132-64-908/14/23 17:160.42 0.15 1
1,2-Dichlorobenzene ND mg/kg 08/15/23 14:11 95-50-108/14/23 17:160.42 0.15 1
1,3-Dichlorobenzene ND mg/kg 08/15/23 14:11 541-73-108/14/23 17:160.42 0.15 1
1,4-Dichlorobenzene ND mg/kg 08/15/23 14:11 106-46-708/14/23 17:160.42 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 08/15/23 14:11 91-94-108/14/23 17:160.85 0.29 1
2,4-Dichlorophenol ND mg/kg 08/15/23 14:11 120-83-208/14/23 17:160.42 0.17 1
Diethylphthalate ND mg/kg 08/15/23 14:11 84-66-208/14/23 17:160.42 0.16 1
2,4-Dimethylphenol ND mg/kg 08/15/23 14:11 105-67-908/14/23 17:160.42 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-1 Lab ID:92681077011 Collected:08/04/23 10:59 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/15/23 14:11 131-11-308/14/23 17:160.42 0.15 1
Di-n-butylphthalate ND mg/kg 08/15/23 14:11 84-74-208/14/23 17:160.42 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/15/23 14:11 534-52-108/14/23 17:160.85 0.40 1
2,4-Dinitrophenol ND mg/kg 08/15/23 14:11 51-28-508/14/23 17:162.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/15/23 14:11 121-14-208/14/23 17:160.42 0.16 1
2,6-Dinitrotoluene ND mg/kg 08/15/23 14:11 606-20-208/14/23 17:160.42 0.16 1
Di-n-octylphthalate ND mg/kg 08/15/23 14:11 117-84-008/14/23 17:160.42 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/15/23 14:11 117-81-708/14/23 17:160.42 0.16 1
Fluoranthene ND mg/kg 08/15/23 14:11 206-44-008/14/23 17:160.42 0.15 1
Fluorene ND mg/kg 08/15/23 14:11 86-73-708/14/23 17:160.42 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 08/15/23 14:11 87-68-308/14/23 17:160.42 0.18 1
Hexachlorobenzene ND mg/kg 08/15/23 14:11 118-74-108/14/23 17:160.42 0.17 1
Hexachlorocyclopentadiene ND mg/kg 08/15/23 14:11 77-47-408/14/23 17:160.42 0.24 1
Hexachloroethane ND mg/kg 08/15/23 14:11 67-72-108/14/23 17:160.42 0.16 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/15/23 14:11 193-39-508/14/23 17:160.42 0.17 1
Isophorone ND mg/kg 08/15/23 14:11 78-59-108/14/23 17:160.42 0.19 1
1-Methylnaphthalene ND mg/kg 08/15/23 14:11 90-12-008/14/23 17:160.42 0.15 1
2-Methylnaphthalene ND mg/kg 08/15/23 14:11 91-57-608/14/23 17:160.42 0.17 1
2-Methylphenol(o-Cresol)ND mg/kg 08/15/23 14:11 95-48-708/14/23 17:160.42 0.17 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/15/23 14:11 15831-10-408/14/23 17:160.42 0.17 1
Naphthalene ND mg/kg 08/15/23 14:11 91-20-308/14/23 17:160.42 0.14 1
2-Nitroaniline ND mg/kg 08/15/23 14:11 88-74-408/14/23 17:162.1 0.35 1
3-Nitroaniline ND mg/kg 08/15/23 14:11 99-09-208/14/23 17:162.1 0.33 1
4-Nitroaniline ND mg/kg 08/15/23 14:11 100-01-608/14/23 17:160.85 0.32 1
Nitrobenzene ND mg/kg 08/15/23 14:11 98-95-308/14/23 17:160.42 0.20 1
2-Nitrophenol ND mg/kg 08/15/23 14:11 88-75-508/14/23 17:160.42 0.18 1
4-Nitrophenol ND mg/kg 08/15/23 14:11 100-02-708/14/23 17:162.1 0.82 1
N-Nitrosodimethylamine ND mg/kg 08/15/23 14:11 62-75-908/14/23 17:160.42 0.14 1
N-Nitroso-di-n-propylamine ND mg/kg 08/15/23 14:11 621-64-708/14/23 17:160.42 0.16 1
N-Nitrosodiphenylamine ND mg/kg 08/15/23 14:11 86-30-608/14/23 17:160.42 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/15/23 14:11 108-60-108/14/23 17:160.42 0.20 1
Pentachlorophenol ND mg/kg 08/15/23 14:11 87-86-508/14/23 17:160.85 0.41 1
Phenanthrene ND mg/kg 08/15/23 14:11 85-01-808/14/23 17:160.42 0.14 1
Phenol ND mg/kg 08/15/23 14:11 108-95-208/14/23 17:160.42 0.19 1
Pyrene ND mg/kg 08/15/23 14:11 129-00-008/14/23 17:160.42 0.17 1
Pyridine ND mg/kg 08/15/23 14:11 110-86-108/14/23 17:160.42 0.13 1
1,2,4-Trichlorobenzene ND mg/kg 08/15/23 14:11 120-82-108/14/23 17:160.42 0.17 1
2,4,5-Trichlorophenol ND mg/kg 08/15/23 14:11 95-95-408/14/23 17:160.42 0.19 1
2,4,6-Trichlorophenol ND mg/kg 08/15/23 14:11 88-06-208/14/23 17:160.42 0.17 1
Surrogates
Nitrobenzene-d5 (S)52 %08/15/23 14:11 4165-60-008/14/23 17:1610-130 1
2-Fluorobiphenyl (S)50 %08/15/23 14:11 321-60-808/14/23 17:1610-130 1
Terphenyl-d14 (S)81 %08/15/23 14:11 1718-51-008/14/23 17:1610-130 1
Phenol-d6 (S)46 %08/15/23 14:11 13127-88-308/14/23 17:1610-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-1 Lab ID:92681077011 Collected:08/04/23 10:59 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)47 %08/15/23 14:11 367-12-408/14/23 17:1610-130 1
2,4,6-Tribromophenol (S)71 %08/15/23 14:11 118-79-608/14/23 17:1610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/10/23 01:45 67-64-108/09/23 16:220.15 0.047 1
Benzene ND mg/kg 08/10/23 01:45 71-43-208/09/23 16:220.0074 0.0029 1
Bromobenzene ND mg/kg 08/10/23 01:45 108-86-108/09/23 16:220.0074 0.0024 1
Bromochloromethane ND mg/kg 08/10/23 01:45 74-97-508/09/23 16:220.0074 0.0022 1
Bromodichloromethane ND mg/kg 08/10/23 01:45 75-27-408/09/23 16:220.0074 0.0028 1
Bromoform ND mg/kg 08/10/23 01:45 75-25-208/09/23 16:220.0074 0.0026 1
Bromomethane ND mg/kg 08/10/23 01:45 74-83-9 v208/09/23 16:220.029 0.023 1
2-Butanone (MEK)ND mg/kg 08/10/23 01:45 78-93-308/09/23 16:220.15 0.035 1
n-Butylbenzene ND mg/kg 08/10/23 01:45 104-51-808/09/23 16:220.0074 0.0046 1
sec-Butylbenzene ND mg/kg 08/10/23 01:45 135-98-808/09/23 16:220.0074 0.0032 1
tert-Butylbenzene ND mg/kg 08/10/23 01:45 98-06-608/09/23 16:220.0074 0.0026 1
Carbon tetrachloride ND mg/kg 08/10/23 01:45 56-23-508/09/23 16:220.0074 0.0028 1
Chlorobenzene ND mg/kg 08/10/23 01:45 108-90-708/09/23 16:220.0074 0.0042 1
Chloroethane ND mg/kg 08/10/23 01:45 75-00-308/09/23 16:220.015 0.0057 1
Chloroform ND mg/kg 08/10/23 01:45 67-66-308/09/23 16:220.0074 0.0062 1
Chloromethane ND mg/kg 08/10/23 01:45 74-87-308/09/23 16:220.015 0.0062 1
2-Chlorotoluene ND mg/kg 08/10/23 01:45 95-49-808/09/23 16:220.0074 0.0026 1
4-Chlorotoluene ND mg/kg 08/10/23 01:45 106-43-408/09/23 16:220.0074 0.0041 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/10/23 01:45 96-12-808/09/23 16:220.0074 0.0029 1
Dibromochloromethane ND mg/kg 08/10/23 01:45 124-48-108/09/23 16:220.0074 0.0041 1
1,2-Dibromoethane (EDB)ND mg/kg 08/10/23 01:45 106-93-408/09/23 16:220.0074 0.0032 1
Dibromomethane ND mg/kg 08/10/23 01:45 74-95-308/09/23 16:220.0074 0.0016 1
1,2-Dichlorobenzene ND mg/kg 08/10/23 01:45 95-50-108/09/23 16:220.0074 0.0027 1
1,3-Dichlorobenzene ND mg/kg 08/10/23 01:45 541-73-108/09/23 16:220.0074 0.0023 1
1,4-Dichlorobenzene ND mg/kg 08/10/23 01:45 106-46-708/09/23 16:220.0074 0.0019 1
Dichlorodifluoromethane ND mg/kg 08/10/23 01:45 75-71-8 L1,v108/09/23 16:220.015 0.0075 1
1,1-Dichloroethane ND mg/kg 08/10/23 01:45 75-34-308/09/23 16:220.0074 0.0030 1
1,2-Dichloroethane ND mg/kg 08/10/23 01:45 107-06-208/09/23 16:220.0074 0.0049 1
1,1-Dichloroethene ND mg/kg 08/10/23 01:45 75-35-408/09/23 16:220.0074 0.0030 1
cis-1,2-Dichloroethene ND mg/kg 08/10/23 01:45 156-59-208/09/23 16:220.0074 0.0025 1
trans-1,2-Dichloroethene ND mg/kg 08/10/23 01:45 156-60-508/09/23 16:220.0074 0.0063 1
1,2-Dichloropropane ND mg/kg 08/10/23 01:45 78-87-508/09/23 16:220.0074 0.0022 1
1,3-Dichloropropane ND mg/kg 08/10/23 01:45 142-28-908/09/23 16:220.0074 0.0023 1
2,2-Dichloropropane ND mg/kg 08/10/23 01:45 594-20-708/09/23 16:220.0074 0.0056 1
1,1-Dichloropropene ND mg/kg 08/10/23 01:45 563-58-608/09/23 16:220.0074 0.0035 1
cis-1,3-Dichloropropene ND mg/kg 08/10/23 01:45 10061-01-508/09/23 16:220.0074 0.0020 1
trans-1,3-Dichloropropene ND mg/kg 08/10/23 01:45 10061-02-608/09/23 16:220.0074 0.0025 1
Diisopropyl ether ND mg/kg 08/10/23 01:45 108-20-308/09/23 16:220.0074 0.0020 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-1 Lab ID:92681077011 Collected:08/04/23 10:59 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/10/23 01:45 100-41-408/09/23 16:220.0074 0.0034 1
Hexachloro-1,3-butadiene ND mg/kg 08/10/23 01:45 87-68-308/09/23 16:220.015 0.012 1
2-Hexanone ND mg/kg 08/10/23 01:45 591-78-608/09/23 16:220.074 0.0071 1
Isopropylbenzene (Cumene)ND mg/kg 08/10/23 01:45 98-82-808/09/23 16:220.0074 0.0025 1
p-Isopropyltoluene ND mg/kg 08/10/23 01:45 99-87-608/09/23 16:220.0074 0.0036 1
Methylene Chloride ND mg/kg 08/10/23 01:45 75-09-208/09/23 16:220.029 0.020 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/10/23 01:45 108-10-108/09/23 16:220.074 0.0071 1
Methyl-tert-butyl ether ND mg/kg 08/10/23 01:45 1634-04-408/09/23 16:220.0074 0.0028 1
Naphthalene ND mg/kg 08/10/23 01:45 91-20-308/09/23 16:220.0074 0.0039 1
n-Propylbenzene ND mg/kg 08/10/23 01:45 103-65-108/09/23 16:220.0074 0.0026 1
Styrene ND mg/kg 08/10/23 01:45 100-42-508/09/23 16:220.0074 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/10/23 01:45 630-20-608/09/23 16:220.0074 0.0028 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/10/23 01:45 79-34-508/09/23 16:220.0074 0.0019 1
Tetrachloroethene ND mg/kg 08/10/23 01:45 127-18-408/09/23 16:220.0074 0.0023 1
Toluene ND mg/kg 08/10/23 01:45 108-88-308/09/23 16:220.0074 0.0051 1
1,2,3-Trichlorobenzene ND mg/kg 08/10/23 01:45 87-61-608/09/23 16:220.0074 0.0060 1
1,2,4-Trichlorobenzene ND mg/kg 08/10/23 01:45 120-82-1 IK08/09/23 16:220.0074 0.0062 1
1,1,1-Trichloroethane ND mg/kg 08/10/23 01:45 71-55-608/09/23 16:220.0074 0.0038 1
1,1,2-Trichloroethane ND mg/kg 08/10/23 01:45 79-00-508/09/23 16:220.0074 0.0024 1
Trichloroethene ND mg/kg 08/10/23 01:45 79-01-608/09/23 16:220.0074 0.0059 1
Trichlorofluoromethane ND mg/kg 08/10/23 01:45 75-69-408/09/23 16:220.0074 0.0041 1
1,2,3-Trichloropropane ND mg/kg 08/10/23 01:45 96-18-408/09/23 16:220.0074 0.0037 1
1,2,4-Trimethylbenzene ND mg/kg 08/10/23 01:45 95-63-608/09/23 16:220.0074 0.0044 1
1,3,5-Trimethylbenzene ND mg/kg 08/10/23 01:45 108-67-808/09/23 16:220.0074 0.0025 1
Vinyl acetate ND mg/kg 08/10/23 01:45 108-05-408/09/23 16:220.074 0.015 1
Vinyl chloride ND mg/kg 08/10/23 01:45 75-01-408/09/23 16:220.015 0.0037 1
Xylene (Total)ND mg/kg 08/10/23 01:45 1330-20-708/09/23 16:220.015 0.0042 1
m&p-Xylene ND mg/kg 08/10/23 01:45 179601-23-108/09/23 16:220.015 0.0050 1
o-Xylene ND mg/kg 08/10/23 01:45 95-47-608/09/23 16:220.0074 0.0033 1
Surrogates
Toluene-d8 (S)101 %08/10/23 01:45 2037-26-508/09/23 16:2270-130 1
4-Bromofluorobenzene (S)100 %08/10/23 01:45 460-00-408/09/23 16:2270-130 1
1,2-Dichloroethane-d4 (S)108 %08/10/23 01:45 17060-07-008/09/23 16:2270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.4 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.7 %08/10/23 07:0708/10/23 06:581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-1 Lab ID:92681077011 Collected:08/04/23 10:59 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/14/23 19:55 18540-29-908/13/23 18:151.30 0.333 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-2 Lab ID:92681077012 Collected:08/04/23 11:05 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.20 mg/kg 08/13/23 16:51 7440-38-208/10/23 09:481.44 0.144 5
Barium 25.3 mg/kg 08/13/23 16:51 7440-39-308/10/23 09:483.61 0.220 5
Cadmium ND mg/kg 08/13/23 16:51 7440-43-908/10/23 09:481.44 0.124 5
Chromium 632 mg/kg 08/13/23 17:18 7440-47-308/10/23 09:4872.2 4.28 50
Lead 15.3 mg/kg 08/13/23 16:51 7439-92-108/10/23 09:482.89 0.143 5
Selenium 0.837J mg/kg 08/13/23 16:51 7782-49-2 J08/10/23 09:483.61 0.260 5
Silver ND mg/kg 08/13/23 16:51 7440-22-408/10/23 09:480.722 0.125 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0313J mg/kg 08/15/23 14:25 7439-97-6 J08/14/23 20:110.0578 0.0260 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/15/23 14:39 83-32-908/14/23 17:160.45 0.16 1
Acenaphthylene ND mg/kg 08/15/23 14:39 208-96-808/14/23 17:160.45 0.16 1
Aniline ND mg/kg 08/15/23 14:39 62-53-308/14/23 17:160.45 0.18 1
Anthracene ND mg/kg 08/15/23 14:39 120-12-708/14/23 17:160.45 0.15 1
Benzo(a)anthracene ND mg/kg 08/15/23 14:39 56-55-308/14/23 17:160.45 0.15 1
Benzo(a)pyrene ND mg/kg 08/15/23 14:39 50-32-808/14/23 17:160.45 0.16 1
Benzo(b)fluoranthene ND mg/kg 08/15/23 14:39 205-99-208/14/23 17:160.45 0.15 1
Benzo(g,h,i)perylene ND mg/kg 08/15/23 14:39 191-24-208/14/23 17:160.45 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/15/23 14:39 207-08-908/14/23 17:160.45 0.16 1
Benzoic Acid ND mg/kg 08/15/23 14:39 65-85-008/14/23 17:162.2 0.97 1
Benzyl alcohol ND mg/kg 08/15/23 14:39 100-51-608/14/23 17:160.90 0.34 1
4-Bromophenylphenyl ether ND mg/kg 08/15/23 14:39 101-55-308/14/23 17:160.45 0.17 1
Butylbenzylphthalate ND mg/kg 08/15/23 14:39 85-68-708/14/23 17:160.45 0.19 1
4-Chloro-3-methylphenol ND mg/kg 08/15/23 14:39 59-50-708/14/23 17:160.90 0.32 1
4-Chloroaniline ND mg/kg 08/15/23 14:39 106-47-808/14/23 17:160.90 0.35 1
bis(2-Chloroethoxy)methane ND mg/kg 08/15/23 14:39 111-91-108/14/23 17:160.45 0.19 1
bis(2-Chloroethyl) ether ND mg/kg 08/15/23 14:39 111-44-408/14/23 17:160.45 0.17 1
2-Chloronaphthalene ND mg/kg 08/15/23 14:39 91-58-708/14/23 17:160.45 0.18 1
2-Chlorophenol ND mg/kg 08/15/23 14:39 95-57-808/14/23 17:160.45 0.17 1
4-Chlorophenylphenyl ether ND mg/kg 08/15/23 14:39 7005-72-308/14/23 17:160.45 0.17 1
Chrysene ND mg/kg 08/15/23 14:39 218-01-908/14/23 17:160.45 0.16 1
Dibenz(a,h)anthracene ND mg/kg 08/15/23 14:39 53-70-308/14/23 17:160.45 0.17 1
Dibenzofuran ND mg/kg 08/15/23 14:39 132-64-908/14/23 17:160.45 0.16 1
1,2-Dichlorobenzene ND mg/kg 08/15/23 14:39 95-50-108/14/23 17:160.45 0.16 1
1,3-Dichlorobenzene ND mg/kg 08/15/23 14:39 541-73-108/14/23 17:160.45 0.16 1
1,4-Dichlorobenzene ND mg/kg 08/15/23 14:39 106-46-708/14/23 17:160.45 0.17 1
3,3'-Dichlorobenzidine ND mg/kg 08/15/23 14:39 91-94-108/14/23 17:160.90 0.30 1
2,4-Dichlorophenol ND mg/kg 08/15/23 14:39 120-83-208/14/23 17:160.45 0.18 1
Diethylphthalate ND mg/kg 08/15/23 14:39 84-66-208/14/23 17:160.45 0.16 1
2,4-Dimethylphenol ND mg/kg 08/15/23 14:39 105-67-908/14/23 17:160.45 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-2 Lab ID:92681077012 Collected:08/04/23 11:05 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/15/23 14:39 131-11-308/14/23 17:160.45 0.16 1
Di-n-butylphthalate ND mg/kg 08/15/23 14:39 84-74-208/14/23 17:160.45 0.15 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/15/23 14:39 534-52-108/14/23 17:160.90 0.42 1
2,4-Dinitrophenol ND mg/kg 08/15/23 14:39 51-28-508/14/23 17:162.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 08/15/23 14:39 121-14-208/14/23 17:160.45 0.17 1
2,6-Dinitrotoluene ND mg/kg 08/15/23 14:39 606-20-208/14/23 17:160.45 0.16 1
Di-n-octylphthalate ND mg/kg 08/15/23 14:39 117-84-008/14/23 17:160.45 0.18 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/15/23 14:39 117-81-708/14/23 17:160.45 0.17 1
Fluoranthene ND mg/kg 08/15/23 14:39 206-44-008/14/23 17:160.45 0.15 1
Fluorene ND mg/kg 08/15/23 14:39 86-73-708/14/23 17:160.45 0.16 1
Hexachloro-1,3-butadiene ND mg/kg 08/15/23 14:39 87-68-308/14/23 17:160.45 0.19 1
Hexachlorobenzene ND mg/kg 08/15/23 14:39 118-74-108/14/23 17:160.45 0.18 1
Hexachlorocyclopentadiene ND mg/kg 08/15/23 14:39 77-47-408/14/23 17:160.45 0.26 1
Hexachloroethane ND mg/kg 08/15/23 14:39 67-72-108/14/23 17:160.45 0.17 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/15/23 14:39 193-39-508/14/23 17:160.45 0.18 1
Isophorone ND mg/kg 08/15/23 14:39 78-59-108/14/23 17:160.45 0.20 1
1-Methylnaphthalene ND mg/kg 08/15/23 14:39 90-12-008/14/23 17:160.45 0.16 1
2-Methylnaphthalene ND mg/kg 08/15/23 14:39 91-57-608/14/23 17:160.45 0.18 1
2-Methylphenol(o-Cresol)ND mg/kg 08/15/23 14:39 95-48-708/14/23 17:160.45 0.18 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/15/23 14:39 15831-10-408/14/23 17:160.45 0.18 1
Naphthalene ND mg/kg 08/15/23 14:39 91-20-308/14/23 17:160.45 0.15 1
2-Nitroaniline ND mg/kg 08/15/23 14:39 88-74-408/14/23 17:162.2 0.37 1
3-Nitroaniline ND mg/kg 08/15/23 14:39 99-09-208/14/23 17:162.2 0.35 1
4-Nitroaniline ND mg/kg 08/15/23 14:39 100-01-608/14/23 17:160.90 0.34 1
Nitrobenzene ND mg/kg 08/15/23 14:39 98-95-308/14/23 17:160.45 0.21 1
2-Nitrophenol ND mg/kg 08/15/23 14:39 88-75-508/14/23 17:160.45 0.19 1
4-Nitrophenol ND mg/kg 08/15/23 14:39 100-02-708/14/23 17:162.2 0.87 1
N-Nitrosodimethylamine ND mg/kg 08/15/23 14:39 62-75-908/14/23 17:160.45 0.15 1
N-Nitroso-di-n-propylamine ND mg/kg 08/15/23 14:39 621-64-708/14/23 17:160.45 0.17 1
N-Nitrosodiphenylamine ND mg/kg 08/15/23 14:39 86-30-608/14/23 17:160.45 0.16 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/15/23 14:39 108-60-108/14/23 17:160.45 0.21 1
Pentachlorophenol ND mg/kg 08/15/23 14:39 87-86-508/14/23 17:160.90 0.44 1
Phenanthrene ND mg/kg 08/15/23 14:39 85-01-808/14/23 17:160.45 0.15 1
Phenol ND mg/kg 08/15/23 14:39 108-95-208/14/23 17:160.45 0.20 1
Pyrene ND mg/kg 08/15/23 14:39 129-00-008/14/23 17:160.45 0.18 1
Pyridine ND mg/kg 08/15/23 14:39 110-86-108/14/23 17:160.45 0.14 1
1,2,4-Trichlorobenzene ND mg/kg 08/15/23 14:39 120-82-108/14/23 17:160.45 0.18 1
2,4,5-Trichlorophenol ND mg/kg 08/15/23 14:39 95-95-408/14/23 17:160.45 0.21 1
2,4,6-Trichlorophenol ND mg/kg 08/15/23 14:39 88-06-208/14/23 17:160.45 0.19 1
Surrogates
Nitrobenzene-d5 (S)58 %08/15/23 14:39 4165-60-008/14/23 17:1610-130 1
2-Fluorobiphenyl (S)58 %08/15/23 14:39 321-60-808/14/23 17:1610-130 1
Terphenyl-d14 (S)81 %08/15/23 14:39 1718-51-008/14/23 17:1610-130 1
Phenol-d6 (S)54 %08/15/23 14:39 13127-88-308/14/23 17:1610-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-2 Lab ID:92681077012 Collected:08/04/23 11:05 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)55 %08/15/23 14:39 367-12-408/14/23 17:1610-130 1
2,4,6-Tribromophenol (S)82 %08/15/23 14:39 118-79-608/14/23 17:1610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/10/23 02:37 67-64-108/09/23 23:150.17 0.056 1
Benzene ND mg/kg 08/10/23 02:37 71-43-208/09/23 23:150.0087 0.0035 1
Bromobenzene ND mg/kg 08/10/23 02:37 108-86-108/09/23 23:150.0087 0.0028 1
Bromochloromethane ND mg/kg 08/10/23 02:37 74-97-508/09/23 23:150.0087 0.0026 1
Bromodichloromethane ND mg/kg 08/10/23 02:37 75-27-408/09/23 23:150.0087 0.0034 1
Bromoform ND mg/kg 08/10/23 02:37 75-25-208/09/23 23:150.0087 0.0031 1
Bromomethane ND mg/kg 08/10/23 02:37 74-83-9 v208/09/23 23:150.035 0.027 1
2-Butanone (MEK)ND mg/kg 08/10/23 02:37 78-93-308/09/23 23:150.17 0.042 1
n-Butylbenzene ND mg/kg 08/10/23 02:37 104-51-808/09/23 23:150.0087 0.0055 1
sec-Butylbenzene ND mg/kg 08/10/23 02:37 135-98-808/09/23 23:150.0087 0.0038 1
tert-Butylbenzene ND mg/kg 08/10/23 02:37 98-06-608/09/23 23:150.0087 0.0031 1
Carbon tetrachloride ND mg/kg 08/10/23 02:37 56-23-508/09/23 23:150.0087 0.0033 1
Chlorobenzene ND mg/kg 08/10/23 02:37 108-90-708/09/23 23:150.0087 0.0050 1
Chloroethane ND mg/kg 08/10/23 02:37 75-00-308/09/23 23:150.017 0.0067 1
Chloroform ND mg/kg 08/10/23 02:37 67-66-308/09/23 23:150.0087 0.0073 1
Chloromethane ND mg/kg 08/10/23 02:37 74-87-308/09/23 23:150.017 0.0073 1
2-Chlorotoluene ND mg/kg 08/10/23 02:37 95-49-808/09/23 23:150.0087 0.0031 1
4-Chlorotoluene ND mg/kg 08/10/23 02:37 106-43-408/09/23 23:150.0087 0.0048 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/10/23 02:37 96-12-808/09/23 23:150.0087 0.0034 1
Dibromochloromethane ND mg/kg 08/10/23 02:37 124-48-108/09/23 23:150.0087 0.0049 1
1,2-Dibromoethane (EDB)ND mg/kg 08/10/23 02:37 106-93-408/09/23 23:150.0087 0.0038 1
Dibromomethane ND mg/kg 08/10/23 02:37 74-95-308/09/23 23:150.0087 0.0019 1
1,2-Dichlorobenzene ND mg/kg 08/10/23 02:37 95-50-108/09/23 23:150.0087 0.0031 1
1,3-Dichlorobenzene ND mg/kg 08/10/23 02:37 541-73-108/09/23 23:150.0087 0.0027 1
1,4-Dichlorobenzene ND mg/kg 08/10/23 02:37 106-46-708/09/23 23:150.0087 0.0023 1
Dichlorodifluoromethane ND mg/kg 08/10/23 02:37 75-71-8 v108/09/23 23:150.017 0.0089 1
1,1-Dichloroethane ND mg/kg 08/10/23 02:37 75-34-308/09/23 23:150.0087 0.0036 1
1,2-Dichloroethane ND mg/kg 08/10/23 02:37 107-06-208/09/23 23:150.0087 0.0058 1
1,1-Dichloroethene ND mg/kg 08/10/23 02:37 75-35-408/09/23 23:150.0087 0.0036 1
cis-1,2-Dichloroethene ND mg/kg 08/10/23 02:37 156-59-208/09/23 23:150.0087 0.0030 1
trans-1,2-Dichloroethene ND mg/kg 08/10/23 02:37 156-60-508/09/23 23:150.0087 0.0074 1
1,2-Dichloropropane ND mg/kg 08/10/23 02:37 78-87-508/09/23 23:150.0087 0.0026 1
1,3-Dichloropropane ND mg/kg 08/10/23 02:37 142-28-908/09/23 23:150.0087 0.0027 1
2,2-Dichloropropane ND mg/kg 08/10/23 02:37 594-20-708/09/23 23:150.0087 0.0066 1
1,1-Dichloropropene ND mg/kg 08/10/23 02:37 563-58-608/09/23 23:150.0087 0.0042 1
cis-1,3-Dichloropropene ND mg/kg 08/10/23 02:37 10061-01-508/09/23 23:150.0087 0.0024 1
trans-1,3-Dichloropropene ND mg/kg 08/10/23 02:37 10061-02-608/09/23 23:150.0087 0.0030 1
Diisopropyl ether ND mg/kg 08/10/23 02:37 108-20-308/09/23 23:150.0087 0.0024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-2 Lab ID:92681077012 Collected:08/04/23 11:05 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/10/23 02:37 100-41-408/09/23 23:150.0087 0.0041 1
Hexachloro-1,3-butadiene ND mg/kg 08/10/23 02:37 87-68-308/09/23 23:150.017 0.014 1
2-Hexanone ND mg/kg 08/10/23 02:37 591-78-608/09/23 23:150.087 0.0084 1
Isopropylbenzene (Cumene)ND mg/kg 08/10/23 02:37 98-82-808/09/23 23:150.0087 0.0030 1
p-Isopropyltoluene ND mg/kg 08/10/23 02:37 99-87-608/09/23 23:150.0087 0.0043 1
Methylene Chloride ND mg/kg 08/10/23 02:37 75-09-208/09/23 23:150.035 0.024 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/10/23 02:37 108-10-108/09/23 23:150.087 0.0084 1
Methyl-tert-butyl ether ND mg/kg 08/10/23 02:37 1634-04-408/09/23 23:150.0087 0.0033 1
Naphthalene ND mg/kg 08/10/23 02:37 91-20-308/09/23 23:150.0087 0.0046 1
n-Propylbenzene ND mg/kg 08/10/23 02:37 103-65-108/09/23 23:150.0087 0.0031 1
Styrene ND mg/kg 08/10/23 02:37 100-42-508/09/23 23:150.0087 0.0023 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/10/23 02:37 630-20-608/09/23 23:150.0087 0.0033 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/10/23 02:37 79-34-508/09/23 23:150.0087 0.0023 1
Tetrachloroethene 0.0064J mg/kg 08/10/23 02:37 127-18-408/09/23 23:150.0087 0.0028 1
Toluene ND mg/kg 08/10/23 02:37 108-88-308/09/23 23:150.0087 0.0060 1
1,2,3-Trichlorobenzene ND mg/kg 08/10/23 02:37 87-61-608/09/23 23:150.0087 0.0070 1
1,2,4-Trichlorobenzene ND mg/kg 08/10/23 02:37 120-82-1 IK08/09/23 23:150.0087 0.0073 1
1,1,1-Trichloroethane ND mg/kg 08/10/23 02:37 71-55-608/09/23 23:150.0087 0.0045 1
1,1,2-Trichloroethane ND mg/kg 08/10/23 02:37 79-00-508/09/23 23:150.0087 0.0029 1
Trichloroethene ND mg/kg 08/10/23 02:37 79-01-608/09/23 23:150.0087 0.0070 1
Trichlorofluoromethane ND mg/kg 08/10/23 02:37 75-69-408/09/23 23:150.0087 0.0048 1
1,2,3-Trichloropropane ND mg/kg 08/10/23 02:37 96-18-408/09/23 23:150.0087 0.0044 1
1,2,4-Trimethylbenzene ND mg/kg 08/10/23 02:37 95-63-608/09/23 23:150.0087 0.0052 1
1,3,5-Trimethylbenzene ND mg/kg 08/10/23 02:37 108-67-808/09/23 23:150.0087 0.0029 1
Vinyl acetate ND mg/kg 08/10/23 02:37 108-05-408/09/23 23:150.087 0.018 1
Vinyl chloride ND mg/kg 08/10/23 02:37 75-01-408/09/23 23:150.017 0.0044 1
Xylene (Total)ND mg/kg 08/10/23 02:37 1330-20-708/09/23 23:150.017 0.0050 1
m&p-Xylene ND mg/kg 08/10/23 02:37 179601-23-108/09/23 23:150.017 0.0060 1
o-Xylene ND mg/kg 08/10/23 02:37 95-47-608/09/23 23:150.0087 0.0038 1
Surrogates
Toluene-d8 (S)101 %08/10/23 02:37 2037-26-508/09/23 23:1570-130 1
4-Bromofluorobenzene (S)104 %08/10/23 02:37 460-00-408/09/23 23:1570-130 1
1,2-Dichloroethane-d4 (S)111 %08/10/23 02:37 17060-07-008/09/23 23:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.6 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 69.2 %08/10/23 12:4808/10/23 12:311
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DP-2 Lab ID:92681077012 Collected:08/04/23 11:05 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.66 mg/kg 08/14/23 20:10 18540-29-908/13/23 18:151.44 0.368 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DUP-1 Lab ID:92681077013 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.96 mg/kg 08/13/23 16:55 7440-38-208/10/23 09:481.64 0.164 5
Barium 282 mg/kg 08/13/23 17:21 7440-39-308/10/23 09:488.19 0.498 10
Cadmium 0.144J mg/kg 08/13/23 16:55 7440-43-9 J08/10/23 09:481.64 0.140 5
Chromium 46.7 mg/kg 08/13/23 16:55 7440-47-308/10/23 09:488.19 0.485 5
Lead 15.8 mg/kg 08/13/23 16:55 7439-92-108/10/23 09:483.28 0.162 5
Selenium 3.96J mg/kg 08/13/23 16:55 7782-49-2 J08/10/23 09:484.10 0.295 5
Silver ND mg/kg 08/13/23 16:55 7440-22-408/10/23 09:480.819 0.142 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 08/15/23 14:27 7439-97-608/14/23 20:110.0655 0.0295 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/15/23 15:07 83-32-908/14/23 17:160.53 0.19 1
Acenaphthylene ND mg/kg 08/15/23 15:07 208-96-808/14/23 17:160.53 0.19 1
Aniline ND mg/kg 08/15/23 15:07 62-53-308/14/23 17:160.53 0.21 1
Anthracene ND mg/kg 08/15/23 15:07 120-12-708/14/23 17:160.53 0.17 1
Benzo(a)anthracene ND mg/kg 08/15/23 15:07 56-55-308/14/23 17:160.53 0.18 1
Benzo(a)pyrene ND mg/kg 08/15/23 15:07 50-32-808/14/23 17:160.53 0.18 1
Benzo(b)fluoranthene ND mg/kg 08/15/23 15:07 205-99-208/14/23 17:160.53 0.18 1
Benzo(g,h,i)perylene ND mg/kg 08/15/23 15:07 191-24-208/14/23 17:160.53 0.21 1
Benzo(k)fluoranthene ND mg/kg 08/15/23 15:07 207-08-908/14/23 17:160.53 0.19 1
Benzoic Acid ND mg/kg 08/15/23 15:07 65-85-008/14/23 17:162.6 1.1 1
Benzyl alcohol ND mg/kg 08/15/23 15:07 100-51-608/14/23 17:161.1 0.40 1
4-Bromophenylphenyl ether ND mg/kg 08/15/23 15:07 101-55-308/14/23 17:160.53 0.20 1
Butylbenzylphthalate ND mg/kg 08/15/23 15:07 85-68-708/14/23 17:160.53 0.22 1
4-Chloro-3-methylphenol ND mg/kg 08/15/23 15:07 59-50-708/14/23 17:161.1 0.37 1
4-Chloroaniline ND mg/kg 08/15/23 15:07 106-47-808/14/23 17:161.1 0.42 1
bis(2-Chloroethoxy)methane ND mg/kg 08/15/23 15:07 111-91-108/14/23 17:160.53 0.22 1
bis(2-Chloroethyl) ether ND mg/kg 08/15/23 15:07 111-44-408/14/23 17:160.53 0.20 1
2-Chloronaphthalene ND mg/kg 08/15/23 15:07 91-58-708/14/23 17:160.53 0.21 1
2-Chlorophenol ND mg/kg 08/15/23 15:07 95-57-808/14/23 17:160.53 0.20 1
4-Chlorophenylphenyl ether ND mg/kg 08/15/23 15:07 7005-72-308/14/23 17:160.53 0.20 1
Chrysene ND mg/kg 08/15/23 15:07 218-01-908/14/23 17:160.53 0.19 1
Dibenz(a,h)anthracene ND mg/kg 08/15/23 15:07 53-70-308/14/23 17:160.53 0.20 1
Dibenzofuran ND mg/kg 08/15/23 15:07 132-64-908/14/23 17:160.53 0.19 1
1,2-Dichlorobenzene ND mg/kg 08/15/23 15:07 95-50-108/14/23 17:160.53 0.19 1
1,3-Dichlorobenzene ND mg/kg 08/15/23 15:07 541-73-108/14/23 17:160.53 0.19 1
1,4-Dichlorobenzene ND mg/kg 08/15/23 15:07 106-46-708/14/23 17:160.53 0.20 1
3,3'-Dichlorobenzidine ND mg/kg 08/15/23 15:07 91-94-108/14/23 17:161.1 0.36 1
2,4-Dichlorophenol ND mg/kg 08/15/23 15:07 120-83-208/14/23 17:160.53 0.21 1
Diethylphthalate ND mg/kg 08/15/23 15:07 84-66-208/14/23 17:160.53 0.19 1
2,4-Dimethylphenol ND mg/kg 08/15/23 15:07 105-67-908/14/23 17:160.53 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DUP-1 Lab ID:92681077013 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 08/15/23 15:07 131-11-308/14/23 17:160.53 0.19 1
Di-n-butylphthalate ND mg/kg 08/15/23 15:07 84-74-208/14/23 17:160.53 0.18 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/15/23 15:07 534-52-108/14/23 17:161.1 0.49 1
2,4-Dinitrophenol ND mg/kg 08/15/23 15:07 51-28-508/14/23 17:162.6 1.6 1
2,4-Dinitrotoluene ND mg/kg 08/15/23 15:07 121-14-208/14/23 17:160.53 0.20 1
2,6-Dinitrotoluene ND mg/kg 08/15/23 15:07 606-20-208/14/23 17:160.53 0.19 1
Di-n-octylphthalate ND mg/kg 08/15/23 15:07 117-84-008/14/23 17:160.53 0.21 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/15/23 15:07 117-81-708/14/23 17:160.53 0.21 1
Fluoranthene ND mg/kg 08/15/23 15:07 206-44-008/14/23 17:160.53 0.18 1
Fluorene ND mg/kg 08/15/23 15:07 86-73-708/14/23 17:160.53 0.19 1
Hexachloro-1,3-butadiene ND mg/kg 08/15/23 15:07 87-68-308/14/23 17:160.53 0.23 1
Hexachlorobenzene ND mg/kg 08/15/23 15:07 118-74-108/14/23 17:160.53 0.21 1
Hexachlorocyclopentadiene ND mg/kg 08/15/23 15:07 77-47-408/14/23 17:160.53 0.30 1
Hexachloroethane ND mg/kg 08/15/23 15:07 67-72-108/14/23 17:160.53 0.20 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/15/23 15:07 193-39-508/14/23 17:160.53 0.21 1
Isophorone ND mg/kg 08/15/23 15:07 78-59-108/14/23 17:160.53 0.24 1
1-Methylnaphthalene ND mg/kg 08/15/23 15:07 90-12-008/14/23 17:160.53 0.19 1
2-Methylnaphthalene ND mg/kg 08/15/23 15:07 91-57-608/14/23 17:160.53 0.21 1
2-Methylphenol(o-Cresol)ND mg/kg 08/15/23 15:07 95-48-708/14/23 17:160.53 0.22 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/15/23 15:07 15831-10-408/14/23 17:160.53 0.21 1
Naphthalene ND mg/kg 08/15/23 15:07 91-20-308/14/23 17:160.53 0.18 1
2-Nitroaniline ND mg/kg 08/15/23 15:07 88-74-408/14/23 17:162.6 0.43 1
3-Nitroaniline ND mg/kg 08/15/23 15:07 99-09-208/14/23 17:162.6 0.42 1
4-Nitroaniline ND mg/kg 08/15/23 15:07 100-01-608/14/23 17:161.1 0.40 1
Nitrobenzene ND mg/kg 08/15/23 15:07 98-95-308/14/23 17:160.53 0.25 1
2-Nitrophenol ND mg/kg 08/15/23 15:07 88-75-508/14/23 17:160.53 0.23 1
4-Nitrophenol ND mg/kg 08/15/23 15:07 100-02-708/14/23 17:162.6 1.0 1
N-Nitrosodimethylamine ND mg/kg 08/15/23 15:07 62-75-908/14/23 17:160.53 0.18 1
N-Nitroso-di-n-propylamine ND mg/kg 08/15/23 15:07 621-64-708/14/23 17:160.53 0.20 1
N-Nitrosodiphenylamine ND mg/kg 08/15/23 15:07 86-30-608/14/23 17:160.53 0.19 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/15/23 15:07 108-60-108/14/23 17:160.53 0.25 1
Pentachlorophenol ND mg/kg 08/15/23 15:07 87-86-508/14/23 17:161.1 0.52 1
Phenanthrene ND mg/kg 08/15/23 15:07 85-01-808/14/23 17:160.53 0.17 1
Phenol ND mg/kg 08/15/23 15:07 108-95-208/14/23 17:160.53 0.24 1
Pyrene ND mg/kg 08/15/23 15:07 129-00-008/14/23 17:160.53 0.21 1
Pyridine ND mg/kg 08/15/23 15:07 110-86-108/14/23 17:160.53 0.17 1
1,2,4-Trichlorobenzene ND mg/kg 08/15/23 15:07 120-82-108/14/23 17:160.53 0.21 1
2,4,5-Trichlorophenol ND mg/kg 08/15/23 15:07 95-95-408/14/23 17:160.53 0.24 1
2,4,6-Trichlorophenol ND mg/kg 08/15/23 15:07 88-06-208/14/23 17:160.53 0.22 1
Surrogates
Nitrobenzene-d5 (S)63 %08/15/23 15:07 4165-60-008/14/23 17:1610-130 1
2-Fluorobiphenyl (S)53 %08/15/23 15:07 321-60-808/14/23 17:1610-130 1
Terphenyl-d14 (S)37 %08/15/23 15:07 1718-51-008/14/23 17:1610-130 1
Phenol-d6 (S)57 %08/15/23 15:07 13127-88-308/14/23 17:1610-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DUP-1 Lab ID:92681077013 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)54 %08/15/23 15:07 367-12-408/14/23 17:1610-130 1
2,4,6-Tribromophenol (S)67 %08/15/23 15:07 118-79-608/14/23 17:1610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/10/23 02:54 67-64-108/09/23 23:150.23 0.072 1
Benzene ND mg/kg 08/10/23 02:54 71-43-208/09/23 23:150.011 0.0045 1
Bromobenzene ND mg/kg 08/10/23 02:54 108-86-108/09/23 23:150.011 0.0037 1
Bromochloromethane ND mg/kg 08/10/23 02:54 74-97-508/09/23 23:150.011 0.0033 1
Bromodichloromethane ND mg/kg 08/10/23 02:54 75-27-408/09/23 23:150.011 0.0044 1
Bromoform ND mg/kg 08/10/23 02:54 75-25-208/09/23 23:150.011 0.0040 1
Bromomethane ND mg/kg 08/10/23 02:54 74-83-9 v208/09/23 23:150.045 0.035 1
2-Butanone (MEK)ND mg/kg 08/10/23 02:54 78-93-308/09/23 23:150.23 0.054 1
n-Butylbenzene ND mg/kg 08/10/23 02:54 104-51-808/09/23 23:150.011 0.0071 1
sec-Butylbenzene ND mg/kg 08/10/23 02:54 135-98-808/09/23 23:150.011 0.0050 1
tert-Butylbenzene ND mg/kg 08/10/23 02:54 98-06-608/09/23 23:150.011 0.0040 1
Carbon tetrachloride ND mg/kg 08/10/23 02:54 56-23-508/09/23 23:150.011 0.0042 1
Chlorobenzene ND mg/kg 08/10/23 02:54 108-90-708/09/23 23:150.011 0.0065 1
Chloroethane ND mg/kg 08/10/23 02:54 75-00-308/09/23 23:150.023 0.0087 1
Chloroform ND mg/kg 08/10/23 02:54 67-66-308/09/23 23:150.011 0.0094 1
Chloromethane 0.032 mg/kg 08/10/23 02:54 74-87-308/09/23 23:150.023 0.0095 1
2-Chlorotoluene ND mg/kg 08/10/23 02:54 95-49-808/09/23 23:150.011 0.0040 1
4-Chlorotoluene ND mg/kg 08/10/23 02:54 106-43-408/09/23 23:150.011 0.0063 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/10/23 02:54 96-12-808/09/23 23:150.011 0.0044 1
Dibromochloromethane ND mg/kg 08/10/23 02:54 124-48-108/09/23 23:150.011 0.0063 1
1,2-Dibromoethane (EDB)ND mg/kg 08/10/23 02:54 106-93-408/09/23 23:150.011 0.0050 1
Dibromomethane ND mg/kg 08/10/23 02:54 74-95-308/09/23 23:150.011 0.0024 1
1,2-Dichlorobenzene ND mg/kg 08/10/23 02:54 95-50-108/09/23 23:150.011 0.0041 1
1,3-Dichlorobenzene ND mg/kg 08/10/23 02:54 541-73-108/09/23 23:150.011 0.0035 1
1,4-Dichlorobenzene ND mg/kg 08/10/23 02:54 106-46-708/09/23 23:150.011 0.0029 1
Dichlorodifluoromethane ND mg/kg 08/10/23 02:54 75-71-8 v108/09/23 23:150.023 0.011 1
1,1-Dichloroethane ND mg/kg 08/10/23 02:54 75-34-308/09/23 23:150.011 0.0046 1
1,2-Dichloroethane ND mg/kg 08/10/23 02:54 107-06-208/09/23 23:150.011 0.0075 1
1,1-Dichloroethene ND mg/kg 08/10/23 02:54 75-35-408/09/23 23:150.011 0.0046 1
cis-1,2-Dichloroethene ND mg/kg 08/10/23 02:54 156-59-208/09/23 23:150.011 0.0039 1
trans-1,2-Dichloroethene ND mg/kg 08/10/23 02:54 156-60-508/09/23 23:150.011 0.0096 1
1,2-Dichloropropane ND mg/kg 08/10/23 02:54 78-87-508/09/23 23:150.011 0.0034 1
1,3-Dichloropropane ND mg/kg 08/10/23 02:54 142-28-908/09/23 23:150.011 0.0035 1
2,2-Dichloropropane ND mg/kg 08/10/23 02:54 594-20-708/09/23 23:150.011 0.0085 1
1,1-Dichloropropene ND mg/kg 08/10/23 02:54 563-58-608/09/23 23:150.011 0.0054 1
cis-1,3-Dichloropropene ND mg/kg 08/10/23 02:54 10061-01-508/09/23 23:150.011 0.0031 1
trans-1,3-Dichloropropene ND mg/kg 08/10/23 02:54 10061-02-608/09/23 23:150.011 0.0039 1
Diisopropyl ether ND mg/kg 08/10/23 02:54 108-20-308/09/23 23:150.011 0.0030 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DUP-1 Lab ID:92681077013 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 08/10/23 02:54 100-41-408/09/23 23:150.011 0.0053 1
Hexachloro-1,3-butadiene ND mg/kg 08/10/23 02:54 87-68-308/09/23 23:150.023 0.018 1
2-Hexanone ND mg/kg 08/10/23 02:54 591-78-608/09/23 23:150.11 0.011 1
Isopropylbenzene (Cumene)ND mg/kg 08/10/23 02:54 98-82-808/09/23 23:150.011 0.0038 1
p-Isopropyltoluene ND mg/kg 08/10/23 02:54 99-87-608/09/23 23:150.011 0.0055 1
Methylene Chloride ND mg/kg 08/10/23 02:54 75-09-208/09/23 23:150.045 0.031 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/10/23 02:54 108-10-108/09/23 23:150.11 0.011 1
Methyl-tert-butyl ether ND mg/kg 08/10/23 02:54 1634-04-408/09/23 23:150.011 0.0042 1
Naphthalene ND mg/kg 08/10/23 02:54 91-20-308/09/23 23:150.011 0.0059 1
n-Propylbenzene ND mg/kg 08/10/23 02:54 103-65-108/09/23 23:150.011 0.0040 1
Styrene ND mg/kg 08/10/23 02:54 100-42-508/09/23 23:150.011 0.0030 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/10/23 02:54 630-20-608/09/23 23:150.011 0.0043 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/10/23 02:54 79-34-508/09/23 23:150.011 0.0030 1
Tetrachloroethene ND mg/kg 08/10/23 02:54 127-18-408/09/23 23:150.011 0.0036 1
Toluene ND mg/kg 08/10/23 02:54 108-88-308/09/23 23:150.011 0.0078 1
1,2,3-Trichlorobenzene ND mg/kg 08/10/23 02:54 87-61-608/09/23 23:150.011 0.0091 1
1,2,4-Trichlorobenzene ND mg/kg 08/10/23 02:54 120-82-1 IK08/09/23 23:150.011 0.0095 1
1,1,1-Trichloroethane ND mg/kg 08/10/23 02:54 71-55-608/09/23 23:150.011 0.0059 1
1,1,2-Trichloroethane ND mg/kg 08/10/23 02:54 79-00-508/09/23 23:150.011 0.0037 1
Trichloroethene ND mg/kg 08/10/23 02:54 79-01-608/09/23 23:150.011 0.0091 1
Trichlorofluoromethane ND mg/kg 08/10/23 02:54 75-69-408/09/23 23:150.011 0.0062 1
1,2,3-Trichloropropane ND mg/kg 08/10/23 02:54 96-18-408/09/23 23:150.011 0.0057 1
1,2,4-Trimethylbenzene ND mg/kg 08/10/23 02:54 95-63-608/09/23 23:150.011 0.0067 1
1,3,5-Trimethylbenzene ND mg/kg 08/10/23 02:54 108-67-808/09/23 23:150.011 0.0038 1
Vinyl acetate ND mg/kg 08/10/23 02:54 108-05-408/09/23 23:150.11 0.023 1
Vinyl chloride ND mg/kg 08/10/23 02:54 75-01-408/09/23 23:150.023 0.0057 1
Xylene (Total)ND mg/kg 08/10/23 02:54 1330-20-708/09/23 23:150.023 0.0064 1
m&p-Xylene ND mg/kg 08/10/23 02:54 179601-23-108/09/23 23:150.023 0.0077 1
o-Xylene ND mg/kg 08/10/23 02:54 95-47-608/09/23 23:150.011 0.0050 1
Surrogates
Toluene-d8 (S)100 %08/10/23 02:54 2037-26-508/09/23 23:1570-130 1
4-Bromofluorobenzene (S)103 %08/10/23 02:54 460-00-408/09/23 23:1570-130 1
1,2-Dichloroethane-d4 (S)107 %08/10/23 02:54 17060-07-008/09/23 23:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 38.4 %08/08/23 13:37 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 61.0 %08/10/23 12:4808/10/23 12:311
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 75 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:DUP-1 Lab ID:92681077013 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.21 mg/kg 08/14/23 20:16 18540-29-908/13/23 18:151.64 0.418 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 76 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:TB Lab ID:92681077014 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/10/23 01:43 67-64-125.0 5.1 1
Benzene ND ug/L 08/10/23 01:43 71-43-21.0 0.34 1
Bromobenzene ND ug/L 08/10/23 01:43 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 08/10/23 01:43 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 08/10/23 01:43 75-27-41.0 0.31 1
Bromoform ND ug/L 08/10/23 01:43 75-25-21.0 0.34 1
Bromomethane ND ug/L 08/10/23 01:43 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 08/10/23 01:43 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 08/10/23 01:43 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 08/10/23 01:43 108-90-71.0 0.28 1
Chloroethane ND ug/L 08/10/23 01:43 75-00-31.0 0.65 1
Chloroform ND ug/L 08/10/23 01:43 67-66-31.0 0.43 1
Chloromethane ND ug/L 08/10/23 01:43 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 08/10/23 01:43 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 08/10/23 01:43 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 08/10/23 01:43 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 08/10/23 01:43 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 08/10/23 01:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 08/10/23 01:43 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 08/10/23 01:43 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 08/10/23 01:43 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 08/10/23 01:43 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/10/23 01:43 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 08/10/23 01:43 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 08/10/23 01:43 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 08/10/23 01:43 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 08/10/23 01:43 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 08/10/23 01:43 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 08/10/23 01:43 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 08/10/23 01:43 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/10/23 01:43 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 08/10/23 01:43 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 08/10/23 01:43 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 08/10/23 01:43 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 08/10/23 01:43 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 08/10/23 01:43 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/10/23 01:43 87-68-32.0 1.5 1
2-Hexanone ND ug/L 08/10/23 01:43 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 08/10/23 01:43 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 08/10/23 01:43 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/10/23 01:43 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 08/10/23 01:43 1634-04-41.0 0.42 1
Naphthalene ND ug/L 08/10/23 01:43 91-20-31.0 0.64 1
Styrene ND ug/L 08/10/23 01:43 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 08/10/23 01:43 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 136
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Sample:TB Lab ID:92681077014 Collected:08/04/23 00:00 Received:08/07/23 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 08/10/23 01:43 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/10/23 01:43 127-18-41.0 0.29 1
Toluene ND ug/L 08/10/23 01:43 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/10/23 01:43 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 08/10/23 01:43 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 08/10/23 01:43 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 08/10/23 01:43 79-00-51.0 0.32 1
Trichloroethene ND ug/L 08/10/23 01:43 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 08/10/23 01:43 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 08/10/23 01:43 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 08/10/23 01:43 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 08/10/23 01:43 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 08/10/23 01:43 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 08/10/23 01:43 179601-23-12.0 0.71 1
o-Xylene ND ug/L 08/10/23 01:43 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %08/10/23 01:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/10/23 01:43 17060-07-070-130 1
Toluene-d8 (S)99 %08/10/23 01:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2111353
3051
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3960013-1
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 08/13/23 14:290.100
Barium mg/kg 0.154J 2.50 J08/13/23 14:290.152
Cadmium mg/kg ND 1.00 08/13/23 14:290.0855
Chromium mg/kg ND 5.00 08/13/23 14:290.297
Lead mg/kg ND 2.00 08/13/23 14:290.0990
Selenium mg/kg ND 2.50 08/13/23 14:290.180
Silver mg/kg ND 0.500 08/13/23 14:290.0865
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3960013-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 93.1100 93.1 80.0-120
Barium mg/kg 85.8100 85.8 80.0-120
Cadmium mg/kg 90.9100 90.9 80.0-120
Chromium mg/kg 92.0100 92.0 80.0-120
Lead mg/kg 86.1100 86.1 80.0-120
Selenium mg/kg 95.9100 95.9 80.0-120
Silver mg/kg 18.120.0 90.4 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3960013-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681077004
R3960013-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg ML15680.2 75.0-12570.9 12.0 201562.05 127 113
Barium mg/kg ML15623.1 75.0-12512.0 9.20 20156161197180
Cadmium mg/kg 156 95.9 75.0-12584.2 12.9 201560.260 150 132
Chromium mg/kg MH15612475.0-125138 9.01 2015646.9 241 263
Lead mg/kg ML15670.9 75.0-12557.8 14.8 2015637.3 148 128
Selenium mg/kg 156 89.4 75.0-12581.7 8.91 201561.45 141 129
Silver mg/kg 31.3 94.5 75.0-12582.8 13.2 2031.3ND 29.6 25.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2111648
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3960947-1
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 08/15/23 13:240.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3960947-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.4990.500 99.7 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3960947-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1643999-07
R3960947-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.545 95.1 75.0-125112 16.5 200.545ND 0.519 0.612
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
792275
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077005, 92681077006, 92681077007, 92681077008,
92681077009, 92681077010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4105733
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077005, 92681077006, 92681077007, 92681077008,
92681077009, 92681077010
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/08/23 23:260.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 08/08/23 23:260.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/08/23 23:260.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 08/08/23 23:260.0017
1,1-Dichloroethane mg/kg ND 0.0050 08/08/23 23:260.0021
1,1-Dichloroethene mg/kg ND 0.0050 08/08/23 23:260.0021
1,1-Dichloropropene mg/kg ND 0.0050 08/08/23 23:260.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/08/23 23:260.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 08/08/23 23:260.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 IK08/08/23 23:260.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/08/23 23:260.0030
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/08/23 23:260.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/08/23 23:260.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 08/08/23 23:260.0018
1,2-Dichloroethane mg/kg ND 0.0050 08/08/23 23:260.0033
1,2-Dichloropropane mg/kg ND 0.0050 08/08/23 23:260.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/08/23 23:260.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 08/08/23 23:260.0016
1,3-Dichloropropane mg/kg ND 0.0050 08/08/23 23:260.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 08/08/23 23:260.0013
2,2-Dichloropropane mg/kg ND 0.0050 08/08/23 23:260.0038
2-Butanone (MEK)mg/kg ND 0.10 08/08/23 23:260.024
2-Chlorotoluene mg/kg ND 0.0050 08/08/23 23:260.0018
2-Hexanone mg/kg ND 0.050 08/08/23 23:260.0048
4-Chlorotoluene mg/kg ND 0.0050 08/08/23 23:260.0028
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/08/23 23:260.0048
Acetone mg/kg ND 0.10 08/08/23 23:260.032
Benzene mg/kg ND 0.0050 08/08/23 23:260.0020
Bromobenzene mg/kg ND 0.0050 08/08/23 23:260.0016
Bromochloromethane mg/kg ND 0.0050 08/08/23 23:260.0015
Bromodichloromethane mg/kg ND 0.0050 08/08/23 23:260.0019
Bromoform mg/kg ND 0.0050 08/08/23 23:260.0018
Bromomethane mg/kg ND 0.020 v208/08/23 23:260.016
Carbon tetrachloride mg/kg ND 0.0050 08/08/23 23:260.0019
Chlorobenzene mg/kg ND 0.0050 08/08/23 23:260.0029
Chloroethane mg/kg ND 0.010 08/08/23 23:260.0039
Chloroform mg/kg ND 0.0050 08/08/23 23:260.0042
Chloromethane mg/kg ND 0.010 08/08/23 23:260.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/08/23 23:260.0017
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 81 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4105733
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077005, 92681077006, 92681077007, 92681077008,
92681077009, 92681077010
Matrix:Solid
AnalyzedMDL
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/08/23 23:260.0014
Dibromochloromethane mg/kg ND 0.0050 08/08/23 23:260.0028
Dibromomethane mg/kg ND 0.0050 08/08/23 23:260.0011
Dichlorodifluoromethane mg/kg ND 0.010 08/08/23 23:260.0051
Diisopropyl ether mg/kg ND 0.0050 08/08/23 23:260.0014
Ethylbenzene mg/kg ND 0.0050 08/08/23 23:260.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/08/23 23:260.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/08/23 23:260.0017
m&p-Xylene mg/kg ND 0.010 08/08/23 23:260.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 08/08/23 23:260.0019
Methylene Chloride mg/kg ND 0.020 08/08/23 23:260.014
n-Butylbenzene mg/kg ND 0.0050 08/08/23 23:260.0032
n-Propylbenzene mg/kg ND 0.0050 08/08/23 23:260.0018
Naphthalene mg/kg ND 0.0050 08/08/23 23:260.0026
o-Xylene mg/kg ND 0.0050 08/08/23 23:260.0022
p-Isopropyltoluene mg/kg ND 0.0050 08/08/23 23:260.0025
sec-Butylbenzene mg/kg ND 0.0050 08/08/23 23:260.0022
Styrene mg/kg ND 0.0050 08/08/23 23:260.0013
tert-Butylbenzene mg/kg ND 0.0050 08/08/23 23:260.0018
Tetrachloroethene mg/kg ND 0.0050 08/08/23 23:260.0016
Toluene mg/kg ND 0.0050 08/08/23 23:260.0034
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/08/23 23:260.0042
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/08/23 23:260.0017
Trichloroethene mg/kg ND 0.0050 08/08/23 23:260.0040
Trichlorofluoromethane mg/kg ND 0.0050 08/08/23 23:260.0028
Vinyl acetate mg/kg ND 0.050 08/08/23 23:260.010
Vinyl chloride mg/kg ND 0.010 08/08/23 23:260.0025
Xylene (Total)mg/kg ND 0.010 08/08/23 23:260.0028
1,2-Dichloroethane-d4 (S)%108 70-130 08/08/23 23:26
4-Bromofluorobenzene (S)%102 70-130 08/08/23 23:26
Toluene-d8 (S)%100 70-130 08/08/23 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4105734LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.370.5 74 70-130
1,1,1-Trichloroethane mg/kg 0.380.5 77 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.390.5 79 70-130
1,1,2-Trichloroethane mg/kg 0.370.5 73 70-130
1,1-Dichloroethane mg/kg 0.400.5 80 70-130
1,1-Dichloroethene mg/kg 0.410.5 82 70-130
1,1-Dichloropropene mg/kg 0.410.5 81 70-130
1,2,3-Trichlorobenzene mg/kg 0.360.5 72 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4105734LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane mg/kg 0.400.5 80 70-130
1,2,4-Trichlorobenzene mg/kg 0.36 IK0.5 72 70-130
1,2,4-Trimethylbenzene mg/kg 0.390.5 77 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.350.5 70 67-130
1,2-Dibromoethane (EDB)mg/kg 0.370.5 75 70-130
1,2-Dichlorobenzene mg/kg 0.350.5 71 70-130
1,2-Dichloroethane mg/kg 0.400.5 80 70-130
1,2-Dichloropropane mg/kg 0.400.5 80 70-130
1,3,5-Trimethylbenzene mg/kg 0.400.5 80 70-130
1,3-Dichlorobenzene mg/kg 0.370.5 74 70-130
1,3-Dichloropropane mg/kg 0.380.5 76 70-130
1,4-Dichlorobenzene mg/kg 0.380.5 75 70-130
2,2-Dichloropropane mg/kg 0.370.5 74 67-130
2-Butanone (MEK)mg/kg 0.821 82 66-130
2-Chlorotoluene mg/kg 0.390.5 78 70-130
2-Hexanone mg/kg 0.751 75 70-130
4-Chlorotoluene mg/kg 0.400.5 79 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.771 77 70-130
Acetone mg/kg 0.771 77 67-130
Benzene mg/kg 0.380.5 77 70-130
Bromobenzene mg/kg 0.380.5 75 70-130
Bromochloromethane mg/kg 0.370.5 74 70-130
Bromodichloromethane mg/kg 0.370.5 74 70-130
Bromoform mg/kg 0.370.5 73 70-130
Bromomethane mg/kg 0.33 v30.5 66 53-175
Carbon tetrachloride mg/kg 0.380.5 77 70-130
Chlorobenzene mg/kg 0.380.5 76 70-130
Chloroethane mg/kg 0.430.5 85 70-135
Chloroform mg/kg 0.390.5 78 70-130
Chloromethane mg/kg 0.440.5 87 64-130
cis-1,2-Dichloroethene mg/kg 0.410.5 83 70-130
cis-1,3-Dichloropropene mg/kg 0.370.5 75 70-130
Dibromochloromethane mg/kg 0.380.5 75 70-130
Dibromomethane mg/kg 0.370.5 74 70-130
Dichlorodifluoromethane mg/kg 0.500.5 100 63-145
Diisopropyl ether mg/kg 0.400.5 79 68-130
Ethylbenzene mg/kg 0.380.5 76 70-130
Hexachloro-1,3-butadiene mg/kg 0.370.5 74 70-130
Isopropylbenzene (Cumene)mg/kg 0.390.5 78 70-130
m&p-Xylene mg/kg 0.751 75 70-130
Methyl-tert-butyl ether mg/kg 0.360.5 73 70-130
Methylene Chloride mg/kg 0.400.5 80 67-130
n-Butylbenzene mg/kg 0.390.5 78 70-130
n-Propylbenzene mg/kg 0.390.5 77 70-130
Naphthalene mg/kg 0.370.5 75 70-130
o-Xylene mg/kg 0.390.5 77 70-130
p-Isopropyltoluene mg/kg 0.390.5 79 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4105734LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene mg/kg 0.390.5 78 70-130
Styrene mg/kg 0.390.5 78 70-130
tert-Butylbenzene mg/kg 0.350.5 69 64-130
Tetrachloroethene mg/kg 0.360.5 72 70-130
Toluene mg/kg 0.360.5 72 70-130
trans-1,2-Dichloroethene mg/kg 0.410.5 82 70-130
trans-1,3-Dichloropropene mg/kg 0.350.5 71 70-130
Trichloroethene mg/kg 0.370.5 74 70-130
Trichlorofluoromethane mg/kg 0.400.5 81 70-130
Vinyl acetate mg/kg 0.831 83 70-134
Vinyl chloride mg/kg 0.390.5 79 68-130
Xylene (Total)mg/kg 1.11.5 76 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4105735MATRIX SPIKE SAMPLE:
MSSpike
Result
92681077001
1,1,1,2-Tetrachloroethane mg/kg 1.00.97 103 58-140ND
1,1,1-Trichloroethane mg/kg 1.20.97 121 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.960.97 99 52-139ND
1,1,2-Trichloroethane mg/kg 1.00.97 106 56-140ND
1,1-Dichloroethane mg/kg 1.10.97 116 58-145ND
1,1-Dichloroethene mg/kg 1.20.97 123 57-158ND
1,1-Dichloropropene mg/kg 1.20.97 121 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.900.97 94 48-149ND
1,2,3-Trichloropropane mg/kg 1.00.97 104 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.92 IK0.97 95 51-151ND
1,2,4-Trimethylbenzene mg/kg 1.10.97 109 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.840.97 87 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.960.97 100 60-138ND
1,2-Dichlorobenzene mg/kg 0.940.97 98 59-147ND
1,2-Dichloroethane mg/kg 1.10.97 116 57-139ND
1,2-Dichloropropane mg/kg 1.10.97 112 62-145ND
1,3,5-Trimethylbenzene mg/kg 1.10.97 111 47-159ND
1,3-Dichlorobenzene mg/kg 1.00.97 103 58-144ND
1,3-Dichloropropane mg/kg 0.990.97 102 60-142ND
1,4-Dichlorobenzene mg/kg 0.960.97 99 57-143ND
2,2-Dichloropropane mg/kg 1.00.97 107 37-144ND
2-Butanone (MEK)mg/kg 1.91.9 100 28-146ND
2-Chlorotoluene mg/kg 1.00.97 109 55-158ND
2-Hexanone mg/kg 1.81.9 93 44-141ND
4-Chlorotoluene mg/kg 1.00.97 107 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 2.01.9 101 50-138ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4105735MATRIX SPIKE SAMPLE:
MSSpike
Result
92681077001
Acetone mg/kg 1.51.9 79 20-136ND
Benzene mg/kg 1.10.97 113 60-145ND
Bromobenzene mg/kg 0.960.97 100 59-145ND
Bromochloromethane mg/kg 0.970.97 101 57-143ND
Bromodichloromethane mg/kg 1.10.97 109 53-133ND
Bromoform mg/kg 0.920.97 95 48-133ND
Bromomethane mg/kg 1.3 v30.97 134 10-167ND
Carbon tetrachloride mg/kg 1.20.97 124 57-147ND
Chlorobenzene mg/kg 1.00.97 104 61-144ND
Chloroethane mg/kg 1.6 M10.97 166 10-153ND
Chloroform mg/kg 1.10.97 112 58-141ND
Chloromethane mg/kg 1.20.97 127 54-165ND
cis-1,2-Dichloroethene mg/kg 1.10.97 117 59-144ND
cis-1,3-Dichloropropene mg/kg 1.00.97 104 56-137ND
Dibromochloromethane mg/kg 0.980.97 101 53-139ND
Dibromomethane mg/kg 0.970.97 100 60-136ND
Dichlorodifluoromethane mg/kg 1.9 M10.97 201 49-177ND
Diisopropyl ether mg/kg 1.10.97 109 53-136ND
Ethylbenzene mg/kg 1.10.97 109 53-150ND
Hexachloro-1,3-butadiene mg/kg 1.00.97 104 42-186ND
Isopropylbenzene (Cumene)mg/kg 1.10.97 111 62-154ND
m&p-Xylene mg/kg 2.01.9 106 49-156ND
Methyl-tert-butyl ether mg/kg 0.980.97 102 54-133ND
Methylene Chloride mg/kg 1.10.97 115 50-153ND
n-Butylbenzene mg/kg 1.00.97 106 44-174ND
n-Propylbenzene mg/kg 1.00.97 106 52-157ND
Naphthalene mg/kg 0.880.97 91 37-150ND
o-Xylene mg/kg 1.10.97 110 54-150ND
p-Isopropyltoluene mg/kg 1.00.97 108 50-164ND
sec-Butylbenzene mg/kg 1.10.97 112 58-161ND
Styrene mg/kg 1.10.97 109 60-148ND
tert-Butylbenzene mg/kg 0.960.97 99 44-151ND
Tetrachloroethene mg/kg 0.960.97 100 53-151ND
Toluene mg/kg 1.00.97 103 52-148ND
trans-1,2-Dichloroethene mg/kg 1.10.97 111 60-148ND
trans-1,3-Dichloropropene mg/kg 0.970.97 100 55-133ND
Trichloroethene mg/kg 1.10.97 111 60-148ND
Trichlorofluoromethane mg/kg 1.10.97 118 10-154ND
Vinyl acetate mg/kg 2.11.9 108 50-149ND
Vinyl chloride mg/kg 1.20.97 123 57-157ND
Xylene (Total)mg/kg 3.12.8 107 52-153ND
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681077002
4105736SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND IK30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND v230ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681077002
4105736SAMPLE DUPLICATE:
m&p-Xylene mg/kg 0.0099J 300.012J
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg 0.016 300.011J
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg 0.016J 300.023
1,2-Dichloroethane-d4 (S)%107108
4-Bromofluorobenzene (S)%106105
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
792281
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4105749
Associated Lab Samples:92681077011
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/09/23 21:430.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 08/09/23 21:430.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/09/23 21:430.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 08/09/23 21:430.0017
1,1-Dichloroethane mg/kg ND 0.0050 08/09/23 21:430.0021
1,1-Dichloroethene mg/kg ND 0.0050 08/09/23 21:430.0021
1,1-Dichloropropene mg/kg ND 0.0050 08/09/23 21:430.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/09/23 21:430.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 08/09/23 21:430.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 IK08/09/23 21:430.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/09/23 21:430.0030
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/09/23 21:430.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/09/23 21:430.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 08/09/23 21:430.0018
1,2-Dichloroethane mg/kg ND 0.0050 08/09/23 21:430.0033
1,2-Dichloropropane mg/kg ND 0.0050 08/09/23 21:430.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/09/23 21:430.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 08/09/23 21:430.0016
1,3-Dichloropropane mg/kg ND 0.0050 08/09/23 21:430.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 08/09/23 21:430.0013
2,2-Dichloropropane mg/kg ND 0.0050 08/09/23 21:430.0038
2-Butanone (MEK)mg/kg ND 0.10 08/09/23 21:430.024
2-Chlorotoluene mg/kg ND 0.0050 08/09/23 21:430.0018
2-Hexanone mg/kg ND 0.050 08/09/23 21:430.0048
4-Chlorotoluene mg/kg ND 0.0050 08/09/23 21:430.0028
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/09/23 21:430.0048
Acetone mg/kg ND 0.10 08/09/23 21:430.032
Benzene mg/kg ND 0.0050 08/09/23 21:430.0020
Bromobenzene mg/kg ND 0.0050 08/09/23 21:430.0016
Bromochloromethane mg/kg ND 0.0050 08/09/23 21:430.0015
Bromodichloromethane mg/kg ND 0.0050 08/09/23 21:430.0019
Bromoform mg/kg ND 0.0050 08/09/23 21:430.0018
Bromomethane mg/kg ND 0.020 v208/09/23 21:430.016
Carbon tetrachloride mg/kg ND 0.0050 08/09/23 21:430.0019
Chlorobenzene mg/kg ND 0.0050 08/09/23 21:430.0029
Chloroethane mg/kg ND 0.010 08/09/23 21:430.0039
Chloroform mg/kg ND 0.0050 08/09/23 21:430.0042
Chloromethane mg/kg ND 0.010 08/09/23 21:430.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/09/23 21:430.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/09/23 21:430.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4105749
Associated Lab Samples:92681077011
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 08/09/23 21:430.0028
Dibromomethane mg/kg ND 0.0050 08/09/23 21:430.0011
Dichlorodifluoromethane mg/kg ND 0.010 v108/09/23 21:430.0051
Diisopropyl ether mg/kg ND 0.0050 08/09/23 21:430.0014
Ethylbenzene mg/kg ND 0.0050 08/09/23 21:430.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/09/23 21:430.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/09/23 21:430.0017
m&p-Xylene mg/kg ND 0.010 08/09/23 21:430.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 08/09/23 21:430.0019
Methylene Chloride mg/kg ND 0.020 08/09/23 21:430.014
n-Butylbenzene mg/kg ND 0.0050 08/09/23 21:430.0032
n-Propylbenzene mg/kg ND 0.0050 08/09/23 21:430.0018
Naphthalene mg/kg ND 0.0050 08/09/23 21:430.0026
o-Xylene mg/kg ND 0.0050 08/09/23 21:430.0022
p-Isopropyltoluene mg/kg ND 0.0050 08/09/23 21:430.0025
sec-Butylbenzene mg/kg ND 0.0050 08/09/23 21:430.0022
Styrene mg/kg ND 0.0050 08/09/23 21:430.0013
tert-Butylbenzene mg/kg ND 0.0050 08/09/23 21:430.0018
Tetrachloroethene mg/kg ND 0.0050 08/09/23 21:430.0016
Toluene mg/kg ND 0.0050 08/09/23 21:430.0034
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/09/23 21:430.0042
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/09/23 21:430.0017
Trichloroethene mg/kg ND 0.0050 08/09/23 21:430.0040
Trichlorofluoromethane mg/kg ND 0.0050 08/09/23 21:430.0028
Vinyl acetate mg/kg ND 0.050 08/09/23 21:430.010
Vinyl chloride mg/kg ND 0.010 08/09/23 21:430.0025
Xylene (Total)mg/kg ND 0.010 08/09/23 21:430.0028
1,2-Dichloroethane-d4 (S)%109 70-130 08/09/23 21:43
4-Bromofluorobenzene (S)%106 70-130 08/09/23 21:43
Toluene-d8 (S)%102 70-130 08/09/23 21:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4105750LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.430.5 87 70-130
1,1,1-Trichloroethane mg/kg 0.460.5 92 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.430.5 85 70-130
1,1,2-Trichloroethane mg/kg 0.440.5 87 70-130
1,1-Dichloroethane mg/kg 0.450.5 90 70-130
1,1-Dichloroethene mg/kg 0.490.5 99 70-130
1,1-Dichloropropene mg/kg 0.460.5 93 70-130
1,2,3-Trichlorobenzene mg/kg 0.450.5 90 70-130
1,2,3-Trichloropropane mg/kg 0.450.5 91 70-130
1,2,4-Trichlorobenzene mg/kg 0.46 IK0.5 92 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4105750LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.490.5 99 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.400.5 80 67-130
1,2-Dibromoethane (EDB)mg/kg 0.420.5 84 70-130
1,2-Dichlorobenzene mg/kg 0.430.5 85 70-130
1,2-Dichloroethane mg/kg 0.450.5 91 70-130
1,2-Dichloropropane mg/kg 0.440.5 89 70-130
1,3,5-Trimethylbenzene mg/kg 0.490.5 97 70-130
1,3-Dichlorobenzene mg/kg 0.450.5 91 70-130
1,3-Dichloropropane mg/kg 0.430.5 86 70-130
1,4-Dichlorobenzene mg/kg 0.440.5 89 70-130
2,2-Dichloropropane mg/kg 0.440.5 88 67-130
2-Butanone (MEK)mg/kg 0.821 82 66-130
2-Chlorotoluene mg/kg 0.480.5 95 70-130
2-Hexanone mg/kg 0.851 85 70-130
4-Chlorotoluene mg/kg 0.470.5 94 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.861 86 70-130
Acetone mg/kg 0.811 81 67-130
Benzene mg/kg 0.450.5 90 70-130
Bromobenzene mg/kg 0.440.5 88 70-130
Bromochloromethane mg/kg 0.410.5 82 70-130
Bromodichloromethane mg/kg 0.440.5 87 70-130
Bromoform mg/kg 0.420.5 84 70-130
Bromomethane mg/kg 0.36 v30.5 71 53-175
Carbon tetrachloride mg/kg 0.480.5 96 70-130
Chlorobenzene mg/kg 0.440.5 87 70-130
Chloroethane mg/kg 0.490.5 97 70-135
Chloroform mg/kg 0.440.5 88 70-130
Chloromethane mg/kg 0.470.5 94 64-130
cis-1,2-Dichloroethene mg/kg 0.460.5 92 70-130
cis-1,3-Dichloropropene mg/kg 0.440.5 87 70-130
Dibromochloromethane mg/kg 0.440.5 89 70-130
Dibromomethane mg/kg 0.420.5 84 70-130
Dichlorodifluoromethane mg/kg 0.73 L1,v10.5 146 63-145
Diisopropyl ether mg/kg 0.440.5 87 68-130
Ethylbenzene mg/kg 0.450.5 90 70-130
Hexachloro-1,3-butadiene mg/kg 0.470.5 94 70-130
Isopropylbenzene (Cumene)mg/kg 0.450.5 91 70-130
m&p-Xylene mg/kg 0.891 89 70-130
Methyl-tert-butyl ether mg/kg 0.410.5 82 70-130
Methylene Chloride mg/kg 0.460.5 91 67-130
n-Butylbenzene mg/kg 0.470.5 94 70-130
n-Propylbenzene mg/kg 0.470.5 94 70-130
Naphthalene mg/kg 0.430.5 87 70-130
o-Xylene mg/kg 0.470.5 93 70-130
p-Isopropyltoluene mg/kg 0.460.5 92 70-130
sec-Butylbenzene mg/kg 0.470.5 95 70-130
Styrene mg/kg 0.450.5 91 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4105750LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.420.5 84 64-130
Tetrachloroethene mg/kg 0.440.5 89 70-130
Toluene mg/kg 0.430.5 85 70-130
trans-1,2-Dichloroethene mg/kg 0.460.5 93 70-130
trans-1,3-Dichloropropene mg/kg 0.420.5 84 70-130
Trichloroethene mg/kg 0.440.5 87 70-130
Trichlorofluoromethane mg/kg 0.550.5 109 70-130
Vinyl acetate mg/kg 0.911 91 70-134
Vinyl chloride mg/kg 0.450.5 90 68-130
Xylene (Total)mg/kg 1.41.5 90 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4105751MATRIX SPIKE SAMPLE:
MSSpike
Result
92681476001
1,1,1,2-Tetrachloroethane mg/kg 0.470.55 84 22-166ND
1,1,1-Trichloroethane mg/kg 0.550.55 100 23-172ND
1,1,2,2-Tetrachloroethane mg/kg 0.470.55 84 21-158ND
1,1,2-Trichloroethane mg/kg 0.490.55 88 25-160ND
1,1-Dichloroethane mg/kg 0.550.55 99 22-166ND
1,1-Dichloroethene mg/kg 0.610.55 110 18-183ND
1,1-Dichloropropene mg/kg 0.580.55 104 20-181ND
1,2,3-Trichlorobenzene mg/kg 0.470.55 84 10-161ND
1,2,3-Trichloropropane mg/kg 0.470.55 85 21-147ND
1,2,4-Trichlorobenzene mg/kg 0.48 IK0.55 87 10-159ND
1,2,4-Trimethylbenzene mg/kg 0.520.55 93 17-1700.0071
1,2-Dibromo-3-chloropropane mg/kg 0.370.55 66 10-135ND
1,2-Dibromoethane (EDB)mg/kg 0.470.55 85 30-154ND
1,2-Dichlorobenzene mg/kg 0.460.55 83 26-162ND
1,2-Dichloroethane mg/kg 0.530.55 96 23-161ND
1,2-Dichloropropane mg/kg 0.530.55 95 29-165ND
1,3,5-Trimethylbenzene mg/kg 0.540.55 97 20-172ND
1,3-Dichlorobenzene mg/kg 0.500.55 90 22-164ND
1,3-Dichloropropane mg/kg 0.490.55 88 27-156ND
1,4-Dichlorobenzene mg/kg 0.490.55 88 20-161ND
2,2-Dichloropropane mg/kg 0.490.55 88 10-159ND
2-Butanone (MEK)mg/kg 0.861.1 77 13-143ND
2-Chlorotoluene mg/kg 0.530.55 96 21-166ND
2-Hexanone mg/kg 0.801.1 72 19-145ND
4-Chlorotoluene mg/kg 0.530.55 96 19-163ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.871.1 79 21-151ND
Acetone mg/kg 0.781.1 71 10-133ND
Benzene mg/kg 0.550.55 99 29-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4105751MATRIX SPIKE SAMPLE:
MSSpike
Result
92681476001
Bromobenzene mg/kg 0.470.55 85 25-161ND
Bromochloromethane mg/kg 0.490.55 88 27-158ND
Bromodichloromethane mg/kg 0.490.55 89 23-158ND
Bromoform mg/kg 0.430.55 78 19-152ND
Bromomethane mg/kg 0.58 v30.55 104 10-152ND
Carbon tetrachloride mg/kg 0.560.55 101 18-172ND
Chlorobenzene mg/kg 0.500.55 90 26-166ND
Chloroethane mg/kg 0.670.55 121 10-130ND
Chloroform mg/kg 0.550.55 99 25-161ND
Chloromethane mg/kg 0.640.55 115 27-197ND
cis-1,2-Dichloroethene mg/kg 0.570.55 103 28-165ND
cis-1,3-Dichloropropene mg/kg 0.490.55 89 23-159ND
Dibromochloromethane mg/kg 0.490.55 88 21-151ND
Dibromomethane mg/kg 0.470.55 84 38-158ND
Dichlorodifluoromethane mg/kg 0.95 v10.55 171 10-200ND
Diisopropyl ether mg/kg 0.510.55 93 23-160ND
Ethylbenzene mg/kg 0.520.55 93 22-1630.0031J
Hexachloro-1,3-butadiene mg/kg 0.590.55 107 10-192ND
Isopropylbenzene (Cumene)mg/kg 0.540.55 97 24-173ND
m&p-Xylene mg/kg 1.01.1 92 22-1710.013
Methyl-tert-butyl ether mg/kg 0.470.55 85 25-153ND
Methylene Chloride mg/kg 0.530.55 96 10-165ND
n-Butylbenzene mg/kg 0.540.55 97 10-186ND
n-Propylbenzene mg/kg 0.530.55 95 16-171ND
Naphthalene mg/kg 0.430.55 75 10-1590.0064
o-Xylene mg/kg 0.510.55 92 23-1710.0053J
p-Isopropyltoluene mg/kg 0.540.55 97 13-184ND
sec-Butylbenzene mg/kg 0.560.55 101 16-182ND
Styrene mg/kg 0.530.55 96 25-169ND
tert-Butylbenzene mg/kg 0.490.55 87 20-174ND
Tetrachloroethene mg/kg 1.30.55 95 14-1710.75
Toluene mg/kg 0.500.55 89 24-1660.011
trans-1,2-Dichloroethene mg/kg 0.570.55 103 24-170ND
trans-1,3-Dichloropropene mg/kg 0.450.55 82 22-157ND
Trichloroethene mg/kg 0.520.55 94 23-176ND
Trichlorofluoromethane mg/kg 0.580.55 104 10-138ND
Vinyl acetate mg/kg 0.981.1 89 11-166ND
Vinyl chloride mg/kg 0.620.55 112 21-200ND
Xylene (Total)mg/kg 1.51.7 92 23-1700.019
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681476002
4105752SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND IK30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND v230ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND v130ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681476002
4105752SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg 0.26 3 300.27
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%110112
4-Bromofluorobenzene (S)%104104
Toluene-d8 (S)%101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
792501
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4106940
Associated Lab Samples:92681077004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/09/23 22:130.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 08/09/23 22:130.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/09/23 22:130.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 08/09/23 22:130.0017
1,1-Dichloroethane mg/kg ND 0.0050 08/09/23 22:130.0021
1,1-Dichloroethene mg/kg ND 0.0050 08/09/23 22:130.0021
1,1-Dichloropropene mg/kg ND 0.0050 08/09/23 22:130.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/09/23 22:130.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 08/09/23 22:130.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 08/09/23 22:130.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/09/23 22:130.0030
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/09/23 22:130.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/09/23 22:130.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 08/09/23 22:130.0018
1,2-Dichloroethane mg/kg ND 0.0050 08/09/23 22:130.0033
1,2-Dichloropropane mg/kg ND 0.0050 08/09/23 22:130.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/09/23 22:130.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 08/09/23 22:130.0016
1,3-Dichloropropane mg/kg ND 0.0050 08/09/23 22:130.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 08/09/23 22:130.0013
2,2-Dichloropropane mg/kg ND 0.0050 08/09/23 22:130.0038
2-Butanone (MEK)mg/kg ND 0.10 08/09/23 22:130.024
2-Chlorotoluene mg/kg ND 0.0050 08/09/23 22:130.0018
2-Hexanone mg/kg ND 0.050 08/09/23 22:130.0048
4-Chlorotoluene mg/kg ND 0.0050 08/09/23 22:130.0028
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/09/23 22:130.0048
Acetone mg/kg ND 0.10 08/09/23 22:130.032
Benzene mg/kg ND 0.0050 08/09/23 22:130.0020
Bromobenzene mg/kg ND 0.0050 08/09/23 22:130.0016
Bromochloromethane mg/kg ND 0.0050 08/09/23 22:130.0015
Bromodichloromethane mg/kg ND 0.0050 08/09/23 22:130.0019
Bromoform mg/kg ND 0.0050 08/09/23 22:130.0018
Bromomethane mg/kg ND 0.020 08/09/23 22:130.016
Carbon tetrachloride mg/kg ND 0.0050 08/09/23 22:130.0019
Chlorobenzene mg/kg ND 0.0050 08/09/23 22:130.0029
Chloroethane mg/kg ND 0.010 08/09/23 22:130.0039
Chloroform mg/kg ND 0.0050 08/09/23 22:130.0042
Chloromethane mg/kg ND 0.010 08/09/23 22:130.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/09/23 22:130.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/09/23 22:130.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4106940
Associated Lab Samples:92681077004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 08/09/23 22:130.0028
Dibromomethane mg/kg ND 0.0050 08/09/23 22:130.0011
Dichlorodifluoromethane mg/kg ND 0.010 v108/09/23 22:130.0051
Diisopropyl ether mg/kg ND 0.0050 08/09/23 22:130.0014
Ethylbenzene mg/kg ND 0.0050 08/09/23 22:130.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/09/23 22:130.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/09/23 22:130.0017
m&p-Xylene mg/kg ND 0.010 08/09/23 22:130.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 08/09/23 22:130.0019
Methylene Chloride mg/kg ND 0.020 08/09/23 22:130.014
n-Butylbenzene mg/kg ND 0.0050 08/09/23 22:130.0032
n-Propylbenzene mg/kg ND 0.0050 08/09/23 22:130.0018
Naphthalene mg/kg ND 0.0050 08/09/23 22:130.0026
o-Xylene mg/kg ND 0.0050 08/09/23 22:130.0022
p-Isopropyltoluene mg/kg ND 0.0050 08/09/23 22:130.0025
sec-Butylbenzene mg/kg ND 0.0050 08/09/23 22:130.0022
Styrene mg/kg ND 0.0050 08/09/23 22:130.0013
tert-Butylbenzene mg/kg ND 0.0050 08/09/23 22:130.0018
Tetrachloroethene mg/kg ND 0.0050 08/09/23 22:130.0016
Toluene mg/kg ND 0.0050 08/09/23 22:130.0034
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/09/23 22:130.0042
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/09/23 22:130.0017
Trichloroethene mg/kg ND 0.0050 08/09/23 22:130.0040
Trichlorofluoromethane mg/kg ND 0.0050 08/09/23 22:130.0028
Vinyl acetate mg/kg ND 0.050 08/09/23 22:130.010
Vinyl chloride mg/kg ND 0.010 08/09/23 22:130.0025
Xylene (Total)mg/kg ND 0.010 08/09/23 22:130.0028
1,2-Dichloroethane-d4 (S)%109 70-130 08/09/23 22:13
4-Bromofluorobenzene (S)%99 70-130 08/09/23 22:13
Toluene-d8 (S)%101 70-130 08/09/23 22:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4106941LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.470.5 93 70-130
1,1,1-Trichloroethane mg/kg 0.480.5 96 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.480.5 95 70-130
1,1,2-Trichloroethane mg/kg 0.450.5 89 70-130
1,1-Dichloroethane mg/kg 0.480.5 95 70-130
1,1-Dichloroethene mg/kg 0.520.5 104 70-130
1,1-Dichloropropene mg/kg 0.500.5 100 70-130
1,2,3-Trichlorobenzene mg/kg 0.430.5 86 70-130
1,2,3-Trichloropropane mg/kg 0.430.5 87 70-130
1,2,4-Trichlorobenzene mg/kg 0.450.5 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4106941LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.490.5 98 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.400.5 80 67-130
1,2-Dibromoethane (EDB)mg/kg 0.450.5 89 70-130
1,2-Dichlorobenzene mg/kg 0.460.5 92 70-130
1,2-Dichloroethane mg/kg 0.460.5 93 70-130
1,2-Dichloropropane mg/kg 0.460.5 91 70-130
1,3,5-Trimethylbenzene mg/kg 0.490.5 99 70-130
1,3-Dichlorobenzene mg/kg 0.480.5 95 70-130
1,3-Dichloropropane mg/kg 0.450.5 90 70-130
1,4-Dichlorobenzene mg/kg 0.450.5 90 70-130
2,2-Dichloropropane mg/kg 0.450.5 90 67-130
2-Butanone (MEK)mg/kg 0.871 87 66-130
2-Chlorotoluene mg/kg 0.480.5 96 70-130
2-Hexanone mg/kg 0.881 88 70-130
4-Chlorotoluene mg/kg 0.490.5 99 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.891 89 70-130
Acetone mg/kg 0.841 84 67-130
Benzene mg/kg 0.460.5 91 70-130
Bromobenzene mg/kg 0.480.5 96 70-130
Bromochloromethane mg/kg 0.480.5 96 70-130
Bromodichloromethane mg/kg 0.450.5 90 70-130
Bromoform mg/kg 0.460.5 92 70-130
Bromomethane mg/kg 0.500.5 100 53-175
Carbon tetrachloride mg/kg 0.500.5 100 70-130
Chlorobenzene mg/kg 0.470.5 95 70-130
Chloroethane mg/kg 0.480.5 97 70-135
Chloroform mg/kg 0.470.5 95 70-130
Chloromethane mg/kg 0.500.5 100 64-130
cis-1,2-Dichloroethene mg/kg 0.480.5 95 70-130
cis-1,3-Dichloropropene mg/kg 0.440.5 87 70-130
Dibromochloromethane mg/kg 0.470.5 93 70-130
Dibromomethane mg/kg 0.450.5 90 70-130
Dichlorodifluoromethane mg/kg 0.82 L1,v10.5 163 63-145
Diisopropyl ether mg/kg 0.450.5 90 68-130
Ethylbenzene mg/kg 0.440.5 88 70-130
Hexachloro-1,3-butadiene mg/kg 0.480.5 97 70-130
Isopropylbenzene (Cumene)mg/kg 0.480.5 96 70-130
m&p-Xylene mg/kg 0.951 95 70-130
Methyl-tert-butyl ether mg/kg 0.420.5 85 70-130
Methylene Chloride mg/kg 0.480.5 95 67-130
n-Butylbenzene mg/kg 0.510.5 101 70-130
n-Propylbenzene mg/kg 0.490.5 97 70-130
Naphthalene mg/kg 0.470.5 94 70-130
o-Xylene mg/kg 0.470.5 95 70-130
p-Isopropyltoluene mg/kg 0.500.5 100 70-130
sec-Butylbenzene mg/kg 0.480.5 96 70-130
Styrene mg/kg 0.490.5 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4106941LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.480.5 95 64-130
Tetrachloroethene mg/kg 0.470.5 95 70-130
Toluene mg/kg 0.460.5 92 70-130
trans-1,2-Dichloroethene mg/kg 0.490.5 97 70-130
trans-1,3-Dichloropropene mg/kg 0.420.5 85 70-130
Trichloroethene mg/kg 0.470.5 94 70-130
Trichlorofluoromethane mg/kg 0.580.5 116 70-130
Vinyl acetate mg/kg 0.941 94 70-134
Vinyl chloride mg/kg 0.470.5 95 68-130
Xylene (Total)mg/kg 1.41.5 95 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4106942MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681531008
4106943
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 0.66 90 22-16697 7 300.66ND 0.60 0.64
1,1,1-Trichloroethane mg/kg 0.66 96 23-17299 3 300.666.3J ug/kg 0.64 0.66
1,1,2,2-Tetrachloroethane mg/kg 0.66 86 21-15887 2 300.6640.4 ug/kg 0.61 0.62
1,1,2-Trichloroethane mg/kg 0.66 84 25-16089 6 300.66ND 0.56 0.59
1,1-Dichloroethane mg/kg 0.66 89 22-16692 3 300.66ND 0.59 0.61
1,1-Dichloroethene mg/kg 0.66 103 18-183103 0 300.66ND 0.69 0.69
1,1-Dichloropropene mg/kg 0.66 99 20-181100 1 300.66ND 0.66 0.66
1,2,3-Trichlorobenzene mg/kg 0.66 89 10-16186 4 300.66ND 0.59 0.57
1,2,3-Trichloropropane mg/kg 0.66 79 21-14782 4 300.66ND 0.52 0.54
1,2,4-Trichlorobenzene mg/kg 0.66 98 10-15991 7 300.66ND 0.65 0.60
1,2,4-Trimethylbenzene mg/kg 0.66 98 17-17093 5 300.6657.4 ug/kg 0.71 0.67
1,2-Dibromo-3-
chloropropane mg/kg 0.66 77 10-13579 3 300.66ND 0.51 0.53
1,2-Dibromoethane (EDB)mg/kg 0.66 87 30-15491 5 300.66ND 0.58 0.61
1,2-Dichlorobenzene mg/kg 0.66 93 26-16292 2 300.66ND 0.62 0.61
1,2-Dichloroethane mg/kg 0.66 85 23-16186 1 300.66ND 0.57 0.57
1,2-Dichloropropane mg/kg 0.66 88 29-16590 2 300.66ND 0.59 0.60
1,3,5-Trimethylbenzene mg/kg 0.66 101 20-17297 4 300.6631.7 ug/kg 0.70 0.68
1,3-Dichlorobenzene mg/kg 0.66 98 22-16493 5 300.66ND 0.65 0.62
1,3-Dichloropropane mg/kg 0.66 87 27-15689 3 300.66ND 0.58 0.59
1,4-Dichlorobenzene mg/kg 0.66 90 20-16188 2 300.66ND 0.60 0.58
2,2-Dichloropropane mg/kg 0.66 73 10-15974 2 300.66ND 0.48 0.49
2-Butanone (MEK)mg/kg 1.3 76 13-14375 1 301.3ND 1.0 1.0
2-Chlorotoluene mg/kg 0.66 93 21-16693 0 300.66ND 0.62 0.62
2-Hexanone mg/kg 1.3 81 19-14585 5 301.3ND 1.1 1.1
4-Chlorotoluene mg/kg 0.66 96 19-16395 1 300.66ND 0.64 0.63
4-Methyl-2-pentanone
(MIBK)mg/kg 1.3 77 21-15181 4 301.3ND 1.0 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4106942MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681531008
4106943
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone mg/kg 1.3 59 10-13352 13 301.3ND 0.78 0.69
Benzene mg/kg 0.66 90 29-15692 3 300.66ND 0.60 0.61
Bromobenzene mg/kg 0.66 96 25-16198 2 300.66ND 0.64 0.65
Bromochloromethane mg/kg 0.66 91 27-15892 2 300.66ND 0.60 0.61
Bromodichloromethane mg/kg 0.66 83 23-15886 3 300.66ND 0.55 0.57
Bromoform mg/kg 0.66 87 19-15291 5 300.66ND 0.58 0.61
Bromomethane mg/kg 0.66 32 10-15232 1 300.66ND 0.21 0.21
Carbon tetrachloride mg/kg 0.66 88 18-17290 3 300.66ND 0.58 0.60
Chlorobenzene mg/kg 0.66 95 26-16697 2 300.66ND 0.63 0.64
Chloroethane mg/kg 0.66 28 10-13029 5 300.66ND 0.18 0.19
Chloroform mg/kg 0.66 91 25-16193 2 300.66ND 0.61 0.62
Chloromethane mg/kg 0.66 110 27-197114 3 300.66ND 0.73 0.76
cis-1,2-Dichloroethene mg/kg 0.66 90 28-16592 2 300.6681.7 ug/kg 0.68 0.70
cis-1,3-Dichloropropene mg/kg 0.66 79 23-15982 3 300.66ND 0.53 0.54
Dibromochloromethane mg/kg 0.66 88 21-15191 4 300.66ND 0.58 0.60
Dibromomethane mg/kg 0.66 85 38-15890 5 300.66ND 0.57 0.60
Dichlorodifluoromethane mg/kg v10.66 168 10-200169 1 300.66ND 1.1 1.1
Diisopropyl ether mg/kg 0.66 84 23-16085 1 300.66ND 0.56 0.56
Ethylbenzene mg/kg 0.66 88 22-16387 1 300.6622.2 ug/kg 0.61 0.60
Hexachloro-1,3-butadiene mg/kg 0.66 153 10-192141 8 300.66ND 1.0 0.94
Isopropylbenzene
(Cumene)mg/kg 0.66 101 24-17399 2 300.66ND 0.67 0.66
m&p-Xylene mg/kg 1.3 96 22-17196 0 301.361.4 ug/kg 1.3 1.3
Methyl-tert-butyl ether mg/kg 0.66 80 25-15381 2 300.66ND 0.53 0.54
Methylene Chloride mg/kg 0.66 88 10-16589 1 300.66ND 0.58 0.59
n-Butylbenzene mg/kg 0.66 114 10-186104 10 300.66ND 0.76 0.69
n-Propylbenzene mg/kg 0.66 100 16-17194 6 300.66ND 0.67 0.63
Naphthalene mg/kg 0.66 88 10-15987 1 300.6628.6 ug/kg 0.62 0.61
o-Xylene mg/kg 0.66 96 23-17198 2 300.6612.3 ug/kg 0.65 0.66
p-Isopropyltoluene mg/kg 0.66 109 13-184100 9 300.6617.2 ug/kg 0.74 0.68
sec-Butylbenzene mg/kg 0.66 107 16-18299 8 300.66ND 0.71 0.66
Styrene mg/kg 0.66 97 25-16998 1 300.66ND 0.64 0.65
tert-Butylbenzene mg/kg 0.66 80 20-17475 6 300.66ND 0.53 0.50
Tetrachloroethene mg/kg 0.66 91 14-17191 0 300.66772 ug/kg 1.4 1.4
Toluene mg/kg 0.66 90 24-16692 2 300.6617.1 ug/kg 0.62 0.63
trans-1,2-Dichloroethene mg/kg 0.66 91 24-17092 1 300.66ND 0.61 0.61
trans-1,3-Dichloropropene mg/kg 0.66 78 22-15780 3 300.66ND 0.52 0.53
Trichloroethene mg/kg 0.66 95 23-17697 1 300.66617 ug/kg 1.2 1.3
Trichlorofluoromethane mg/kg 0.66 34 10-13836 6 300.66ND 0.22 0.24
Vinyl acetate mg/kg 1.3 77 11-16679 3 301.3ND 1.0 1.1
Vinyl chloride mg/kg 0.66 87 21-20089 2 300.66ND 0.58 0.59
Xylene (Total)mg/kg 2 96 23-17096 1 30273.7 ug/kg 2.0 2.0
1,2-Dichloroethane-d4 (S)%102 70-130100
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
792570
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077012, 92681077013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4107337
Associated Lab Samples:92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/09/23 21:260.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 08/09/23 21:260.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/09/23 21:260.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 08/09/23 21:260.0017
1,1-Dichloroethane mg/kg ND 0.0050 08/09/23 21:260.0021
1,1-Dichloroethene mg/kg ND 0.0050 08/09/23 21:260.0021
1,1-Dichloropropene mg/kg ND 0.0050 08/09/23 21:260.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/09/23 21:260.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 08/09/23 21:260.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 IK08/09/23 21:260.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/09/23 21:260.0030
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/09/23 21:260.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/09/23 21:260.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 08/09/23 21:260.0018
1,2-Dichloroethane mg/kg ND 0.0050 08/09/23 21:260.0033
1,2-Dichloropropane mg/kg ND 0.0050 08/09/23 21:260.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/09/23 21:260.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 08/09/23 21:260.0016
1,3-Dichloropropane mg/kg ND 0.0050 08/09/23 21:260.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 08/09/23 21:260.0013
2,2-Dichloropropane mg/kg ND 0.0050 08/09/23 21:260.0038
2-Butanone (MEK)mg/kg ND 0.10 08/09/23 21:260.024
2-Chlorotoluene mg/kg ND 0.0050 08/09/23 21:260.0018
2-Hexanone mg/kg ND 0.050 08/09/23 21:260.0048
4-Chlorotoluene mg/kg ND 0.0050 08/09/23 21:260.0028
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/09/23 21:260.0048
Acetone mg/kg ND 0.10 08/09/23 21:260.032
Benzene mg/kg ND 0.0050 08/09/23 21:260.0020
Bromobenzene mg/kg ND 0.0050 08/09/23 21:260.0016
Bromochloromethane mg/kg ND 0.0050 08/09/23 21:260.0015
Bromodichloromethane mg/kg ND 0.0050 08/09/23 21:260.0019
Bromoform mg/kg ND 0.0050 08/09/23 21:260.0018
Bromomethane mg/kg ND 0.020 v208/09/23 21:260.016
Carbon tetrachloride mg/kg ND 0.0050 08/09/23 21:260.0019
Chlorobenzene mg/kg ND 0.0050 08/09/23 21:260.0029
Chloroethane mg/kg ND 0.010 08/09/23 21:260.0039
Chloroform mg/kg ND 0.0050 08/09/23 21:260.0042
Chloromethane mg/kg ND 0.010 08/09/23 21:260.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/09/23 21:260.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/09/23 21:260.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4107337
Associated Lab Samples:92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 08/09/23 21:260.0028
Dibromomethane mg/kg ND 0.0050 08/09/23 21:260.0011
Dichlorodifluoromethane mg/kg ND 0.010 v108/09/23 21:260.0051
Diisopropyl ether mg/kg ND 0.0050 08/09/23 21:260.0014
Ethylbenzene mg/kg ND 0.0050 08/09/23 21:260.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/09/23 21:260.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/09/23 21:260.0017
m&p-Xylene mg/kg ND 0.010 08/09/23 21:260.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 08/09/23 21:260.0019
Methylene Chloride mg/kg ND 0.020 08/09/23 21:260.014
n-Butylbenzene mg/kg ND 0.0050 08/09/23 21:260.0032
n-Propylbenzene mg/kg ND 0.0050 08/09/23 21:260.0018
Naphthalene mg/kg ND 0.0050 08/09/23 21:260.0026
o-Xylene mg/kg ND 0.0050 08/09/23 21:260.0022
p-Isopropyltoluene mg/kg ND 0.0050 08/09/23 21:260.0025
sec-Butylbenzene mg/kg ND 0.0050 08/09/23 21:260.0022
Styrene mg/kg ND 0.0050 08/09/23 21:260.0013
tert-Butylbenzene mg/kg ND 0.0050 08/09/23 21:260.0018
Tetrachloroethene mg/kg ND 0.0050 08/09/23 21:260.0016
Toluene mg/kg ND 0.0050 08/09/23 21:260.0034
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/09/23 21:260.0042
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/09/23 21:260.0017
Trichloroethene mg/kg ND 0.0050 08/09/23 21:260.0040
Trichlorofluoromethane mg/kg ND 0.0050 08/09/23 21:260.0028
Vinyl acetate mg/kg ND 0.050 08/09/23 21:260.010
Vinyl chloride mg/kg ND 0.010 08/09/23 21:260.0025
Xylene (Total)mg/kg ND 0.010 08/09/23 21:260.0028
1,2-Dichloroethane-d4 (S)%110 70-130 08/09/23 21:26
4-Bromofluorobenzene (S)%102 70-130 08/09/23 21:26
Toluene-d8 (S)%100 70-130 08/09/23 21:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4107338LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.440.5 88 70-130
1,1,1-Trichloroethane mg/kg 0.480.5 95 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.440.5 87 70-130
1,1,2-Trichloroethane mg/kg 0.430.5 85 70-130
1,1-Dichloroethane mg/kg 0.460.5 93 70-130
1,1-Dichloroethene mg/kg 0.510.5 102 70-130
1,1-Dichloropropene mg/kg 0.480.5 95 70-130
1,2,3-Trichlorobenzene mg/kg 0.440.5 87 70-130
1,2,3-Trichloropropane mg/kg 0.460.5 92 70-130
1,2,4-Trichlorobenzene mg/kg 0.44 IK0.5 88 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4107338LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.480.5 96 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.390.5 78 67-130
1,2-Dibromoethane (EDB)mg/kg 0.440.5 88 70-130
1,2-Dichlorobenzene mg/kg 0.420.5 84 70-130
1,2-Dichloroethane mg/kg 0.480.5 95 70-130
1,2-Dichloropropane mg/kg 0.450.5 90 70-130
1,3,5-Trimethylbenzene mg/kg 0.470.5 95 70-130
1,3-Dichlorobenzene mg/kg 0.430.5 87 70-130
1,3-Dichloropropane mg/kg 0.440.5 88 70-130
1,4-Dichlorobenzene mg/kg 0.440.5 87 70-130
2,2-Dichloropropane mg/kg 0.440.5 88 67-130
2-Butanone (MEK)mg/kg 0.841 84 66-130
2-Chlorotoluene mg/kg 0.460.5 93 70-130
2-Hexanone mg/kg 0.851 85 70-130
4-Chlorotoluene mg/kg 0.460.5 93 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.881 88 70-130
Acetone mg/kg 0.871 87 67-130
Benzene mg/kg 0.460.5 91 70-130
Bromobenzene mg/kg 0.420.5 84 70-130
Bromochloromethane mg/kg 0.430.5 85 70-130
Bromodichloromethane mg/kg 0.440.5 88 70-130
Bromoform mg/kg 0.420.5 85 70-130
Bromomethane mg/kg 0.39 v30.5 79 53-175
Carbon tetrachloride mg/kg 0.480.5 97 70-130
Chlorobenzene mg/kg 0.450.5 89 70-130
Chloroethane mg/kg 0.490.5 97 70-135
Chloroform mg/kg 0.460.5 91 70-130
Chloromethane mg/kg 0.490.5 97 64-130
cis-1,2-Dichloroethene mg/kg 0.480.5 96 70-130
cis-1,3-Dichloropropene mg/kg 0.440.5 89 70-130
Dibromochloromethane mg/kg 0.450.5 90 70-130
Dibromomethane mg/kg 0.420.5 84 70-130
Dichlorodifluoromethane mg/kg 0.73 v10.5 145 63-145
Diisopropyl ether mg/kg 0.450.5 90 68-130
Ethylbenzene mg/kg 0.460.5 93 70-130
Hexachloro-1,3-butadiene mg/kg 0.450.5 89 70-130
Isopropylbenzene (Cumene)mg/kg 0.470.5 94 70-130
m&p-Xylene mg/kg 0.911 91 70-130
Methyl-tert-butyl ether mg/kg 0.420.5 85 70-130
Methylene Chloride mg/kg 0.470.5 93 67-130
n-Butylbenzene mg/kg 0.460.5 92 70-130
n-Propylbenzene mg/kg 0.460.5 92 70-130
Naphthalene mg/kg 0.430.5 86 70-130
o-Xylene mg/kg 0.460.5 93 70-130
p-Isopropyltoluene mg/kg 0.460.5 93 70-130
sec-Butylbenzene mg/kg 0.460.5 93 70-130
Styrene mg/kg 0.480.5 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4107338LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.440.5 89 64-130
Tetrachloroethene mg/kg 0.440.5 89 70-130
Toluene mg/kg 0.420.5 85 70-130
trans-1,2-Dichloroethene mg/kg 0.480.5 95 70-130
trans-1,3-Dichloropropene mg/kg 0.410.5 83 70-130
Trichloroethene mg/kg 0.440.5 88 70-130
Trichlorofluoromethane mg/kg 0.540.5 108 70-130
Vinyl acetate mg/kg 0.941 94 70-134
Vinyl chloride mg/kg 0.450.5 91 68-130
Xylene (Total)mg/kg 1.41.5 92 70-130
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4107339MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681207001
4107340
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg M1,R10.64 36 22-16612 99 300.64ND 0.23 0.078
1,1,1-Trichloroethane mg/kg M1,R10.64 41 23-17216 85 300.64ND 0.26 0.10
1,1,2,2-Tetrachloroethane mg/kg M1,R10.64 35 21-15814 88 300.64ND 0.23 0.088
1,1,2-Trichloroethane mg/kg M1,R10.64 38 25-16014 91 300.64ND 0.24 0.090
1,1-Dichloroethane mg/kg M1,R10.64 40 22-16616 84 300.64ND 0.26 0.10
1,1-Dichloroethene mg/kg R10.64 47 18-18318 88 300.64ND 0.30 0.12
1,1-Dichloropropene mg/kg M1,R10.64 43 20-18117 87 300.64ND 0.28 0.11
1,2,3-Trichlorobenzene mg/kg R10.64 35 10-16114 84 300.64ND 0.22 0.091
1,2,3-Trichloropropane mg/kg M1,R10.64 37 21-14713 94 300.64ND 0.24 0.085
1,2,4-Trichlorobenzene mg/kg IK,R10.64 35 10-15916 76 300.64ND 0.22 0.10
1,2,4-Trimethylbenzene mg/kg R10.64 44 17-17019 79 300.64ND 0.28 0.12
1,2-Dibromo-3-
chloropropane mg/kg R10.64 32 10-13510 101 300.64ND 0.20 0.067
1,2-Dibromoethane (EDB)mg/kg M1,R10.64 37 30-15413 93 300.64ND 0.23 0.085
1,2-Dichlorobenzene mg/kg M1,R10.64 35 26-16215 81 300.64ND 0.22 0.094
1,2-Dichloroethane mg/kg M1,R10.64 40 23-16117 81 300.64ND 0.26 0.11
1,2-Dichloropropane mg/kg M1,R10.64 40 29-16515 93 300.64ND 0.26 0.094
1,3,5-Trimethylbenzene mg/kg M1,R10.64 42 20-17217 83 300.64ND 0.27 0.11
1,3-Dichlorobenzene mg/kg M1,R10.64 38 22-16416 80 300.64ND 0.24 0.10
1,3-Dichloropropane mg/kg M1,R10.64 37 27-15614 87 300.64ND 0.23 0.092
1,4-Dichlorobenzene mg/kg M1,R10.64 37 20-16115 84 300.64ND 0.24 0.096
2,2-Dichloropropane mg/kg R10.64 36 10-15915 82 300.64ND 0.23 0.096
2-Butanone (MEK)mg/kg M1,R11.3 32 13-14312 89 301.3ND 0.41 0.16
2-Chlorotoluene mg/kg M1,R10.64 41 21-16616 86 300.64ND 0.26 0.10
2-Hexanone mg/kg M1,R11.3 32 19-14512 94 301.3ND 0.41 0.15
4-Chlorotoluene mg/kg M1,R10.64 39 19-16316 82 300.64ND 0.25 0.10
4-Methyl-2-pentanone
(MIBK)mg/kg M1,R11.3 35 21-15113 93 301.3ND 0.44 0.16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4107339MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681207001
4107340
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone mg/kg R11.3 38 10-13319 67 301.3ND 0.49 0.24
Benzene mg/kg M1,R10.64 40 29-15616 85 300.64ND 0.26 0.10
Bromobenzene mg/kg M1,R10.64 38 25-16115 85 300.64ND 0.24 0.096
Bromochloromethane mg/kg M1,R10.64 41 27-15815 93 300.64ND 0.26 0.095
Bromodichloromethane mg/kg M1,R10.64 36 23-15814 85 300.64ND 0.23 0.092
Bromoform mg/kg M1,R10.64 33 19-15212 93 300.64ND 0.21 0.078
Bromomethane mg/kg R1,v30.64 53 10-15228 63 300.64ND 0.34 0.18
Carbon tetrachloride mg/kg R10.64 45 18-17218 86 300.64ND 0.29 0.11
Chlorobenzene mg/kg M1,R10.64 38 26-16615 85 300.64ND 0.24 0.097
Chloroethane mg/kg R10.64 69 10-13039 57 300.64ND 0.44 0.25
Chloroform mg/kg M1,R10.64 40 25-16116 86 300.64ND 0.25 0.10
Chloromethane mg/kg M1,R10.64 49 27-19722 77 300.64ND 0.31 0.14
cis-1,2-Dichloroethene mg/kg M1,R10.64 43 28-16517 85 300.64ND 0.27 0.11
cis-1,3-Dichloropropene mg/kg M1,R10.64 37 23-15914 90 300.64ND 0.24 0.090
Dibromochloromethane mg/kg M1,R10.64 36 21-15113 92 300.64ND 0.23 0.086
Dibromomethane mg/kg M1,R10.64 35 38-15813 93 300.64ND 0.22 0.081
Dichlorodifluoromethane mg/kg R1,v10.64 71 10-20027 90 300.64ND 0.45 0.17
Diisopropyl ether mg/kg M1,R10.64 36 23-16014 88 300.64ND 0.23 0.090
Ethylbenzene mg/kg M1,R10.64 40 22-16317 81 300.64ND 0.26 0.11
Hexachloro-1,3-butadiene mg/kg R10.64 39 10-19216 83 300.64ND 0.25 0.10
Isopropylbenzene
(Cumene)mg/kg M1,R10.64 40 24-17317 83 300.64ND 0.26 0.11
m&p-Xylene mg/kg M1,R11.3 39 22-17116 84 301.3ND 0.50 0.20
Methyl-tert-butyl ether mg/kg M1,R10.64 35 25-15313 90 300.64ND 0.23 0.086
Methylene Chloride mg/kg R10.64 43 10-16518 65 300.6455.4 ug/kg 0.33 0.17
n-Butylbenzene mg/kg R10.64 39 10-18617 81 300.64ND 0.25 0.11
n-Propylbenzene mg/kg R10.64 40 16-17117 83 300.64ND 0.25 0.11
Naphthalene mg/kg R10.64 35 10-15915 81 300.64ND 0.22 0.095
o-Xylene mg/kg M1,R10.64 40 23-17115 91 300.64ND 0.26 0.096
p-Isopropyltoluene mg/kg R10.64 38 13-18415 85 300.64ND 0.24 0.097
sec-Butylbenzene mg/kg R10.64 40 16-18218 77 300.64ND 0.25 0.11
Styrene mg/kg M1,R10.64 40 25-16915 91 300.64ND 0.25 0.095
tert-Butylbenzene mg/kg M1,R10.64 35 20-17415 79 300.64ND 0.23 0.098
Tetrachloroethene mg/kg R10.64 36 14-17115 86 300.64ND 0.23 0.093
Toluene mg/kg M1,R10.64 37 24-16615 84 300.64ND 0.24 0.097
trans-1,2-Dichloroethene mg/kg M1,R10.64 43 24-17017 87 300.64ND 0.27 0.11
trans-1,3-Dichloropropene mg/kg M1,R10.64 34 22-15713 91 300.64ND 0.22 0.083
Trichloroethene mg/kg M1,R10.64 40 23-17616 85 300.64ND 0.26 0.10
Trichlorofluoromethane mg/kg R10.64 42 10-13817 83 300.64ND 0.27 0.11
Vinyl acetate mg/kg R11.3 33 11-16611 103 301.3ND 0.42 0.14
Vinyl chloride mg/kg M1,R10.64 45 21-20019 82 300.64ND 0.29 0.12
Xylene (Total)mg/kg MS,RS1.9 39 23-17016 86 301.9ND 0.75 0.30
1,2-Dichloroethane-d4 (S)%105 70-130104
4-Bromofluorobenzene (S)%103 70-130105
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
792401
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4106151
Associated Lab Samples:92681077014
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/10/23 00:300.31
1,1,1-Trichloroethane ug/L ND 1.0 08/10/23 00:300.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/10/23 00:300.22
1,1,2-Trichloroethane ug/L ND 1.0 08/10/23 00:300.32
1,1-Dichloroethane ug/L ND 1.0 08/10/23 00:300.37
1,1-Dichloroethene ug/L ND 1.0 08/10/23 00:300.35
1,1-Dichloropropene ug/L ND 1.0 08/10/23 00:300.43
1,2,3-Trichlorobenzene ug/L ND 1.0 08/10/23 00:300.81
1,2,3-Trichloropropane ug/L ND 1.0 08/10/23 00:300.26
1,2,4-Trichlorobenzene ug/L ND 1.0 08/10/23 00:300.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/10/23 00:300.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/10/23 00:300.27
1,2-Dichlorobenzene ug/L ND 1.0 08/10/23 00:300.34
1,2-Dichloroethane ug/L ND 1.0 08/10/23 00:300.32
1,2-Dichloropropane ug/L ND 1.0 08/10/23 00:300.36
1,3-Dichlorobenzene ug/L ND 1.0 08/10/23 00:300.34
1,3-Dichloropropane ug/L ND 1.0 08/10/23 00:300.28
1,4-Dichlorobenzene ug/L ND 1.0 08/10/23 00:300.33
2,2-Dichloropropane ug/L ND 1.0 08/10/23 00:300.39
2-Butanone (MEK)ug/L ND 5.0 08/10/23 00:304.0
2-Chlorotoluene ug/L ND 1.0 08/10/23 00:300.32
2-Hexanone ug/L ND 5.0 08/10/23 00:300.48
4-Chlorotoluene ug/L ND 1.0 08/10/23 00:300.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/10/23 00:302.7
Acetone ug/L ND 25.0 08/10/23 00:305.1
Benzene ug/L ND 1.0 08/10/23 00:300.34
Bromobenzene ug/L ND 1.0 08/10/23 00:300.29
Bromochloromethane ug/L ND 1.0 08/10/23 00:300.47
Bromodichloromethane ug/L ND 1.0 08/10/23 00:300.31
Bromoform ug/L ND 1.0 08/10/23 00:300.34
Bromomethane ug/L ND 2.0 v208/10/23 00:301.7
Carbon tetrachloride ug/L ND 1.0 08/10/23 00:300.33
Chlorobenzene ug/L ND 1.0 08/10/23 00:300.28
Chloroethane ug/L ND 1.0 08/10/23 00:300.65
Chloroform ug/L ND 1.0 08/10/23 00:300.43
Chloromethane ug/L ND 1.0 08/10/23 00:300.54
cis-1,2-Dichloroethene ug/L ND 1.0 08/10/23 00:300.38
cis-1,3-Dichloropropene ug/L ND 1.0 08/10/23 00:300.36
Dibromochloromethane ug/L ND 1.0 08/10/23 00:300.36
Dibromomethane ug/L ND 1.0 08/10/23 00:300.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4106151
Associated Lab Samples:92681077014
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 08/10/23 00:300.35
Diisopropyl ether ug/L ND 1.0 08/10/23 00:300.31
Ethylbenzene ug/L ND 1.0 08/10/23 00:300.30
Hexachloro-1,3-butadiene ug/L ND 2.0 08/10/23 00:301.5
m&p-Xylene ug/L ND 2.0 08/10/23 00:300.71
Methyl-tert-butyl ether ug/L ND 1.0 08/10/23 00:300.42
Methylene Chloride ug/L ND 5.0 08/10/23 00:302.0
Naphthalene ug/L ND 1.0 08/10/23 00:300.64
o-Xylene ug/L ND 1.0 08/10/23 00:300.34
p-Isopropyltoluene ug/L ND 1.0 08/10/23 00:300.41
Styrene ug/L ND 1.0 08/10/23 00:300.29
Tetrachloroethene ug/L ND 1.0 08/10/23 00:300.29
Toluene ug/L ND 1.0 08/10/23 00:300.24
trans-1,2-Dichloroethene ug/L ND 1.0 08/10/23 00:300.40
trans-1,3-Dichloropropene ug/L ND 1.0 08/10/23 00:300.36
Trichloroethene ug/L ND 1.0 08/10/23 00:300.38
Trichlorofluoromethane ug/L ND 1.0 08/10/23 00:300.30
Vinyl acetate ug/L ND 2.0 08/10/23 00:301.3
Vinyl chloride ug/L ND 1.0 08/10/23 00:300.39
Xylene (Total)ug/L ND 1.0 08/10/23 00:300.34
1,2-Dichloroethane-d4 (S)%101 70-130 08/10/23 00:30
4-Bromofluorobenzene (S)%100 70-130 08/10/23 00:30
Toluene-d8 (S)%98 70-130 08/10/23 00:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4106152LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.920 104 70-130
1,1,1-Trichloroethane ug/L 19.820 99 70-130
1,1,2,2-Tetrachloroethane ug/L 20.420 102 70-130
1,1,2-Trichloroethane ug/L 20.420 102 70-130
1,1-Dichloroethane ug/L 19.720 99 70-130
1,1-Dichloroethene ug/L 20.720 104 70-130
1,1-Dichloropropene ug/L 20.920 104 70-130
1,2,3-Trichlorobenzene ug/L 20.120 101 70-130
1,2,3-Trichloropropane ug/L 19.520 98 70-130
1,2,4-Trichlorobenzene ug/L 19.820 99 70-130
1,2-Dibromo-3-chloropropane ug/L 19.720 98 70-131
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130
1,2-Dichlorobenzene ug/L 20.520 103 70-130
1,2-Dichloroethane ug/L 20.020 100 70-130
1,2-Dichloropropane ug/L 20.120 101 70-130
1,3-Dichlorobenzene ug/L 20.920 104 70-130
1,3-Dichloropropane ug/L 20.020 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4106152LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 20.120 101 70-130
2,2-Dichloropropane ug/L 19.320 96 68-135
2-Butanone (MEK)ug/L 39.340 98 70-134
2-Chlorotoluene ug/L 20.220 101 70-130
2-Hexanone ug/L 41.740 104 70-131
4-Chlorotoluene ug/L 20.320 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 40.240 100 70-130
Acetone ug/L 38.840 97 70-133
Benzene ug/L 20.320 101 70-130
Bromobenzene ug/L 20.020 100 70-130
Bromochloromethane ug/L 20.420 102 70-130
Bromodichloromethane ug/L 19.820 99 70-130
Bromoform ug/L 19.620 98 70-130
Bromomethane ug/L 14.2 v3207145-151
Carbon tetrachloride ug/L 21.020 105 70-130
Chlorobenzene ug/L 20.320 101 70-130
Chloroethane ug/L 20.320 102 39-152
Chloroform ug/L 20.120 100 70-130
Chloromethane ug/L 16.820 84 58-130
cis-1,2-Dichloroethene ug/L 19.920 100 70-130
cis-1,3-Dichloropropene ug/L 19.520 97 70-130
Dibromochloromethane ug/L 20.120 101 70-130
Dibromomethane ug/L 20.220 101 70-130
Dichlorodifluoromethane ug/L 20.720 103 54-133
Diisopropyl ether ug/L 18.920 94 70-130
Ethylbenzene ug/L 20.220 101 70-130
Hexachloro-1,3-butadiene ug/L 20.420 102 70-135
m&p-Xylene ug/L 40.340 101 70-130
Methyl-tert-butyl ether ug/L 18.120 91 70-130
Methylene Chloride ug/L 19.220 96 66-130
Naphthalene ug/L 21.420 107 70-130
o-Xylene ug/L 20.220 101 70-130
p-Isopropyltoluene ug/L 20.720 104 70-130
Styrene ug/L 20.320 101 70-130
Tetrachloroethene ug/L 20.320 101 70-130
Toluene ug/L 19.720 98 70-130
trans-1,2-Dichloroethene ug/L 20.420 102 70-130
trans-1,3-Dichloropropene ug/L 19.420 97 70-130
Trichloroethene ug/L 20.720 104 70-130
Trichlorofluoromethane ug/L 19.520 97 62-130
Vinyl acetate ug/L 40.040 100 70-144
Vinyl chloride ug/L 16.120 80 62-130
Xylene (Total)ug/L 60.660 101 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4106153MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681261010
4106154
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 131 70-141121 8 3020ND26.3 24.1
1,1,1-Trichloroethane ug/L 20 136 70-150125 8 3020ND27.1 25.0
1,1,2,2-Tetrachloroethane ug/L 20 125 69-142119 5 3020ND25.0 23.8
1,1,2-Trichloroethane ug/L 20 125 70-138117 6 3020ND25.0 23.5
1,1-Dichloroethane ug/L 20 131 70-150120 8 3020ND26.2 24.1
1,1-Dichloroethene ug/L 20 145 70-156136 6 3020ND29.0 27.3
1,1-Dichloropropene ug/L 20 142 70-150130 9 3020ND28.5 26.0
1,2,3-Trichlorobenzene ug/L 20 127 70-148116 9 3020ND25.5 23.3
1,2,3-Trichloropropane ug/L 20 122 70-140113 7 3020ND24.4 22.7
1,2,4-Trichlorobenzene ug/L 20 124 70-146113 9 3020ND24.8 22.6
1,2-Dibromo-3-
chloropropane ug/L 20 124 68-146117 6 3020ND24.9 23.3
1,2-Dibromoethane (EDB)ug/L 20 125 70-138116 7 3020ND25.0 23.3
1,2-Dichlorobenzene ug/L 20 127 70-141115 10 3020ND25.4 22.9
1,2-Dichloroethane ug/L 20 125 69-143115 8 3020ND25.0 23.0
1,2-Dichloropropane ug/L 20 127 68-156118 7 3020ND25.5 23.7
1,3-Dichlorobenzene ug/L 20 126 70-143118 7 3020ND25.3 23.6
1,3-Dichloropropane ug/L 20 122 70-138111 9 3020ND24.3 22.3
1,4-Dichlorobenzene ug/L 20 126 70-142117 8 3020ND25.3 23.3
2,2-Dichloropropane ug/L 20 142 52-170130 8 3020ND28.3 26.1
2-Butanone (MEK)ug/L 40 119 60-157115 3 3040ND47.7 46.2
2-Chlorotoluene ug/L 20 123 70-147116 6 3020ND24.6 23.1
2-Hexanone ug/L 40 126 68-146117 8 3040ND50.3 46.6
4-Chlorotoluene ug/L 20 126 70-142119 6 3020ND25.3 23.9
4-Methyl-2-pentanone
(MIBK)ug/L 40 122 70-141116 5 3040ND48.8 46.3
Acetone ug/L 40 116 58-157109 6 3040ND47.8 45.0
Benzene ug/L 20 127 70-142120 6 3020ND25.5 24.0
Bromobenzene ug/L 20 125 70-143117 6 3020ND24.9 23.4
Bromochloromethane ug/L 20 128 70-146119 7 3020ND25.6 23.8
Bromodichloromethane ug/L 20 122 70-139113 7 3020ND24.3 22.6
Bromoform ug/L 20 125 64-140119 6 3020ND25.1 23.7
Bromomethane ug/L 20 115 28-192115 0 3020ND23.0 22.9
Carbon tetrachloride ug/L 20 140 70-148129 8 3020ND28.0 25.8
Chlorobenzene ug/L 20 126 70-141118 7 3020ND25.3 23.6
Chloroethane ug/L 20 127 58-191119 6 3020ND25.4 23.8
Chloroform ug/L 20 130 70-148116 11 3020ND26.0 23.3
Chloromethane ug/L 20 119 43-162110 8 3020ND23.7 22.0
cis-1,2-Dichloroethene ug/L 20 130 68-151122 6 3020ND26.0 24.5
cis-1,3-Dichloropropene ug/L 20 127 70-139121 5 3020ND25.5 24.2
Dibromochloromethane ug/L 20 130 70-144120 8 3020ND25.9 23.9
Dibromomethane ug/L 20 126 70-139117 8 3020ND25.2 23.3
Dichlorodifluoromethane ug/L 20 161 39-171149 8 3020ND32.2 29.8
Diisopropyl ether ug/L 20 122 67-142113 7 3020ND24.3 22.6
Ethylbenzene ug/L 20 126 70-143116 8 3020ND25.2 23.3
Hexachloro-1,3-butadiene ug/L 20 139 64-163128 8 3020ND27.7 25.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4106153MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681261010
4106154
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 128 70-144116 8 304011.2 62.2 57.5
Methyl-tert-butyl ether ug/L 20 118 65-143110 7 3020ND23.7 22.1
Methylene Chloride ug/L 20 122 62-149113 8 3020ND24.6 22.8
Naphthalene ug/L 20 126 67-147118 6 3020ND25.2 23.7
o-Xylene ug/L 20 127 70-145116 9 3020ND25.3 23.2
p-Isopropyltoluene ug/L 20 132 70-147121 8 3020ND26.3 24.3
Styrene ug/L 20 127 70-143118 7 3020ND25.4 23.6
Tetrachloroethene ug/L 20 126 70-145118 7 3020ND25.3 23.6
Toluene ug/L 20 125 70-142117 7 3020ND25.0 23.3
trans-1,2-Dichloroethene ug/L 20 136 70-151126 8 3020ND27.2 25.2
trans-1,3-Dichloropropene ug/L 20 123 70-139117 5 3020ND24.6 23.4
Trichloroethene ug/L 20 128 62-146119 7 3020ND25.6 23.8
Trichlorofluoromethane ug/L 20 142 63-153132 7 3020ND28.3 26.4
Vinyl acetate ug/L 40 128 61-162118 8 3040ND51.2 47.3
Vinyl chloride ug/L 20 117 61-163110 6 3020ND23.4 22.0
Xylene (Total)ug/L 60 127 70-143116 8 306011.2 87.5 80.6
1,2-Dichloroethane-d4 (S)%101 70-13099
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
793123
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4109953
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 08/13/23 10:190.13
1,2-Dichlorobenzene mg/kg ND 0.33 08/13/23 10:190.12
1,3-Dichlorobenzene mg/kg ND 0.33 08/13/23 10:190.12
1,4-Dichlorobenzene mg/kg ND 0.33 08/13/23 10:190.12
1-Methylnaphthalene mg/kg ND 0.33 08/13/23 10:190.11
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 08/13/23 10:190.15
2,4,5-Trichlorophenol mg/kg ND 0.33 08/13/23 10:190.15
2,4,6-Trichlorophenol mg/kg ND 0.33 08/13/23 10:190.13
2,4-Dichlorophenol mg/kg ND 0.33 08/13/23 10:190.13
2,4-Dimethylphenol mg/kg ND 0.33 08/13/23 10:190.14
2,4-Dinitrophenol mg/kg ND 1.6 08/13/23 10:191.0
2,4-Dinitrotoluene mg/kg ND 0.33 08/13/23 10:190.13
2,6-Dinitrotoluene mg/kg ND 0.33 08/13/23 10:190.12
2-Chloronaphthalene mg/kg ND 0.33 08/13/23 10:190.13
2-Chlorophenol mg/kg ND 0.33 08/13/23 10:190.12
2-Methylnaphthalene mg/kg ND 0.33 08/13/23 10:190.13
2-Methylphenol(o-Cresol)mg/kg ND 0.33 08/13/23 10:190.13
2-Nitroaniline mg/kg ND 1.6 08/13/23 10:190.27
2-Nitrophenol mg/kg ND 0.33 08/13/23 10:190.14
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 08/13/23 10:190.13
3,3'-Dichlorobenzidine mg/kg ND 0.65 08/13/23 10:190.22
3-Nitroaniline mg/kg ND 1.6 08/13/23 10:190.26
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 08/13/23 10:190.30
4-Bromophenylphenyl ether mg/kg ND 0.33 08/13/23 10:190.13
4-Chloro-3-methylphenol mg/kg ND 0.65 08/13/23 10:190.23
4-Chloroaniline mg/kg ND 0.65 08/13/23 10:190.26
4-Chlorophenylphenyl ether mg/kg ND 0.33 08/13/23 10:190.12
4-Nitroaniline mg/kg ND 0.65 08/13/23 10:190.25
4-Nitrophenol mg/kg ND 1.6 08/13/23 10:190.63
Acenaphthene mg/kg ND 0.33 08/13/23 10:190.11
Acenaphthylene mg/kg ND 0.33 08/13/23 10:190.11
Aniline mg/kg ND 0.33 08/13/23 10:190.13
Anthracene mg/kg ND 0.33 08/13/23 10:190.11
Benzo(a)anthracene mg/kg ND 0.33 08/13/23 10:190.11
Benzo(a)pyrene mg/kg ND 0.33 08/13/23 10:190.11
Benzo(b)fluoranthene mg/kg ND 0.33 08/13/23 10:190.11
Benzo(g,h,i)perylene mg/kg ND 0.33 08/13/23 10:190.13
Benzo(k)fluoranthene mg/kg ND 0.33 08/13/23 10:190.11
Benzoic Acid mg/kg ND 1.6 08/13/23 10:190.70
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4109953
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009
Matrix:Solid
AnalyzedMDL
Benzyl alcohol mg/kg ND 0.65 08/13/23 10:190.25
bis(2-Chloroethoxy)methane mg/kg ND 0.33 08/13/23 10:190.14
bis(2-Chloroethyl) ether mg/kg ND 0.33 08/13/23 10:190.12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 08/13/23 10:190.13
Butylbenzylphthalate mg/kg ND 0.33 08/13/23 10:190.14
Chrysene mg/kg ND 0.33 08/13/23 10:190.12
Di-n-butylphthalate mg/kg ND 0.33 08/13/23 10:190.11
Di-n-octylphthalate mg/kg ND 0.33 08/13/23 10:190.13
Dibenz(a,h)anthracene mg/kg ND 0.33 08/13/23 10:190.13
Dibenzofuran mg/kg ND 0.33 08/13/23 10:190.12
Diethylphthalate mg/kg ND 0.33 08/13/23 10:190.12
Dimethylphthalate mg/kg ND 0.33 08/13/23 10:190.12
Fluoranthene mg/kg ND 0.33 08/13/23 10:190.11
Fluorene mg/kg ND 0.33 08/13/23 10:190.11
Hexachloro-1,3-butadiene mg/kg ND 0.33 08/13/23 10:190.14
Hexachlorobenzene mg/kg ND 0.33 08/13/23 10:190.13
Hexachlorocyclopentadiene mg/kg ND 0.33 v208/13/23 10:190.19
Hexachloroethane mg/kg ND 0.33 08/13/23 10:190.12
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 08/13/23 10:190.13
Isophorone mg/kg ND 0.33 08/13/23 10:190.15
N-Nitroso-di-n-propylamine mg/kg ND 0.33 08/13/23 10:190.12
N-Nitrosodimethylamine mg/kg ND 0.33 08/13/23 10:190.11
N-Nitrosodiphenylamine mg/kg ND 0.33 08/13/23 10:190.12
Naphthalene mg/kg ND 0.33 08/13/23 10:190.11
Nitrobenzene mg/kg ND 0.33 08/13/23 10:190.15
Pentachlorophenol mg/kg ND 0.65 08/13/23 10:190.32
Phenanthrene mg/kg ND 0.33 08/13/23 10:190.11
Phenol mg/kg ND 0.33 08/13/23 10:190.15
Pyrene mg/kg ND 0.33 08/13/23 10:190.13
Pyridine mg/kg ND 0.33 08/13/23 10:190.10
2,4,6-Tribromophenol (S)%81 10-131 08/13/23 10:19
2-Fluorobiphenyl (S)%69 10-130 08/13/23 10:19
2-Fluorophenol (S)%67 10-130 08/13/23 10:19
Nitrobenzene-d5 (S)%71 10-130 08/13/23 10:19
Phenol-d6 (S)%64 10-130 08/13/23 10:19
Terphenyl-d14 (S)%87 10-130 08/13/23 10:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4109954LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 72 43-130
1,2-Dichlorobenzene mg/kg 1.21.7 68 43-130
1,3-Dichlorobenzene mg/kg 1.21.7 68 43-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4109954LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene mg/kg 1.21.7 69 44-130
1-Methylnaphthalene mg/kg 1.21.7 73 47-130
2,2'-Oxybis(1-chloropropane)mg/kg 1.11.7 67 29-130
2,4,5-Trichlorophenol mg/kg 1.31.7 74 47-130
2,4,6-Trichlorophenol mg/kg 1.31.7 77 47-130
2,4-Dichlorophenol mg/kg 1.21.7 71 45-130
2,4-Dimethylphenol mg/kg 1.21.7 73 45-130
2,4-Dinitrophenol mg/kg 4.08.5 47 27-140
2,4-Dinitrotoluene mg/kg 1.21.7 70 46-130
2,6-Dinitrotoluene mg/kg 1.21.7 73 48-130
2-Chloronaphthalene mg/kg 1.21.7 72 46-130
2-Chlorophenol mg/kg 1.31.7 74 43-130
2-Methylnaphthalene mg/kg 1.21.7 74 47-130
2-Methylphenol(o-Cresol)mg/kg 1.21.7 71 42-130
2-Nitroaniline mg/kg 2.53.4 74 41-130
2-Nitrophenol mg/kg 1.31.7 76 48-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.21.7 73 39-130
3,3'-Dichlorobenzidine mg/kg 2.53.4 73 41-130
3-Nitroaniline mg/kg 2.53.4 73 37-130
4,6-Dinitro-2-methylphenol mg/kg 2.13.4 61 38-141
4-Bromophenylphenyl ether mg/kg 1.41.7 80 47-130
4-Chloro-3-methylphenol mg/kg 2.43.4 72 44-130
4-Chloroaniline mg/kg 2.53.4 75 41-130
4-Chlorophenylphenyl ether mg/kg 1.31.7 77 45-130
4-Nitroaniline mg/kg 2.43.4 69 42-130
4-Nitrophenol mg/kg 6.38.5 74 39-131
Acenaphthene mg/kg 1.31.7 75 49-130
Acenaphthylene mg/kg 1.31.7 74 50-130
Aniline mg/kg 1.11.7 65 38-130
Anthracene mg/kg 1.31.7 76 49-130
Benzo(a)anthracene mg/kg 1.31.7 79 51-130
Benzo(a)pyrene mg/kg 1.41.7 83 51-130
Benzo(b)fluoranthene mg/kg 1.41.7 84 49-130
Benzo(g,h,i)perylene mg/kg 1.31.7 79 48-140
Benzo(k)fluoranthene mg/kg 1.41.7 84 51-130
Benzoic Acid mg/kg 2.08.5 23 22-130
Benzyl alcohol mg/kg 2.53.4 73 43-130
bis(2-Chloroethoxy)methane mg/kg 1.31.7 75 43-130
bis(2-Chloroethyl) ether mg/kg 1.21.7 72 42-130
bis(2-Ethylhexyl)phthalate mg/kg 1.31.7 74 43-130
Butylbenzylphthalate mg/kg 1.21.7 73 44-131
Chrysene mg/kg 1.31.7 79 51-130
Di-n-butylphthalate mg/kg 1.31.7 76 46-130
Di-n-octylphthalate mg/kg 1.31.7 76 45-130
Dibenz(a,h)anthracene mg/kg 1.31.7 79 48-130
Dibenzofuran mg/kg 1.21.7 72 10-130
Diethylphthalate mg/kg 1.31.7 75 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4109954LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethylphthalate mg/kg 1.31.7 75 48-130
Fluoranthene mg/kg 1.31.7 79 48-130
Fluorene mg/kg 1.31.7 75 48-130
Hexachloro-1,3-butadiene mg/kg 1.21.7 71 39-130
Hexachlorobenzene mg/kg 1.41.7 82 47-130
Hexachlorocyclopentadiene mg/kg 0.83 v31.7 49 17-130
Hexachloroethane mg/kg 1.21.7 70 40-130
Indeno(1,2,3-cd)pyrene mg/kg 1.31.7 77 50-130
Isophorone mg/kg 1.21.7 73 41-130
N-Nitroso-di-n-propylamine mg/kg 1.21.7 73 36-130
N-Nitrosodimethylamine mg/kg 1.21.7 69 34-130
N-Nitrosodiphenylamine mg/kg 1.31.7 77 48-130
Naphthalene mg/kg 1.21.7 74 46-130
Nitrobenzene mg/kg 1.21.7 69 39-130
Pentachlorophenol mg/kg 2.73.4 80 42-130
Phenanthrene mg/kg 1.31.7 78 50-130
Phenol mg/kg 1.21.7 72 42-130
Pyrene mg/kg 1.31.7 77 50-130
Pyridine mg/kg 0.691.7 41 26-130
2,4,6-Tribromophenol (S)%97 10-131
2-Fluorobiphenyl (S)%76 10-130
2-Fluorophenol (S)%76 10-130
Nitrobenzene-d5 (S)%73 10-130
Phenol-d6 (S)%75 10-130
Terphenyl-d14 (S)%76 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4109955MATRIX SPIKE SAMPLE:
MSSpike
Result
92681194010
1,2,4-Trichlorobenzene mg/kg 1.11.8 60 16-130ND
1,2-Dichlorobenzene mg/kg 0.961.8 52 19-130ND
1,3-Dichlorobenzene mg/kg 0.951.8 52 19-130ND
1,4-Dichlorobenzene mg/kg 0.961.8 52 20-130ND
1-Methylnaphthalene mg/kg 1.31.8 70 19-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 0.951.8 52 10-130ND
2,4,5-Trichlorophenol mg/kg 1.21.8 66 19-130ND
2,4,6-Trichlorophenol mg/kg 1.21.8 66 18-130ND
2,4-Dichlorophenol mg/kg 1.21.8 68 16-130ND
2,4-Dimethylphenol mg/kg 0.931.8 48 10-130ND
2,4-Dinitrophenol mg/kg 4.49.1 48 10-143ND
2,4-Dinitrotoluene mg/kg 1.21.8 65 19-130ND
2,6-Dinitrotoluene mg/kg 1.31.8 69 22-130ND
2-Chloronaphthalene mg/kg 1.01.8 57 18-130ND
2-Chlorophenol mg/kg 1.11.8 59 20-130ND
2-Methylnaphthalene mg/kg 1.21.8 68 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4109955MATRIX SPIKE SAMPLE:
MSSpike
Result
92681194010
2-Methylphenol(o-Cresol)mg/kg 0.991.8 55 13-130ND
2-Nitroaniline mg/kg 2.03.7 55 18-130ND
2-Nitrophenol mg/kg 1.21.8 66 19-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.8 61 13-130ND
3,3'-Dichlorobenzidine mg/kg ND M13.7 0 10-130ND
3-Nitroaniline mg/kg 1.2J3.7 33 22-130ND
4,6-Dinitro-2-methylphenol mg/kg 1.83.7 49 10-144ND
4-Bromophenylphenyl ether mg/kg 1.51.8 81 18-130ND
4-Chloro-3-methylphenol mg/kg 2.43.7 66 16-130ND
4-Chloroaniline mg/kg 0.943.7 26 17-130ND
4-Chlorophenylphenyl ether mg/kg 1.41.8 74 17-130ND
4-Nitroaniline mg/kg 0.923.7 25 21-130ND
4-Nitrophenol mg/kg 5.59.1 60 13-131ND
Acenaphthene mg/kg 1.11.8 62 20-130ND
Acenaphthylene mg/kg 1.11.8 61 21-130ND
Aniline mg/kg 0.16J M11.8 9 10-130ND
Anthracene mg/kg 1.21.8 66 19-130ND
Benzo(a)anthracene mg/kg 1.21.8 68 17-130ND
Benzo(a)pyrene mg/kg 1.21.8 65 14-130ND
Benzo(b)fluoranthene mg/kg 1.41.8 71 11-134ND
Benzo(g,h,i)perylene mg/kg 1.21.8 67 12-130ND
Benzo(k)fluoranthene mg/kg 1.31.8 69 15-130ND
Benzoic Acid mg/kg 5.69.1 61 10-130ND
Benzyl alcohol mg/kg 2.23.7 59 20-130ND
bis(2-Chloroethoxy)methane mg/kg 1.11.8 62 16-130ND
bis(2-Chloroethyl) ether mg/kg 1.11.8 61 18-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.31.8 66 11-130ND
Butylbenzylphthalate mg/kg 1.21.8 68 10-130ND
Chrysene mg/kg 1.31.8 70 17-130ND
Di-n-butylphthalate mg/kg 1.11.8 60 16-130ND
Di-n-octylphthalate mg/kg 1.31.8 64 16-130165J ug/kg
Dibenz(a,h)anthracene mg/kg 1.21.8 65 13-130ND
Dibenzofuran mg/kg 1.21.8 65 19-130ND
Diethylphthalate mg/kg 1.21.8 67 22-130ND
Dimethylphthalate mg/kg 1.21.8 63 23-130ND
Fluoranthene mg/kg 1.21.8 64 14-130ND
Fluorene mg/kg 1.21.8 66 19-130ND
Hexachloro-1,3-butadiene mg/kg 1.21.8 65 12-130ND
Hexachlorobenzene mg/kg 1.41.8 78 17-130ND
Hexachlorocyclopentadiene mg/kg 0.63 v31.8 34 10-130ND
Hexachloroethane mg/kg 0.941.8 52 14-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.21.8 65 13-130ND
Isophorone mg/kg 1.11.8 62 17-130ND
N-Nitroso-di-n-propylamine mg/kg 1.11.8 59 10-130ND
N-Nitrosodimethylamine mg/kg 0.961.8 53 16-130ND
N-Nitrosodiphenylamine mg/kg 1.11.8 54 19-130ND
Naphthalene mg/kg 1.11.8 61 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4109955MATRIX SPIKE SAMPLE:
MSSpike
Result
92681194010
Nitrobenzene mg/kg 1.01.8 55 15-130ND
Pentachlorophenol mg/kg 66.2 M13.7 -1390 10-130117000 ug/kg
Phenanthrene mg/kg 1.21.8 67 17-130ND
Phenol mg/kg 1.11.8 58 15-130ND
Pyrene mg/kg 1.61.8 75 31-130207J ug/kg
Pyridine mg/kg 0.481.8 27 10-130ND
2,4,6-Tribromophenol (S)%92 10-131
2-Fluorobiphenyl (S)%56 10-130
2-Fluorophenol (S)%55 10-130
Nitrobenzene-d5 (S)%58 10-130
Phenol-d6 (S)%56 10-130
Terphenyl-d14 (S)%74 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681194011
4109956SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681194011
4109956SAMPLE DUPLICATE:
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg 3.8 303470J ug/kg
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND v230ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg 1090 3 301060000
ug/kg
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%0 S40
2-Fluorobiphenyl (S)%0 S4
2-Fluorophenol (S)%0 S40
Nitrobenzene-d5 (S)%0 D3,S4
Phenol-d6 (S)%0 S40
Terphenyl-d14 (S)%0 S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
793448
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077010, 92681077011, 92681077012, 92681077013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4111544
Associated Lab Samples:92681077010, 92681077011, 92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 08/15/23 15:000.13
1,2-Dichlorobenzene mg/kg ND 0.33 08/15/23 15:000.12
1,3-Dichlorobenzene mg/kg ND 0.33 08/15/23 15:000.12
1,4-Dichlorobenzene mg/kg ND 0.33 08/15/23 15:000.12
1-Methylnaphthalene mg/kg ND 0.33 08/15/23 15:000.11
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 08/15/23 15:000.16
2,4,5-Trichlorophenol mg/kg ND 0.33 08/15/23 15:000.15
2,4,6-Trichlorophenol mg/kg ND 0.33 08/15/23 15:000.13
2,4-Dichlorophenol mg/kg ND 0.33 08/15/23 15:000.13
2,4-Dimethylphenol mg/kg ND 0.33 v108/15/23 15:000.14
2,4-Dinitrophenol mg/kg ND 1.6 v108/15/23 15:001.0
2,4-Dinitrotoluene mg/kg ND 0.33 08/15/23 15:000.13
2,6-Dinitrotoluene mg/kg ND 0.33 08/15/23 15:000.12
2-Chloronaphthalene mg/kg ND 0.33 08/15/23 15:000.13
2-Chlorophenol mg/kg ND 0.33 08/15/23 15:000.12
2-Methylnaphthalene mg/kg ND 0.33 08/15/23 15:000.13
2-Methylphenol(o-Cresol)mg/kg ND 0.33 08/15/23 15:000.13
2-Nitroaniline mg/kg ND 1.6 08/15/23 15:000.27
2-Nitrophenol mg/kg ND 0.33 08/15/23 15:000.14
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 08/15/23 15:000.13
3,3'-Dichlorobenzidine mg/kg ND 0.65 08/15/23 15:000.22
3-Nitroaniline mg/kg ND 1.6 08/15/23 15:000.26
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 08/15/23 15:000.30
4-Bromophenylphenyl ether mg/kg ND 0.33 08/15/23 15:000.13
4-Chloro-3-methylphenol mg/kg ND 0.65 08/15/23 15:000.23
4-Chloroaniline mg/kg ND 0.65 08/15/23 15:000.26
4-Chlorophenylphenyl ether mg/kg ND 0.33 08/15/23 15:000.12
4-Nitroaniline mg/kg ND 0.65 08/15/23 15:000.25
4-Nitrophenol mg/kg ND 1.6 08/15/23 15:000.63
Acenaphthene mg/kg ND 0.33 08/15/23 15:000.11
Acenaphthylene mg/kg ND 0.33 08/15/23 15:000.11
Aniline mg/kg ND 0.33 08/15/23 15:000.13
Anthracene mg/kg ND 0.33 08/15/23 15:000.11
Benzo(a)anthracene mg/kg ND 0.33 08/15/23 15:000.11
Benzo(a)pyrene mg/kg ND 0.33 08/15/23 15:000.11
Benzo(b)fluoranthene mg/kg ND 0.33 08/15/23 15:000.11
Benzo(g,h,i)perylene mg/kg ND 0.33 08/15/23 15:000.13
Benzo(k)fluoranthene mg/kg ND 0.33 08/15/23 15:000.11
Benzoic Acid mg/kg ND 1.6 08/15/23 15:000.70
Benzyl alcohol mg/kg ND 0.65 08/15/23 15:000.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4111544
Associated Lab Samples:92681077010, 92681077011, 92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.33 08/15/23 15:000.14
bis(2-Chloroethyl) ether mg/kg ND 0.33 08/15/23 15:000.12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 08/15/23 15:000.13
Butylbenzylphthalate mg/kg ND 0.33 08/15/23 15:000.14
Chrysene mg/kg ND 0.33 08/15/23 15:000.12
Di-n-butylphthalate mg/kg ND 0.33 08/15/23 15:000.11
Di-n-octylphthalate mg/kg ND 0.33 08/15/23 15:000.13
Dibenz(a,h)anthracene mg/kg ND 0.33 08/15/23 15:000.13
Dibenzofuran mg/kg ND 0.33 08/15/23 15:000.12
Diethylphthalate mg/kg ND 0.33 08/15/23 15:000.12
Dimethylphthalate mg/kg ND 0.33 08/15/23 15:000.12
Fluoranthene mg/kg ND 0.33 08/15/23 15:000.11
Fluorene mg/kg ND 0.33 08/15/23 15:000.11
Hexachloro-1,3-butadiene mg/kg ND 0.33 08/15/23 15:000.14
Hexachlorobenzene mg/kg ND 0.33 08/15/23 15:000.13
Hexachlorocyclopentadiene mg/kg ND 0.33 v208/15/23 15:000.19
Hexachloroethane mg/kg ND 0.33 08/15/23 15:000.12
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 08/15/23 15:000.13
Isophorone mg/kg ND 0.33 08/15/23 15:000.15
N-Nitroso-di-n-propylamine mg/kg ND 0.33 08/15/23 15:000.12
N-Nitrosodimethylamine mg/kg ND 0.33 08/15/23 15:000.11
N-Nitrosodiphenylamine mg/kg ND 0.33 08/15/23 15:000.12
Naphthalene mg/kg ND 0.33 08/15/23 15:000.11
Nitrobenzene mg/kg ND 0.33 08/15/23 15:000.15
Pentachlorophenol mg/kg ND 0.65 08/15/23 15:000.32
Phenanthrene mg/kg ND 0.33 08/15/23 15:000.11
Phenol mg/kg ND 0.33 08/15/23 15:000.15
Pyrene mg/kg ND 0.33 08/15/23 15:000.13
Pyridine mg/kg ND 0.33 08/15/23 15:000.10
2,4,6-Tribromophenol (S)%64 10-131 08/15/23 15:00
2-Fluorobiphenyl (S)%56 10-130 08/15/23 15:00
2-Fluorophenol (S)%54 10-130 08/15/23 15:00
Nitrobenzene-d5 (S)%67 10-130 08/15/23 15:00
Phenol-d6 (S)%58 10-130 08/15/23 15:00
Terphenyl-d14 (S)%65 10-130 08/15/23 15:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4111545LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.01.6 63 43-130
1,2-Dichlorobenzene mg/kg 0.991.6 60 43-130
1,3-Dichlorobenzene mg/kg 0.961.6 59 43-130
1,4-Dichlorobenzene mg/kg 0.991.6 60 44-130
1-Methylnaphthalene mg/kg 1.21.6 71 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4111545LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 0.941.6 57 29-130
2,4,5-Trichlorophenol mg/kg 1.11.6 67 47-130
2,4,6-Trichlorophenol mg/kg 1.11.6 68 47-130
2,4-Dichlorophenol mg/kg 1.11.6 69 45-130
2,4-Dimethylphenol mg/kg 1.7 v11.6 101 45-130
2,4-Dinitrophenol mg/kg 6.2 v18.2 76 27-140
2,4-Dinitrotoluene mg/kg 1.41.6 85 46-130
2,6-Dinitrotoluene mg/kg 1.31.6 81 48-130
2-Chloronaphthalene mg/kg 0.981.6 60 46-130
2-Chlorophenol mg/kg 1.01.6 63 43-130
2-Methylnaphthalene mg/kg 1.11.6 68 47-130
2-Methylphenol(o-Cresol)mg/kg 1.11.6 67 42-130
2-Nitroaniline mg/kg 2.23.3 68 41-130
2-Nitrophenol mg/kg 1.21.6 71 48-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.6 70 39-130
3,3'-Dichlorobenzidine mg/kg 2.43.3 72 41-130
3-Nitroaniline mg/kg 2.33.3 71 37-130
4,6-Dinitro-2-methylphenol mg/kg 2.63.3 79 38-141
4-Bromophenylphenyl ether mg/kg 1.11.6 68 47-130
4-Chloro-3-methylphenol mg/kg 2.53.3 77 44-130
4-Chloroaniline mg/kg 1.93.3 57 41-130
4-Chlorophenylphenyl ether mg/kg 1.21.6 72 45-130
4-Nitroaniline mg/kg 2.43.3 75 42-130
4-Nitrophenol mg/kg 7.48.2 90 39-131
Acenaphthene mg/kg 1.11.6 69 49-130
Acenaphthylene mg/kg 1.11.6 68 50-130
Aniline mg/kg 0.751.6 46 38-130
Anthracene mg/kg 1.11.6 66 49-130
Benzo(a)anthracene mg/kg 1.21.6 75 51-130
Benzo(a)pyrene mg/kg 1.61.6 98 51-130
Benzo(b)fluoranthene mg/kg 1.61.6 96 49-130
Benzo(g,h,i)perylene mg/kg 1.41.6 84 48-140
Benzo(k)fluoranthene mg/kg 1.71.6 102 51-130
Benzoic Acid mg/kg 3.18.2 38 22-130
Benzyl alcohol mg/kg 2.13.3 63 43-130
bis(2-Chloroethoxy)methane mg/kg 1.01.6 62 43-130
bis(2-Chloroethyl) ether mg/kg 0.951.6 58 42-130
bis(2-Ethylhexyl)phthalate mg/kg 1.31.6 78 43-130
Butylbenzylphthalate mg/kg 1.31.6 77 44-131
Chrysene mg/kg 1.31.6 80 51-130
Di-n-butylphthalate mg/kg 1.21.6 75 46-130
Di-n-octylphthalate mg/kg 1.31.6 80 45-130
Dibenz(a,h)anthracene mg/kg 1.51.6 91 48-130
Dibenzofuran mg/kg 1.11.6 70 10-130
Diethylphthalate mg/kg 1.41.6 83 48-130
Dimethylphthalate mg/kg 1.31.6 80 48-130
Fluoranthene mg/kg 1.31.6 82 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4111545LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.21.6 75 48-130
Hexachloro-1,3-butadiene mg/kg 1.11.6 70 39-130
Hexachlorobenzene mg/kg 1.11.6 67 47-130
Hexachlorocyclopentadiene mg/kg 0.58 v31.6 35 17-130
Hexachloroethane mg/kg 0.991.6 61 40-130
Indeno(1,2,3-cd)pyrene mg/kg 1.51.6 89 50-130
Isophorone mg/kg 1.21.6 71 41-130
N-Nitroso-di-n-propylamine mg/kg 1.11.6 68 36-130
N-Nitrosodimethylamine mg/kg 0.881.6 53 34-130
N-Nitrosodiphenylamine mg/kg 1.11.6 64 48-130
Naphthalene mg/kg 1.11.6 65 46-130
Nitrobenzene mg/kg 1.11.6 65 39-130
Pentachlorophenol mg/kg 2.13.3 63 42-130
Phenanthrene mg/kg 1.21.6 72 50-130
Phenol mg/kg 1.11.6 67 42-130
Pyrene mg/kg 1.21.6 73 50-130
Pyridine mg/kg 0.731.6 45 26-130
2,4,6-Tribromophenol (S)%78 10-131
2-Fluorobiphenyl (S)%62 10-130
2-Fluorophenol (S)%59 10-130
Nitrobenzene-d5 (S)%68 10-130
Phenol-d6 (S)%63 10-130
Terphenyl-d14 (S)%70 10-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4111546MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681207001
4111547
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene mg/kg 1.8 60 16-13059 1 301.8ND 1.1 1.1
1,2-Dichlorobenzene mg/kg 1.8 57 19-13055 3 301.8ND 1.0 0.99
1,3-Dichlorobenzene mg/kg 1.8 55 19-13053 5 301.8ND 0.98 0.94
1,4-Dichlorobenzene mg/kg 1.8 55 20-13054 3 301.8ND 0.99 0.95
1-Methylnaphthalene mg/kg 1.8 66 19-13066 1 301.8ND 1.2 1.2
2,2'-Oxybis(1-
chloropropane)mg/kg 1.8 55 10-13053 4 301.8ND 0.98 0.94
2,4,5-Trichlorophenol mg/kg 1.8 60 19-13058 3 301.8ND 1.1 1.0
2,4,6-Trichlorophenol mg/kg 1.8 58 18-13056 4 301.8ND 1.0 1.0
2,4-Dichlorophenol mg/kg 1.8 65 16-13065 0 301.8ND 1.2 1.2
2,4-Dimethylphenol mg/kg v11.8 97 10-13096 0 301.8ND 1.7 1.7
2,4-Dinitrophenol mg/kg v18.8 79 10-14377 3 308.9ND 7.0 6.8
2,4-Dinitrotoluene mg/kg 1.8 74 19-13074 0 301.8ND 1.3 1.3
2,6-Dinitrotoluene mg/kg 1.8 71 22-13071 1 301.8ND 1.3 1.3
2-Chloronaphthalene mg/kg 1.8 53 18-13050 5 301.8ND 0.94 0.90
2-Chlorophenol mg/kg 1.8 62 20-13058 5 301.8ND 1.1 1.0
2-Methylnaphthalene mg/kg 1.8 62 18-13063 1 301.8ND 1.1 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4111546MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681207001
4111547
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)mg/kg 1.8 68 13-13070 3 301.8ND 1.2 1.2
2-Nitroaniline mg/kg 3.6 59 18-13058 2 303.6ND 2.1 2.1
2-Nitrophenol mg/kg 1.8 71 19-13070 0 301.8ND 1.3 1.3
3&4-Methylphenol(m&p
Cresol)mg/kg 1.8 68 13-13070 3 301.8ND 1.2 1.2
3,3'-Dichlorobenzidine mg/kg 3.6 55 10-13055 1 303.6ND 2.0 1.9
3-Nitroaniline mg/kg 3.6 58 22-13058 1 303.6ND 2.1 2.1
4,6-Dinitro-2-methylphenol mg/kg 3.6 73 10-14471 2 303.6ND 2.6 2.5
4-Bromophenylphenyl ether mg/kg 1.8 64 18-13063 2 301.8ND 1.1 1.1
4-Chloro-3-methylphenol mg/kg 3.6 72 16-13075 4 303.6ND 2.6 2.7
4-Chloroaniline mg/kg 3.6 54 17-13054 0 303.6ND 1.9 1.9
4-Chlorophenylphenyl ether mg/kg 1.8 66 17-13064 3 301.8ND 1.2 1.1
4-Nitroaniline mg/kg 3.6 62 21-13063 1 303.6ND 2.2 2.2
4-Nitrophenol mg/kg 8.8 77 13-13177 1 308.9ND 6.8 6.9
Acenaphthene mg/kg 1.8 62 20-13060 3 301.8ND 1.1 1.1
Acenaphthylene mg/kg 1.8 59 21-13058 3 301.8ND 1.1 1.0
Aniline mg/kg 1.8 41 10-13038 6 301.8ND 0.72 0.68
Anthracene mg/kg 1.8 58 19-13058 0 301.8ND 1.0 1.0
Benzo(a)anthracene mg/kg 1.8 64 17-13063 1 301.8ND 1.1 1.1
Benzo(a)pyrene mg/kg 1.8 76 14-13076 0 301.8ND 1.4 1.4
Benzo(b)fluoranthene mg/kg 1.8 75 11-13475 1 301.8ND 1.3 1.3
Benzo(g,h,i)perylene mg/kg 1.8 64 12-13068 6 301.8ND 1.1 1.2
Benzo(k)fluoranthene mg/kg 1.8 79 15-13078 1 301.8ND 1.4 1.4
Benzoic Acid mg/kg 8.8 55 10-13056 1 308.9ND 4.9 5.0
Benzyl alcohol mg/kg 3.6 57 20-13055 2 303.6ND 2.0 2.0
bis(2-
Chloroethoxy)methane mg/kg 1.8 58 16-13055 4 301.8ND 1.0 0.99
bis(2-Chloroethyl) ether mg/kg 1.8 55 18-13052 4 301.8ND 0.97 0.93
bis(2-Ethylhexyl)phthalate mg/kg 1.8 64 11-13063 2 301.8ND 1.1 1.1
Butylbenzylphthalate mg/kg 1.8 65 10-13062 4 301.8ND 1.2 1.1
Chrysene mg/kg 1.8 68 17-13068 0 301.8ND 1.2 1.2
Di-n-butylphthalate mg/kg 1.8 65 16-13065 1 301.8ND 1.1 1.2
Di-n-octylphthalate mg/kg 1.8 66 16-13067 2 301.8ND 1.2 1.2
Dibenz(a,h)anthracene mg/kg 1.8 72 13-13077 6 301.8ND 1.3 1.4
Dibenzofuran mg/kg 1.8 61 19-13060 2 301.8ND 1.1 1.1
Diethylphthalate mg/kg 1.8 72 22-13070 2 301.8ND 1.3 1.3
Dimethylphthalate mg/kg 1.8 68 23-13066 3 301.8ND 1.2 1.2
Fluoranthene mg/kg 1.8 67 14-13070 4 301.8ND 1.2 1.2
Fluorene mg/kg 1.8 64 19-13062 2 301.8ND 1.1 1.1
Hexachloro-1,3-butadiene mg/kg 1.8 65 12-13062 5 301.8ND 1.2 1.1
Hexachlorobenzene mg/kg 1.8 62 17-13061 2 301.8ND 1.1 1.1
Hexachlorocyclopentadiene mg/kg v31.8 29 10-13027 6 301.8ND 0.52 0.49
Hexachloroethane mg/kg 1.8 57 14-13055 3 301.8ND 1.0 0.97
Indeno(1,2,3-cd)pyrene mg/kg 1.8 68 13-13072 7 301.8ND 1.2 1.3
Isophorone mg/kg 1.8 68 17-13067 1 301.8ND 1.2 1.2
N-Nitroso-di-n-propylamine mg/kg 1.8 66 10-13066 0 301.8ND 1.2 1.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4111546MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681207001
4111547
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine mg/kg 1.8 53 16-13047 11 301.8ND 0.94 0.85
N-Nitrosodiphenylamine mg/kg 1.8 59 19-13058 2 301.8ND 1.0 1.0
Naphthalene mg/kg 1.8 62 18-13061 2 301.8ND 1.1 1.1
Nitrobenzene mg/kg 1.8 61 15-13060 1 301.8ND 1.1 1.1
Pentachlorophenol mg/kg 3.6 50 10-13051 2 303.6ND 1.8 1.8
Phenanthrene mg/kg 1.8 63 17-13064 1 301.8ND 1.1 1.1
Phenol mg/kg 1.8 62 15-13066 7 301.8ND 1.1 1.2
Pyrene mg/kg 1.8 61 31-13058 4 301.8ND 1.1 1.0
Pyridine mg/kg 1.8 19 10-13019 301.8ND 0.34J 0.34J
2,4,6-Tribromophenol (S)%61 10-13157
2-Fluorobiphenyl (S)%52 10-13047
2-Fluorophenol (S)%53 10-13049
Nitrobenzene-d5 (S)%61 10-13056
Phenol-d6 (S)%58 10-13053
Terphenyl-d14 (S)%61 10-13055
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
792169
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681037021
4104766SAMPLE DUPLICATE:
Percent Moisture %26.9 N2162522.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92680964006
4104767SAMPLE DUPLICATE:
Percent Moisture %55.7 N252553.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 136
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2111245
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92681077001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3959152-1
Associated Lab Samples:92681077001
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 08/10/23 06:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3959152-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1643999-08
R3959152-3SAMPLE DUPLICATE:
Total Solids %81.8 0.247 1081.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2111246
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007, 92681077008,
92681077009, 92681077010, 92681077011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3959154-1
Associated Lab Samples:92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007, 92681077008,
92681077009, 92681077010, 92681077011
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/10/23 07:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3959154-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681077002
R3959154-3SAMPLE DUPLICATE:
Total Solids %58.9 0.372 1059.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2111517
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92681077012, 92681077013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3959290-1
Associated Lab Samples:92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/10/23 12:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3959290-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681077012
R3959290-3SAMPLE DUPLICATE:
Total Solids %68.2 1.45 1069.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2111181
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3960578-1
Associated Lab Samples:92681077001, 92681077002, 92681077003, 92681077004, 92681077005, 92681077006, 92681077007,
92681077008, 92681077009, 92681077010, 92681077011, 92681077012, 92681077013
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/14/23 18:040.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3960578-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.710.0 107 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3960578-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92681077001
R3960578-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 33.7 105 75.0-125106 1.29 2033.70.690 35.9 36.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3960578-5MATRIX SPIKE SAMPLE:
MSSpike
Result
92681077001
Chromium, Hexavalent mg/kg 1450 MH108013475.0-1250.690
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681077003
R3960578-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92681077010
R3960578-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Result may be biased high due to carryover from previously analyzed sample.C8
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.PH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 136
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
ANALYTE QUALIFIERS
RPD value was outside control limits.R1
The RPD value in one of the constituent analytes was outside the control limits.RS
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 136
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92681077001 2111353 2111353P2-5 3051 EPA 6020B
92681077002 2111353 2111353P2-10 3051 EPA 6020B
92681077003 2111353 2111353E2-5 3051 EPA 6020B
92681077004 2111353 2111353E2-10 3051 EPA 6020B
92681077005 2111353 2111353E1-5 3051 EPA 6020B
92681077006 2111353 2111353E1-10 3051 EPA 6020B
92681077007 2111353 2111353P3-5 3051 EPA 6020B
92681077008 2111353 2111353P3-10 3051 EPA 6020B
92681077009 2111353 2111353P1-5 3051 EPA 6020B
92681077010 2111353 2111353P1-10 3051 EPA 6020B
92681077011 2111353 2111353DP-1 3051 EPA 6020B
92681077012 2111353 2111353DP-2 3051 EPA 6020B
92681077013 2111353 2111353DUP-1 3051 EPA 6020B
92681077001 2111648 2111648P2-5 7471A EPA 7471B
92681077002 2111648 2111648P2-10 7471A EPA 7471B
92681077003 2111648 2111648E2-5 7471A EPA 7471B
92681077004 2111648 2111648E2-10 7471A EPA 7471B
92681077005 2111648 2111648E1-5 7471A EPA 7471B
92681077006 2111648 2111648E1-10 7471A EPA 7471B
92681077007 2111648 2111648P3-5 7471A EPA 7471B
92681077008 2111648 2111648P3-10 7471A EPA 7471B
92681077009 2111648 2111648P1-5 7471A EPA 7471B
92681077010 2111648 2111648P1-10 7471A EPA 7471B
92681077011 2111648 2111648DP-1 7471A EPA 7471B
92681077012 2111648 2111648DP-2 7471A EPA 7471B
92681077013 2111648 2111648DUP-1 7471A EPA 7471B
92681077001 793123 793297P2-5 EPA 3546 EPA 8270E
92681077002 793123 793297P2-10 EPA 3546 EPA 8270E
92681077003 793123 793297E2-5 EPA 3546 EPA 8270E
92681077004 793123 793297E2-10 EPA 3546 EPA 8270E
92681077005 793123 793297E1-5 EPA 3546 EPA 8270E
92681077006 793123 793297E1-10 EPA 3546 EPA 8270E
92681077007 793123 793297P3-5 EPA 3546 EPA 8270E
92681077008 793123 793297P3-10 EPA 3546 EPA 8270E
92681077009 793123 793297P1-5 EPA 3546 EPA 8270E
92681077010 793448 793823P1-10 EPA 3546 EPA 8270E
92681077011 793448 793823DP-1 EPA 3546 EPA 8270E
92681077012 793448 793823DP-2 EPA 3546 EPA 8270E
92681077013 793448 793823DUP-1 EPA 3546 EPA 8270E
92681077001 792275 792361P2-5 EPA 5035A/5030B EPA 8260D
92681077002 792275 792361P2-10 EPA 5035A/5030B EPA 8260D
92681077003 792275 792361E2-5 EPA 5035A/5030B EPA 8260D
92681077004 792501 792616E2-10 EPA 5035A/5030B EPA 8260D
92681077005 792275 792361E1-5 EPA 5035A/5030B EPA 8260D
92681077006 792275 792361E1-10 EPA 5035A/5030B EPA 8260D
92681077007 792275 792361P3-5 EPA 5035A/5030B EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 130 of 136
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92681077008 792275 792361P3-10 EPA 5035A/5030B EPA 8260D
92681077009 792275 792361P1-5 EPA 5035A/5030B EPA 8260D
92681077010 792275 792361P1-10 EPA 5035A/5030B EPA 8260D
92681077011 792281 792598DP-1 EPA 5035A/5030B EPA 8260D
92681077012 792570 792597DP-2 EPA 5035A/5030B EPA 8260D
92681077013 792570 792597DUP-1 EPA 5035A/5030B EPA 8260D
92681077014 792401TBEPA 8260D
92681077001 792169P2-5 SW-846
92681077002 792169P2-10 SW-846
92681077003 792169E2-5 SW-846
92681077004 792169E2-10 SW-846
92681077005 792169E1-5 SW-846
92681077006 792169E1-10 SW-846
92681077007 792169P3-5 SW-846
92681077008 792169P3-10 SW-846
92681077009 792169P1-5 SW-846
92681077010 792169P1-10 SW-846
92681077011 792169DP-1 SW-846
92681077012 792169DP-2 SW-846
92681077013 792169DUP-1 SW-846
92681077001 2111245 2111245P2-5 SM 2540 G SM 2540G
92681077002 2111246 2111246P2-10 SM 2540 G SM 2540G
92681077003 2111246 2111246E2-5 SM 2540 G SM 2540G
92681077004 2111246 2111246E2-10 SM 2540 G SM 2540G
92681077005 2111246 2111246E1-5 SM 2540 G SM 2540G
92681077006 2111246 2111246E1-10 SM 2540 G SM 2540G
92681077007 2111246 2111246P3-5 SM 2540 G SM 2540G
92681077008 2111246 2111246P3-10 SM 2540 G SM 2540G
92681077009 2111246 2111246P1-5 SM 2540 G SM 2540G
92681077010 2111246 2111246P1-10 SM 2540 G SM 2540G
92681077011 2111246 2111246DP-1 SM 2540 G SM 2540G
92681077012 2111517 2111517DP-2 SM 2540 G SM 2540G
92681077013 2111517 2111517DUP-1 SM 2540 G SM 2540G
92681077001 2111181 2111181P2-5 3060A EPA 7199
92681077002 2111181 2111181P2-10 3060A EPA 7199
92681077003 2111181 2111181E2-5 3060A EPA 7199
92681077004 2111181 2111181E2-10 3060A EPA 7199
92681077005 2111181 2111181E1-5 3060A EPA 7199
92681077006 2111181 2111181E1-10 3060A EPA 7199
92681077007 2111181 2111181P3-5 3060A EPA 7199
92681077008 2111181 2111181P3-10 3060A EPA 7199
92681077009 2111181 2111181P1-5 3060A EPA 7199
92681077010 2111181 2111181P1-10 3060A EPA 7199
92681077011 2111181 2111181DP-1 3060A EPA 7199
92681077012 2111181 2111181DP-2 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92681077
SOUTH BOULEVARD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92681077013 2111181 2111181DUP-1 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/16/2023 04:20 PM
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Page 132 of 136
Page 133 of 136
Page 134 of 136
Page 135 of 136
Page 136 of 136
ANALYTICAL REPORT
August 25, 2023
Revised Report
ECS Carolinas LLP - Raleigh, NC
Sample Delivery Group:L1642105
Samples Received:08/03/2023
Project Number:49-15946E
Description:South Blvd Site
Site:SOUTH BLVD (1601)
Report To:Mr. Scott Young
5260 Greens Dairy Road
Raleigh, NC 27616
Entire Report Reviewed By:
August 25, 2023
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 1 of 24
August 25, 2023
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 1 of 24
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SS-1 L1642105-01 5
SS-2 L1642105-02 7
SS-3 L1642105-03 9
SS-DUP L1642105-04 11
Qc: Quality Control Summary 13
Volatile Organic Compounds (MS) by Method TO-15 13
Gl: Glossary of Terms 22
Al: Accreditations & Locations 23
Sc: Sample Chain of Custody 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 2 of 24
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SS-1 L1642105-01 Air Randy Cavallier 08/01/23 14:48 08/03/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2107223 1 08/04/23 02:49 08/04/23 02:49 MNP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2107864 10 08/04/23 16:50 08/04/23 16:50 MNP Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-2 L1642105-02 Air Randy Cavallier 08/01/23 14:05 08/03/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2107223 1 08/04/23 03:36 08/04/23 03:36 MNP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2107864 200 08/04/23 17:16 08/04/23 17:16 MNP Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-3 L1642105-03 Air Randy Cavallier 08/01/23 13:30 08/03/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2107223 1 08/04/23 04:22 08/04/23 04:22 MNP Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG2107874 20 08/04/23 14:26 08/04/23 14:26 DAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-DUP L1642105-04 Air Randy Cavallier 08/01/23 00:00 08/03/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG2107874 1 08/04/23 18:59 08/04/23 18:59 DAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 3 of 24
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 3 of 24
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
Report Revision History
Level II Report - Version 1: 08/06/23 21:04
Level II Report - Version 2: 08/11/23 15:32
Level II Report - Version 3: 08/14/23 12:56
Level II Report - Version 4: 08/14/23 13:01
Project Narrative
Revised to update format per client request.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 4 of 24
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ECS Carolinas LLP - Raleigh, NC 49-15946E L1642105 08/25/23 09:15 4 of 24
SAMPLE RESULTS - 01
L1642105
SS-1
Collected date/time: 08/01/23 14:48
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 51.3 1 WG2107223
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2107223
Benzene 71-43-2 78.10 0.228 0.639 0.738 1 WG2107223
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2107223
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2107223
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2107223
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2107223
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2107223
Carbon disulfide 75-15-0 76.10 0.317 0.622 3.67 1 WG2107223
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2107223
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2107223
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2107223
Chloroform 67-66-3 119 0.349 0.973 1.92 1 WG2107223
Chloromethane 74-87-3 50.50 0.213 0.413 1.11 1 WG2107223
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2107223
Cyclohexane 110-82-7 84.20 0.259 0.689 5.75 1 WG2107223
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2107223
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2107223
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2107223
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2107223
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2107223
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2107223
1,1-Dichloroethane 75-34-3 98 0.290 0.802 U 1 WG2107223
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2107223
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2107223
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2107223
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2107223
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2107223
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2107223
1,4-Dioxane 123-91-1 88.10 0.300 0.721 U 1 WG2107223
Ethanol 64-17-5 46.10 0.500 4.71 26.0 1 WG2107223
Ethylbenzene 100-41-4 106 0.362 0.867 0.767 J 1 WG2107223
4-Ethyltoluene 622-96-8 120 0.384 0.982 U 1 WG2107223
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 1.49 1 WG2107223
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 5.64 1 WG2107223
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 0.730 J 1 WG2107223
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2107223
Heptane 142-82-5 100 0.425 0.818 0.622 J 1 WG2107223
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2107223
n-Hexane 110-54-3 86.20 0.726 2.22 1.08 J 1 WG2107223
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2107223
Methylene Chloride 75-09-2 84.90 0.340 0.694 1.29 1 WG2107223
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 2.35 J 1 WG2107223
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 7.22 1 WG2107223
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 1.41 J 1 WG2107223
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2107223
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2107223
Naphthalene 91-20-3 128 1.83 3.30 U 1 WG2107223
2-Propanol 67-63-0 60.10 0.649 3.07 6.93 1 WG2107223
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2107223
Styrene 100-42-5 104 0.335 0.851 1.13 1 WG2107223
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2107223
Tetrachloroethylene 127-18-4 166 5.53 13.6 740 10 WG2107864
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2107223
Toluene 108-88-3 92.10 0.328 1.88 3.19 1 WG2107223
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2107223
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1642105
SS-1
Collected date/time: 08/01/23 14:48
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2107223
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2107223
Trichloroethylene 79-01-6 131 0.364 1.07 1.37 1 WG2107223
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 1.14 1 WG2107223
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 U 1 WG2107223
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 U 1 WG2107223
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2107223
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2107223
Vinyl acetate 108-05-4 86.10 0.408 0.704 U 1 WG2107223
Xylenes, Total 1330-20-7 106.16 0.586 2.61 3.41 1 WG2107223
m&p-Xylene 1330-20-7 106 0.585 1.73 2.16 1 WG2107223
o-Xylene 95-47-6 106 0.359 0.867 1.24 1 WG2107223
(S)
1,4-Bromofluorobenzene 460-00-4 175 98.6 60.0-140 WG2107223
(S)
1,4-Bromofluorobenzene 460-00-4 175 89.6 60.0-140 WG2107864
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1642105
SS-2
Collected date/time: 08/01/23 14:05
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 36.6 1 WG2107223
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2107223
Benzene 71-43-2 78.10 0.228 0.639 4.44 1 WG2107223
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2107223
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2107223
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2107223
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2107223
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2107223
Carbon disulfide 75-15-0 76.10 0.317 0.622 1.23 1 WG2107223
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2107223
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2107223
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2107223
Chloroform 67-66-3 119 0.349 0.973 8.47 1 WG2107223
Chloromethane 74-87-3 50.50 0.213 0.413 0.925 1 WG2107223
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2107223
Cyclohexane 110-82-7 84.20 0.259 0.689 U 1 WG2107223
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2107223
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2107223
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2107223
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2107223
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2107223
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2107223
1,1-Dichloroethane 75-34-3 98 0.290 0.802 U 1 WG2107223
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2107223
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2107223
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2107223
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2107223
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2107223
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2107223
1,4-Dioxane 123-91-1 88.10 0.300 0.721 U 1 WG2107223
Ethanol 64-17-5 46.10 0.500 4.71 27.5 1 WG2107223
Ethylbenzene 100-41-4 106 0.362 0.867 1.67 1 WG2107223
4-Ethyltoluene 622-96-8 120 0.384 0.982 0.425 J 1 WG2107223
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 1.99 1 WG2107223
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 3.96 1 WG2107223
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 1.43 J 1 WG2107223
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2107223
Heptane 142-82-5 100 0.425 0.818 2.28 1 WG2107223
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2107223
n-Hexane 110-54-3 86.20 0.726 2.22 3.60 1 WG2107223
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2107223
Methylene Chloride 75-09-2 84.90 0.340 0.694 U 1 WG2107223
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2107223
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 7.34 1 WG2107223
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 0.807 J 1 WG2107223
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2107223
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2107223
Naphthalene 91-20-3 128 1.83 3.30 U 1 WG2107223
2-Propanol 67-63-0 60.10 0.649 3.07 4.84 1 WG2107223
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2107223
Styrene 100-42-5 104 0.335 0.851 2.04 1 WG2107223
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2107223
Tetrachloroethylene 127-18-4 166 111 272 64100 200 WG2107864
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2107223
Toluene 108-88-3 92.10 0.328 1.88 5.05 1 WG2107223
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2107223
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1642105
SS-2
Collected date/time: 08/01/23 14:05
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 1.16 1 WG2107223
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2107223
Trichloroethylene 79-01-6 131 0.364 1.07 235 1 WG2107223
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 2.29 1 WG2107223
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 0.746 J 1 WG2107223
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 0.710 J 1 WG2107223
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2107223
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2107223
Vinyl acetate 108-05-4 86.10 0.408 0.704 U 1 WG2107223
Xylenes, Total 1330-20-7 106.16 0.586 2.61 5.25 1 WG2107223
m&p-Xylene 1330-20-7 106 0.585 1.73 3.22 1 WG2107223
o-Xylene 95-47-6 106 0.359 0.867 2.03 1 WG2107223
(S)
1,4-Bromofluorobenzene 460-00-4 175 98.4 60.0-140 WG2107223
(S)
1,4-Bromofluorobenzene 460-00-4 175 92.8 60.0-140 WG2107864
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 03
L1642105
SS-3
Collected date/time: 08/01/23 13:30
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 27.8 59.4 2470 20 WG2107874
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2107223
Benzene 71-43-2 78.10 0.228 0.639 5.81 1 WG2107223
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2107223
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2107223
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2107223
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2107223
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2107223
Carbon disulfide 75-15-0 76.10 0.317 0.622 1.20 1 WG2107223
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2107223
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2107223
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2107223
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2107223
Chloromethane 74-87-3 50.50 0.213 0.413 0.636 1 WG2107223
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2107223
Cyclohexane 110-82-7 84.20 0.259 0.689 3.40 1 WG2107223
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2107223
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2107223
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2107223
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2107223
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2107223
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2107223
1,1-Dichloroethane 75-34-3 98 0.290 0.802 U 1 WG2107223
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2107223
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2107223
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2107223
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2107223
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2107223
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2107223
1,4-Dioxane 123-91-1 88.10 0.300 0.721 U 1 WG2107223
Ethanol 64-17-5 46.10 9.99 94.3 402 J3 20 WG2107874
Ethylbenzene 100-41-4 106 0.362 0.867 30.1 1 WG2107223
4-Ethyltoluene 622-96-8 120 0.384 0.982 2.13 1 WG2107223
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 1.85 1 WG2107223
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 1.72 1 WG2107223
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 U 1 WG2107223
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2107223
Heptane 142-82-5 100 0.425 0.818 2.87 1 WG2107223
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2107223
n-Hexane 110-54-3 86.20 0.726 2.22 3.18 1 WG2107223
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2107223
Methylene Chloride 75-09-2 84.90 0.340 0.694 U 1 WG2107223
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 38.5 1 WG2107223
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 175 1 WG2107223
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 29.4 1 WG2107223
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2107223
MTBE 1634-04-4 88.10 0.233 0.721 3.05 1 WG2107223
Naphthalene 91-20-3 128 1.83 3.30 U 1 WG2107223
2-Propanol 67-63-0 60.10 0.649 3.07 204 1 WG2107223
Propene 115-07-1 42.10 0.160 2.15 10.8 1 WG2107223
Styrene 100-42-5 104 0.335 0.851 26.2 1 WG2107223
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2107223
Tetrachloroethylene 127-18-4 166 11.1 27.2 141 20 WG2107874
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2107223
Toluene 108-88-3 92.10 0.328 1.88 38.8 1 WG2107223
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2107223
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 03
L1642105
SS-3
Collected date/time: 08/01/23 13:30
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2107223
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2107223
Trichloroethylene 79-01-6 131 0.364 1.07 2.03 1 WG2107223
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 8.39 1 WG2107223
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 4.54 1 WG2107223
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 24.2 1 WG2107223
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2107223
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2107223
Vinyl acetate 108-05-4 86.10 0.408 0.704 U 1 WG2107223
Xylenes, Total 1330-20-7 106.16 0.586 2.61 38.6 1 WG2107223
m&p-Xylene 1330-20-7 106 0.585 1.73 21.4 1 WG2107223
o-Xylene 95-47-6 106 0.359 0.867 17.2 1 WG2107223
(S)
1,4-Bromofluorobenzene 460-00-4 175 105 60.0-140 WG2107223
(S)
1,4-Bromofluorobenzene 460-00-4 175 99.7 60.0-140 WG2107874
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1642105
SS-DUP
Collected date/time: 08/01/23 00:00
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
Acetone 67-64-1 58.10 1.39 2.97 40.4 1 WG2107874
Allyl chloride 107-05-1 76.53 0.357 0.626 U 1 WG2107874
Benzene 71-43-2 78.10 0.228 0.639 0.648 1 WG2107874
Benzyl Chloride 100-44-7 127 0.311 1.04 U 1 WG2107874
Bromodichloromethane 75-27-4 164 0.471 1.34 U 1 WG2107874
Bromoform 75-25-2 253 0.757 6.21 U 1 WG2107874
Bromomethane 74-83-9 94.90 0.381 0.776 U 1 WG2107874
1,3-Butadiene 106-99-0 54.10 0.230 4.43 U 1 WG2107874
Carbon disulfide 75-15-0 76.10 0.317 0.622 3.42 1 WG2107874
Carbon tetrachloride 56-23-5 154 0.461 1.26 U 1 WG2107874
Chlorobenzene 108-90-7 113 0.385 0.924 U 1 WG2107874
Chloroethane 75-00-3 64.50 0.263 0.528 U 1 WG2107874
Chloroform 67-66-3 119 0.349 0.973 U 1 WG2107874
Chloromethane 74-87-3 50.50 0.213 0.413 1.23 1 WG2107874
2-Chlorotoluene 95-49-8 126 0.427 1.03 U 1 WG2107874
Cyclohexane 110-82-7 84.20 0.259 0.689 1.36 1 WG2107874
Dibromochloromethane 124-48-1 208 0.618 1.70 U 1 WG2107874
1,2-Dibromoethane 106-93-4 188 0.554 1.54 U 1 WG2107874
1,2-Dichlorobenzene 95-50-1 147 0.770 1.20 U 1 WG2107874
1,3-Dichlorobenzene 541-73-1 147 1.09 1.20 U 1 WG2107874
1,4-Dichlorobenzene 106-46-7 147 0.335 1.20 U 1 WG2107874
1,2-Dichloroethane 107-06-2 99 0.283 0.810 U 1 WG2107874
1,1-Dichloroethane 75-34-3 98 0.290 0.802 U 1 WG2107874
1,1-Dichloroethene 75-35-4 96.90 0.302 0.793 U 1 WG2107874
cis-1,2-Dichloroethene 156-59-2 96.90 0.311 0.793 U 1 WG2107874
trans-1,2-Dichloroethene 156-60-5 96.90 0.267 0.793 U 1 WG2107874
1,2-Dichloropropane 78-87-5 113 0.351 0.924 U 1 WG2107874
cis-1,3-Dichloropropene 10061-01-5 111 0.313 0.908 U 1 WG2107874
trans-1,3-Dichloropropene 10061-02-6 111 0.331 0.908 U 1 WG2107874
1,4-Dioxane 123-91-1 88.10 0.300 0.721 U 1 WG2107874
Ethanol 64-17-5 46.10 0.500 4.71 26.8 J3 1 WG2107874
Ethylbenzene 100-41-4 106 0.362 0.867 0.715 J 1 WG2107874
4-Ethyltoluene 622-96-8 120 0.384 0.982 0.488 J 1 WG2107874
Trichlorofluoromethane 75-69-4 137.40 0.460 1.12 1.33 1 WG2107874
Dichlorodifluoromethane 75-71-8 120.92 0.678 0.989 U 1 WG2107874
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.608 1.53 U 1 WG2107874
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.622 1.40 U 1 WG2107874
Heptane 142-82-5 100 0.425 0.818 U 1 WG2107874
Hexachloro-1,3-butadiene 87-68-3 261 1.12 6.73 U 1 WG2107874
n-Hexane 110-54-3 86.20 0.726 2.22 U 1 WG2107874
Isopropylbenzene 98-82-8 120.20 0.382 0.983 U 1 WG2107874
Methylene Chloride 75-09-2 84.90 0.340 0.694 2.13 1 WG2107874
Methyl Butyl Ketone 591-78-6 100 0.544 5.11 U 1 WG2107874
2-Butanone (MEK)78-93-3 72.10 0.240 3.69 5.54 1 WG2107874
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 0.313 5.12 U 1 WG2107874
Methyl methacrylate 80-62-6 100.12 0.359 0.819 U 1 WG2107874
MTBE 1634-04-4 88.10 0.233 0.721 U 1 WG2107874
Naphthalene 91-20-3 128 1.83 3.30 U 1 WG2107874
2-Propanol 67-63-0 60.10 0.649 3.07 7.13 1 WG2107874
Propene 115-07-1 42.10 0.160 2.15 U 1 WG2107874
Styrene 100-42-5 104 0.335 0.851 0.476 J 1 WG2107874
1,1,2,2-Tetrachloroethane 79-34-5 168 0.511 1.37 U 1 WG2107874
Tetrachloroethylene 127-18-4 166 0.553 1.36 616 1 WG2107874
Tetrahydrofuran 109-99-9 72.10 0.216 0.590 U 1 WG2107874
Toluene 108-88-3 92.10 0.328 1.88 U 1 WG2107874
1,2,4-Trichlorobenzene 120-82-1 181 1.10 4.66 U 1 WG2107874
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 04
L1642105
SS-DUP
Collected date/time: 08/01/23 00:00
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.MDL RDL Result Qualifier Dilution Batch
Analyte ug/m3 ug/m3 ug/m3
1,1,1-Trichloroethane 71-55-6 133 0.400 1.09 U 1 WG2107874
1,1,2-Trichloroethane 79-00-5 133 0.422 1.09 U 1 WG2107874
Trichloroethylene 79-01-6 131 0.364 1.07 0.873 J 1 WG2107874
1,2,4-Trimethylbenzene 95-63-6 120 0.375 0.982 U 1 WG2107874
1,3,5-Trimethylbenzene 108-67-8 120 0.382 0.982 U 1 WG2107874
2,2,4-Trimethylpentane 540-84-1 114.22 0.621 0.934 U 1 WG2107874
Vinyl chloride 75-01-4 62.50 0.243 0.511 U 1 WG2107874
Vinyl Bromide 593-60-2 106.95 0.373 0.875 U 1 WG2107874
Vinyl acetate 108-05-4 86.10 0.408 0.704 U 1 WG2107874
Xylenes, Total 1330-20-7 106.16 0.586 2.61 1.86 J 1 WG2107874
m&p-Xylene 1330-20-7 106 0.585 1.73 1.29 J 1 WG2107874
o-Xylene 95-47-6 106 0.359 0.867 0.572 J 1 WG2107874
(S)
1,4-Bromofluorobenzene 460-00-4 175 98.4 60.0-140 WG2107874
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107223
Volatile Organic Compounds (MS) by Method TO-15 L1642105-01,02,03
Method Blank (MB)
(MB) R3956558-3 08/03/23 10:37
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Acetone U 1.39 2.97
Allyl chloride U 0.357 0.626
Benzene U 0.228 0.639
Benzyl Chloride U 0.311 1.04
Bromodichloromethane U 0.471 1.34
Bromoform U 0.757 6.21
Bromomethane U 0.381 0.776
1,3-Butadiene U 0.230 4.43
Carbon disulfide U 0.317 0.622
Carbon tetrachloride U 0.461 1.26
Chlorobenzene U 0.385 0.924
Chloroethane U 0.263 0.528
Chloroform U 0.349 0.973
Chloromethane U 0.213 0.413
2-Chlorotoluene U 0.427 1.03
Cyclohexane U 0.259 0.689
Dibromochloromethane U 0.618 1.70
1,2-Dibromoethane U 0.554 1.54
1,2-Dichlorobenzene U 0.770 1.20
1,3-Dichlorobenzene U 1.09 1.20
1,4-Dichlorobenzene U 0.335 1.20
1,2-Dichloroethane U 0.283 0.810
1,1-Dichloroethane U 0.290 0.802
1,1-Dichloroethene U 0.302 0.793
cis-1,2-Dichloroethene U 0.311 0.793
trans-1,2-Dichloroethene U 0.267 0.793
1,2-Dichloropropane U 0.351 0.924
cis-1,3-Dichloropropene U 0.313 0.908
trans-1,3-Dichloropropene U 0.331 0.908
1,4-Dioxane U 0.300 0.721
Ethanol U 0.500 4.71
Ethylbenzene U 0.362 0.867
4-Ethyltoluene U 0.384 0.982
Trichlorofluoromethane U 0.460 1.12
Dichlorodifluoromethane U 0.678 0.989
1,1,2-Trichlorotrifluoroethane U 0.608 1.53
1,2-Dichlorotetrafluoroethane U 0.622 1.40
Heptane U 0.425 0.818
Hexachloro-1,3-butadiene U 1.12 6.73
n-Hexane U 0.726 2.22
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107223
Volatile Organic Compounds (MS) by Method TO-15 L1642105-01,02,03
Method Blank (MB)
(MB) R3956558-3 08/03/23 10:37
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Isopropylbenzene U 0.382 0.983
Methylene Chloride U 0.340 0.694
Methyl Butyl Ketone U 0.544 5.11
2-Butanone (MEK)U 0.240 3.69
4-Methyl-2-pentanone (MIBK)U 0.313 5.12
Methyl methacrylate U 0.359 0.819
MTBE U 0.233 0.721
Naphthalene U 1.83 3.30
2-Propanol U 0.649 3.07
Propene U 0.160 2.15
Styrene U 0.335 0.851
1,1,2,2-Tetrachloroethane U 0.511 1.37
Tetrahydrofuran U 0.216 0.590
Toluene U 0.328 1.88
1,2,4-Trichlorobenzene U 1.10 4.66
1,1,1-Trichloroethane U 0.400 1.09
1,1,2-Trichloroethane U 0.422 1.09
Trichloroethylene U 0.364 1.07
1,2,4-Trimethylbenzene U 0.375 0.982
1,3,5-Trimethylbenzene U 0.382 0.982
2,2,4-Trimethylpentane U 0.621 0.934
Vinyl chloride U 0.243 0.511
Vinyl Bromide U 0.373 0.875
Vinyl acetate U 0.408 0.704
Xylenes, Total U 0.586 2.61
m&p-Xylene U 0.585 1.73
o-Xylene U 0.359 0.867
(S) 1,4-Bromofluorobenzene 96.3 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3956558-1 08/03/23 09:02 • (LCSD) R3956558-2 08/03/23 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Acetone 8.91 8.51 8.65 95.5 97.1 70.0-130 1.66 25
Allyl chloride 11.7 11.9 12.1 101 103 70.0-130 2.09 25
Benzene 12.0 12.6 12.5 105 104 70.0-130 0.510 25
Benzyl Chloride 19.5 20.3 20.2 104 104 70.0-152 0.513 25
Bromodichloromethane 25.2 25.9 25.9 103 103 70.0-130 0.000 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107223
Volatile Organic Compounds (MS) by Method TO-15 L1642105-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3956558-1 08/03/23 09:02 • (LCSD) R3956558-2 08/03/23 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Bromoform 38.8 40.3 40.5 104 104 70.0-130 0.513 25
Bromomethane 14.6 15.1 15.1 103 104 70.0-130 0.257 25
1,3-Butadiene 8.30 8.12 8.19 97.9 98.7 70.0-130 0.814 25
Carbon disulfide 11.7 12.1 12.3 104 105 70.0-130 1.28 25
Carbon tetrachloride 23.6 23.9 24.2 101 102 70.0-130 1.31 25
Chlorobenzene 17.3 18.2 18.1 105 104 70.0-130 0.510 25
Chloroethane 9.89 10.8 10.6 109 107 70.0-130 1.48 25
Chloroform 18.3 18.7 18.9 103 104 70.0-130 1.03 25
Chloromethane 7.75 7.66 7.77 98.9 100 70.0-130 1.34 25
2-Chlorotoluene 19.3 20.8 20.5 107 106 70.0-130 1.25 25
Cyclohexane 12.9 13.8 14.1 107 109 70.0-130 1.73 25
Dibromochloromethane 31.9 33.5 33.4 105 105 70.0-130 0.254 25
1,2-Dibromoethane 28.8 30.5 30.7 106 106 70.0-130 0.503 25
1,2-Dichlorobenzene 22.5 24.0 24.0 107 107 70.0-130 0.000 25
1,3-Dichlorobenzene 22.5 24.0 23.8 106 106 70.0-130 0.755 25
1,4-Dichlorobenzene 22.5 24.6 24.5 109 109 70.0-130 0.245 25
1,2-Dichloroethane 15.2 16.0 15.8 105 104 70.0-130 1.28 25
1,1-Dichloroethane 15.0 15.5 15.6 103 104 70.0-130 0.774 25
1,1-Dichloroethene 14.9 15.5 15.6 104 105 70.0-130 0.764 25
cis-1,2-Dichloroethene 14.9 15.7 15.8 105 106 70.0-130 0.757 25
trans-1,2-Dichloroethene 14.9 15.6 15.6 105 105 70.0-130 0.254 25
1,2-Dichloropropane 17.3 18.2 18.1 105 105 70.0-130 0.509 25
cis-1,3-Dichloropropene 17.0 18.1 18.0 106 106 70.0-130 0.503 25
trans-1,3-Dichloropropene 17.0 18.3 18.3 107 107 70.0-130 0.248 25
1,4-Dioxane 13.5 15.1 15.1 111 112 70.0-140 0.239 25
Ethanol 7.07 5.07 4.88 71.7 69.1 55.0-148 3.79 25
Ethylbenzene 16.3 17.3 17.3 106 106 70.0-130 0.251 25
4-Ethyltoluene 18.4 20.0 19.9 109 108 70.0-130 0.493 25
Trichlorofluoromethane 21.1 21.4 21.4 101 101 70.0-130 0.000 25
Dichlorodifluoromethane 18.5 16.9 16.9 91.2 91.2 64.0-139 0.000 25
1,1,2-Trichlorotrifluoroethane 28.7 29.3 29.4 102 102 70.0-130 0.261 25
1,2-Dichlorotetrafluoroethane 26.2 27.7 27.8 106 106 70.0-130 0.252 25
Heptane 15.3 16.4 16.5 107 108 70.0-130 0.745 25
Hexachloro-1,3-butadiene 40.0 42.4 41.8 106 105 70.0-151 1.27 25
n-Hexane 13.2 14.2 14.3 107 109 70.0-130 0.988 25
Isopropylbenzene 18.4 20.3 20.2 110 110 70.0-130 0.485 25
Methylene Chloride 13.0 13.4 13.4 103 103 70.0-130 0.000 25
Methyl Butyl Ketone 15.3 16.1 16.2 105 106 70.0-149 0.506 25
2-Butanone (MEK)11.1 11.4 11.4 103 103 70.0-130 0.000 25
4-Methyl-2-pentanone (MIBK)15.4 16.8 16.7 109 109 70.0-139 0.734 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107223
Volatile Organic Compounds (MS) by Method TO-15 L1642105-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3956558-1 08/03/23 09:02 • (LCSD) R3956558-2 08/03/23 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Methyl methacrylate 15.4 16.7 16.3 109 106 70.0-130 1.99 25
MTBE 13.5 14.4 14.5 106 107 70.0-130 0.749 25
Naphthalene 19.6 21.4 21.8 109 111 70.0-159 1.94 25
2-Propanol 9.22 9.05 9.12 98.1 98.9 70.0-139 0.812 25
Propene 6.46 6.11 6.16 94.7 95.5 64.0-144 0.842 25
Styrene 16.0 17.7 17.7 111 111 70.0-130 0.241 25
1,1,2,2-Tetrachloroethane 25.8 26.9 26.9 105 104 70.0-130 0.255 25
Tetrahydrofuran 11.1 11.9 12.0 108 108 70.0-137 0.494 25
Toluene 14.1 15.0 15.2 106 107 70.0-130 0.998 25
1,2,4-Trichlorobenzene 27.8 30.0 30.1 108 109 70.0-160 0.493 25
1,1,1-Trichloroethane 20.4 21.0 21.1 103 103 70.0-130 0.517 25
1,1,2-Trichloroethane 20.4 21.4 21.5 105 106 70.0-130 0.760 25
Trichloroethylene 20.1 21.4 21.4 107 106 70.0-130 0.250 25
1,2,4-Trimethylbenzene 18.4 20.5 20.5 111 111 70.0-130 0.000 25
1,3,5-Trimethylbenzene 18.4 20.2 20.4 110 111 70.0-130 0.726 25
2,2,4-Trimethylpentane 17.5 18.7 19.1 107 109 70.0-130 1.73 25
Vinyl chloride 9.59 9.94 9.97 104 104 70.0-130 0.257 25
Vinyl Bromide 16.4 17.4 17.3 106 105 70.0-130 0.505 25
Vinyl acetate 13.2 12.7 13.0 96.0 98.7 70.0-130 2.74 25
Xylenes, Total 49.1 53.0 53.0 108 108 70.0-130 0.000 25
m&p-Xylene 32.5 35.2 35.3 108 109 70.0-130 0.369 25
o-Xylene 16.3 17.6 17.6 108 109 70.0-130 0.493 25
(S) 1,4-Bromofluorobenzene 96.9 96.4 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107864
Volatile Organic Compounds (MS) by Method TO-15 L1642105-01,02
Method Blank (MB)
(MB) R3957193-3 08/04/23 11:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Tetrachloroethylene U 0.553 1.36
(S) 1,4-Bromofluorobenzene 90.5 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957193-1 08/04/23 08:57 • (LCSD) R3957193-2 08/04/23 11:12
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Tetrachloroethylene 25.5 23.6 24.0 92.8 94.1 70.0-130 1.43 25
(S) 1,4-Bromofluorobenzene 99.5 99.5 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107874
Volatile Organic Compounds (MS) by Method TO-15 L1642105-03,04
Method Blank (MB)
(MB) R3957087-3 08/04/23 10:40
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Acetone U 1.39 2.97
Allyl chloride U 0.357 0.626
Benzene U 0.228 0.639
Benzyl Chloride U 0.311 1.04
Bromodichloromethane U 0.471 1.34
Bromoform U 0.757 6.21
Bromomethane U 0.381 0.776
1,3-Butadiene U 0.230 4.43
Carbon disulfide U 0.317 0.622
Carbon tetrachloride U 0.461 1.26
Chlorobenzene U 0.385 0.924
Chloroethane U 0.263 0.528
Chloroform U 0.349 0.973
Chloromethane U 0.213 0.413
2-Chlorotoluene U 0.427 1.03
Cyclohexane U 0.259 0.689
Dibromochloromethane U 0.618 1.70
1,2-Dibromoethane U 0.554 1.54
1,2-Dichlorobenzene U 0.770 1.20
1,3-Dichlorobenzene U 1.09 1.20
1,4-Dichlorobenzene U 0.335 1.20
1,2-Dichloroethane U 0.283 0.810
1,1-Dichloroethane U 0.290 0.802
1,1-Dichloroethene U 0.302 0.793
cis-1,2-Dichloroethene U 0.311 0.793
trans-1,2-Dichloroethene U 0.267 0.793
1,2-Dichloropropane U 0.351 0.924
cis-1,3-Dichloropropene U 0.313 0.908
trans-1,3-Dichloropropene U 0.331 0.908
1,4-Dioxane U 0.300 0.721
Ethanol U 0.500 4.71
Ethylbenzene U 0.362 0.867
4-Ethyltoluene U 0.384 0.982
Trichlorofluoromethane U 0.460 1.12
Dichlorodifluoromethane U 0.678 0.989
1,1,2-Trichlorotrifluoroethane U 0.608 1.53
1,2-Dichlorotetrafluoroethane U 0.622 1.40
Heptane U 0.425 0.818
Hexachloro-1,3-butadiene U 1.12 6.73
n-Hexane U 0.726 2.22
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107874
Volatile Organic Compounds (MS) by Method TO-15 L1642105-03,04
Method Blank (MB)
(MB) R3957087-3 08/04/23 10:40
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/m3 ug/m3 ug/m3
Isopropylbenzene U 0.382 0.983
Methylene Chloride U 0.340 0.694
Methyl Butyl Ketone U 0.544 5.11
2-Butanone (MEK)U 0.240 3.69
4-Methyl-2-pentanone (MIBK)U 0.313 5.12
Methyl methacrylate U 0.359 0.819
MTBE U 0.233 0.721
Naphthalene U 1.83 3.30
2-Propanol U 0.649 3.07
Propene U 0.160 2.15
Styrene U 0.335 0.851
1,1,2,2-Tetrachloroethane U 0.511 1.37
Tetrachloroethylene U 0.553 1.36
Tetrahydrofuran U 0.216 0.590
Toluene U 0.328 1.88
1,2,4-Trichlorobenzene U 1.10 4.66
1,1,1-Trichloroethane U 0.400 1.09
1,1,2-Trichloroethane U 0.422 1.09
Trichloroethylene U 0.364 1.07
1,2,4-Trimethylbenzene U 0.375 0.982
1,3,5-Trimethylbenzene U 0.382 0.982
2,2,4-Trimethylpentane U 0.621 0.934
Vinyl chloride U 0.243 0.511
Vinyl Bromide U 0.373 0.875
Vinyl acetate U 0.408 0.704
Xylenes, Total U 0.586 2.61
m&p-Xylene U 0.585 1.73
o-Xylene U 0.359 0.867
(S) 1,4-Bromofluorobenzene 97.8 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957087-1 08/04/23 09:05 • (LCSD) R3957087-2 08/04/23 09:54
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Acetone 8.91 8.58 8.53 96.3 95.7 70.0-130 0.556 25
Allyl chloride 11.7 12.8 12.2 109 104 70.0-130 5.00 25
Benzene 12.0 12.6 12.6 106 105 70.0-130 0.760 25
Benzyl Chloride 19.5 20.5 20.4 105 105 70.0-152 0.509 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107874
Volatile Organic Compounds (MS) by Method TO-15 L1642105-03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957087-1 08/04/23 09:05 • (LCSD) R3957087-2 08/04/23 09:54
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
Bromodichloromethane 25.2 25.8 25.9 103 103 70.0-130 0.259 25
Bromoform 38.8 41.1 40.3 106 104 70.0-130 2.04 25
Bromomethane 14.6 15.3 15.3 105 105 70.0-130 0.000 25
1,3-Butadiene 8.30 8.32 8.05 100 97.1 70.0-130 3.24 25
Carbon disulfide 11.7 12.3 12.2 105 105 70.0-130 0.509 25
Carbon tetrachloride 23.6 24.0 23.9 102 101 70.0-130 0.526 25
Chlorobenzene 17.3 18.0 18.1 104 105 70.0-130 0.512 25
Chloroethane 9.89 11.0 10.8 111 109 70.0-130 2.18 25
Chloroform 18.3 19.1 19.1 105 105 70.0-130 0.255 25
Chloromethane 7.75 7.85 7.68 101 99.2 70.0-130 2.13 25
2-Chlorotoluene 19.3 21.2 21.2 110 110 70.0-130 0.243 25
Cyclohexane 12.9 14.5 14.3 113 110 70.0-130 1.91 25
Dibromochloromethane 31.9 33.4 33.4 105 105 70.0-130 0.000 25
1,2-Dibromoethane 28.8 30.4 30.4 105 106 70.0-130 0.253 25
1,2-Dichlorobenzene 22.5 24.7 24.6 110 109 70.0-130 0.488 25
1,3-Dichlorobenzene 22.5 24.5 23.9 109 106 70.0-130 2.48 25
1,4-Dichlorobenzene 22.5 25.1 24.8 111 110 70.0-130 1.21 25
1,2-Dichloroethane 15.2 15.9 15.8 105 104 70.0-130 0.768 25
1,1-Dichloroethane 15.0 15.6 15.6 104 104 70.0-130 0.000 25
1,1-Dichloroethene 14.9 15.7 15.7 105 106 70.0-130 0.253 25
cis-1,2-Dichloroethene 14.9 16.1 16.1 109 108 70.0-130 0.493 25
trans-1,2-Dichloroethene 14.9 15.8 15.5 106 105 70.0-130 1.52 25
1,2-Dichloropropane 17.3 18.3 18.3 106 106 70.0-130 0.000 25
cis-1,3-Dichloropropene 17.0 17.8 17.9 105 105 70.0-130 0.508 25
trans-1,3-Dichloropropene 17.0 17.8 18.1 105 106 70.0-130 1.52 25
1,4-Dioxane 13.5 15.5 15.2 114 112 70.0-140 1.88 25
Ethanol 7.07 6.39 4.90 90.4 69.3 55.0-148 J3 26.4 25
Ethylbenzene 16.3 17.7 17.5 109 108 70.0-130 0.985 25
4-Ethyltoluene 18.4 20.6 20.5 112 111 70.0-130 0.717 25
Trichlorofluoromethane 21.1 21.2 20.9 101 99.2 70.0-130 1.34 25
Dichlorodifluoromethane 18.5 16.3 15.9 88.0 85.9 64.0-139 2.45 25
1,1,2-Trichlorotrifluoroethane 28.7 30.0 29.7 104 103 70.0-130 0.770 25
1,2-Dichlorotetrafluoroethane 26.2 28.0 27.9 107 106 70.0-130 0.500 25
Heptane 15.3 16.6 16.5 108 107 70.0-130 0.495 25
Hexachloro-1,3-butadiene 40.0 42.4 42.3 106 106 70.0-151 0.252 25
n-Hexane 13.2 14.8 14.5 112 110 70.0-130 1.68 25
Isopropylbenzene 18.4 21.1 20.7 115 112 70.0-130 2.12 25
Methylene Chloride 13.0 13.4 13.3 103 102 70.0-130 1.30 25
Methyl Butyl Ketone 15.3 16.0 16.1 104 105 70.0-149 0.766 25
2-Butanone (MEK)11.1 11.8 11.4 107 103 70.0-130 3.56 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2107874
Volatile Organic Compounds (MS) by Method TO-15 L1642105-03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3957087-1 08/04/23 09:05 • (LCSD) R3957087-2 08/04/23 09:54
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/m3 ug/m3 ug/m3 %%%%%
4-Methyl-2-pentanone (MIBK)15.4 16.6 16.6 108 108 70.0-139 0.247 25
Methyl methacrylate 15.4 16.9 16.7 110 109 70.0-130 1.46 25
MTBE 13.5 14.9 14.6 110 108 70.0-130 1.96 25
Naphthalene 19.6 21.3 21.7 109 110 70.0-159 1.71 25
2-Propanol 9.22 9.19 9.17 99.7 99.5 70.0-139 0.268 25
Propene 6.46 6.18 6.08 95.7 94.1 64.0-144 1.69 25
Styrene 16.0 18.2 18.0 114 113 70.0-130 1.18 25
1,1,2,2-Tetrachloroethane 25.8 27.8 27.7 108 107 70.0-130 0.248 25
Tetrachloroethylene 25.5 27.4 27.3 107 107 70.0-130 0.248 25
Tetrahydrofuran 11.1 12.1 12.0 110 109 70.0-137 1.22 25
Toluene 14.1 15.2 15.3 108 109 70.0-130 0.740 25
1,2,4-Trichlorobenzene 27.8 29.5 30.0 106 108 70.0-160 1.49 25
1,1,1-Trichloroethane 20.4 21.3 21.1 105 103 70.0-130 1.03 25
1,1,2-Trichloroethane 20.4 21.5 21.8 106 107 70.0-130 1.01 25
Trichloroethylene 20.1 21.4 21.4 106 106 70.0-130 0.000 25
1,2,4-Trimethylbenzene 18.4 21.2 21.1 115 114 70.0-130 0.465 25
1,3,5-Trimethylbenzene 18.4 21.1 20.8 114 113 70.0-130 1.17 25
2,2,4-Trimethylpentane 17.5 19.2 19.2 110 109 70.0-130 0.487 25
Vinyl chloride 9.59 9.97 9.92 104 103 70.0-130 0.514 25
Vinyl Bromide 16.4 17.7 17.5 108 107 70.0-130 1.24 25
Vinyl acetate 13.2 12.6 12.8 95.5 97.1 70.0-130 1.66 25
Xylenes, Total 49.1 54.7 54.3 112 111 70.0-130 0.797 25
m&p-Xylene 32.5 36.4 35.9 112 111 70.0-130 1.32 25
o-Xylene 16.3 18.3 18.1 113 111 70.0-130 1.43 25
(S) 1,4-Bromofluorobenzene 98.7 97.7 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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APPENDIX C
Boring Logs
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING7.9 Sample NumberDP-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML
DescripƟon
(ML) SILT, rock fragments, red/ brown
END OF DRILLING AT 5.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:DP-1
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:Track Mounted Geo
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING7.2 Sample NumberDP-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
DescripƟon
(ML/CL) CLAYEY SILT, red/ brown
END OF DRILLING AT 5.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:DP-2
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:Track Mounted Geo
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING47.7
7.3 Sample NumberE-1
E-1
E-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
DescripƟon
(ML/CL) CLAYEY SILT, brown
(ML) SILT, brown, wet at 12'
END OF DRILLING AT 15.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:E-1
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:15
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING47.7
7.3 Sample NumberE-2
E-2
E-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML
ML
DescripƟon
(ML) SILT, red/ brown
(ML) SILT, brown, wet at 12'
END OF DRILLING AT 15.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:E-2
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:15
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING7.1
7.0 Sample NumberP-1
P-1
P-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
DescripƟon
(ML/CL) CLAYEY SILT, dark red
(ML) SILT, brown/ tan, wet at 14'
END OF DRILLING AT 15.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:P-1
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:Track Mounted Geo
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING7.0
7.4
7.5 Sample NumberP-2
P-2
P-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML
ML
DescripƟon
(ML) SILT, brown
(ML) SILT, brown, moist, wet at 11'
END OF DRILLING AT 15.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:P-2
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:Track Mounted Geo
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID READING7.0
7.1 Sample NumberP-3
P-3
P-3 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
DescripƟon
(ML/CL) CLAYEY SILT, red/brown
(ML) SILT, red/brown, wet at 13'
END OF DRILLING AT 15.0 FT
Project Name:1601 South Boulevard Site -BrownĮelds
Assessment Svcs
Client:Sterling Bay Companies
Site LocaƟon:1601-1609 South Boulevard, CharloƩe,
North Carolina, 28203
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:P-3
Project No.:49:15946-E
Driller:3D Drilling Drill Rig:15
WL (First Encountered)Boring Started:Aug 04 2023
WL (CompleƟon)Boring Completed:Aug 04 2023
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy H. Cavallier
Roger A Smith
APPENDIX D
NCDEQ Risk Calculator Output
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 1601 South Boulevard Site
Exposure Unit ID: Site Wide
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.0E-04 5.0E+01 YES
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
APPENDIX E
Brownfields Receptor Survey
Form and Figures
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:1601 South Boulevard Site
Address:1601-1617 South Boulevard and 1612 Cleveland Avenue
City:Charlotte
County:Mecklenburg
Brownfields Project Number: 2607-22-060
Date 9/7/2023
Property and Building Characteristics
a. Provide occupancy and use information.
The current site structures currently vacant. They were previously utilized as two restaurants (1601 South
Bouelvard) and an office building (1612 Cleveland Avenue)
1601 South Boulevard - 1 story brick structure
1612 Cleveland Avenue - 1 story brick structure
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The foundations of the current site structures are commercial slab
1601 South Boulevard - Forced air-not ducted
1612 Cleveland Avenue - Heat Pump
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
Unknown
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets
as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may be
needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved 10
8530
NA
0
5
0
Size of Property (acres)
% of property that is wooded/brush
0.846
10
10
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?).
0
50
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
N NA NA
Y ~100 E
N NA NA
Utilities
Is there a septic system on-site? (Y or N) ____N_____
Please provide the utility providers for the subject property
a. Natural Gas __Piedmont Natural Gas____
b. Sewer __Charlotte Water_________
c. Electricity __Duke Energy____________
d. Other __________________________
For surrounding properties, please complete the following table with available information.
Y 5'NW
Y 5'NE
N NA NA
Y 5'NE
Y 5'NE
N NA NA
N NA NA
Same
Same
Same
Is there a basement within 1,000 ft of the Property
NA
Is there a residence within 1,000 ft of the Property?
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
211 E Park Ave
NA
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Light Commercial/Residential
Residential
Light Commercial
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information can
then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses. Various residential properties are located to the south and east of the subject property. The location of
the closest is referenced above.
Distance
(ft)
DirectionDistance
(ft)Address
Same
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
Light Commercial
Zoning/Land Use Proposed Usage Current Use/Occupant
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public __X____ Private ______
N NA NA NA
N NA NA NA
N NA NA NA
Surface Water & Wetlands
NA
An unnamed tributary to Irwin Creek is located approximately
1,900 feet west of the subject site.
No
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the property?
If no wetlands on-site, are wetlands suspected
on adjoining properties?
NA
NA
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
b d?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the
vicinity of the Property.
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
a. Is the water body naturally developed or
man-made?NA
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be utilized;
however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested
radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please
note, the PM may opt for a more extensive water supply well survey if needed.
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
Distance
(ft)Direction Address
No
Rev. 09/2015 Page 3 of 3
FIGURE E1
RECEPTOR SURVEY MAP
1601 SOUTH BOUELVAR PROPERTY
1601 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:15946-E
APPROXIMATE BROWNFIELDS SITE BOUNDARY
LEGEND
APPROXIMATE WATER/SEWER UTILITY LINE
APPROXIMATE NATURAL GAS UTILITY LINE
APPROXIMATE STORMWATER UTILITY LINE
SOURCE:
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED JUNE 20, 2023
SCALE:
AS SHOWN